WQ0014868_Residual Annual Report 2020_20210208

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0014868
Applicant/Permittee Smithfield Fresh Meats Corp
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff
Name * Brent Collins
Email Address*
[e-mail]
electronic subnittal, confirmation of receipt, and other correspondence.
Project Information
........ ......... .......................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
3363993646
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
r Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* W00014868
Has Current Existing permt number
Applicant/Permittee Address* PO Box99, Tar Heel, NC 28392
Facility Name * Smithfield Fresh Meats Corp. RLAP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Fora} Engineering Rans, Specifications, Calculations, Etc.)
2020 Smithfield Fresh Meats Annual Report -
10.38M6
WQ0014868.pdf
Upload only 1 PCF docurrent (less than 250 NE). Maniple docurrents must be combined into one FDF file unless file is larger than
upload linit.
* W By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
o 0041, W
Submission Date 2/8/2021

February 8, 2021
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2020 Annual Report — Smithfield Packing Co.
Treatment and Land Application of Residuals
Permit No. WQ0014868
Dear Sir or Madam:
Enclosed is one copy of the 2020 Annual Report for the above referenced land
application permit.
During 2020 EMA Resources, Inc. land applied 482.39 dry tons of wastewater residuals
to 460.5 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Z�fz G;2�
Brent Collins
Director of Technical Services
brent.collins(cr,,emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014868 County: Bladen Year:
Facility Name (as shown on permit): Smithfield Fresh Meats Corp.
Land Application Operator:
EMA Resources Inc.
2020
Phone: 336-75 l -1441
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the en -nit:
37
Total number of fields utilized for land application during the year:
13
Total amount of dry tons applied during the year for all application sites:
482.39
Total number of acres utilizes for land application during the year:
460.5
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. L7 Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in I SA NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 1 I 1 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donovan Owens - General Manager
Pe c Name and Titl type or print) Signature of Permittee Date
c� 2/ 1 /2021
Signature of Preparer*
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and
Date Signature of Land Applier Date
(if different from Permittee and Preparer)
15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can he reported in FORM RSSF - B
WQ Permit Number: WQ0014868
Facility Name: Smithfield Fresh Meats Corp.
Residual Source WQ # or NCO078344
NPDES #:
WWTP Name: Tarheel Plant WWTP
Residnal Analvcic Tintn
Laboratory: I ) Waypoint Analytical
2)
3)
4)
5)
Conc.
Sample or Corn osite Date
Parameter
(mg/kg)
Limit
m /k a
ESB
1/9/20
ESB
3/11/20
ESB
3/26/20
ESB
4/9/20
Average
Percent Solids (%}
NA
2.43
2.01
2.08
1.16
1.92
Arsenic
75
17.5
32.2
21
38.1
27.2
Cadmium
85
2.06
3.81
1 2.48
4.5
3.21
Copper
4.300
667
1000
476
67.8
552.7
Chromium
NA
59.6
63.8
40.5
17.3
45.3
Lead
840
31
22.9
25.00
13.5
23.1
Mercury
57
0.131
0.243
0.172
0.345
0.22
Molybdenum
75
9.21
13
7.9
11.8
10.47
Nickel
420
52.1
66.9
53.5
15
46.88
Selenium
100
20.4
37.7
24.5
44.5
31.78
Zinc
7,500 2390 3680
2190 323 2145.751
Total Phosphorus
NA 64200 92300
1 80500 13500 62625
TKN
NA 50400 45200
35100 22200 38225
Ammonia -Nitrogen
NA 12500 24800
13000 16600 16725
Nitrate and Nitrite
NA 204 362
241 444 312.75
'' For surface disposal facilities
the ceiling concentration limits listed
in this form are not annlicAlP
RPfPTPf1CP }�lP 1l ltl\,: in�i nPr,,,rt
f » mnMl
I: .:r
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penal es fo submitting Pals armation, including the possibility of fines and imprisonment for Knowing violations."
z2' f
Signature of Preparer * Date
*Preparer is defined in 40 C)=R Part 503.9(r) and 15A NCAC 2T .I 102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0014868 Laboratory: 1) Waypoint Analytical
Facility Name: Smithfield Fresh Meats Corp. 2)
Residual Source
NPDES # or WQ#:
NCO078344
WWTP Name: Tarheel Plant WWTP
Residual Analysis Data
3)
4)
5)
Sample or Com osite Date
Parameter
(mg/kg)
ESB
1/9/20
ESB
YI1120
ESB
3/26120
ESB
4/9/20
Average
Aluminum
61300
82300
78500
11600
58425
Calcium
42500
61500
60000
11100
43775
Magnesium
11800
17700
24300
7990
15447.5
pH
7
7.2
7.2
7.2
7.15
Potassium
7250
11100
7650
7550
8387.5
Sodium
25800
42800
28500
43500
35150
PAN
14034
16842
11161
9864
12975.3
SAR
4.44
5.53
3.57
8.24
5.45
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signi fit penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer-4
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
3 _W1
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
21.6 Acres Permitted: 21.6 Site #: SF03 Field #:
5.72
6.4
LaB
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
M1111m
mammon
Non
no
0
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
0.27
Arsenic
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Cadmium
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.293
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.293
Chromiuni
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Lead
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
denum
Nickel
0.025
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.025
Selenium
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Zinc
1.137
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.137
Total
Phos-
33.191
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
33.191
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 1 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 5.72 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.6
21.6
6.4
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/2
45500
1.92
0.169
Tarheel WWTP
S
4.230
NA
Bermuda
4/3
26000
1.92
0.096
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
2.417
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
7tsoo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
6.647
FO.000
Lime Applied
Annuallbs/acre
0.014
0.002
0.293
0.024
0.012
0.000
0.006
0.025
0.017
1.137 33.191
167.728
168.865
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.243
0.091
40.568
2.293
0.618
0.021
1.218
3.579
0.327
12/21
2000
Current Cumulative lbs/ac
0.257
0.093
40.861
2.317
0.630
0.021
1.224
3.604
0.344
Permitted C. P. L. R. * * * *
1 9
250
1000
1
250
1
Permit PAN Limit 1 st/2nd Crop
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
13.3 Acres Permitted:
13.3 Site #: SF03 Field #:
27.58
8.3
Cc
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
01111m
mammon
Non
no
0
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
2.07
Arsenic
0.113
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
2.293
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.293
Chromiuni
0.188
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.188
Lead
0.096
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.096
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
denum
Nickel
0.194
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.194
Selenium
0.132
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.132
Zinc
8.901
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.901
Total
Phos-
259.769
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
259.769
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 2 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 27.58 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 168
Ce
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
13.3
13.3
8.3
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/1
156000
1.92
0.939
Tarheel WWTP
S
23.553
NA
Bermuda
6/2
188500
1.92
1.135
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
28.460
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
344500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
52.013
FO.000
Lime Applied
Annuallbs/acre
0.113 0.013 2.293 0.188 0.096 0.001 0.043 0.194 0.132 8.901 259.769
0.249 0.079 45.394 1.972 0.71 0.021 1.143 3.997 0.313 169.237
0.362 0.092 47.687 2.160 0.806 0.022 1.186 4.191 0.445 178.138
1 9 250 1000 1 250 1 500
1 1 168
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
21.3 Acres Permitted: 21.3 Site #: SF03 Field #:
59.85
6.1
Cc
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.81
Arsenic
0.153
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.153
Cadmium
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Copper
3.106
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.106
Chromiuni
0.255
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.255
Lead
0.130
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.130
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
denum
Nickel
0.263
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.263
Selenium
0.179
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.179
Zinc
12.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.059
Total
Phos-
351.953
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
351.953
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 3 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 59.85 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 168
Ce
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.3
21.3
6.1
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/26
208000
1.92
0.782
Tarheel WWTP
S
19.609
NA
Bermuda
6/3
84500
1.92
0.318
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
7.966
NA
Bermuda
6/4
273000
1.92
1.026
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
25.737
NA
Bermuda
6/5
182000
1.92
0.684
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
17.158
NA
Bermuda
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
747500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
70.470
0.005
Lime Applied
Annuallbs/acre
0.153 0.018 3.106 0.255 0.130 0.001 0.059 0.263 0.179 12.059 351.953 1
0.218 0.088 37.937 1.527 0.55 0.017 0.923 3.1 0.269 139.101
0.371 0.106 41.043 1.782 0.680 0.018 0.982 3.363 0.448 151.160
1 9 250 1000 1 250 1 500
1 168
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Cro
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
19 Acres Permitted:
19 Site #: SF03 Field #:
17.18
9.8
0
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.90
Arsenic
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.999
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.999
Chromium
0.082
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.082
Lead
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
denum
Nickel
0.085
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.085
Selenium
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Zinc
3.880
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.880
Total
Phos-
113.226
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
113.226
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 4 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 17.18 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Corn
Predominant Soil Series:
Crop 1 Max. PAN: 150
Wh
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
19
19
9.8
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/7
214500
1.92
0.904
Tarheel WWTP
S
1 22.670
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
214500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
22.670
0.000
Lime Applied
Annuallbs/acre
0.049
0.006
0.999
0.082
0.042
0.000
0.019
0.085
0.057
3.880 113.2261
85.896
89.776
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.101
0.049
16.364
1.555
0.291
0.011
0.631
1.894
0.128
Current Cumulative lbs/ac
0.150
0.055
17.363
1.637
0.333
0.011
0.650
1.979
0.185
Permitted C. P. L. R. * * * *
1 9
250
1000
1
250
1
Permit PAN Limit 1 st/2nd Crop
1 150
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
Acres Permitted:
Site #: SF03 Field #:
16.66
7.8
LaB
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
2.08
Arsenic
0.113
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
2.301
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.301
Chromiuni
0.189
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.189
Lead
0.096
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.096
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
denum
Nickel
0.195
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.195
Selenium
0.132
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.132
Zinc
8.935
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.935
Total
Phos-
260.771
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
260.771
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 5 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 16.66 Site #: SF03 Acres Permitted:
Steve Dunham
Crop 1 Name: Bermuda -Pasture
Predominant Soil Series:
Crop 1 Max. PAN: 147
LaB
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
8
8
7.8
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
6/2
45500
1.92
0.455
Tarheel WWTP
S
11.421
NA
Bermuda
6/3
162500
1.92
1.626
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
40.788
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
2os000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
52.209
FO.000
Lime Applied
Annuallbs/acre
0.113
0.013
2.301
0.189
0.096
0.001
0.044
0.195
0.132
8.935 260.771 1
103.195
112.130
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.172
0.069
27.348
1.302
0.347
0.013
0.687
2.187
0.223
Current Cumulative lbs/ac
0.285
0.082
29.649
1.491
0.443
0.014
0.731
2.382
0.355
Permitted C. P. L. R. * * * *
1 9
250
1000
1
250
1
Permit PAN Limit 1 st/2nd Crop
1
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
67.62
9.8
Operator: Vance Tyson Owner: Vance Tyson Predominant Soil Series: De
Acres Used: 79 Acres Permitted: 79 Site #: SF06 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.86
Arsenic
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Cadmium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.946
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.946
Chromium
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Lead
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
denum
Nickel
0.080
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.080
Selenium
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Zinc
3.674
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.674
Total
Phos-
107.214
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
107.214
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp.
Vance Tyson
Operator: Vance Tyson
Crop 1 Name: Corn
WQ Permit #: WQ0014868 Field #:
Annual Dry Tons Applied: 67.62 Site #:
Predominant Soil Series: De
Crop 1 Max. PAN:
120
Crop 2 Name:
Acres Utilized: 79
SF06 Acres Permitted: 79
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/8
169000
1.92
0.171
Tarheel WWTP
S
4.296
NA
Corn
4/15
182000
1.92
0.184
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.626
NA
Corn
4/16
201500
1.92
0.204
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
5.122
NA
Corn
4/17
221000
1.92
0.224
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
5.617
NA
Corn
4/18
1
71500
1.92
0.072
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
1.817
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
o
ss000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
1 21.478
o.000
Lime Applied
Annuallbs/acre
0.047
0.005
0.946
0.078
0.040
0.000
0.018
0.080
0.054
3.674 107.2141
49.753
53.427
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.052
0.031
13.454
0.424
0.202
0.005
0.305
1.665
0.057
2000
Current Cumulative lbs/ac
0.099
0.036
14.400
0.502
0.242
0.005
0.323
1.745
0.111
Permitted C. P. L. R. * * * *
1
1 9
250
1000
250
1
Permit PAN Limit 1 st/2nd Crop
1
1 120
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/l/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
40.58
5.3
Operator: Vance Tyson Owner: Vance Tyson Predominant Soil Series: De
Acres Used: 77 Acres Permitted: 77 Site #: SF06 Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.53
Arsenic
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.583
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.583
Chromium
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Lead
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
denum
Nickel
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Selenium
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Zinc
2.262
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.262
Total
Phos-
66.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
66.007
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp.
Vance Tyson
Operator: Vance Tyson
Crop 1 Name: Corn
WQ Permit #: WQ0014868 Field #:
Annual Dry Tons Applied: 40.58 Site #:
Predominant Soil Series: De
Crop 1 Max. PAN:
120
Crop 2 Name:
Acres Utilized: 77
SF06 Acres Permitted: 77
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/18
71500
1.92
0.074
Tarheel WWTP
S
1.865
NA
Corn
4/19
201500
1.92
0.210
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
5.255
NA
Corn
4/22
234000
1.92
0.243
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
6.102
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
o
So7000
As
Cd
Cu
Cr
Pb
Hg,
Mo
Ni
Se
Zn
P
13.222
o.000
Lime Applied
Annuallbs/acre
0.029 0.003 0.583 0.048 0.024 0.000 0.011 0.049 0.033 2.262 66.007
0.0155 0.0103 2.4683 0.3829 0.0543 0.0021 0.1125 0.3493 0.0259 13.8421
0.044 0.014 3.051 0.431 0.079 0.002 0.124 0.399 0.059 16.104
1 1 9 250 1000 250 500
1 1 120
Date
lbs/ac
Prior Years Cumulative lbs/ac
2000
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/l/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Richard Dunham Owner: Bonnie Meeker Predominant Soil Series:
Acres Used: 21.3 Acres Permitted: 21.3 Site #: SF07 Field #:
28.09
5.9
WmB
9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.32
Arsenic
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.458
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.458
Chromiuni
0.120
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.120
Lead
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
denum
Nickel
0.124
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.124
Selenium
0.084
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.084
Zinc
5.660
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.660
Total
Phos-
165.205
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
165.205
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp.
Bonnie Meeker
Operator: Richard Dunham
Crop 1 Name: Bermuda -Pasture
WQ Permit #: WQ0014868 Field #:
Annual Dry Tons Applied: 28.09 Site #:
Predominant Soil Series: WmB
Crop 1 Max. PAN:
210
Crop 2 Name:
9 Acres Utilized: 21.3
SF07 Acres Permitted: 21.3
Cation Exchange Capacity (non 503): 5.9
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/4
71500
1.92
0.269
Tarheel WWTP
S
6.741
NA
Bermuda
4/6
234000
1.92
0.880
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
22.060
NA
Bermuda
4/7
45500
1.92
0.171
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.289
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
3st000
As
Cd
Cu
Cr
Pb
Hg,
Mo
Ni
Se
Zn P
33.090
o.000
Lime Applied
Annuallbs/acre
0.072
0.008
1.458
0.120
0.061
0.001
0.028
0.124
0.084
5.660 165.205
152.101
157.761
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.235
0.108
34.323
4.029
0.779
0.018
1.071
3.307
0.29
2000
Current Cumulative lbs/ac
0.307
0.116
35.781
4.149
0.840
0.019
1.099
3.431
0.374
Permitted C. P. L. R. * * * *
1
1 9
250
1000
250
Permit PAN Limit 1 st/2nd Crop
1
1 210
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/l/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Hinton King Owner: Linda King/Sheila Sellers Predominant Soil Series:
Acres Used: 7.5 Acres Permitted: 7.5 Site #: SF08 Field #:
7.28
4.0
GoA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
MWE
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
1 C
11
12
DT/Ac./
App.
Event
0.97
Arsenic
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.073
Chromiuni
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
Lead
0.045
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
denum
Nickel
0.091
0.000
0.000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.091
Selenium
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Zinc
4.167
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.167
Total
Phos-
121.618
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
121.618
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 1 Acres Utilized:
Linda King/Sheila Sellers Annual Dry Tons Applied: 7.28 Site #: SF08 Acres Permitted:
Hinton King
Crop 1 Name: Corn
Predominant Soil Series:
Crop 1 Max. PAN: 147
GoA
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
7.5
7.5
4.0
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/31
91000
1.92
0.971
Tarheel WWTP
S
1 24.364
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
9t000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
24.364
0.000
Lime Applied
Annuallbs/acre
0.053
0.006
1.073
0.088
0.045
0.000
0.020
0.091
0.062
4.167 171.6181
28.7325
32.900
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.0296
0.0093
5.9376
0.7369
0.0973
0.0037
0.2085
0.6114
0.0505
Current Cumulative lbs/ac
0.082
0.016
7.011
0.825
0.142
0.004
0.229
0.702
0.112
Permitted C. P. L. R. * * * *
1 9
250
1000
1
250
1
Permit PAN Limit 1 st/2nd Crop
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Hinton King Owner: Linda King/Sheila Sellers Predominant Soil Series:
Acres Used: 17 Acres Permitted: 17 Site #: SF08 Field #:
16.13
4.8
GoA
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.95
Arsenic
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.052
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.049
Chromiuni
0.086
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Lead
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.044
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
denum
Nickel
0.089
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Selenium
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.060
Zinc
4.073
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.073
Total
Phos-
118.862
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
118.862
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 2 Acres Utilized:
Linda King/Sheila Sellers Annual Dry Tons Applied: 16.13 Site #: SF08 Acres Permitted:
Hinton King
Crop 1 Name: Corn
Predominant Soil Series:
Crop 1 Max. PAN: 147
GoA
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
17
17
4.8
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/30
117000
1.92
0.551
Tarheel WWTP
S
13.820
NA
Corn
3/31
84500
1.92
0.398
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
9.981
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
2otsoo
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
23.801
FO.000
Lime Applied
Annuallbs/acre
0.052
0.006
1.049
0.086
0.044
0.000
0.020
0.089
0.060
4.073 118.862
29.2731
33.346
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.0288
0.0093
6.0937
0.7202
0.1002
0.0037
0.2147
0.614
0.0529
Current Cumulative lbs/ac
0.080
0.015
7.143
0.806
0.144
0.004
0.235
0.703
0.113
Permitted C. P. L. R. * * * *
1 9
250
1000
1
250
1
Permit PAN Limit 1 st/2nd Crop
1
1 147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/1/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Hinton King Owner: Elizabeth King/Hinton Kind Predominant Soil Series:
Acres Used: 89.5 Acres Permitted: 89.5 Site #: SF08 Field #:
112.95
4.4
MaA
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.26
Arsenic
0.069
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.395
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.395
Chromiuni
0.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.114
Lead
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
denum
Nickel
0.118
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Selenium
0.080
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.080
Zinc
5.416
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.416
Total
Phos-
158.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
158.066
horus
1
1
1
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 3 Acres Utilized:
Elizabeth King/Hinton King Annual Dry Tons Applied: 112.95 Site #: SF08 Acres Permitted:
Hinton King
Crop 1 Name: Corn
Predominant Soil Series:
Crop 1 Max. PAN: 120
MaA
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
89.5
89.5
4.4
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/16
117000
1.92
0.105
Tarheel WWTP
S
2.625
NA
Corn
3/18
201500
1.92
0.180
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.521
NA
Corn
3/19
188500
1.92
0.169
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.229
NA
Corn
3/20
110500
1.92
0.099
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
2.479
NA
Corm
3/27
1
240500
1 1.92
0.215
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
5.396
NA
Corn
3/28
208000
1.92
0.186
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.667
NA
Corn
3/29
234000
1.92
0.209
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
5.250
NA
Corn
3/30
110500
1.92
0.099
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
2.479
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
0
1410500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
31.646
F0. 000
Lime Applied
Annuallbs/acre
0.069 0.008 1.395 0.114 0.058 0.001 0.026 0.118 0.080 5.416 158.066
0.053 0.026 10.573 1.377 0.187 0.007 0.34 1.132 0.091 50.284
0.122 0.034 11.968 1.491 0.245 0.008 0.366 1.250 0.171 55.700
1 1 9 250 1000 1 250 1 500
1 1 120
Date
lbs/ac
Prior Years Cumulative lbs/ac
2/20
2000
Current Cumulative lbs/ac
Permitted C. P. L. R. * * * *
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/l/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Hinton King Owner: Elizabeth King/Hinton Kind Predominant Soil Series:
Acres Used: 64.5 Acres Permitted: 64.5 Site #: SF08 Field #:
60.37
4.9
NoA
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
0.94
Arsenic
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.051
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.035
Chromiuni
0.085
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.085
Lead
0.043
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
denum
Nickel
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
Selenium
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Zinc
4.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.017
Total
Phos-
117.234
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
117.234
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #:
Elizabeth King/Hinton King Annual Dry Tons Applied: 60.37 Site #:
Operator: Hinton King
Crop 1 Name: Corn
4 Acres Utilized: 64.5
SF08 Acres Permitted: 64.5
Predominant Soil Series: NoA Cation Exchange Capacity (non 503): 4.9
Crop 1 Max. PAN:
131
Crop 2 Name:
Crop 2 Max. PAN:
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/10
130000
1.92
0.161
Tarheel WWTP
S
4.047
NA
Corn
3/11
136500
1.92
0.169
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.250
NA
Corn
3/12
136500
1.92
0.169
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
4.250
NA
Corn
3/13
214500
1.92
0.266
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
6.678
NA
Corn
3/14
1
71500
1.92
0.089
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
2.226
NA
Corn
3/16
65000
1.92
0.081
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
2.024
NA
Corn
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
754000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
23.474
F0. 000
Lime Applied
Annuallbs/acre
0.051
0.006
1.035
0.085
0.043
0.000
0.020
0.088
0.059
4.017 117.234
37.109
41.126
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.038
0.019
7.334
0.567
0.131
0.005
0.271
0.741
0.068
2/20
2000
Current Cumulative lbs/ac
0.089
0.025
8.369
0.652
0.174
0.005
0.291
0.829
0.127
Permitted C. P. L. R. * * * *
1
1 9
250
1000
1
250
1
Permit PAN Limit 1 st/2nd Crop
1
1 131
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/l/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
22.38
7.7
Operator: Hinton King Owner: Hinton King Predominant Soil Series: NoA
Acres Used: 21.5 Acres Permitted: 21.5 Site #: SF08 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
OWN
Total
Phos-
phonisMENEENEENEEN
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
LOJ
11
12
DT/Ac./
App.
Event
1.04
Arsenic
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.151
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.151
Chromiuni
0.094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.094
Lead
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
denum
Nickel
0.098
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.098
Selenium
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Zinc
4.467
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.467
Total
Phos-
130.385
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
130.385
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�fz 4; 2/l/2021
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 6 Acres Utilized:
Hinton King Annual Dry Tons Applied: 22.38 Site #: SF08 Acres Permitted:
Hinton King
Crop 1 Name: Corn
Predominant Soil Series:
Crop 1 Max. PAN: 125
NoA
Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.5
21.5
7.7
O
N
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Dry
Precip.
Past 24
Hrs.
inches
<.5"
a
F '5
w
*
o
o'
0.5
7�
* N
o
0.2
TKN
mg/kg
36050
o
mg/kg
16725
Nitrate
and
Nitrite
mg/kg
312.75
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
3/31
32500
1.92
0.121
Tarheel WWTP
S
3.035
NA
Corn
4/3
182000
1.92
0.678
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
16.998
NA
Corn
4/4
65000
1.92
0.242
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
36050
16725
312.75
6.071
NA
Corn
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications
totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
0
27950o
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
26.105
0.000
Lime Applied
Annuallbs/acre
0.057
0.007
1.151
0.094
0.048
0.000
0.022
0.098
0.066
4.467 130.385
28.7325
33.200
500
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.0296
0.0093
5.9376
0.7369
0.0973
0.0037
0.2085
0.6114
0.0505
2/20
2000
Current Cumulative lbs/ac
0.086
0.016
7.088
0.831
0.145
0.004
0.230
0.709
0.117
Permitted C. P. L. R. * * * *
9
250
1000
250
Permit PAN Limit 1 st/2nd Crop
125
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/l/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
1 /22/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-010-0058
Client Project Description: Smithfield Tar Hill
2790 Whitten Road, Memphis, TIN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/10/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
Mississippi California #2904
Kentucky #90047 Tennessee #TN02027
VA NELAP #460181
NC #415
EPA #TN00012
Texas #T104704180 Arkansas #88-0650
Oklahoma #9311 SC #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 7

Waypoint
ANALYTICAL
Report Number: 20-010-0058
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Client Project Description: Smithfield Tar Hill
Lab No Client Sample ID
Matrix Date Collected Date Received
92902 Smithfield Tar Heel ESB Solids 01/09/2020 09:00 01/10/2020
Page 2 of 7

Waypoint
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield Tar Hill
Lab Report Number: 20-010-0058
Date: 1/22/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 92916
Analyte: Aluminum
QC Batch No: L472729
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92902 (Smithfield Tar Heel ESB)
Analyte: Lead
QC Batch No: L472729/L472416
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 3 of 7

i
Wa2790 Whitten Road, Memphis, TN 38133
ypoint.Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Smithfield Tar Hill Report Date : 01/22/2020
755 Yadkinville Rd Information : Received : 01/10/2020
Mocksville , NC 27028
Report Number : 20-010-0058 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 92902
Matrix: Solids
Sample ID : Smithfield Tar Heel ESB
Sampled:
1/9/2020
9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.6
%
0.010
1
01/13/20 16:26
ADM
SW-DRYWT
Ammonia Nitrogen
12500
mg/Kg -
dry
1040
1
01/21/20 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<204
mg/Kg -
dry
204
204
1
01/20/20 16:10
ZBD
4500NO3F-2011
Organic N
37960
mg/Kg -
dry
72.50
3617
1
01/14/20 16:16
CALCULATION
pH
7.0
S.U.
1
01/21/20 05:24
JSL
9045D
Total Solids
2.43
%
0.010
0.010
1
01/13/20 16:26
ADM
2540G-2011
Total Volatile Solids
49.9
%
0.010
0.010
1
01/13/20 16:26
ADM
2540G-2011
Total Kjeldahl Nitrogen
50400
mg/Kg -
dry
3620
1
01/14/20 16:16
CLP 4500NORGD-2011
Phosphorus
64200
mg/Kg -
dry
107
208
1
01/14/20 02:23
BKN
6010D
Aluminum
61300
mg/Kg -
dry
84.6
208
1
01/14/20 02:23
BKN
6010D
Arsenic
<17.5
mg/Kg -
dry
17.5
20.8
1
01/14/20 02:23
BKN
6010D
Cadmium
<2.06
mg/Kg -
dry
2.06
4.17
1
01/14/20 02:23
BKN
6010D
Calcium
42500
mg/Kg -
dry
700
1040
1
01/14/20 02:23
BKN
6010D
Chromium
59.6
mg/Kg -
dry
7.92
10.4
1
01/14/20 02:23
BKN
6010D
Copper
667
mg/Kg -
dry
6.04
10.4
1
01/14/20 02:23
BKN
6010D
Iron
11100
mg/Kg -
dry
177
208
1
01/14/20 02:23
BKN
6010D
Lead
<31.0
mg/Kg -
dry
31.0
62.5
5
01/14/20 16:51
BKN
6010D
Magnesium
11800
mg/Kg -
dry
92.5
208
1
01/14/20 02:23
BKN
6010D
Manganese
679
mg/Kg -
dry
7.63
20.8
1
01/14/20 02:23
BKN
6010D
Mercury
<0.131
mg/Kg -
dry
0.131
0.596
1
01/15/20 16:18
TJS
7471A
Molybdenum
9.213
mg/Kg -
dry
5.42
10.4
1
01/14/20 02:23
BKN
6010D
Nickel
52.1
mg/Kg -
dry
6.88
10.4
1
01/14/20 02:23
BKN
6010D
Potassium
7250
mg/Kg -
dry
124
208
1
01/14/20 02:23
BKN
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 4 of 7

i
Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-010-0058
Lab No : 92902
Sample ID : Smithfield Tar Heel ESB
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield Tar Hill
Information :
REPORT OFANALYSIS
Report Date : 01/22/2020
Received : 01/10/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/9/2020 9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<20.4
mg/Kg -
dry
20.4
20.8
1
01/14/20 02:23
BKN
6010D
Sodium
25800
mg/Kg -
dry
322
1040
1
01/14/20 02:23
BKN
6010D
Zinc
2390
mg/Kg -
dry
45.0
52.1
1
01/14/20 02:23
BKN
6010D
Sulfur
14800
mg/Kg -
dry
204
208
1
01/14/20 02:23
BKN
6010D
Sodium Absorption Ratio
4.41
Ratio
2.22
5.00
1
01/14/20 02:23
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 5 of 7

•
WayPAoi nt ..(2) 2790 Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 9fl1.213.2400 °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-010-0058
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#70
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: rRory Phillips Date & Time: 01/10/2020 10:48:28
Page 6 of 7

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #45245
755 Yadkinviile Rd
Mocksville, NC 27028
Project Description
Project/Site Location {City/State)
RUSH - Additional charges apply
Me d of Shl ment
Matrix Key
1 +
j
it I
Special Detection Limit(s)
Date Results Needed
Fed Ex UPS OUSPS
Courier Client Drop Off
wW - Wastewater GW - Groundwater
DW - Drinking Water 5 - Soil /Solid 0- ail
' y
P - Product M - Mis[
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID p
336-399-3646
#[e-mail]
Z
0
A Cool a SRC NQ5203 (Micro Only)
W
�
O
_
-
a Cool s= 6C
/'�
Waypoi nt
C H2SO4 pHQ
x
a
p
M
O
D None Required
ANALYTICAL
o
°
c
(J)
r^
UJ
F N&OH p6i�lU
2790 Whitten Road
Unless
cJ
w
U
M
Q
D
T
V J
U
F HN[i3 pH�2
G HCL pHr2
Memphis TN 38133
noted, all containers
ct
a
Z
@
H H3PC14
(901 ) 213.24pri
per Table Il of 4t7 CFR Part
E
-
a)�
�
10
�
�
r '
LJ
pH<2
I Cool <= 6C NA25203
136.
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a
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`
Date
Tim4i,
5 a mp le Identification
Required
Analysis I Preservative
Comments/Notes
g:oo
% c5,
I
✓
MetaIs:A1,As,Ca,Cd,Cr,Cu,Fe.Pb
µc ��EU �
Mn, Mg,Mo, Hg,Ni,Se, Na, P,S, K,Zn
IIII Il II ICI Illll Illll IIIN lul IIIIII Ill I IIIII Illu III IIII 6�
2020
EMA Resources Inc TO-47 58
Smdhvdie Tar Hill
For Laboratory Use Only
Sa [Na - Print)
oy sr.�
Client Remarks/Comments
Sludge Samples -Report Dry Weight
Ice-
Custody
Lab Comments
Seals
Relin i e TORE]
O t Time
Receive by: {SIGNATURE}
Date Time
�J N
Slank� ooler Temp 1
R nquis b : (SIGN E]
a e Time
Receive y: IG TURE]
Date Time
Iry�
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Relinquished by: [SIGNATURE]
Date Time
Rece : (SIG A RE)
J
Date Tithe
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Page 7 of 7

Waypointo
ANALYTICAL
3/24/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-072-0025
Client Project Description: Smithfield ESB
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 3/12/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
ne:C
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/28/2021
Arizona
State Program
AZ0816
8/30/2020
Arkansas
State Program
88-0650
2/7/2021
California
State Program
2904
5/10/2020
Georgia
State Program
C044
5/10/2020
Georgia
State Program
04015
6/30/2020
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
6/30/2020
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
04015
6/30/2020
Mississippi
State Program
MS
5/10/2020
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
8/31/2020
Pennsylvania
State Program
- NELAP
68-03195
5/31/2020
South Carolina
State Program
84002
5/10/2020
South Carolina
State Program
84002
6/30/2020
Tennessee
State Program
02027
2/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
9/30/2020
Virginia
State Program
- NELAP
460181
9/14/2020
Washington
State Program
C1018
7/31/2020
Page 1 of 1 00001/20-072-0025
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 20-072-0025
Client Project Description: Smithfield ESB
Lab No Client Sample ID
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
94801 Smithfield ESB - Sludge Solids 03/11/2020 06:00 03/12/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield ESB
Lab Report Number: 20-072-0025
Date: 3/24/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Total, Fixed, and Volatile Solids Method 254OG-2011
Analyte: Total Volatile Solids
QC Batch No: L482576
Relative percent difference (RPD) for the duplicate analysis was outside of the allowable quality control limits.
The sample and duplicate results are less than ten percent. At this level, RPD is not applicable. The data is
considered to be acceptable.
Page 4 of 8

WayP
�'��' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalyiical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Smithfield ESB Report Date : 03/24/2020
755 Yadkinville Rd Information : Received : 03/12/2020
Mocksville , NC 27028
Q�ln
Report Number : 20-072-0025 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 94801
Matrix: Solids
Sample ID : Smithfield ESB - Sludge
Sampled:
3/11/2020
6:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.7
%
1
03/20/2017:10
JDT
SW-DRYWT
Ammonia Nitrogen
24800
mg/Kg -
dry
1920
1
03/23/20 11:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<362
mg/Kg -
dry
362
362
1
03/18/20 09:57
ZBD
4500NO3F-2011
Organic N
20380
mg/Kg -
dry
7692
1
03/23/20 11:00
CALCULATION
pH
7.2
S.U.
1
03/23/20 05:12
JSL
9045D
Total Solids
2.01
%
0.010
0.010
1
03/16/20 17:35
ADM
2540G-2011
Total Volatile Solids
50.4
%
0.010
0.010
1
03/16/20 17:35
ADM
2540G-2011
Total Kjeldahl Nitrogen
45200
mg/Kg -
dry
7690
1
03/24/20 12:36
ZBD 4500NORGD-2011
Phosphorus
92300
mg/Kg -
dry
198
385
1
03/17/20 20:46
KKM
6010D
Aluminum
82300
mg/Kg -
dry
156
385
1
03/17/20 20:46
KKM
6010D
Arsenic
<32.2
mg/Kg -
dry
32.2
38.5
1
03/17/20 20:46
KKM
6010D
Cadmium
<3.81
mg/Kg -
dry
3.81
7.69
1
03/17/20 20:46
KKM
6010D
Calcium
61500
mg/Kg -
dry
1290
1920
1
03/17/20 20:46
KKM
6010D
Chromium
63.8
mg/Kg -
dry
14.6
19.2
1
03/17/20 20:46
KKM
6010D
Copper
1000
mg/Kg -
dry
11.2
19.2
1
03/17/20 20:46
KKM
6010D
Iron
17700
mg/Kg -
dry
326
385
1
03/17/20 20:46
KKM
6010D
Lead
22.93
mg/Kg -
dry
11.5
23.1
1
03/17/20 20:46
KKM
6010D
Magnesium
17700
mg/Kg -
dry
171
385
1
03/17/20 20:46
KKM
6010D
Manganese
1000
mg/Kg -
dry
14.1
38.5
1
03/17/20 20:46
KKM
6010D
Mercury
<0.243
mg/Kg -
dry
0.243
1.10
1
03/18/20 12:12
TJS
7471A
Molybdenum
13.03
mg/Kg -
dry
10.0
19.2
1
03/17/20 20:46
KKM
6010D
Nickel
66.9
mg/Kg -
dry
12.7
19.2
1
03/17/20 20:46
KKM
6010D
Potassium
11100
mg/Kg -
dry
229
385
1
03/17/20 20:46
KKM
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-072-0025
Lab No : 94801
Sample ID : Smithfield ESB - Sludge
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield ESB
Information :
REPORT OFANALYSIS
Report Date : 03/24/2020
Received : 03/12/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 3/11/2020 6:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<37.7
mg/Kg - dry
37.7
38.5
1
03/17/20 20:46
KKM
6010D
Sodium
42800
mg/Kg - dry
594
1920
1
03/17/20 20:46
KKM
6010D
Zinc
3680
mg/Kg - dry
83.1
96.2
1
03/17/20 20:46
KKM
6010D
Sulfur
21800
mg/Kg - dry
376
385
1
03/17/20 20:46
KKM
6010D
Sodium Absorption Ratio
4.46
Ratio
2.22
5.00
1
03/17/20 20:46
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-072-0025
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T90
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: IHannah R. Brown Date & Time: 03/12/2020 11:31:31
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
MOcksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSH — Additionalcharges apply
Method of Shipment
Matrix Key
Special Detection Limits)
Fed Ex UPS �USPS
WW — Wastewater GW —Groundwater
Date Results Needed
Courier Client Drop Off
DW — Drinking Water S — Soil /Solid 0 — Oil
P - Product M - Misc
Other
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID Of
336-399-3646
brent.coil ins@emarescurces-com
Z
N
A COOT < 10C Na25203 1Micro Only]
t2
°:
C
0
-0
B Cool <= &C
Waypoi„
n
r
p
C HZSa4 pH�2
,1
ro
v
ae
a
p
lw
C13
Q
D None Required
ANALYTICAL
�
$
E
�
E
a]
O
W
r�
W
E NaDH pH>10
2790 WhlttCn Road
Unless noted, all containers
a
�j
N
(4
Q
Z
C�
U
F HNO3 pH<2
G HCL pH'2
Memphis. I'N 38133
a
o
>
H H3PO4
[phone]
per Table 11 of 40 CFR Part
x
ro
.r
pk<2
I Cool <- 6C NA25203
136.
2
F—
2
V
DatF
Time
Sample Identification
Required
Analysis I Preservative
Comments/Notes
310
&Ww"
/
51 Jr
C
✓
,�
✓
,!
,/
✓
Metals :Al,As,Ca.Cd.Cr, Cu, Fe, Pb
Mn, Mg • Mo, Hg, N i, Se, Na, P,S. K,Zn
�2 zo02o5
EMA Resources Inc 11.28.20
Smithfield ESB
For Laboratory Use Only
Sampled by (Name — Print)
gf-e4f 411�r
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
Custody
Seals
Lab Comments
�F1�} N
Lam'
Relin uished by-. (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
)c
Bla Coa� emp
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
[► a L..
Relinquished by: (SIGNATURE)
Date Time
Re . ed by: (51 NATURE)
Date Tim

Waypointo
ANALYTICAL
4/6/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-087-0069
Client Project Description: Smithfield Tar Heel
Tar Heel, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 3/27/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/28/2021
Arizona
State Program
AZ0816
8/30/2020
Arkansas
State Program
88-0650
2/7/2021
California
State Program
2904
5/10/2020
Georgia
State Program
C044
5/10/2020
Georgia
State Program
04015
6/30/2020
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
6/30/2020
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
04015
6/30/2020
Mississippi
State Program
MS
5/10/2020
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
8/31/2020
Pennsylvania
State Program
- NELAP
68-03195
5/31/2020
South Carolina
State Program
84002
5/10/2020
South Carolina
State Program
84002
6/30/2020
Tennessee
State Program
02027
2/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
9/30/2020
Virginia
State Program
- NELAP
460181
9/14/2020
Washington
State Program
C1018
7/31/2020
Page 1 of 1 00001/20-087-0069
Page 2 of 8

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 20-087-0069
Client Project Description: Smithfield Tar Heel
Tar Heel, NC
Lab No Client Sample ID
99233 Smithfield Tar Heel ESB
Matrix Date Collected
Solids 03/26/2020 08:00
Date Received
03/27/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield Tar Heel
Lab Report Number: 20-087-0069
Date: 4/6/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 99233 (Smithfield Tar Heel ESB)
Analyte: Aluminum
QC Batch No: L484764/L484432
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L484764/L484432
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L484764/L484432
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L484764/L484432
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

WayP
�'��' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalyiical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Smithfield Tar Heel Report Date : 04/06/2020
755 Yadkinville Rd Information : Tar Heel, NC Received : 03/27/2020
Mocksville , NC 27028
Q�ln
Report Number : 20-087-0069 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 99233
Matrix: Solids
Sample ID : Smithfield Tar Heel ESB
Sampled:
3/26/2020
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.0
%
1
03/30/2011:25
JDT
SW-DRYWT
Ammonia Nitrogen
13000
mg/Kg -
dry
1250
1
04/06/20 13:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<241
mg/Kg -
dry
241
241
1
04/01/20 14:37
ZBD
4500NO3F-2011
Organic N
22050
mg/Kg -
dry
93.50
4680
1
04/06/20 13:30
CALCULATION
pH
7.2
S.U.
1
04/06/20 05:45
JSL
9045D
Total Solids
2.08
%
0.010
0.010
1
03/30/20 16:43
ADM
2540G-2011
Total Volatile Solids
44.2
%
0.010
0.010
1
03/30/20 16:43
ADM
2540G-2011
Total Kjeldahl Nitrogen
35100
mg/Kg -
dry
4680
1
04/06/20 14:38
CLP 4500NORGD-2011
Phosphorus
80500
mg/Kg -
dry
129
250
1
03/30/20 23:36
KKM
6010D
Aluminum
78500
mg/Kg -
dry
102
250
1
03/30/20 23:36
KKM
6010D
Arsenic
<21.0
mg/Kg -
dry
21.0
25.0
1
03/30/20 23:36
KKM
6010D
Cadmium
<2.48
mg/Kg -
dry
2.48
5.00
1
03/30/20 23:36
KKM
6010D
Calcium
60000
mg/Kg -
dry
840
1250
1
03/30/20 23:36
KKM
6010D
Chromium
40.5
mg/Kg -
dry
9.50
12.5
1
03/30/20 23:36
KKM
6010D
Copper
476
mg/Kg -
dry
7.25
12.5
1
03/30/20 23:36
KKM
6010D
Iron
11300
mg/Kg -
dry
212
250
1
03/30/20 23:36
KKM
6010D
Lead
25.0
mg/Kg -
dry
7.45
15.0
1
03/30/20 23:36
KKM
6010D
Magnesium
24300
mg/Kg -
dry
111
250
1
03/30/20 23:36
KKM
6010D
Manganese
600
mg/Kg -
dry
9.15
25.0
1
03/30/20 23:36
KKM
6010D
Mercury
<0.172
mg/Kg -
dry
0.172
0.780
1
04/01/20 11:43
DDB
7471A
Molybdenum
7.853
mg/Kg -
dry
6.50
12.5
1
03/30/20 23:36
KKM
6010D
Nickel
53.5
mg/Kg -
dry
8.25
12.5
1
03/30/20 23:36
KKM
6010D
Potassium
7650
mg/Kg -
dry
149
250
1
03/30/20 23:36
KKM
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-087-0069
Lab No : 99233
Sample ID : Smithfield Tar Heel ESB
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield Tar Heel
Information : Tar Heel, NC
REPORT OFANALYSIS
Report Date : 04/06/2020
Received : 03/27/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 3/26/2020 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<24.5
mg/Kg - dry
24.5
25.0
1
03/30/20 23:36
KKM
6010D
Sodium
28500
mg/Kg - dry
386
1250
1
03/30/20 23:36
KKM
6010D
Zinc
2190
mg/Kg - dry
54.0
62.5
1
03/30/20 23:36
KKM
6010D
Sulfur
15500
mg/Kg - dry
245
250
1
03/30/20 23:36
KKM
6010D
Sodium Absorption Ratio
3.50
Ratio
2.22
5.00
1
03/30/20 23:36
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-087-0069
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
® UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
#45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: lKristinaA. McAdams Date & Time: 03/27/2020 12:01:38
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (City/State)
RUSH - Additional charges apply
Method of Shipment
Matrix Key
Special Detection Limit(s)
❑ Fed Ex OuPs ElusPS
WW -wastewater GW - Groundwater
r��
!++ lat
Sm'-rT(frZ(-�
Imo,,
�R C
Date Results Needed
Courier Client Prop Off
❑ ❑
OW - Drinking Water S - Soil /Solid 0 - Oil
AR f
11
f [ ��
�
P - Product M - Misc
Other
Project Number
Project Manager Phone q
Project Manager Email
Purchase Order Number
Site/Facllity ID q
336-399-3646
[e-mail]
G
M
Z
(n
A Cool c 10C Na25203 (Micro Only)
Wa�',
(IJ
y
�=
o
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8 Cool cz 6C
C H2504 pHs2
!�
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ANALYTICAL
m
c
o
>t
°
°a
E
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E
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�/
LIJ
D None Required
E NaOH pi-1a10
2790 Whitten Koad
Unless noted, all containers
`�
°
V
N
Q
a
ro
V 1
F HNO3 pH42
G HCt pHc2
Memphis, TN 38133
Z
i0
A.-
T
>
(9[]1) 213-29DD
per Table II of 40 CFR Part
E
x
H COOOQ 6C NA25203
136.
�
m
C7
Date
Time
Sample Identification
r Required
alysis / Preservati
CommentS/Notes
51X 7141ZA - C
GV1
V1Metals:Al,As,Ca.Cd,Cr,Cu.Fe,Pb
M n, Mg , Mo, Hg . N i, Se, N a. P , S, K, Zn
� 6�;�9
1�1i41�11N41111111i1�111�1�1«�I�III���l�1��11111���
EMA Resources Irrc
Smrthrietd Tar Heel
]==T7
For laboratory Use Only
Sampled by (Name - Print)
T�Ken
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
CuSeaNy
Lab Comments
N
oy
y �
Relinqu" b : [ 7 E} _
Da rme
Received by: (SIGNATURE)
pate rme
81,019RICooter Temp
Relin hed by; (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
�)j
VIl,3124,
3.jvr�
It- l
Relinquished by: (SIGNATURE)
Date Time
Rec '
Date Time
2ZIINITURE)

Waypointo
ANALYTICAL
4/23/2020
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 20-101-0060
Client Project Description: Smithfield
Tarheel, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/10/2020 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Ijp,
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
2/28/2021
Arizona
State Program
AZ0816
8/30/2020
Arkansas
State Program
88-0650
2/7/2021
California
State Program
2904
5/10/2020
Georgia
State Program
C044
2/18/2023
Georgia
State Program
04015
6/30/2020
Illinois
State Program
- NELAP
200078
10/10/2020
Kentucky
State Program
80215
6/30/2020
Kentucky
State Program
KY90047
12/31/2020
Louisiana
State Program
- NELAP
04015
6/30/2020
Mississippi
State Program
MS
5/10/2020
North Carolina
State Program
415
12/31/2020
Oklahoma
State Program
9311
8/31/2020
Pennsylvania
State Program
- NELAP
68-03195
5/31/2020
South Carolina
State Program
84002
5/10/2020
South Carolina
State Program
84002
6/30/2020
Tennessee
State Program
02027
2/11/2023
Tennessee
A21LA ISO 17025:2017
4313.01
10/31/2021
Texas
State Program
- NELAP
T104704180
9/30/2020
Virginia
State Program
- NELAP
460181
9/14/2020
Washington
State Program
C1018
7/31/2020
Page 1 of 1 00001/20-101-0060
Page 2 of 8

Waypoint
ANALYTICAL
Report Number: 20-101-0060
Client Project Description: Smithfield
Tarheel, NC
Lab No Client Sample ID
87925 Smithfield Tarheek ESB
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected
Solids 04/09/2020 08:00
Date Received
04/10/2020
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield
Lab Report Number: 20-101-0060
Date: 4/23/2020
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: L486995
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

WayP
�'��' 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalyiical.com
46245
EMA Resources Inc
Mr. Brent Collins Project Smithfield Report Date : 04/23/2020
755 Yadkinville Rd Information : Tarheel, NC Received : 04/10/2020
Mocksville , NC 27028
Q�ln
Report Number : 20-101-0060 REPORT OFANALYSIS Danyale Love
Project Manager
Lab No : 87925
Matrix: Solids
Sample ID : Smithfield Tarheek ESB
Sampled:
4/9/2020
8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.9
%
1
04/13/2016:06
JDT
SW-DRYWT
Ammonia Nitrogen
16600
mg/Kg -
dry
2270
1
04/20/20 12:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
444
mg/Kg -
dry
444
444
1
04/16/20 14:11
ZBD
4500NO3F-2011
Organic N
5545
mg/Kg -
dry
4545
1
04/20/20 12:00
CALCULATION
pH
7.2
S.U.
1
04/21/20 05:09
JSL
9045D
Total Solids
1.16
%
0.010
0.010
1
04/14/20 16:59
ADM
2540G-2011
Total Volatile Solids
44.3
%
0.010
0.010
1
04/14/20 16:59
ADM
2540G-2011
Total Kjeldahl Nitrogen
22200
mg/Kg -
dry
4550
1
04/23/20 14:33
CLP 4500NORGD-2011
Phosphorus
13500
mg/Kg -
dry
234
455
1
04/13/20 17:49
TJS
6010D
Aluminum
11600
mg/Kg -
dry
185
455
1
04/13/20 17:49
TJS
6010D
Arsenic
<38.1
mg/Kg -
dry
38.1
45.5
1
04/13/20 17:49
TJS
6010D
Cadmium
<4.50
mg/Kg -
dry
4.50
9.09
1
04/13/20 17:49
TJS
6010D
Calcium
11100
mg/Kg -
dry
1530
2270
1
04/13/20 17:49
TJS
6010D
Chromium
<17.3
mg/Kg -
dry
17.3
22.7
1
04/13/20 17:49
TJS
6010D
Copper
67.8
mg/Kg -
dry
13.2
22.7
1
04/13/20 17:49
TJS
6010D
Iron
1660
mg/Kg -
dry
385
455
1
04/13/20 17:49
TJS
6010D
Lead
<13.5
mg/Kg -
dry
13.5
27.3
1
04/13/20 17:49
TJS
6010D
Magnesium
7990
mg/Kg -
dry
202
455
1
04/13/20 17:49
TJS
6010D
Manganese
96.4
mg/Kg -
dry
16.6
45.5
1
04/13/20 17:49
TJS
6010D
Mercury
0.3453
mg/Kg -
dry
0.317
1.44
1
04/14/20 11:47
DDB
7471A
Molybdenum
<11.8
mg/Kg -
dry
11.8
22.7
1
04/13/20 17:49
TJS
6010D
Nickel
<15.0
mg/Kg -
dry
15.0
22.7
1
04/13/20 17:49
TJS
6010D
Potassium
7550
mg/Kg -
dry
271
455
1
04/13/20 17:49
TJS
6010D
Qualifiers/ DF Dilution Factor
J
Estimated value
Definitions L Limit Exceeded
MQL
Method Quantitation Limit
Page 5 of 8

waypANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 20-101-0060
Lab No : 87925
Sample ID : Smithfield Tarheek ESB
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Project Smithfield
Information : Tarheel, NC
REPORT OFANALYSIS
Report Date : 04/23/2020
Received : 04/10/2020
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/9/2020 8:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Selenium
<44.5
mg/Kg - dry
44.5
45.5
1
04/13/20 17:49
TJS
6010D
Sodium
43500
mg/Kg - dry
702
2270
1
04/13/20 17:49
TJS
6010D
Zinc
323
mg/Kg - dry
98.2
114
1
04/13/20 17:49
TJS
6010D
Sulfur
4410
mg/Kg - dry
445
455
1
04/13/20 17:49
TJS
6010D
Sodium Absorption Ratio
8.0
Ratio
2.2
5.0
1
04/13/20 17:49
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 20-101-0060
Shipping Method
® Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
t45
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
! Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
® Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
® N/A
Water - VOA vials free of headspace
0 Yes
0 No
® N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes ® No
Comments:
Signature: ICarleen Qualls Date & Time: 04/10/2020 10:40:40
Page 7 of 8

Client Name/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Aeeount #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (city/State)
- Additional charges apply
Shipment
Matrix KeySpecial
HRUSH
Detection LimA(sj
Date Results Needed
Ydof
Ex Lips �USPS
Courier e Client Drop Off
WW -Wastewater GW-Groundwater
DW - Drinking Water 5 - Soil /Solid O -Oil
L r
rR G4 A
P Product M - Misc
���n7
71,go Heel C
I !
Other
•
Project Number
Project Manager Phone #
Project Manager Email
Purchase Order Number
Site/Facility ID #
336-399-3646
brent.collinsCcDemaresources.com
Z
i)
A Coal < IOC Na25203 (Micro On IV
GB
CD
Cool <= SC
Waypoin}.
'=
O
C
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'rf�/ ``
ANALYTICAL
�
aC
°
❑
E
d
�
F
cC
a'
❑
t f]
W
None it
0 None Required
E NaOH pH>10
2790 Whitten Road
"
:'
a
-
F HNO3 pHQ
Memphis, IN 38133
Unless noted, all containers
o
cp
Z
T
M
G HCL pHr2
[phone]
per Table II of 40 CFR Part
p
v
E
x
m
CJ
2
_
Q
1-1
H H3p04 pH[Z
Cool �= 6C NA25203
13b'
3
m
Z
❑.7Iv
Time
Sample Identification
Required Required
Analysis / Pre ervativ
Comments/Notes
Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,M9,M0,H9,Ni,Se,Na, PPS, K, Zn
I imll IIIII I� Illla I III Ian IIII lill 11111111111111 � oo 2020°
EMA Resources lnc 10 40:p9
Smithfield
For Laboratory Use Only
Sampled by (Name - Print)
oY
Client Remarks/Comments
ht
Sludge Samples - Report Dr Weight
Ice
Y,
Custody
Seals
Lab Comments
ReP
Ti me
Received by: (SIGNURE)
Date Time
o •y
L
Blank/ oolerT p
FrOin ' hed by: (SIGNATUR
Date Time
Received by: (SIGNATURE)
Date Time
4•!9 3 'x�fi
d-g0
Relinquished by: (SIGNATURE)
Date Fime
Received :(SIG TUBE
Date Time
`J L C
v

aceAnalytical
National Center for Testing & Innovation
AW
ANALYTICAL REPORT
January 21, 2020
EMA Resources
Sample Delivery Group: L1178363
Samples Received: 01/10/2020
Project Number: SMITHFIELD TAR HEEL
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
JJwkC4V1--
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE. *
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
SMITHFIELD TAR HEEL L1178363-01
Qc: Quality Control Summary
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
7
7
8
9
10
11
12
14
16
17
18
20
21
22
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50
PAGE:
2 of 22

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
SMITHFIELD TAR HEEL L1178363-01 Waste Roy Whitaker 01/09/2009:00 01/10/2009:00 t C
P
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Preparation by Method 1311
WG1410079
1 01/13/20 09:07
01/13/20 09:07
IDW
Preparation by Method 1311
WG1410099
1 01/13/20 08:47
01/13/20 08:47
BAA
Wet Chemistry by Method 9012 B
WG1412106
1 01/16/201151
01/17/2013:24
JER
Wet Chemistry by Method 9034-9030B
WG1411620
1 01/16/20 2106
01/16/20 2106
MJA
Wet Chemistry by Method 9045D
WG1412940
1 01/17/201100
01/17/2012:00
MSP
Wet Chemistry by Method D93/1010A
WG1413920
1 01/21/2012:25
01/21/2012:25
MJA
Mercury by Method 7470A
WG1410658
1 01/14/2010:46
01/14/20 20:53
TCT
Metals (ICP) by Method 6010D
WG1410815
1 01/15/20 07:28
01/15/2010:07
CCE
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1410537
1 01/14/2018:51
01/14/2018:51
BMB
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1412927
1 01/17/20 08:30
01/17/20 20:49
MT-1
Pesticides (GC) by Method 8081B
WG1410888
1 01/15/20 06:59
01/15/2018:30
HMH
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1412188
1 01/16/2010:44
01/16/20 20:14
JNJ
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
Mt. Juliet, TN
�GI
SAI
RC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50
PAGE:
3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
FC
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 4 of 22

SMITHFIELD TAR HEEL
Collected date/time: 01/09/20 09:00
Preparation by Method 1311
SAMPLE RESULTS - 01
L1178363
Result Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
1/13/2020 9:07:16 AM
WG1410079
TCLP ZHE Extraction -
1/13/2020 8:47:14 AM
WG1410099
Fluid 1
1/13/2020 9:07:16 AM
WG1410079
Initial pH 7.40
1/13/2020 9:07:16 AM
WG1410079
Final pH 5.05
1/13/2020 9:07:16 AM
WG1410079
Wet Chemistry by Method 9012 B
Result Qualifier
RDL Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
01/17/202013:24
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Batch
WG1412106
Dilution Analysis Batch
date / time
1 01/16/2020 2106 WG1411620
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 7.34 T8 1 01/17/202012:00 WG1412940
Sample Narrative:
L1178363-01 WG1412940: 7.34 at21.3C
Wet Chemistry by Method D93/1010A
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
Fc
�GI
SAI
Rc
Result
Qualifier
Dilution
Analysis
Batch
Analyte Deg. F
date / time
Ignitability DNI at170
1
01/21/202012:25
WG1413920
Mercury by Method 7470A
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Mercury ND
0.0100
0.20
1 01/14/2020 20:53
WG1410658
Metals (ICP) by Method 6010D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Arsenic ND
0.100
5
1 01/15/202010:07
WG1410815
Barium ND
0.100
100
1 01/15/202010:07
WG1410815
Cadmium ND
0.100
1
1 01/15/202010:07
WG1410815
Chromium ND
0.100
5
1 01/15/202010:07
WG1410815
Lead ND
0.100
5
1 01/15/202010:07
WG1410815
Selenium ND
0.100
1
1 01/15/202010:07
WG1410815
Silver ND
0.100
5
1 01/15/202010:07
WG1410815
Volatile Organic Compounds (GC/MS) by Method
8260D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
Benzene ND
0.0500
0.50
1 01/14/202018:51
WG1410537
Carbon tetrachloride ND
0.0500
0.50
1 01/14/202018:51
WG1410537
Chlorobenzene ND
0.0500
100
1 01/14/202018:51
WG1410537
Chloroform ND
0.250
6
1 01/14/202018:51
WG1410537
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
EMA Resources
SMITHFIELD
TAR HEEL
L1173363
01/21/20 15:50 5 of 22

SMITHFIELD TAR HEEL SAMPLE RESULTS
Collected date/time: 01/09/20 09:00 L1178363
Volatile Organic Compounds (GC/MS) by Method 8260D
- 01
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
01/14/202018:51
WG1410537
1,1-Dichloroethene
ND
0.0500 0.70 1
01/14/202018:51
WG1410537
2-Butanone (MEK)
ND
J3 J4 0.500 200 1
01/14/202018:51
WG1410537
Tetrachloroethene
ND
0.0500 0.70 1
01/14/202018:51
WG1410537
Trichloroethene
ND
0.0500 0.50 1
01/14/202018:51
WG1410537
Vinyl chloride
ND
0.0500 0.20 1
01/14/202018:51
WG1410537
(S) Toluene-dH
104
80.0-120
0111412020 18.51
WG1410537
(S) 4-Bromofluorobenzene
93.1
77.0-126
0111412020 18.51
WG1410537
(S) 1,2-Dichloroethane-d4
107
70.0-130
011141202018.51
WG1410537
Chlorinated Acid Herbicides (GC) by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) 2,4-Dichlorophenyl Acetic Acid 53.2
Pesticides (GC) by Method 8081B
Result
Analyte
mg/I
Chlordane
ND
Endrin
ND
Heptachlor
ND
Lindane
ND
Methoxychlor
ND
Toxaphene
ND
(S) Decochlorobiphenyl
74.5
(S) Tetrochloro-m-xylene
76.7
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 01/17/2020 20:49
WG1412927
0.00200
10
1 01/17/2020 20:49
WG1412927
14.0-158
0111712020 20.49
WG1412927
Qualifier RDL Limit
mg/I mg/I
0.00500 0.03
0.00500 0.02
0.00500 0.0080
0.00500 0.40
0.00500 10
0.0100 0.50
10.0-128
10.0-127
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Dilution Analysis
date / time
01/15/202018:30
01/15/202018:30
01/15/202018:30
01/15/202018:30
01/15/202018:30
01/15/202018:30
0111512020 18.30
0111512020 18.30
Batch
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
WG1410888
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1 01/16/2020 20:14
WG1412188
2,4-Dinitrotoluene
ND
0.100
0.13
1 01/16/2020 20:14
WG1412188
Hexachlorobenzene
ND
0.100
0.13
1 01/16/2020 20:14
WG1412188
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 01/16/2020 20:14
WG1412188
Hexachloroethane
ND
0.100
3
1 01/16/2020 20:14
WG1412188
Nitrobenzene
ND
0.100
2
1 01/16/2020 20:14
WG1412188
Pyridine
ND
0.100
5
1 01/16/2020 20:14
WG1412188
3&4-Methyl Phenol
ND
0.100
400
1 01/16/2020 20:14
WG1412188
2-Methylphenol
ND
0.100
200
1 01/16/2020 20:14
WG1412188
Pentachlorophenol
ND
0.100
100
1 01/16/2020 20:14
WG1412188
2,4,5-Trichlorophenol
ND
0.100
400
1 01/16/2020 20:14
WG1412188
2,4,6-Trichlorophenol
ND
0.100
2
1 01/16/2020 20:14
WG1412188
(S) 2-Fluorophenol
33.1
10.0-120
0111612020 20.14
WG1412188
(S) Phenol-d5
17.6
10.0-120
0111612020 20.14
WG1412188
(S) Nitrobenzene-d5
49.6
10.0-127
0111612020 20.14
WG1412188
(S) 2-Fluorobiphenyl
64.4
10.0-130
0111612020 20.14
WG1412188
(S) 2,4, 6-Tribromophenol
72.0
10.0-155
0111612020 20.14
WG1412188
(S) p-Terphenyl-d14
66.0
10.0-128
0111612020 20.14
WG1412188
ONE LAB. NATIONWIDE. *
Fp
Fc
FS
Fn
FA
Fc
�GI
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 6 of 22

WG1412106
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3491750-1 01/17/201315
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
L1178363-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1178363-01
(OS) L1173363-01 01/17/20 13:24 • (DUP) R3491750-5 01/17/20 13:27
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Cyanide ND 0.000 1 0.000 20
L1179007-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1179007-01 01/17/2013:33 • (DUP) R3491750-6 01/17/2013:34
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3491750-2 01/17/20 1316
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg
Reactive Cyanide 2.50 2.48 99.3
Rec. Limits LCS Qualifier
50.0-150
L1176623-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1176623-01 01/17/20 1319 • (MS) R3491750-3 01/17/2013:20 • (MSD) R3491750-4 01/17/2013:21
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 0.310 0.459 18.6 27.5 1 75.0-125 J6 J3 J6 38.7 20
L1179770-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1179770-02 01/17/2013:46 • (MS) R3491750-7 01/17/2013:47 • (MSD) R3491750-8 01/17/2013:43
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg
Reactive Cyanide 1.67 ND 1.36 1.21 73.1 64.5
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
1 75.0-125 J6 J6 11.1 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 7 of 22

WG1411620
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3491651-1 01/16/20 2106
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
7.63 25.0
L1178358-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1178363-01
(OS) L1173353-01 01/16/20 21:06 • (DUP) R3491651-3 01/16/20 2106
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %_
Reactive Sulfide ND ND 1 0.000 20
L1178942-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1173942-01 01/16/20 21:06 • (DUP) R3491651-4 01/16/20 2106
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3491651-2 01/16/20 2106
Spike Amount LCS Result
Analyte mg/kg mg/kg
Reactive Sulfide 100 95.6
LCS Rec. Rec. Limits LCS Qualifier
95.6 70.0-130
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 3 of 22

WG1412940 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1178363-01
L1178942-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1173942-01 01/17/2012:00 • (DUP) R3491754-2 01/17/2012:00
Original Result DUP Result Dilution DUP RPD
Analyte su su
Corrosivity by pH 8.50 8.55 1 0.587
Sample Narrative:
OS: 8.5 at22C
DUP: 8.55 at21.8C
Laboratory Control Sample (LCS)
(LCS) R3491754-1 01/17/20 12:00
Spike Amount LCS Result
Analyte su su
Corrosivity by pH 10.0 9.95
Sample Narrative:
LCS: 9.95 at18.6C
DUP Qualifier DUP RPD
Limits
LCS Rec. Rec. Limits LCS Qualifier
99.5 99.0-101
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 9 of 22

WG1413920 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1178363-01
L1178253-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1173253-02 01/21/2012:25 • (DUP) R3492610-2 01/21/2012:25
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F
Ignitability 110 107 1 2.77
L1179547-01 Original Sample (OS) • Duplicate (DUP)
DUP Qualifier DUP RPD
Limits
i
10
(OS) L1179547-01 01/21/20 12:25 • (DUP) R3492610-3 01/21/20 12:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Deg. F Deg. F
Ignitability DNI at170 DNI at170 1 0.000 10
Laboratory Control Sample (LCS)
(LCS) R3492610-1 01/21/2012:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte Deg. F Deg. F
Ignitability 82.0 81.8 99.7 97.0-103
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 10 of 22

WG1410658 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1178363-01
Method Blank (MB)
(MB) R3490773-1 01/14/20 20:00
MB Result MB Qualifier
MB MDL MB RDL
Analyte mg/I
mg/I mg/I
Mercury U
0.00330 0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490773-2 01/14/20 20:02 • (LCSD) R3490773-3 01/14/20 20:04
Spike Amount LCS Result
LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I
mg/I
Mercury 0.0300 0.0292
0.0294 97.2 98.1 80.0-120 0.919 20
L1178219-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1173219-02 01/14/20 20:06 • (MS) R3490773-4 01/14/20 20:03 • (MSD) R3490773-5 01/14/20 20:10
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0286
0.0287 95.2 95.8 1 75.0-125 0.614 20
L1178302-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173302-02 01/14/20 20:12 • (MS) R3490773-6 01/14/20 20:14 • (MSD) R3490773-7 01/14/20 20:22
Spike Amount
Original Result
MS Result
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I
mg/I
mg/I
mg/I
Mercury 0.0300
ND
0.0293
0.0296 97.5 98.8 1 75.0-125 1.28 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 11 of 22

WG1410815
Metals (ICP) by Method 6010D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1178363-01
(MB) R3490900-1 01/15/20 0931
MB Result
Analyte mg/I
MB Qualifier MB MDL
mg/I
MB RDL
mg/I
Arsenic U
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium U
0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490900-2 01/15/20 09:33 • (LCSD) R3490900-3 01/15/20 09:36
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
Arsenic
10.0
9.85
9.91
98.5
99.1
80.0-120
0.643
20
Barium
10.0
10.1
10.2
101
102
80.0-120
0.834
20
Cadmium
10.0
9.77
9.86
97.7
98.6
80.0-120
0.928
20
Chromium
10.0
9.76
9.75
97.6
97.5
80.0-120
0.113
20
Lead
10.0
9.82
9.92
98.2
99.2
80.0-120
1.03
20
Selenium
10.0
10.1
10.2
101
102
80.0-120
0.681
20
Silver
2.00
1.85
1.83
92.3
91.5
80.0-120
0.785
20
L1178499-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173499-04 01/15/20 09:39 • (MS) R3490900-5 01/15/20 09:44 • (MSD) R3490900-6 01/15/20 09:46
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
U
9.57
9.54
95.7
95.4
Barium
10.0
U
10.3
10.2
102
101
Cadmium
10.0
U
9.69
9.65
96.9
96.5
Chromium
10.0
U
9.72
9.70
97.2
97.0
Lead
10.0
U
9.76
9.66
97.6
96.6
Selenium
10.0
U
9.74
9.64
97.4
96.4
Silver
2.00
U
1.82
1.82
91.1
91.0
ONE LAB. NATIONWIDE. *
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.237
20
1 75.0-125
0.845
20
1 75.0-125
0.454
20
1 75.0-125
0.148
20
1 75.0-125
1.09
20
1 75.0-125
1.04
20
1 75.0-125
0.0881
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 12 of 22

WG1410815 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1178363-01
L1178878-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173373-01 01/15/20 09:49 • (MS) R3490900-7 01/15/20 09:51 • (MSD) R3490900-8 01/15/20 09:54
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits MS Qualifier
Analyte
mg/I
mg/I
mg/I
mg/I
Arsenic
10.0
ND
9.97
9.95
99.7
99.5
1 75.0-125
Barium
10.0
0.388
10.4
10.5
100
101
1 75.0-125
Cadmium
10.0
ND
9.88
9.93
98.8
99.3
1 75.0-125
Chromium
10.0
ND
9.73
9.70
97.3
97.0
1 75.0-125
Lead
10.0
ND
9.84
9.91
98.4
99.1
1 75.0-125
Selenium
10.0
ND
10.2
10.2
101
102
1 75.0-125
Silver
2.00
ND
1.86
1.86
93.2
93.1
1 75.0-125
ONE LAB. NATIONWIDE. *
MSD Qualifier RPD
RPD Limits
0.200
20
0.544
20
0.525
20
0.329
20
0.701
20
0.498
20
0.0688
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 13 of 22

WG1410537 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1178363-01
ONE LAB. NATIONWIDE. *
Method Blank (MB)
(MB) R3490638-8 01/14/201326
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetrachloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-dH
103
80.0-120
(S) 4-Bromofluorobenzene
94.8
77.0-126
(S) 1,2-Dichloroethane-d4
104
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3490638-1 01/14/20 09:04 • (LCSD) R3490638-3 01/14/201120
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
0.277
0.287
111
115
70.0-123
Carbon tetrachloride
0.250
0.254
0.266
102
106
68.0-126
Chlorobenzene
0.250
0.244
0.267
97.6
107
80.0-121
Chloroform
0.250
0.276
0.288
110
115
73.0-120
1,2-Dichloroethane
0.250
0.267
0.288
107
115
70.0-128
1,1-Dichloroethene
0.250
0.278
0.279
ill
112
71.0-124
2-Butanone (MEK)
1.25
1.65
2.18
132
174
44.0-160
Tetrachloroethene
0.250
0.239
0.253
95.6
101
72.0-132
Trichloroethene
0.250
0.248
0.253
99.2
101
78.0-124
Vinyl chloride
0.250
0.259
0.291
104
116
67.0-131
(S) Toluene-dH
102
103
80.0-120
(S) 4-Bromofluorobenzene
95.6
96.6
77.0-126
(S) 1,2-Dichloroethane-d4
104
103
70.0-130
LCS Qualifier
LCSD Qualifier RPD
3.55
4.62
9.00
4.26
7.57
0.359
J3 J4 27.7
5.69
2.00
11.6
RPD Limits
20
20
20
20
20
20
20
20
20
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 14 of 22

WG1410537 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1178363-01
ONE LAB. NATIONWIDE. *
L1178220-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173220-02 01/14/20 14:03 • (MS) R3490633-4 01/14/20 11:45 • (MSD) R3490633-5 01/14/20 12:06
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.320
0.328
128
131
Carbon tetrachloride
0.250
ND
0.300
0.315
120
126
Chlorobenzene
0.250
ND
0.278
0.290
ill
116
Chloroform
0.250
ND
0.311
0.320
124
128
1,2-Dichloroethane
0.250
ND
0.297
0.305
119
122
1,1-Dichloroethene
0.250
ND
0.318
0.330
127
132
2-Butanone (MEK)
1.25
ND
1.95
2.02
156
162
Tetrachloroethene
0.250
ND
0.279
0.283
112
113
Trichloroethene
0.250
ND
0.280
0.286
112
114
Vinyl chloride
0.250
ND
0.320
0.324
128
130
(S) Toluene-dH
103
103
(S) 4-Bromofluorobenzene
95.4
97.7
(S) 1,2-Dichloroethane-d4
104
104
L1178556-04 Original Sample (OS) • Matrix Spike (MS)
(OS) L1173556-04 01/14/20 14:27 • (MS) R3490633-6 01/14/2012:26
Spike Amount
Original Result
MS Result
MS Rec. Dilution
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.311
124 1
Carbon tetrachloride
0.250
ND
0.299
120 1
Chlorobenzene
0.250
ND
0.280
112 1
Chloroform
0.250
ND
0.317
127 1
1,2-Dichloroethane
0.250
ND
0.295
118 1
1,1-Dichloroethene
0.250
ND
0.315
126 1
2-Butanone (MEK)
1.25
ND
1.81
145 1
Tetrachloroethene
0.250
ND
0.280
112 1
Trichloroethene
0.250
ND
0.275
110 1
Vinyl chloride
0.250
ND
0.314
126 1
(S) Toluene-dH
103
(S) 4-Bromofluorobenzene
95.8
(S) 1,2-Dichloroethane-d4
104
Rec. Limits
17.0-158
23.0-159
33.0-152
29.0-154
29.0-151
11.0-160
10.0-160
10.0-160
10.0-160
10.0-160
80. 0-120
77.0-126
70.0-130
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 17.0-158
2.47
27
1 23.0-159
4.88
28
1 33.0-152
4.23
27
1 29.0-154
2.85
28
1 29.0-151
2.66
27
1 11.0-160
3.70
29
1 10.0-160
J5 3.53
32
1 10.0-160
1.42
27
1 10.0-160
2.12
25
1 10.0-160
1.24
27
80.0-120
77.0-126
70.0-130
MS Qualifier
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 15 of 22

WG1412927
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1178363-01
(MB) R3491837-1 01/17/201507
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
2,4-D U
0.000667
0.00200
2,4,5-TP (Silvex) U
0.000667
0.00200
(S) Z4-Dichlorophenyl Acetic 68.6
14.0-158
Acid
Laboratory Control Sample (LCS)
(LCS) R3491337-2 01/17/20 15:20
Spike Amount
LCS Result
LCS Rec.
Rec. Limits
Analyte mg/I
mg/I
2,4,5-TP (Silvex) 0.0500
0.0320
64.0
50.0-125
2,4-D 0.0500
0.0323
64.6
50.0-120
(S) Z4-Dichlorophenyl Acetic
60.6
14. 0-158
Acid
LCS Qualifier
L1178359-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE. *
(OS) L1173359-01 01/17/20 20:03 • (MS) R3491337-3 01/17/20 20:22 • (MSD) R3491337-4 01/17/20 20:35
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
2,4,5-TP (Silvex)
0.0500
ND
0.0323
0.0331
64.6
66.2
1 50.0-125
2.45
20
2,4-D
0.0500
ND
0.0316
0.0339
63.2
67.8
1 50.0-120
7.02
20
(S) Z4-Dichlorophenyl Acetic
54.8
56.6
14.0-158
Acid
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 16 of 22

WG1410888
Pesticides (GC) by Method 8081B
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1178363-01
(MB) R3491227-1 01/15/201524
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0.00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
85.8
10.0-128
(S) Tetrochloro-m-xylene
74.2
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3491227-2 01/15/20 15:36
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
Gamma BHC
0.0100
0.00876
87.6
55.0-129
Endrin
0.0100
0.00926
92.6
57.0-134
Heptachlor
0.0100
0.00951
95.1
27.0-132
Methoxychlor
0.0100
0.0111
ill
54.0-155
(S) Decachlorobiphenyl
78.5
10.0-128
(S) Tetrochloro-m-xylene
68.4
10.0-127
L1177678-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1177673-01 01/15/201614 • (MS) R3491227-3 01/15/20 16:26 • (MSD) R3491227-4 01/15/20 16:39
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
Analyte
mg/I
mg/I
mg/I
mg/I
Gamma BHC
0.0100
ND
0.00873
0.00890
87.3
89.0
1 14.0-141
1.93
Endrin
0.0100
ND
0.00907
0.00929
90.7
92.9
1 10.0-160
2.40
Heptachlor
0.0100
ND
0.00946
0.00961
94.6
96.1
1 16.0-136
1.57
Methoxychlor
0.0100
ND
0.0102
0.0103
102
103
1 10.0-160
0.976
(S) Decachlorobiphenyl
71.9
75.0
10.0-128
(S) Tetrochloro-m-xylene
67.1
68.4
10.0-127
ONE LAB. NATIONWIDE. *
RPD Limits
40
39
40
34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 17 of 22

WG1412188 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1178363-01
Method Blank (MB)
(MB) R3491629-2 01/16/201752
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
U
0.0333
0.100
2,4-Dinitrotoluene
U
0.0333
0.100
Hexachlorobenzene
U
0.0333
0.100
Hexachloro-1,3-butadiene
U
0.0333
0.100
Hexachloroethane
U
0.0333
0.100
Nitrobenzene
U
0.0333
0.100
2-Methylphenol
U
0.0333
0.100
3&4-Methyl Phenol
U
0.0333
0.100
Pentachlorophenol
U
0.0333
0.100
2,4,5-Trichlorophenol
U
0.0333
0.100
2,4,6-Trichlorophenol
U
0.0333
0.100
Pyridine
U
0.0333
0.100
(S) 2-Fluorophenol
35.1
10.0-120
(S) Phenol-d5
20.5
10.0-120
(S) Nitrobenzene-d5
59.1
10.0-127
(S) 2-Fluorobiphenyl
72.4
10.0-130
(S) 2,4, 6-Tribromophenol
70.0
10. 0-155
(S) p-Terphenyl-d14
72.5
10.0-128
Laboratory Control Sample (LCS)
ONE LAB. NATIONWIDE. *
(LCS) R3491629-1 01/16/201731
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
1,4-Dichlorobenzene 0.500
0.336
67.2
18.0-120
2,4-Dinitrotoluene 0.500
0.403
80.6
49.0-124
Hexachlorobenzene 0.500
0.401
80.2
44.0-120
Hexachloro-1,3-butadiene 0.500
0.327
65.4
19.0-120
Hexachloroethane 0.500
0.321
64.2
15.0-120
Nitrobenzene 0.500
0.304
60.8
27.0-120
2-Methylphenol 0.500
0.277
55.4
28.0-120
3&4-Methyl Phenol 0.500
0.275
55.0
31.0-120
Pentachlorophenol 0.500
0.367
73.4
23.0-120
2,4,5-Trichlorophenol 0.500
0.427
85.4
44.0-120
2,4,6-Trichlorophenol 0.500
0.370
74.0
42.0-120
Pyridine 0.500
0.182
36.4
10.0-120
(S) 2-Fluorophenol
35.2
10.0-120
(S) Phenol-d5
21.8
10.0-120
(S) Nitrobenzene-d5
49.9
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
SMITHFIELD TAR HEEL L1178363 01/21/20 15:50 18 of 22

WG1412188 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1178363-01
Laboratory Control Sample (LCS)
(LCS) R3491629-1 01/16/201731
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/I mg/I
(S) 2-Fluorobiphenyl 77.2 10.0-130
(S) 2,4, 6-Tribromophenol 86.5 10. 0-155
(S) p-Terphenyl-d14 77.3 10.0-128
L1178358-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1173353-01 01/16/20 20:59 • (MS) R3491629-3 01/16/20 21:20 • (MSD) R3491629-4 01/16/20 2141
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
1,4-Dichlorobenzene
0.500
ND
0.247
0.228
49.4
45.6
2,4-Dinitrotoluene
0.500
ND
0.359
0.338
71.8
67.6
Hexachlorobenzene
0.500
ND
0.356
0.333
71.2
66.6
Hexachloro-1,3-butadiene
0.500
ND
0.239
0.233
47.8
46.6
Hexachloroethane
0.500
ND
0.217
0.206
43.4
41.2
Nitrobenzene
0.500
ND
0.268
0.245
53.6
49.0
2-Methylphenol
0.500
ND
0.243
0.220
48.6
44.0
3&4-Methyl Phenol
0.500
ND
0.245
0.222
49.0
44.4
Pentachlorophenol
0.500
ND
0.319
0.282
63.8
56.4
2,4,5-Trichlorophenol
0.500
ND
0.379
0.332
75.8
66.4
2,4,6-Trichlorophenol
0.500
ND
0.325
0.284
65.0
56.8
Pyridine
0.500
ND
0.165
0.165
33.0
33.0
(S) 2-Fluorophenol
31.6
27.4
(S) Phenol-d5
19.1
16.8
(S) Nitrobenzene-d5
45.3
40.8
(S) 2-Fluorobiphenyl
70.2
62.0
(S)2,4,6-Tribromophenol
74.0
67.5
(S) p-Terphenyl-d14
68.8
64.9
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 17.0-120
8.00
1 39.0-125
6.03
1 35.0-122
6.68
1 12.0-120
2.54
1 10.0-120
5.20
1 12.0-120
8.97
1 10.0-120
9.94
1 10.0-120
9.85
1 10.0-128
12.3
1 33.0-120
13.2
1 26.0-120
13.5
1 10.0-120
0.000
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
ONE LAB. NATIONWIDE. *
RPD Limits
40
25
24
34
40
30
30
36
37
31
31
37
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 19 of 22

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. *
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
Fp
Fc
FS
Fn
Fr
Fc
SAI
Rc
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 20 of 22

ACCREDITATIONS
& LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide
from one location. One phone call, one point of contact,
one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our
single location laboratory is comparable to the collective
totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory
campus. The model is conducive to accelerated
productivity, decreasing
Cp
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium
quality and prompt service allows us to be YOUR
LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace
National.
Fc
State Accreditations
Alabama 40660
Nebraska
NE-OS-15-05
FS
Alaska 17-026
Nevada
TN-03-2002-34
Arizona AZ0612
New Hampshire
2975
Arkansas 88-0469
New Jersey—NELAP
TNO02
Fn
California 2932
New Mexico
n/a
Colorado TN00003
New York
11742
Connecticut PH-0197
North Carolina
Env375
Fr
Florida E87487
North Carolina'
DW21704
Georgia NELAP
North Carolina 3
41
Georgia' 923
North Dakota
R-140
Fc
Idaho TN00003
Ohio—VAP
CL0069
Illinois 200008
Oklahoma
9915
7G1
Indiana C-TN-01 f
Oregon
TN200002
Iowa 364
Pennsylvania
68-02979
Kansas E-10277
Rhode Island
LA000356
Kentucky' 6 90010
South Carolina
84004
Kentucky 2 16
South Dakota
n/a
Louisiana A130792
Tennessee'"
2006
Louisiana' LA180010
Texas
T104704245-18-15
Rc
Maine TN0002
Texas 5
LABO152
Maryland 324
Utah
TN00003
Massachusetts M-TNO03
Vermont
VT2006
Michigan 9958
Virginia
460132
Minnesota 047-999-395
Washington
C847
Mississippi TN00003
West Virginia
233
Missouri 340
Wisconsin
9980939910
Montana CERT0086
Wyoming
A2 LA
Third Party Federal Accreditations
A2LA— ISO17025 1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5 1461.02
DOD
1461.01
Canada 1461.01
USDA
P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
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NE
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WVI NY
MI T
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Mo
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FL
ME
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources SMITHFIELD TAR HEEL L1173363 01/21/20 15:50 21 of 22

Billing Information:
A
alvsis
Containpr
! Preservative
Chain of Custudy Page of
EMA Resources
Mr. Brent Collins Pres
755 Yadkinville Road Chk
�2cleAwlyfia*
755 Yadkinville Road
Mocksville, NC 27028
Mocksville, NC 27028
12065 Lebanon Rd # �
Mount JulieLTN37122 sy.�
Report to:
Mr. Brent Collins
Email To [e-mail]
Phone: [phone],y Y
Phone: [phone] } -�• 999
rax 61s-7sa-sas9 �i ' ,�f,a•
Project
City/state _/
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Please Circle:
Description: Sludge
Collected: � YkZ
PT MT CT ET
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Phone: [phone]
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Fax: [phone]
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Coll e y (p int)-
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same Day _ Five Day
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_ Next Day _ 5 Day (Rad Only) Date Results Needed
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Two Day _ 10 Day (Rad Only) No,
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* Matrix:Remarks:
GW - Groundwater B - Bioassay
Lied. r[:ester,;
COC Signed/Accura 1
WW Wastewater
Flow
Other
Bottles arrive intact: �?_N
DW - Drinkin Water
g
Correct bottles used: _N
Samples ret edvia:
Sufficient volume sent: N
LIPS e x ouner
— — —
VOA Zero Headspace: Y N
Preservation Correct/Chec:ted: N
afar
Date
Time:
Received by, (Signature)
Trip BlankReceived: Yes/
HCL/MeoH
Rpn Screen <0.5 mR/hr: y N
—
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Reli uis ed by: (Signature)
t
Time:
Received by: (Signature)
Temp:
°C Bottles Received:
If preservation required by Login: Date/Time
Relinquished by : (Signature)
Date:
Time:
Received fo ab by: (Signature)
Date:
Titre:
Hold:
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NCF / O

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number: WQOO14868
WWTP Name: Tarheel WWTP NPDES Number: NCO078344
Monitoring Period: From l/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tenip) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
ThermophiIic ❑
Beta Ray ❑
Gatntna Ray ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate `*Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ 1 Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
V.
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Excee- Number o
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Min
Geo. Mean
Maximum
Units
Fecal CoGforrt�
2 x 10 to the
6th power
per gram of
total solids
MPN
CF[]
35I
360
367
CFU/g
0
Quarterly
Y
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) ❑�
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC
Pre er Name and Ti (type or print)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and T%�tlitlee (if applicable)(type or print)
CQ- Z, " =5 l_ 41ele'l 2/1/2021
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)
Date
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 01/09/2020
Reported: 01 /13/2020
For: Smithfield TarHeel
Comments: Geometric Mean= 948 MPN/g MPN(most probable number)
STATESVILLE
C ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
200109-24-01
Fecal Coliforms
SF-1
755
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-01
Percent Solids
SF-1
2.65
%
SM2540B-2011
01/10/2020
CL
200109-24-02
Fecal Coliforms
SF-2
775
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-02
Percent Solids
SF-2
2.58
%
SM2540B-2011
01/10/2020
CL
200109-24-03
Fecal Coliforms
SF-3
1613
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-03
Percent Solids
SF-3
2.48
%
SM2540B-2011
01/10/2020
CL
200109-24-04
Fecal Coliforms
SF-4
1460
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-04
Percent Solids
SF-4
2.74
%
SM2540B-2011
01/10/2020
CL
200109-24-05
Fecal Coliforms
SF-5
803
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-05
Percent Solids
SF-5
2.49
%
SM2540B-2011
01/10/2020
CL
200109-24-06
Fecal Coliforms
SF-6
784
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-06
Percent Solids
SF-6
2.55
%
SM2540B-2011
01/10/2020
CL
200109-24-07
Fecal Coliforms
SF-7
<791
MPN/g
SM92210E-2006
01/10/2020
CL
200109-24-07
Percent Solids
SF-7
2.53
%
SM2540B-2011
01/10/2020
CL
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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Client:
oc.ctC-C L
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STATESVILLE ANALYTICAL
Address: �^� u a /
7J �y D% GF /cff/9!/
122 Court street • P.O. Box 228
Statesville, NC 28687
[phone]
n J OG/r v� VZCZ�— ` �n Q
(
Contact Person:
Phone 11336 PAX#
Chain of
PO #
Requisitioned by: (Time Dater
Custody Record
Customer
Sample ID#
lab Ip
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
a
Matrix
SW9. I r+ I WW
Parameters requested for analysis
/7�a
!'—s—
Relinquished by:
Received by:
Relinquished by:
Received by:
Composite Sampling #1:
Time begin am, pm Date / /
Time end am, pm Date _/_/_
Composite Sampling #2:
Time begin am, pm Date
Time end am, pm Date —I I_
Time O.Z arffm>ate 2/-<
Time Jam, pm Date !` r d
Time am, pm Date _/ /
Time am, pm Date —/ /
Lab Comments:
Sampled by: p
Transported by:
Holding times met:
Compliance work:
Non-compliance work:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number:
WWTP Name: Tarheel W WTP NPDES Number:
Monitoring Period: From l/l/2020 To 12/31/2020
WQ0014868
NCO078344
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Therinophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
.
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the followin
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g tY
umber o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
355
403
448
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
Of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. I (VS reduction) 0
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (AIk. Stabilization ❑
Alt 7 (Drying - Stable) ❑Alt.
8 (Drying - Unstable) ❑
Alt. 9 (injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been trade under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Prepa acne and Titl type or print) Land Applier Name and Tittl�lee (if applicable)(type or print)
.�- 3� 1 4� 2/ 1 /2021
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Page 1
Contact: Brent Collins Report Date: 3/23/2020
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 3/11/2020
Meritech Work Order # 03112014 Sample: Smithfield ESB 1 Grab 3/11/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.13 % 3/13/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <427 col/g dry wt 3/11/20 427 col/g dry wt SM 9222D
Meritech Work Order #
03112015 Sample: Smithfield ESB 2 Grab
3/11/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.56 % 3/13/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<355 col/g dry wt 3/11/20
355 col/g dry wt
SM 9222D
Meritech Work Order #
03112016 Sample: Smithfield ESB 3 Grab
3/11/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.41 % 3/13/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
377 col/g dry wt 3/11/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
03112017 Sample: Smithfield ESB 4 Grab
3/11/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.03 % 3/13/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
448 col/g dry wt 3/11/20
130 col/g dry wt
SM 9222D
Meritech Work Order #
03112018 Sample: Smithfield ESB 5 Grab
3/11/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.23 % 3/13/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<408 col/g dry wt 3/11/20
408 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
LL
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech Work Order # 03112019 Sample: Smithfield ESB 6 Grab
Parameters Result Analysis Date
% Total Solids 2.12 % 3/13/20
Fecal Coliform (Sludge) 429 col/g dry wt 3/11/20
Meritech Work Order # 03112020 Sample: Smithfield ESB 7 Grab
Parameters Result Analysis Date
% Total Solids 2.38 % 3/13/20
Fecal Coliform (Sludge) <382 col/g dry wt 3/11/20
Page 2
Report Date: 1/14/2020
Date Sample Rcvd: 1/6/2020
3/11/20
Reporting Limit Method
0-100 % SM 254013
130 col/g dry wt SM 9222D
3/11/20
Reporting Limit Method
0-100 % SM 254013
382 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016
Chain of Custody Record (COO)
NPDES#:
Client: EMA Resources Inc. Phone:_
755 Yadkinville Rd Fax:
Mocksville NC 27028 Email:_
Project:
P.O.#:
Attention:_ Brent Collins
How would you like your report sent?
Circle all that apply: mail referred), Fax, Mail
336-751-1441
336-751-1442
[e-mail]
Turn Around Time*
*RUSH work needs prior approval.
Stcl soda s) 3-s Days 1 24 - 49 Hrs
M E R ITE C H INC'
\ 1Address:_
t a, ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
Test(s) Required_
pq Ice?
e / No
pH OK?
Cl OK?
Date
Time
Date
Time
3/1 I
fecal r 1; 4 n^
2-
3
1�
9
V
7
v
(�
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination (<0,5 m) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field
prior to preservation.
Comments:
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes
10' No ❑
Report results in: mg/L ❑
mg/kg Rr ug/L ❑
Hand Delivery
Relinquished by: Date:
?////z0
Time:
; D. 3
Received by:
Date: Time:
❑ Other
Relinquished by: Date:
Time:
Received by:
Date: Time:
Relinquished by: Date: Time:
ved b
�atz jT'
'1�

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number:
WWTP Name: Tarheel WWTP NPDES Number:
WQ0014868
NCO078344
Monitoring Period: From 1/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment El
Tltermophilic ❑
Beta Ray ❑
Garnnia K-ay ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density l7
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significandy Reduce Pathogens":
Lime Stabilization ❑ T Air Drying ❑
composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitor
in data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech-ni u
q e
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
351
360
367
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 gams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt. i (VS reduction) R1
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC Brent Collins; Director of Technical Services
Pr er Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
a ^ S - � i 2/1/2021
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Page 1
Report Date: 4/7/2020
Date Sample Rcvd: 3/26/2020
Meritech Work Order #
03262008 Sample: Smithfield Tar Heel 1 Grab
3/26/20
Parameters
Result Analysis Date Reporting Limit
Method
% Total Solids
2.48 % 3/31/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
<367 col/g dry wt 3/26/20 367 col/g dry wt
SM 9222D
Meritech Work Order #
03262009 Sample: Smithfield Tar Heel 2 Grab
3/26/20
Parameters
Result Analysis Date Reporting Limit
Method
% Total Solids
2.59 % 3/31/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
<351 col/g dry wt 3/26/20 351 col/g dry wt
SM 9222D
Meritech Work Order #
03262010 Sample: Smithfield Tar Heel 3 Grab
3/26/20
Parameters
Result Analysis Date Reporting Limit
Method
% Total Solids
2.50 % 3/31/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
364 col/g dry wt 3/26/20 130 col/g dry wt
SM 9222D
Meritech Work Order #
03262011 Sample: Smithfield Tar Heel 4 Grab
3/26/20
Parameters
Result Analysis Date Reporting Limit
Method
% Total Solids
2.51 % 3/31/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
<362 col/g dry wt 3/26/20 362 col/g dry wt
SM 9222D
Meritech Work Order #
03262012 Sample: Smithfield Tar Heel 5 Grab
3/26/20
Parameters
Result Analysis Date Reporting Limit
Method
% Total Solids
2.52 % 3/31/20 0-100 %
SM 2540B
Fecal Coliform (Sludge)
<361 col/g dry wt 3/26/20 361 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date: 4/7/2020
Date Sample Rcvd: 3/26/2020
Meritech Work Order # 03262013 Sample: Smithfield Tar Heel 6 Grab 3/26/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.54 % 3/31/20 0-100 % SM 2540B
Fecal Coliform (Sludge) 358 col/g dry wt 3/26/20 130 col/g dry wt SM 9222D
Meritech Work Order # 03262014 Sample: Smithfield Tar Heel 7 Grab 3/26/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.54 % 3/31/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <358 col/g dry wt 3/26/20 358 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. .��r ��� k
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5- 2016
Chain of Custody Record (COC)
NPDES#:
MERITSlient:
C H, INC,I N C
/
�j1'If4 W�SouRCcs �c . Phone: S36.75Y- iYY(
•
Address: "%SS YAl)Ks�t��CCC-" GZ� . Fax:
ENVIRONMENTAL LABORATORIES
�oC/�SI/ZGCE �✓C�?o,-�� Email:
i
642 Tamco Rd. Phone: [phone]
Project:�i>!,L7T�.�F2c-0
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: -BgaT C-";c W 5 Turn Around Time*
How would you like your report sent? *RUSH work
needs prior approval.
www.meritechiabs.com
Circle all that apply: Email (preferred), Fax, Mail Stcl 10days)
3 5 Days 2Os
Sampling Dates & Times
Person Takin a (Si /Pri :
o V C.) �f z7 K�%GZ
Lab Use Only
Sample Location and/or ID # Start End
Date Time Date Time
Comp? #of Test(s) Required
Grab?
Cl
Cont.
es N
Yes No 7
OK?
-6 S F- ��7.164 AA
Co
�•
.sr-'L ar A- :03 fkW
G Q
Jr•3 :06
Cs
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(-' - 7 : 0 ,gw
Gr 1
``
r--s AR
G I L
s--(9
G I 13
S (7- '7 .3/AG A0 7 A?
G I l
Temperature Upon
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Receipt:
�/
Shipment:
Comments:
Compositor #
❑ UPS
❑ Fed Ex
Are these Its for regu tort' purposes? Yes
Jug #
No ❑ Report results In: m /L ❑
p g mg/kg ❑ ug/L ❑
Hand Delivery
Relinquished by: Date: Time:
2G
Received b
�l;a?RM y: Date:
Time:
❑ Other
Relinquished by.v C Dat : Time:
Received by: Date:
Time:
Relinquished by: Date: Time:
Rec Lab:
l � _` V Ql-g
Time:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
WWTP Name:
Smithfield Fresh Meats Corp.
Tarheel WWTP
WQ Permit Number:
NPDES Number:
Monitoring Period: From I/l/2020 To 12/31/2020
WQ0014868
NCO078344
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
All. A (time/temp) ❑ Alt B (Alk Treatment)❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
JAIt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ I Air Drying ❑ Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g �
Number o
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
329
362
411
CFU/g
0
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) 21
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 03 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ lAlt.
8 (Drying - Unstable) ❑
Alt. 9 (injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC
Pre re Name and Ti pe or print)
10 �-
Signature o Prepa er* Date
Brent Collins; Director of Technical Services
Land Applier Name and
/Tiitttllee (if applicable)(type or print)
l Z " 2f l /2021
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

A
Contact: Brent Collins
Client: EMA Resources, Inc
755'Yadkinviile Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Meritech Work Order # 12292001 Sample: Smithfield 1 Grab
Parameters Result Analysis Date
% Total Solids 2.45 % 12/30/20
Fecal Coliform (Sludge) <371 col/g dry wt 12/29/20
Meritech Work Order # 12292002 Sample: Smithfield 2 Grab
Page 1
Report Date: 1/4/2021
Date Sample Rcvd: 12/29/2020
12/29/20
Reporting Limit Method
0-100 % SM 2540E
371 col/gdry wt SM 9222D
12/29/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.21 % 12/30/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<411 col/g dry wt 12/29/20
411 col/g dry wt
SM 9222D
Meritech Work Order #
12292003 Sample: Smithfield 3 Grab
12/29/20
Parameters
Result Analysis Date
Reporting Limit
Method
% Total Solids
2.76 %
12/30/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<329 col/g dry wt
12/29/20
329 col/g dry wt
SM 9222D
Meritech Work Order # 12292004 Sample: Smithfield 4 Grab 12/29/20
Parameters Result Analysis Date Reporting Limit Method
% TotaI Solids 2.43 % 12/30/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <374 col/g dry wt 12/29/20 374 col/g dry wt SM 9222D
Meritech Work Order # 12292005 Sample: Smithfield 5 Grab 12/29/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.54 % 12/30/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <358 col/g dry wt 12/29/20 358 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
!�? Laboratory Certification No. 165
Page 2
Contact: Brent Collins Report Date: 1/4/2021
Client: EMA Resources, Inc
75S Yadkinville Road
MocksviIle, NC 27028 Date Sample Rcvd: 12/29/2020
Meritech Work Order # 12292006 Sample: Smithfield 6 Grab 12/29/20
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.61 % 12/30/20 0-100 % SM 2540B
Fecal Coliform (Sludge) <348 col/g dry wt 12/29/20 348 col/g dry wt SM 9222D
Meritech Work Order # 12292007 Sample: Smithfield 7 Grab 12/29/20
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
2.61 %
12/30/20
0-100 %
SM 2540B
Fecal Coliform (Sludge)
<348 col/g dry wt
12/29/20
348 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. 0/,/"/
a 'story Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-r01G
Chain of Custody Record (CCIC)
NPDES#:
M E R I TE C H, INC.
Client: EMA Resources Inc.
Phone:_
336-751-1441
4
e
Address: 755 Yadkinville Rd
Fax:
336-751-1442
ENVIRONMENTAL LABORATORIES
Mocksville NC 27028
Email:
brent.collins emaresourcesinc.com
t• 642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Brent Collins
Turn Around Time*
How would you like your report sent?
*RUSH work needs prior approval.
www.meritechlabs.com
Circle all that apply: oEireferred),,
Fax, Mail
std coda s), a-s DayS 24 - 48 H,s
Sampling Dates & Times
Personking Sam ie (Sign/Pr �t):
��,•,
Lola Use Only
Sample Location
and/or ID #
Start End
Date
comp? oaf Test(s)
Required On Ice? pH ?
Time Date Time Grab? Cont.
Yes / Na Cl OK?
y �'!'f'lG'1 fi7
y'
•�/C�7/OV �rJLGfy!
r/"'
I
! LfG ! • r/ji
V
v-31
�
03
y
le
�W
V
-7
�.
Temperature Up°n
Method of
*** Dechlorination (<0.5 pm of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior
to reservation.
Receipt: , c
Shipment:
Comments:
Compositor 4
❑ Li Ps
❑ Fed Ex
Are these results for regulatory purposes? Yes
©-�No ❑ Report results in: mg/L ❑
Jug #
mg/kg ❑t?' ug/L ❑
Hand Delivery
� Relinquished by: Date-
,9120
Time: Received by:
n.+
Date: Time:
❑ Other
Relinquished by: Date:
Time: Received by:
Date: Time:
Relinquished by: Date:
Time: Rece' y L /� J
Datq: Tim :

Land App ANL Volatile Solids In
Jan 2020
91,650
85,400
93.18
Feb 2020
91,800
87,150
94.93
Mar2020
86,900
81,800
94.13
Apr2020
74,175
71,030
95.76
May 2020
61,9501
58,870
95.03
Jun 2020
132,100
127,800
96.74
Ju12020
74,600
70,700
94.77
Aug 2020
91,500
85,950
93.93
Sep 2020
100,000
95,600
95.60
Oct 2020
83,773
78,992
94.29
Nov 2020
51,450
48,450
94.17
Dec 2020
74,250
71,650
96.50
Minimum
51,450
48,450
Maximum
132,100
121,800
Total
1,014,148
963,392
Average
84,5121
80,283
94.92

Volatile Solids Out
Volatile Solids IN average
% Reduction
1/9/20 ESB
49.9
94.92
94.67
3/11/20 ESB
50.4
94.92
94.56
3/26/20 ESB
44.2
94.92
95.76
4/9/2020 ESB
44.30
94.92
95.74

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031363
�5{i �141..tiL
Client: Steve Dunham
Advisor: Brent Collins
Predictive
2467 Burney Rd.
EMA Resources Inc
;•
White Oak, NC 28399
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Bladen
Links to Helpful Information
Client ID: 169244
Advisor ID: 405413
Sampled: Received: 05/27/2020 Completed: 06/03/2020
Farm: SF03
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1- Bermuda hay/past., M 1.0
180-220 0
90 0 0 0 0
0 0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 1.29 6.4 70 2.0 5.4 517 61
55 10
50 138 100 1744 1744
615 0.1 2
Noah Carolina
i
I Awl'
Futaw frum FwW Curnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL032074
Client:
Steve Dunham
Advisor:
Brent Collins
vo- Predictive
2467 Burney Rd.
EMA Resources Inc
White Oak, NC 28399
755 Yadkinville Rd
.'..,$' Soil Report Mehlich-3
Extraction
Mocksville, NC 27028
_
Sampled County : Bladen
Links to Helpful Information
Client ID: 169244
Advisor
ID: 405413
Sampled: Received: 06/11/2020 Completed: 06/17/2020
Farm: SF03
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 0
80
0 0
0
0
0
0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.43 1.25 8.3 87 1.0 6.3 325 30
70 15
47
85
64
966
966
438
0.1 1
Sample ID: 00003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M 0.0
180-220 0
200
0 0
0
0
0
0
Note: 12
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.56 1.40 6.1 88 0.7 6.2 369 16
69 18
41
123
88
1695
1695
582
0.1 2
Sample ID: 00005
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 0
110
0 0
pH$
0
0
0
Note: 3 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.71 1.36 7.8 97 0.2 7.0 393 14
83 13
30
126
78
1630
1630
541
0.1 1
North Carolina
Tobin w Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

Page 1 of 1
Report No: 20-364-0531
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypo'10 t
ANALYTICAL
Client: Steven Dunham
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: SF03
Date Received: 12/29/2020
Date of Report: 12/30/2020
Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-1 K-1 S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
109124 04 MIN 2.0 6.5 0.7 118 18 12 1025 0 0 160 160 155 9.8 93 81 10 0.9 0.1 I
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031366
�5{i �141..tiL
Client:
Vance Tyson
Advisor: Brent Collins
Predictive
4925 NC Hwy 87 S
EMA Resources Inc
;•
Fayetteville, NC 28306
755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction
+_
Mocksville, NC27028
Sampled County : Cumberland
Links to Helpful Information
Client ID: 508814
Advisor ID: 405413
Sampled: Received: 05/27/2020 Completed: 06/03/2020
Farm: SF06
Sample ID: 00006
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, silage 0.3
180-220 0
110
0 0
0
0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Organic
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
8.24 0.75 9.8 53 4.6 4.9 68 42
41 10
58
29
50
200
332
70 0.1 1
Sample ID: 00007
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, silage 1.2
180-220 0
160
0 0
0
0
0 0
Note: 3
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
1.61 1.22 5.3 60 2.1 5.2 149 21
48 10
39
36
39
131
131
86 0.1 2
Noah Carolina
I Awl'
Futacii frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY20-SL031361
�5{i �141..tiL Client: Bonnie Meeker Advisor: Brent Collins
Predictive 19850 Hwy 87 W EMA Resources Inc
;• Tar Heel, NC 28392 755 Yadkinville Rd
f'. Soil Report Mehlich-3 Extraction Mocksville, NC27028
+_
Sampled County : Bladen
Links to Helpful Information
Client ID: 440578 Advisor ID: 405413
Sampled: Received: 05/27/2020 Completed: 06/03/2020 Farm: SF07
Agronomist's Comments:
This report provides Test Results and Recommendations for each sample submitted for testing. Look for Lime Recommendations and N-P-K Fertilizer Recommendations.
The lime recommendation is always listed next to the first crop and will be based on the higher target pH if the pH targets for crop 1 and crop 2 differ. Application at the
indicated rate will raise soil pH to the optimal level for the plant you specified and should be sufficient for 2 to 3 years, depending on soil type. Common target pH values
are as follows: 5.0 for azalea, camellia, rhododendron and mt. laurel; 5.5 for centipedegrass; 6.0 for other lawn grasses, shrubbery, and; flowering plants; and 6.5 for
vegetable gardens. N-P-K Recommendations are based on the nitrogen (N) needs of the plants being grown and the soil test results for phosphorus (P-1) and potassium
(K-I); a 50 to 70 index for either is optimum. If the exact fertilizer cannot be found, find the closest match and adjust the rate accordingly. Refer to "Understanding the Soil
Report" last page of this report) for additional explanation and links to helpful information.
Sample ID: 00009
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.6 120-200 0 80 0 0 0 0 0 0
Note: 12
2- 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.27 1.14 5.9 73 1.6 5.6 549 27 62 9 34 175 122 1959 1959 970 0.1 2
Noah Carolina
i
I Awl'
Futacii frum fuWCurnml5skm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY20-SL031364
Client:
Hinton Mack (HM) King
Advisor:
Brent Collins
vo- Predictive
831 King Rd
EMA Resources Inc
Saint Pauls, NC 28384
755 Yadkinville Rd
.'..,$' Soil Report
Mehlich-3 Extraction
Mocksville, NC 27028
_
Sampled County : Robeson
Links to Helpful Information
Client ID: 196895
Advisor
ID: 405413
Sampled: Received: 05/27/2020 Completed: 06/03/2020
Farm: SF08
Sample ID: 00001
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage
0.0
180-220 0
80
0 0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 1.36 4.0 79 0.8 6.1
156 59
56 16
28
115
84
424
424
182
0.1 3
Sample ID: 00002
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage
0.0
180-220 0
100
0 0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 1.34 4.8 80 1.0 6.1
321 48
57 18
30
129
93
727
727
273
0.1 2
Sample ID: 00003
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage
0.8
180-220 10
80
0 0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.76 1.28 4.4 60 1.7 5.5
77 58
40 14
40
57
51
197
197
118
0.1 2
North Carolina
Tobin w Trust f wW Ctwninisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone:
[phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY20-SL031364
Hinton Mack (HM) King
Page 2 of 3
Sample ID: 00004
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage
1.1
180-220 50
90
0
0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
1.49 1.30 4.9
56 2.1 5.4
43 53
37 13
46
48
46
186
186
72 0.1
2
Sample ID: 00006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, silage
1.2
180-220 0
80
0
0
0
0
0
0
Note: 3
2-
0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-I
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
2.08 1.14 7.7
69 2.4 5.4
120 57
50 16
33
57
51
267
267
160 0.1
1

For customer Inquiries contact us at: MULTI -USE ACCOUNT NUMBER 28115.97754 Pac1F 2 of
1.800.356.9033 ❑r visit us online: EMA RESOURCES INC
MyJDFAccount.com 755 YADKINViLLE RD
JOHN ❑EERE MOCKSVILLE, NC 27028.2053
FINANCIAL PHONE: [phone]
POSTED TO YOUR
Fran. Date Invoice # 1 Transaction
Data Posted Reference Program Description Amount
S S C LUMBERTON SERVICE LUMBERTON NC 810-739.9058 --�-- —
12l21120 12/21/20 6246M PURCHASE sj�e— fOrS4 2,979.23
FERTILIZER BULK o
au8ilw Unit Price ]Win T4i,! Invoice Item Descriotlon
0.863 TON TON 0.00 DOLOMITE LIMESTONE GRAN - BULK
1.518 TON TON 0.00 21.0-0 AMMONIUM SULPHATE GR SU
2,472 TON TON 0.00 46-0-0 UREA GRANULAR HULK
2.428 TON TUN 0.00 0-0-60 MOP GRANULAR SULK
7.281 TON TON 0.00 Fertiiizer/Anaiysls: 19-0-20
2,475,53 Total Fertilizer, Seeds and Ch
29.00 ACRE 10.50 ACRE 304,60 FERTILIZER SPREADING
1.00 EACH 4.17 EACH 4.17 STATE FERTILIZER INSPECT FEE
1,00 EACH 0.43 EACH 0.43 STATE LIME INSPECTION FEE
194.60 Tax
PAYMENTS AND OTHER ADJUSTMENTS
Tran. Date Check # Transaction
Data Posted 1 Rehronco Description Amount
12/28120 12128/20 PAYMENT - THANK YOU - 330.27
12/28/20 1212t3120 PAYMENT - THANK YOU - 460.57
12/28/20 12/28120 PAYMENT - THANK YOU - 2.240,37
INTEREST CHARGED
01/08/21 INTEREST CHARGE ON PURCHASES 54.60
TOTAL INTEREST CHARGED FOR THIS PERIOD 54.60 I
NEW BALANCE 3,604.33
E•
2021 TOTALS YEAR-TO-DATE '
TOTAL FEES CHARGED IN 2021 0.00
TOTAL INTEREST CHARGED IN 2021 54.60
Purchases, Returns and Payments made Just prior to the statement date may not appear untll your next statement.
Please contact your merchant for copies of lost or missing involco(sj.

Roy Whitaker
From:
Hinton King <[e-mail]>
Sent:
Thursday, February 20, 2020 12:23 PM
To:
Roy Whitaker
Cc:
Hinton King
Subject:
Lime
Here are the sample results and Nutrien invoice for the lime. All of the lime we used was billed together as you can see
on the invoice. I have separated out your portion which is $7265.02. This is just lime. There are no application or soil
sampling charges inctuded. The lime was $43.50/ton delivered.
334,024lbs or 167.032 tons x $43.50/ton = $7265,02

I , kwolro.36527355
Invoice - 38627.355
Kl,% G FARM 5 - I a - 4 571
LANHIP.John Com me,& Carrier WA
$000
or dju ors
Invoiced Details
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Or
LM240 prepay U"dl $002
Lam "ay MMW6t 002
Grua k"Ckm Tow: 163 AS 70
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2