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HomeMy WebLinkAboutWQ0034806_Residual Annual Report 2020_20210202Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* Annual Report Year* Permit Number (IR)* Applicant/Permittee Email Notifications .......................................................... ............. Does this need review by the hydrogeologist?* Regional Office CO Reviewer Admin Reviewer * Annual Report * Residual Annual Report r Additional Information r Other 2020 WQ0034806 Coastal Farms and Residuals, LLC 0 Yes r No Wilmington Submittal Form Project Contact Information Rease provide information on the person to be contacted by NDB Staff regarding electibnittal, confirmation of receipt, other .......................................................... electronic surece, aner correspondence. _ - Name * Martin Mabe Email Address* martin@Wllcomabesoil.com Project Information ........ ......... .......................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363121396 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 IT Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* W00034806 Fbs Current Existing perm number Applicant/Permittee Address* 8155 Malpass Corner Road, Currie, NC 28435 Facility Name * Coastal Farms and Residuals Land Application Program Please provide comments/notes on your current submittal below. Coastal Farms and Residuals, LLC 2020 Annual Report WQ0034806 At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form} Engineering Rans, Specifications, Calculations, Rc.) Coastal Farms 2020 Annual Report W00034806 24.73M6 (NCDEQ).pdf Upload only 1 PCF docurrent (less than 250 M3). Miltiple docurrents must be combined into one PDF file unless file is larger than upload linit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature ew"2W �W'&"fe Submission Date 2/2/2021 2020 ANNUAL REPORT LAND APPLICATION PROGRAM COASTAL FARMS AND RESIDUALS, LLC PERMIT #WQ0034806 Prepared For: Coastal Farms and Residuals, LLC 8155 Malpass Corner Road Currie, North Carolina 28435 Compiled By: Willcox & Mabe Soil Solutions, PLLC 7231 B Sumnerfield Road Summerfield, North Carolina 27358 February 2021 willcox&mate 5 0 E L S OLUT 10 N S February 2, 2021 NCDEQ-DWR Non -Discharge Compliance Unit 512 North Salisbury Street 9t€' Floor Office# 942X Raleigh, North Carolina 27604 Attention: Non -Discharge Compliance Unit Reference: 2020 LAND APPLICATION ANNUAL REPORT Coastal Farms and Residuals, LLC Permit No. WQ0034806 WMSS Project No, 15-19 Ph:01 Non -Discharge Compliance Unit: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Coastal Farms and Residuals, LLC. WMSS compiled this report using data gathered during the compliance year by Coastal Farms and Residuals, LLC. This data includes: 1) certification form, 2) residuals analyses and pathogen / vector data, 3) application summaries and field loading rate reports, 4) soil analyses. If there is any further infon-nation required or questions regarding this annual report please do not hesitate to contact Coastal Farms and Residuals, LLC or WMSS for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe NC Land Application/Residuals Operator #22753 Enclosures Shared%WMSS Projects12015115-19 Coastal Residuals12020 Annual Report12020 ANNUAL REPORT -COASTAL FARMS.doc Wilcox & Mabe Soil Solutions, PLLC / 7231 B Summeriield Road / Summerfie€d, NC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com TABLE OF CONTENTS SECTION NO. TITLE Certification Form II Residuals Analyses & Pathogen / Vector Attraction Data III 2020 Application Summary and Field Loading Rate Reports IV Soil Analysis CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0034806County: Pender Year: 2020 Facility Name (as shown on permit): Coastal Farms and Residuals, LLC Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. A - Total number of application fields in thepermit: 12 Total number of fields utilized for land application during the year: I Total amount of dry tons applied during the year for al application sites: 482.80 Total number of acres utilized for land application during the year: 93.4 Part B - Annual Comuiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T . l 111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mr. Wesley W000ten, President ,, 1/18/2020 Permittee Name and Title (type or print) Signature o ermittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) RESIDUAL ANALYSES TCLP ANALYSES IF REQUIRED AND PATHOGEN AND VECTOR ATTRACTION REDUCTION COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 1, 2020 Carolina Beach WWTP Permit No. NCO023256 2.35 % Solids R Ir ..0 Parameter % JMg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/K2 (Mg/K2x 0.002) Nitrogen (TKN) 2.500 25,000.000 50,000 Phosphorus 0.675 6,750.000 13.500 Potassium 0.274 2,740.000 5.480 PAN infected)* 1.236 12,355.460 24.711 PAN (surface)* 0.899 8,890.460 17.781 Ammonia Nitrogen 0.693 6,930.000 13.860 Calcium 3.280 32,800,000 65.600 Calcium Carbonate E . ... ... --- Magnesium --- 4,640,000 9.280 Sodium --- 7,530,000 15.060 Sulfur .-- Nitrate N / Nitrite N --- 4.460 0.009 Barium r Chloride _-- ___ --- JI Iron ___ ___ _ - _ Aluminum --- 4,210.00 8.420 Arsenic Cadmium --- --- 46.40 20.60 0.093 0.041 Chromium Copper Lead Mercury --- --- --- --- 21.100 638.00 26.90 0.647 0.042 1.276 0.054 0,001 Molybdenum Nickel --- --- 20.60 20.60 0,041 0.041 Selenium Zinc --- --- 20.60 996.00 0.041 1.992 r Environmental Chemists # 2020-16736 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN SAIL 1.58 Ceiling Concen. Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Plot Detected) or < detection limits are listed as detection limits for calculation purposes. 75 85 840 57 75 420 100 7,501 COASTAL FARMS AND RLSTDUALS, LLC WQ0034806 Carolina Beach WWTP 10/01/20 5,692 3.7553 10/01/20 4,594 3.6622 10/0I/20 3,370 35276 10/01/20 5,395 3.7320 10/01/20 6,641 3.8222 10/01/20 9,768 3.9898 10/01/20 2,618 3.4180 Total 1 25.9071 Average 3.70I0 Geometric Meani€ Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Oct 22, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2020-16736 Project ID: Carolina Beach VWVTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-42809 Site: Sludge 10/9/2020 8:00 AM Solid/Sludge Client Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 00818135to <0.02 mg1L 10/05/2020 Endrin (TCLP) SW 846 Method 808181351a <0.0005 mg/L 10/05/2020 Heptachlor (TCLP) SW 846 Method 8081BI3510 <0.0005 mg/L 10/05/2020 Heptachlor epoxide (TCLP) SW 846 Method 80el B13510 <0.0005 mg1L 10/05/2020 Lindane (TCLP) SW 846 Methad 80818/3510 <0.0005 mg/L 10/05/2020 Methoxychlor (TCLP) SW 846 Method 8081 B1351 0 <0.0005 mg/L 10/05/2020 Toxaphene (TCLP) SW 846 Method 8081B13510 <0.05 mg/L 10/05/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 10/05/2020 2,4,5-Trichlorophenol (TCLP) SW 046 method 8270/3510 <0.050 mg/L 10/05/2020 2,4,6-Trichlorophenol (TCLP) SW 645 method 8270/3510 <0.050 mg/L 10/05/2020 2,4-Dinitrotoluene (TCLP) SW 845 method 827013510 <0.050 mg1L 10/05/2020 Cresol (TCLP) SW 846 method 627013510 <0.050 mg/L 10/05/2020 Hexachloro-1,3-butadiene (TCLP) 5W 846 method 027013510 <0.050 mg/L 10/05/2020 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 1010512020 Hexachlorcethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10/05/2020 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 10105/2020 Nitrobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 10/05/2020 o-Cresol (TCLP) SW 846 method 827013510 <0,050 mg/L 10/05/2020 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0,250 mg/L 10/05/2020 Pyridine (TCLP) SW 846 method 8270/351a <0.050 mg/L 10/05/2020 2,4,5-TP (TCLP) SW848 Method 8151A <0.003 mg/L 10/09/2020 2,4-D (TCLP) SW646 Method 0151A <0.003 mg/L 10/09/2020 1,1-Dichloroethylene (TCLP) SW046 Method 8260/5030 <0.01 mg/L 10/13/2020 1,2-Dichloroethane (TCLP) SW846 Method 026015030 <0.01 mg/L 10/1312020 Benzene (TCLP) SW645 Method 826015030 <0,01 mg/L 10/13/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg1L 10/13/2020 Report #:; 2020.16738 Page 1 of 4 SN ell IB p�` ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910-347,5843 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Oct 22, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID. 14020008 Attention: Report #: 2020-16736 Project ID: Carolina Beach =A f'P Chlorobenzene (TCLP) SW846 Method 8280/5030 <0A1 mg/L 10/13/2020 Chloroform (TCLP) SW846 Method 826015030 <0.01 mg/L 10/13/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260I5030 <0.05 mg/L 10/13/2020 Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 10/13/2020 Trichbroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 10/1312020 Vinyl Chloride (TCLP) SW846 Method 826015030 <0.01 mg/L 1011312020 RCI Cyanide Reporting limit elevated due to EPA 335.4 matrix interference. <0.05 mg/kg 1010612020 Sulfide SM 4500 S D 63.8 mglkg 10/06/2020 Ignitability SW 846 method 1010 ,200 °F 10/08/2020 pH SW 846 Method 9045D 7.25 units 10/12/2020 Sludge Residuals Aluminum EPA200,7 4210mglkg 10/06/2020 Arsenic EPA200,7 46.4mg1kg 10/06/2020 Cadmium EPA 200.7 <20.6 mg/kg 10/06/2020 Calcium EPA 200.7 32800 mg/kg 10/06/2020 Chromium EPA 200.7 21.1 mg/kg 10/06/2020 Copper EPA 200.7 638 mg/kg 10/06/2020 Lead EPA 200.7 26,9 mg/kg 10/06/2020 Magnesium EPA 2003 4640 mg/kg 10/06/2020 Molybdenum EPA 200.7 <20.6 mg/kg 10/06/2020 Nickel EPA 200.7 <20.6 mg/kg 10/06/2020 Potassium EPA 200,7 2740 mg/kg 10/06/2020 Selenium EPA 200.7 <20.6 mg/kg 10/06/2020 Sodium EPA 200.7 7530 mg/kg 10/06/2020 Zinc EPA 200.7 996 mg/kg 10/06/2020 Nitrate+Nitrite-Nitrogen EPA 353,2 4.46 mg/kg 10/02/2020 Total Solids (%) SM 2540 a 2.35 % 10101/2020 Ammonia Nitrogen SM 4500 NH3 C 6930 mg/kg 10/07/2020 Report #:; 2020-16736 Page 2 of 4 ANALYTICAL 8, CONSULTING CHEMISTS Envaironmental. Chemists, Inc. 6602 Windmill Way, WiLniangton, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC, Date of Report: Oct 22, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2020-16736 ProjecflD: Carolina Beach WWTP Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 25000 mg/kg 10/06/2020 Total Phosphorus SM 4500 P F 6750 mg/kg 10/09/2020 Mercury Sw6467471B <0.647mg/kg 10/07/2020 TCLP Metals Arsenic EPA 200.7 <1.0mg/L 10/05/2020 Barium EPA 200.7 <1.0mg/L 10/05/2020 Cadmium EPA 200.7 <1.0mg/L 10/05/2020 Chromium EPA 200.7 <1.0 mg/L 10/05/2020 Lead EPA 200.7 < 1.0 rng/L 10/05/2020 Selenium EPA 200.7 <1.0mg/L 10105/2020 Silver EPA 200.7 <1,0mg/L 10/05/2020 Mercury EPA245.1 <0.0002mg/L 10/07/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-42810 Site: 1 10/1/2020 8:01 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.46 % 10/01/2020 Fecal Density SM 9221C EMPN 24 hr 503 5692 MPN/g 10/01/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-42811 Site: 2 10/1/2020 8:02 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2 83 % 10/01/2020 Fecal Density SM 0221C E MPN 24 hr 503 4594 MPN/g 10/01 /2020 Lab lD Sample ID: Collect Date/Time Matrix Sampled by 20-42812 Site: 3 10/1/2020 8:03 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.73 % 10/01/2020 Fecal Density SM 9221C E MPN 24 hr 503 3370 MPN/g 10/01/2020 Report 2020-16736 Page 3 of 4 4 4 ANALYTICAL & CONSULTiNG CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab . 910.392.44 -4 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Oct 22, 2020 8155 Malpass Corner road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report #: 2020-16736 Project ID: Carolina Beach WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-42813 Site: 4 10/1/2020 8:04 AM Solid/Sludge Client Test Method Total Solids (%) SM 2540 e Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect Date/Time 20-42814 Site: 5 10/1/2020 8:05 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect DatelTime 20-42815 Site: 6 10/1/2020 8:06 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect Date/Time 20-42816 Site: 7 10/1/2020 8:07 AM Test Method Total Solids (%) SM 2640 B Fecal Density 5M 9221C E MPN 24 hr 503 Comment: Sludge residuals reported on a dry weight basis. Reviewed by: Results Date Analyzed 2.41 % 10/01/2020 5395MPN/g 10/01/2020 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 2.56 % 10101 /2020 6641 MPN/g 10/01/2020 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 2.15 % 10/01/2020 9768 MPN/g 10/01/2020 Matrix Sampled by Solid/Sludge Client Results Date Analyzed 2.35 % 10101 /2020 2618MPN/g 10/01/2020 Report #,: 2020-16736 Page 4 of 4 0 av N N V1 U N Z c 41 ❑ 0 a V Fw- o`s M O � w £ LL M w , N V VJ fn :3 Z U] U) (J U) w U) V) N ` It J ~ a o 0 o e \_ II pi ,e ry Q a C CD C C C En C Eft G U) v II U a CD ra) p Q o LL .Z o N U U U U U U U mm O C E LL E1. LL LL LL U. LL lL ixL!I dz 0 ,5 2l3H10 U N W � O fi. = IL y II Z OIHl X X K x X X X } O v/ HOVH Z Q ., Z j Il w w £ONH vaszH o j ~q CL a 13H (� aCi 2 1L 0 3NON x w H w m LLI ,,; H39Wf1NLL +. 1 C U = Q `' � 11 716ur U = U m m to BUIJD143 r z Q � Z z q Li.i w W62zz0 z O H U J W 14- O>- `J 0 OIL w o QO U U fr z w a Z z W a Ill IC Vl N E (D � f3? U J t otf U) E ca LL V1 w i7 o 0 Q H u ea d1 a iale>luo� C� a L7 a C7 (7 a C� a [� d (7 a Cry w !i Q ja U (D U (D U C7 U (9 U (7 U) a)lsoduioo adAjL aldweg E a H c Q a E 0 F- co * l uDl w l I- m L � d y 3 o•mE E ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, T LC WQ Permit Number: WQ0034806 WWTP Name: Carolina Beach WWTP NPDES Number: N00023256 Monitoring Period: From 1/1/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tennp) ❑ Alt B (Alk Treatment) ❑ AIt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Patho ergs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Com ost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑ Beta Ray 01 Gamma Ray ❑ Pasteurization ❑ _ .._....:............. _.... _... Class B: jAlt. (1) Fecal Density p I Alt_ (2) Process to Significantly Reduce Patho ens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air in ❑ composting ❑ Digestion ❑ Anaero bic Digestion ❑ If applicable pp to alternative periormed(Class A ,or Class B),complete 'the fallowing. monitoring data; Parameter Allowable bevel Pathogen Density um er or Frequency Sample Analytical in Slud-eExcee- of AnalysisType Tech- 2 Geo. Mean MaximumUnits ninne 2 x l0 to the MPN 2,618 5,024 9,768 MPN/g '0 Annual Grab 5M92210E 6th power Per gram of CFU Fecal Coliform total solids 100tnpn per gram oftotal0 solid (dry aauiivncua oaucrna 1 iwrn per 4 grams (in lieu of fecal total solid (dry coliform wei ht) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt, 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIL 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ All 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) l] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in I5A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." William Raymond, ORC Wesley Wooten, President Preparer Name and Title (tvne or print) Land Applier Narne and Title (if applicable)(type or print) ZoZo 101 20 Signature of epar� * Date Signature of L d Applier (if applicable) Date *Preparcr is deftned in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 25, 2020 Northwest Resional WRF Permit No. WQ0034367 1.42 % Solids 6.75 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 4.300 43,000.000 86,000 Phosphorus 3.440 34,400.000 68.800 Potassium 0.356 3,560.000 7.120 PAN (iniected)* 1.424 14,240.300 28.481 PAN surface)* 1.33I 13,310.300 26.621 Ammonia Nitrogen 0.186 1,860.000 3.720 Calcium 2.050 20,500.000 41.000 Calcium Carbonate E . --- --- Magnesium --- 2,080.000 4.160 Sodium --- 7,030,000 14.060 Sulfur ___ --- --- Nitrate N 1 Nitrite N --- 38.300 0,077 Barium --- --- --- SAR 1.49 Chloride --- - -- Iron --- -- - Ceiling Concen. (M /K ) Aluminum --- 37,700.00 75.400 Arsenic --- 23.00 0.046 75 Cadmium --- 23.00 0,046 85 Chromium --- 40.800 --- - Copper -- 356.00 0.712 4,300 Lead --- 23.00 0.046 840 Mercury --- 1.210 0.002 57 Molybdenum --- 23.00 0.046 75 Nickel --- 23.00 0.046 420 Selenium --- 23.00 0.046 100 Zinc --- 1,180.00 2.360 7,500 Environmental Chemists # 2020-05012 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Northwest Regional WRF 03/25/20 1,159,421 6.0642 03/25/20 609,272 5.7848 03/25/20 874,317 5.9417 03/25/20 1,134,752 6.0549 03/25/20 621,622 5.7935 03/25/20 1,095,891 6.0398 03/25/20 1,012,659 6.0055 Total F 41.6844 Average 1 5.9549 Geometric Mean Fecal Coiiform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. r� oNWASA May 01, 2020 Mark Young Northwest RWRF 189 Mills Field Rd. Richlands, NC 28574 RE: NW Solids ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910) 389-8511 Enclosed are the results of analyses for samples received by our laboratory on 3/25/2020. If you have any questions concerning this report, please feel free to contact me. Sincerely, Todd A. Roberts For Mark Young Northwest ORC Off° WA,SA Northwest RWRF Project: NW Solids 189 Mills Field Rd. Project Number: Reported: Richlands, NC 28574 Project Manager: Mark Young 05/01/2020 14:17 Analysis Case Narrative NR: No results reported fior Isnitabilit EPA 1030, CC=n- EPA 335.4, Sulfide SM 4500 S D and pH SW846 the contents of thcs nEpott apply to the samples) analyzed to amxdance w M the drain of custody document. No dopthatlon ofthis report is allowed, excepttn ifs entirety. Page 2 of 8 �a ONWVASA Northwest RWRF Project: NW Solids 189 Mills Field Rd. Project Number: Reported: Richlands, NC 28574 Project Manager: Mark Young 05/01/2020 14:17 Sample Results Data Analyzed by: Environmental Chemists, Inc. Sample: NW Digestor B N201324-01(SL) 03/25/2020 08:30 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Aluminum 37,700 mg/K9 03/30/2020 EPA 200.7 Ammonla-N 1860 mg/Kg 03/28/2020 SM 4500 NH3 C Arsenic < 23.0 mg/Kg 03/30/2020 EPA 200.7 Calcium 20,500 mg/Kg 03/30/2020 EPA 200.7 Cadmium < 23.0 mg/Kg 03/30/2020 EPA 200.7 Cyanide NR 0.025 mg/Kg 03125120ZO EPA 335.4 Chromium 40.8 mg/Kg 03/30/2020 EPA 200.7 Copper 356 mg/Kg 03/30/2020 EPA 200.7 Mercury < 0.0002 0.0002 mg/L 04/07/2020 EPA 245.1 Mercury < 1.21 mg/Kg 04/06/2020 SW846 74718 Ignitabllity NR mm/sec 03/25/2020 EPA 1030 Potassium 3560 mg/Kg 03/30/2020 EPA 200.7 Magnesium 2080 mg/Kg 03/30/2020 EPA 200.7 Molybdenum < 23.0 mg/Kg 03/30/2020 EPA 200.7 Sodium 7030 mg/Kg 03/30/2020 EPA 200.7 Nickel < 23.0 mg/Kg 03/30/2020 EPA 200.7 Nitrate+Nitrite-Nitrogen 39.3 mg/Kg 04/06/2020 EPA353.2 Lead < 23.0 mg/Kg 03/30/2020 EPA 200.7 PH 6.75 pH Units 04/02/2020 5M 4500 H 8 PH NR PH Units 03/25/2020 SW846 9045D Selenium < 23.0 mg/Kg 03/30/2020 EPA 200.7 Sulfide < mg/Kg 03/25/2020 SM 1500 5 D Chlordane < 0,02 0.02 mg/L 04/00/2020 SW846 808113/3510 Endrin < 0.0005 0.0005 mg/L 04/08/2020 SW846 80818/3510 Heptachlor < 0.0005 0.0005 mg/L 04/08/2020 SW846 80818/3510 Heptachlor epoxide < 0.0005 O,ODOS mg/L 04/08/2020 SW846 80810/3510 Lindane < 0.0005 0.0005 mg/L 04/08/2020 SW846 80818/3510 Methoxychlor < 0.05 0.05 mg/L 04/08/2020 SW846 808113/3510 Toxaphene < 0.05 0.05 mg/L 04/08/2020 SW846 808113/3510 1,4-Dichlorobenzene < 0.050 0.05 mg/L 04/07/2020 SW846 8270/3510 2,4,5-Trichlorophenol < 0,050 0.05 mg/L 04/07/2020 SW846 8270/3510 2,4,6-Trichorophenol < 0,050 0.05 mg/L 04/07/ZOZO SW846 8270/3510 2,4-Rinitrotoluene < 0,050 0.05 mg/L 04/07/2020 SW846 8270/3510 Cresol 0.985 0.05 mg/L 04/07/2020 SW846 8270/3510 Hexachlorn-1,3-butadiene < 0.050 0.05 mg/L 04/07/2020 SW846 8270/3510 Hexachlorobenzene < 0.050 0.05 mg/L 04/0712020 SW846 8270/3510 Hexachlomethane < 0.050 0.05 mg/L 04/07/2020 SW846 8270/3510 M+P Cresol 0.985 0.05 mg/L 04/07/2020 SW846 8270/3510 Nitrobenzene < 0,050 0.05 mg/L D4/07/2020 SW846 8270/3510 o-Cnesal < 0.050 0.05 mg/L 04/07/2020 SW846 8270/3510 Pentachlomphenol < 0.25 0.25 mg/L 04/07/2020 SW846 8270/3510 Pyridine < 0.050 0.05 mg/L 04/07/2020 SW846 8270/3510 2,4,5-TP < 0.003 0.003 mg/L 04/09/2020 SW846 8151A 2,4-0 < 0.003 0.003 mg/L 04/09/2020 SW846 8151A The contents of D41s reportapply to the samples) analyzod In accordance Wa dre draln ofcustbdy document. No duplicadon of this mport,is allowed, except In Rs enArety. Page 3 of 8 ONWASA Northwest RWRF Project: NW Solids 189 Mills Field Rd. Project Number: Reported: Richlands, NC 28574 Project Manager: Mark Young 05/01/2020 14:17 Sample Results (Continued) Data Analyzed by: Environmental Chemists, Inc. Sample: NW Digestor B (Continued) N201324-01 (SL) 03/25/2020 08:30 Digestor Sludge Reporting Date Analyst Analyte Result Qua[ Limit Units Analyzed Initials Method 1,1-Dichloroethylene < 0.010 0.01 mg/L 03/31/2020 SW846 6260/5030 1,2-Dichlomethane < 0.010 M01 mg/L 03/31/2020 SW816 $260/5030 Benzene < 0.010 0.01 mg/L 03/31/2020 SW846826015030 Carbon Tetrachloride < 0.010 0.01 mg/L 03131/2020 SW846 8260/5030 Chlorobenzene < 0.010 0.01 mg/L 03/31/2020 SW846 8260/5030 Chloroform < 0.010 0.01 mg/L 03/31/2020 SW846 0260/5030 Methyl ethyl ketone < 0.010 0.05 mg/L 03/31/2020 SW846 8260/5030 Tetrachloroethylene < 0.010 0.01 mg/L 03/31/2020 SW846 8260/5030 Trichloroethylene < 0.010 0.01 mg/L 03/31/2020 SW846 8260/5030 Vinyl Chloride < 0.010 0.01 mg/L 03/31/2020 SW846 8260/5030 Arsenic < 1.0 1 mg/L 04/07/2020 EPA 200.7 Barium < 1.0 1 mg/L 04/07/2020 EPA 200.7 Cadmium < 1.0 1 mg/L 04/07/2020 EPA 200.7 chromium < 1.0 1 mg/L 04/07/2020 EPA 2D0.7 Lead < 1.0 1 mg/L 04/07/2020 EPA 200.7 Selenium < 1.0 1 mg/L 04/07/2020 EPA 200.7 Silver < 1.0 1 mg/L 04/07/2020 EPA 200.7 Total Kieldahl Nitrogen 43,000 mg/Kg 03/28/2020 EPA 351.2 Phosphorus, total Sludge 34r400 mg/Kg 04/09/2020 SM 4500 P E Total Solids (u/o) 1.42 % 03/26/2020 SM 2540 G Zinc 118D mg/Kg 03/30/2020 EPA 200.7 Sample: NW Fecal # 1 N201324-02 (WW) 03/25/2020 08:35 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Fecal Density 1,159,421 MPN/9 03/25/2020 SM 9221C E MPN 24hr 503 Total Solids (°/u) 1.38 % 03/26/2020 SM 2540 G Sample: NW Fecal # 2 N201324-03 (WW) 03/25/2020 08:37 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Fetal Density 609,272 MPN/g 03/25/2020 5M 9221C E MPN 24hr 503 Total Solids (%) 1.51 % 03/26/2020 SM 2540 G The mMenrs of this nMtapply to the samples) analyzed in accordance WM dye chain ofcrstody document No dopfttron of this report is allowed, except In As enbrmory Page 4 of 8 ONWASA Northwest RWRF 189 Mills Field Rd. Richlands, NC 28574 Project: NW Solids Project Number: Project Manager: Mark Young Sample Results (Continued) Data Analyzed by: Environmental Chemists, Inc. Sample: NW Fecal # 3 N201324-04 (WW) 03/25/2020 08:38 Digestor Sludge Analyte Result Qual Fecal Density 874,317 Total Solids (Rro) 1.83 Sample: NW Fecal # 4 N201324-05 (WW) 03/25/2020 08:40 Digestor Sludge Analyte Result Qual Feral Density 1,134,752 Total Solids (%) 1.41 Sample: NW Fecal # 5 N201324-06 (WW) 03/25/2020 08:42 Digestor Sludge Analyte Result Qual Fecal Density 621,622 Total Solids (%) 1.48 Sample: NW Fecal # 6 N201324-07 (WW) 03/25/2020 08:43 Digestor Sludge Analyte Result Qual Fecal Density 1,095,891 Total Solids (%) 1.46 Sample: NW Fecal # 7 N201324-08 (WW) 03/25/2020 08:45 Digestor Sludge Analyte Result Qual Fecal Density 1,012,659 Total Solids (%) 1.58 Reporting Limit Units MPN/g Reporting Limit Units MPN/g Reporting Limit Units MPN/4 % Reporting Limit Units MPN/g Reporting Limit Units MPN/g Reported: 05/01/2020 14:17 Date Analyst Analyzed Initials Method 03/25/2020 SM 9221C E MPN 24hr 503 03/26/2020 SM 2540 G Date Analyst Analyzed Initials Method 03/25/2020 SM 9221C E MPN 24hr 503 03/26/2020 SM 2540 G Date Analyst Analyzed Initials Method 03/25/2020 SM 9221C E MAN 24hr 503 03/26/2020 SM 2540 G Date Analyst Analyzed Initials Method 03/Z5/2020 SM 9221C E MPN 24hr 503 03/26/2020 SM 2540 G Date Analyst Analyzed Initials Method 03/25/202o SM 9221C E MPN 24hr 503 03/26/2020 SM 2540 G The cantenks of this A*W apply to Me samples) analy2&1 in acmrdante with the drain ofcunvdy document No dupfttton of this report is allowed, eerept to iL enfirvoy Page 5 or s ONWASA Northwest RWRF 189 Mills Field Rd, Richlands, NC 28574 Project: NW Solids Project Number: Project Manager: Mark Young Notes and Definitions Item Definition Dry Sample results reported on a dry weight basis. ND Analyte NOT DETECTED at or above the reporting limit. Reported: 05/01/2020 14:17 The —MU& of drls +sportapply tome samples) analyzed In a='danw WI& the chain ofcustadp document No duplkRP67R offfils report isallowed, exceptfn Its entrrely. Page 6 of 8 u z r, m W a Z W 2 z 0 W z w 0 U z �i w w c7 > J � r h Q J z `r 1 J U I\ H3H10 ZZ mu C\`. HO"IV Q U � IX COMH -1 Lu (n w Y06LH �� 11 d 4. l7H 11 3NON aaewnN Ol Wri ■UP014D p cl T (E) J fay C? CL C7 ❑. C7 a 0 a_ 0 a (D a_ CD a. 0 a (D �eulc�uQ� j `�. _ 9Qi9 14 U 0 :..} C7 U Cl) 0 (D ( V (D U C7 ■il�adwo7 � •d�1 eldweg CL ~ O UJ U �C\ C O c 4� C � ` r CV CD U w C 3 i 1Z E H Q rr] N q Z z I E E :3 r, z s a 0 9 o` � x ,� I .m o z L o a U 'q rl Ln r\ rb O Ch LJ ro Ln fry L11 O Ln �•-1 V � O v � ru c -� ra C is 0 a Ln Ou N r0 C i 0 b � n j n 12 cr 7 G G n u c ,L G G b O Temp., deg. Celcius at collection Chlorine, mg/L at collection pH Units at collection Disolved Oxygen, mg/L ORP mg/L a 7 LZzG Ws Ai!suaa imi 7 J �c aT+ V o o H v _ . u 2 � 3 U V LL =` � n� U, vz' a arm0 e '" g C tio n z O z 6 6 Vi d C it C i� �J r J C C ' c iL u m o � _ a C � u b� a .--, u i3L'n U z =0 rn rl E ¢i 0 G E a 0 m u Cr o� u V E VI 4 0 0 4 0 0 0 o N O N O fV O N O N O N O N O a N N N N N N N Ln 0 Ln Ln Ln Ln L_m s o N m N rn N ran N ram» N m N rn N m a a ri N n'1 V' N LO r• � L = = 7t = 4 i V L9 V r0 V Id V n3 Li 16 V i6 V E L7LLLL M7 LL LL Lyyl L77L 7LL7 z z z z z z z E u n V CV V U u L LL O I -1� O O `7`7II b V 7 11 ,1 C. 4 y E E, 0 E F- 0 E F- 0 ^' G E ti c J � }_ G E r d a E O u Z j ¢ oc oc u O O Q ry Z Z �+ a .Environmental Chemists, Inc. 6602 Windmill Way, WiLinntgton, NC 28405 ° 910.392.0223 Lab ' 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilm.ington Highway, Jacksonville, NC 28540 • 91.0.347.5843 Lab/Fax itifo@environmentalchernists.com Onsiow Water & Sewer Authority Date of Report: Apr 20, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mark Young Report #: 2020-05012 Project ID: Northwest WRF Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12346 Site: 001 3/25/2020 8:35 AM Solid/Sludge Kary Herndon Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.38 % 03/26/2020 Fecal Density SM92210EMPN 24hr503 1159421 MPN1g 03/25/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12347 Site: 002 3/25/2020 8:37 AM Solid/Sludge Kary Herndon Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.51 % 03/26/2020 Fecal Density SM 9221C EMPN 24 hr 503 609272 MPN/g 03/25/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-12348 Site: 003 3/25/2020 8:38 AM Solid/Sludge Kary Herndon Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.83 % 03/26/2020 Fecal Density SM 9221C E MPN 24 hr 503 874317 MPN/g 03/25/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12349 Site: 004 3/25/2020 8:40 AM Solid/Sludge Kary Herndon Test Method Results Date Analyzed Total Solids (% Fecal Density Lab ID Sample ID: 20-12350 Site, 005 Test Total Solids (%) Fecal Density SM 2540 B SM 9221C E MPN 24 hr 503 Collect Date/Time 3/25/2020 8:42 AM Method SM 2540 B SM 9221 C E MPN 24 hr 503 1.41 % 03/26/2020 1134752 MPN/g 03/25/2020 Matrix Sampled by Solid/Sludge Kary Herndon Results Date Analyzed 1.48 % 03/26/2020 621622 MPN/g 03/25/2020 Report *;: 2020-05012 Page 1 of 5 5 �f-Unvironm.ental Chemists, hie. 6602 Windmill Way, Wilmington, NC 28405 ° 910-392.0223 Lab 6 910.392.4424 Fax 710 Bowsertown.Rood, Manteo, NC 27954 " 252-473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMIST'S info(a7environment.tichemists.com Onslow Water & Sewer Authority Date of Report: Apr 20, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mark Young Report #: 2020-05012 Project ID: Northwest WRF Lab 1D Sample ID: Collect DatefTime Matrix Sampled by 20-12351 Site: 006 3/25/2020 8:43 AM Solid/Sludge Kary Herndon Test Total Solids (%) Fecal Density Lab ID Sample ID: 20-12352 Site:007 Test Total Solids (%) Fecal Density Method Results Date Analyzed SM 2540 B 1.46 % 03/26/2020 SM 9221C E MPN 24 hr503 1095891 MPN/9 03/25/2020 Collect Date/Time Matrix Sampled by 3/25/2020 8:45 AM Solid/Sludge Kary Herndon Method Results Date Analyzed SM 2540 B 1.58 % 03/26/2020 SM 9221C E MP 24 hr 503 1012659 MPN/g 03/25/2020 Report #:: 2020-05012 Page 2of5 Onslow Water & Sewer Authority Date of Report: Apr 20, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mark Young Report #: 2020-05012 Project ID: Northwest WRF Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12353 Site: NW Digester 3/25/2020 8:30 AM Solid/Sludge Kary Herndon Test Method Results Date Analyzed Total Solids (%) SM 2540 8 1.42 % 03/26/2020 Chlordane (TCLP) SW 846 Method B081B13510 <0.02 mg/L 04/08/2020 Endrin (TCLP) SW 846 Method a0818/3510 <0.0005 mg/L 04/08/2020 Heptachlor (TCLP) SW 846 Method 8081B13510 <0.0005 mg/L 04/08/2020 Heptachlor epoxide (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 04/08/2020 Lindane (TCLP) SW 846 Method 8081 B1351 0 <0.0005 mg/L 04/08/2020 Methoxychlor (TCLP) SW 846 Method 8081BI3510 <0,0005 mg/L 04/08/2020 Toxaphene (TCLP) SW 846 Method 8061 B/3510 <0.05 mg/L 04/08/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 04/07/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 827or3510 <0.050 mg/L 04/07/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3610 <0.050 mg/L 04/07/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 827013510 <0.050 mg/L 04/07/2020 Cresol (TCLP) SW 846 method 827013510 0.985 mg/L 04/07/2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method B270/3510 <0.050 mg/L 04/07/2020 Hexachloro benzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2020 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2020 m f p-Cresol (TCLP) SW 846 method 8270/3510 0.985 mg/L 04/07/2020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2020 o-Cresol (TCLP) SW 846 method 8270/3510 <0, 050 mg/L 04/07/2020 Pentachlorophenoi (TCLP) SW 846 method 82701351a <0.250 mg/L 04/07/2020 Pyridine (TCLP) SW 846 method 8270/3510 <0,050 mg/L 04/07/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 04/09/2020 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 04/09/2020 1,1-Dichloroethylene (TCLP) SW846 Method826015030 <0.01 mg/L 03/31/2020 1,2-Dichloroethane (TCLP) SW846 Method826015030 <0.01 mg/L 03/31/2020 Benzene (TCLP) SW846 Method8260/5030 <0.01 mg/L 03/31/2020 Report #:: 2020�05012 Page 3 of 5 trn y �',F.+''�4a,F. f �'k•;q �.{ �.S��nj rrj'�+ YS=� F at��.roGhe ,�7{�L�3 Lc�r� gip& 3✓r �' a �,l ,." 'F:� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc® 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ? 910.392.4424 Fax 710 $owsertown Road, Manteo, NC 27954 O 252.473.5702 Lab/Fax 255-A Wilmington Highway, jacksorlville, NC 28540 ° 910.347.58431,ab/Pax inf'n c env iron men talchorn15ts.com Onslow Water & Sewer Authority Date of Report: Apr 20, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mark Young Report #: 2020-05012 Project ID: Northwest WRF Carbon Tetrachloride (TCLP) SW846 Method 8280/5030 <0.01 mg/L 03/31/2020 Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/31/2020 Chloroform (TCLP) SW846 Method8260/5030 <0.01 mg/L 03/31/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 03/31/2020 Tetrachloroethylene (TCLP) SW846 Method B26015030 <0.01 mg/L 03/31/2020 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/31/2020 Vinyl Chloride (TCLP) SW646 Method 8260/5030 <0.01 mg/L 03/3112020 Sludge Residuals Aluminum EPA 200.7 37700 mg/kg 03/30/2020 Arsenic EPA 200,7 <23.0 mg/kg 03/30/2020 Cadmium EPA 200.7 <23.0 mg/kg 03/30/2020 Calcium EPA 200.7 20500 mg/kg 03/30/2020 Chromium EPA 200.7 40.8mg/kg 03/30/2020 Copper EPA 200.7 356 mg/kg 03/30/2020 Lead EPA 200.7 <23.0 mg/kg 03/30/2020 Magnesium EPA 200.7 2080 mg/kg 03/30/2020 Molybdenum EPA 200.7 <23.0 mglkg 03/30/2020 Nickel EPA 200.7 <23.0 mg/kg 03/30/2020 Potassium EPA 2003 3560 mg/kg 03/30/2020 Selenium EPA 200.7 <23.0 mglkg 03/30/2020 Sodium EPA 200.7 7030mglkg 03/30/2020 Zinc EPA 200.7 1180 mg/kg 03/30/2020 Nitrate+Nitrite-Nitrogen EPA353.2 38.3mg/kg 04/06/2020 pN SM 4500 H B 6.75 units 04/02/2020 Ammonia Nitrogen SM 4500 NH3 C 1860 mg/kg 03/28/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 org a 43000 mg/kg 03/28/2020 Total Phosphorus SM 4500 P F 34400 mg/kg 04/09/2020 Mercury SW846 7471E <1.21 mg/kg 04/06/2020 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 04/07/2020 Report #:: 2020-05012 Page 4 of 5 t r ✓fir k tf�Hfr§ r F� r �' ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc® 6602 Windmill. Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473,5702 Lab/Fax 255-A Wilmvigton Highway, jacksonville, NC 28540 • 910.347.5843 Lab/Fax inro iDenvironmen talchemists,com Onslow Water & Sewer Authority Date of Report: Apr 20, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mark Young Report #' 2020-05012 Project ID: Northwest WRF Barium EPA 200.7 <1.0 mglL 04/07/2020 Cadmium EPA 200.7 <1.0 mglL 04/07/2020 Chromium EPA 200.7 <1.0 mg/L 04/07/2020 Lead EPA 200.7 <1.0 mg1L 04/07/2020 Selenium EPA 200.7 <1.0 mg1L 04/0712020 Silver EPA 200.7 <1.0 mg/L 04/07/2020 Mercury EPA 245.1 <0.0002 mg1L 04/07/2020 Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ; Report #:: 2020.05012 Page'5 of 5 Environrnental Chemist, Inc., Wilmington, NC Lab p94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client:. �2�o Date: Report Number - o f Receipt of sample: Delivered ❑ YES ❑ NO ❑ YES ❑ N/A UPS ClFedEx [] 17ther ❑ 1. Were custody seals present NO on the cooler? N/A 2. If custody seats were present, were they intact/unbroken? Original temure upon receipt perat�� 'C How temperature taken; CorrectI'lled temperature upon receipt ture Blank IR Gun ID: Thomas Traceable Against Bottles ��a� 5/M❑192511657 ❑ YES ❑ NO p IR Gun Correction Factor "C: 0.0 3. If temperature of cooler YES ❑ NO YES exceeded VC, was Project Mgr./qA notified? 4. Were proper Custody Y procedures {relinquished/received) ❑ NO YES ❑ followed? 5• Were sample iD s listed on the COC? NO YES ❑ NO 6. Were samples ID's listed on sample containers? 7. Were collection date and YES ❑ NO YES ❑ time li sted on the COC? 8. Were tests to be performed listed on the COC? NO YES ❑ NO 9. Did samples arrive in proper containers for each test? 10. Did samples arrive in YES ❑ NO YES good condition for each test? I. Was adequate sample volume available?' ❑ NO ❑ YES ❑ NO IZ. Were samples received withi proper holding time for requested tests? 13. Were acid preserved ❑ YES ❑ NO sampin 14.es received at a pH of <2? M Were cyanide samples ❑ YES ❑ NO received at a pH >12? 15. Were sulfide samples ❑ YES ❑ NO ❑ YES ❑ received at a pH >9? 16. Were NH3/TKN/Phenol received at a chlorine NO residual of <p,5 m/L? •* 17, Were Sulfide/Cyanide received at a chlorine residual of <p.5 m/L? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. '* Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed For by adding (circle one): any samples) incorrectly y preserved or with headspace) were received incorrectly preserved and were Time of preservation: adjusted accordingly I12504 HNO3 HCl NaOH If more than one preservative is needed, notate in comments below Nate: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Volatlles Who was notified, date and time: Sample(s) were received with headspace COMMENTS: 7-30C. QA.002 o tNt N 7 E U N O Z M U � O y 2 LT U} C � r E LL u m N e N y ? O C al 3 U w N C O LL La D N ti ry Z W � a.■ LL 0 ❑ O Z x x Q ❑ 2 z U rn 0 Z z Q o Z W d O U LL � w W LL! O � U rbr. Z U Z w N ❑ Lu i� wcm W V1 t!1 try a w © ❑ O H r (n ro ro z aUi m Chi ii u J t0 P1 p E m L a3Hla Z O owl X X X X X X X y( N aHOVN � EONH n w co LU COSZH v Q lOH 7 W 3NON it It 1)6u1 — auk�o3u� > ID ao d) aaukz�uo� w Q COD EL U rl (� d C7 0 d (7 a_ (� 0. (a CL L7 p C7 J 4. geJE) to o aaisoduio� U C7 U U 0. U COD U 0 U C7 adAl aldlueg Cn V3 rJ) GJ U7 U) (f} C 0 C L M �lco1C°.0I�,o silom 110-111 al O O O _ Lfj N N O p N N N O p N LC7 N N O p = Lo = N O N 0 N Lf] N N LO = Lf? N N O to t=[ N O N O N N C i`0. ` #kk# rq t`1 C to CO ti U C U dy LL U N LL U LL U LL U u LL [0 U L.L. l7 L7 Ld. (D E; tm O CDd ti U3 Q O ti N Q p q Q p Q V3 Q CD to Q CD r M CIa Q fn L. O y 0 Z d E w m t, fu o ,�9 �o u N a !x C di .C: 3 L � L � C L. CD C.E m .� O 04F- L3U ONWASA Laboratory 228 Georgetown Road Jacksonville NC 28540 (910) 389-8511 December 14, 2020 Mark Young Northwest RWRF 189 Mills Field Rd. Richlands, NC 28574 RE: NW Solids Enclosed are the results of analyses for samples received by our laboratory on 11/3/2020. If you have any questions concerning this report, please feel free to contact me. Sincerely, Todd A. Roberts For Mark Young Northwest ORC R ONWASA Northwest RWRF 189 Mills Field Rd. Richlands, NC 28574 Project: NW Solids Project Number: Project Manager: Mark Young Sample Results Sample: NW Digestor A N204501-01 (SL) 11/03/2020 07:30 Digestor Sludge Reported: 12/14/2020 10:49 Reporting Date Analyst Anafyte Result Qual Limit Units Analyzed Initials Method Temperature 23.7 deg C 11/03/2020 TAR SM 2550 8 Sample Results Data Analyzed by: Environmental Chemists, Inc. Sample: NW Digestor A N204501-01 (SL) 11/03/2020 07:30 Digestor Sludge Reporting Date Analyst Analyte Result Qual Limit Units Analyzed Initials Method Cyanide 2.03 0.025 mg/Kg 11/17/2020 EPA335.4 Ignitability > 200 F 11/12/2020 EPA 1030 PH 4.27 pH Units 11/05/2020 SM46 9045D Sulfide c 0.5 mg/Kg 11/10/2020 SM 4500 S D The cantents ofthis report apply to the sampkils) analyzed in accordance Kith the drain ara dtody doam=t. No dupgcayon of this repmt is allowed, except in & endmot Page 2 of 5 ONWASA Northwest RWRF 189 Mills Field Rd. Richlands, NC 28574 Item Definition Dry Sample results reported on a dry weight basis. Project: NW Solids Project Number: Project Manager: Marc Young Notes and Definitions ND Analyte NOT DETECTED at or above the reporting limit. Reported: 12/14/2020 10:49 The contenlr of tills reccrt apply M the sample(5)analyzed in acmvvance wNh the dialn afa9tody document No duplkabron ofyls report Is allowed, except in its entirety. Page 3 of 5 0 N O L Ln o c ® 0 ®G ct a nLn � 6' H a a�zo LI H �ry fJ1.iT Q [Ln L�61 7' M� [+'i fY77M y S6 e7 U O L f0 C •� 0 v •X N N N N NON 0 r6Q7 u K d Ct N n- E iSJ �NN � � G. [A\ NQQN 'b.i � - P�� 3 H of v -j�U7 r, to p�O C. r. , + rn 1� •�1p�O_O� .Q z O ,� -4-r J p�j d Ln L} u7 p CO q oo H 000c m o m F p '1 -4 �0 m w o Z co U oN o a mmIODvoo N vo o o ria4 P 6 0 0 6 000Q au C ri C ,-a 7 im 'ONa N N NNNN \ N N N N zzzz CL EO+Mi a C E-4-4 r-ii -ii 0 to Q 1 Ln Ln o o a a 4 a CD CD N Q V O L CD d O rt y Ln 00 m fw_'1 d1 C SA LL �Nm a ,�-r .. � 3 V a C' 73 M �� z 0 m E Z t M d -1 i m ! [a"IA C LL Q 111"' = Vi Ol 3 � 'O 7 a� ++ m id c.r c m S Q c Li v' SUM 1 Q. ' E ifs tD O � .i ?,"ZrL'i o yF� r Y: b C q� 7 ai w �' c ° �j Ln F"' � Q {Q M � ci ,, ,�, G o L aC a° E c y N n a et r+i z ,� a s U in U U cai a Q ii U w c Q. a �L.. Om O ro r�� fh _J Q. :. Ln M M U co r Q U i E D 0 N Ln +y'it rre ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28403 ° 910.392.0223 Lab O 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax info&nvironmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 20, 2020 226 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Report #: 2020-18650 Project ID: Northwest RWRF Sludge Lab ID Sample ID: Collect DateCfime Matrix Sampled by 20-47483 Site: Sludge 11/3/2020 7:30 AM Solid/Sludge Perry Parker Test Method Results Date Analyzed Cyanide pH RCI SM 4500 CH D SM 4500 H 6 Sulfide SM 450o S 0 Reporting limit elevated due to matrix interference. Ignitability SW 645 method 1010 Comment: �) Reviewed by-. 2.03 mg/kg 11/17/2020 4.27 units 11/05/2020 <0.5 mg/kg 11/1012020 >200 OF 11/12/2020 Report#.: 2020-18650 ?age 1 of 1 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: Date: l 3 Report Number:— f8�� Receipt of sample: ECHEM Pickup Client Delivery ❑ UP5 ❑ FedEx ❑ Other ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt 3 . �`'C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COU YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the CDC? YES ❑ NO & Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume availableT YES ❑ NO I) Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >97 ❑ YES ❑ NO I 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** b YES ❑ NO 117. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded an the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately For incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA,002 Rev 1 'C h yti\ CHWASA Sending Facility: Northwest WRF 189 Mills Field Road Richlands, NC 28574 Phone: 910.937.7570 Project Manager: Mark Young Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Work Order: N204501 Northwest RWRF Subcontracted Laboratory: SUBCONTRACT ORDER Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax: (910) 392-4424 NCDENR: DWQ CIRTIFICATION / 94 NCDHHS: DLS CER71FIC 170H a 1777r Sample ID: N204501-01 NW Digestor A Digestor Sludge SL Sampled.- 1X19312020 07:30 S�rmpfed by, PerryP rker Analysis Due Expires EnviroChem Lab ID PH,5W846 11/13/2020 11/03/2020 07:47 Analysis Due Expires EmlroChem Lab ID 5uffide eolorimetric 11/13/2020 11/17/2020 07:30 L.Lnatysis Due Expires EnvlroChem Lab ID Cn- 335.4 11/13/2020 11/17/2020 07:30 Analysis Due Expires EnvlroChem Lab ID lgnita611ity 1030 11/13/2020 12/01/2020 07:30 Con tafners Supplied.- A 1 liter (6) y�y0 3 EnvlroChem Report No: Relinquished By Date R Kiveo Date Page I of 1 ':5� 1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WWTP name. Northwest Regional WRF Monitoring Period: From 1/1/2020 To WQ Permit Number: NPDES Number- 12/31/2020 WQ0034806 W Q0034367 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B {Alk Treatment) ❑ 1 Alt. C (Prior Testin a) ❑ A1tD (No Prior Test) E] Process to Fut1her Reduce Patliogenos ❑ Tf applicable to alternative performed (Class A only.) indicate"Process to Fuither Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ ThennnophiIic ❑ Beta Ray ❑ Garimia Ray ❑ Pasteurization ❑ Class S: Alt- (1) Fecal Density [( Alt (?) Process to Sigilificantly Reduce Pathogens p If applicable to alternative performed (Chris B only) indicate "Process to Significantly Reduce Pathogens": Lithe Stabilization ❑ Air Drying ❑ Com ostin� i`; Aerobic Digestion ❑ Anaerobic Digestion Cl Y If applicable to alternative performed (Class A or Class B) complete the fallowing monitoring data: Allowable Level Pathogen Density aim era natyvca Parameter Excee- Frequency Sample Tech- Minimurr Geo. Ml can klaximu Units Ce of Analysis Type i le 2 x 10 to the NIPNi 609,2 72 901,387 1 159,42I 6th power 1vIPN/g 0 Annual Grab SM92210E per gram of Fecal Coliform total solids CPU 1000 mpn per grarn of total solid (dry Salmonella bacteria 3 MPN per4 grams (in lieu of fecal total solid (dry coli£orm) weight) Vector Attraction Reduction 05A NCAC 02T .1107) - Please indicate alternative performed: Alt.! (VS reduction) ❑ I Alt. 2 (40-day bench) C Alt. 3 (30-day bench) ❑ JAR. 4 (Spec. 0, uptake) [] Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (Alk, Stabilization ❑ Alt 7 (Drying - Stable) 0 1 Alt. 8 (Drying - Unstable) s 1 Alt. 9 (Injection) 71 1 3.1t. 30 (incorporation) i,-t No vector attraction reduction alternatives were performed 1-1 CERTIFICATION STa,TEN11;NT (please cheek the appropriate statement) El `°I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attractions reduction requirement in 1.5A NCAC 02T .1107 have been met," G "I certify, gander penalty of law, that the pathogen requirements in 15A NCAC 02T ,1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "'Phis determination has been made under my direction and supervision in accordance with the system designed to erasure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." iklark Young, ORC Wesley Wooten, President Preparer�+Tame and Titll (type or print) Land Applier Name and Title (if applicable)(type or print) 12/14/20 tg�a' re of Prep e Date Signature of L d Applier (if applicable) Date "Preparer is deli=40 CFR Part 503.9 r and 15A NCAC 2T .1102 26 DENR FORM PVRF 02T (1212006) COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: June 18, 2020 Oak Island WWTP Permit No. WQ0005790 7.26 % Solids 7.11 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton 0.002) Nitrogen (TKN) 4,330 43,300.000 86.600 Phosphorus 1.020 10,200.000 20.400 Potassium 0.142 1,420.000 2.840 PAN (injected)* 1.590 15,901.200 31.802 PAN (surface)* 1.385 13,846.200 27.692 Ammonia Nitrogen 0.411 4,110.000 8.220 Calcium 3.250 32,500.000 65.000 Calcium Carbonate E . --- -- Magnesium - 3,860.000 7.720 Sodium --- 4,330.000 8.660 Sulfur i`litrate N I Nitrite N -- za inn n ntie Barium --- --- --- SAR Chloride --- --- --- 1.63 Iron -- -- - Ceiling Concen. Aluminum --- 3,640.00 7.280 (Mg/Kg) Arsenic --- 16.10 0.032 75 Cadmium Chromium --- --- 6.89 18.700 0.014 0.037 85 --- Copper --- 566.00 1.132 4,300 Lead --- 31.50 0.063 840 Mercury --- 1.33 0.003 57 Molybdenum --- 6.89 0.0I4 75 Nickel --- 13.10 0.026 420 Selenium --- 6.89 0.014 100 Zinc --- 798,00 1.596 7,500 Environmental Chemists# 2020-10050 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) +Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Oak Island WWTP 1?. .g.. 06/18/20 576 2.7604 06/18/20 590 2.7709 06/18/20 258 2.4116 06/18/20 590 2.7709 06/18/20 278 2.4440 06/18/20 1,002 3.0009 06/18/20 609 2.7846 Total 18.9433 Average 2.7062 Geometric Mean0$ Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. s' Environmental. Chemists, Inc. " 9 6602 Windmill Way, Wilmington, NC 28405 > 910.392.0223 Lab u 9"10.392.4424 Fax L Mj 710 $owsertown Road, Manteo, NC 27954 s 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@,environmencalchemists.coni Lewis Farms & Liquid Waste, INC. Date of Report: Jul 07, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-10050 Project ID: sludge LabID Sample ID: Collect Date/Time Matrix Sampled by 20-25126 Site: Sludge 5 6/18/2020 8:40 AM SolidlSludge Wooten Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 3640 mg/kg 07/02/2020 Arsenic EPA 200.7 16.1 mg/kg 07/02/2020 Cadmium EPA 200.7 <6.89 mg/kg 07/02/2020 Calcium EPA 200.7 32500 mg/kg 07/02/2020 Chromium EPA200.7 18.7mglkg 07/02/2020 Copper EPA 200.7 566 mg/kg 07/02/2020 Lead EPA 200.7 31.5 mg/kg 07/02/2020 Magnesium EPA 200.7 3860 mg/kg 07/02/2020 Molybdenum EPA 200.7 <6.89 mg/kg 07/02/2020 Nickel EPA200.7 13.1 mg/kg 07/02/2020 Potassium EPA 200.7 1420 mg/kg 07/02/2020 Selenium EPA 200.7 <6.89 mg/kg 07/02/2020 Sodium EPA 200.7 4330 mg/kg 07/02/2020 Zinc EPA 200.7 798 mg/kg 07/02/2020 Total Kjeldahl Nitrogen (TKN) EPA351.2 43300mg/kg 07/01/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 34,2 mg/kg 06/30/2020 Total Solids (%} SM 2540 8 7.26 % 06/18/2020 pH SM 4500 H a 7.11 units 06/22/2020 Ammonia Nitrogen SM 4500 NH3 C 4110 mg/kg 06/23/2020 Total Phosphorus sM4500 P F 10200 mg/kg 06/25/2020 Mercury SW046 74713 1.33 mg/kg 06/25/2020 Report C 2020-10050 " Page 1 of 3 Lewis Farms & Liquid Waste, INC. Date of Report: Jul 07, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-10050 Project ID: sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-25127 Site: 1 6/18/2020 8:41 AM SolidlSludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 7.82 % 06/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 576 MPN/g 06/18/2020 Lab lD Sample ID: Collect Date/Time Matrix Sampled by 20-25128 Site: 2 6/18/2020 8:42 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (°1°) SM 2540 8 7.64 % 06/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 590 MPN/g 0611812020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-25129 Site: 3 6/18/2020 8:43 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 7.77 % 06/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 258 MPN/g 06/18/2020 Lab lD Sample ID: Collect Date/Time Matrix Sampled by 20-25130 Site: 4 6/18/2020 8:44 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 254013 7.64 % 06/18/2020 Fecal Density SM92210EMPN 24hr5o3 590MPN/g 06/18/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-25131 Site: 5 6/18/2020 8:45 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 7.22 % 06/18/2020 Fecal Density SM 9221 C E MPN 24 hr 503 278 MPN/g 06/18/2020 Report AL:: 2020-10050 Page 2 of 3 Lewis Farms & Liquid Waste, INC. Date of Report: Jul 07, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-10060 Project ID: sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-25132 Site: 6 6/18/2020 8:46 AM SolidlSludge Wooten Test Method Results Date Analyzed Total Solids (%} SM 2540 B 7.79 % 06/18/2020 Fecal Density SM 9221C E MP 24 hr503 1002 MPNlg 06/18/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-25133 Site: 7 6/18/2020 8:47 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids SM 2540 B 7.39 % 06/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 609 MPN/g 06/18/2020 Comment: Sludge residuals and fecal density reported on a dry weight basis, pH reported on an as received basis. Reviewed by: R ill Report #: 2020-10050 Page 3 of 3 - LO cm N N T Z M o p 0 CO cm Eu, m M s N d N, e r > c U (D o L o w O S r+, F- Z Z z a W 1L I i W � z U 00 I o I z 93 0 zU z W �n 0 z a z a Q !L D CL 'a w G L! aid) O .n w � tl7 � 4J LIJ 14 a � a z z o 0 w ¢ w Q m 0 w O a V [C U m �C E ii O! N w U 4 _N Lv A m m v U) 2 u, a 'D 3 m Q I L G p rn a z U } w q Sn C v] C N C (n C (!1 C N C N C Q) 0 O 0 0 v°, ~ U co U U co co U E LL LL LL LL LL I LL LL LL a�1�ua N 11 Z 01H1 X X X X X x X �- o i- HOaN > 4 m 3 eONH 47 ct II EU w roOS�H C. SOH 7 w MON X u e-\ C 01 ovi II -lrBw _ auliol9oUl Q yA F- eaJO u eiuo} IL C'3 IL (D cr) Q (D 0 C7 IL C7 n C7 d (} uj ,LL a IL geaC a W aalsodwoo adA.L oldweg M E m +v N C 3 D Q C CD O PAO � IA l Lasl �j no � E � � Q u� -A—ANUA-LIP-A-TI1.06E-N.A�L4DV-E-CT-0.R-.&T.TRAC-17.0-N-R.-MU�C-.T,IONF0,R-M'(,, T WdRes als,'ILDC 'Oak I �Rad W�WTP 'WQ003'1806 NPDW Numb WQOOOSWO MonitoringPerio Fro]* In12020- To: 12W2 Pathogen Reduction (tiSA N-GAC 02TA10 -t performed:: .61-01P.asq�qdl foig: ,04 v�j 4440.0.4 iLitd 01(prh;# ve 0 Class AA: I Alt- A ftlmeftemn),- M' I A U-n Prior M Patameter in Sludge Fecal 0 om eca. mouln Ci a lieu off=[ total solid<(ary. UtWi:redfttiori) -M 5,:(S-Diay.Aei:biv,) 0 IAIL fa t 0 k.. u r th dr., PN 7. ,(2,.'Process tcj 'fieamdy-'Redu C OM osfing fl or hogenba"nsity- um erj I 78 .508 1,002 -WHIR .1107.) ?-dayr beach 0 cf. .Amuta i - Grab CqWyi uWdOr"PeKWJ . fY df JiLw., Mttth-Q-pafftbgen reqplremeub MTSAI NCAIC WOW and idi6 V-PfUr A*-IkciO!QIt rettefion ke-Wriim,oh.t.ja ISA NCAC 02T.-I-10.7, have -been met ?t Oquirerapijuin ISAMAC- 02TA106.and the. jphjk 16, _C vector attracdon reduction NeA rOZT _A 4107 hovrenot bjein. mu.p� (nease note ,if Yod &eikthis, statement gttac I1.qj(e4-jaigj . i .01i h2vP 'tmigt-due iikr moth On Wh.Y�Y of dmeft4ed toensure4hat palifie 4 pers ongelro. pwygothor "vvAjVate ihkjnfbkWkGOjAsid to determinethat flair fAthugem andvector attraefton'rodiqc9;u:reqxjr-eIneu4 havejgeu IneL f= awareffiatlherO significant p�iiialtiet.��,fti.r,fakd,certMeation. iudixdjug-4q�,-and I -are pris Mark Mom, OR-C r., yae' d Title- (typd, 6r �Lwd Applier Name -qnd.Tjae FrWaie N (if applleabFe) , (hype or prinj) 1 .20 D�fe- .771 ii�aturulof-La LAjp�(;r (if appfiCabje) pate Vrepareris'deft-Wift-40 UkF'artS03-9(r)IW OA NQAQ-2T AIR, (2:6) or=NRFbRM RVRF o2T(I212oor, COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 15, 2020 Pluris Hampstead WWTF Permit No. WQ0037287 1.84 % Solids 7.18 pH Parameter % Mg/Kg Dry Weightl (% x 10,000) Pounds/Dry Ton (MR/K9 x 0.002) Nitrogen (TKN) 5.600 56,000,000 112.000 Phosphorus 2.690 26,900,000 53.800 Potassium 0.432 4,320.000 8,640 PAN injected)* 1.988 19,875.800 39.752 PAN (surface)* 1.769 17,690.800 35.382 Ammonia Nitrogen 0.437 4,370.000 8.740 Calcium 4.300 43,000.000 86.000 Calcium Carbonate E . --- --- Magnesium --- 3,920.000 7.840 Sodium --- 10,300.000 20.600 Sulfur ___ -__ --- Nitrate N / Nitrite N --- 16.800 0.034 Barium Chloride --- --- --- --- --- --- SAR 1.73 Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 4,670.00 9.340 Arsenic --- 31.30 0.063 75 Cadmium --- 25.70 0.051 85 Chromium --- 25.700 0.051 -- Copper --- 465.00 0.930 4,300 Lead --- 25.70 0.051 840 Mercury --- 0.87 0.002 57 Molybdenum --- 25.70 0.051 75 Nickel --- 25.70 0.051 420 Selenium --- 25.70 0.051 100 Zinc --- 3,450.00 6.900 7,500 Environmental Chemists # 2020-17642 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Pluris Hampstead WWTF 10/15/20 1,949 3.2898 10/15/20 1,800 3.2553 10/15/20 1,516 3.1807 10/15/20 712 2.8525 10/15/20 720 2.8573 10/15/20 800 2.9031 10/15/20 910 2.9590 Total 21.2977 Average 1 3.0425 Geometric Mean I L3 I Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. '` �:��'#�'�•`•� sus ANALYTICAL 1£ CONSULTING CHEMISTS Lewis Farms & Liquid Waste, INC. 6155 Malpass Corner Road Currie NC 28435 Attention: Wesley Wooten Lab ID Sample ID: 20-45086 Site: Sludge Test pH Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc Nitrate+Nitrite-Nitrogen Total Solids (%) Ammonia Nitrogen Total Kieldahl Nitrogen (TKN) Total Phosphorus Mercury Finvironmental Chemists, Inca 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab o 910.392.4424 Fax 710 Sowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@cnvironmentalchemists.com Date of Report: Nov 18, 2020 Customer PO #: Customer ID: 14020008 Report #: 2020-17642 Project ID: Pluris-Hampstead Collect Date/Time Matrix 10/15/2020 8:00 AM Solid/Sludge Method SW 045 Method 9045D EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 200.7 EPA 353.2 SM 2540 B SM 4500 NH3 C SM 4500 Crg 8 $M4500PF SW046 7471a Results Sampled by Wooten Date Analyzed 7.18 units 11/17/2020 4670 mglkg 10/20/2020 31.3 mglkg 10/2012020 <25.7 mg/kg 10/20/2020 43000 mglkg 10/20/2020 <25.7 mg/kg 10/20/2020 465 mglkg 10/20/2020 <25,7 mg/kg 10/20/2020 3920 mglkg 10/20/2020 <25.7 mg/kg 10/20/2020 <25.7 mg/kg 10120/2020 4320 mglkg 10/20/2020 <25.7 mg/kg 10/20/2020 10300 mglkg 10/20/2020 3450 mg/kg 10/20/2020 16.8 mg/kg 10/15/2020 1.84 % 10/15/2020 4370 mglkg 10/19/2020 56000 mg/kg 10/19/2020 26900 mg/kg 10/21/2020 <0.870 mg/kg 10/3012020 Report #:: 2020.17542 Page 1 of 3 A a e. a .ice '�� 1�3. ,s>, �;;•;;-.- i§M ANALYTICAL & CONSULTING CHEMISTS 10 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 i 910.392.0223 Lab V 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax inFo@environrnentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report: Nov 18, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-17642 Project ID: Pluris-Hampstead Lab ID Sample ID, Collect Date/Time Matrix Sampled by 20-45087 Site: 1 10/15/2020 8:01 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.31 % 10/15/2020 Fecal Density SM 9221C E MPN 24 hr 503 1949 MPN/g 10/15/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-45088 Site: 2 10/15/2020 8:02 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 s 2.50 % 10/15/2020 Fecal Density SM 9221C E MPN 24 hr 503 1800 MPN/g 10/15/2020 Lab ID Sample ID: Collect DatefTime Matrix Sampled by 20-45089 Site: 3 10/15/2020 8:03 AM Solid/Sludge Wooten Test Total Solids (%) Fecal Density Lab ID Sample ID: 20-45090 Site:4 Test Method Results Date Analyzed SM 2540 a 2-64 % 10/15/2020 SM 9221C E MPN 24 hr 503 1516 MPN/9 10/15/2020 Collect Date/Time Matrix Sampled by 10/15/2020 8:04 AM Solid/Sludge Wooten Method Results Date Analyzed Total Solids (%) SM 2540 8 2.53 % 10/15/2020 Fecal Density SM92210EMPN 24hr503 <712MPN/g 10/15/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-45091 Site: 5 10/15/2020 8:05 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 8 2.50 % 10/15/2020 Fecal Density SM 9221C E MPN 24 hr 503 <720 MPN1g 10/15/2020 Report N.: 2020-17642 Page 2 of 3 y �!• h s ��i3V q��b-tCtil�y-ly,rtL [ ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Lewis Farms & Liquid Waste, INC. Date of Report-, Nov 18, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-17642 Project ID: Pluris-Hampstead Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-45092 Site: 6 10/15/2020 8:06 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%} SM 2540 9 2.50 % 10/15/2020 Fecal Density SM 9221C E MPN 24 hr 503 800 MPNlg 10/15/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-45093 Site: 7 10/15/2020 8:07 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 6 2.20 % 10/15/2020 Fecal Density SM 9221 C E MP N 24 hr 503 910MPN/g 10/15/2020 Comment: Sludge residuals and fecal density reported on a dry weight basis. pig reported on an as received basis. Reviewed by: C/ , Report #:: 2020-17642 Page 3 of 3 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392,0223 f Sample Receipt Checklist Client: L Ewi*, a 1z-m5 Date: t 1� Report Number- ^ J —710 Receipt of sampie: ECHEM Pickup M Client Delivery ❑ UPS ❑ FedEx ❑ Other ❑ YES ❑ NO 4 N/A 1. Were custody seals present on the cooler? ❑ YES 10 NO N/A 12. If custody seals were present, were they intact/unbroken? temperature upon receipt °C Corrected temperature upon receipt 1Original How temperature taken: ❑ Temperature Blank V Against Bottles 1R Gun ID: Thomas Traceable S/N 192511657 iR Gun Correction Factor °C: 0.0 ❑ YES ❑ ND 3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COO qZ YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YE5 ❑ NO 8. Were tests to be performed listed an the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 110. Did samples arrive in good condition for each test? YES ID NO 111. Was adequate sample volume avallable?' YES ❑ NO 112. Were samples received within proper holding time for requested tests? ❑ YES I ❑ NO 113. Were acid preserved samples received at a pH of <2? ❑ YES 10 NO 114. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** I7 YES f❑ ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YE5 ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatifes are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. mple Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 °C � N N4 u E c c 0 yrn�� 2 E LL m t N !9 N y °i E 0 E o c L WCD m w w O c — G I. - re m W" a z Ja z a-�r m F— z z Z O Wa U (E) JC d) 1aule4uo3 CL a t7 [L Ldo- C7 o_1011L a (� a (� u� IL q-E) Q 10 L) 0 a 0U ( U (D ( U C7 U ti C] (7 c a��sodmo� ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name, Coastal Farms and Residuals, LLC WWTP Name: Pluris Hampstead W WTF Monitoring Period: From 1/l/2020 To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative perfor Class A; Alt. A (tinlehenlp) ❑ 1 Alt B (Alit Treatinent) ❑ I Alt. C (Prior Testing) ❑ AIt.D (No Prior Test) ❑ I Process to Further Reduce PaEhogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost q_F Heat Drying ❑ Hent Treatment ❑ Thenuophilic ❑ Beta Ray ❑ Ganuna Ray ❑ Pasteurization ❑ ,.._,.....`;"".,' Class B: llicable to alternative performed Stabilization ❑ robic Digestion 5t1oR Iicable to alternative rnative nerforrr Parameter Allowable Level in Sludge 2 x 10 to the MpN 6th power per gram of CFU Fecal Coliform total solids 1 uvv mpn per gram of total solid {dry uIJIVIKcuu URULt a j iviriv per q grams (in lieu of fecal I total solid (dry WQ Permit Number: WQ0034806 NPDES Number: WQ0037287 12/31/2020 tLY El j_ Alt. (2) Process to Sigllificaal (Chtss B only) indicate "Process to Sign Air Drying ❑ ColnLas tiI ed (Class A or Class B) complete the Pathogen Density nimumj Geo. MeanlMaximunj Units Reduce Pathogens ❑ T aptly Reduce Pathogens": ❑ JAerobic Digestion ❑ Ilowing monitoring data: urricierorlFrequency Sample na is dences of Analysis Type Tech- nirnpe 712 I 1,103 I 1,949 1 MPN/g 1 0 1 Annual I Grab ISM92210E Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed; Alt. 1(VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) 111 Alt. 4 (Spec. 02 uptake) ❑ Alt, 5 (14-Day Aerobic) ❑ AIt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt, 9 (Injection) l7 Alt. 10 (Incorporation) MM No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and tile vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met," (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment," Randy Hoffer, ORC Wesley Wooten, President Preparer Name and Titte,(type,or print) Land Applier Name anndd� Title (if applicable)(type or print) Zt,if/.✓ 11/30/20 Sign 4Li:e of Prepares'" � Dafe Signature of Lan Applies (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 9, 2020 Southeast Brunswick Sanitary District WWTP Permit No. WQ0013200 2.53 % Solids 7.36 pH Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002) Nitrogen (TKN) 5.300 53,000.000 106.000 Phosphorus 2.070 20,700.000 41.400 Potassium 0.337 3,370.000 6.74011 PAN (injected)* 2.365 23,649.000 47.298 PAN (surface)* 1.820 18,199.000 36.398 Ammonia Nitrogen 1.090 10,900.000 21.800 Calcium 2.700 27,000.000 54,000 Calcium Carbonate E . --- --- --- Magnesium - 4,110.000 8.220 Sodium --- 2,380,000 4.760 Sulfur --- --- Nitrate N / Nitrite N --- 119.000 0.238 Barium Chloride --- --- --- --- --- --- SAR 0.57 Iron _-- --- --- Ceiling Concen. MgtK ) Aluminum --- 19,200.00 38.400 Arsenic --- 10.50 0.021 75 Cadmium --- 10.50 0.021 85 Chromium - 41.100 --- — Copper --- 320.00 0.640 4,300 Lead --- 10.90 0.022 840 Mercury --- 0.601 0.001 57 Molybdenum --- 10.50 0.021 75 Nickel --- 20.70 0.041 420 Selenium --- 1 10.50 0.021 100 Zinc --- 771.00 1.542 7,500 Environmental Chemists 4 2020-03979 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. p ` , XMvir®nmental Chemists, Ines •r ° 6602 Windmill Way, Wilmvlgton, NC 28405 e 910.392.0223 Lab e 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 Y 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS infoCwenvir Y onnlenta]c1lemists.com Southeast Brunswick Sanitary District Date of Report: Apr 08, 2020 4350 Sea Pine drive Customer PO #: Southport NC 28461 Customer ID: 09060039 Attention: Bryan McCabe, PE Report #: 2020-03979 Project ID: Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-09689 Site: Sludge 3/9/2020 1:00 PM Solid/Sludge client Test Method Results Date Analyzed Chlordane (TCLP) SW B4B Method 8081813510 <0.02 mg/L 03/19/2020 Endrin (TCLP) SW 846 Method 8081B13510 <0,0005 mg/L 03/19/2020 Heptachlor (TCLP) SW 846 Method 8081B18510 <0.0005 mg/L 03/19/2020 Heptachlor epoxide (TCLP) SW846 Method 6061B13510 <0.0005 mg/L 03/19/2020 Lindane (TCLP) SW 845 Method 8081 W351 0 <0,0005 mg1L 03/19/2020 Methoxychlor (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 03/19/2020 Toxaphene (TCLP) SW 846 Method 8061B13510 <0.05 mg/L 03/19/2020 1,4-Dichlorobenzene (TCLP) SW 846 method e27013510 <0.050 mg/L 03/20/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 827013510 <Q.050 mg/L 03/20/2020 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 Hexachlaro-1,3-butadiene (TCLP) SW 846 method 827413510 <0.050 mg/L 03/20/2020 Hexachlarobenzene (TCLP) SW 846 method 827013510 <0.050 mg1L 03/20/2020 Hexachioroethane (TCLP) SW 845 method 8270/3510 <0.050 mg/L 03/20/2020 rn + p-Cresol (TCLP) SW 846 method 827013,510 <0.050 mg/L 03/20/2020 Nitrobenzene (TCLP) SW 646 method 6270/3510 <0,050 mg/L 03/20/2020 o-Cresol (TCLP) SW 846 method 821013510 <0.050 mg/L 03/20/2020 Pentachlorophenol (TCLP) SW 646 method 827013510 <0.250 mg/L 03/20/2020 Pyridine (TCLP) SW 846 method 827013510 <0.050 mg/L 03/20/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 03/20/2020 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 03/20/2020 1,1-Dichloroethylene (TCLP) SW646 Method 826015030 <0.01 mg/L 03/25/2020 1,2-Dichloroethane (TCLP) SW846 Method 826015030 <0.01 mg/L 03/25/2020 Benzene (TCLP) SW846 Method 820015030 <0.01 mg/L 03/25/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/6030 <0,01 mg/L 03/25/2020 Report A.: 2020-03979 Page 1 of 3 Environmental Chemists, Inc. 11 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab C 910.392.4424.Fax 710 $owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 Y 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info t environnientalchemists.com Southeast Brunswick Sanitary District Date of Report: Apr 08, 2020 4350 Sea Pine Drive Customer PO #: Southport NC 28461 Customer ID: 09060039 Attention: Bryan McCabe, PE Report #: 2020-03979 Project ID: Sludge Chlorobenzene (TCLP) SW848 Method 6260/5030 <0.01 mg/L 03/25/2020 Chloroform (TCLP) SW646 Method 8260/5030 <0.01 mg/L 03/25/2020 Methyl ethyl ketone (TCLP) SW646 Method 8260/5030 <0.05 mg/L 03/25/2020 Tetrachloroethylene (TCLP) SW046 Method 820015030 <0.01 mg/L 03/25/2020 Trichloroethylene (TCLP) SWe46 Method 826015030 <0.01 mg1L 03/25/2020 Vinyl Chloride (TCLP) SW846 Method 6260/5030 <0.01 mg/L 03/25/2020 RCI Cyanide EPA 335.4 0.069 mg/kg 03/18/2020 Sulfide SM 4500 S Q 0.92 mglkg 03/31 /2020 Ignitability SW 846 method i010 >190 7 03/31/2020 pH SW 846 Method 90451) 7.36 units 04/02/2020 Sludge Residuals Aluminum EPA 200.7 19200 mg/kg 03/12/2020 Arsenic EPA 200.7 <10.5 mglkg 0311212020 Cadmium EPA 200.7 <10.5 mglkg 03/12/2020 Calcium EPA 200.7 27000mg/kg 0311212020 Chromium EPA 200.7 41.1 mg/kg 03/12/2020 Copper EPA 200.7 320 mglkg 03/12/2020 Lead EPA200.7 10.9 mglkg 03/12/2020 Magnesium EPA 2001 4110 mg/kg 03/12/2020 Molybdenum EPA 200.7 <10.5 mglkg 03/12/2020 Nickel EPA 200.7 20.7 mg/kg 03112/2020 Potassium EPA 200.7 3370mg/kg 03/16/2020 Selenium EPA200,7 <10.5mg/kg 03/12/2020 Sodium EPA 200.7 2380 mg/kg 03116/2020 Zinc EPA 200.7 771 mglkg 03/12/2020 Nitrate+ Nitrite -Nitrogen EPA353.2 119mg/kg 03/19/2020 Total Solids !.%-, 1 • SM 254o 8 9,53 Q7C 0311?l2Q2r► Ammonia Nitrogen SM 4500 NH3 C 10900 mglkg 0311512020 Total Kjeldahl Nitrogen (TKN) SM 4500 arg a 53000 mg/kg 03/15/2020 Report #:: 2020.03979 Page 2 of 3 Environmental Chemists, Inc. ® 6602 Windmill Way, Wilmington, NC 28405 s 910.392.0223 Lab c 910,392.4424 Fax rM1 710 Bowsertown Road, lvlanteo, NC 27954 u 252.473.5702 Lab/lax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Southeast Brunswick Sanitary District Date of Report: Apr 08, 2020 4350 Sea Pine Drive Customer PO #: Southport NC 28461 Customer ID: 09060039 Attention: Bryan McCabe, PE Report #: 2020-03979 Project ID: Sludge Total Phosphorus SM 4500 P F 20700 mg/kg 03/20/2020 Mercury SW8467471B <0.601 mg/kg 0311312020 TCLP Metals Arsenic EPA200.1 <1.0 mg/L 03/19/2020 Barium EPA 200.7 <1.0 mg/L 03/19/2020 Cadmium EPA 200.7 <1.0 mg1L 03/19/2020 Chromium EPA 200.7 <1.0mg/L 03/19/2020 Lead EPA 200.7 <1.0 mg1L 03/19/2020 Selenium EPA200.7 <1.0mg/L 03/19/2020 Silver EPA 200.7 <1.0 mg1L 03/19/2020 Mercury EPA 245A <0.0002 mg/L 03/19/2020 Comment: Sludge residual results reported on dry weight basis. Reviewed by: -PIA . , , Report #.: 2020-03979 c Page 3 of 3 Enviranmentar Chemist, Inc., Wilmington, NC Lab i#94 6602 Windmill Way Wilmington, NC 28405 910,392.0223 Sample Receipt Checklist Client: Receipt Dater Report Number - of sampie. YES ❑ NO 13 YES Delivered UPS ❑ FedEx ElOther ❑ N/A 1• Were custody ❑ seals present an the c NO N/A 2. !f custody seals were Originalpresent, were riginal temperature open receipt they intact/unbroken? 5 ,_C Haw temperature taken: Corrected temperature upon receipt oC IR Gun ID: hoBlank Tmas Traceable 5/a1g25 1557ture Against Bottles ❑ YES ❑ NO Gun rwas YES © NO 0 3. If temperature of cooierlexceeded 6'C,R I YES ❑ NO Pra'ett M 4• Were proper Gusto 1 gr / notifred? dy procedures (rellnquished/received) YES ❑ NO p followed? S. Were sample Ip s listed an the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? 7• W ere collection date YES ❑ NO and time fisted on the COc? S. Were tests to be YES❑ NO performed listed on the COC? g• Did samples arrive in YES Q NO YES ❑ proper containers 10. Dld samples arrifor each test? ve in good condition NO YES❑ NO for each test? 11. Was adequate sampie volume available?' ❑ YES ❑ NO 12• Were samples received within proper holding time for requested 13• Were acid q sled tests? ❑ YES ❑ NO ❑ YES preserved Samples received at a PH of �2? 14. Were cyanide samples received P ❑ NO ❑ YES ❑ NO at a pH �12? 16 Were sulfide samples received at a pH ;g? ❑ ❑ yES NO 16, Were NFi3/7KN/Phenol received at a chlorine residual of <0.5 mIL? •• 17. Were Sulfede/Cyanide received at a chlorine residual of 0,5 MIL? TOC/Valatlles are pH checked at tfine of analysis and recorded on the benchsheet. ' « Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsh Sample Preservatl in: Bet (Must be completed for sampie{s j any samplejsj incorrectly preserved by adding l3 {circle one): or with headspace were received incorrectly preserved and were adjusted H250< HNOj Time of preservation: HCl accordingly NaOH Note: Trot; fy customer service immediately If more than one preservative is needed, notate in Com for incorr�ly preserved menu notify the state lab if directed to below samples. Obtain a new sam anatyxed b n nie or Y the customer, Who Volatiles sample(s) was notified, date and timer vere received with headspace COMMENTS: ,: A.002 §z I01 �nr1�7I I 1 E 7 I , O 0 iu y T� Ih a "' ��� r N e� � N } C ` T. 1 Q c} `� d all) go o �. ) 0 Q O Z Z O ca `0 a3Nlo U w 17[ O R. a � � rr z orrli oa EDNH x Q is ui ui roses o C (L iON a tu a �lj W 3NON li LU 10 rL � ' � N3ewnN � 9 r� Q� a alBtl1 _] ❑ 4 ui i w C" (o to d) �eurejuo� 'U 0. C7 Q z z tjj C7 cL C'3 Q C3 t1 C7 FO= W V z O z Z O m qelD I 1 E IC co ullsodwoa U U U U C7 U C7 C7 U U C`3 U U' U (� `.10 Z w [L ll] Q O >- o o LUfL 0 edA1 sidwog U n CC o z � w 2 C Q []. 0 m cn m E m COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Southeast Brunswick Sanitary District WWTF 12/17/20 22,041 4.3432 12/17/20 9,524 3.9788 12/17/20 9,339 3.9703 12/17/20 5,328 3.7266 12/17/20 5,200 3.7160 12/17/20 2,746 14387 12/17/20 13,780 4.1392 Total 1 27.3129 Average 1 3.9018 Geometric Mean Fecal Coliform MPN 1 gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. 13 ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Wa}% Wilnlblgton, NC 28405 • 910.392.0223 Lab ' 910.392. 4424 Fax 710 Bowsertotvn Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax i a ro(u:;env i roiimcn to Ichem ists.coiii Lewis Farms & Liquid Waste, INC. Date of Report: Dec 29, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Report 9: 2020-21419 Project ID: SEBR Lab ID Sample ID: Collect Date[Time Matrix Sampled by 20-54380 Site: 1 12/17/2020 7:51 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%} SM 2540 B 2.45 % 12/17/2020 Fecal Density SM 9221C E MPN 24 hr 503 22041 MPN/g 12/17/2020 Lab lD Sample ID: Collect Date[Time Matrix Sampled by 20-54381 Site: 2 12/17/2020 7:52 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.52 % 42/17/2020 Fecal Density SM 9221C E MPN 24 hr 503 9524 MPN/g 12/17/2020 Lab ID Sample ID: Collect Date[Time Matrix Sampled by 20-54382 Site: 3 12/17/2020 7:53 AM Solid/Sludge Client Vest Method Results Date Analyzed Total Solids (%} SM 2540 B 2.57 % 12/17/2020 Fecal Density SM 9221C E MPN 24 hr 503 9339 MPN/g 12/17/2020 Lab iD Sample ID: Collect DatelTime Matrix Sampled by 20-54383 Site: 4 12/17/2020 7:54 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.44 % 12/17/2020 Fecal Density SM 9221C E MPN 24 hr 503 53281MPN/0 12/17/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-54384 Site: 5 12/17/2020 7:55 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.50 % 12/17/2020 Fecal Density SM 9221C E MPN 24 hr 503 5200 MPN/g 12/17/2020 Reoorl #. 2020-21419 Page 1 of 2 r- 7 viroehem ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way Wilmington, NC 2840.5 0 9I0.3910223 Lab a 9I0.392.4424 Fax 71C Bowsertoivn Road, klanteo, NC 27954 V 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 Q 910.347.5843 Lab/Fax in fa@envi ro nnien to Ichemists.Coill Lewis Farms & Liquid Waste, INC. bate of Report: Dec 29. 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attentions Report #: 2020-21419 Project ID: SEER Lab tD Sample ID: Collect DatelTime Matrix Sampled by 20-54385 Site: 6 12/17/2020 7:56 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids SM 2540 B 2.55 % 12/17/2020 Fecal Density SM 9221C E MP 24 hr 503 2746 MPN/g 12/17/2020 Lab ID Sample ID: Collect Date/Tlme Matrix Sampled by 20-54386 Site: 7 12/17/2020 7:57 AM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.54 % 12/17/2020 Fecal Density SM 9221 C E MPN 24 hr 503 13780MPN/g 12/1712020 Comment.- Reported on a dry weight basis. Reviewed by: Reportk: 2020-21419 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist Client. L J S Eggm5 Date/ U Report Number: 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Qo _gl (419 Receipt of sample: ECHEM Pickup ❑ Client Delivery UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt oC How temperature taken: ElTemperature Blank Against Bottles IR Gun ID; Thomas Traceable S/N 192511657 IR Gun Correction factor °C: 0.0 ❑ YES ❑ NO 3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5 Were sam I in, I YES ❑ NO p e s isted on the COC? 6. Were samples ID's listed on sample containers? l,$ YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within Droner holdinp tirna f,, ❑ YES ❑ NO ❑ YES ❑ NO ❑ YES ❑ NO ❑ YES ❑ NO ❑ YES ❑ NO ❑ YES ❑ NO ested tests? 13. Were acid preserved samples received at a pH of <2? 14, Were cyanide samples received at a pH >12? J.S. Were sulfide samples received at a pH >9? 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: if more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. obtain a new sample or notify the state lab if directed to analyzed bythe customer. who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 0 N Z m 41 O i_ W C? O W O r CO y a O1 a xa� E yy W s N w us u, U) 3 � vi z r _ � �jj N II c LL " Z Q c o z z« ?]3H10 0. 0. II Z O]H1 n (Y ¢ONH U) Z H w LLI VOsm 0 m a Q lOH ss O x r►�j� I— 0 3NON G W W"" � a+ 11 w aaewnN a _r m O o° air aledl r1 2 z � V a a Q 7.16ur J Z V y au1.10143 rn Q } 7 C_ a- Z � L!J m Jaulejuo3 ca 101 � _ w w w of rn in CD o Q IV a U U U U w L U- L_ I.L li LL U- CL U- r X1 xI X1 xl X1 xI x r. T�.r ��' Ili• W. 1�,r awn �^ r X1 xI X1 xl X1 xI x r. T�.r ��' Ili• W. 1�,r awn �^ M�1� ©w�w� E rz w �? a, ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) F il- ae �fy Name: Coastal Farms and Residuals, LLC WWTP Name: Brunswick Sanitary District WWTP WQ Permit Number: WQ0034806 Monitoring Period; From NPDES Number: WQ0013200 _ 1/I/2020 To I2/3.1/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tiinelterrt) ❑ Alt B (Alk Treatment) ) ❑ —"!Alt. C (Prior Testing)❑ (No Prior Test) ❑ Process to Further Reduce Patho en s ❑ if applicable to alternative performed (Class A only) indicate "Process to Further Reduce Patlio ens": POM ost ❑ Heat D in ❑ Heat Treatment ❑ Za ❑Oaittma Ra Thertrio hiIic ❑ ❑ Pasteurization ❑ Class 1S: Alt. (l) Fecal Densi y p I Alt. (2) Process to Si iificaiitl Reduce Patho ens ❑ .If applicable to alternative Pet -formed (Class B only) indicate "P1'ocess to Significantly Reduce Pathogens": ,iine Stabilization ❑ Air. D to ❑ Coin stip ❑ Aerobic Digestion EEIE] knaeroblc LJ1.-Oinn 1--1 ............�:. �:::.:::.�:..:::.. _. lI ap licable to alternative erformed (£ Parameter Allowable Level in Sludge Minima 2 x IQ to the MP1V 5,200 6th power per gram of Fecal Coliforrri total solids CFU I00o mpn per gram of total solid (dry ,•........rua vn�acna 1vir1V per 4 grams (in lieu of fecal total solid (dry ss A or Class B) complete the fallowing monitoring data: Pathogen Density um 6 er o Frequency Sample Analy is Excee- Geo. Mean aximu Units enresof Analysis Type Techa 7,977 122,041 I MPNIg I Q I Annual I Crab I sM922i -- - --- -•-�- _ •ij�.� - riea�e tnatcate alternative performed: Alt.1 (VS seduction) EL Alt. 2 (40-day bench) ❑ AIt. 3 (30-day bench) ❑ lAlt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) El Alt. 10 (Incorporation) El No vector. attraction reduction. alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify; under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the Vector attraction reduction requirement in 15A NCAC 02T .1107 have not been. met." (Please note if you check this statement attach an explanation why you have not met one or both of the finis aetermmation has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Stephanie Moore, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) gnature of Prparer—*_ Date Signature 4Ld (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 16, 2020 Summerhouse 1.14 % Solids 7.27 t)H Permit No. WQ0029945 Parameter % Mg/Kg DryWeight (% x 10,000) Pounds/Dry Ton (M&Ez x 0.002) Nitrogen (TKN) 7.740 77,400.000 154.800 Phosphorus 2.280 22,800.000 45.600 Potassium 0.912 9,120.000 18.240 PAN (injected)* 2.841 28,405.200 56.810 PAN (surface)* 2.473 24,730.200 49.460 Ammonia Nitrogen 0.735 7,350.000 14.700 Calcium 2.280 22,800.000 45.600 Calcium Carbonate E . --- --- Magnesium --- 2,740.000 5.480 Sodium --- 6,680,000 13.360 Sulfur --- Nitrate N / Nitrite N --- 40.200 0.080 Barium Chloride --- --- --- --- --- --- SAR 2.60 Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 1,980.00 3.960 Arsenic - - 12.50 0.025 75 Cadmium --- 12.50 0.025 85 Chromium --- 22.700 --- w Copper --- 99,10 0.198 4,300 Lead --- 12.50 0,025 840 Mercury --- 1.47 0.003 57 Molybdenum --- 12.50 0.025 75 Nickel --- 12.50 0.025 420 Selenium --- 12.50 0.025 100 Zinc --- 1,700,00 3,400 7,500 Environmental Chemists # 2020-00870 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS & RESIDUALS, LLC WQ0034806 Summerhouse 01/16/20 800,000 5.9031 01/16/20 280,000 5.4472 01/16/20 415,385 5.6185 01/16/20 696,970 5.8432 01/16/20 428,572 5.6320 01/16/20 261,195 5.4170 01/16/20 271,318 5.4335 Total 1 39.2944 Average 1 5.6135 Geometric Mean fro: Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction requirement. Environmental Chemists, Inc. t 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax SY� TO Bowsertown Road, Mantea, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highwav, Jacksonville, NC 28540 • 910.347.3843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inlo@environmentalchemists.com Onslow Water R Sewer Authority Date of Report: Jan 30, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Todd Roberts Report #: 2020-00870 Project ID: Summerhouse Lab ID Sample ID: SH Fecal #1 Collect DatelTime Matrix Sampled by 20-02180 Site: Q200330 01 1/16/2020 9:05 AM Solid/Sludge Anthony Padgett Test Method Results Date Analyzed Total Solids (%) Fecal Density Lab ID Sample ID: SH Fecal #2 20-02181 Site: 0200330-02 Test SM 2540 G SM 9221C E MPN 24 hr 503 Method Collect DatelTime 1/16/2020 9:05 AM Total Solids (%) SM 2540 G Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: SH Fecal #3 Collect DatelTime 20-02182 Site: 0200330-03 1/16/2020 9:06 AM Test Method Total Solids (%) SM 2540 G Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: SH Fecal #4 Collect DatelTime 20-02163 Site: Q200330-04 1/16/2020 9:06 AM Test Total Solids (%) Fecal Density Lab ID Sample ID: SH Fecal #5 20-02184 Site: Q200330-05 Test Method SM 2540 G SM 9221 C E MPN 24 hr 503 Method Collect DatelTime 1/16/2020 9:07 AM 1.15 % 01 /17/2020 800000 MPNIg 01/16/2020 Matrix Sampled by Solid/Sludge Anthony Padgett Results Date Analyzed 1.25 % 01/17/2020 280000MPN/g 01/16/2020 Matrix Sampled by Solid/Sludge Anthony Padgett Results Date Analyzed 1.30 % 01 /1712020 415385 MPN/g 01/16/2020 Matrix Sampled by Solid/Sludge Anthony Padgett Results Date Analyzed 1.32 % 01 /17/2020 696970MPNIg 01/16/2020 Matrix Sampled by Solid/Sludge Anthony Padgett Results Date Analyzed Total Solids (%) SM 2540 G 1,26 % 01/17/2020 Fecal Density SM 9221Q E MPN 24 hr 503 428572 MPNIg 01/16/2020 Report C 2020-00870 Page 1 of 3 Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Attention: Todd Roberts Lab ID Sample ID: SH Fecal #6 20-02185 Site: Q200330-06 Test Total Solids (%) Fecal Density Lab ID Sample 1D: SH Fecal #7 20-02186 Site: Q200330-07 Test Total Solids (%) Fecal Density Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910,392.0223 Lab " 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax infoGenvironmentalchemists.com Date of Report: Jan 30, 2020 Customer PO #: Customer ID: 08100092 Report #: 2020-00870 Project ID: Summerhouse Collect Date/Time 1/16/2020 9:07 AM Method SM 2540 G SM 9221 C E AWN 24 hr 503 Collect Date/Time 1116/2020 9:08 AM Method SM 254a G SM 9221 C E MPN 24 hr 503 Matrix Sampled by Solid/Sludge Anthony Padgett Results Date Analyzed 1.34 % 01/17/2020 261195 MPN/g 01/16/2020 Matrix Sampled by Solid/Sludge Anthony Padgett Results Date Analyzed 1.29 % 01 /17/2020 271318 MPNIg 01/16/2020 Report #:: 2020.00870 Page 2 of 3 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4 t24 Fax `M 710 Bowsertown Road, iManteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoLenvironmentalcltemists.com Onslow Water & Sewer Authority 228 Georgetown Road Date of Report: Jan 30, 2020 Customer PO #: Jacksonville NC 28540 Customer 0: 08100092 Attention: Todd Roberts Report #: 2020-00870 Project ID: Summerhouse Lab ID Sample ID. SH Digestor Collect Dateffime Matrix Sampled by 20-02187 Site: Q200330-08 1/16/2020 9:08 AM Solid/Sludge Anthony Padgett Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 1980mg/kg 01/21/2020 Arsenic EPA 200.7 <12.5 m /k 9 9 01I2112020 Cadmium EPA 200.7 <12.5 mg/kg 01121/2020 Calcium EPA 2007 mg/kg 9 22800 mIkg 01/21/2020 Chromium EPA200.7 22.7m g 01/21/2020 Capper EPA 200.7 99•i m /kg 9 01121/2020 Lead [:PA 200.7 <12.5mg/kg 01/21/2020 Magnesium EPA 200.7 2740 m /kg g 01/21/2020 Molybdenum EPA 200.7 <12.5 m Jkg 9 01121/2020 Nickel EPA 200.7 12.5mglkg 01/21/2020 Potassium EPA 200.7 9120 m /kg 9 01/21/2020 Selenium EPA 2ao.7 <12.5 mg/kg 01/21/2020 Sodium EPA 2aa,7 Ik 6680 mg g 01/21/2020 Zinc EPA 200.7 1700 mg/kg g g 01/21/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 Total Solids (%) SM 2540 a 40 2 m Ik 9 g 01/24/2020 pH 1.14 01/17/2020 SM 45aa H a 7.27 units 01/20/2020 Ammonia Nitrogen SM 4500 NH3 C 7350 m Ik 9 g 01/21/2020 Total Kjeldahl Nitrogen (TKN) SMasoo org a Total Phosphorus SM 4500 P F 77400 m Ik g g 01/22/2020 Mercury SW846 22800 m /k 9 g 01123/2020 7471 e <1.47 m /k g g 0112412020 Comment: SI residuals, except pH, reported on a dry weight basis. pH reported on an Reviewed by:Qp, as received basis. Report #:: 202a•00870 Page 3 of 3 4 NS -�o11uuE9 raullmy: Summer House WRF Twining Rase Lane Holly Ridge, NC 28445 Phone: 910.369.8511 Project Manager: Todd A. Roberts Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Subcontracted Laboratorv: SUBCONTRACT ORDER 4M Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax: (910) 392-4424 NCDENR: OWQ CERTIFICATION S 94 NCOMS: dLs CERTIFTCAnou s 3"29 Work Order: Q200330 Summer House WRF Sample ID: Q200330-01 SH Fecal # 1 SL Sampled. 01/16/2020 09;05 Sampled by; Air 0kaLPa&w Analysis Fecal Density Due Expires EnviraChem Lab ID 01/26/2020 01/16/2020 ISM Analysis Total Solids (%} Due Expires P EnvlrcLhem Lab ID 01/26/2020 01/23/2020 09:05 Contalners Supplied; 120 Sterile Na2S203 (A) Sample ID: Q200330-02 SH Fecal # 2 SL Sampled.01/16/2020 09.OS Sampled by; Anthony Padauff Analysis Fecal Density Due Expires EnviraChem Lab ID 01/26/.020 01/16/2020 15:05 Total Solids Containers Supplied.• 120 Sterile Na2S203 (A) Sample ID: Q200330-03 SH Fecal # 3 Analysis Fecal Oemlty Total Solids (%) Containers Supplied- 120 Sterile Na2S203 (A) Sample ID: Q200330-04 SH Fecal # 4 Fecal Total Solids (%) Containers Supplied- 120 Sterile N825203 (A) Sample ID: g200330-05 SH Fecal # 5 Due Expires EnviraChem Lab ID 01/26/2020 0!/23/2020 09:05 SL Sampled; 01 J16/2020 09; 05 Sampled by: 0 I 1 Due Expires EnviraChem Lab ID d� Due 01/26/2020 01/16/2020 15:06 r-11 —1. nvuwL.nem Lan iLi 01/23/2020 09:06 SL Sampled: 61/16/2020 09.-06 SamP1edbY-'Aa&0jVLLdggff D Due Expires EnviroChem Lab ID 01/26/2020 01/16/2020 15:06 Due Expires EnviroChem Lab ID 01/26/2020 01/23/2020 09:06 SL Sampled: 01116/2020 09;07 Sampled by: &U=j2g4= oc� / p v EnviroChem Report No: Vim. I✓Vd / a - • •��-� ire z,, _ t T �rau j f�� Relinquished By Date Received By pate lk"� Page 1of3 { Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Work Order: Q200330 (Continued) Summer House WRF SUBCONTRACT ORDER (Continued) Sample ID. Q200330-05 SH Fecal # 5 SL Sampled: 0111612029 09.07 Sampled by: AnthonyPadnett 0,18 Y Analysls Due Expires EnviroChem Lab ID Fecal Density 01/26/2020 01/16/2020 15:07 Analysis Due Expires _ EnviroChem Lab ID Total Solids (%) 01/26/2020 01/23/2020 09:07 Containers Supplied.' 120 Sterile Na2S203 (A) Sample ID: Q200330-06 SH Fecal # 6 SL Sampled; 0111612020 09:07 Sampled by: AathoQv Padgett D z 9S Analysis Due Expires EnviroChem Lab ID Fecal Density 01/26/2020 01/16/2020 15:07 Analysis Due Expires EnviroChem Lab 10 Total Solids (%) 01/26/2020 01/23/2020 09:07 Containers Supplied; 120 Sterile Na25203 (A) Sample 10. Q200330-07 SH Fecal # 7 SL Sampled.* 0111612020 09:08 Sampledby. Anthony Padaett Q a 18 Analysis Due Expires EnviroChem Lab ID Fecal Density 01126/2020 01/16/2020 15.08 Analysis Due Expires EnviroChem Lab ID Total Solids (%) 01/26/2020 01/23/2020 09:08 Containers Supplied; 120 Sterile Na25203 (A) Sample ID. Q200330-08 SH D[gestor SL Sampled: 0111612020 09.08 Sampled by. Anthony Padaeft I O 4 Analysis -__ _ Due Expires EnviroChem Lab ID Cd 200.7 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID Al 200.7 01/26/2020 01/16/2020 09:68 Analysis Due Expires EnviroChem Lab ID Na 200.7 01/2612020 01/16/2020 09:08 j Analysis Due Expires EnviroChem Lab ID I As 200.7 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID NI 200.7 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID Ca 200.7 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID Mo 200.7 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID Mg 200.7 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID K 200.7 01/26/2020 01/16/Z020 09:08 Relinquished By Date EnviroChem Report No j V — ✓ 0? -�() _ d ,1. 1 go Receiv,,h By Date Page 2 of 3 Onslow Water & Sewer Authority 228 Georgetown Road Jacksonville NC 28540 Work Order: Q200330 {Continued} Summer House WRF SUBCONTRACT ORDER (Continued) Sample ID: Q200330-08 SH Digestor St Sampled; 01/16/7020 09.08 Sampled by: Antholrr Padvett O 1 if Analysis Due Expires EnviroChem Lab ID Hg SW846 7471D 01/26/2020 01/16/2020 09:08 Analysis Due Expires EnviroChem Lab ID pH 01/26/2020 01/16/2020 09:25 Analysis Due Expires EnviroChem Lab ID Total Solids (%} 01/26/2020 01/23/2020 09:08 Analysis Due Expires EnviroChem Lab ID Se 200.7 01/26/2020 01/30/2020 09:08 AnaTysis Due Expires EnviroChem Lab ID Zn 200.7 01/26/2020 01/30/2020 09.08 Analysis Due Expires EnviroChem Lab ID Ammonia Nitrogen 01/26/2020 02/13/2020 09:08 Analysls Due Expires EnviroChem Lab ID Total Phosphorus 01/Z6/2020 02/I312020 09:08 Analyses Due Expires EnviroChem Lab ID Total Kjeldahl Nitrogen (TKN) 01/26/2020 02/13/2020 09;06 Analysis Due Expires EnviroChem Lab ID Nitrate+Nitrite-Nitrogen 01/26/2020 02/13/2020 09:08 Analysis Due Expires EnviroChem Lab ID Pb 200.7 01/26/2020 07/14/2020 09:08 Analysis Due Expires EnviroChem Lab ID Cu 200.7 01126/20ZO 07/14/2020 09:08 Analysis Due Expires EnviroChem Lab ID Cr 200.7 01/26/2020 07/14/7020 09;08 Containers Supplied. P 112 Gal (A) Relinquished By EnviroChem deport No: a 0 7 l7 9 11 lt� Date R elved By Date Page 3 of 3 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806 WWTP Name: Summerhouse WWTP NPDES Number: WQ0029945 Monitoring Period: From l/l/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .11 Class A: Alt. A (time/temp) ❑ AIt.D (No Prior Test) If applicable to alternative performed (Class Compost ❑ Heat Drying ❑ Beta Ray 11 Gamma Ray ❑ Class B: JAR. (1) Fecal Density If applicable to alternative performed (Ch Lime Stabilization ❑ Air Anaerob ic Digestion n If applicable to alternative performed.; Parameter Allowable Level in Sludge 6—in Fecal Coliform Wmonella bacterii (in lieu of fecal _ coliform) rector Attracts 2x10tothe rCFU 6th power per gram of total solids iuuu mpn per gram of total solid (dry MPN per 4 grams total solid (dry 06) - Please indicate level achieved and alternative performed: Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing)[] :1 1 Process to Further Reduce Pathogengs ❑ A only) indicate "Process to Further Reduce Pathogens": Heat Treatment ❑ Thermonlime r-I Alt. (2) Process to Si ificantly Reduce Pathogens ❑ 13 only) indicate °''Process to Significantly Reduce Pathogens": iii ❑ COTEosting ❑ Aerobic Digestion ❑ ass A or Class B) complete the following monitoring data: Pathogen Density um er o Frequency Sample a ync Bxcee- Teeh- Geo. Mean aximu Units aces of Analysis Type liYf311P. 261,I95 1410,660 1800,0001 MPN/g I 0 I Annual I Grab I SM9221 - Please indicate alternative perfor Alt I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAR. 4 (Spec. 0, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ AIt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) ElAlt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) a Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) l] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." ction Mike Lutz, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 2126120 Z,� 2/17/20 Signature of Preparer* Date Signature of Land pplier (i —applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) COASTAL RESIDUALS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: June 11, 2020 Surf City WWTP 1.75 % Solids 7.11 pH Permit No. WQ0000795 Parameter I % lMg/KgDryWeight (% x 10,000) Pounds/Dry Ton LMgLKg x 0.002) Nitrogen (TKN) 5.750 57,500.000 1I5.000 Phosphorus 2,810 28,100.000 56.200 Potassium 0.419 4,190.000 8.380 PAN injected)* 1.736 17,360.997 34.722 PAN surface)* 1.736 17,358.142 34.716 Ammonia Nitrogen 0.001 5.710 0.011 Calcium 4.790 47,900.000 95.800 Calcium Carbonate E , --- _-- --- Magnesium --- 4,360.000 8.720 Sodium --- 11,100.000 22,200 Sulfur __. __ Nitrate N / Nitrite N --- 107.000 0.214 Barium Chloride --- --- --- --- --- SAR 1.72 Iron --- --- --- Ceiling Concen. (Mg/Kg) Aluminum --- 4,970.00 9.940 Arsenic --- 36.60 0.073 75 Cadmium --- 28.60 0.057 85 Chromium -- 28.600 0.057 --- Copper -- 519.00 1.038 4,300 Lead --- 28.60 0.057 840 Mercury --- 1.060 0.002 57 Molybdenum --- 28.60 0.057 75 Nickel --- 28.60 0.057 420 Selenium --- 28.60 0.057 100 Zinc --- 3,920.00 1 7.840 7,500 Environmental Chemists # 2020-09631 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D- (Not Detected) or < detection limits are listed as detection limits for calculation purposes. LEWIS FARMS WQ0000455 Surf City WWTP .:1?. :g. : - 06/11/20 6,047 3.7815::: 06/11/20 5,604 3.7485 06/11/20 3,562 3.5517 06/11/20 11,220 4.0500 06/11/20 4,889 3.6892 06/11/20 3,595 3.5557 06/11/20 3,697 3.5678 Total 1 25.9445 Average 1 3.7064 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. 4 r-Anvironmental Chemists, Inc. c 6602 Windmill Way, Wilmington, NC 28405 6 91.0-392.0223 Lab 4 9I0.392.4424 Fax `+ rsrn) 7:1.0 Bowsertown Road, Manteo, NC 27954 o 252-473.5702 Lab/Fax 255-A Wilmington Highwav, lac:ksonville, NC 28540 a 910.347.5843 Lab/.Fax ANALYTICAL & CONSULTING CHEMISTS infofhenvironmcntalclrernists.coral Town of Surf City Date of Report: Jul 15, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2020-09631 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-24059 Site: Sludge 6/11/2020 8:00 AM Solid/Sludge Lewis Farms Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 8051 B1351 0 <0.02 mg/L 06/23/2020 Endrin (TCLP) SW 846 Method 6081B13510 <0.0005 mg/L 06/23/2020 Heptachlor (TCLP) SW 846 Method 8081B13510 <0.0005 mg/L 06/23/2020 Heptachlor epoxide (TCLP) SW 846 Method 8081813510 <0,0005 mg/L 06/23/2020 Lindane (TCLP) SW 846 Method eoel Br3510 <0.0005 mg/L 06/23/2020 Methoxychlor (TCLP) SW 846 Method B081B13510 <0.0005 mg/L 06/23/2020 Toxaphene (TCLP) SW 846 Method 80e11313510 <0.05 mg/L 06/23/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 827013540 <0.050 mg/L 06/23/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 06/23/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/23/2020 2,4-Dinitrotoiuene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/23/2020 Cresol (TCLP) 5W 846 method 8270/3510 <0.050 mg/L 06/23/2020 Hexachloro-1,3-butadiene(TCLP) SW 846 method827013510 <0.050mg/L 06/23/2020 Hexachlorobenzene (TCLP) SW 846 method a27013510 <0.050 mg/L 06/23/2020 Hexachloroethane (TCLP) SW a46 method 827013510 <0.050 mg/L 06/23/2020 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/23/2020 Nitrobenzene (TCLP) SW 846 method 0270/3510 <0.050 mg/L 06/23/2020 o-Cresol (TCLP) 5W 846 method 82701351a <0.050 mg/L 06/23/2020 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 06/2312020 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/23/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 06/24/2020 2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 06/24/2020 1,1-Dichloroethylene (TCLP) SW046 Method 8260/5030 <0.01 mg/L 06/25/2020 1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0,01 mg/L 06/25/2020 Benzene (TCLP) SW846 Method 826015030 <0.01 mg/L 06/25/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/25/2020 Report #:: 2020-08631 Page i of 4 VA"Wironmental Chemists, Inc® 6602 Windmill Way, Wilmington, NC 28405 c 910-392.022 c10.392.4424 Fax __ 3 Lab n J IS 7I0 Dowsertown Road, Mantes, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington 1-fighway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS ifiCofc�ertvimumcntalcl�einists,com Town of Surf City Date of Report: Jul 15, 2020 Post Office BOX 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2020-09631 Project ID: Sludge Chlorobenzene (TCLP) SW846 Method 82601503E <0.01 mg/L 06/25/2020 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 m /L g 06/25/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 Tetrachloroethylene (TCLP) SW846 Method8260/5030 <0.05 m /L 9 06/25/2020 <0,01 m /L g 06125/2020 Trichloroethylene (TCLP) SW846 Method826015030 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 m /L g 06/25/2020 RCI <0.01 mg/L 06/25/2020 Cyanide EPA 335.4 Reporting limit elevated due to matrix interference. <0.05 mg/kg 06/29/2020 Sulfide SM 4500 & D 3.94 mg/kg 06/16/2020 Ignitability SW 846 method 10io Sludge Residuals >195 °F 07/10/2020 Aluminum EPA 200.7 4970 m /k g g 06/19/2020 Arsenic EPA 20o.7 36.6 m /k 9 9 06/16/2020 Cadmium EPA 200.7 <28.6 m /k g g 06116/2020 Calcium EPA 200.7 47900 m Ik 9 9 06/16/2020 Chromium EPA 200.7 <28.6 m /k g 9 06/16/2020 Copper EPA 20Q.7 519 m /k 9 9 06/16/2020 Lead EPA 200.7 <28.6 m /k g 9 06/16/2020 Magnesium EPA 200.7 4360 m /k 9 9 06116I2020 Molybdenum EPA 200,7 <28.6 m /k g 9 06/16/2020 Nickel EPA 200.7 <28.6 m /k g 9 06/16/2020 Potassium EPA 200,7 4190 mg/kg 06/16/2020 Selenium EPA 200.7 <28.6 mg/kg 06/16/2020 Sodium EPA W0.7 11100 m /k g 9 06/19/2020 Zinc EPA 200.7 3920 m /k 9 9 06/19/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 107 m /k g g 06/20/2020 Total Solids (%) SM 2540 a 1.75 D6/1112020 pH SM 4500 H 8 7.11 units 06/1512020 Ammonia Nitrogen SM 4500 NH3 C <5.71 m /k 9 g 06/12/2020 Report #:: 2020.09631 Page.2 of 4 Environmental Chemists, Inc. 6002 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab 6 910,392.4424 Fax w 710 Bowscrtown Road, Manteo, NC 27954 6 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoFcDenvironnientalcheniists.com Town of Surf City Date of Report: Jul 15, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2020-09631 Project ID: Sludge Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 5750D mg/kg 06/12/2020 Total Phosphorus SM 4500 P F 28100 mglkg 06/19/2020 Mercury swags 7a71a 1.06 mglkg 06/15/2020 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 06/25/2020 Barium EPA 200.7 <1.0 mg/L 06/25/2020 Cadmium EPA200.7 <1.Omg/L 06/25/2020 Chromium EPA 200.7 <1.0mg/L 06/25/2020 Lead EPA 2007 <1.0 mg/L 06/25/2020 Selenium EPA 200.7 <1.0 mg/L 06/25/2020 Silver EPA 200.7 <1.0 mg1L 06/25/2020 Mercury EPA 245.1 <0.0002 mg/L 06/25/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-24060 Site: 1 6/11/2020 8:02 AM Solid/Sludge Lewis Farms Test Method Results Date Analyzed Total Solids (%) SM 2540 a 2.15 % 06/11 /2020 Fecal Density SM 9221C E MPN 24 hr 503 6047 MPN/g 06/11/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-24061 Site: 2 6/11/2020 8:03 AM Solid/Sludge Lewis Farms Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.32 % 06/11 /2020 Fecal Density SM 9221C E MPN 24 hr 503 5604 MPN/g 06/11 /2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-24062 Site: 3 6/11/2020 8:04 AM Solid/Sludge Lewis Farms Test Method Results Date Analyzed Total Solids N SM 2540 8 2,19 % 06/11 /2020 Fecal Density SM 9221C E MPN 24 hr 503 3562 MPN/g 06/11/2020 Reporl #': 2o20.09631 Page 3 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910-392.0223 Lab e 910.392.4' 24 Fax (sra- 710 Bowsertown Road, Manteo, NC 27954 ,252,473.5702 Lab/Fax � 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infor�enviraiunentalchemists.cnm Town of Surf City Date of Report: Jul 15, 2020 Post Office Box 2475 Customer PO #: Surf City NC 28445 Customer ID: 08110024 Attention: Steve Smith Report #: 2020-09631 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-24063 Site: 4 6/11/2020 8:05 AM Solid/Sludge Lewis Farms Test Method Results Elate Analyzed Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect DatelTime 20-24064 Site: 5 6/11/2020 8:06 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect DatelTime 20-24065 Site: 6 6/11/2020 8:07 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221 C E MPN 24 hr 503 Lab ID Sample ID: Collect DatelTime 20-24066 Site: 7 6/11/2020 8:08 AM Test Method 2.05 % 06/11/2020 11220MPN/g 06/11/2020 Matrix Sampled by Solid/Sludge Lewis Farms Results Date Analyzed 2.25 % 06/11/2020 4889 MPN/g 06/11/2020 Matrix Sampled by Solid/Sludge Lewis Farms Results Date Analyzed 2,17 % 06/11/2020 3595MPN/g 06111/2020 Matrlx Sampled by Solid/Sludge Lewis Farms Results Date Analyzed Total Solids (%) SM 254o B 2.11 % 06/11/2020 Fecal Density SM 9221C E MPN 24 hr 503 3697 MPN/9 06/11/2020 Comment: Results, except pH, reported on a dry weight basis, pH reported on an as received basis. Reviewed by: I I',-(& Reportk. 2020.09631 Pape 4 of 4 LO CD 04 4 z m Eo 0 0 u; O w U E � � ; 1 Ir LL 3 (D 11 uj r > m N [!J n Ci n c17 F- c!) F- U) co c f ie a m •c c c ca c m c +n C in 3 U • C� O II O y �Ly" a a b c N tD d .0 E z w w CD Q7 a Z ,7v i0 H3H1,0 Ia. li T r II Z rO OIHi X ?C ?C X X X ?C QHOVN w > CCCONN ■+ II LU lw DOSZH 00 U 43 7 10H V� FE 3NON i< Lu ❑ W II Lu (A {a y :: bosom 1N a 9 tea, '✓ O O 7+ r ,r olOVl V) Z = :Er o Q Iv Ilbw Z V M y P aulJOl49 rn ❑ N Q ro z Z Q 2 U. y Z 0 z Q Q w8ozzoJ O w W ui }' w }I' W JO d) IL r �aule;uOa ( 0 IL 0 Q w CL geJE) ¢ ,o U C7 U C3 U N allsodwoo a Q1 Q, n H Q G 5 Q Gx ui E U Q J_ Inl m1 r-- w E E ro 0 a CL 9 5, / in 2 U c a •� c as a C, (D E m N O r N !^- ❑ U ANNUAL PATHOGEN AND 'VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806 WWTP Name: Surf City WWTP NPDES Number: WQ0000795 Monitoring Period: From 1/l/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate Ivel achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ I Process to Farther Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce pathogens"; Com ost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑ Beta Ray ❑ Gaunna Ray ❑ Pasteurization ❑ _,.,.. Class B: Alt_ (1) Fecal Density pplicable to alternative performed (Ch to Stabilization ❑ Air aerobic Di esti On El l pplicable to alternativeperformed Parameter Allowable Level in Sludge Minim Fecal Coliform (in lieu of fecal 2 x 10 to the PCFU 6th power . per gram of total solids tuuu mpn per gram of total solid (dn virtu per 4 grams total solid (dry Alt. (2) Process to Sign ifce ]B only) indicate "Process to Sig n ❑ Coin os ass A or Class B) complete th Pathogen Density Geo. MeanMaximunj Units ficantly Reduce Pathogens',.- Z ❑ lAerobic Digestion ❑ following monitoring data: 7n,er a Frequency Sample a tc (A.p Teoh-.Pc O4 N[alySSS �V 3,562 I 5,086 111,220 I MPN/g I 0 I Annual I' Grab I SM922 vector Attraction Reduction (15A NCAC 02T .1101) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt 3 (30-day bench) ❑ JAIL 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Allc. Stabilization ❑ AIt 7 (Drying - Stable) ❑ IAIL 9 (Drying - Unstable) ❑ Alt. 9 (Injection) El Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements,) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Steve Smith, ORC Wesley Wooten, President Preparer Name nd Tile (type or print) Land Applier Name and Title (if applicable)(type or print) 7Dateo Signature of Preparer* Date Signature of Land plier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) DFNR FORM PVRF 02T (1212006) COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 15, 2020 Swansboro 2.35 % Solids 6.14 pH Permit No. WQ0034806 Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (M x 0.002) Nitrogen (TKN) 4.260 42,600.000 85.200 Phosphorus 1.510 15,100.000 30.200 Potassium 0.291 2,910.000 5.820 PAN (injected)* 2.293 22,934.000 45.868 PAN (surface)* 2.227 22,274.000 44.548 Ammonia Nitrogen 0.132 1,320.000 2.640 Calcium 3.660 36,600.000 73.200 Calcium Carbonate E . --- -_- --- Magnesium --- 1,730.000 3.460 Sodium --- 4,340.000 8.680 Sulfur --- --- --- Nitrate N 1 Nitrite N --- 9,230.000 18.460 Barium Chloride --- --- --- --- --- __. SAR 3.39 Iron --- --- --- Ceiling Concert. (Mg/Kg) Aluminum --- 3,280.00 6.560 Arsenic --- 20.90 0.042 75 Cadmium --- 20.90 0.042 85 Chromium --- 20.900 --- -- Copper --- 289.00 0.578 4,300 Lead --- 20.90 0.042 840 Mercury --- 3.86 0.008 57 Molybdenum --- 20.90 0.042 75 Nickel --- 20.90 0.042 420 Selenium --- 20.90 0.042 100 Zinc --- 3,840.00 7.680 7,500 Environmental Chemists # 2020-06314 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Swansboro 04/15/20 5,778 3.7618 04/15/20 7,392 3.8688 04/15/20 9,830 3.9926 04/15/20 7,143 3.8539 04/15/20 5,580 3.7466 04/15/20 7,360 3.8669 04/15/20 11,112 4.0458 Total 27.1363 Average 1 3.8766 Geometric Mean ' = ? ':77.1 7 € € + Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction requirement. 12in.vironmental Chemists, Inc. ® p 6602 Windinill Way, Wilmington, NC 28405 ° 910.392,0223 Lab C 910,392.4424 Fax -� 710 Iiowsertown Road, Manteo, NC 27954 O 252.473.5702 Lab/Fax 255-A Wilmington Highway Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS iii(o@environinentalclieniists.com On -slow Water & Sewer Authority Date of Report: Apr 29, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mike Lutz Report #: 2020-06314 Project ID: Swansboro Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-15515 Site: #1 4/15/2020 9:11 AM Solid/Sludge Mike Lutz Test Method Results Date Anniuvarl Total Solids (%) SM 2540 B 2.25 % 04/20/2020 Fecal Density SM 9221C E MAN 24 hr 503 5778 MPNIg 04/15/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-15528 Site: #2 4/15/2020 9:12 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.30 % 04/20/2020 Fecal Density SM 9221C E MPN 24 hr 503 7392 MPNIg 04/15/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-15529 Site: #3 4/15/2020 9:13 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect Date/Time 20-15530 Site: #4 4/15/2020 9:14 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 Lab ID Sample ID: Collect DatelTime 20-15531 Site: #5 4/15/2020 9:15 AM Test Method Total Solids (%) SM 2540 B Fecal Density SM 9221C E MPN 24 hr 503 2.34 % 04/20/2020 9830 MPN/g 04/15/2020 Matrix Sampled by Solid/Sludge Mike Lutz Results Date Analyzed 2.38 % 04/20/2020 7143 MPNIg 04/15/2020 Matrix Sampled by Solid/Sludge Mike Lutz Results Date Analyzed 2.33 % 04/20/2020 5580 MPN/g 04/15/2020 Report M! 2020-06314 Page 1 of 3 Env4ironmental vironmen.t . Chemists, Inc. bb02 Windmill Way, Wilmington, NC 28405 ° 910.392,0223 Lab ° 910.392.4424 Fax 1710 Bowsertown Road, Manteo, NC 27954 " 252.473.5702 Lab/Fax 255-A Wilmington Highway; Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(�ienvironmentalctaeiuists.coin Onslow Water & Sewer Authority Date of Report: Apr 29, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mike Lutz Report #: 2020-06314 Project ID: Swansboro Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-15532 Site: #6 4/15/2020 9:16 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%j SM 2540 a 2,31 % 04/20/2020 Fecal Density SM 9221C E MPN 24 hr 503 7360 MPN/g 04/15/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-15533 Site: #7 4/15/2020 9:17 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Total Solids (%j SM 2540 a 2.43 % 04/20/2020 Fecal Density SM 9221C E MP 24 hr503 11112 MPNIg 04/15/2020 Report #:: 2020-06314 Page 2 of 3 Onslow Water & Sewer Authority Date of Report: Apr 29, 2020 228 Georgetown Road Customer PO #: Jacksonville NC 28540 Customer ID: 08100092 Attention: Mike Lutz Report #: 2020-06314 Project 1D: Swansboro Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-15534 Site: Digester 4/15/2020 9:10 AM Solid/Sludge Mike Lutz Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 20o.7 3280 mg/kg 04/22/2020 Arsenic EPA 200.7 <20.9 mg/kg 04/22/2020 Cadmium EPA 200.7 <20.9 mg/kg 04/22/2020 Calcium EPA 200.7 36600 mglkg 04/22/2020 Chromium EPA 200.7 <20.9mglkg 04122/2020 Copper EPA 200.7 289 mg/kg 04/22/2020 Lead EPA 200.7 <20.9 mg/kg 04/22/2020 Magnesium EPA 200.7 1730mg/kg 04/22/2020 Molybdenum EPA 2o0.7 <20.9 mglkg 04/22/2020 Nickel EPA 200.7 <20.9 mglkg 04/22/2020 Potassium EPA 2o0.7 2910 mg/kg 04/22/2020 Selenium EPA 200.7 <20.9 mg/kg 04/22/2020 Sodium EPA 2oo.7 4340 mglkg 04/28/2020 Zinc EPA 200.7 3840mg/kg 04/22/2020 Nitrate+Nitrite-Nitrogen EPA353.2 9230mglkg 04/23/2020 Total Solids 5M 2540 8 2.35 % 04/20/2020 pH SM 4500 H B 6.14 units 04120I2020 Ammonia Nitrogen SM 4500 NH3 C 1320 mg/kg 04/16/2020 Total Kjeldahl Nitrogen (TKN) SM 4500 Dry B 42600 mg/kg 04/16/2020 Total Phosphorus SM 4500 P F 15100 mglkg 04/24/2020 Mercury SW846 7471 B 3.86 mg/kg 04/21 /2020 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by:�� Report #:: 2020.06314 page 3 of 3 Environmental Chemist, Inc,, Wilmington, NC Lake r!#94 6602 Windmill Way Wilmington. NC 2840S 910.392 D223 Sample Receipt Checklist Client:ot'�Sll�(hl �;IjT�Z Date! � � I Report Number: Receipt of sample: Delivers ❑ YES O NO NIA EJPS ❑ FedEx ❑ Other ❑ I. Were Custody ❑ YES ❑ NO seals present on the cooler? N/A 2. If custody seals were present, were they Intact/unbroken? Original temperature upon receipt gt` HOW temperature taken: Corrected temperature upon receipt QO Blank IR Gun ID: Thomas Traceable S/�1925 1657ture Against Bottles ❑ YES ❑ NO P IR Gun Carrection Factor -C: O.D 3. If temperature of cooler YES ❑ NO exceeded VC, was Project proMgr ./C1A notified? ,4. Were P Per custody YES ❑ NO procedures (relinquished/received) followed? 5. Were sample ID's listed YES ❑ NO on the COC? 5. Were samples ID's listed on ES ❑ NO sample containers? 7. Were collection date and time listed YE5 ❑ NO on the­111111 COCIII ? B. Were tests to be fSd YES ❑ NO iserformed listed on the CDC? 9. Did samples arrive in ICE YES ❑ NO proper containers for each test? 10. Did samples arrive in $ YES ❑ NO good condition far each test? 11. Was adequate YES ❑ NO sample volume available?' 12. Were samples received within ❑ ❑ YES YES ❑ NO ❑ proper holding time for requested tests? 13. Were acid preserved samples received at ❑ YES NO ❑ NO a pH of c2? 14. Were cyanide samples received at a pH s12? ❑ YES ❑ NO S. Were sulfide samples received at a pH a9? ❑ YES ❑ NO 15. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? •• 17. Were Sulfide/Cyanide received at a chlorine residual of a0.5 m/�? TGC/Volatiles are pH checked at time of analysis and recorded on the benchsheet " Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet 5arnplie PreserVx;ion; (Must be completed for any samples) "correctly y Preserved or with headspace) by addin were received incorrectly preserved and were adjusted accordingly g (circle one); H2SO' HNO3 HCI Time of preservation: NaOH If more than one preservative is needed. notate In comments below Notif- Note customer service immediatety for incorrect reservea s notify the state lab If dir tY P amaies. Obtain a new sample o� steed to analysed by the customer. Who was notified, date and time Valatiles Sample(s) were received with headspace COMMENTS: Ll'1. VVc Sending Facility: Swansboro WWFF 228 Georgetown Road Jacksonville, NC 28540 Phone: 910.389.8511 Project Manager: Mike Lutz Ons#ow Water & Sewer Authority SUBCONTRACT 228 Georgetown Road Jacksonville NC 28540 ODDER Subcontracted Laboratory: Environmental Chemists, Inc. 6602 Windmill Way Wilmington, NC 28405 Phone:(910) 392-0223 Fax:(910) 392-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: US CERTIFICATION # 37729 Work Order: S200319 Swansboro WRF Sample ID: S200319-01 Swan Fecal #1 WW Sampled: 0411512020 09:11 Sampled by: Mike Lutz Analysis Due Expires EnviroChem Lab ID Fecal Density 04/25/2020 04/15/2020 15:11 Containers Supplied: Sample ID: S200319-02 Swan Fecal #2 Analvsis AnarysEs Total Solids: (%) Containers Supplied. - Sample ID: S200319-03 Swan Fecal #3 Analysis Fecal Density s EnwroChem Lab ID-, 09;11 WW Sampled.' 0411512020 09:12 Sampled by; Mike Lutz lue Expires EnviroChem Lab ID 5/2020 04/15/2020 15:12 sue ::.: .•..Expires;. " .,.EnviroChem I,ab ID ',, , 5/,2020 '.:91122/2020 ,09 12 .`. WW Sampled: 0411512020 09.13 Sampled by; Mike Lutz lue Expires EnviroChem Lab ID 5/2020 04/15/2020 15:13 AnelyslS Due Ezp�res EnviroChem lab ID otaE:Solids.{%} 04/251`202Q ; 04/22/2020 99a3 .-.7771 Containers Supplied. Sample ID: S200319-04 Swan Fecal #4 WW Sampled- 0411512020 09.14 Sampled by: Mike Lutz Analysis Due Expires EnviroChem Lab ID Fecal Density 04/25/2020 04/15/2020 15:14 Analysis Due; Expires ;. ifnvirpChem Lab ID : ; T- LOWI Solids,{o/o) 04/2S/2020 , ,'04�2Z%Z�20 09;1�} . Containers Supplied: Sample ID: S200319-05 Swan Fecal #5 WW Sampled' 0411512020 09:15 Sampled by. Mike Lutz EnviroChem Report No:_ -2 0 2 c) —66-3 1 -1 Relinquished By Date Received By Date Page 1 of 3 V, W-V UP Onslow Water & Sewer Authority SUBCONTRACT 228 Georgetown Road Jacksonville ORDER 3 lfti' 5 A NC 28540 (Continued) Work Order: S200319 (Continued) Swansboro WRF Sample ID: S200319-08 Sboro Digestor A 001 SL Sampled, 0411512020 094-10 Sampled by,, Mike L rriz Analysis lue Due em Ch"'i Wb.D ..-�46 7471.B ..nyjro;.. Analysis Due Expires EnviroChem Lab ID pH 04/25/2020 04/15/2020 09:27 ,Ap:R lysj� 'D expires nVirQ010hi l;-abjP, 70W Sdiids 0 Analysis Due Expires EnviroChem[56 il) Se 2003 04/25/2020 04/29/2020 09:10 Mal Analysis "Puis Expires ;-;heFWLab Zn 200.7 04/25/2020 04/29/2020705:10 -Analysis Due Expires EnviroChem Lab rb Ammonia Nitrogen 04/25/2020 05/13/2020 09:10 Analysis Expires"," FfiVlroChiarfi-Ldb Total Mosiahorus 04/,.25/"202P..- Q5II,3/19 20 ftj Analysis Due Expires EnviroChem Lab ID Total Kjeldahl Nitrogen (TKN) 04/25/2020 05/13/2020 09:10 "Nitr6te+N.ItRte-N Ft 0412512020 i05/13/202Q.'Mlo IJ. Analysis Due Expires EnviroChem Lab ID Pb 200.7 04/25/2020 10/12/2020 09:10 ol VMS.: :Due Expires Efi MjrpChpm:Lab ID Cu 20! 04/25/2pZp 10/12/4-20, 09. Analysis Due Expires EnviroChem Lab ID Cr 200.7 04/25/2020 10/12/2020 09:10 Containers Supplied., EnviroChem Report No: Relinquished By Date Received By Date Page 3 of 3 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Coastal Farms and Residuals, LLC WWTP Name: Swansboro WWTP Monitoring Period: From 1/1/2020 To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tune/temp) ❑ Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ AILD (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Fui4her Reduce Pathogens"; Compost ❑ Hent Drying ❑ Heat Treatment ❑ Thenmophilic ❑ Beta Ray D1 Gamma Ray ❑ Pasteurization ❑ _ _ Class B: Alt. (1) Fecal Density El I Alt. (2) Process to Significantl.. Reduce Pathogens ❑ ' If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air D ing ❑ Com ostin ❑ Aerobic Digestion ❑ Anaerobic Digestion If ap plicable to alternative lternative performed (C1ass,A .or Class B)complete .the .following,monitoring data; Allowable Level Pathogen Density Number o na is Parameter in Sludge g ty Excee- Frequency Sample Tech - in Minimu Geo. Mean Maximu Units of Analysis Type 2 x 10 to the MPN 5,580 7,527 11,112 MPN/g 0 Annual Grab SM92214 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry AMU11 ua oaciena .3 mYIV per 4 grams (in lieu of fecal total solid (dry WQ Permit Number: WQ0034806 NPDES Number: WQ0023261 12/31/2020 Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ AIt. 9 (Injection) El Alt. 10 (Incorporation) F1 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 17 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not meet one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mike Lutz, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land Applier Name and /Title (if applicable)(type or print) 7ALL4e 4/30/2020 4/30/20 Signature of Preparer* Date Signature of Land pplier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26) DENR FORM PVRI= 02T (12/2006) COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled. May 19, 2020 The Cane 1.10 % Solids 6.39 PH Permit No. NC0057703 EParameter % I Mg/leg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg(Mg/Kg x 0.002) Nitrogen (TKN) 8.830 1 88,300.000 176.600 Phosphorus 1,390 13,900.000 27.800 Potassium 0.455 4,550.000 9.100 PAN injected)* 3.271 32,714.000 65.428 PAN (surface)* 2,828 28,284.000 56.568 Ammonia Nitrogen 0.886 8,860,000 17.720 Calcium 1.750 17,500.000 35.000 Calcium Carbonate E . --- ___ --- Magnesium --- 2,650.000 5.300 Sodium --- 8,540.000 17.080 Sulfur ___ --- --- Nitrate N / Nitrite N --- 22.000 0.044 Barium --- --- --- SAR 1.66 Chloride --- --- --- Iron --- --- --- Ceiling Concen. (Mg/]Kg) Aluminum --- 1,850.00 3.700 Arsenic --- 13.50 0.027 75 Cadmium --- 9.I8 0.018 85 Chromium --- 12.200 Copper --- 155.00 0.310 4,300 Lead --- 9.18 0.018 840 Mercury --- 1.420 0.003 57 Molybdenum --- 9.18 0.018 75 Nickel --- 9.18 0.018 420 Selenium --- 9.18 0.018 100 Zinc --- 709.00 1.418 7,500 Environmental Chemists, lnc. # 2020-08178 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N * Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. COASTAL FARMS AND RESIDUALS, LLC WQ0034806 The Cape W WTP 05/19/20 229,509 5.3608 05/19/20 142,858 5.1549 05/19/20 141,667 5.1513 05/19/20 301,076 5.4787 05/19/20 170,000 5.2304 05/19/20 209,524 5.3212 05/19/20 288,660 5.4604 Total 37.1577 Average 5.3082 Geometric Mean o I Fecal Coliform MPN / gram Geometric Mears of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Environmental Chemists, Inca 6602 Windmill Way, Wilmington, NC 28405 e 9t0.392.0223 Lab = 910.392.4424 Fax 'sa) 710 Bowsertown Road,-Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@enviranmento-ticllcmists.com Lewis Farms & Liquid Waste, INC. Date of Report: Jun 08, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-08178 Project ID: AquaNC-The Cape WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-20105 Site: Sludge 5/19/2020 9:50 AM Solid/Sludge Wooten Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 1850mg/kg 05/29/2020 Arsenic EPA 200.7 13.5 mg/kg 05/29/2020 Cadmium EPA 200.7 <9.18 mg/kg 05/29/2020 Calcium EPA 200.7 17500mglkg 06/29/2020 Chromium EPA 200.7 12.2 mg/kg 05/29/2020 Copper EPA 200.7 155 mg/kg 0512912020 Lead EPA 200,7 <9.18 mg/kg 05/29/2020 Magnesium EPA 200.7 2650mglkg 05/29/2020 Molybdenum EPA 200.7 <9.18 mg/kg 05/29/2020 Nickel EPA 200.7 <9.18 mg/kg 05/29/2020 Potassium EPA 200.7 4550 mg/kg 05/29/2020 Selenium EPA 200.7 <9.18 mg/kg 0512912020 Sodium EPA 200.7 8540 mg/kg 06/03/2020 Zinc EPA 2007 709 mg/kg 05/29/2020 Total Kjeldahl Nitrogen (TKN) EPA351.2 88300mg/kg 05/28/2020 Nitrate+Nitrite-Nitrogen EPA353.2 22.0mglkg 05/23/2020 Total Solids (%) SM 2540 a 1.10 % 05/19/2020 pH SM 4500 H a 6.39 units 05/26/2020 Ammonia Nitrogen SM 4500 NH3 0 8860 mg/kg 05/20/2020 Total Phosphorus SM 4500 P F 13900 mg/kg 05/26/2020 Mercury SW0467471B <1.42mg/kg 05/27/2020 Report k: 2020-08178 Page t of 3 -Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 o 910.392,0223 Lab o 910.392,4424 Fax 710 Bowser town load, Man teo, INC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 4 910,347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS in[ana�.Cnvirontncn(ttichemists.coln Lewis Farms & Liquid Waste, INC. Date of Report: Jun 08, 2020 8155 Malpass Corner Road Customer PO #: Currie NO 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-08178 Project ID: AquaNC-The Cape WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-20106 Site: 1 5/19/2020 9:55 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%} SM 2540 B 1.22 % 05/19/2020 Fecal Density SM 9221C E MPN 24 hr 503 229509 MPN/g 05/19/2020 Lab il) Sample ID: Collect DatelTime Matrix Sampled by 20-20107 Site: 2 5/19/2020 9:56 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.19 % 05/19/2020 Fecal Density SM 9221C E MPN 24 hr 503 142858 MPN/g 05/19/2020 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-20108 Site: 3 5/19/2020 9:57 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.20 % 05/19/2020 Fecal Density SM 9221C E MPN 24 hr 503 141667 MPN/g 06/19/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-20109 Site: 4 5/19/2020 9:58 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids (%) SM 2540 8 0.93 % 05/19/2020 Fecal Density SM 9221C E MPN 24 hr 503 301076 MPNIg 05/19/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-20110 Site: 5 5/19/2020 9:59 AM Solid/Sludge Wooten Test Method — Results Date Analyzed Total Solids (%) 5M 2540 B 1.00 % 05/19/2020 Fecal Density SM 9221C E MPN 24 hr 503 170000 MPN/g 05/19/2020 Report 9:: 2020-0817e Page 2of3' rinvironmental Chemists, Inc. 6602 Windmill Way, Wilmuigtori, NC 28405 O 910.392.0223 Lab a 910.392,4424 Fax 710 Sowsertown Road, Ivlanteo, NC 27954 6 252.473.5702 L.ab/Fax ` 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS into rLenvironment tichen3isfs.cnm Lewis Farms & Liquid Waste, INC. Date of Report: Jun 08, 2020 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2020-08178 Project ID: AquaNC-The Cape WWTP Lab ID Sample ID: Collect DatefTime Matrix Sampled by 20-20111 Site: 6 5/19/2020 10:00 AM Solid/Sludge Wooten Test Total Solids (%) Fecal Density Lab ID Sample ID: 20-20112 Site:7 Method SM 2540 B Results Date Analyzed 1.05 % 05/19/2020 SM 9221C E MPN 24 hr 503 209524 MPN/g 05/19/2020 COIIeCt Date/Time Matrix Sampled by 5/19/2020 10:01 AM Solid/Sludge Wooten Test Method Results Date Analyzed Total Solids N 0.97 % 05/19/2020 Fecal Density SM 9221C E MPN 24 hr 503 288660 MPN/g 05/19/2020 Comment: Sludge residuals and Fecal Density reported on a dry weight basis. pH reported on an as received basis. Reviewed by: wj SM 2540 B Report #:: 2020.08178 -- - Page 3 of 3 . Envircinmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 2840S 910,392.0223 Client: ,Ck�-7t` CU GLiI -Nt-:71 Date: i 9l �20 2 C) Report Number: c1...� Receipt of sample: ❑ YES ❑ t Delivered UPS ❑ FedEx ❑ ❑ ❑ YES ❑ NO NO N/A N/A 1. Were custody seals present on the cooler? Original temperature upon N/A 2. If custody seals were present, were they intact/unbroken? receipt ^C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank IR Gun 1D: Thomas Traceable B es- S/N 192511657 ❑ YES ❑ NO IR Gun CorrectiongFactoainst C:10.0 3. If temperature of cooler exceeded VC, YES ❑ NO was Project Mgr./QA notified? 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO S. Were sample Vs listed on the COC? YE5 YES ❑ ❑ NO 6. Were Samples 1D's listed on sample containers? NO 7, Were collection date and time listed on the COC? 8. Were tests to be performed listed on the COC? 9. Did samples arrive in proper containers for each test? MSCI 10. Did samples arrive in good condition for each test? 11. Was adequate sample volume available?' 12. Were samples received within proper holding time for requested tests? ❑ YES ❑ 11 Were acid preserved samples received at a pH of <2? ❑ NO 14. Were cyanide samples received at a PH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ f ES YES ❑ ❑ NO NO 16, Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ❑ YE5 ❑ iV0 17, Were Sulfide/Cyanide received at a chlorine residual of <0.5 rn/L? 18. Were orthophosphate samples filtered in the field within 15 minutes? TOC/Voilatiles are pH checked at time of analysis and recorded on the benchsheet, Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation; (Must be completed for any samples) incorrectly y preserved or with headspace) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H SO HNO z a s HCI NaOH Time of preservation: if more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles 5ampleis) were received with headspace COMMENTS: - DOC. QA.002 L) z M Vi E w L) F- z w z 0py D..c z w [C w U m N E W r hMo U m fr Z3 ul r C w N 'i U b'@ ld C Q LU a (E) JO dl Jauieluoo 0 ('} U` a U 4 U' d ('3 U a w a qeJ� Q J° Lo ags°dwn ANNUAL PA11-110CFN AND VECTOR ATTRACTION REDUCTION FORIM 102T Rules) Facility nle: Coastal Farms and Residuals, LLC WWTP i\;tme: The Cape W W r-P ylonitoring Period: From III12020 To Pathogen Red tic tinn (1i 1 Nl!'n!' nrr 1 in4% n,.-.... L...1:....+., l., W'Q 1'crmil Nun[ber-: WQ0034806 NPI)FS Number: NCO057703 1213 112020 ,nI o hinvnrl -Intl filtPrn:ItiVV tlflrtnrriled: - --- -I--- —. .I aVV) - x 7CA 14 141-1.,II. ,L, — wrr. -­ ...... '-''----- .. , Class A; Alt. A (timeltemp) ❑ Alt B (A1k Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Plut:eSs 10 Further Reduce Pathagertgs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce NthogezW': Compost ❑ Heat Drying ❑ Hcat Treattnenr ❑ Therniophdic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt, (i ) Fecal Density It. (2) Proccss to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class D only) indicate `Process to Si-nificanily Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting, ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Atiowable level Pathogen Density um cr o Parameter Frequency Sample na yuc�r in Sludge Excee- of Tech - in Geo. Mean �laximun Units � Type 2 x 10 to [he I 601 power WIN per gram of Fecal Coliform total solids CFU 1000 nlpn per gnnl nftoralsolid (dry [41,667 203,351 301,076 1<4PiN/g 0 Annual � Grab SM92210E wcighQ SaImonellabacteria 3MPNper 4ornms (in lieu of fecal total solid (dry coliform) wzi2ht) Vpetnr Atlrnrtinn RPduetinn (1 RA N( a' tOT 11fl'M _ Prnnen :.,,ti,-.,tn nlr.,.., 44t —4--A. Alt.l (VS reduction) Alt.l (VS reduction) ❑ All. 2 (40-day bench) ❑ Alt. 3 (30-dav bench) ❑ a[t. 4 (Spot:. 0- uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk_ Stabilization ❑ Alt 7 (Drying- Stable) ❑ Alt 8{Drying - Unstable i ❑ Alt. 9 (Injection) ElAh. 10 (Incorporation) EJ No vector attraction reduction alternatives were perfomlcd ❑ CERTIFICATION STATEMENT (please check the appropriate statement) l] "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogert requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC AZT .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or bolls of the requirements.) "This determination has been made tinder my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to derer mine that the pathogen and vector attraction reduction requirements have been met- l am a,,%are that there are significant penalties for false certification including line and imprisonment." Eric Youngs, ORC Weslev Wooten, President Preparer Name and Title (type or print) Land Applier Name and Title (if applicab lel(iype or print) (-29-zdzl — 4 rrsr_azn Signature of Pre Date Signature of L d Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) COASTAL FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 17, 2020 Morehead City 14.90 % Solids 6.57 nH Permit No. NCO026611 Parameter % Mg/Kg Dry Weight Pounds/Dry Ton (% x 10,000) (Mg/Kg (Mg/Kgx 0.002) Nitrogen (TKN) 6.310 63,100.000 126.200 Phosphorus 2.430 24,300.000 48.600 Potassium 0.388 3,880.000 7.760 PAN (injected)* 1.928 3,869.500 7.739 PAN (surface)* 1.904 3,777.000 7.554 Ammonia Nitrogen 0.048 476.000 0.952 Calcium 2.980 29,800.000 59.600 Calcium Carbonate E . --- ___ Ma nesium 0.423 4,230.000 8.460 Sodium 0.510 5,100.000 10.200 Sulfur --. Nitrate N / Nitrite N --- 15.000 0.030 Barium --- --- --- SAR Chloride --- --- 2.82 Iron --- --- --- Ceiling Concen. 1[ (Mg/Kg) Aluminum --- 8,740.00 17.480 Arsenic --- 5.53 0.011 75 Cadmium --- 3.35 0.007 85 Chromium --- 12.900 --- -.._ Copper --- 608.00 1.216 4,300 Lead --- 12.20 0.024 840 Mercury --- 0,659 0,001 57 Molybdenum --- 5.39 0.011 75 Nickel --- 12.70 0.025 420 Selenium --- 5.54 0.011 100 Zinc --- 673.00 1.346 7,500 Environmental Chemists, Inc. 2020-04492 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application; (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 9 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, ivlanteo, NC 27954 m 252.473,5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.51343 Lab/Fax i n ro(cbenvi rcni men to [chemis t s.com Town Of Morehead City Date of Report: Apr 14, 2020 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: Nate Johnson Report #: 2020-04492 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11058 Site: class b sludge 3/17/2020 10:05 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 80818/3510 <0.02 mg/L 03119/2020 Endrin (TCLP) SW 846 Method 80816/3610 <0.0005 mg/L 03/19/2020 Heptachlor (TCLP) SW 846 Method 8081B13510 <0.0005 mg/L 03/19/2020 Heptachlor epoxide (TCLP) SW 846 Method 8091B13510 <0.0005 mg/L 03/19/2020 Lindane (TCLP) SW 846 Method 8001 B13510 <0.0005 mg/L D3/19/2020 Methoxychlor (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 03/19/2020 Toxaphene (TCLP) SW 846 Method 8001 B1351 0 <0.05 mg/L 03/19/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 2,4,6-Trichlorophenol (TCLP) SW 646 method 8270/3510 <0.050 mg/L 03/20/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/20/2020 Cresol (TCLP) SW 646 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachloro-1,3-butadiene (TCLP) $W 846 method 8270/3510 <0.050 mg/L 03/20/2020 Hexachlorobenzene (TCLP) SW 846 method 6270/3610 <0.050 mg/L 03/20/2020 Hexachloroethane (TCLP) SW 845 method 827013510 <0.050 mg/L 03/20/2020 m + p-Cresol (TCLP) SW 646 method 827013510 <0.050 mg/L 03/20/2020 Nitrobenzene (TCLP) SW 846 method 8270/35€0 <0.050 mg/L 03/20/2020 o-Cresol (TCLP) SW 846 method 8270f3510 <0.050 mg/L 03/20/2020 Pentachlorophenol (TCLP) SW 846 method 827013510 <0.250 mg/L 03/2012020 Pyridine (TCLP) SW 646 method 827013510 <0.050 mg/L 0312012020 Paint Filter Test SW 846 Method 9095 A pass 04/14/2020 2,4,5-TP (TCLP) SW846 Method at 51A <0.003 mg/L 03/20/2020 2,4-D (TCLP) SW846 Method 6151A <0.003 mg/L 03/20/2020 1,1-Dichloroethylene (TCLP) SW846 Method8260/5030 <0.01 mg/L 03/31/2020 1,2-Dichloroethane (TCLP) SW846 Method 826015030 <0.01 mg/L 03/31/2020 Benzene (TCLP) SW846 Method 826015030 <0.01 mg/L 03/31/2020 Report #:: 2020-04492 Page 1 of 4 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 s 910.392.0223 Lab a 910.392,4424 Fax si3�s, 710 Bowsertown Road, Manteo, NC 27954 m 2.52.473.5702 Lab/Fax 255-A Wilmington fiighway, Jacksonville, NC 28540 9 910.347,5843 Lab/Fax ANALYTfCAL & CONSULTING CHEMISTS info[r17,cin+imnmentalcliemists.cotia Town Of Morehead City Date of Report: Apr 14, 2020 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: Nate Johnson Report #: 2020-04492 Project ID: Sludge Carbon Tetrachloride (TCLP) SW846 Method 826015030 <0.01 mg/L 03/31/2020 Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/31/2020 Chloroform (TCLP) SW646 Method 826015030 <0.01 mg/L 03/31/2020 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0,05 mg/L 03/31/2020 Tetrachloroethylene (TCLP) SW846 Method 6260/5030 <0,01 mg/L 03/31/2020 Trichloroethylene (TCLP) SW846 Method82601503a <0,01 mg/L 03/31/2020 Vinyl Chloride (TCLP) SWB46Method 826015030 <0.01 mg/L 03/31/2020 RCI Ignitabiiity EPA 1030 <0.8 mmisec 03/2712020 Cyanide EPA 335.4 <0.123 mg/kg 03/25/2020 Sulfide SM4500S0 0,39mg/kg 03/31/2020 Sludge Residuals Aluminum EPA 200.7 8740 mg/kg 03/30/2020 Arsenic EPA 2001 5.53 mg/kg 03/24/2020 Cadmium EPA 200.7 <3.35 mg/kg 03/24/2020 Calcium EPA 200.7 29800 mg/kg 03/24/2020 Chromium EPA 200.7 12.9mg/kg 03/2412020 Copper EPA 2oo,7 608 mg/kg 03/24/2020 Lead EPA 2007 12.2 mglkg 03/24/2020 Magnesium EPA 200.7 4230 mg/kg 03/24/2020 Molybdenum EPA 200.7 5.39mg/kg 03/24/2020 Nickel EPA 200.7 12,7 mg/kg 03/24/2020 Potassium EPA 200.7 3880 mglkg 03/24/2020 Selenium EPA 200.7 5.54mglkg 03/24/2020 Sodium EPA 20a.7 5100 mglkg 03/24/2020 Zinc EPA 2o0.7 673 mg/kg 03/24/2020 Nitrate+ N itrite-N itrogen EPA353.2 15.0mg/kg 04/01/2020 Total Solids (%) SM 2540 8 14.9 % 0311812020 pH SM 45oa H e 6.57 units 04/10/2020 Ammonia Nitrogen SM 4500 NH3 C 476 mg/kg 03/18/2020 Report *;: 2020.04492 Paae 2 of 4' n.vironm.en.tal Chemists, Inc. 6602 Windmill Way; Wilmington, NC 28405 a 910.392,0221 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ` 252.473.5702 Lab/Fax (s+�` 255-A Wilmington Highway, Jacksonville., NC 28540 a 9'10.347.5843 Lab/Pax ANALYTICAL & CONSULTING CHEMISTS info a@environnieiilalcliemists.cprm Town Of Morehead City Date of Report: Apr 14, 2020 706 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: Nate Johnson Report #: 2020-04492 Project ID: Sludge Total Kjeldahl Nitrogen (TKN) SM 4500 arg B 63100 mg/kg 03/20/2020 Total Phosphorus 5M 4500 P F 24300 mg/kg 04/01/2020 Mercury SW840 7471e 0.6590 mg/kg 03/19/2020 TCLP Metals Arsenic EPA 200.7 <1 mg/L 03/23/2020 Barium EPA 200.7 <1 mg/L 03/23/2020 Cadmium EPA 200.7 <1 mg/L 03/231202D Chromium EPA 200.7 <1 mg/L 03/23/2020 Lead EPA 200.7 <1 mg/L 03/23/2020 Selenium EPA 200.7 <1 mg/L 03/23/2020 Silver EPA 200.7 <1 mg/L 03/23/2020 Mercury EPA 245.1 <0, 0002 mg/L 03/25/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11065 Site: 001 3/17/2020 10:10 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids (%) SM 2540 B 30.4 % 03/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 30304 MPNIg 03/1712020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11066 Site: 002 3/17/2020 10:12 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids (%) SM 2540 B 16.0 % 03/18/2020 Fecal density SM 9221C E MPN 24 hr 503 57393 MPN/q 03/17/2020 Lab lD Sample ID: Collect Date/Time Matrix Sampled by 20-11067 Site: 003 3/17/2020 10:14 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids (°/a) SM 2540 6 24.1 % 03/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 66281 MPN/g 03/17/2020 Report M: 2020-04492 PaeP 3 nE 4 Environment l Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 = 910.392.0223 Lab o 910.392.4424 Fax 5 h} 710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.34T5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infofa3environmenttilcliemists.com Town Of Morehead City Date of Report: Apr 14, 2020 106 Arendell Street Customer PO #: Morehead City NC 28557 Customer ID: 09020011 Attention: Nate Johnson Report #: 2020-04492 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11068 Site: 004 3/17/2020 10:16 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids (%) SM 2540 B 17.3 % 03/18/2020 Fecal Density SM 9221C E MPN 24 hr 503 53303 MPN/g 03/17/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11069 Site: 005 3/17/2020 10:18 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids (%) SM 2540 B 18.0 % 03/18/2020 Fecal Density SM 9221 C E MPH 24 hr 503 51112 MPN/g 03M 7/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11070 Site. 006 3/17/2020 10:20 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids SM 2540 B 23.9 % 03118/2020 Fecal Density SM 9221C E MPH 24 hr 503 22585 MPN/g 03/17/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-11071 Site: 007 3/17/2020 10:22 AM Solid/Sludge Nate Johnson Test Method Results Date Analyzed Total Solids (%) SM 2540 B 16.6 % 03/18/2020 Fecal Density SM 9221C E MPH 24 hr 503 96677 MPN/g 03/17/2020 Comment: Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2020-04492 Pape 4 of 4 6"Wronrnental Chemist, inc., 'Nilminoon, NC Lab 994 602 Windmill `Nay .Vilmington, .VC 284O5 310.342.0223 Sample Receipt Checklist Client; � J Date: qepvrt Number. V Rt of sa eceipmple: ❑ YES y0 Delivered �IPS p FedEx ❑ Other p ❑ YES 13 VO N/A 1. ere custody seals present on the covler7 N/A 2. if custody CJriginall temperature upon receipt T—'C seals were present, were they intact/unbroken? °w temperature taken; Corrected temflerature voan receipt IR Gu11 n ICi: Thomas Traceable 5/ly 192g}1fi57ture Blank R Gun Correcti; . . ainsi Bottles ❑ YES 0 VO 3, if tem -actor -C. 0.p YES temperature of Cooler exceeded b'C, was Project M VO 4. Were proper custo Br•/OA notified? p V0 dY procedures (relinquished/received► followed? 5, Nere samplt Ip's Iisttd an the COC7 'rE5 i❑ VO 6 Were samples 10'5 listed an same}e containers? YES 3 VO 7. 'Nere collection date and time listed an the CaC7 YES 0 VO 8, 'Nert tests to be YES Q V0 p performed listed on the COC7 9. 0id samples arrive rn proper containers for each test? f ES VO 15. Did samples arnve in f ES D VD 1I• 'Nas adequate sa11 mple good ume available? r each test? 1E$ ❑ VO 12. `Nere samples received within qro ❑ {ES D V0 o per h'0 r`i p YES 12 Were aced reserved sarr+oles received at a time forrequestedtests? 40 14. 'Nere cyanide samples received at a oN > pal of <27 ❑ /E5 D VQ 15• Were sulfide samples r 11? YES D VO q received at a pH ,g� C3 r£5 0 VO 16• Were NFf3%TI(N/Phenol received at a chlorine residual or <�.5 m/L? 17. were Sesifide/Cyanide received at a chlorine residual of < f ' 0.5 m/E7 r• i r ccNolatiles are 13H checked at time of anafvsis and recorded on the benchsheet. Bacteria samples are checked for Chlorine at time of analvses and recar ded an the benchsheet Sampft PrestrvatIon: 41ust be completed for an 71 Sample{s) V sample{s1 incorrect! by adding vere reterved ;ncorrectl y preserved Or with headspaCe? (circfe one):-I,SC}d -{NO V preserved and were adjusted accordingly 11 7;,ne of oreservation: �Cl 'laoH Note: *lot+fy customer sery ce :mm f more than one ore5ery 5 ediatery for n aCIVe needed, n notify the state lad d die , corra�pV preserved sam ata[e :n Comm ected .o anaivted b r Dies. Cbtarn a ew sam i Comments oeloW Voiatlles v •he "us, Nh 0 e flr Samole[5j Q waz r'or'f'ed, late and rirne, MMENT5: vere received with n111 eadsaace �C? 'C 4 N N a",, Z C � O w rn rnX r- LL cv rya fVdD C N W c7 b� U_ N iL W k. tD z C Lpp� I M U z 0 a F- U u w Q cY s a W 2 LU Q U z COASTAL FARMS AND RESIDUALS, LLC WQ0034806 Morehead City WWTP a_c41foikzii 03/17/20 0,304 4.4815 03/17/20 57,393 4.7589 03/17/20 66,281 4.8214 03/17/20 53,303 4.7268 03/17/20 51,112 4.7085 03/17/20 22,858 4.3590 03/17/20 96,677 4.9853 Total 1 32.8414 Average 1 4.6916 Geometric Mean ':1':€€€€ Fecal Coliform MPN 1 gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. ANNUAL PATHOGEN ANO YFCrOR ATTRACTION RuwcriO!N FORM (503 Rules) Facility Nwne: C'rrasaal Fitrttls ;And RCsidtlals, LLC' WQ Permit IVutniter: WQ0034$O6 WVVTP Nance: Town a7t:Morehend City LXPDES Number: NCO026611 Nionitorin;Period: From _ [A;-1]20 Tn 12�3l1?i)2tF Pathogen Reduction (40 C:f~ lx .15OS32) - I'1e39e indicate level achieved and alternative performed: Class A: Alternative E — -�1'1�11` '❑ Altcmativt:3 L:Aterrtali� e �i 0 ❑ — alltemtt[ive G ❑ lrapplicuble to altertaatis°e Performed (Clusx A Dais) indicate "Process to Further Reduce Pq#iuleens": Conloost C7 Flcat Dtyina [] lie rt Trcaatinent LJ i'hcrtttop[►iiic ❑ -- Beta Ray El Gamma RaY L Pc, .teurizntiola Class B. I Alternative I > f applicable to alternative perfora-ted I.inie Stabilization ❑ Anaerobic Digaslion ❑ If applicable, to alternative ierfe Paratn,tcr Allowablu Level ita ,�tt:cigti � !0 #o th_ htnhi 6th Power po., graln of Fecal Colifonti ta3tat solids t FU iijOD inpn per +Sraan of total solid (dry we'g tt) almonella bractcris ? MIN pert grams (cu lies, of 1a�3! total solid (dry colif6an)wai!I41) Air 8 unlr•j Indic;ttr "t'1'Oces5 to Class A or Clam I3) co PathDgen DLnsity inintural Geo, the folio mutrj Units EXCCC- 22,858 1 119,162 196.h77 1 l'vll-IN/g, 1 0 Reduce Pnthoaens": Aerobic DiEestivil U lM1 monitoring data: rr Fuen�y Sample7`11iyltcta. Analysis VM .+l ecli- Annual I Grab J sstmz.LCE Vector Attraction Reduction (40 CFR -503,33) - Please indicate option performed: :Alt. i (1.'S rciluetion (=i rift. 2 (40-day bench) Cl Alt. 3 00-day btneh) Ll JAIt. 4 (Spec, d, tiptake) `7 :Alt. a (14-Day Acrobic) ❑ Alt. 5 (Alk_ Stabilization ❑ Alt 7 tDrying - Stable) ❑ tAll. A(I}rying - Unstable) G Aft. 9 (injection) ❑ Alt. 10 (incorporation) [ vector �ttr�ctirzta radtaClion altulraatives ��et+ perfr�rmcd ❑ CERTI FICATFON STATEMENT (please check (lie appropriate statement) "1 certify, under penalty tjlasv, that The pathogen requirernents in Oft CFR 503.32 and the vector atiraction reduction requirement in 40 CFR 503-33 have been wet." 1;7 "I certify, under penalty of law, thaat the p:athoacn requirearaents in 40 CFR 503,32 and the vector attraction reduction requirement in .40 CFR 503,3; Inive not been met." (Please note iryaLi clteCk y this statement attach an ex Ianation why yott have not met olte (ar botit of the requirements.) "Thiti delet•mltlation [ins been made under my direction and snpet-vision in accordance with the system designed to eusrlre that qualified personnel properly gather and evaluate the inl'ormatimi used to determine thal Ilse p;rtiiogen and vector attraction reduction requirements have been met. I Lim '11w are that there are significant penatlties for false cerli(icalion including fans: and iniprisonment." Chad Sutton. 14rVrP Superintendent Wesley Wooter, President Preparer Nance a d ritle type ter punt) l.:artd Applier NL111ae and'Fidt: (if applicablc){ttpe Dr Ftlt:t) Sismatttr ul'I'rcparc�r* l7ais Si =nature ot'Lalpplier (it"upplscahle,I -�Y [late 'Preparcr is dchned in 40 C:rk fart 503.9(ri ;and !.)-A X'C'rACYI 1 102 (26 ) DEER FORM PVRF 503 (12i7008i 2020 APPLICATION SUMMARY c \ \ \ \ \ \ \ \ \ \ . - 52 : :a|.lam r:;,A,=!im _ �lEI�:Q;°,u;• _ §[`i2:m: CC :;:.,-:■:: |(! :�:•. : \} 3 �k (Oq uv \) � /) /kA k� k� k�\ \} 3 �k (Oq uv \) � /) /kA k� k� k�\ FIELD APPLICATION SUMMARIES ))/ K § k�} fn CD 10 (��:�: §: E! «�§!!;l: RM ».a:&:I!?!I! am-: ! 2 f:�: • : : : !!!� k( .§ ! vftZ §27 ( § u ) § (/\ «E! | / � W w z 0 o e o 0 P O Q o O P1 O 00 O 4 0 0 0 N i : 0 7 1 1 : : m O CDe p O C 6 O O O a p O O O p O d O o O O O O O O O p p O d o O O O O O G6 00 W 00 00 00 GO G6 00 c0 W 00 � v e e a v � a v � •r e O O b n vs 0 0 0 0 0 0 0 0 C 0 4 oo 0 o 0 0 vl i I 6 1 i I 2 , CC � ()` � $ ' \ } } } a !<;»:0101 ;zl± ( J7 �( 7m« ur7 @ \! aR/ 2G- ®�} /q« 4§I § } k�\ § z / J§� ■ ;��� E dw2 �,�, - W w � 3 a a G Fs. r .cs U w cq O O C? d d � N N : � E° '• n m g o :� m E � E�� coo E i u? v S C C e c O C 1 to o O M A O � f o � M � 1 1 I 0 i 0 1 I u c�� :cl)€ z€ ❑ \/\ )7/ uG) u u@ƒ u J k�\ 27« «A§ k�\ (E:=:=:�:�: 2:I:§:4:�:-��:k�\:\|/| ( FIELD LOADING RATE REPORTS � Q N T 6Mi a � N •� � S - G K v 6 Y •� N c r� U Y� O G q Z u VR' � O O _ a p c O U � 3 z t Gn ca z ry r ee E LQ. N = 'a U m e � m a Q O CO 3 O w m 6 10 _ E w `" � M C a a Q' IS 9 e G r ^ a � � U � � d o W E 0 u: G U> d � .. C L E Y O R. 6 - c O a C w a u M N o O e q o o h O d Z c o ei e e c o o Ic c d Y a �' N INII VMI N T u 7 a — Q LM IG VI M � N 9 0. rn Na n vi C N n G N vO1i N �n n N] ao c C a CI h o Q a w fJ q� ceo Ci Qe `�' •may ,o °D � a rs pMp ep � ry o c e e c o o c p p c o G G o G CI G p p Cf � p M 0 o d o o d c e c ei ei c� c e o 0 v o c o o c 0 e e e c o o c o e a Q Gi a ei w erS O O O O O C O O G O C C p ^O N VI e7 N O Ci Ci p p p om N m U •n d In m Q o In F M © N M VO O O G O O O C O 0• O O C C O C O p O p n+ Ci O W O M 0 In E R E E u s r y s E U VI e F M eV „Q,•j '•f N r m YI N F M P1 b O Y vni M e � r o omo n N 'o Q n vei vFi n n n tf O q p p O O O O e p `D 0 o D .e O ' D � 4 � O Y DG Cp .Gi y O qp O C � A t C O F � F G O c w � v o ^ L' a 7 N `v p � d V O N CC b s nL u 3 � G T O o a •s - c o = W w F C• C a � m O d C R w0 4 O y Y V 0 a 0 N N_ LL Uj a. O 6L Of Z w O SOIL ANALYSIS REPORTS It should also be noted that the Wilbur Corbett — Field WC -I contained a pH of 5.6 and contained a recommendation of 0.3 tons of lime per acre recommendation. The current pH on these fields are not reflective of the liming amendments applied to the field in late December of 2019 (1 ton/acre). Coastal Farms and Residuals, LLC will continue to monitor this field in the future and make any necessary adjustments to pH as needed. Martin Mabe Agronomist §kk k§/ tea/ k/f § �LLL �}2 /k $m #� rl S � U)co kd§ kEn ®U )-§ $§J \ 7 k E E 0 § k i <