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WQ0000701_Regional Office Historical File_20171231 (11)
Mr, `el Crowe, Plant Manager Tyson Poultry. Inc. P. , Box 158 Harmony, North Carolina 28634 Y*Michael F."Easley Governor William G. Ross, Jr.'Sacrstary North Carolina Department of Environment and Natural Resources Koff T. Stevens, Director Division of Water Quality DIVISION OF WATER QUALITY June 27, 2001 Permit No. ' `Q0000701 Tyson Poultry, Inc. Harmony, NC rendering Plant lredell County, NC Bear Mr, Crowe: Our records show that Permit No. WQ00 0701 was issued on June 15, 2001 for the land application of sludge generated by your wastewater treatment facility, The purpose of this letter is to advise your of die importance of the Permit and the liabilities in the event of failure to comply with the terms and' conditions of the Permit, If you have not already done so, it is requested that you and other appropriate employees thoroughly read the Permit. The Pe it sets forth specific perfortnance standards, operation and maintenance ce requirements, monitoring requirements, including annual reporting and groundwater monitoring activities to be pet onraed'by the Pennitt e, plus general conditions applicable to non -discharge perinits, Failure to comply - with the terms and conditions of the permit subjects the Permittee to enforcement action pursuant to Section 143-215.6 of the North Carolina. general Statutes, A civil penalty of u a to $1,0,000 per violation may be assessed for such violations: Please saute that the subject Permit expires on May 31, 2006, Condition No. VI, No, 8 of the Permit requires that a renewal request be submitted at least sip () months prior to expiration, Also the Permit is non -transferable until such time that the Permittee has requested a name change to the new Permittee. s mentioned previously, the purpose of this lever is to advise you of the importance of vour Permit. Please read the <Permit and contact this office at 704/663-1699 in Mooresville ifvou have any questions or need: clarification. We loop forward to providing any assistance, Sincerely D. Rex Gleason, P.E. 'Water Quality Regional Supervisor \.Tyssu.r D,tf l to:dee 9 if JOA Customer SerAce Mooresville Regional Office, 919 forth Main Street, Mooresville, NC 261 is PHONE i c4l 666-1699 1 800 6•77 (704) 66 -6040 NORTH CAROLINA ENVIRONMENTAL MANAGEINIFNTCOAL'IISSIONN DEPARTMENT OF ENVIRONMENT AND NATURAL RESOUTR"ES RALEIGH RESIDUALS LAND APPLICATION PER -MIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS 14EREBY GRANTED TO Tyson Foods, Inc. Wilkes County FOR THE operation of a wastewater residuals land application program consisting of the application of 4,071 dry tons per year of residuals from the sources listed in Condition 115, to approximately 2,270 acres of land in Alexander, Davie, Rowan, Yadkin., and Wilkes Counties with no discharge of wastes to the surface waters, pursuant to the correction request received on March 25, 1998, and in conformity with the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until April 30, 2000, shall void Permit No. WQ0000701 issued March 5, 1998, and shall be subject to the following specified conditions and limitations: I. PERFORN—IANCE STANDARDS I The Mooresville Regional Office (for all new sites located in Alexander County), telephone number (704) 663-1699, or the Winston-Salem Regional Office (for all new sites located in Wilkes County), telephone number (910) 771-4600, and the appropriate local governmental official (counry manager/city manager) shall be notified at least twvnty-four (24) hours prior to the initial application of the residuals to a site so that an inspection can be made of the application sites and application method. Such notification to the regional supervisor shall be made during the normal office hours from 8:00 a,m, until 5:00 p.m. on 110onday through Friday, excluding State Holidays. In addition, the Alexander and 'vVilkes County Manager's office must be notified prior to the initial application so that they will be aware that the operation has commenced, 2, This permit shall become voidable if the soils fail to adequately assimilate the wastes and may be rescinded unless the sites are maintained and operated in a manner Nvhich will protect the assigned water quality standards of the surface waters and ground waters. 3� The land application program shall be, effectively maintained and operated as a non -discharge system to prevent the discharge of any wastes resulting from the operation of this program. 4The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwaters resulting from the operation of this program. State of North Carolina Department of Environment and Natural Resources Division of Water Quality James 8, Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director March 31, 1998 Lawrence R. Sampson, Jr., Project Engineer Tyson Foods., Inc, Post Office Box 88 Wilkesboro, North Carolina 28697 NORTH CAROUNA DEPARTmEN7 OF ENVIRONMENT AND NATURAL RF-SOURCES Subject: Fom"ItN&IWQ0000701�, Land Application of Wastewater Residuals WiltsCounty- Dear Mr. Sampson C, In accordance with the correction request received on March 25, 1998, we are forwarding herewith Permit No. WQ0000701 as corrected, dated March 31., 19'98.1 to the Tyson Foods, Inc, for the continued operation of a wasteNvater residuals land application program. This Pe it is being corrected to delete the TCLP analysis from the subject permit. Originally required annually, the TCLP was reduced to once per permit cycle, however, the Division has now deleted this requirement altogether. This permit shall be effective from the date of issuance until April 30, 2000.1 shall void Permit No. NVQ0000701 issued March 51, 1998, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring and reporting requirements contained in this permit, failure to 3 establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems, If any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of this permit. This request must be in the form of a written petition, conforining to Chapter 150B of North Carolina General Statutes, and filed with the Office of Administrative Hearings, P,O. Drawer 27447, Raleigh,, NC 27611-7447. Unless such demands are made this permit shall be final and binding. If you need additional information concerning this matter, please contact Mr, Michael D, Allen at (919) 733-5083 extension 547. sr Sincere., '--A. Preston Howard, Jr., P.E. ce- Alexander, Davie, Rowan, Yadkin, and Wilkes County Health Departments Terra Renewal Senviees, Inc. Mooresville Regional Office, Water Quality Section Mooresville Regional Office, Groundwater Section Winston-Salem Regional Office, Water Quality Section Winston-Salem Regional Office, Groundwater Section Bob Check, Groundwater Section. Central Office Technical Assistance and Certification Unit (no revised rating) Non -Discharge Compliance/Enforcement Unit PO Box 29535, Raleigh, North Carolina 27626-0535 Telephone (919) 733-5083 Fax (919) 733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/10% post -consumer paper A suitable vegetative cover, as listed in condition 114, shall be maintained in accordance with the crop management plan outlined by the local Extension Office, the Department of Agriculture, the Natural Resource Conservation Service, or other agronomist, and approved by this Division. 3, An acceptable PH must be maintained in the soil, residual and lime mixture, greater than 6.0, on all land application sites to insure optimum yield for the crop(s) specified below, The agronomist shall provide information on the PH best suited for the specified crop and the soil type. 4. The application rates shall not exceed the following for the specified crops' !C r PAN lb, PAN Qb.Lacre/vr.) Alfalfa 200 Forest (Hardwood & Softwood) 75 Bermuda Grass (Hay, Pasture) 220 Milo 100 Blue Grass 120 Small Grain (Nklheat, barley, oats) 100 Co m (Grain) 160 Sorghum, Sudex (Pasture) 180 Corn (Silage) 200 Sorghum, Sudex (Silage) 220 Cotton 70 Soybeans 200 Fescue 250 Timothy, Orchard, & Rye Grass 200 5- No residuals other than the following are hereby approved for land application in accordance with this permit: Permit Volume Source Count),,, NT u rn be r (dry ton wear) Harmony Plant; DAY, Stickwater, CL, Iredell NCO005126 2,250 Wilkesboro Plant; DAF Wilkes Town of Wilkesboro Included Above Pretreatment No, 1003-1 Case Farms Facility DAF Burke WQ0007511 1,064 Townsend Foods, Inc. Chatham NCO026441 757 6. The lifetime heavy metal loadings (lbs./acre) shall not exceed the following for the corresponding Cation Exchange Capacities (CEQ: Parameter CEC < 5 CEC 5 to 15 CEC > 15 Lead 500 1000 2000 Zinc 250 Soo 1000 Copper 125 250 500 Nickel 125 250 500 Cadmium 4,5 9 18 7. Upon classification of the facility by the Water Pollution Control System Operators Certification Commission (WPCSOCC'), the Permittee shall employ a certified land application/residuals operator to be in responsible charge (ORC) of the land application program. The operator must hold a certificate of the type classification assigned to the land application program by the WPCSOCC. The Permittee must also employ a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8A.0202. K Adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters, 9. Surface applied residuals will be plowed or disced within twenty-four (24) hours after application on lands 'with no cover crop established. 10, For areas that are prone to flooding or within the I lift -year flood elevation, residuals may be applied only during periods of dry weather. The residuals must be incorporated into the soil within t-,verity-four (24) hours after application. 3 5. In the event that the land application program is not operated satisfactorily, including the cre� nuisance conditions, the Permittee shall cease applying residuals to the sites and take any irn 1`14 corrective actions as may be required by the Division of Water Quality (Division). 6. Some of the buffers specified below may not have been included in previous permits for this land application operation. However, any sites or fields that are included in this permit, but were approved with different applicable buffers shall be reflagged to comply with the below buffers. The following buffer zones shall be maintained: a) 400 feet from residences or places of public assembly under separate ownership for surface application method- however, the buffer zone requirement may be reduced to a minimurn of 100 pp feet upon written consent of the owner and approval from the appropriate regional office, b) 200 feet from residences or places of public assembly under separate ownership for subsurface residual injection method; however, the buffer zone requirement may be reduced to a minimum of 100 feet LIP011 written consent of the owner and the appropriate regional office, c) 100 feet from any public or private water supply source, waters classified as SA or SB, and any Class or Class 11 impounded reservoir used as a source of drinking water for both methods, d) 100 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for surface application, e) 50 feet from any streams classified as WS or B, any other stream, canal, marsh or coastal waters and any other lake or impoundment for subsurface application, ft 50 feet from property lines for both surface and subsurface application methods; g) 50 feet from public right of ways for both application methods, h) 10 feet from upslope interceptor drains and surface water diversions for both application methods, i) 25 feet from downslope interceptor drains, surface water diversions, groundwater drainage systems and surface drainage ditches for both application methods, J) 100fyet firom rock outcrol)s, 7. A cop), of this permit shall be maintained at the land application site when residuals are being applied during the life of this permit, A spill prevention and control plan shall be maintained in all residuals transport and application vehicles. 8, Specific residual application area boundaries shall be clearly marked on each site prior to and during application, 9. No residuals at any time shall be stored at any application site, unless approval has been requested and obtained from the Division. 10. Maximum slope for residual application shall be 10% for surface application and 18% for subsurface applications. 11, When wastewater residuals containing a contrihutionfi-om domestic '�iwsteivater are applied, the Class B pathogen requirements as defined in 40 CFR Part-503 or the Process to Significantly Reduced Pathogens (PSRP) as defined in 40 CFR Part 257 Appendix 11 shall be met. Additionally, an evaluation must be performed wbich demonstrates the residuals ability to comply with this requirement. Upon request, a copy of this evaluation must be submitted including all test results and calculations. 11 In order to reduce potential odor problems created by the land application of materials from the animal processing facilities, sufficient lime will be added to the residuals to create a uniform mixture and Z-- achieve a pH of 10 for thirty minutes prior to injection into the soil. OPERATION AND MAINTENANCE REQUIREMENTS I The facilities and application sites shall be properly maintained and operated at all times. 2 Appropriate measures must be taken to control public access to the land application sites during active site site use and for the 12-month period following the last residual application event. Such controls may include the posting of signs indicating the activities being conducted at each site. 12, Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from the residuals application area onto the adjacent property or into any surface waters. 13. Residuals shall not be applied in inclement weather or until 4 hours following a rainfall event of 1/2- inch or greater in 24 hours. Any emergency residuals disposal measures must first be approved by the Division, 14, Residuals shall not be applied to any, land application site that is flooded, frozen or snow-covered, 15. Residuals shall not be applied at rates greater than agronomic rates, unless authorized by the Division, 1Animals shall not be grazed on an application site for 30 days after residuals application. Application sites that are to be used for grazing shall have fencing that will be used to prevent access after each application. 17. Food crops. feed crops and fiber crops that do not come in contact with the residuals shall not be harvested for 30 days after residuals application. 18, Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (ex, tobacco, melons, cucumbers, squash, etc.) shall not be harvested for 14 months after residuals application. 19. Food crops with harvested parts below the surface of the land (root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for 20 months after application of residuals when the residuals remain on the land surface for four (4) months or longer prior to incorporation into the soil. 20. Food crops with harvested parts below the surface of the land shall not be harvested for 38 months after application of residuals when the residuals remain on the land surface for less than four (4) months prior to incorporation into the soil. 21. Turf shall not be harvested for I year after residuals application if the turf is to be placed on land with a high potential for public exposure. TH. MONITORING ANT REPORTILN!�.I�U�IREM�ENT§ I Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to insure protection of the environment will be established and an acceptable sampling and reporting schedule shall be followed. 2. Proper records shall be maintained by the pert-nittee tracking all application activities. These records shall include, but are not necessarily limited to the following information: a. source of residuals b. date of residual application c. location of residual application (site, field, or zone 4) d. method of application e. weather conditions (sunny, cloudy, raining, etc.) f. soil conditions g. type of crop or crops to be grown on field h. volume of residuals applied in gallons/acre, dry tons/acre or kilograms/bectarc (continued on area page) 4 H i. annual and cumulative totals of dry tons/acre of residuals, annual and cumulativ( each heavy metal (which shall include, but not be limited to cadmiurm copper, I zinc), annual pounds/acre of plant available nitrogen (PAN), and annual POLinds/act applied to each field, A representative annual soils analysis (Standard Soil Fertility Analysis) shall be conducted on each site receiving residuals in the respective calendar year and the results maintained on file by the Permittee for a minimum of five years. The Standard Soil Fertility Analysis shall include, but is not necessarily limited to, the following parametcrs� Acidity Manganese Potassium Calcium Percent Humic Matter Sodium Copper PH Zinc Magnesium Phosphorus Base Saturation (by calculation) Cation Exchange Capacity 4. A residuals analysis will be, conducted annually from the date of permit issuance by the Permittee and the results maintained on file by the Permittee for a minimum of five years, If land application occurs at a frequency less than annually, a residuals analysis will be required for each instance of land application. The residuals analysis shall include but is not necessarily limited to the following parameters: Aluminum Ammonia -Nitrogen Calcium Magnesium Nitrate -Nitrite Nitrogen '/"o Total Solids pH Phosphorus Potassium Sodium TKN Plant Available Nitrogen (by calculation) In addition to the above, the following pollutants shall be tested in each residual once prior to renewal: Cadmium Copper Lead Nickel Zinc 5, All residuals included in this permit must be monitored annually from the date of permit issuance, for compliance with condition I I I and/or 12 of this permit (if necessary), Data to verify stabilization of I the residuals must be maintained by the Permittee. The required data is specific to the stabilization process utilized, but should be sufficient to clearly demonstrate compliance the Class B pathogen requirements as defined in 40 CFR Part 503 or the Process to Significantly Reduced Pathogens (PSRP) as defined -in 40 CFR. Part 257 Appendix 11. 6, Three copies of all required monitoring and reporting requirements as specified in conditions 111 1, 111 2, 1113, 111 4, and 111 5 shall be submitted annually on or before March I of the following year to the following address� NC Division of Water Quality Water Quality Section Non -Discharge Compliance/Enforcement Unit Post Office Box 29535 Raleigh, North Carolina 27626-0535 5 PF7- rN0 neompliance Notification: The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (910) 771-4600, for sites located in Davie, Yadkin, and Wilkes Counties, and the Mooresville Regional Office, telephone number (704) 663- 1699, for sites located in Alexander and Rowan Counties, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the land application prograrn which results in the land application of significant amounts of wastes which are abnormal in quantity, or characteristic. b. Any failure of the land application program resulting in a release of material to receiving waters, c. Any time that self -monitoring information indicates that the facility has gone out of compliance with the conditions and limitations of this permit or the parameters on which the system was designed, & Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system transporting residuals to the application site, Persons reporting such occurrences by telephone shall also file a written report in letter form within five (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS I The COMPLIANCE BOUNDARY for the disposal system is specified by regulations in 15A NCAC 2L, Groundwater Classifications and Standards. The Compliance Boundary is for the disposal system constructed after December 31, 1983 is established at either (1) 250 feet from the waste disposal area, or (2) 50,feet within the property boundary, whichever is closest to the waste disposal area. An exceedance of Groundwater Quality Standards at or beyond the Compliance Boundary is subject to immediate remediation action in addition to the penalty provisions applicable under General Statute 143-21 5,6A(a)(1), In accordance with 15A NCAC 2L, a REVIEW BOUNDARY is established around the disposal systenis midway between the Compliance Boundary and the perimeter of the waste disposal area. Any exceedance of standards at the Review Boundary shall require rernediation action on the part of the permittee. 2. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided, 1 No land application of waste activities shall be, undertaken when the seasonal high water table is less than three feet below land surface. V. INSPECTIONS I Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials , enter and inspect any property, premises or place on or related to the application site or facility at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy, any records that must be kept under tile to and conditions of this permit-, and may obtain samples of groundwater, surface water, or leachate. 6 fa r lead Permittee '11 1 The Permittee or his designee shall inspect the residuals storage, transport, and application a prevent malfunctions and deterioration, operator errors and discharges which may cause or lead release of wastes to the environment, a threat to human health, or a nuisance. The Permittee sh maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shal I be made available to the Division or other permitting authority, upon request. V1. GENERAL CONDITIONS I This permit shall become voidable unless the land application activities are carried out in accordance with the conditions of this permit, the supporting materials, and in the manner approved by this Division. 2, This permit is effective only with respect to the nature and volume of wastes described in the application and other supporting data. 3. This permit is not automatically transferable. In the event that there is a desire for the facilities to change ownership or a name change of the Permittee, a formal permit request must be submitted to the Division accompanied by an application fee, documentation from the parties involved, and other supporting materials as may be appropriate. The approval of this request will be considered on its merits and may or may not be approved. 4The following are approved sites for residuals application (see attached map[sj): Application Area [acres] Site No, Ownerfl-essee (excludingbuffers) Alexander Count-y AL 1-01 John Henry Barnes 8.5 AL 1-02' John Henry Barnes 9.8 AL 1-03' John Henry Barnes 165 AL 1-04 John HeM, Barnes 155 AL 2-01 Michael Bowles WO AL 2-02 Michael Bowles 5,5 At, 2-03 Michael Bowles lU AL 3-01 Vaughn Rogers 17.4 AL 3-0 aughn Rogers 23 2 AL 3 - 0 3 Vaughn Rogers 3&8 AL 3-04 b Vaughn Rogers 13,2 AL 3-05 b Vaughn Rogers 12.8 AL 3-06 Vaughn Rogers 18.3 AL 3-07 Vaughn Rogers 14.1 AL 3-08 Vaughn Rogers 10.1 AL 3-09 Vaughn Rogers 4.6 AL 3-10 b Vaughn Rogers 18.0 AL 3-11 '1 b Vaughn Rogers 119 AL 3-12 b Vaughn Rogers 29A AL 3-13 Vaughn Rogers l&6 AL 3-14 Vaughn Rogers 29;9 AL 3-15 Vaughn Rogers 8.0 AL 3-16 Vaughn Rogers 10.9 AL 3-17 Vaughn Rogers 29;9 AL 3-18 Vaughn Rogers 30.6 7 TOTAL ACRES IN COUNTY 422.3 Application Area [acres] Site No, OwnerF Lesse excludin buffers) Davie County HD -ill Herbert Dooley l-ilk- 22 Herbert Dooley 183 GD-ill Gregg Dooley 23,E TOTAL ACRES IN COUNTY 83.3 Rowan County 13 Dr. Richard Adams 2 .11 r. Richard Adams 13. R Dr, Richard Adams 30,0 Dr._ Richard Adams 60.0 K Dr, Richard Adams 60,0 Dr. Richard Adams 150.0 Dr. Richard Adams X0 r. Richard Adams 93.0 Dr, Richard .Adams W R Dr. Richard Adaaaas 253 O, Dr. Richard d Adams 30.0 TOTAL ACRES IN COUNTY WO `dikes Count), \V 1-01 Diana Pardue Mathis 6436; WK 2 pl Villas Hudspeth 39.05 WK 2-02, Dallas Hudspeth 14.34 WK 2-0 "rim Hudspeth 64.90 AkK 3-02. Donald and Mae Duncan, 51.70 WK 4- 1 Donald Duncan 3 8.81 TOTAL ACRES IN COUNTY 273,15 Yadkin County YK 1- 1 Lemuel Chamberlain 40M YK 1-02 Lenuel Chamberlain 49.91 YK 1- 3 Lemuel Chamberlain 161 YK 1. 3 Lemuel Chamberlain 18A7 "t`K 1-06 Lenuel Chamberlain 44.0 YK 1-07 Lemuel Chamberlain 8 ,8t7 YK 1-08 Lemuel Chamberlain 19,4 YK 1-09 Lemuel Chamberlain 12.34 YK 1-10 Lemuel Charitberlaiaz 9.40 YK 1-11 Lemuel Chamberlain 61.65 YK 1-12 Lemuel Chamberlain 25.10 Y% 1-13 Lemuel Chamberlain 4.19 YK 1-14 Lemuel Chamberlain 7 33 YK 1-13 Lemuel Chamberlain 3062 YK 1-16 Lemuel Chamberlain 1 ;'1 YID 1-17 Lemuel Chamberlain 6A8 YID 1-18 Lemuel Chamberlain 13.69 (Continued on next page) Application Area [acres] Site No, Owner/Lessee (excluding buffers YK 1-19 Lenuel Chamberlain 2436 YK 1.2p Lenuel Chamberlain 1164 YK 1 -2 1 Lenuel Chamberlain 1193 YK I - 22 2 Lenuel Chamberlain 635 YK 1-23 Lenuel Chamberlain 4738 YK 1-24 Lenuel Chamberlain 8m56 YK 1 -2 5 Lenuel Chamberlain 21.95 YK 1-26 Lenuel Chamberlain 5.34 YK 2-01 Thomas Peachey 8,09 YK 2-02 Thomas Peachey 24.23 YK 2-03 Thomas Peachey 26,07 YK 2-04 Thomas Peachey 3111 YK 2-05 Thomas Peachey 5,66 YK 2-06 Thomas Peachey 35.04 YK 2-07 Thomas Peachey 13.73 YK 2-08 Thomas Peachey 3T03 YK 2-09 Thomas, Peachey 10,73 YK 2-10 Thomas Peacbey 10.05 YK 2-11 Thomas Peachey &00 YK 2-12 Thomas Peachey 11,22 YK 5-01 Ronald C. Howard 7.00 YK 5-02 Claude and Ralph Howard 2 6,210 YK 5-03 John'. Howard 36.00 TOTAL ACRES IN COUNTY 8W85 TOTAL AVAILA13LE ACRES 2,270.00 This land application site is partially covered in soils having a seasonal high water table at depths ranging from zero to three feet below land surface. No residuals shall be applied to this field during the period front November through April, inclusive, unless angering on the site verifies that the apparent water table is greater than three feet below land surface. Approval must be obtained from the Mooresville Regional Office, telephone number (704) 663-1699, Prior to beginning land application operations on this field„ This field has slopes up to 18% therefore, all residuals niust be injected. In addition, this field must be monitored closely to ensure that no runoff occurs. 6. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statute 143-215.6A to 143-215.6C, 6, The annual administering and compliance fee must be paid by the Pernirttee within thirty (30) days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this pen -nit as specified by 15 NCAC 2H 0205 (c)(4), T The issuance of this permit does not preclude the Pennittee from complying with any and all statutes, rules, regulations, or ordinances which may be imposed by other government agencies (local', state, and federal) which have jurisdiction. I 11r_ Tile Permittee, at least six (6) months; prior to the expiration of this pert -nit, shall request its extension® Upon receipt of the request. the Commission will review the adequacy of the facilities described therein, and if warranted, will extend the permit for such period of time and under such conditions and litttitations as it may deem appropriate. p, This permit may be modified, med, or revoked and reissued to incorporate any conditions, limitations and monitoring requirements the Division deems necessary in order to adequately protect the environment and public health. 1€ , This permit shall become voidable awnless the agreements between the Perrnittee and the Ian do��ners/]essees are in full force and effect. The land owner agreements are considered expired concurrent with the expiration date of the permit and must be renewed at the same time the permit is renewed. Permit issued this the: thirty-first day of larch, 1998 NORTH X INA T IRO F ITAL ANAGEMENT COMMISSION r s , Freston Howard, Jr., P.., Director Division of Water Quality y .Authority of the Environmental Management Commission Permit Number bemr* WQ000 701 10 EVe p .,° t TV Sludge Land Applications/Disposal Report Form Annual Sludge Analysis 19 1 Per ittee: Holly Farms Poultry Industries, Inc. ( r-mon Plait) Permit No.: t 100RESVIIIE REGIUKALPEKE Sludge Sample No.1Z Date Collected Location arplin Parameter Wet Concentration *Dry Concentration **Dry Loading ( I) ( �` ) (Ib dty ton) PO4 as p 6 a a ra NH3as N . 4 ., N2 I+ N2 61-N 0. 1 d Oil & Grease A CU 4 � PCP N i,, . 5 Pb 0 , .< 2 i. I e idua Chlorine P.A.N. I ubsur ac - (2) Surface Applied Total. Solids O pH (.u.) e sludge p (circle as applicable): I) compost, DAP, aerobic digested, anaerobic digested, drying beds,. centrifuge, belt press, other (specify) 'r concentration g - t 5 ( J`k ) ref concentration (� /l) x 100 solids *Dry loading (lb t /dry° ton) - .002 x mg/kg (I) If applied by subsurface injection: P.A.N. ('Plant Available Nitrogen) ; .2 (T .CNN as N - N 2 N ) (NH3as N + N 2 N ) 2) It surface applied: .2 (T _ ` as N - NO2 e, N 2,) - 5 (NH3as N NO2+Not i Page I of 3 Sludge Land Applications/Disposal Report Form Annual Sludge Analysis WK-KMOOM Pe itt e# Holly Farms Poultry Industries, Inc. ( Plant) Permit No. 000v to Sludge Sample No. �V Tate Collected 1 - -10 Location of Sampling .ParameterWet Concentration *Dry Concentration **Dry Loading ( /l) (mg/kg) Ubs�dry ton) TKO qo2da NH3 as N zol_. N 2 + NO3 .d Oil & Greaseto 0oo � u 11040 PCB i b 9 Residual Chlorine MtA (2) Surface Applied Total ,Solids ( ;. PH (su.) " Type of sludge (circle as applicable): T) compost;, DAF, aerobic digested anaerobic digested drying bads,, centrifuge} belt press, other (specify) *Dry concentration (mg/kg) wet concentration (m /l) - 100 solids **Dry fading (l s./dr toy) = .002 x mg/kg (1) If applied by subsurface injection: * *P.A. . (plant Available Nitrogen) .2 (T NH as N - NO2 - )" + (NH3as N N 2 O ) (2) If surface applied: Page 1 of 3 . Sludge Land Applications/Disposal Repor Annual Sludge Analysis Permittee, dolly Farms Poultry Industries, Inc. Permit No. w Sludge Sample No. Date Collected _ Location of Sampling Parameter Wet Concentration *Dry Concentration Dry Loading (m) ) lbs/dry ton) PO4 as TKIN NH3as N 5-920 NO2 0 Cd 0.001 Oil & Crease Cu PCB Ni Pb 2n ^ Residual. Chlorine P.A.N. () Subs fac r (2) 'Saar ode pplied -Z` Total Solids )r pd s.U.) Type of sludge (circle as applicable). 1)- compost, DAF, aerobic digested anaerobic digested, drying beds centrifuge, belt press, other V (specify) *Dry concentration (mg/kg) - wet concentration (mg/1) x 100 solids ' Dry loading (lbs./dry tor) .002 x mg/kg ) If applied by subsurface injection: P. .N. (Plant ,availableNitrogen) .2 (TKN-NH3as N - NOZ 03) ( as N + 02- C ) 2 If surface applied: .2 (TKN-NH3 as N - NO2 - IBC .5 s - NO2+NO ) RE PORI' NUNWER A & L EASTERN AGRICULTURAL LABORATORIES, INC HU1r—U4L 7621 hi in Road # Richmond Virginia 23237 * 004) 743-9401 SAMPLFS S f. N D SUBMITTED T rl HULLY FORMS rWi �, MAINI f;Rf1b1jFR, P u nEM— 3UZ"�;L' BY, v () 3 0 x ,Ii ;J WILid EShOR0 NC ?,tO'Yf DATE OP REPOW I VA C; F,, I SOIL ANALYSIS REPORT ORGANIC PHOSPHOAUS POTASSIUM MAGNESIUM CALCIUM SODIUM PH Cation HYDR01 RASE SATIJAAIION ICOMPOTED) MATtER P-2 --------- GEN Exchaftge -- I - ---- LAD K N19 Ca Na SOIL BUFFER copaltity . . (WE4�81avj N,,HC(),4 P % SAMPLE NUMBER ENO .... EEC K PAD Na NUMBER RATt IbAJA opm P RAI( pok" f RAI ppm K RAI E ppahEIRATE PRO Ck RATE ppm ft* __RAT PH ON RvM11 000 Ineq/11)(RE J21 u 414 4 J. H V H 5 0 0 5 L "I G.0 4 . '17 . "i a5 j 4A tj 4! 4 3 4, 1 eJ 1� I I z� ;11 4 Aj H r 10 fw,� 4f VL 6,. h 5.11 0 1 '1� d 3 . 4 o.0 — U L, 4 6 YI I M f 11 If fn, VH 4,� 4 �U ivi 4j VL 6.5 U . r� C) 1.5 i,t./ 40.e 2 1 C1 Z 4 t Z. I 1 0 M I L 20 L 1T 9 M ,804 Vti� 7 44 1 J M 4f VL 6.5 6.Y C . o f 3.4 4 J 3 7 .5 2.7 ISEE EXPLANATION ON HACK) PARTWAL SIZE ANALYSIS MANUA, So I LISLE Moiye- SAMPLE PKrRATE SULFUR ZINC NESE [RON COPPER BORON EXCESS SALTS C"LORIDE UENUM LIME SOIL NUMBER NO3 S Ma Fe Cu RATE CI Mo TEST r URE -fo RATE "a -Co RATE spWO RATIF Q RATE pp*M6 RATE y S RAIL I! T, ppeWRATE ppo ppw SAND SILT CLAY Mk,l I CV. It, I�UJ I, F PPLV kL,U L t !I N r, P I,, W SM WS le5lod, samoies one -U-144 a r rlakw—n 0 jh,1,Jy days alto, 10stirly, A & L EASTERN AGRICULTUAAL LABORATORIES, INC, C. tXNMAIN Jf)N,-,:; C /277'RvW&'w C1�14,) A G L EASTERN AGRICULTURAL LABORATORIES, INC Whiteptne Road # RichmondVirginia 3 . ®4) 743-9401 @9') SAMPLES Attu 1 4 ") SENO submiT"T to HOLLY R14,;', t--N6 S AIN GROWER0 ,60 BY: HOLLY °ARMS 1: I ATTN: OI I TAYLUK , 0 6 0 x 3�11 DATE OF t.E"MI I i; .� �� r �� � P AGL SOIL ANALYSIS { ORGANIC PHOSPHORUS POTASSIUM MAGNESIUM CALCIUM SODIUM PH cation PERCENT MATTER_,.... : _...... _. __ ..,,.. __ .._ µ HYDRO ExchangeSASE SAT°URATMN03OMPUTED) 9 �.. �. �: __.._ 77- AMPLE Ea tWeijk Dray) N,,HC��.R.R m. .:, .� % % Go- NUMBER C ' EEIU Ca R O NUMBER SATE Ilt IR pps(a P RATE ow" A RATE p m K FRAY, pp+� p WE ppm Co RATE ppm N w RiAI E PR ON me4fl 0 hC�yd lUilE IS 1L ,'. � 1 :T2 VtI t V " I '39 h 5 "'tt � 43 L 6. o _ .. . .d i .R, 4Y.5 3.7 0 ��U14 ,R . `Lt d I a`li G H y r' "1 6 0 "06 vH 550 M 4 0 L . V' 0.1 J . . 3 33.1 .) J . 1 1.5 . RU 4 11U b j ` 5n Vtt� I Vt a4 F .d Vfit( 5540 ?1 4J L 0.5 o.i t�.4 4.1 Vie. ail. � IT.5 4.0 FI u z 1 Z. -:RIM 4 5 Vh N ri tt 4 L 30 Vh 7t.t � T V'"� t.` U.1 .`� . . :1 . . � .1 s MA A, SOLUBLE PaMULYU• PARTICALSIZE ANALYSIS NITRATE SULFUR ZINC IdR l IRCiR� GtMPPLG Uf7RCR EXCESS SALTS CHLORIDEDENUM p S §A PLE LIME % � % % SUIT MUSE 3 S CA EMrs Ea CRR $ RATE Ct AMA TEXTURE ttt!Q3 __.� _ATE ..,m LAY d pa 9 aaS RAY pp.r K� RctTR.�� �a� iGtaaSC pp�raRA�zRRA7I5 To WE pproaC.Ai&TK RiC�§TC maivat»kmplAip Rpm GlT#p.i pp.�RM,oRRp.ifC SAND SILT I G� .�.�_,�u«�.... ...... 1 , :I roQwot aamp"ej 00y V' wo w"'pwjo 10it� [3 Say wel ar. u'.wmsit & At S k�uP tlaa o91 to O F ly twY5 dQtit lo'O"g, A A L EASTERN AGRICULTURAL LABORATORIES, , INC, CeM A N jON o ca v s��e,=u,;. �Gd ftiaTiPJ fi`s "JAitl'3i`a Mh+:R °t $.k 6�Y"ut'it l��=d�.�NGe �..?� isxaTr tE Pio ;+".t 1.�Ewt-+.eve tx�. «.,y '}c ki'r waar Av: OL hill "Y" Ti 4E.' H='S41AS nN 0µ9nt fly46 Y h,E. CCMU'k.FrY 0 Lf3s. Pt R ACRE �'�"Ub t tad r [#.&LAP t,t,�;�E}s 6�tuF,R�Pa4 f4k.E Ma4,a: ».aa rm,.;vJ�6kI'dc'1Ylin:. r#., a'.l i�.z sN �ca.9 di „8&=}��4381 E.S$T '4U &kl.a, 6iC Va 4rtk R". ,t; . -:. _ ... _.:. _ ..,.ue �...�. ..xb;.ai.,v_. aarvsmu.emx �»�s is t'L..�..�rv�.t+w..t]m.:.ma,be1._,•:s ,k ate.* Lx.v� _� 1 1 Whitepine Road Richmond Virginia ALL) ` N 4 a ." AMPL FSEND SuEIN1111 T0, HULLY FARMS j N MAI N GROWER P 0 — .ByHULLY :a RM'0' L MAIN 1TN: DAVID TAYU011 P 0 sox 613 ORGANIC e PUOSPHORU5 PUTA SIU t MAGNESIUM � CALCIUM SODIUM PR Cation MATTER hEYbRUh Exchange BASE SATURATION (COMPUTED) LAB PT P K CIO 0 Na SULK; BUFFER CEN Cap atq SAMPLE@@ N �. iw.,A Mail : N,�r�GOIP !� %NtIIR�SFR p LNR N C'Ex NUMBER .a.S Ca R Na ERATbl.rAaaRT.,,,,.._"m _p!!.RAlk pout M9 n,CaRATf uaaraaIATI pW 019 JTIIIR �._,. _�.. ... rR. ._...� �L.x. �iU - ..1 1 U4 El i^ is :,)0 H 1H SL 5 V fi 190 L � 6 VL 6. 1 6 , 1.1 3 . e 4.3 51.j 4 ta.Z 1 . 0 2.5 L I L d:;,.a Ji.1 6'-, 411 UI1 1 14 V 14!1 M V H,-' 1010 h 41 VL` 1.3 U.Q 13.6 15'41.2 0.0 1.5 f jt 4.0 U6111 H 56 Li 120 h 199 VH t 1.1 iM 10 L 6.4 6.9.t 1.4 4.3 33. 5 49.1 9.0 4.1 I � ' i I (SET: LXPLANA ION ON BACK) h9ANCaA• SOLUBLE FLYS PARTICAL SIZE ANALYSIS SAMPLE NITRATE SULFUR ZINC NFSE IRON COPPER BOVION EXCESS, SALTS CHLORIDE DENUM — j. .,_m.---_1— _ — LI E % I a % SOIL NUMBER 903 S za Non F* Cu U RATE CI Ma� IE�T RE P +NiTdafa XE aP ^StiATE aAATI. ppm-MnRAU pp -"feRATE Wpoa-C.RATE ERATE Imb GRATE ## CI RATE foo-04RATf SAND $IL.T..�. xILA`P »n... _..w_ ... ,.� LL I t, utttsvxP VL V d.+).e'x". pq I ..� h.143L F'k6 S b� P4€Ey fik .a4RL,C f#d &I CJ [3,AUy ..w; -'fmr va:ax �r9 aaa a, m;xi fy t€r €na. q ,iav s+taut 8e.,.d%rw "i�sarlUs s a¢e mart ac�la�ca A A L EASTERN rwAGRICULTUAAt. LASOAATOFUE , INC, Ry sokmpI F, ACCI 4 kXq I.Nad,4 SUBWf G ED I-(, i LL o 8, � & MAIN G140u ERw P 0 BY: HA-LY F At.r i s" i.s MAIN DAVID TAYLJR P aox 16 ORGANIC PHOSPHORUS POTASSIUM MAGNESIUM CALCIUM SODIUM pII xtlzR PERCENT' _,." _ HY RO- BASE SATURATION (COMPUTEER LAIC MATTER PI P1 IC Mo CA GEN Exchafive SOIL SUFfEIT AMPLE � (wf,.k Sf ly) I�a1'rCO3T f, � Cplpaclty t� % NONCIiE EAR » H F C NCFDMELi ��.� ..m RATE Ibs /A pp- A RATE ..: Own p RAIE ....._'p 9 x IIATE i p# MjAAII, PAM CA RATE.. _ pprso- aAATf p pp /ffi p M04/'1689 i U NA I L A : „# 4.1 113CI 1 H � � � M 121 H Vii Iw 10 L 6 5, L 6 . 3 0.4 U. I 1. 51.0 � 14.5 F u2 101, 1� 1 41.L v i e � M e � 4" ' vili 5 69 V H 1 U t,I) L 1 .0 U.1 11 .1 6. 9 42., _ 0. 2.f) 4»A #" M., ;X ' A 6 l : C, 'p S 105 4 E d 'tlM 0. Y R. 1 +N 0 G . U 9.1 2.8 . 8 M 10 . Zi E MANGA, SOLUOLL Nil ILY& PARTICAL SIZE ANALYSIS SAMPLE Cw1iRr4TF ULFUR ZINC NESE IRON COPPER BORON EXCESS SALTS CHLORIDE DENUMLIME SOILN0 NUMBER ap,�auTx�A�c PAA S So Ma Fe OR G RATE ICI n TEXTURE $ DATE peat �a RATE ppca o RATE pp It RATE powty HATE Po RATE m sihm RATE pp •C# RATE pp a RAT SAND SILT Ct AY i � I "9 t ti Aac a1s. apples Q,fiy to th. Sd t^tt.gcl WsUl'u tamwas 4r0 iata(iPed d eSYu x8a 11 as i1 PMd tr.,tM ujy4 aftew ::G fttn A A E EASTERN AGRICULTURAL. LABORATORIES, INC. {r ............ ..... z_._ ,..,.....,..,.,.. .....F w._..... _, .I,.:,...._.... ,.. r_ _:,_ _..,_ ,, a na;,sk, tS Hlkl iN— tti We k O'W i Fi § 3t u M aiF4 . 1.,1 ,. .,! @� 1 tI, tet ^' t' ktI .I t l „�. "�4,. I, ._ x$bi n... PAUt T C8w ➢it l'k k Ik,r v&). I PkY as T. t 0 k,k N4'k i}T 'y0 k BS Pt A'iC 8F. T'°44.11, a C"4't F wk r ttt h m T'; fN opm fiw 2,4 TO i 1Pw51.i4" f t? R..t `..a e"LN dCVU, K- _._...,W �a. s eou� r a...r,� a. �.a:u, r. ., ,.:_ ,,•E�."a *.,..;xt % i `i4'C$ti ��k'.2': Nc11f,S D 10PJdeE RUIZ—U4U 7621 Whitepine Road * Richmond Virginia 23237 * (804) 743-9401 RL CC APLI, SEND SUBMITTED� To ULLY FARM,i o, MAIN GROWER: c 01 f a Y. He-iLL,Y FARMS LN(a MAIN r N: DAVID TAYLOR 6ex 6 W .. E aaxeO 4 N SOIL ANALYSIS REPORT ORGANIC PHOSPHORUS POTASSIUM MAGNESIUM CALCRI4 SODIUM PH cation . m ...... _._..._.._ _. m .. _-- NCI N• SASE SATURATION (f.'O a1PUTEIT¢ F�AT�EI3 ,,.._..a r. � _ E�ss:I��� LAB PI PT }6 14y C N GEE} �. SAMPLE 1we44 814y) t�,tRC03 SI7t SL EP N C Iu III % % T6 NuMBE. i . 11ift SAT£ aww�a._.�..... r H C EC, CaNUMIER ffib�,�A ���rRATE n�A��pR�IE PR#RAT€ p�ERAtE pc�a��ArE N � ttII4 Raall34 a; r � i (SCE EXPLANATION ON RACK) Ea9A NOa A- SOLUBLE MCF L'Y S PARTICAL SIZE ANALYSIS SAMPLENITRATE SULFUR ZINC NESE IRON COPPER 80"ON EXCESS SALTS EHLORIDE ISENU _ I._.�_. LIME m .. g W) S des A E CRR ATE CI Ma SOILNLIII ETi TEXTURE RA p na 401 N1E p.R w4 RATE p,Zo RATE pp Ma RATE P " Ea RATE Ep v RATE : 4 RATE r � mh#ol'' RATE wa+-ER RATE PRAT£ SANE) SILT" CLAY 9 ai € rra„oma nprrtEmt aavvgy fbr ar.a ,airs, pit" �.aMares sra r6e4 ,arod A IE L P YCtT A NI LTLTLIFfiAL tt IT tiITIES, I l LB FYeA 1"$Na".s VkiP Y te. Ni VLI, Ll:••:+':0 "i,it l: "e,e.a=e,t..fq •t, .w`'d, as dt ti ... hh4d4.8IPLY N 4v3',.. R SS.ALTS F t l ltPM tilt 4,6 TO 9.ONVk UT TO LUs P'Lw, 4,Fdk I` Cay „raa i 6hfitTT' ci T^>a1 R'btiJ�a E,PY m?: a P P ,'F€ �.e��srl ...°, k2vJ k, ,' I 5:. € :.rfl I'Po ll, Ei'r 5 7= 1"o T llU at i° i➢ k„S h^€.ikr Fae:"El' a£.�'.'s REPORT U Ups LABORATORIES AUIO-U4L 7621 1 "HITEPINE RD. RICHMOND VA.23237 04-743-9401 SEND TO. HOLLY F A ,c i °i i"A i is CUSTOMER ACCI rt45346 AVNI: DAVID TA YL04? P ".: - 0'id rI P i f SAMPLES rom S: , C q 0 NC e SUBMITTED By: i W_i f k : jai r, tad DATE P REPORT � � � „ � PAGE t SAIL ANALYSIS REPORT SAMPLE AU Nitrogen phru « phoru a urttlt�u t eng - Patel i itii Mrera SulfurCalcium slum noslu ti Sod� nose ,�rttrrtente Nitrate Copper in pp Nitrogen Nitrogen IDENT NO: % ° P" � , R � U QUA %Mgpptrt Pe ppt AWN ppmCu palls n PPui ppm A 10243 140 32 55 {44 252 I A 10245 1001 18 51 P5 145 92& 28 3 10247 781 28 40 LAB Cadmium Cure- mium Mickel Lead t�rgerlt Arsenio Mercury Selenium Nitrogen NO. pan d ppCr pp Ni pp, Pb ppr A pp g pp a 143 '. 5 2 10244 <0 5 5 1 10245 0 5 5 15 10246 <0.5 5 5 Valuos on this roport art the total mount of the sampt , Our reports and lattara are tear iha oxchonwa and confiadnnal uaa of our olionts, and may not be roproducird to whole or to part, not may any reference be made This report applies only to the sample(s) lost ad, Samples its to the work, the raar>lls, or Ilia company in any advertising, newts ralaaaa, or other public announcements without obtaining our prior wrrittan anthrui ati n. retained At maximum of thirty days attar tasting: (A(, A 4 t, EASTERN AGRICULTURAL LABORATORIES INC. .I. la Ph.D. C REPORT NUMBER A & L EASTERN AGRICULTURAL LABORATORIES INC. ILA SEND ftmL TO: H 0 L L Y F A k t N' t 'I A I i�, CUSTOMER A C T 4 4 5 j 4') P 0 sox 68 SAMPLES vJ1L'KL';!i�1,0RU NC Zb6i'l( SUBMITTED DATE REPORT� , � c{OTyg ANALYSIS PAGE SOILREPORT SAMPLE LA Tirtr �k Phis- t s� , Sulfur Calcium µ Sodium Iron AluminumMen rus um noslutrf n s Copperzincitlti�kt fii t�ttrst Nitrogen NitrogenNitrogenn I P NO,h � �s PPS IMP At E� K : T�IYF :.. Pp Mn n Cuppm PPS P rn.. PPP 10248 35 15 4 0 10249 77931 35 5 10250 335 23 3 10251 343 26 4 G 10252 4G 29 53 LAB �tdmiui' tkr rtstukri rii Mickel Lead Arsenic Mercury S leniur Organic Nitrogen III P aI RpmCr f�P lit larrt Pbrn As 10248 1 <0.5 5 30 114 .5 5 1 10250 < 0.5 5 10 105 0.5 5 30 52 0.5 5 35 Valuos on this report art the betel ' mount of the sampi , Our ropods and tartars are tear aril exclusive and confiedrifial use of rarer ctidnt , and may not be rafrnadocadin whole or in port, near may any reforonca be made This f8projapplioS only ko the satrtpio(sl taxi . Samples are to kh,r work, tho t,&4uits of the company to any advertising, news release, or other public, announcomanis without obtaining our prior written authorization, retained a maximum of thirty days attar tasting. A & L EASTERN AGRICULTURAL LA130RATORIES INC. by �. � �:�' t I'•� �. it d'M: Paul .:t d . Chu, Ph.D.". REPORT NUMBER A & L EASTERN AGRICULTURAL LABORATORIES INC. 8U i -(J4 i 7621 WHITEPINE RD. RICHMOND VA. 23237 4-743-94 1 EN 6 C X is d SAMPLES ,W1LKLS,W,'Z0 NC 18697 UBMITTED Y RATE OF REPORT �w° .' PAGE SOIL ANALYSIS REPORT SAMPLE LA Nitrogen pkt - �' tSulfur Mutts � odium Iron AluminuManm � Copper inn �tirttrrtnnN Nitrate i E T. N� photos lure nn tum, Nei % � tprn En ppm At mesa Nitrogen Nitrogen pprrt Cif ppm n 1- 10253 05 33 41 10254 122 21 5 10255 164 26 34 L 1256 432 59 11 10257 577 45 68 LAB Cadmium hro- r tium Nickel Lead Arsenic Mercury rtium Organic Nitrogen pptff d pprnCr pp Ni pprrt Pbpprrt pp pprra So 1 253 0.5 5 15 10254 <0.5 5 15 10255 � w 5 5 5 10256 0.5 10 35 1025 5 10 1 Values aan thsa ra rt arq the total ' mount at the eai �rpl Our refxc its and Irrtturs Are for the exclusive and conf8edrund teas of rrur clients, and may not be reprraducad to wu la or in part, not may any reference be made This report applies only to the satrtrpleN i tested arnmes are to the wotir, the trrsuns, or the company in any advertising, no s taleasel,tar other pub t6c rtnouncanrestte a lthttut �t ain n our prior written authorization, ratamad a maximum of thirty days after i ling, caul L EASTERN A rNRN NJLT RAL LABORATORIES INC. try i�ii�i .r a ces I N C 0 R R 0 R A T E 0 REPORT OF LABORATORY ANALYSIS THE A3$URAKCE OF allALIff Holly Farms Foods December 04, 1990 P.O. Box 88 PACE Project 1600 River Road Number: 601101503 Wilkesboro, NC 28697 Attn: Mr. Danny Wyatt PACE Sample Number: 92 0545109 92 0545117 Date Collected: 10/31/90 10/31/90 Date Received: 11/01/90 11/01/90 Stick H2O Stick H2O Parameter Units MOL 1&2 10-31 1&2 10-31 (1) INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 0.260 NO - Calcium mg/kg 2.63 908 - Chloride mg/kg 26.3 5815 - Chromium mg/kg 0.657 1.61 - Copper, mg/kg 0.260 50.0 - Lead mg/kg 2.63 NO - Magnesium mg/kg 2.63 234.2 - Nickel mg/kg 0.530 3.684 - Nitrogen, Ammonia mg/kg 1.32 3368 - Nitrogen, Kjeldahl mg/kg 1.32 33816 - Nitrogen, Nitrate mg/kg 2.63 NO - Nitrogen, Nitrite mg/kg 0.105 3.87 - Phosphorus, Total mg/kg 0.53 22816 - Plant Available Nitrogen, by calculation mg/kg 2.63 9637 - Potassium mg/kg 0.260 1274 - Sodium mg/kg 0.260 1574 - lids, Percent Total % 0.01 3.,8 - Sulfate mg/kg 26.3 658 - Zinc mg/kg 1,320 29.7 - pH 0.1 4.21 - TCLP METALS Arsenic mg/L 0.050 - NO Barium mg/L 0.050 - 2.69 (1) All analysis performed on Toxic Characteristic Leachate. MDL Method Detection Limit NO Not detected at or above the MDL. 1700 Univenify Commicief Mete Offices Serving: Sri is, mifflescits Los Angew, California An Equal Opportunity EMP10YOV Chatiotte, NC 28213 Tarnp, Fiorillo Charloac North Carolina TEL: 704-697-9464 low$ city, Iowa Ashovifie, North Catefioa FAX: 704-597,8455 Sot Ffamisco, cafifoonia New nark, New York Kansas City, Missouri piltsbur2h, pormylvaris 4 paces ` it R F 0 R A T' E ti THE ASSURANCE at GUALI IT Mr. Danny Wyatt December 04, 1990 Page 2 PACE Project Number: 60110150 PACE Sample umber: 92 0545109 92 054511 Date Collected: 10/ 1/90 10/ 1/90 Date Received: 11/01/9011/01/90 Stick H2O Stick H2O Parameter' Units MDL l&2 10- 1 lit ; 10- 1 INORGANIC ANALYSIS TCLP METALS Cadmium mg/L 0.010 - NO Chromium mg/L 0.025 NO Lead mg/L 0.10 - ND Mercury mg/L 0.0005 NO Selenium mg/L 0.050 - NO Silver m /L 0.010 - NO ORGANIC' ANALYSIS TCLP PESTICIDES -OHC (Li dare) u9/L 0.002 - 0.34 Endri ug/L 0a00 - NO Nethexychler ug/L 5`•0 - NO TeaRhee ug/L 1-.0 - NO Chlordane ug/L 0.10 N Heptachlor ug/L 0.001 ` - 1.9 TCLP CHLOROPHENO YS ,4-0 ug/L I - NO Sil e ug/L I - NO 1 All analysis performed on Toxin Characteristic Lea hate DL Method Detection Limit NO Net detected at or above the MDL 1700 University Cammencial Place Offices S itg: Minnospolis, Minnesota Us Angeles, California An Equal Opportunity Employer Caailatte. NC 28213 Tampa. Florida Charlotte, North Carolina TEE: 704- 97-A464 Iowa City. hma Asheville, North Carolina FAX' 704"507 5455 San Francisco, California New York, Now ''fora Kansas City. Missouri Fitiallurgh, perevylvaris PI N T14E ASSURA149E OF dUA1.11Y Mr. Danny Wyatt December 04, 1990 Page 3 PACE Project Number: 601101503 The data contained in this report were obtained using EPA'or other approved methodologies. All analyses were performed by me or under my supervision. Charles M. Cabaniss Manager, Inorganic Chemistry Stimus Manager, Organic Chemistry 1700 University Commercial Place Wines Saying: momeopok minnatote Los Angeles, California An Equal Onortunity Eavloyer Minim, NC 28213 Tampa, Florkis chadalm Nmth Carolina TEL. 704M7-804 Iowa city, laws Ashoadle, North Carolina W: 704-597-8455 San Frw4sce. California Navy Yark New Yolk Kansas City: Missouri Filtswo. pemsylvatria THE ASSURANCE OF QUALITY Holly Farms 'Foods December 04, 1990 P.U. Box 88 PACE Project 1600 River Road Number: 601026504 Wilkesboro, NC 28697 Attn: fir, Danny Wyatt PACE Sample Number. 92 0543947 92 0543955 92 0543963 Date Collected: 10/ 5/9 10/` 5/9 10/ 5/9 Date Received 1 / /9 1 / 6/90 10/ 6/9 Harmony Harmony Rr edon Parameter Units HUL UAF Sludge DAF Sludge UAF Sludge' 1 INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 0.013 0.020 Cadmium mg/kg0.00 - - ND Calcium mg/kg 1.0 - - 3,7 Calcium mg/kg 1.3 6 -, Chloride mg/kg 10 4656 Chloride mg/kg 3.4 - - 41 Chromium mg / kg 0.010 -- 0.089 Chromium mg/kg 0.130 0.17 - Copes mg/kg 0.025 - 0.17 Copper mg/kg 0.033 1. Lead mg/kg 0.130 2.94 - Lead mg/kg 1.0 - R N Magnesium mg/kg 0.100 .96 Magnesium mg/kg 0.130 10.4 Nickel mg/kg 0.013 0.156 Nickel mg/kg 0.020 - 0.04 Nitrogen, Ammonia mg/kg 0.17 m - 1454 Nitrogen, Ammonia mg/kg 0.5 44 _, Nitrogen, Kjeldahl mg/kg .17 - - 9181 Nitrogen, Kjeldahl mg/kg 045 354 Nitrogen, Nitrate erg/kg 0.34 _ - NU Nitrogen, Nitrate mg/kg NU' Nitrogen, Nitrite mg/kg .0140 - NO Nitrogen, Nitrite mg/kg 04 ND a ( ) All analysis performed on Toxic Characteristic Leachater MOIL Method Detection Limit NU Not detected at or above the IUL- 1700 University Commercial Place Offices SerV4, mireteapoks, miftnasola Los Angeles, Califattes An Equal Opportunity Employer Gharlotte, NG 28213 Tama, Florida Charlotte, Norlb Coeur 7 L 704. S7•84 4 Iowa City, tows Asheville. North Carolina FAX: 704-597-8465 San Framisco, Cali€ntnta Now York, Now York Kansas City, wissouri PittsburIgh. Pennsylvania pt,D R P THE ASSUAANCE OF allALITY Mr. Danny Wyatt December 04, 1990 Page 2 PACE Project Number: 601026504 PACE Sample Number: 92 0543947 92 0543955 92 0543963 Date Collected: 10/25/90 10/25/90 10125/90 Date Received: 10/26/90 10/26/90 lo/26/90 Harmony Harmony Breeden Parameter Units MDL DAF Judd e 28LIlud2e p8f _11 udqe INORGANIC ANALYSIS (1) INDIVIDUAL PARAMETERS Phosphorus, Total mg/kg .070 - - 758 Phosphorus, Total mg/kg 0.21 7781 - - Plant Available Nitrogen, by calculation mg/kg Oa3 - - 2804 Plant Available Nitrogen, by calculation mg/kg 10 9000 - - Potassium mg/kg 0.10 - - 3.09 Potassium mg/kg 0.130 12.6 - - Sodium mg/kg 26 146 - - Sodium mg/kg 8.5 - - 4.10 Solids, Percent Total % 0.1 9.6 - Sulfate 29.3 Sulfate mg/kg 10 3125 - - Zinc mg/kg 3.4 - - 341 mg/kg 0.05 - - 0.614 Zinc mgg 0.65 2.94 - - pH 0.1 6.36 - 5.21 TCLP METALS Arsenic mg/L 0.050 - ND Barium mg/L 0.50 - 1.47 Cadmium mg/L 0.010 - ND Chromium mg/L 0.025 - ND Lead mg/L 0.10 - ND Mercury mg, L 0.0005 - ND Selenium mg/L 0.050 - ND Silver mg/L 0.010 - ND (1) All analysis performed on Toxic Characteristic Leachate. MDL Method Detection Limit ND Not detected at or above the MDL. 1700 University commerew piece Offices Serving: mirmapdm memscia Los Angeles. Caffortria An Equal Opporturaty Employer Charlotte, MC Charlotte, Tanva, FWW* Charlotte, North Carrifin TEL: 704a5974454 Iowa City, Iowa Asheville, North Carolina FAX: 704-697.8455 San Francisco, California Now York, New York Kansas City, Missouri Pittsburgh, Perwisyfwartia pace. THE A$sURANCE OF QUALITY Mr. Danny Wyatt December 04 I990 Page 3 PACE Project Number. 60IC26504 PACE Sample Number: 92 0543947 92 0543955 92 0543963 Date Collected. I 25 10/25 '9 1 /25/9 Cate Received. 10/26 90 10/26, 90 1 26/99 Harmony Harmony Breedon Parameter Units M L D F SJjqqe DAF Sludge AF Sludge ORGANIC ANALYSIS TCLP PESTICIDES g-R L Linda a ug/L 0.002 - ND Endri ug , 0.007 M Mathxychlu ugL 5, - Tuxahrla ugL I. MC Chlordane ugL 0.10 Heptachlor ug 0.001 - ND TCLP CMLORCP EMC YS 2,4-C ugL 1 - 24 Sit ugL I - ND } 1All analysis performed on Toxic Characteristic Leachate. M L Method Detection Limit E Not detected at or above the MIL. 1700 University Commercial Place Of fim setyin#; minnespok, minveseta Los Anplas, Cahfairris An Equal OpporturitY Cate later Charlotte, NC 28213 Torthra, Sorids Char tte, North Camlitta to 704•5744 Iowa City, Iowa Asheville: North Car fas FAX: 704M)`14 h soft Ftrowisco, cafifornsir Now York{ Now ratit Karns" Cult. Missouri piltswookytv pace. REPORT OF LABORATORY ANALYSIS THE ASSUIRANct Of QUAWT Mr. Danny Wyatt December 04, 1990 Page 4 PACE Project Number: 601026504 PACE Sample Number: 92 0543971 Date Collected: 10/25/90 Data Received: 1090 Breedon Parameter Units MDL DAF Sl iydg—e -7T) INORGANIC ANALYSIS TCLP METALS Arsenic mg/L 0.050 ND Barium mg 0.50 1.34 Cadmium lag /L 0.010 ND Chromium mg/L 0.025 ND Lead mg/L 0.10 ND Mercury mg/L 0.0005 ND Selenium mg/L 0.050 ND Silver mg/L 0.010 ND ORGANIC ANALYSIS TCLP PESTICIDES 9-BHC (Lindane) ug/L 0.002 ND Endrin ug/L 0.007 ND Methoxychlor ug/L 5.0 ND Toxaphene ug/L 1.0 ND Chlordane ug/L 0.10 ND Heptachlor ug/L 0.001 0.17 TCLP CHLOROPHENOXYS 2,4-D ug/L I NO Silvex ug/L I ND (1) All analysis performed on Toxic Characteristic Leachate. MDL Method Detection Limit ND Not detected at or above the MOL. 1700 University CGMff*fCnn Place Officts Sol*q: Nfinneepoks, mimwsots Los Angeots. California An Equal Opportmity Employer Charlotte, NC 28213 Tompe, Florida Chadolte, North Carolina TEL 704-508454 law# City, Iowa Asheville, North Carefins FAX: 704-597-8455 San Francisco, cafifefflis Now York, New York Its City Missmi Pittsburgh, Peonsylvaris pN'� C R R R 5 R A I E THf ASSURANCE Of MUALITY r. Danny Myatt December 04, 1990 Page 5 PACE project Number: CICSC The data contained in this report were obtained using EPA or other G approved methodologies. All analyses were performed by me or under my supervision. Charles M. Ca aniss Manager, Inorganic Chemistry Jelin T. Stimus Manager, Organic Chemistry 1700 University Commercial a oftex arq. mirvaAW4. Kawats Cos Aolties, Calilornis A4 Equal Gpawtvoily Einlriatot Charlotte, NBC 28213 ieeapa, FirwhIs Charlotte, North Catalina TEE: 704.557. 4 4 low# city, low# AshaviRe North Car FAX. 704�5 7 $4 5 San ffemivm CaNlf rraa New Yet , New 7w 5 as W Misswri pittlimugh, pennsylvainut P, REPORT OF LABORATORY ANALYSIS THE ASSURANCE Of 4UAW1 Holly Farms Foods December 05, 1990 P.O. Box 88 PACE Project 1600 River Road Number: 601030500 Wilkesboro, NC 28697 Attn: Mr. Danny Wyatt PACE Sample Number: 92 0544293 92 0544307 92 0544315 Date Collected: 10/29/90 10/29/90 10/29/90 Date Received: 10/30/90 10/30/90 10/30/90 Harmony Harmony Wilkesboro Chlorine Chlorine Sludge Parameter Units MOL Basin Basin DAF INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Cadmium mg/kg 0.045 - - 0.045 Cadmium mg/kq 0.320 0.613 - - Calcium mg/kg o.45 - - 151.1 Calcium mg/kg 3.23 3323 - - Chloride mg/kg 32 4645 - - Chloride mg/kg 4.5 - - 959 Chromium mg/kg 0.113 - - 2.00 Chromium mg/kg 0.806 6.677 - - Copper mg/kg 0.045 - - 70.6 Copper mg/kg 0.320 46.45 - - Lead mg/kg 0.45 - - ND Lead mg/kg 3.22 35.2 - Magnesium mg/kg 0.45 Magnesium mg/kg 3.20 732 - - Nickel mg / kg 0.090 - - 1.98 Nickel m-/kq 0.645 5.871 - - Nitrogen, Amon i a mg/kg C. - - 2099 Nitrogen, Ammonia mg/kg 1.61 1797 - - Nitrogen, Kldahl mg/kg 0.23 - - 38914 Nitrogen, Kjeldahl mg/kg 1.61 78387 - - Nitrogen, Nitrate mg/kg 0.45 - - NO Nitrogen, Nitrate mg/kg 3.23 ND - Nitrogen, Nitrite mg/kg 0.02 - - NO (1) All analysis performed on Toxic Characteristic Leachat e. MOL Method Detection Limit ND Not detected at or above the MDL. I I act University Commercial Place offices Serviv mawnt"ofis, minnesdia Lot Angeles, CaRfornia An Equal Opportunity Employer Charlotte. NC 28213 TwVa, Florida Charlotte. North Carolina TEL. 704-5974454 Iowa City, lowEr Asheville, North Caref na FAX: 704-597-8455 San trancisca, Cafilatris New York, New York Kansas City, Mwouri pittstualih, ftmeyfirenis THE ASSURANCE OF QUALITY _. r. Danny Wyatt December CS, 1990 Page 2 PACE Project Number: 60I03500 PACE Sample Number: " 92 0544293 92 0544307 92 0544315 Date Collected: 10/29/90 10/29/90 10/29/90 Date Received. 1 /3C/9C 10/30/90 10/3 /9 Harmony Harmony Wilkesboro Chlorine Chlorine _ Sludge Parameter~ Units` NNL Bashi Basin NAF INORGANIC ANALYSIS 1 INDIVIDUAL PARAMETERS Nitrogen, Nitrite mg/kg 0W129 3.87 Phosphorus, Total mg/kg .CS 6258 - T Phosphorus, Total mg/kg 0.09 - 164 Plant Available Nitrogen, by calculationmg/kg 0.45 - - 10461 Plant Available Nitrogen, by calculation mg/kg 3.22 222 _ - Potassium mg/kg 0.045 - - 19 Potassium mg/kg 0.322 1848 - Sodium mg/kg 0.045 - - 190 Sodium mg/kg ,3 3290 Solids, Percent Total 0.01 3. - 22.1 Sulfate mg/kg 32:3 1613 Sulfate mg/kg 4. - 679 Zinc mg/kg 0.045 - - 12.9 Zinc mg/kg 1.610 109. PN 0.1 6.83 PN 0m10 - - 4.75 TCLP METALS Arsenic mg/L 0.050 NO Barium mg/L 0.050 .966 Cadmium mg/L 0.1 - NO - Chromium mg/L 0.025 - 0.025 Lead m/L 0.10 - NC_ Mercury mg/L 0.0005 - NO Selenium mg/L 0.10 - NO Silver mg/L 0.1 - N 1) All analysis Performed on Toxic Characteristic Leachate NL Method Detention Limit ND Not detected at or above the MDL Data subject to final' review, 1700 University commertnal Piece Offices Sartir g: Mkmeapoft, Minnesota Las Amphis, CaliforniaAn Equal OppipTurtity Employer Charlotte, NC 28213 nmqias FloWs Charlotte„ North catorms TEL 704.597.8 54 lovint City a; Asher , North Caralats FAk 704,597 8455 San Francisco, Cafiforras Now York.how York K as City, misswo Nusbutgh, Pmrsylvarsa Ce. REPORT OF LABORATORY ANALYSIS THE ASSURANCE Of SUALITY Mr. Danny Wyatt December 05 A 1990 Page 3 'PACE Project Number: 601030500' PACE Sample Number: 92 0544293 92 0544307 92 0544315 Date Collected: 10/29/90 10/29190 10/29/90 Date Received: 10/30/90 10/30/90 10/30/90 Harmony Harmony Wilkesboro Chlorine Chlorine Sludge Parameter Units MDL Basin Basin DAP ORGANIC ANALYSIS TCLP CHLOROPHENOXYS 2,4-D ug/L I -1.1 Silvet ug/L 1 - NO - TCLP PESTICIDES g-BNC (Lindane) ug/L 0.002 Endrin ug/L Methoxychlor ug/L S. - ND - Toxaphene ug/L 1.0 - NO - Chlordane ug/L 0.10 - ND - Heptachlor ug/L 0.001 - ND - (1) All analysis performed on Toxic Characteristic Lea hate MOL Method Detection Limit NO Not detected at or above the L. 1700 University Commercial Place officas Serving: Minneapolis, Minnesota Los Angeles, California Art Equal OpporturkY ERVICYOr Charlotte, NC 28213 TwMa, Florida Chadatta, North Carolina TEL: 704,591-8454 laws 0% lows Ashevillit, North Cam fina FAX; 704-597-8455 San Francisco, California New York, New York Kaness City, hilli Pittsburgh, pewsylvonis REPORT OF LABORATORY ANALYSIS pcice. THE tSSURANCr Of OUAlt7r Mr. Danny Wyatt December 05 1990 Page 4 PACE Project; Number: 601030500 PACE Sample Number: r 92 0544323 Data Collected: 10/ /gg" Date Received: 103C/' C Wilkesboro Sludge Parameter Units M L DAP 1 INORGANIC ANALYSIS TCLP METALS Arsenic g/L 0.10 N Barium g/L 0.050 2.00 Cadmium tg/L 0.010 NO Chromium atg/L 0.035 N Lead mg/L 0.10 Nil Mercurytag/L 0.0005 NO Selenium g/L 0.10 NO Silver g/L 0.010 Ng ORGANIC ANALYSIS TCLP CHLOROPHENOXYS 4- ug/L I NO Silver ug/L 1 1. TCLP PESTICIDES g-5 C Lindan ug/L 0.002 g Lndrin ' ug/L 0.00N Mthnychlnr ug/L- 5.0 Ng, Tuaphnn ug/L 1.0 ND Chlordane ug/L 0.10 ND Heptachlor ug/L 0.001 Ng 1 All analysis performed on Toxic Characteristic Leachate. MOL Method Detection Limit Ng Not detected at or above the M L® Data subject to final review. 1700 University Commmial Puce afftes arviug; Nfiwwzpoka mimosets Los Angeles, Cater is An Equal Opwturuly Employer Madam, NC 252 13 Tampa, Rorktio Chmrtati , North Carotin TEL 704•5 7.5454 towis City, Iowa Asheville, North C r ` 4 FAX, 704,597,8455 Carr Francisco, Catit rrwak New York Now YAik Kantsit City, Missouri Pittsburgtr. Pennsylvania pace. REPORT OF LABOMTORY ANALYSIS cr THE ASSURANtf OF OUALI TY Mr. Danny Wyatt December 05, 1990 Page 5 PACE Project Number: 601030500 The data contained in this report were obtained using EPA or other approved methodologies. All analyses were performed by me or under my supervision. Charles M. Cabaniss Manager, Inorganic Chemistry John T. Stimus Manager, Organic Chemistry 1700 University Commercial flace Offices Se"irw. Mk"Spok» Wm"Mto Lee Angeles, California Ao Equal Oppottatity Employer Charlotte, NC 282 13 Tao". Fkaids Charlotte. North Carolina TEL: 704-597-8454 tMa City, lowsr Asher a, North Cortifes FAX: 704-597-8455 Son Fr " aP California Kow York, Raw York Karm" City, Missouri frittowo, periftsylvaras FEE-14--'91 THU 1: ID:PACE LPROPATCPIES T L N s, —5977— REPORT OF LASOMTORY ANALYSIS PTNI A11u��f Mc1 s Foy February 14�, 1 P.O.sox PACE Project Number., 111 1600 River Road Wilkesboro, NC 28697 Attn:r DannyWyatt Sle 2 000615112 4i 51 Date Col Number: 1 1 9 1 1 1 Date ec i Breeden STICK Parameter Units MOL $f udge WATER SUBCONTRACT ANALYSIS INDIVIDUAL PARAMETERS Moisture t1 93.6 A INORGANIC AL INDIVIDUAL PARAMETERS Cadmium 'k ...1 Calcium mg/kg 1.50 347.5 Chloride / kg 1. Chromicm mg/ko 0.15. Copper mg/kq 0.154.1 Lead mgJkq 1 6 Nitrogen, Kja1 0 . Nitrogen, Nitrate k 1.6 67.2 Nitrogen, Nitrite g 0.06 0.18 Oil and Grease mg/kg120 Phosphorus Total mglkg 0.02 1630 - Plant Avaiiable Nitrogen, by calculation mg/kq 0.06 13243 Potassiummg/kg .0 $odium mg/kg 15.0 943.3 Solids, Percent Total % 0.1 Sulfate kg 15.0 1007 Zinc mg/kg mg/kg0.15 .4 P 0.1 5.41 I Method Detection Limn_ 1700 Uniarvity ComweW PWO 0ftrs fiVIM: a al Ut Anqqwln NIHON# AA f4al = yv FEE-°° 1 —1 i THU 1 2 D FACE LASORATCRIES T L : 704- S7— Z rDanny Wyatt February 14, 1991 Page 2 PACE ProJect r. 610118604 ANumber: Date Cod ct �=8reoden I I 1 Data * iit j' 1123 1 - STICK Parameter Units MOL Sludge _77— INORGANIC ANALYSIS 7LF METALS Arsenic g L O.2S NO N Barium L 5.0 NO NO CadmiumL 0.05 NO NO Chromium L 0.25 NO NO Lead mg/L 0.25 NO NO Mercury L 0.01 NO ND Selenium mq L 0.05 NO NO Silver L 0.25 ND NO ORGANIC,ANALYSISTCLP VOLATILES By GC/MS Carbon tetrachloride mg,/L 0.050 NO NO C I orob nz n L 10 NO No Chloroform L 0.60 NO NO 1,4 ithl r n n L 7.5 NO NO Mathyl ethyl ketone mg/L 20 NO NO 1,1,2,24 c 1oroethy ens L tr nrnnt yin mg L 0.070 Vinyl chloride L 0,020 NO Vinyl chlorideL 0,07 I, ichloro than L O.S All analysis performed on Toxic L t L Method ` Detection Limit NO Not detected at or above the MDL. Aft ,l CoWhoft L410 FEES--14— 91 TLC 1 :2? ID-PPCE LABGRA70RIES ..._ T ? NO:704-597-845S #038 POS N`CQ�EQ r, Danny Wyatt REPORT OF LABORATORY February ANALYSIS 14, 1991 Page 3 PACE Project Number: 610118SO4 CC S m l Numbers CC6a1 C 00 t Col ct `, 01 1 91 1 21 1 Date Received; 01/18/91 01/23/91 rtedeft STICK Parameter n u a A ORGANIC ANALYSIS TCLP ACID rtho-rep l g, 04 NO NO to Cr sol L 200 NO NO r&-Cr sol 'L 200 NO ND e tachlor l g/L 1i NO NO -inch c henol L 40 O NO ,4,_richlr h nod 2 initr ' l n L 0.13 NO ND 14- H#xachlorobenzenaL 0.13 Hexathloroathansg ND NO itroban Pyridine mq�L 5 50.5 NO NO achl crc ut i en L NO NO P i NO NO TCLP PESTICIDES - NC Lin / 4 n r NI} NO the chlcr L 1C oxa hey L C NO ND Chlordane 0.0030 atachl r L 0.0009 NO NO Natachl or spoxide mg/L 0.0008 NO NO 1All analysis Performed on Toxic Characteristic L acha. e. L Mothod Detection Limit NO Not t cte t or above the MOL. I70 V*wy CMMVCw fts 0*iMts, SC 21111 Offices + M Ott s Angtial.O c Ta"Va, flWuha6wt, Mwtk 0 . # An Wel 4WuMY 11T TEL ia+�g3l> at t l Oa x 1 1 0 5 814 C"iNvil Now YA N FEEB-14—'91 THU 18:27 IMPACE LASCRATORTES TEL NOs704-597—e4S5 #038 P06 ANALYSIS ttxaros Guar Mr, Danny Wyatt REPORT OF LABORATORY February 14, 1991 Page 4 PACE Project Number., 610118504 The data contained in this report were obtained using EPA or other approved methodologies. All analyses were performed by me or under my supervision. Charles N. Cabaniss Manager, Inorganic Chemistry Manager, organic Chemistry 1700 Ww4fty emnere-4114m offal streiq mkmoak, mimmou T" Florida W A"$. Cant amit C)rpriolts, MGM GM01% OW10% RC 2#213 TV4 104-074444, Iowa M. low# A OWAL Rofth CWO*4 FAX: 104-641,9455 $,a Jfv44r*� CaRfmit Ntw York N** YWk THE 4SS0RAkt1 OF OUAWY Holly Farms Foods February 05, 1991 P.C. Box 88 PACE. Project umber: 610130500 1600 River Plod Wilkesboro, NC 28697 Attn: Mr. Danny Wyatt PACE Sample Number: 92 0009762 92 000977092 0009789 Cate Collected; 1/29/91 01/ 9 91 01 9 91 Date Received: 91 3 91, 01/3 '91 1/36 91 Harmony Harmony Wilkesboro CL2 Basin DAF CAF Parameter Grits ML Sl d e Sludge 51 ude 1MCPCAIC ANALYSIS INDIVIDUAL PARAMETERS Oil and Crease m9L 1. 300 26400 1600 MCL Method Detection Limit The data contained in this report were obtained using EPA or other approved methodologies. All analyses were performed by ate or under my supervision. Charles M. Cabaniss Manager, inorganic Chemistry 1790 University Commercial place Charlotte„ NC '78213 TEL: 704.5974454 FAk 704,597,8455 8ffwes Serving: minnesparls, mi escta Tampa, flontla laws City, laws San Francisa, California Kansas City, Missouri nEPORT NUMBE13 A & L EASTERN AGRICULTURAL LABORATORIES INC. 4 u I IL _U4L 7621 WHITEPINE RD. RICHMOND VA. 23237 804-743-9401 SC PiL SAMPLES NC ie5VZ SUl13MITT1 M;m LY rA.'?V' ; ' 5f;11L ANALYSIS REPORT SAMPLE�. ho - Dotes. Nitrogen Sulfur IIfrrrf g- It Iran Irrflfrrrft� Mange. arlrrtmonir Nitrate err ��t li . NO. _ N , rrt turn � rt rrr � N rrt rrr AlCu f rrr Ufa Nitrogen Nitrogen h 10258 1182 10259 389 46 5 10260 205 33 90 1261 270 29 16 10262 164 26 76 L hrt- Cadmium r rrtau Nickel Lead Arsenic ni Organic Mercury Selenium l�itr n : N m r Ni re,Pb rrr rrt H g 10258 - 0.5 5 1025 .5 10 15 125 <.5 5 11 10261 0.5 5 65 122 a 5 4 5 30 Values an fhls report ' arf the total amount rag the sarnpl 0or reports and taattara are tor the exclusive and coot uirdlal use of our Ptftrnte, and may not be reproduced In whole or In part, not may any rateran a be made This report applies only to the sample(s) lasted, Sammas are to ttma Wale, time re-SWIS, or the uornpany to any aadvItitisin , maws release, or rather put lic anotruntam rtte without obtaining *ut prior written authorization, re idnital a maximum of thirty bays sass resort , U EASTERN AGRICULTURAL LABORATORIES INC. t REPORT NUMBERA & L EASTERN AGRICULTURAL LABORATORIES INC. r1toIe-04t SEND j TO, L L Y F ANi S a to I N' CUSTOMER ACCT 4 4 S 34 TN: 0AV11 VA L01t 1' 0 #Em-30 Is U box 1318 yy[g g qq� r,,,,,, ��yy 1�yy q 9 f SUBMITTED B 6 xi TE L t - 0 "1 Ill PAGE SOIL ANALYSIS REPORT PLE LA Nitrogen F�1tu - p t - Sulfur Calcium Sodium 1r Aluminum Mange- Copper zinc Ammonia Nitrate IDENt NO. phoru slum rt lur %N %S ppm p pp Al Rose Nitrogen Nitrogen ppCu pmn ra p � g pp pp pp 10263 222 41 74 10264 189 72 52 LAB Cadmium rrs- Nickel Lead Arsenic Mercury Selenium rttt rrtt rrt NO, pp pprrlCr Nitrogen prrt Ni pprrr Pbpptrt pp ppm so 10263 < 5 5 55 10264 5 5 35 VaWas on this report art the tonal amount of the sampt to reports anti 9attaars ara for the extlusiva and confiedruiat use of our clients,, and may not be reproduced in whole or in part, nor may any rotarance be mad : T t,% report a pli only to the sample(s) tasted, Samplas are to tho work, lha thta company in any advertising, news release, or other public ntt�t` menu walthout obtainingour prior written a thor`txation; retained m ximui tat thirty days after testing, L EAR T RN A GRICULTU A L LABORATORIESINC. PaulC.H. Chu, Ph, By T. � . Sludgerya Application/Disposal ReportApplication/DiForm Annual Loading Summary PPlication l Application Mudge dotal Gallons Meta s and Nutrient Loading, *Total. DrY Tons Nirrogen s r s i s/acre Application Gallons Per Acre Dry "Tans Per Acre . .fit, as G opper in Date W 0,,47 S011"- PR annuallyUal solids n .. Cad na i i i A 040.1 PUV p o " 000 �00' ) 0. 0 0'0 1- i SUOT� snao P � ,Psi lug P ��s� � `��c�� �5� Ts as ra xz uO TIVOTTddy P Pla P"I Tvnuuy of aaodald TvsodsT(r/UOT2v-3TTddVP'l Sludge Land Application/Disposal Report Form Annual Loading sumnary _ + pl..icati.. n Me r-h 1 Sl d a Application Sludge Total Gallons **Total Metals and Nutrient Loading. Dry Tons Nitrogen 'osphorus O&G " lb ac re Application Gallons Per acre Dry Iona per Acre F.A.N.a P Capper Zinc Date Cu Zn try IZ� 2. - two 6.0 k, .V Annual oafina analyzedor reported I solids S ♦ �Pctrr ° i Sludged /Disposal Report Form Annual al. Sty mmary Ow-nert)V Fuld cx �'�°�' � tic. 94. �. p Application i t l Application pplication Sludge Total. Ga lon Metals and Nutrient Loading, **Total Dry Tons NitrogenPhosphorus O lbs/acr Application Gallons Per Ac e Dry TonsPer Acre; '. .N. �' a Copper in a toCu Zn RN do r t 0. . is caa t & w adreporlted, , j { SludgeLand Application/Disposal Report Form Annual Loading Summary At)Atf�- Field No. No. Acres :3 Field Crop Application qtrtf-: lud a ppi itst on Sludge To t a I Gallons **Total Metals and Nutrient Loading. Dry Tons Nitrogen Phosphorus i s/acre pp icac o Gallons Per Acre Dry Tons per A,cre P.A.N. PO, as p upper Zin Date Ch n P yy i 4 aY�OR ypq d� y qM(� �r a ed, aunvally " (circle): s ris � s s i { f H I Page Sludge e pplicati n/Di osal Report Form Annual Loading - application Method (circle): surfa e subsa�r a 1 lueApplication Sludge Total Gallons Total Meta a and Nutrient Loading, Dry Tons Nitrogen Phosphorus O&G i s/acre �. Supple itions Application Gallons Per Acre Dr Tons Per Acre P.A.N. Po- as Copper Zinc Lea is e apt. ' 1' ime €gate u n Pbl Cd "5x � a I� i " �. k solids Sludge Land pplica /Disposal Report Form Annual Loading Summary er ld �3 re `i,eid ru Pp.ii.catiuu 1 Siud e Application Sludge Total. Gallons **Total Me a a and Nutrient Loading, Dry Trams Nitrogen Phosphorus O& lb/acre Application Gallons Per acre Dry Tans Per -Acre P.A.N. POD Copper Zin, Date Cu Zn �u e14Z 0 qj t Lg M . ,U'analyzed and reported annually Or wi, tm &-GaI16US x X solids Pal cirie urace1 a surface SuPP i do ad Nickel ' PCB Li b :Ni I Sludgeo- APPlicatiOU/Disposal Report Form Annual Loading Su=mary Application aid e Application Sludge Total. Gallons **TotalDry Metals and Nutrient Loading. Toms Nitrogen Phosphorus O&G /acre Application Gallows Per Acre Dry Tons Per Acre F_A. . CopperZinc Date Zn a IqS;0OOI Z4 1 - , " 7- 1- 9, " 500 a . 1(0) ]t 'a �Jjjnx .'45 " .. d reported wmually Sludgy Land Applicatiort/DisposalReport Annual Loading Su=ary PPlication Me P � lud pplcaf Sludge tad ally **Total a d 3 u ran cad ng. Vans Nitrogen Phosphorus O&G l1 cr Application Gallons Per Acre Dry Tons per Acre P.A.N.P a p Copper :zinc Date u Zn ! - a tJ.IVZ { tag ar SZ- repor.ted annually Pas ..cl r surface z trac ; supp itiol Nickel Cad Limy Nid .s. 00 TN gyp...PO •�y �#)TN �} �y "C g n, 2 IT em= P0320404 Puv p mm "d 1. 50 01 bov 0010 !" q g ggigg 14 I i sv laa SUOLx1 aawT snaoqdsoqd TN C '. . gy. M }TT id3V S TT 301 a2±CP" TS 4 Sfigfi a "mme j Page Sludge Land Application/Disposal Report Form Annual Loading rg Pl cati n Method (circle): surface surface a Application 10 Sludge Vital llo **Tota , Meta red Nutrient Loading, lb/acre Dry ions;; itr en Phosphorus ",ti Supple Application ll n Per , c Dr Togas Per Acre P.A.N. , a Copper Lead Nickel Cad.' s ' th nc d 1121500 qo r, 0P N :�' `' I oo . 70 J 5. " .1 `�d reported. annually Sludge Land Application,/Disposal Report Form Annual Loading Summary pplicatlon Methc iud a Application Sludge 'Total. Gallons *Totals Meta a and Nutrient Loading, Dry Tons Nitrogen Phosphorus lb/acre Application Gallons Per Acre Dry "Togas Pet tr� P..N. P as Co p r to Date as 3 11500 x 4. KK 0.m OIJ oa .m t brad- ep rl PO TN MTV a aat p ddn as s asejans Sad U' w u w. Ot 30 a 4 T ladd d " *' "d lad L a xts�dsd UOL AI away ad s z s a a a a do olaa s T ' pa ua � paw a 'V" a a pnT a 3vOT ^ d p u+a-dd d ad a :)V ONP pad guTPROI Tvnnuv uuoa laodox T sad a dd^ a2pnIS Sludge nd Application/Disposal Report Form Waal Loading sum=ry Field No. No. acres qO Held Crop lif � Application Metho, Sludge APPlication Sludge Total Gallons T t l Metals and Nutrient Loading, Tons Nitrogen -'-Phosphorus lbs/ cre ApplicationGallons Per acre Dry Tans per Acre P.A.N. p P Copper Zinc I Date Cu Zn 14 1+ o a . 00 w ot 1 g ash reported, P, Sludgy Land Applicatioa/Disposal Report Form to l Loading Su=ary pli'tin Me ` O glud a Application Sludge Total Gallons **Total Metals and Nutrient Loading, Dry Tons Nitrogen Phosphorus O&G lbs/acre AppliCation Gallons Per acre Dry 'inns Per Acre P.A.N.P Copper Zinc D.Cu Zn C Ito a` � q 5 ` r t It, ark g i Oz , a ' and reported annually _x,•:be'sualyzed Mid *n ircle): surf Sup iti` Nic l Cad.-P Lim i Cd Sludge dApplication/Disposal Report Form Annual Loading Su=ary Pplication Method (circle): surfar r d i ti x7Slueta Total Sludgetiol i *Total and tri nt Load3� , Dry Tons NitrogenPhosphorus h r �n : i. aiicaa 'r tr r Toys Per Acre P.A.R. ' a p Copper'- Zinc Lead Nickel dad.' a DApplate uZn ph ti a Cd 251400 _ Z Mo M Zotal Annual ILA 41m;k t fi d reported annually ,`Z solids a � n u State of North Carolina 441f Department of Natural Resourcesand CommunityDevelopment Division of E nvirrinniental Mmi-,v rn nt 512 North Salisbury Street # Raleigh, North an- ina 27611 rne� G. Martin, Governor . Paul fir'"roc r illiarrr � obey, Jr., Secretary January 26, 1989 Director Mr. David Taylor NC Division Engineer Holly Farms Foods, Inc k P.O. Box 88 Wilkesboro, NC 28697 SUBJECT: Permit No. NG0021717 IE Authorization to Construct Holly farms cods'. Inc. Dear bra-. Taylor: Your request was received by the Divi i. n cif Environmental Management on January 25, 1989., Your request to delay the decision on the EPT System until February 27, 1989 is being reviewed the Division's staff. You will b notified of theDivision's position upon completion of this review: If you have any questions on this matter, please call'the undersigned at 919/733-5083, Sinc erely, y, Arthur Mou erry, P.E. Supervisor, � sr Pe rmits nei Engineering M/t l e.Winston-Sines Regional Office Mooresville Regional f fu Permit file Are Errual C noorturrrrvr Affirmanve hrtr— P-1 HOLLY FARMS FOODS, INC. 203 9 ° � Ra,7 ki .� 1,-., :2 P C� Nyx . 1 iat...b o Nopl°� F m, f \ ,t January , 1989 } r p t71,.. .. r Arthur Mouberry North Carolina inao Depar.rtment of Natural Resources and t;csmmurri.t..y Development Permits and Engineering Unit 512 North Salisbury Street: Raleigh, NC 27611 SUBJECT: Permit No. caret, 0 1 7 i t' Authorization to Cos zstruct Not,.a:, _ ..._ Prey -treatment Facilities Holly Farms Foods, Inc. Wilkesboro Complex Wilkes County, North Carolina Dear Mr. ouberr; ...k wren, A,. This is to confirm our conversation concerning the wastewater Pre-treatment system at the Holly Farms Foods Plant in Wilkesboro, North Carolina. As You are aware, we are evaluating the EPI Wastewater Treatment System that was installed at, the Holly Farms Plant:. in Harrisonburg, Virginia. Because of factors beyond our control, we have not been able to c011ect sufficient data t determine the s stem's feasibility. The PPI System in Harrisonburg .has not operated continuously to produce sufficient results because of non -operating days at the Harrisonburg plant: and continuing difficulties with the sewer mains in they City of Harrisonburg. I regret that, I must request another extension of the decisiosn, date. As we discussed, two dates are of Prime importance to the Division of Environmental Management, the September's, 1 988 compliance date for the Holly ;Farm pre-treatment effluent and the December 30, 1989 deadline for storage at the land application site in Rowan County. Holly Farms requests that the decision date be scat- for February 27, 1989. Everyone involved with the project at Wilkesboro has committed that the compliance dates will be met if the project decisions is made on or before this date, t is; understood by the management of Holly Farms that the Division of Environmental Management ement can impose enforcement actions against Holly_ Farms, Everyone involved is working to insure that. the Division is not forced to take these actions Mr. Arthur Mouberry - - 1 greatly appreciate Your patience and understanding concerning the EPI Wastewater Technology. s I have indicated I believe that: the water treatment has great; promise, both in resulting water quality and in reuse of the waste material generated. If You have questions concerning this situation or require other information, Please contact t# me in Wilkesboro, Sincerely, acid T a l or, .0 , Division Engineer T/mf rSteve Mooney - NCDNRCD, Winston-Salem Red Gleason - NCDNRCD, Mooresville Gary ottomley -Senior Vice president SkiPper Solomon - Vice President. Frank Tara ide Charles Case< Ray Burris x, u SECTION SITE SOIL REVIEW The personnel of Holly Farms Foods, Inc., have selected nine proposed sludge application sites to add to the original Sledge Disposal Permit On July 20 and 21, 1988, ,these sites were examined by d soil scientist to evaluate in detail the soil profile descriptions, their physical properties, and their landscape positions as these factors relate to a successful laud application program. The preliminary review of the soils in Ronan and Wilkes Counties (Figures 1 and , reflect moderate to deep soil profiles with a rapid infiltration and moderate subsoil hydraulic conductivities. Based on the aerial photographs the sites also appear to be nearly level to moderately sloping. e first ,five sites are located in the northwestern portion of Rowan County (Figure 3). These farms can be easily accessed from Interstate 40 and U.S. 64 South to Statesville, Borth Carolina, From U.S. 64, all of the secondary roads to the sites are paved, Field '(Figure contains approximately 29 acres,_ and is located at the northwest portion of the intersection of SR 1980 and SR 1981. The remaining tour sites, (fields A, , C, and D,; `igur'e 3) dotal approximately 128 acres and are located 1 miles east of the SR 1978 intersection with SR 1977. These five sites are ideally situated in close proximity to one another and are only separated by 5 miles. The agricultural settings in Rowan County are characterized by nearly level to gently sloping lands. Some slopes may exceed 10 percent around drainage or stream channels. 4 One hundred and two acres divided into four smaller fields are located in the southeastern portion of Wilkes County. These sites are located only 10 miles southeast of Wilkesboro, forth Carolina, and more specifically; on the east side of NC 11.5, approximately 5 miles south o the intersection between NC 115, and U.S. Route 421. Again, these four fields are easily reached by major and secondary roads. Field "a"° is roughly 35 acres, Field " 19 acres, Field " ";approximately 25 acres, and Field " "" 23 acres. Fields "A, B, and " are proposed sites for sludge application, while Field "C" has been proposed, as a construction site for a sludge holding lagoon (Figure . Wilkes County and the respective four land sites ire located in a x ,mountainous region, .n the state of North Carolina Steep slopes and narrow valleys are quite common in this area. Slopes of.15 percent or more are typical in many pastures and grass cover fields in Wilkes County thus, thinner .soils and site limitations may require specific management techniques to successfully utilize an area for the land application program. .1 ROWAN COUNTY SITES e proposed Field "" site (Figure 5) is located in an agricultural area with surrounding scattered residences and churches. At the time of the soil field review, here were no homes or churches observed within 400 feet of the property boundary* around the site. Also absent from the area were ponds and s,treams. Foods lined the western and northern sides of the _property, as SS 1980 and SR 1951 served as boundaries on the east and south sides, respectively. Slopes generally were level to gentle: 5 e soils were examined by probing a hand, auger through the sail profile., Soil samples were delineated and described at each hori:onat'ion to record the textural class, Munsell colors, structures, depths, boundaries and any other observations that may be;of value when preparing a management plan* Since a modern soil survey of Rowan County has not yet been published, the soil series for these samples cannot he depicted.. ree soil cores were angered in a diagonal transect across the field, and three similar, yet, varied soils were described. The first soil sampled in Field "S"was located in the southwest corner of the field, approximately 150 feet from the road and Brooded , boundary line. This soil is well drained to excessively drained through a hori onati:on of Ap- - -Btl- t2-g - (Table 2). e textural classes through the profile range from fine sandy loam to a sandy clay loam, The chroma colors, of this soil, are indicative of its excessively drained y nature, all of which are greater than 2. The second soil sampled across Field "S was as close to the center of the field as possible , and. approximately 225 feat from. Roane Road. 1980. This soil too, as all of : the adjacent ent soils, are well drained to excessively ivel.y drained.. The hori onati.on expresses an Ap- -g - tl-iit2- (Table 3). The textures again grade from a fine sander loam surface soil down to a clay subsoil. Soil water readily infiltrates into the Ap horizon and moves downward through the soil profile to the least limiting layer, The least limiting layer usually reflects an increase in clay content, or a change in structure. Therefore, water movement will be , somewhat reduced when it contacts the clayey Bt horizon:. The final soil sample from the transect across Field " " is quite mailer to the previous soil descriptions, with a minor difference being fewer horizons (Table . With a Field average ph of 6.8 (attached data sheets), all of these soils appear well suited for sludge application and the level to gently sloping landscape will definitely enhance Infiltration. The well mixed and aerated Ap-horizon will also provide an excellent medium for sludge decomposition, whether the plan calls for surface applications or injections, e same procedures used is sampling and describing the soils in Field 'IS", were implemented in the fields at the intersection of SR 1977 and SR 1978. Located only 5 miles southwest of Field "", Fields '"A, B, C, and D" were all similar to those soils previously described (Tables 5, 6, 7, And m As -;a result of the similarities among the soils, a preliminary survey of each f ield was made prior to any soil sampling and descriptions. After the initial survey, one locale was declared as e representative position for the soil: description work In Field "A", forests surround the entire acreage and present, an excellent outline of the property boundary. Erosion control terraces also sculpted the landscape and appeared to rain parallel with the hil.lsldpe contours. These terraces not only decrease the veracity of surface water runoff, bent•_ also channel this energy and re -distribute the water over a greater field .area. present in the field area were 3 partial drainage ways that, with the increase in slope around these drainages, help to remove excesssurface water after heavy rainfall events. The soil itself s deeply drained and exhibits a well developed soil. profile. A significant increase in clay is identified in the subsoil horizon at L_ r approximately 22 inches in depth. These fields in Rowan County, (A" B, C, and are currently being utilized for pasture grass and hays operations. With the exception of two rented homes adjacent to Field " "d, no father homes or wells were observed within 400 or 100 feet,_respectively. The slopes in Fields "A"" "B", and "C" were generally -6 percent in grade, while those observed on site """ were 'slightly higher in grades of 6-10 percent. Field "g" was characterized by having a fine sandy loam surface, a clayey subsoil_, and a sandy loam -horizon around 50 inches in depth. This profile was deeper (56 inches plus) and observations indicate ;the water table to be at a depth of more than 5 fetes Fields "C" and "D" are separated: by SR 1978 and due to their similarities will be discussed together. Of the two, " tales on the upland topographical landscape definition with near level to gentle slopes. Field " , just on the opposite side of the road, has increased 4 side slopes and an intermittent drainage way thrown the middle of the acreage: The soils are quite similar, exhibiting sandy loam surfaces, sandy clay subsoils, and returning to massive sandy to -horizons. The depths of the horizons vary only,within "inches, as the introduction of the clayey subsoil,, horizons for fields "" and. "";are 13 and 7 inches with depth, respectively. Being located in the lower landscape positions may create some important limitations to the suitability of Field "D . These limitations are the increased side slopes and the moderate soil profile permeability,. 3.2 WILKES COUNTY SITE The Wilkes County sites are divided into ;four fields and labeled "A", "err "" " and "r" 3 Fields "A", "" , and "" are proposed sites for land sludge application and Field " " has been proposed ;for the construction o d sludge holding lagoon. Currently, Fields "A"" " ", and "D" are i pasture grass and red clover" and presently grazed., Fiel. "C"has not been cultivated for sometime, as grasses, weeds, and small shrubs cover` the area, It appears that the most important limitations for these sites are slopes in excess of 15 percent, the landscape erosion down these slopes, and the soil depths to lbedroc: From a soils standpoint, Fields "A" an "C" exhibit similar characteristics, as do the soils in Fields " and "" The soils i Fields "A any " depict an A-Btl-BO-BO-BC-C soil horizon designation with a clear difference in the depth of the soils in Field "A". Twenty to thirty inch depth differences were consistently observed between Field " and Field. "" . The initial reason and cause for these differences appeared to be the increased slope gradient, and thus" surface erosion of the soils in Field " ". Sandy loams and sandy clay loam textures were common and the colors only varied from red: and yellow -brown surfaces to reds and yellow -red subsoils' e buffer zone requirement around Field "A" appears to be verb straight- forward requiring a 100 foot buffer around the property line and 0 foot buffer zone around a farm house at the: base of a 10-15 percent ,lope on the southern portion of the property. Field ""'" is more complicated for a number of masons, First of all., the slopes are on the magnitude ude of 10-15 percent" with some areas recording 15-25 percent. These slopes have obviously influenced the presence of drainage channels and streams it the northeastern an southwestern portions of the property. Moderate to severe surface erosion can also he observed near these channels. The growth of ;gasses and shrubs have also created a non -distinct property boundary with the adjacent forested trees. e snails in Fields """ and " " are very simi.l.ar. Surface soils are typically sandy loams and range to 7 inches in depth. Subsoil horizons are more sandy clay loams and are approximately 28 inches thick to the top of the -horizon. Both of these soils appear to he limited by the depth to bedrock and the presence of coarse rock fragments in the surface horizons. For the most part, the slopes in field "B" range from -15 percent with some isolated areas on the outermost edges of the property increasing to 1 - 5 percent, These are the areas of drainage channels and moderate erosion. Most of the slopes in Field " " are 1. - 5 percent in grade, These slopes limit the site suitability because they tend to be; the cause for moderate to suer erosion on the side slopes and: weathering of the soil down to the underlying bedrock outcrops, A stream also runs in a north and south direction through and with the length of the property. At the northern portion of the field the stream is approximately 100 feet from the eastproperty line and narrows to less than 40 feet as it exits the southern property line, 10" SECTION RECOMMENDATIONS FOR LAND TREATMENT To determine the suitability of a specific site for a land application.. program, a number of factors should be considered. These factors of consideration include; the current and planned land use, the soil characteristics, the topography and landscape positions, and the sludge characteristics. The DEK devised a rating system to evaluate potential land sites for the treatment and application of sludges. Their ratings systems for site evaluations are based on specific soil factors such as; soil depth to bedrock or the saturated zone, slope, cation exchange -capacity El, and soil pH. e design application rate is based on the nutrient requirements of the crop, soil characteristics, and the metals loading. The plant ,available nitrogen is typically used as the limiting .ng nutrient for application, since PAN is a major nutrient for crop production. Compared to phosphorus and potassium, two other common fertilizer constituents, most crops grown in North Carolina require greater amounts of available nitrogen. The North Carolina Department of Agriculture Soil. Testing Laboratory has developed nitrogen recommendations for typical crops grown in the State (Table 1 Another factor which influences the sludge application rate to agricultural land is the ability of a soil to incorporate and assimilate the sludge metal concentrations*_ The soil cation exchange capacity, CEC ,, has been selected by the DEK as a soil parameter to predict the soil tolerable levels for metal loading;. Sails with lour E+'s _S meq 100 can only receive lair metal loading while souls with higher "s can receive steadily increasing amounts (Table l For these proposed sites in Rowan and Giles counties, the Ni and Cd. concentrations in the sludge must be laboratory analyzed before an accurate recommendation can be determined. However, the mail f `s for the proposed sites, range from 3,9 meq/100g In field "" in Wilkes County to 12.0 meq/100g for Field "" " in Rowan County; e availability of metals and CEC are further influenced by the soil etals are generally more soluble in acidic soils, thus, by raisin the pH to more neutral conditions, the solubility of the metals decrease. In North Carolina the DEM requires the soil pH to he adjusted to at least 6.5 for agricultural fields. Based on the attached soil test results, liming will be a. required amendment on an annual basis to maintain a proper soil pH., Upon the compilation of the information obtained form the site review, the criteria established by the regulatory review agencies, and previous experience, all of the sites in Rowan County appear to be suitable for land application. Likewise all of the sites in Wilkes County are suitable, with the exception of Field """ which is unsuitable, The soil depth to bedrock, , the presence of coarse rock fragments in the surface horizons," the steep slopes, and the - low "s all influenced this recommendation to withdraw Field "D" from the: proposal. Field "" in Wilkes County may experience some of the same problems as field "D", but to a smaller degree. In addition, Field. " ": s only to be used as a site for a holding lagoon: Westinghouse EnvironmentalServices Holly Farms Poultry Industries, Inc. 1600 River Road Wilkesboro, North Carolina 28697 Attention: David "Taylor Engineering/Technical Services, Reference: Additional Land Application Acreage 0 3500-8 egencfiF °r .r, ac 0 Box 1308 FAX li; 4} 481 r80 Holly Farms, Foods, Inc: Jar Mr. Taylor Westinghouse Environmental Engineering (formerly has completed the attached Land Application site report. Included in the report are discussions and data related to the proposed land treatment And utilization program. Based on similar land treatment projects, cts, the enclosed report should provide the necessary information for the proposed land treatment site evaluation performed by the North Carolina Division of Environmental Management (HEM). Westinghouse suggests three copies of this report and a land application permit fee 0.00 be submitted to the DEM-Regional office. A. cover latter should also note that Holly Farms Foods, Inc. is requesting land to add to their original land treatment permit. If you have any questions, please contact me at your convenience. Sincerely, Westinghouse Environmental Services David Burk Staff Soil Scientist 640*10VAROM Environmental E.nginpennq *d fis a 6v,, ian of SWE i;1c t,t Nonu: 'va o,,i 3offering :rt?i't`R es as S&V—E .;s:par. smhi: ,. M � TABLE OF CONTENTS JL SLUDGE CHARACTERISTICS AND LANDT' SITE SOIL REVIEW 3.1 OWSITES 5 3.2 WILKES COUNTY SITES RECOM14ENDATIONS FOR LAND TREATMENT 11 APPENDICES LIST OF TABLES Table No,- Title 1 Sludge Chemical and Physical Analysis for Selected Parameters. 2-4 Soil Profile Characteristics, Field "S", Rowan County, 5 Soil Profile Characteristics, Field "A", Rowan County, 6 Soil Profile Characteristics, Field "B", Rowan County, 7 Soil Profile Characteristics, Field "C", Rowan County. 8 Soil Profile Characteristics, Field "D", Rowan County. 9 Soil Profile Characteristics, Field "A", Wilkes County. 10 Soil Profile Characteristics, Field "B", Wilkes County. 11 Soil Profile Characteristics, Field "C", Wilkes County, 12 Soil Profile Characteristics, Field "D", Wilkes County. 13 PAN Requirements for Typical Crops Grown in Wilkes County, North Carolina and Respective Sludge Application Rates. 14 Current DEM Regulations and Guidelines for Various Metal Applications with Respect to Soil CEC. LIST OF FIGURES pl&urn Fig. litle Location Flap " Location Map - Wilkes County Topography Sites n Rowan County 4 Soil. Map of Sites in Wilkes County Field "S" - Rowan County SECTION 1 INTRODUCTION Westinghouse Environmental Services, at the request of Mr. David Taylor of Molly Farms Foods Inc., has surveyed proposed land sites for the purpose of applying du ri.al sludge on an annual basis for several locations in Rowan and Wilkes Counties, North Carolina. Three new land sites; totalling 157 acres in Rowan County, and 102 acres in Wilkes County, have been submitted as additions to the original Holly Farms Sludge Disposal permit. Our survey was initiated for the purpose of site assessment; soil evaluations, and overall general descriptions of the proposed areas Soil has a significant capacity to decompose and incorporate organic materials, thus, the utilization of sludge, as a soil amendment and a fertilizer, in an agricultural production program. The effectiveness of the sludge as a fertilizeris dependant upon the soil physical and chemical properties, as well as the sludge nutrient contents and characteristics, and the crop requirements. n determining the field loading rate of a "good quality" sludge, the nitrogen requirement of the crop and the plant available nitrogen (PAN),, content of the sludge is used. Since crops require different amounts of PAN to reach maturity, sludge application rates vary for specific crops;.. However, in North Carolina., most agronomic crops require 50 to 350 pounds per acre of P 11 SECTION SLUDGE CHARACTERISTICSD TREATMENT Holly Farms foods, Inc., for the operating year of 1987, applied nearly 1600 dry tons of sludge through a land application process. This sludge was generated from a dissolved air floatation system and subsequent aeration lagoons; Table l depicts the analyzed constituents of a sludge sample for the Holly Farms Rendering Plant in Harmony, North Carolina$ The data reflects reasonable information and appears suitable for agricultural use in a crop production progr e greatest concern in the maintenance of local environmental quality and the agricultural community is the presence of metals in the land -applied sludge. The sludge was analyzed for selected heavy metals ',including: Cu, Fe, Pb, Se, and Zn. Heavy metal concentration in most *. food -processing waste waters are very low and are not likely to have an adverse effect on a land application site. e purpose of the land treatment program specified by holly Farms Foods, Inc., will be the successful utilization of sludge as a fertilizer' source and a soil amendment. The North Carolina Department of natural Resources and Community Development Division of Environmental Management ( has; set. standards where annual sludge applications are not to exceed the determined annual soil loading rates for metals and a PAN application rate not to exceed. 200 lbs./acre/"year. In accordance with the above standards, all of the other "Safe Standard Levels'established and adopted by the EPA and USDA :are to be maintained. Buffer zones, in which no sludge will be injected, near property lines, residences and wells,; streams, and ponds, etc. are to be strictly observed. TABLE 1 Rally Farms Foods, Inc. Sludge Chemical an Physical Analysis for eleed Parameters Westinghouse Job No. 4116-88-608 rgirmLete-ri Conditlt pH 4.8 Total Solids 21.* mg/Kg, NH3 N 22 mg/Kg mg/Kg Total Phosphorus Potassium mg/Kg u 4.9 mg/Kg" zu 28 mg/Kg d ND Pb 31 mg/Kg i ND TABLE 2" Soil Profile Characteristics Field " " Westinghouse .lob No. 411 - -0 Mun a l Textural b ..a bolo ` lass o (in.) Ap -4 ICE YR 4/3fine sandy loam weak granular 4 ®9 7.5 YR 5/4 sandy loam weak granular BE -18 2.5 sandy loam weak aubangular blocky tl 1 -21 2.5 YR 5 8 sandy clay moderate subangular blocky t2 21-29 2a 4 clay moderate subangular blocky BC 29-44 2.5 YR 4/8 clay loam veakauban ular blocky " 4+ 5 5/8 sandy loam weak subangular blocky 3 Soil Profile Characteristics - Field " Westinghouse Job No. 4116`-88- 0 unsell "Textural a*c t o1or Structure- in.) AP 0-8 10 YR 4/4 fine sandy loan weak granular -17 1 /3 sandy loam weak. granular BE 17-24 10 YR 4 3 sandy clay loan weak subangular blocky Btl 24-32 7. 8 fine sandy clay moderate subangular blocky Et2 32-47 7.5 YR 5/g sandy clay weak subangular blocky 47+ 1 8 sand loam massive TABLE 4 Soil Profile Characteristics_ Field "S" Westinghouse Job No. 11 -88-60 unsall Textural a iDszui Class iu (in.) ApR 0- 4/6 fine sandy loam weak granular' b 1 7-19 2.5 4/6 sandy clay moderate subangular blocky B 2 19-32 2> 8 sandy clay moderate subangular blocky b -56 2. 4/6 sandy clay loam creak subangular blocky 56+ 5 YR 5/6 sandy loam massive TABLE Soil profile Characteristics_ Field "A" Rowan County Westinghouse Job No. 4116-88-608 unscll Textural Horizon Dgep_th C212rClass Structure in. A -5 l fine sandy loam moderate granular A -15 1 5 sandy clay loam weak subangular blocky b l 15-22 1 sandy clay moderato subangular blocky bt2 22-30 lei YR 4, clay moderate subangular blocky BO - 9 10 YR 5/8 clay moderate subangular, blocky BC - 4 7.5 5 "8 sandy clay loam weak subangular blocky + 7.5 YR 6/8 sandy loam massive TABLE Soil Profile Characteristics Field "B" Rowan County Westinghouse Job No. 4116-88-608 Munsell Textural Hor 2 h Color laaa Structure (in.) Ap 0-3 10 YR 4/2 fine sandy loam wreak granular -7 � 4 "4 sandy loam wreak ;granular BE -11 5 YR 4/8 sandy clay loam wreak aubanBular blocky Btl 11-30 2.5 YR 4/8 clay moderate subangular blocky Bt7 -40 clay weak suban8ular blocky BC 4 -45 2.5 YR 5/8 clay loam wreak subangularblocky 45-5 .5 YR 5 8 sandy loam massive TABLE Sail Profile Maracteristics Field "C" Rowan'County Westinghouse Job No. 116-88-6 8 Munsell Textural Horizon o w` � Class Structure n.) ,p -6 10 YR 4/3 fine sandy loam moderate granular g -13 10 YR 6/3 very fine sandy clay loam weak granular btl 13-22 10 sandy clay moderate ub n ula 'blocky 22-29 7. '6 clay weak subangular blocky gC 29-40 7.5 sandy loam weak su angular blocky + 5 YR 6/8 sandy y loam massive TABLE ` Soil Profile Characteristics Field ®' " Rowan 'County Westinghouse Job No.4116-88-608 tun ell Textural b ...c` Ptah Colorlass Structure (in.) Ap -7 lea YR 5/3 sandy loam moderate granular 1 -11 " 1 /6 sandy clay loam weak subangular blocky 11-27 7.sandy clay moderate subangular blocky BC -34 7.5 YR 5/4 sandy clay loan weak subangular blocky 3 a- 6+ coarse sandy loam massive TABLE 9 Soil Profile Characteristics Field "A" `lea County Westinghouse tinghous Job No. ' 4116-88-6 8 Munaell Textural Horizon Color Class 8t cure (in.) •1C 2. 4/6 fine sandy loam moderate granular Btl 1 -14 2.5 YR 4,/8 sandy clay loam moderate subangular blocky Bt2 1 -21 2.5 YR 4/6 sandy clay moderate subangular blocky BO 2 -4 /'8 clay moderate sub,angular blocky BC 4 - 7 5/4 mottles o 7. /8 sandy clay loam weak auhangular blocky C 70+ 5 YR 5/8 sandy clay loam massive. ABLE 10 Sul Profile Characteristics Feld "B" Wilkes County Westinghouse Job No. 4116-88-608 unsell 'textural ff_orizon n c class S u ure (fin- 0-8 1 /4 sandy loam weave granular BA 8-13 1 ,✓4 sandy loam creak granular B l 1 -17 sandy clay loam weak subangular blocky Bt2 17-24 2, sandy clay loam moderate suhan` lar blocky BC 24-39 7. 4 sanely loam ea supangular blocky 2. mottles of 7. 5 '4 sandy loam massive TABLE11 Soil Profile Characteristics Field "" Wilkes County Westinghouse Job No. 4116-88-608 unsel Textural Horizon RMUI Color Structure (in.) 7¢ '6 sandy loam moderate granular ul 7-18 5 YR 4/3 sandy'elay loam weak subangular blocky' Bt2 18- , 6 sandy clay moderate subangular blocky Bt3 -3 6 clay moderate subangular blocky BC 30-48 2a54 6 sandy'; clay loam weak subangular blocky . sandy loam massive 4 TABLE1 Boil Profile Characteristics' Field I'D" Wilkes County Westinghouse Job No. 116-88-6 8 unsell Textural Horizon t _ColorMass Structure- i.n. A -6 1 sandy loam moderate granular BA 6-10 l '6 sandy clay loam weak subangular blocky Bt 10!-24 7. B sandy clay moderate subangular blocky BC 24-346 sandy clay loam weak subangular blocky C 34-42 5 YR 6/8 coarsesandy to 'massive TABLE1 PAN Requirements for Typical Crops Grown`in Wilkes County, North Carolina and Respective Sludge Application Rates' N. Reggirld W&I Amliaaslm* (lbs. "ac a) (dry tons) Corn 160 5. Small Grain 100 2.5 Alfalfa 200 4. Bluegrass 120 3. u`nras 220 5.4 Fescue (Tim) 200 4.9 *Based on PAN of 40.6 lbs 'dry ton TABLE 1 Current DER Regulations, and Guidelines for Various Metal Applications with Respect to Soil CEC Pb 500 lbs. 1,000 lbs. 2,000 lb . n 250 500 1,000 u 125 250 500 Ti 125 250 500 Cd 5 8.9 18 Annual Cd application cannot exceed .5 pounds per acre per year. Yam. NOW fiFW Yi A 9FF lamb aeap 8b&9� ktWa 4 a MYW Y�id92 ePMi�t#AwalgfkY YtiM�fYt 1* to l ti w OWN% sft jp out yq py UK am i lwwr Y * f Y .G PPS°y nit tlu au as ern Y m P ,aa '...t lut �w y J{ma i ima. e !jai � 4 xG ML S Waw'` y + fm 7 B ok t� ergo w^a s & Y Land Treatment tp Wilkes Co. mom 1 m VA 42r's u + Syr' p , - ° w «*t t r 41 1*4 M* AL „w we �R A Not scale Holly Farms Lard 'dr at � . �+ � � �- �i Soil Map of Sitar in Wilk I County. WON M -4 a r s r p n P 1 , ff 00 » ° ati t x, . x u a r re u • 'k .+`' # s ;tAe , "�4,c<psa r x ^ °+�...:a + s'�i° � 'm ` � t r a� s T .�,. ^r'�'`s.„� a4 � . ry a . r„'m"'• " ,�` � w a »� a i x e a P .. n j; • "' E t m x �° "w - „ ».a w'u s • t, „ "r ;: � . , ' a , t r 1� x. b y 9 • ri Px t�i' . �I` PU. " e :✓ ... *i P .a,n Y LW e'h mow, d PROJECT S7 ALE n Not to scale Holly Farms Land Treatment Field "S" -- Rowan County01 -- APPENDIX C SOIL BORATORY RESULTS v � »:»� d<� � < � � � � � � � � � i� d2� � �\ d .� � y §� <f \� � .,� � d� , � ©2 ± n� � \\� °®^~° �� ~� ^� � 22\< � \\: y m y� f: � >: . ...»g°« y�� t«» : »- d©� »� � � � � � ? © . a � � � :«< . �©� v :z.a :.«>� «xa� : \� � ©� <y� »� � <� <� � � � � ? 2� m� dw«e2� � � � � � � � » HOLLY FARMS FOODS, INC. FRESH RETAIL DIVISION, TYSON FOODS, INC. 1600 River Road, P.O. Box 88 Wwbwo, NWh Carolbia 28697,0088 w NIM SW2171 loops Wo"ImWom am""" 199DJanuary 31, 1990 somm awful Mr. Michael L. Parker, North Carolina Department of Environment, Health and Natural Resources Mooresville Regional Office 919 North Main Street Mooresville, NC 28115 SUBJECT: 1989 Annual Report, Permit No. WQ0000701 Holly Farms Foods, Inc. Harmony Rendering Plant Land Application Permit Rowan County, North Carolina Dear Mr. Parker: Attached you will find the annual report of the disposal activities conducted by Holly Farms in Rowan County. As we recently discussed, phosphorus, PCB, and residual chlorine tests were inadvertently omitted. Samples of the skimmings have been sent to the laboratory to obtain these values and will be sent to you as soon as possible. Please contact me if you have any questions concerning this report or require any further information. Sincerely, Lawrence R. Sampson Jr., P.E. N.C. Division Engineer LRS/mf Attachment cc: Ben Laws a * Offices: Minneapolis, Minnesota P10ce REPORT OF LABORATORY iLI Tampa, Florida h o T inC, oraly lle, Iowa Novato, California t Leawood, Kansas Irvine, California Asheboro, North Carolina PACE Client No.: 510025 December 7, 1999 PACE Project Number: 69102 504 Client: Holly Farms Foods, Inc. Address; Technical Services Complex 1600 River Wilkesboro, NC 2597 Attn: Daniel C. Wyatt Sample Location: Harmony Sludge, Direct Cate Sample(s) Collected. 10 17/89 Date Sample(s) Received; 10 20/89 PACE Sample Number: 91247 PARAMETERS UNITS RESULTS PARAMETERS UNITS RESULTS SCU, 5-Day mg/kg 205,000 __ Silver mg/kg L C, Alkalinity mg CaCO3 L L 200 Arsenic mg/kg 12.0 COD mg/kg 2,509,000 Boron mg/kg L 400 Ammonia -Nitrogen mg/kg 3000 Barium mg/kg 20 Total Nitrogen mg/kg 50,041 Calcium mg/kg 2800 TKN mg/kg 50,000 Cadmium mg/kg L 0•5 Nitrate -Nitrogen mg/kg' 28 Total Chromium um mg/kg 5.8 Nitrite -Nitrogen mg/kg 13 Copper mg/kq 5. Oil and Crep. mg/kq 644,006 Iron mg/kg 2700 pH units 5.3 Mercury ma/kg L 0.01 Percent Solids 10.12 Potassium It k 940 Sulfate mg/kg L 50 Magnesium mg/kg 23 Manganese mg/kg' SS Sodium mq/kg 750 Ni c kal mg/kg .9 Lead mg/kq 4.6 Selenium mg/kg L 0.5 Zinc mg/kg 150 All mg/kg results are dry -height basis. C Greater than L Less than The; data contained in this report were obtained using EPA or tither approved methodologies. All analyses were performed by me or under my direct supervision. 9_dqjL_��J, J. Allen S ivo,v- Manager, Analytical Laboratory P.O. Box 6 0 Asheboro, NC 27-:03 0 phone 1 are equal opp artunhy° adapt r Offices - Minneapolis, Minnesota acc, L "YSI Tampa, Flori a (oralvilla, Iowa aborationes, inc, Novato, California ,Kansas Irvine, California Asheboro, Ndrlh CaroR7na PACE Client .: 61003 December 7, 19E9 PACE Project Number: 691020504 Client: Holly Farms Foods, Inc, Address: Technical Services Complex 1600 River Wilkesboro, NC 3697 Attn: Daniel O. Wyatt Sample Location: Wilkesboro Grease Trap Sludge, Direct Data Sample(s) Collected: 10/17/9 Date Sample(s) Received. 10/0/ RACE Sample Number: 91246 PARAMETERS UNITS RESULTS PARAMETERS UNITS RESULTS � --- EODSD�,��.�_m_�-�� �,/-------- _-mm- 1�30,000 Silver rng/ L 0 Alkalinity mg CaCO3/L L 200 Arsenic mg/kq 1.1 COD mg/'kg 3, 5 00, 3 00 Enron mg/K" I I, i0 Amm i a -Nitrogen mg/kq 300 Barium mg/kg 3.4 Total Nitrogen ma/kg t9 Calciummg/kg 44 TENRig/kg 8900 Cadmium mR/kR 1m 0.1 Nitrate -Nitrogen mg/kg 7.4 Total Chromic mg/kg 0. s Nitrite -Nitrogen mg/kg 0.3 Copper mg/kg 12.8 Oil and Grease mg k9 670,000 Ironmg/kq 1.70 pH units 4.5 Mercury mglk0,.01 Percent Solids 31.24 Potassium mq/kg 1 Ail Sulfate mg/kg L 16 Magnesium /kg 13.0 Manganese erg/kg 3.4 Sodium rig/kg 237 Nickelmg/kg 0.4 Lead mg/kg 1.1 Selenium mg/kg L 0.3 Zinc mg/kg 35. i All mg/kg results are dry -weight basis. 0 Greater than Less than The data contained in this report were obtained using ERA or other approved methodologies. All analyses were performed by me or under my direct supervision 9AA4� d a Allen Spivey Manager, Analytical Laboratory P.O.Box6 C1 Asheboro, NC27203 0 Phone (919) 625-0923 an ec ua! opportunity rptoyer offices: F Minneapolis Minnesota Tampa, lorida, I t REPORT OF LABORATORY ANALYSIS 'P 'Pace F laboratories, Inc. Coralville, Iowa Novato, California Leawood, Kansas Irvine, California Asheboro, North Carolina owner and Location Holly Farms Foods of Sample Source: P. 0. Box 88 Wilesboro, NC 28697 Attn: Mrs Danny Wyatt Laboratory: at PACE Laboratories, Inc. 110 West Avenue Asheboro, NC 27203 USEPA Lab No. NCO02 NCNRCD Lab No. 18 NCSDWA Lab N. 37700 Sample Collected by: David Stone Date Sampled: October 11, 1989 Date Received in Lab: October 12, 1989 Sample Location: Wilkesboro Grease Trap Sludge Harmony Sludge Physical Characteristics: Laye- -- none -�UTFT—ayer B&V Sample Number: 91139 (Wilkesboro Sludge) 91140 (Harmony Sludge) Client 1.D. Number: 610028 Date Reported: November 27, 1989 Offices: , ► Minneapolis, Minnesota REPORT F LABORATORY ANALYSIS Tampa,Florida * lobora nit z oralville, Co q Novato, California " , Leawood, Kansas Irvine, California Asheboro, North Carolina Cli nt: Holier Farms Foods -2- Sample: 91139-L Location; Wilkesboro Grease Trap Sludge Project. 69101250 E P TOXICITY LEACHATE PROCEDURE AND TEST DATA <HAZARDOUS WASTE TESTING PROCEDURE ------------------------------------ The sample was analyzed for eight metals and six organics listed in the regulations and according to the extraction and filtration procedures detailed in CFF, Vol. 45, No. 98, Monday, May 19, 1980, pp. 33121-3312 . I ANALYTICAL INSTRUMENTS USED: Mettler A -1w5C Analytical Balance Perkin-Elmer HGA- CC Graphite Eoe el Desiccators Furnace Fisher Isotellrp Ovens B&L 5pectronic 70 Spectrophotometer_ Corning AC-11 Class Stills Perkin-Elmer 5000 Atomic Absorption Millipore Pressure Filtration Spectrophotometer and Extraction Assemblies Perkin-Elmer Sigma 28 Gas Perkin-Elmer PR -1C Painter Chr matograph Fisher Accument Model 520 pH meter LEACHATE TEST DATA: — s — ern' — w a — — — m m ------ ,Acetic acid requirements were determined from one sample, as listed below- E Time Saslol e , Wei ghtµ 200.9 grains Checked rills Added r. w w arv,..— s are. wn... fi ..... w i r w —.. .. ... — — .5 N Acetic Acid) i leis of 0.5 N Initial C acetic acid 15 min. C required to 30 min. 0' adjust to 1 hr. 9 50 +_" 0.2 2 hr. C at different 3 hr. C- time intervals 4 hr. C 24 hr'. C _2 hr.--------- Total CHARACTERISTICS OF SLUDGE: --------------------------- Cor°rosivit,y:; pH (initial) 4a2 PH (after leachate Ignitability (F)* P.O. Box 6 1:3 Asheboro, NC 0 � Phone( C - an equal o p f 4%.Mng qT Y�' �r Offices. Minneapolis, Minnesota REPORT LABORATORY ANALYSIS pampa, Florida laboratones, nc, oralrrill, Iowa Novato, California Leawood, Kansas Irvine, California Asheboro, North Carolina ; Cl i P nt» Holly Farts Foods - - Sample: 91139 Location. Wilkesboro Grease Trap Sludge Project: 691012504 { 1 F P TOXICITY L6AHATF TEST RESULTS EPA HAZARDOUS WASTE MAXIMUM LEVEL NUMBERCONTAMINANT ANT CONCENTRATION DETECTED i 1 (1 )' 6 4 Arsenic 5 L 0.005 D005 Barium 100.0 L 0.5 D006 Cadmium 1.0 L 0.003 D007 Chromium, Hexavalent 5.0 L 0.10 Chromium, Total 5.0 0.09 D008 Load 5.6 L 0.03 DOIO Selenium 1.0 L 0.005 11 Silver 5.0 L 0.005 D012 Fndrin (1, ,5,4,10,1 H chi r -1, -, _ 0.02 L 0.005 1,4,4a,5,6, , ,6a octahydro 1,4,_-o do, ndo-5,6-dimhanonaphtha lono) 1 Lindano (1,,,4,5,6 L Il.l5 Hoachlorocyclohoano, gamma isomer) D01.4 tho ychlor (1,1,1-Trichloro 16, f L 4LI 5 ,-bis(p-mothoyphonyl)than D 15 To;aph no (Technical chlorinated .5 L 0.005 camph no, 6 -69 chlorine) D 16 ,4- _, ( ,4 Dichloro h no ,ya oti 10.0 L 0.005 acid) D017 2,4,5-TP( ll o ( ,4,5- 1.0 L 0.005 Trichlorophono ypropionic acid P6FL Xb—o-r orTInc- 11769 x 6 � s Asheboro, NC 272030 Phone 1625-0923 an e auaal onDortvoity emoJover pacevREPORT OF LABORATORY ANALYSIS laboratones, inc, Client: Holly Farms Foods -2- Location: Harmony Sludge E P TOXICITY LEACHATE PROCEDURE AND TEST DATA Offices: Minneapolis, Minnesota Tampa, Florida Coralville, Iowa Novato, California Leawood, Kansas Irvine, California Asheboro, North Carolina Sample: 91140-L Project: 691012504 HAZARDOUS WASTE TESTING PROCEDURE: ------------------------------------ The sample was analyzed for eight metals and six organics listed in the regulations and according to the extraction and filtration procedures detailed in CFR, Vol. 45, No. 98, Monday, May 19, 1980, pp. 33121-33128. ANALYTICAL INSTRUMENTS USED: --------------------------- Mettler AK-160 Analytical Balance Perkin-Elmer HGA-400 Graphite Bne!vel pegCcators Furnace Fisher Isotemp Ovens B&L Spectronic 70 Spectrophotometer Corning AG-11 Glass Stills Perkin-Elmer 5000 Atomic Absorption Millipore Pressure Filtration Spectrophotometer and Extraction Assemblies Perkin-Elmer Sigma 28 Gas Perkin-Elmer PRS-10 Printer Chromatograph Fisher Accument Model 520 pH Meter LEACHATE TEST DATA: ------------------ Acetic acid requirements were determined from one sample, as listed below: Time Sample Weight: C. grams Checked mls Added --------- --------- (0.5 N Acetic Acid) mls of 0.5 N Initial 0 acetic acid 15 min. 0 required to 30 min. 0 adjust to I hr. 0 5.0 +/- 0.2 2 hr. 0 at different 3 hr. 0 time intervals 4 hr. 0 24 h r . 0 28 hr. --------- --------- Total 0 CHARACTFR7STICS OF SLUDGE: --------------------------- Corrosivity: PH (initial) 4.9 pH (after leachate) 4.9 RC. Box 6 0 Asheboro, NC 27203 0 Phone (919) 625-0923 an pnual cmorlunitv GMD10ver Offices: Minneapolis, Minnesota pacem REPORT OF LABORATORY ANALYSIS Tampa, Florida Coralville, Iowa laboratories, nc. Novato, California Leawood, Kansas Irvine, California Asheboro, North Carolina Client: Holly Farms Foods -3- Sample: 91140 Location: Harmony Sludge Project: 691012504 E P TOXICITY LEACHATE TEST RESULTS EPA HAZARDOUS WASTE MAXIMUM LEVEL NUMBER CONTAMINANT CONCENTRATION DETECTED -------- ------------------------ ------------- (mg/1) -------- (mg/1) D004 Arsenic S. L 0.005 D005 Barium 100.0 L U.S D006 Cadmium 1.0 L 0.003 D007 Chromium, Hexavalent 5.0 L 0.01 Chromium, Total S. L O:005 D008 Lead S. L 0.03 D009 Mercury 0.2 L 0.001 D010 Selenium 1.0 L Ow005 D011 Silver 5.0 L 0.005 D012 Endrin ('1,2,3,4,10,10- Hexachloro-1,7-epoxy- 0.02 L 0.005 1,4,,4a.5.6,7,8,8a- octahydro-1,4,-endo, endo-5,8-dim ethanonaphtha- lene) D013 Lindane (1,2,3,4,5,6- 0.4 L 0.005 Hexachlorocyclohexane, gamma isomer) D014 Methoxychlor (1,1,1-Trichloro- 10.0 L 0.005 2,2-bis(p-meth oxyphenyl)ethane) D015 Toxaphene (Technical chlorinated 0.5 L 0.005 camphene, 67-69% chlorine) D016 2,4-D, (2,4-Dichlorophenoxyacetic 10.0 L 0.005 acid) D017 2,4,5-TP (Silvex) (2,4,5- 1.0 L 0.005 Trichlorophenoxypropionic acid) P.O. Box 6 [--,, Asheboro, NC 27203 0 Phone (919) 625-0923 an gatial noonrrimitv amnlovpr Page 1 of 3 Sludge Land Applications/Disposal Report Form Annual Sludge Analysis Permittee: Holly Farms Poultry Industries, Inc. (Harmony Plant) Permit No.: 791IR2 ql�2q,7 Sludge Sample No. -- Date Collected 1011:11_ Location of Sampling_ Parameter Wet Concentration *Dry Concentration **Dry Loading (m 1/kk) (lbs/dry ton) PO4 as P TKN '54) oo 0 10o.0 NH3 as N 0 NO2 + NO3 Cd o Oil & Grease 4"1111141000 12-44 Cu PCB Ni O* 010 Pb Zn ISO Residual Chlorine ***P.A.N. (1) Subsurface Total Solids JO.12 pH (s.u.) 5g3 Type of sludge (circle as applicable): 1) compost, DAF, aerobic digested, anaerobic digested, drying beds, centrifuge, belt press, other (specify) *Dry concentration (mg/kg) = wet concentration (mg/1) x 100 % solids **Dry loading (lbs./dry ton) = .002 x mg/kg (1) If applied by subsurface injection: ***P.A.N. (Plant Available Nitrogen) = .2 (TKN-NH3 as N - NO2 - NO3) + (NH3 as N + NO2-NO3) (2) If surface applied: .2 (TKN-NH3 as N - NO2 - NO3) + .5 (NH3 as N + NO2+NO3) Page I of 3 Sludge Land Applications/Disposal Report Form Annual Sludge Analysis WJLtc,E',f0A() Permittee: Holly Farms Poultry Industries, Inc. (Razzoay Plant) Permit N. 7911R2 Sludge Sample No. Date Collected 10:tj-:JLocation of Sampling_ Parameter Wet Concentration *Dry Concentration **Dry Loading (mL/ kj�) (lbstdry ton) PO4 as P TKN Moo vv% NH3 as N NO2 + NO3 Cd Oil & Grease (01101 000 L340 CU 121 01OZ6 PCB Ni Pb ud Zn Residual Chlorine ***P.A.N. (1) Subsurface Total Solids M 31.2±— ph (su.) Type of sludge (circle as applicable): 1) compost, DAF, aerobic digested, anaerobic digested, drying beds, centrifuge, belt press, other (specify) *Dry concentration (mg/kg) = wet concentration x 100 solids **Dry loading (lbs./dry ton) - .002 x mg/kg (1) If applied by subsurface injection: ***P.A.N. (Plant Available Nitrogen) = .2 (TKN-NH3 as N - NO2 - NO3) + (NH3 as N + NO2-NO3) (2) If surface applied: .2 (TKN-NH3 as N - NO2 - NO3) + .5 (NH3 as N + NO2+NO3)