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WQ0039924_Modification_20210201
Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0039924 Applicant/Permittee von Drehle Corporation Applicant/Permittee Address von Drehle Corporation - Cordova, INC Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Organization Facility Name von Drehle Corporation DCAR County Richmond Fee Category Major Is this a complete application?* c Yes r No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Fee Amount $395 Complete App Date 02/01/2021 Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff Name * Robert T. Branch Email Address* bbranch@branchrs.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ......... .......................................................................................................................................... Application/Document Type* r New (Fee Req ui red) c Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3363129007 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WO0039924 Fbs Current Existing permt number Applicant/Permittee * von Drehle Corporation Applicant/Permittee Address* von Drehle Corporation - Cordova, NC Facility Name * von Drehle Corporation DCAR Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Spec'rfications, Calculations, Rc.) vd_2021_mod Jan 25.pdf 3.09MB upload only 1 RCF docurrent (less than 250 NS). NL@iple documents nest be corrbined into one RDF file unless file is larger than upload limit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 1/25/2021 % State of North Carolina Department of Environmental Quality Division of Water Resources WATER QUALITY REGIONAL OPERATIONS SECTION NON -DISCHARGE APPLICATION REVIEW REQUEST FORM Dlvislon of Water Resources February 1, 2021 To: FRO-WQROS: Trent Allen / Mark Brantley From: Erick Saunders, Water Quality Permitting Section - Non -Discharge Branch Permit Number: WQ0039924 Applicant: von Drehle Corporation Owner Type: Organization Facility Name: von Drehle Corporation DCAR Signature Authority: Justin Dawkins Address: 126 First St., Cordova, NC 28330 Fee Category: Non -Discharge Major Permit Type: Distribution of Residual Solids (503 Exempt) Project Type: Major Modification Owner in BIMS? Yes Facility in BIMS? Yes Title: Plant Manager County: ' Richmond Fee Amount: $395 - Major Modification Comments/Other Information: justin.dawkins@vondrehle.com;.bbranch@branchrs.com Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 45 calendar days, please take the following actions: ® Return this form completed. ® Return a completed staff report. ❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification. When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact person listed above. RO-WQROS Reviewer: J •��j� Date: 3 Z (P /Z/ FORM: WQROSNDARR 09-15 Page 1 of 1 State of North Carolina Division of Water Resources Water Quality Regional Operations Section Environmental Staff Report Quality To: ❑ NPDES Unit ® Non-Dischar eg Unit Attn:' ` Erick Saunders From: Jim Barber Fayetteville Regional Office Application No.: W00039924 Facility name: von Drehle Corporation — Cordova Class A (503 Exempt) . Note: This form has been adapted from the non -discharge facilt staff report to document the review of both non discharge and NPDES permit applications and/or renewals. Please complete all sections as they are applicable. I. GENERAL AND SITE VISIT INFORMATION 1. Was a site visit conducted? Z Yes or ❑ No a. Date of site visit: 9 February 2021 b. Site visit conducted_by: Jim Barber . c. Inspection report attached? ❑ Yes or ® No d. Person contacted: Chris Fowler and'their contact information: 9( 10) 410 - 9131 ext. e. Driving directions: From Rockingham, take US Hwy 1 South approximately 3 miles and turn right at the intersection of US 1 and Rosalyn road. Drive approximately 2 miles and the von Drehle plant is on the right. 2. Discharge Point(s): N/A: Both Class A and Class B residuals are stored behind the main production plant, adiacent to belt press. The coordinates below are the approximate center of the storage area. Latitude: 34.918454 Latitude: Longitude:-79.828977 Longitude: 3. Receiving stream or affected surface waters: N/A (Hitchcock Creek is adjacent to the von Drehle production plant site Classification: "C" River Basin and Subbasin No:: Yadkin -Pee Dee dYAD16) `(13-39-10) Describe receiving stream features and pertinent downstream uses: From the von Drehle plant site to the Pee Dee River is forest/woodlands on both sides the Hitchcock Creek. H. PROPOSED FACILITIES: NEW APPLICATIONS 1. Facility Classification: Proposed flow: Current permitted flow: 2. Are the new treatment facilities adequate for the type of waste and disposal, system? ❑ Yes or ❑ No If no, explain: 3. Are site conditions (soils, depth to water table, etc) consistent with the submitted reports? ❑ Yes ❑ No ❑ N/A If no, please explain FORM: WQROSSR 04-14 Page 1 of 6 4. Do the plans and site map represent the actual site (property lines, wells, etc.)? ❑ Yes ❑ No ® N/A If no, please explain: 5. Is the proposed residuals management plan adequate? ® Yes ❑ No ❑ N/A If no, please explain: 6. Are the proposed application rates (e.g., hydraulic, nutrient) acceptable? ® Yes ❑ No ❑ N/A If no, please explain: 7. Are there any. setback conflicts for proposed treatment, storage and disposal sites? ❑ Yes or ❑ No If yes, attach a map showing conflict areas.. 8. Is the proposed or existing groundwater monitoring program adequate? ❑ Yes ❑ No ❑ N/A If no, explain and recommend any changes to the groundwater monitoring program: 9. For residuals, will seasonal or other restrictions be required? ❑ Yes ❑ No ❑ N/A If yes, attach list of sites with restrictions (Certification B) Describe the residuals handling and utilization scheme: 10. Possible toxic impacts to surface waters: 11. Pretreatment Program (POTWs only): III. EXISTING FACILITIES: MODIFICATION AND RENEWAL APPLICATIONS 1. Are there appropriately certified Operators in Charge (ORCs) for the facility? ® Yes ❑ No ❑ N/A ORC: Chris Fowler Certificate #: LA-1003082 'Backup ORC: Bob Branch Certificate #: LA-15676 2. Are the design, maintenance and operation of the treatment facilities adequate for the type of waste and disposal system? ® Yes or ❑ No If no, please explain: Description of existing facilities: Paper recycling facility that produces press cake residual. At the current. time, von Drehle has a Class A and Class B permit (WO0005135—12,500 DTs/year) and two land application farms for residuals that can't meet Class A standards. Proposed flow: The current modification request is 35,000 DTs/year. Current permitted. flow: Current Dry Tons allowed to be land applied under the Class A permit is 16,499 DTs/year. Explain anything observed during the site visit that needs to be addressed by the permit, or that may be important for the permit writer to know (i.e., equipment condition, function, maintenance; a change in facility ownership, etc.) 3. Are the site conditions (e.g., soils, topography, depth to water table, etc) maintained appropriately and adequately assimilating the waste? ® Yes or ❑ No If no, please explain: 4. Has the site changed in any way that may affect the permit (e.g., drainage added, new wells inside the compliance boundary, new development, etc.)? ❑ Yes or. ® No If yes, please explain: 5. Is the residuals management plan adequate? ® Yes or ❑ No If no, please explain: 6. Are the existing application rates (e.g., hydraulic, nutrient) still acceptable? ® Yes or ❑ No If no, please explain: 7. Is the existing groundwater monitoring program adequate? ❑ Yes ❑ No ® N/A If no, explain and recommend any changes to the groundwater monitoring program: 8. Are there any setback conflicts for existing treatment, storage and disposal sites? ❑ Yes or ® No If yes, attach a map showing conflict areas. FORM: WQROSSR 04-14 Page 2 of 6 9. Is the description of the facilities as written in theexisting permit correct? ® Yes or ❑ No If no, please explain: 10. Were monitoring wells properly constructed and located? ❑ Yes ❑ No ® N/A If no, please explain: FORM: WQROSSR 04-14 Page 3 of 6 11. Are the monitoring well coordinates correct in BIMS? ❑ Yes ❑ No ® N/A If no, please complete the following (expand table if necessary): Monitoring Well Latitude Longitude O 1 It O 1 II O 1 It O 1 II O / 11 O I 11 O I If O / 11 O I 11 O I If 12. Has a review of all self -monitoring data been conducted (e.g., DMR, NDMR, NDAR, GW)? ® Yes or ❑ No Please summarize any findings resulting from this review: Residuals produced are primarily being land applied under the von Drehle Class B permit on two farms; one located outside of Hamlet and one along U.S. Hwy 1 south of Cordova near the South Carolina/North Carolina line. Provide input to help the permit writer evaluate any requests for reduced monitoring, if applicable. 13. Are there any permit changes needed in order to address ongoing BIMS violations? ❑ Yes or ® No If yes, please explain: 14. Check all that apply: ® No compliance issues ❑ Notice(s) of violation ❑ Current enforcement action(s) ❑ Currently under JOC ❑ Currently under SOC ❑ Currently under moratorium Please explain and attach any documents that may help clarify answer/comments (i.e., NOV, NOD, etc.) If the facility has had compliance problems during the permit cycle, -please explain the status. Has the RO been working with the Permitfee? Is a solution underway or in place? Have all compliance dates/conditions in the existing permit been.satisfied? ❑ Yes ❑ No ® N/A If no, please explain: 15. Are there any issues related to compliance/enforcement that should be resolved before issuing this permit? ❑ Yes -® No ❑ N/A If yes, please explain: 16. Possible toxic impacts to surface' waters: N/A 17. Pretreatment Program (POTWs only): N/A FORM: WQROSSR 04-14 Page 4 of 6 1 i IV. REGIONAL OFFICE REC01MUNDATIONS 1. Do you foresee any problems with issuance/renewal of this permit? ❑ Yes or ® No If yes, please explain: 2. List any items that you would like the NPDES Unit or Non -Discharge Unit Central Office to obtain through an - additional information request: Item Reason 3. ,List specific permit conditions recommended to be removed from the permit when issued: Condition Reason 4. List specific special. conditions or compliance schedules recommended to be included in the permit when issue Condition Reason 5. Recommendation: ❑ Hold, pending receipt and review of additional information by regional office ❑ Hold, pending review of draft permit by regional office ❑ Issue upon receipt of needed additional information ® Issue ❑ Deny (Please state reasons: 6. Signature of report preparer: Signature of regional superviE Date: Z FORM: WQROSSR 04-14 Page 5 of 6 V. ADDITIONAL REGIONAL STAFF REVIEW ITEMS Von Drehle is requesting an increase in tonnage for managing Class A cake residuals, with most of the paper residuals managed under the Class A permit marketed to farmers in Richmond, Scotland, Anson and Moore counties that have sandy soil profiles as a'soil amendment (i.e Candor, Wagram, Wakulla, etc.). Some Class A residuals may also be land applied in South Carolina, as in past history. South Carolina DBEC will require von Drehle or Bionomics to apply for a industrial land application permit if Class A residual is to be land applied. Also at this time, Bionomics (residuals contractor for von Drehle) is currently requesting modification of their Class B permit (W00038570) to add von Drehle as a source, along with other nutrient sources and the von Drehle farm sites. The other nutrient sources being request in the Bionomics modification also have their own land application permits that Bionomics administer, hence the von Drehle site will be a secondM permit for residuals management. Once the von Drehle Class A permit is modified and the Bionomics Class B permit modified; von Drehle intends to rescind their Class B permit. Wastewater from belt pressed residuals and domestic flow are discharge to the City of Rockingham collection system/wastewater treatment plant. FORM: WQROSSR 04-14 Page 6 of 6 Barber, Jim From: Thornburg, Nathaniel Sent:. Monday, February 1, 2021 10:31,AM To: Allen, Trent; Brantley, Mark, Barber, Jim Cc: Williams, Kendall; Saunders, Erickson G Subject: [STAFF REPORT REQUEST] WQ0039924 - von Drehle Corporation DCAR, Major Modification Application Attachments: WQ0039924 WQROSNDARR 210201.pdf RO Supervisors — Please assign this project to one of your staff for review. y APPLICATION LINK:. , https://edocs.dell:nc.gov/Wat'erkesodrees/`DocView.asr)x?id=1577669&dbid=0&repo=WaterResources. Kendall, Please process the subject application received February 1, 2021 in BIMS. I've included the RO review request form for your use. I also included the Applicant email addresses in the comment section of RO review request form. Please copy the RO, Reviewer, and myself on the acknowledgement letter that you send to the Applicant. J Thank you, Nathaniel D. Thornburg Branch Chief Non -Discharge Branch Department of Environmental Quality 919 707,3653 office nathaniel.thornburg@ncdenr.gov 512 N. Salisbury St. 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. 1 G, I� �o�Z3 05 14T �� �� c6L/ 3"`:z, N,cb /�, 93 , 93 1 (rvp of SF jcJ- .cu� v ✓ Z jvp �T sF p� 6 Barber, Jim From: Bob Branch <bbranch@branchrs.com> Sent: Tuesday, January 26, 2021 4:44 PM To: Barber, Jim; Martin Mabe Subject: [External] von Drehle Permit Modification Attachments: vd_2021_mod Jan 25.pdf CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam.<mailto:report.spam@nc.gov> All, Attached is von Drehle's permit modification for their Class A. I intend to request to rescind the Class B application upon verification that Bio-Nomic's permit will be accepted. Hope all are doing well. M. 1 PERMIT MODIFICATION FOR THE DISTRIBUTION OF RESIDUAL SOLIDS WQ0039924 VON DREHLE CORPORATION CORDOVA, NC FACILITY FIBER CLAY CORDOVA, NORTH CAROLINA Prepared For: von Drehle Corporation 126 First Street Cordova, NC 28330 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. — Suite 103-291 Rock Hill, SC 29732 January 2021 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd. Suite 103-291, Rock Hill, SC 29732 PHONE (336) 510-0340 • Cell (336) 312-9007 January 25, 2021 NCDEQ -Division of Water Resources Non -Discharge Branch Mail Service Center 1617 Raleigh, North Carolina 27699-1617 Attention: Mr. Nathaniel Thornburg Reference: MODIFICATION PERMIT WQ0039924 von Drehle Corporation — Cordova Facility Cordova, North Carolina BR&S Job No. 2014-110 Dear Mr. Thornburg: Branch Residuals & Soils, LLC is under contract with the von Drehle Corporation to prepare to modify the current Class A distribution permit. von Drehle has transferred land that they own to Bio-Nomics so that applications can continue to be made and a potential nitrogen source that will aid in the breakdown of the fiber clay. This land was previously permitted under von Drehle's permit WQ0005135 for the land application of Class B residual solids. The generated Fiber Clay has no domestic input but is derived from woody sources that are known to have interference with fecal coliform values (Klebsiella sp.). Based on the false positive interferences with the fecal coliform testing procedures, von Drehle will be performing Salmonella testing. Distribution avenues will include application in accordance with soil lime requirements, distribution as a soil amendment (either alone or in concert with other products), distributed to facilities that may blend soil amendments and mulch, and as a daily landfill cover. Please contact me immediately if you require additional information or have questions in the review of the permit application. Sinc , Robert T. Branch, L. S. S. Project Manager cc: Mr. Chris Fowler — von Drehle Corporation — Cordova Facility TABLE OF CONTENTS Section No. Title I DISTRIBUTION OF RESIDUAL SOLIDS APPLICATION FORM Copy of Existing Permit II RESIDUALS SOURCE CERTIFICATION ATTACHMENT — FIBER CLAY Vicinity Map Process Flow Diagram and Narrative Justification of Residuals Production Rate Sampling Plan Residual Analytical Reports III MANAGEMENT PLAN Overview of Process and Residual Solids Handling Distribution Methods for Reuse Transportation and Logistics Monitoring and Recordkeeping Leachate Collection IV VON DREHLE CORDOVA FIBER CLAY LABEL AND PRODUCT INFORMATION SHEET V VON DREHLE CORDOVA FIBER CLAY RESIDUALS RECEIPT FORM VI SPILL CONTROL PLAN VII APPLICATION RATES SECTION I DISTRIBUTION OF RESIDUAL SOLIDS APPLCIATION FORM State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans, specifications, etc. ® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit I Major Modification I Major (residuals permitted for distribution > 3,000 dry tons/year) F $1,310 Minor (residuals permitted for distribution < 3,000 dry tons/year) 1 $810 $395 $245 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Pagel of 3 D. Program Information (All Application Packages) ® Provide a narrative explaining the following: ® How the materials will be handled and transported from where the residuals were produced to where it will be treated. ® How the residuals will be processed/treated (attach process flow diagram). ® How leachate collection will be handled. ® Where the residuals will be stored until processed. ® How the final product will be distributed (packaging, bulk, etc.) ® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ® Name and address of the person who prepared the residual that is sold or given away. ® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ® Information on all applicable setbacks in accordance with 15A NCAC 02T . 1108(b). ® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T .I 108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN -- NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). G. Environmental Assessments (Maybe Required— See 15A NCAC 1 C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) ® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .I 110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: By Courier/Special Delivery: 1617 MAIL SERVICE CENTER 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27699-1617 RALEIGH, NORTH CAROLINA 27604 TELEPHONE NUMBER: (919) 807-6464 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: von Drehle Corporation Applicant type: ❑ Individual N Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Justin Dawkins Title: Plant Manager Applicant's mailing address: 126 First Street City: Cordova State: NC Zip: 28330- Telephone number: (910) 410-9131 Email Address: iustin.dawkinsavondrehle.com 2. Consultant's name: Branch Residuals & Soils, LLC License Number (for P.E.): Affiliation: ❑ On Staff N Retained (Firm: ) Consultant's mailing address: 1735 Heckle Blvd. - Suite 103-291 City: Rock Hill State: SC Zip: 29732- Telephone number: (336) 312-9007 Email Address: bbranch@branchrs.com 3. Fee submitted: $395.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): N new, N modified, ❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00039924 Date of most -recently issued permit: June 28, 2018 Date of most -recently certified Attachment A (if different than the permit): III. FACILITY INFORMATION: 1. Name of residuals processing facility: von Drehle Corporation - Cordova City: Cordova State: NC Zip: 28330- Coordinates: Latitude: 34' 55' 2." Longitude: 79 49' 42" Datum: NAD 83 Level of accuracy: 1' Method of measurement: Man County where facility is located: Richmond 2. Facility contact (person familiar with residuals preparation): Name: Chris fowler Title: Land Application ORC Mailing address: 126 First Street City: Cordova State: NC Zip: 28330- Telephone number: (910) 410-9131 E-mail address: chris.fowlerna vondrehle.com FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 5 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); See Attached Management Plan Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added er 1.0 dry ton of residuals (dry ton None None 3. Approximate amounts of the residuals received and processed at the facility: 22,500 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 35,000 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Residuals are kept on small storage pad prior to loading onto trucks 6. Does the facility have a stormwater management plan? ® Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Due to % solids, free water is not generated, rainwater rewets solids. V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. Residuals Source Certification FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineers Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; I, Justin Dawkins Plant Manager (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for von Drelile Corporation— Cordova, NC Facility (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attacluuents are not included, this application package will be returned to time as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: a�T 1 2d'L1 FORM: DCAR 06-16 Page 3 of 3 Copy of Existing Permit Water Resources ENVIRONMENTAL QUALITY June 28, 2018 JUSTIN DAWIGINS —.PLANT MANAGER VON DREHLE CORPORATION 126 FIRST STREET CORDOVA, NORTH CAROLINA 28330 Dear Mr. Dawkins: ROY COOPER Gvvo-no, MICHAEL S. REGAN se retury LINDA CULPEPPER tnierim Director Subject: Permit No. WQ0039924 von Drehle Corporation DCAR Distribution of Class A Industrial Byproduct Residuals Richmond County In accordance with your permit application request received April 16, 2018, we are forwarding herewith Permit No. WQ0039924 dated June 28, 2018, to the von Drehle Corporation for the start-up and operation of the subject residuals management program. This permit shall be effective from the date of issuance until May 31, 2023, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. In response to questions raised during the review of the permit, the following responses were given: 1. Q: Condition 11.2. How will the damages be assessed in the event of a "third" party or a contractor? A: Condition 111.12 comes into play for part of the answer to this question. If the Permittee knew of the overapplication and did not report it, the Permittee would bear part of the responsibility. If the Permittee knew of the overapplication and did report it, the Permittee would bear none of the responsibility. If the Permittee did not know, then it will become a matter of demonstrating lack of knowledge with a presumption that the Permittee did not know. 2. Q: Condition 11.5. Since von Drehle will have both a Class A and a Class B permit, can Class A pathogen testing be utilized to meet Class B requirements for the Class B permit? A: Yes, as long as they are less than a year old and it passes the Class A requirements. ' ctl irq Compares' ' ., State of North Carolina ( Environmental Quality Water Resources I Water Quality Permitting I Non -Discharge Permitting 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919-807-6332 Mr. Justin Dawkins June 28, 2018 Page 2 of 2 3. Q: Condition H.6. Are these setbacks applicable to temporary 60 days' storage and if not are there any additional requirements? Spelling treatment instead of reatment. A: Yes the setbacks would apply to the temporary storage as well. The 60 days' storage would be considered a temporary facility. And thanks for catching spelling error. 4. Q: Condition IV.6f. Application of this material will not be made based on the Agronomic RYE rates. Use of these rates could provide a false justification of over -application. A: This is a very valid point. Condition IV.6.f has been modified to account for a non -limiting nutrient other than nitrogen. If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need additional information concerning this permit, please contact Troy Doby at (919) 807- 6336 or troy dobyL vngdetingov. Sincerely, �-mda Culpepper, Interim Director J Division of Water Resources cc : Richmond County Health Department (Electronic Copy) Fayetteville Regional Office, Water Quality Regional Operations Section (Electronic Copy) Bob Branch, LSS — Branch Residuals & Soils, LLC (Electronic Copy) Laserfiche File (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Files NORTH CAROLINA ENVIRONMENTAL NIANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH DISTRIBUTION OF CLASS A INDUSTRIAL BYPRODUCT RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO von Drehle Corporation Richmond County FOR THE operation of a residuals management program for von Drehle Corporation and consisting of the distribution of Class A industrial byproduct residuals generated by the approved facility listed in Attachment A with no discharge of wastes to surface waters, pursuant to the application received April 16, 2018, and in conformity with other supporting data subsequently filed and approved by the .Department of Environmental Quality and considered a part of this pen -nit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from the date of issuance until May 31, 2023, and shall be subject to the following specified conditions and limitations: I. SCHEDULES I . No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. [ 15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109] II. PERFORMANCE STANDARDS 1. The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease distribution of residuals, contact the Fayetteville Regional Office supervisor, and take any immediate corrective actions. [G.S. 143-215.1] 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [I SA NCAC 02B .0200, 02L .0100] WQ0039924 Version 1.0 Shell Version 171103 Page 1 of 10 3. Only residuals generated by the facility listed in Attachment A are approved for distribution in accordance with this permit. [G.S. 143-215.1] 4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis): Ceiling Concentration Monthly Average Parameter (milligrams per kilogram) Concentration (milligrams per kilogram) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum Nickel 75 420 n/a 420 Selenium l00 100 Zinc 7,500 , 2,800 [15A NCAC 02T .1105] 5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1106] 6. Setbacks for treatment and storage facilities shall be as follows: Setback Description I Setback Habitable residence or place of public assembly under separate ownership or not to 100 be maintained as part of the prqject site Property lines ( 50 Private or public water supply 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and 50 E wetlands) Wells with exception to monitoring wells 1 100 [15A NCAC 02T. 11081 WQ0039924 Version 1.0 Shell Version 171103 Page 2 of 10 7. Setbacks for Class A land applied bulk residuals shall be as follows: Setback by residual type Setback Description (feet) Liquid Cake' Private or public water supply 100 100 Surface waters (streams — intermittent and perennial, 100 25 perennial waterbodies, and wetlands) Surface water diversions (ephemeral streams, 25 0 waterways, ditches Groundwater lowering ditches (where the bottom of 25 0 the ditch intersects the SHWT) Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15% solids by weight and can be stacked without flowing, as well as can be handled, transported and spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast spreader or other equipment designed for handling solid materials) without leaving any significant liquid fraction behind. [I 5A NCAC 02T .1 108] 8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science(littp:,/nutrients.soil.ncsu.edu/vields/index.L�hp). A copy shall be kept on file and reprinted every five years in accordance with Condition 1V.6. c. Tf the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 .Interagency Group - Guidance Document: Chapter 1 (http://www.ncacr.cov/SWCI'tecli/documctits!9tli Guidance Doc 100109.10). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards (tip:/Mp-fo,sc.e,-,ov.usda.iov,'N[IQ practice-standards/staridards'590. )di . d. if the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [15A NCAC 02T .I 109(b)(1)(k)] WQ0039924 Version 1.0 Shell Version 171103 Page 3 of 10 9. The Permittee shall not distribute Class A industrial byproduct residuals that have a sodium adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAR content; has agreed on proper residual application rates; and has agreed to operational considerations to ensure that the high SAR content will not adversely impact the receiving sites. Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist. [15A NCAC 02T .0108(b)(1)] Ill. OPERATION AND MAINTENANCE REQUIREMENTS The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [ 15A NCAC 02T .1110] 2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a. Operational functions; b. Maintenance schedules; c. Safety measures; d. Spill response plan; e. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f. Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen reduction requirements (e.g. facilities that distribute multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [ 15A NCAC 02T .1100] WQ0039924 Version 1.0 Shell Version 171103 Page 4 of 10 3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .020 1. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition IIL2.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and:Enforcement Branch at (919) 707-9105. At the time of this permit issuance, a certified ORC is not required for the subject Distribution of Class A Residuals program. [15A NCAC 02T .01 17] 4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. [15A NCAC 02T .0108(b)(1)] 5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. [15A NCAC 02T .1110] 6. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. [G.S. 143-215.1 ] 7. When the Permittec land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. [15A NCAC 02T .1109(b)(1)] 8. Bulk residuals shall not be land applied under the following conditions a. if the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. if the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; i. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; j. If the vertical separation of bedrock and the depth of residuals application is less than one foot; k. Application exceeds agronomic rates. [15A NCAC 02T .l 109] W00039924 Version 1.0 Shell Version 171 t03 Page 5 of 10 9. The Permittee shall notify all third -party entities receiving bulk distributed Class A industrial byproduct residuals that land application activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T .1108(b)(1) and 02T .1109(b) (i.e., Conditions II.8. and III.8., respectively). [15A NCAC 02T .1103(5)] 10. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third - party entity. If bulk residuals are to be applied, the residuals may be staged at the application site for up to 30 days for biological residuals, and 60 days for non -biological residuals. if an alternate storage site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)] 11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land application, or an information sheet shall be provided to the person who receives Class A residuals. At a minimum, the label or information sheet shall contain the following: a. The name and address of the person who prepared the residuals; b. A statement that residual land application is prohibited except in accordance with the instructions on the label or information sheet; c. A statement identifying that this material shall be prevented from entering any public or private water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.); d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its intended use. [15A NCAC 02T .1109(a)] 12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the conditions of this permit. The Permittee shall report to the Fayetteville Regional Office as per reporting conditions under Condition W.8. any person or entity known to be applying residuals contrary to the condition of this permit. [15A NCAC 02T . 1103(a)] WQ0039924 Version 1.0 Shell Version 171103 Page 6 of 10 IV. MONITORING AND REPORTING REQUIREMENTS 1. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [ 15A NCAC 02'1' .0108(c)] Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five year. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) I 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) I 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) I 1,.1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) j 2.4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) j Hexachloroben-zene (0.13) Tetrachloroethylene (0.7) I Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0 008) Toxaphene (0.5) I Chloroform (6.0) Chromium (5.0) I Hexachloro-.l,3-butadiene (0.5) Hexachloroethane (3.0) 1 Trichloroethylene (0.5) 2,4.5-Trichlorophenol (400.0) in -Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxyehlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Pennittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. [15A NCAC 13A .0102(b), 02T .1 101, 02T .1 105] WQ0039924 Version 1.0 Shell Version 171103 Page 7 of 10 3. An analysis shall be conducted on the residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum--- ---Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen I Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH I Zinc Lead Phosphorus Magnesium I Plant Available Nitrogen L (by calculation) [15A NCAC 02T .]101] 4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .l 111(c)] 5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .0505] 6. The Permittee shall maintain records tracking all bulk residual distribution or land application events performed by the Permittee. At a minimum, these records shall include the following: a. Source of residuals; b. Date of distribution/land application; c. Name and address of recipient of residuals; d. Volume of residuals distributed to each recipient; e. Intended use of residuals; f. If land application events performed by the Permittee: i. When the agronomic rate is on the basis of Nitrogen, then the Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years). ii. When the agronomic rate is on the basis of some other nutrient than Nitrogen, then this shall be included as part of the Operations & Maintenance Plan required in Condition III.2. A set of calculations shall be performed to show that the residuals are being applied at an agronomic rate on the basis of this limiting nutrient. These records shall be kept for a minimum of five years and shall be available for inspection. [15A NCAC 02T .0108(a)] WQ0039924 Version 1.0 Shell Version 171103 Page 8 of 10 7. Three copies of an annual report shall be submitted on or before March I". The annual report shall meet the requirements described in the Instructions for Residuals At1plication Annual Reporting Forms. Instructions for reporting and annual report forms are available at Lap:41decl.nc. Lov/aboLiUdivisions!water-resourceshvater-resources-i)erm its!wastewater-brancll!non- discharae-pernnittins,-unit/rei)ortini,-forms, or can be obtained by contacting the Non -Discharge Permitting Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [I 5A NCAC 02T .1111(a)] 8. Noncompliance Notification The Permittee shall report by telephone to the Fayetteville Regional Office, telephone number (910) 433-3300, as soon as possible. but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Distribution of residuals abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to surface waters. c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(l), 02T .0108(b)(1)] V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. [ 15A NCAC 02T .0108(b)] 2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator errors that could result in discharges to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the distribution sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)] WQ0039924 Version 1.0 Shell Version 171103 Page 9 of 10 VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to 143-215.6C. [G.S. 143-215.6A to 143-215.6C] 2. This permit shall become voidable if the residuals distribution events are not carried out in accordance with the conditions of this permit. [ 15A NCAC 02T .0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. [G.S. 143-215.1] 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO10000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [15ANCAC 02T .0105(c)(6)] 5. 1n the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. [15A NCAC 02T .0104] 6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [ 15A NCAC 02T .0110] 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). [15A NCAC 02T .0120] 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T .0105(e)(3)] Permit issued this the 281h day of June 2018 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSIONi ?Linda Culpepper, Interim Director Division of Water Resources By Authority of the Environmental Ma tipacn ent Commission Permit Number `'VQ0039924 WQ0039924 Version 1.0 Shell Version 171103 Page 10 of 10 ATTACHMENT A — Approved Residual Sources Certification Date: June 28, 2018 von Drehle Corporation Permit Number: WQ0039924 Version: 1.0 Maximum Monitoring Monitoring Monitoring Frequency for Approved Owner Facility Name County Permit Biological Dry Tons Frequency for I Frequency for Pathogen & Mineralization Number Residuals Per Year 1 Non -hazardous = Metals and s's Vector Attraction Rate Characteristics Nutrients Reductions' S 6 von Drehle Corporation von Drehle Corporation W WTP Richmond WQ0039924 No 1G,499 f Annually See Footnote 5 See lbotnote 5 - - _--• 0 1 -—_......_.._.,�. Total i 16,499 I . Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP. ignitability, reactivity, and corrosivity) as stipulated under permit Condition 1V.2 3. Testing of metals and nutrients as stipulated under permit Condition iV.3 4. Analyses of pathogen reductions as stipulated under permit Condition IVA. 5 Monitoring frequencies are based on the actual dry torts applied per year using the table below, unless specified ahove. Dry Tons Distributed 1 Monitoring Frequency (short tons per year} (Established in 40 CFR 503 and ISA NCAC 02T.1111) <319 11 - - _ I/Yedr =>3I9 - t1,650 _ _ I Quaver i4 times per year => 1,650 - <16,500 1/60 Days (6 times per year =>16,500 I 1/month (l2 times peryutr) — 6. Class A industrial byproduct residuals arc exempt from meeting the vector attraction reduction requirements in Condition IVA, provided they are not mixed with residuals that have been geiierdled during the treatment of domestic wastewater, the treatment of animal processing wastewater. or die biological treatment of industrial wastewater. The Class A industrial byproduct residuals must be treated and processed in a manner as to not meet the definition of"Biological Residuals" as defined in 15A NCAC 02T.1102(6). If no distribution events occur during a required sampling period (e.g. no distribution of residuals occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. W00039924 Version 1.0 Attachment A Paae I of I SECTION II RESIDUALS SOURCE CERTIFICATION ATTACHMENT - FIBER CLAY DWR State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and sunportine documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: von Drehle Corporation, Cordova, NC facility Status a Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed N Von Drehle Corporation Cordova, NC Richmond 16,499 35,000 'Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 Division of Water Resources I. II. State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: von Drehle Corporation 2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ® Private. Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Chris Fowler, Land Application ORC Complete mailing address: 126 First Street City: Cordova State: NC Zip: 28330- Telephone number: (910) 410-9131 E-mail address: chris.fowler(o-)vondrehle.com 4. Facility physical address: 126 First Street City: Cordova State: NC Zip: 28330- Coordinates: Latitude: 34' 55' 2.73" Longitude: 79' 49' 42.77" Datum: NAD 83 Level of accuracy: 1' Method of measurement: Man 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ® treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ❑ Yes ® No 7. Facility permitted/design flow: 0.395 MGD and facility average daily flow: 0.272 MGD 8. Average amount of residuals being generated at this facility 35,000 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Separation and Belt Press Type and volume of residuals storage (i.e., outside of residuals treatment units): Storage pad 150 cubic yards RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ❑ 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ❑ Biological ® Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Microbac and Date of analysis: March 6, 2020 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: WNI IF (> 140°F) Passed reactivity test: ® yes ❑no. HCN: <10.0 mg/kg (<250) & H2S: <100 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (m9/1) Result (mg/1) Arsenic 5.0 <0.200 Hexachlorobenzene 0.13 <0.05 Barium 100.0 0.246 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.05 Hexachloroethane 3.0 <0.05 Cadmium 1.0 <0.0200 Lead 5.0 <0.2 Carbon Tetrachloride 0.5 <0.05 Lindane 0.4 <0.0005 Chlordane 0.03 <0.0005 Mercury 0.2 <0.002 Chlorobenzene 100.0 <0.05 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.05 Methyl Ethyl Ketone 200.0 <0.10 Chromium 5.0 <0.0500 Nitrobenzene 2.0 <0.05 m-Cresol 200.0 <0.05 Pentachlorophenol 100.0 <0.25 o-Cresol 200.0 <0.05 Pyridine 5.0 <0.25 p-Cresol 200.0 <0.05 Selenium 1.0 <0.35 Cresol 200.0 <0.15 Silver 5.0 <0.10 2,4-D 10.0 <0.02 Tetrachloroethylene 0.7 <0.05 1,4-Dichlorobenzene 7.5 <0.05 Toxaphene 0.5 <0.01 1,2-Dichloroethane 0.5 <0.05 Trichloroethylene 0.5 <0.05 1, 1 -Dichloroethylene 0.7 <0.05 214,5-Trichlorophenol 400.0 <0.05 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.05 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0.002 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.1 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Microbac and Date of analysis: November 23, 2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mglk-g) (mglkg) (mglkg) Arsenic 75 41 <1.8900 Cadmium 85 39 0.1990 Copper 4,300 1,500 32.0000 Lead 840 300 <1.8900 Mercury 57 17 <0.6580 Molybdenum 75 n/a <5.6700 Nickel 420 420 <3.7800 Selenium 100 100 <1.8900 Zinc 7,500 2,800 74.3000 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/hg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 42.3 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutnent parameters: Laboratory: Microbac and Date of analysis: November 23, 2020 Parameter Result (mg1kg) Aluminum 1,3 60.00 Ammonia -Nitrogen <4.50 Calcium 21,900.00 Magnesium 2,220.00 Nitrate -Nitrite Nitrogen 0.69 pH (Standard Unit) 8.20 Phosphorus 3.50 Potassium <94.50 Sodium 805.00 Total Kjeldahl Nitrogen 1,940.00 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.90 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.40 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mg1kg) (mg/kg) Surface 777 1,164 Injection/Incorporation 779 1,166 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ® A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T. 1 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] -Injection. . ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] -Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T. 1107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of Vicinity Map I� Von Drehle Corporation a CoTdova'ic y� d} her 9y r G�ry� ry` c+ ` sy� 0 G '4 C, Gr 6 G'd ode •o 0 ° r R Q. �� °men Cir Os c q o � Carlo C' Trent S Grc� Ca Sources Esri, HE E, Del_or e, USGS, Intermap, INCREMENT P. NRCan, Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri''V (Thailand), Mapmylndia, NOGG, © OpenStreetMap contributors, and the GIS User Community o SCALE: 1 "= 1,500 ft Triple S Farms Facility CHECKED BY: RTB Land Application Program Vicinity RTB BRANCH von Drehle Corporation Mapty DRAWN BY: RESIDUALS DATE: 1/8/2021 81 SOILS, LLC Project No. 2014-110 Process Flow Diagram and Narrative FIBER CLAY PROCESS NARRATIVE Recycled paper in bales is released and placed in the pulping process. There, mixed with water, the recycled paper is reduced to pulp. The pulp is sent through a de -trashing system, where large metals and plastics such as plastic bags or soda cans are removed. These large rejects are deposited in an indoor pit to be removed to landfill. From here, the accepted material is sent to a holding chest where it is fed into the pulp cleaning and screening system. The first stage of the cleaning and screening system is responsible for the removal of dense contaminants such as glass and small metal pieces such as staples. The next stage is the coarse screening stage which removes smaller plastics that are slightly larger than .06 inches in diameter; these plastics, as well as the glass and small metals, are ultimately deposited in the previously mentioned indoor pit. Following this stage is the centrifugal forward cleaning stage. In this stage, lighter, but still relatively dense particles, such as sand and dirt, are separated by centrifugal force from pulp and ultimately rejected to the mill sump. The final stage of cleaning and screening is the fine screening stage. In the fine screening stage, very small (slightly larger than. 005 inches), light contaminants s u c h a s s t i c k i e s, ink particles and smaller dirt particles are removed and ultimately sent to the mill sump as well. From the mill sump, these rejected solids are sent to a Krofta DAF clarifier where they are coagulated, floated and skimmed off the surface and sent to a belt press where it is dewatered to approximately 40% solids and deposited onto the fiber clay pad outside. The accepted material from the fine screening stage is sent to a Variosplit washing system where through a dewatering process of the pulp, very fine ash and fiber fines are removed. These rejects are sent to a Tauro DAF clarifier where they are removed in a similar fashion as with the Krofta and sent to the belt press to be dewatered and deposited on the fiber clay pad. Accepted pulp from the washing stage is sent to a screw press for further dewatering, and the pulp is then fed into a high temperature dispersion system, where any remaining small contaminants such as dirt and stickies are pulverized to a size smaller than what can be seen with the human eye. The pulp is also mixed with a bleaching agent at high temperature and is sent to a bleaching tower to allow the bleaching process to take place and increase pulp brightness. The pulp is then mixed with water and diluted to 5% solids and sent to the paper machines. At the paper machines, the pulp is applied to a press felt, while simultaneously being dewatered with a poly wire belt; a sheet of paper is formed, which is pressed, dried, and rolled up to be shipped. In this process, more ash and fines are removed and are ultimately sent to a Megacell DAF clarifier where, as with the other DAF units, a fiber clay blanket is formed, sent to the belt press and then the fiber clay pad. The water from each of these DAF units is generally re -used in the process, with the excess being discharged to the City of Rockingham wastewater treatment system. Following is the process flow schematic diagram for the water and solids in von Drehle Corporation Cordova's Paper Process. Recycled Paper Process for von Drehle Corporation Recycled Paper in Bales Fail Dump Chest HD Cleaner Coarse Screen Fail Fine Screens Chemicals Pulping Water Process Trash & Size Pass Screens Fail Pass VarioSplit Screw Press Tauro rifical Krofta Reject Fail Centrifugal DAF Chest t Cleaning Landfill Belt Press Fiber Clay ,and Applicatioi Or Distribution Process Water Recycled or sent to City of Rockingham Bleaching Tower Paper Machines Justification of Residuals Production Rate JUSTIFICATION OF RESIDUALS PRODUCTION RATE von Drehle Corporation produces approximately 22,500 dry tons of the Fiber Clay annually. In order to account for variability, the dry ton permit limit will be set at 35,000 dry tons. Sampling Plan FIBER CLAY SAMPLING PLAN von Drehle Fiber Clay is transported by conveyor from the belt presses to the storage pad in the back at von Drehle's facility in Cordova. Fiber Clay will be distributed by placement onto sealed trailers that will be routed to one of several marketing sites, non-specific receiver sites or to the landfill as daily cover. Based on the amount of residual to be distributed, von Drehle Fiber Clay will be sampled monthly from the belt presses. Representative samples of von Drehle Fiber Clay will be collected and composited prior to the beginning of the preceding monthly cycle so that data will be made available prior to that distribution period. Seven independent grab samples will be collected monthly for Salmonella analysis. These samples will be immediately placed on ice and delivered to a lab certified in the testing protocol. Since there are no labs that are certified for the state of North Carolina for the Salmonella testing, at a minimum this lab has certification such as Nation Environmental Laboratory Accreditation Conference (NELAC). If at an any point, North Carolina has a lab that becomes accredited and is close enough to meet the necessary hold times, they will be used. All samples will be sent to qualified laboratories that are familiar with the environmental sample preparation and standards required. Annually, a residuals solid sample will be analyzed for toxicity characteristics leaching procedure (TCLP). TCLP parameters are listed below: Arsenic Cadmium Chlorobenzene o-Cresol Cresol 1,2-Dichloroethane Endrin Hexachloroethane Lindane Methyl ethyl ketone Pyridine Tetrachloroethylene 2,4,5-Trichlorophenol Vinyl chloride Barium Benzene Carbon tetrachloride Chlordane Chloroform Chromium m-Cresol p-Cresol 2, 4-D 1,4-Dichlorobenzene 1, 1 -Dichloroethylene 2,4-Dinitrotoluene Hexachlorobenzene Heptachlor (and its hydroxide) Lead Hexachloro-1,3-butadiene Mercury Methoxychlor Nitrobenzene Pentachlorophenol Selenium Silver Toxaphene Trichloroethylene 2,4,6-Trichlorophenol 2,4,5-TP (Silvex) Monthly (prior to the end of the preceding monthly period,) a composite Fiber Clay residual solid sample will be collected and analyzed for: Cadmium, Copper, Lead, Nickel, Zinc, Aluminum, Ammonia — Nitrogen, Nitrate -Nitrite, Nitrogen, % Total Solids, pH, Phosphorus, Potassium, TKN, and Calcium Carbonate Equivalency (CCE). From this information, the Plant Available Nitrogen (PAN) and Agricultural Lime Equivalency (ALE) will be calculated. This will be the basis for the application rates that will be used in the next monitoring period and changes will be made to the product label to reflect the most recent analytical data. Residual Analytical Reports VMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Project Description Residuals Sample -Annual For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Friday, March 6, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 14 ��0MICROBAC° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOBO372 Von Drehle Corporation Project Name: Residuals Sample - Annual Mr. Chris Fowler Project / PO Number: 2030767 126 First Street Received: 02/25/2020 Cordova, NC 28330 Reported: 03/06/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from paper plant KOB0372-01 Solid Grab 02/25/20 12:09 02/25/20 14:57 Page 2 of 14 IMICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Analytical Testing Parameters Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOB0372-01 Collection Date: 02/25/2020 12 0 Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Inorganics Total Result RL Units Dilution Note Prepared Analyzed Analyst EPA 9045D pH 8.4 S.U. 1 H4 03/05/20 1526 03/05/20 1630 EPT SW-846 7.3.3.2 Reactive Cyanide <10.0 10.0 mg/kg 1 y 03/06/20 1110 03/06/20 1146 JRH SW-846 7.3.4.1 Reactive Sulfide <100 100 mg/kg 1 y 03/06/20 1006 03/06/20 1048 EPT General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst ASTM D2216-10 Percent Solids 38.0 1.00 % (by wt.) 1 y 03/03/20 1327 03/04/20 0609 CEi EPA 1030 Ignitability of Solids �2 2 2.2 mm/sec 1 y 03/04/20 0000 CSH Metals TCLP by AA Result RL Units Dilution Note Prepared Analyzed Analyst EPA 7470A Mercury <0.00200 0.00200 mg/L 1 03/02/20 0656 03/03/20 1013 TMM Metals TCLP by ICP Result RL Units Dilution Note Prepared Analyzed Analyst EPA 6010E Arsenic <0.200 0.200 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Barium 0.246 0.100 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Cadmium <0.0200 0.0200 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Chromium <0.0500 0.0500 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Lead <0.200 0.200 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Selenium <0.350 0.350 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Silver <0.100 0.100 mg/L 1 y 03/02/20 0714 03/02/20 1640 KHL Volatile Organic Compounds TCLP Result RL Units Dilution Note Prepared Analyzed Analyst by GCMS EPA 8260B Benzene <50.0 50.0 uglL 10 03/04/20 1723 ZTL 2-Butanone <100 100 ug/L 10 03/04/20 1723 ZTL Carbon tetrachloride <50.0 50.0 ug/L 10 03/04/20 1723 ZTL Chlorobenzene <50.0 50.0 ug/L 10 03/04/20 1723 ZTL Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NIC 28306 1910.864.1920 p I www.microbac.com I Page 3 of 14 (t-DMICRORAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOB0372-01 Collection Date: 02/25/2020 12 '9 Volatile Organic Compounds TCLP Result RL Units Dilution Note Prepared Analyzed Analyst by GCMS Chloroform <50.0 50.0 ug/L 10 03/04/20 1723 ZTL 1,2-Dichloroethane <50.0 50.0 ug/L 10 y 03/04/20 1723 ZTL 1,1-Dichloroethene <50.0 50.0 ug/L 10 y 03/04/20 1723 ZTL Tetrachloroethene <50.0 50.0 ug/L 10 03/04/20 1723 ZTL Trichloroelhene <50.0 50.0 ug/L 10 03/04/20 1723 ZTL Vinyl chloride <100 100 ug/L 10 03/04/20 1723 ZTL Surrogate: 4-Bromofluorobenzene 104 Limit: 86-115 % Rec 10 03/04/20 1723 ZTL Surrogate: Dibromofluoromethane 95.9 Limit: 86-118 % Rec 10 03/04/20 1723 ZTL Surrogate:1,2-Dichloroethane-d4 93.5 Limit: 80-120 % Rec 10 03/04/20 1723 ZTL Surrogate: Toluene-d8 104 Limit: 88-110 % Rec 10 03/04/20 1723 ZTL Herbicides TCLP by GC/ECD Result RL Units Dilution Note Prepared Analyzed Analyst EPA 8151A 2,4,5-TP (Silvex) [2C] <2.00 2.00 ug/L 1 03/02/20 1600 03103120 2006 ECL 2,4-D [2C] <20.0 20.0 ug/L 1 03/02/20 1600 03/03/20 2006 ECL Surrogate: 2,4-Dichloropenylacetic acid 53.7 Limit: 20-144 % Rec 1 03/02/20 1600 03/03/20 2006 ECL [2C] Pesticides TCLP by GC/ECD Result RL Units Dilution Note Prepared Analyzed Analyst EPA 8081A alpha -Chlordane <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL Endrin <0.500 0.500 ug/L 1 03/02/20 0910 03/04120 2152 ECL gamma Chlordane <0.500 0.500 ug/L 1 03/02/20 0910 03/04120 2152 ECL gamma-BHC (Lindane) <0.500 0.500 ug/L 1 03/02/20 0910 03/04120 2152 ECL Heptachlor <0.500 0.500 ug/L 1 03/02/20 0910 03/04120 2152 ECL Heptachlor epoxide <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL Methoxychlor <0.500 0.500 ug/L 1 03/02/20 0910 03/04/20 2152 ECL Toxaphene <10.0 10.0 ug/L 1 03/02/20 0910 03/04/20 2152 ECL Surrogate: 2,4,5,6-Tetrachloro-m-xylene 74.0 Limit: 20-130 % Rec 1 03102/20 0910 03/04/20 2152 ECL Surrogate: Decachlorobiphenyl 49.9 Limit: 25-140 % Rec 1 03/02/20 0910 03/04/20 2152 ECL (BZ-209) Semivolatile Organic Compounds Result RL Units Dilution Note Prepared Analyzed Analyst TCLP by GCMS EPA 8270C Pyridine <250 250 ug/L 1 y 03/02/20 1350 03/03120 1716 SCB 1,4-Dichlorobenzene <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03120 1716 SCB 2-Methylphenol <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03120 1716 SCB 3-,4-Methylphenol <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB Hexachloroethane <50.0 50.0 ug/L 1 y 03/02/20 1350 03103/20 1716 SCB Nitrobenzene <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 Of 14 ('-.VMICROBAC`� Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K060372-01 Collection Date: 02/25/2020 12 Semivolatile Organic Compounds TCLP by GCMS Hexachlorobutadiene 2,4, 6-Trichlorophenol 2,4, 5-Trichlorophenol 2,4-Dinitrotoluene Hexachlorobenzene Pentachlorophenol Surrogate: 2-FI uorophenol Surrogate: Phenol-d5 Surrogate: Nitrobenzene-d5 Surrogate: 2-Fluorobi phenyl Surrogate: 2,4,6-Tribromophenol Surrogate: p-Terphenyl-d14 Result RL Units Dilution Note Prepared Analyzed Analyst <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB <50.0 50.0 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB <250 250 ug/L 1 y 03/02/20 1350 03/03/20 1716 SCB 59.0 Limit: 19-119 % Rec 1 03/02/20 1350 03/03/20 1716 SC8 36.0 Limit: 10-120 % Rec 1 03/02/20 1350 03/03/20 1716 SCB 89.7 Limit: 35-114 % Rec 1 03/02/20 1350 03/03120 1716 SCB 94.9 Limit: 43-116 % Rec 1 03/02/20 1350 03/03120 1716 SCB 149 Limit: 22-142 % Rec 1 S1 03/02/20 1350 03/03/20 1716 SCB 84.3 Limit: 10-130 % Rec 1 03/02/20 1350 03/03/20 1716 SCB Microbac Laboratories. Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 0 14 ff >,y M i f' Irl R, A C 1_..; Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes Batch B00O292 - Wet Chem -Default Prep - EPA 9045D LCS (B00O292-BS1) Prepared &Analyzed: 03/05/2020 pH 6.0 S.U. 6.03 99.6 0-200 LCS (B00O292-BS2) Prepared & Analyzed: 03/05/2020 pH 9.0 S.U. 9.01 100 0-200 Duplicate (B00O292-DUP1) Source: KOB0372-01 Prepared &Analyzed: 03/05/2020 pH 8.6 S.U. 8.4 1.89 5 Batch B000321 - Wet Chem -Default Prep - SW-846 7.3.4.1 Blank (B000321-BLK1) Prepared &Analyzed: 03/06/2020 Reactive Sulfide <100 100 mg/kg LCS (B000321-BS1) Prepared &Analyzed: 03/06/2020 Reactive Sulfide <100 100 mg/kg 474 50-150 LCS (B000321-BS2) Prepared & Analyzed: 03/06/2020 Reactive Sulfide 1250 100 mg/kg 1580 79.1 50-150 Duplicate (B000321-DUP1) Source: MOB2142-01 Prepared &Analyzed: 03/06/2020 Reactive Sulfide <100 100 mg/kg ND 50 Batch B000326 - Reactive Cyanide/Sulfide - SW-846 7.3.3.2 LCS (B000326-BS1) Prepared &Analyzed: 03/06/2020 Reactive Cyanide <500 500 mg/kg 0.5-100 Duplicate (B000326-DUP7) Source: MOB2142-01 Prepared &Analyzed: 03/06/2020 Reactive Cyanide <10.0 10.0 mg/kg ND 50 Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000130 - Wet-Solids-S - ASTM D2216-10 Blank (B000130-BLK1) Prepared: 03/03/2020 Analyzed: 03/04/2020 Percent Solids 100 1.00 % (by wt.) LCS (B000130-BS1) Prepared: 03/03/2020 Analyzed: 03/04/2020 Percent Solids 77.6 % (by 80.0 97.0 90-110 wt.) Duplicate (B000130-DUP1) Source: KOB0372-01 Prepared: 03/03/2020 Analyzed: 03/04/2020 Percent Solids 38.2 1.00 % (by 38.0 0.499 10 wt.) Batch B000168 - Ignitability Prep - EPA 1030 LCS (B000168-BSI) Prepared &Analyzed: 03/04/2020 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 14 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000168 - Ignitability Prep - EPA 1030 LCS (B000168-BSI) Ignitability of Solids 2.5 Metals TCLP by AA Result Batch B000010 - EPA 245.1 & EPA 7470A - EPA 7470A Prepared & Analyzed: 03/04/2020 2.2 mm/sec 2.4 102 88-111 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Blank (B000010-BLK1) Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury <0.000200 0.000200 mg/L LCS (B000010-BSI) Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.00388 0.000200 mg/L 0.00400 96.9 80-120 Matrix Spike (B000010-MS1) Source: MOB1975-03 Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.0378 0.00200 mg/L 0.0400 ND 94.4 75-125 Matrix Spike Dup (B000010-MSD1) Source: MOB1975-03 Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.0373 0.00200 mg/L 0.0400 ND 93.2 75-125 1.31 Post Spike (B000010-PS1) Source: MOB1975-03 Prepared: 03/02/2020 Analyzed: 03/03/2020 Mercury 0.965 ug/L 1.00 0.00927 95.6 85-115 20 Spike Source %REC RPD Metals TCLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000013 - 3015A 6010 -EPA 6010E Blank (B000013-BLK1) Prepared & Analyzed: 03/02/2020 Arsenic <0.0250 0.0250 mg/L Barium <0.0125 0.0125 mg/L Cadmium <0.00250 0.00250 mg/L Chromium <0.00625 0.00625 mg/L Lead <0.0250 0.0250 mg/L Selenium <0.0438 0.0438 mg/L Silver <0.0125 0.0125 mg/L LCS (B000013-BS1) Prepared & Analyzed: 03/02/2020 Arsenic 0.242 0.0250 mg/L 0.250 97.0 80-120 Barium 0.627 0.0125 mg/L 0.625 100 80-120 Cadmium 0.0311 0.00250 mg/L 0.0313 99.6 80-120 Chromium 0.314 0.00625 mg/L 0.313 101 80-120 Lead 0.321 0.0250 mg/L 0.313 103 80-120 Selenium 0.236 0.0438 mg/L 0.250 94.5 80-120 Silver 0.247 0.0125 mg/L 0.250 98.9 80-120 Matrix Spike (B000013-MS1) Source: MOB1971-02 Prepared & Analyzed: 03/02/2020 Arsenic 0.243 0.0250 mg/L 0.250 ND 97.3 75-125 Barium 0.666 0.0125 mg/L 0.625 0.0255 103 75-125 Cadmium 0.0313 0.00250 mg/L 0.0313 ND 100 75-125 Chromium 0.319 0.00625 mg/L 0.313 ND 102 75-125 Lead 0.323 0.0250 mg/L 0.313 ND 103 75-125 Selenium 0.239 0.0438 mg/L 0.250 ND 95.6 75-125 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 oE471 l,�).)MICROBAC'` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Metals TCLP by ICP Result Batch B000013 - 3015A 6010 - EPA 6010E RL Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Matrix Spike (B000013-MS1) Source: MOB1971-02 Prepared &Analyzed: 03/02/2020 Silver 0.252 0.0125 mg/L 0.250 ND 101 75-125 Matrix Spike Dup (B000013-MSD1) Source: MOB1971-02 Prepared & Analyzed: 03/02/2020 Arsenic 0.248 0.0250 mg/L 0.250 ND 99.1 75-125 1.75 20 Barium 0.662 0.0125 mg/L 0.625 0.0255 102 75-125 0.617 20 Cadmium 0.0311 0.00250 mg/L 0.0313 ND 99.6 75-125 0.681 20 Chromium 0.318 0.00625 mg/L 0.313 ND 102 75-125 0.133 20 Lead 0.321 0.0250 mg/L 0.313 ND 103 75-125 0.590 20 Selenium 0.245 0.0438 mg/L 0.250 ND 97.9 75-125 2.40 20 Silver 0.249 0.0125 mg/L 0.250 ND 99.6 75-125 1.13 20 Post Spike (B000013-PS1) Source: MOB1971-01 Prepared &Analyzed: 03/02/2020 Arsenic 0.193 mg/L 0.200 0.000963 95.9 75-125 Barium 0.512 mg/L 0.500 0.0143 99.5 75-125 Cadmium 0.0247 mg/L 0.0250 0.000036( 98.7 75-125 Chromium 0.249 mg/L 0.250 0.000450 99.4 75-125 Lead 0.252 mg/L 0.250 0.00155 100 75-125 Selenium 0.189 mg/L 0.200 -0.000378 94.5 75-125 Silver 0.196 mg/L 0.200 -0.000288 98.2 75-125 Spike Source %REC RPD Volatile Organic Compounds Result RL Units Level Result %REC Limits RPD Limit Notes TCLP by GCMS Batch B000167 - 5030 8260 - EPA 8260E Blank (B000167-BLK1) Benzene 2-Butanone Carbon tetrachloride Chlorobenzene Chloroform 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogate: 4-Bromo tl uorobenzene Surrogate: Dibromolluoromethane Surrogate: 1, 2-Dichloroethane-d4 Surrogate: Toluene -dB LCS (B000167-BSI) Benzene 2-Butanone Carbon tetrachloride Chlorobenzene Chloroform Prepared & Analyzed: 03/04/2020 <5.00 5.00 ug/L <10.0 10.0 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <5.00 5.00 ug/L <10.0 10.0 ug/L 24.4 ug/L 25.0 97.6 86-115 23.7 ug/L 25.0 94.7 86-118 23.4 ug/L 25.0 93.6 80-120 24.5 ug/L 25.0 98.1 88-110 Prepared & Analyzed: 03/04/2020 20.6 5.00 ug/L 20.0 103 80-121 20.5 10.0 ug/L 20.0 103 10-170 18.5 5.00 ug/L 20.0 92.5 65-140 20.6 5.00 ug/L 20.0 103 80-120 18.8 5.00 ug/L 20.0 94.1 80-125 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 14 ?iMICR0RA!� Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Volatile Organic Compounds Result TCLP by GCMS Batch B000167 - 5030 8260 - EPA 8260B LCS (B000167-BSI) 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogate: 4-Bromofluorobenzene Surrogate: Dibromoiluoromethane Surrogate: 1, 2-Dichloroethane-d4 Surrogate: Toluene-d8 LCS Dup (B000167-BSD1) Benzene 2-Butanone Carbon tetrachloride Chlorobenzene Chloroform 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: 1, 2-Dichloroethane-d4 Surrogate: Toluene-d8 18.4 20.1 19.0 19.1 16.8 20.6 20.9 18.2 20.8 18.7 18.2 19.7 19.2 19.1 16.7 Herbicides TCLP by GC/ECD Result Batch B000069 - 8151 WATER - EPA 8151A Blank (B000069-BLK_I)) 2,4,5-TP (Silvex) [2C] <0.200 2,4-D [2C] <2.00 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Prepared & Analy_zed: 03/04/2020 _ �92.0 --- 5.00 ug/L 20.0 80-129 5.00 ug/L 20.0 100 80-132 5.00 ug/L 20.0 94.8 80-124 5.00 ug/L 20.0 95.6 80-122 10.0 ug/L 20.0 84.2 50-170 23.0 ug/L 25.0 92.1 86-115 23.8 ug/L 25.0 95.2 86-118 23.0 ug/L 25.0 91.8 80-120 24.2 ug/L 25.0 97.0 88-110 Prepared & Analyzed: 03/04/2020 5.00 ug/L 20.0 103 80-121 0.215 20 10.0 ug/L 20.0 104 10-170 1.58 20 5.00 ug/L 20.0 91.0 65-140 1.61 20 5.00 ug/L 20.0 104 80-120 1.11 20 5.00 ug/L 20.0 93.7 80-125 0.441 20 5.00 ug/L 20.0 91.2 80-129 0.825 20 5.00 ug/L 20.0 98.3 80-132 2.13 20 5.00 ug/L 20.0 96.0 80-124 1.23 20 5.00 ug/L 20.0 95.4 80-122 0.236 20 10.0 ug/L 20.0 83.6 50-170 0.711 20 23.9 ug/L 25.0 95.6 86-115 24.5 ug/L 25.0 98.2 86-118 23.9 ug/L 25.0 95.4 80-120 24.7 ug/L 25.0 99.0 88-110 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Prepared: 03/02/2020 Analyzed: 03/03/2020 0.200 ug/L 2.00 ug/L Surrogate: 2,4-Dichloropenylaceticacid [2C] 4.90 ug/L 5.00 98.1 20-144 LCS (B000069-BS1) _ Prepared: 03/02/202OAnalyze__d: 03/03/2020 2,4,5-TP (Silvex) [2C] 0.427 0.200 ug/L 0.500 85.4 25-120 2,4-D [2C] 4.34 2.00 ug/L 5.00 86.8 20-110 Surrogate: 2,4-Dichloropenylacetic acid (2C) 5.03 ug/L 5.00 101 20-144 LCS Dup (B000069-BSD1) Prepared: 03/02/2020 Analyzed: 03/03/2020 2,4,5-TP (Silvex) [2C] 0.354 0.200 ug/L 0.500 70.7 25-120 18.9 30 2,4-D [2C] 3.74 2.00 ug/L 5.00 74.8 20-110 14.8 30 Surrogate 2,4-Dichloropenylacetrc acid [2C] 4.19 ug/L 5.00 83.9 20-144 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 14 "0IVIWRO 3AC'- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source Pesticides TCLP by GC/ECU Result RL Units Level Result Batch B000027 - 351 OC 8081 -EPA 8081A %REC %REC Limits RPD RPD Limit Notes Blank (B000027-BLK1) Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane <0.0500 0.0500 ug/L Endrin <0.0500 0.0500 ug/L gamma Chlordane <0.0500 0.0500 ug/L gamma-BHC (Lindane) <0.0500 0.0500 ug/L Heptachlor <0.0500 0.0500 ug/L Heptachlor epoxide <0.0500 0.0500 ug/L Methoxychlor <0.0500 0.0500 ug/L Toxaphene <1.00 1.00 ug/L Surrogate:2,4,5,6-Tetrachloro-m-xylene 0.141 ug/L 0.200 70.4 20-130 Surrogate: Decachlorobiphenyl (BZ-209) 0.155 ug/L 0,200 77.4 25-140 LCS (B000027-BSI) Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane 0.536 0.0500 ug/L 0.500 107 40-120 Endrin 0.544 0.0500 ug/L 0.500 109 40-138 gamma Chlordane 0.543 0.0500 ug/L 0.500 109 40-136 gamma-BHC (Lindane) 0.559 0.0500 ug/L 0.500 112 30-134 Heptachlor 0.519 0.0500 ug/L 0.500 104 40-130 Heptachlor epoxide 0.473 0.0500 ug/L 0.500 94.7 40-120 Methoxychlor 0.558 0.0500 ug/L 0.500 112 40-150 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 0.153 ug/L 0.200 76.6 20-130 Surrogate. Decachlorobiphenyl (BZ-209) 0.154 ug/L 0.200 76.9 25-140 LCS (B000027-BS2) Prepared: 03/02/2020 Analyzed: 03/04/2020 Toxaphene 1.71 1.00 ug/L 2.00 85.3 41-126 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 0.147 ug/L 0.200 73.7 20-130 Surrogate: Decachlorobiphenyl (BZ-209) 0.147 ug/L 0.200 73.7 25-140 LCS Dup (B000027-BSD1) Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane 0.566 0.0500 ug/L 0.500 113 40-120 5.44 30 Endrin 0.563 0.0500 ug/L 0.500 113 40-138 3.40 30 gamma Chlordane 0.558 0.0500 ug/L 0.500 112 40-136 2.80 30 gamma-BHC (Lindane) 0.589 0.0500 ug/L 0.500 118 30-134 5.18 30 Heptachlor 0.543 0.0500 ug/L 0.500 109 40-130 4.63 30 Heptachlor epoxide 0.492 0.0500 ug/L 0.500 98.3 40-120 3.81 30 Methoxychlor 0.578 0.0500 ug/L 0.500 116 40-150 3.49 30 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 0.164 ug/L 0.200 82.1 20-130 Surrogate Decachlorobiphenyl (BZ-209) 0.158 ug/L 0.200 79.1 25-140 Matrix Spike (B000027-MS1) Source: MOB1987-01 Prepared: 03/02/2020 Analyzed: 03/04/2020 alpha -Chlordane 5.30 0.500 ug/L 5.00 ND 106 40-120 Endrin 5.54 0.500 ug/L 5.00 ND 111 40-138 gamma Chlordane 5.38 0.500 ug/L 5.00 ND 108 40-136 gamma-BHC (Lindane) 5.65 0.500 ug/L 5.00 ND 113 30-134 Heptachlor 4.70 0.500 ug/L 5.00 ND 93.9 40-130 Heptachlor epoxide 4.74 0.500 ug/L 5.00 ND 94.7 40-120 Methoxychlor 5.44 0.500 ug/L 5.00 ND 109 40-150 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 1.39 ug/L 2.00 69.3 20-130 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p ) www.microbac.com Page 10 of 14 t4 �)M1CROBAC�- Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC RPD Pesticides TCLP by GC/ECU Result RL Units Level Result %REC Limits RPD Limit Notes Batch B000027 - 3510C 8081 - EPA 8081A Matrix Spike (B000027-MS1) Source: MOB1987-01 Prepared: 03/02/2020 Analyzed: 03/04/2020 Surrogate: Decachlorobiphenyl (BZ-209) 0.849 ug/L 2.00 42.5 25-140 Semivolatiie Organic Result Compounds TCLP by GCMS Batch B000055 - 3510C 8270 - EPA 8270C Blank (B000055-BLK1) Pyridine <25.0 1,4-Dichlorobenzene <5.00 2-Methylphenol <5.00 3-,4-Methylphenol <5.00 Hexachloroethane <5.00 Nitrobenzene <5.00 Hexachlorobutadiene <5.00 2,4,6-Trichlorophenol <5.00 2,4,5-Trichlorophenol <5.00 2,4-Dinitrotoluene <5.00 Hexachlorobenzene <5.00 Pentachlorophenol <25.0 Surrogate, 2-Fluorophenol Surrogate, Phenol-d5 Surrogate: Nitrobenzene-d5 Surrogate: 2-Fluorobiphe n yl Surrogate: 2,4, 6-Tribromophenol Surrogate: p-Terphenyl-d 14 Blank (B000055-BLK2) Pyridine <25.0 1,4-Dichlorobenzene <5.00 2-Methylphenol <5.00 3-,4-Methylphenol <5.00 Hexachloroethane <5.00 Nitrobenzene <5.00 Hexachlorobutadiene <5.00 2,4,6-Trichlorophenol <5.00 2,4,5-Trichlorophenol <5.00 2,4-Dinitrotoluene <5.00 Hexachlorobenzene <5.00 Pentachlorophenol <25.0 Surrogate: 2-Fluorophenol Surrogate: Phenol-d5 Surrogate: Nitrobenzene-d5 Surrogate: 2-FI uo ro b i p h e n yl Surrogate: 2, 4, 6-Tribromophenol Surrogate. p-Terphenyl-d14 Spike Source %REC RPD RL Units Level Result %REC Limits RPD Limit Notes Prepared: 03/02/2020 Analyzed: 03/03/2020 25.0 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 25.0 ug/L 58.4 ug/L 100 58.4 19-119 36.8 ug/L 100 36.8 10-120 41.1 ug/L 50.0 82.3 35-114 44.1 ug/L 50.0 88.2 43-116 124 ug/L 100 124 22-142 53.5 ug/L 50.0 107 10-130 Prepared: 03/02/2020 Analyzed: 03/04/2020 25.0 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 5.00 ug/L 25.0 ug/L 58.4 ug/L 100 58.4 19-119 35.8 ug/L 100 35.8 10-120 41.5 ug/L 50.0 82.9 35-114 43.9 ug/L 50.0 87.9 43-116 128 ug/L 100 128 22-142 52.2 ug/L 50.0 104 10-130 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 11 of 14 7-)}MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Spike Source %REC Semivolatile Organic Result RL Units Level Result %REC Limits Compounds TCLP by GCMS Batch B000055 - 351 OC 8270 - EPA 8270C RPD RPD Limit Notes LCS (B000055-BS1) Prepared: 03/02/2020 Analyzed: 03/03/2020 Pyridine <25.0 25.0 ug/L 50.0 48.8 10-100 1,4-Dichlorobenzene 38.9 5.00 ug/L 50.0 77.7 29-112 2-Methylphenol 43.3 5.00 ug/L 50.0 86.5 30-120 3-,4-Methylphenol 40.4 5.00 ug/L 50.0 80.9 20-130 Hexachloroethane 38.1 5.00 ug/L 50.0 76.2 21-115 Nitrobenzene 46.1 5.00 ug/L 50.0 92.2 40-120 Hexachlorobutadiene 47.8 5.00 ug/L 50.0 95.5 22-124 2,4,6-Trichlorophenol 55.3 5.00 ug/L 50.0 111 50-135 2,4,5-Trichlorophenol 55.6 5.00 ug/L 50.0 111 53-123 2,4-Dinitrotoluene 58.4 5.00 ug/L 50.0 117 57-128 Hexachlorobenzene 57.9 5.00 ug/L 50.0 116 53-125 Pentachlorophenol 60.5 25.0 ug/L 50.0 121 35-138 Surrogate:2-Fluorophenol 57.5 ug/L 100 57.5 19-119 Surrogate. Phenol-d5 38.4 ug/L 100 38.4 10-120 Surrogate: Nitrobenzene-d5 41.8 ug/L 50.0 83.6 35-114 Surrogate:2-Fluorobiphenyl 44.1 ug/L 50.0 88.1 43-116 Surrogate. 2,4,6-Tribromophenol 129 ug/L 100 129 22-142 Surrogate: p-Terphenyl-d14 53.7 ug/L 50.0 107 10-130 LCS Dup (B000055-BSD1) Prepared: 03/02/2020Analyzed: 03/03/2020 Pyridine <25.0 25.0 ug/L 50.0 48.6 10-100 0.528 30 1,4-Dichlorobenzene 38.8 5.00 ug/L 50.0 77.6 29-112 0.125 30 2-Methylphenol 43.2 5.00 ug/L 50.0 86.5 30-120 0.0516 30 3-,4-Methylphenol 39.7 5.00 ug/L 50.0 79.5 20-130 1.70 30 Hexachloroethane 38.9 5.00 ug/L 50.0 77.9 21-115 2.16 30 Nitrobenzene 47.7 5.00 ug/L 50.0 95.5 40-120 3.54 30 Hexachlorobutadiene 47.6 5.00 ug/L 50.0 95.3 22-124 0.267 30 2,4,6-Trichlorophenol 56.6 5.00 ug/L 50.0 113 50-135 2.42 30 2,4,5-Trichlorophenol 55.1 5.00 ug/L 50.0 110 53-123 0.943 30 2,4-Dinitrotoluene 59.1 5.00 ug/L 50.0 118 57-128 1.24 30 Hexachlorobenzene 60.1 5.00 ug/L 50.0 120 53-125 3.71 30 Pentachlorophenol 62.8 25.0 ug/L 50.0 126 35-138 3.62 30 Surrogate:2-Fluorophenol 58.3 ug/L 100 58.3 19-119 Surrogate: Phenol-d5 38.9 ug/L 100 38.9 10-120 Surrogate: Nitrobenzene-d5 42.1 ug/L 50.0 84.2 35-114 Surrogate:2-Fluorobiphenyl 44.8 ug/L 50.0 89.6 43-116 Surrogate: 2,4,6-Tribromophenol 132 ug/L 100 132 22-142 Surrogate: p-Terphenyl-d14 54.2 ug/L 50.0 108 10-130 Microbac Laboratories. Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 12 of 14 lt�) M I(-R0BAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOB0372 Definitions % (by wt.): Percent by Weight 1-114: The test was performed outside of the EPA recommended holding time of 15 minutes. mg/kg: Milligrams per Kilogram mg/L: Milligrams per Liter mm/sec: Millimeter per Second 03: LCS recovery is below acceptance limits. The reported value is estimated. 04: ICV recovery is above acceptance limits. The reported value is estimated. R1: Duplicate RPD is outside of acceptance limits. RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units S1: Surrogate recovery is above acceptance limits. ug/L: Micrograms per Liter ug/mL: Micrograms per Milliliter Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 8.3IC Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and subject to Microbac's standard terms and conditions which can be located and Administration reviewed at<httos://www.microbac.com/standard•terms-conditions>. Reported: 03/06/2020 19:15 Microbac Laboratories. Inc 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 13 of 14 'K060372' Microbae-Fayetteville ,1 C&MICROBAC� 2592 Hope Milts Rd. CHAIN OF CUSTODY RECOR ION 111j I qqq �.I II1II 111111111111 E111��1 p! Fayetteville, NC 25305 Number I ,Y���IY 1 I Instruc0ons on back Lab Report Address Invoice Address Turnaround Time TO BE COMPLETED BYMICA Client Namc: 1i0401 n ]r Client Name: ❑ Routine (5 to 7 business days) Temp. Upon Receipt rC)E. 3 Therm 10 Address: Address: [] RUSH' (notify lab) Holding Time City, State, Zip: eke v4 City, Sate, Zip: (needed by) Samples Received on to s No N/A .. nt Coact: �..,� Contact: Report Type Custody Seals Intact? es o WA Telephone No.: _ Telephone No.: Results Only [ ] Level t [ ] Level 2 [ ] Level3 [ ] Level 4 [ - D .. -- _Send ReEoortvia: _[lam . I 1 Faz IXI.a-met_ _ Send Invoicavia_ _ _[_J Mail _.I I Fax_.I1 :mail Protect_ _ _ocation_ PO No.: _ Com I nee Mon[j Yesitoring? L ] No. j_j Agency/Propra'tt - ,Sampledby.(PRIND_v 4U4/L� Spmpier Signetur �— _Sampler Phane Np_ ' Matrix Types: Soil/Solid (S), Sludge, Oil, Wipe, Drinking Water (OW), eundvater(OW), Surlece Water (SW), Waste Water (WW), Other (specify) Praservallve Types _(1) HNO3, (22) H2SO4_(3)HCI, j4LNa0H_(5J Zte Acetate, (5) Methard, Cn Sodim Blsuifale, (0) Sodium Thiosuifate, (9) Hexane, (U) Unprescrved ClientSamplelD .�Emml FIAMIN111M JMMMMMIMM COME ■W■_._■■■■_■NO ON O�O�v■■■_■■■ MENNEN 0 IME __�■■■_■_■_■v■■■ �0_�■■■■_._■■■■■■■ -Possible Hazard Identificatio [] Hazardous [] Non -Hazardous [1 Radioactive Sam [j Dispose as approprlate• [] Return [] Archive Relin • e ture tJTI e R cet By (signature) atetrme z Lq-1'7 Q: S—o .� alasl2 >3� REVIEWED Rali caM. shed By (signature) Datame Received By (signature) Oate>Tme G\' Relinquished By (signature) Dato/Time Rouived By (signature) DateMme Paae 14 0[ 14 VMICROBAC r Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJ0203 Project Description Residuals Sample - 60 day For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Monday, November 23, 2020 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are reported on a 'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 12 {f'D � I C R O B A C" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO2O3 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: N/A 126 First Street Received: 10/12/2020 Cordova, NC 28330 Reported: 11/23/2020 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from Paper Plant, KOJ0203-01 Solid Grab 10/12/20 12:23 10/12/20 15:57 Grab Page 2 of 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Analytical Testing Parameters Client Sample ID: Residual from Paper Plant, Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOJO203-01 Collection Date: 10/12/2020 12 23 Inorganics Total Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Sodium Adsorption Ratio, SAR 0.330 NA 1 11/09/20 1943 BNS EPA 9045D pH at 25 °C 8.2 1.0 S.U. 1 H 11/03/20 1151 11/02/20 1527 TBM SM 4500-NH3 G-2011 Ammonia as N <4.50 4.50 mg/kg 1 y 11/02/20 1701 Jo SM 4500-P F-2011 Phosphorus, Total (as P) 3.5 0.59 mg/kg dry 1 10/22/20 0024 10/22/20 0044 JAW General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst Calculation Plant Available Nitrogen 582 mg/kg 1 11/06/20 1324 11/06/20 1324 BNS EPA 300.0, Rv. 2.1 (1993) Nitrate as N 0.685 0.0591 mg/kg dry 1 11/03120 1246 11/03/20 1251 JDW Nitrite as N <1.18 1.18 mg/kg dry 1 11/03/20 1246 11/03/20 1251 JDW SM 2540 G-2011 Solids 42.3 1,00 % 1 10/14/20 0954 TBM Analyses Subcontracted to: ECI General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst EPA 351.2, Rv. 2 (1993) Total Kjeldahl Nitrogen 1940 0.5 mg/kg 1 10/12/20 1223 11/05/20 0000 RP Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH General Parameters Result RL Units Dilution Note Prepared Analyzed Analyst ASTM D2216-10 Percent Solids 36.2 1.00 % (by wt.) 1 y 10/16/20 0719 10/19/20 0710 JMH Metals Total by AA Result RL Units Dilution Note Prepared Analyzed Analyst EPA 7471 A Mercury <0.658 0.658 mg/kg dry 1 10/19/20 0724 10/20120 1212 TMM Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Client Sample ID: Residual from Paper Plant. Grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KOJO203-01 Collection Date: 10/12/2020 12:23: Metals Total by ICP Result EPA 601 OB Aluminum 1360 Arsenic <1.89 Cadmium 0.199 Calcium 219000 Copper 32.0 Lead <1.89 Magnesium 2220 Molybdenum <5.67 Nickel <3.78 Phosphorus 142 Potassium <94.5 Selenium <1.89 Sodium 805 Zinc 74.3 RL Units Dilution Note Prepared Analyzed Analyst 37.8 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 1.89 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 0.189 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 9450 mg/kg dry 100 D3 11/05/20 0540 11/09/20 1203 KHL 1.89 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 1.89 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 47.2 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 5.67 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 3.78 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 94.5 mg/kg dry 1 Y 11/05/20 0540 11/09/20 1032 KHL 94.5 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 1.89 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 47.2 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL 1.89 mg/kg dry 1 11/05/20 0540 11/09/20 1032 KHL Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 12 MICR0B.AC'. Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Batch Log Summary Method Batch Laboratory ID Client I Source ID EPA 351.2, Rv. 2 (1993) (none] BATCH-BLK1 (Solid) BATCH-BS1 (Solid) BATCH-BS1 (Solid) BATCH-MS1 (Solid) BATCH-MS1 (Solid) KOJO203-01 KOJO203-01 BATCH-BLK1 (Solid) Residual from Paper Plant Grab Residual from Paper Plant, Grab Method Batch Laboratory ID Client I Source ID ASTM D2216-10 BOJO893 BOJO893-DUP1 KOJO203-01 BOJO893-BS1 BOJO893-BLK1 KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client I Source ID EPA 7471A BOJ1022 BOJ1022-BLK1 130J1022-13S1 B0J1022-BSD1 BOJ1022-MRL1 BOJ 1022-PS 1 MOJ0921-01 BOJ1022-PS2 MOJ0922-01 BOJ1022-PS4 MOJ0995-02 BOJ1022-PS5 MOJ1117-02 KOJO203-01 Residual from Paper Plant Grab BOJ1022-PS6 KOJO203-01 BOJ1022-PS7 MOJ1192-01 BOJ1022-PS8 MOJ1282-04 BOJ1022-PSA MOJ1364-01 BOJ1022-PS9 MOJ1307-01 BOJ1022-PSB MOJ1117-01 BOJ1022-SRL1 MOJ1307-01 Method Batch Laboratory ID Client I Source ID EPA 601 OB BOK0235 BOK0235-MRL1 BOK0235-BLK1 BOK0235-BS1 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab BOK0235-PS1 KOJO203-01 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 12 t ;t (`I I C R O B A ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 EPA 601 OB BOK0235 BOK0235-SRL1 KOJO203-01 BOK0235-MS1 MOK0141-20 BOK0235-MSD1 MOK0141-20 KOJO203-01 RE 1 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID SM 2540 G-2011 KJO1306 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab KJO1306-DUP1 KOJO203-01 KJO1306-BLK1 KJO1306-BLK1 KJO1306-DUP1 KOJO203-01 Method Batch Laboratory ID Client / Source ID EPA300.0, Rv. 2.1 (1993) KJO1410 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID SM 4500-P F-2011 KJ02103 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID EPA 9045D KKO0309 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID SM 4500-NH3 G-2011 KKO0310 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID Calculation KKO0528 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Method Batch Laboratory ID Client / Source ID Calculation KKO0906 KOJO203-01 Residual from Paper Plant, Grab KOJO203-01 Residual from Paper Plant, Grab Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch KJ01306 - Wet Chem Solid - SM 2540 G-2011 Blank (KJO1306-BLK1) Prepared &Analyzed: 10/14/2020 % Solids <1.00 1.00 % Duplicate (KJO1306-DUP1) Source: KOJO203-01 Prepared &Analyzed: 10/14/2020 % Solids 41.9 1.00 % 42.3 1 10 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 0 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch Quality Control Summary: Microbac Laboratories Inc., - Marietta, OH Spike Source %REC RPD General Parameters Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOJO893 - Wet-Solids-S -ASTM D2216-10 Blank (BOJO893-BLK1) Percent Solids LCS (BOJ0893-BSI) Percent Solids Duplicate (BOJO893-DUP1) Percent Solids Metals Total by AA Batch BOJ1022 - 7471 - EPA 7471A 100 80.2 1.00 Source: KOJO203-01 36.2 1.00 Prepared: 10/16/2020 Analyzed: 10119/2020 (by wt.) Prepared: 10/16/2020 Analyzed: 10/19/2020 % (by 80.0 100 90-110 wt.) Prepared: 10/1612020 Analyzed: 10/19/2020 % (by 36.2 0.145 20 wt.) Spike Source %REC RPD Result RL Units Level Result %REC Limits RPD Limit Notes Blank (BOJ1022-BLK1) Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury <0.250 0.250 mg/kg wet LCS (BOJ1022-BS1) Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 0.315 0.250 mg/kg 0.267 118 80-120 wet LCS Dup (BOJ1022-BSD1) Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 0.314 0.250 mg/kg 0.267 118 80-120 0.318 wet Post Spike (BOJ1022-PSI) Source: MOJ0921-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 2.98 ug/L 1.00 1.77 121 80-120 Post Spike (BOJ1022-PS2) Source: MOJ0922-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.50 ug/L 1.00 0.318 119 80-120 Post Spike (BOJ I 022-PS4) Source: MOJ0995-02 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 4.68 ug/L 1.00 3.33 136 80-120 Post Spike (BOJ1022-PS5) Source: MOJ1117-02 Prepared. 10/19/2020 Analyzed: 10/20/2020 Mercury 1.52 ug/L 1.00 0.252 127 80-120 Post Spike (BOJ1022-PS6) Source: KOJO203-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.05 ug/L 1.00-0.0221 105 80-120 Post Spike (BOJ1022-PS7) Source: MOJ1192-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 0.752 ug/L 1.00 -0.133 75.2 80-120 Post Spike (BOJ 1 022-PS8) Source: MOJ1282-04 Prepared: 10/19/2020 Analyzed: 10/2012020 Mercury 3.06 ug/L 1.00 1.66 140 80-120 Post Spike (BOJ1022-PS9) Source: MOJ1307-01 Prepared: 10/19/2020 Analyzed: 10/21/2020 Microbac Laboratories, Inc. 20 M5 M5 M5 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 7 of 12 ��'iM1CROsAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD Metals Total by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOJ1022 - 7471 -EPA 7471A Post Spike (BOJ1022-PS9) Source: MOJ1307-01 Prepared: 10/19/2020 Analyzed: 10/21/2020 Mercury 6.93 ug/L 1.00 3.92 301 80-120 M5 Post Spike (130J1022-PSA) Source: MOJ1364-01 Prepared: 10/19/2020 Analyzed: 10/20/2020 Mercury 1.19 ug/L 1.00 0.338 85.5 80-120 Post Spike (BOJ1022-PSB) Source: MOJ1117-01 Prepared: 10/19/2020 Analyzed: 10/21/2020 Mercury 5.04 ug/L 1.00 4.10 93.9 80-120 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOK0235 - 3051 A6010 -EPA 6010E Blank (BOK0235-BLK1) Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum <20.0 20.0 mg/kg wet Arsenic <1.00 1.00 mg/kg wet Cadmium <0.100 0.100 mg/kg wet Calcium <50.0 50.0 mg/kg wet Copper 0.00 1.00 mg/kg wet Lead 0.00 1.00 mg/kg wet Magnesium <25.0 25.0 mg/kg wet Molybdenum <3.00 3.00 mg/kg wet Nickel <2.00 2.00 mg/kg wet Phosphorus <50.0 50.0 mg/kg wet Potassium <50.0 50.0 mg/kg wet Selenium 0.00 1.00 mg/kg wet Sodium <25.0 25.0 mg/kg wet Zinc <1.00 1.00 mg/kg wet LCS (BOK0235-BS1) Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum 238 20.0 mg/kg 250 95.2 80-120 wet Arsenic 9.05 1.00 mg/kg 10.0 905 80-120 wet Calcium 255 50.0 mg/kg 250 102 80-120 wet Copper 12.3 1.00 mg/kg 12.5 98.3 80-120 wet Microbac Laboratories. Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 12 .'MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOK0235 - 3051A 6010 - EPA 6010E LCS (BOK0235-BS1) Prepared: 11/05/2020 Analyzed: 11/09/2020 Lead 12.4 1.00 mg/kg 12.5 98.9 80-120 wet Magnesium 260 25.0 mg/kg 250 104 80-120 wet Molybdenum 26.1 3.00 mg/kg 25.0 105 80-120 wet Nickel 12.4 2.00 mg/kg 12.5 99.2 80-120 wet Phosphorus 234 50.0 mg/kg 250 93.7 80-120 wet Potassium 1270 50.0 mg/kg 1250 101 80-120 wet Selenium 9.27 1.00 mg/kg 10.0 92.7 80-120 wet Sodium 1270 25.0 mg/kg 1250 101 80-120 wet Zinc 24.2 1.00 mg/kg 25.0 96.9 80-120 wet Matrix Spike (BOK0235-MS1) Source: MOK0141-20 Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum 11600 18.6 mg/kg 233 11100 196 75-125 dry Arsenic 11.3 0.932 mg/kg 9.32 3.58 83.3 75-125 dry Calcium 1870 46.6 mg/kg 233 1100 330 75-125 dry Copper 20.5 0.932 mg/kg 11.6 10.3 88.2 75-125 dry Lead 21.8 0.932 mg/kg 11.6 13.3 72.4 75-125 dry Magnesium 696 23.3 mg/kg 233 405 125 75-125 dry Molybdenum 23.7 2.79 mg/kg 23.3 ND 102 75-125 dry Nickel 14.8 1.86 mg/kg 11.6 1.63 114 75-125 dry Phosphorus 462 46.6 mg/kg 233 249 91.6 75-125 dry Potassium 1500 46.6 mg/kg 1160 330 101 75-125 dry Selenium 10.7 0.932 mg/kg 9.32 5.30 58.4 75-125 dry Sodium 1140 23.3 mg/kg 1160 ND 97.9 75-125 dry Zinc 43.4 0.932 mg/kg 23.3 13.3 129 75-125 dry Matrix Spike Dup (BOK0235-MSD1) Source: MOK0141-20 Prepared: 11/05/2020 Analyzed: 11/09/2020 Aluminum 12200 19.8 mg/kg 247 11100 437 75-125 5.23 20 dry Arsenic 11.3 0.989 mg/kg 9.89 3.58 78.2 75-125 0.233 20 dry Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com I Page 9 of 12 Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Spike Source %REC RPD Metals Total by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch BOK0235 - 3051A 6010 - EPA 6010E Matrix Spike Dup (BOK0235-MSD1) Source: MOK0141-20 Prepared: 11/05/2020 Analyzed: 11/09/2020 Cadmium 1.26 0.0989 mg/kg 1.24 102 75-125 200 20 dry Calcium 1480 49.4 mg/kg 247 1100 153 75-125 23.3 20 dry Copper 18.6 0.989 mg/kg 12.4 10.3 67.7 75-125 9.70 20 dry Lead 21.3 0.989 mg/kg 12.4 13.3 64.2 75-125 2.34 20 dry Magnesium 767 24.7 mg/kg 247 405 147 75-125 9.69 20 dry Molybdenum 24.6 2.97 mg/kg 24.7 ND 99.4 75-125 3.46 20 dry Nickel 14.5 1.98 mg/kg 12.4 1.63 104 75-125 2.13 20 dry Phosphorus 435 49.4 mg/kg 247 249 75.5 75-125 5.93 20 dry Potassium 1600 49.4 mg/kg 1240 330 102 75-125 6.00 20 dry Selenium 10.6 0.989 mg/kg 9.89 5.30 53.3 75-125 1.62 20 dry Sodium 1190 24.7 mg/kg 1240 ND 96.4 75-125 4.45 20 dry Zinc 39.6 0.989 mg/kg 24.7 13.3 106 75-125 9.24 20 dry Post Spike (BOK0235-PS1) Source: KOJO203-01 Prepared: 11/05/2020Analyzed: 11/09/2020 Aluminum 17.9 mg/L 5.00 12.9 99.6 80-120 Arsenic 0.199 mg/L 0.200 0.00154 99.0 80-120 Cadmium 0.0262 mg/L 0.0250 0.00190 97.0 80-120 Copper 0.545 mg/L 0.250 0.305 96.1 80-120 Lead 0.245 mg/L 0.250 0.00846 94.5 80-120 Magnesium 26.0 mg/L 5.00 21.2 96.3 80-120 Molybdenum 0.560 mg/L 0.500 0.0454 103 80-120 Nickel 0.242 mg/L 0.250 0.0109 92.5 80-120 Phosphorus 6.32 mg/L 5.00 1.35 99.3 80-120 Potassium 26.4 mg/L 25.0 0.529 104 80-120 Selenium 0.198 mg/L 0.200 0.000117 99.1 80-120 Sodium 33.1 mg/L 25.0 7.67 102 80-120 Zinc 1.18 mg/L 0.500 0.707 93.7 80-120 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 10 of 12 LI1MICROBAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KOJO203 Definitions %: Percent % (by wt.): Percent by Weight D3: Dilution was performed due to high target analyte concentration. H: Analyte was prepared and/or analyzed outside of the analytical method holding time M5: Post digestion spike is outside of acceptance limits. MDL: Minimum Detection Limit mg/kg: Milligrams per Kilogram NA: Not Applicable RL: Reporting Limit RPD: Relative Percent Difference S.U.: Standard Units Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp- 7.3°C Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody (COC) Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC (Name, Date & Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace, or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc., - Marietta, OH 583 NC Dept. of the Environment and Natural Resources Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included. The services were provided under and Administration subject to Microbac's standard terms and conditions which can be located and reviewed at <httos:/Avww.microbac.com/standard-terms-conditions>. Reported: 11I23I2020 08:20 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 11 of 12 -KOJO203` Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 (910) 864-1920 / 864-8774 fE CHAIN OF CUSTODY RECORD PAGE 1 OF 1 CLIENTNAME a ADDRESS: VonDrehle Corp. 126 First Street Cordova, NC 28330 Por PROJECT I LOCATION: Cordova - 60-day Series NOF B o T T L E S TYPE OF ANALYSIS PRESERVATION CODE E N U E C E Q = E u W U a Q �, rL o(D U E V > !n c m J > N CO C a° - s' Z (� _ O c N E a fn ¢ p o Z m Z Z a IL F Z H n 01 Cn g o CODE: A = None B = HNO3 (pH<2) + <4°C C = H2SO4 (pH<2) + <4°C D=NaOH+c4°C E= zN Acetate + <4°C F= HG CONTACT PERSON. Mr. Chris Fowler PHONE: 910-410-9131 SAMPLER. �1,fk�o (/r;stil DATE I METHOD OF SHIPMENT: Microbac LAB ID R SAMPLE TYPE DATE TIME COMP GRAB pH D.C. TEMP •C CH ORINE Residual from paper plant 1 O�r t Z° 11,13 X 2 A A A A A A A A A I J 1 A A A A I A A A A I A Relin uls Oare Time Re s (Signature) ogle Time Relinquished br )ate Time Received by: (Signature) Due Time 3 4 Relinquished by Dare Time Re -Ned by. (Signature) Cate Time 5 6 Camm is or SDecal Hazards: l5 `5� REVIIEE\WED ^X W Page 12 of 12 inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, /NC. December 01, 2020 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7 BCS ID: 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC alysis _ Method monella JEPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES llama=:�1RA' Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-1 Sample Date/Time: November 23, 2020 13:48 BCS Sample ID: 2011362 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 36.1 Amount Analyzed: 30.02 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11AS Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-2 Sample Date/Time: November 23, 2020 13:50 BCS Sample ID: 2011363 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 40.0 Amount Analyzed: 29.96 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES PC-r-%F, ilaC-WA A1`16 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-3 Sample Date/Time: November 23, 2020 13:52 BCS Sample ID: 2011364 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 41.0 Amount Analyzed: 30.00 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-4 Sample Date/Time: November 23, 2020 13:54 BCS Sample ID: 2011365 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 46.5 Amount Analyzed: 29.96 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ►"ft' :lac=eAAAB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-5 Sample Date/Time: November 23, 2020 13:56 BCS Sample ID: 2011366 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 42.5 Amount Analyzed: 29.92 g Analysis Start: November 24, 2020 11:45 Analyst: Robert Pimentel Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Stop Date: December 01, 2020 9:15 Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-6 Sample Date/Time: November 23, 2020 13:58 BCS Sample ID: 2011367 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 41.2 Amount Analyzed: 30.08 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-7 Sample Date/Time: November 23, 2020 14:00 BCS Sample ID: 2011368 Sample Description: Biosolid Date Received: November 24, 2020 10:14 Amount Submitted:100 mL bottle % Solids: 41.0 Amount Analyzed: 30.00 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: November 24, 2020 11:45 Analysis Stop Date: December 01, 2020 9:15 Analyst: Robert Pimentel Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Mom Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Via'` . . I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: December 01, 2020 Page 7 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011369 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification ordelayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2011362, 2011363, 2011364, 2011365, 2011366, 2011367, 2011368 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES F' ilac-MRA AP6 K CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A inc FL DOH Laboratory #E82924, EPA# FLO1147 Gainesville, FL 32609 4a S %fit Tel. (352) 377-9272, Fax. (352) 377-5630 Client Name and Address: K PI (J 7 � iC 3. 2`j I Compliance Monitoring? CYes❑ No City/Slate/Zip: 202 Project ID: Z L)tq —I1 Project Manager: 9'), Facility/Site: 1--44-v,, lyL Telephone Number: 336 'i2 �Ct'} Fax No.: Report To: -till� Sampler Name: (Print) Email: j,l f��i L�• �t�A ���.:—' Sampler Signature: L, {� Invoice To: yd c Branch Residuals and Soils Matrix Analysis VD-6 w 2011367 v ro 2 > 0 U 111241202010:14 n o _ Branch Residuals and Soils L 12 N $ m y m v C w C, °e ``(` N d E X 0 a' aU a d VD-7 2011368 a a v n c E V .. u= q �� u c o a o �a m U U 0 c 11/24l202010:14 m� rn m = u °i °v v o t N o, c 3 3 n �. '0 5 m `o ii m E L2 .� m m m o a g t i Q $ c v_ o U ii m m c U ._ o " U c c .4 o d D ry u! m= L ~ Sample ID ! Description z° cs _ c F g u, °� z o ' rn S ° o L 0 ° r U U. x rn o ui a cO1 o c w H a a n� > w z o o: ` ( ! � � 1~3. 1 .._{{ { �• Branch Residuals and Soils V-P 7 (, 13. S V C fl 1 !� VD-1 4 13. d / 2011362 111241202010:14 L{ 1 j'j'� .� i % Branch Residuals and Sods T 111363 �: s X, ;,1, }` 11124/202D 10:14 Branch Residuals and Sods T VD-3 Branch Residuals and Soils Branch Residuals and Sods 2011364 VD4 VD-5 1 V24,2o20 10-14 T— 2011365 2011366 I . Special Instructions: 11!241202010.14 11124i202010:14 -aboratory Comments: Y� Method of Shipment: U P,5/Poslal FEDEX Other Temp. @ recp't t ' ` •C Relinquished byy:' Dale Time Received by:` —�� Dale Time IR- ! Y Corrected for R 1, - r CustodySeai: Intact Broken WA Presence of visable Ice Y N Relinquished by: Dale Time Received by BCS Laboratories: Date Tme Presence of Ice papks N 11%'t/! I HoldTime// SECTION III MANAGEMENT PLAN von Drehle Corporation produces Fiber Clay from its Cordova, North Carolina facility as a bi-product of paper towel production using recycled paper. These residual solids are produced by non -biological processes that separate clay non -suitable fibers out during the production processes. Plastics are also separated and are sent to the land fill and are not to be considered as part of this Class A permit application. These residuals have no domestic contribution. Based on the pathogen testing and the no -biological nature of the treatment process, vector attraction reduction testing is not required. von Drehle wishes to distribute their Fiber Clay in the following ways: • Use as a landfill daily cover, • Admixture for composts, soil amendments, and potting soils, and • As a replacement for commercial lime (or most limiting application factor) on nonspecific agricultural receiver sites. For direct application, von Drehle Corporation or it's assigned representative will identify local landowners and/or other property as receiver sites. Application made to all sites will be based on the ability of the crop and the land to properly assimilate the residual solids. Application thickness of the application rate, percent solids of the residuals applied, the type, whether the field can or will be incorporated, thickness of the vegetative cover, and the lime requirement of the soil will be predominant application factors. The nitrogen needs of the crop will be secondary since it is expected that additional nitrogen will need to be applied to correct the carbon -nitrogen ratio to all the proper growth of the crop. von Drehle, plans to take all of these into account to be conservative and will distribute these residuals based on the most restrictive of these application rates. For uses of these residuals in other processes other than direct application, von Drehle makes no claim for their consistency or properties. Use by other entities will be without their responsibility to determine and accept as is, with no liability or other implication to von Drehle Corporation. Overview of Process and Residual Solids Handling Overview of Process and Residual Solids Handling von Drehle Corporation Cordova facility is located at 126 First Street in Richmond County, North Carolina. This facility produces, approximately 22,500 dry tons of Fiber Clay annually through separation and fractionation processes from their feed stock recycled paper. The processes remove all plastics which are sent to the landfill. The majority of the recycled paper is repulped for von Drehle's paper making process. The clay and short fibers that are separated out in the various screening and fractionation processes are run through a belt press and Fiber Clay is made. Fiber Clay is a product of non -biological processes and has no domestic contribution. Fiber Clay can be placed in sealed trucks have three potential types of destinations: • To a landfill for use as daily cover, • To an offsite blending operation for the inclusion in composts, soil amendments, and potting soils or • As a replacement for commercial lime (or most limiting application factor) on nonspecific agricultural receiver sites. Distribution Methods for Reuse Distribution Methods for Reuse The Fiber Clay may be distributed in the following manner: • Use as a landfill daily cover, • Admixture for composts, soil amendments, and potting soils, and • As a replacement for commercial lime on nonspecific agricultural receiver sites. For direct application to nonspecific receiver sites, von Drehle Corporation or its assigned representative will identify local landowners and/or other property as receiver sites. Application made to all sites will be based on the ability of the crop and the land to properly assimilate the residual solids. Application thickness of the application rate, percent solids of the residuals applied, and the type and thickness of the vegetative cover will be the determining factors. These materials have very little nitrogen value so application will be based on: • application thickness or • lime needs of the soil. whichever of these accounts for the most restrictive application rate. Application thickness of the application rate, percent solids of the residuals applied, the type, whether the field can or will be incorporated, thickness of the vegetative cover, and the lime requirement of the soil will be predominant application factors. The nitrogen needs of the crop will be secondary since it is expected that additional nitrogen (above what is required for crop growth) will need to be applied to correct the carbon -nitrogen ratio to all the proper growth of the crop. von Drehle, plans to take all of these into account to be conservative and will distribute these residuals based on the most restrictive of these application rates. For other distribution points regarding the use of this residual in other processes or as admixtures, von Drehle makes no claim for their consistency or properties. Use by other entities will be without their responsibility to determine and accept as is with no implication to von Drehle. Transportation and Logistics Transportation and Logistics von Drehle Corporation Fiber Clay will be loaded into sealed sludge trailers. These trailers will be routed to various points for distribution, land application to nonspecific receiver sites, or sent a landfill as daily cover. Trucks will travel on major traffic routes to the application and or distribution sites. Individuals, agencies, or companies wishing to receive either of the von Drehle Fiber Clay will be issued a product information sheet, the most recent copy of the analytical information, and Product Receipt Form. The product information sheet will specify the buffer requirements for von Drehle's Fiber Clay as well as application restrictions. Each Product Receipt Form will document: • Amount of Fiber Clay received, • The name, address and telephone number of the person who prepared the Fiber Clay, • The name, address and telephone number of the person distributing/land applying the residuals, • A description of the processes that generated the residuals, • A summary of the results from the most recent residuals sampling event, • A summary of the type and volume of residuals distributed/land applied per acre, • A summary of the nutrients land applied per acre, and • A list of recommendations to the recipient of the residual regarding field use, soil testing, pH adjustment, and other relevant agronomic information. Both the Product Label and the Product Receipt Form will be required to ensure receipt of this information and for the removal volume. Copies of this information will be retained by the von Drehle Cordova and will be available for review upon request The distribution receiver, the land applier, and the site receiver will be instructed as to the proper use of this material as listed below: • Applications should be made in accordance with approved application standards. • Application shall not be made to land that is flooded, frozen, or snow covered. • Application and storage must be performed to prevent runoff from the application or storage site to any surface water. • Buffer or "no application" zones as described in the approved permit and Product Information Sheet. • Applications must not be applied so thick as to cover existing vegetation. Additional nitrogen may need to be applied to offset nitrogen deficient symptoms due to improper carbon to nitrogen ratio. Monitoring and Recordkeeping Monitoring and Recordkeeping The von Drehle Corporation Cordova facility requests that the Fiber Clay (Fiber Clay) be monitored monthly for residuals analysis based on the amount of these residuals expected to be distributed. A set of seven (7) Salmonella analyses will be performed prior to the end of the preceding month. A TCLP analysis will be performed annually. Fiber Clay samples will be collected and delivered to a laboratory qualified to analyze residual solids and that is familiar with routine environmental sample preparation and standards. Records pertinent to the successful management of the land applications program will be maintained for the benefit of the farm operator, DWR, land applicator, and permittee. These records will contain at a minimum: • Source of the residuals, • Type of the residuals, • Date of the residual application/ distribution receiver, • Information regarding the location of the residual application / distribution receiver ( i.e. field owner name, address, and telephone number, approximate field location, and field number) • Method of application / intended distribution, • Weather conditions (if applicable), • Soil conditions (if applicable), • Type of crop or crops to be grown on the field or type of distribution receiver and intended use, • Volume or weight of residuals applied to the field or provided to distribution receiver, • Annual totals of dry tons per acre of residuals, annual pounds of plant available nitrogen, and annual pounds of phosphorus applied to the field or annual total of dry tons given to distribution receiver if distributed as a non -land application alternative. Each year an annual summary of the activities of the program will be prepared and delivered to the appropriate agencies and participants on or before the 1 st of March. The Fiber Clay annual summary will include: A) Summary of the Fiber Clay, B) Volume/Weight of the distributed amount of Fiber Clay, C) Name of the receiver of the distributed Fiber Clay, D) Intended use(s) of the Fiber Clay, E) Volume/Weight of other Amendments or Bulking Agents, F) Annual totals of dry tons/acre of the Fiber Clay, G) pounds of plant available nitrogen (PAN), phosphorus, and lime applied from the Fiber Clay, if distributed to non-specific receiver sites and H) pounds of nitrogen needed to offset organic carbon applied through Fiber Clay. 2. Monthly - nutrients and metals will be analyzed of. Aluminum, Ammonia, Arsenic, Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel, Nitrate -Nitrite, Zinc, % Total Solids, CCE, pH, Phosphorus, Potassium, TKN, Selenium, and Sodium will be collected and analyzed by a qualified laboratory. From this information, the Plant Available Nitrogen (PAN) will be calculated. If land application occurs at a frequency of less than monthly, nutrient and metal analyses will be required for each distribution event. 3. Once a permit cycle a Toxicity Characteristics Leaching Procedure (TCLP) analysis with ignitability, reactivity, and corrosivity of the von Drehle Fiber Clay will be collected and analyzed by a qualified laboratory. Leachate Collection Leachate Collection No provision is made for leachate collection since the residuals are not designed to undergo any mixing with other productions on -site. The storage pad at the facility is sloped to the back to the drainage feature. Below the drainage feature is a screen to capture any solids that are washed to the drain. Once these residuals have been transported to the potential application sites or for other uses, the fiber clay can be stockpiled in a covered facility or covered on the ground similar to other Class A products. Once covered this material will remain covered until the time of application. SECTION IV VON DRHLE CORDOVA FIBER CLAY LABEL AND PRODUCT INFORMATION SHEET The von Drehle Corporation Cordova Fiber Clay Label Produced By Preparer von Drehle Corporation Chris Fowler (910) 410-1313 Wastewater Treatment Plant 126 First Street Cordova, North Carolina 28330 Cordova, North Carolina 28330 For information on this product contact von Drehle Corporation Cordova, NC facility at (910) 410-9131 Fiber Clay from the von Drehle Corporation Cordova NC are the clay and short fibers excluded from the repulping process of recycled paper production. The generated residuals have no domestic source percentage and are an exceptional quality residual solid that is permitted for bulk distribution. Approved used for von Drehle Fiber Clay: • Amendment for creation of soil mixture to be further distributed to the public, • Amendment for compost to be further distributed to the public, • Use as a daily landfill cover, • Application to potential receiver sites for use as a soil amendment or replacement for agricultural lime. Provisions for application are listed below. Provisions for Application Application of von Drehle Fiber Clay are prohibited except in accordance with the provisions specified in the Application Information Sheet. Application must conform to standards identified in Permit No. WQ0039924 and include but are not limited to: Maximum slope for the land application of these residuals is 10 % for surface applications and 18% for subsurface applications Distance Buffer Items (feet) Public or private water supply source, waters classified as SA or SB, and any Class I or Class 11 impounded reservoir used as a source of drinking water for both surface and subsurface methods 100 Surface waters (intermittent streams, perennial streams, perennial surface water bodies and wetlands) 100 Surface water diversions (ephemeral streams, ditches, groundwater lowering ditches, or waterways) 0 Application can not occur to: • adversely affect a threatened or endangered species or it's critical habitat, • within the 100-year flood plain unless solids are incorporated within a 24-hour period, • cause prolonged nuisance conditions, • create conditions where runoff will occur, • within the 100-year flood plain unless solids are incorporated within a 24-hour period, or • during a measurable rainfall event or 24-hours following a 0.5 inch cumulative rainfall event (over 24-hours). Application Information Sheet von Drehle Fiber Clay 1. von Drehle Fiber Clay shall not be applied to flooded, frozen, or snow-covered areas. 2. Application and storage of von Drehle Fiber Clay must be conducted in such a way as to prevent runoff or erosion from the application or storage site to any surface water. 3. Applications of von Drehle Fiber Clay must not be applied so thick as to cover existing vegetation. Application that is made to sites with less than 50 percent ground cover should be incorporated unless incorporation will result in violation of other federal program. 4. Applications of von Drehle Fiber Clay shall be applied uniformly at a rate equal to amount that can be adequately assimilated into the soil through incorporation, will not smother any current living crop on the surface of the soil if material will not be incorporated, or the agronomic rate of the crop as specified by the permit and the most recent residual analysis, or the lime requirement of the soil and most recent residuals analysis; whichever is most limiting. 5. An acceptable soil pH (greater than 6.0) see appropriate state extension service for crop specific optimal soil pH on individual receiver sites. The soil pH should be verified annually with a soil sample with recommendations. These recommendations should be followed as they relate to optimal crop growth, monitoring and adjustment of the exchangeable sodium percentage, potential for calcium and magnesium deficiency, as well as other relevant agronomic information. Additional fertilizer, lime, or other nutrients may need to be added as directed by the soil sample results. 6. Applications and loading rates of von Drehle Fiber Clay shall be applied at rates that comply with realistic yield expectations based on the soil series and crops found at: http://nutrients.soil.ncsu.edu/yields/ von Drehle Corporation Cordova Fiber Clay Approximately Contain: 42.30 Percent Solids 1.55 Plant Available Nitrogen surface land applied) pounds per dry ton 1.56 Plant Available Nitrogen (incorporated or injected pounds per dry ton 0.02 Phosphate 205pounds per dry ton 0..4 Potash K2Opounds per dry ton 802 Liming agent pounds per dry ton 8.2 pH of Fiber Clay See von Drehle Corporation Cordova WWTP for a copy of the most recent residuals analysis and loading rates. SECTION V WON DREHLE FIBER CLAY RECEIPT FORM VON DREHLE CORPORATION CORDOVA FIBER CLAY RECEIPT FORM I , (printed name) have received wet tons of von Drehle Corporation Cordova Fiber Clay, a von Drehle Fiber Clay product label, and a copy of the most recent analysis of the product. I have read these documents and agree to adhere to the directions specified on the Application Information Sheet and the Product Label. My intended use of this product is Contact Information: Name Address City, State, Zipcode Phone Number Email Address Signature of Receiver Date of Receipt SECTION VI SPILL CONTROL PLAN SPILL CONTROL PLAN VON DREHLE CORPORATION CORDOVA FIBER CLAY CORDOVA, NORTH CAROLINA In the case of a spill, the following actions shall be taken immediately: Halt the source of the spill: Damaged truck or trailer tank unit. 2. Contain spill: Use straw bales to form a barrier. Straw hay bales can be obtained from several sources for this purpose. Soil near the site can also be used to form a barrier for containment. 3. Clean up: Use residual solids application equipment to recover as much of the material as possible. After the application equipment has recovered as much material as possible, it will be land applied as per operation plan. 4. Final Clean up: Any unrecoverable material will be scraped and swept from the road surface and incorporated into an adjacent tillable area. 5. Notification: As soon as possible after a spill occurs notify: A. von Drehle Corporation - (910) 410-9131 B. Department of Environment and Natural Resources Fayetteville Regional Office at (910) 433-3300 or appropriate regional office C. The appropriate County Sheriffs Department D. Fire Department if assistance is required for washdown 6. Management of clean-up efforts: The ORC or applicator shall take immediate charge of the clean-up activities. Additional labor will be requested from the treatment plant and other departments as needed. 7. Reporting: Within 5 days of notifications, a written report will be prepared detailing the cause of the spill, all actions taken in response to the spill, and proposed actions to be taken to ensure spill does not recur.. APPLICATION RATES APPLICATION RATES Prior to a distribution event, a private land owner will contact von Drehle Corporation Cordova to initiate an application. This land owner will indicate the type of crop to be grown and the size of the field to have the residuals distributed. A recent soil sample will be needed to determine lime requirements. A recent sample of Fiber Clay generated from von Drehle Corporation Cordova will be used to calculate the application rates for the crop based on the soil liming needs and the crop and soil assimilation characteristics. Prior to the distribution event, the potential receiver sites will be reviewed to insure the crop has been identified correctly and the field size is correct. Soils data will be checked at that time. Application rates will be determined based on the solids content of the residuals, the height of the crop on the receiver site, smothering potential of the crop, the lime requirement of the soil, lime requirements of the soils analysis, and nitrogen needs of the crop to be grown. Application rates will be limited based on either: application thickness, lime needs of the soil, or nitrogen needs of the crop; whichever of the three accounts for the most restrictive application rate. Based on my knowledge of potential receiver sites, application thickness should be no more than 10 wet tons per acre if it is to be spread on the surface of the soil with an actively growing crop, depending on the percent solids of the residuals. The incorporated amount will be reduced if the incorporation equipment fail to properly turn the residual under depending on slope, cover, soil assimilation. Application should not occur at a rate that the residuals may experience runoff or erosion from the receiver site. Re -application of sites will be based on these same factors. If there are questions concerning an individual application rate for a receiver site, consult a licensed soil scientist. Application of Fiber Clay has been shown to create an imbalance in the soil carbon to nitrogen ratio. This is particularly important as it relates to specific time periods in a crop's growth cycle. It may be necessary to apply additional nitrogen to achieve the crop results. The application rates listed below outline the lime -added values from the following applications. At this point application rates should be limited to lime needs of the soil. Wet Tons/ Acre Dry Tons/ Acre PAN #/Acre Lime Tons/Acre 1 0.42 0.66 0.17 2 0.85 1.31 0.34 3 1.27 1.97 0.51 4 1.69 2.63 0.68 5 2.12 3.29 0.85 6 2.54 3.94 1.02 7 2.96 4.60 1.19 8 3.38 5.26 1.36 9 3.81 5.92 1.53 10 4.23 6.57 1.70 11 4.65 7.23 1.87 12 5.08 7.89 2.04 13 5.50 8.55 2.21 14 5.92 9.20 2.37 15 6.35 9.86 2.54 16 6.77 10.52 2.71 17 7.19 11.18 2.88 18 7.61 11.83 3.05 19 8.04 12.49 3.22 20 8.46 13.15 3.39