WQ0013263_Residual Annual Report 2020_20210202

Initial Review
Reviewer Thornburg, Nathaniel
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00013263
Applicant/Permittee Town of Boone
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes r No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Rease provide inforrafion on the person to be contacted by N B Staff regarding electronic subnittal, confirmation of receipt, and other correspondence.
................................................... _......... . . . ...... . . . ......... . . .... . . ...... _ -
Name * Mike Everett
Email Address*
[e-mail]
Project Information
........ ......... .................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
828-268-6270
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0013263
Fbs Current Existing pernit number
Applicant/Permittee Address* 201 Casey Ln, Boone, NC 28607
Facility Name * Town of Boone DCAR
Please provide comments/notes on your current submittal below.
listed physical address
mailing address is PO Drawer 192, Boone 28607
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Biosolids report.pdf 5.11MB
Upload only 1 PrTdocurrent (less than 250 vB). Miltiple documents rust be corrbined into one RJFfile unless file is larger than
upload lirrit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date
hf�x "' rr
2/2/2021

Towle oiBoone
January 29 2021
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Attached is the Town of Boone's 2020 Class A Residuals annual report.
Our system employs a thermal drier by a natural gas steam generator. Heat is transferred to the
residuals through a hollow rotor via a series of concentric disks in the drier. The system is
manufactured by Atlas-Stord, Inc. The enclosed report includes a technical specification section
for your reference.
To assist your review, we have included summaries on production volume, the quantity
distributed, and information on each recipient.
We tested for quarterly for metals and fecal coliform and all our test results were within our
permitted requirements.
We will promptly provide any additional records you may request to verify compliance of this
system with the regulations for Class A residuals distribution. If there is any need please contact
me at [phone]
Sincerely,
Mike Everett
Chief Operator
cc: Rudy Broschinski, Wastewater Treatment Superintendent
Rick Miller, Director of Public Utilities
P.O. DRAWER 192 • BOONE, NORTH CAROLINA 28607

ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
FACILITY NAME: Town of Boone Jimmy Smith WWTP PERMIT #: WQ0013263 COUNTY: Watauga
FACILITY TYPE(please check one): = Surface Disposal (complete Part A (Sources(s) and "Residual IN" Volume Only) and Part C)
ODistribution and Marketing (complete Parts AB, and C)
WAS THE FACILITY IN OPERATION DURING TBE PAST CALENDAR YEAR? YES X NO If NO, skip Parts A Band C and certify form below.
Part A*
Part B*
Month
Sources
(Include NPHS # if applicable)
Volume
Recipient Information
Amendment/
Bulding Agent IN
Residual IN
Product OUT
Name(s) Volume Intended Use(s)
(dry tons)
January
Town of Boone Permit # NCO020621
None
***
58.94
0.0
February
Town of Boone Permit # NCO020621
None
59.48
Please see attachment for
0.0
Please see attachment
March
ITown of Boone Permit # NCO020621
None
73.38
recipient information on
290.00
April
Town of Boone Permit # NCO020621
None
48.29
a monthl basis.
158.0
May
Town of Boone Permit # NCO020621
None
46.98
153.75
June
Town of Boone Permit # NCO020621
None
73.52
0.0
July
Town of Boone Permit # NCO020621
None
58.12
0.0
August
Town of Boone Permit # NCO020621
None
11.56
0.0
September
Town of Boone Permit # NCO020621
None
102.93
77.5
October
Town of Boone Permit # NCO020621
None
59.02
10.00
November
Town of Boone Permit # NCO020621
None
45.31
0.0
December
Town of Boone Permit # NCO020621
None
85.72
26.3
Totals:
Annual (dry tons)
723.25
715.5
Amendment(s) used: None Bulking Agent(s) used: None
*If more space is required than geiven, please use the comment space provided below or attach additional sheet(s).
Comments:
Part C
Facility was compliant during calendar year 2020 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality x YES NO. If NO, please provide a written description of why the facility was not compliant.
1. All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified lab results are attached.
2. All operations and maintenance requirements were compiled with or, in the case of deviation, prior to authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
'I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING
ORMATION, CLUDING THE POSSIBILITY OF FIRES AND Ui1PRISONMENTS FOR SNOWING VIOLATIONS."
S TURE OF PERM[TTEE DATE ` SIGNATURE OF PREPA ERDATE _ vZ
(If different from Permittee) *Preparer is defined in 40 CFR Part 503.9®

BACKGOUND INFORMATION
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
City Boone State NC Zip 28607
Facility Contact Mike Everett Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. REPORTING PERIOD 4. NPDES PERMIT NUMBER
YEAR MO DAY IYEARI MO DAY NCO020621
FROM 20 1 1 TO 20 1 12 1 31
6. FACILITY STATUS 7. TOTAL ANNUAL VOLUME OF SEWAGE SLUDGE
X Preparer of sewage sludge
Land applier 11 0.0 1 0.0 T-2--9-0.0-1 21158.01153.81 0.0
Owner/operator of surface disposal site
Owner/operator of incinerator 31 0.0 1 0.0 1 77.5 1 41 10.0 1 0.0 1 26.3
Units: M
(metric tons; dry weight)
Other: dry tons
5. SLUDGE PERMIT NUMBER
WQ0013263
8. FINAL USE AND DISPOSAL METHOD
Land application
Surface disposal
Unlined or OLined
Incineration
X Other, explain Bulk Distribution
See cover letter
9. Name and address of persons performing final use or disposal (attach additional sheets if necessary)
OX Same as preparer
Facility Name
Facility Name
Address
Address
City State Zip
City State Zip
Facility Contact Phone
Facility Contact Phone
Volume of sludge received from preparer
Volume of sludge received from preparer
Final use/disposal method for sludge
Final use/disposal method for sludge
Facility Name
Facility Name
Address
Address
City State Zip
City State Zip
Facility Contact Phone
Facility Contact Phone
Volume of sludge received from preparer
Volume of sludge received from preparer
Final use/disposal method for sludge
Final use/disposal method for sludge
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared umder my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Area Code and Phone
Mike Everett Chief Operator
[phone]
Signature
Ad'ootd,
Fmen-Tb-
Date Signed
l-a�-al

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY 2. NAME AND ADDRESS OF FACILITY OWNER
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant Facility owner's Name Town of Boone
Address 201 Casey Lane Address P.O. Box 192
P.O. Box 192
City Boone State NC Zip 28607 City Boone
Facility Contact Mike Everett Phone [phone] State NC Zip 28607
Signatory
3. MONITORING PERIOD 4. NPDES PERMIT NUMBER F 5. SLUDGE PERMIT NUMBER
YEARI MO I DAY I IYEARIMO DAY NCO020621 WQ0013263 (Class A)
FROM 20 1 1 TO 20 3 31
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
11,800
-
MG/KG
1
Grab
SW846-601OD
Sample Measurement
1.26
75
MG/KG
1
Grab
SW846-601 OD
Sample Measurement
0.962
85
MG/KG
1
Grab
SW846-6010D
Sample Measurement
18,100
-
MG/KG
1
Grab
SW846-601OD
Sample Measurement
358
4300
MG/KG
1
Grab
SW846-601OD
Sample Measurement
12.1
840
MG/KG
1
Grab
SW846-601 OD
Sample Measurement
3010
-
MG/KG
1
- Grab
SW846-601OD
Sample Measurement
0.513
57
MG/KG
1
Grab
SW8467471 B
Sample Measurement
3.72
75
MG/KG
1
Grab
SW846-601 OD
Sample Measurement
13
420
MG/KG
1
Grab
SW846-601 OD
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike E verett Chief Operator
Area Code and Phone
[phone]
Signature A
Date Signed

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact Mike E verett Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City
State
Boone
NC
Zip 28607
3. MONITORING PERIOD 1 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY I YEAR MO DAY NCO020621 W00013263 (Class A)
FROM 20 1 1 1 TO 1 0 1 3 31
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry wei ht)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
4,360
-
MG/KG
1
Grab
SW846-601OD
Sample Measurement
2.49
100
MG/KG
1
Grab
SW846-601 OD
Sample Measurement
1,860
-
MG/KG
1
Grab
SW846-601OD
Sample Measurement
769
7500
MG/KG
1
Grab
SW846-601OD
Sample Measurement
94.8
-
MG/KG
1
Grab
SM 2540B
Sample Measurement
8,590
-
MG/KG
1
Grab
SM4500NH3D
Sample Measurement
3.3
-
MG/KG
1
Grab
SM450ONO3E
Sample Measurement
33,200
-
MG/KG
1
Grab
SM450OPE
Sample Measurement
30200
-
MG/KG
1
Grab
SM45000rgB
Sample Measurement
5.5
-
su
1
Grab
SM 4500-H-B
NA
10800
-
NA
1
Grab
Calculation
I NA
3.37
9.99
NA
1
Grab
I Calculation
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Mike Everett Chief Operator [phone]
Signature Date Signed
J-aq✓a�

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone
Facility Contact
Signatory
State NC
Mike Everett
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. MONITORING PERIOD 4. NPDES PERMIT NUM F 5. SLUDGE PERMIT NUMBER
YEAR MO DAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 20 4 1 TO 20 6 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry wei ht)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Sample Measurement
12,300
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
1.84
75
MG/KG
1
Grab
SW846601 OD
Sample Measurement
0.674
85
MG/KG
1
Grab
SW846601 OD
Sample Measurement
18,200
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
288
4300
MG/KG
1
Grab
SW846601 OD
Lead
Magnesium
Sample Measurement
11.7
840
MG/KG
1
Grab
SW846601 OD
Sample Measurement
2630
-
MG/KG
1
Grab
SW846601 OD
Mercury
Molybdenum
Nickel
Sample Measurement
0.231
57
MG/KG
1
Grab
SW8467471 B
Sample Measurement
3.49
75
MG/KG
1
Grab
SW846601 OD
Sample Measurement
12.7
420
MG/KG
1
Grab
SW846601 OD
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike Everett Chief Operator
Area Code and Phone
[phone]
Signature ,)y) A
Date Signed l

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone
Facility Contact
Signatory
State NC
Mike Everett
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip
28607
3. MONITORING PERIOD 1 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 20 4 1 TO 1 0 1 6 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Sample Measurement
3900
-
MG/KG
1
Grab
SW846601OD
Sample Measurement
1.56
100
MG/KG
1
Grab
SW846601OD
Sample Measurement
1,510
-
MG/KG
1
Grab
SW8466010C
Sample Measurement
702
7500
MG/KG
1
Grab
SW846601 OD
Sample Measurement
90.2
-
MG/KG
1
Grab
SM 2540B
Sample Measurement
8,890
-
MG/KG
1
Grab
SM4500NH3D
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
1.2
-
MG/KG
1
Grab
SM450ONO3E
Sample Measurement
32,300
-
MG/KG
1
Grab
SM450OPE
Sample Measurement
31000
-
MG/KG
1
Grab
SM4500NOrgB
Sample Measurement
6.0
-
su
1
Grab
SW8469045
NA
11100
-
NA
1
Grab
Calculation
F- NA
1 2.76
9.99
NA
1
Grab
Calculation
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Mike Everett Chief Operator [phone]
Signature &OLOL
Date Signed /�� a
a

CLASS A RFSint IAI S PCII I I ITANT I IRA C
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone
Facility Contact
Signatory
State NC Zip 28607
Mike Everett Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip
28607
3. MONITORING PERIOD 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEARI MO I DAY I IYEAR MO DAY NCO020621 W00013263 (ClassA)
FROM 20 1 7 1 1 1 TO 1 20 1 9 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
18,000
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
2.4
75
MG/KG
1
Grab
SW846601 OD
Sample Measurement
4.29
85
MG/KG
1
Grab
SW846601 OD
Sample Measurement
18,000
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
390
4300
MG/KG
1
Grab
SW846601 OD
Sample Measurement
15.9
840
MG/KG
1
Grab
SW846601 OD
Sample Measurement
2920
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
0.43
57
MG/KG
1
Grab
SW8467471 B
Sample Measurement
6.49
75
MG/KG
1
Grab
SW846601 OD
Sample Measurement
15.5
420
MG/KG
1
Grab
SW846601 OD
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike Everett Chief Operator
Area Code and Phone
[phone]
Signature#W-W—L d &�F
Date Signed 1,��
/ -al

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact Mike Everett Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. MONITORING PERIOD 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 20 7 1 1 1 TO L 20 1 9 1 30
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
I Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
3510
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
2.37
100
MG/KG
1
Grab
SW846601 OD
Sample Measurement
1320
-
MG/KG
1
Grab
SW846601 OD
Sample Measurement
952
7500
MG/KG
1
Grab
SW846601 OD
Sample Measurement
96.0
-
MG/KG
1
Grab
SM 2540B
Sample Measurement
11,900
-
MG/KG
1
Grab
SM4500NH3D
Sample Measurement
0.5
-
MG/KG
1
Grab
SM450ONO2B
Sample Measurement
31700
-
MG/KG
1
Grab
SM450OPE
Sample Measurement
41400
-
MG/KG
1
Grab
SM4500NOrgB
Sample Measurement
6.1
-
su
1
Grab
SW8469045
NA
14800
-
NA
1
Grab
Calculation
NA
1.7
9.99
NA
1
Grab
I Calculation
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Mike Everett Chief Operator [phone]
Signature AdLoRL
Date Signed
0 >� aq- D1

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY 2. NAME AND ADDRESS OF FACILITY OWNER
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant Facility owner's Name Town of Boone
Address 201 Casey Lane Address P.O. Box 192
P.O. Box 192
City Boone State NC Zip 28607 City Boone
Facility Contact Mike Everett Phone [phone] State NC Zip 28607
Signatory
3. MONITORING PERIOD 4. NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEAR MO DAY YEAR MO DAY NCO020621 WQ0013263 (Class A)
FROM 20 10 1 TO 20 1 12 31
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Sample Measurement
15300
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
2.60
75
MG/KG
1
Grab
EPA6010D
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Sample Measurement
1.5
85
MG/KG
1
Grab
EPA601 OD
Sample Measurement
14,200
-
MG/KG
1
Grab
EPA601OD
Sample Measurement
443
4300
MG/KG
1
Grab
EPA6010D
Sample Measurement
17.2
840
MG/KG
1
Grab
EPA6010D
Sample Measurement
2820
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
0.3200
57
MG/KG
1
Grab
EPA7471B
Sample Measurement
4.9
75
MG/KG
1
Grab
EPA6010D
Nickel
Sample Measurement
16.1
420
MG/KG
1
Grab
EPA6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike Everett Chief Operator
Area Code and Phone
(828 268-6270
Signature
Date Signed a✓ ;,Q, i7l

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact Mike Everett Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC Zip 28607
3. MONITORING PERIOD C4_NPDES PERMIT NUMBER 5. SLUDGE PERMIT NUMBER
YEARI MO DAY EAR MO DAY NCO020621 W00013263 (Class A)
FROM 20 r20
10 1 TO 12 1 31
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sample Measurement
3510
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
3.1
100
MG/KG
1
Grab
EPA6010D
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Sample Measurement
1090
-
MG/KG
1
Grab
EPA601 OD
Sample Measurement
829
7500
MG/KG
1
Grab
EPA601 OD
Sample Measurement
89.9
-
MG/KG
1
Grab
SM2540G
Sample Measurement
683
-
MG/KG
1
Grab
EPA350.1
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
31.3
-
MG/KG
1
Grab
EPA353.2
Sample Measurement
14,000
-
MG/KG
1
Grab
EPA365.1
Sample Measurement
35600
-
MG/KG
1
Grab
EPA351.2
Sample Measurement
6.0
-
su
1
Grab
EPA9045D
NA
10800
-
NA
1
Grab
Calculation
NA 1
2.74
9.99
NA
1
Grab
Calculation
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print) Area Code and Phone
Mike E verett Chief Operator 1(828)268-6270
Signature jDate Signed / _ -Q � r)
l� - 1

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be analyzed than thise requred to be summarized on this form.
Permit Number WQ0013263 _ Laboratory 1) Research & Analytical Labs Inc.
Facility Name Town of Boone 2Water Quality Services, Inc.
NPDES # NC0020621 3)Pace Analytical Services LLC
or WQ # (residual only facilities)
WWTP Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Residual Analvsis Data
Date Sampled (Grab)
I Ceiling Con
1/10/2020
4/23/2020
7/16/2020
Quarter
Limit mg/kgl
1st
I 2nd
1 3rd
110/28/20201
4th
17-61`4MULers t1ny1R9 ury
weight)
Aluminum
NA 11,800
12300
18,000
15,300
Arsenic
75 1.26
1.84
2.4
2.6
Cadmium
85 0.96
0.674
4.29
1.5
Calcium
NA 18,100
18200
18,000
14,200
Copper
4300 358
288
390
443
Lead
840 12.1
11.7
15.9
17.2
Magnesium
NA 3,010
2,630
2,920
2,820
Mercury
57 0.5130
0.2310
0.43
0.3200
Molybdenum
75 3.72
3.49
6.49
4.90
Nickel
420 13.0
12.7
15.5
16.1
Potassium
NA 4,360
3,900
3,510
3,510
Selenium
100 2.49
1.56
2.37
3.10
Sodium
NA 1860
1,510
1,320
1,090
Zinc
7500 769
702
952
829
Ammonia Nitrogen
NA 8590
8,890
11,900
683
Nitrate -Nitrite Nitrogen
NA 3.3
1.21
0.6
31.3
Total Phosphorous
NA 33200
32,300
31,700
14,000
Total K'eldahl Nitrogen
NA 30200
31000
41,400
35600
pH
NA 5.5
6.0
6.1
6
PAN
NA 10800
11,100
14,800
10800
SAR
9.99
3.37
2.76
1.70
2.74
% Total Solids
NA
94.8
90.2
96.0
89.9
X &Ir(SIGNATURE OF`TA, F E RE / -ATE/ a'
( )
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
Significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From l/l/2020 To 3/31/2020
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 Ll
Alternative 2 Ll
Alternative 3
Alternative 4 El
Alternative 5 Rl
I Alternative 6 El
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost 11
Heat Drying Rl
Heat Treatment El
Thermophilic
Beta Ray Cl
Gamma Ray Ll
Pasteurization El
It
Class B:
Alternative 1 El
Alternative 2 Ll
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air DryingL1
Com osting
Aerobic Digestion
Anaerobic Digestion
...... . , ........ .
.. . .::: ............................
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
n
Frequency
of Analcesysis
Sample
Type
Analytical -
Tech -
i e
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
16
22
30
MPN/g
Quarterly
grab
9221-E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) El
Alt. 2 (40-day bench) D
Alt. 3 (30-day bench) El
Alt. 4 (Spec. Oz uptake) El
Alt. 5 (14-Day Aerobic) El
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) R1
Alt. 8 (Drying - Unstable) El
Alt. 9 (Injection) El
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed C]
CERTIFICATION STATEMENT (please check the appropriate statement)
Rl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator NA
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
, 9W ad,4, )-a -a
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 4/l/2020 To 6/30/2020
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 El
Alternative 2 E]
Alternative 3 El
Alternative 4 D
Alternative 5 +'1
Alternative 6 E"]
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost El
Heat Drying R1
Heat Treatment
Thermophilic
Beta Ray D
Gamma Ray C]
Pasteurization
Class B:
Alternative 1 D
Alternative 2
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization D
Air Dryings
I Composting El
I Aerobic Digestion El
Anaerobic Digestion g
......................_........._............................._...................................
.:.:...:: .. .: .:::.. .. :::... .. .::.. ...........::::: ..:>:: .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excees
dencenioue
Frequency
of Analysis
Sample
Type
Analytical
Tech-
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
17
27
44
MPN/G
Quarterly
grab
9221 E
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.I (VS reduction) El
Alt. 2 (40-day bench) El
Alt. 3 (30-day bench) El
Alt. 4 (Spec. 02 uptake) El
Alt. 5 (14-Day Aerobic) El
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable) R1
Alt. 8 (Drying - Unstable) El
Alt. 9 (Injection) El
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed Ll
CERTIFICATION STATEMENT (please check the appropriate statement)
Rl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator
Preparer Name and Title (type or print)
&I AA A . &EMkL
Signature of Preparer*
NA
Land Applier Name and Title (if applicable)(type or print)
I-aq,_ al
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 7/l/2020 To 9/30/2020
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 El
Alternative 2
Alternative 3 El
Alternative 4 Ej
Alternative 5 Rl
Alternative 6 El
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost El
Heat Drying Rl
Heat Treatment D
Thermophilic
Beta Ray D
Gamma Ray D
Pasteurization D
Class B:
Alternative 1 D
Alternative 2
.......................................
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization D
Air Drying®
Composting
Aerobic Digestion El
Anaerobic Digestion
. .. .::...:.... ................ .. .
...... ........................
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number of
Excee-
s
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
nioue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
19
62
200
MPN/G
Quarterly
grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
Alt. 2 (40-day bench) D
Alt. 3 (30-day bench) El
Alt. 4 (Spec. Oz uptake)
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) R1
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) El
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed E7
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator
Preparer Name and Title (type or print)
A AJ001 461 &1��
-a -a
Signature of Preparer* Date
NA
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 10/1/2020 To 12/31/2020
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 L3
Alternative 2 01
1 Alternative 3
Alternative 4 L1
Alternative 5 21
Alternative 6
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost El
Heat Drying Rl
Heat Treatment El
Thermophilic El
Beta Ra El
Gamma Ray
Pasteurization
Class B:
Alternative 1 D
Alternative 2
.........................,............................
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization El
Air Drying
composting 11
Aerobic Digestion El
Anaerobic Digestion
If applicable to alternative erformed Class A or Class B complete the following
P ( ) p g
monitoring
toying data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
denc
Frequency
of Analysis
Sample
Type
57 ytrca
Tech -
niaue
Minimum
Geo. Mean
Maximurr
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight
19
44
103
MPN/G
Quarterly
grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4 grams
total solid (dry
weight)
vector Attraction Reduction (40 c F-K 503.33) -Please indicate option performed:
Alt.1 (VS reduction) El
Alt. 2 (40-day bench)
Alt. 3 (30-day bench) [J
Alt. 4 (Spec. 02 uptake) Ej
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) R1
Alt. 8 (Drying - Unstable) El
Alt. 9 (Injection) El
Alt. 10 (Incorporation) E]
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
Rl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator
Preparer Name and Title (type or print)
Signature of Preparer*
NA
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

I

EXHAUST VAPOR OUT -LET
SEALED ACCESS COVER
SCRAPER 'BAR
'VAPOR DOME
DISC
STEAM CONDENSATE PIPE
-BAFFLE PLATE,
STATOR,
SUPPORT SADDLE
MATERIAL OUTLET
FOUNDATION
END .VIEW ,SECTION
MATERIAL INLET
EXHAUST VAPOR OUTLET
VAPOR DOME
SCRAPER*BARS.
MATERIAL INLET
ROTOR -ARMS
LjII SEAL
f
h SEAL.
ROTOR. BEARING
144-
fi T SIPHON. -TUBE
ROTOR AIR VEN
CONDENSATE OUTLET
CONNECTION
'HOLLOW SHAFT. -
STEAM JOINT
GEARBOX ili f i STEAM INLET
ROTOR SHAFT
STEAM
CONDENSATE PIPES
PADDLES MATERIAL OUTLET
FOUNDATION
SUPPORT SADDLE'
SIDE VIEW SECTION
Atlas-Sto-rd ROTADIsco
INDIRECT HEATED DISC DRIER
Figure 1

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12/29/98

Drier Log
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12/29/98

Drier Log
-DATV Jl- 0 qA
0 MIMI
In's
Doll, rJen
12/29/98

Town of Boone Wastewater Treatment Plant
2020 Class A Residuals Production
Run
Gallons
Digester
Total
No.
Run Date
Processed
% Solids
Dry Tons Notes
1
1/6/2020
150,086
2.34
14.65
2
1/13/2020
157,908
2.27
14.95
3
1/21/2020
118,378
2.67
13.18
4
1/27/2020
160,868
2.41
16.16
5
2/3/2020
162,770
2.74
18.59
6
2/ 10/ 2020
169,112
2.39
16.85
7
2/17/2020
147,973
2.41
14.87
8
2/24/2020
90,897
2.42
9.17
9
3/2/2020
147,973
2.98
18.38
10
3/9/2020
152,208
2.91
18.46
11
3/16/2020
126,834
2.61
13.80
12
3/30/2020
215,617
2.53
22.74
13
4/13/2020
329,768
2.05
28.19
14
4/ 27/ 2020
196,592
2.46
20.10
15
5/4/2020
145,859
2.22
13.50
16
5/11/2020
219,845
2.00
18.34
17
5/18/2020
162,770
2.23
15.14
18
6/1/2020
186,023
2.85
22.10
19
6/8/2020
186,023
2.55
19.78
20
6/15/2020
141,631
2.51
14.82
21
6/22/2020
152,200
2.65
16.82
22
6/29/2020
202,934
2.25
19.04
23
7/6/2020
215,618
2.37
21.30
24
7/ 27/ 2020
158,542
2,69
17.78
25
8/3/2020
90,898
3.05
11.56
26
9/8/2020
253,668
2.69
28.45
27
9/14/2020
253,668
2.59
27.40
28
9/21/2020
171,226
2.56
18.28
29
9/28/2020
285,377
2.42
28.80
30
10/5/2020
177,568
2.20
16.29
31
10/12/2020
192,365
2.56
20.53
32
10/19/2020
169,112
2.20
15.51
33
10/26/2020
80,328
2.00
6.69
34
11/2/2020
152,200
1.89
11.99
35
11/16/2020
158,543
2.82
18.64
36
11 /23/2020
29,595
1.92
2.37

37
11/30/2020
103,581
2.85
12.31
38
12/7/2020
262,124
2.65
28.97
39
12/14/2020
232,529
2.76
26.76
40
12/21 /2020
181,795
2.42
18.19
41
12/28/2020
143,745
1.97
11.80
TOTALS 6,783,083 723.25

Town of Boone Wastewater Treatment Plant
M20 Class A Residuals Distibution Log
Qtr
Month
Date
Reci ient
TDry'
Address '
Tons
Intended Use
Month
Total
1
MAR.
3-Mar
Trathen Cheek
570 Am Cheek Rd Fleetwood NC 28626
85.0
Pasture
27-Mar
David G -
311 Pine St Butler Tn 37640
7.5
Pasture
28-Mar
Jerry Bare
348 Bare Ridge Rd West Jefferson NC 28694 197
197.5
Pasture
290
2
APR
15-A r
George Ashley
186 Edna St Boone NC 28607
10.0
Pasture
15-A r
Jeff Roten
860 Joines Rd Creston NC 28615
40.0
Pasture
17-A r
Llo d Lam ert
635 Harless R West Jefferson NC 28694
108.0
Pasture
158
MAY
5-Ma
Russell Norman
P.O Box 91 Elk Park NC
58.8
Hay Fields
12-May
Chad Denny6175
Big Laurel Rd Creston NC 28615
95.0
Pasture
154
3
SEPT.
22-Sep
Lloyd Lambert
635 Harless Rd West Jefferson NC 28694
77.5
Pasture
78
4
OCT.
14-Oct
Jimmy Barnes
2025 Chestnut Hill Rd Crum ler NC 28617
10.0
Pasture
10
DEC
3-Dec
Charles Norris
419& Big Hill Rd Todd NC 28684
26.3
Pasture
26
Qtr'
Month
Date
Recipient
Address
Dry;
Tons
Intended Use
Month
Total
TOTAL
736',

M91h country 6-1-0 Mos®Q6ds
Produced by the Town of Boone
P.O. Drawer 192, Boone, NC 28607
High Country 6-1-0 (HC 610) is a high organic content fertilizer manufactured by the Town of Boone
Wastewater Treatment Facility. This product produces superior results on lawns, flower beds and
shrubs providing nutrients at the rates indicated below:
Guaranteed Analysis
Total Nitrogen .......................
Water Insoluble Nitrogen ..................... 6%
Available Phosphoric"""""'"""
Acid3.5%
................... '
Soluble Potash ................ 1%
........................... 0%
Iron ..........................
Recommended Application Rates
Lawn -Sod Establishment: Apply HC 610 at rate of 30 Ibs per 1000 sq feet.
Turf Maintenance: 'Apply HC 610 at a rate of 10-15 Ibs per 1000 sq feet.
Plant Bed Establishment: Apply HC 610 at a rate of 2 lbs per 100 sq feet into soil.
Planting Bed Maintenance: Apply HC 610 at a rate of 2 Ibs per 100 sq feet in Spring/Fall
Warnings: HC 610. is environmentally safe when used as directed, but can become a hazard if
mismanaged. This product should not be used bn soils intended for food crop production.
Cover HC 610 with a tarp or plastic during transportation. Store HC 610 in a dry area away from wells
or surface water where it could be washed into strea
areas. ms; keep product away from children's play
Limited Warranty and Disclaimer; The Town of Boone warrants that HC 610 meets the specifications
stated above, and that the heavy metal content is less than or equal to the limitations specified In the
EPA and NC Dept of Environmental and Natural Resources sludge quality criteria for land application.
If HC 610 fails to meet its specification, the buyer's sole remedy shall be the recovery of the purchase
price. Under no circumstances shall the Town of Boone be liable for any other 'damages, Including
direct, Indirect, consequential or special damages.
The undersigned Buyer agrees to abide by the following Restrictions:
HC 610 shall not be applied to land except in accordance with the instructions contained herein.
HC 610 shall not be applied to any site that is flooded, frozen, or snow-covered.
HC 610 shall not be applied within 100 feet of any water supply, stream, river, or lake.
Adequate measures shall be provided to prevent surface runoff from carrying this product into any
surface waters.
Buyer Signature
Date
Name (Print): Quantity:
Ibs/tons
Street/Route: Intended Use:. _
City/State/Zip: Amount Collected:
Telephone: Loaded By:

RESEARCh&ANA[YTiCA1
OAK LAORATORiES INC.
For: Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Attn: Mike Everett
Report of Analysis
1./20/2021
Iy{#III#IJR11
U' y NC #34 Z'.
0 S NC#37701
Client Sample ID: Biosolids #1
Lab Sample ID: 76980-01
Site: Town of Boone WWTP
Collection Date: 1/10/2020 9:10
I.Parameter , ,: _
Method "
-
Result
_Units -Analyst :Analysis DaWrime_ = -_.
Hardness, Total
Calculation
57600
mg/kg
PAN
Calculation
10800
Sodium Adsorption Ratio
Calculation
3.37
% Solids
SM 2540B
94.8
%
AW
1/10/2020
pH
SM 4500 H+B-2000
5.45
Std, Units
AB
1/13/2020 1243
Total Kjedjahl Nitrogen
SM 4500 N Org B (NH3 D-
30200
mg/kg
FK
2/4/2020
2011)
Ammonia Nitrogen
SM 4500 NH3 D-1997
8590
mg/kg
FK
2/4/2020
Nitrate + Nitrite
SM 4500 NO3 E-2011
3.26
mg/kg
DW
1/16/2020 1510
Total Phosphorous
SM 4500 P E-1999
33200
mg/kg
BJ
1/27/2020
Aluminum, Total
SW 846 6010D
11800
mg/kg
SK
1/14/2020
Arsenic, Total
SW 846 601OD
1,26
mg/kg
SK
1/12/2020
Cadmium; Total
SW 846 601 OD
0.962
mg/kg
SK
1/12/2020
Calcium, Total
SW 846 6010D
18100
mg/kg
SK
1/14/2020
Copper, Total
SW 846 6010D
358
mg/kg
SK
1/12/2020
Lead, Total
SW 846 6010D
12.1
mg/kg
SK
1/12/2020
Magnesium, Total
SW 846 6010D
3010
mg/kg
SK
1/12/2020
Molybdenum, Total
SW 846 6010D
3.72
mg/kg
SK
1/12/2020
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] wwmrandalabs.com Page 1
ral coa bo3i+ n,-)ftL 'l

�� �- 8& �� , �
��������`�� �� ����U��U��U
N D ° INC.Report
N ���o� �K�� �,�.°~^U&/�0��v^"".^" �/°.+y
�������� {�� �K���U����~��
- ' Analysis
' -� ^^~
1/20/2021
Client Sample |D�
Binsohda#1
Lab Sample ID:
70980~01
Site:
Town ofBoone VVVVTP
Collection Date:
1/102020 810
Method
Result
Units
Anblyst Analysis DatelTime
Potassium, Total 8VV8468O10D
4300
mg/kg
SK
1h4/2020
Selenium, Total
8YV84OOO18D
2.48
mg/kg
SK
1/12/2020
Silver, Total
SVV840GO1OD
<1.04
mg/kg
SK
1/12/2020
Sodium, Total
3VV84OOO1OD
1860
mg/kg
8K
1/12/2020
Zinc, Total
8VV8468O10D
789
mg/kg
SK
1/14/2020
Mercury, Total
8YV8467471B
0.513
mg/kg
MM
1/15/2020
Nx= not analyzed
P.0box 4731noShort S- treet�

(5/19/2020) Mike Everette - Biosolids #2.pdf Page 2
t a
RESEA°_ ,aLAWRATORI'IESI? INC.
For: Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Attn: Mike Everett
Client Sample ID: Biosolids Shed
Site: Town of Boone
WWTP
Parameter
Method
SAR
Cale
Hardness
Calculation
PAN
Calculation
% Solids
SM 2540B
Total Kjeidahi Nitrogen
SM 4500 N Org B-1997 (NH3
D-1997)
Ammonia Nitrogen
SM 4500 NH3 D-1997
Total Phosphorus
SM 4500 P E
Nitrate + Nitrite
SM4500 NO3E
Aluminum, Total
SW 846 6010D
Arsenic, Total
SW 846 6010D
Cadmium, Total
SW 846 6010D
Calcium, Total
SW 846 601oD
Copper, Total
SW 846 6010D
Lead, Total
SW 846 6010D
Magnesium, Total
SW 846 601 OD
Molybdenum, Total
SW 846 601 OD
Potassium, Total
SW 846 601 OD
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284
Report of Analysis
5/19/2020
1,000111/0/00
C;4'®III
�7
Ucy o
Z=•
=tr;to NC1134 a
S NC 1137701
.ram+r •..�/A�aP'y\ye�4®;
Lab Sample ID: 81344-01
Collection Date: 4/23/2020 9:40
Result
Units
Anal st Analysis DatelTime
2.76
56300
mgikg
SK
5/4/2020
11100
90.2
%
AW
4130/2020
31000
mg/kg
FK
5/14/2020
8890
mg/kg
FK
6/14/2020
32300
mg/kg
BJ
5/4/2020
1.21
mg/kg
DW
5/14/2020 1210
12300
mgikg
SK
5/4/2020
1.84
mgikg
SK
5/4/2020
0.674
mgikg
SK
5/4/2020
18200
mgikg
SK
5/4/2020
288
mg/kg
SK
5/4/2020
11.7
mgikg
SK
5/4/2020
2630
mg/kg
SK
5/4/2020
3.49
mg/kg
SK
5/4/2020
3900
mgikg
SK
5/4/2020
Tel: [phone]
Fax: [phone]
vAvw.randalabs.com Page 1

(5/19/2020) Mike Everette - Biosolids #2.pdf Page 3
ANAYTiCA1
Report of Analysis
LAORATORiES, INC.
5/19/2020
Client Sample ID:
Biosolids Shed
Lab Sample ID: 81344-01
Site:
Town of Boone WWTP
Collection Date: 41/23/2020 9:40
Parameter
Method
Resul
Units
Analyst Analysis Date/Time `
Selenium, Total
SW 846 601 OD
1.56
mg/kg
SK 5/4/2020
Silver, Total
SW 846 6010D
<1.11
mg/kg
SK 5/4/2020
Zinc, Total
SW 846 6010D
702
mg/kg
SK 5/4/2020
Mercury, Total
SW846 7471 B
0,231
mg/kg
MM 4/29/2020
Nickel, Total
SW846 Method 6010 C
12.7
mg/kg
SK 5/4/2020
Sodium, Total
SW846 Method 6010 C
1510
mg/kg
SK 5/4/2020
pH
SW846 Method 9045
6.00
Sid. Units AB 5/15/2020
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 2

Analysis
INC. 8/17/2020
For: Town of Boone WWTP
�� •''„as.r."�
,� � �• rr ���
PO Drawer 192
Y '
���• ��
Boone, NC 28607
•o
10 y NC 1134 : cn
NC 1137701
Attn: Mike Everett
�.
�1� D AVA
Client Sample ID: Biosolids Shed
Lab Sample ID:
84833-01
Site: Town of Boone
WWTP
Collection Date:
7/16/2020 8:10
Parameter
Method
Result
Units
.�
Anal s Analysis Date/Time j
SAR -
Calc
1.70
Total Nitrogen
Calc
41400
mg/kg
Hardness
Calculation
57000
mg/kg
MM
7/30/2020
PAN
Calculation
14800
% Solids
SM 2540B
96.0
%
AW
7/16/2020
Total Kjeldahl Nitrogen
SM 4500 N Org B-2011 (NH3
41400
mg/kg
FK
8/5/2020
D-2011)
Nitrite Nitrogen
SM 4500 NO2B
<0.104
mg/kg
DW
7/20/2020 1320
Ammonia Nitrogen
SM 4500 NH3 D-2011
11900
mg/kg
FK
8/5/2020
Nitrate + Nitrite
SM 4500 NO3 E-2011
0.558
n1g/kg
DW
7/20/2020 1320
Total Phosphorus
SM 4500 P E-2011
31700
mglkg
BJ
8/8/2020
Nitrate Nitrogen
SM4500 NO3E
0.548
mg/kg
DW
7/20/2020 1320
Aluminum, Total
SW 846 6010D
18000
mg/kg
MM
7/30/2020
Arsenic, Total
SW 846 601 OD
2.44
mg/kg
MM
7/30/2020
Cadmium, Total
SW 846 601 OD
4.29
mg/kg
MM
7/30/2020
Calcium, Total
SW 846 601 OD
18000
mg/kg
MM
7/30/2020
Copper, Total
SW 846 6010D
390
mg/kg
MM
7/30/2020
Lead, Total
SW 846 6010D
15.9
mg/kg
MM
7/30/2020
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel:
336-996-2841
Fax: 336-996-Q326 www.randalabs.com Page 1

Client Sample ID: Biosolids Shed
Site:
Town of Boone WWTP
Parameter
Method
Result
Magnesium, Total
SW 846 601 OD
2920
Molybdenum, Total
SW 846 6010D
6.49
Nickel, Total
SW 846 601 OD
15.5
Potassium, Total
SW 846 601 OD
3510
Selenium, Total
SW 846 6010D
2.37
Silver, Total
SW 846 601 OD
<1.03
Sodium, Total
SW 846 601 OD
1320
Zinc, Total
SW 846 601 OD
952
Mercury, Total
SW846 7471 B
0.429
pH
SW846 Method 9045
6.10
Report of Analysis
rr
Lab Sample ID:
84833-01
Collection Date:
7/16/2020 8:10
Units
Analyst Analysis Date/Time
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
MM
7/30/2020
mg/kg
EW
7/22/2020
Std. Units
AB
7/20/2020 1656
NA = not analyzed
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 2

(�IaceAnai(Xical'
www.pacalabsxam
January 25, 2021
Mr. Sid Champion
Research &Analytical Labs
106 Short Street
Kernersville, NC 27284
RE: Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
Dear Mr. Champion:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
Revised to add back % Moist result to report off Dry weight
Revised Report - Report revised to remove % moist result and addtional Total Solid result
If you have any questions concerning this report, please feel free to contact me.
Sincerely, *
Stephanie Knott for
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 27

aceAnalytical
www.pacelabs.com
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92602983
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification M TN00003
Connecticut Certification* PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification M 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification* E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification M LA180010
Maine Certification #: TN0002
Maryland Certification M 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification M TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification M TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification M 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate M 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LABO152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification M VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification M 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A21-A 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 27

aceAnalyfical
www.pacBlabs.com
SAMPLE ANALYTE COUNT
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92502983001 BIOSOLIDS SHED EPA 601OD
BG2
14
PASI-A
EPA 7471 B
SOO
1
PASI-A
SW-846
KDF
1
PASI-C
SM 2540G
KDW
1
PAN
Calculated
CCE
1
PAN
EPA 9045D
SMK
1
PASI-A
None
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJL
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 3 of 27

aceAnalj6cal
www,pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
Sample: BIOSOLIDS SHED
Lab ID: 92502983001 Collected:
10/28/20 08:30
Received: 10/29/20 10:14 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Pace Analytical Services - Asheville
Aluminum
15300 mg/kg
47.7
5
11/08/2014:50
11/09/2014:57
7429-90-5
M1
Arsenic
2.6 mg/kg
0.95
1
11108/2014:50
11/09/2013:48
7440-38-2
Cadmium
1.5 mg/kg
0.095
1
11/0812014:50
11/09/2013:48
7440-43-9
Calcium
14200 mg/kg
47.7
5
11/08/2014:50
11/09/2014:57
7440-70-2
M1
Copper
443 mg/kg
0.48
1
11/08/2014:50
11/09/2013:48
7440-50-8
M1
Lead
17.2 mg/kg
0.48
1
11/08/2014:50
11/09/2013:48
7439-92-1
Magnesium
2820 mg/kg
9.5
1
11/08/2014:50
11/0912013:48
7439-95-4
Molybdenum
4.9 mg/kg
0.48
1
11/08/2014:50
11109/2013:48
7439-98-7
Nickel
16.1 mg/kg
0.48
1
11/08/2014:50
11/09/2013:48
7440-02-0
Potassium
3510 mg/kg
477
1
11/08/2014:50
11/09/2013:48
7440-09-7
Selenium
3.1 mg/kg
0.95
1
11/0812014:50
11/09/2013:48
7782-49-2
Silver
3.0 mg/kg
0.48
1
11/0812014:50
11/09/2013:48
7440-22-4
M1
Sodium
1090 mg/kg
477
1
11/08/2014:50
11/09/2013:48
7440-23-5
Zinc
829 mg/kg
0.95
1
11/08/2014:50
11/0912013:48
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Pace Analytical Services -Asheville
Mercury
0.32 mg/kg
0.030
5
11108/2016:09
11/09/2013:11
7439-97-6
M1
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
8.1 %
0.10
1
11/04/20 16:26
Total Solids 2540 G-2011
Analytical Method: SM 2540G Preparation
Method:
SM
2540 G
Pace National - Mt. Juliet
Total Solids
89.9 %
1
11/12/20 05:09
11/12/20 05:16
Calculated Results
Analytical Method: Calculated Preparation
Method:
Calc
Pace National - Mt. Juliet
Sodium Adsorption Ratio
2.74
1
11/16/20 10:16
11/16/20 10:16
SAR
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.0 Sid. Units
0.10
1
11/09/20 16:02
H3
Plant Available Nitrogen
Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen
10800 mg/kg
0.12
1
11/12/20 16:29
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0
1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
683 mg/kg
9.2
1
11/11/20 13:32
11/12/20 08:05
7664-41-7
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ANALYTICAL RESULTS
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BIOSOLIDS SHED Lab ID: 92502983001 Collected: 10/28/20 08:30 Received: 10/29/20 10:14 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Kjeldahl, Total
35600 mg/kg 2470 50 11/11/20 11:30 11/12/20 06:48 7727-37-9
353.2 Nitrogen, N021NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
31.3 mg/kg 4.2 1 11/10/20 22:05 11/11/20 00:55 H1,H2
Nitrogen, Nitrate
31.3 mg/kg 4.2 1 11/10/20 22:05 11/11/20 00:55 14797-55-8
Nitrogen, Nitrite
ND mg/kg 4.2 1 11/10/20 22:05 11/11/20 00:55 14797-65-0 H1,H2
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
14000 mg/kg 989 1000 11/05/20 22:33 11/06/20 18:07 7723-14-0 M6
Date: 01/25/2021 09:23 AM
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QUALITY CONTROL DATA
Project: Boone Biosolids # 4 10128
Pace Project No.: 92502983
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 578785
Analysis Method:
EPA 7471B
QC Batch Method: EPA 7471 B
Analysis Description:
7471 Mercury
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92502983001
METHOD BLANK: 3062380
Matrix: Solid
Associated Lab Samples: 92502983001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0060 11/09/2010:36
LABORATORY CONTROL SAMPLE: 3062381
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
0.083 0.083
100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3062382 3062383
MS MSD
92502983001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Quai
Mercury mg/kg 0.32
0.083 0.08 0.46
0.43 168 138 75-125 6 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
QC Batch: 578778 Analysis Method: EPA6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92502983001
METHOD BLANK: 3062344
Associated Lab Samples: 92502983001
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Aluminum
mg/kg
ND
10.0
11/09/2015:50
Arsenic
mg/kg
ND
1.0
1110912015:50
Cadmium
mg/kg
ND
0.10
11/0912015:50
Calcium
mg/kg
ND
10.0
11/09/2015:50
Copper
mg/kg
ND
0.50
11/0912015:50
Lead
mg/kg
ND
0.50
11/0912015:50
Magnesium
mg/kg
ND
10.0
11/09/2015:50
Molybdenum
mg/kg
ND
0.50
11/09/2015:50
Nickel
mg/kg
ND
0.50
11/09/2015:60
Potassium
mg/kg
ND
500
11/09/2015:50
Selenium
mg/kg
ND
1.0
11/09/2015:50
Silver
mg/kg
ND
0.50
11/09/2015:50
Sodium
mg/kg
ND
500
11/09/2015:50
Zinc
mg/kg
ND
1.0
11/09/2015:50
LABORATORY CONTROL SAMPLE:
3062345
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Qualifiers
Spike
Conc,
LCS
Result
LCS
% Rec
% Rec
Limits
500
479
96
80-120
50
48.6
97
80-120
50
49.7
99
80-120
500
495
99
80-120
50
49.8
100
80-120
50
48.9
98
80-120
500
467
93
80-120
50
50.7
101
80-120
50
50.2
100
80-120
500
ND
95
80-120
50
46.4
93
80-120
25
23.9
96
80-120
500
474J
95
80-120
50
48.5
97
80-120
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3062346
3062347
MS
MSD
92502983001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
15300
469
469
19300
16500
857
259
75-125
16 M1
Arsenic
mg/kg
2.6
46.9
46.9
42.7
43.6
86
87
75-125
2
Cadmium
mg/kg
1.5
46.9
46.9
40.9
41.6
84
86
75-125
2
Calcium
mg/kg
14200
469
469
17700
14600
758
97
75-125
19 M1
Copper
mg/kg
443
46.9
46.9
511
508
144
139
75-125
0 M1
Lead
mg/kg
17.2
46.9
46.9
57.4
57.5
86
86
75-125
0
Magnesium
mg/kg
2820
469
469
3350
3330
112
109
75-125
0
Molybdenum
mg/kg
4.9
46.9
46.9
45.6
46.3
87
88
75-125
2
Nickel
mg/kg
16.1
46.9
46.9
56.5
57.0
86
87
75-125
1
Potassium
mg/kg
3510
469
469
4010
4000
107
105
75-125
0
Selenium
mg/kg
3.1
46.9
46.9
42.6
43.6
84
86
75-125
2
Silver
mg/kg
3.0
23.5
23.5
23.2
23.6
86
88
75-125
2
Sodium
mg/kg
1090
469
469
1540
1540
96
97
75-125
0
Zinc
mg/kg
829
46.9
46.9
877
881
103
111
75-125
0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Boone Biosolids # 4 10128
Pace Project No.: 92502983
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 1574068
Analysis Method:
SM 254OG
QC Batch Method: SM 2540 G
Analysis Description:
Total Solids 2540 G-2011
Laboratory:
Pace National - Mt. Juliet
Associated Lab Samples: 92502983001
METHOD BLANK: R3592290-1
Matrix: Solid
Associated Lab Samples: 92502983001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Solids
%
0.00100
11/12/20 05:16
LABORATORY CONTROL SAMPLE: R3592290-2
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Solids
%
50.0 50.0
100 85.0-115
SAMPLE DUPLICATE: R3592290-3
L1282693-09 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Solids
%
85.8 85.6 0.241
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
QC Batch: 578770
QC Batch Method: EPA 9045D
Associated Lab Samples: 92502983001
SAMPLE DUPLICATE: 3062332
Parameter Units
pH at 25 Degrees C Std. Units
SAMPLE DUPLICATE: 3062333
Parameter
pH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
Laboratory: Pace Analytical Services -Asheville
92503250001 Dup
Result Result RPD Qualifiers
6.2 6.1 1 H3
92504081001 Dup
Units Result Result
Std. Units 6.3 6.3
RPD Qualifiers
0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
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Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
QC Batch: 579530
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92502983001
METHOD BLANK: 3065752
Associated Lab Samples: 92502983001
Parameter Units
Nitrogen, Ammonia mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 9.4 11/12/20 08:00
LABORATORY CONTROL SAMPLE: 3065753
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits
Nitrogen, Ammonia mg/kg 481 480 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3065756
MS
92502983001 Spike
Parameter Units Result Conc.
Nitrogen, Ammonia mg/kg 683 523
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3066170
MS
92503758001 Spike
Parameter Units Result Conc.
Nitrogen, Ammonia mg/kg 2450 6810
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
3065757
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
544 1180 1230 95 101 90-110 4
3066171
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
6810 8950 8980 95 96 90-110 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
Qual
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
QC Batch: 579432
Analysis Method:
EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description:
351.2 TKN
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92502983001
METHOD BLANK: 3065367
Matrix: Solid
Associated Lab Samples: 92502983001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 50.0 11/12/20 04:24
LABORATORY CONTROL SAMPLE: 3065368
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000 1030
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3065369 3065370
MS MSD
92504198001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec Limits RPD Qua]
Nitrogen, Kjeldahl, Total mg/kg 194
1320 1450 1460 1570 96 95 90-110 7 H3
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
QC Batch: 579363 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92502983001
METHOD BLANK: 3065223
Associated Lab Samples: 92502983001
Parameter Units
Nitrogen, Nitrate mg/kg
Nitrogen, Nitrite mg/kg
Nitrogen, NO2 plus NO3 mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 4.0 11/11/20 00:53
ND 4.0 11/11/20 00:53
ND 4.0 11/11/20 00:53
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 3065224
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 15.6 104 90-110
Nitrogen, Nitrite mg/kg 10 9.7 97 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.3 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3065225
3065226
MS
MSD
92504942001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone,
Result
Result
% Rec '
% Rec
Limits RPD Qua]
Nitrogen, Nitrate
mg/kg
ND
15.1
15.1
16.5
16.4
109
109
90-110 0
Nitrogen, Nitrite
mg/kg
ND
10.1
10.1
9.6
9.6
93
94
90-110 0
Nitrogen, NO2 plus NO3
mg/kg
ND
25.2
25.2
26.1
26.1
99
99
90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /25/2021 09:23 AM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
QC Batch: 578343 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92502983001
METHOD BLANK: 3059927
Associated Lab Samples: 92502983001
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 3059928
Parameter Units
Phosphorus mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.96 11/06/2018:05
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
46.3 46.6 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3059929 3059930
MS MSD
92502983001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 14000 52.3 54.4 15000 15000 1950 1930 90-110 0 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit,
MDL -Adjusted Method Detection Limit,
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyivinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H2 Extraction or preparation conducted outside EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Boone Biosolids # 4 10/28
Pace Project No.: 92502983
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92502983001
BIOSOLIDS SHED
EPA3050B
578778
EPA 601OD
578796
92502983001
BIOSOLIDS SHED
EPA 7471B
578785
EPA 7471B
578791
92502983001
BIOSOLIDS SHED
SW-846
580926
92502983001
BIOSOLIDS SHED
SM 2540 G
1574068
SM 2540G
1574068
92502983001
BIOSOLIDS SHED
Calc
1576834
Calculated
1576834
92502983001
BIOSOLIDS SHED
EPA9045D
578770
92502983001
BIOSOLIDS SHED
None
580031
92502983001
BIOSOLIDS SHED
EPA 350.1 Rev 2.0 1993
579530
EPA 350.1 Rev 2.0 1993
579625
Mod.
Mod.
92502983001
BIOSOLIDS SHED
EPA 351.2 Rev 2.0 1993
579432
EPA 351.2 Rev 2.0 1993
579787
92502983001
BIOSOLIDS SHED
EPA 353.2 Rev 2.0 1993
579363
EPA 353.2 Rev 2.0 1993
579369
92502983001
BIOSOLIDS SHED
EPA 365.1 Rev 2.0 1993
578343
EPA 365.1 Rev 2.0 1993
578663
Date: 01/25/2021 09:23 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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w 0#092502983
RESEARCH G`LANALyriCA,1
ILAboRATOR-IES, INC. 92502983
Analytical /Process Consultations
'Phone [phone]
LIN OF CUSTODY RECORD
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REMARKS:
SAMPLE TEMPERATURE AT RECEIPT

aceAnaiyticai® ANALYTICAL REPORT
National Center for Testing & Innovation November 16, 2020
i
FC]
1
I 3SS
Pace Analytical - Asheville, NC
Sample Delivery Group: L1282698 4Cn
I
Samples Received: 11/06/2020 5Sr
IProject Number: 92502983
Description: �Qc
Site: 001
GI
Report To: Christopher Derouen
i 2225 Riverside Drive 'ql
Asheville, NC 28804
FS
Entire Report Reviewed By:
Christl M Wagner
Project Manager
Results relate only to the Items tested or calibrated and are reported as rounded values. This lest report shall not be
reproduced, except In full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National Is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling, conducted by the customer, results relate to the accuracy of the Information provided,
and as the samples are received.
rg
0115
'J C"
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Asheville, NC 92502983 L1282698 11/16/2014:34 1 of 10

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover page
1
Tc: Table of Contents
2
Ecl
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
rs
DIOSOLIDS SHED L1282698-01
5
4Cn
Qc: Quality Control Summary
6
Total Solids by Method 2540 G-2011
6
FrGI:
Glossary of Terms
7
Accreditations & Locations
8
RAI:
Sc: Sample Chain of Custody
9
F
Page 19 of 27 -
ACCOUNT: PROJECT: SDG DATEMME: PAGE:
Pace Analytical - Asheville, NC 92502983 L1282698 11/16/2014:34 2 of 10

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
DIOSOLIDS SHED L1282698-01 Solid 10/28/2008:30 11/06/2009:00
Method
Calculated Results
Total Solids by Method 2540 G-2011
Batch Dilution Preparation Analysis Analyst
date/time date/time
WG1576834 1 11/16/2010:16 11/16/2010:16 CCE
WG1574068 1 11/12/20 05:09 11/12/20 05:16 KDW
Location
Mt. Juliet, TN
Mt. Juliet, TN
Page 20 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Asheville, NC 92502983 L1282698 11/16/201434 3 of 10

CASE NARRATIVE ONE LAB, NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples PChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my rs
s
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
5
Sr
FC
�GI
Christ[ M Wagner
Project Manager -AI
9
Sc
_ Page 21 of 27
ACCOUNT: PROJECT: SDG DATE/TIME: PAGE:
Pace Analytical - Asheville, NC 92502983 L1282698 11/16/2014:34 4 of 10

DIOSOLIDS SHED SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 10/28/20 08:30 L1282698
Calculated Results
Result Qualifier Dilution Analysis Batch
Analyte date / time
- -- ----------
Sodium Adsorption Ratio 2.74 1 11[16/2020 10:16 WG1576834
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte % date time
Total Solids 89.9 1 11/12/2020 05:16 WG1574068
Page 22 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical -Asheville, NC 92502983 L1282698 11/16/20 14:34 5 of 10

WG1574068 QUALITY CONTROL SUMMARY - ONE LAB. NATIONWIDE.
Total Solids by Method 2540 G-2011 L1282698-01
Method Blank (MB) ,
(MB) R3592290-1 11/12/20 05:16
MB Result MB Qualifier MB MDL MB RDL
-TC
Analyte % % %
Total Solids 0.00100
__._ _. _. m _._.......... _. _.
FS
L1282693-09 Original Sample (OS) • Duplicate (DUP)
(OS) L1282693-09 11/12/20 05:16 • (DUP) R3592290-3 11/12/20 05:16
Fn
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
s
Analyte % % %
%
Total Solids 85.8 85.6 1 0.241
10
Laboratory Control Sample (LCS)
F
(LCS) R3592290-2 11/12/20 05:16
:AI
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte %%
Total Solids 50.0 50.0 100 85.0-115
9Sc
ACCOUNT:
Pace Analytical -Asheville, NC
PROJECT: - SDG
92502983 L1282698
DATE/TIME:
11/16/2014:34
PAGE:
6 of 10

GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below
is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
H
intended as a comprehensive
explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
ITC
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and
Definitions
rs
MDL
RDL
Method Detection Limit.
Reported Detection Limit.
FC
Rec.
Recovery.
RPD
Relative Percent Difference,
SDG
Sample Delivery Group.
Fr
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
QC
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or °% difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
A)
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RED) from a quality control
sample. The Original Sample may not be included within the reported SDG.
9
This column provides a letter and/or number designation that corresponds to additional information concerning the result
SC
Qualifier
reported. If a Qualifier Is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported,
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
ACCOUNT:
Pace Analytical - Asheville, NC
Page 24 of 27
PROJECT: SDG: DATE/TIME: PAGE:
92502983 L1282698 11/16/2014:34 7 of 10

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accreditedkertified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory Is comparable to the collective totals of the network
laboratories in our Industry. The most significant benefit to our one location design Is the design of our laboratory campus. The model Is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
i—P
-Tc
Alabama
--— ----- ..
40660
Nebraska
NEOS15-05
Alaska
17-026
Nevada
TN 03 2002-34FS
Arizona
AZ0612
New Hampshire
2975
Arkansas
88 0469
New Jersey NELAP
TNO02
F]n
California
— -- -- — ---
2932 —
New Mexico'
—_
n/a -
Colorado
--
TN00003
_. _._ —
New York
--- ----
11742
Connecticut
PH-97
01
North Carolina
N
E nv375
Sr
-- -
Florida
- — - -
E87487
-
North Carolina'
—
DW21704
Georgia
-- — --
NELAP
-- -- --
North Carolina'
--
41
-- —
Georgia
923
North Dakota
R-140
C
Idaho
TN00003
Ohio VAP
— CL0069
Illinois
Indiana
200008
C TN-01
Oklahoma
Oregon
—
9915
TN200002
Iowa
364
Pennsylvania— --
-- 68-02979
Kansas
Kentucky' c
E-10277
90010
Rhode Island
South Carolina
LA000356
84004
Kentucky 2
16
South Dakota
n/a
Loulslana
Louisiana'
A130792
LA180010
Tennessee'"
Texas
2006
T104704245-18-15
R
— .....—....__.... — .._._....._._._._......--------.........------
Maine
---- -----......__.._....._........_—.....__...—._....-------
--...—.....--- — ....--- - .—._..... -
TN0002
— -- ...._...— — — --
--....__..._..__._...- .._... --- -- -.....
Texas' .__—.____.—__._._.—......_.—LA80152_
— xas.__._... — ---
---......-----—._......-- - —
__--_..__-
Maryland
324
Utah
TN00003
Massachusetts
-- —....---------...........--...... — ------
M-TNO03
--...--- --...----....
Vermont
— —-....----------.._.......---...._.__......—..
VT2006
-- -
Michigan
---.._....- —...---..—._._._—..._..—
9958
-- ...
Virginia
--- ---- ---- — _.........--
460132
...- — —..-- -...----.... --------
Minnesota
— -- --—...-----...---.._—...— ---
047-999-395 ..._ _............
Washington
-------._.....— — — -- - —
C847
-- — — ---...-----...._
Mississippi
_.—.__....._—...------... ------ --- ---
TN00003
— --- — —
West Virginia
------------- --- ------
233
------—._.....
Missouri
._.—..._...... --- —
340
----..._.. ---- .—... ...._...------
Wisconsin
------ ._....— ---- ---
9980939910 ......
---
Montana
CERT0086
Wyoming
-
A2LA
Third Party Federal Accreditations
A2LA— ISO 17025
1461.0
EMLAP
100789
... —... —.—_._—. s_........—
A2LA — ISO 17025
----......._..._._.._.....
—
1461.02
—AIHA.-._L.A..—P—,LLC
DOD
----..._—.-_
1461.01 ._...__._..__....
-------- .....
Canada
-----.—......—. ....._..._._—...-- ---
1461.01
—_—.__...—..—_...—....._.__...-----....... __...—
USDA
---.._....._...—_...__—.. -- --- .....—._.—...
P330-15-00234
—... ----------- .__..
EPA—Crypto
TN00003
Drinking Water z Underground Storage Tanks
'Aquatic Toxicity ' ChemicaVMlcrobiological s Mold 'Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one ofour support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
S 'A'A
- h.ST �- NO - �. CtiSE A
OR tow
SO W1 NY
WY
MI
ti NE IA � --_�� h � PA �!
NV
ff
KS
UT ? CO? /- tn.'V
CA KS 1`14 0
�AZ
NK-1 U AR SC- r
.--.- tIS A� T GA l�
TX LA
AK
Page 25 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Asheville, NC 92502983 L1282698 11/16/2014:34 8 of 10

Internal Transfer Chain of Custody
F-1 samples Pre -Logged into eCOC. State Of Origin: NC
Cert.,.Needed: t2"Yes Cl No
Workorder 92502983 Workorder Name: Boone Biosolids 4 4 10/28 Owner Received Datet 10/29/2(V0 RP_,cajft_cz RPnzjP_-_tM Rv- 111Q/9M10
,,R9p*rt�,T*1,,1*&,'M1, 77-77,777,77
Chris Derouen Pace Analytical National
Pace Analytical Asheville 12065 Lebanon Rd
2225 Friverside Dr. N4tJurJetTN 37122
15
Asheville, NC 28804 Phone [phone]
�
Phone [phone]
.2
ix',,,Prez*kved CoMalnemx
R,
5d
1
"01,,AI,,
-1Q'
Q0
W" I&
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q,
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t
LAB USE ONLY
I B10SOUDS SHED
PS I a/2812020 08:30
92502983001
Solid
I
X.
✓ 0
4
777
7 7,7,7,
"Mew
Transfers
Re 421S:64 -
DateMme
Received By
DatwTitme
61
2
3
Cooler Temperature on Receipt (,,7.c-- CuStOdySeal Y orI— Received
on IcVT or N Sam Intact
.pies r N
-in orverto maintain client confidentiaft locatiori1name Of the saTPA79 site, sampfe,"`s name and signature may not be provided on this COC docum—ent
This chain of custody is considered complete as is since this informmfic n is available in the owner laboratory.
-IL
. . . .. . ........ ... . . .......
A069C e a- En-, 71
1-7 T7 5"C2111"/7
Thursday. November 05, 2020 2,-48.-32 PM FN1'P ALL-C-002rev.00 24March2W9 Page I of 1
Page 26 of 27

aceAnarytical
ti,pte�lrbt.tprn
INTgAJABORATORY WORK ORDER # 92502983
(Tobe completed by sending lab)
Sending Projecl.No
92,502983
Receiving Project No
Check -Box for Consolidated Invoice
()ate Prepared
it/05/20
REQUESTED COMPLETION DATE
jl 9/2026
Sending Re,gtgp
tR92-ChMotta
Ssnding Project Mgr,_
Chris DefoUon
Receiving Region.
IR850-Pace Natlonat
External Client
Research &Analytieat Labs
Siatont Samp12:Origin
NC; :.-
QC Doliverable
STD REPORT
All quostiopq shouid ladaddress$d to sending project mnnagaa
Requested Roportable.Units ReportWgtor Dr, Weight? Dry Weight IRWO Lab Need to run? Cert. Needed„ ,
i r
;' :,tM1IOF K RSQU STEP r,. a
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�ampkrprTYpd
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Amount
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SUbbed Sodium Absorbtion Ration
WGFU
�.,
Un nerved
t
30 0
I $0.0
Speclal Requlr0mants, Report B, Standard Retaort (0) FR 00 no EDD m
r
r >:tedetv)ng Raton=dspa�itneflt � ',
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54,,0
0,0
$0.9
custom nrrtcnuannocalan
22,
P it AffAL'rTICAL Wo, "' O�+1pI:ETED.,TH1. IS.SEOTIC�N
Return Samples to -sending Region: Ely No
Thursday, November,05, 2020 2:48:82 PM FMT-ALL-C-00 i revAO 24
t
lC
Page i of t

a 04myr-re 1 2FR z-1"fv-zl will# 7Y., own ut Eloone 1,11111T Va—ge -A,
FEB/24/2020/MON 04:57 PM FAX No, P'001/001
WATER QUALITY LAB & OPERATIONS. INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192
CITY: BOONE
STATE. NC ZIP 28607
ID#; NCO020621
SAMPLER: MICHAEL EVERETT
RECEIVED DATE; 16-Jan-20
REPORTED DATE: 24-Fob-20
ALYW�'
.... ......
YA.
:-:;:WdLA:
* . .....
:::::u*m(t-$�'::�::M
IL:8::'
A `,V,
..........
..........
TOTAL SOLIDS
1
90,11
%
SLUDGE
---
WPS
FECAL COLIFORM
19
2
MPN/q
SLUDGE
17-Jan-20
Pt
TOTAL SOLIDS
2
92.4
%
SLUDGE
WPS
FECAL COLIFORM
24
2
1 MPN/q
SLUDGE
17-Jan-20
PI
TOTAL SOLIDS
3
91.3
0/0
SLUDGE
WPS
FECAL COLIFORM
19
2
MPN/g
SLUDGE
17-Jan-20
P1
TOTAL SOLIDS
4
91.2
%
SLUDGE
WPS
FECAL COLIFORM
16
2
MPN/g
SLUDGE
17-Jan-20
PI
TOTAL SOLIDS
5
90.4
% .
SLUDGE
WPS
FECAL COLIFORM
25
2
MPN/g
SLUDGE
17-Jan-20
Pi
TOTAL SOLIDS
a
91.1
%
SLUDGE
WPS
FECAL COLIFORM
29
2
MPN/g
SLUDGE
17-Jan-20
P)
TOTAL SOLIDS
7
913
%
SLUDGE
wps—
FECAL COLIFORM
30
2
MPN/g
SLUDGE
17-Jan-20
P1
REPORTED BY: NC CERTIFIED LAB # 644.
PAUL )SENHOUR, SUPERVISOR

JUN/08/2020/MON 12:11 PM FAX No, P,001/001
WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NO 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192
CITY: BOONE
STATE: NC ZJP 28607
109: NCO020621
$AMPLER: MIKE EVERETT
RECEIVED DATE: 16-Apr-20
REPORTED DATE; 24-Apr-20
............
'013-AT)ON
TOTAL SOLIDS
1
91.0
0.1
%
SLUDGE
FECAL COLIFORM
19
1
MPN/g
SLUDGE
17-Apr-20
Pi
TOTAL SOLIDS
2
93.0
0.1
%
SLUDGE
FECAL COLIFORM
30
1
MPN/g
SLUDGE
17,Apr-20
PI
TOTAL SOLIDS
3
93.0
0.1
%
SLUDGE
FECAL COLIFORM
36
1
MPNlg
SLUDGE
17-Apr-20
Pi
TOTAL SOLIDS
4
91,0
0.1
%
SLUDGE
FECAL COLIFORM
44
1
MPNlq*
SLUDGE
17-Apr-20
PI
TOTAL SOLIDS
5
92.0
0.1
%
SLUDGE
FECAL COLIFORM
17
1
MPNlg
SLUDGE
17-Apr-20
I P1
TOTAL SOLIDS
6
92.0
0.1
%
SLUDGE
FECAL COLIFORM
19
1
MPN/g
SLUDGE
17-Ap 20
Pi
TOTAL SOLIDS
7
93.0
0.1
%
SLUDGE
FECAL COLIFORM
33
1
MPN/g
SLUDGE
17-Apr-20
PI
REPORTED BY: NO CERTIFIED LAB # 644
PAUL ISENHOUR, SUPERVISOR

AUG/31/2020/MON 02:14 PM FAX No, P,002/002
WATER QUALITY LAB & OPERATIONS, INC,
P.O, BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF 130ONE WWTP LOGIN TIME:
ADDRESS: P.O, BOX 192 SAMPLER:
CITY: BOONE RECEIVED DATE: 9-,Jul-20
STATE: NC ZIP 28607 REPORTED DATE: 17-Jul-20
I D#. NCO020621
ANAL,Y3k5::
: 3Y4; ;:
i4AlA� Ig
•s;::
IT
PG
:ANi4L••l!31IA*
T
•
�k�:A't"lpT�l
f�CV
» �f~
TOTAL SOLIDS
1
93.1
0,1
%
SLUDGE
FECAL COLIFORM
19
1
M PN/g
SLUDGE
10-Jul-20
PI
TOTAL SOLIDS
2
92.5
0.1
%
SLUDGE
FECAL COLIFORM
133
1 1
MPN/g
SLUDGE
10-Jul-20
PI
TOTAL SOLIDS
3
92.8
0.1
%
SLUDGE
FECAL. COLIFORM
200
1
MPN/g
SLUDGE
10-JUI-20
PI
TOTAL SOLIDS
4
93.3
0.1
%
SLUDGE
FECAL-COLIFORM
73
1
MPN/g
SLUDGE
10-Jul-20
Pi
TOTAL SOLIDS
5
91.8
0.1
%
SLUDGE
FECAL COLIFORM
28
1
MPN/g
SLUDGE
10-Jul-20
PI
TOTAL SOLIDS
6
91.6
0.1
%
SLUDGE
FECAL COLIFORM
48
1
MPN/g
SLUDGE
10-Jul-20
PI
TOTAL SOLIDS
7
92,2
0.1
%
SLUDGE
FECAL COLIFORM
19
1
MPN/g I
SLUDGE 1
10-Jul-20
PI .
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

-• i r$lwzfrAo lot, WA*#� • • • • :•• - TT
My u
NOV/20/2020/FRI 03:59 PM FAX No, P.002/002,
WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NO 28604
[phone]
CLIENT: TOWN OF BOONE WWTP LOGIN TIME:
ADDRESS: P.O. BOX 192 SAMPLER:
CITY: POONE RECEIVED DATE: 8-Oct-20
STATE: NC ZIP 28607 REPORTED DATE: 6-Nav-20
ID#: NCO020621
ANALcsr<
NALYStJ
: .LVxgL's::
::iJtV ITS :
<SANiP•,L6>;
:;ANALNM-5 :.
, ::It�T•.:';::::
TOTAL SOLIDS
1.
91.3
�
%
SLUDGE
FECAL COLIFORM
19
MPN/g
SLUDGE
9-Oct-20
PI
TOTAL SOLIDS
2
92.1
°/a
SLUDGE
FECAL COLIFORM
27
MPN/g
SLUDGE
9-Oct-20
PI
TOTAL SOLIDS
3
91.7
%
SLUDGE
FECAL COLIFORM
43
MPN/g
SLUDGE
9-Oct-20
PI
TOTAL SOLIDS
4
92.0
%
SLUDGE
PECAN COLIFORM
27
MPN/
SLUDGE
9-Oct•-20
p{
TOTAL SOLIDS
5
91.9
%
SLUDGE
FECAL COLIFORM
43
MPN/9
SLUDGE
9-0at-20
PI
TOTAL SOLIDS
6
91.1
%
SLU,D­GE
FECAL COLIFORM
19
MPN/p
SLUDGE
9-Oct-20
PI
TOTAL SOLIDS
7
92.1
°/a
SLUDGE
FECAL COLIFORM
103
MPN/g I
SLUDGE
9-Oct-20
PI
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR