WQ0001026_Residual Annual Report 2020_20210208

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00001026
Applicant/Permittee City of Washington
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Washington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide inforration on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363993646
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0001026
Fbs Current Existing permt number
Applicant/Permittee Address* PO Box 1988, Washington, NC 27028
Facility Name * City of Washington RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Washington Annual Report - WQ0001026.pdf 6.05MB
Upload only 1 FDF docurrent (less than 250 NB). NLRiple documents rust be contained into one FDF file unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
ff &kgw
Submission Date 2/8/2021

February 8, 2021
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report - Washington
Treatment and Land Application of Residuals
Permit No. WQ0001026
Dear Sir or Madam:
Enclosed is one copy of the 2020 Annual Report for the above referenced land
application permit.
During 2020 EMA Resources, Inc. land applied 165.94 dry tons of wastewater residuals
to 64.02 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Z�fz G;2�
Brent Collins
Director of Technical Services
brent.collins(cr,,emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001026 County:
Facility Name (as shown on permit):
Land Application Operator:
Beaufort County, NC
Year: 2020
City of Washington
EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
'V.
Total number of amlication fields in the permit: 54
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 165.94
Total number of acres utilizes for land application during the year: 64.02
Part B - Annual Comoiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Adam Waters - Public Works Director
Name and Title (type or print)
of
Signature of Permittee ������ Date
;e—e 2- 2/ 1 /2021
Date Signature of Land Applier
Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0001026 Laboratory: 1) Waypoint Analytical
Facility Name: City of Washington 2)
Residual Source WQ # or NCO020648 3)
NPDES #: 4)
WWTP Name: Washington WWTP 5)
Residual Analvsis Data
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
5/6/20
5/14/20
Spring
Avcrage
Percent Solids (%)
NA
3.8
3.61
3.71
Arsenic
75
7.22
13.5
10.4
Cadmium
85
0.917
2.7
1.8
Copper
4,300
220
210
215.0
Chromium
NA
18.4
17.6
1 &0
Lead
840
19.1
18.4
18.8
Mercury
57
1.13
1.62
1.4
Molybdenum
75
6.42
6.76
6.6
Nickel
420
12.4
13.1
12.8
Selenium
100
8.89
13.5
11.2
Zinc
7,500
589
535
562.0
Total Phosphorus
NA
28600
26500
27550
TKN
NA
31900
33800
32850
Ammonia -Nitrogen
NA
10800
8300
9550.0
Nitrate and Nitrite
NA
136
135
135.5
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
pena ties for submittialse =or'on, including the possibility of fines and impri onment for knowing violations."
Signature of Preparer Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WQ0001026
City of Washington
NCO020648
WWTP Name: Washington WWTP
Residual Analvsis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter(mg/kg)1
I 1
�---------
1 1 1 1
• :11
• • 11
---------
Potassium
:1
' 1 1
---------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * I j
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
,"4
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Washington Total Dry Tons Applied (Annual):
WQ0001026 Cation Exchange Capacity (non 503 only):
Hunter Roost Farms Owner: Hunter Roost Farms Predominant Soil Series:
64.02 Acres Permitted: 64.02 Site #: BF210 Field #:
165.94
GoA
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phonis
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.59
Arsenic
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Cadmium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
1.115
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.115
Chromiuni
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Lead
0.097
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.097
Mercury
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
denum
Nickel
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Selenium
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Zinc
2.913
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.913
Total
Phos-
142.819
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
142.819
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 2/1/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Washington
Hunter Roost Farms
Operator: Hunter Roost Farms
WQ Permit #: WQ0001026 Field #:
Annual Dry Tons Applied: 165.94 Site #:
Predominant Soil Series: GoA
Crop 1 Name: Soybeans Crop 1 Max. PAN:
176
Crop 2 Name:
4 Acres Utilized: 64.02
BF210 Acres Permitted: 64.02
Cation Exchange Capacity (non 503): 0
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
F '5
w
*
o
o'
7�
* N
* w
o
TKN
mg/kg
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/4
78000
3.71
0.188
Washington
D
<.5"
S
0.5
0.3
1 32850
9550
1 136
4.486
NA
Beans
5/5
156000
3.71
0.377
Washington
D
<.5"
S
0.5
0.3
32850
9550
136
8.973
NA
Beans
5/7
136500
3.71
0.330
Washington
D
<.5"
S
0.5
0.3
32850
9550
136
7.851
NA
Beans
5/8
227500
3.71
0.550
Washington
D
<.5"
S
0.5
0.3
32850
9550
136
13.085
NA
Beans
5/9
247000
3.71
1 0.597
Washington
D
<.5"
S
0.5
0.3
32850
9550
136
14.207
NA
Beans
5110
1
227500
3.71
0.550
Washington
D
<.5"
S
0.5
0.3
1 32850
9550
1 136
13.085
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
0.000
0.000
TOTALS:
01
1072500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
61.689
0.000
Lime Applied
Annuallbs/acre
0.054
0.009
1.115
0.093
0.097
0.007
0.034
0.066
0.058
2.913 142.8191
16.291
19.204
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.161
0.053
6.412
0.984
0.82
0.034
0.166
0.562
0.127
C.C.E.
1180
Current Cumulative lbs/ac
0.215
0.062
7.527
1.077
0.917
0.041
0.200
0.628
0.185
Permitted C. P. L. R. * * * *
36
34
1338
1 267
15
1
374
89
Permit PAN Limit 1 st/2nd Crop
1
1 176
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
5/19/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-129-0070
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 5/8/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/28/2021
Arizona
State Program
AZ0816
8/30/2020
Arkansas
State Program
88-0650
2/7/2021
California
State Program
2904
5/10/2020
Georgia
State Program
C044
2/18/2023
Georgia
State Program
04015
6/30/2020
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
6/30/2020
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
04015
6/30/2020
Mississippi
State Program
MS
5/10/2020
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
8/31/2020
Pennsylvania
State Program
- NELAP
68-03195
5/31/2020
South Carolina
State Program
84002
5/10/2020
South Carolina
State Program
84002
6/30/2020
Tennessee
State Program
02027
2/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
9/30/2020
Virginia
State Program
00106
6/30/2020
Virginia
State Program
- NELAP
460181
9/14/2020
Washington
State Program
C1018
7/31/2020
Page 1 of 1 00001/20-129-0070
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 20-129-0070
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix
96074 Washington, NC WWTP
Solids
Date Collected
05/06/2020 09:00
Date Received
05/08/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 20-129-0070
Date: 5/19/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 96074 (Washington, NC WWTP)
Analyte: Calcium
QC Batch No: 1-491105/1-490877
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-491105/1-490877
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 96308
Analyte: Mercury
QC Batch No: L491212
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 4 of 8

• ...'. ®.
Way
P' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalyiical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Washington, NC Report Date : 05/19/2020
755 Yadkinville Rd Information : Received : 05/08/2020
Mocksville , NC 27028
Report Number : 20-129-0070 REPOR T OF ANAL YSIS Danyale Love
Project Manager
Lab No : 96074
Matrix: Solids
Sample ID: Washington, NC WWTP
Sampled:
5/6/2020
9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.4
%
1
05/13/2015:45
JDT
SW-DRYWT
Ammonia Nitrogen
10800
mg/Kg -
dry
694
1
05/19/20 14:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<136
mg/Kg -
dry
136
136
1
05/11/20 13:45
ZBD
4500NO3F-2011
Organic N
21140
mg/Kg -
dry
277.8
13890
1
05/12/20 16:32
DH
CALCULATION —
pH
10.8
S•U.
1
05/18/20 05:32
JSL
9045D
Total Solids
3.80
%
0.010
0.010
1
05/12/20 16:50
CJR
2540G-2011
Total Volatile Solids
55.0
%
0.010
0.010
1
05/12/20 16:50
CJR
2540G-2011
Total Kjeldahl Nitrogen
31900
mg/Kg -
dry
13900
10
05/12/20 16:32
CLP 4500NORGD-2011
Phosphorus
28600
mg/Kg -
dry
76.7
139
1
05/11/20 20:10
KKM
6010D
Aluminum
33300
mg/Kg -
dry
128
139
1
05/11/20 20:10
KKM
6010D
Arsenic
7.223
mg/Kg -
dry
6.67
13.9
1
05/11/20 20:10
KKM
6010D
Cadmium
0.9173
mg/Kg -
dry
0.556
2.78
1
05/11/20 20:10
KKM
6010D
Calcium 102000
mg/Kg -
dry
1080
1390
1
05/11/20 20:10
KKM
6010D
Chromium
18.4
mg/Kg -
dry
6.56
6.94
1
05/11/20 20:10
KKM
6010D
Copper
220
mg/Kg -
dry
8.61
13.9
1
05/11/20 20:10
KKM
6010D
Iron
14100
mg/Kg -
dry
237
278
1
05/11/20 20:10
KKM
6010D
Lead
19.1
mg/Kg -
dry
5.00
8.33
1
05/11/20 20:10
KKM
6010D
Magnesium
2860
mg/Kg -
dry
71.7
139
1
05/11/20 20:10
KKM
6010D
Manganese
489
mg/Kg -
dry
9.03
13.9
1
05/12/20 11:10
TJS
6010D
Mercury
1.13
mg/Kg -
dry
0.0892
0.406
1
05/12/20 11:22
DDB
7471A
Molybdenum
6.423
mg/Kg -
dry
3.75
6.94
1
05/11/20 20:10
KKM
6010D
Nickel
12.4
mg/Kg -
dry
3.33
6.94
1
05/11/20 20:10
KKM
6010D
Potassium
2520
mg/Kg -
dry
172
278
1
05/11/20 20:10
KKM
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation
Limit
Page 5 of 8

0
waypAo0nt,.
NALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-129-0070
Lab No : 96074
Sample ID: Washington, NC WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
REPORT OF ANALYSIS
Report Date : 05/19/2020
Received : 05/08/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 5/6/2020 9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<8.89
mg/Kg - dry
8.89
13.9
1
05/11/20 20:10
KKM
6010D
Sodium
2530
mg/Kg - dry
361
694
1
05/11/20 20:10
KKM
6010D
Zinc
589
mg/Kg - dry
22.5
34.7
1
05/11/20 20:10
KKM
6010D
Sulfur
9360
mg/Kg - dry
144
278
1
05/11/20 20:10
KKM
6010D
Neutralizing Value (%CCE)
22.8
% - dry
0.1
1
05/12/20 09:07
DXT
AOAC 955.01
Sodium Absorption Ratio
0.40
Ratio
1
05/11/20 20:10
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-129-0070
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
t98
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ICarleen Qualls Date & Time: 05/08/2020 12:34:17
Page 7 of 8

ro
w
LQ
m
Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
MDcksvOle, NC 27028
Project Description
project/site Location (City/State)
RUSH —Additional charges apply
M d of Shipme9t
Matrix Key
y,�
& Toni AC
/ `r
�� 5�tZA��6ry /Yc
Special Detection Limit(s)
date Resuits Needed
ed Ex ❑LISPS
Courier Client Drop off
WW —Wastewater GW —Groundwater
❑W—➢rinking Water S — Soil /Solid 0—oil
P - Product M - Misr
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
[e-mail]
z
�
A Coot r 10C Na25203 (Micro Cinly)
_
.0
Ca
0
U
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B Coo[ <=&C
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C H2SO4 pH<2
ANALYTICALc
is
Y
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a
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0 None Required
E NaOH pH�10
2790 Whitten Road
Memphis, TN 38133
Unless noted, all containers
u
°
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-
1
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F HNO3 pHe2
G HCL pH<2
o
Z
i
(90i 1 213.2400
per Table II of RO CFR Part
x
m
r ,
Cool gC�NnzS2o3
135.
l7
`J
Date
Time
Sample Identification
Required
Analysis/ Preservative
Comments/Notes
.LYJ
' L
W S#�S Cori
[
►
✓
Metais:Al,As,Ca, Cd,Cr,Cu,Fe, Pb
Mn, Mg, Mo, H9, Ni, Se,Na, P.S, K,Zn
111111EI 111111111111111111111111111111111111 05��op
EMA Ri:nxirces Inc 123322
Washmuton. NC
For Laboratory Use Only
Sam y {Name— Print)
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Seats
Lab Comments
0
ty
y /
Relin
Da a Time
Received by: [SIGNATURE)
Date Time
Blank/ ooler Temp
Relinclfished by: {SIGNATURE}
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Received by: (SIGNATURE)
Date Time
G
Relinquished by: (51GNATUREj
Date Time
ce' d .BSI HAi E}
Date
W�

Waypointo
ANALYTICAL
5/29/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-136-0098
Client Project Description: Washington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 5/15/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/28/2021
Arizona
State Program
AZ0816
8/30/2020
Arkansas
State Program
88-0650
2/7/2021
California
State Program
2904
5/10/2020
Georgia
State Program
C044
2/18/2023
Georgia
State Program
04015
6/30/2020
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
6/30/2020
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
04015
6/30/2020
Mississippi
State Program
MS
5/10/2020
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
8/31/2020
Pennsylvania
State Program
- NELAP
68-03195
5/31/2021
South Carolina
State Program
84002
5/10/2020
South Carolina
State Program
84002
6/30/2020
Tennessee
State Program
02027
2/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
9/30/2020
Virginia
State Program
00106
6/30/2020
Virginia
State Program
- NELAP
460181
9/14/2020
Washington
State Program
C1018
7/31/2020
Page 1 of 1 00001/20-136-0098
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 20-136-0098
Client Project Description: Washington, NC
Lab No Client Sample ID
98108 Washington WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 05/14/2020 07:00 05/15/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Washington, NC
Lab Report Number: 20-136-0098
Date: 5/29/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 98108 (Washington WWTP)
Analyte: Mercury
QC Batch No: 1-492095/1-491925
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

WayP
�'��' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalyiical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Washington, NC Report Date : 05/29/2020
755 Yadkinville Rd Information : Received : 05/15/2020
Mocksville , NC 27028
Q�ln
Report Number : 20-136-0098 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 98108
Matrix: Solids
Sample ID: Washington WWTP
Sampled:
5/14/2020
7:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.3
%
1
05/15/2015:50
JDT
SW-DRYWT
Ammonia Nitrogen
8300
mg/Kg -
dry
676
676
1
05/27/20 14:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<135
mg/Kg -
dry
135
135
1
05/19/20 14:23
ZBD
4500NO3F-2011
Organic N
25490
mg/Kg -
dry
2549
1
05/27/20 14:30
DH
CALCULATION —
pH
10.1
S.U.
1
05/27/20 06:41
JSL
9045D
Total Solids
3.61
%
0.010
0.010
1
05/20/20 17:49
FMM
2540G-2011
Total Volatile Solids
58.7
%
0.010
0.010
1
05/20/20 17:49
FMM
2540G-2011
Total Kjeldahl Nitrogen
33800
mg/Kg -
dry
2550
1
05/29/20 15:06
CLP 4500NORGD-2011
Phosphorus
26500
mg/Kg -
dry
74.6
135
1
05/21/20 18:53
TJS
6010D
Aluminum
31600
mg/Kg -
dry
125
135
1
05/21/20 18:53
TJS
6010D
Arsenic
<13.5
mg/Kg -
dry
6.49
13.5
1
05/21/20 18:53
TJS
6010D
Cadmium
<2.70
mg/Kg -
dry
0.541
2.70
1
05/21/20 18:53
TJS
6010D
Calcium
93800
mg/Kg -
dry
1050
1350
1
05/21/20 18:53
TJS
6010D
Chromium
17.6
mg/Kg -
dry
6.38
6.76
1
05/21/20 18:53
TJS
6010D
Copper
210
mg/Kg -
dry
8.38
13.5
1
05/21/20 18:53
TJS
6010D
Iron
13100
mg/Kg -
dry
230
270
1
05/21/20 18:53
TJS
6010D
Lead
18.4
mg/Kg -
dry
4.86
8.11
1
05/21/20 18:53
TJS
6010D
Magnesium
2730
mg/Kg -
dry
69.7
135
1
05/21/20 18:53
TJS
6010D
Manganese
486
mg/Kg -
dry
8.78
13.5
1
05/21/20 18:53
TJS
6010D
Mercury
1.62
mg/Kg -
dry
0.0868
0.395
1
05/18/20 11:43
DDB
7471A
Molybdenum
<6.76
mg/Kg -
dry
3.65
6.76
1
05/21/20 18:53
TJS
6010D
Nickel
13.1
mg/Kg -
dry
3.24
6.76
1
05/21/20 18:53
TJS
6010D
Potassium
2280
mg/Kg -
dry
167
270
1
05/21/20 18:53
TJS
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-136-0098
Lab No : 98108
Sample ID: Washington WWTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Washington, NC
Information :
REPORT OFANALYSIS
Report Date : 05/29/2020
Received : 05/15/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 5/14/2020 7:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<13.5
mg/Kg - dry
8.65
13.5
1
05/21/20 18:53
TJS
6010D
Sodium
2450
mg/Kg - dry
351
676
1
05/21/20 18:53
TJS
6010D
Zinc
535
mg/Kg - dry
21.9
33.8
1
05/21/20 18:53
TJS
6010D
Sulfur
7350
mg/Kg - dry
140
270
1
05/21/20 18:53
TJS
6010D
Sodium Absorption Ratio
0.41
Ratio
1
05/21/20 18:53
CALCULATION
Neutralizing Value (%CCE)
11.2
% - dry
0.1
1
05/19/20 07:43
DXT
AOAC 955.01
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-136-0098
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
It56
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ICarleen Qualls Date & Time: 05/15/2020 13:40:18
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinvil#e Rd
Mocksville, NC 27028
Project Description
Project/Slte Location {City/State]
RUSH - Additipnal charges apply
redf Shipment Matrix Key
}Special
' ` f� r � r�6 �O �+ �C-
�n5' f f 1I ��
•7 1T Q/y
Detection Limits)
Date Results Needed
x Ups �USPS WW --Wastewater GW-Groundwater
Courier ❑Client Drop Off DW - Drinking Water 5 - Soil /Solid 0 - oil
{�(J J H
(�
P - Product M - Misc
Other
Project Number
Project Manager Phone It
Project Manager Email
Purchase Order Number
Site/Facility ID 11
336-399-3646
[e-mail]
1�
Lv
z N
A Cool t 10C Na25703 (Micro only)
C
y
a Cool s= 6C
Waypoint
ANALYTICAL
�?
>:
a
q.
a
r
C]
CO
Q
a
iCO
C H2504 pH<2
D None Required
2790 Whitten Road
e
t'
!
a
sj
rn
C
Q
E NaOH pH>10
F HNO3 pHe2
Memphis, '1'N 38133
Unless noted, all containers
a
n
@
r '
�+
G H[t pH<2
[phone]
per Table 11 of 40 CFR Part
0)�[
Q
^
0
H H3p04 pHc2
136-
3
l7
j—
2 I—
I root r= 6C NA25203
Date
Time
5ample Identification
RequFred Analysis / Preservative
Comments/Notes
0 7:M
4-)ASJ/z- G zo-1v &L)iw
✓
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo, Hg,Ni,Se,Na,P,S, K,Zn
��11�1111V1K11111131I11iI$1111 lk1111111111111111 98
� 5-022020
EMA Resou'"% Inc 13:3956
Washinalon- NC
Client Remarks/Comments
Sludge Samples - Report Dry Weight
For Laboratory Use Only
5a by {Name - Print]
�,J � �T Kh
T
FSI
Ice
N
Custody
Lab Comments
Relin by R
_
❑ Znv
Receiv d by: (SIGNATURE)
Dat Time
L .
L' '
Y/
Blank/C er Te
Relin i b : SIGNATURE]
Da[ Time
Received by: ISTGNATURE)
Date Time
Q
Relinquished by: (SIGNATURE)
Date Time
*i q yry: (SIGNATURE)
Date Time
ce

aceAnalytical
National Center for Testing & Innovation
ANALYTICAL REPORT
May 18, 2020
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
L1216465
05/08/2020
WASHINGTON NC
Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: Jw C4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/2015:39 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
WASHINGTON WWTP L1216465-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
8
9
10
11
12
14
16
17
18
20
21
22
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources WASHINGTON NC L1216465 05/13/2015:39
PAGE:
2 of 22

WASHINGTON WWTP L1216465-01 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
I
SAMPLE SUMMARY
Collected by
Roy Whitaker
Batch
WG1473847
WG1474010
WG1474607
WG1475389
WG1474445
WG1475669
WG1474404
WG1474419
WG1474322
WG1474931
WG1474329
WG1474627
Dilution Preparation
date/time
1 05/11/20 08:59
1 05/11/2013:47
1 05/12/2015:24
1 05/14/20 00:00
1 05/12/201100
1 05/17/2016:40
1 05/12/20 09:50
1 05/12/2010:49
1 05/12/20 2120
1 05/13/20 00:19
1 05/12/2019:38
1 05/13/20 23:07
ONE LAB. NATIONWIDE. *
Collected date/time Received date/time
05/07/20 09:30 05/08/20 08:45
Cp
Analysis
date/time
05/11/20 08:59
05/11/2013:47
05/13/2012:15
05/14/20 00:00
05/13/2013:45
05/17/2016:40
05/12/20 2134
05/12/2017:55
05/12/20 2120
05/14/20 02:46
05/14/20 00:05
05/14/201150
Analyst
TM
IDW
BAM
LDT
KEG
JIC
TCT
EL
BMB
LEL
LEL
AO
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG:
EMA Resources WASHINGTON NC L1216465
DATE/TIME: PAGE:
05/13/20 15:39 3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/2015:39 4 of 22

WASHINGTON WWTP
Collected date/time: 05/07/20 09:30
Preparation by Method 1311
SAMPLE RESULTS - 01
L1216465
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
5/11/2020147:28 PM
WG1474010
TCLP ZHE Extraction -
5/11/2020 8:59:48 AM
WG1473847
Fluid 1
5/11/2020147:28 PM
WG1474010
Initial pH 7.07
5/11/2020147:28 PM
WG1474010
Final pH 4.86
5/11/2020147:28 PM
WG1474010
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
05/13/202012:15 WG1474607
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide 57.0 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 05/14/2020 00:00 WG1475389
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.15 T8 1 05/13/202013:45 WG1474445
Sample Narrative:
L1216465-01 WG1474445: 7.15 at22.3C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 05/17/202016:40 WG1475669
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Arsenic
ND
0.100 5
Barium
ND
0.100 100
Cadmium
ND
0.100 1
Chromium
ND
0.100 5
Lead
ND
0.100 5
Selenium
ND
0.100 1
Silver
ND
0.100 5
Volatile Organic
Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit
Analyte
mg/I
mg/I mg/I
Benzene
ND
0.0500 0.50
Carbon tetrachloride
ND
0.0500 0.50
Chlorobenzene
ND
0.0500 100
Chloroform
ND
0.250 6
ACCOUNT:
PROJECT:
EMA Resources
WASHINGTON NC
Dilution Analysis Batch
date / time
1 05/12/2020 2134 WG1474404
Dilution Analysis
Batch
date / time
1 05/12/202017:55
WG1474419
1 05/12/202017:55
WG1474419
1 05/12/202017:55
WG1474419
1 05/12/202017:55
WG1474419
1 05/12/202017:55
WG1474419
1 05/12/202017:55
WG1474419
1 05/12/202017:55
WG1474419
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Dilution Analysis
Batch
date / time
1 05/12/2020 2120
WG1474322
1 05/12/2020 2120
WG1474322
1 05/12/2020 2120
WG1474322
1 05/12/2020 2120
WG1474322
SDG:
DATE/TIME: PAGE:
L1216465
05/13/20 15:39 5 of 22

WASHINGTON
WWTP
SAMPLE RESULTS
- 01
Collected date/time: 05/07/20 09:30
L1216465
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit Dilution
Analysis
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
05/12/2020 2120
1,1-Dichloroethene
ND
0.0500 0.70 1
05/12/2020 2120
2-Butanone (MEK)
ND
0.500 200 1
05/12/2020 2120
Tetrachloroethene
ND
0.0500 0.70 1
05/12/2020 2120
Trichloroethene
ND
0.0500 0.50 1
05/12/2020 2120
Vinyl chloride
ND
0.0500 0.20 1
05/12/2020 2120
(S) Toluene-dH
101
80.0-120
0511212020 21.20
(S) 4-Bromofluorobenzene
86.6
77.0-126
0511212020 21.20
(S) 1,2-Dichloroethane-d4
136
11 70.0-130
051121202021.20
Chlorinated Acid Herbicides (GC)
by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) 2,4-Dichlorophenyl Acetic Acid 57.0
Pesticides (GC) by Method 8081B
Batch
WG1474322
WG1474322
WG1474322
WG1474322
WG1474322
WG1474322
WG1474322
WG1474322
WG1474322
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 05/14/2020 02:46
WG1474931
0.00200
10
1 05/14/2020 02:46
WG1474931
14.0-158
0511412020 02.46
WG1474931
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 05/14/2020 00:05
WG1474329
Endrin
ND
0.00500
0.02
1 05/14/2020 00:05
WG1474329
Heptachlor
ND
0.00500
0.0080
1 05/14/2020 00:05
WG1474329
Lindane
ND
0.00500
0.40
1 05/14/2020 00:05
WG1474329
Methoxychlor
ND
0.00500
10
1 05/14/2020 00:05
WG1474329
Toxaphene
ND
0.0100
0.50
1 05/14/2020 00:05
WG1474329
(S) Decochlorobiphenyl
94.2
10.0-128
0511412020 00.05
WG1474329
(S) Tetrochloro-m-xylene
86.5
10.0-127
0511412020 00.05
WG1474329
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 05/14/202011:50
WG1474627
2,4-Dinitrotoluene
ND
0.100
0.13
1 05/14/202011:50
WG1474627
Hexachlorobenzene
ND
0.100
0.13
1 05/14/202011:50
WG1474627
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 05/14/202011:50
WG1474627
Hexachloroethane
ND
0.100
3
1 05/14/202011:50
WG1474627
Nitrobenzene
ND
0.100
2
1 05/14/202011:50
WG1474627
Pyridine
ND
0.100
5
1 05/14/202011:50
WG1474627
3&4-Methyl Phenol
ND
0.100
400
1 05/14/202011:50
WG1474627
2-Methylphenol
ND
0.100
200
1 05/14/202011:50
WG1474627
Pentachlorophenol
ND
0.100
100
1 05/14/202011:50
WG1474627
2,4,5-Trichlorophenol
ND
0.100
400
1 05/14/202011:50
WG1474627
2,4,6-Trichlorophenol
ND
0.100
2
1 05/14/202011:50
WG1474627
(S) 2-Fluorophenol
39.3
10.0-120
0511412020 11.50
WG1474627
(S) Phenol-d5
24.5
10.0-120
0511412020 11.50
WG1474627
(S) Nitrobenzene-d5
62.2
10.0-127
0511412020 11.50
WG1474627
(S) 2-Fluorobiphenyl
82.8
10.0-130
0511412020 11.50
WG1474627
(S)2,4,6-Tribromophenol
74.0
10.0-155
051141202011.50
WG1474627
(S) p-Terphenyl-d14
91.3
10.0-128
0511412020 11.50
WG1474627
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 6 of 22

WG1474607
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9012 B
L1216465-01
Method Blank (MB)
C p
(MB) R3527423-1 05/13/201201
MB Result MB Qualifier
MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
TC
I
Reactive Cyanide -10.0390
0.250
FS
Original Sample (OS) • Duplicate (DUP)
[�n]
(OS) • (DUP) R3527423-3 05/13/2012:10
Original Result DUP Result
Dilution
DUP RPD DUP Qualifier DUP RPD
Limits
5
Sr
Analyte mg/kg
Reactive Cyanide ND
1
—
0.000 20
Laboratory Control Sample (LCS)
GI
(LCS) R3527423-2 05/13/20 12:02
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
FAI
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.73
109
85.0-115
1—Sc
Original Sample (OS) • Matrix Spike (MS)
• Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527423-4 05/13/20 12:11 • (MSD) R3527423-5 05/13/2012:14
Spike Amount Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/kg
mg/kg
mg/kg
Reactive Cyanide 1.67
1.22
1.23 73.4 74.1 1 75.0-125 J6 J6 0.940
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 7 of 22

WG1475389
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3527646-1 05/14/20 00:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide U 7.63 25.0
Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1216465-01
(OS) • (DUP) R3527646-3 05/14/20 00:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg %_
Reactive Sulfide ND 1 0.000 20
Original Sample (OS) • Duplicate (DUP)
(OS) • (DUP) R3527646-4 05/14/20 00:00
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg
Reactive Sulfide ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3527646-2 05/14/20 00:00
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
Reactive Sulfide 100 88.1 88.1 70.0-130
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527646-5 05/14/20 00:00 • (MSD) R3527646-6 05/14/20 00:00
Spike Amount Original Result MS Result MSD Result MS Rec.
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide 100 95.4 95.1 95.4
MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
95.1 1 70.0-130 0.327
ONE LAB. NATIONWIDE. *
Cp
ITC]
FSS
[Cn]
5
Sr
�GI
1711
FSCI
RPD Limits
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 3 of 22

WG1474445 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1216465-01
Laboratory Control Sample (LCS)
(LCS) R3527428-1 05/13/201345
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su
Corrosivity by pH 10.0 9.98 99.8 99.0-101
Sample Narrative:
LCS: 9.98 at20.2C
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 9 of 22

WG1475669
Wet Chemistry by Method D93/1010A
Original Sample (OS) • Duplicate (DUP)
(OS) • (DUP) R3523324-3 05/17/2016:40
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F
Ignitability 71.0 1 5.48
L1215923-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1216465-01
DUP Qualifier DUP RPD
Limits
10
(OS) L1215923-01 05/17/2016:40 • (DUP) R3523324-4 05/17/2016:40
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability 133 139 1 4.41 10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3528824-1 05/17/20 16:40 • (LCSD) R3528824-2 05/17/20 16:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg.F Deg.F Deg.F
Ignitability 82.0 85.0 85.0 104 104 95.6-104 0.000 10
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 10 of 22

WG1474404 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1216465-01
Method Blank (MB)
(MB) R3527133-1 05/12/20 20:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Mercury U 0.00330 0.0100
Laboratory Control Sample (LCS)
(LCS) R3527188-2 05/12/20 2100
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
Mercury 0.0300 0.0262 87.3
Rec. Limits LCS Qualifier
80.0-120
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) • (MS) R3527133-3 05/12/20 21:04 • (MSD) R3527133-4 05/12/20 2106
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0312 0.0301 104 100 1 75.0-125 3.61 20
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527133-5 05/12/20 21:10 • (MSD) R3527133-6 05/12/20 2112
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
Mercury 0.0300 0.0296 0.0286 98.6 95.3 1 75.0-125 3.40 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 11 of 22

WG1474419
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3527172-1 05/12/201705
MB Result
MB Qualifier MB MDL
Analyte mg/I
mg/I
Arsenic U
0.0333
Barium U
0.0333
Cadmium U
0.0333
Chromium U
0.0333
Lead U
0.0333
Selenium U
0.0333
Silver U
0.0333
Laboratory Control Sample (LCS)
(LCS) R3527172-2 05/12/20 17:07
Spike Amount
LCS Result
LCS Rec.
Analyte mg/I
mg/I
Arsenic 10.0
9.87
98.7
Barium 10.0
10.2
102
Cadmium 10.0
9.86
98.6
Chromium 10.0
9.98
99.8
Lead 10.0
9.81
98.1
Selenium 10.0
10.0
100
Silver 2.00
1.88
94.1
QUALITY CONTROL SUMMARY
L1216465-01
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
Rec. Limits
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
80.0-120
LCS Qualifier
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527172-4 05/12/2017:16 • (MSD) R3527172-5 05/12/20 1713
Spike Amount Original Result MS Result MSD Result MS Rec.
Analyte mg/I mg/I mg/I
Arsenic
10.0
9.90
9.94
99.0
Barium
10.0
10.4
10.4
102
Cadmium
10.0
9.92
9.92
99.2
Chromium
10.0
10.1
10.1
101
Lead
10.0
9.90
9.89
98.7
Selenium
10.0
10.1
10.1
101
Silver
2.00
1.89
1.90
94.4
ONE LAB. NATIONWIDE. *
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
99.4
1 75.0-125
0.394
20
102
1 75.0-125
0.216
20
99.2
1 75.0-125
0.0376
20
101
1 75.0-125
0.0598
20
98.6
1 75.0-125
0.104
20
101
1 75.0-125
0.0169
20
95.2
1 75.0-125
0.895
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 12 of 22

WG1474419 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1216465-01
ONE LAB. NATIONWIDE. *
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527172-6 05/12/20 17:23 • (MSD) R3527172-7 05/12/20 17:26
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.62
9.62
96.2
Barium
10.0
10.4
10.4
104
Cadmium
10.0
9.73
9.75
97.3
Chromium
10.0
10.0
10.0
100
Lead
10.0
9.76
9.75
97.6
Selenium
10.0
9.64
9.71
96.4
Silver
2.00
1.87
1.86
93.6
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
96.2
1 75.0-125
0.0426
20
104
1 75.0-125
0.104
20
97.5
1 75.0-125
0.242
20
100
1 75.0-125
0.284
20
97.5
1 75.0-125
0.0655
20
97.1
1 75.0-125
0.778
20
93.1
1 75.0-125
0.600
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 13 of 22

WG1474322 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1216465-01
Method Blank (MB)
(MB) R3527039-2 05/12/201303
MB Result MB Qualifier
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-dH
98.6
(S) 4-Bromofluorobenzene 83.4
(S) 1,2-Dichloroethane-d4 121
Laboratory Control Sample (LCS)
(LCS) R3527039-1 05/12/20 0920
Spike Amount
LCS Result
Analyte
mg/I
mg/I
Benzene
0.250
0.241
Carbon tetrachloride
0.250
0.261
Chlorobenzene
0.250
0.211
Chloroform
0.250
0.250
1,2-Dichloroethane
0.250
0.266
1,1-Dichloroethene
0.250
0.234
2-Butanone (MEK)
1.25
1.12
Tetrachloroethene
0.250
0.236
Trichloroethene
0.250
0.236
Vinyl chloride
0.250
0.225
(S) Toluene-dH
(S) 4-Bromofluorobenzene
(S) 1,2-Dichloroethane-d4
MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
0.0167
0.0167
0.0167
LCS Rec.
96.4
104
84.4
100
106
93.6
89.6
94.4
94.4
90.0
96.0
87.5
118
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
77.0-126
70.0-130
Rec. Limits LCS Qualifier
70.0-123
68.0-126
80.0-121
73.0-120
70.0-128
71.0-124
44.0-160
72.0-132
78.0-124
67.0-131
80.0-120
77.0-126
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 14 of 22

ONE LAB. NATIONWIDE. *
WG1474322 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1216465-01
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527039-3 05/12/20 22:27 • (MSD) R3527039-4 05/12/20 22:50
Spike Amount
Original Result MS Result
MSD Result MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
Benzene 0.250
0.272
0.254 109
102
1 17.0-158
6.84
27
Carbon tetrachloride 0.250
0.334
0.298 134
119
1 23.0-159
11.4
28
Chlorobenzene 0.250
0.219
0.210 87.6
84.0
1 33.0-152
4.20
27
Chloroform 0.250
0.278
0.268 ill
107
1 29.0-154
3.66
28
1,2-Dichloroethane 0.250
0.306
0.265 122
106
1 29.0-151
14.4
27
1,1-Dichloroethene 0.250
0.289
0.260 116
104
1 11.0-160
10.6
29
2-Butanone (MEK) 1.25
1.20
1.22 96.0
97.6
1 10.0-160
1.65
32
Tetrachloroethene 0.250
0.265
0.263 106
105
1 10.0-160
0.758
27
Trichloroethene 0.250
0.277
0.253 ill
101
1 10.0-160
9.06
25
Vinyl chloride 0.250
0.292
0.259 117
104
1 10.0-160
12.0
27
(S) Toluene-dH
92.5
96.1
80.0-120
(S) 4-Bromofluorobenzene
83.1
86.9
77.0-126
(S) 1,2-Dichloroethane-d4
121
122
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
WASHINGTON NC
L1216465
05/13/20 15:39
15 of 22

WG1474931
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3527693-1 05/14/20 0103
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S) Z4-Dichlorophenyl Acetic 59.8
Acid
QUALITY CONTROL SUMMARY
L1216465-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS)
(LCS) R3527693-2 05/14/20 0125
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I
2,4-D 0.0500 0.0282 56.4
2,4,5-TP (Silvex) 0.0500 0.0315 63.0
(S) Z4-Dichlorophenyl Acetic 54.2
Acid
Rec. Limits LCS Qualifier
50.0-120
50.0-125
14.0-158
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527693-3 05/14/20 01:57 • (MSD) R3527693-4 05/14/20 02:14
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
Analyte
mg/I
mg/I
mg/I
2,4-D
0.0500
0.0275
0.0306
55.0
2,4,5-TP (Silvex)
0.0500
0.0303
0.0345
60.6
(S) Z4-Dichlorophenyl Acetic
58.8
Acid
MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
61.2 1 50.0-120 10.7
69.0 1 50.0-125 13.0
63.4 14.0-158
ONE LAB. NATIONWIDE. *
RPD Limits
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 16 of 22

WG1474329
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1216465-01
(MB) R3527804-1 05/13/20 2137
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
103
10.0-128
(S) Tetrochloro-m-xylene
84.0
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3527804-2 05/13/20 22:02
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00983
98.3
55.0-129
Endrin
0.0100
0.0103
103
57.0-134
Heptachlor
0.0100
0.00852
85.2
27.0-132
Methoxychlor
0.0100
0.0108
108
54.0-155
(S) Decachlorobiphenyl
98.6
10.0-128
(S) Tetrochloro-m-xylene
81.8
10.0-127
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527304-3 05/13/20 22:39 • (MSD) R3527304-4 05/13/20 22:51
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/I
mg/I
mg/I
Gamma BHC
0.0100
0.00978
0.0105
97.8
105
1 14.0-141
7.10
Endrin
0.0100
0.0103
0.0108
103
108
1 10.0-160
4.74
Heptachlor
0.0100
0.00833
0.00756
83.3
75.6
1 16.0-136
9.69
Methoxychlor
0.0100
0.0110
0.0116
110
116
1 10.0-160
5.31
(S) Decachlorobiphenyl
98.2
99.3
10.0-128
(S) Tetrochloro-m-xylene
84.2
88.7
10.0-127
ONE LAB. NATIONWIDE. *
RPD Limits
40
39
40
34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/20 15:39 17 of 22

WG1474627 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1216465-01
Method Blank (MB)
(MB) R3527636-2 05/14/20 0712
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
Pyridine
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
(S) Nitrobenzene-d5
67.5
10.0-127
(S) 2-Fluorobiphenyl
85.1
10.0-130
(S) p-Terphenyl-d14
90.8
10.0-128
(S) Phenol-d5
24.4
10.0-120
(S) 2-Fluorophenol
42.3
10.0-120
(S) 2,4, 6-Tribromophenol
79.0
10. 0-155
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3527686-1 05/14/20 06:51
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.383
76.6
18.0-120
2,4-Dinitrotoluene 0.500
0.447
89.4
49.0-124
Hexachlorobenzene 0.500
0.415
83.0
44.0-120
Hexachloro-1,3-butadiene 0.500
0.361
72.2
19.0-120
Hexachloroethane 0.500
0.370
74.0
15.0-120
Nitrobenzene 0.500
0.361
72.2
27.0-120
Pyridine 0.500
0.0758
15.2
10.0-120
2-Methylphenol 0.500
0.326
65.2
28.0-120
3&4-Methyl Phenol 0.500
0.319
63.8
31.0-120
Pentachlorophenol 0.500
0.486
97.2
23.0-120
2,4,5-Trichlorophenol 0.500
0.430
86.0
44.0-120
2,4,6-Trichlorophenol 0.500
0.415
83.0
42.0-120
(S) Nitrobenzene-d5
61.7
10.0-127
(S) 2-Fluorobiphenyl
85.2
10.0-130
(S) p-Terphenyl-d14
89.8
10.0-128
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
WASHINGTON NC L1216465 05/18/20 15:39 18 of 22

WG1474627 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1216465-01
Laboratory Control Sample (LCS)
(LCS) R3527686-1 05/14/20 06:51
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) Phenol-d5 25.6 10.0-120
(S) 2-Fluorophenol 43.5 10.0-120
(S) 2,4, 6-Tribromophenol 81.0 10. 0-155
Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) • (MS) R3527686-3 05/14/20 12:34 • (MSD) R3527686-4 05/14/20 12:55
Spike Amount
Original Result MS Result
MSD Result
MS Rec.
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
0.313
0.334
62.6
2,4-Dinitrotoluene
0.500
0.377
0.399
75.4
Hexachlorobenzene
0.500
0.339
0.368
67.8
Hexachloro-1,3-butadiene
0.500
0.287
0.304
57.4
Hexachloroethane
0.500
0.307
0.321
61.4
Nitrobenzene
0.500
0.301
0.322
60.2
Pyridine
0.500
ND
ND
14.1
2-Methylphenol
0.500
0.274
0.285
54.8
3&4-Methyl Phenol
0.500
0.277
0.289
55.4
Pentachlorophenol
0.500
0.412
0.438
82.4
2,4,5-Trichlorophenol
0.500
0.359
0.386
71.8
2,4,6-Trichlorophenol
0.500
0.352
0.380
70.4
(S) Nitrobenzene-d5
52.4
(S) 2-Fluorobiphenyl
65.9
(S) p-Terphenyl-d14
76.3
(S) Phenol-d5
22.6
(S) 2-Fluorophenol
37.9
(S) 2,4, 6-Tribromophenol
68.0
MSD Rec.
66.8
79.8
73.6
60.8
64.2
64.4
15.6
57.0
57.8
87.6
77.2
76.0
55.0
70.1
80.7
22.9
39.6
73.5
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 17.0-120
6.49
1 39.0-125
5.67
1 35.0-122
8.20
1 12.0-120
5.75
1 10.0-120
4.46
1 12.0-120
6.74
1 10.0-120
9.83
1 10.0-120
3.94
1 10.0-120
4.24
1 10.0-128
6.12
1 33.0-120
7.25
1 26.0-120
7.65
10.0-127
10.0-130
10.0-128
10.0-120
10.0-120
10.0-155
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
37
30
36
37
31
31
ACCOUNT:
EMA Resources
PROJECT:
WASHINGTON NC
SDG: DATE/TIME:
L1216465 05/13/20 15:39
PAGE:
19 of 22

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J1
Surrogate recovery limits have been exceeded, values are outside upper control limits.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
Fp
Fc
FS
Fn
Fr
Fc
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources WASHINGTON NC L1216465 05/13/2015:39 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7C71
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR
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VWY
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ACCOUNT: V PROJECT:
EMA Resources WASHINGTON NC
ME
MN
WVI NY
MI T
IA T PA 4
OH
Mo
IL Ihi
T T WV
VAT
KY
N * r�
AR _<
MS AL GA
LA
FL
SDG: DATE/TIME: PAGE:
L1216465 05/13/20 15:39 21 of 22

Billing Information:
A
ialvsis /
Container
ervative
C'hain of Custody Page of
�EMA Resources
Mr. Brent Collins LChk
755 Yadkinville Road
C2Af18 I
755 Yadkinville Road
Mocksville, NC 27028
hsnwe cnwrw.srsxv m n�
Mocksville, NC 27028
12065 Lebanon Rd
Report to:
Email To: [e-mail]
Mr. Brent Collins
Mount Juliet TN 17122
Ij
Phone: [phone] \`
Phone_ 800.767.5859 r
fax [phone] Q.
Project
CityeState
Please Circle
Description Sludge
�/
Collected: IVG�pN C
PT MT CT ET
Client Project SI
Lab Protect p
SDG #
Phone: [phone]
1 GAOU� v5
Fax: [phone]
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Tabl
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print):
Site/Facility ID B
P.O. #
��� e
7
Acctnurm tMARES
`J
l
Template:T11413
Collect (signat r
Rush. (Lab MUST Be Notified) Q uote #
Same Day Five Day
ap
J
Prelogin: P748421
_ Next Day _ 5 Day iRad Only) Date Results Needed
PM: 807-Justin Carr
Immediately
_Two Day _ 10 Day (Rad Only) No.
C
PB. ! 1 L
Packed on Ice N _ Y
Three Day of
_J
r
Shipped via: FedEX Standard
Sample ID
Comp/Grab
Matrix
Depth
Date
Time
ntrs
U
U
Remarks Sample a(lab only)
[�—
SS
2
X
X
_ b
i
_..._.
"Matrix: Remarks: Sammie Rece t C rkl.'^^'.
pH Temp COC Seal Pres nt/IntaclFli _Y_
SS -Soil AIR -Air F- Filter --
COC Signe ccura_ te: Y N
GW - Groundwater 8 - Bioassay
WW - WasteWa[er Flaw Other Battles arrive intact; Y _N
Correct bottles used: Y N
DW - Drinking Water Sufficient volume sent: Y N
Samples re ned via: p r�L �S —
OT Other Trackingk If Anolicable
- t p
UPS FedEx Courier VOA Zero HeadsQate: Y N
Relin h b at a Time: Received b (Signature) Trip Blank Received: Yes No preservation Correct/Checked: y _N
q y' Y'( g ) p
RAD Screen <0.5 mR/hr; Y N
�� 3 aD p HCL/ eoH — —
TSR
R inqu' ed by : (Signature)
Date: Time
Received by: (Signatunej
T oC Bottles Received:
If preservation required by Login: Date/Time
t- : IL3 2
Relinquished by : (Signature)
Date: Time,
Received for lab by: (Signature)
Date Time:
Hold:
Condit io
NCF / O

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Pre arer Name and Title (t e o rint)
A
W
Signature of Pr arer* ate
Facility Name: City of Washington
WWTP Name: Washington WWTP
Monitoring Period: From 1/1/2020 To
WQ Permit Number: WQ0001026
NPDES Number: NCO020648
12/31 /2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:71
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray❑
Gamma Rav [3
Pasteurization ❑
.
Class B: I Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ JAerobic Digestion ❑
_ _ _....
....
Anaerobic Digestion ❑ .......................:........:........................................................
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Allowable Level
Pathogen Density
NumDer of
Excee-
Frequency
Sample
Analytical
Parameter
in Sludge
g
inimur
Geo. Mean
aximu
Units
nces
of Analysis
Type
Tech-nique
2 x 10 to the MPN
4500
8267
82500
MPN/g
0
Quarterly
G
SM92210E
6th power
per gram of
Fecal Coliform
total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform)
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please maicare alternative periurttieu:
Alt.I (VS reduction) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 2 (40-day bench) ❑
Alt. 6 (Alk. Stabilization ❑
Alt. 3 (30-day bench) 0
Alt 7 (Drying - Stable) ❑
Alt. 4 (Spec. 02 uptake) ❑
JAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Hope Woolard - Water Resources Superintendent Brent Collins; Director of Technical Services
Land Applier Name and TTittllee (if applicable)(type or print)
� !1 4v 1�1 - 2/1/2021
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Summary Sheet
Fecal Coliforms
Date: 4/27/2020
Location #
MPN/g
Log
1
4500
3.6532
2
4000
3.6021
3
4500
3.6532
4
4500
3.6532
5
4500
3.6532
6
82500
4.9165
7
19500
4.2900
8267
Geometric Means/g
Total Dry Solids
Signature

NM DATE I TIME
Sampled By
Lt
Received B y
Analyzed By
Calculated By
Checked By
24 hr. Check
48 hr. Check 1412119,0,
72 hr. Check �00/Ac,
Teinp OC
Llq'soc
Sample Location Slud2e # /
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
I fill
AMIN
0.0000001
noun
'm
W0100000M
WIMMINWOM
mmom
Fecal Coliform Test
0.0000001
000000001
ion
=MMMMM
MWOM
MPN Fecal Coliform/g = 10 x MPN index / 100 ml MPN/g = 10 x
largest volume X % dry solids tested
Sterility Control PAU/9-
Quality Control Tubes
Double Strength (DS) Control
10 mL
Single Strength (SS) Control
Ale
EC Broth Control
Revised 5-23-16

NAE DATE / TIME
Sampled By
Received By 2rc
Analyzed By
Calculated By
Checked By 51) -2 if
24 hr. Check
48 hr. Check Lil,?Lqb�-O //32,JtL,�
72 hr. Check
Temp '350 OC
L-ILA'Soc
Sample Location Sludge # /
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
E
o®��o®eeavw000®esee����_����
��WMMMM=Onn=
MMMMMOM0011=01
Wnmm
M
Fecal Coliform Test
0.0000001
t, /� 9 MPN Fecal Coliform/g 10 x MPN index / 100 ml MPN/— 10x =
largest volume X % dry solids tested x
Sterility Control
Quality Control Tubes 10 mL
Double Strength (DS) Control
Single Strength (SS) Control
t, 0 A aj-, rp—
EC Broth Control I W� e=
\j
Revised 5-23-16
c, 00
4C7

A E DATE / TIME
NG'
Sampled 1$y
� �'�
`�t z�
Received By
Analyzed By
= ^\� �
`�"a ' ac i 1045-
Calculated By
Checked By
C�LJl1�S
f l
24 hr. Check of , air 9,3�
48 hr. Check f4 C3 J
72 hr. Check, ct k 'CorZL,)
Temp U °C
4LA,S°C
Sample Location Slugs #
Sample Type: Crab x Composite _
Preservation: NONE
FECAL, C®L.IFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumntive Test
�
I I1
1 111
11111
111111
� I lllllli
I I111�1II
"
Fecal Coliform Test
mL Sample 0.001 0.0001 0.00001 0.000001 0.0000001
24 hours — —
MPN Fecal Coliform/g = 1.0 x MPN index / 100 ml � MPN/g = 10 x , • Q = 1�7c
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
r' e i VT
Single Strength (SS) Control
EC Broth Control
v
Revised 5-23-16
0.00000001 1 MPN
u

NAME,, I)E1TE /TIME
Sampled By
Received By
Analyzed By 1,/45
Calculated Byu
Checked By -5 '-o
24 hr. Check It ao loa �
48 hr. Check Libglao 3a Vl
72 hr. Check
Temp 35 C) °C
LlL�,SoC
Sample Location Slue # 3
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
� 1 11
I III
1 1111
I IIIII
i I IIII11
Fecal Coliform Test
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes 10 mL
Double Strength (IDS) Control =�
Single Strength (SS) Control
EC Broth Control
v
Revised 5-23-16
SMPN/g= 10 x /P —
c
0 O CW

Sampled By L
�G'�%%/�
Received By
Analyzed By
Calculated By
Checked By
DATE/TIME
24 hr. Check q
48 hr. Check tib'q ao 3-t
72 hr. Check V"dac
Temp '35 0 °C
Sample Location Sludge # 4
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM 'TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive 'Pest
Fecal Coliform Test
1 1 1 I 1 1 1
I HUM l
��t
1 1 1 1 1 1
I l l i l l�� I I 1 1 1 1 1 1
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
` e , /�
Single Strength (SS) Control
EC Broth Control
/U w '
Revised 5-23-16
MPN/g = 10 x
u L
17
O 'ool�
-'
r

NA E
Sampled By /r�G!L'�eYc
Received By
Analyzed By
Calculated By
Checked By
DATE / TIME
24 hr. Check 4t/,-',S1aO j
48 hr. Check 9),-,
72 hr. Checl(4,/ ;0/20
1 1 , I , 10e- 7 TDLL)
Temp '5,C) OC
4Li,Soc
Sample Location Sludae #
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
I fill
000001
AN
MMMMM
Fecal Coliform Test
0.0000001
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
V&C
Single Strength (SS) Control
t,
A) e a, (1-J-; vC,
EC Broth Control
A44 W� gi
Revised 5-23-16
f�
MPN/g = 10 x E
C) , 00/�

NA E- DATE / TIME
Sampled By
Received By
q ISC7 blo
Analyzed By
Calculated By
3
Checked By
lu al
Temp `350 Oc
,1q,SOC
Sample Location Sludze # (,0
24 hr. Check qj,"Sla(D Sample Type: Grab x Composite
48 hr. Check 14jagla-0 /130. j-*,bt-,' Preservation: NONE
72 hr. Check
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
man
MUMMMO
MW
Fecal Coliform Test
===NMI,
M
MWOOM
1MMMI
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
t,
Sterility Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
Single Strength (SS) Control
0 (fl-; VC
EC Broth Control
w
Revised 5-23-16
MPN/g
lox 33.0 5 3 0
CC)
0,00/1 50 0 �,X/
k,

� / DATE TIME
Sampled By
LN MA%
Lt
Received By
Analyzed By
Calculated By
I
L L
Checked By
24 hr. Check qb�s—Lao,
48 hr. Check 1412,91ac it'
72 hr. Check + C iOO5,--)73Cj
L71da
'350 OC
Temp 41 . ,60C
Sample Location Sludge #7-
Sample Type: Grab x Composite
Preservation: NONE
FECAL COLIFORM TEST
Standard Methods 9221 C E-2006(MPN)(Aqueous)
Presumptive Test
I IlIff
0.00000001
MMOM,
01000,MNIMMOMM,
MMM
'Im
MMIM
V
Fecal Coliform Test
—0"
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
MPN Fecal Coliform/g = 10 x MPN index / 100 ml
largest volume X % dry solids tested
Sterilitv Control
Quality Control Tubes
10 mL
Double Strength (DS) Control
JQaj`� "T
Single Strength (SS) Control
a VC
EC Broth Control
I
Revised 5-23-16
MPN/g= 10x 4-9

CITY OF WASHINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By 9�r�
Received By d S/- Time on water bath
Analyzed By Time in oven
Calculated By B Time out of oven
Checked By _ - L Time weighed
Sample #--
Evaporating Dish #
A
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
119a5IQ.
Wet Weight + Dish Weight
3_ S9 ,
Dish Weight
(q I6a •
Dish Weight
Wet Weight
501 &
Wet Weight
1st Dry Weight + Dish Weight
—I r.� D.-7 ,
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
—7 1 .3 DT , I
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
j
1 -1.,1
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
i��`
t
% Dry Solids ((Dry Weight / Wet
Weight) x 100)�
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By
Received By Lde 3t� 111-A-P Time on water batl
Analyzed By a-T -40 Iio?q Time in over
Calculated By �02q , Time out of over
Checked By �� a�_FD S_ /- Z Time weighec
Sample #
�
Evaporating Dish #
Sample #
Evaporating Dish #�
Wet Weight + Dish Weight
Wet Weight + Dish Weight
3("�Lj
Dish Weight
97a5Lt,9
Dish Weight
Wet Weight
Wet Weight
1st Dry Weight + Dish Weight
S TKAi9
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Q
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
o
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
C r
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
% Dry Solids ((Dry Weight / Wet
Weight) 100)
�
x
ew
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By'?
Received By9�t,= .1-7 1 2vO d5,1/ Time on water bath
Analyzed By , A . I ISL+ Time in oven
Calculated By Time out of oven
Checked By �� %! "� aZ I G%4 Time weighed
Sample #
Evaporating Dish #
ti
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
I
Wet Weight + Dish Weight
Dish Weight
1Z
Dish Weight
Wet Weight
t
Wet Weight
1 st Dry Weight + Dish Weight
L7v r
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
1 o(-\ I 'D� ,
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dish Weight (2nd - 1 st)
Dry Weight (2nd Dry Weight+ Dish
Weight Dish Weight)
Dry Weight (2nd Dry Weight+ Dish
-
1 i
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
y
% Dry Solids ((Dry Weight / Wet
Weight) 100)
x
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHINGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By °-tf37
Received By ti 9�-7 3ti
Analyzed By ,
Calculated By
Checked By
�- Time on water bath
Time in oven
11,+'Z:— Time out of oven
191, Time weighed
Sample #
Evaporating Dish #
GA
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
aq ,
Wet Weight + Dish Weight
Dish Weight
�� ,
Dish Weight
Wet Weight
SO 0
Wet Weight
1 st Dry Weight + Dish Weight
__7 ra a, i Q,_
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
19 -D,93,
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight +
0
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
= �
�`'
% Dry Solids ((Dry Weight / Wet
Weight) 100)
x
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHIGTO
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By �, �r , ' � C1
Received By Q Time on water bath
Analyzed By Lt D-Z 'D-o Time in oven
Calculated By ,14� Time out of oven
Checked By ,S 4-ac� s 7 Time weighed
Sample #
Evaporating Dish #
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
Wet Weight + Dish Weight
Dish Weight
�cl�,�
Dish Weight
Wet Weight
5WSE Q
Wet Weight
1st Dry Weight + Dish Weight
i
{
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
—7,19
2nd Dry Weight + Dish Weight
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
0
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
e
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
3^ �� D7
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By ) �D_7
Received By 1 -0­7 6 75'/- Time on water bath
Analyzed By Time in oven
Calculated By qij Time out of oven
Checked By /L Yt--ee Time weighed
Sample #
Evaporating Dish #
1 +e
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
30
Wet Weight + Dish Weight
Dish Weight
'_60S
Dish Weight
Wet Weight
Wet Weight
1 st Dry Weight + Dish Weight
C
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
C);
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
r
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
9 %,
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
I
�" '� `
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

CITY OF WASHINGTON
SLUDGE
Standard Methods 2540 G-201 1 (Aqueous)
Na Date/Time
Sampled By
Received By D-73U CSV Time on water t
Analyzed By Time in o
Calculated By i i 111 3019c) N1 Time out of o
Checked By Le, G�qL�-,c -4 S1-i-1 Time weig
Sample #
SL#-7
Evaporating Dish #
Sample #
Evaporating Dish #
Wet Weight + Dish Weight
Al 959
Wet Weight + Dish Weight
Dish Weight
11559,E
Dish Weight
Wet Weight
50 • V
Wet Weight
1 st Dry Weight + Dish Weight
�-7•�
1 st Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
2nd Dry Weight + Dish Weight
Difference in 1 st & 2nd Dry Weight +
Dish Weight (2nd - 1st).
Difference in 1st & 2nd Dry Weight +
Dish Weight (2nd - 1st)
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
s
Dry Weight (2nd Dry Weight + Dish
Weight - Dish Weight)
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
, �"•�L4 . -
% Dry Solids ((Dry Weight / Wet
Weight) x 100)
*Note -Differences should agree within 4% or 0.5 mg, which ever is less
Revised 9/26/19 JDW

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 11/06/2020
Reported: 12/15/2020
For: Washington WWTP
Comments:
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
201106-04-01 % Volatile Solids Washington 1.54 % SM2540G 11/06/2020 WC
WWTP
201106-04-01 30 Day Benchscale Washington 7.6 % EPA625-R-92/0 11/06/2020 MD
WWTP
201106-04-01 Percent Solids Washington 2.61 % SM2540B-2011 11/06/2020 WC
WWTP
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 201106-04-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Parameter Schedule:
Parameter Schedule:
Received on Ice
Received on Ice
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

Client: /!
r /
_
/�
C
STATESVILLE ANALYTICAL
Address:
rC`
122 Court Street • P.O. Box 228
Statesville,NC 28687
[phone]
Contact Person:
?
Phone #
�1
FAX#
Chain of
Custody Record
PO # Requisitioned by: (Time Date)111119.11
Customer
Sample lo#
/
Lab -ID k
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
a
Matrix
Parameters requested for analysis
w
fd� t4GJGT�+�
ij
% I We •
�I
r' 4 Pµ
O
D 4
C
Q+ggt4 rN�T
,4&
o
�L
0 Logw ?
Relinquished by:
bujReceived by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date / /_
Time end am, pm Date _/ /_
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date 1_
Time ' ar o Date&//6 202Fmpled by: o`/
Time l tJ am, joate I // Transported by
Time am, pm Date _/_/ Holding times met:
Time am, pm Date / , /�
Compliance work: V
Non-compliance work:
Lab Comments,
n
00
1.0
00
N
U
z
ai
v1
ai
N
00
N
N
X
O
m
0
d

Client:
STATESVILLE ANALYTICAL
122 CSr tesvuurt Sveetille, NCP28687 x 228
Address: �,. C �,
oC :tom -
70
[phone]
Contact Person:
o
Phone #
FAX#
Chain of
Custody Record
PO # [.tJ / 1 o 4C Requisitioned by: (Time Dale)
Customer
Sample IDM
Lab -ID #
Time Sampled
(Grab Only)
Dale Sampled
(Grab Only)
a
Matrix
swag.
Paremelers requested for analysis
Wl4t�Gi'
k1w -Ou
�} rr
�V i �iUl•
rOa
of o
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date
Time end am, pm Date
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date
_/ !_
_//
Time ''D6apm Date / I 1 .20 sampled by: &0;e
' V�14 Time L�m Date 1 l llcl Transported b
Time am, pm Date _/ �_ Holding times met: V
Time am, pm Date �/ / Compliance work:
Non-compliance work:
Lab comments:
n
W
1.0
W
N
U
z
ai
N
Ln
N
00
N
N
X
O
m
0
a-

30 Day Bench Worksheet Sample ID # 2C//OG- t7V
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
2
3
Avera e:
p- 57
768
WEEK 2
-Samples
Total Solids
Volatile Solids
% Volatile Fraction
I
a. 4
V
0.
2
e,47
3
-Q9
7
0
Average:
a, 47
7
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
I
U
- ✓��
2
3
V. 5V 7t3
Average:
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
_ Illy (0
_
5
2
-
3
_
Average:
�_
�!
8
WEEK 5
Sam les
Total Solids
Volatile Solids
% Volatile Fraction
1
4
0'
2
a!iw�.7
3
4M7
Avera e:
QQ
sly
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
_
2
-
61 7
3
Avera e:
g/
r7 -6
y
Van Kleeck Reduction: Initial % Vol, Frac. - Final % Vol Frac. X 100 = %
Initial % Vol. Frac. - ( Initial % Vol. Frac. X Final % Vol. Frac.)
FINAL RESULT t . 6
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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031360
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Client: Harvey Williamson
Advisor: Brent Collins
Predictive
Hunters Roost Farm Septic Service
EMA Resources Inc
;•
5365 US Hwy 17 N
755 Yadkinville Rd
$. Soil Report Mehlich-3 Extraction
Washington, NC 27889
Mocksville, NC 27028
Links to Helpful Information
Sampled County : Beaufort
Client ID: 282102
Advisor ID: 405413
Sampled: Received: 05/27/2020 Completed: 06/03/2020 Farm: BF210
Sample ID: 00004
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Soybean 1.0 0 0
30 0 0 0 0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.71 1.16 5.7 67 1.9 5.4 201 59 47 15
42 69 51 110 110
101 0.1 2
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Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture