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HomeMy WebLinkAboutWQ0000795_Monitoring - 11-2020_20201222SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: EM1617 DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P. Non -Discharge WQ0000795 UIC Permit Name (if different): NPDES Other Facility Address: P.O. BOx 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: 30 Acre Storage Pond No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): PZ-13 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: units Temp. 000lo: °C DRY at Depth to Water Level 82546: 16.1 ft. below measuring point Screened Interval: 10 ft. to 25 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/5/2020 Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L AI -Aluminum o1105 �mg/L pH (Lab) 00403 units Ba - Barium o1007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 'Pug/L. Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type 12/15/2020 GW-59 Rev.2/2010 SIIRMIT FORM ON YELLOW PAPER ONLY • . - DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: � • DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please PnntClearly orType PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P. Non -Discharge WQ0000795 UIC Permit Name (if different): NPDES Other Facility Address: P.O. BOx 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery - ❑� Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: 30 Acre Storage Pond No, of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): PZ-14 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: units Temp. 000lo: °C DRY at time ofsampling, Depth to Water Level 82546: 15.6 ft. below measuring point Screened Interval: 10 ft. to 25 ft. Spec. Cond. 00094: µMhos Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: check Volume of water pumped/bailed before sampling: gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/5/2020 Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 1100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L AI -Aluminum ol1o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VUc Kemovar io Zachary Butler ORC Permiftee (or Authorized Agent) Name and Title - Please print or type Signature of 12/15/2020 GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: �116117 DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P. Non -Discharge W00000795 UIC Permit Name (if different): NPDES Other Facility Address: P.O. BOx 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: 30 Acre Storage Pond No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): PZ-15 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 25 ft. Well Diameter: 2 in. pH 00400 units Temp. 000lo: °C DRY at Depth to Water Level 82546: 14.2 ft. below measuring point Screened Interval: 10 ft. to 25 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/5/2020 Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N omis mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al -Aluminum o11o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N, Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal /o Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type Agent) 12/15/2020 GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P. Non -Discharge WQ0000795 UIC Permit Name (if different): NPDES Other Facility Address: P.O. BOx 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City -° NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: 30 Acre Storage Pond No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): PZ-16 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: units Temp. 000lo: °C DRY at Depth to Water Level 82546: 11.9 ft. below measuring point Screened Interval: 10 ft. to 25 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/5/2020 Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N OU620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum o1105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type 12115/2020 (Date) GW-59 Rev.2/2010 ;SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 & 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 06, 2020 Post Office Box 2475 Customer PO M Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18941 Project ID: Juniper Site Piezometer Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48214 Site: PZ-13 11/5/2020 1:25 PM Water Eric McHorney Test Method Results Date Analyzed Depth to water, ft. Depth to water, Ft. 16.1 feet 11 /05/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 2048215 Site: PZ-14 11/5/2020 1:20 PM Water Eric McHorney Test Method Results Date Analyzed Depth to water, ft. Depth to water, Ft. 15.6 feet 11 /05/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48216 Site: PZ-15 11/5/2020 1:15 PM Water Eric McHorney Test Method Results Date Analyzed Depth to water, ft. Depth to Water, Ft 14.2 feet 11 /05/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48217 Site: PZ-16 11/5/2020 1:10 PM Water Eric McHorney Test Method Results Date Analyzed Depth to water, ft. Depth to Water, Ft 11.9 feet 11 /05/2020 Comment: Reviewed by: u t Report #:: 2020-18941 Page 1 of 1 4=w ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-3924424 Info@environmentalchemists.com Client: Town of Surf City PROJECT NAME: Juniper Site - Piezometer REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: f.+ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification ollection el CL F x 9 a C'� c°r m_ 5(9 c 8 = m S� `o O1 u E z Qw m g i PRESERVATION ANALYSIS REQUESTED Date Time Temp i °z = �, _ o = o z g 1 o PZ-13 C P tt f��I`l Depth to Water: 1Cf It S �. 1: ys G G PZ-14 C P iflf Depth to Water: t : �.oP G G PZ-15 C P Q ll` Depth to Water: 1:1 S G G PZ-16 k: * I C P Depth to Water: 1443 G G C P G G C P G G C P G G C P G G C P G I G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Accepted: Rejected: Resample Requested: Delivered By: Received By: Date: Time: Comments: TURNAROUND: SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: ME1617 DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P Non -Discharge w90000795 UIC Permit Name (if different): NPDES Other Facility Address: PO Box 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery Ol Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Zone 4 No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): Well 3 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 18.2 ft. Well Diameter: 2 in. pH 00400: 6.6 units Temp. o0olo: 22.0 °C DRY at Depth to Water Level 82546: 6.3 ft. below measuring point Screened Interval: 17 ft. to 18.2 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3.4 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance It yellow/clear here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: see Report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oos15 .05 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 1 /100ml- Nitrate (NO3) as N 00620 .09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 1.25 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 357 mg/L Al - Aluminum o1105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 25 mg/L Ca - Calcium 00916 mg/L Chloride 00940 130 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 .4 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type (or 12/1512020 GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY EPAOF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: jD1VIS1=WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P Non -Discharge wg0000795 UIC Permit Name (if different): NPDES Other Facility Address: PO Box 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Zone 1 No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): well 4 Date sample collected: 11/512020 FIELD ANALYSES: WAS Well Depth: 18.4 ft. Well Diameter: 2 in. pH 00400: 6.9 units Temp. 000lo: 22.9 °C DRY at Depth to Water Level 82546: 4.0 ft. below measuring point Screened Interval: 16.4 ft. to 18.4 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 2.2 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: see report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <,02 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO.) as N 00620 .17 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 .85 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 621 mg/L AI -Aluminum olim mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 5.2 mg/L Ca - Calcium oo916 mg/L Chloride 0094o 230 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Capper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance o0095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia ooslo <.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% SUBMIT FORM ON YELLOW PAPER ONLY EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: MIUDIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P Non -Discharge wg0000795 UIC Permit Name (if different): NPDES Other Facility Address: PO Box 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Zone 15 No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): Well 7 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 28.2 ft. Well Diameter: 2 in. pH 00400: 7.4 units Temp. 000lo: 19.3 °C DRY at Depth to Water Level 62546: 0.0 ft. below measuring point Screened Interval: 26.2 ft. to 28•2 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 1.7 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 0.5 (dry) gallons Appearance very clear here: ❑ Samples for metals were collected unfiltered: El YES El NO and field acidified: ❑ YES El NO LABORATORY INFORMATION Date sample analyzed: see report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 •51 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 234 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.8 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia oo6lo <•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type 12/15/2020 GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P Non -Discharge wg0000795 UIC Permit Name (if different): NPDES Other Facility Address: PO Box 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Zone 6 No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): Well 8 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 5.2 ft. Well Diameter: 2 in. pH 00400: 5.3 units Temp. 000lo: 20.7 °C DRY at Depth to Water Level 82546: 5.3 ft. below measuring point Screened Interval: 4.99 ft. to 9.99 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 3.0 ft. above land surface Relative M.P. Elevation: ft. Odor o0085: none check Volume of water pumped/bailed before sampling: 5 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: see report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 .03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 44 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 4.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 <•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type 12/15//2020 GW-59 Rev.2/2010 F"007— -71 Environmental Chemists, Inc. envirochem me6602 Windmill Way, Wihnington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax (sM 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's Lab ID Sample ID: Collect Date/Time Matrix Sampled by 2048184 Site: MW-3 11/5/2020 10:20 AM Water Eric McHorney Test Method Results Date Analyzed Color Color Lt Yellow/Clear 11/05/2020 Depth to water, ft. Depth to water, Ft 6.3 feet 11/05/2020 Ammonia Nitrogen EPA350.1 0.4mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/05/2020 Odor Qualitative None 11/05/2020 Total Dissolved Solids (TDS) SM 2540 c 357 mg/L 11/06/2020 Temperature SM 2550 B 22.0 C 11/05/2020 Chloride SM 4500 Cl E 130 mg/L 11/10/2020 pH SM 4500 H B 6.6 units 11/05/2020 Total Phosphorus SM 4500 P F 1.25 mg/L 11/18/2020 Total Organic Carbon (TOC) SM 5310 B 25.0 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM62008 <0.5Ng/L 11/06/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1, 2-Trichloroethane SM 620013 <0.5 pg/L 11/06/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1,1-Dich loropropene SM 6200B <0.5 pg/L 11/06/2020 1, 2, 3-Trich lorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 62008 <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 Report #:: 2020.18934 Page 1 of 15 SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5943 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1, 3,5-Tri methyl benzene SM 6200B <0.5 pg/L 11/06/2020 1, 3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1, 3-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 62008 <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 62008 <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 62008 <0.5 pg/L 11/06/2020 Ch loromethane SM 6200B <0.5 pg/L 11/06/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis-1, 3-Dich loropropene SM 62008 <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0.5 pg/L 11/06/2020 Naphthalene SM 62008 <0.5 pg/L 11/06/2020 Report #.: 2020-18934 Page 2 of 15 :enviroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's n-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 62008 <0.5 pg/L 11/06/2020 Styrene SM 6200B <0.5 pg/L 11/06/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Tetrachloroethene SM 5200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1 ,2-Dichloroethene SM 62008 <0.5 pg/L 11/06/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 11/06/2020 Trichloroethene SM 6200B <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 pg/L 11 /0612020 Fecal Coliform SM 9222D MF 1 Colonies/100ml- 11/05/2020 Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA 353.2 0.05 mg/L 11/05/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.14mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method 0.09 mg/L 11/13/2020 Report #:: 2020-18934 Page 3 of 15 :"envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO M Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48188 Site: MW-4 11/5/2020 10:40 AM Water Eric McHorney Test Method Results Date Analyzed Color Color Clear 11 /05/2020 Depth to water, ft. Depth to water, Ft. 4.0 feet 11 /05/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /05/2020 Odor Qualitative None 11 /05/2020 Total Dissolved Solids (TDS) SM 2540 C 621 mg/L 11/06/2020 Temperature SM 2550 B 22.9 C 11/05/2020 Chloride SM 4500 Cl E 230 mg/L 11 /10/2020 pH SM 4500 H B 6.9 units 11 /05/2020 Total Phosphorus SM 4500 P F 0.85 mg/L 11 /18/2020 Total Organic Carbon (TOC) SM 5310 B 5.2 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM e200B <0.5 pg/L 11/06/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1, 2,2-Tetrachloroethane SM 62006 <0.5 pg/L 11/06/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloroethane SM 5200B <0.5 pg/L 11/06/2020 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1, 2, 3-Trichloropropane SM 62008 <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 62008 <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 Report #:: 2020-18934 Page 4 of 15 Environmental Chemists, Inc. LL envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention. Report #: 2020-18934 Project ID: Sarge Martin Site MW's 1,2-Dichloropropane SM 62008 <0.5 pg/L 11/06/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200s <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 62008 <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 62008 <0.5 pg/L 11/06/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 62008 <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 62008 <0.5 pg/L 11/06/2020 Isopropylbenzene SM 62009 <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0.5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 Report #:: 2020-18934 Page 5 of 15 --77 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax LM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info()environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's n-Butylbenzene SM 62006 <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/06/2020 ortho-Xylene SM 62008 <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Styrene SM 6200B <0.5 pg/L 11/06/2020 tert-Butyl benzene SM 6200B <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/06/2020 Trans-1,3-dichloropropene SM 6200B <0.5pg/L 11/06/2020 Trichloroethene SM 6200B <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/06/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 11/05/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/05/2020 Nitrate+Nitrite-Nitrogen EPA353.2 0.17mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method 0.17 mg/L 11/13/2020 Report #:: 2020-18934 Page 6 of 15 Environmental Chemists, Inc. enviroChem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48188A Site: MW-4 11/5/2020 10:40 AM Water Eric McHorney Test Method Results Date Analyzed 1,1,1,2-Tetrach loroethane SM 6200B <0.5 pg/L 11 /06/2020 1,1,1-Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/06/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1,1-D ichloropropene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichloropropane SM 62008 <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloropropane SM 62008 <0.5 pg/L 11/06/2020 1, 3, 5-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 62006 <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Report # 2020.18934 Page 7 of 15 "07 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax (srn 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(a environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 6200B <0.5 pg/L 11/06/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis-1,3-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 62008 <0.5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 n-Butylbenzene SM 6200e <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 8200B <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Styrene SM 6200B <0.5 pg/L 11/06/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1,2-Dichloroethene SM6200B <0.5pg/L 11/06/2020 Trans- 1,3-dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Report #:: 2020-18934 Page 8 of 15 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax in fo(aenvironmen talchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's Trichloroethene SM 6200B <0.5 pg/L 11 /06/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11 /06/2020 Vinyl chloride SM 6200B <0.5 pg/L 11 /06/2020 Report #. 2020-18934 Page 9 of 15 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48189 Site: MW-7 11/5/2020 11:00 AM Water Eric McHorney Test Method Results Date Analyzed Color color Very Clear 11/05/2020 Depth to water, ft. Depth to water, Ft 0.0 feet 11/05/2020 Ammonia Nitrogen EPA350.1 <0.2mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 0.5 (dry) gallons 11/05/2020 Odor Qualitative None 11/05/2020 Total Dissolved Solids (TDS) SM 2540 c 234 mg/L 11/06/2020 Temperature SM 2550 B 19.3 C 11/05/2020 Chloride SM4500 Cl E 7 mg/L 11/10/2020 pH SM4500 H B 7A units 11/05/2020 Total Phosphorus SM 4500 P F 0.51 mg/L 11 /18/2020 Total Organic Carbon (TOC) SM 5310 B 1.8 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM 62008 <0.5 pg/L 11 /0612020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/06/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2, 3-Trichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 6200E <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 8200B <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 Report #. 2020.18934 Page 10 of 15 :envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichloropropane SM 6200s <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 62008 <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 6200B <0.5 pg/L 11/06/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 620013 <0.5 pg/L 11/06/2020 Ethylbenzene SM 62008 <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0.5 pg/L 11/06/2020 Naphthalene SM 62008 <0.5 pg/L 11/06/2020 Report #.. 2020-18834 Page 11 of 15 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax in foCsenvironmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's n-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Styrene SM 6200B <0.5 pg/L 11/06/2020 tert-Butyl benzene SM 62008 <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/06/2020 Trans- l ,3-dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Trichloroethene SM 6200B <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM e200B <0.5 pg/L 11/06/2020 Vinyl chloride SM 62DOB <0.5 pg/L 11/06/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 11/05/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/05/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 11/13/2020 Report #.: 2020-18934 Page 12 of 15 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax (sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info(aenvironmentalchemists com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Nov 20, 2020 Customer PO #• Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48190 Site: MW-8 11/5/2020 10:00 AM Water Eric McHorney Test Method Results Date Analyzed Color color Clear 11/05/2020 Depth to water, ft. Depth to Water, Ft 5.3 feet 11/05/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/05/2020 Odor Qualitative None 11/05/2020 Total Dissolved Solids (TDS) SM 2540 c 44 mg/L 11/06/2020 Temperature SM 2550 B 20.7 C 11/0512020 Chloride SM4500c1E 11 mg/L 11/10/2020 pH SM 4500 H B 5.3 units 11/05/2020 Total Phosphorus SM 4500 P F < 0.04 mg/L 11 /18/2020 Total Organic Carbon (TOC) SM 5310 B 4.1 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloroethene SM 62008 <0.5 pg/L 11/06/2020 1,1-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1, 2, 3-Trichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 62008 <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 Report #:: 2020-16934 Page 13 of 15 FF07— Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18934 Project ID: Sarge Martin Site MW's 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1, 3, 5-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 6200B <0. 5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 6200B <0.5 pg/L 11/06/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis-1, 3-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 62008 <0.5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 Report # 2020-18934 Page 14 of 15 r000--- Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18934 Project ID: Sarge Martin Site MW's n-Butylbenzene SM 6200B <0.5 pg/L 11 /06/2020 n-Propylbenzene SM 62008 <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 62008 <0.5 pg/L 11 /06/2020 sec-B utyl benzene SM 6200B <0.5 pg/L 11/06/2020 Styrene SM 62008 <0.5 pg/L 11/06/2020 tert-Butyl benzene SM 62008 <0.5 pg/L 11/06/2020 Tetrach loroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/06/2020 Trans-1 ,3-dichloropropene SM 62008 <0.5 pg/L 11/06/2020 Trichloroethene SM 62008 <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/06/2020 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/05/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 < 0.02 mg/L 11/05/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 0.03 mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method 0.03mg/L 11/13/2020 Comment: Reviewed by: Report #.: 2020-18934 Page 15 of 15 C rtificat;ona 94 Date: l o--� Facility dame: (TWr� e�tt at�y f{,y M4l s Analyst: ' IALi411, r PermitN:_ pH Reference Method SM4300 H-B .2011 Instrument ID Calibration Time Cal Buffer 4.0 s u Cal Buffer 10 0 s u Check Buffer 7.0 s u Comments 4. *4„A. `10 & 7 'pH check buffer must read within±0 1 pH units ofthe buffer's true value 4 su buffer Low'. Ricca 2001 B20 Exp 1/2022 7 su buffer Lou!: Ricca 2008993 Exp. 71,7022 10 su buffer Lou _ Ricca LOO 1791 72021 Sample location Sample Collection Times Sample Analysis Time♦ pH Result ►Post -analysis Buffer s u Check value s u Comments Data Qualifiers 7.3 M W S L u t v#A-'- ► Post anal} sis buffer check is required «hen performing analyses at multiple sampling locations and must be within = 0 1 units of the buffer's true salue All pH %alues in pFi units (i e , s u ) Record all data to the nearest 0.01 s u and report to the nearest 0 1 s u Total Residual Chlorine (TRC) Reference Method SM 4500 CI-G2011: Fiach 8167 HR: ( Please circle applicable Method Instrument ID Daily Check Post -analysis Time check Sample Sample Standard Result Check Std Sample TRC Result Comments Data uali Standard Collection Anal} su a L or me L (whenanahzing Location Q hers µe L or mg L at multiple sites) Analyzed Time Time µ- TRC Daily Check Standard true %atue _ µg/L or mg/I, acceptance range µg` . or mg/t Check standards must reco%cr within t 10% of the check standard's true value Annual Calibration Cune Verification Date: LOT aY Exp. Date: Reagenl Blank Value _ _.(�1hen applicable. Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference hlethod:SI,145000 G.-201 1 Instrument ID Calibration Calibration unable Meter reading • Post -analysis calibration Venficauon a verification (schen necessary) or .o efficiency Comments Time Barometnc after calibration Theoretical Calculated Temperature ressure Value m>~t Value met I I I I I I I Use this row when performing a verification instead of Sample Location I Time Sample Collection I •TSample Analysis I mRt DO reading Comments Data Qualifiers ime • When performing anal) ses at multiple locations, the meter must be -calibrated at each site before analysis or a post -analysis calibration verification must be performed If sample is measured direct)} in the stream and or onsite, only time analyzed would be recorded with a note that they are measured in situ or immediately Temperature Reference Method SM 2550 B-2010 Instrument ID. Sample 'Sample Temperature Sample Location Collection Analysis 'C Comments Data Qualifiers Time Time ,tit W - 3 M (Al-#7L /t'tw-/1 bv. -a :&0A— to :a.�-�• ..�.c . "� ' If sample is measured directly in the stream andor on site, only time Annual Verification Date _L=MQZ-G_ would be recorded, with a note that they are measured in situ or Field Personnel Note: Rev 9-2020 QA.001 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 h, 1 Sample Receipt Checklist Client-(�.R.F t�l. W�( Date: It 5c2O Report Number: — 1 0 1 A Receipt of sample: ECHEM Pickup Client Delivery ❑ JUPS ❑ FeclEx ❑ Other ❑ ❑ YES I0 NO §Q N/A 1. Were custody seals present on the cooler? ❑ YES 10 NO Jtq N/A 12. If custody seals were present, were they intact/unbroken? Original temperature uoon receipt A— "r rnrrprtarl tamnarntimm iinnn rar in+ How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO _4_7 Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COU YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? EX YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 112. Were samples received within proper holding time for requested tests? YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES CI NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** YES 10 NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 Analytical & Consulting Chemists 4= ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: Town of Surf City PROJECT NAME: Sarge Martin MW's REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: 'E` r-A.y SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Strearn_ SO = Snil SI = SliirinP nthar- Sample Identification ollection ad E c :: o E `o eC9 `o 0 a 0 E " W cog z PRESERVATION ANALYSIS REQUESTED Date Time Temp z $ _ N _ o 0 Z 0 = o MW # 3 'A • o C P X Chloride, TDS 1 S 30 10:yo4- G G Gallons Bailed: S a. X NO3, TP, NH3 G G u Depth to Water: ` C P X TOC G G L-4. 4C If ew Color: U• ,L v- C P X Fecal G G Odor: P.l-t C P X VOC (November) G G pH (field) `• SS C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received Delivered By: u Comments: C: OL- S Accepted: �/ Rejected: Resample a nested: Received By: _l��L«. �--�� Date: !I S' Time:.1 TURN ROUND: Analytical & Consulting Chemists 4= ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [_(ll 1 F('Tlrl1U Alidn r WAIAI nC r`1I4ZTr%r-tV 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info a@environmentalchem ists.com CLIENT: Town of Surf City PROJECT NAME: Sarge Martin MW's REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Saml,led Bv: f_ v ; t /v►.Av t •.A_% CAMPI P TVDF• 1 = 1.0. f G - FKl..er.4 w — uveu cr — cn _ c_a ct _ Sample Identification Collection m 'm a E o d c C7 o a c J 86 t E " x O w m 'z PRESERVATION ANALYSIS REQUESTED Date Time Temp z $ u _ 'o m _ o = xo Z O ~ m x o MW # C P X Chloride, TDS G G Gallons Bailed: S C P1- �' X NO3, TP, NH3 G G �I Depth to Water: Li % C P X TOC G G Color: C'�eo-✓ C P X Fecal G G Odor: C P X VOC (November) G G H (field) (p . Q Q C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. I cmNrraLurC wnen r[eGelveu %I: .[. a Accepieu: f Kejectea: Delivered By: Received By: .� Comments: Kesam ple : ///S�� Time: — TURNAROUND: • ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION ANn CHAIN OF r_[ISTnnv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: Town of Surf City PROJECT NAME: Sarge Martin MW's REPORT NO: )-o - ( F9 '? ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: r•.�.� SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludoe_ Other Sample Identification Collection °C E ~ n c C7 « `o a c o rn " E W m g Z PRESERVATION J ANALYSIS REQUESTED Date Time Temp z o _ 'o _ o = Z o w o MW # 3 C P ftf" X Chloride, TDS G G Gallons Balled: V• S C P L`r"s X /% )- Z, TP, NH3 G G Depth to Water: C P X TOC G G Color: \Iffl cic o v C P I X Fecal G G Odor: N V ftt C P X VOC (November) G G pH (field) "?� C P `f G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1_ 2. Temperature when Received °C: SS Accepted: Rejected: Resample eq ested: Delivered By: Received By: .tic y Date: i,fJ_z. Time: Comments: TURNAROUND: r - � Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392- 424 info@environmentalchemists.com CLIENT: Town of Surf City PROJECT NAME: Sarge Martin MW's REPORT NO: --I— - 8 S T ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: 4�-v, c. SAMPLE TYPE: I = Influent E = Effluent W = Well ST = Stream SO = Soil SL = Slud a Other Sample Identification Collection m w m0. rn wPRESERVATION � a C `o o cf7 15 `o o a c� `o , v E ow m g z 9 ANALYSIS REQUESTED Date Time Temp i o z = 'o N = 0 = = 0 a z o = ~ W mr o MW # -7 C P 6 15° X Chloride, TDS G G Gallons Bailed: S C P � I X 6 NO3, TP, NH3 G G �� Depth to Water: & C4 C P X TOC G G Color: Gltz-✓ C P X Fecal G G Odor: No-*- C P X VOC (November) G G r pH (field) 7• ;L C P G G C P G G C P G G C P G G Transfer Relinquished By: DatelTime Received By: Date/Time 1. 2. I cmNerawre when rieueivea C. -A , Accepted: +/ Rejected: Delivered By: fit-G�-ti jLy Received By: 4 c. Comments: :Zesample eq sted: Date: /'S }a Time: TU NAROUND: JUCSMI I rVKM VIN TCLLVVV rmrt:m VIVLT ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Facility Name: Surf City W.W.T.P: Permit Name (if different): Facility Address: P.O. Box 2475 Surf City Please Print Clearly or NC 28445 County Onslow IContact Person: Zachary Butler Telephone#: 910-329-1011 Well Location/Site Name: Zone H No. of wells to be sampled: 1 L ID NUMBER (from Permit): MW-9 Depth: 12 ft. h to Water Level 82546: 2 ft. below measuring point luring Point is 2.5 ft. above land surface ne of water pumped/bailed before sampling: 5 31es for metals were collected unfiltered: ❑ YES ❑ Date sample collected: 11/5/2020 Well Diameter: 2 in. Screened Interval: 2 ft. Relative M.P. Elevation: gallons DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUAUTYaNFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGK NC 27699-1817 Phone: (919) 733-3221 PERMIT Number: WQ0000795 Expiration Date: 2-28-22 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery M Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to 12 ft. ft. NO and field acidified: ❑ YES ❑ NO FIELD ANALYSES: PH 00400: 4.5 units Spec. Cond. 00094: Odor 00085: none Appearance clear If WELL Temp. 000to: 21.0 °C DRY at uMhos I time of late sample analyzed: see report Laboratory Name: Envirochem Certification No. 94 ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <.02 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 .11 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 .44 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): ssolved Solids:Total 7030o 416 mg/L AI - Aluminum of t05 mg/L PH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 5.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 190 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 .5 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 Of 12/15/2020 N1 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000795 Expiration Date: 2128/22 Facility Name: Surf City W.W.T.P. Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: P.O. Box 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Zone D No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 0040o: 4.4 units Temp. 000lo: 21.4 °C DRY at Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: 2 ft. to 12 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5 gallons Appearance clear/It yellow here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: see report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 .<.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 .03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 •55 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 130 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC om8o 1.1 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 43 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 <.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type 12/15/2020 (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT 3 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: �16117 DIVISION OF WATER OUALITYdNFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (alc) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 2/28/22 Facility Name: Surf City W.W.T.P. Non -Discharge W0000795 UIC Permit Name (if different): NPDES Other Facility Address: P.O. Box 2475 TYPE OF PERMITTED OPERATION BEING MONITORED Surf City NC 28445 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑� Spray Field ❑ Remediation: Contact Person: Zachary Butler Telephone#: 910-329-1011 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Zone C No. of wells to be sampled: 1 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11 Date sample collected: 11/5/2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 4.7 units Temp. 00010: 21.1 °C DRY at Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: 2 ft. to 12 ft. Spec. Cond. 00094: µMhos — time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5 gallons Appearance ltyellow/turb here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: see report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 .07 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 1 /100mL Nitrate (NO3) as N 00620 <.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.04 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 113 mg/L AI - Aluminum o1105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 3.5 mg/L Ca - Calcium 00916 mg/L Chloride 00940 133 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 <.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH,as N; Amrania Nitrogen, Total) Mn - Manganese 01055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC Permittee (or Authorized Agent) Name and Title - Please print or type 12115/2020 G W-59 Rev. 212010 SUBMIT FORM ON YELLOW PAPER ONLY OUNDWATER QUALITY MONITORING: MPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Surf City W.W.T.P. Permit Name (if different): Facility Address: P.O. Box 2475 Surf City NC 28445 County Onslow IContact Person: Zachary Butler Well Location/Site Name: Zone A WELL ID NUMBER (from Permit): MW-12 Well Depth: 12 ft. Depth to Water Level 82546: 3.1 ft. below measuring point Measuring Point is 2.5 ft. above land surface Volume of water pumped/bailed before sampling: 5.0 SamDles for metals were collected unfiltered: ❑ YES ❑ Telephone#: 910-329-1011 No. of wells to be sampled: 1 Date sample collected: 11/5/2020 Well Diameter: 2 in. Screened Interval: 2 ft. Relative M.P. Elevation: gallons DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 7333221 PERMIT Number: WQ0000795 Expiration Date: 2/28/22 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑� Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge to 12 ft. ft. NO and field acidified: ❑ YES ❑ NO ❑ Water Source Heat Pump ❑ Other FIELD ANALYSES: pH 0040o: 5.6 units Spec. Cond. 00094: Odor 00085: none Appearance yellow/turb Temp. 00010: 19.9 °C DRY at uMhos I time of Date sample analyzed: See report Laboratory Name: Envirochem Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal ,31616 7 /100mL Nitrate (NO3) as N 00620 .03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 .55 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 439 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 20.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 199 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 000m µMhos K - Potassium 00937 mg/L VOC 78732: method # Total Ammonia 00610 .4 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Zachary Butler ORC 12/15/2020 Permittee (or Authorized Agent) Name and Title - Please print or type Sign of Permitt (or Authorized Agent) (Date) GW-59 Rev.2/2010 [a] F0007- I Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48200 Site: MW-9 11/5/2020 12:00 PM Water Eric McHorney Test Method Results Date Analyzed Color Color Clear 11/05/2020 Depth to water, ft. Depth to Water, Ft. 2.0 feet 11 /05/2020 Ammonia Nitrogen EPA 350.1 0.5 mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11 /05/2020 Odor Qualitative None 11 /05/2020 Total Dissolved Solids (TDS) SM 2540 C 416 mg/L 11/06/2020 Temperature SM 2550 B 21.0 C 11 /05/2020 Chloride SM4500CIE 190mg/L 11/10/2020 pH SM 4500 H B 4.5 units 11 /05/2020 Total Phosphorus SM 4500 P F 0.44 mg/L 11 /18/2020 Total Organic Carbon (TOC) SM 5310 B 5.2 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM 5200B <0.5 pg/L 11 /06/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/06/2020 1,1,2-Trichloroethane SM 620oB <0.5 pg/L 11/06/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloropropene sM6200s <0.5pg/L 11/06/2020 1,2, 3-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichloropropane SM 6200B <0.5pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 8200B <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 8200E <0.5 Ng/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM 6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5pg/L 11/06/2020 1,2-Dichloroethane SM 62008 <0.5 pg/L 11/06/2020 Report #:: 2020-18937 Page 1 of 12 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18937 Project ID: Juniper Site MWs 1,2-Dichloropropane SM 62006 <0.5 pg/L 11/06/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1, 3-Dich lorobenzene SM 62008 <0.5 pg/L 11/06/2020 1, 3-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Ch lorotol uene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 62006 <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 62008 <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 620OB <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 620DB <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 6200B <0.5 pg/L 11/06/2020 cis-1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis- 1,3-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0.5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 Report #:: 2020-16937 Page 2 of 12 Eenvirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18937 Project ID: Juniper Site MWs n-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200E <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200E <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11 /0612020 Styrene SM 6200E <0.5 pg/L 11/06/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1,2-Dichloroethene SM 6200B <0.5pg/L 11/06/2020 Trans- 1, 3-d ichloropropene SM 6200B <0.5pg/L 11/06/2020 Trichloroethene SM 62008 <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/06/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 11 /05/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 3532 < 0.02 mg/L 11/05/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.11 mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method 0.11 mg/L 11/13/2020 Report #.: 2020-18937 Page 3 of 12 r- Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 4M' 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48201 Site: MW-10 11/5/2020 12:20 PM Water Eric McHorney Test Method Results Date Analyzed Color Color Lt Yellow/Clear 11 /05/2020 Depth to water, ft. Depth to water, Ft 5.2 feet 11 /05/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/05/2020 Odor Qualitative None 11 /05/2020 Total Dissolved Solids (TDS) SM 2540 C 130 mg/L 11/06/2020 Temperature SM 2550 B 21.4 C 11/05/2020 Chloride SM 4500 Cl E 43 mg/L 11/10/2020 pH SM 4500 H B 4.4 units 11/05/2020 Total Phosphorus SM 4500 P F 0.55 mg/L 11 /18/2020 Total Organic Carbon (TOC) SM 5310 B 1.1 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1, 1 -Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/06/2020 1,1,2-Trichloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 1,2, 3-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM6200B <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 Report #.: 2020-18837 Page 4 of 12 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab , 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoL!environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18937 Project ID: Juniper Site MWs 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,3,5-Trimethylbenzene SM 6200B <0.5pg/L 11/06/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1, 3-Dichloropropane SM 52008 <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM62006 <0.5pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 6200B <0.5 pg/L 11/06/2020 cis- 1,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis-1, 3-Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 I sopropylbenzene SM 6200e <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0.5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 Report # 2020-18937 Page 5 of 12 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@)environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs n-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/06/2020 ortho-Xylene SM 62008 <0.5 pg/L 11/06/2020 p-lsopropyltoluene SM 62008 <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 62008 <0.5 pg/L 11/06/2020 Styrene SM 6200B <0.5 Ng/L 11/06/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 ug/L 11/06/2020 Trans- 1,2-Dichloroethene SM 62008 <0.5 pg/L 11/06/2020 Trans- 1,3-dichloropropene SM 6200B <0.5ug/L 11/06/2020 Trichloroethene SM 6200B <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 ug/L 11/06/2020 Fecal Coliform SM 92220 MF <1 Colonies/100ml- 11/05/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 11 /05/2020 Nitrate+ N itrite-Nitrogen EPA 353.2 0.03 mg/L 11 /09/2020 Nitrate Nitrogen Subtraction Method 0.03 mg/L 11/13/2020 Report #.: 2020-18937 Page 6 of 12 envirochem C) ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC 28445 Attention: Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-48202 Site: MW-11 11/5/2020 12:40 PM Water Eric McHorney Test Method Results Date Analyzed Color Color Lt Yellow/Turb 11/05/2020 Depth to water, ft. Depth to Water, Ft. 5.8 feet 11/05/2020 Ammonia Nitrogen EPA350.1 < 0.2 mg/L 11/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0gallons 11/05/2020 Odor Qualitative None 11/05/2020 Total Dissolved Solids (TDS) SM 2540 C 113 mg/L 11/06/2020 Temperature SM 2550 B 21.1 C 11/05/2020 Chloride SM 4500 Cl E 133 mg/L 11 /10/2020 pH SM 4500 H B 4.7 units 11/05/2020 Total Phosphorus SM 4500 P F < 0.04 mg/L 11 /18/2020 Total Organic Carbon (TOC) SM 5310 B 3.5 mg/L 11/06/2020 1, 1, 1,2-Tetrachloroethane SM 6200B <0.5 pg/L 11/06/2020 1,1,1-Trichloroethane SM 6200E <0.5 pg/L 11/06/2020 1,1,2,2-Tetrachloroethane SM 6200B <0.5pg/L 11/06/2020 1,1,2-Trichloroethane SM 6200E <0.5 pg/L 11/06/2020 1, 1 -Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 1, 1 -Dichloropropene SM 6200B <0.5 pg/L 11/06/2020 1,2,3-Trichlorobenzene SM 6200E <0.5 pg/L 11/06/2020 1,2,3-Trichloropropane SM 82008 <0.5 pg/L 11/06/2020 1,2,4-Trichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2,4-Trimethyl benzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dibromo-3-Chloropropane SM62COB <0.5pg/L 11/06/2020 1,2-Dibromoethane SM 6200E <0.5 pg/L 11/06/2020 1,2-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,2-Dichloroethane SM 6200B <0.5 pg/L 11/06/2020 Report # 2020-16937 Page 7 of 12 (SJi ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18937 Project ID: Juniper Site MWs 1,2-Dichloropropane SM 62008 <0.5 pg/L 11/06/2020 1, 3,5-Trimethyl benzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichloropropane SM 6200E <0.5 pg/L 11/06/2020 1,4-Dichlorobenzene SM 62008 <0.5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 6200B <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200E <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 6200B <0.5 pg/L 11/06/2020 Chloromethane SM 6200B <0.5 pg/L 11/06/2020 cis-1,2-Dichloroethene SM 62008 <0.5 pg/L 11/06/2020 cis-1, 3-Dichloropropene SM 62008 <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 6200B <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 62008 <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 I sopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200B <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0. 5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 Report # 2020-18937 Page 8 of 12 r7� -I-q I envirochem Ai `SM� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax i nfoL envi ronmentalchemists.com Town of Surf City Date of Report: Nov 20, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Report #: 2020-18937 Project ID: Juniper Site MWs n-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 n-Propylbenzene SM 6200B <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 62008 <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Styrene SM 62DOB <0.5 pg/L 11/06/2020 tert-Butyl benzene SM 620OB <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 6200B <0.5 pg/L 11/06/2020 Trans-1 ,2-Dichloroethene SM 6200e <0.5 pg/L 11/06/2020 Trans- 1,3-dichloropropene SM6200B <0.5pg/L 11/06/2020 Trichloroethene SM 6200e <0.5 pg/L 11/06/2020 Trichlorofluoromethane SM 6200B <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 pg/L 11/06/2020 Fecal Coliform SM 9222D MF 1 Colonies/100ml- 11/05/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.07 mg/L 11/05/2020 Nitrate+Nitrite- Nitrogen EPA353.2 0.03mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method <0.02mg/L 11/13/2020 Report #. 2020-18937 Page 9 of 12 FF117- -77 envirochem (sM ANALYTICAL & CONSULTING CHEMISTS Town of Surf City Post Office Box 2475 Surf City NC Attention: Lao lu sample lu: 20-48203 Site: MW-12 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 20, 2020 Customer PO #: 28445 Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) 1, 1, 1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1, 1 -Dichloroethane 1, 1 -Dichloroethene 1, 1 -Dichloropropene 1,2,3-Trichlorobenzene 1,2, 3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2-Dich lorobenzene 1,2-Dichloroethane Collect Date/Time Matrix 11/5/2020 1:00 PM Water Method Color Depth to Water, Ft EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 Cl E SM 4500 H B SM 4500 P F SM 5310 B SM 6200B SM 6200B SM 6200B SM 6200B SM 62008 SM 6200B SM 6200B SM 6200B SM 6200B SM 6200B SM 6200B SM 6200B SM 6200B SM 6200B SM 6200B Results Sampled by Eric McHorney Date Analyzed Lt Yellow/Turb 11/05/2020 3.1 feet 11/05/2020 0.4 mg/L 11 /09/2020 5.0gallons 11/05/2020 None 11/05/2020 439 mg/L 11/06/2020 19.9 C 11/05/2020 199 mg/L 11/10/2020 5.6 units 11/05/2020 0.55 mg/L 11/18/2020 20.8 mg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 <0.5 pg/L 11/06/2020 Report # 2020-18937 Page 10 of 12 SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs 1,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 1,3,5-Trimethylbenzene SM 6200B <0.5 pg/L 11/06/2020 1, 3-D ichlorobenzene SM 6200B <0.5 pg/L 11/06/2020 1,3-Dichloropropane SM 6200B <0.5 pg/L 11 /06/2020 1,4-Dichlorobenzene SM 6200B <0, 5 pg/L 11/06/2020 2,2-Dichloropropane SM 6200B <0.5 pg/L 11/06/2020 2-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 4-Chlorotoluene SM 6200B <0.5 pg/L 11/06/2020 Benzene SM 6200B <0.5 pg/L 11/06/2020 Bromobenzene SM 6200B <0.5 pg/L 11/06/2020 Bromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromodichloromethane SM 6200B <0.5 pg/L 11/06/2020 Bromoform SM 62008 <0.5 pg/L 11/06/2020 Bromomethane SM 6200B <0.5 pg/L 11/06/2020 Carbon tetrachloride SM 6200B <0.5 pg/L 11/06/2020 Chlorobenzene SM 6200B <0.5 pg/L 11/06/2020 Chloroethane SM 6200B <0.5 pg/L 11/06/2020 Chloroform SM 62008 <0.5 pg/L 11/06/2020 Chloromethane SM 6200e <0.5 pg/L 11/06/2020 cis-1, 2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 cis-1, 3-Dich loropropene SM 6200B <0.5 pg/L 11/06/2020 Dibromochloromethane SM 6200B <0.5 pg/L 11/06/2020 Dibromomethane SM 62008 <0.5 pg/L 11/06/2020 Dichlorodifluoromethane SM 6200B <0.5 pg/L 11/06/2020 Ethylbenzene SM 6200B <0.5 pg/L 11/06/2020 Hexachlorobutadiene SM 6200B <0.5 pg/L 11/06/2020 Isopropylbenzene SM 6200B <0.5 pg/L 11/06/2020 M+P Xylene SM 6200E <1.0 pg/L 11/06/2020 Methylene chloride SM 6200B <0.5 pg/L 11/06/2020 Naphthalene SM 6200B <0.5 pg/L 11/06/2020 Report #. 2020-18937 Page 11 of 12 'M ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoC environmentalchemists.com Town of Surf City Post Office Box 2475 Surf City NC Attention: 28445 Date of Report: Nov 20, 2020 Customer PO #: Customer ID: 08110024 Report #: 2020-18937 Project ID: Juniper Site MWs n-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 n-Propylbenzene SM 62008 <0.5 pg/L 11/06/2020 ortho-Xylene SM 6200B <0.5 pg/L 11/06/2020 p-Isopropyltoluene SM 6200B <0.5 pg/L 11/06/2020 sec-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Styrene SM 6200B <0.5 pg/L 11/06/2020 tert-Butylbenzene SM 6200B <0.5 pg/L 11/06/2020 Tetrachloroethene SM 6200B <0.5 pg/L 11/06/2020 Toluene SM 62008 <0.5 pg/L 11/06/2020 Trans-1 ,2-Dichloroethene SM 6200B <0.5 pg/L 11/06/2020 Trans- 1, 3-d ichloropropene SM 6200B <0.5 pg/L 11/06/2020 Trichloroethene SM 6200B <0.5 Ng/L 11/06/2020 Trichlorofluoromethane SM 62008 <0.5 pg/L 11/06/2020 Vinyl chloride SM 6200B <0.5 Ng/L 11/06/2020 Fecal Coliform SM 9222D MF 7 Colonies/100ml- 11/05/2020 Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 11/05/2020 Nitrate+Nitrite-Nitrogen EPA 3532 0.03mg/L 11/09/2020 Nitrate Nitrogen Subtraction Method 0.03mg/L 11/13/2020 Comment: Reviewed by: Report #:: 2020-16937 Page 12 of 12 Date: Analyst: C - Me..17+ Ir� pr,�ti�ication q 91 Facility Same: O Permit#: PtvY A i n i Calibration Time Cal Buffer 4 0 s u Neterence Method SX14500 H-B -201 1 Cal Buffer 10 0 s u Check Buffer 7.0 s u Instrument ID Comments A`' y 7� *PH check buffer must read within i 0 1 pH units ofthe buffer's true value 4 su buffer Lot:.'. Ricca 20011320 Exn 1/2022 7 su buffer Lot',,: Ricca 2008993 Exp. 7/70 2 10 su buffer Lotf.Ricca 1001791 7L2021 Sample location Sample Collection Sample Analysis pH Result ► Post -analysis Buffer Time Time•41-)6 s u Check value s.0 Comments Data Qualifiers �♦ ti.yj .q ► Post analysis buffer check is required when performing analyses at multiple sampling locations and must be within 0 I units of the buffer's true salue All PH values in PH units (i.e , s u ) Record all data to the nearest 001 s u and report to the nearest 0.1 s u Total Residual Chlorine (TRC) Reference Method: S,1,1 4500 CI-G201 1: Hach 8167 HR ( Please circle applicable Method Instrument ID Daih Check I Post -analysis Time check Sam le Sam le Check Std. p Sample Standard Result Standard p Collection Anal%si; TRC Result etorm L ("'henanalyzine Location Comments Data uahfiers N' _ g at multiole sites) analyzed Time Time µ$ L or mgt Q TRC Daily Check Standard true value pg/L or mg/I, acceptance range lig'l. or mgrL Check standards must recover within 110°/u of the check standard's true value Annual Calibration Cun•e Verification Date: LOT " Exp. Date: Rcaeent blank Value:(When applicable. Analyze and document a reagent blank when standards, sample dilutions or PT Samples are prepared) Dissolved Oxygen (DO) Reference Method:SM 45000 G,-2011 Instrument 1D. Calibration Calibration%ariable Meterreadine •Post-anahsiscalibrauon Verification or 'a efFicienn verification (when necessap) Time Comments Temperature Barometric after calibration Theoretical Calculated pressure Value mgL i Value mRL Use this row when Performing a verification instead of Sample Location Sample Collection •Sample Analysis DO reading Time Time met Comments.'Data Qualifiers • When performing analyses at multiple locations, the meter must be recalibrated at each site before analysis or a post -analysis calibration verification must be performed ' If sample is measured directly in the stream and or onsite, on]) time analyzed would be recorded with a note that they are'measured in situ or immediately Temperature Reference Method SM 2550 B-2010 Instrument ID Sample Location Sample Collection •Sample Analysis Temperature 'C Time Time Comments Data Qualifiers 0%w-10 1i:7�.P-. �i rlt� It.L4 �10v-13, :fir« �:�3P 1q.0I (sample is measured directly in the stream and'or on site, only time analyzed would be recorded, with a note that they are measured in situ or nual Verification Date 1"'2n7p Personnel Note: QA.001 ?020 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client:&kr� Ct � Qv-) i Date: (� 5 Z(i Report Number: '-)-o — Receipt of sample: Echem Pick up 151 Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑ ❑ YES I ❑ NO JCf N/Al 1. Were custody seals present on the cooler? ❑ YES I ❑ NO Iq N/Al 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt 'C Corrected temperature upon receipt 'C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6`C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? ES V ❑ NO 9. Did samples arrive in proper containers for each test? ES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ NO 13, Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC.QA.002 Rev 1 602 ilWay ilmington, NC 28405 ENVIRONMENTAL CHEMISTS, I N C OFFICE: 9r10 I392-0223 FAX 910-392-4424 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: Town of Surf City PROJECT NAME: Juniper MW's REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil_ St = SludnP Other - Sample Identification Collection ro E 0 a E o cc9 o o a c o m = E " x ow m z PRESERVATION ANALYSIS REQUESTED Date Time Temp z O z 0 '� 8 z x 0 z o x W o MW # C P JLJ 0} X Chloride, TDS G G r Gallons Bailed: J C P 4C' X .lG� N�3, TP, NH3 G G N Depth to Water: 2 C P X TOC G G Color: G C P X Fecal G G Odor: C P X VOC (November) G G pH (field) Lt-`4 q C P G G C P G G— C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. l emperature when Received �G: r • Accepted: V Rejected: Resample Requested:_ Delivered By: C-,-44-4- ._ Received By:� Date: /� f Time: Comments: TURNAROUND: 4= ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: Town of Surf City PROJECT NAME: Juniper MW's REPORT NO: )45 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By:a c- SAMPLE TYPE: I = Influent. E = Effluent. W = Well_ ST = Stream_ SO = Snil_ SL = Shi inP (Ithar- Sample Identification ollection m E F N 0 E `o 6 o c f7 3 `o o a m c c �' U E n W 0° g z PRESERVATION ANALYSIS REQUESTED Date Time Temp i ° z z ao N 0 = = 0 a Z ° = w ° MW # to C P t{ �� 1 X Chloride, TDS G I G Gallons Balled: S C P X i `f c ).- NO3, TP, NH3 G G Depth to Water: (p? � C P X TOC G G L-- -t 1,-w Color: aSK a. I&V C P X Fecal G G Odor: a ^ C P X VOC (November) G G pH (field) �'3 C P G G _ C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received 'C: L• S Accepted: 9/ -Rejected: Resample ec ested: Delivered B �'`'c'` ` y: Received By: Diu-- Date: !/ S L-' 7ime:-- Comments: ell, TURNAROUND: ngton ENVIRONMENTAL CHEMISTS, INC OFFCE:910f392-0223F'AX910-3 2-4424$ Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentaichemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: Town of Surf City PROJECT NAME: Juniper MW's REPORT NO: - kc4 'j 7 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: r. a GI / SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludge. Other: Sample Identification Collection F �' _2 48o a a _ o a J o m u E o W m g z z PRESERVATION ANALYSIS REQUESTED Date Time Temp Z Z _ o 0 Z _ 0 < z o W o MW # C P LM Y X Chloride, TDS G G Bailed: S • X W-41-14- IJ03, P, NH3 G G .. Depth to Water: C P X TOC G G L4. Kf,AD.- Color: C P X Fecal G G Odor: nl C P X VOC (November) G G pH (field) •7 C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: Delivered By: Comments: / cepted: Rejected: Resampleyeq ested: _Received By: Date: 1,(1 .'�-G Time: .2 TURNAROUND: 4= ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 f'C%l 1 M—ri lwl AKIM n1-1A1161 r%r- i 1�e.rr..-.v 6602 Windmill Way Wilmington, NC 28406 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: Town of Surf City PROJECT NAME: Juniper MW's REPORT NO: ),5 — ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: email: aarnatea tsv: �••�iv 1. w. CAUDI C TVDC. 1 - L.il. .....a c _ ==I . 1u - , Sample Identification Collection am F w .o a E `o ct7 o a c J t E " � W g g z PRESERVATION ANALYSIS REQUESTED Date Time Temp LU z $ _ N "_ o _ ox i O m o MW # �Ct•q C P X Chloride, TDS I� 5 �. :190 .... G G Gallons Bailed: S C P X NO3, TP, NH3 G G « Depth to Water: 38 C P X TOC G G ll+- •ta Lie, w Color: v% i of —V..6_ C P X Fecal G G Odor: C P I X VOC (November) G G pH (field) �' $ C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. T-- 11 . - - - Delivered By: Comments: i -•�+�+• r 1%W-1W% VU. mesampie eq stea: ReceivedBy: ,� Date: /� Time: % = 3a/— __ TURNAROUND: