WQ0021577_Residual Annual Report 2020_20210201

Initial Review
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* W00021577
Applicant/Permittee WestRock Kraft Paper, LLC
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Raleigh
CO Reviewer
Admin Reviewer [e-mail]

Submittal Form
Project Contact Information
Reese provide inforrration on the person to be contacted by N B Staff regarding electronic subnittal, confirmation of receipt, and other correspondence.
.......................... . . . . . . ...... . . . ......... . . .... . . ...... _ -
Name * Chris Williams
Email Address*
chris.m.\Mlliams@\Nestrock.com
Project Information
........ ......... ............................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
2525336237
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0021577
Ras Current Existing permit number
Applicant/Permittee Address* 100 Gaston Road Roanoke Rapids NC 27870
Facility Name * WestRock Kraft Paper - Roanoke Rapids Mill
Please provide comments/notes on your current submittal below.
2020 Annual Report for Distribution of Residuals WQ0021577
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
Annual Report Submittal.pdf 3.35MB
Upload only 1 FDF docurrent (less than 250 IvB). Multiple documents rust be contained into one RJF file unless file is larger than
upload lirrit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
C��ssrt. f�! �lll
Submission Date 2/1/2021

� WestRock
February 1, 2021
NCDENR-DWR
Water Quality Permit Section
Non -Discharge Permitting Unit
Attn: Information Processing Unit
6'h Floor
Division of Water Resources
512 N. Salisbury Street
Raleigh, NC 27699
To Whom It May Concern:
100 Gaston Road office: 252.533,6000
Roanoke Rapids, NC 27870 www.westrock.conn
WQ0021577 requires submission of an annual Distribution of Residuals Solids report. Enclosed you will
find our Annual Report for CY2020. WQ0021577 was renewed April 29, 2020 and is effective through
September 30, 2026.
There were no distribution of residuals events in 2020. All residuals were disposed of in the Roanoke
Rapids Mill Landfill in compliance with WQ0000436 for CY2020.
Please feel free to contact me at 252-533-6237 with any questions or concerns
Sincerely,
/4/
Christopher M. Williams
Environmental Engineer

Annual Distribution of Residuals Report CY2020
WQ0021577
KapStone Kraft Paper Corporation
Roanoke Rapids, NC
Table of Contents
Annual Land Application Certification Form
1
Form DMSDF — Primary Clarifier Residuals Annual Certification 2020
2
Form RSSF — Primary Clarifier Residuals Sampling Summary
3
Form RSSF (B) -- Primary Clarifier Residuals Sampling Summary (B)
4
Sample Analysis — Primary Clarifier Residuals
5
TCLP Sample Analysis— Primary Clarifier Residuals
10
Form PVRF 02T— Primary Clarifier Residuals Annual Pathogen Reduction Form
15
Form DMSDF — Flyash Residuals Annual Certification 2020
16
Form RSSF — Flyash Residuals Sampling Summary
17
Form RSSF (B) — Flyash Residuals Sampling Summary (B)
18
Sample Analysis -- Flyash Residuals
19
TCLP Sample Analysis — Flyash Residuals
24
Form PVRF 02T— Flyash Residuals Annual Pathogen Reduction Form
29

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0021577 County: Halifax Year:
2020
Facility Name (as shown on permit):
Land Application Operator:
WestRock Kraft Paper
Chris Williams Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes R1 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generate(] but not land applied, please attach an explanation on lrow the residuals were handled.
Part A - Residuals Application Summarv:
Total number of a lication fields in the ermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
252-533-6237
Part B - Annual Coin fiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division. of Water Resources. ® Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
b) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in I SA NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources,
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I a1n aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Benjamin P. White, General Manager
Permittee Name and Title (type or print)
Lij- 6_
1. z: J_- IL
�" /'
aa2l
Signat re of Permittee Date
Signature of Preparer*
Date Signature of Land Applier
Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) 10FNR FORM ACF (12/2006)

Form DMSDF
Primary Clarifier Residuals
Annual Certification
2020

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Form RSSF
Primary Clarifier Residuals Sampling
Summary

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Form RSSF (B)
Primary Clarifier Residuals Sampling
Summary (B)

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Sample Analysis
Primary Clarifier Residuals

Meritech, Inn.
Environmental Laboratory
E Laboratory Certification No.165
Contact: Chris Williams
Client: WestRock Roanoke Rapids Mill
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 010920127
Parameters Results
Sample: Primary Clarifier Residuals Grab
Analysis Date Analyst
% Total Solids
40.3 %
1/10/20
BF
Ammonia, Nitrogen
111 mg/kg
1/13/20
NW
TKN
1,700 mg/kg
1/17/20
NW
Nitrate/Nitrite Nitrogen
<24.8 mg/kg
1/14/20
NW
Nitrogen, total
1,700 mg/kg
1/17/20
NW
Aluminum, total
6,670 mg/leg
1/16/20
ED
Arsenic, total
4.86 mg/kg
1/16/20
ED
Barium, total
283 mg/kg
1/16/20
ED
Cadmium, total
1.74 mg/kg
1/16/20
ED
Calcium, total
46,200 mg/kg
1/16/20
ED
Chromium, total
15.7 mg/kg
1/16/20
ED
Copper, total
46.9 mg/kg
1/16/20
ED
Lead, total
3.85 mg/kg
1/16/20
ED
Magnesium, total
2,480 mg/kg
1/16/20
ED
Mercury, total
0.025 mg/kg
1/14/20
MR
Molybdenum, total
0.891 mg/kg
1/16/20
ED
Nickel, total
16.3 mg/kg
1/16/20
ED
Phosphorous, total
821 mg/kg
1/16/20
ED
Potassium, total
1,750 mg/kg
1/16/20
ED
Selenium, total
<1.24 mg/kg
1/16/20
ED
Sodium, total
2,510 mg/kg
1/16/20
ED
Zinc, total
155 mg/kg
1/16/20
ED
SAR
1.96 -
1/16/20
ED
pH
7.7 S.il,
1/13/20
JM
CCE*
<1 %
1/16/20
LH
* Results not for regulatory purposes
Report Date:
1/22/2020
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
1/9/2020
Reporting ,Limit
0-100 %
10 mg/kg
20 mg/kg
24.8 mg/kg
20 mg/kg
5.00 mg/kg
1.00 mg/kg
0.500 mg/kg
0.100 mg/kg
10.0 mg/kg
0100 mg/kg
1.00 mg/kg
0.500 mg/kg
10.0 mg/kg
0.02 mg/kg
0,500 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
1.24 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 -14.0 SM
1%
1/9/20
Method
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 2003
EPA 200.7
SM 4500 H B
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Chris Williams
Report Date:
1/20/2020
Client: WestRock Roanoke Rapids Mill
NPDCS#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids,
NC 27870
Date Sample Rcvd:
1/9/2020
Meritech Work Order #
010920118 Sample: PCR A 1/2020 Grab t
1/9/20
Parameters
Results Analysis Date An� alyst
Reporting Limit
Method
% Total Solids
37.0 % 1/14/20 jM
0-100 %
SM 2540B
Fecal Coliform
<246 col/ g dry 1/9/20 CD
246 cal/ g dry
SM 9222 D
Meritech Work Order # 010920119 Sample: PCR B 1/2020 Crab 1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
38A %
1/14/20
jM
0-100 %
SM 2540B
Fecal Coliform
<239 col/ g dry
1/9/20
CD
239 col/ g dry
SM 9222 D
Meritech Work Order #
010920120 Sample: PCR C 1/2020 Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limi
Method
% Total Solids
36.9 %
1/14/20
jM
0-100 ©/o
SM 2540B
Fecal Coliform
<246 col/ g dry'
1/9/20
CD
246 cal/ g dry
SM 9222 D
Meritech Work Order #
010920121 Sample: PCR D 1/2020 Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
37.7 %
1/14/20
jM
0-100 %
SM 2540B
Fecal Coliform
<241 col/ g dry
1/9/20
CD
241 col/ g dry
SM 9222 D
Meritech Work Order #
010920122 Sample: PCR E 1/2020 Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
39.3 %
1/1.4/20
jM
0-100 %
SM 2540B
Fecal Coliform
<231 col/ g dry
1/9/20
CD
231 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laborator
y
ry
Laboratory Certification No. 165
NO
Page
Contact: Chris Williams Report Date: 1/20/2020
CIient: WestRock Roanoke Rapids Mill' NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 1/9/2020
Meritech Work Order # 010920123 Sample: PCR F 1/2020 Grab 1/9/20
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids 38.4 % 1/14/20 jM 0-100 % SM 2540B
Fecal Coliform <237 col/ g dry 1/9/20 CD 237 col/ g dry SM 9222 D
Meritech Work Order # 010920124 Sample: PCR G 1/2020 Grab 1/9/20
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids
36.1 %
1/14/20
jM
0-100 %
SM 2540B
Fecal Coliform
252 col/ g dry
1/9/20
CD
187 col/ g dry
SM 9222 D
I hereby certify that I have reviewed and approve these data. zz�L�
Laboratoty Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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TCLP Sample Analysis
Primary Clarifier Residuals

Contact: Chris Williams
Client: WestRock Roanoke Rapids Mill
100 Gaston Rd.
Roanoke Rapids, NC 27870
Page 1
Report Date: 8/26/2020
NPDES#: WQ0021S77
WQ0000436
Date Sample Rcvd: 8/6/2020
Meritech Work Order # 08062084 Sample: Primary Clarifier Grab 8/6/2020
1311 - TCLP Metals
Parameter
Results
Analysis Date
Analyst
Det. Limit
Reg. Limit
Method
Arsenic
<0A00 mg/L
8/17/2020
ED
0.100
5.0
EPA 200.7
Barium
0.756 mg/L
8/17/2020
ED
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
8/17/2020
ED
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
8/17/2020
ED
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
8/17/2020
ED
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
8/20/2020
MR
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
8/17/2020
ED
0.100
1.0
EPA 200.7
Silver
<0.050 mg/L
8/17/2020
ED
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date
nal st
Reporting Limit
Method
Volatiles 8260
Attached
8/11/2020
VV
-
B260
Semi Vol. 8270
Attached
8/24/2020
PM
-
8270
Other Tests
Parameter
Results
Analysis Date
Analyst
Reporting Limit
Method
Cyanide, total
<OM00 mg/kg
8/11/2020
LH
0.500 mg/kg
EPA 335.4
Sulfide
<10 mg/kg
8/10/2020
LH
10 mg/kg
SW 846 9038
Ignitability
Will Not Ignite
8/18/2020
NW
-
EPA 1030
Corrositivity (pH)
7.9 S.U.
8/14/2020
BF
1.0 -14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Chris Williams Report Date: 8/26/2020
Client: WestRock Roanoke Rapids Mill NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 8/6/2020
Meritech. Work Order # 08062084 Sample: Primary Clarifier Grab 8/6/2020
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
Endrin
Attached - - - -
Chlordane
Attached - - - -
Toxaphene
Attached - - - -
Methoxychlor
Attached - - - -
Heptachlor
Attached - - - -
Lindane
Attached - - - -
Herbicides - SW-846 8151A
Parameter
2,4-D
2,4,5-TP (5ilvex)
Results Analysis Date An_ alyst Det. Limit Reg. Limit Dilution Factor
Attached
Attached
I hereby certify that I have reviewed and approve these data. AkCL QCA;e.
Laboratoty Representative
642 Tanico Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH,INC.
Environmental Laboratories
Laboratory Certificate #165
Client: WestRock Roanoke Rapids Mill
Project: Monthly
Client Sample ID: Primary Clarifier Residuals
Sample Collection: 08/06/20
Meritech Sample ID: 08062084
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 08/11 /20
Extraction:
08/ 10/20
Analyst: V W V
Report Date:
08/13/20
Parameter
Result
Units
Det. Limit
Reg. limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroetliane
<0.0100
mg/L
0,0100
0.50
10
1, 1 -Dichloroethene
< 0A100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
< 0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 08/24/20
Extraction:
08/10/20
Analyst: I'M
Report Date:
08/25/20
Parameter
Result
Units
Det. Limit
Rea. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexaehloroethane
<0.100
rng/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0,100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0,100
2.00
10
2,4-Dinitr6toiuene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and
approve
these data.
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]
12

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Form PVRF 02T
Primary Clarifier Residuals
Annual Pathogen Reduction Form

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: WestRock Kraft Paper WQ Permit Number: WQ0021577
WWTP Name: WestRock Kraft Paper
NPDES Number: NCO000752
Monitoring Period: From 1/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (tithe/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) R1
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs
If applicable to alternative perforated (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thelmophilic ❑
Beta Ray Lirn
Gama RayEl
Pasteurization ❑
_
Class B:
JAIL (1) Fecal Density ❑
I Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Line Stabilization ®
T Air Drying ®
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ®
` .:..:.. ......
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Num er o
dece s
deuces
Frequency
of Analysis
Sample
Type
na ytica
nieue
Mininnrn
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MIN
CFU
1000 mph per gram
of total solid (dry
weight)
<231
241.6
252
col/g dry
0
Annual
Fecal
9222D
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑Alt.
4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying •- Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
R1
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, tinder penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation wiry you have not met one or Moth of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Christopher M. Williams, Env. Engineer No Distribution in 2020
Preparer Narne and Title (type or print) Land Applier Name and Title (if applicable) (type or print)
6e:� rpq
Signature of Preparer" Date Signature of Land Applier (if applicable) Date
'`Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21'.1 102 (26)
15
DENR FORM PVRF 02T (12/2006)

Form DMSDF
Flyash Residuals
Annual Certification
2020

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Form RSSF
Flyash Residuals Sampling
Summary

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Form RSSF (6)
Flyash Residuals Sampling
Summary (B)

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Sample Analysis
Flyash Residuals

Report Date: 1/22/2020
Contact: Chris Williams NPDES#: WQ0021577
Client: WestRock Roanoke Rapids Mill WQ0000436
100 Gaston Rd. Project: Monthly
Roanoke Rapids, NC 27870 Date Sample Rcvd; 1/9/2020
Meritech Work Order #
010920125 Sample: Flyash Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
52.1 %
1/10/20
BF
0-100 %
SM2540B
Ammonia, Nitrogen
81.4 mg/kg
1/13/20
NW
10 mg/kg
EPA 350.1
TKN
361 mg/kg
1/17/20
NW
20 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
<19.1 mg/kg
1/14/20
NW
19.1 mg/kg
EPA 353.2
Nitrogen, total
361 mg/kg
1/17/20
NW
20 mg/kg
EPA 353.2
Aluminum, total
13,200 mg/kg
1/16/20
ED
5.00 mg/kg
EPA 200.7
Arsenic, total
10.5 mg/kg
1/16/20
ED
1.00 mg/kg
EPA 200.7
Barium, total
240 mg/kg
1/16/20
ED
0.500 mg/kg
EPA 200.7
Cadmium, total
0.415 mg/kg
1/16/20
ED
0.100 mg/kg
EPA 200.7
Calcium, total
61550 mg/kg
1/16/20
ED
10.0 mg/kg
EPA 200.7
Chromium, total
18.2 mg/kg
1/16/20
ED
0.100 mg/kg
EPA 200.7
Copper, total
40.5 mg/kg
1/16/20
ED
1.00 mg/kg
EPA 200.7
Lead, total
10.6 mg/kg
1/16/20
ED
0.500 mg/kg
EPA 200.7
Magnesium, total
1,180 mg/kg
1/16/20
ED
10.0 mg/kg
EPA 200.7
Mercury, total
0.058 mg/kg
1/14/20
MR
0.02 mg/kg
EPA 245.1
Molybdenum, total
1.20 mg/kg
1/16/20
ED
0.500 mg/kg
EPA 200.7
Nickel, total
21.3 mg/kg
1/16/20
ED
1.00 mg/kg
EPA 200.7
Phosphorous, total
620 mg/kg
1/16/20
ED
2.00 mg/kg
EPA 200.7
Potassium, total
4,590 mg/kg
1/16/20
ED
20.E mg/kg
EPA 200.7
Selenium, total
<0.960 mg/kg
1/16/20
ED
0.960 mg/kg
EPA 200.7
Sodium, total
1,390 mg/kg
1/16/20
ED
20.0 mg/kg
EPA 200.7
Zinc, total
33.4 mg/kg
1/16/20
ED
1.0 mg/kg
EPA 200.7
SAR
3.00 -
1/16/20
ED
-
-
pH
7.6 S.U.
1/13/20
JM
1.0 - 14.0 S.U.
SM 4500 H B
CCE*
<1 %
1/16/20
LH
1 %
AOAC 955.01
* Results not for regulatory purposes
I hereby certify that I have reviewed and approve these data. Aman(iuAw(r%u
Lab ratory kepi entative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
�,. Environmental Laboratory
Laboratory Certification No.165
a
Page 1
Contact: Chris Williams ReportDate: 1/20/2020
Client: WestRock Roanoke Rapids Mill NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 1/9/2020
Meritech Work Order # 010920111 Sample: Flyash AA 1/2020 Grab 1/9/20
Parameters
Results
Analysis Date
Analyst
Re ortin Limit
Method
% Total Solids
50A %
1/14/20
JM
0-100 %
SM 2540B
Fecal Coliform
<180 col/ g dry
1/9/20
CD
180 col/ g dry
SM 9222 D
Meritech Work Order #
010920112 Sample: Flyash BB 1/2020 Grab .
1/9/2,0
Parameters
Results
Analysis Date
Analyst
Reporting_ Limit
Method
% Total Solids
S0.1 %
1/14/20
)M.
07100 %
SM 2540B
Fecal Coliform
<181 col/ g dry
1/9/20 '
CD` `
181 col/ g dry
SM 9222 D
Meritech Work Order #
010920113 Sample: Flyash CC 1/2020 Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limi
Method
% Total Solids
49.9 %
1/14/20
JM
0-100 %
SM 2540B
Fecal Coliform
<182 col/ g dry
1/9/20
CD
182 col/ g dry
SM 9222 D
Meritech Work Order #
010920114 Sample: Flyash DD 1/2020 Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
49.8 %
1/14/20
JM
0-100 %
SM 2540B
Fecal Coliform
<183 col/ g dry
1/9/20
CD
183 col/ g dry
SM 9222 D
Meritech Work Order #
01092011S Sample: Flyash EE 1/2020 Grab
1/9/20
Parameters
Results
Analysis Date
Analyst
Reporting Limit
Method
% Total Solids
SU %
1/14/20
]M
0-100 %
SM 2540B
Fecal Coliform
<181 col/ g dry
1/9/20
CD
1B1 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
t Laboratory Certification No.165
a Page 2
Contact: Chris Williams Report Date: 1/20/2020
Client: WestRock Roanoke Rapids Mill NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 1/9/2020
Meritech Work Order # 010920116 Sample: Flyash FF 1/2020 Grab 1/9/20
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids 49.1 % 1/14/20 jM 0-100 % SM 2540B
Fecal Conform <185 col/ g dry 1/9/20 CD 185 col/ g dry SM 9222 D
Meritech Work Order # 010920117 Sample: Flyash GG 1/2020 Grab 1/9/20
Parameters
Results
Anal sis Date
Analyst
Reporting Limit
Method
% Total Solids
50.0 %
1/14/20
jM
0-100 %
SM 2540B
Fecal Coliform
<182 col/ g dry
1/9/20
CD
182 col/ g dry
SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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TCLP Sample Analysis
Flyash Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Chris Williams
Client: WestRock Roanoke Rapids Mill
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
Page 1
8/26/2020
WQ0021577
WQ0000436
8/6/2020
Meritech Work Order # 08062082 Sample: Flyash Grab 8/6/2020
1311 - TCLP Metals
Parameter Results Analysis Date Analyst Det, Limit Reg. Limit Method
Arsenic
<0.100 mg/L
8/17/2020
ED
0.100
5.0
EPA 200.7
Barium
1.15 mg/L
8/17/2020
ED
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
8/17/2020
ED
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
8/17/2020
ED
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
8/17/2020
ED
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
8/20/2020
MR
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
8/17/2020
ED
0.100
1,0
EPA 200.7
Silver
<0.050 mg/L
8/17/2020
ED
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date Analyst
Reporting
Limi
Method
Volatiles 8260
Attached
8/11/2020
VV
-
8260
Semi Vol. 8270
Attached
8/24/2020
PM
-
8270
Other Tests
Parameter
Results
Analysis Date
Analyst
Reporting Limit
Method
Cyanide, total
<0.500 mg/kg
8/11/2020
LH
0.500 mg/kg
EPA 335.4
Sulfide
<10 mg/kg
8/10/2020
LH
10 mg/kg
SW 846 9038
Ignitability
Will Not Ignite
8/18/2020
NW
_
EPA 1030
Corrositivity (pH)
8.1 S.U.
8/14/2020
BF
1.0 - 14.0 S.U.
SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Chris Williams Report Date: 8/26/2020
Client: WestRock Roanoke Rapids Mill NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 8/6/2020
Meritech Work Order # 08062082 Sample: Flyash Grab 8/8/2014
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
Endrin
Attached - - - -
Chlordane
Attached - - - -
Toxaphene
Attached - - - -
Methoxychlor
Attached - - - -
Heptachlor
Attached - - - -
Lindane
Attached - - - -
Herbicides - SW-846 8151A
Parameter Results Analysis Date Analyst Det. Limit Reg. Limit Dilution Factor
2,4-D Attached - - - -
2,4,5-TP (Silvex) Attached - - - -
I hereby certify that I have reviewed and approve these data. Jfflwnd a nme
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
Environmental Laboratories
Laboratory Certificate #165
Client: WestRock Roanoke Rapids Mill
Project: Monthly
Client Sample ID: Flyash
Sample Collection: 08/06/20
Meritech Sample ID: 08062082
1311 - TCLP araanics
Volatiles: SW-846 8260
Analysis: 08/ 11 /20
Extraction:
08/10/20
Analyst: V W V
Report Date:
08/13/20
Parameter
Result
Units
Det. Limit
Reg Limit
Dilution Factor
Benzene
<0,0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0,0100
0.50
10
Chlorobenzene
<0.0100
mg/L
0.0100
100
10
Chloroform
<0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
<0.0100
mg/L
0.0100
0.50
10
l,l-Dichloroethene
<0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
<0,100
mg/L
0.100
200
10
Tetrachloroethylene
< 0,0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
t0
Semi-Volatiles: SW-846 8270
Analysis: 08/24/20
Extraction:
08/10/20
Analyst: PM
Report Date:
08/25/20
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
trng/L
0,100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L,
0.100
0.5
10
I lexachloroethane
<0,100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mgIL
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100 `
mg/L
0,100
5.0
10
2,4,5-Trichlorophenol
<D.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
►ng/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0,13
10
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail] 26

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Form PVRF 02T
Flyash Residuals
Annual Pathogen Reduction Form

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: WestRock Kraft Paper WQ Permit Number: WQ0021577
WWTP Name: WestRock Kraft Paper NPDES Number: NCO000752
Monitoring Period: From l/l/2020 To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (tune/temp) ❑
I Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) 01
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Therniophilic ❑
Beta Ray ❑
Gamina Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion
If applicable to alternative performed (Class A or Class R) complete the
following monitoring data:
Allowable l..,evel
Parameter Sludge
in
Pathogen Density
g y
Number o
Bence-
deuces
Frequency
of Analysis
Sample
Type
Analytical
InTech-
Minimui
Geo. Mean
Maximo
Units
2 x 10 to the MPN
6th power
pet, grain of
Fecal Coliform total solids CFU
1000 mpn per grain
of total solid (dry
weight)
<180
182
<185
col/g dry
0
Annual
Fecal
9222D
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
eoliforni) weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) ❑
AIL 4 (Spec. OZ uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable) ❑
JAIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed R
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Christopher M. Williams, Env. Engineer
Preparer Name and Title (type or print)
Signature of Preparer*
No Distributions in 2020
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 1 SA NCAC 2T .1102 (26)
29
DENR FORM PVRF 02T (12/2006)