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HomeMy WebLinkAboutWQ0005910_Monitoring - 11-2020_20201221GW-59A COMPLIANCE REPORT FORM Permit #-WQ 0005gtiQ (Submit one each tit oniloring period with GW-59 forms.) i Enter date monitoring results were due. (12-30-20) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? ,// 2 Was any required information missing on the GW-59 report forms? YES NO iF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. / 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)" If the answer is "Yes", cortlacl the Regional Once for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO if the answer to question 4 is 'NO", skip to section 8. if the answer to question 4 is "YES" list the affected wells individually with constituents) and concentrations) / exceeding standards in the space provided below: "t'okal O.wAVV\Q w - -Yvlw 100 5 For the constituents identified In question 4 abovq, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question '5 is NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each welt with constituents) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). `711���0— tt•32, z1��i�0- $12 -11ai110 — SSI-111311q,- toti 3130110 — G 1 `I 511\o Wt - tcLt$ 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days, • an evaluation may be required to determine the impact the waste disposal system Is having at the review and compliance boundaries surrounding this facility, Failure to do so maV subiect the permittee to a Notice of Violation, fines and/or penalties. r,r ry 8 The person completing this poi n (GW-59A) of the monitoring report should sign below and submit this y form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I'hereby1acknowledge.that the above lnfofmation was dVal'u�ated a"nd the Iriformatfbn �subm ttekd` n thyi�s, report (Compliaric e ort .. ,-59 Js true and complete to,the best of my Knowladget ;;�;, ,, i¢+. ••s.i M� Signature of PeWe ( Authorized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: N4,0cu LLC Permit Name (if different): Facility Address: F evv ",III (Sueel) 7-14S-7 County-- 1 (cuy) lsieie) (zip) p 2S2-4 t Person: hone #: �2-� 133 Contact Telephone Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): MW-S Well Depth: Zt-1 .—ft. Well Diameter: 2- in Screened Interval: IS ft. to 2.2 ft. Depth to Water Level: _�ft. below measuring point. Measuring Point (M.P.) is:ft. above land surface. Re Gallons of water pumped/bailed before sampling: 5_ Field analysis: pHL+--IL , Specific Conductance Temp. 23 5 °C, Odor W O one. Ap For Groundwater Treatment Systems Check 0ne: ❑ Influent (98) ❑ Effluent (99) lative M.P. Elevation in ft.: Date sample collected: %\-\\-?- uMhos pearance PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid samples) S(vs Dissolved Solids: Total mg/I pH (when analyzed) units TOC 3.05 mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia o-N mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-1636 Phone: (919) 733-32, PERMIT #: • EXPIRATION DATE: 10 31 20 Non Discharge " 000541 D UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: 11I ICI;p - 1� 1 I -�'0 Laboratory Name: Lnu iicOMCAA Certification No. V) v YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N <-0. mg/I sphorus: Total as P z- 0 - mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 3S S mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. ach lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method if = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Awo(u LLC_ Permit Name (if different): Facility Address: F f, VV !d'll (Streeq WC 2-14S-7 County 1 (Ciry) (Stale) (zip) Contact Person: +cif► Gow'cr Telephone #: 2S2 4�2-2133 Well Location/ Site Name: No. of Wells to be Sampled: (from Pe Wit) Well Identification Number (from Permit): MQ3- For Groundwater Treatment Systems Well Depth: � ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: 3 ft. to I P)_ ft. ❑ Effluent (99) Depth to Water Level: 4.7 ft. below measuring point. Measuring Point (M.P.) is: 2 ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: SJ Date sample collected: \\2( Field analysis: pHSpecific Conductance uMhos Temp. 9- 4 °C, Odor ate- Appearance (aecc.f DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-1636 Phone: (919) 733-32: PERMIT #: , EXPIRATION DATE: 10 -M 2 y Non -Discharge WQ 000591 O UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: — \,;" ) \ a� Laboratory Name: Env ►xc0nm Certification No. ko PARAMETERS (Samples for metals were collected unfiltered y_YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 Coliform: MF Total /100ml Phosphorus: Total as P O. 0 mg/I (Note: Use MPN method for highly turbid sa pies) Orthophosphate mg/I Dissolved Solids: Total 2. mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC LA. 0,5 mg/I Ca - Calcium 5.933 mg/I Chloride 1—I mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia O.O-1 mg/I Mg - Magnesium mg/I TKN as N mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. ach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = method ff = 01 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Aj)(a L.LC, Permit Name (if different): Facility Address: 9)y I IgvOca V60--In Rocca cvv i-t'll (Street) N(-. Z-14S-7 J Qar�;e- ("'n � �! ) (z°) County Telephone #:2SZ'4 -�1 Co ntactac t Person: Well Location/ Site Name: No. of Wells to be Sampled: 11-5 (from Permit) Well Identification Number (from Permit): N\WFor Groundwater Treatment Systems Well Depth: ft. Well Di meter: Z in. Check One: ❑ Influent (98) Screened Interval: 3 ft. to Vb ft. ❑ Effluent (99) Depth to Water Level: (o•1 it. below measuring point. DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: • EXPIRATION DATE: Non -Discharge W Q 000591 c) UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery V Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Measuring Point (M.P.) is: 2- ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: S Date sample collected: 1—11-2rJ Date sample analyzed: Field analysis: pH (0- S 1 , Specific Conductance uMhos Laboratory Name: An Temp. Zy•(n °C, Odor Q ov.A, Appearance C.lepuy, Certification No. V) PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid mpies) TIT Dissolved Solids: Total mg/I pH (when analyzed units TOC 21 - 00 mg/I Chloride Z3 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia O.9(_n mg/I TKN as N mg/I YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N _ < n . oL4 mg/I sphorus: Total as P 4.4;1'l mg/I Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium l(„•"l mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) 4 Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Oach lab report.) Report Attached? Yes V (1) No (0) VOC : method # = method # = method if = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Awo(u PLC Permit Name (if different): Facility Address: 1r ' (street) PI(Z"1 . Q5-7 County (city), (state) (zip) 252 4 Contact Person: Telephone #: Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): ski -9 For Groundwater Treatment Systems Well Depth: ZZ.90 .—ft. Well Diameter: 2- in. Checkone: ❑ Influent (98) Screened Interval: 10 ft. to ft. ❑ Effluent (99) Depth to Water Level: it. below measuring point. DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: • EXPIRATION DATE: 10 31 20 4 Non -Discharger Q 000591 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation in ft.: 11 Gallons of water pum ed/biz(fed before sampling: �J Date sample collected: \ �— 1'20 Date sample analyzed: Field analysis: pH � •1` , Specific Conductance uMhos Laboratory Name: �1riv �Yptnw�e,n'� Temp. 23.4 *C, Odor 11, 0-4L Appearance Lleax✓ Certification No. PARAMETERS (Samples for metals were collected unfiltered COD mg/1 Nitri Coliform: MF Fecal /1 ooml Nitr Coliform: MF Total /100m1 Pho (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 2-(o9 mg/I pH (when analyzed) units TOC mg/I Chloride 2- mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia 0 . mg/I TKN as N mg/I YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N mg/I sphorus: Total as P 0.2-H mg/I Orthophosphate mg/1 Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium t-1 16, O LA I mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. At h lab report.) Report Attached? Yes (1) No (0) VOC : method # = method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: No(cL PLC• Permit Name (if different): Facility Address:A1JQCx'1ravvn Road C.VV µ•it, (Sheep N(.. 2.14S7 County (city) (state) (tip) Contact Person: ,ei,n �+�� Telephone #: 2S2 4�2-� 133 Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): KW - 1 O For Groundwater Treatment Systems Well Depth: Z.P __ft. Well Diameter: 2- in. Check One: ❑ Influent (98) Screened Interval: s ft. to '2..0 ft. ❑ Effluent (99) Depth to Water Level: S-L4 ft. below measuring point. Measuring Point (M.P.) is: 2- ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pum ed/bailed before sampling: _; Date sample collected: Field analysis: pH 935 , Specific Conductance uMhos Temp. 24 • Co °C, Odor Lj o Appearance L\-? ' PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid sam les) Dissolved Solids: Total 3Q)`I mg/I pH (when analyzed) units TOC I • 5L4 mg/I Chloride LAq mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia < O C)4 mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: • EXPIRATION DATE Non -Discharge w Q 00054 i O UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: - NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Laboratory Name: �1RV ►YnY�w+¢ Certification No. io YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N co23 mg/I sphorus: Total as P u mg/I Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 3S .1 mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) q Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. P ach lab report.) Report Attached? Yes (1) No (0) VOC method # = method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Awt)(a LLC, Permit Name (if different): Facility Address:-9)y 1 P+vacc. Fa.-Yn Roacl tvv 4-l'll (St,eet) 1N(. 7--14S-7 County (City) (state) (zip) +ZSZ y Contact Person: Telephone #: 162-�;t1S3 Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): - k I For Groundwater Treatment Systems Well Depth: 2-2- _ft. Well Diameter: in. Check One: ElInfluent (98) Screened Interval:. 7 ft. to 2-2- ft. ❑ Effluent (99) Depth to Water Level: 13,i ft. below measuring point. Measuring Point (M.P.) is: 2- ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pum ed/ iled before sampling: 9 Date sample collected: Field analysis: pH , Specific Conductance uMhos Temp. y OC, Odor WOw2� Appearance 0.1�V DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: • EXPIRATION DATE: Non -Discharge UOQ 000541 O UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: �21 Z.rJ Laboratory Name: -Etf1v ►Yco nme ni Certification No. ko PARAMETERS (Samples for metals were collected unfiltered V YES NO and field acidified COD mg/I Coliform: MF Fecal /100mi Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total (o92- mg/I pH (when analyzed) units TOC C� • —tCo mg/I Chloride 2.L9 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia \2., lb O mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N e_a o4 mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 0 • U1 mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Mach lab report.) Report Attached? Yes/ (1) No (0) VOC : method # = method # = method # = 11 0) GREE AVOCA, LLC (WASTEWATER) MR. BRIAN CONNER ID#: 3.32 Drinking Water ID: 37725 P.O. BOX 129 DATE COLLECTED: 11/11/20 MERRY HILL ,NC 27957 DATE REPORTED : 12/02/20 REVIEWED BY: Effluent Well #4 Well #5 Well N7 Well //8 Analysis Method PARAMETERS Date Analyst Code BOD, mg/I 3290 11/12/20 KDS 521OB-11 Total Suspended Residue, mg/i 367 11/13/20 HJO 2540D-11 Ammonia Nitrogen as N, mg/I 0.51 Nlissing 0.14 0.07 0.96 1 t/13/20 KES 350.1 112-93 Total Kjeldahl Nitrogen as N,mg/I 51.24 11/17/20 ICES 351.2 R2-93 Nitrate -Nitrite as N, mg/t (talc) 0.81 353.2 R2-93 Nitrate Nitrogen as N, mg/l 0.23 Missing <0.04 0.64 <0.04 11/12/20 DTL 353.2 R2-93 Nitrite Nitrogen as N, ing/I 0.58 11/12/20 TLH 353.2 I12-93 Total Phosphorus as P, mg/l 23.32 Nlissing 11/17/20 TLH 365.4-74 Total Phosphorus as P, mg/I <0.04 0.08 4.87 11/20/20 KES 365.4-74 Total Organic Carbon, mg/I Missing 3.05 4.03 25.00 11/12/20 SEJ 531OC-11 Bromide, mg/I Missing Chloride, mg/1 82 Nlissing 32 17 23 11/16/20 KDS 45000LB-1I Total Dissolved Residue, mg/I 920 Missing 565 218 378 11/17/20 HJO 2540C-11 Calcium, ug/l 26615 Nlissing 35250 5933 16735 11/13/20 LFJ EPA200.7 Magnesium, ug/l 3976 11/13/20 LI+J EPA200.7 Sodium, ug/I 142850 12/01/20 NAB 3111B-11 Sodium Adsorption Ratio (talc) 0.6 Total Nitrogen, mg/l (talc) 52.05 Environment 1 Incorporate) 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 AVOCA, LLC (WASTEWATER) MR. BRIAN CONNER P.O. BOX 129 MERRY HILL ,NC 27957 Drinking Water ID: 37715 FAX (252) 756-0633 ID#: 132 DATE COLLECTED: 11/11/20 DATE REPORTED : 12/02/20 REVIEWED BY: ;e-�— N9 Well #10 Well #11 Analysis Method PARAMETERS Date Analyst Code Ammonia Nitrogen as N, mg/I 0.07 <0.04 12.80 11/13/20 KES 350.1 112-93 Nitrate Nitrogen as N, mg/I 2.16 6.23 <0.04 11/12/20 DTL 353.2 R2-93 Total Phosphorus as P, mg/l 0.24 <0.04 1.62 11/20/20 KES 365.4-74 Total Organic Carbon, mg/l 1.07 1.34 6.76 11/12/20 SEJ 531OC-11 Chloride, mg/I 28 44 26 11/16/20 l(DS 4500C1.13-11 Total Dissolved Residue, mg/I 269 387 692 11/17/20 HJO 2540C-11 Calcium, ug/1 48042 35100 17671 11/13/20 LFJ EPA200.7 Environment 1, in arporated Drinking Water ID: 37715 GREENVILLE, N.C. 27858 FAX CLIENT: AVOCA, LLC (WASTEWATER) CLIENT ID: 132 MR. BRIAN CONNER P.O. BOX 129 ANALYST: DTL MERRY HILL, NC 27957 DATE COLLECTED: 11/11/20 DATE ANALYZED: 11/24/20 DATE REPORTED: 12/02/20 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 620OC-11 Page: 1 PARAMETERS, ug/l Well #7 Well k8 Well N9 Well #10 Well #11 1. Benzene <0.50 <0.50 <0.50 <0.50 <0.50 2. Bromobenzene <0.50 <0.50 <0.50 <0.50 <0.50 3. Bromochloromethane <0.50 <0.50 <0.50 <0.50 <0.50 4. Bromodichloromethane <0.50 <0.50 <0.50 <0.50 <0.50 5. Bromoform <0.50 <0.50 <0.50 <0.50 <0.50 6. Bromomethane <0.50 <0.50 <0.50 <0.50 <0.50 7. N-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 8. Sec-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 9. Tert-Butylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 10. Carbon Tetrachloride <0.50 <0.50 <0.50 <0.50 <0.50 11. Chlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 12. Chloroethane <0.50 <0.50 <0.50 <0.50 <0.50 13. Chloroform <0.50 <0.50 <0.50 <0.50 <0.50 14. Chloromethane <0.50 <0.50 <0.50 <0.50 <0.50 15. 2-Chlorotoluenc < 0.50 < 0.50 <0.50 < 0.50 < 0.50 16. 4-Chlorotolaene <0.50 <0.50 <0.50 <0.50 <0.50 17. Dibromochloromethane <0.50 <0.50 <0.50 <0.50 <0.50 18. 1,2-Dibromo-3-Chloropropane <0.50 <0.50 <0.50 <0.50 <0.50 19. 1,2-Dibromocthane <0.50 <0.50 <0.50 <0.50 <0.50 20. Dibromomethane <0.50 <0.50 <0.50 <0.50 <0.50 21. 1,2-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 22. 1,3-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 23. 1,4-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 24. Dichlorodifluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 25, 1,1-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 26. 1,2-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 27. 1,1-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 28. Cis-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 29. trans-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 30. 1,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 31. 1,3-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 32. 2,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 33. 1,1-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 34. Cis-1,3-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 35. trans-1,3-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 36. Ethylbenrene <0.50 <0.50 <0.50 <0.50 <0.50 37, Hexachlorobutadiene <0.50 <0.50 <0.50 <0.50 <0.50 38. Isopropylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 39. 4-1sopropyltoluene <0.50 <0.50 <0.50 <0.50 <0.50 40. Methylene Chloride <0.50 <0.50 <0.50 <0.50 <0.50 41. Naphthalene <0.50 <0.50 <0.50 <0.50 <0.50 42. Propyibenzene <0.50 <0.50 <0.50 <0.50 <0.50 43. Styrene <0.50 <0.50 <0.50 <0.50 <0.50 44. 1,1,1,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 <0.50 45. 1,1,2,2-Tetrachloroe thane <0.50 <0.50 <0.50 <0.50 <0.50 46. Tetrachloroethene <0.50 <0.50 <0.50 <0.50 <0.50 47. Toluene <0.50 <0.50 <0.50 <0.50 <0.50 48. 1,2,3-Trichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 Environment 1f Incorporated! GREENVILLE, N.C. 27858 CLIENT: AVOCA, LLC (WASTEWATER) MR. BRIAN CONNER P.O. BOX 129 MERRY HILL, NC 27957 REVIEWED BY: VOLATILE ORGANICS emn MFinannG r9toor-ll Drinking Water ID: 37715 FAX (252) 756-0633 CLIENT ID: 132 ANALYST: DTL DATE COLLECTED: 11/11/20 Page: 2 DATE ANALYZED: 11/24/20 DATE REPORTED: 12/02/20 PARAMETERS, ug/1 Well #7 Well N8 Well N9 Well #10 Well #11 49. 1,2,4-Trichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 50. 1,1,1-Trichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 51. 1,1,2-Trichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 52. Trichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 53. Trichlorofluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 54. 1,2,3-Trichloropropaue <0.50 <0.50 <0.50 <0.50 <0.50 55, 1,2,4-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 56. 1,3,5-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 <0.50 57. Vinyl Chloride <0.50 <0.50 <0.50 <0.50 <0.50 58. Total Xylenes < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 59, Methyl Tert Butyl Ether < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 Environment 1,1ne. CHAIN OF CUSTODY RECORD P.O. Box 7085, 114 Oakmont Dr. Page I of 2 Greenville, NC 27858 environment] iiac.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208'• Fax (252) 756-0633 ❑ CHLORINE CLIENT: 132 Week: 50 UV G '� L Z pH CHECK (LAB) AVOCA, LLC (WASTEWATER) ❑ NONE P P P P P P P P P P P P P G CONTAINER TYPE,NG MR. BRIAN CONNER P.O. BOX 129 ❑ A A C C C A A C C A A A A A E CHEMICAL PRESERVATION MERRY FULL NC 27957 m 0 A - NONE D - NAOH EUj (252) 482-2133 z J M z ¢ cc z R = o m -� a B- HNO, E- HCL 00 v z v 7 C3 b Z o, , o -- z w C - H,SO, F -ZINC ACETATE/NAOH W COLLECTION ¢ w o _ _ a L M U _ = o ¢ G- NATHLOSULFATE SAMPLE LOCATION DATE TIME o a n. cc l�`�l-1� l0`.rj0 �-�' 8 w':::'• it ,.. ... ..., ... .. .... P:•FCi: CLASSIFICATION: E;ilnent ... Il u�' Well -li- t � 1 2 n n ❑ WASTEWATER PDES � i 1 3� 1 f� Sb 3.G 10 n. INKIN WA DR G TER Well ¢7 tt- � � 1 �t 10 ..... .... n... s .}.. .... .. .... ... X DVVRIGW S Z.ID Z 10 Well HS W ECTi SOLID WASTE S ON K. well a9 tl -it- � 1�. l 2 1 0 .. 5 ;o T MAINTAINED F CUSTODY (SEAL) CHAIN CUS S C O RelI;Y10 t DURING 1PMENTlDELIVERY y s11 Wei. � 1 �D t 1' � S 22 Y N SAMPLES COLLECTED BY: (Please Pnnt) Sy-, C.0 CLn SAMPLES RECEIVED IN LAB AT V °C RE (SHED DATEMME REC (SIG.) 1 ! DATE/11ME COMMENTS: TS�G."IAMPLIR) 11-11 z 13 : tok Z111 2: t me RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (S DATE l IMEIj # .5 CO ZUL h ? nn REUWUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATEMME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FORM #5 Grab sample in the blocks above for each parameter requested. N0 s 385405 Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085. 114 Oakmont Dr. Page 2 of 2 UleenVt11G. 1141- LIOJ0 -nvironment 1 inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 •Fax (252) 756-0633 CHLORINE CLIENT: 132 Week: 50 UV Z j,"L L2 pH CHECK(UaB) G G G G CONTAINER TYPE,P/G VOCA, LLC (WASTEWATER) ❑ NONE [R. BRIAN CONNER .O. BOX 129 [ERRY HILL NC 27957 E E E E CHEMICAL PRESERVATION o E z 111 0 o 0 j o CCUj � 'k-' tR CC Q a N �. _ U c 0 y Oc o �v- U r Cn :52) 482-2133 COLLECTION A-NONE D-NAOH � B-HNO, E-HCL w C- H,SO, F- ZINC ACETATE/NAOH LU Cr G - NATHIOSULFATE a a SAMPLE LOCATION DATE TIME Effluent \I.1 1�5�f• 8 CLASSIFICATION: ❑ WASTEWATER (NPDES) Well #4 11-\t- eD 12 ?' .. p, #5 -t _� 11.5D 23 5 to ::FA DRINKING WATER ,all # 7 t\-tt-� 10 (_�k Lj DWR/GW A.: #8 V as y tc to SOLID WASTE SECTION —Avell Well9 ll-1\'�fJ iZ't0 ni 10 'sx< Well \i-\�-]`1 =3� 2�1•� 10 <` <'<''` CHAIN OF CUSTODY (SEAL) MAINTAINED DURING S IPMENT/DELIVERY Well nil SAMPLES D BY: (Please Print) SAMPLES RECEIVED IN LAB AT � °C RELINQUISHED BY (SIG.) (SAMPLER) DATEJTIME RECEIVE IG.) i DATEMME COMMENTS: �•11-�0 13 :10 RELINQUISHED BY (SIG.) DATEMME RECEIVE BY (1 DATEMME RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATEMME Sampler must place a "C" for composite sample or a "T for PLEASE READ Instructions for completing this form on the reverse side. FORM #5 Grab sample in the blocks above for each parameter requested. N ® 385404 ... ..... . ... SG__$__ yF' Orl The results set forth. herein are provided by SGS North America Inc. Technical Report for Environment 1, Inc AVOCA LLC; Merry Hill, NC 132 SGS Job Number: FA79941 Sampling Date: 10/14/20 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@enviromnentline.com ATTN: Ann Brown Total number of pages in report: 1.3 a s Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. e Hardcopy 2.0 Arrtornnted Report Norm Farmer Technical Director Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(I2022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SOS. Test results relate only to samples analyzed. SOS North America Inc. • 4405 Vineland Road - Suite C-15 • Orlando, FL 32911 • tel: 407-425.6700 • t'ax� 407-425-0707 SUS is the sole aullwrity Ivr authorizing edits or modifications to this document. Please share your ideas about Unauthorized modification of this repoit is strictly prohibited. how we can sorvc you letter at: �_ Review standard terms at: hlryt:'iwww.sgs.cont/eiVterms-and-conditions Eli S.t1S,Custumertare(u!sgs.cont i of 13 FA79941 .E Table of Contents Sections: r -1- Section1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 VNI Section3: Sample Results........................................................................................................ S 3.1: FA79941-1: DIGESTER SLUDGE.............................................................................. b Section4: Misc. Forms............................................................................................................ 11 4.1: Chain of Custody........................................................................................................... 12 2of13 - FA79941 SGS North America Inc. Sample Summary Environment 1, Inc AVOCA LLC; Merzy Hill, NC Project No: 132 Job No: FA79941 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID T.report ntae followngap"pltej Organics ND = Not detected above the MDL FA79941-1 10/14/20 18:0013C 10/17/20 AQ Water DIGESTER SLUDGE 3 of 13 FA79941 Summary of Hits Job Number: FA79941 Account: Environment 1, Inc Project: AVOCA LLC; Merry Hill, NC Collected: 10/ 14/20 Lab Sample ID Client Sample ID Result/ Analyte Qua1 RL MDL Units Method FA79941-1 DIGESTER SLUDGE . .......... ... 2-Butanone (MEK) 1.67 0.050 0.020 mg/1 SW846 8260B Page 1 of I ._.S_LiS_ ff°° 4of13 _ FA79941 m i Orlando FL r °So� Results Report of Analysis Section 3 5of13 SMS, _ FA79941 SGS North America Inc. Report of Analysis it Sample ID: DIGESTER SLUDGE Sample ID: FA79941-1 rix: AQ - Water hod: SW846 8260B SW846 1311 ect: AVOCA LLC; Merry Hill, NC File ID DF Analyzed By #1 C0144547.1) 10 10/29/2014:37 SO #2 Purge Volume Run # 1 5.0 ml Run #2 VOA TCLP List CAS No. Compound 71-43-2 Benzene 78-93-3 2-Butanone (MEK) 56-23-5 Carbon Tetrachloride 108-90-7 Chlorobenzene 67-66-3 Chloroform 106-46-7 1,4-Dichlorobenzene 107-06-2 1,2-Dichloroethane 75-35-4 1,1-Dichloroethylene 127-18-4 Tetrachloroethylene 79-01-6 Trichloroethylene 75-01-4 Vinyl Chloride CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 17060-07-0 1,2-Dichloroethane-D4 2037-26-5 "Toluene-D8 460-00-4 4-Bromofluorobenzene Page 1 of 1 s Date Sampled: 10/14/20 Date Received: 10/17/20 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 10/20/20 09:15 OP82562 VC5800 Result HW# MCL RL ND DO18 0.50 0.010 L67 D035 200 0.050 ND D019 0.50 0.010 ND D021 100 0.010 ND ! D022 6.0 0.010 ND `. D027 7.5 0,010 ND D028 0.50 0,010 ND D029 0.70 0.010 ND D039 0.70 0.010 ND D040 0.50 0.010 ND D043 0.20 0.010 Run# 1 Run# 2 Limits 102%- 83-118% 103% 79-125% 97% 85-112% 99% 83-118% TCLP Leachate method SW846 1311 MDL Units Q 0.0031 mg/I 0.020 mg/1 0.0036 mg/1 0.0020 mg/i 0.0030 mg/1 0.0026 mg/I 0.0031 mg/I 0.0032 mg/I 0.0022 mg/I 0.0035 mg/I 0.0041 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Sid_, 6 of 13 FA79941 SGS North America Inc. Report of Analysis Page I of I a Client Sample ID: DIGESTER SLUDGE Lab Sample ID: FA79941-1 Date Sampled: 10/14/20 Matrix: AQ - Water Date Received: 10/17/20 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: AVOCA LLC; Merry Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a 6F06952.D 2 10/29/20 15:11 MV 10/28/20 08:45 OP82710 S617269 Run #2 Initial Volume Final Volume un #1 100 ml 1.0 ml un #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenol ND D023 200 0.10 0.011 mg/1 3&4-Methylphenol ND D024 200 0.10 0.020 mg/l 87-86-5 Pentachlorophenol b ND D037 100 0.50 0.10 mg/1 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.10 0.015 mg/1 88-06-2 2,4,6-Trichlorophenol NTH '. D042 2.0 0.10 0.015 mg/l 106-46-7 1,4-Dichlorobenzene ND. D027 7.5 0.10 0.010 mg/1 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.10 0,016 mg/l 118-74-1 Hexachlorobenzene ND D032 0.13 0.10 0.014 mg/1 87-68-3 Hexachlorobutadiene ND_ : D033 0.50 0.10 0.010 mg/1 67-72-1 Hexachloroethane ND, D034 3.0 0.10 0.033 mg/1 98-95-3 Nitrobenzene ND:, D036 2.0 0.10 0.019 mg/l 110-86-1 Pyridine ND s D038 5.0 0.20 0.040 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 15% ` 14-67% 4165-62-2 Phenol-M 10% 10-50% 118-79-6 2,4,6-Tribromophenol 530/4 33-118% 4165-60-0 Nitrobenzene-d5 39% ° 42-108% 321-60-8 2-Fluorobiphenyl 41% : 40-106% 1718-51-0 Terphenyl-dl4 440//o 39-121% (a) Dilution required due to matrix interference. (b) Associated CCV outside of control limits high, sample was ND. (c) Outside control limits due to matrix interference. Confirmed by batch DUP. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound c�%%��' 7 of 13 SGS.... FA79941 SGS North America Inc. Report of Analysis Page 1 of I 1 Client Sample ID: DIGESTER SLUDGE Lab Sample ID: FA79941-1 Date Sampled: 10/14/20 Matrix: AQ - Water Date Received: 10/17/20 Method: SW846 8151A SW846 3510C Percent Solids: n/a Project: AVOCA LLC; Merry Hill, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC071386.1) 1 10/29/20 19:43 JA 10/28/20 10:00 OP82711 GCC1750 Run #2 Initial Volume Final Volume Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result IIW# MCL RL MDI, Units Q 94-75-7 2,4-D ND D016 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) ND D017 L0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 85% ' 39-135% ND = Not detected MDL _ Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N Indicates presumptive evidence of a compound jj�!�! 8 of 13 _SGS, FA79941 SGS North America Inc. Report of Analysis Client Sample ID: DIGESTER SLUDGE Lab Sample ID: FA79941-1 Matrix: AQ - Water Method: SW846 8081B SW846 3510C Project: AVOCA LLC; Merry Hill, NC File ID DF Analyzed By Run #1 KK99321.D 1 10/27/20 21:08 WH Run #2 Initial Volume Final Volume Run #1 100 ml 5.0 ml Run #2 Page 1 of 1 Date Sampled: 10/14/20 Date Received: 10/17/20 Percent Solids: n/a Prep Date Prep Batch Analytical Batch 10/23/20 09:07 OP82630 GKK3176 Pesticide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) a ND D013 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/l 76-44-8 Heptachlor a ND D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide ND `. D031 0.0080 0.00010 0.000020 mg/l 72-43-5 Methoxychlor a ND D014 10 0,00020 0.000050 mg/I 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 54%. 42-127% 2051-24-3 Decachlorobiphenyl 30%` 27-127% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of13 MS.- FA79944 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: DIGESTER SLUDGE Lab Sample 1D: FA79941-1 Date Sampled: 10/14/20 Matrix: AQ - Water Date Received: 10/17/20 Percent Solids: n/a Project: AVOCA LLC; Merry Hill, NC Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method ...................... . Arsenic <0.10 D004 5.0 0.10 mg/l 1 10/29/20 10/29/20 LM SW8466010D2 SW8463010A4 Barium <2.0 D005 100 2.0 mg/1 1 10/29/20 10/29/20 LM SW846 6010D 2 SW846 3010A 4 Cadmium < 0.050 D006 1.0 0.050 mg/1 1 10/29/20 10/29/20 LM SW846 6010D 2 SW846 301OA 4 Chromium < 0.10 D007 5.0 0.10 mg/1 1 10/29/20 10/29/20 LM SW846 6010D 2 SW846 3010A 4 Lead < 0.050 D008 5.0 0.050 mg/I 1 10/29/20 10/29/20 LM SW846 6010D 2 SW846 3010A 4 Mercury < 0.0050 D009 0.20 0.0050 mg/1 1 10/22/20 10/22/20 is SW846 7470A 1 SW846 7470A 3 Selenium <0.10 DO W 1.0 0.10 mg/l 1 10/29/20 10/29/20 LM SW846 6010D 2 SW846 3010A 4 Silver <0.10 DO11 5.0 0.10 mg/1 1 10/29/20 10/29/20 LM SW846 601OD 2 SW846 3010A 4 (1) Instrument QC Batch: MA17159 (2) Instrument QC Batch: MA17189 (3) Prep QC Batch: MP38012 (4) Prep QC Batch: MP38054 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) SGS' 10 of 13 FAM41 S-Gg-- Orlando FL by r3 ^ y=s Misc. ;Forms Custody Documents and Other Forms Includes the following where applicable; • Chain of Custody Section 4 0 11 of 13 FA79941 Environment 1, Inc. P.O. Box 7095, 114 Oakmont DT. CHAIN OF CUS+ODY RECORD W ` IA1 Page I_ of l J�CL'n VI11�, ,�V. c.u✓,. :nvicanmant I inacom DISINI LCIIO N CHLORINE NEUTAALI2E0ATC0LLECTION Phone (252) 756-6208 • Fax (252) 756-0633 ❑ CHLORINE pH CHECKIIAB) CLIENT: 132 A Week-. 45 I y UV (❑� CONTAINERTYPE,P/G VOCA, ),LC (WASTFWATRR) NONE G G G G it. BRIAN CONNBR R BOX 129 CHEMICALPRES9iVATION IRRRY IBLT, NC 21957 A A I A A s A -NONE D-NACH G SP p a n B 19�, E HCl .52) 482-2133 0 c� ; a 5 £ C- H�SO, F - ZINC ACETATFJNAOH CCLLECTK)V rv- o k-' tR H °a E- a� a 0-NATHOSULFATE SAMPLE LOCATION 047E TIME (9.00 �i� CIASSFICATION: Di cuter Sludge 10 )410 3 I� WASTEWATER(NPOES) 'H I ❑ DRINKINGWATER fc ��N ❑ DWR)GW ❑ SOUOWASTESECTLON CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY 0 N SAMPLES COLLECTED BY: (Please Print) v� SAMPLES RECEIVED IN IAEt AT o `C RE NOUISIiEDBY (SIG.)(SAMPLER) DATFlRM£ RE, CES1Ef�Y(S1G:) t� )C,/�5/� ytEiLn CONAJENTS: I J 1 pp9JDUIS BY(S1G) OATL9fIME RE- �6BY(Bl(i.) OATFJr1ME -7;00 R ISHED.BY � - E DBY TEf1ME FORM MS PLEASE READ Instructions for completinginls torm on loe reverse slue. �;Oj e. Grab sample In the blocks above for each parameter requested. N ° 385751 `p Q FA79941: Chain of Custody Page 1 of 2 01 12 of 13 FA79941 SGS Sample Receipt Summary Job Number: FA79941 Client: ENVIROMENTAL 1 Project: AVOCA WASTEWATER Date / Time Received: 10117/202012:D5:00 PM Delivery Method: FEDEX Alrbill #'s: 90043372674 Therm ID; IR 1; Therm CF: -0.2; 11of Coolers: 1 Cooler Temps (Raw Measured) 'C: Cooler 1: (3.8); Cooler Temps (Corrected) °C: Cooler 1: (3.6); 1. Custody Seale Present 6d ❑ 1. Sample labels present on bottles ® ❑ 2. Custody Seals Intact ® ❑ 2. Samples preserved properly ® ❑ 3. Temp criteria achieved ® ❑ 3. Sufficient volume/containers recvd for analysis: ® ❑ 4. Cooler tamp vergicatlon IR Gun 4. Condition of sample leieci 5. Cooler media lea (Baal 5. Sample recvd within HT ® ❑ 6. Dates/TimeSADs on COC match Sample Label ® ❑ Trip Blank Information Y or N N/A 7. VOCa have headspace ❑ ❑ Ed 1. Trip Blank present / molar ❑ ❑ ® 8. Bottles received for unspecified tests ❑ 2. Trip Blank listed on CDC ❑ ❑ ® 9. Compositing Instructions clear ❑ 0 W or S NlA 10. Voe Soll Klls/Jars received pest 48hre? ❑ ❑ 11. % Solids Jar received? ❑ ❑ 3. Type Of TB Received ❑ ❑ 8 12. Residual Chlorine Present? ❑ ❑ SE Misc. Information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Teat Strip Lot lis: pH 0-3 230315 pH 10.12 219813A Other: (Specify) Resldual Chlorine Teat Strip Lot M. Comments scoot Rw. Dab OSrlV 17 Technician: MAGALEAK Date: 10/17/202012:05:00 Reviewer. Date: FA79941: Chain of Custody Page 2 of 2 A La 13 of 13 FA79941 Environment 1, Inc. PO. Box 7085, 114 Oakmont Dr. (;reenville NC 27RSR CHAIN OF CUSTODY RECORD Page I of _ I environnientl ine.com DISINFECTION CHLORINE NEUTRALIZED ATCOLLECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE CLIENT: 132 A Week: 45 pH CHECK (LAB) UV G G G G CONTAINER TYPE,P/G VOCA, LLC (WASTEWATER) ❑ NONE iR. BRIAN CONNER .O. BOX 129 CHEMICAL PRESERVATION TERRY HILL NC 27957 A A A A c o A -NONE D-NAOH :52) 482-2133 1= V "' ? `-�` ui Z cr w > u ° = w C cn B HNO a E HGL O = �- cc O � w Z Cn ° ? = ±Q w C H;SO, F - ZINC ACETATE/NAOH COLLECTION U Cr uj =i w¢ o y G - NA THIOSULFATE SAMPLE LOCATION DATE TIME Digester Sludge :O-1�F 20 1w• 00 4e) 3 a CLASSIFICATION: WASTEWATER (NPDES) DRINKING WATER DWR,KGW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY 0 N SAMPLES COLLECTED BY: (Please Print) ��1d✓v SAMPLES RECEIVED IN LAB AT o °C RELINQUI�FIED BY (SIG.) (SAMPLER) DATFITIME RECEIVED BY (SIG.) j� j� DATEM E COMMENTS: RELINQUISHED BY (SIG.) DATErnME RECEIVED BY (SIG.) DATErnME 100wzf, 1 7;oc. RELINQUISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG.) DATE/TIME PLEASE READ Instructions for completing this form on the reverse side. FORM #5 Sampler must place a "C" for composite sample or a "G" for Grab sample in the blocks above for each parameter requested. N 0 385751