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Home My WebLink AboutWQ0004972_Monitoring - 12-2020_20210204Monitoring Report Submittal ............................................................................................................................................ Permit Number #* WQ0004972 Name of Facility:* Month:* December Report Information Forest Lakes Preserve ELS Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter:* Signature: Date of submittal: Initial Review Year:* 2020 Upload Document* Forest Lakes_Dec.pdf 1.8MB FDF Cnly Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-t, NDAR-2, NDMLR, GW-59). Jessica. Mize@pacelabs.com Jessica Mize jus l oil Reviewer: Williams, Kendall 2/3/2021 This will be filled in automatically Is the project number correct? * WQ0004972 Is the monitoring report r Yes r No accepted?* Regional Office * Winston-Salem Accepted Date: 2/4/2021 Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00004972 MONTH: December YEAR: 2020 FACILITY NAME: Forest Lakes Preserve ELS COUNTY: Davie Flow Monitoring Point: Effluent: Influent: Parameter Monitoring Point: Effluent: Influent:LJ I Surface Water(SW : SW CodelName: LJ Was There Effluent Flow for this Month Generated At This Facility: Yes: No: Lj D A T Operator Arrival Time 2400 Clock Operator Time on Site ORC on Site? 50050 OD400 50%11 00310 00610 D0530 31616 00655 00625 00630 D06M 00620 70300 0094D Daily Rate (Flour) Into Treatment Symm pH Rcsidul Chlorine BOD-5 20"C NH-3-N TSS Feca# Colifo m (Ge wwric Mean') Total Phos Total Kjddhal Nitrogen 1402+NO3 Total Nitrogen Nitrate NO3-N Taal Dissa cd Solids Chloride HRS YfN GPD HNITS M51L NIGfL MG,L KJM /1UUNIL i(7 61GfL NIGrL M&L M rL 1 r hl rL Continuous . Drat v rant v rant r on, � am v ant y i Drat y = om y -TLam , y , ryes - ryeu I 1424 0.50 Y 13,119 6.00 <10 1518 0.25 Y 10,276 5.93 <110 3 1103 0.50 Y 10.0111 5.92 <10 4 1218 0.25 Y 10.944 5.94 <10 s 13,332 6 13,332 7. 0718 1 0.50 Y 1 13,332 5.94 1 <10 a 1525 0.25 B 10.877 5.98 <If) 9 1539 0.50 B 9,911 5.96 <10 10 1.118 0.25 Y 9.849 5.99 <10 11 1339 0.25 V 9,662 5.98 <10 I'- 14,971 13 1 14,871 14 1216 1 0,25 Y 14,871 5.98 <10 15 1511 0.25 B 10,763 6.03 --11) 16 1549 11.25 B 10,142 6.01 <I I( 17 1540 0.25 - B 9,29111 5.97 <11) Is 0825 0.25 Y 9,738 5.96 <10 19 14,003 20 14,003 21 1411 1 0.25 Y 14,003 1 5.99 1 <10 2: 0937 11'5 Y 9,905 5.92 <10 23 1405 0.50 Y 9,863 5.94 <10 24 1410 (ISO B 9.144 5.99 <Ifl 2s 16.222 Holida • - ---------------------------------------------------------------------------- ----------------------------- 26 16,222 '7 16-27 :s 0710 0.50 Y 16,222 1 6.00 <10 29 1232 025 Y 10,041 6.01 <10 - 9.0 28.7 10.8 -,2420 8.2 30.11 <0.040 30.1 <0.30 30 1 1451 1 0.25 B 9.997 6,114 <10 31 1 1406 1 0.25 B 8,286 Clio <I0 Average 12,043 QO 10.8 0.0 < . 0.1 <0.30 Daily maximum 16,222 5.04 <10 00.8 >2420 8.2 75 <0. < . Daily Minimum 8,286 _4.92 <10 9.0 28.7 10.8 >2420 8.2 30.0 <0.04 30.1 <0.30 Monthly Limits (s) 24400 Composite 0 / Grab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: II Phone: 336-996-2841 Check Box if ORC Has Changed ORC Certification Number: 987931/20771 Certified Laboratories (l): Pace Analytical Serivices (2): Person(s) Collecting Satrapies: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X- - - DENR (SIGNATURE OFOPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant (Y,N) L Does all monitoring data and sampling frequencies meet permit requirements? If the facility isnon-compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N Riverside Plaza . Suite 800 Chicago, Il 60606 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivi 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 3/31/21 (Permit Exp. Date) 0060 0 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN(Plant Available 00400 pH 32730 Phenols 40665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting faeilit.,�s permit for reporting data * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W 004972 MONTH: December YEAR: 2020 FACILITY NAME: Forest Lakes Preserve ELS. COUNTY: Davie Formulas; Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (pubic feettgallon) x 12 (incheslfoot)) f (Area Sprayed (arras) x 43,560 (square feet/acre) or = [Volume Applied (gallons) I (Area Sprayed (acres) x 27,152 (gallonslacreArirh), Maximum Hourly Loading (inches) = Daily Loading (inches) I [Time irrigated (minutes)160 iminutes/hour)i Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total pinches) = Sum of this months Monthly Loading (inches) and previous 11 moriffs Monthly Loadings (inches) Average Weekly Loading (inches) = [Monlhty Loading (Inchestmonth) f Number of days in the month (days/monih )) x 7 (dayslweek) •. Irrigation r D. Irrigation Occur • •. Irrigation Occur On yesEl NoE3YeLlN No. 0 ■ ■ Area Sprayed (arraii); OWN.", Fli Peramitted • • • fill ®®®®®®®®®®® A �� ter• ��■� �� ■� �� ■�■ ®■� � ■ter. � ■�� ■� �� m �®®��Ziii��■r•��i��■�iiiiii� E�1�'lIN1�a1�■'*.�IIp11aPt�la�t.,��l�rr�ii. _ -:-�-- _ Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-284I ORC Certification Number: 987931/20771 Check Box if ORC Has Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center RALEIGH, NC 27699-1617 nged: 0 (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) By this signature, I certify that this report is accurate and complete to the best of my knowledge. DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) ,N) I. The application rate(s) did not exceed the limit(s) specified in the permit. Compliant (Y 2. Adequate measures were taken to prevent wastewater runoff from the site(s). T� 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the Q limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." _3-a r (Signature of Permitee)* Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 2N. Riverside Plaza. Suite 800 Chicago, Il 60606 (Pernvttee Address) Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 31/2021 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). 1�;a'ceAnalyfical" www.pacelabs.com January 08, 2021 Tracy Overdurf Forest Lake 192 Thousand Trails Dr. Advance, NC 27006 RE: Project: Forest Lakes Effluent Pace Project No.: 92514044 Dear Tracy Overdurf: Pace Analytical Services, LLC 106 Short St. Kernersville. NC 27254 336-996-2841 Enclosed are the analytical results for sample(s) received by the laboratory on December 29, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie,knott@pacelabs.com 336-996-2841 Project Manager Enclosures Q A«FO 'T ;' I ORA1p REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 ;5ceAnalyficalo r WwmPacelass.com Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification P 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This retort shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L.L.C. Page 2 of 15 1�55'neAnalj&al" 1 www.pacelabs.com I SAMPLE ANALYTE COUNT Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kernersvil e, NC 27284 336-996-2841 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92514044001 Effluent HACH 10206 AMI 1 PASI-E SM 2540D-2011 AMI 1 PASI-E SM 5210E-2011 MWF 1 PASI-E Colilert-18 THP 1 PASI-E TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 350.1 Rev 2.01993 JKG 1 PASI-A EPA 351.2 Rev 2.01993 MFO 1 PASI-A EPA 353.2 Rev 2.01993 KDF1 1 PASI-A EPA 365.1 Rev 2.01993 KDF1 1 PASI-A PASI-A = Pace Analytical Services -Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 15 aceAnalytical e www.pacolabs.com t ANALYTICAL RESULTS Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kernersviile, NC 27284 336-996-2841 Sample: Effluent Parameters Lab ID: 92514044001 Collected: 12/29/20 12:38 Received: 12/29120 14:45 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual HACH 10206 Nitrogen, Nitrate Analytical Method: HACH 10206 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.30 1 12/31/20 09:41 14797-55-8 2540D Total Suspended Solids Analytical Method: SM 264OD-2011 Pace Analytical Services - Eden Total Suspended Solids 10.8 mg1L 4.7 1 12/31/20 11:35 5210E SOD, 5 day EDN Analytical Method: SM 521OB-2011 Preparation Method: SM 5210E-2011 Pace Analytical Services - Eden BOD, 5 day 9.0 mg/L 2.0 1 12/30/20 12:10 01/04/21 14:46 R6 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Cotiforms 2420 MPN/100mL 1.0 1 12/29120 18:06 12/30/20 12:60 El Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 30.1 mg1L 0.52 1 01107/21 11:43 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 28.7 mg/L 0.50 5 01107121 12:19 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 30.0 mg/L 2.5 5 01/04/21 13:29 01/05/21 04:57 7727-37-9 . 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 ND mg1L 0.040 1 01/06/21 11:56 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 8.2 mg/L 0.15 3 01/04/2118:12 01/05/2115:36 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01108/2021 02:25 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 1�5a'cmnalytical" www.pacelabsxcra i QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 QC Batch: 590199 Analysis Method: HACH 10206 QC Batch Method: HACH 10206 Analysis Description: 10206 Nitrogen, Nitrate Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92514044001 METHOD BLANK: 3116511 Matrix: Water Associated Lab Samples: 92514044001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.30 12/31/20 09:41 LABORATORY CONTROL SAMPLE: 3116512 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.0 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3116513 3116514 MS MSD 92514218007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 5 5 5.0 5.0 101 101 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01108/2021 02:25 PM without the written consent of Pace Analytical Services, U-C. Page 5 of 15 �55'ceAnalj6cal") www.pacalabs.coro QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kemersviile, NC 27284 336-996-2841 QC Batch: 590165 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92514044001 METHOD BLANK: 3116439 Matrix: Water Associated Lab Samples: 92514044001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 12/31/20 11:31 LABORATORY CONTROL SAMPLE: 3116440 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 270 108 90-110 SAMPLE DUPLICATE: 3116441 92513955001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L NO NO SAMPLE DUPLICATE: 3117223 92514057001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 11.0 11.3 3 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 01 /08/2021 02:25 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 15 1�l5aceAnalj4icalo srww pacelabs.cam QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 QC Batch: 590012 Analysis Method: SM 521 OB-2011 QC Batch Method: SM 521OB-2011 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92514044001 METHOD BLANK: 3115679 Associated Lab Samples: 92514044001 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 01/04/2113:08 Pace Analytical Services, LLC 106 short St. Kemersville. NC 27284 336-996-2841 LABORATORY CONTROL SAMPLE: 3115680 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOO, 5 day mg/L 198 189 96 84.6-115.4 SAMPLE DUPLICATE: 3115682 92514060001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 63.1 70.0 28 D6 Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2021 02:25 PM without the written consent of Pace Analytical Services, I.L.C. Page 7 of 15 1�5a'ucv.Analytical www.pacolabs.com Project: Forest Lakes Effluent Pace Project No.: 92514044 QC Batch: 589907 QC Batch Method: Colilert-18 Associated Lab Samples: 92514044001 SAMPLE DUPLICATE: 3115373 Parameter Units Fecal Coliforms MPN/100mL QUALITY CONTROL DATA Analysis Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EON Laboratory: Pace Analytical Services - Eden 92513998002 Dup Result Result RPD Qualifiers ND ND Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 Results presented on this page are In the units indicated by the -Unls' column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2021 02:25 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 15 Mnalytical" www.paeelaba.eom I QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kemersvilie, NC 27284 336-996-2841 QC Batch: 591149 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92514044001 METHOD BLANK: 3120846 Matrix: Water Associated Lab Samples: 92514044001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 01/07/21 11:45 LABORATORY CONTROL SAMPLE: 3120847 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3120848 3120849 MS MSD 92513994003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 307 5 5 314 313 148 128 90-110 0 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3120850 3120851 MS MSD 92514004001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Nitrogen, Ammonia mg/L 0.23 5 5 5.3 5.2 100 100 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/0812021 02:25 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 /55'ceAnalytical jJ www.pacelabs com I QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kemersvilie, NC 27284 336-996-2841 QC Batch: 590422 Analysis Method: EPA 351.2 Rev 2.01993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92514044001 METHOD BLANK: 3117493 Matrix: Water Associated Lab Samples: 92514044001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 01/05/21 03:43 LABORATORY CONTROL SAMPLE: 3117494 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.3 93 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3117495 3117496 MS MSD 92514245001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 80.8 10 10 102 102 214 214 90-110 0 M6 Results presented on this page are In the units Indicated by the'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2021 02:25 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 1�5aceAnalj4icale lwiumpacslabilcom QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 QC Batch: 590875 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92514044001 METHOD BLANK: 3119404 Associated Lab Samples: 92514044001 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE: 3119405 Parameter Units Nitrogen, NO2 plus NO3 mg/L Pace Analytical Services, LLC . 106 Short St. Kemersvilie, NC 27284 336-996-2841 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 01106/2111:41 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3119406 3119407 MS MSD 92513980002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.98 2.5 2.5 3.2 3.2 87 89 90-110 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3119408 3119409 MS MSD 92513980003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.5 2.5 2.5 3.7 3.7 89 90 90-110 1 M1 Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2021 02:25 PM without the written consent of Pace Analytical Services, LLC. Page 111 of 15 1�5aa'ccieAnaljdical' www.pacelabs.com t QUALITY CONTROL DATA Project: Forest Lakes Effluent Pace Project No.: 92514044 QC Batch: 590515 Analysis Method: EPA 365.1 Rev 2.0 1993 OC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92514044001 METHOD BLANK: 3117897 Associated Lab Samples: 92514044001 Parameter Units Phosphorus mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 01/05/2115:24 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 LABORATORY CONTROL SAMPLE: 3117898 Spike LCS LCS % Rec Parameter Units Conc. Result eta Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3117899 3117900 MS MSD 92514325003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Fesult Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.062 2.5 2.5 2.6 2.6 100 103 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3117901 3117902 MS MSD 92514325004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 102 102 90-110 0 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. Date: 01/08/2021 02:25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 15 Pace Analytical Services, LLC ;an Malytical ® ,ofi short St. Kemersville, NC 27284 www.paulabs.com t 338-998-2841 t QUALIFIERS Project: Forest Lakes Effluent Pace Project No.: 92514044 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/08/2021 02:25 PM without the written consent of Pace Analytical Services, L.L.C. Page 13 of 15 aceAnalyficai® www.pacelabs.com t QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lakes Effluent Pace Project No.: 92514044 Pace Analytical Services, LLC 106 Short St. Kemersvilie, NC 27284 336-996-2841 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92514044001 Effluent HACH 10206 590199 92514044001 Effluent SM 254OD-2011 590165 92514044001 Effluent SM 62108-2011 590012 SM 521OB-2011 590077 92514044001 Effluent Colilert-18 589907 Colilert-18 589908 9251044001 Effluent TKN+NO3+NO2 591263 Calculation 92514044001 Effluent EPA 350.1 Rev 2.01993 591149 92514044001 Effluent EPA 351.2 Rev 2.01993 590422 EPA 351.2 Rev 2.0 1993 590601 92514044001 Effluent EPA 353.2 Rev 2.01993 590875 92514044001 Effluent EPA 365.1 Rev 2.0 1993 590515 EPA 365.1 Rev 2.0 1993 590697 REPORT OF LABORATORY ANALYSIS This report shall not to reproduced, except in full, Date: 01/08/2021 02:25 PM without the written consent of Pace Analytical Services, I.I.C. Page 14 of 15 W0#:92514044 F�Z�CHAIN-OF-CUSTDDY Analytical Request Document LAB VS umber or Chaifi oi-Custody is a LCGAL DOCUMENT - Comp€ete all re€event fields 16 cempt.ny: Forc-stLakp-s ;13inindtrrhtrrnatinrl: 92514044 w CQ rr Sddress: i--.__CS _— "_t'_L_'Jr,: Fyln bPrujerlManag[r. lntiine £ �ta _._ _._ Rerurt To - - -- - Clna;l To: �. vresr>r va 8 §:§ {i litit' Types: {]I nitric acid, 17) sulfuric and, (3) hydrochloric acid, lA) sodium hydroxide, (S) zinc acetate. (S) ntethanul. (7) salium bistdiate, 10) sodlum thiosulrate, 01 hexane, W ascorbic acid, (B) ammonium sulfate, i CGf+y To: !Slip Col ei lion li r€olA: dre.u: lCj amrrranRini hyrhuxlde, ID) T SP. {{i) Uupi eserved. 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