NCG500250_Regional Office Historical File Pre 2018

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
John Nims
Parkdale Mills, Inc.
1630 West Garrison Boulevard
Gastonia, NC 28053
Dear Permittee:
1••
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JUL 14 1998
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Subject: Certificate of Coverage No. NCG500250
Renewal of General Permit
Linn Plant
Rowan County
In accordance with your application for renewal of the subject Certificate of Coverage, the Division is forwarding
the enclosed General Permit. This renewal,is valid until July 31, 2002. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North
Carolina and the U.S. Environmental Protection Agency dated December 6, 1983. If any parts, measurement
frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to request
an individual permit by submitting an individual permit application. Unless such demand is made, this certificate
of coverage shall be final and binding.
The Certificate of Coverage for your facility is not transferable except after notice to the Division. Use the enclosed
Permit Name/Ownership Change form to notify the Division if you sell or otherwise transfer ownership of the
subject facility. The Division may require modification or revocation and reissuance of the. Certificate of Coverage.
If your facility ceases discharge of wastewater before the expiration date of this permit, contact the Regional
Office listed below at [phone]. Once discharge from your facility has ceased, this permit may be rescinded.
This permit does not affect the legal requirements to obtain other permits which may be required by the Division of
Water Quality, the Division of Land Resources, Coastal Area Management Act or any other Federal or Local
governmental permit that may be required. .
If you have any questions concerning this permit,.please contact the NPDES Group at the address below.
Sincerely,
(11­� A. Preston Howard, Jr., P.E.
cc: Central Files
Mooresville _Regional Office
NPDES File
Facility Assessment Unit
P.O. Box 29535, Raleigh, North Carolina 27626-0535 [phone] FAX [phone] p&[e-mail]
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STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF" WATER QUALITY
GENERAL PERMIT NO. NCG500000
CERTIFICATE OF COVERAGE. NO. NCG500250
TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER
BLOWDOWN, CONDENSATE, EXEMPT STORMWATER, COOLING WATERS ASSOCIATED WITH
HYDROELECTRIC OPERATIONS, AND SIMILIAR WASTEWATERS UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Parkdale Mills, Inc.
is hereby authorized to discharge
cooling tower blowdown and other similar wastewaters
from a facility located at
Linn Plant
100 South Main Street
Landis
Rowan County
to receiving waters designated as subbasin 30712 in the Yadkin River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth
'in Parts I, II; III and IV of General Permit No. NCG500000 as attached.
This certificate of coverage shall become effective August 1, 1997.
This certificate of coverage shall remain in effect for the duration of the General Permit.
Signed this day July 24,1997.
r�
A. Preston Howard, Jr., P.E., Director �
Division of Water Quality
By Authority of the Environmental
Management Commission

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
�EHNR
N.C. DI PT. OF
E1,PARONTY1E,NT, ICE NI,Th
& NATURAL RESOD :CK"d
November 18, 1996 _
—NOT 25 1996
Mr. John Nims
Vice President OIVIS1611 OF ENVI"ONIAI MU
1630 West Garrison Boulevard
Gastonia, North Carolina 28053 I�a,lESV1�1E REGIONAL OFFICE
Subject: Permit Modification -Name and
Ownership Change
Parkdale Mills, Inc.
(formerly Dominion Yarn Corp.)
COC NCG500250
Rowan County
Dear Mr. Nims:
In accordance with your request received July 22, 1996, the Division is forwarding the subject
permit. The only change in this permit regards name and ownership. All other terms and
conditions in the original permit remain unchanged and in full effect. This permit modification is
issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of Agreement between North Carolina and the U. S: Environmental Protection
Agency dated December 6, 1983.
This permit does not affect the legal requirement to obtain other permits which may be
required by the Division of Environmental Management or permits required by the Division of
Land Resources, Coastal Area Management Act, or any other Federal or Local governmental
permit that may be required.
I apologize for the delay in processing your request. If you have any questions concerning
this permit, please contact Ms. Jennifer Wolfe at telephone number [phone], extension 538.
Sincerely,
w4t � C414 t)K
A.eston Howard, Jr., P.E.
cc: Central Files
rMooresville_Re`gional Office; Water Quality Section
Permits and Engineenng Unit
P.O. Box 29535, Raleigh, North Carolina 27626-0535 TAlephone 919-733-7015 FAX [phone]
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STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER
BLOWDOWN, CONDENSATE.AND SIMILAR WASTEWATERS UNDER THE
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Parkdale'Mills, Inc.
is hereby authorized to discharge non -contact cooling water from a facility located at
Parkdale Mills, Inc.
Linn Plant
Rowan County
to receiving waters designated as an unnamed tributary to Grants Creek in the Yadkin -Pee Dee River
Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in
Parts I, II, III and IV of General Permit No. NCG500000 as attached,
This certificate of coverage shall become effective November 18, 1996
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day November 18, 1996
A. Preston Howard, Jr., P.E.,Director
Division of Water Quality
By Authority of the Environmental Management Commission

ROAD CLASSIFICATION
PRIMARY HIGHWAY LIGHT -DUTY ROAD, HARD OR
HARD SURFACE IMPROVED SURFACE
SECONDARY HIGHWAY
HARD SURFACE ® UNIMPROVED ROAD
Latitude 35032'51"
Map # El 6SE
Longitude 80136'44"
Sub -basin 03-07-04
Stream Class C
Discharge Class Non -Contact Cooling Water
Receiving Stream UT to Grants Creek
Design Q variable Permit expires 7/31 /97
SCALE 1:24 000
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Parkdale Mills, Inc.
NCG500250
Rowan County

2. d DEPT. aF NA'I URAL
State of North Carolina RESOURCES
AND
COMMUNITY DEW" "ITT
Department of Environment,
Health and Natural Resources SEP 3 0 1993
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
E. T. HAYNES
DOMINION YARN CORP.(LINN PLANT
C. O. BOX 8105
LANDIS NC 28088
Dear Permittee:
DIVISION Of [Wf
HOORESVILtE FIN1 6zftt
September 30,1993
0W.401TTA
�QMOM
E3 FE F1
SEP 2 S 1993 d
Subject: DOMINION YARN CORP.(LINN PLANT
Certificate of Coverage NCG500250
General Permit NCG500000
Formerly NPDES Permit NCO080039
Rowan County
The Division of Environmental Management has recently evaluated all existing individual permits for potential
coverage under general permits currently issued by the Division. 15A N.C.A.C. 2H .0127 allows the Division to
evaluate groups of permits having similar discharge activities for coverage under general permits and issue
coverage where the Division finds control of the discharges more appropriate in this manner. The Division has
determined that the subject discharge qualifies for such coverage. Therefore, the Division is hereby issuing the
'subject Certificate of Coverage under the state-NPDES general permit no. NCG500000 which shall void NPDES
Permit NC0080039. This Certificate of Coverage is issued pursuant to the requirements of North Carolina and the
US Environmental Protection Agency Memorandum of Agreement dated December 6,1983 and as subsequently
amended.
If any parts, measurement frequencies or sampling requirements contained in this general permit are unacceptable to
you, you have the right to submit an individual permit application, associated processing fee and letter requesting
coverage under an individual permit. Unless such demand is made, this decision shall be final and binding. Please
take notice this Certificate of Coverage is not transferable. Part II, EA. addresses the requirements to be followed
in case of change of ownership or control of this discharge.
In the event that the facilities fail to perform satisfactorily, including the creation of nuisance conditions, the
Permittee shall take immediate corrective action, including those as may be required by this Division, such as the
construction ofj additional or replacement wastewater treatment or disposal facilities. Construction of any
wastewater treatment facilities will require' issuance of an Authorization to Construct from this Division.
Failure to abide by the requirements contained in this Certificate of Coverage and respective general permit may
subject the Permittee to an enforcement action by the Division of Environmental Management in accordance with
North Carolina General Statute 143-215.6A to 143-215.6C. Please note that the general permit does require
monitoring in accordance with federal law. The monitoring data is not required to be submitted to the Division
unless specifically requested, however, the permittee is required to maintain all records for a period of at least
three (3) years.
Post Office Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
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Page 2
E. T. HAYNES
DOMINION YARN CORP.(LINN PLANT
Certificate of Coverage No. NCG500250
The issuance of this Certificate of Coverage is an administrative action initiated by the Division of
Environmental Management and therefore, no fees are due at this time. In accordance with current rules, there
are no annual administrative and compliance monitoring fees for coverage under general permits. The only fee
you will be responsible for is a renewal fee at the time of renewal. The current permit expires July 31,1997.
This coverage will remain valid through the duration of the attached general permit. The Division will be
responsible for the reissuance of the general permit and at such time, you will be notified of the procedures to
follow to continue coverage under the reissued permit. Unless you fail to follow the procedures for continued
coverage, you will continue to be permitted to discharge in accordance with the attached general permit.
The issuance of this Certificate of Coverage does not preclude the Permittee from complying with any and all
statutes, rules, regulations, or ordinances which may be required by the Division of Environmental Management
or permits required by the Division of Land Resources, the Coastal Area Management Act or any Federal or
Local other governmental permit that may be required.
If you have any questions or need additional information regarding this matter, please contact either the
Mooresville Regional Office, Water Quality Section at telephone number [phone], or a review engineer in
the NPDES Group in the Central Office at telephone number 919/733-5083.
cc: Mooresville Regional Office
Central Files
,Lerely,'
�A. Preston Howar r., P.E.

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
GENERAL PERMIT NO. NCG500000
CERTIFICATE OF COVERAGE No. NCG500250
TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER BLOWDOWN,
CONDENSATE AND SIMILIAR WASTEWATERS UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulatior
promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water
Pollution Control Act, as amended,
DOMINION YARN CORP.(LINN PLANT
is hereby authorized to discharge non -contact cooling water, cooling tower and boiler blowdown wastewater from a
facility located at
DOMINION YARN CORP.(LINN PLANT
Rowan County
to receiving waters designated as the UT GRANTS CREEK/YADKIN-PEE DEE RV BS
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III ar
IV of General Permit No. NCG500000 as attached.
This certificate of coverage shall become effective November 1, 1993.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day, September 30,1993.
A. Preston Howar , Jr., P.E.,Director
Division of Environmental Management
By Authority of the Environmental Management Commission

State of North Carolina
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor
William W. Cobey, Jr., Secretary
E. T. Haynes
P. O. Box 8105
Landis, NC 28088
George T. Everett, Ph.D
Director
Permit No. NCO080039
,9t'�. Dominion Yarn Corporation
County % Rowan
Dear Mr. Haynes:
4� �f/JIy'/
In accordance with your applicatio�r f urge permit received on December 12, 1990, we
are forwarding herewith the subject state - ;S permit. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement
between North Carolina and the US Environmental Protection agency dated December 6, 1983.
May 1, 1991
ob
ZIP
4e�, A�Subject.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within
thirty (30) days following receipt of this letter. This request must be in the form of a written
petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the
Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina 27611
-7447. Unless such demand is made, this decision shall be final and binding.
Please take notice this permit is not transferable. Part II, E.4. addresses the requirements to
be followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may be
required by the Division of Environmental Management or permits required by the Division of
Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit
that may be required.
If you have any questions concerning this permit, please contact Mr. Jule Shanklin at
telephone number 919/733-5083.
Sincerely,
Original sigiwefty
Dale Overcash for
George T. Everett
cc: Mr. Jim Patrick,
ooresville-Regional-Offiee
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Permit No. NC0080039
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, . .
other lawful standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Dominion Yarn Corporation
Cod, sot r o
is hereby authorized to dischftq, w& % ,fr_o-m a facility located at
©� inn Plant
South Main Street
®Ns ^� ?Ir Landis
Rowan County
�e'F
to receiving waters designated as utributary to Grants Creek in the Yadkin -Pee Dee River
Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in
Parts I, II, and III hereof.
This permit.shall become effective May 1, 1991
This permit and the authorization to discharge shall expire at midnight on. October 31, 1994
Signed this day May 1, 1991
Original sigaed.by
Date Overcash for.
George T. Everett, Director
Division of Environmental Management
By Authority of the Environmental _Management Commission

Permit No. NC0080039
SUPPLEMENT TO PERMIT COVER SHEET
Dominion Yarn Corporation
is hereby authorized to:
1. Continue to operate a cooling water system located at Linn Plant, 100 South Main Street,
Landis, Rowan County (See Part III of this Permit), and
2. Discharge from said treatment works at the location specified --on the attached map into unnamed
tributary to Grants Creek which 'is classified Class C waters.in the Yadkin -Pee Dee River Basin.

50
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A. (). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL
Permit No. NC0080039
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial number 001. Such discharges shall be limited and monitored by the permittee as specified below:
Effluent Characteristics
Discharge Limitations Monitoring
Requirements
Lbs/day Units (specify) Measurement
Sample
*Sample
Mon. Avg. Daily Max Mon, Ava, Daily Max. Frequency
Type
Location
Flow
Monthly
Instantaneous
E
Temperature
" ' Monthly
Grab
E, U, D
Total Residual Chlorine***
Monthly
Grab.
E .
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.
*Sample Locations: E - Effluent, U - Upstream, D - Downstream
**The. temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream -of more than 2.8 °C and in
no case cause the ambient water temperature to exceed 32 'C.
***Monitoring requirements only apply if chlorine is added to the cooling water.
The permittee shall obtain authorization from the Division of Environmental Management prior to utilizing any biocide in the cooling water (See -
Part III of this Permit).
The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored monthly at the effluent by grab
sample.
There shall be no discharge of floating solids or visible foam in other than trace amounts.

PART I
Section B. Schedule of Compliance
1. The permittee shall comply with Final Effluent Limitations specified for discharges in
accordance with the following schedule:
Permittee shall comply with Final Effluent Limitations by the effective date of the
permit unless specified below.
2. Permittee shall at all times provide the operation and maintenance necessary to operate the
existing facilities at optimum efficiency.
I No later than 14 calendar days following a date identified in the above schedule of
compliance, the permittee shall submit either a report of progress or, in the case of specific
actions being required by identified dates, a written notice of compliance or noncompliance.
In the latter case, the notice shall include the cause of noncompliance, any remedial actions
taken, and the probability of meeting the next schedule requirements.

Part II
Page 1 of 14
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
SECTION A. DEFINITIONS
1. Permit Issuing Authority
The Director of the Division of Environmental Management.
2. DEM or Division
Means the Division of Environmental Management, Department of Environment, Health
and Natural Resources.
3. EMC
Used herein means the North Carolina Environmental Management Commission.
4. Act or "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended,
33 USC 1251, et. seq.
5. Mass/Day Measurements
a. The "monthly average discharge" is defined as the total mass of all daily discharges
sampled and/or measured during a calendar month on which daily discharges are
sampled -and measured, divided by the number of daily discharges sampled and/or
measured during such month. It is therefore, an arithmetic mean found by adding the
weights of the pollutant found each day of the month and then dividing this sum by the
number of days the tests were reported. The limitation is identified as "Monthly
Average" in Part I of the permit.
b. The "weekly average discharge" is defined as the total mass of all daily discharges
sampled and/or measured during the calendar week (Sunday - Saturday) on which daily
discharges are sampled and measured, divided by the number of daily discharges
sampled and/or measured during such week. It is, therefore, an arithmetic mean found
by adding the weights of pollutants found each day of the week and then dividing this
sum by the number of days the tests were reported. This limitation is identified as
"Weekly Average" in Part I of the permit.
c. The "maximum daily discharge" is the total mass (weight) of a pollutant discharged
during a, calendar day. If only one sample is taken during any calendar day the weight
of pollutant calculated from it is the "maximum daily discharge." This limitation is
identified as 'Daily Maximum," in Part I of the permit.

Part H
Page 2 of 14
d. The "average annual discharge" is defined as the total mass of all daily discharges
sampled and/or measured during the calendar year on which daily discharges are
sampled and measured, divided by the number of daily discharges sampled and/or
measured during such year. It is, therefore, an arithmetic mean found by adding the
weights .of pollutants found each day of the year and then dividing this sum by the
number of days the tests were reported. This limitation is defined as "Annual Average"
in Part I of the permit.
6. Concentration Measurement
a. The "average monthly concentration," other than for fecal coliform bacteria, is the sum
of the concentrations of all daily discharges sampled and/or measured during a calendar
month on which daily discharges are sampled and.. measured, divided by the number of
daily discharges sampled and/or measured during such month (arithmetic mean of the
daily concentration values). The daily concentration value is equal to the concentration
of a composite sample or in ,the case of grab samples is the arithmetic mean (weighted
by flow value) of all the samples collected during that calendar day. The average
monthly count for fecal coliform bacteria is the geometric mean of the counts for
samples collected during a calendar month. This- limitation is identified as "Monthly
Average" under "Other Units" in Part I of the permit.
b. The "average weekly concentration," other than for fecal coliform bacteria, is the sum
of the concentrations of all daily discharges sampled and/or measured during a calendar
week (Sunday/Saturday) on which daily discharges are sampled and measured divided
by the number of daily discharges sampled and/or measured during such week
(arithmetic mean of the daily concentration values). The daily concentration value is
equal to the concentration of a composite sample or in the case of grab samples is -the
arithmetic mean (weighted by flow value) of all the samples collected during that
calendar day. The average weekly count for fecal coliform bacteria is the geometric
mean of the counts for samples collected during a calendar week. This limitation is
identified as "Weekly Average" under "Other Units" in Part I of the permit.
c. The "maximum daily concentration" is the concentration of a pollutant discharge during
a calendar day.. If only one sample is taken during any calendar day the concentration
of pollutant calculated from it is the "Maximum Daily Concentration". It is identified
as "Daily Maximum" under "Other Units" in Part I of the permit.
d. The "average annual concentration," other than for fecal coliform bacteria, is the sum of
the concentrations of all daily discharges sampled and/or measured during a calendar
year on which daily discharges are sampled and measured divided by the number of
daily discharges sampled and/or measured during such year (arithmetic mean of the
daily concentration values). The daily concentration value is equal to the concentration
of a composite sample or in the case of grab samples is the arithmetic mean (weighted.
by flow value) of all the samples collected during that calendar day . The -average
yearly count for fecal coliform bacteria is the geometric mean of the counts for samples
collected during a calendar year.
e. The "daily average concentration" (for dissolved oxygen) is the minimum allowable
amount of dissolved oxygen required to be available in the effluent prior to discharge
averaged over a calendar day. If only one dissolved oxygen sample is taken over a
calendar day, the sample is considered to be the "daily average concentration" for the
discharge. It is identified as "daily average" in the text of Part I.

Part II
Page 3 of 14
f. The "quarterly average concentration" is the average of all samples taken over a
calendar quarter. It is identified as "Quarterly Average Limitation" in the text of Part I
of the permit.
g. A calendar quarter is defined as one of the following distinct periods: January through
March, April through June, July through September, and October through December.
7. Other Measurements
a. Flow, (MGD): The flow, limit expressed in this permit is the 24 hours average flow,
averaged monthly. It is determined as the arithmetic mean of the total daily flows
recorded during the calendar month.
b. An "instantaneous flow measurement" is a measure of flow taken at the time of
sampling, when both the sample and flow will be representative of the total discharge.
c. A "continuous flow measurement" is a measure of discharge flow from the facility
which occurs continually without interruption throughout the operating hours of the
facility. Flow shall be monitored continually except for the infrequent times when
there may be no flow or for infrequent maintenance activities on the flow device.
8. Types of Samples
a. Composite Sample: A composite sample shall consist of:
(1) a series of grab samples collected at equal time intervals over a 24 hour period of
discharge and combined proportional to the rate of flow measured at the time of
individual sample collection, or
(2) a series of grab samples of equal volume collected over a 24 hour period with the
time intervals between samples determined by a preset number of gallons passing
the sampling point. Flow measurement between sample intervals shall be
determined by use of a flow recorder and totalizer, and the present gallon interval
between sample collection fixed at no greater than 1/24 of the expected total daily
flow at the treatment system, or
(3) a single, continuous sample collected over a 24 hour period proportional
to the rate of flow.
In accordance with (1) above, the time interval between influent grab samples shall be
no greater than once per hour, and the time interval between effluent grab samples shall
be no greater than once per hour except at wastewater treatment systems having a
detention time of greater than 24 hours. In such cases, effluent grab samples may be
collected at time intervals evenly spaced over the 24 hour period which are equal in
number of hours to the detention time of the system in number of days. However, in
no case may the time interval between effluent grab samples be greater than six (6)
hours nor the number of samples less than four (4) during a 24 hour sampling period.
b.--Grab Sample: Grab samples are individual samples collected over a period of time not
exceeding 15 minutes; the grab sample can be taken manually.
9. Calculation of Means
a Arithmetic Mean: The arithmetic mean of any set of values is the summation of the
individual values divided by the number of individual values.

Part 11
Page 4 of 14
b. Geometric Mean: The geometric mean of any set of values. is the Nth root of the
product of the individual values where N is equal to the number of individual values.
The geometric mean is equivalent to the antilog of the arithmetic mean of the logarithms
of the individual values. For purposes of calculating the geometric mean, values of
zero (0) shall be considered to be one (1).
c. Weighted by, Flow Value: Weighted by flow value means the summation of each
concentration -times its respective flow divided 'by the summation of the respective
flows.
10. Calendar Day
A calendar day is defined as the period from midnight of one day until midnight of the next
day. However, for purposes of this permit, any consecutive 24-hour period that
reasonably represents the calendar day may be used for sampling.
11. Hazardous Substance
A hazardous substance means any substance designated under 40 CFR Part 116 pursuant
to Section 311 of the Clean Water Act.
12. Toxic Pollutant
A toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean Water
Act.
SECTION B. GENERAL CONDITIONS
1. Duty to Comply_
The permittee must comply with all conditions of this permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for
permit termination, revocation and reissuance, or modification; or denial of a permit
renewal application.
a. The permittee shall comply with effluent standards or prohibitions established under
section 307(a) of the Clean Water Act for toxic pollutants and with standards for
sewage sludge use or disposal established under section 405(d) of the Clean Water Act
within the time provided in the regulations that establish these standards or
prohibitions, even if the permit has not yet been modified to incorporate the
requirement.
b. The Clean Water Act provides that any person who violates a permit condition is
subject to a civil penalty not to exceed $25,000 per day for each violation.
Any person who negligently violates any permit condition is subject to criminal
penalties of $2,500 to $25,000 per day of violation, or imprisonment for not more than
1 year, or both. Any person who knowingly violates permit conditions is subject to
criminal penalties of $5,000 to $50,000 per day, of violation, or imprisonment for not
more than 3 years, or both. Also, any person who violates a permit condition may be
assessed an administrative penalty not. to exceed $10,000 per violation with the
maximum amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33
U.S.C. 1319 and 40 CFR 122.41 (a)]

Part H
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c. Understate law, a daily civil penalty. of not more than ten thousand dollars ($10,000)
per violation may be assessed against any person who violates or fails to act in
accordance with the terms, conditions, or requirements of a permit. [Ref: North
Carolina General Statutes § 143-215.6 (a)]
2. Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge in
violation of this permit which has a reasonable likelihood of adversely affecting human
health or the environment.
3. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part II, B-3) and "Power
Failures" (Part II, B-6), nothing in this permit shall be construed to relieve the permittee
from any responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS
143-215.3, 143-215.6 or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the
permittee. is responsible for consequential damages, such as fish kills, even though the
responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or
relieve the permittee from any responsibilities, liabilities, or penalties to which the permittee
is or may be subject to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act,
33 USG 1321. Furthermore, the permittee is responsible for consequential damages, such
as fish kills, even though the responsibility for effective compliance may be temporarily
suspended.
5. Property Rights_
The issuance of this permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury. to private property or
any invasion of personal rights, nor any infringement of Federal, State or local laws or
regulations.
6. Onshore or- Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore
physical structures or facilities or the undertaking of any work in any navigable waters.
7. Severability
The provisions of this permit are severable, and if any provision of this permit, or the
application of any provision of this permit to any circumstances, is held invalid, the
application of such provision to other circumstances, and the remainder of this permit, shall
not be affected thereby.

Part H
Page 6 of 14
8. Duty to Provide Information
The permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any
information which the Permit Issuing Authority may request to determine whether cause
exists for modifying, revoking and reissuing, or terminating this permit or to determine
compliance with this permit. The permittee shall also furnish to the Permit Issuing
Authority upon request, copies of records required to be kept by this permit.
9. Duty to Reapply
If the permittee wishes to continue an activity regulated by this permit after the expiration
date of this permit, the permittee must apply for and obtain a new permit.
10. Expiration of Permit
The permittee is not authorized to discharge after the expiration date. In order to receive
automatic authorization to discharge beyond the expiration date, the permittee shall submit
such information, forms, and fees as are required by the agency authorized to issue permits
no later than 180 days prior to the expiration date. Any discharge that has not requested
renewal at least 180 days prior to expiration, or any discharge that does not have a permit
after the expiration and has not requested renewal at least 180 days prior to expiration, will
subject the permittee to enforcement procedures as provided in NCGS 143-215.6 and 33
USC 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be
signed and certified.
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this
Section, a responsible corporate officer means: (a) a president, secretary, treasurer
or vice president of the corporation in charge of a principal business function, or
any other person who performs similar policy or decision making functions for the
corporation, or (b) the manager of one or more manufacturing production or
operating _facilities employing more than 250 persons or having gross annual sales
or expenditures exceeding 25 million (in second quarter 1980 dollars), if authority to
sign documents has been assigned or delegated to the manager in accordance with
corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal
executive officer or ranking elected official.
b. All reports required by the permit and other information requested by the Permit Issuing
Authority shall be signed by a person described. above or by a duly authorized
representative of that person. A person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility
for the overall operation of the regulated facility or activity, such as the position of
plant manager, operator of a well or well field, superintendent, a position of

Part II
Page 7 of 14
equivalent responsibility, or an in or position having overall responsibility
for environmental matters for the company. (A duly authorized representative may
thus be either a named individual or any individual occupying a named position.);
and
(3) The written authorization is submitted to the Permit Issuing Authority.
c. Certification. Any person signing a -document under paragraphs,a. orb. of this section
shall make the following certification:
"I certify, under penalty: of law,. that this document and all attachments were prepared
under my -direction,or supervision in accordance with a system 'designed to assure th"at
qualified personnel properly gather and evaluate the information submitted., Based on
my inquiry -of the person or persons who manage the system, or those persons directly -
responsible for- gathering the information, the information submitted is, to the best of
my knowledge and believe, true, accurate, and complete. I am aware -that there are
significant penalties for submitting false information, including the possibility of fines .
and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified; revoked and reissued," or terminated for cause.The filing of a
request by the permittee for a. permit -modification, revocation and reissuance, or
termination, or a notification of planned changes or anticipated noncompliance does not
stay. any permit condition.
13. Permit Modification. Revocation and Reissuance. or Termination
The issuance of this permit does not prohibit the permit issuing. authority from reopening
and modifying the permit, revoking and reissuing the "permit, or terminating the permit as
allowed by the laws, rules, and regulations contained in Title 40, Code of Federal
Regulations, Parts 122 and 123; Title 15A of the North Carolina Administrative Code,
Subchapter 2H .0100; a nd.North:Carolina General Statute 143-215.1 et. al.
14. Previous Permits
All previous National Pollutant Discharge Elimination System Permits issued to this
facility, whether for operation or discharge, are hereby revoked by issuance of this permit.
.The conditions, requirements, terms, andprovisions of this permit authorizing discharge -
under the National Pollutant Discharge Elimination System govern. discharges from this
facility.
SECTION C. OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
1..Certified Operator
Pursuant to Chapter 90A-44 of North Carolina General Statutes, the permittee shall
employ a certified wastewater treatment plant operator in responsible charge (ORC) of the
wastewater treatment facilities. Such operator must hold a certification of the grade
equivalent to or greater- than the classification assigned to the wastewater treatment
facilities. The permittee shall notify the Division's Operator Training and Certification Unit
within thirty days of any change in the ORC status.

Part H
Page 8 of 14
2. Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities. and systems of
treatment and control (and related appurtenances) which are installed or used by the
permittee to achieve compliance with the conditions of this permit. Proper operation and
maintenance also includes adequate laboratory controls and appropriate quality assurance
procedures. This provision requires the operation of back-up or auxiliary facilities or
similar systems which are installed by a permittee only when the operation is necessary to
achieve compliance with, the conditions of the permit.
3. Need to Halt or Reduce not a Defense
- It shall not be -a defense for a permittee in an enforcement action -that it would have been.
necessary to halt or reduce the permitted activity in order to maintain compliance with the
condition of this permit.
4.. Bypassing of Treatment Facilities
a. Definitions
(1) "Bypass" means the known diversion. of waste streams from any portion of a
treatment facility including the collection system, which is not a designed or
established or operating mode for the facility.
(2) "Severe property damage" means substantial physical damage to property,- damage
to the treatment. facilities which causes them to become inoperable, or substantial
and permanent loss of natural resources which can reasonably be expected to occur
in the absence of a bypass. Severe property damage does not mean economic loss
caused by delays in production. _
b. Bypass not exceeding limitations.
The permittee may allow any bypass, to occur which does not cause effluent limitations
to be exceeded, but only if it also is for essential maintenance to assure efficient
operation. These bypasses are not subject. to the provisions of Paragraphs c. and d. of
this section.
c. Notice
(1) Anticipated bypass. If the permittee knows.in advance of the need for a bypass, it
shall submit prior notice, if.possible at least ten days before the date of the.bypass;
including an evaluation .of the anticipated quality and affect of the bypass:
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated bypass
as required in Part II, E. 6. of this permit. (24-hour notice).
d. Prohibition of Bypass
(1) Bypass is prohibited and the Permit Issuing Authority may take enforcement action
against a permittee for bypass, unless:
(a) Bypass was unavoidable to prevent loss of life, personal injury or severe
property damage;

Part H
Page. 9 of 14
(b) There were no feasible alternatives to the bypass, such as the use of auxiliary
treatment facilities, retention of untreated wastes or maintenance during normal
periods of equipment downtime. This condition is not satisfied if adequate
backup equipment should have been installed in the exercise of reasonable
engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance; and
(c) The permittee submitted notices as required under Paragraph c. of this section.
(2) The Permit Issuing Authority may approve an anticipated bypass, after considering
its adverse affects, if the Permit Issuing Authority determines that it will meet the
three conditions listed above in Paragraph d. (1) of this section.
5. Upsets
a. . Definition.
"Upset " means an exceptional incident in which there is unintentional and
temporary noncompliance with technology based permit effluent limitations because of
factors beyond the reasonable control of the permittee. An upset does not include
noncompliance to the extent caused by operational error, improperly designed treatment
facilities, inadequate treatment facilities, lack of preventive maintenance, or careless or
improper operation.
b. Affect of an upset.
An upset constitutes an affirmative defense to an action brought for
noncompliance with such technology based permit effluent limitations if the
requirements of paragraph c. of this condition are met. No determination made during
administrative review of claims that noncompliance was caused by upset, and before an
action for noncompliance, is final administrative action subject to judicial review.
c. Conditions necessary for a demonstration of upset.
A permittee who wishes to establish the affirmative defense of upset shall demonstrate,
through properly signed, contemporaneous operating logs, or other relevant evidence
that:
(a) An upset occurred and,that the permittee can identify the cause(s) of the upset;
(b) The permittee facility was at the time being properly operated; and
(c) The permittee submitted notice of the upset as required in Part II, E. 6. (b) (B) of
this permit.
(d) The permittee complied with any remedial measures required under Part H, B. 2. of
this permit.
d. Burden of proof.
In any enforcement proceeding the permittee seeking to establish the occurrence of an
upset has the burden of proof.

Part II
Page 10 of 14
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or
control of wastewaters shall be disposed of in accordance with NCGS 143-215.1 and in a
manner such as to prevent any pollutant from such materials from entering waters of the
State or navigable waters of the United States. The permittee shall comply with all existing
federal regulations governing the disposal of sewage sludge. Upon promulgation of 40
CFR Part 503, any permit issued by the Permit Issuing Authority for the disposal of sludge
may be reopened and modified, or revoked and reissued, to incorporate applicable
requirements at 40 CFR Part 503. The permittee shall comply with applicable 40 CFR Part
503 Standards for the Use and Disposal of Sewage Sludge (when promulgated) within the
time provided in the regulation, even if the permit is not modified to incorporate the
requirement. The permittee shall notify the Permit Issuing Authority of any significant
change in its sludge use or disposal practices.
7. Power Failures
The permittee is responsible for maintaining adequate safeguards as required by DEM
Regulation, Title 15A, North Carolina Administrative Code, Subchapter 2H, .0124
Reliability, to prevent the discharge of untreated or inadequately treated wastes during
electrical power failures either by means of alternate power sources, standby generators or
retention of inadequately treated effluent.
SECTION D. MONITORING AND RECORDS
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the
volume and nature of the permitted discharge. Samples collected at a frequency less than
daily shall be taken on a day and time that is characteristic of the discharge over the entire
period which the sample represents. All samples shall be taken at the monitoring points
specified in this permit and, unless otherwise specified, before the effluent joins or is
diluted by any other wastestream, body of water, or substance. Monitoring points shall
not be changed without notification to and the approval of the Permit Issuing Authority.
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each
month and reported on a monthly Discharge Monitoring Report (DMR) Form (DEM No.
MR 1,1.1, 2, 3) or alternative forms approved by the Director, DEM, postmarked no later
than the 30th day following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in
the case of a new facility, on the last day of the month following the commencement of
discharge. Duplicate signed copies of these, and all other reports required herein, shall be
submitted to the following address:
Division of Environmental Management
Water Quality Section
ATTENTION: Central Files
Post Office Box 27687
Raleigh, North Carolina 27611

Part II
Page 11 of 14
3. Flow Measurements
Appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements
of the volume of monitored discharges. The devices shall be installed, calibrated and
maintained to ensure that the accuracy of the measurements are consistent with the accepted
capability of that type of device. Devices selected shall be capable of measuring flows with
a maximum deviation of less than 10% from the true discharge rates throughout the range
of expected discharge volumes. Once -through condenser cooling water flow which is
monitored by pump logs, or pump hour meters as specified in Part I of this permit and
based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations
published pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts,
and to regulations published pursuant to Section 304(g), 33 USC 1314, of the Federal
Water Pollution Control Act, as Amended, and Regulation 40 CFR 136.
To meet the intent of the monitoring required by this permit, all test procedures must
produce minimum detection and reporting levels that are below the permit discharge
requirements and all data generated must be reported down to the minimum detection or
lower reporting level of the procedure. If no approved methods are determined capable of
achieving minimum detection and reporting levels below permit discharge requirements,
then the most sensitive (method with the lowest possible detection and reporting level)
approved method must be used.
5. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly
renders inaccurate, any monitoring device or method required to be maintained under this
permit shall, upon conviction, be punished by a fine of not more than $10,000 per
violation, or by imprisonment for not more than two years per violation, or by both.
6. Records Retention
The permittee shall retain records of all monitoring information, including all calibration
and maintenance records and all original strip chart recordings for continuous monitoring
instrumentation, copies of all reports required by this permit, for a period of at least 3
years from the date of the sample, measurement, report or application. This period may be
extended by request of the Director at any time.
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the
permittee shall record the following information:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.

Part II
Page 12 of 14
8. Inspection and Entry
The permittee shall allow the Director, or an authorized representative, upon the
presentation of credentials and other documents as may be required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the
conditions of this permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any
location.
SECTION E. REPORTING REQUIREMENTS
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this
permit. The discharge of any pollutant identified in this permit more frequently than or at a
level in excess of that authorized shall constitute a violation of the permit.
2. Planned Changes
The permittee shall give notice to the Director as soon as possible of any planned physical
alterations or additions to the permitted facility. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for
determining whether a facility is a new source in 40 CFR Part 122.29 (b); -or
b. The alteration or addition could significantly change the nature or increase the quantity
of pollutants discharged: This notification applies to pollutants which are subject
neither to effluent limitations in the permit, nor to notification requirements under 40
CFR Part 122.42 (a) (1).
3. Anticipated Noncompliance
The permittee shall give advance notice to the Director of any planned changes in the
permitted facility or activity which may result in noncompliance with permit requirements.
4. Transfers
This permit is not transferable to any person except after notice to the Director. The
Director may require modification or revocation and reissuance of the permittee and
incorporate such other requirements as may be necessary under the Clean Water Act.

Part H
Page 13 of 14
5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit.
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See
Part II. D. 2. of this permit).
b. If the permittee monitors any pollutant more frequently than required by the permit,
using test procedures specified in Part II, D. 4. of this permit, the results of this
monitoring shall be included in the calculation and reporting of the data submitted in the
DMR.
c. Calculations for all limitations which require averaging of measurements shall utilize an
arithmetic mean unless otherwise specified by the Director in the permit.
6. Twenty-four Hour Reporting
a. The permittee shall report to the'central office or the appropriate regional office any
noncompliance which may endanger Health or the environment. Any information shall
be provided orally within 24 hours from the time the permittee became aware of the
circumstances. A written submission shall also be provided within 5 days of the time
the permittee becomes aware of the circumstances. The written submission shall
contain a description of the noncompliance, and its cause; the period of noncompliance,
including exact dates and times, and if the noncompliance has not been corrected, the
anticipated time it is expected to continue; and steps taken or planned to reduce,
eliminate, and prevent reoccurrence of the noncompliance.
b. The following shall be included as information which must be reported within 24 hours
under this paragraph.
(A) Any unanticipated bypass which exceeds any effluent limitation in the permit.
(B) Any upset which exceeds any effluent limitation in the permit.
(C) Violation of a maximum daily discharge limitation for any of the pollutants listed by
the Director in the permit to be reported within 24 hours.
c. The Director may waive the written report on a case -by -case basis for reports under
paragraph b. above of this condition if the oral report has been received within 24
hours.
7. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under Part II. E. 5
and 6. of this permit at the time monitoring reports are submitted. The reports shall contain
the information listed in Part H. E. 6. of this permit.
8. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in a permit
application, or submitted incorrect information in a permit application or in any report to the
Director, it shall promptly submit such facts or information.

Part II
Page 14 of 14
9. Noncompliance Notification
The permittee shall report by telephone to either the central office or the appropriate regional
office of the Division as soon as possible, but in no case more than 24 hours or on the next
working day following the occurrence or first knowledge of the occurrence of any of the
following:
a. Any occurrence at the water pollution control facility which results in the discharge of
significant amounts of wastes which are abnormal in quantity or characteristic, such as
the dumping of the contents of a sludge digester; the known passage of .a slug of
hazardous substance through the facility; or any other unusual circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate wastewater treatment such as mechanical or electrical'failures of
pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass
directly to receiving waters without treatment of all or any portion of the influent to
such station or facility.
Persons reporting such occurrences by. telephone shall also file a written report in letter
form within'5 days following first knowledge of the occurrence.
10. Availabili y of Reports
Except for data determined to be confidential under NCGS 143 -215.3 (a) (2) or Section 308
of the Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be
available for public inspection at the offices of the Division of Environmental Management.
As required by the Act, effluent data shall not be considered confidential. Knowingly
making any false statement on any such report may result in the imposition of criminal
penalties as provided for in NCGS 143-215.1(b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement,
representation, or certification in any record or other document submitted or required to be
maintained under this permit, including monitoring reports or reports of compliance or
noncompliance shall, upon conviction, be punished by a fine of not more than $10,000 per
violation, or by imprisonment for not more than two years per violation, or by both.

PART III
OTHER REQUIREMENTS
A. Construction
No construction of wastewater treatment facilities or additions to add to the plant's treatment
capacity or to change the type of process utilized at the treatment plant shall be begun until Final
Plans and Specifications have been submitted to the Division of Environmental Management
and written approval and Authorization to Construct has been issued.
B. Groundwater Monitoring
The permittee shall, upon written notice from the Director of the Division of Environmental
Management, conduct groundwater monitoring as may be required to determine the compliance
of this NPDES permitted facility with the current groundwater standards.
C. Changes in Discharges of Toxic Substances
The permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to
believe:
a. That any activity has occurred or will occur which would result in the discharge, on a
routine or frequent basis, of any toxic pollutant which is not limited in the permit, if that
discharge will exceed the highest of the following "notification levels";
(1) One hundred micrograms per liter (100 ug/1);
(2) Two hundred micrograms per liter (200 ug/1) for acrolein and acrylonitrile; five hundred
micrograms per liter (500 ug/1) for 2.4-dinitropheno1 and for
2-methyl-4.6-dinitrophenol; and one milligram per liter (1 mg/l) for antimony;
(3) Five (5) times the maximum concentration value reported for that pollutant in the permit
application.
b. That any activity has occurred or will occur which would result in. any discharge, on a
non -routine or infrequent basis, of a toxic pollutant -which is not limited in the permit, if
that discharge will exceed the highest of the following "notification levels";
(1) Five hundred micrograms per liter (500 ug/1);
(2) One milligram per liter (1 mg/1) for antimony;
(3) Ten 00) times the maximum concentration value reported for that pollutant in the permit
application.

Part III
Permit No. NCO080039
D. The permittee shall not use any biocides except those approved in conjunction with the permit
application. The permittee shall notify the Director in writing not later than ninety (90) days prior
to instituting use of any additional biocide used in cooling systems which may be toxic to aquatic
life other than those previously reported to the Division of Environmental Management. Such
notification shall include completion of Biocide Worksheet Form 101 and -a map locating the
discharge point and receiving stream.

PART IV .
ANNUAL ADMINISTERING AND COMPLIANCE MONITORING FEE REQUIREMENTS
A. The permittee must pay the annual administering and compliance monitoring fee within 30
(thirty) days after being billed by the Division. Failure to pay the fee in a timely manner in
accordance with 15A NCAC 2H .0105(b)(4) may cause this Division to initiate action to
revoke the permit.

To: Permits and Engineering Unit
Water Quality Section
Date: January 15, 1991
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Rowan
NPDES Permit No.: NCO080039
MRO No. 91-12
PART I - GENERAL INFORMATION
1. Facility and Address: Linn Plant
Dominion Yarn Corporation
Post office Box 8105
Landis, North Carolina 28088-8105
2. Date of Investigation: January 10, 1991
3. Report Prepared By: Allen Hardy, Environmental Engineer I
4. Person Contacted and Telephone Number: E. T. Haynes;
704/857-1121
5. Directions to Site: From Mooresville travel into Landis on
Highway 153 to the intersection of Zion Street. Turn left
and travel approximately 0.25 mile. The plant will be on
the right.
6. Discharge Point(s), List for all discharge Points: -
Latitude: 350 32' 51"
Longitude: 800 36' 44"
Attach a USGS Map Extract and indicate treatment plant site
and discharge point on map.
USGS Quad No.: E 16 SE
7. Size (land available for expansion and upgrading): There
did not appear to be any land available for expansion and
upgrading.
8. Topography (relationship to flood plain included): The
topography consists of gently rolling hills with slopes from
9. Location of Nearest Dwelling: The nearest dwelling was
approximately 100 feet from the discharge location.
10. Receiving Stream or Affected Surface Waters: Unnamed
tributary to Grdnts Creek.
a _
a. Classification: C

Page Two
b. River Basin and Subbasin No.: Yadkin; 03-07-12
C. Describe receiving stream features and pertinent
downstream uses: The receiving stream appeared to be
the headwaters of an unnamed tributary to Grants Creek.
The bulk of the stream appeared to be from the subject
discharge. The receiving stream had a well defined
channel with a typical sandy bottom.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. Type of Wastewater: 0% Domestic
100% Industrial
a. Volume of Wastewater: 0.08 MGD (Design Capacity)
b. Types and quantities of industrial wastewater: The
industrial wastewater is produced from 13 air washers
and 3 cooling towers. The maximum discharge consists
of approximately 80,000 gallons. of wastewater.
C. Prevalent toxic constituents in wastewater: The
Company is presently using a biocide (See Pages II-7
and II-8 in the application) in the air washers and.
cooling tower. The types of biocides will be submitted
by the applicant.
d. Pretreatment Program (POTWs only): N/A
2. Production Rates (industrial discharges only) in Pounds:
N/A
3. Description of Industrial Process (for industries only) and
Applicable CFR Part and Subpart: Part 41.0 - Textile Mills
Point Source Category, Subpart H - Nonwoven Manufacturing
Subcategory
4. Type of Treatment (specify whether proposed or existing):
There is no formal treatment prior to discharge.
5. Sludge Handling and Disposal Scheme: N/A
6. Treatment Plant Classification: Less than 5 points; no
rating (include rating sheet). N/A
7. SIC Code(s): 2281
Wastewater Code(s):
Primary: 17
Secondary:
PART III - OTHER PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grants
Funds (municipals only)? No
2. Special monitoring requests: No

Page Three
3. Additional effluent limits requests: No
4. Air Quality and/or Groundwater concerns or hazardous waste
utilized at this facility that may impact water quality, air
quality or groundwater? No air or groundwater concerns are
expected from this project; nor is hazardous waste utilized
at this facility.
5. Other: N/A
PART IV - EVALUATION AND RECOMMENDATIONS
The applicant, Dominion Yarn Corporation, has applied to
discharge approximately 80,000 gpd of industrial wastewater
produced from 13 air washers and 3 cooling towers at the Linn
Plant. The wastewater is intermixed with stormwater at numerous
locations throughout the plant and eventually converges into one
outf all which is then piped to the receiving stream.
The Company is located within the city limits of Landis and
has access to a city sewer system;.but the complexity involved
with piping all the above discharged to one outfall, the economic
feasibility and the physical obstacles of such a change has
eliminated connection as a_viable alternative.
it is recommended that the discharge be permitted provided
receipt, review and approval of the forthcoming biocide
worksheet.
i�lq(- w WL:2��- -
Signature of Report P p rer Dat'�ej
Water Quality Regiona Supervisor ate

:.,I U,
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U
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Mt Morifill
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t C Or
A. 62iz
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.7
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Linn Plan't?934
Discharge Lo ati
E16SE
AV,. 10
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VI
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ro
6 6
BLA rH
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N. C. DEPT. OF NATURAL
o^T�� •SOUR ES AND
c -y
��oP ri�xN�
JAN : 9 1991
/ State of North Carolina oIVlGlrr "F Erd'1n0;;t EiiA� rsNAG
Department of Environment, Health, and Natural Resc I- ;ItIE REGIONAL OFFICE;
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Govemor George T. Everett, Ph.D.
William W. Cobey, Jr., Secretary Director
12/28/90 7
E. T. Haynes, Engr.Dir.
Dominion Yarn Corporation Subject: NPDES Permit Application
Po Box 8105 NPDES Permit NO.NC0080039
Landis, NC 28088-8105 Linn Plant
Dear .Mr•: Haynes Rowan County
.Th'is.!- is t"o, acknowledge, receipt of the following documents on December 12, 1990 c
Applicat on`•F•orm.
Engineering Proposal (for proposed control 'facilities),
Request ,for •permit: renewal,
Applica,t,ion -Processing ` Fee of $400.00,
Other
The items checked below are needed before review can begin:
Application 'Form, ,
Engineering proposal... (see. attachment)
Application' Processing Fee of
Delegation of Authority (see attached)
Biocide Sheet ,:'(see attached).
Other .Map showing discharge points;'Biocide worksheet (later)
-If the appli'cation''is not made complete within,,thirtIy 11 ' (30) days; it will b.e
returned to you sand may,be resubmitted ..when complete
This application has been assigned to Jule shanklin
(919/733-5083) of our Permits Unit for rev ew. You will e advised of any
comments recommendations, questions or other information necessary'for the
review of the application.
I am, by copy of this letter; requesting .that our Regional Office
Supervisor prepare a staff report and recommendations regarding this
discharge. If you have any questions regarding this applications,
please contact the review person listed above.
S ' erely,
CC: Mooresville Regional Office M. D le Overcash, P.E.
PoDution Prevenlon Pays
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]

NORTH CAROLINA,, DEPT OF NATURAL RESOURCES ' 1t0I1tilI1 iY DEVELOPMENT DEG a 1990
• fs' DIVISION OF ENVIRONMENTAL MANAGEMENT, P.O. BOX 27687, RALEIGH,.NC'27611:
Pr rkITC R rn!rt°�rFRtnlr, PERMITS � FNf1!N7cRtnlG
/NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSf�EM
To be filed only by persons engaged in manufacturing and mining
No.03?ozV
t�cJb•da
Do not attempt to complete this form before reading accompanying instructions
Please print or type
APICATION NUMBER
APPLICATION FOR PERMIT TO DISCHARGE - SH$RT FORM C FOR
AGENCY
USE
To be filed only by persons engaged in manufacturing and mining
No.03?ozV
t�cJb•da
Do not attempt to complete this form before reading accompanying instructions
Please print or type
PL
G p
DATE RECEIVED
YEAR Mo. DAY
RECEIVED
"WON OF ENVIRONMENTAL MANASEMENJ
1. Name, address, location, and telephone number of facility r dpcing scharge DEC 71 1990
A. Name __ Dominion Yarn Corporation /p inn'lant
AWR SV I LE
B. Mailing address eEoloMAt oF>
1, street adoreP • 0. Box 8105
Landis NC
2. City. 3. State
4. County Rowan 5. ZIP Z , 1 d C
c. Location: .100 South Main Street
.1. Street
2. City Landis 3. County Rowan
4. State NC
D. Telephone No. 704 857-1121
Area
Code
2. S I C t-1_3_LJ
(Leave blank)
3. Number of employees 207
If all your waste is discharged 'into a publicly owned waste treatment facility
and to the best of your knowledge you are not required to obtain a discharge
permit, proceed to item 4. Otherwise proceed directly to item 5.
4. if you meet the condition stated above, check here o and supply the information
'asked for below. After completing these items, please complete the date, title,
and signature blocks below and return this form to the proper reviewing office
without completing the remainder of the form.
A. Name of organization responsible for receiving waste
B. Facility receiving waste:
1. Name
2. Street address
3. City 4. County
5. State 6. ZIP
5. o Principal product, ❑ raw material (Check one)
`6. Principal process
7. Maximum amount of principal product produced or raw material consumed per (Check one)
Basis
YEAR Mo. DAY
RECEIVED
"WON OF ENVIRONMENTAL MANASEMENJ
1. Name, address, location, and telephone number of facility r dpcing scharge DEC 71 1990
A. Name __ Dominion Yarn Corporation /p inn'lant
AWR SV I LE
B. Mailing address eEoloMAt oF>
1, street adoreP • 0. Box 8105
Landis NC
2. City. 3. State
4. County Rowan 5. ZIP Z , 1 d C
c. Location: .100 South Main Street
.1. Street
2. City Landis 3. County Rowan
4. State NC
D. Telephone No. 704 857-1121
Area
Code
2. S I C t-1_3_LJ
(Leave blank)
3. Number of employees 207
If all your waste is discharged 'into a publicly owned waste treatment facility
and to the best of your knowledge you are not required to obtain a discharge
permit, proceed to item 4. Otherwise proceed directly to item 5.
4. if you meet the condition stated above, check here o and supply the information
'asked for below. After completing these items, please complete the date, title,
and signature blocks below and return this form to the proper reviewing office
without completing the remainder of the form.
A. Name of organization responsible for receiving waste
B. Facility receiving waste:
1. Name
2. Street address
3. City 4. County
5. State 6. ZIP
5. o Principal product, ❑ raw material (Check one)
`6. Principal process
7. Maximum amount of principal product produced or raw material consumed per (Check one)
Basis
Amount
1-99
(1)
100-199
(2)
200-499
(3)
500-999
(4)
1000-
4999
(5)
5000-
9999
(6)
10,000-
49.999
(7)
50,000
or more
(8)
A. Day
B. Month
C. Year
PREVIOUS EDITION MAY BE USED UNTIL 5UPPLY IS EXHAUSTED - -

rm amount of pr:nOlial pr-ri�lurl. prudu�ed or 'r4w mnlerlirl'rnn.uiiN•d, reported
tern./, above, Is measured - In (thetk one):
A.o pounds B.o tons C.0 barrels D.o busFiehs E:0 square feet
i i F.0 gallons G.0 pieces or units H.o other; specify
(a) Check here if discharge occurs all year �j , or
(b) Check the month(s) discharge occurs:
1.o January 2. o February 3. 0 Mar'cn 4.0 April,' S.0 may 6.0 June
7.0 July 8.0 August 9.❑ Septemler 10.0 October I I . 0 November 12.0 December.
(c) Check how many days per week: 1.01 2.o 2-3 3.0 4-5 4.cy,6-7
10. Types of waste water discharged to surface waters only (check as applicable)
Volume treated before
F low. gallons per operating day
discharging (percent)
Discharge per
operating day
0.1-999
1000-4999
5000-9999
10,000-
50,000-
None
0.1-
30-
65-
95-
49,999
or more
29.9
64.9
94.9
1
100
(1)
(2)
(3)
(4)
(5)
(6)
(7)
(B)
(9)
(10)
A. Sanitary, daily
average
B. Cooling water, etc-
X
X
daily average
C. Process water,
daily average
)_ Maximum per operat-
ing day for total
X
discharge (all types
H. If an, c-f the three types of waste identified in iteM 10.eiiher treated or untreated.
are Oischarged to u'--ace; other Char. surface water-., check below as applicable_
Average'flow, gallons per operating day
waste_ water is
dischargrd to:
0.1-999
(1)
1000-4999
(2)
5000-9999
(3)
10,000-49,999
(4)
50,00.0 or More
(5)
A. Municipal serer system
B. Underground well.
C. Septic tank
D. Evaporation laq�on or pond
E. Otner, specify
12. Number of separate discharge points
13. Name of receiving water or waters _
A.Xl B.02-3 C.o4-5 D.06 or more
14. Does your discharge contain or is it possible for your discharge to contain
one or more of the following substances added as a result of your operations,
activities, or processes: ammonia, cyanide, aluminum, beryllium, cadmium,
chromium, copper, lead, mercury, nickel, selenium, zinc, phenols, oil and
grease, and chlorine (residual). A.0 yes B.0 no
I certify that 1 am familiar with the information contained in the application and
that to the best of my knowledge and belief such information is true, complete, and
accurate.
E. T. Haynes Engineering Director
Printed Name of Person Signing Ti
12/7/90
Date Application Signed Signature of Applickit
North Carolina General Statute 143-215.6(b)(2) provides that: Any person who knowingly makes
any false statement representation, or certification in any application, record, report, plan,
or other document files or required to be maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article.,' or who falsifies, tampers with,
or knowly renders inaccurate any recording or monitoring device or.method required to be
operated, or maintained under Article 21 or regulations of„the, *EnvironmentalManagement Commissio
implementing that Article, shall be guilty of a misdemeanor:pumishable by a fine not to exceed
$10,000, or -by-risonment not to exceed six months, or by both.. (18 U.S.C. Section 1001 provid
a punishment-.bj•,' fine of not. more than $10,000 or imprisonment -,not more than 5%years, or both,

APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
STANDARD FORM C — MANUFACTURING AND COMMEROAhL
SECTION 1. APPLICANT AND FACILITY DESCRIPTION
Unless otherwise specified -on this form all Items are to be Coo led. If ah hens k not &PPlkable Indicate -
NA. -ADDITIONAL INSTRUCTIONS FOR SELECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INylItIAVEO: RMI%TO
BOOKLET BEFORE FILLING OUT THESE ITEMS.
Pli)l w Print or Type
1. L"al Name of APPllcant
(aw Instructions)
!.' Mal11M Address N Applicant
(see Instructions)
Number L Street
City
State
Zip Code
7. Applicant's Authorized Agent
(nee Instructions)
Name. and Title
Number L Street Addresf
City.
State
Zip Code
Telephone
4. "lous Application
If a previous appllUtlon for a
Nat.onal or Federal discharge Per-
mit has been made, gave the date
of application Use numeric
103b
103C
1434
�i • 107e
IOit'
v
Area Number
Code
designation for date. (.104 1 YR MO DAY -
1 certify that 1 am familiar with the Information Contained In this application and that to the best of my knowse40e and beef Duch Infomation
k t►ue, complete, and accurate. -
1f 4
Printea Name of Parson Signing. This
YR MO DAY
too
Signature of Applicant of Authorized Agent Data APpikatlon Slmned
Korth Carolina General Statute 143-215.6 (b) (2) provides that: Any person who Imawringly makes
a=y false statement ,rearesentetion,,or cartif icat on in any application, record, report, plan,
or other. document files or required to be maintained under Article 21 or regulations of the
Enviroa)lentsl Management Co= ission implementing that. Article, or who falsifies, tampers with,
or Imawly readers. inaccurate say recording or monitoring device or 1.method required.to be
oneratee.cr-maintained =der Article 21 or regulations of. -the Eaviroamental Nzaagemtnt Commissic
implementing that "Article, .shell be guilty. of, a misdemeanor Ya'aisha_ ble by a fine slot -to ezeeed .
$10,00-1, or by imprisonment not to exceed six months,:or_by' both. (18 D.S.C. Section 1001 pravip
e ptmis'tmiez-V by..a. sine of 'rot more than $10,000 -or lmprisomoent net, Clore -then 'S years, r rboth, -
for .a. size far crfersr:.)

a; t►&slpty/Activity (we_instructlohs)
Give the name. ow inhip. and
Ohytieal location of the Dianl or
Omsk operating facility where-dls-
CharM(t) does Or will occur.
Name ....:
Ownership (Public. P►Ivate or
Both Public and Private)
Check block If Federal Faclilty
and give GSA Inventory Control
) / Number
Location
stmet a Number
City
County
state
a. Haw e N.wina+ state the
nature of the business conducted
at the plant or operating faculty.
7. Facility Intake Water (see Instruc-
lions) Indicate water Intake volume
per day by sources. Estimate
&"rage v,Olume per day In thousand
sallow. -per day.
Municipal Of private water lystem
surface water
Groundwater
Other'
Total Item 7
*If there It Intake water from
-other.' Specify the source.
1. IF aeMity Water the Estimate '
a"rega volume per day In thousand
9NIOM per day for the following
typo of w&ter u"" at tIN facility.
(tee InSUV dons)
Noncontact cooling water
holler feed crater
hoot" water (Including contact
coding water)
Sanitary water
Other •
' Total Ilem a
elf thereOrl'-dlschargN to
'other; Specify.
H thim IS Vanitary' water use. Live
the number of Psopla "road.,
t
1
r
"a
6K
fad
loaf
loss
lash
IKa
tgab j
ta7,.
taTa
sale
ta7d
107s
her
1Ni
tub
[3PUB JOPRV ❑OPP
❑ FED
Sales Yarn
AGENCY USE
80, thousand galions per day
thousand gallons Par day
thousand lotions Per day
tnoUS" gallons Par day
thousand gallons per day
68
thousand gemms per day
thousand gallons por day
t M e "Wmfy phone Per day
sand 10 alou+.rra pliorri per W
1*00 .2 thilaaand rmom lac ally
f: 8 0 atWAIrM loom W day

S.
cl "
F60 AGE USE
1;.._ AN Facility Diic ir7ei and *that
L*ues; NuniNr ins Dischane (see
Instructions) Volume Soapily the
-
-
number of tlii6jaige points and the
' volume Of:viiter eacnarpea or
lost from the.feClllty according tothe
categories tiilow. Estimate
Number of
TOM Volume Used -
avers" volume per day In thousand "
Dlschar"
or Discharged,
"lions per day.
Punts
Thousand Gal/Day
CiM*2
1.2
Surface Water
:M:;
13
Sanitary wastewater transport
!flirt
�2
system
storm water transport system
>}Mel
`•IMe!
Combined sanitary and storm
water transport system
It1i�l
son
Surface Impoundment with no
effluent
1fN1
low
Underground percotatioo
lffft
1ff12
Weil Injection
7flg1
SSW
Waste acceptance firm
IfMt
Ifflt2
5 5
Evaporation
,lilt
!f!p
Consumption
seep
jNj2
Other*
1Nt/
/Mk2
Facility discharges and volume
80
Total Item 2.
Iflil
IMI2
• If there are dlacargee to 'other.'
specify.
1faT1
10. 14rmlts. Licensee and Applications
Ust all existMg, pending or deniso permits, licenses and apolicatlons related to discharges from this facility (we Instructions).
Ittuing AyencY•
For Agency Use . I
Type of permit
or License
ID Number
Date
Filed
YQ/MO/DA
Date
Issued
YR/MOA
/D
Date
Dor d
YR/MO/D A
Expiration'
Date
YR/MOIDA
1*)
{01
{c)
pal
t*1
pl
�.: �
• fh)
11. ceps and Drawin*1
Attach all required maps and drawings to the back Of this soplication.(see Instructions)
12. ANIIIonat Information
♦/� Item Number Information

or opt AGENCY USC
STANDARD FORM C - MANUFA&URING AND COMMERCIAL
SECTIONU.. BASIC DISCHARGE DESCRIPTION
Complete Inns section for aach discharge indicated in Section 1, Item 9, that is to surface water&. This includes discharges to municipal seweragc
systems in which the wastewater don not to through a Ifeatmtnl, work& prior to being discharged to surface waters. Discharges to wells must
be described where there are also d.schafgtt to Surface waters fril.11 this facility. SEPARATE DESCRIPTIONS OF EACH DISCHARGE ARE
QL REUIRED EVEN IF SEVERAL DISCHARGES ORIGINATE IN THE SAME FACILITY. All values for an falsling discharge should be Feint
sentative of the twelve previous months Of Operation. If this Is a prOPaaed discharge, values should reflect bast engineering estimates.
ADDITIONAL INSTRUCTIONS FOR SELECTED ITEMS APPEAR IN SEPARATE INSTRUCTION BOOKLET AS INDICATED. REFER
TO BOOKLET BEFORE Fit LING OUT THESE ITEMS.
1. "Charge Serial No. and Name _ -
a. Discharge Serial No. 20ta "
(see instructions)
b. Di&ehar,t_Name nib Cooling Tower & Air Washer Bleed,
Give name of discharge, of any.
(see instructions) I.
c Previous Discharge Serial No.
If previous permit application was made for. this discharge (see nic
Item 4. Section 1). provide _prev.- .
Ous discharge serial number -
2" Discharge Optrating Dates
a. Discharge eagan Dale It Inc
atscnarge described btiov..t rn -
ope-ation, give the aate fw•in.n 202a
best estimatel the antharge YR MO .
began
b. -Discharge to Begin Date if tnc
aist harge nai never occurred but
is planned for some future date, 202b
give lite date (With.n best c51.• YR MO
mate) the -discharge wilt beg•r.
c Discharge to End Dale it a.s•
Cnar9e N SCnC0.1IC0 to be O-Stnl-
linuca within the ne .t -� yci-s, 202C_..-
q.-C the date fw•ln.n bttt es'. Y R MO
ma1C) the clatnargC w.i. , nc
7. Engineering Report Available "
Lhcc. of an engineering reDOrt .s
ava•laole td reviewing agency ubOn
reouest Isee instruct.onsl 203
4. Discharge Location Name Cite .
pol.tical boundaries within wn.cn
the point of discharge is locates`
State
County
(if aphimable) City Or row.:
S. Discharge•t•oint Description
DisCharge 16 into (check One):
(see mstructtons)
Stream (includes ditches, arroyos.
and Other intermittent watercourses)
Lake
Ocean
Municipal Sanitary Wa&tewalet
Transport System
Municipal Combined Sanitary a"
Storm Transport System
n4e
304111,
204C
Agency Use
NC
Rowan
Landis
tKt '
loss I 6ST R
❑LKE
❑OCE .
❑MTS
0MCS
This .section "lletaisas y pages.

DISCHARGE;SERIAL NUMBER
Municipal Storm Water Transoort
System
Well (Injection)
Other
If 'other' it Checked, "City
S. Diseharge Point— Lot/Long Give
the pfeCl$e location Of tne'voint
of discharge to the Clearest MCOnO.
L a it lode
Longitude
7. 01$tMfge ReeetvlM water Name
Namf the waterway at the point
Of dlfCharge•(see Instructions)
1f the discharge is through an out.
fall that OxItnos beyond the shore-
line Or Is below the main low
water line. Complete Item a.
S. Offshore Discharge
a. Discharge Dlttanct from Short
D. Discharge Depth Below water
Surface
g. Di$eharga Tyte and Occurrence
a. Type of Discharge Check
wnether the ottCharge rs Con-
tinuous or intermittent.
pee instructions)
b. Discharge Occurrence DaYs per
Week Enter the average num
ber Of days per week (dunng
period$ Of discharge) this di$•
charge Occurs.
C. Discharge Occurrence —Months
11 this discharge nOrmat-y
operates (either intermittentry.
or Continuously) on Nis than
a year around basis (excluding
shutdowns for routine msrnte-
hance). Check the months dur•
Mg the year when the discharge
I$ Operating. (sea Instructions)
:orhptete Items 10 and 11 If Wnter-
-ttttent" to cocked In Item 9A.
)therwke, proceed to Item 12.
C. Intermittent )discharge Quantity
State the average volume Per CIS'
Chat" Occurrence in thoutands Or
gallons.
11. Ifiteratlttalri Discharge Duration
ash Frequency
a 1t4ermitterd Discill a Duration
Per pay State the evarage
number Of hour$ per day the.
discharge I$ Operating.
a lalermlttent Discharge
pre"ricy State the average
number of discharge occur-
aences Vor day ding aye
when discharging.
12. Matttthvin Flew Versed Give the
Jim* Wlod In which the maximum
NOW Of this 01$Charge OCCure.
FOR AGENCY USE
STS
OWEL
OTH
sees
2Nt
Me
2076
2083
20eD
IOga
209b
Me
lie
211a
2111
212
DEG __MIN __SEC
DEG _MIN __SEC
For Agency Use For A envy Use
Mal Or Minor Sub 703c
12f17t _
_feel
_ _feet
(con) Continuous
❑ tint) intermittent
_days per week
tfy,lAN J]FEB X3MAR [JAPR Year Round Cooling
[�MAv �JuN �JuL [ Auc Tower in Summer
Air Washer in Winter
USEP �bOCT YINOV [XOEC
' thou$and gallons tear discharge Occurrence.
_hour$ pet day
1 I _dhchargt occurrence$ per day
From S to 10
month Month

DISCHARGE SERIAL NUMBER
FOR AGENCY USE,
13. ACUtlly Description Give s _
narrative description of activity I 913a
producing this dlscharge.(set
Instructions) Bleed water from cooling tower and air__
washer operation
14. Activity Causint Oischarlt For
each SIC Code which describe/
the aLtrvsty Causing this discharge.
Supply the type and maximum
amount Of either the raw material
COnaumed (Item 14a) or the product
D•oducad (item lab) In the units
Specified in Table I of the Instruc.
lion Boa.let. For SIC Coder not
listed in 1 able 1. use raw material
a production units normally usec
for measuring prpduClson.(see
instructions)
A. Raw Materials
SIC Code
2144
b. Products
SIC Code
tool
Maximum Unit Snared Discharges
Name Amount/Osy (See Table 11 Iiarial Numeert
Maximum Unit Shared Discharges
Name Ameunt/Dav (See Table It 09-1.1 ar..... 1

tmctfARr SF.tNl1l NUMIf
• -
FOR AGENCY USE
IS. Waite Abatement
_._.
a• waste Abatement Practice/
abatement
tale Narral�vt:—.—..—
Dtscribe the waste
practical ufeO On this d,scharge
with a brlef narrative. (see
Instructions)
(J)
b. Waste Abaterent Cedes
21sb (1)
.'
16) ��-
Using the codes listed In Table
(e) -� •
(S) ���
II at the Instruction Booklet.
l9)
describe the waist abatement
(�)
'
processes for this d-schar9e 'n
(12) -�
ant Order in WhrCh they Occur
(10)
1111 �--�'
tf Possible-
(151 -
(131 ��.
(1a1.�—�'
(171
(IN) -
(161
(191
(23)
(24)
122)
(251
11-4

p
lav ap nwipow pus •2pm!f--i
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• DIfCHAROE'a;ERIAL NUMBER
l
FOR AQ"CY USE
Description of Intake and Otacharfa
For each of the parltrnebrs listed below, enter In the appropriate box tM value or Codi setter are aliad f0r.(W kMti Ctlons)
In addition, enter the parameter name and code and NI requirk values fix any of tne following parameters If they
wen checked In Item 26;
ammonia, cyanida, aluminum, arianiC,'berylllum, cadmium, chfom+lum4 COpper, lead. nwrcury, nickel, aalenlum, tine
phends, oil and greatt.
and Chlorine (residual).
Influent
Effluent
Z
r
a t u
rar m.eter and Code = g > `o
�< C�rri Q
>
!ill;` $ate a�
b
E.2I c
CaA� G ZiaK2b<
:i$Wb
(11 (2) (3) 1 (4)
(S)
(6) (7) l)l) I
Flow*
Gariow per day
00056
pH
Unlu
00400
Temperature (winter)
�F
74028
Tatspestlue (Ammer)
.F
74027
DkxheatiW Omen Demuid
(DOD "y)
mill
00310
Clamial Oxypn Demand (COD)
mi/1
•
00340
Total Sw xsad.W (noealtmbk)
Solids
00530
Spedtk Conductance
Waombot/cm at 25e C
00095
Settleable Matter OtWue)
u11/1
OW45
00dw dlacbwF% s uz* intake now (aerial numbm)jwc instructions)
12,

ratatnetet and code
Influent
E(flucnt
W
C p_
(1)
y
Y
(2)
(3)
E
ii
(4)
rrD
• M
Eg
� .10 z
(5)
V
(6)
(7)
(8)
la. Plant Controls Check If the fol-
lowing plant controls are ayallable
for this discharge.
Al ternale power source for major
Pumping facility.
i
Alarm or emergency procedure for
power. or equipment failure
Complete Item 29 If discharge It
from cooling and/or steam water
generation and water treatment
additty" are used
19. skater Treatment Additives If -the
dltcharp is treated with any con•
dltIofW. Inhibitor. of alglclde,
answer the following:
a. P/ame of Matersal(s)
b. name and address of manu-
facturer
c. Quantity (pounds added per
million Gallons of water treated).
all
D APs
13 ALM
aac
Hydrofene II, Waterene 560,
Microbiacide 76, Lester P-3
Lester Laboratories, Inc.
2370 Lawrence Street
Atlanta, GA 30344.

DISCHARGESERIAL NUMtIER
FOR AGENCY Usk
Sodium Molybdate
-
�• � `�-=-. - d. Chem" compoatlono f thus �'IN
—
additives ("aInstructlons).
Surfactants Polymers
Compton Items 20.25 If there Is • therrtsal discharge
(• g . auoclated with a Stsam and/or power generation
- -
plant. Steel frNll, Petroleum refinery, or any other
manufacturing Process) ane the total discharge flow Is
10 muUon gallons per dry of nsors. to" ktstructlons)
tf. Thormei "Chart♦• Source Check
She appropriate Item(s) indicating a.
the source of the discharge. (we '+•` '
.
. WA uctiam) .
j
8404W Slowdown -
`"
❑ OLt10
Oaltar Chemical Claaning
❑ OCCL
Ash ForW OwrOowv
pAPOF
lgolar Water Treatment — Evapera- _.:'
p EPOO
tar Olowdown
Oil or Coal Find Plants — Effluent
❑OCFP
from Aif faollutlon Control Devicat
-
condense Cooling Water
❑COND
Cooling Tower Olowdown
❑ CTOO
Manufacturing Process
pMFPR
Other
❑ OTH R
21. Dlsshargs/Receiving Water Temper -
atare Difference
a" the maximum temperature
' dtf"nce between the dlscharpe
and receiving waters for summer
and winter operating conditions.
Summer (a" Instructions)
221 a
OF.
Winter 2216
OF.
22.. Discharge Temperature, Rate of
Change hr Hour *22—OF./hour
olve the maximum cosslble felt of
tampersture change per hour of
41144har(le undor operating con-
atlons. (ses Matrvctlons)
23. Water Temperature, Percentile
Report (Frequency of Occurrence)
In the table below, onler the
temperature which Is exceeded 10%
Of the year, Sty of the year, 1% of
the year and not at all (maximum
VWIY t*MP*Mtun). (a•• Matructfons)
Frequency of oeeurrenco
a Intake Water Temperature
tlL
l%
Is►
Maxlmum
OF
of
of
to natural chengas)ILUctsar
I-F(Sublact
Or Water Temperature
Rt2O
of
of
of
24. Water Intake V•loelty ., feet/Nc
(ses Instructions),
2S. ReMntieh Tema Olve the I•ngth of
time, In mksutea, from start of
water temperature ri" to dlechsrgs
Of Coo(Ing water.'(eoa instructions)
11-8

r ,e
OiSCHARGE SERIAL NUMBER
FOR AGENCY USE
.'94 ..:
Si. AddiGooal information
20
11-9
All

FOR AGENCY USE
STANDARD FORM C - MANUFACTURING AND COMMERCIAL
SECTION M. WASTE ABATEMENT REQUIREMENTS & IMPLEMENTATION (CONSTRUCTION) >;CHEDGLE .
This section ►eQuirm Information On any uncompleted IMPlementstlOn schedule which may have been Mnposed for COrlitrYCtlOn Of waste abate
ment teclttt{ea Such requirements and Implementation schedules may han been established by local. State, d f of o etructio Of by court
action In addition to compfeting tM 1Wlowireg items, a Copy of an Official Nnpfementatlon schedule should be attached tO this &Pollution.
IF YOU ARE SUDJECT TO SEVERAL DIFFERENT IMPLEMENTATION SCHEDULES, EITHER BECAUSE OF DIFFERENT LEVELS OF
AUTHORITY IMPOSING DIFFERENT SCHEDULES (Item Is-)'AND/Olt STAGED CONSTRUCTION OF SEPARATE OPERATION UNITS
(Its- lc). SUMMIT ASEPARATE SECTION III FOR EACH ONE.
1. Iwkorevements FOR AGENCY USE
a DYM4rse Serial Number
Affected Lit the discharge a fu
lariat numbem. assigned In Po
Section II. that are Covered by y
this Implementation echedula
b. Authority Imposing Resale-
Imemts 'Chock the appropriate
item Ind"ting the authority for
ImPMmentation schadula if -
the Identical Implementation
schedule has Dean ordered by
more than one authOrbty•Check
tha appropriate Items. (see
Instructions)
Locally derMoped plan y+u ❑LOC
Areawids Plan ❑qRE
Bask Plan
❑sAS
State approvsd Implementa-
tion schedule ❑SQS
Federal approved water -
Quality standards Implaments-
t►on Plan. 0WQS
Fedora ILenforcement procoo-
care Of action _ ❑ENF
Stale court order [-]CRT
Federal. court Order ❑ FED -
c_ Facility Requirement. Specify
the 3-character code Of those
ksted below that Deft describes 3-character
In general term& the e require.
(ffeneral)
ment Of the Implementation-
_ schedule.and the appllcable six. >•IC,
character abatement coot(s)
from Table If Of the Instruction -
booklet. It more than one' Silts 6-character
schedule apPlles to the facility (specitic)
because Of a staffed Construction (eN Table 11)
schedule. state the staffs of con-
stnrctiOn ding described here
with the apDroprists general
action coda. Submit a separate
Section III for each stage of
COMAMCtlon ptanned• .
.. t
New Facility
NEW
Modification (no Increase -in CapaCltY Or treatment) MOD
Increase In Caliaclty'
INC
Increase In Treatment Level
INT
Both Increase in Treatment La", and C&Wlty ICT
PrOCOU Change .
Elimination Of Discharge PRO
ELl
This section contains ? lasted.
``,

. i
r iC
♦
l .
t•OR AGENCY USE
_
L 2..: IsflpM�wemt+tlen sahpMim ar+d:`.;l.AtpY CMMMHM.QaMa
•� anY actYal'dates Or tanW!tIon for {fn♦NRMRunOn saps Hated tlNow.
{ri _
provide data Imposed DY ichedul0
pee Instructions)
Indicate dates as accurately as ppiseM• .
hnplernentttlon Steps 2. Schedule (Yr4Mlo./Day)
i. Actual Completion (Yr./M0./DeY)
a. P Mhn(Nry plan complete
b. I" plan Submission
C. final plan complete
t. flnw4inS Complete i Contract am~
•
4L Site acquired
'
f. DeVn action (4-9., CONSMKtIcn)
/ /
< •
�J�/
S. End action (4L.9, construction)
h. Oltcharfe Haan
.it
L Ogerstlonallevel attained

DEPARTMENT OF NATURAL RESOURCES &.COMMUNITY DEVELOPMENT
ENVIRONMENTAL MANAGEMENT COMtIISSION_
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
APPLICATION FOR PERMIT TO DISCHARGE
ADDITIONAL.REOUIRED INFORMATION
jj
APPLICATION NUMBER
DISCHARGE SERIAL NUMBER
REFER TO DIRECTIONS ON REVERSE SIDE BEFORE ATTEMPTING,.TO COMPLETE THIS FORM
Pantneter
(Code)
'XS01)
REMARKS:
2.t -
� K
as
�3<
�C
�<
E
w
Eje
w>
c
V�
Fc
°.
o.c
G
I Candy that I am faMR18f with the Information eontaMad to this nport'and that to the
belt of my knowledge and belief such IMormatlon Is true, Complete and accurate.
J
Date Form Completed
Name.of Authorttad'Agent
54nature

(Domestic•nly,
Nd�lnsurance
Coverager
r-r
u For delivery Information
-,site at
,cam,
7
visit our
I
,.,
u
D
D $
d
Postage
u
Certified Fee
b
D
Post
;ark
Return Receipt Fee
N
��J
r`e
3 (Endorsement Required)
7
Restricted Deliver Fee
:1 (Endorsement Required)
-
MR LEE THOMAS, EXEC. VP OF
se PARKDALE AMERICA
s& PO BOX 1787
or GASTONIA NC 28053-1787 ..............
°" swp/wb 9/4/07

'ertified Mail Provides: `
t A mailing receipt
t A unique identifier for your mailpiece
A record of delivery kept by the Postal Service for two years
mportant Reminders:
Certified Mail may ONLY be combined with First -Class Mail® or Priority Mail,
t Certified Mail is not available for any class of international mail.
i NO INSURANCE COVERAGE IS PROVIDED with Certified Mail. Fc
valuables, please consider Insured or Registered Mail.
t For an additional fee, a Return Receipt may be requested to provide proof a
delivery. To obtain Return Receipt service, please complete and attach a Returr
Receipt (PS Form 3811) to the article and add applicable postage to cover tht
fee. Endorse mailplece "Return Receipt Requested". To receive a fee waiver foi
a duplicate return receipt, a USPS® postmark on your Certified Mail receipt it
required.
r For an additional fee, delivery may be restricted to the addressee o
addressee's authorized agent. Advise the clerk or mark the mailpiece with thi
endorsement "Restricted -Delivery".
t If a postmark on the Certified Mail receipt is desired, please present the arti
cle at the post office for postmarking. If a postmark on the Certified Mai
receipt is not needed, detach and affix label with postage and mail.
MPORTANT, Save this receipt and present it when making an inquiry.
IS Form 3800, August 2006 (Reverse) PSN 7530-02-000.9047

UV, _ .y
r
o �c
September 4, 2007
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
7007 0710 0005 2882 0274
Michael F. Easley, Governor
William G. Ross Jr., Secret
North Carolina Department of Environment and Natural Resources
Mr. Lee Thomas, Executive Vice President ofParkdale America
Post Office Box 1787
Gastonia, North Carolina 28053-1787
Dear Mr. Thomas:
Coleen H. Sullins. Director
Division of Water Quality
Subject: Notice of Violation
Compliance Evaluation Inspection
Parkdale Mills/Plant 23
NPDES Permit No. NCG500250
Rowan County, N.C.
Tracking #: NOV-2007-PC-0564
Enclosed is a copy of the Compliance Evaluation Inspection (CEI) Report for the
inspection conducted at the subject facility on August 22, 2007, by Mr. Wes Bell of this Office.
This report is being issued as a Notice of Violation (NOV) due to the facility's failures to
comply with the Permit's effluent monitoring requirements; violations of the subject NPDES
Permit and North Carolina General Statute (G.S.) 143-215.1, as detailed in the Record Keeping
and Effluent Sampling Sections of the attached report. Pursuant to G.S. 143-215.6A, a civil
penalty of not more than twenty-five thousand dollars ($25,000.00) may be assessed against any
person who violates or fails to act in accordance with the terms, conditions, or requirements of
any permit issued pursuant to G.S: 143-21-5.1.
It is requested that a written response be submitted to this Office by September 25, 2007
addressing the above -noted violations in the attached report. In responding to the violations,
please address your comments to the attention of Mrs. Marcia Allocco.
NCDENR
ine
f Carolina
WNaturally
Mooresville Regional Office Division of Water Quality Phone [phone] Customer Service
Internet: www.ncwaterquality.om 610 East Center Ave, Suite 301 Mooresville, NC 28115 Fax [phone]
An Equal Opportunity/Affirmative Action Employer-50% Recycled110% Post Consumer Paper

Mr. Lee Thomas
Page Two
September 4, 2007
The report should be self-explanatory; however, should you have any questions
concerning this report, please do not hesitate to contact Mrs. Marcia Allocco or Mr. Bell at (704)
663-1699.
Sincerely,
Robert B. Krebs
Surface Water Protection Regional Supervisor
cc: Randall Ferguson, Parkdale
Cecil Ward, Parkdale Mills/Plant 23
Rowan County Health Department

'�W'
United States Environmental Protection Agency
Form Approved.
EPA Washington, D.C. 20460
OMB No. 2040-0057
Water Compliance Inspection Report
Approval expires 8-31-98
Section A: National Data System Coding (i.e., PCS).
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 LI 2 15I 3I NCG500250 111 121 07/OB/22 117 18I CI 19I SI 20III
Remarks
21( III I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I 116
Inspection Work Days Facility Self -Monitoring Evaluation Rating 61 QA ---- —------------- —----- Reserved ----------------------
67I 1.5 169 70I l I 711 NJ 721 N• 73I I 174 751 I I I I I I 180
—! l_i�
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include
Entry Time/Date
Permit Effective Date
POTW name and NPDES permit Number)
Parkdale Mills / Plant 23 `
11:00 AM 07/08/22
02/08/01
Exit Time/Date
Permit Expiration Date
100 S Main St
Landis NC 28088
11:55 AM 07/08/22
07/07/31
Name(s) of Onsite Representative(s)/Titles(s)/Phone and Fax Number(s)
Other Facility Data
Cecil Ward/Manager Plant/704-855=3164 ext 2301/
Randall Ferguson/Corporate Engineer/336-243-2141 ext 0371/3362431813
Name, Address of Responsible Official/Title/Phone and Fax Number
Contacted
Lee Thomas,PO Box 1787 Gastonia NC 28053/Executive VP of Parkdale
Ameri6a/704-874-5100/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance Records/Reports
Self -Monitoring Program Facility Site Review Effluent/Receiving Waters' Laboratory
Section D: Summary of Find in/Comments Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
`
Wesley N Bell MRO WQ//704-663-1699 Ext.231/
Sign a ure of Management Q�Revie��e�r J Agency/Office/Phone and Fax Numbers Date
Marcia A^locco MRO WQ//704-235-2204/
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page # 1

NPDES yr/mo/day Inspection Type
3I NCG500250 I11 12I 07/0.8/22 1
17 18ICI
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
Page # 2

Permit: NCG500250
Inspection Date: 08/22/2007
Owner - Facility: Parkdale Mills / Plant 23
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes
No
NA
NE
Is the plant generally clean with acceptable housekeeping? ■
❑
❑
❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ❑
❑
■
fl
Judge, and other that are applicable?
Comment: The site grounds were well maintained. The effluent is discharged from the
facility's chiller systems.
Record Keeping Yes
No
NA
NE
Are records kept and maintained as required by the permit? ❑
■
❑
Cl
Is all required information readily available, complete and current?
❑
■
❑
❑
Are all records maintained for 3 years (lab, reg. required 5 years)?
❑
IN
❑
❑
Are analytical results consistent with data reported on DMRs?
❑
❑
■
❑
Is the chain -of -custody complete?
❑
❑
■
❑
Dates, times and location of sampling
❑
Name of individual performing the sampling
❑
Results of analysis and calibration
❑
Dates of analysis
❑
Name of person performing analyses
❑
Transported COCs
❑
Are DMRs complete: do they include all permit parameters?
❑
Cl
■
❑
Has the facility submitted its annual compliance report to users and DWQ?
❑
❑
■
❑
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift?
❑
❑
■
❑
Is the ORC visitation log available and current?
❑
❑
■
❑
Is the ORC certified at grade equal to or higher than the facility classification?
❑-
❑
■
❑
Is the backup operator certified at one grade less or greater than the facility classification?
110
■
❑
Is a copy of the current NPDES permit available On site?
❑
■
❑
❑
Facility has copy of previous year's Annual Report on file for review?
❑
❑
■
❑
Comment: A copy of the Permit was not available on -site. No records were being kept
due to the facility's failure to monitor the effluent discharge as required by the Permit.
See Effluent Sampling Section.
Laboratory
Yes
No
NA
NE
Are field parameters performed by certified personnel or laboratory?
❑
❑
■
❑
Are all other parameters(excluding field parameters) performed by a certified lab?
❑
❑
■
❑
Page # 3

Permit: NCG500250 Owner - Facility: Parkdale Mills / Plant 23
Inspection Date: 08/22/2007 Inspection Type: Compliance Evaluation
Laboratory
Yes
No
NA
NE
# Is the facility using a contract lab?
❑
n
■
❑
Is proper temperature set for sample storage (kept at 1.0 to 4.4 degrees Celsius)?
❑
❑
■
❑
Incubator (Fecal Coliform) set to 44.5 degrees Celsius+/- 0.2 degrees?
❑
0
■
❑
Incubator (BOD) set to 20.0 degrees Celsius +/- 1.0 degrees?
Q
n
■
❑
Comment: The facility staff must ensure the effluent pH and temperature are analyzed
by a laboratory certified by the State of North Carolina (field or commercial certifications)
in wastewater analyses.
Effluent Sampling
Yes
No
NA
NE
Is composite sampling flow proportional?
❑
❑
■
Q
Is sample collected below all treatment units?
❑
❑
■
n
Is proper volume collected?
❑
❑
■
❑
Is the tubing clean?
❑
❑
■
❑
Is proper temperature set for sample storage (kept at 1.0 to 4.4 degrees Celsius)?
❑
❑
■
❑
Is the facility sampling performed as required by the permit (frequency, sampling type representative)?
❑
■
❑
n
Comment: The facility failed to comply with the effluent monitoring requirements (twice
per year) of the Permit. The facility staff must ensure flow measurements are performed
during the sampling events.
Effluent Pipe
Yes
No
NA
NE
Is right of way to the outfall properly maintained?
n
n
■
❑
Are the receiving water free of foam other than trace amounts and other debris?
■
n
❑
❑
If effluent (diffuser pipes are required) are they operating properly?
❑
❑
■
❑
Comment: The effluent appeared clear with no floatable solids or foam. The effluent
is discharged to Grants Creek via stormwater drainage system.
r,__—:a
V..
Nn
MA
h!F
(If the present permit expires in 6 months or less). Has the permittee submitted a new application?
n
❑
■
❑
Is the facility as described in the permit?
■
❑
❑
n
# Are there any special conditions for the permit?
n
❑
■
n
Is access to the plant site restricted to the general public?
■
n
❑
❑
Is the inspector granted access to all areas for inspection?
■
❑
❑
❑
Comment:
Page # 4

■ Complete items 1, 2, and 3. Also complete A. Signature
item 4 if Restricted Delivery is desired.
■ Print your name and address on the reverse
so that we can return the card to you. Received by (Print d Name)
■ Attach this card to the back of the mailpiece,
or on the front if space permits.
1. Article Addressed to:
D. Is delivery
If YES, en
J ❑ Agent
❑ Addressi
C. Date of Delive
tem 1? ❑ Yes
to ❑ No
! MR LEE THOMAS, EXEC. VP OF �cr 1 2007
PARKDALE AMERICA
PO BOX 1787 3. Service
GASTONIA NC 28053-1787 Certified I tS r��k�
swp/wb 9/4/07 ❑ Registered M ece
❑ Insured Mail ❑ C.O.D.
for Merchandi:
4. Restricted Delivery? (Extra Fee) ❑ Yes
2,i 271`d 6bid S 2�882 74
oc c....... Zi211 =-k—..... nnnn n............. o,...,.., o,.....,... .n..�,.� n., ...�

UNITED STATES POSTAL SERVICE 111111
Sender: Please print your name, adyr-qss, and ZIP+4 in
Y ` '
NCDENR C) 10
e"
SUFACE WAT1 R`PROTECTIN
610 EAST CENTER AVE
'SUITE 301
o
IMOORESVILLE NC 28115ri
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Postage & Fees Paid
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P ,mit uo. G-10

September 26, 2007
Mr Wes Bell:
Per your request enclosed is the water test results from Parkdale 23.
If you have questions, please feel to call.
Thank You
Mr M. Cecil Ward
Plant Manager
Parkdale 23
Landis, NC
SEP , 24 -1
E MR -
ON" o Wofor Rotft t
W oT '
o
U
/N U.

lk

/26/2007 11:46 7045BB8333 PAR LABS.CHAR NC
PAR Lmbora4ories, Inc.
P� R 2217 Graham Park Drive
cneoRaroare9, INC PO Box 41 1.c483
Charlotte, NC 282AI-1483
Phone:, 7bA_588-8333; Fa,(: 704.588-8335
NC Cerr N 20: sc Cerr x 99003
www parlabs.com
REPORT Oy ANALYSES
Attn: CECIL WARD
PROJECT'NAME: SEP 0''
PARYDALE MILLS -PLANT 22 DATE•'Oq/25/D1
100 S. MAIN STREET
LANDIS, .NC 28088-
S.AMPLI NUMBER- 80357 SAMPLE ID- SEWER GR11TE
DATE SAMPLED- 09/24/07
DATE RFCEIVF.D- 09/25/07 SAMPLE...- GJ
TIME RECEIVED- 0900 DELIVERED BY- G-7
Page 1 of 1
ANALYSIS
F"TELD TEMPERATURE
PH VALUE
FLOW
PAGE 02
SAMPLE MATRIX- WW
TIME SAMPLED- 1690
RECETVED BY- CT
TYPE SAMPLE- Grab
,;NALYBTS
METHOD
DATE
TTt4E
BY
THERM.
09/24/07
153i;
GJ
:L6
degrees r
EPA''150.1
09/24/07
1630
GJ
6.2
units
PLOW METER
09/24/.07
163C
GJ
+/-2.5
GPM
LABORATORY
DJRECTOR-•=—

rAl
NCDENR
North -Carolina Department of Environment and Natural Resources.
- Division of Water Quality
Michael F. Easley, .Governor William G. Ross; Jr.; Secretary
Alan W. Klimek;. P.E., Director
November 15, 2006
Randall Ferguson .
Parkdale America
100 Mill St
Lexington, NC 27295
Subject: NPDES Permit NCG500000 renewal .
Certificate of Coverage (CoC) NCG500250
Parkdale Mills / Plant 23
Rowan County
Dear Permittee:
The facility listed above is covered under NPDES General Permit NCG500000. NCG500000 expires
on July 31, 2007. Federal.(40 CFR 122.41).and North Carolina (15A NCAC 2H.0105(e)) regulations require
that permit renewal applications must be filed at least 180 days prior to -expiration of the. current permit. If
you have already mailed a, renewal request, you may -disregard this notice.
To satisfy this requirement, the Division must receive a renewal request postmarked no later than
February 1; 2007. Failure to request renewal. by this date may result in- a civil penalty assessment. Larger -
penalties may be assessed depending upon the delinquency of the request: This renewal notice is being sent
well in advance of the due date so`that you,have adequate time .to prepare your application.
If any discharge previously covered under NCG500000 will occur after July 31,.2007, the
CoC must be renewed. Discharge of wastewater without a valid permit would violate North Carolina' .
General Statute 143-215-.1; unpermitted discharges of wastewater maybe assessed civil penalties of up to. .
$25,000 per day.
If. all discharge has ceased at, your facility and you. wish to rescind this CoC [or if you, have other
questions], contact me at the telephone number or e-mail address listed below.
Sincerely, _ �.��.r=,
!l!.7i6;
Charles H. Weaver, Jr.
NPDES Unit. _ nroV 1
cc: Central Files
NPDES File
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
512 North SalisburyStreet,: Raleigh, North Carolina 27604
Phone: [phone], extension 511 / FAX [phone] / [e-mail]
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post.Consumer Paper
'One
NofthCarolina
Naturally

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Alan W. Klimek, P.E., Director
July 26, 2002
MIKE SMITH
PARKDALE MILLS INCORPORATED -PLANT 23
531 COTTON BLOSSOM CIRCLE
GASTONIA, NC 28053
Dear Permittee:
1�•
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Subject: Reissue - NPDES Wastewater Discharge Permit
Parkdale Mills Incorporated -Plant 23
COC Number NCG500250
Rowan County
In response to your renewal application for continued coverage under general permit NCG500000, the Division of
Water Quality (DWQ) is forwarding herewith the reissued wastewater general permit Certificate of Coverage
(COC). This COC is reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of Agreement between the state of North Carolina and the U.S. Environmental Protection Agency,
dated May 9, 1994 (or as subsquently amended).
The following information is included with your permit package:
* A copy of the Certificate of Coverage for your treatment facility
* A copy of General Wastewater Discharge Permit NCG500000
* A copy of a Technical Bulletin for General Wastewater Discharge Permit NCG500000
Your coverage under this general permit is not transferable except after notice to DWQ. The Division may require
modification or revocation and reissuance of the Certificate of Coverage. This permit does not affect the legal
requirements to obtain other permits which may be required by DENR or relieve the permittee from responsibility
for compliance with any other applicable federal, state, or local law rule, standard, ordinance, order, judgment, or
decree.
If you have any questions regarding this permit package please contact Aisha Lau of the Central Office Stormwater
and General Permits Unit at [phone], ext. 578
cc: Central Files
Stormwater & General Permits Unit Files
Mooresville Regional Office
Sd+ DEPT. OF ENVIRRONADII 1,
A9 ,ID i',1i iai;A P EG0LJI! E3
wvva
for Alan W. Klimek, P.E. JUL 3 1 2002
Sincerely,
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Carolina
Department of Environment,
Health and Natural Resources_
�1/ Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. E. T. Haynes, Corporate Engineer
Dominion Yarn Corporation
P.O. Box 8105
Landis, North Carolina 28088 - 8105
Dear Mr. Haynes:
/AM
••
ED FE F1
June 19; 1995L•
I�Ii �iJi jK. a:a : .c...
i 21 1` 95P
w1swi; 6f E;!'dlszatBP�Eti(iti I;i�idt�CL%? id'i
Subject: NPDES Permit
Biocide Additives
Dominion Yarn Corp._7.Linn-Plan
NCG500250. - Rowan County
Dominion Yarn Corp. - Corriher Plant
NCG500249 - Rowan County
The Division of Environmental Management (DEM) has reviewed the information in your letter of
May 8, 1995 to the Mooresville Regional Office, concerning the use of the biocide Ancocide 4050 at
Dominion Yarn Corporation's Linn and Corriher Plants. Our review has revealed that the biocide additive
should be appropriate for use in your application at the stated dosage rate and discharge conditions.
The Division grants approval to Dominion Yarn Corporation, Linn and Corriher Plants, for the use
of the above mentioned additive in its process water.
Should you utilize a different additive in the future, you should contact this office and submit the
appropriate information for approval prior to the change.
If you have any questions, please contact Susan Wilson at [phone], extension 555.
Sincerely,
1�3� 7Z� qdvl,�
A. Preston Howard, Jr., P.E.
cc: lkoresuille Regional --Office
Aquatic Toxicology
Central Files
P.O. Box 29535, Raleigh, North Carolina 27626-0535 . Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

DIVISION OF ENVIRONMENTAL MANAGEMENT
June 1, 1995
MEMORANDUM:
To: Susan Wilson
Through: Matt Matthews ( ' From: Melissa Rosebrock4/
Subject: Dominion Yarn Corporation - Linn Plant
Use of Biocides
NPDES No. - NCG500250 (formerly NC0080039)
Rowan County
N.C. DE PT. Or
ENVIRONZM NT, HEa LT' a.
& NATUP.AL RESOURICES
,SUN 8 1995
Dh`ESIuil GF E'ci�'If?GamITAL FAMAGENEHI
VQQRESVIUE RESIOFIAI OFFICE J
Dominion Yarn Corporation (Linn Plant) has submitted Ancocide 4050 for biocide approval.
Data submitted by the subject facility concerning the dosage rate of the compound, system volume,
average daily discharge, degradation, toxicity of the active ingredient and/or breakdown product, and
minimum stream flow have also been reviewed and evaluated.
Toxicity data supplied by the facility was for rainbow trout (whole product LC50 = 20.0 mg/1).
Given the geographical location of the facility, the more appropriate toxicity data would be for the
Daphnids (whole product LC50 = 24.8 mg/1). This revision did not alter the final analysis portion of the
worksheet (part IV, page three).
Calculations summarized on the accompanying worksheet predict that the use of Ancocide 4050
at the stated dosage rate and discharge conditions will not result in toxic impact to aquatic life in the
receiving stream. Therefore, the use of this product as a biocide at the Dominion Yarn Corporation Linn
Plant is deemed acceptable. If there are questions regarding this review please contact me at (919) 733-
2136.
Attachments
cc: .Rex Gleason-MRO
Central files

Dominion Yarn -Linn Plant BIOCIDE WORKSHEET
PERMIT#: NCO080039
RECEIVING STREAM: UT Grant Creek
7Q10 (cfs): 0.00
I.W.C.%: 100.00
PRODUCT: Ancocide 4050
ACTIVE INGREDIENT: 5% 2,2,-Dibromo-3-nitrilopropionamide
HALF LIFE (DAYS):
LC50 OF SELECTED TOX DATA (MG/L)
DECAY RATE:
DOSAGE RATE (GRAMS/DAY):
AVG DAILY DISCHARGE (MGD):
VOLUME OF SYSTEM (MIL. GAL'S):
0.02
STEADY STATE DISC CONC:
0.9990
24.80
DEGRADATION FACTOR:
34.757
34.50
APPLICATION FACTOR:
0.050
4600.00
0.009
INSTREAM BIOCIDE CONC:
0.999
0.035
REGULATED LIMITATION:
1.240
PASS/FAIL:
PASS

iv • V+ U nit 141 601L IL
NI)ERSU\T CfiEN CO 002
A
AMCG
I,UAUrY SERVICE
April 26, 1995
Mr. E.T. Haynes
Dominion Yarns, Inc:
P.O. Box 81.05
LAndis, NC 28M8-8105
Dear Mr. Haynes:
This letter is to certify that our biocide product; ANCOCIDE 4.050, does not contain any
metal compounds.
If you have any further requests, please feel free to call on us.
Sincerely,
ANDERSON CHEMICAL COMPANY, INC.
Steven R. Fennell
Laboratory Supervisor
Anderson Chemical Co., Inc. P.O. Fm 45M Mawr. Georgia 31213 Pkne [912) 745.OQU Fimf M2) 7Q-5382 AACO U a carperare. HeWquarms
Qher kcetias Austra" = Camda 0 Caikm ■ CanU-aI America 5 Korea ■ Medea ■ 5otith Ame-ite

BIOCIDE/CHEMICAL TREATMENT
WORKSHEET-FORM.101
The following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
North Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
retumed yvith all appropriate data entered into the designated areas with calculations performed as indicated.
I. Facility Name Dominion Yarn — Linn Plant
NPDES#NC 0080039
County Rowan
Receiving Stream UT Grant Creek 7010 0 (cis)
(All above information supplied by the Division of Environmental Management)
What is -the Average Daily Discharge (A.D.D.) volume of the water handling systems to the receiving water body?
A.D.D. = 0.009 (in M.G.D.) (9000 gal/.day)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
(A.D.D.) x 100 . _ (.009) X 100
IWC = (7Q10 x 0.646) + (A.D.D.) — ( 0 )(.0.646) + (.009 )
100
This value (IWC) represents the waste concentration to the'receiving stream during low flow conditions.
II. What is the name of the whole product chemical treatment proposed for use in the discharge identified in Part I?
Ancocide 4050
Please list the active ingredients and percent•composition:
2,2 — Dibromo — 3 - nitrilopropionamide 5.0 %
Note: If ingredients contain the metals copper, chromium, or zinc, also complete page 4, Sun0emental Metals A-etvsis
)What feed or dosage rate (D.R.) is used in this application? The units must be converted to grams of whole
product used per day. _
D.R.= 4, 6 0 0 grams/day
D.E.M. Form 101 (7/92) 1

rcill:ty'Nam'e:.
Dominion Linn Plant NPDES #: NC 0080039
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for this. estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.)
Volume= 0.035 million gallons (35,600 gallons)
s .
What is the pH of the handling system prior to biocide addition?. If unknown, enter N/A. 7.5 — 2 .5
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk.
The degradation must be stated at pH level within 1/2 pH standard unit within handling system. Enter the -half
life (Half Life is the time required for the initial product to degrade to half of its original. concentration). Please
provide copies of the sources of this data.
H.L. = 0.0 2 Days ,► �Q ' q5 j
The decay rate is equal to ; X 0.69 = 3 4.5 =Decay Rate (D.K.)
Calculate degradation factor (D.F.)..This is the first order loss coefficient.
OQ9
D.F. _ (Volume)' + (D.K.) _ ( . 0 3 5 + (34.5
Calculate Steady State Discharge Concentration:
Dischg Conc. _ (D.R.) _ ( 4 , 6 0 0 ) 0.99 mgil
(D.F.)(Volume)(3785) ( 34.8 ) ( .. 035 ) (3 78 5 )
Calculate concentration of biocide instream during low flow- conditions.
(Receiving Stream Concentration)
(Discho. Conc.) x (IWC%) _ ( ) x ( ) = mg/I
100 100
Receiving Stream Concentration
III. Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be
in mg/1). Please provide copies of the sources of this data.
Organism
Bluegill Sunfish
Rainbow Trout
Fathead Minnow
Daphnids
Largemouth Bass Fingerlings
Test Duration
96— hr
96— hr
96— hr
96— hr
96— hr
LC50 (mg/1) * .
1.3
1.0
1.36 `i
1.24 �I�I�
1.63
D.E.M. Form 101.(7/92) 1. ' 2
*Active Ingredient Data
*Rainbow trout LC'50 =_1.0 mg/L
Active Ingredient = 5%

Facility Name:" Dominion Yarn Linn Plant NPDES #: NC 0080039
Choose the lowest LC50 listed above:
Enter the LC50: 20* Whole Product LC50 = 1.0 20
If the half fife (H.L.) is less than 4 days,. perform the following calculation. 0 5
Regulated Limitation 0.05 x LC50.— 1.0 m9/I
fi the half life (H.L.) is greater than 4 days or unknown, perform the following calculation.
Regulated Limitation 0.01 x LC50 =mg/l
- Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
1.00 mg/liter.
From Part li enter the receiving stream concentration:
0.9 9 mg/liter,
IV. Analysis.. .
If the receiving stream concentration is greater than the calculated regulated limitation, then this biocide is
unacceptable for use.
Name (Print)
J
-
.�re
Person m p°
Res nsible Charge �` v
D.E.M. Form 101 (7/92) 3 ' .

rdity Name:
suoolemental Metals AnW4112
If copper; zinc, or chromium are present in the proposed biocid'ai compound, complete this worksheet. A
separate form must be used for each metal and/or metal compound present
the conblocid . Lisf the metalt the etal,
its chemical formula,_ molecular weight (MW), formula weight (FW),
andomplete a separate form for every metal present in the biocide.
compound in the biocide (MCC). C
NPDES #: NC
eht of Metal Formula Weight Concentration in Biocide
Metal . 0—hemical Formula Molecular Wig
EXAMPLE
Copper CuSO4 5F•!20 63.546 g/mole 249.630 g/mole 0.2
Dosage rate of Biocide (DR) (from page 1):
DR grams/day
Average Daily Discharge (ADD) (from page U
ADD million gallons/day
Discharge Concentration (DC) of Bloclde:
DR grams/day) _ = grams/million gallons
DC = ADD = ! million gallons/day)
Convert DC to micrograms/liter (ppb),
1 x 106 uq/a
DC (µg/I) _ _ C (grams/million gal) x 3.785 x 106, liters/million gal.
Calculate the fraction of metal in the metal -containing compound (MF):
grams/mote) _
MF = _ grams/mole)
Calculate the fraction of metal in the biocidal compound (BF):
MCC % % _
BF = MF x 10 = x (T00)
Calculate the concentration of metal in the discharge (M):
M=DCxBF=
ug/i x
Calculate the instream metal concentration (IMC) at low -flow conditions:
°
IMC = M x 00% a ig/I x 100 % _ � I
Regulated iimitatlon of metal (from below):-------J19/i
General Statutes 15 1-1 a me:
quality action level* Zinc-•50 µgn water quality action level*
Copper- 7 µg/l water
Chromium- 50 µg/l water quality standard
(•Values which exceed action levels must be addressed directly by aquatic toxicity testing.)
D.E.M. Form 101(7/92) 1 4

DOMINION YARN
C 0 R P 0 R A T 1 0 N
May 8, 1995
Mr. Kim H. Colson, P.E. R�G'F�U
State of North Carolina ��i �;, so
Department Environment Health and Natural Resources
919Non Street
P.
0Box 950
Mooresville, NC 28115
Dear Mr. Colson:
�s
Attached are the biocide worksheets 101 tht.�jt you requested for
Dominion Yarn jinn Plant NPDES Permit NCO080039 and Corriher
Plant NPDES NC0080021.. N-JC CD -c,cl)
Please note that sheet number 4 is not filled out because the
biocide that we -are using does not contain metal.. (See
Attachments)
Sincerely,
DOMIN .ON YARN CORPORATION
E. T. Hay es
Corporate Engineer
ETH/bfw
Attachments
c: Allen O'Shields
- VP Manufacturing
Dan Wiggers
- Plant
Manager
Joe Purvis
- Plant
-Engineer
Bill Crocker
- Plant
Manager
Mike Overcash
- Plant
Engineer
P.O. BOX 8105 i LANDIS• NORTH CAROLINA 28080-8105 / 7041857.1121 1 FAX [phone]

05/30/95 14:17
'aM 741 8812 kNDERSON CHEM CO
a 001
MESSAGE T0:
COMPANY NAME:
TELEPAX NO.:
REFERENCE:
_.. a
ti F �iF.ti
k DATE:{ TII:
rnr-ssAGE FnTA: ,Steve Ftnnell
Lab SU.0euVI-q0 '
„irdinler Yamns7 NI ES Blecide WOrk Shut
NU. OF PAGES:
Here is the doeume ►iation you rcgimstLd. I have contacted Mr. Bob
Karbowst, Technical Representative of DOW Che ilieal C0xUp4My.
He ' reports they half ]if(,- data is roporte d by Exaer, J.H. net al. in a
report titled "Rates ord Products of Deeoui- itio� or D I '1.
Agricul n l and food �� 9�, is, Vol 21, No. 5 �g 83�-842, �.9'�3. 1
was un ablo to gol a coo-py of ` s report. I-Iovvcyer
r. Karbowsld is going to Tnaff me a copy.
Along with this fax I m.., sending you epee is frog? Me Dow
publication "Dow _Antim-k-kobiad' 7287.2 . This is tip sovrce, of 111C
toxicology to aquatic Leo table 20 page 33). , .
MM204
Aridepsan C,emica! Company, Inc. 1840 �lllatervilla Road P0, pox g507 N18L.oll, Georgia 31213
Phone (9icj 745-0466 Fax [phone] -

05/30/95 14:17 V912 741 8812 . ANDERSON CIM CO
U-002
-e
Sure+' o
reaction
and increasing eithcr or both will incrcasc
the decomposition rate. Hydrotv�is i.9 relatively
rapid at neutral to slightly alkaline pH. This
is Important bec2,usc anwin! :eaters in most
rivers, e5 F--Ually in uidustrial arcas, �.tv
(typie�lly) slightly alkaline.
In determining. the hydrolysis products of
DOW DBNPA, the concentrations of DOYV
D13NPA (ca. 12,MO-15,(M ppm) were, of
necessity, considerably higher than thoso of
use conditions (ca. 1 ni). The pH profile for
the hydroOi'Vlysis of DDBi IFA at 25°C, is
shrn,�i in Fguro.10.
pFI vs. Rate of Fly&oivsi4 or
DOW DDNPA at25°C
DOW DBDTPA possestwo ccter-
zed
istics 1lial maim it unique amoIlg nonoridIzIng
3.0
biocidGS: extMXnely fast gntimicrabrr1 QCtiort
and mpld &Wmdatioa to relatively r. on -toxic
2.0
e: td products. The dotajtlant degadadon path-
v,T, under use conditions involves reaction
1.0
with nucleopliilie subsw-nces car org-,wsic m;te-
rial invariably found in water.
-
Addidotla! dWat �tion reactions include
PD dependant hydrolysis, reaotion with soil,
�-
o l•0
and breakdown via exposure to ultraviolet
rt diation.
Figure 9 sliaws thegpieal degradation
2(I ,
path�ys for DOW DDNFA.
-3.0
?ate o hydsol�s of )DOW 02-NaA
The carat hydral sic of S3ANPA
-f 0
y y 2 0 2 d G 8 t0 12
ha; been suldied in duute solutions avadom
p1 levels. The reactior_ proceeds via d:�xbox pH
yIation to dibromoaacctouitrle. The rate of `
by droiys is a function (,if PII and L=perattare, '
FICLIIO 9 — Decomposition Ruthways of DOW DBNPA
Vucicophiles
Light
Y �
NCCH,CONH, + 20f'
111,0
ttiCCII,CO,I r
H,0 .
\CGN,CO,H
till j
1I0.-CCz, i,CO,N
t ilr liydralysis
NC II -, pH 7,4 T,:, = 9 hours
6r NI[; -SU
NCCFIRr_ + CO, 4. NH,
1)117.4 Tu, = 21 dnya
I Br,cFlcor;Ft,i.
Br,Ci ICQ,11 + NI I,
pFt 7.4 T,,, 100 days
\CCO,FI + 2 nr
H/
IID,Cco,H il" ` z Co,
31

14:17
912 741 8812 . ANDERSON CMI CO
D,�gmdfatjon of 130W UUNPA
in the Pres=00 of soil
DBNPA is also degraded by a number
of nueleophilys such aS sulfite, bisulfim,
diiosuffate, and sulfide. Thy compounds
debrominate DBNPA instantaneously to form
eyanoacetamide. Soil, which is a source of
a number of nucteophiles, also accelerates the
dograda6an of DBNPA. This lies, baen demon-
strated in a number of experiments in which
traces of DBNTPA were added to an aqueous
suspension of a number of difforent types of
soil. Typically, half-lives of 4 hours wcsre
observed at neutral pH, and 15 hours at pH 5.
The disappearance of IOW DBNPA
solutions in the preen+-w of soil (Table i9)
could bedue to absorption,ehemicat dcgrada-
tion, microbial debadation, or hydrolysis.
Microbial degradation of DBNPA has been
dcmonstmWd by tic use of tracur techniques.
Rapid reaction in the Soil occurs with a
variety of nucleoophilic reagents to form
cyanoacatatzlide, a compoutdd which is biu-
degradable and winch can hydrolyze furtlw:r
to biodc-Mdalble such Ps rnalonio
acid.
t""Herob'sw1 deg sdadmaa of r)gN A
In addition to degradation by hydrolysis,
phowdogradation, arld reaction w4h nucleo-
pUes,DBNPA Faso dcgrvdesto carbon dioxide
4?1003
under nucrobial attack, This microbial de-
gradation has bin documented under varying
laboratory conditions by crac:er technigm-,s,
Tho fats of the degradgtes .,` DBNPA is falrther
hydrolysis and biodegradability.
Benctior, of DOW D B-MA 1Y1th sual3ie'lad
DccompcsiL;aa tests show that DBNPA
is de8rnded by sunlight with the for laiiorrot
iriorgatlic bromide ion. Ilt one expclitnent,
dilute aqueous DBNPA was maintained in a
scaled tube in cm outdoor environment for 28
clays (pH 4). Icss than 1 percent of th4 DBNPA
mmained and more Own.95 percent of the
theoretical amount of bromide `vas formed.
The ha.if-life Nv,s thus estimated to be 7 days
under ambient climatic conditions. Exposure
of a dilute solution of OBNPA to a sunlamp
in a labordtciry rc,-sultcd In a half-life of lms
than f day.
The amoumt of DOW DBNPA remaining
after exposure to sunlight for 28 days is fens
t1t--a I peaz:eltt of all original test concentration
of 4000 ppm. The percent of DOW DBNPA
from tale same. solution after 28 days in dark
um is 91 perccnr, Thus, photolytic degrvdaiion
of DOW bBrgpA is rabid, and in fact, is 5i'n-li-
ficantly L�ct relaiive to hydrolysis at pH loss
than 5.
LacbIG 19 — i-lalr•lito of DOW DBNPA in Various Soil `lYpcs
PH of
D,cscription
sand
silt
Clay
carbon
slurry
. T,;, hr
Sanely loam
724
21.2
4rt
0.46
-.7.5
4
Lwrn
15.0
41.0
21.0
23 %
4.8
12
SutY loam
13.6
64.0
224
27-6
5.8
15
Sandy loam
59.0
2M
13.0
1-16
6.5
15
Loamy sand
M
11.6
5.4
170
5-0
G
Silty clay loon
IU.0
62.0
24.0
I.f-8
5.1
25
Loam
- M.6
47.0
244
Is,6
-M
15
32

05/30/95
14:18 U912 741 8812 . ANDERSON CHEM CO
[a 004
I
;..'fill v¢lve4 Zwcd on active Pr
DBNPA
'95ja"rar:ftdeltt8 irrtffrval
PercvnwFa of abnormall ,
+1 devalo/--ed larwe (not
rngMliv)
F)sh dPtnd wfluMfe to3dC1'Alog,
Table 20 pmvic: s info.rmation about the
toFicity of DOW Dl :'IPA to aquatic, marine,
and avian wildlife.
Table 20 —. Eeaiu=don of li azards of
2�-ai�mma3-
nia�. �copiou? ;ride (�HT�;P!'e)
to `'t L{': ilt•
AquaLc Life
Blucgill +tnfisch, 96-hour LC�v
UI (1.0-1.6)a mG/1
Rtinbmv trwt, 9trhjur LC�
1.0 Et ,e IS) mg11
Fathead mimiow.96-hour"t"
13b (I-2A-AA) mil
Dnphn1d-, -'.3-hour LGy
1.2.1(1.Q5-I.qq) mgA
Lurv:MUUQ` bass
95-hour LC., .
1.62. ? 1.51.1.71) ,nyjl
Nlarine Life
F-i- stern oysters (ta.mc),
48-tour i�
>055,-<Lo mg/1
Fiddler crab, 96-hour I-C.,
14 (53- 6) mg/I
Pink siiri?tp, 96ehour
>l.i . <3.2 Mo
Glace shrimp, 96-hour LC
115 (8.69=15.22) Ri /i
A iatic clsm. 96-hour LC,
>8r ngll
lirac%:;it `siAtCr Cl..rtl,
24-hour IC,,,
20 m—&I
Shcopshead niianow.
c,�i-hour [ C,,
1.4 (I.0-2-0) in /l
Avian I,.ife
Mallud duck, oral LDI 5
Mslc
Famal--
205 n �g
216 mg/l.g
Bob Whitc gtra-d, oral LD,
Imalc
i emote
166 nrg/kb
150 r s; 4a
Toxicityhtm-d fo 9sh -
Based on the se*eral degradiation path-
vr`aysofDFI`bMntldiisinteri," aatedgrradates,
tho proper use of DMA in industrial water
systems results only in traces of the compound
in discharge water. Chemical acid biological
decomposition, and dilution of (tic oifluent
vmter, result in ropid disuppcururwo of these
trace9. Tl=efore,.DBNPA does not present a
Serious fish toxicity 1IM--ardwhen used properly,
However, all discharges of DBIgPA inre lakes,
tfregni.t. ponds, or public tvste:e must be in
accordance-vitliaNational PolluLan tDisch.-roe
Flunination Sysfern (NMES) perrnit. The cut -
mat data indicatethat DBMAhas thepotendal
;or localized fish kill only if a large amount
of biocide is discharged into a lake or river.
For further guidance, contact your local EPA
regional office.
33

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ANCO°
QUALITY SERVICE
February 1, 1995
Mr. E.T. Haynes, Corp. Eng.
Dominion Yarn Corporation
P.O. Box 8105
Landis, NC 28088/8105
Dear Mr. Haynes:
IV.C. WEPT. OP
ENVIRGPdNr;,l _r REALTF3
NA'rtJAL F t� R ,
FES 2 1 € 9 95
a ' "11�4 .:._...ti4• nl; y,7iVv e,h,iia�j
Your Service Representative, Mr. Scott Jordan, advises you require information on the
water treatment products that we have recommended to replace the existing products at
Corriher Plant.
Corriher Plant: You currently use these products:
1. HYDROFENE I
2. HYDROFENE II
3. BAC-20
4. LESTER L-1
5. WATERENE 560 POSITIVE
Yellow metal corrosion inhibitor
Corrosion and scale inhibitor
Dibromonitrilopropionamide
Less than 9% solution of Hydrogen peroxide
Antistat
We would use the equivalent products as follows:
1. ANCOOL 3113
2. ANCOCIDE 4050
3. ANCOSPERSE 3810
4. D-O-Stat
Corrosion and scale inhibitor
Dibromonitrilopropionamide
A low foaming Anionic Surfactant
Antistat
ANCOOL 3113: All organic based, multi -metal corrosion inhibitor and deposit control
product. Formulated for waters which tend to be more corrosive and less scaling contains
metal cleanse for unproved corrosion inhibition.
Components: organophosphonate, synthetic polymer blend, tolyltriazole (yellow metal
corrosion inhibitor), organic corrosion (inhibitor for ferrous metals) and metal cleanse II
(Dihydroxy Alcohol).
Anderson Chemical Co., Inc. P.O. Box 4507 Macon, Georgia 31213 Phone [912] 745-0466 Fax [912] 742-6332 ANCO U.S. Corporate Headquarters
Other locations: Australasia 0 Canada ■ Caribbean 0 Central America ■ Korea ■ Mexico 0 South America

Page 2
Dominion Yarn (Corriher Plt)
Landis, NC
ANCOCIDE 4250: Is our dibromonitrilopropionamide (DBNPA) product. This is a non -
oxidizing biocide effective against all biological growth. ANCOCIDE 4050 degrades quickly
reducing environmental concern.
Components: 5% Dibromonitrilopropionamide
ANCOSPERSE 3810: Is a specially formulated low foaming anionic surfactant designed to
disperse airborne debris, oil and sludge in cooling water systems and air washers.
ANCOSPERSE 3810 is low foaming, biodegradable modified ethoxylate based product.
Components: Ethoxylated surfactants, sodium hydroxide.
D-O-Stat: Is a quaternary ammonium compound. The catabolic nature of this product
makes it the most highly surface active to control static charges in air.
Component: Quaternary ammonium compound
All these products that we have recommended are equivalent to the existing Lester's
products. We realize that you have a current NPDES permit to allow you to discharge the
overflow and bleed for your air washers and cooling towers into the storm drains.
Therefore we are trying to duplicate the current program already approved. I also
understand that the holding time for biocide at Corriher plant is 0.2 hour. Our biocide
program will meet this requirement.
Should you have any questions or require any additional information after reviewing the
contents of this letter, please do not hesitate to contact us. We thank you for your time
and consideration.
Kind regards,
Y n . g C4.
ran . Jain, .D.
R & D Manager
KBJ:sd; KJ157

MATERIAL
SAFETY
DATA
SHEET
SUPERIOR WATER TREAT]NG SERVICE
HAZARD RATING
4 = SEVERE
3 = SERIOUS
2 = MODERATE
1 = SLIGHT
0 = MIIdIMAL
DATE: 1/20/90 REVISION: 6/24/92 ISSUE DATE: 8/3/92 CHEMTREC PHONE NUMBER: (8W)424-93W
:iiti}•:ti}+?i:{k:i ti'::iiS'}:iiii:k}:iii;}Y i +,:j{{ •. •:.. r
................................................................ w:::::;.....••v:n:vii}rir}�.:v:nv::.x,•.w::.v:.v:::::.v::::....... w:::::::.v:. ...............................
nv.� :•:::: nv: v.v:::::::::::: w:::.v::. •x:•w.:w•:u::.:.:.v:::nv::•}:•}r:•:{•:.v.v:. +.... ......:::::::•:.•:::vv:::::::::.v ::.nv. v::.}: }::.v••.v'4r}}.... ....,.n...........'•%{•r?'•}:;:.}:?:trh:•Y }:{•rr;:{:{: {{•iky ,n., .. 4...x ...
............................:..........r...r.:....r................. ...... ...... :........ ..., a. .... .. ....................... :.......x•....k....,..+�..,.............rx......+..:......... r:.....:.:.:.: ... .R... „�. •,::: }.•.kC+}.........,..
..........t....{....................................................tr......t..... r..........,t....tt..:.,t...r.t......................f....... ........ .' .. }
v.. f.....:.......:: r:::.t :::}:;r}+•y:•}:•ry:•r:::kk-:::::.;x::'•}:y:':.{:;:}?•{''<i�: �''}::<:k`:;:>:;•}i}:r r:.}:..:•}:•>
::rt:•r:•r:{}�»::�.r:.r:{:.r:.r.'•:{.ri:{.rrr:-i:., .. ..: f•:...::.::::..... ,...: f•.: �:-::::.{t+,•.,. `�{•.,............. r:..
::,•:.,•:::.,::.tt•.:....+..r..{.:.:::::::::.::>:: :•-::::.+.-:: :•:::: •:::..... rt.:•: ~.•::: r:.p'Q ..... � •.: ,. ..}r(;4?3:•+.}:::::S:�rk�:k�'4ri:}::kk�i::;:;::::::�i{�•:•::'S:};:ti:::>!:�:�i ....
....v........v.t....v...:.4.......................v ................... n............ .. ....... .......... \.n......: n:v.:...:: • :•::....... 4.rnx•�.::: k: ii:£4�i:}iv.}::::: xj}: �::.
TRADE NAME: ANCOOL 3113
CHEMICAL NAME: Aqueous Solution: Organophosphonates; Triazole; Synthetic Polymers
FORMULA: Proprietary Formulation
CHEMICAL FAMILY: Scale and Corrosion Inhibitor
Sodium Hydroxide 1310732 TLV = 2 mg/m3 (ceiling limit)
LD50 = 240 mg/kg (rat)
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
.. ............n t.................................v..........{....v.. ....... n..::::::...:::::::.........n•:.v:nv\-..4ri}}::}:?^v.......... •r{J.... ...................
ir:•}:•••}?}:4}r}i i:k:}:•}}:^}:•}:•r:J:.v::::::: v::::r::::::::::::};:.�••rvv:}:}}:: ir:•+}:•:•}.... w:.v; .:.
•:{?�:v} L:6'•r::vr:v::;{•ii}}:•}:•rife}:•}:k•}}}•{: {.;.}:^:v..... ::•: w::::::::::::::::w.
. ..... n..:.......... ........... .. .:........... w:.:::; :,•::::: }:::.:v:::r\vvnv: v:: :w. . .. .. .. .: :•::: .: .: •: •:.� -v: -: :• •...... v... ;... •.:.....................:..8... •:....1...::::::A{n{
� ::: fv.• v.vv::: n.v::::.::v::: nv.v:.v.:: n.v::.::vn: n. • • • vvf �: '• }{•: r:vvv h:4:{::k:ik•rr}:{^:k::
................t......:...............................:.... r..... .............................. }:: :. ;•} .r:{•}:: - ... ... v v' .if>' r m:::-v::::.::•v: •.
...................................: ........v ........................... ..r.. '}::::::•.:v•w:: •:•::•::•:::::::.iv.:}:}Y.y:.w:.'i ...Y...v:..r
:::: v. •: •::n.r.::•::v::v::::..r.;..;.-,:....••h:vv:w::::::::: wx::: }.•:::.v,v: ..yyaa���j' aY #
..........v. }:.......vv .. ............... Lif :. .:..:{yM:�YY.11:{?4:?{•}}::}tir}:J}i}rrrrr::4}}}.;^:v:v::vv}r}}viii: ii'r{•}'•:}.: .. }:}
.......................x..;..::::w............w::::::.}v}::.}}vy{;vx•{.}•::::.v...:..:::::: ::v.v:. v:::.: v::::r:•.;.y::::::::::::vv::::::::::::::....:::.:.v::.v::x: .;vr.ry:}r }: i::ti}•}r:.+r>.vey;.
....:..............:.vnx ... ........................x::!i:•}N}:::::.{+•}......:?}:?{.}}:•}:4:•...... :. . ......................... ..w: w................x.v.v.v:.:v:::: :•: :::?•: %4. ..... . .. . ... ''''}•}
::::::n.....�............................ r...........v :..: r.. r.........:.......................v.......n..... ........... n.... n..... n.... r..................
BOILING POINT (-F) @ 760 mm Hg 212 SPECIFIC GRAVITY (HZO = 1). 1.04-1.06
VAPOR PRESSURE (mm Hg @ 20'C) Like Water PERCENT VOLATILE BY VOLUME (%) Like Water
VAPOR DENSITY (AIR = 1) Like Water EVAPORATION RATE ( = 1) Like Water
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE Clear Brown Liquid. I ODOR Slight Aromatic.
FLASH POINT None
AUTOIGNITION
TEMP. Nonflammable
EXTINGUISHING
MEDIUM
SPECIAL FIRE FIGHTING
PROCEDURES
UNUSUAL FIRE AND EXPLOSION
HAZARDS
STABILITY
FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
LOWER NA
_ WATER FOG -FOAM _ COz _ DRY CHEMICAL -OTHER NA
Wear full protective clothing and use self contained breathing apparatus.
None
STABLE X CONDITIONS
TO AVOID: NA
UNSTABLE
CHEMICAL None
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of nitrogen (NOX) and carbon.
DECOMPOSITION PRODUCTS
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION TO AVOID: NA
DOES NOT OCCUR X
(CONTINUED ON REVERSE SIDE)

THRESHOLD LIMIT VALUE No TLV established.
EFFECTS OF OVEREXPOSURE:
EYE CONTACT
May cause severe irritation.
SKIN CONTACT
A�
May cause severe irritation.
INHALATION
May cause severe irritation to the mucous membranes.
INGESTION
May cause severe irritation to the mucous membranes and stomach.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT
Immediately flush eyes with large amounts of water for at least 15 minutes. Washing eyes within one minute is essential to achieve
maximum effectiveness. Seek medical attention immediately.
SKIN CONTACT
Flush contacted area with water.
INHALATION
Remove subject to fresh air.
INGESTION
Drink a large amount of water. If discomfort persists, seek medical attention.
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
SPILLED
WASTE DISPOSAL
METHOD
Dilute with water and flush to waste with excess water.
Dispose of in accordance with local, state and federal regulations for liquid and solid wastes.
VENTILATION LOCAL EXHAUST X ACCEPTABLE
REQUIREMENTS X MECHANICAL (GENERAL) PREFERRED
OTHER NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield and splash HAND
PROTECTION proof goggles. PROTECTION Impermeable Gloves.
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions. Do not transfer to
aluminum or galvanized containers.
OTHER PRECAUTIONS: Handle with care. Avoid eye and skin contact.
Kiran B. Jain, Ph.D.
PREPARED BY
ANDERSON CHEMICAL COMPANY. INC
posr OFFICE BOX 45M, MACON, GA. 31Z13
MACON M MPHIS DAIL\.S
(9M704(901)"&"l gm)6 Isis

c MATERIAL
SAFETY
DATA
SHEET
DATE: 03/30/89
TRADE NAME: ANCOSPERSE 3810
CHEMICAL NAME: Aqueous Solution: Modified Ethoxylate
FORMULA: Proprietary Formulation
CHEMICAL FAMILY: Surfactant
Sodium Hydroxide
1310732
471-nNTIR EC PHONE Ni TKIBER. iam\nA mn
TLV = 2 mg/m' (ceiling limit)
LD50 = 240 mg/kg (rat)
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
BOILING POINT ('F) @ 760 mm Ho 214 SPECIFIC GRAVITY (H2O = 1). 1.04 - 1.06
VAPOR PRESSURE (mm Ho @ 20'C) NA PERCENT VOLATILE BY VOLUME (%-) NA
VAPOR DENSITY (AIR = 1) NA EVAPORATION RATE ( = I) NA
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE Light Yellow Liquid I ODOR Mild
FLASH POINT None FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
AUTOIGNITION L.O\VI•:It NA
TEMP. Nonflammable
EXTINGUISHING _ WATER FOG —FOAM _CO, DRY C HEMICAI. OTHER NA
MEDIUM
SPECIAL FIRE FIGHTING Wear full protective clothing and use self contained breathing apparatus.
PROCEDURES
UNUSUAL FIRE AND EXPLOSION None
HAZARDS
STABILITY STABLE t
CONDITIONS
TO AVOID: NA
UNSTABLE
CHEMICAL Strong oxidizing or reducing compounds, aluminum, zinc or magnesium.
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of carbon.
DECOMPOSITION PRODUCTS
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION TO AVOID: NA
DOES NOT OCCUR X
(CONTINUED ON RI VISRSI? SIDE)

PAGE 2
THRESHOLD LIMIT VALUE No TLV established.
EFFECTS OF OVEREXPOSURE:
EYE CONTACT May cause severe irritation.
SKIN CONTACT May cause severe irritation.
INHALATION May cause severe irritation.to the mucous membranes.
I N G ESTI0N May cause severe irritation to the mucous membranes and stomach.
I'.Yl. CUN IAU 1 I lnlmealalely I[US11 eyes WAIT large amounts UI water Mr al least 1J uuuUlca, vra�uwp cyw .vuuw Vuc ulwuw 1� w�cu ual w awla .
SKIN CUN I AU I viusn contactea area wnn water.
INHALATION Remove subject to fresh air:
INGESTION Drink a large amount of water. If discomfort persists, seek medical attention.
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
WASTE DISPOSAL.
METHOD
Dilute with water and flush to waste with excess water.
utspose of in accoraance wnn local, state anU ICUCri11 1UgU1a11V11J IVI uyulu auu -- ---
VENTILATION LOCAL EXHAUST X ACCEPTABLE
REQUIREMENTS X MECHANICAL (GENERAL) _ PREFERRED
OTHER NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield and splash proof HAND
PROTECTION goggles. PROTECTION Impermeable gloves.
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions. Do not transfer to
aluminum or galvanized containers.
OTHER PRECAUTIONS: Handle With care. Avoid eye and skin contact.
ANDERSON C11EMICAL COMPANY, INC
POST OMCE BOX 4507, MACON, GA. 31213
MACON MEMPI11S DALLAS
(912)745--0 (901)91 "l [phone]
Kiran B. Jain, Ph.D. _ .. .
PREPARED BY
ANCO DOCUMENT' NUMBER AS3810.MSD

HAZARD RATING 2
'C� MATERIAL 0 4wSEVEREIOUFLAMMABILITY 0
SAFETY pMCC) 2=,MODERATE 0
DATA SHEET I =SLIGHT PERSONAL D
SIIPFRIOR WATER -TREATING SERVICE 0 = MINIMAL PROTECTION
DATE: 1/US/6/
REVISION DATE: 12/04/89
TRADE NAME: D-0 STAT
CHEMICAL NAME:
FORMULA:
CHEMICAL FAMILY
EMERGENCY PHONE NUMBER: [phone]
CHEMTREC PHONE NUMBER: [phone]
Aqueous Solution: n-Alkyldimethylbenzylammonium Chloride
(R)N(CH3)2(C7H7)+Cl-
(1»atcrnary Ammnni nm qn1 i'
MATERIAL CAS# HAZARD DATA
n-Alkyldimethylbenzylamonium Chloride 139082 No TLV established
LD50 = 550 mg/kg (rat)
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
SECTION III -- PHYSICAL DATA
BOILING POINT (°F) ® 760 mm Hg 212 SPECIFIC GRAVITY (H2O=4
VAPOR PRESSURE (mm Hg ® 20°C)
0.98-0.99
Water I PERCENT VOLATILE BY VOLUME (%) I Like Water
VAPOR DENSITY (AIR = 1) (Like Water I EVAPORATION RATE ( =1) I Like Water
SOLUBILITY IN WATER ❑ NEGLIGIBLE ❑ SLIGHT ❑ MODERATE ❑ APPRECIABLE V COMPLETE
APPEARANCE Clear Colorless Liquid ODOR Slight .Almond
FLASH POINT None
FLAMMABLE LIMITS UPPER NA
AIR (% by Volume) LOWER NA
AUTOIGNITION TEMP. Nonflammable
EXTINGUISHING [A WATER FOG %] FOAM RICO, DRY CHEMICAL ❑ OTHER
MEDIUM
SPECIAL
FIRE FIGHTING Wear full protective clothing and use self contained breathing apparatus.
PROCEDURES
UNUSUAL FIRE During a fire, irritating and/or toxic gases and aerosols from the
AND EXPLOSION decomposition/combustion products may be present.
HAZARDS
STABLE X CONDITIONS Under normal conditions,.the material is
STABILITY UNSTABLE TO AVOID: stable.
CHEMICAL Strong acids
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may.yield oxides of nitrogen (NOX) and
DECOMPOSITION PRODUCTS carbon. Ammonia and HC1 Ras may also evolve.
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION DOES NOT OCCUR g TO AVOID: NA
ILInKMIKII ICn nK1 OCVCGCC CInM

•'' PAGE 2
THRESHOLD LIMIT VALUE No TLV established.
EFFECTS OF OVEREXPOSURE:
EYE CONTACT May cause irritation.
SKIN CONTACT May cause irritation.
INHALATION May cause irritation to the mucous membranes.
INGESTION May be harmful if swallowed. May cause irritation to the mucous
membranes and stomach.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT Flush eyes with clean water for 15 minutes. If irritation persists,
seek medical attention.
SKIN CONTACT Flush contacted area with water.
INHALATION Remove subject to fresh air.
INGESTION Induce vomiting. Give large quantities of water. Seek.medical attention..
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
SPILLED
WASTE DISPOSAL
METHOD
VENTILATION
REQUIREMENTS
Dilute with water and flush to waste with excess water.
Dispose of in accordance with local, state and federal regulations for
liquid and solid wastes.
❑ LOCAL EXHAUST
® MECHANICAL (GENERAL)
❑ OTHER
ACCEPTABLE
❑ PREFERRED
❑ NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield or splash proof IHAND OTECTION Impermeable Gloves
PROTECTION onQQles
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or rubber apron.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING & STORING
Protect containers from extreme temperature —co iions
OTHER PRECAUTIONS
Handle with care. Avoid e3re and skin contact,
ANDERSON CHEMICAL COMPANY, INC. D.H. Patterson, Ph.D.
Post Office Box 4507 O Macon, Georgia 31213
. ". "1 .11 r%, I I A DOCDARGn RV

�+ 'MATERIAL
SAFETY
DATA
SHEET
SUPERIOR WATER TREATING SERVICE
HAZARD RAZING
4 = SEVERE
3 = SERIOUS
2 = MODERATE
1 = SLIGHT
0 = MINIMAL
DATE: 3-28-89 REVISION: 7-24-92 ISSUE DATE: 7-29-92 CHEMTREC PHONE NUMBER: [phone]
TRADE NAME: ANCOCIDE 4050
CHEMICAL NAME: Aqueous Solution: 2,2-Dibromo-3-Nitrilopropionamide
FORMULA: C4H4Br2NO
CHEMICAL FAMILY: Biocide
2,2-Dibromo-3-Nitrilopropionamide
010222-01-2
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
TLV = 2 mg/m3
LD50 = 800 mg/kg (rat)
BOILING POINT (F-) @ 760 mm Hg 212 SPECIFIC GRAVITY (H20 = 1). 1.14-1.17
VAPOR PRESSURE (mm Hg @ 20'C) Like Water PERCENT VOLATILE BY VOLUME (%) Like Water
VAPOR DENSITY (AIR = 1) Like Water EVAPORATION RATE ( = 1) Like Water
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE Pale yellow liquid ODOR Mildly aromatic
FLASH POINT None FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
AUTOIGNITION LOWER NA
TEMP. Nonflammable
EXTINGUISHING X WATER FOG X FOAM X CO2 X DRY CHEMICAL OTHER
MEDIUM
SPECIAL FIRE FIGHTING Wear full protective clothing and use self contained breathing apparatus. Use water spray to cool fire
PROCEDURES exposed containers.
UNUSUAL FIRE AND EXPLOSION During a fire, irritation and/or toxic gases and aerosols from the decomposition/combustion products may be
HAZARDS present.
STABILITY STABLE X CONDITIONS
TO AVOID: NA
UNSTABLE
CHEMICAL Avoid strong alkalis (caustic soda, etc.)
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of carbon and nitrogen (NOX), hydrogen bromide, bromine (Br2) and
DECOMPOSITION PRODUCTS cyanogen bromide may be evolved.
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION TO AVOID: NA
DOES NOT OCCUR X
(CONTINUED ON REVERSE SIDE)

PAGR 2
.. ... .. ....... .r. r....................... r..........................:i:: v:. �: /^Y��ry•/��t pr.... .. .. �• v. ':. v w::.w:::::::: x::: x::::::. �:::::: v; ......,� ..... �.v:.v: r.� ... :.; 4•'•ii:}
$:'... .
{�
3 .
:•.4vii
THRESHOLD LIMIT VALUE No TLV established.
EFFECTS OF OVEREXPOSURE:
KXE CONTACT I May cause severe irritation.
SKIN CONTACT I May cause severe irritation.
INHALATION I May cause severe irritation to the mucous membranes.
INGESTION I May cause severe irritation to the mucous membranes and stomach.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT Immediately flush eyes with large amounts of water for at least 15 minutes. Washing eyes within one minute is essential to achieve
maximum effectiveness. Seek medical attention immediately.
SKIN CONTACT Flush contacted area with water.
INHALATION Remove subject to fresh air.
INGESTION Drink a large amount of water. If discomfort persists, seek medical attention.
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
SPILLED
WASTE DISPOSAL
METHOD .
Dilute with water and flush to waste with excess water.
Dispose of in accordance with local, state and federal regulations for liquid and solid wastes.
VENTILATION _ LOCAL EXHAUST X ACCEPTABLE
REQUIREMENTS X MECHANICAL (GENERAL) —PREFERRED
OTHER NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield and splash HAND
PROTECTION proof goggles PROTECTION Impermeable gloves
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions. Do not transfer to
aluminum or galvanized containers.
OTHER PRECAUTIONS: Handle with care. Avoid eye and skin contact.
ANDER.SON CHFMICAL COMPANY, INC.
POST' OPPICH BOX 450r4 MACON. GA. 31213
MACON MI>MPHIS DAILIS
(912)7454W (901)M4i51 (214)6381526
Kiran B. Jain, Ph.D
PREPARED BY
ANCO DOCUMINI' NUMBtR AC405OLMSD

i � l
WWJANCO
QUALITY SERVICE
February 1, 1995
Mr. E.T. Haynes, Corp. Eng.
Dominion Yarn Corporation
P.O. Box 8105
Landis, NC 28088/8105
Dear Mr. Haynes:
It is with pleasure that I enclose the following information regarding our water treatment
program that we have recommended to replace the existing products at Linn Plant.
You currently use the following products:
1. HYDROFENE II
2. LESTER L-1
3. MICROBIOCIDE 76
4. MICROBIOCIDE 80
5. WATERENE 560 POSITIVE
Corrosion and scale inhibitor
Less than 9% solution of Hydrogen peroxide
1.5% isothiazolones
Sodium dichloro-s-triazine trione
Antistat
We would use the equivalent products as follows:
1. ANCOOL 3113 Corrosion and scale inhibitor
2. ANCOCIDE 4070 1.5% isothiazolones
3. ANCOCIDE 4230 Sodium dichloro-s-triazine trione
4. ANCOSPERSE 3810 A low foaming Anionic Surfactant
5. D-O-Stat Antistat
ANCOOL 3113: All organic based, multi -metal corrosion inhibitor and deposit control
product. Formulated for waters which tend to be more corrosive and less scaling contains
metal cleanse for improved corrosion inhibition.
Components: organophosphonate, synthetic polymer blend, tolyltriazole (yellow metal
corrosion inhibitor), organic corrosion (inhibitor for ferrous metals) and metal cleanse II
(Dihydroxy Alcohol).
Anderson Chemical Co., Inc. P.O. Box 4507 Macon, Georgia 31213 Phone (912] 745-0466 Fax [phone] ANCO U.S. Corporate Headquarters
Other locations: Australasia ■ Canada 0 Caribbean ■ Central America 0 Korea ■ Mexico ■ South America

Page 2
Dominion Yarn
Landis, NC
ANCOCIDE 4070: Is 1.5% active isothiazolones based biocide. This is very effective non -
oxidizing biocide which works well to control slime, fungi and algae.
Component: 1.5% Isothiazolones.
ANCOCIDE 4230: Is a dry, granulated, chlorine release product. ANCOCIDE 4230 is
highly effective oxidizing biocide which releases the active toxicant, hypochlorous acid, the
same active toxicant as generated with chlorine gas. However, ANCOCIDE 4230 being a
dry product, precludes the significant safety hazard associated with gaseous chlorine.
Components: Sodium dichloro-s-triazine-trione
ANCOSPERSE 3810: Is a specially formulated low foaming anionic surfactant designed to
disperse airborne debris, oil and sludge in cooling water systems and air washers.
ANCOSPERSE 3810 is low foaming, biodegradable modified ethoxylate based product.
Components: Ethoxylated surfactants, sodium hydroxide.
D-O-Stat: Is a quaternary ammonium compound. The cationic nature of this product
makes it the most highly surface active to control static charges in air.
Component: Quaternary ammonium compound
All these products that we have recommended are equivalent to the existing Lester's
products. We realize that you have a current NPDES permit to allow you to discharge the
overflow and bleed for your air washers and cooling towers into the storm drains.
Therefore we are duplicating the current program already approved. I also understand that
the holding time for biocide at Linn Plant is 2 days. Our biocide program will meet this
requirement.
Should you have any questions or require any additional information after reviewing the
contents of this letter, please do not hesitate to contact us. We thank you for your time
and consideration.
Kind regards,
1 YGYI • Q • ^d`�
Kiran B. Jam,
R & D Manager
J

MATERIAL
SAFETY
DATA
SHEET
ANCO
SUPERIOR WATER TREATING SERVICE
HAZARD RATING
4 = SEVERE
3 = SERIOUS
2 = MODERATE
1 = SLIGHT
0 = MINIMAL.
DATF.-- 1/20/90 REVISION: 624/92 ISSUE DATE: 8/3/92 CHEMTREC PHONE NUMBER: [phone]
TRADE NAME: ANCOOL 3113
CHEMICAL NAME: Aqueous Solution: Organophosphonates; Triazole; Synthetic Polymers
FORMULA: Proprietary Formulation
CHFMICAT. FAMILY: Scale and Corrosion Inhibitor
MATERIAL CAS# HAZARD DATA
Sodium Hydroxide 1310732 TLV = 2 mg/m3 (ceiling limit)
LD50 = 240 mg/kg (rat)
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
:.vw.:n.:.::...v i. n................ f..:................................ n:::: �:v :::•.:v •v{?v; �µ ...v v::::.:.v:•..w:{}i}::{{{•:.,.�.}:
.. n.................{{................. r............ .... }:.....x :. � �..... y :.}:• w::::.v::•:::.v:::: v.:v:::•v::qv:::•.:''fh:•}:4:}:•}:•}:•}:v;.}}};!.y;.}}}::•;�•w::::.}}:4i}}}•..:.......
........ .. .. ... ..n.:::::::: x:: ^:::: ?vw.w;r:r :}:; :; !: ::yy�;y�y••:::.yy�: ,. :} i '#. �i:j}:?i{�i:�ii'i�iiii<:iii:�:?•}}i}i}r:fi:•}::•: �}:ti:}}{:•%?::tii:: �iii:•..r..
�: nw.v:::::.v:.v::...,. n.. rnx .................v....:... .............................{ Vii�. ....
BOILING POINT ff) @ 760 mm Hg 212 SPECIFIC GRAVITY (1420 = 1). 1.04-1.06
VAPOR PRESSURE (mm Hg @ 20'C) Like Water PERCENT VOLATILE BY VOLUME (%) Like Water
VAPOR DENSITY (AIR = 1) Like Water EVAPORATION RATE ( = 1) Like Water
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE Clear Brown Liquid. ODOR Slight Aromatic.
FLASH POINT None
AUTOIGNITION
TEMP. Nonflammable
EXTINGUISHING
MEDIUM
SPECIAL FIRE FIGHTING
PROCEDURES
UNUSUAL FIRE AND EXPLOSION
HAZARDS
STABILITY
FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
LOWER NA
_ WATER FOG _ FOAM _ CO2 _ DRY CHEMICAL _ OTHER NA
Wear full protective clothing and use self contained breathing apparatus.
None
STABLE X CONDITIONS
TO AVOID: NA
UNSTABLE
CHEMICAL None
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of nitrogen (NOX) and carbon.
DECOMPOSITION PRODUCTS
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION TO AVOID: NA
DOES NOT OCCUR X
(CONTINUED ON REVERSE SIDE)

THRESHOLD LIMIT VALUE No TLV established.
EFFECTS OF OVEREXPOSURE:
EYE CONTACT May cause severe irritation.
SKIN CONTACT I May cause severe irritation.
INHALATION
INGESTION
May cause severe irritation to the mucous membranes.
May cause severe irritation to the mucous membranes and stomach.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT Immediately flush eyes with large amounts of water for at least 15 minutes. Washing eyes within one minute is essential to achieve
maximum effectiveness. Seek medical attention immediately.
SKIN CONTACT Flush contacted area with water.
INHALATION Remove subject to fresh air.
INGESTION Drink a large amount of water. If discomfort persists, seek medical attention.
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
SPILLED
WASTE DISPOSAL
METHOD
Dilute with water and flush to waste with excess water.
Dispose of in accordance with local, state and federal regulations for liquid and solid wastes.
VENTILATION LOCAL EXHAUST X ACCEPTABLE
REQUIREMENTS X MECHANICAL (GENERAL) PREFERRED
OTHER NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield and splash HAND
PROTECTION proof goggles. PROTECTION Impermeable Gloves.
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions. Do not transfer to
aluminum or galvanized containers.
OTHER PRECAUTIONS: Handle with care. Avoid eye and skin contact.
Kiran B. Jain, Ph.D.
PREPARED BY
ANDEPSON Q LENW-AL COMPANY, INC
P06T OFFKM BOX *a. MACOK GA. 31M
MAODN NCUAPM DAIlA.S
(912)7450466 (901)9S6 OtS1 (Z14)63&15Z6
ANCO DOCUMIM NUNMEP- AC3113��

MATERIAL
1� SAFETY
DATA
SHEET
SUPERIOR WATER TREATING SERVICE
I4AZARD RATING
4 = SEVERE-
3 = SERIOUS
2 = MODERATE
1 = SLIGHT
0 = MINIMAL
DATE: 3-30-89 REVISION: 2-24-92 ISSUE DATE: 7-29-92 CHEMTREC PHONE NUMBER: [phone]
TRADE NAME:
ANCOCIDE 4070
CHEMICAL NAME:
Aqueous Solution: 5-chloro-2-methyl4-isothiazolin-3-one;2-methyl-4-isothiazolin-3-one
FORMULA:
C4H4C1NOS; C4H5NOS
CHEMICAL. FAMILY:
Biocide
s« :>: ;:
`:; <<:
z>:``
::::: cv<::::
................................................................................................................................
MATERIAL CAS# HAZARD DATA
5-chloro-2-methyl-4-isothiazolin-3-one 26172-55-4 TLV = 0.1 mg/m3
2-methyl4-isothiazolin-3-one 2682-204 TLV = 0.1 mg/m3
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
BOILING POINT (-F) @ 760 mm Hg 212 SPECIFIC GRAVITY (HZO = 1). 1.02-1.04
VAPOR PRESSURE (mm Hg @ 20'C) Like Water PERCENT VOLATILE BY VOLUME (%). Like Water
VAPOR DENSITY (AIR = 1) Like Water EVAPORATION RATE �_ = 1) Like Water
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE Pale Green Liquid ODOR Mildly aromatic
FLASH POINT None FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
AUTOIGNITION LOWER NA
TEMP. Nonflammable
EXTINGUISHING _ WATER FOG —FOAM _CO2 DRY CHEMICAL —OTHER NA
MEDIUM
SPECIAL FIRE FIGHTING Wear full protective clothing and use a self contained breathing apparatus. Use water spray to cool fire
PROCEDURES exposed containers.
UNUSUAL. FIRE AND EXPLOSION During a fire, irritating and/or toxic gases and aerosols from the decomposition/combustion products may be
HAZARDS present. Do not allow solution to evaporate to dryness; dry nitrates in combination with organic material
can be explosive.
STABILITY
STABLE X CONDITIONS
UNSTABLE TO AVOID: NA
CHEMICAL. None
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of carbon, sulfur, nitrogen and hydrogen chloride gas.
DECOMPOSITION PRODUCTS
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION 11 TO AVOID: NA
•llOES NOT OCCUR X
(CONTINUED ON REVERSE SIDE)

PAGE 2
THRESHOLD LIMIT VALUE No TLV established - LD50 = 457 mg/kg (rat)
EFFECTS OF OVEREXPOSURE:
EYE CONTACT
May cause severe irritation and corneal injury. ,
SKIN CONTACT
May cause severe irritation. Material is a skin sensitizer even at low concentrations in susceptible individuals.
INHALATION
May cause irritation of the mucous membranes of the nose and throat.
INGESTION
May cause irritation and/or burns of the mucous membranes.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT I Immediately flush eyes with large amounts of water for at least 15 minutes. Washing eves within one minute is essential to achieve
maximum effectiveness. Seek medical attention immediately.
SKIN CONTACT I Immediately flush contacted area with large amounts of water. Remove contaminated clothing and wash before reuse.
INHALATION I Remove subject to fresh air. If breathing becomes difficult, administer oxygen and seek medical attention.
INGESTION I Do not induce vomiting. Give large quantities of milk, egg white or gelatin solution. If unavailable, give large quantity of water.
Avoid alcohol. Seek medical attention immediately.
STEPS TO BE
Contain spill. Deactivate spilled material with decontamination solution (13% calcium hypochlorite (HTH: 65% active), 10%
TAKEN IN CASE
sodium hydroxide (50%) R 77% water). Collect decontaminated material with an inert absorbent such as sand, sawdust or
MATERIAL IS
vermiculite. Scoop up and place in an appropriately markedcontainer for proper disposal. Keep spill out of municipal sewers
RELEASED OR
and open bodies of water. Wear recommended protective clothing and equipment.
SPILLED
WASTE DISPOSAL
Liquid should be considered for reuse. Absorbed material should stand for 48 hours in vented containers to avoid pressure
METHOD
buildup. It may be disposed of in a secured landfill in accordance with local, state and federal regulations.
VENTILATION
REQUIREMENTS
RESPIRATORY (SPECIFY TYPE)
PROTECTION
EYE Face shield or splash
PROTECTION proof goggles
OTHER PROTECTIVE CLOTHING
AND EQUIPMENT
LOCAL EXHAUST X ACCEPTABLE
X MECHANICAL (GENERAL) —PREFERRED
OTHER NA
Not required under normal handling conditions. Wear MSHA/NIOSH approved respirator if aerosol or
mist is encountered.
HAND
PROTECTION Impermeable gloves
Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions.
OTHER PRECAUTIONS: Material is a strong irritant to skin and eyes. Avoid bodily contact. Workers should wash after each use and shower at end
of work period. Material may be a skin sensitizer in susceptible individuals.
Kiran B. Jain, Ph.D
PREPARED BY
ANDERSON CIMMICAL COMPANY, INC.
POST OFFICE BOX 4507, MACON, GA. 31213
MACON MF1"HI3 DALLAS
(912)745-0,W (901)9188t51 (214)6481526
ANCO DOCUAII'Xr NTJMBM- AC4MMSD

MATERIAL.
SAFETY
DATA
SHEET
ANCO
SUPERIOR WATER TREATING SERVICE
HAZARD RATING
4 = SEVERE
3 = SERIOUS
2 = MODERATE
1 = SLIGH'I'
0 = MINIMAL
DATE: 3-28789 REVISION: 5-29-92 ISSUE DATE: 8-5-92 CHEMTREC PHONE NUMBER: [phone]
TRADE NAME:
ANCOCIDE 4230
CHEMICAL NAME:
Sodium Dichloro-s-triazine trione
FORMULA:
C3N303CI,Na
CHEMICAL FAMILY:
Biocide Oxidizin;
'<�x `z's�'�''<t<:�:;<.::::biz::::?::�:::«::«::i�::z:;>:�:>�>:�>:'•:::>.:.`.%::.?::
MATERIAL CAS# HAZARD DATA
Sodium Dichloro-s-triazinetrione 2893-78-9 No TLV Established
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
BOILING POINT ('F) @ 760 mm H. NA SPECIFIC GRAVITY (H2O = 1). NA
VAPOR PRESSURE (mm Hg @ 20'C) NA PERCENT VOLATILE BY VOLUME (%) NA
VAPOR DENSITY (AIR = 1) NA EVAPORATION RATE ( = 1) NA
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE White, Crystalline Solid ODOR Faint Halogen
FLASH POINT NA
AUTOIGNITION
TEMP. NA
EXTINGUISHING
MEDIUM
SPECIAL FIRE FIGHTING
PROCEDURES
UNUSUAL FIRE AND EXPLOSION
HAZARDS
FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
LOWER NA
X WATER FOG —FOAM _ CO, _ DRY CHEMICAL —OTHER
If fires fueled by other materials, may release hydrogen chloride, chlorine or phosgene. Wear self contained
breathing apparatus. Ammonium phosphate fire extinguishers should not be used.
None
STABILITY STABLE X CONDITIONS Do not mix anything other
TO AVOID: than water.
UNSTABLE
CHEMICAL Organics and any other readily oxidizable materials: reducing agents.
INCOMPATIBILITY
HAZARDOUS Hydrogen chloride, chlorine, phosgene: oxides of carbon and nitrogen.
DECOMPOSITION PRODUCTS
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION j TO AVOID: None
DOES NOT OCCUR X
(CON-17Nl1I11) ON REVERSE SIDI;

PAGE 2
THRESHOLD LIMIT VALUE No TLV Established
EFFECTS OF OVEREXPOSURE:
EYE CONTACT Corrosive to eye tissues. May result in permanent eye injury.
SKIN CONTACT Corrosive to skin tissues. May cause severe skin irritation.
INHALATION Can cause mild irritation of the mucous membranes to severe pneumonitis depending on severity of exposure.
INGESTION May cause gastrointestinal irritation or ulceration and burns to the mouth and throat.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT Immediately flush eves with large amounts of water for at least 15 minutes. Washing eyes within one minute is essential to achieve
maximum effectiveness. Seek medical attention immediately.
SKIN CONTACT' Immediatelv flush contact area with large amounts of water. Remove contaminated clothing and wash before reuse.
INHALATION Remove subject to fresh air. Seek medical attention.
INGESTION Do not induce vomiting. Feed bread soaked in milk, followed by olive oil or cooling oil. Seek medical attention.
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
SPILLED
WASTE DISPOSAL
METHOD
Sweep up spilled material and place in a clean, suitable containers. Avoid contact with skin, eyes or clothing. Avoid inhalation of
dusts. Wash area of spill with large amounts of water.
Dispose of in accordance with local, state and federal regulations for liquid and solid wastes. RCRA hazardous waste - Type
D001 and D003.
VENTILATION X LOCAL EXHAUST _ ACCEPTABLE
REQUIREMENTS _ MECHANICAL (GENERAL) X PREFERRED
OTHER NA
RESPIRATORY (SPECIFY TYPE) If product is used in a poorly ventilated area or dusting occurs, use a NIOSH approved dust mask.
PROTECTION
EYE Face shield and splash HAND
PROTECTION proof goggles. PROTECTION Impermeable gloves
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions. Keep containers sealed
when not in use. Keep away from other chemicals.
OTHER PRECAUTIONS: Handle with great care. Avoid eye and skin contact. Avoid breathing dust. Wash after each use and shower at the end of
the work period.
Kiran B. Jain. Ph.D
PREPARED BY
ANDTRSON CtiGBCAL COMPANY, INC
POST OFFICE BOX 4567. MACON, GA. 31213
MACON MEMPHIS DAlltiS
(912)745- 1 (901)919-061 (214)639-1s26
ANCO DOCUMINr N1IMBFR: AC42XMSD

MATERIAL
SAFETY
DATA
SHEET
ANCO
SUPERIOR WATE11717REATING SERVICE
HAZARD RAPING
4 = SEVERE
3 = SERIOUS
2 = MODERATE
1 = SLIGHT
0 = MINIMAL
DATE: 03/30/89 REVISION: 08/18/92 ISSUE DATE: 08/18/92 CHFm nzFC PI iONF N1 rn nETP- iFame��mm
TRADE NAME:
CHEMICAL NAME:
FORMULA:
CHEMICAL FAMILY
::::::.:.............. Del .:.. .:. .. ....:........::...........................:.....:.::::::::.::.:;.:::::;.................:..:.
ANCOSPERSE 3810
Aqueous Solution: Modified Ethoaylate
Proprietary Formulation -
Surfactant
:i:?:}:i::ii::!:iiiiiii:?:ijiiiij:v}:ij:>i:;;yjii?<:i:!:i:ii{i{:}'::i:::'sy:Si::F:' yjji::::':':}{ � i'.+;:;:;:<?iyj}jf•S:si:isi:;:j:;:i;}:iii:::':::::ji:S:<:;:Si>yi:?:i:%: iii:v''ri'::%:i'i:}i: � is:;:;:;:;isi}':isi}:i'>.:':':iiiii:?:::i�4ii}'+iiiiii::':::i::isi:`ii'.=ii::'i:i................:...:::::
............ �.. �� is :i: .: NMI
MATERIAL CAS# HAZARD DATA
60dmm hydroxide 1310732 TLV = 2 mg/m3 (ceiling limit)
LD50 = 240 mg/k- (rat)
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
BOILING POINT ('F) @ 760 mm Hg 214 SPECIFIC GRAVITY (H2O = 1). 1.04 - 1.06
VAPOR PRESSURE (mm Ha @ 20'C) NA PERCENT VOLATILE BY VOLUME (%) NA
VAPOR DENSITY (AIR = 1) NA EVAPORATION RATE ( = 1) NA
SOLUBILITY IN WATER NEGLIGIBLE SLIGHT MODERATE APPRECIABLE X COMPLETE
APPEARANCE Light Yellow Liquid ODOR Mild
FLASH POINT None FLAMMABLE LIMITS UPPER NA
AIR (% by Volume)
AUTOIGNITION IOWIIt NA '^
TEMP. Nonflammable
EXTINGUISHING _ WATER FOG —FOAM CO, —DRYCHEMICAL EMICAI" OTHER NA
MEDIUM — -
SPECIAL FIRE FIGHTING Wear full protective clothing and use self contained breathing apparatus.
PROCEDURES
UNUSUAL FIRE AND EXPLOSION None
HAZARDS
STABILITY STABLE X CONDITIONS
1'0 AVOID: NA
UNSTABLE
CHEMICAL Strong oxidizing or reducing compounds, aluminum, zinc or magnesium.
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of carbon.
DECOMPOSITION PRODUCTS
HAZARDOUS MAY OCCUR CONDITIONS
POLYMERIZATION TO AVOID: NA
DOES NOT OCCUR X
(CONTINUED ON RI VISRSIi SII)I;)

' PAGE 2
THRESHOLD LIMIT VALUE No TL.V established.
I?FFECTS OF OVEREXPOSURE:
I -YE CONTACT
May cause severe irritation.
SKIN CONTACT
May cause severe irritation.
INHALATION
May cause severe irritation to the mucous membranes.
INGESTION
May cause severe irritation to the mucous membranes and stomach.
EMERGENCY AND FIRST AID PROCEDURES:
I:Yfi CONTACT
Immediately flush eyes with large amounts of water for at least 15 minutes. Washing eyes within one minute is essential to achieve
maximum effectiveness. Seek medical attention immediately.
SKIN CONTACT
Flush contacted area with water.
INHALATION
Remove subject to fresh air.'
INGESTION
Drink a large amount of water. if discomfort persists, seek medical attention.
STEPS TO BE
TAKEN IN CASE
MATERIAL IS
RELEASED OR
SPILLED
WASTE DISPOSAL.
METHOD
Dilute with water and flush to waste with excess water.
Dispose of in accordance with local. state and federal regulations for liquid and solid wastes.
VENTILATION LOCAL EXHAUST X ACCEPTABLE
REQUIREMENTS X MECHANICAL (GENERAL) _ PREFERRED
OTHER NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield and splash proof HAND
PROTECTION goggles. PROTECTION Impermeable gloves.
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or apron. Emergency eyewash and shower in work area.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING AND STORING: Protect containers from extreme temperature conditions. Do not transfer to
aluminum or galvanized containers.
OTHER PRECAUTIONS: Handle with care. Avoid eye and skin contact.
ANDERSON CI 1EMICAL COMPANY. INC
POSE OFFICE BOX 4507, MACON, GA. 31213
MACON MEMPI11SS DAILIS
(912)745-N" (901)418"l [phone]
Kiran B. Jain, Ph.D.
PREPARED BY
ANCO DOCUMEN r NUMBER• AS381QMSD

Y HAZARD RATING 2
MATERIAL. 3: SERIOUS FLAMMABIUTY 0
SAFETY NCO
2= MODERATE 0
DATA SHEET 1=SLIGHT PERSONAL D
SUPERIOR WATER -TREATING SERVICE o=MINIMAL PROTECTION
DATE: 1/05/t
TRADE NAME:
CHEMICAL NAME:
FORMULA:
EMERGENCY PHONE NUMBER: [phone]
D-0 STAT
Aqueous Solution: n-Alkyldimethylbenzylammonium Chloride
(R)N(CH3)2(C7H7)+Cl-
MATERIAL CAS# HAZARD DATA
n-k1ky1dimethy1benzy1aumonium (blonde 139082 No TLV established
LDS0 = 550 mg/kg (rat)
THIS PRODUCT CONTAINS NO KNOWN OR SUSPECTED CARCINOGENS.
SECTION► DATA
BOILING POINT (°F) ® 760 mm Hg 212 SPECIFIC GRAVITY (H2O=1). 0.98-0.99
VAPOR PRESSURE (mm Hg ® 20°C) Like Water PERCENT VOLATILE BY VOLUME (%) Like Water
VAPOR DENSITY (AIR = 1) Like Water EVAPORATION RATE ( —1) Like Water
SOLUBILITY IN WATER ❑ NEGUGIBLE ❑ SLIGHT ❑ MODERATE ❑ APPRECIABLE jV COMPLETE
APPEARANCE Clear Colorless Liquid ODOR Slight .Almond
FLASH POINT None FLAMMABLE LIMITS UPPER NA
AIR (% by Volume) LOWER AUTOIGNITION TEMP. Nonflammable NA
EXTINGUISHING
UFmii i" I [M WATER FOG %] FOAM 10 CO, DRY CHEMICAL ❑ OTHER
SPECIAL
FIRE FIGHTING Wear full protective clothing and use self contained breathing apparatus.
PROCEDURES
UNUSUAL FIRE During a fire, irritating and/or toxic gases and aerosols from the
AND EXPLOSION decomposition/combustion products may be present.
HAZARDS
STABLE X CONDITIONS Under normal conditions, the material is
STABILITY TO AVOID: stable.
UNSTABLE
CHEMICAL Strong acids
INCOMPATIBILITY
HAZARDOUS Thermal decomposition may yield oxides of nitrogen (NOX) and
DECOMPOSITION PRODUCTS rnrhnn _ Ammnni n and 14C1 nac may nl .cn Avnl va _
HAZARDOUS
MAY OCCUR
CONDITIONS
POLYMERIZATION
TO AVOID: NA
DOES NOT OCCUR
X
1r%r%K1'r1k11 IC11 f%kl M011t! U%t7 C�Illl-%

+ 7 PAGE 2
THRESHOLD LIMIT VALUE No TLV established.
EFFECTS OF OVEREXPOSURE:
EYE CONTACT May cause irritation.
SKIN CONTACT May cause irritation.
INHALATION May cause irritation to the mucous membranes.
INGESTION May be harmful if swallowed. May cause irritation to the mucous
membranes and stomach.
EMERGENCY AND FIRST AID PROCEDURES:
EYE CONTACT Flush eyes with clean water for.15 minutes. If irritation persists,
seek medical attention.
SKIN CONTACT Flush contacted area with water.
INHALATION Remove subject to fresh air.
INGESTION Induce vomiting. Give large quantities of water. Seek.medical attention..
STEPS TO BE
TAKEN IN CASE
MATERIAL IS Dilute with water and flush to -waste with excess water.
RELEASED OR
SPILLED
WASTE DISPOSAL Dispose of in accordance with local, state and federal regulations for
METHOD liquid and solid wastes.
SECTIONPROTECTION INF• •
VENTILATION ❑ LOCAL EXHAUST W ACCEPTABLE
REQUIREMENTS ® MECHANICAL (GENERAL) ❑ PREFERRED
❑ OTHER ❑ NA
RESPIRATORY (SPECIFY TYPE) Not required under normal handling conditions.
PROTECTION
EYE Face shield or splash proof HAND Impermeable Gloves
PROTECTION goQQmles PROTECTION p
OTHER PROTECTIVE CLOTHING Impermeable boots and coveralls or rubber apron.
AND EQUIPMENT
PRECAUTIONS TO BE TAKEN IN HANDLING & STORING
Protect containers from extreme temperature conditions,
OTHER PRECAUTIONS
Handle with care Avoid eye and skin contact.
ANDERSON CHEMICAL COMPANY, INC.
Post Office Box 4507 0 Macon, Georgia 31213
D.H., Patterson, Ph.D.

C b N
DOMINION YARN
C O R P O R A T I O N
February 17, 1995
flNVIL.ONIV!ti•7:�', I%;'�y.I_?I �
& NATl1R _ , a� lSOUIRC
FEB2 1 1995
lbFliSl ESV:st1.? "'"it i,`,•� (�'��fi���v�y'
Mr. Keith Colson
N. C. Department of Environment, Health & Natural Resources
919 North Main Street
Post Office Box 950
Mooresville, North Carolina 28115
Dear Keith:
As we discussed on 1/30/95, we are changing water treatment
companies for our HVAC systems from Lester Labs to Anderson
Chemical Company. As you requested, I have attached our MSDS
Sheets for the new water treatment we will be using. Also
attached is a comparison with the new water treatment with the
old water treatment.
I am requesting that these changes be made on NPDES Permit
#NC0080039, Linn Plant, Rowan County, and NPDES #NCG500000,
Corriher Plant, Rowan County.
If you should need further information, please give me a
call.
Sincerely,
DOMINI N YARN CORPORATION
E. T. Haynes
Corporate Engineer
ETH/bfw
Attachments
c: Bill Crocker
Allen O'Shields
Mike Overcash
Joe Purvis
Dan Wiggers
P.O. BOX 8105 / LANDIS, NORTH CAROLINA 28088-8105 / 704/857-1121 / FAX [phone]
Member of ft DOMINION TEXTILE

V'
DOMINION YARN
C O R P O R A T 1 O N
May 8, 1995
Mr. Kim H. Colson, P.E.
State of North Carolina
Department of Environment
Health and Natural Resources
919 North Main Street
P. O. Box 950
Mooresville, NC 28115
Dear Mr. Colson:
N.C. DEFT. OF
ENVIROI�iP:E^ 'i ,& NATURAL
DIVISIm
maRoVIUbE 1S�Wt iVtL 4J:1�:.tu
Attached are the biocide.worksheets 101 that you requested for
Dominion Yarn Linn Plan PDES 'Permit-NC;QO.800'39�'1 and Corriher
Plant NPDES NC0080021.
Please note that sheet number 4 is not filled out because the
biocide that we are using does not contain metal. (See
Attachments)
ETH/bfw
Attachments
c: Allen O'Shields
Dan Wiggers
Joe Purvis
Bill Crocker
Mike Overcash
Sincerely,
DOMTT.Hay
N YARN CORPORATION
E. es
Corporate Engineer
- VP Manufacturing
- Plant Manager
- Plant Engineer
- Plant Manager
- Plant Engineer
P.O. BOX 8105 / LANDIS, NORTH CAROLINA 28088-8105 / 704/857-1121 / FAX [phone]
Member of W DOMINION TEXTILE

04i 27! 15 15: 5'7 $912 741 8812 ANDERSON CHEH CO U 002
QUALITY SERVICE
April 26, 1995
Mr. E.T. Haynes
Dominion Warns, Inc,
P.O. Boa 8105
Landis, NC. 28088-8105
Dear Mr. Haynes:
This letter is to certify that our biocide product, ANCOCIDE 4050, does not contain any
metal compounds,
If you have any further requests, please feel free to call on us.
Sincerely,
ANDERSON CHEMICAL COMPANY, INC.
Steven R. Fennell
Laboratory Supervisor
ash 192
Ar&rson Chemical Ca, Inc. P.G. Bax 4507 Macon, Georgia 31213 Phpite (3121745-0466 FOX (9121742-5332 ANCO LI.5. Corporate Headquarters
Other lacs ors: Australasia ■ Camd2 ■ C.Tibbean 0 Central America ■ Korea 0 Mexico ■ South Arrfica

04/18/95 14:15
'0012 741 8812 ANDERSON CHER CO
is 002
SIOCI DE/CHEMICAL TREATMENT
WORKSHEET-FORM 101
The following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
North Carolina. This worKsheet must be oomplptad separately for each biocidal product in use- -MS Wo%heet i9 to be
returned with all appropriate data entered into the designated a•ea9 with calculations performed as indicated.
Dominion Yarn corp/corriher Plant
{. Facility Name
NPDES#NC 0080021
county Rove 7010 0 (CIS)
Receiving Stream UT Coidwate r Cr��
(All abova Information sUppiied by the DlvisiOn Of Environmental Management)
What is -the Average Bally Discharge (A•D•O-) volume of the water handling systems t0 the receiving water body?
A.D.D. 0.0275 (in M.G.D•)
Please valoulat® the lnstream WaSts Concentration (IVIC in percent) of this discharge using the data entered.
I.
above.
(A-D.D.) x 100Li.�. i o )(Q.646) 1D0
NVC ( gj0X x O.6 + (A. �. 027.5)'
100
This value (IWC) represents the waste concentration :o the-irecaiving stream during low flow Conditions.
p• what is the name Of the whole product crsemical treat-nent prvposgd far use in the discharge identified in Part I7
please list the active ingredients and percent compositic;n'
5 : t] qo
OilaR11 G' �_°r/v
�a
0I
/O
(Q
.ram
�•7?,i S
Note-, if ingrediants contain the metals copper, chromium, or zinc, also oompleto pogo A.
What feed or dosage rate (D-R.) is used in this application? The units must be converted to grams of whole
p:oduot used per day -
a grarns/day
D.S.M. Form 101 (7192) 1

t.04/18/95 14:16 C912 T41 8812 ANDERSON CHEN CO 003
Facility Name:
DOMmi : on Yarn Cor Corr ' rx DES M NC 0 0 8 0 0 21
Estimate total volume of the water handling System between entry of blocldal product and 14PD59 discharge
point. On an attached Sheet please provide jusiitication for this estimate (system volume, averac_ cycles per
,)lowdown, holding lagoon size, etC.)
Volume= 0.0Ar, million gallons
What is the pH of the handling system prior to biocide addition? If unknown, enter NIA. -
What is the decay rate (D.K.) of M product? if unknown, assume no decay (O.K-=0) and proceed to asterisk.
The, degradation must be stated at pH level within 112 pH standard unit Within handling system. Enter the hall
file (Hall Lice is the time required for the initial product to degrade to half of its original concentration). Please
provide copies of the sources of this data.
14-L - Days
1 X i7.69 34.5 -Decay mate AM
decal► rate is equal to NL
Calculate degradation factor (l _1q. This is the first order toes CO2ificlent.
A.D.D. j- (DA-) _ —�' Q� %� + 34.5 ) = 35.1.
D.F. (volume) �( 0.045
Calculate Steady State Discharge Concentration' 34 p _ 0.57 mgrl
dwohg +;Ora. = (DX )(Volume)(3755) ( 35. I ) ( 0.045
) ( 7 s s )
Calculate concentration Of biorlde 1nsVsam during low flow conditions-
(Feceiving Stream Concentration)
I ott . conc.)x IWG°/a _ 4.21 x 1 = 0.57 moll
100 100
Receiving Strew Concentration
Ill. Calculate regulated tirnitatian.
whale product according to the following ccxiurnns_ (Note that units should be
List all LCStJ data available for the
in mgll). please provide copies of the sources of this data. LC51 (�)
C� %st f3uraiior►
Bluegill Sunfish-
1_0
17
Fathead x1nnoW
48-hours 1-24
Largemouth BSSs fin erlin 4 hr,1Ya,^B -G
'a-ct.ive ingredient data
D-E.M. Form 101 (7192) Z

04/18/95 14:16 %2912 T41 8812 ANDERSON CHEN CO
121 004
1. Fdc�ii;y Name: D
omininion Yarn Corp/Corriher P1RPbE,q#: NC 0080021
* Rainbow trout LC-50 = 1.0 Mg/L
Choose the lowest LC50 listed above: Active Ingredient = 5%
;enter the L050: 20* whole Praduet IC ' 50 = 1�0 _ 20
it the haft life (M.t._) is less than 4 days, perform the ;allowing calcuiaiicn. .05
Regulated Limitation = 0.05 x LC50 = 1 mg/t
It Me nag life (H.L.) is greaterthan 4days or unknown. perform the toilowing calculation.
Regulated Limitation = 0.01 x L050 = mg/l
Choose the apprppriate regulated limitation from the calculations Immediately above and place in this blank:
1.0 rngtliter
t"rom Part it enter the receiving stream concentration:
0.57 rngltiter
IV. An2lysis.
it the receiving stream Concentration is greater than the caleulatad regulated limitation, then this biocide is
unacceptabla for uSe.
Name (P(rn)
Person in Responsible Charge
I
DX_M, Form 101 (7192) 3

NPDES #: NC
Facility Name:
Sugalemental Metals Analysis
It copper, zinc, or chromium are present in the proposed biocidal compound, complete this worksheet. A
separate form must be used for each metal and/or metal compound present in the biocide. List the metal,
its chemical formula, molecular weight (MW), formula weight (FW), and the concentration of the metal
compound in the biocide (MCC). Complete a separate form for every metal present in the biocide.
Metal Chemical Formula Molecular Weight of Metal Formula Weight Concentration in Biocide
EXAMPLE
63.546 g/mole 249.680 g/mole. 0.2 °�
Copper CuSO4 5l-12O
Dosage rate of Biocide (DR) (from page 1):
DR = grams/day
Average Daily Discharge (ADD) (from page-1):
ADD = million gallons/day
Discharge Concentration (DC) of Blocide:
DR ( grams/day) = grams/million gallons
DC = ADD = ( million gallons/day)
Convert DC to micro gram siliter (ppb):
1 x 106 u9/9 = ug/I
DC (µg/I) = DC (grams/million gal) x 3.785 x 106 liters/million gal.
Calculate the fraction of metal in the metal -containing compound (MF):
grams/mole) _
MF = _ grams/mole)
FW
Calculate the fraction of metal In the biocidal compound (BF):
MCC% %_
BF = MF x 1 0 1= X (100)
Calculate the concentration of metal in -thee discharge:: (M):
M = DC BF = ug/l x
Calculate the Instream metal concentration (IMC) at low -flow conditions:
IWC%)
IMC = M x 1100 _ u9/1 x 100
Regulated limitation of metal (from below):
ug/l.
-- ,^An9PM9i1 e ine:
rr� l7Hllulal .-... ---
copper- 7 µg/I water quality action levbl' Zinc- 50 µg/l -water quality action lave
Chromium- 50 µg/l water quality standard
(*Values which exceed action levels must be addressed directly by aquatic to testing.)
a
D.E.M. Form 101 (7/92) 4

04/27/95 15:57 V912 741 8812
ANDERSON CHEM CO U 002
WV,s�r0�
QUALITY SBRViCE
April 26, 1995
Mr. E.T. Haynes
Dominion Yarns, Inc.
P.O. Box 81.05
Landis, NC 28088-8105
Dear Mr. Haynes:
This letter is to certify that our biocide product, ANC OCIDE 4050, does not r_ozltain any
metal compounds.
If you have any further requests, please feel free to call on us.
Sincerely,
ANDERSON CHEMICAL COMPANY, INC.
Steven R. Fennell
Laboratory Supervisor
nsJa[192
AndersonChemicel Co., Inc. P.O. Bax 4507 Macon. Georgia 31213 Phone )912) 745-0450 Fax [phone] ajCo u.8. Corporate Headquarters
Other bretiarw Australasia ■ Casada ■ Can'hhean ■ Central America ■ Kama ■ Mexico ■ South America
19

BIOCIDE/CHEMICAL TREATMENT
WORKSHEET-FORM 101
The following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
North Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
returned With all appropriate data entered into the designated areas with calculations performed as indicated.
Facility Name Dominion Yarn — Linn Plant
NP.DES#NC 0080039
County
Rowan
Receiving Stream UT Grant Creek
7Q10 0 (cfs)
(All above information supplied by the Division of Environmental Management)
What is -the Average Daily Discharge (A.D.D.) volume of the water handling systems to the receiving water body?
A.D.D. = 0.009 (in M.G.D.) (9000 gal/.day)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
(A.D.D.) x 100 _ (.009) X 100
IWC = (7Q10 x 0.646) + (A.D.D.) — ( 0 )(0.646) + (.009 )
This value (IWC) represents the waste concentration to the 'receiving stream during low flow conditions.
What is the name of the whole product chemical treatment proposed for use in the discharge identified in Part I?
Ancocide 4050
Please list the active ingredients and percent composition:
2,2 — Dibromo — 3 — nitrilopropionamide 5.0
Note: If ingredients contain the metals copper, chromium, or zinc, also complete page 4, Sul2plemental Metals Aialysis
What feed or dosage rate (D.R.) is used in this application? The units must be converted to grams of whole
product used per day.
D.R.= 4 , 6 0 0 grams/day
D.E.M. Form 101 (7/92) 1

Facility Name:
Dominion Linn Plant
NPDES #: NC 0080039
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for this estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.)
Volume= 0.035 million gallons (35,000 gallons)
What is the pH of the handling system prior to biocide addition? If unknown, enter N/A. 7.5 - 8-9
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk.
The degradation must be stated at pH level within 1/2 pH standard unit within handling system. Enter the half
life (Half Life is the time required for the initial product to degrade to half of its original concentration). Please
provide copies of the sources of this data.
H.L. = 0.02 Days
The decay rate is equal to H 1 L.
X 0.69 34.5 . =Decay Rate (D.K.)
Calculate degradation factor (D.F.). This is the first order loss coefficient.
049
Vo
D.F. _ (A.D.D.) + (D.K.) _ ( . 035 + (34.5 ) = 34. R
Calculate Steady State Discharge Concentration:
Dischg Conc. _ (D.R.) _ ( 4,600 ) - 0.99 mg/l
(D.F.)(Volume)(3785) { 34.8 ) ( . .035
) (3 7 8 5 )
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischg. Conc.) x (IWC%) _ l ) x l ) = mg/I
100 100
Receiving Stream Concentration
III. Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be
in mg/1). Please provide copies of the sources of this data.
Organism Test Duration LC50 (mgO)
Bluegill Sunfish 96- hr 1.3
Rainbow Trout 96- hr 1.0
Fathead Minnow 96- hr 1.36
Daphnids 96- hr 1.24
Large mouth Bass Fingerlings 96--hr 1.63
*Active Ingredient Data
*Rainbow trout LC50 = 1.0 mg/L
D.E.M. Form 101 (7/92) 2 Active Ingredient = 5 %

• Dominion Yarn Linn Plant NPDES #: NC 0080039
Facifity Name:
Choose the lowest LC50 listed above:
Enter the LC50: 20* Whole Product LC50 = 1.0 = 20
If the half life (H.L.) is less than 4 days, perform the following calculation. .05
Regulated Limitation = 0.05 x LC50 =
1.0 mg/I
If the half life (H.L.) is greater than 4 days or unknown, perform the following calculation.
Regulated Limitation = 0.01 x LC50 = mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
1.00 mg/liter
From Part II enter the receiving stream concentration:
0.99 mg/liter
IV. Analysis.
is greater than the calculated regulated limitation, then this biocide is
If the receiving stream concentration
unacceptable for use.
Name (Print)
S' re
Person in Responsible Charge
i
5
Date
D.E.M. Form 101 (7/92) 3

Facility Name: NPDES
Supplemental Metals Analysis
if copper, zinc, or chromium are present in the proposed biocidal compound, complete this worksheet. A
separate form must be used for each metal and/or metal compound present in the biocide. List the metal,
its chemical formula, molecular weight (MW), formula weight (FW), and the concentration of the metal
compound in the biocide (MCC). Complete a separate form for every metal present in the biocide.
Metal . Chemical Formula Molecular Weight of Metal Formula Weight
EXAMPLE
Copper CUSO45H2O 63.546 g/mole 249.680 g/mole
Dosage . rate of Biocide (DR) (from page 1):
DR = drams/day
Average Daily Discharge (ADD) (from page 1):
ADD = million gallons/day
Discharge Concentration (DC) of Biocide:
Concentration in•Biocide
0.2 %
DR ( drams/day) = grams/million gallons
DC = ADD = ( million gallons/day)
Convert DC to micrograms/liter (ppb):
1 x 106 u9/g __ ug/l
DC (µg/I) = DC (grams/million gal) x 3.785 x 106 liters/million gal.
Calculate the fraction of metal in the metal -containing compound (MF):
grams/mole) _
MF �
= F—VI/ _ grams/mole)
Calculate the fraction of metal In the biocidal compound (BF):
' MCC % %_
BF = MF x 100 = x (100)
Calculate the concentration of metal in the discharge (M):
M = DC x BF '= ug/I x
Calculate the instream metal concentration (IMC) at low -flow conditions:
IWC 0/0 = %
IMC = M x 100 ug/I x 100
Regulated limitation of metal (from below): ug/I
General tatutes 15 CAC 28.0211 cetine:
Copper- 7 µg/1 water quality action level' Zinc- 50 µg/l water quality action level'
Chromium- 50 µg/I water quality standard
(*Values which exceed action levels must be addressed directly by aquatic toxicfty testing.)
D.E.M. Form 101 (7/92) 4