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HomeMy WebLinkAboutWQ0000485_Monitoring - 07-2020_20201222�1 VALLEY PROTEINS, INC. ' December 17, 2020 Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 - o Re: Ground Water Quality Monitoring Report (GWQMR) Valley Proteins Inc. — Rose Hill r L To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of November 2020 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, Darr Sanford General Manager cc: VP Corporate Office Making a Sustainable Difference. 469 Yellow Cut Road Rose Hill, NC 28458 O 540.8772590 • 866.5%.0994 Transportation • 866.651.8175 valleyproteins.com SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES COMPLIANCE REPORT FORM • • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ElLand Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other. from Permit SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-1 Date sample collected: 7/11/2020 FIELD ANALYSES: If WELL WAS Well Depth: 12.46 ft. Well Diameter: 2 in. pH4500HB 5.00 units Temp. 000lo: 2U.4 °C DRY at Depth to Water Level 62546: 3.4 Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 000w: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec�j Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here:u LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.6 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.27 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 144.00 mg/L Al - Aluminum o11o5 mg/L Sodium 5.67 mg/L pH (Lab) oo4w 5.00 units Ba - Barium 01007 ug/L TOC oo68o 1.3 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00652 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 78 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) p No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia o0610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese oio55 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # r-Of rxcmCu•auvn aybwms uniy tAuacn LaD Keports): Intluent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Darrell Sanford - General Manager Permittee (or Authorized Aclent) Name and Title - Please print or type Sronature�tttee (or Authorized Agent) f (Date) GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: or�mrurv� mrvMn"M r tvry If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in, pH4500HB 6.40 units Temp. 000lo: 205 °C DRY at Depth to Water Level 82546: 10.8 ft. below measuring point Screened Interval: 30.15 ft. to 20.15 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water um ed/bailed before sampling: 5.0 p p p g: gallons Appearance Clear check here:❑ Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES I-1 NO Date sample analyzed: 07/11/2020-07/2912020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.18 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.43 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 284.00 mg/L Al - Aluminum oilo5 mg/L Sodium 10.2 mg/L pH (Lab) 00403 6.40 units Ba - Barium 01007 ug/L TOC 00680 1.5 mg/L Ca - Calcium oo916 mg/L Chloride 00940 10 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 7 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia omio <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, N1­13as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to tl�e best of my knowledge and belief. the information DY/R-:ert,lfed laboratory. I am aware that there are significant submitted penalties for in this report is true accurate, and complete, submitting false information. including the and that the laboratory analytical possibility of fines and imprisonment data was produced using approved methods ofanalysis by a for knowing violations. Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type Stgnatu rmlttee (or Aut orized Agent) (Date) GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon g ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW4 Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 6.60 units Temp. 000lo: 19.2 eC DRY at Depth to Water Level 82546: 4.3 ft. below measuring point Screened Interval: 28.93 ft. to 18.93 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan check here: El Samples for metals were collected unfiltered: X YES 0 NO and field acidified: X YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 m /L Zn - Zinc 01092 g mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.47 mg/L (NoteUse MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 207.00 mg/L At - Aluminum 01105 mg/L Sodium 9.60 mg/L pH (Lab) 00403 6.60 units Ba - Barium 01007 ug/L TOC 00680 0.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 <5.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-ceffed laboratory I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.8/2013 TER QUALITY MONITORING: E REPORT FORM I-AGILIIY INFUKMATIUN Please Print CleartyorType Facility Name: Valley Proteins Inc.- Rose Hill Permit Name (if different): Facility Address: 469 Yellow Cut Rd. Rose Hill, NC 28458 County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name: No. of wells to be sampled: 11 (from Perm ) NG UMT ne. sis-sar-col; Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW-7A Date sample collected: 7/11/2020 FIELD ANALYSES: If WELL WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.50 units Temp. oamo: 20.2 0C DRY at Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: Whos time of Measuring Point is 2.42 ft. above land surface Relative M.P. Elevation: ft. Odor doom: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checl Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES ❑ NO here: LABORATORY INFORMATION Date sample analyzed: 07111/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N o0615 <0.02 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg1L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.48 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 139.00 mg/L Al - Aluminum o11o5 mg/L Sodium 12.9 mg/L pH (Lab) 00403 4.50 units Ba - Barium 01007 ug/L TOC om8o <0.5 mg/L Ca - Calcium ow16 mg/L Chloride oo94o 60 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 21 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) p No (0) Specific Conductance o0085 4Mhos K - Potassium oo937 mg/L VOC 78732. method # SM 6200C Total Ammonia oo6lo <0.2 mg/L Mg - Magnesium oo927 mg/L method # (Ammonia Nitrogen; N4as N; Ammonia Nitrogen. Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Darrell Sanford - General Manager Permiftee (or Authorized Agent) Name and Title - Please print or type GROUNDWATER QUALITY MONITORING: . • • - DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill NC 28458 County Duplin SWIE' X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name Field 5 - damaged by farm equip I to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter:. 2 in. pH45001-t© 5.00 units Temp. 000lo: 203 °C DRY at Depth to Water Level 82546: 5.9 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: ItMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chect]u Samples for metals were collected unfiltered: X YES Q NO and field acidified: X YES El NO here: LABORATORY INFORMATION Date sample analyzed: 07111/2020-07/2912020 Laboratory Name: Environmental Chemists, Inc. Certification No. DW0#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 1.17 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 315o4 /100mL Phosphorus: Total as P 00665 0.46 mg/L (Note: Use MPN method for highly turold samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids -Total 70300 60.00 mg/L Al - Aluminum ol105 mg/L Sodium 1.86 mg/L pH (Lab) 00403 5.00 units Ba - Barium o1007 ug/L TOC oo68o 0.90 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils oo552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oio45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 23 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 ItMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia Como <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NFj as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # I -or Kemeolation,ystems Unly (Attacn Lab Keports): Influent total VOCS: Darrell Sanford - General Ma Permittee (or Authorized Agent) Name and Title -Please print or type mg/L Effluent Total VOCs: mg/L VOC Removal% ROUNDWATER QUALITY MONITORING: DMPLIANCE REPORT FORM AGILITY INFORMATION Please Print Clearly or Type acility Name: Valley Proteins Inc.- Rose Hill 'ermit Name (if different): acility Address: 469 Yellow Cut Rd. Rose Hill, NC 28458 County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name No. of wells to be sampled: 11 (from Permit) kRTMENT OF ENVIRONMENT & NATURAL RESOURCES ;ION OF WATER RESOURCES - INFORMATION PROCESSING UNIT MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 IT Number: Date: on -Discharge UIC PDES Other PPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: �.... _.. ..... ... WELL ID If WELL NUMBER (from Permit): MW-9 Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 6.60 units Temp. 000to: 13 °C DRY at Depth to Water Level 82546: 4.1 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec. Cond. 000m: ltMhos time of Measuring Point is 3.50 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan checl� Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here: LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 23 /100mL Nitrate (NO3) as N o062o 0.30 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.37 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 249.00 mg/L Al - Aluminum ol1o5 mg/L Sodium 7.30 mg/L pH (Lab) 00403 6.60 units Ba - Barium 01007 ug/L TOC oomo 43.2 mg/L Ca - Calcium 00916 mg/L Chloride oog4o 17 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 16 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 pMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: Nyas N. Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 1.4 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted DWR-cenified laboratory. I am aware that there are significant penalties for submitting Darrell Sanford - General Manager in this report is true, accurate. and complete, and false information. including the possitiNty that the laboratory of fines and �.�C� analytical imprisonment for data was produced using approved methods ofanaysis knowing violations by a f'�� Permittee (or Authorized Agent) Name and Title - Please print or type ture of Permit Authorized Agent) (Dat GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM IIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 thALALI I Y INI-OHMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge NPDES UIC Other Permit Name (if different): Facility Address. 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION ❑ Lagoon BEING MONITORED ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County. Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of well to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (tram Permit) SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-10A Date sample collected: 7/11/2020 FIELD ANALYSES: If WELL WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.60 units Temp. 000lc 161 oC DRY at Depth to Water Level szsas 3.6 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Red Tint checl�--I Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO H— l I LABORATORY INFORMATION Date sample analyzed. 07/11/2020-07/29/2020 Laboratory Name. Environmental Chemists PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO?) as N oo615 <0.02 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.04 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P00665 0.27 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L lissolved Solids:Total 70300 642.00 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 4.60 units Ba - Barium 01007 ug/L TOC o068o 3.5 mg/L Ca - Calcium 00916 mg/L Chloride 00940 295 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total wom ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 ug/L Sulfate oo945 100 mg/L Hg - Mercury 71900 ug/L pecific Conductance 00095 tiMhos K - Potassium 00937 mg/L Total Ammonia oo6to 0.50 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen: NNas N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L, TKN as N 00625 0.60 mg/L Ni - Nickel01067 ug/L Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type Certification No. DWQ#94 Pb - Lead olo51 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): Sodium 98.9 mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? Yes (0) ❑ No(0) VOC 78732: method # SM 6200C method # method # method # plete, and that the laboratory analytic possibility of fines and imprisonment / a 000110 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM A1,ILI I T INt' VKMA I IUN Please Print Clearly or Type acility Name: Valley Proteins Inc.- Rose Hill 'ermit Name (if different): acility Address: 469 Yellow Cut Rd. Rose Hill, NC 28458 County Duplin Contact Person: Corey Lanier Telephone#: (910) 660-1173 Well Location/Site Name No. of wells to be sampled: 11 (from Permit) IIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: -• .•-.- -.. _ .... _. _ WELL ID NUMBER (from Permit): MW-11A Date sample collected: 711112020 Well Depth: 16 ft. Well Diameter: 2 in. Depth to Water Level 82546: 5.8 Screened Interval: 16 ft. to 6 ft. Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfittered: X YES M NO and field acidified: X YES NO FIELD ANALYSES: pH4500Ha 5.00 units Temp. 000i( Spec. Cond. 00094: Odor 0ao85: None Appearance Clear 191 °C ItMhos If WELL WAS DRY at time of sampling, checl� here: LABORATORY INFORMATION —J Date sample analyzed. 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.35 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.76 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): lissolved Solids:Total 70300 456.00 mg/L Al -Aluminum 01105 mg1L Sodium 71.6 mg/L pH (Lab) 00403 5.00 units Ba - Barium 01007 ug/L TOC 006e0 2.70 mg/L Ca - Calcium 00916 mg/L Chloride 00940 150 mg/L Cd - Cadmium 01027 ug/L Arsenic01002 ug/L Chromium: Totaloio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 165.0 mg/L Hg - Mercury 719W ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 tiMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. N" as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # =or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Darrell Sanford - General Manager Permtttee (or Authorized Agent) Name and Title - Please print or type nature of Perm ttuthorized Agent) (Date) DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled. 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH45o0FIB: 4.80 units Temp. 00010: 19 °C DRY at Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: iiMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear chec" Samples for metals were collected unfiltered: XYESM NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0,02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 315N /100mL Phosphorus: Total as P 00665 0.74 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 233.00 mg/L Al - Aluminum of lo5 mg/L Sodium 52.5 mg/L pH (Lab) 00403 4.80 units Ba - Barium 01007 ug/L TOC oow 1.60 mg/L Ca - Calcium oo916 mg/L Chloride 00940 76 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 85 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance OW95 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. Wjas N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg1L Effluent I otal VUCs: Darrell Sanford - General Manager Penniree (or Authorized Agent) Name and Title - Please print or type Authorized Agent) mg/L VUt: Kemoval /e GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM I-AGILIIY INFORMATION Please Print Clearly or Type Facility Name: Valley Proteins Inc.- Rose Hill Permit Name (if different): Facility Address: 469 Yellow Cut Rd, Rose Hill, NC 28458 County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name: No. of wells to be sampled. 11 (from Permit) DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-907-6306 PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: ... �,. ., If WELL WELL ID NUMBER (from Permit): MW-13A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.30 units Temp. 000lo: 19.9 °C DRY at Depth to Water Level 82546: 5.1 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance White Tint checlt — Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES n NO hPrP I ite sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 iRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.12 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oos65 0.09 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total 70300 36.00 mg/L At - Aluminum of 1o5 mg/L Sodium 5.62 mg/L pH (Lab) 00403 5.30 units Ba - Barium 01007 ug/L TOC oo68o 0.60 mg/L Ca - Calcium oo916 mg/L Chloride oo94o <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 7.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) acific Conductance 00095 uMhos K - Potassium o0937 mg/L VOC 76732: method # SM 6200C Total Ammonia oo610 <0.20 mg/L Mg - Magnesium o0927 mg/L method # (Ammonia Nitrogen, Nlj as N; Ammonia Nitrogen, Total) Mn - Manganese o1o5s 9 ug/L ,method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # r Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Darrell Sanford - General Manager ���,�ri��- /I14//' 0 �11 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permit(e Authorized Agent) ate� Please Print Clearly or Type Iliey Proteins Inc.- Rose Hill ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Facility Name: Permit Name (if different): Facility Address: 469 Yellow Cut Rd, Rose Hill, NC 28458 County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name No. of wells to be sampled: 11 (from Permit) DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW-14A Date sample collected: 7/11/2020 FIELD ANALYSES: If WELL WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.70 units Temp. 0oo1c 202 °C DRY at Depth to Water Level 82546: 4.6 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cond. 00094: ItMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checl�—� Samples for metals were collected unfiltered: X YES f 1 NO and field acidified: X YES n NO 1— l I LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Coliform: MF Fecal 31616 <2 /100mL Nitrate (NO3) as N 00620 6.47 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.07 mg/L (Note- Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L lissolved Solids:Total 70300 844.00 mg/L Al - Aluminum or1o5 mg/L pH (Lab) 00403 5.70 units Ba - Barium 01007 ug/L TOC oo68o 3.60 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 285 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron olo45 ug/L Sulfate o0945 202 mg/L Hg - Mercury 71900 ug/L specific Conductance 00095 ItMhos K - Potassium 00937 mg/L Total Ammonia oo610 <0.20 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen, Nyas N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L :or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Darrell Sanford - General Manager �� Penmttee (or Authorized Agent) Name and Title - Please print or type Signature of Certification No. DWQ#94 Pb - Lead oiml ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): Sodium 118 mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ■ Yes (0) ❑ No (0) VOC 78732: method # SM 6200C method # method # method # Authorzed Agent) mg/L Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 14A November-20 642 844 July-20 592 908 March-20 659 1180 November-19 637 1120 July-19 535 903 March-19 736 1220 November-18 659 1160 pH 6.5-8.5 1 2 7A 8A l0A 11A 12B 13A 14A November-20 5.00 6.40 4.50 5.00 4.60 5.00 4.80 5.30 5.70 July-20 4.90 6.20 5.10 5.60 5.60 4.30 4.20 5.00 5.80 March-20 5.00 4.00 5.40 4.90 5.10 5.00 4.90 5.20 November-19 5.29 5.42 4.98 5.03 4.62 5.55 5.39 July-19 5.78 5.33 5.41 4.88 5.93 5.93 March-19 5.60 5.51 3.83 5.59 4.18 4.60 4.21 5.23 4.95 November-18 5.63 5.74 4.78 5.25 4.90 1 4.78 4.34 5.47 4.90 TOC 10 9 November-20 43.2 July-20 37.7 March-20 November-19 46.1 July-19 March-19 42.5 November-18 46.2 Chloride 250 10A 14A November-20 295 285 July-20 299 March-20 339 November-19 288 July-19 March-19 286 November-18 291 GW-59A CONIPLIANCE REPORT FORM Permit k NVQ1100041• (gnhmit nne ach narnitrrring Prriud u•hh 01'.19 f rrra,.l I Enter date monitoring results were due. (12131/2020) Will this monitoring report (GW-69 and GW-59A) be submitted after the established due date? No 2 Was any required information missing on the GW-59 report forms' No IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC, moving the replacement well 10' due North per DEQ direction. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missingidentification plate, area overgrown, etc.)' lfthe ansv-er is "Yes ", contact the Regional Once for guidance. No 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 6. f the answer to question 4 Is "YES" list the affected wells individually with constiluent(s) and concentration($) exceeding Standards in the space provided below: SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 For the constituents Identified In question 4 above, have standards been exceeded previously for the same consthuent(s) in the same well(s) In the last two years? YES If the answer to question 5 is "NO', skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer Is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division Involving this groundwater quality problem? YES If the answerto question 7 is 'YES', describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility, Failure to do so may subject the permittee to a Notice of Violation fines and/or enatties. Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office. g The parson completing this portion (G W-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form, 1 hereby acknowledge that the above information was evaluated and the Information submitted in this report (Compliance Report GW-69A) Is true and complete to the best of my knowledge. Signature of Pertnittee (or A gent) Data envirochem SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(d environmentaIchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50673 Site: MW-1 11/21/2020 11:48 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 11/21/2020 Depth to water, ft. Depth to water, Ft 3.4 feet 11/21/2020 Sodium EPA 200.7 5.67 mg/L 11/25/2020 Sulfate EPA 300.0 78 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2020 Odor Qualitative None 11121 /2020 Total Dissolved Solids (TDS) SM 2540 C 144 mg/L 11/23/2020 Temperature SM 2550 B 20.4 C 11/21/2020 Chloride SM 4500 CI E 7 mg/L 11/30/2020 pH SM 4500 H B 5.0 units 11121 /2020 Total Phosphorus SM 4500 P F 0.27 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 1.3 mg/L 11 /23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethene SM62008 <0.5pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2,3-Trichloropropane SM0200B <0.5pg/L 11/26/2020 1,2,4-Trichlorobenzene SM62008 <0.5pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 8200B <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 62008 <0.5 pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 Report # 2020.19896 Page 1 of 33 010�- envirochem ANALYTICAL $ CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info6d environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 62008 <0.5pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichlorobenzene SM62oo6 <0.5pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 62008 <0.5pg/L 11/26/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 62008 <0.5pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 62008 <0.5 pg/L 11/26/2020 Chloroform SM 62008 <0.5 pg/L 11/26/2020 Chloromethane SM 6200B <0.5 pg/L 11/26/2020 cis- 1,2-Dich loroethene SM 6200B <0.5 pg/L 11/26/2020 cis- 1, 3-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Dibromomethane SM 62008 <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11126/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 I sopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B < 1.0 pglL 11/26/2020 Report # 2020.19896 Page 2 of 33 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 # 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200E <0.5 pg/L 11/26/2020 n-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 62008 <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 62005 <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 µg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 11/23/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.60 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0.60 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeidahl Nitrogen (TKN) EPA 351.2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen 0.6 mg/L 12/05/2020 Report # 2020-19896 Page 3 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50674 Site: MW-2 11/21/2020 12:04 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 11/21/2020 Depth to water, ft. Depth to water, Ft 10.8 feet 11/21/2020 Sodium EPA 200.7 10.2 mg/L 11/25/2020 Sulfate EPA 300.0 7 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.Ogallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 C 284 mg/L 11/23/2020 Temperature SM 2550 8 20.5 C 11/21/2020 Chloride SM 4500 Cl E 10 mg/L 11 /30/2020 pH SM 4500 H B 6.4 units 11/21/2020 Total Phosphorus SM 4500 P F 0.43 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 1.5 mg/L 11 /23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,1-Thchloroethane SM 62008 <0.5 pg1L 11/26/2020 1,1,2,2-Tetrachloroethane SM 62008 <0.5pg/L 11/26/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 1, 1 -Dichloropropene SM 6200E <0,5 pg/L 11/26/2020 1,2, 3-Trichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 62008 <0.5pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 62008 <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM8200B <0.5Ng/L 11/26/2020 1,2-Dibromoethane SM 62008 <0.5 pg/L 11/26/2020 Report # 2020.19896 Page 4 of 33 :envirochem ANALYTICAL S CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info,a environmentalchemistscom Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene sMe200B <0.5pg/L 11/26/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 1112612020 Bromochloromethane SM 6200B <0.5 pg/L 11 /2612020 Bromodichloromethane SM 62008 <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5pg/L 11/26/2020 Chlorobenzene SM 6200B <0,5pg/L 11/26/2020 Chloroethane SM 62008 <0.5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 62008 <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 cis- 1, 3-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Dibromomethane SM 8200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 62008 <0.5 pg/L 11/26/2020 Ethylbenzene SM 62008 <0.5pg/L 11/26/2020 Hexachlorobutadiene SM 62008 <0.5 pg/L 11/26/2020 Isopropylbenzene SM 62008 <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Report # : 2020-19896 Page 5 of 33 envirochem6602 (sM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252A73.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoiaenvironmentalchemists com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 62008 <0.5 Ng/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 n-Propylbenzene SM 8200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 82006 <0.5 pg/L 11/26/2020 Styrene SM 6200E <0.5 pg/L 11/26/2020 tert-Butylbenzene SM e200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/26/2020 Toluene SM 62008 <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5 ug/L 11/26/2020 Trans- 1,3-dichloropropene SM 62008 <0.5pg/L 11/26/2020 Trichloroethene SM 62008 <0.5pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 Ng/L 11/26/2020 Vinyl chloride SM 62008 <0.5 Ng/L 11/26/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/23/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.18 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0 18 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 12/05/2020 Report # 2020-19896 Page 6 of 33 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(g environmentalchemistscom Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50675 Site: MW-4 11/21/2020 10:50 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Tan 11/21/2020 Depth to water, ft. Depth to water. Ft 4.3 feet 11 /21/2020 Sodium EPA 200.7 9.60 mg/L 11 /25/2020 Sulfate EPA 300.0 <5 mg/L 11/24/2020 Ammonia Nitrogen EPA350.1 <0.2mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2640 C 207 mg/L 11/23/2020 Temperature SM 2550 8 19.2 C 11/21/2020 Chloride SM 4500 Cl E < 5 mg/L 11/30/2020 pH SM 4500 H B 6.6 units 11/21/2020 Total Phosphorus SM 4500 P F 0.47 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 0,7 mg/L 11/23/2020 1, 1, 1,2-Tetrachloroethane SM 8200B <0.5 pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM62008 <0.5pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2-Trichloroethane SM 6200B <0.5pg/L 11/26/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2, 3-Trichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 52008 <0.5 ug/L 11/26/2020 1,2-Dibromoethane SM 6200E <0.5 pg/L 11/26/2020 Report # 2020.19896 Page 7 of 33 rw�-- Environmental Chemists, Inc. nvirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax SM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5943 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 62008 <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM62008 <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200E <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 62008 <0.5 pg/L 11/26/2020 Bromobenzene SM82008 <0.5 pg/L 11/26/2020 Bromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Bromodichloromethane SM 62008 <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 /L p9 11/26/2020 Chloroform SM 6200B <0.5 /L p9 11/26/2020 Chloromethane SM 6200B <0.5 /L p9 11/26/2020 cis- 1,2-Dichloroethen e SM 62008 <0.5pglL 11/2612020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Dibromomethane SM 6200E <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 62008 <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 62008 <0.5pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Report # 2020-19896 page 8 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax srn 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 8200B <0.5 pg/L 11/26/2020 p4sopropyltoluene SM 62008 <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 8200B <0.5 Wt. 11/26/2020 Toluene SM 6200B <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans-1,3-dichloropropene SM 62008 <0.5ug/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 11/26/2020 Vinyl chloride SM 620013 <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <1Colonies/100mL 11/21/2020 Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA 3532 <0.02mg/L 11/23/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/05/2020 Total Nitrogen (Caic) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 12/05/2020 Report # 2020-19896 Page 9 of 33 F"'Pw' -- —:'4447 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax - 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50676 Site: MW-7A 11/21/2020 11:25 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 11/21/2020 Depth to water, ft. Depth to wafer. Ft. 5.2 feet 11/21/2020 Sodium EPA 200.7 12.9 mg/L 11/25/2020 Sulfate EPA300.0 21 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0gallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 c 139 mg1L 11/23/2020 Temperature SM 2550 B 20.2 C 11/21/2020 Chloride SM4500ClE 60mg/L 11/30/2020 pH SM 4500 H B 4.5 units 11/21/2020 Total Phosphorus SM 4500 P F 0.48 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 8 <0.5 mg/L 11 /23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5Ng/L 11/26/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,1-Dichioroethene SM 6200B <0.5pg/L 11/26/2020 1,1-Dichloropropene SM62008 <0.5pg/L 11/26/2020 1,2,3-Trichlorobenzene SM62008 <0.5pg/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 8200B <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 Report #. 2020-19896 • Page 10 of 33 rl"- Environmental Chemists, Inc. envir nvirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392,0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sMs 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200E <0.5 pg/L 11/26/2020 1,2-Dichloroethane SM 62008 <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 62008 <0.5pg/L 11/26/2020 IA-Dichlorobenzene SM 62008 <0,5 pg/L 11/26/2020 2,2-Dichloro ro ane p p SM 6200E <0.5 pg/L 11/26/2020 2-Chiorotoluene SM 62008 <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 6200E <0.5 pg/L 11/26/2020 Bromobenzene SM 6200E <0.5 pg/L 11/26/2020 Bromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5pg/L 11/26/2020 Chlorobenzene SM 6200E <0.5 pg/L 11/26/2020 Chloroethane SM 6200E <0.5 pg/L 11/26/2020 Chloroform SM 6200E <0.5 pg/L 11/26/2020 Chloromethane SM 6200E <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 cis- 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 6200E <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200E <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200E <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200E <0.5 pg/L 11/26/2020 lsopropylbenzene SM 6200E <0.5 pg/L 11 /2612020 M+P Xylene SM 6200E <1.0 pg/L 11/26/2020 Report # . 2020-19096 Page 11 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 26458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 5200B <0.5 Ng/L 11 /26/2020 n-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 n-Propylbenzene SM 62008 <0.5 Ng/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p4sopropyltoluene SM 6200B <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 62008 <0.5 pg/L 11/26/2020 tert-Butylbenzene SM 62008 <0.5 iJg/L 11/26/2020 Tetrachloroethene SM 82008 <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 pg/L 11/26/2020 Trans- 1,2-Dich loroethene SM 6200B <0.5pg/L 11/26/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 Ng/L 11/26/2020 Fecal Coliform SM 92220 MF <1 Colonies/100ml- 11 /21 /2020 Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/23/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg1L 11 /30/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/05/2020 Total Nitrogen (Caic) Total Kjeldahl Nitrogen (TKN) EPA 351.2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 12/05/2020 Report # 2020-19896 Page 12 of 33 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax srn 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50677 Site: MW-8A 11/21/2020 11:35 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 11/21/2020 Depth to water, ft. Depth to Water, Ft 5.9 feet 11/21/2020 Sodium EPA 200.7 1.86 mg/L 11/25/2020 Sulfate EPA300.0 23mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 C 60 mg/L 11/23/2020 Temperature SM 2550 B 20.3 C 11/21/2020 Chloride SM 4500 Cl E 5 mg/L 11 /30/2020 pH SM4500 H B 5.0 units 11/21/2020 Total Phosphorus SM 4500 P F 0.46 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 0.9 mg/L 11/23/2020 1,1,1,2-Tetrachloroethane SM 62008 <0.5pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 8200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 8200B <0.5 pg/L 11/26/2020 1,1,2-Trichloroethane SM 62008 <0.5 pg/L 11/26/2020 1,1-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,1-Dichloroethene SM 6200B <0.5 ug/L 11/26/2020 1,1-Dichloropropene SM 62008 <0.5 pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5u9/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM e200B <0.5 pg/L 11/26/2020 1, 2,4-Tdmethylbenzene SM 6200B <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 62008 <0.5ug/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 Report# 2020-19898 Page 13 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910,392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200B <0,5pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 62008 <0.5pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5 pg/L 11/26/2020 2-Chlorotoiuene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 Benzene SM 6200E <0.5 pg/L 11/26/2020 Bromobenzene SM 62008 <0.5pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 62008 <0.5pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11/26/2020 Chloroform SM 62008 <0.5 pglL 11/26/2020 Chioromethane SM 6200B <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM8200B <0.5pg/L 11/26/2020 cis-1,3-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 62008 <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 62006 <0.5 pg/L 11/26/2020 Isopropylbenzene SM 62008 <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Report # 2020.19896 Page 14 of 33 Environmental Chemists, Inc. envirochem w 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax srn 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 09, 2020 Customer PO #: Customer ID: 08100027 Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200E <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11 /26/2020 n-Propylbenzene SM 62008 <0.5pg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 62008 <0.5 pg/L 11/26/2020 Toluene SM e2008 <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans- 1, 3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 62008 <0.5pg/L 11/26/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 pg/L 11 /26/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 11/23/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 1.17 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 1.17 mg/L 12/05/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 3512 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen 1.2 mg/L 12/05/2020 Report # 2020-19696 Page 15 of 33 r- 7 � --,qqqN Environmental Chemists, Inc. enviroch(I.Im6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax `sl` 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50678 Site: MW-9 11/21/2020 10:59 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan 11/21/2020 Depth to water, ft. Depth to water, Ft. 4.1 feet 11/21/2020 Sodium EPA 200.7 7.30 mg/L 11 /25/2020 Sulfate EPA 300.0 16 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 c 249 mg/L 11 /23/2020 Temperature SM 2550 B 17.3 C 11/21/2020 Chloride SM 4500 Cl E 17 mg/L 11/30/2020 pH SM 4500 H B 6.6 units 11/21/2020 Total Phosphorus SM 4500 P F 0.37 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 43.2 mg/L 11/2312020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 dig/L 11/26/2020 1, 1, 1 -Trichloroethane SM 5200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/2612020 1,1,2-Trichloroethane SM 8200B <0.5 pg/L 11/26/2020 1,1-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,1-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5 ug/L 11126/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5Ng/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11 /26/2020 1,2,4-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 62008 <0.5 dig/L 11/26/2020 1,2-Dibromoethane SM 62008 <0,5 pg/L 11/26/2020 Report 0 2020.19896 ..� Page 16 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax SM, 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infora,environmentalchemistscom Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM62008 <0.5 pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62006 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 62008 <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11 /2612020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11126/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SMe200B <0.5pg/L 11/26/2020 cis-1,2-Dichloroethene SM62008 <0.5pg/L 11/26/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM62008 <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200E <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 82008 <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+PXylene SM 6200B <1.0pg/L 11/26/2020 Report # 2020-19896 Page 17 of 33 Lenvirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoCa.envi ronmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 62006 <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5Ng/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 62008 <0.5 Ng/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-Butylbenzene SM8200B <0.5pg/L 11/26/2020 Tetrachloroethene SM 6200B <Q 5 ug/L 11/26/2020 Toluene SM 6200B <0.5 Ng/L 11/26/2020 Trans-1,2-Dichloroethene SM 8200B <0.5 pg/L 11/26/2020 Trans- 1, 3-dichloropropene SM 62008 <0.5pg/L 11/26/2020 Trichloroethene SM 62006 <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5pg/L 11/26/2020 Fecal Coliform SM 9222D MF 23 Colonies/100ml- 11/21 /2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.05 mg/I 11/23/2020 Nitrate+ Nitrite-N itrogen EPA 353 2 0.35 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0.30 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA3512 1.4mg/L 12/02/2020 Total Nitrogen Total Nitrogen 1.8 mg/L 12/05/2020 teport # 2020.19896 Page 18 of 33 F7� 7 Environmental Chemists, Inc. envirochem 6692 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sn+: 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO M Rose Hill NC 28458 Customer ID: 08100027 Attention: Report M 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50679 Site: MW-10A 11/21/2020 9:40 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear/Red Tint 11/21/2020 Depth to water, ft. Depth to Water Ft 3.6feet 11/21/2020 Sodium EPA 200 7 98.9 mg/L 11 /25/2020 Sulfate EPA 300 0 100 mg/L 11/24/2020 Ammonia Nitrogen EPA 3501 0.5 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.Ogallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 C 642 mg/L 11/23/2020 Temperature SM 2550 B 16.1 C 11121/2020 Chloride SM 4500 Cl E 295 mg/L 11 /30/2020 pH SM 4500 H B 4.6 units 11/21/2020 Total Phosphorus SM 4500 P F 0.27 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 3.5 mg/L 11 /23/2020 1, 1, 1,2-Tetrachloroethane SM 62008 <0.5 pg/L 11/26/2020 1,11-Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM6200B <0.5ug/L 11/26/2020 1,1,2-Trichloroethane SMa200B <0.5pg/L 11/26/2020 1,1-Dichloroethane SM6200B <0.5pg/L 11/26/2020 1,1-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM5200s <0.5ug/L 11/26/2020 1,2,3-Trichlorobenzene SM5200B <0.5pg/L 11/26/2020 1,2,3-Trichloropropane SM6200B <0.5Ng/L 11/26/2020 1,2,4-Trichlorobenzene SM 8200E <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 6200E <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM6200B <0.5Ng/L 11/26/2020 1,2-Dibromoethane SM 6200E <0.5 pg/L 11/26/2020 Report #:: 2020-19895 Page 19 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichloroethane SM 62008 <0.5 pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,3,5-Tdmethylbenzene SM 6200B <0.5pg/L 11/26/2020 1, 3-Dichlorobenzene SM 6200B <0, 5 pg/L 11/26/2020 1,3-Dichloropropane SM62006 <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM82008 <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 Benzene SM 62008 <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 6200e <0.5 pg/L 11/26/2020 Bromomethane sM e200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 62aoB <0.5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 pg/L 11/26/2020 Chloromethane SM 6200B <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 Dibromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 52008 <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200e <1.0 pg/L 11/26/2020 Report #. 2020-19696 Page 20 of 33 Environmental Chemists, Inc. ,,envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Date of Report: Dec 09, 2020 Customer PO #: Customer 10: 08100027 Report #: 2020-19896 Project ID: November- Monitoring Wells Methylene chloride SM 62008 <0.5 pg/L 11/2612020 Naphthalene SM 62008 <0.5pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200E <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200B <0.5pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-B utyl benzene SM 6200B <0.5pg/L 11/26/2020 Tetrachloroethene SM 62008 <0.5 pg/L 11/26/2020 Toluene SM 62008 <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans- 1,3-dichioropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 62008 <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200a <0.5 pg/L 11/26/2020 Vinyl chloride SM 62008 <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/23/2020 Nitrate+ Nitrite-N itrogen EPA 353 2 0.04 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0.04 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2 0.6 mg/L 12/02/2020 Total Nitrogen Total Nitrogen 0.6 mg/L 12/05/2020 report # 2020-19696 Page 21 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 14- 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report M 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50680 Site: MW-11A 11/21/2020 10:21 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 11/21/2020 Depth to water, ft. Depth to Water, Ft. 5.8 feet 11/21/2020 Sodium EPA 200.7 71.6 mg/L 12/01/2020 Sulfate EPA 300.0 165 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.Ogallons 11/21/2020 Odor Qualitative None 11121 /2020 Total Dissolved Solids (TDS) SM 2540 C 456 mg/L 11/23/2020 Temperature SM 2550 8 19.1 C 11/21/2020 Chloride SM 4500 Cl E 150 mg/L 11/30/2020 pH SM450011B 5.0units 11/21/2020 Total Phosphorus SM 4600 P F 0.76 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 2.7 mg/L 11/23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 62008 <0.5 Ng/L 11/26/2020 1,1,2-Trichloroethane SM 6200E <0.5 pg/L 11/26/2020 1,1-Dichloroethane SM 62008 <0.5 pg/L 11/26/2020 1, 1 -Dichloroethene SM 6200B <0.5 Ng/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 62008 <0.5 pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200S <0.5 pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 ug/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 62008 <0.5pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5pg/L 11/26/2020 Report # 2020-19896 Page 22 of 33 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sn+, 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists coin Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 62008 <0.5pg/L 11/26/2020 1,2-Dichloroethane SM 62008 <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 62008 <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 62008 <0.5pg/L 11/26/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 2-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 6200E <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200E <0.5 pg/L 11/26/2020 Bromochloromethane SM e200B <0.5 pg/L 11/26/2020 Bromodichloromethane SM 82008 <0.5 pg/L 11/26/2020 Bromoform SM e200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/26/2020 Chlorobenzene SM e2008 <0.5 pg/L 11/26/2020 Chloroethane SM 62008 <0.5pg/L 11/26/2020 Chloroform SM e200B <0.5 pg/L 11/26/2020 Chloromethane SM 62008 <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM e200B <0.5 pg/L 11/26/2020 cis-1,3-Dichloropropene SM 62008 <0.5pg/L 11/26/2020 Dibromochloromethane SM e200B <0.5 pg/L 11/26/2020 Dibromomethane SM e200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 62008 <1.0 pg/L 11/26/2020 Report # 2020-19695 Page 23 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 5M, 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 62008 <0.5 pg/L 11/26/2020 Naphthalene SM 6200s <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 n-Propylbenzene SM 62008 <0.5 pgJL 11/26/2020 ortho-Xylene SM 62008 <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200s <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/26/2020 Toluene SM 62008 <0.5 pg/L 11/26/2020 Trans-1,2-Dichloroethene SM 62008 <0.5pg/L 11/26/2020 Trans-1,3-dichloropropene SM 62008 <0.5pg/L 11/26/2020 Trichloroethene SM52008 <0.5pg/L 11/26/2020 Trichlorofluoromethane SM 6200s <0.5 pg/L 11/26/2020 Vinyl chloride SM 62008 <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 11 /23/2020 Nitrate+Nitrite-Nitrogen EPA 3532 0.35mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0.35 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 12/05/2020 Report*: 2020-19696 Page 24 of 33 AM SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab s 9I0.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50681 Site: MW-12B 11/21/2020 9:55 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 11/21/2020 Depth to water, ft. Depth to Water, Ft. 5,5 feet 11/21/2020 Sodium EPA 200.7 52.5 mg/L 11/25/2020 Sulfate EPA 300.0 85 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 c 233 mg/L 11/23/2020 Temperature SM 2550 8 19.0 C 11/21/2020 Chloride SM4500 Cl E 76 mg/L 11/30/2020 pH SM4500HB 4.8units 11/21/2020 Total Phosphorus SM 4500 P F 0.74 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 1.6 mg/L 11/23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5Ng/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/26/2020 1,1,2-Trichloroethane SM62008 <0.5ug/L 11/26/2020 1,1-Dichloroethane SM 6200B <0.5ug/L 11/26/2020 1, 1 -Dichloroethene SM 6200B <0.5 ug/L 11/26/2020 1, 1 -Dichloropropene SM 6200E <0.5 pg/L 11/26/2020 1,2,3-Trichlorobenzene SM8200B <0.5Ng/L 11/26/2020 1,2,3-Trichloropropane SM82008 <0.5pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 62008 <0.5 pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5 pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 Report # 2020-19896 Page 25 of 33 7 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2-Dichloroethane SM 62008 <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 62008 <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichloropropane SM62006 <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5pg/L 11/26/2020 2-Chlorotoluene SM8200B <0.5pg/L 11/26/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 Benzene SM 6200B <0.5 pg/L 11/26/2020 Bromobenzene SM 6200B <0.5 pg/L 11/26/2020 Bromochloromethane SM 62008 <0.5pg/L 11/26/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5pg/L 11/26/2020 Chlorobenzene SM 62008 <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11/26/2020 Chloroform SM 62008 <0.5pg/L 11/26/2020 Chioromethane SM 8200B <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 62008 <0,5pg/L 11/26/2020 cis-1,3-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Dibromomethane SM 52008 <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 62008 <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Report #. 2020-19896 Page 26 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemistacom Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 62008 <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 Ng/L 11/26/2020 ortho-Xylene SM 62006 <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 62008 <0.5 pg/L 11/26/2020 sec -Butyl benzene SM 6200B <0.5 pg/L 11/26/2020 Styrene SM 6200B <0.5 pg/L 11/26/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 82008 <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 pg/L 11/26/2020 Trans- 1, 2-Dich loroethene SM 6200B <0.5pg/L 11/26/2020 Trans- l,3-dichloropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 62008 <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 62008 <0.5 pg/L 11/26/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 11/21 /2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11 /23/2020 Nitrate+ Nitrite-N itrogen EPA 353 2 0.09 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0.09 mg/L 12/05/2020 Total Nitrogen (Calc) Total Keldahl Nitrogen (TKN) EPA 351.2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 12/05/2020 ieport # 2020-19896 Page 27 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sm, 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50682 Site: MW-13A 11/21/2020 10:14 AM Water jcblenvirochem Test Method Results Date Analyzed Color color White Tint 11/21/2020 Depth to water, ft. Depth to Water, Ft. 5.1 feet 11/21/2020 Sodium EPA 200.7 5.62 mg/L 11 /25/2020 Sulfate EPA 300.0 7 mg/L 11 /24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0gallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 C 36 mg/L 11/23/2020 Temperature SM 2550 B 19.9 C 11/21/2020 Chloride SM 4500 CI E < 5 mg/L 11/30/2020 pH SM 4500 H B 5.3 units 11/21/2020 Total Phosphorus SM 4500 P F 0.09 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 0.6 mg/L 11/23/2020 1, 1, 1,2-Tetrachloroethane SM 82008 <0.5 pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 62008 <0.5 pg/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/26/2020 1,1,2-Trichloroethane SM 62008 <0.5 pg/L 11 /26/2020 1,1-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1, 1 -Dichloroethene SM 62008 <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/26/2020 1,2,3-Trichloropropane SM 6200B <0.5pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2,4-Trimethylbenzene SM62006 <0.5pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 62008 <0.5pg/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/26/2020 Page 28 of 33 Report #. 2020-19896 :enviroc7he)m ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252-473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemismcom Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM6200B <0.5pg/L 11/26/2020 1,2-Dichloroethane sM6200s <0.5pg/L 11/26/2020 1,2-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11126/2020 1,3-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5pg/L 11/26/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM 62008 <0.5pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 Benzene SM 62008 <0.5 pg/L 11/26/2020 Bromobenzene SM 6200E <0.5 pg/L 11/26/2020 Bromochioromethane SM 6200B <0,5pg/L 11/26/2020 Bromodichloromethane SM 62008 <0.5 pg/L 11/26/2020 Bromoform SM 62008 <0.5 pg/L 11/26/2020 Bromomethane SM 6200E <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 62008 <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 62008 <0.5 pg/L 11/26/2020 Chloroform SM 62006 <0.5 pg/L 11/26/2020 Chloromethane SM 62008 <0.5 pg/L 11/26/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/26/2020 cis- 1, 3-Dich loropropene SM 6200B <0.5pg/L 11/26/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/26/2020 Dibromomethane SM 62008 <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 6200B <1.0 pg/L 11/26/2020 Report # 2020.19896 Page 29 of 33 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252,473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL $ CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 62008 <0.5 pg/L 11/26/2020 Naphthalene SM 62008 <0.5 pg/L 11/26/2020 n-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/26/2020 p-Isopropyltoluene SM 6200E <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 6200B <0,5pg/L 11/26/2020 Styrene SM 62008 <0.5 pg/L 11/26/2020 tert-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 Tetrachloroethene SM 8200E <0.5 pg/L 11/26/2020 Toluene SM 6200B <0.5 pg/L 11 /2612020 Trans- l,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans- 1,3-dich loropropene SM 6200B <0.5pg/L 11/26/2020 Trichloroethene SM 6200B <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 8200B <0.5 pg/L 11/26/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 0.03 mg/L 11 /23/2020 Nitrate+ N itrite-N itrogen EPA 363.2 0.15mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 0.12 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 12/05/2020 Report# 2020-19896 Page 30 of 33 ;sM: ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-50683 Site: MW-14A 11/21/2020 11:15 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 11121 /2020 Depth to water, ft. Depth to Water, Ft 4.6 feet 11/21/2020 Sodium EPA 200.7 118 mg/L 11 /25/2020 Sulfate EPA 300.0 202 mg/L 11/24/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/30/2020 Gallons bailed before sampling Gallons Bailed before sarnong 5.Ogallons 11/21/2020 Odor Qualitative None 11/21/2020 Total Dissolved Solids (TDS) SM 2540 C 844 mg/L 11/23/2020 Temperature SM 2550 B 20.2 C 11/21/2020 Chloride SM 4500 CI E 285 mg/L 11 /30/2020 pH SM 4500 H B 5.7 units 11/21/2020 Total Phosphorus SM 4500 P F 0.07 mg/L 12/07/2020 Total Organic Carbon (TOC) SM 5310 B 3.6 mg/L 11/23/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5pg/L 11/26/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 Ng/L 11/26/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/26/2020 1,1,2-Trichloroethane SM 6200B <0.5 Ng/L 11/26/2020 1,1-Dichloroethane SM62006 <0.5pg/L 11/26/2020 1, 1 -Dichloroethene SM 6200E <0.5 pg/L 11/26/2020 1,1-Dichloropropene SM 62008 <0.5 ug/L 11/26/2020 1,2,3-Trichiorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2,3-Trichloropropene SM 6200B <0,5pg/L 11/26/2020 1,2,4-Trichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2,4-Trimethylbenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0_5 u9/L 11/26/2020 1,2-Dibromoethane SM 6200B <0.5 Ng/L 11/26/2020 Report # 2020-19696 Page 31 of 33 :envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab # 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO M Rose Hill NC 28458 Customer ID: 08100027 Attention: Report M 2020-19896 Project ID: November - Monitoring Wells 1,2-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloroethane SM 6200B <0.5pg/L 11/26/2020 1,2-Dichloropropane SM62008 <0.5pg/L 11/26/2020 1,3,5-Trimethylbenzene SM 62008 <0.5pg/L 11/26/2020 1,3-Dichlorobenzene SM 6200B <0.5pg/L 11/26/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/26/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 11/26/2020 2,2-Dichloropropane SM62oo8 <0.5pg/L 11/26/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/26/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/26/2020 Benzene SM 62008 <0.5 pg/L 11/26/2020 Bromobenzene SM 62008 <0.5 pg/L 11/26/2020 Bromochloromethane SM 62008 <0.5 pg/L 11/26/2020 Bromodichloromethane SM 62008 <0.5pg/L 11/26/2020 Bromoform SM 6200B <0.5 pg/L 11/26/2020 Bromomethane SM 6200B <0.5 pg/L 11/26/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/26/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/26/2020 Chloroethane SM 6200B <0.5 pg/L 11/26/2020 Chloroform SM 6200B <0.5 ug/L 11126/2020 Chloromethane SM 6200B <0.5 p9/L 11/26/2020 cis-1,2-Dichloroethene SM8200B <0.5pg/L 11/26/2020 cis-1,3-Dichloropropene SM 6200B <0.5pg/L 11/26/2020 Dibromochloromethane SM 62008 <0.5pg/L 11/26/2020 Dibromomethane SM 6200B <0.5 pg/L 11/26/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/26/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/26/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/26/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/26/2020 M+P Xylene SM 62008 <1.0 pg/L 11/26/2020 Report # 2020-19896 Page 32 or 33 r7---7q9 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 4 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Dec 09, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Report #: 2020-19896 Project ID: November - Monitoring Wells Methylene chloride SM 6200B <0.5 pg/L 11/26/2020 Naphthalene SM 6200B <0.5 pg/L 11/26/2020 n-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/26/2020 ortho-Xylene sM 62008 <0.5 pg/L 11/26/2020 p4sopropyltoluene SM 6200B <0.5 pg/L 11/26/2020 sec-Butylbenzene SM 62008 <0.5 pg/L 11/26/2020 Styrene SM 62008 <0.5pg/L 11/26/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/26/2020 Tetrachloroethene SM 62008 <0.5 pg/L 11/26/2020 Toluene SM 62008 <0.5 pg/L 11/26/2020 Trans- 1,2-Dichloroethene SM 6200B <0.5pg/L 11/26/2020 Trans-1,3-dichloropropene SM5200B <0.5pg/L 11/26/2020 Trichloroethene SM 62008 <0.5 pg/L 11/26/2020 Trichlorofluoromethane SM 6200B <0.5pg/L 11/26/2020 Vinyl chloride SM 62008 <0.5 pg/L 11/26/2020 Fecal Coliform SM9222DMF <2Colonies/100ml- 11/21/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 11 /23/2020 Nitrate+ N itrite-N itrogen EPA 353.2 6.47 mg/L 11/30/2020 Nitrate Nitrogen Subtraction Method 6.47 mg/L 12/05/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2 < 0.5 mg/L 12/02/2020 Total Nitrogen Total Nitrogen 6.5 mg/L 12/05/2020 Comment: Reviewed by: Report # 2020-19896 Page 33 of 33 ,! L �� Date: // ye /L Facilje-ity dame: -Certification to 94 _ A,.- � Analyst: _ Z� Permit N: pH Reference Method SM4500 H-B -2011 Instrument ID v Calibration Time Cal Buffer 4 0 s u Cal Buffer 10 0 s u Check Buffer 7.0 s u Comments 'pH check buffer must read %ithin t 0 I pH units of the buffer's true value 4 su buffer Lot#: Ricca 20011320 Exo 1/2022 7 su buffer Lots . Ricca 2008993 Exo 70022 Sample location Sample Collection Sample Analysts pH Result ►Post -analysis Bu Time• Time♦ su Check value s u Auu -t Arw f" /irI it 019-)- o- f 3 /ia /Srl /44- //4- fVa 'ea t g �P1L �/•6 2 YR f .— ► Post analy sis buffer check is required when performing analyses at multiple sampling locations and must be %%it All pH values inpH units t i e , s u i Record all data to the nearest 0 01 s u and report to the nearest 0 1 s u Total Residual Chlorine (TRC) Reference Method: SM 4500 CI-G2011 Hach 8167 HR ( Please circle applicable N. Daily Check Post -analysis Check Sid I Time check 1 Sample I Sample 10 su buffer Lot#. Ricca 1001791 7/2021 Comments Data Qualifiers 0 1 units of the buffer's true value 117 Standard Result I Standard Sample I Collection Analysis TRC Result ( µeL or mg "L When analyzing ' Location Analyzed µgL or mg'L Comments Data Qualifiers I at mulhnln crtP<1 I Time I Tume 1 ----- --- -- ---- '—.. --I 11 TRC Dad) Chuck Standard true %aluc µg/L or mg/L acceptance range" _ _ �.,µg 1. or mg L �•� Check standards must recover within f 10°0 of the check standard's true value Annual Calibration Curve Verification Date: LOT # __ Exp, Date: __ ca�cnt Blank Value _ (When applicable Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared) Dissolved 6xygen (DO) Reference Method SM 4500 G G.-2011 Instrument ID Calibration Calibrationvanable yleterreading •Post-anaksts calibration Verification or °. efficiency venftcatiorn %%hen necessary i Time Comments TTemperatureBarometric after calibration Theoretical Calculated ress.,e _ Value mg L Value ma L ro% %hen performing a verification instead of ISample Location Sample Collection I •Sample Analysis DO readingTime Time I mg L Comments Data Qualifers • When performing analyses at multiple locations, the meter must be recahbrated at each site before analysis or a post -analysis calibration verification must be performed ' If sample is measured directly in the stream and or onsiie, only time anal%zed would be recorded with a note that they are measured in situ or immediately Temperature Reference Method SM 2550 B-2010 Instrument ID / Sample Location to •( 7 Sample 'Sample Temperature Collection Anaysis .0 Time Time /o A-- /t /-/1 /1 _._.._ • If sample measured Ldirectly m �,hs,,e.. Annual Verification Date Field P r onnN . ote: /i• L A l -C.- ,U•3 , -J 4/ / ,/ C ro e / 9,I s C or on site, only time jn, La•L C- Comments.Data Qualifiers recorded, with a note that they are measured in situ or Q.t.00I RP,, a -,)inn Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392 m.)-4 ` Sample Receipt Checklist Client: Date: Report Number: Receipt of sample: ❑ YES ❑ NO ECHEM PickupV Client Delivery ❑ UPS ❑ FedEx ❑ Other NJA ❑ 1. Were custody seals present on the cooler? YES Original temperature ❑ NO upon N/A 2. If custody seals were present, were they intact/unbroken? receipt °C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES YES ❑ NO ❑ 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified? YES NO ❑ 4. Were proper custody procedures (relinquished/received) followed? NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO B. Were tests to be performed listed on the COC? YES fiQ YES ❑ NO ❑ 9. Did samples arrive in proper containers for each test? NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? YES O ❑ NO 14. Were cyanide samples received at a pH >12? YES ❑ NO IS. Were sulfide samples received at a pH >9? YES t7 YES O NO ❑ 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES NO ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrect) preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to an by the customer. Who was notified, date and time: Volatiles Samples) were received with headspace COMMENTS: DOC. QA.002 Rev 1 'C 6602 Windmill Way ton ENVIRONMENTAL CHEMISTS, INC OFFICE:: 0392-0223'IFAX99103 2-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 3T729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2—O — /97 7 if ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: ;Zej SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream SO = Soil SL = Sludge Other: Sample Identification Collection E T g o e o e o o a U o �, U E? ®m z PRESERVATION ANALYSIS REQUESTED Date Time Temp �, o Z = a N = z °a Z T m a MW. MW X NO2, Chloride, TDS, Sulfate G G n Depth to water: C P X NO3, NH3, TP, TN (calc) G G Gallons bailed: S� C P X I Na G G pH (field): N• �7 4- C P X I Fecal Coliform G G Odor: na^'- C P X TOC G G Color: ;(c c i C P X I VOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Datelrime Received By: DateJTime 1. 2. o Temperature When Received -U: 3 C. Accepted: Rejected: Resample a uested: Delivered By: _ Received By: `G P✓ Date: Time: Comments: TUR AROUND: —T ENVIRONMENTAL CHEMISTS, INC OFFI E:910-392-0223FAX910-3 2-44824$ Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN of cusrnnv Client: Valley Proteins -Rose Hill PROJECT NAME Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: 1 = influent F = Ffflupnf W = Wpli ST = cf—..,. ¢n - Q-'.§ ci = Cl..A Sample Identification Collectior 4) E y r- 12PRESERVATION S o 2 c 0 U o c a o m t E " m m ? g Z ANALYSIS REQUESTED Date Timeemp �, o Z u in _" = _ a _ o = o MW: 2-MW 11L. 9A �t sy L o.� C P X NO2, Chloride, TDS, Sulfate G G ., Depth to water. C P X NO3, NH3, TP, TN (talc) G G Gallons bailed: C P X Na G G pH (field): 3� C P X Fecal Coliform G G Odor: *io..L C P X TOC G G Color: C P X VOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. 0 Temperature when Received C: Accepted: Rejected: Resample Requested: Delivered By: Received By: Date: Time: Comments: _ TURNAROUND: Way ton ENVIRONMENTAL CHEMISTS, INC of E:910'392-0223'FAX9103 2-44245 Analytical $ Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: sampled By: SAMPLE TYPE: I = Influent E = Effluent W = Well ST = Stream SO = S 1 SL = SI d Sample Identification Collection a m y~ 2 .o .n c° 0 1 c C9 4 t 0.c U " c= E " O w g j z PRESERVATION , a , u ge, Other. ANALYSIS REQUESTED Date Time Temp p Z u = H _" z = p z o MW: / /� IiC- MW X IN02, Chloride, TDS, Sulfate G G ^ Depth to water: C P I I X NO3, NH3, TP, TN (calc) G G Gallons bailed: C P X Na G G H field): 3 C P X Fecal Coliform G G Odor: A,,,` C P X TOC G G Color: C'" c Ili C P I X1 I JVOC (November only) G G C P G G C P G G C I P G G Transfer Relinquished By: Date/Time Received By: Dateirtme 1. 2. Tmm�nr�4..re ...L..... �......:.....a o/+. .....�,.,.......� ..,,", .�ca.c.rc.a ... r►ccepEea: Kefectea: Resample Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: 6602 Windmill Way , NC ton ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-392-02 3'IFAX9910-392- 4245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@_)environmentalchemists.com (Y1I 1 =t TInKI AAlll f`IJAlki nr r+i wn-rrim Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: oarnpleu Dy: JV7 celuDI F TVDF• E Sample Identification Collection nm `E F c a o o 0 r o a " ` c L E " O W m j z PRESERVATION ANALYSIS REQUESTED Date Time Temp z a =_ N o _ o _ g w o MW: -� 11 1r s, UL o Le'L `' MW C p X NO2, Chloride, TDS, Sulfate G G ti Depth to water: GL C P X NO3, NH3, TP, TN (calc) G G Gallons bailed: s C P X Na G G pH (field). y S/ C P X Fecal Coliform G G Odor: nO^C- C P X TOC G G Color: C P X VOC (November only) G G C P G G _ C P G G CI P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Tmmn 4�+ ...k__ b.--;.....j on. - - - --- -- - r.....�4,.� . rwyuUmm; Kesampie Kequested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: Analytical E• Consulting Chemists 4= ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 fill I GrTIn Kl AWN r1UAM nc: PY iicTr%nv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: sampler bv: RAIIAPI F TVPF• 1 - I-A.,e..• c - CKI.. ,. UU - 1AL11 cT _ _ Sample Identification P Collection a o. Ea 1- ao E 0 ° � " c o ° a � = sm L E v � m m a "r z PRESERVATION ANALYSIS REQUESTED Date Time Temp w z ° z = ° - N ., o z = o ¢ Z ° _ ' m _ o MW: �4- re •.1 t, %r L� 3 L MW C P I X NO2, Chloride, TDS, Sulfate G I G -• Depth to water: % C P X NO3, NH3, TP, TN (calc) G G Gallons bailed: C P X I Na G G H (field): y S a C P X I Fecal Coliform G G Odor: .4 ova C P X I TOC G G Color: �"� C P X 1VOC (November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date rime Received By: Date/Time 1. 2. • ���•-emu r.cceNtru: metectea: Kesample Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: 4= Analytical & Consulting Chemists Client: Valley Proteins -Rose Hill ADDRESS: Sampled By: ton, NC ENVIRONMENTAL CHEMISTS' INC 6602 Windmill WayOFFICE: 910-392-0223'ImingFAX910-392-44245 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME: Monitoring Wells REPORT NO: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: S®MD! 9= TVDC• 1 - I-01 Sample Identification Collection E r 2PRESERVATION a g 12 `E c� " a -- - ----•_-•._, Z5-6 U _ o m g z _.....,,..., -- - ..,,.., v. — vucanc, aV —Jun, �� = swage, umer. ANALYSIS REQUESTED Time Temp z i = = e g w o MW: Depth to water: Gallons bailed: =Qate �'L��e MW C P X X X NO2, Chloride, TDS, Sulfate NO3, NH3, TP, TN (talc) Na G G G C G P G G pH (field): C P X Fecal Coliform G G Odor: /ts«c C P X TOC G G Color: C P -T-X1- VOC (November only) G C G P G G C P G G C C P I T G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Tarnnarn4nrn usk— Do. ^; -- A or. __- - --- -- - raa.a.cFsacaa. metectea: Resample Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: ton 1 � � ENVIRONMENTAL CHEMISTS, INC OFFICE: 9 01392- 223FAXg910392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com mill 1 Of'"ri kil AIUr% rIJAt6r i'%r- i+r re+•rw r.v - Client: Valley Proteins -Rose Hill �• vv r vv r PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: u=I II"lctl vY Y. SA WADI G TVDC• I — 1•.p.. ..a _ �ttr..__. ... _ , -- Sample Identification p Collection a 5, r a ° m o° 8 o a _ - � = = " � m m j g z PRESERVATION o/uuge, vtner: ANALYSIS REQUESTED Date Time Temp Z z =_ o = 0 z 0 = o MW. N t 14 2 `l7"01 r MW C P X NO2, Chloride, TDS, Sulfate G G •. Depth to water: y3 C P TX NO3, NH3, TP, TN (talc) G G Gallons bailed: S� C P T X Na G G pH (field): y G 3 C P X Fecal Coliform G G Odor: A Ae C P X TOC G G Color. C P I Ix VOC (November only) G G C P G G C P _T G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 9. 2. Tmmnornfurn when D-.•o:. A -t-. w_-- - -- - r•_• LClcctt u: Kesample Kequested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: 4= Analytical & Consulting Chemists Client: Valley Proteins -Rose Hill ENVIRONMENTAL CHEMISTS, INC6602 Windmill Way OFFICE: 9 0-3 2-0223'ImingtonFAX910392-4424b NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME. Monitoring Wells REPORT NO: ACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE• I = Infl E - Effl Sample Identification p Collection 2 a b c° 0 v m _ ii a ` -' t E m g E z uent, PRESERVATION W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: ANALYSIS REQUESTED ate Time Temp z $ _ o�' _ $ _ o _ o = o // A MW: i J�/ De th to water: Gallons bailed: !/i� lot/ o G MW C P X X X NO2, Chloride, TDS, Sulfate NO3, NH3, TP, TN (calc Na G C G P G C G P G G pH (field): -cl � C P X Fecal Coliform G G Odor: &-a C P J TOC G G Color: c.(�,�/ C P X VOC (November only) G C G P G G C P G G C P _T_ G G Transfer Relinquished By: Date/Time Received By: Datefrime 1. 2. Tmmnnrm+"► .uh. 0e..e:.....1 or. - hccepxea: Rejectecl: Resample Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: • - •� Analytical & Consulting Chemists Client: Valley Proteins -Rose Hill ADDRESS: ENVIRONMENTAL CHEMISTS, INC 6602 l E' 9 01392- 22'FAX9103 2�245 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY PROJECT NAME: Monitoring Wells REPORT NO: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: Sample Identification Date SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Collection PRESERVATION E a ` = " m � ►- U ca u a r E g Z z = = i ¢ o i ANALYSIS REQUESTED Time[Temp i; MW: IL /3 R Depth to water: �` i Gallons bailed: S MW X X X NO2, Chloride, TDS, Sulfate G C G P NO3, NH3, TP, TN (calc) Na G C G P G G pH (field): C P Ix Fecal Coliform G G Odor: C P X TOC G G I Color: < <&✓ G P I X IVOC (November only) G C G P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: Delivered By: Comments: Accepted: Rejected: Received By: Resample Requested: Date: Time: TURNAROUND: Analytical & Consulting Chemists 4= Temperature when Received °C: Accepted: Rejected: Resampte Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentatchemists.com enviroche 6602 Windmill Way ton, NC 1 ENVIRONMENTAL CHEMISTS' INC OFFICE: 910392 223iIFAXg910392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com i'nl 1 C!'TIAAI Aklr% ^I w,., — e� Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: PO NO: ADDRESS: CONTACT NAME: Susan Price REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: v4e1110 ,U 1 uy._ RAIUDI K TVDG• 1 - 1-91.. . a c -. =cs,.._ . u. - - Sample Identification Collection E a N r n 6" o 0 i; a =' ° " E o m °° E g z PRESERVATION ANALYSIS REQUESTED Date Time Temp z Z=_ d o $ = o z o w o MW: �7 i� L�•t c MW C P I X NO2, Chloride, TDS, Sulfate G I G ^ Depth to water: SS C P X NO3, NH3, TP, TN (calc G G Gallons bailed: Sr C P X Na G G pH (field): f �1 c P IT X Fecal Coliform G G Odor: ✓►-.n C P X 1 I ITOC G G Color: C P X VOC (November only) G C G P G G C P G G C P G G Transfer Relinquished By: DateTTime Received By: DatelTime 1. 2. Ta_mnarntnra whoa A____._ ---- -- YRCjCl3lCU. Kesample tzequested:_ Delivered By: Received By: Date: Tim Comments: TURNAROUND: