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HomeMy WebLinkAboutWQ0011244_Renewal Application_20210129Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0011244 Applicant/Permittee City Of Oxford Applicant/Permittee Address 300 Williamsboro Street Oxford, NC 27565 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Municipal Facility Name City of Oxford RLAP County Granville Fee Category Major Fee Amount $0 Is this a complete application?* r Yes r No Complete App Date 01/29/2021 Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff Name * Ryan Copeland Email Address* rcopeland@synagro.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 336-607-4494 O Modification - Minor G Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0011244 Fbs Current Existing permt number Applicant/Permittee * City Of Oxford Applicant/Permittee Address* 300 Williamsboro Street Oxford, NC 27565 Facility Name * City of Oxford RLAP Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Spec'rfications, Calculations, Rc.) 202101291139.pdf 29.99MB upload only 1 RCF docurrent (less than 250 NS). Ma@iple documents nest be corrbined into one RJF file unless file is larger than upload limit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature �a Cajoel"Od Submission Date 1/29/2021 I ' I ; ! I l { oxford Land Application Permit Renewal PERMIT NO. w Q0011244 pp Land Application of Oxford, NC Residuals Prepared by: SYNAGRO CENTRAL, LL, 284 Boger Road Mocksville, NC 27028 P 336.998-7150 F 336.998. January 15, 2Q21 SYNAGRO January 14, 2021 N.C. Department of Environment and Natural Resources Division of Water Resources Water Quality Permitting Section — Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 ATTENTION: Mr. Nathaniel Thornburg REFERENCE: APPLICATION FOR RENEWAL OF PERMIT ft WQ0011244 CITY OF OXFORD Dear Mr. Thornburg: On behalf of the City of Oxford, Synagro is submitting this application to renew the referenced residuals land application permit. All fields are listed, on for "LASC", as "renew" with the exception of sits GR-2 & GR-3 which are listed as "deleted". Forms RLAP, LASC, and RSC are included, along with other required forms and documentation. The following sites are listed as "renewed" with no changes: o GR-1. GR-4 (all fields) o OR-13 (all fields) GR-60 (all fields) The following sites are listed as "deleted": • GR-2 (all fields) =117;1c' This application package should contain all of the information necessary to complete the requested renewal of the City of Oxford's permit. However, if you require additional information or have further questions, please contact me at (336) 607-4494 or rcopeland@synag_ro.com. Thank you in advance for the timely and efficient review of this renewal application. Sincerely, Ryan Copeland Z�,J�o 6, own 284 Boger Road, Mocksville, NC 27028 • Phone: (336) 998-7150. Fax: (336) 998-8450 State of North Carolina Department of Environmental Quality DWR Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 - RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use tine following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce time amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two co ies of the a1DJll1C1ti0fl and supporting do_cumentation For mare information, visit the Water Quality Permitting Section's Non -Discharge Permitting U►tif General This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application sites) under i 5A NCAC 02T .I 100. Unless otherwise noted, the Applicant sliall submit one original and hvo copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): ® Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06 16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The Applicant's Certification oil Page 5 of this form shall be signed in accordance with I SA NCAC 02T .0106 b . An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 021 .0106 b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing pennit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic fiords transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Classification New Permit Facility - Major Modification' -F 4395 Major (land are pennitted for > 300 acres) $1,310 Minor (land are permitted for < 300 acres) $810 $245 —E� —_ - - m - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (Ali Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (May be Required - See 15A NCAC I C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) fi-om the Enviromnental Assessment (EA) that inpact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of tine subject facilities. Page 1 of 3 INSTRUCTIONS FOR FORM: RLAP 06-16 E. Operation and Maintenance Plan (New and Renewal Application Packages) ® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .I 110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. Maintenance schedules; may include equipment calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the duality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during whiter months when pathogen reduction is most Rely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination ❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T .1102(12). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. ❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. ❑ Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information ❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of I I" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, takes, ponds, and other surface drainage features within 500 feet of the land application site(s). ❑ Delineation of the reviewandcompliance boundaries ❑ Setbacks as required by 15A NCAC 02T. 1108 ❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show cacti nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. ❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans maybe labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 t include new sites) I. Project Evaluation and Receiver Site Management Plan (All New Application Packages i re conMnendatians co� ce Wining cover c ops ❑ Submit a project evaluation and a receiver site management plan (if applicabie) wit and their ability to accept the proposed application rates. J. Hydrogeologie Report (All New Application Packages or Modifications with 15Anvolving NCAC 02T a1ong 104td 4 total and current Division Policy ❑ Submit a detailed hydrogeologic evaluation in accordance available at: i tt ://w%v%v.ncwater.or /Rules Policies and Re ulations/. The document shall be signed, sealed and dated by a qualified professional. pplication Packages with fixed irrigation facilities or irrigation K. Engineering Design Documents (Ail New or Modification A facilities fed through fixed supply system) ❑ Submit engineering design documents that have 1bSA NCeen signed, 02TI.1104 ( �edFor Modificationby a NC s, submit an updated site nmap Professional Land Surveyor in accordance wills specific to the modification(s) only. ❑ The design documents must include the following minimum s they are directly tied into the new items: ❑ Engineering plans for the facility and equipment except those previously permitted unles units or are critical to the understanding of the complete process; Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. ❑ Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages sr Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) ❑ Submit a completed and accurate water balance in accordance with 15A NCAC 02T . L 104 d 5 and current Division Policy available at: Intt ://www.ncwater.or Rules Poes and Re ulationsJ_ M. Property Ownership Documentation (All New or Modification Application Packages involving new mid/or relocated treatment or irrigation components) ❑ Property ownership documentation shall consist of one of the following: ❑Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or ❑Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or ❑ An easement running with the land specifically indicating the intended use of the property and meeting the requirements of ! SA NCAC 02L .0107�f , or gn y g p P rty, p ❑ A written notarized lease agreement si ed b both parties, indication the intended use of the roe as well as a at or survey map. ONE ORIGINAL AND TWO COPIES OFTHE CO� SHALD APPLICATION PACKAGE, INCLUDING BE SENT TO THE FOLLOWING ADDRESS: SUPPORTING INFORMATION AND MATERIALS, NORTH CAROLINA ISION OF WATER RESOURCES NT OF ENVIRONMENTAL QUALITY WATER QUALITY PERMITTING SECTION NON-DISCIIARGE PERMITTING UNIT By U.S Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 B LCourlerlS eclat Delive 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3 State of North Carolina Department of Environmental Quality Division of Water Resources DIvlsion of %Vatcr Resources 15A NCAC 02T .1100 —RESIDUALS LAND APPLICATION PROGRAM LAAP 06- 6 I. APPLICANT INFORMATION: 1. Applicant's name: Ci Of Oxford Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Ainy Rattt Title: Ci En ineer Applicant's mailing address: 300 Williamsboro St, City: Oxford State: NC Zip: 27565- Telephone number: (219) 603- t 113 Email Address: aratliff ,oxfordne.or 2. Consultant's name: Ryan Copeland License Number (for P.E.): Affiliation: N On Staff ❑ Retained (Firm: Consultant's mailing address: 284 Boger Road City: Mocksville State: NC Zip: 27028- Telephone number: 336 607-4494 Email Address: ropeland r± syna9ro,co11l 3. Agronomist's name: Affiliation: ❑ NIA ❑ On Staff Agronomist's mailing address: City: State: Telephone number: (—) 4. Soil Scientist's name: Affiliation: ❑ N/A ❑ On Staff License Number: ❑ Retained (Firm: ------ Zip: - Email Address: License Number: ❑ Retained (Firm: ) Soil Scientist's mailing address: City: State: Zip: - Telephone number: (_,) _- Email Address: S. Fee submitted: ' (See Instruction B) II, PERMIT INFORMATION: pp ❑ modified, ® renewed permit 1. Application is for (check all that ay): ❑ new, , 2. 1f this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W 0� 011244 Date of most -recently issued permit: 4/5/2016 Date of most -recently certified Attachment A (if different than the permit): 4/5/2016 Date of most -recently certified Attachment B (if different than the permit): 4/5/2016 Page 1 of 5 DORM: RLAP 06-16 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 1649 New Commerce Dr. City: Oxford State: NC Zip: 27565- Coordinates: Latitude: 36' 17' 20" Longitude: 78' 34' 49" Datum: NAD 84 Method of measurement: MAP Level of accuracy: Second 2. County where residuals land application program is headquartered: Granville 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Ryan C. Copeland Synagro, LLC 1008530 Back -Up ORC Robert N. Roth Synagro, LLC 1001672 Additional Back -Up ORCs if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Ni ro eti Summor : Determine the maxiinum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 1200 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 26.69 37.69 32,026 45,226 Five -Year Maximum Adjusted 36.83 47.83 44,199 57,399 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently ccriified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops Hay 126.4 Pasture 237.8 Total: 364.20 Methods Surface 364.20 Incorporation or Injection Total: 364.20 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application SumuniZa: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate flbs PAN/ac )O Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 640.5 940.5 884 1148 100 320.3 452.3 442.0 574.0 150 213.5 301.5 294.7 382.7 200 160,1 226.1 221.0 287.0 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated If Dedicated specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source CerliTcation and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Site Certification.doc FORM: RLAP 06-16 Page 3 of 5 Note: Item Vt. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM I. The irrigation system is: ❑ Spray ❑ Drip 2. Disposal system is: ❑ existing ❑ proposed, 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 021.0505 requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? ❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Recommended Recommended Soil Series Fields within Soil Area Loading Rate I Loading Rate 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? ❑ Yes or ❑ No If No, explain why 15A NCAC 02T .0505(nl is not met: 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field /Zone Design Area Number of Maximum Application Design Annual Loading (ft') Nozzles Rate allons/hr Rate(gallons / r Total Spray Irrigation Design Element Wetted diameter of nozzles Wetted area of nozzles Nozzle capacity Nozzle manufacturer / model Elevation of highest nozzle ft tie ft Plan Sheet I Specification Number l Page Number FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106); 'he applicant or any affiliate has 'lot been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02"T .0105. ® Yes ❑ No, Explain; I, (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for � (Faci14 Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, Which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package Will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, Which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: —42� Date: FORM: RLAP06-16 Page 5 of 5 OPERATIONS AND MAINTENANCE PLAN SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0003226 (Town of Siler City NC WTP/WWTP) Inspection Plan inspections will be conducted on a weekly basis at the land application site during activities of this project. inspection frequency is based on the time frame to complete the project and the amount of dry applied tons to bl as Ind appectilie from the facility. The inspections will consist of inspecting a field that is currently being andom fields that have been completed. These inspections will consist of: 1. Verifying that the "Pre -Operations Check List' has been completed and signed by both operational and technical staff. lied. 2. Checking the calculated loads to insure the correct amount of residuals are being land applied, 3. Insuring that all manned equipment has a copy of the spill control plan, the permit, and the operations and maintenance plan. 4. Insuring that the field has been flagged properly and that all buffers are being adhered to. 5. Insuring that the "Crop and Landowner Verification" form has been filled out. 6. Verifying that the residuals have been adequately sampled to confirm compliance. The records will be kept in the project files in the respective office for the project. The Permittee or Inspector shall report by telephone to the NCDENR/DWQ Raleigh Regional Office at 919-791-4200, as soon as possible, but no later than 24 hours after, or the next working day, following the occurrence or first knowledge of the occurrence of the following. Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. • Any failure of the program that results in a release of material to surface waters. Any time that self -monitoring information indicates that the program has gone out of compliance with the permit. Any process unit failure that results in the system not adequately treating the residuals. • Any spill or discharge from a vehicle or piping system during residuals transportation. Any release that requires immediate reporting outside of normal business hours shall be called in to DENR at 800-858- 0368, or 919-791-4200. These numbers are to be called in the event of a release to surface waters or the imminent failure of a storage system when the event occurs outside of normal business hours. Within 5 days of the first notice of on occurrence, a written response in the form of a letter shall be sent to DENR outlining the actions taken or proposed actions taken to ensure that the problem does not recur. Persons responsible for inspections on this project are as follows; Ryan Copeland, Technical Services Specialist, or his designee. OPERATIONS AND MAINTENANCE PLAN SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0003226 (Town of Slier City NC WTP/WWTP) Sampling Plan Sampling for this project consists of sampling the residuals just before land application is to occur. Based on the dry tonnage of this plant, there will be four samples for each parameter per year. The residuals shall be sampled annually for the following: (Regulatory level in milligrams per liter in parentheses.) Arsenic (5.0) 1, 4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1, 2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1, 1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2, 4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13 Tetra chloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachlorethane (3.0) 2,4,5-Trlchlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5 TP ( Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl Chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) The residuals will also be sampled, based on the chart below, for the following constituents Dry Tons Generated (short tons per year) Monitoring Frequency (Established in 40 CFR 503 and 15A NCAC 02T.1111) <319 1 time per year =>319-<1,650 1 per Quarter (4 times per year) =>1,650-<16,500 1 every 60 days (6 times per year) =>16,500 1 every month (12 times per year) Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Sodium Adsorption Ratio (SAR) Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium pH Plant Available Nitrogen (calculation) Selenium Sodium %Total Solids Total Kjeldahl Nitrogen Zinc All samples will be taken from the thickening basin. Additional samples will be taken for TCLP/RCI and nutrients and metals analysis. Methods of sampling will follow the conditions of the permit and applicable regulations. The following people are responsible for sampling: Ryan Copeland, Technical Services Specialist, or his designee. a 4 OPERATIONS AND MAINTENANCE PLAN SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0011244 (City of Oxford NC WWTP) Operational Functions The operational function of this project involves land application of residuals for the City of Oxford's wastewater treatment facility. This material will be loaded onto tractor trailers or "spreader trucks" and hauled to land application sites. Tractor trailers will be off loaded to liquid applicators and spread in a uniform manner. The residuals will be spread at agronomic rates, as determined by a recently analyzed nutrients and metals sample. The material will be land applied with a liquid applicator that will use pressure to achieve a consistent spread pattern. The fields applied will have a crop, either established or planted soon after application, which is to be utilized for animal consumption. Safety Measures Synagro believes in operating in a safety -conscious manner and has all employees participate in quarterly online safety courses. These courses are designed to help employees recognize safety issues and take steps to prevent accidents from occurring. In addition, all Synagro employees have the authority to stop operations if they think any aspect of the operation could cause environmental or personal harm. Maintenance Schedule Synagro will follow the maintenance schedule specified by their fleet management section for the equipment necessary to complete the job. Residuals Sampfing Plan Synagro Residuals Land Application for 'i Q0011244 City of Oxford NC WWTP Nutrients and Metals Analysis • Sampling Point: Lagoon • Sampling Frequency: 4/yr (Volume Dependent) • Sample Type: Composite • Lab: Pace Analytical / Waypoint Analytical Pathogen Reduction (Fecal Coliform Density Demonstration) • Sampling Point: Lagoon • Sampling Frequency: 4/yr (Volume Dependent) • Sample Type: Grab — Fecal Coliform Demonstration • Lab: Meritech Inc. Environmental Lab Vector Attraction Reduction (30-Day Bench) TCLP A • Sampling Point: Lagoon • Sampling Frequency: 4/yr (Volume Dependent) • Sample Tyne: Composite • Lab: Meritech Inc. Environmental Lab • Sampling Point: Lagoon • Sampling Frequency: Once per permit cycle • Sample Type: Composite • Lab: Summit Environmental Technologies, Inc c r SPILL RE, SPONSE PLAN r'ROJECT: City of Oxford Permit W00011244 IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTION_ S SHALL BE TAKEN IMMEDIATELY: 1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Synagro Operations Manager shall take immediate charge and initiate clean-up activities. Synagro labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the City of Oxford NC or the NC Department of Transportation, and other private contractors as necessary. 2. HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3. CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Synagro Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lone, and other items necessary to complete the clean- up operation, i.e., local farmers, farm supply centers, nurseries, etc. 4. CLEAN-UP: Tmploy fi-ont-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as Alrrch of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5, FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction of the property owner- and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6. NOTIFICATION• As soon as possible after the spill occurs, the Synagro Operations Manager or assistant will notify the Synagro Central office, and they will then be responsible for notifying other key Synagro personnel. 7. REPORTING: Synagro Central personnel will notify the Raleigh Regional office at (919) 791-4200 for the City of Oxford as soon as possible, but not more than 24 hours after, or oil the next working day following the occurrence. The Operations Manager shall provide a written report within 48 hours of the spill to the Technical Services Director. The report shall list all relative information and actions taken. Synagro Central personnel will file a written report to the Raleigh Regional office of the NCDENR within 5 days of the occurrence. For after hours reporting the Division's emergency number shall be called to report all incidences (1-800-858-0368) or (919-733-3300). m State of North Carolina D_ WR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supporting documentation For more inforinalion, visit the [Valor Quality Permitting Soclion's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T . 1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and rnects all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified Iaboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page I of I RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: City Of Oxford Status Maximum Dry Tons Per Year Facility Permit Holder Facility Name County Permit Number Code Current b Proposed R City Of Oxford Oxford WWTP Granville NCO025054 1200 1200 2 Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) + D (Deleted) b The amount of residuals currently permitted for distribution. land application, or disposal (i.e. not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina nWR Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION Division of Water Resources FORM: RSC 06-16 1. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): L. Facility Name: Oxford WWTP 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Govermnent, or ❑ Private. Facility pennit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: _ _)- 3. Facility contact person and title: Antoine Lewis Complete mailing address: 1649 New Commerce Drive City: Oxford State: NC Zip: 27565 Telephone number: QL9) 69378783 E-mail address: alewis oxfordnc.or 4. Facility physical address: 1649 New Commerce Drive City: Oxford State: NC Zip: 27565- Coordinates: Latitude: 36' 17' 20" Longitude: 78' 34' 49" Datum: NAD 84 Level of accuracy: Second Method of measurement: Map 5. Purpose of the facility: ® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages:. % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: Yes ❑ No 7. Facility permitted/design flow: 335 MGD and facility average daily flout: 1_3 MGD 8. Average amount of residuals being generated at this facility dry tons per year, 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 800.000 Gal. Aerobic Digesters Type and volume of residuals storage (i.e., outside of residuals treatment units): 4 Million Gal, Concrete Lined Basins it. RESIDUALS QUALITY INFORMATION (See Instruction C.): i . Specify if residuals are regulated under: ® 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestichnunicipal wastewater treatment processes are regulated under "i0 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102 6 as: ® Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, anima processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Pagel of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261,31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ®iio. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Sumit Environmental Technologies INC and Date of analysis: 12/29/2020 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >140 °F (> 140°F) Passed reactivity test: [Dyes ❑no. HCN: I rng/kg (<250) & H2S; mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/J) TCLP Parameter Limit (ing/1) Result (mg/0 Arsenic 5.0 ND Hoxachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadicne 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0A ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1, l-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 'I, Metals Determination: Complete one of the following tables (i.e,, as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T ,1 105, a. For Dlslrihutiofr/Land ADDlicalion: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Pace Analyical and Date of analysis: 10123/2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (CtassA & ClassB) (Crass A Only) (ing4g) (ing4g) (nrg/kg) Arsenic 75 41 3.8 Cadmium 85 39 1.1 Copper 4,300 1,500 450 Lead 840 300 30 Mercury 57 17 ND3. Molybdenum 75 n/a 8.5 Nickel 420 420 12 Selenium 100 100 7.5 Zinc 7,500 2,800 1800 b. For Surface Dis osal Uult larul rll : Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory; and Date of analysis: Distance from Disposal Arsenic Unit to Boundary to Chromium Nickel Closest Property Line (meters check one) (irrg/k� (nrg/k� (irrg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 4�270 240 ❑ >_ 50 but < 75 39 260 ❑ 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (irg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 3.39 %. b. rill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Pace Analytical and Date of analysis: 10/23/2020 Parameter Result (mg4g) Aluminum 46,000 Ammonia -Nitrogen 11,000 Calcium 16,000 Magnesium 4,200 Nitrate -Nitrite Nitrogen 62 pH (Standard Unit) 7.5 Phosphorus 18,000 Potassium 2,900 Sodium 2,100 Total Kjeldahl Nitrogen 37,000 C. Using the results listed in Item H. 5b. above, calculate the sodium adsorption ration (SAR): .70 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): 0 default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (0) Year PAN Five -Year (,rrg/kg) Maximum Adjusted PAN (ing4g) Surface 13,344 18,4I6 Injection/Incorporation 18,844 23,916 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: 70 FORM: RSC 06-16 Page 4 of 5 Pathogen Reduction: Per 15A NCAC 02T.1 106 specify how residuals ►vill meet the pathogen reduction requirements: a. For Dislribullort/Laud Avnlicalioit of Class A or Eguivalenl: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or El A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [ 15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T. I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [I5A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.1106R 3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: El composting, heat drying, [] heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application o Class B: ® Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ AIternative 2 [15A NCAC 02T.I 106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Sur ace Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alteratives in Item II.7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II.7b. above. ❑ Exempt -If Daily Cover AIternative is chosen in Item I1.8. below [15A NCAC 02T. 1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Vector Attraction Reduction (VAR). Per 15A NCAC 02T.1 107 specify how residuals will meet the VAR requirements: ® AIternative I [15A NCAC 02T.1107(a)(01 - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion), ❑ Alternative 2 [I5A NCAC 02T.1107(a)(2)1- 40-Day Bench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ AIternative 5 [15A NCAC 02T.I 107(a)(5)] - I4-Day Aerobic Processes. ® Alternative 6 [15A NCAC 02T.1 107(a)(6)] - AlkaIine Stabilization. ❑ Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ® Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ® Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - SoiUOther Material Cover [15A NCAC 02T.1 107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 A VTCINITY MAP SYNAGr o l it Ruirbrull rtilr��ra�eure�u (:��,�l�rrny oWNE©,c Derma E 0 ,i { cc ! f9 fy LL CY) � M ce) -m � I� �� s SECTION 2 PROCESS DESCRIPTION 2.0 General Sewage at the City of Oxford Treatment Plant is treated by ten basic processes: 1. Screening 6. UV disinfection 2. Grit removal 7. Post aeration I Biological reactor (Oxidation Ditch) S. Aerobic sludge digestion 4. Secondary clarification 9. Sludge storage 5. Tertiary filtration 10. Land application of sludge The headworks consists of a new mechanical bar screen, a new aerated grit chamber, a new Parshall flume with flowmeter, and a new triplex pump station. The mechanical screen is utilized to remove large objects from the influent flow which could cause damage, clogging or jamming of units of the plant. A manual bypass bar screen can be used for screening when the mechanical screen is not in operation. The aerated grit chamber removes inorganic abrasive particles that could cause excessive wear and solids deposition within the plant. The grit removal system is comprised of an aerated chamber with grit removal via chains and buckets. Grit is conveyed into a cart for disposal in a landfill. Secondary treatment begins with a new three stage oxidation ditch featuring anaerobic, anoxic, and aerobic zones with internal recycle between tine aerobic and anoxic zones. The three zones work together to remove nitrogen and phosphorous in addition to BOD reduction. The secondary clarifiers remove settleable solids and scum for further processing in the sludge system. Three clarifiers operate in parallel. The tertiary treatment consists of a new traveling bridge tertiary filter to treat wastewater to meet tertiary limits. The effluent then passes through a UV disinfection chamber. This disinfection is provided to destroy any disease -causing organisms that may remain in the effluent. Finally, the effluent is mechanically aerated before being discharged to Fishing Creek through an outfall line. The waste activated sludge is pumped to the aerobic digesters for further treatment and subsequent removal to the sludge storage basin for holding until ultimate disposal by land application. 0 Quantitative 3118ti.fication for Residuals P"Oduction Efate Oxford W WTP Between the years of 2015 and 2019, the City of Oxford land applied approximately 413.56 dry tons of material each year. Based on the calculations shown below, the Oxford WWTP would produce approximately 584 dry tons/year if operating at the 3.5 million gallon permitted flow. The proposed 1200 dry tons/per year maximum to be produced at this plant, should allow plenty of room far any increase in plant flow or plant expansions. Calculations: Based on rule -of -thumb that average daily flow is approximate to annual volume of residuals produced: 3.5 x 1 Q^6 al/ r x 4% solids x 8.341bs/ aI = 583.8 dt/yr (2,000 lbs/ton) Di tons land applied between 2019 and 2015. Year Dry Tons 2019 733.82 2018 209.18 2017 423.11 2016 449.34 2015 252.33 r�. Residuals Samplitig l� aIjj Synagro Residuals Land Application for WQ0011244 City of Oxford NC WWTP Nutrients and Metals Analysis • Sampling Point: Lagoon • Sampling Frequency: 4/yr (Volume Dependent) • Sample Type: Composite • Lab: Pace Analytical I Waypoint Analytical Pathogen Reduction (Fecal Coliform Density Demonstration) • Sampling Point: Lagoon • Sampling Frequency: 4/yr (Volume Dependent) • Sample Type: Grab — Fecal Coliform Demonstration • Lab: Meritech Inc. Environmental Lab Vector Attraction Reduction (30-Day Bench) TCLP • Sampling Point: Lagoon • Sampling Frequency: 4/yr (Volume Dependent) • Sample Type: Composite • Lab: Meritech Inc. Environmental Lab • Sampling Point: Lagoon • Sampling Frequency: Once per permit cycle o Sample Type: Composite ® Lab: Summit Environmental Tecluiologies, Inc Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Ryan Copeland Project Name. Oxford Lot Number:VJ16006 Date Completed:10/23/2020 10/28/2020 3:24 PM Approved and released by: Project Manager II: Lucas Odom s accREo 407 4W i TNI I00%"k(IfAWeria� \� �eQAR� AC C R E OITE0 T UNI Ll--, kTf The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel; 803-791-9700 Fax: 803-791-9111 www.pacelabs.com Page I of PACE ANALYTICAL SERVICES, LLC SC ❑HEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VJ16006 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP Due to low percent solids, sample -001 was weighed out at 3 times the normal amount. The LOQ has been elevated to reflect the dilution. Pace Analytical services, LLC (fornieify Shealy Emftnmelal Services, Inc.) 106 Vantage Point drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vnwr.pacelabs.com Client: Synagro Description: OXFORO N&M Date Sampled:10/1412020 1005 Dale Received: 1011612020 Laboratory ID:VJ16006-001 Matrix: Solid % Solids: 3.39 10/17/2020 0144 Inor anic non-metals 1 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch (% Solids) SM 254OG 1 10/17/2020 0144 LSH 1 350.1 (Ammonia - N ) 350.1 10 10/19/2020 1724 DRD 70234 1 (Nitrate - N) 9056A 1 10/21/2020 1932 AMR 70365 1 (Nitrite - N) 9056A 1 10/21/2020 1932 AMR 70656 1 1 (Phosphorus) 365.1 25 10/20/2020 1740 DMA 10/20/2020 1300 70657 70385 (Soil pH meas) 9045D 1 10/20/2020 2239 AAB 2 351.4 (TKN) 351.2 1 10/21/2020 1737 DMA 10/21/2020 1201 70569 70594 Parameter CAS Analytical Solids Number Method Result Q LOQ DL Units Run Ammonia - N (gas diffusion)SM 2540G 3.39 % 1 Nltrate - N (soluble) 350.1 11000 300 160 mglkg 1 Nitrite - N (soluble) 9056A 44 15 3.0 mglkg 1 Phosphorus 9056A 98 5.9 3.0 mglkg 1 Soli pH measured in water @ 19.3 C ° 7723-14.0 365.1 18000 3700 740 mglkg 1 TKN 9045D 7.5 su 1 351.2 37000 740 740 mglkg 2 CVAA Run Prep Method 1 Analytical Method Dilution Analysis Date Analyst Prep Date Batch 7471 B 7471 B 1 10/20/2020 1342 JAB2 10/20/2020 0910 70438 Parameter CAS Analytical Mercury Number Method Result Q LOQ DL Units Run 7439-97-6 7471E Np 2.3 0.56 mglkg 1 ICP-AES Run Prep Method 1 3050B Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 3050B 6010D 1 10/22/2020 0131 KSH2 10/17/2020 1518 70258 6010D 1 10/22/2020 1406 KSH2 10/17/2020 1518 70258 Parameter CAS Analytical Aluminum Number Method Result Q LOQ DL Units Run Arsenic 7429-90-5 6010D 46000 200 73 mglkg 1 Cadmium 7440.3$•2 60100 3.8 J 7.3 2.4 mglkg 1 Calcium 7440-43-9 6010D 1.1 J 2.4 0.62 mglkg 1 Chromium 7440-70-2 6010D 16000 2400 310 mg/kg 1 Copper 7440�7-3 6010D 42 4.9 1.2 mglkg i Iron 7440-50-8 6010D 450 4.9 2,2 mg/kg 1 Lead 7439-89-6 6010D 18000 49 22 mglkg 1 Magnesium 7439-92-1 6010D 30 4•9 22 mg/kg 1 Manganese 7439-95-4 6010D 4200 2400 310 mglkg 1 Molybdenum 7439-96-5 6010D 670 7.3 2.9 mglkg 1 7439-98-7 6010D 8.5 J 20 4.9 mg/kg 1 Q = Limit of Quanlitauon 13 = Detected in the method blank E = QuanVlafion or com = Not deteged at or above the DL N = n, • Pound exceeded the calibration range DL = Detection Limit Recove is out of criteria P = The RPD behveen two GC columns exceeds 40 J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight bass - Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 3 Vantage Point Drive Wes[ Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 vnvw.pacelabs.com Page 3 of 7 Giant: Synagro Description: OXFORO N&M Date Sampled:10/14/2020 1005 Date Received:10116/2020 Laboratory ID: VJ16006.001 Matrix. Solid % Solids- 3.39 10/17/2020 0144 ICP-AES N Prep Method 3050E Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 30508 601 OD 1 10/22/2020 0131 KSH2 10/17/2020 1518 70258 6010D 1 10122/20201406 KSH2 10/17/2020 1518 70258 Parameter mb S Analytical Nickel Nu Method Result Q LOQ DL Units Run Potassium 7440-02-0 6010D 12 J 20 5.1 mglkg 2 Selenium 7440.09-7 6010D 2900 2400 310 mglkg 1 Sodium7782.49-2 6010D 7.5 J 9.8 4.0 mglkg 1 Zinc 7440-23-5 6016D 2100 J 2400 310 mg/kg 1 7440-66.6 6010D 1800 24 6.1 mglkg 1 I = Limit of Quantitation B = Detected in the malhnd blank E = Quanlitation of compound exceeded t = Fiot detected at or above the DL N = he calitxalion range DL = Detection Limit Recovery is out of criteria P = The RPD between two GC columns exceeds 409; Out of holding timo W = Reported on wet weight basis J =Estimated result < LOQ and > DL Analytical Services, LLC (fomterfy Shealy Environmenlal Services, Inc.) Vantage Point Drive West Columbia, SC 29172 (m) 791-9700 Fax (803) 791-9111 wwvrmpacelabs.com Page 4 of 7 and Miscellanoom Docm rig nbq Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com I O CEO r i a t y L re L d17o O S. L l rn d d tr � ti y yY3 tlilh pp � l O B 4y ■■■M■■■■I♦INE■ r■rl• ONE ■■WEE No ■■■E■I■t/I'�� Noun loon r!`lIM, 9-:0 NoIN 0 ' MWEINU■ . P.1■■IIIII■ Z MEMO ■■AI■" 0 MINE■ t ®O■M■I♦NO■■IrSMENUMINEN 11:1WE■■■WER „ ri- IF-� Da L riouas�x�llvdr3J. at,+,n� O U. tu i 1 r � � u I.a1:t:rt1 1PAJI JI :llAt 314M � � � 1 g � 6lr k++Da tt��� 1gr17 x1J1►l�E tto rt a �i�tigg3. rc �SYiC.�6s � r1 f V ci 2 X r Lu I[_ g t a, Cr [1 tee 'p -_._ 9 xg �_ �. � . f � �� r►r3Jt �1 a Pace Anaty&cal Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 7 Pi\'( f.-: ANA11-.1/`WAL SERVICES, LLC Sb!a's Gr.ri�tnet:nr l Stl � s..y, L:�, 1xsm:at lawn}ar 11.1};nlbC-14 ryty I ut' I crn�u.Y rrafe. s+�1+:18 SAn>ple Receipt Checklist (SRC.) rim: SYIvlIM0 _ Cnoler htsp.�cted b ,'elate: HNIG, i icllirlan I n I if. V1i(OOb l4lutns nP rp epipt- ❑ SrSI ❑Client QJ UP'S d Yes 011n L %cm custo Seats present Gat the Cooler? CIAC31 LJNV1NA 3. if"cusint seals t,verc. r03E111. wore tP:t;y infect and unhi•nRen? "FEE Strip lip: NA ... Chlorale SIJp ID: NA T _ Tcs' d b ,c y': _ t�riaina: Will pvrnlure upolt receipt! Nrived (C'orreetetl) Inulperalu.-c upon :rceip: !!Solid 5 tzlt4cllp if ): 20.1t)56 -C. NA /NA. --f C NA /N'A ,(., NA INA "C \7ctitUfJ: C]Titrtprrtllurc Blank (�4Sainst I�ot#las IR Guo il):. 5 A (i 111 Correcik , school, 0 "C -Madind of conlant; 0 wet ivt Ft Icu iw+ S ❑ 1),y Ico J Now Ycs h'n [j Q 1, If temperature of my cooler e,tcredecl 6.4"(', u;tis Project MSnag r Notifte-d? � ivn ' PM was Nolil:cd_by; phone Iemal) f iacc-feel +ce. (ci,.::c a tcj, ® Ya.; ❑ No ❑ KA 4. Is the commerciol courier's uaukiug Slip itttacl:cd to Ili's form`? {71 Yes ❑ No 5, Ware propCi'uui((:dy prncMures (relin uishedrreazived) folloN+-c ? V1 Yes ❑ No -Yes G. Were solllplt: it),, listed an the COC? ® ❑ Nip 7. Wrrr. sam le IDs ;istcd on nl! sample cnnlni i rs7 Ycs Q No S. 1Vos vulicction date Ar, 'inir. HUM oil the COC? ❑ Yes ®yn V. Vdtls collrction date fi 'ilrw listed on a:l sa;nple eQnlai<ie,;;? Ali Y s Q No Ib. iJiti all container label infomtn#iols (In, dale, time) agree �rillr Hl COC' T 111�'etc lasts to he perf',rtmet# lised on the CULT®Atu t�Km[]No 12. Did ull y.triples rrrive in lho proper eai.tuint rti For rich test a tell, r in good ; onJitissn (unbrokoll, lids U11, Ctc,)? T Yes ❑ No 13. Wa.;1XIe4 ttrte sample vnhratr. s,va:lable`) Ycs 0 No 14. Were all samples i'ece:ircti wilhir% ;4 the holding time or 48liour5 wllichetier cvglcs 11ts1'? Yes ONO 15, Were Inv samples ruruAiuc'rs missi:tgh:xcess (circle ore) sanlpkr No! lis ed an r0(' L] Ye, ❑ I�r) NA 7pay rIof the von vials? ❑ Ye, No, hFJ SPA i?. Werou rill DRO/melalsint:lriert samples tell iaetl f# a ptI of ?? -�`--" ❑ Ycs El Mil ®,NA 18, Were ail tvilitidc snmlllt : rrreivri at a PH r• 12 attd sulfide sa:unics rrccived of a '- irl ❑ Yes j] No pl 0 NA 19' 'rrc a app:iGtblc N1i,,f I"KNA:-y4atitk1p tcno rfi2S (<` (I,;nig, s rrgd:s f1YC al':cRldlF.11 _ Cla(11'1114? _ ❑ Yes 0 No NA ?0. Wem client remarkstreilursis (i.e. requeslccl dilutions. MSllv1SD esip.ttalusn r, etc...) cor•reetty ininwribed front the COC inro dia txnnn:cu# wlion In L1A! ? ❑ 1'rti Na 2 L Wa.c'hn tLetc nuntt,er' l:stcd on the rnntainnr label? I#' cs, uotc M 1071 .�— Suo1PIC PITHervalion (�Itlst be ctllrl#,lcled for any satttplc(s) i,IcallvctlY pmwr%Td or %vlth lac spat c.; 5antp:e(sl NA were received lncorrCcUy prescrvcG all ►verr. adjusted accordingly' lit sample rcvciving with NA _ ntl_ oicircle One; H2SO4, IIN03, HC1, KaOM Irein; Sit # Nr1 irate of pr- sbwyadnn NA If "utro than one oreserva:ivc :s needed, plutimi "ore in the c InlucHts below, S:;mple(s) NA wale rcceiwd with btia les - G rnm in diannder. St ulples(%) NA v urc rcc: ived wish TPtC ,- Q,5 ltlkrl, (f 019 '.s tin) find were ><djusted acrnrciingly in snrnPk neeivin,g whit sodium thitssul(irlc (vs2Safla) with Shealy II); N SK Gaxode laws applied hy: 11M.G tlalr. 10? 02010 r`o•nmenls: ' Pace Anaiyucal Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com ProjeC#; Sodium Absorption Ratio Calculation (SAR) % Solids 3.39 Na (mg/kg) 2100.00 Ca (mg/kg) 16000.00 Mg (mglkg) 4200.00 Na (mg/L) 71.19 Ca (mg/L) 542.40 Mg (mg1L) 142.38 Na (meq) 3.10 Ca (meq) Mg (meq) 27.07 11.72 SAR = 0.70 LEGEND Fill in this area with data from the analysis sheets These areas are calculated automatically Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Ryan Copeland Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech Work Order # 10082043 Sample: Oxford 1 Grab Parameters Results Analysis Date % Total Solids 3.85 % 10/9/20 Fecal Coliform (Sludge) <236 col/g dry wt 10/8/20 Meritech Work Order # 10082044 Sample: Oxford 2 Grab Parameters % Total Solids Fecal Coliform (Sludge) Results Analysis Date 2.91 % 10/9/20 <312 col/g dry wt 10/8/20 Page 1 Report Date: 10/16/2020 Project: Oxford Date Sample Rcvd: 10/8/2020 10/8/20 Reporting Limit Method 0-100 % SM 2540B 236 col/g dry wt SM 9222D 10/8/20 Reporting Limit Method 0-100 % SM 2540B 312 col/g dry wt SM 9222D Meritech Work Order # 10082045 Sample: Oxford 3 Grab 10/8/20 Parameter Results Analysis Date Reporting Limit Method % Total Solids 3.79 % 10/9/20 0-100 % SM 2540B Fecal Coliform (Sludge) <240 col/g dry wt 10/8/20 240 col/g dry wt SM 9222D Meritech Work Order # 10082046 Sample: Oxford 4 Grab 10/8/20 Earameters Results AnalysiN Date Reporting Limit Method % Total Solids 3.91 % 10/9/20 0-100 % SM 2540B Fecal Coliform (Sludge) <232 col/g d2y wt 10/8/20 232 col/g dry wt SM 9222D Meritechi Work Order # 10082047 Sample: Oxford 5 Grab 10/8/20 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.08 % 10/9/20 0-100 % SM 2540B Fecal Coliform (Sludge) <223 col/g dry wt 10/8/20 223 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 fleritech, r(nc. Environmental Laboratory Laboratory Certification No.165 Contact: Ryan Copeland Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech Work Order # 10082048 Sample: Oxford 6 Grab Parameters Results Analysis Date Page 2 Report Date: 10/16/2020 Project: Oxford Date Sample Rcvd: 10/8/2020 10/8/20 Reporting Limit Method % Total Solids 4.01 % 10/9/20 0-100 % SM 2540B Fecal Coliform (Sludge) <227 col/g dry wt 10/8/20 227 cal/g dry wt SM 9222D Meritech Work Order # 10082049 Sample: Oxford 7 Grab 10/8/20 Parameters Results Analysis Date Reporting Limit Method % Total Solids 4.25 % 10/9/20 0-100 % SM 2540B -al Coliform (Sludge) <214 col/g dry wt 10/8/20 214 col/g dry wt SM 9222D ti ereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record (COC) NPDES#: MERITECH., INC. Client: Phone: Address: 2 V(L Fax: �4 ENVIRONMENTAL LABORATORIES �� ASC. Email: tv(��rAN±, 4, 642 Tamco Rd. Phone: 336-342-4749 Project: CAEOM Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@ meritechlabs.com Attention: yhry1J65P6ZANr> Turn Around Time* www.meritechiabs.com How would you like your report sent? *RUSH work needs prior approval, el>:,r �s n �l Std o ,5) 3-5 Da s 24 �18Hrs Circle all that apply Emai (preferred) , Fax, Mai[ ❑ Sampling Dates & Times Person Taking Sample (Sign/Print): n, _ l uoo;;� Lab Use Only Sample Location and/or ID # start End!�-fj�} Date Time comp? of Test(s) Required pH Date Time Grab? cant. K? es N yes / No Cl OK? FE<8 L r recht- v 2 � 3 � Temperature Upon Method of Dechlorination (<0,5 pm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Receipt: Shipment: Comments: Compositor # ❑ UPS ❑ Aed Ex Are these results for regulatory purposes? Yes V No ❑ Report results in: mg/L ❑ Jug # mg/kg ❑ ug/L ❑ Hand Delivery Relinquished by: 690 Time: /�� Date: (p"g�3 Received b S by: Date: Time; ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by; Date: Time: Rece' by ab: Ci FECAL DATA SHEET Lab result Log 236 2.37 Min 214 312 2.49 Max 312 240 2.38 Geometric Mean 239 232 2.37 223 2.35 227 2.36 214 2.33 Average 2.38 Meritech, 1h� -" Environmental Laboratory Laboratory Certification No. 165 Contact: Ryan Copeland Report Date: 11/11/2020 Client: Synagro 284 Boger Road Project: Oxford Mocksville, NC 27028 Date Sample Rcvd: 10/8/2020 Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test Meritech Work Order # 10082050 Sample: Oxford Grab 10/8/20 Total Solids Volatile SolidS % Volatile Solids Week 1 1.46 0.800 0.551 Week 2 1.32 0.740 0.561 Week 3 1.59 0.880 0.556 Week 4 1.44 0.800 0.555 Week 5 1.60 Van Kleeck Reduction (%): 8.59 I hereby certify that I have reviewed and approve these data. 0.529 Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 8/9/i8 Chain of Custody Record (COC) NPDES#: Client: S yma� Phone: Address:_ 7yl &&1EQ- &f- - Fax: M E R IT E C H� INC. ENVIRONMENTAL LABORATORIES &J�iJh-GI~ AJ Email: f�LflpEf /�l� Si' 642 Tamco Rd. Phone: 336-342-474$ Pro ect: Q Reidsville NC 27320 Fax: 336-342-1522 ` P.O.#: Email: info@ meritechlabs.com www.meritechlabs.com t pPELM Turn Around Time* Attention: `x, *RUSH work needs prior approval, How would you like your report sent? C iarnes a i Circle all that apply: ma (preferred), FaX, Mail Stcl 10 s) 3s 214rs Sample Location and/or ip # Sampling Dates & Times Person Taking Sample (Sign/Print): fzi"970 Lab Use Only Start End Comp? # of Test(s) Required On Ice? pH OK?? Date Time Date Time Grab? Cont. Yes / No Cl OK? 20 is I-Yo u Temperature Upon Method Of Dechlorination (<0.5 ppm) ofAmmonia, Cyanide, Phenol andTKN samples must be done in the field priorto preservation. *** Receipt: c, 2L 1> Shipment: Comments: Compositor # ❑ UPS Jug # ❑ ed Ex Are these results for regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L ❑ Hand Delivery Relinquished by: Date: Time: /d-8-� 0; Received by: Hate: Time: ❑ Other Relinquished by: Date: Time; Received b Y: Date: Time: Relinquished by: Date: Time: R ved Lab: f �j f CJat h TIR ,T �1 %VSR (older, more conservative method %VS in 0.5510 Enter in %VS out 0.5290 decimai form %VSR- %VS in - %VS out ((%VS in - (%VS in x %VS out)) %VSR= 8.48 (method from p.132 of WH manual) %VSR-_ %VS in - %VS out %VS in i( ric - • ■ - - -_-_ _ -- _ _----- - -- -_ _ SUMM11r Summit Environmental Technologies, Inc. 3310 Win St. ENVIRONMENTAL TECI$t401,0GIF1. IW' Cuyahoga Falls, Ohio 44223 AFWyilcal Laborarorlec TEL: (330) 253-8211 FAX.- (330) 253.4489 if ebsire: http✓/wunv.settek.com December 29, 2020 Ryan Copeland Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: OXFORD Dear Ryan Copeland: Order No,: 20121123 Summit Environmental Technologies, Inc. received 1 sample(s) on 12/18/2020 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance litnits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, r Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC F.87688, Idaho 01-100923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (undergmwid Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH909232020-1, New Hampshire 2996, New Jersey 014006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DNV, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA00031[7, South Carolina 92016001, Texas TI04704466.19-16, Utah OH009232020-12, Virginia VF.LAP 10381, West Virginia9957C Page 1 of 30 Summiar Srtrrrnril Errvirorrrrrenlal 33roLYin sr. TechnologiesM A Case Narrative ENVIRUNRiFNTAt- TrC"U01()GIF +, ,: Cuyahoga Falls, Ohio 44223 w0#: 20121123 Analytical Cahorelortes TEL.- (330) 253-8211 FAX (330) 253-4489 Website. hil .-Mvwrvsellek.com Date: 12/29/2020 CLIENT: Synagro Project: OXFORD WorkOrder Narrative: 20121123: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Enviromnental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Report" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 20121123-OOIA FlashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to 250 RPM as required by the method. Analytical Sequence QC Notes: LCS-R121667 FlashPt_S(1010): Z = Method deviation, due to instrument limitations could not stir to 250 RPM as required by the method. Original b.,..,. n _-V on 1 i f Stmimi! Environmental Technologies, lne. 3310 Win S1. Workorder E1.VII�UiJId[NrhR it G.HU010Rff-R, i ;r Cuyahoga Falls, Ohio44223 Sample Summary Analyfleal labor rtorles TEL: (330) 253-8211,VAX-- (330) 253-4489 WON: 20121123 Ilrebsite: hftp:/hvttRvsettekcam 29 Dec-20 CLIENT: Synagro Project: OXFORD Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 20121123-001 OXFORD TCLP 12/17/2020 8:00:00 AM 12/18/2020 10:20:00 AM Sludge PanpAnf-'4n U, Summit Environmental Technologies, Inc. DATES REPORT 3310 Win Sr. E;ZLOOII Snt LIJVNVI RON MENTAL TECKNOLAGIES. Cugahoga Falls, Ohio 44223 WO#: 20121123 A,wlyVcal = ^r3rorles TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: htm:/1www.settek.c2m 29 Dec-20 Client: Sytlagro ]Project: OXFORD Saran➢e ID Client Sample ID Col?ee:icr. Date N'atrLx Test Name Leachate Date Prep Date Analysis Date 20121123-001A OXFORD TCLP 12/17/2020 9:00:00 AM Slwc c Flashpoint Determination (1010) 12/22/2020 1:51:08 PN pH (SW9045D) 12/22/2020 11:31:06 AM Reactive Cyanide (9014/7.3.3.2)-Solid 12/21/2020 2:38:00 PM Reactive Sulfide (9034)/7.3.4.2 12/21/2020 2:38:00 PM TCLP herbicides by EPA 832113 12/22/2020 5.00.00 PM 12/24/2020 12:36:00 PM TCLP Mercury Analysis (SW1311/74712/22/2020 5:00:00 PM 12/28/2020 9:40:00 AM 12/28/2020 4:18.00 PM TCLP Metals Analysis (SW 13l l/601412/22/2020 5:00!00 PM 12123/2020 12:25:00 P 12/23/2020 6:15:S3 PM TCLP Pesticides Analysis (SW1311/8f 12122/2020 5:00:00 PM 12/22/2020 12:00:00 P 12/23/2020 7:02:00 PM IR TCLP Pesticides Analysis (SW1311/8(12/22/2020 5:00:00 PM 12/22/2020 12:00.00 P 12/23/2020 7:02:00 PM a� TCLP Senni-Volatiies .Analysis 12/22/2020 5:00:00 PM 12/23/2020 12:00:00 P 12/23/2020 8:02:00 PM (5)W1311/8270) TCLP Volatiles Analysis 12/22/2020 5:00:00 PM 12/24/2020 9:58,00 AM Original Page 5 of 30 I SUMMIM,�_ PA1190NIAENTAL TECHN01 OWFS, Mr. A114lyflcal I aborarorles Srsi,jniirFtjviroltnleltialTeeltologie,Ic. 3310 Win Sr. Cityalraga Falls, Ohio 44223 TFG: (330) 253-8211 FAX.- (330) 253-4489 Websile: It1rn:14nvmse1rek.com Analytical Report (base report) WOM 20121123 Date Reported: 12/29/2020 CLIENT: Sytiagro Tag Number: Matrix: SLUDGE Collection Date; 12/17/2020 8:00:00 AM Lab ID: 20121 123-001A Project: OXFORD Client Sample ID OXFORD TCLP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: ERA TCLP MERCURY ANALYSIS (SW131117470) TCLP Mercury ND 0.00500 mglL 1 12128/20204:18:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP METALS ANALYSIS (SW131116010) TCLP Arsenic(As) ND TCLP Barium(Ba) ND TCLP Cadmlum(Cd) ND TCLP Chromium(Cr) ND TCLP Lead(Pb) ND TCLP Seienium(Se) ND TCLP Silver(Ag) ND RCI FLASHPOINT DETERMINATION (1010) Flashpoint (140°F) >140 SW6010D SW3010A Analyst: EAM 0.500 mglL 1 12/23/2020 6:15:53 PM 5.00 mg1L 1 12/23/2020 6:15:63 PM 0.100 mg/L 1 12/23/2020 6:15:53 PM 0.200 mglL 1 12/23/2020 6:15:53 PM 0.500 mglL 1 12/23/2020 6:15:53 PM 0.0500 mglL 1 12/23/2020 6:15:53 PM 0.500 mg1L 1 12/23/2020 6:15:63 PM SW1010 Analyst: TAH Z IF 1 12/22/2020 1:51:08 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 SW3510C Analyst: SFG TCLP SEMI-VOLATILES ANALYSIS (SW131118270) 1,4-Dichlorobenzene ND 0.200 mg1L 2 12/23/2020 8:02:00 PM 2,4,5-Trichlorophenol ND 0.500 mg1L 2 12/23/2020 8:02:00 PM 44,6-Trichlorophenol ND 0.500 mg1L 2 12/23/2020 8:02:00 PM 2,4-Dinitrotoluene ND 0.100 mg1L 2 12/23/2020 8:02:00 PM Cresols, Total ND 10.0 mglL 2 12/23/2020 8:02:00 PM Hexachloro-1,3-butadiene ND 0.0400 mg1L 2 12/23/2020 8:02:00 PM Hexachlorobenzene ND 0.100 mglL 2 12/23/2020 8:02:00 PM Hexachloroethane ND 0.200 mg1L 2 12/23/2020 8.02:00 PM Nilrobenzene ND 0.200 mglL 2 12/23/2020 8:02:00 PM Pentachlorophenol ND 0.500 mglL 2 12/23/2020 8:02:00 PM Pyridine ND 0.500 mglL 2 12/23/2020 8:02:00 PM Surr: 2-Fluorophenol 66.7 10 -157 m %Rec 2 12/23/2020 8:02:00 PM Sum Phenol-d6 68A 10 - 169 %Rec 2 12/23/2020 8:02:00 PM Surr: Nilrobenzene-0 83.8 32.1 -130 %Rec 2 12/23/2020 8:02:00 PM Qualifiers: B Analyte detected in the associated Mctlmd Blank 8 Value above quanIitation range 14 Holding firnes for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit, N Tentatively identified compounds ND Not Detected P Second column confirmation exceeds PL Pennit Lintit R RPD outside accepted recovery limits Original RL Reporting Detection Limit U Samples with CalcVal <MDL Page 6 of 30 u ,, SununitBnWronmentaiTechnologies,hte. I 3310 Win St. ENV1110NMENTAL TfCHN01 rIG"' : i':' CuyahogaFnlls, Ohio 44223 AriMytical t aboratorie­ TEL: (330) 253.8211 FAX: (330) 253-4489 Website: hyp:1Avwwse1tekcorn Analytical Report (base report) WO#: 20121123 Date Reported: 12/29/2020 CLIENT: Synagro Tag Number: Matt'ix: SLUDGE Collection Date: 12/17/2020 8:00:00 AM Lab ED: 20121 t23-001A Project: OXFORD Client Sample ID OXFORD TCLP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 SW3510C Analyst: SFG TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270) Surf: 2,4,6-Tribromophenol 106 45.4 - 166 %Rec 2 12/23/2020 8:02:00 PM Surf: 2-Fluorobiptienyl 94.7 35.7 - 130 %Rec 2 12123/2020 8:02:00 PM Surr: p-TerphenylA14 116 74.7 - 145 %Rec 2 12123/2020 8:02:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP PESTICIDES ANALYSIS (SW131118081) Chlordane, total ND Toxaphene ND Endrin ND gamma-BHC ND Heptachlor ND Heptachlor epoxide ND Methoxychlor ND Surr. TCMX 84.9 Surr: DCB 103 TCLP HERBICIDES BY EPA 8321B 2,4-D ND 2,4,5-TP ND Surr: 2,4-Dichlorophenylacetic aci 106 TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 1,2-Dichloroethane ND MEK ND Benzene ND Carbon tetrachloride ND Chlorobenzene ND Chloroform ND Tetrachloroethene ND SW8081 SW3510C Analyst: CSS 0.0250 mg1L 1 12123/2020 7:02:00 PM 0.0500 mg/L 1 12123/2020 7:02:00 PM 0.00250 mg/L 1 12123/2020 7:02:00 PM 0.00250 mg1L 1 12123/2020 7:02:00 PM 0.00250 mglL 1 12123/2020 7:02:00 PM 0.00250 mg/L 1 12123/2020 7:02:00 PM 0.00250 mg[L 1 12123/2020 7:02:00 PM 10 - 119 %Rec 1 12123/2020 7:02:00 PM 10 - 119 %Rec 1 12/23/2020 7:02:00 PM SW8321A SW1311M Analyst: TM 1.00 mg/L 100 12124/2020 12:36:00 PM 1.00 mg/L 100 12/24/2020 12:36:00 PM 70 - 130 %Rec 100 12124/2020 12:36:00 PM SW8260 SW1311 M Analyst: SLV 0.250 mg]L 50 12124/2020 9:58:00 AM 0.250 mg1L 50 1D2412020 9:58:00 AM 5.00 mg/L 50 12/24/2020 9:58:00 AM 0.260 mg/L 50 12/24/2020 9:58:00 AM 0.250 mg/L 50 12/24/2020 9:58:00 AM 2.50 mg/L 50 12124/2020 9:58:00 AM 0.250 mg]L 50 12/24/2020 9:68:00 AM 0,250 mg1L 50 12124/2020 9:58:00 AM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. NI) Not Detected PL Pennit Limit RL Reporting Detection Limit E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds P Second column confirmation exceeds R RPD outside accepted recovery limits Original U Samples with CalcVal < MDL Paqe 7 of 30 � sumu— Sunrurrt EnvirOttnre�eta/Technologies, Inc. -, £NVIR01164ENTAC TfCht1(1l.0r.!F%, }..; 3310 IYin St. Analytical Report fi""'j;'t '3!l�rborntarivs rtrC Crryahaga Fads, Ohio 44223 TEL: (330) 253-8211 FAX- (330) 253-4489 (baserclwrt) lVehsite: h0:1Avrvty.settek c0m W0#: 20121123 Date Reported: 12129/2024 CLIENT: 5yllagro _ _ Matrix: SLUDGE Tag Number: Lab ID: 20121123-001A Collection Date: 12/17/2020 8:00:00 AM Project: OXFORD Client Sample ID OXFORD TCLP Analyses _ ——— Result ————— —--—— RL Qua] Units —— — —- Dr Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS SW8260 SW1311M Analyst: SLV Trichloroethene Vinyl chloride ND 0.250 m91L 50 12/24/2020 9:58:00 AM Surr: 4-Sramofluorobenzene ND 94.6 0.100 mg/L 50 12/24/2020 9:58:00 AM Sum Dibrom0flummethane 101 70 - 130 %Rec 70 130 50 12/24/2020 9:58:00 AM Surf; Toluene-d8 99.7 - %Rec 70 - 130 50 12/24/2020 9:58:00 AM %Rec 50 12/2412020 9:58:00 AM RCI REACTIVE CYANIDE (901417.3.3.2)-SOLID SW9014 Analyst: MS Cyanide, Reactive ND 0.485 mg/Kg 1 12/21/2020 2:38:00 PM RCI PH (SW9045D) SW9045D Analyst VVK pH 7.2 s.u.@20.2C 1 12/22/2020 11:31:06 AM RCI REACTIVE SULFIDE (9034)17.3.4.2 SW9034 Analyst: MS Sulfide, Reactive ND 25.0 mg/Kg 1 12/21/2020 2:38:00 PM Qualifiers: B Aualyte detected in the associated Method Blank E Value above quantitalion range H MC Holding times forprcparation or analysis cxcceded Value is below Minimum Compound Limit. M Manual Integration used to determine arty response ND Not Detected N Tentatively identified compounds PL Permit Limit P Second colunm conrimultion escceds RL Reporting Detection Limit R RPD outside accepted recovery limits Original U Samples with CaleVal <MDL Parip R of qn f SUMM11, - Srrnrnrit Enviroaurrental Technologies, r„G. Accreditation Program 3310 Win St.Anal tes Report p EPtVtflptilhENi'At_ TEGHHOInr ' ;, In,'CuyalrogaFalls, Ohio 44223 23 J . - 1? n7tytleal lah,u,�fc"1c TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 20121123 Website. http://unvivsettek.com 29 Dec 20 Client: Synagro State: NW Project: OXFORD Program Name: NC_WW SCM Sample ID Matrix Test Name Analyte Status 20121123-OOIA Sludge Flashpoint Detennination (1010) Flashpoint (140°F) U Sludge pH (SW9045D) Hydrogen Ion (pH) A Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive N Sludge Reactive Sulfide (9034y7.3.4.2 Sulfide, Reactive N Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A Sludge TCLP Herbicides by EPA 8321B 2,4-D A Sludge TCLP Mercury Analysis (SW1311/7470) Mercury A Sludge TCLP Metals Analysis (SW 1311/6010) Arsenic A Sludge TCLP Metals Analysis (SW 1311/6010) Barium A Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A Sludge TCLP Metals Analysis (SW1311/6010) Chromium A Sludge TCLP Metals Analysis (SW1311/6010) Lead A Sludge TCLP Metals Analysis (SW 131116010) Selenium A Sludge TCLP Metals Analysis (SW 1311/6010) Silver A Sludge TCLP Pesticides Analysis (SWI311/8081) Chlordane, lotal A Sludge TCLP Pesticides Analysis (SW1311/8081) 8ndrin A Sludge TCLP Pesticides Analysis (SW131118081) gamma-BHC A Sludge TCLP Pesticides Analysis (SW[311/8081) Heptachlor A Sludge TCLP Pesticides Analysis (SW131118081) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (SW1311/8081) Melhoxychlor A Sludge TCLP Pesticides Analysis (SW 1311/8081) Toxaphene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,5-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4,6-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 2,4-Dinitrololuene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Cresols, Total A Sludge TCLP Semi-Volatiles Analysis (SW131118270) Hexachlorobenzene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A Sludge TCLP Semi-Volatiles Analysis (SW131118270) Hexachloroetltane A Sludge TCLP Semi-Volatiles Analysis (SW1311I8270) Nitrobenzene A Sludge TCLP Seri-Volatiles Analysis (SW1311/9270) Pentachlorophenol A Sludge TCLP Semi-Volatiles Analysis (SWt31118270) Pyridine A Key Key key NC WW SCM A Accredited NC WW SCM N Not Accredited NC WW SCM U Unavailabl Original #1 Paae 9 of 30 ( Srrmmil Environmental Technologies, i St. l 3310 fl'i�r S1. Lu SUMMIT, Cay�alrogaFalls 01do44223 tlraalytlaal tvborvroriot, TEL: (330) 253-8211 rAX. (330) 253-4489 Websire. 1,11v:1Avnay.settek c0m Accreditation Program Alla1 teS Report Y p WO#: 20121123 29-Dec-20 Client: Synagro State: NW Project: OXFORD Program Name: NG WW SCM Sample ID Matrix Test Name Analyte Status 20121123-OOIA Sludge TCLP Volatiles Analysis I,1-Dichloroethene A Sludge TCLP Volatiles Analysis 1,2-Dichloroethnne A Sludge TCLP Volati les Analysis 2-Butanone A Sludge TCLP Volatiles Analysis Benzene A Sludge 'TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volaliles Analysis Chlombenzenc A Sludge TCLP Volatiles Analysis Chloroform A Sludge TCLP Volatiles Analysis Teirachloroethene A Sludge TCLP Volatiles Analysis Trichlorectlrene A Sludge TCLP Volatiles Analysis Vinyl chloride A Key Key NC_W%V SCM A Accredited NC_WW SCM N Not Accredited Key NC WW SCM U Uuavailab] Original #1 Page 10 of 30 VMM II Summit Environmental Technologies, Inc.S 3310 Win St. r �� SUMMARY J Y REPORT ENVIA0NMENi4L TCCHN0L0 MES - Cuyahoga Falls, Ohio 44223 Analyrlcal Laboraror�,-s TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 20121123 Website: httn:/frovwrv.settek.com 29-Dec-20 Client: Synagro Project: OXFORD BatchED: 46992 'ample ID: ME-46992 SampType: MBLK TestCode: TCLP-VOC-M Units: mg1L Prep Date: 12/22/2020 RunNo: 121812 ;lient ID: PBS Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12/2412020 SegNo: 3134102 �nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 11,1-Dichloroethene ND 0.250 1,2-Dichioroethane ND 0.250 MEK ND 5,00 Benzene ND 0.250 Carbon tetrachloride ND 0.250 Chlorobenzene ND 2.50 Chloroform ND 0.250 Tetrachloroethene ND 0.250 Trichloroethene ND 0.250 Vinyl chloride ND 0.100 Surr: 4-Bromofluorobenzene 2400 Surr: Dibromofluoromethane 2510 Surr: Toluene-d8 2480 2500 96.0 70 130 2500 100 70 130 2500 99.2 70 130 Sample ID: LCS-46992 SampType: LCS TestCode: TCLP-VOC-M Units: mglL Prep Date: RunNo: 121812 client ID: LCSS Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12124/2020 SegNo: 3134103 \nalyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.986 0.250 1.00 0 98.6 64.7 136 1,2-Dichloroethane 0.930 0.250 1.00 0 93.0 70 130 MEK ND 5.00 5.00 0 92.1 55.1 149 Benzene 0.954 0.250 1.00 0 95.4 70 130 Qaatifiers: 13 Analyte detected in the associated Method Blank E Value above quantitation range H Holding times For preparation or anal; J Analyte detected below quantitation limits M Manual integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S. Spike Recove ry ery outside accepted reco Page 11 of 30 T summ- Summit Environmental Technologies, Inc. 3310WinSr. QC SUMMARY REPORT EKVMONMENTALTCCHNOLOC�__ -' Cuyahoga Fulls, Ohio 44223 Rra81l1Uca! Lab_^ !^�:c TEL: (330) 253-8211 PAX. (330) 253-4489 W04: 20121123 Websire: htfi:/Avww.settek.com 24 Dec-20 Client: Synagro Project: OXFORD BatchED: 46992 Sample ID: LCS-46992 SampType: LCS TestCode: TCLP-VOC-M Units: mglL Prep Date: RunNo: 121812 Client 1D: LCSS Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12/24/2020 SegNo: 3134103 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Carbon tetrachloride 1.06 0.250 1.00 0 106 70 130 Chlorobenzene ND 2.50 1.00 0 98.9 70 130 Chloroform 0.987 0.250 1.00 0 98.7 70 130 Tetrachloroethene 0.984 0.250 1.00 0 98.4 70 134 Trichloroethene 0.972 0.250 1.00 0 97.2 62.8 160 Vinyl chloride 1.10 0.100 1.00 0 110 67.1 130 Surr:4-Bromofluorobenzene 2500 2500 100 70 130 Surr: Dibromofluoromethane 2540 2500 102 70 130 Surr: Toluene-d8 2510 2500 100 70 130 Sample ID: 20121123-001AMS SampType: MS TestCode: TCLP-VOC-M Units: mglL Prep Date: RunNo: 121812 Client ID: OXFORD TCLP Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12124/2020 SegNo: 3134111 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene 0.946 0.250 1.00 0 94.6 13.6 202 1,2-Dichloroethane 0.896 0.250 1.00 0 89.6 55.7 138 MEK ND 5.00 5.00 0 90.8 65.3 118 Benzene 0.932 0.250 1.00 0 93.2 49.2 145 Carbon tetrachloride 1.05 0.250 1,00 0 105 26.7 156 Chlorobenzene ND 2.50 1.00 0 95.6 33.7 159 Chloroform 0.957 0,250 1.00 0 95.7 48.5 145 Tetrachloroethene 0.936 0.250 1.00 0 93.6 19.2 191 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times For preparation or analt 7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 12 of 30 91 3310Win St. SUMMIT Summit EnvironmenSal Technologies,in St. QC SUMMARY REPORT ENVIRONMENTALTECHNOt-OGt£S, =r; - Cuyahoga Falls, Ohio 44223 Ar[atyricaf Lobo•srori&S TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 20121123 Website: htan://www.se[tek.com 29-Dec-20 Client: Synagro Project: OXFORD BatchID: 46992 Sample 1D: 20121123-001AMS SampType: MS TestCode: TCLP VOC-M Units: mg1L Prep Date: RunNo: 121812 Client ID: OXFORD TCLP Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12124/2020 SegNo: 3134111 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Trichloroethene 0.953 0.250 1.00 0 95.3 38.4 167 Vinyl chloride 1.12 0.100 1.00 0 112 27.3 161 Surr:4-Bromofluorobenzene 2510 2500 100 70 130 Surr: Dibromofluoromethane 2540 2500 102 70 130 Surr: Toluene-d8 2510 2500 101 70 130 Sample ID: 20121123-ODIAMSD SampType: MSD TestCode: TCLP-VOC-M Units: mglL Prep Date: RunNo: 121812 Client 0: OXFORD TCLP Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12124I2020 SegNo: 3134112 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 1,1-Dichloroethene 0.983 0.250 1.00 0 98.2 13.6 202 0.946 3.79 25 1,2-Dichloroethane 0.944 0,250 1.00 0 94.4 55.7 138 0.896 5.22 25 MEK ND 5.00 5.00 0 97.4 65.3 130 0 0 25 Benzene 0,975 0.250 1.00 0 97.5 49.2 145 0.932 4.51 25 Carbon tetrachloride 1.07 0.250 1.00 0 107 26.7 156 1.05 1.98 25 Chlorobenzene ND 2.50 1.00 0 98.9 33.7 159 0 0 25 Chloroform 0.995 0.250 1.00 0 99.5 48.5 145 0.957 3.89 25 Tetrachloroethene 0.976 0.250 1.00 0 97.6 19.2 191 0.936 4.08 25 Trichloroethene 0.974 0.250 1.00 0 97.4 38.4 167 0.953 2.18 25 Vinyl chloride 1.15 0.100 1.00 0 115 27.3 161 1.12 2.91 25 Surr:4-Bromofluorobenzene 2490 2500 99.7 70 130 0 25 Surr: Dibromofluoromethane 2570 2500 103 70 130 0 25 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anaLv J Analyte detected below quantization limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 13 of 30 ffJ l! 7rR _ Summit Environmental Technologies, Inc. - 3370 Win St. QC SUMMARY REPORT ENVIFI0f4M XTAL TEC- %Z� L _: , : , Cuyahoga Falls, Ohio 44223 TEL: (330) 153-821I Fill:- (330) 253-4489 WO#: 20121123 Website: httn:11www.setrek_com 29 Dec-2D Client: Synago Project: OXFORD BatchlD: 46992 Sample ID: 20121123-001AMSD SampType: MSD TestCode: TCLP VOC-M Units: mglL Prep Date: RunNo: 121812 Client ID: OXFORD TCLP Batch ID: 46992 TestNo: SW8260 SW1311M Analysis Date: 12124/2020 SegNo: 3134112 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Surr: Toluene-d8 2540 Qualifiers: B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits 2500 102 70 130 0 25 E Value above quantitation range H Holding times for preparation or anah M Manual Integration used to detertnine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Permit Limit RL Reporting Detection Limit S Spike Recovery outside accepted reco Original Page 14 of 30 smpw._ _ Summit Environmental Technologies, lnc. __331oWinSt.QC SUMMARY REPORT ENYtROCuyahoga Falls, Ohio 44223 - - TEL: (330) 2534211 FAY' (330) 253-4489 WO##: 20121123 Wehsite: h :/1ww wsertek c m 29 Dec-20 Client: Synagro Project: OXFORD Sample ID: 20121280-001AMS SampType: MS TestCode: SVOC-BNA T Units: m91L Client ID: SatchQC Batch ID: 46996 TestNo: SW8270 SW3510C Analyte 1,4-Dichlorobenzene 2,4, 5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dinitrotoluene o-Cresol Cresols, Total Hexachloro-1,3-butadiene Hexachlorobenzene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine Surr: 2-Fluorophenol Surr: Phenol-d6 Surr: Nitrobenzene-d5 Surr: 2,4,6-Tribromophenol Surr: 2-FI uorobiphenyl Surr: p-Terphenyl-d14 Result PQL SPK value SPK Ref Val SatchED: Prep Date: 12/23/2020 Analysis Date: 12/24/2020 %REC LowLimit HighUrnit RPD Ref Val 0.517 0.8000 64.7 33.8 126 0.788 0.8000 98.5 28.7 144 0.771 0.8000 96.4 12,8 153 0-752 0.8000 0 94.0 20.4 155 0.620 0.8000 77.5 10 148 ND 1.600 78.0 10 148 0.532 0.8000 66.5 29 130 0.715 0.8000 89.4 33.7 134 0.467 0.8000 58.4 32.8 132 0.563 0.8000 0 70.4 20 158 0.771 0.8000 96.4 10 176 ND 0.8000 28.7 10 130 0.704 1.000 70.4 3.39 130 0.814 1.000 81.4 5 130 0.730 1.000 73.0 14.5 154 1.01 1.000 101 19.5 130 0.846 1.000 84.6 34.4 130 1.10 1.000 110 8.86 156 0,200 0.500 0.500 0.100 0.500 10.0 0.0400 0.100 0.200 0.200 o.5ao 0.500 Qualifiers: 13 Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted mcovery limits 0 0 0 0 D 0 0 0 0 4 E Value above quantitation range M Manual Integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit 46996 RunNo: 121831 SegNo: 3134706 %RPD RPDLimit Qua[ H Holding times for preparation or anal MC Value is below Minimum Compound PL Permit Limit S Spike Recovery outside accepted reco mQCf Original Page 15 of 30 0,200 0.500 0.500 0.100 0.500 10.0 0.0400 0.100 0.200 0.200 o.5ao 0.500 Qualifiers: 13 Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted mcovery limits 0 0 0 0 D 0 0 0 0 4 E Value above quantitation range M Manual Integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit 46996 RunNo: 121831 SegNo: 3134706 %RPD RPDLimit Qua[ H Holding times for preparation or anal MC Value is below Minimum Compound PL Permit Limit S Spike Recovery outside accepted reco mQCf Original Page 15 of 30 .Summit Environmental7'echnpfogies, Inc. QC SUMMARY REPORT SUMOW6- 3310 Win St, ENVIRONMENTALTECHNOLCf,, 't- ` Cuyahoga Falls, Ohio 44223 Ar7aly0ca1 Laborato"s TEL: (330) 253-8211,F'AX.• (330) 253-4489 WO#: 20121123 Website: http:llwww.sertekcom 29-Dec-20 Chent: Synagro Project: OXFORD BatchID: 46996 Sample ID: 20121280-001AMSD SampType: MSD TestCode: SVOC-BNA T Units: mg1L Prep Date: 12/2312020 RunNo: 121831 Client ID: Batch= Batch ID: 46996 TestNo: SW8270 SW3510C Analysis Date: 12/24/2020 SegNo: 3134707 Ana[yte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ 1,4-Dichlorobenzene 0.635 0.200 0.8000 0 79.4 33.8 126 0.5172 20.5 30 2,4,5-Trichlorophenol 0.870 0,500 0.8000 0 109 28.7 144 0.7880 9.89 30 2,4,6-Trichlorophenol 0,877 0.500 0.8000 0 110 12.8 153 0.7708 12.9 30 2,4-Dinitrotoluene 0.825 0.100 0.8000 0 103 20.4 155 0.7520 9.28 30 o-Cresol 0.738 0.500 0.8000 0 92.2 10 148 0.6200 17.4 30 Cresols, Total NO 10.0 1.600 0 92.3 10 148 0 0 30 Hexachloro-1,3-butadiene 0.648 0.0400 0.8000 0 81.0 29 130 0.5320 19.7 30 Hexachlorobenzene 0.776 0.100 0.8000 0 97.0 33.7 134 0.7152 8.10 30 Hexachloroethane 0.584 0.200 0.8000 0 73.0 32.8 132 0.4672 22.2 30 Nitrobenzene 0.672 0.200 0.8000 0 84.0 20 158 0.5632 17.6 30 Pentachlorophenol 0,827 0.500 0.8000 0 103 10 176 0.7708 7.01 30 Pyridine NO 0,500 0.8000 0 35.4 10 130 0 0 30 mQC+ Surr:2-Fluorophenol 0,870 1.000 87.0 3.39 130 0 Sum Phenol-d6 0.978 1.000 97.8 10 130 0 Surr: Nitrobenzene-d5 0.870 1.000 87.0 14.5 154 0 Surr: 2,4,6-Tribromophenol 1.11 1.000 111 19.5 130 0 Surr:2-Fluorobiphenyl 0.932 1,000 93.2 34.4 130 0 Surr: p-Terphenyl-dl4 1.23 1.000 123 8.86 156 0 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal] 7 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Otiginal R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 16 of 30 V mm k�,�-�S�_ Summit Environmental Technologies, Inc. 3310 tin St. QC SUMMARY REPORT £N:VIRONMENTAL TECHNOLOGi"� Awiyiical Cuyahoga Falls. Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 20121123 Website: htt :1Avww.venek. m 29-Dec-20 Client: Synagr o Project: OXFORD BatchID: 46996 Sample ID: MB-46996 SampType: MBLK TestCode: SVOC-BNA T Units: mglL Prep Date: 12123/2020 RunNo: 121785 Client ID: PBS Batch 1D: 46996 TestNo: SW8270 SW3510C Analysis Date: 1212312020 SegNc: 3133120 Analyte Result POL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzene NO 0.100 2,4,5-Trichlorophenol NO 0.250 2,4,6-Trichlorophenol ND 0.250 2,4-Dinitrotoluene ND 0.0500 o-Cresol ND 0.250 Cresols, Total ND 5.00 Hexachloro-1,3-buta6ene NO 0.0200 Hexachlorobenzene NO 0.0500 Hexachloroethane NO 0.100 Nitrobenzene NO 0.100 Pentachlorophenol NO 0.250 Pyridine NO 0.250 Surr. 2-Fiuorophenol 0.764 1,000 76.4 10 130 Surr: Phenol-d6 0.729 1.000 72.9 10 130 Surr: Nitrobenzene-d5 0.761 1.000 76.1 19 130 Surr: 2,4,6-Tribromophenol 0.852 1.000 85.2 10 130 Surn 2-Fluorobiphenyl 0.840 1.000 84.0 22 130 Surr: p-Terphenyl-d14 1.03 1.000 103 34 130 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H HoIding times for preparation or ands J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 17 of 30 r0-1� Summit Environmental Technologies, Inc. UMJV___ ___ ;d 3310Win St. QC SUMMARY REPORT ENVIRONMENTAL ^-1!J0! - CuyahogaFafls, Ohio44223 %�":'' = = "- - TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 20121123 Website: htt1,.L1Www.settek,com 29-Dec-20 Client: Synagro Project: OXFORD Sample ID: LCS- 46996 SampType: LCS TestCode: SVOC-BNA T Units: mg1L Client ID: LCSS Batch ID: 46996 TestNo: SW8270 SW3510C Analyte Result PQL SPK value SPK Ref Val BatchlD: 46996 Prep Date: 12/23/2020 RunNo: 121785 Analysis Date: 12/23/2020 SegNc: 3133121 %REC Lowl-imit Highl-imit RPD Ref Val 1,4-Dichlorobenzene 0.576 0.100 0.8000 0 72.0 36.4 130 2.4,5-Trichlorophenol 0.689 0.250 0.8000 0 86.2 31.7 132 2,4,6-Trichlorophenol 0.681 0,250 0.8000 0 85.1 31.1 133 2,4-Dinitrotoluene 0.703 0.0500 0.8000 0 87.9 43.3 130 o-Cresol 0.642 0.250 0.8000 0 80.2 32.9 130 Cresols, Total ND 5.00 1.600 0 81.5 31.7 130 Hexachloro-1,3-butadiene 0.560 0.0200 0.8000 0 70.0 31.4 130 Hexachlorobenzene 0.717 0.0500 0.8000 0 89.7 43.1 130 Hexachloroethane 0.553 0.100 0.8000 0 69.1 36.5 130 Nitrobenzene 0.636 0.100 0.8000 0 79.5 39.5 130 Pentachlorophenol 0.791 0.250 0.8000 0 98.9 34 130 Pyridine ND 0.250 0.8000 0 21.6 10 130 Surr: 2-Fiuorophenol 0.779 1.000 77,9 17.1 130 Surr: Phenol-d6 0.744 1.000 74A 10 130 Surr: Nitrobenzene-d5 0.724 1.000 72.4 32.6 130 Surr:2,4,6-Tribromophenol 0.945 1.000 94.5 4.43 130 Surr:2-Fluorobiphenyl 0.818 1.000 81.8 41.8 130 Surr: p-Terphenyl-d14 1.08 1.000 108 36.4 130 Qualifiers: B Analyte detected in the associated Method Blank J Analyte detected below quamitation limits ND Not Detected R RPD outside accepted recovery limits %RPD RPDLim[t Qua[ E Value above quantitation range H Holding times For preparation or anal! M Manual Integration used to determine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Permit Limit RL Reporting Detection Limit S Spike Recovery outside accepted reco m Original Page 18 of 30 Summit Environmental Technologies, Inc. 3310 Win St, E nsh, c,?i d rqt TEt:tl at aGtEr. Cuyahoga Falls, Ohio 44223 Arra+i�rlcat LaL+oratortc�.s _ TEL: (330) 253-8211 FAX..- (330) 253-4489 Websire: h ://wwtiv.settelc m Client: Synago Project: OXFORD Sample ID: MS-47029 Client ID: PBS Analyte TCLP Mercury Sample ID: LCS-47029 Client ID: LCSS Analyte TCLP Mercury Sample ID: 20121404-001AMS Client ID: BatchQC Analyte TCLP Mercury SampType: MBLK Batch10: 47029 Result ND SampType: LCS Batch ID: 47029 Result 0.00389 SampType: MS Batch ID: 47029 Result 0.00389 Sample ID: 20121404-001AMSD SampType: MSD Client ID: gatchQC Batch ID: 47029 Analyte Result TCLP Mercury 0.00395 TestCode: HG_TCLP(74 Units: PpM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 TestCode: HG_TCLP(74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 0,00400 0 TestCode: HG_TCLP(74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 0.00400 0 TestCode: HG TCLP(74 Units: PpM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 0.00400 0 Qualifiers: B Analytc detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits QC SUMMARY REPORT WO#: 20121123 29 Dee-20 BatchED: 47029 Prep Date: 12/28/2020 RunNo: 121864 Analysis Date: 12/28/2020 SegNo: 3135860 %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Prep Date: 12/28/2020 Analysis Date: 12/28/2020 %REC Lowl-imit HighLimit RPD Ref Val 97.2 80 120 Prep Date: 12/28/2020 Analysis Date: 12/28/2020 %REC Lowl-imit HighLimit RPD Ref Val 97.2 75 125 Prep Date: 12/28/2020 Analysis Date: 12/28/2020 %REC LowLimit HighLimit RPD Ref Val 98•8 75 125 0.00389 E Value above quantitation range M Manual Integration used to determine area response P Second column conf=ation exceeds R.L. Reporting Detection Limit RunNo: 121864 SegNo: 3135861 %RPD RPDLimit Qual RunNo: 121864 SegNo: 3135863 %RPD RPDLimit Qual RunNo: 121864 SegNo: 3135864 %RPD RPDLimit Qual 1.53 20 H Holding times for preparation or anal, MC Value is below Minimum Compound PL Permit Limit S Spike Recovery outside accepted reco Original Page 19 of 30 Ezzmoplsummr- SumrniiEnvironmental Technologies, St, 3310 Win St. QC SUMMARY REPORT L. ENVIR0?4MI5NTAL'rEC"':f-' ^. ,'�S, .'—IJ A�Ta"cof Laboraft. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 WOE: 20121123 Website: http;//www..gettek.com 29-Dec-20 Client: Synagro Project: OXFORD SatchlD: 47029 Sample ID: 20121404-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 12/28/2020 RunNo: 121864 Client ID: Batch QC Batch ID: 47029 TestNo: SW7470A SW7470A Analysis Date: 1212812020 SegNo: 3135864 Analyte Result PQL SPK value SPK Ref Val %REC Lowiimit HighLimit RPD Ref Val %RPD RPDLimit Qual Sample ID: TCLP Blankl 12-21- SampType: MBLK Client ID: PBS Batch ID: 47029 Analyte TCLP Mercury Result ND Sample ID: TCLP Blankl 12-22- SampType: MBLK Client ID: PBS Batch ID: 47029 Analyte TCLP Mercury Result ND Sample ID: TCLP Blankl 12-22- SampType: MBLK Client ID: PBS Batch ID: 47029 Analyte TCLP Mercury Result ND TestCode: HG_TCLP(74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 TestCode: HG TCLP(74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0.00200 TestCode: HG_TCLP(74 Units: PPM TestNo: SW7470A SW7470A PQL SPK value SPK Ref Val 0,00200 Qualifiers: S Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits Prep Date: 12/28/2020 Analysis Date: 12/28/2020 %REC Lowl-imit HighLimit RPD Ref Val Prep Date: 12128=20 Analysis Date: 12/28/2020 %REC Lowl-imit HighLimit RPD Ref Val Prep Date: 12/28/2020 Analysis Date: 12/28/2020 %REC Lowl-imit HighLimit RPD Ref Val RunNo: 121864 SegNo: 3135968 %RPD RPDLimit Qual RunNo: 121864 SegNo: 3135969 %RPD RPDLimit Qua] RunNo: 121864 SegNo: 3135970 %RPD RPDLimit Qual E Value above quantitation range H Holding times for preparation or anal, M Manual Integration used to determine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Permit Limit RL Reporting Detection Limit S Spike Recovery outside accepted reco Original Page 20 of 30 Summit Environmental Technologies, Inc. 3310 Win Sr.SU SUMMARY QC REPORT \L ENVIRONMENTAL TEC, A77alyrico ='" ^' Cuyahoga Falls, Ohio 44223 TEL: (330) 2534211 FAX.- (330) 253-4489 WO#: 20121123 Website: htm:11www., e&k,gom 29-Dec-20 Client: Synab o Project: OXFORD BatchID: R121658 Sample ID: CHECK 7 SampType: LCS TestCode: pH_S(9045D) Units: s.u.@20.6C Prep Date: RunNo: 121658 Client ID: LCSS Batch ID: R121658 TestNo: SW9045D Analysis Date, 12/22/2020 SegNo: 3129603 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDUmit Qual pH 7.0 7.0 0 101 90 110 Quali£ers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal, 7 Analyte detected below quantitation limits M Manual fntearation used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 21 of 30 P411 Summr Summit Errvironmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT Cuyahoga Falls, Ohio 44223 A yalyr;CaJ 1 �bar�lortc. TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 20121123 Website: http:/1yLtpv,senek.co7n 29-Dec-20 Client: Synagro Project: OXFORD BatchED: R121658 Sample ID: 20121292-001ADUP SampType: DUP TestCode: pH_Oil(9045D Units: s.u.@20-3C Prep Date: Client ID: SatchQC Batch ID: R121658 TestNo: SW9045D Analysis Date: 12/22/2020 Analyte pH Result PQL SPK value SPK Ref Val 6.5 0 %REC LowLimit HighLimit RPD Ref Val 0 6.5 RunNo: 121658 SegNo: 3129871 %RPD RPDLimit 0.3 10 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Qual Original Page 22 of 30 SU MM l Summit Environmental Technologies, Inc. QC SUMMARY REPORT 3.�10 Win St. _ ENVIRONMENTALTECt1HOLO0!-- Cuyahoga Falls, Ohio 44223 Anatyticaf Laboratories TEL: (330) 253-8211 FAX- (330) 253-4489 WO#: 20121123 1T'ebsite: httn:1/wwwsettek.com 29-Dec-10 Client: Synagro Project- OXFORD SatchED: R121658 Sample ID: LCS-R121658 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@20.9C Prep Date: RunNo: 121658 Client ID: LCSW Batch ID: R121658 TestNo: SW9045D Analysis Date: 12/2212020 SegNo: 3129592 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual PH 7.0 7.0 0 100 98.6 101.4 Sample ID: 20121133-001DDUP SampType: DUP TestCode: pH_NPW(450 Units: s.u.@20.3C Prep Date: RunNo: 121658 Client 1D: BatchQC Batch ID: R121658 TestNo: SW9045D Analysis Date: 1212212020 SegNo: 3129594 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual PH 6.9 7.0 0.3 5 H Sample ID: CHECK 7 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@20.4C Prep Date: RunNo: 121658 Client 1D: LCSW Batch ID: R121658 TestNo: SW9045D Analysis Date: 12/2212020 SegNo: 3129878 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual PH 7.0 7.0 0 101 98.6 101.4 Qualifiers: B Analyte detected in the associated Method Blank J Analyte detected below quantization limits ND Not Detected R RPD outside accepted recovery limits E Value above quantitation range H Holding times for preparation or anal; M Manual Integration used to determine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Permit Limit RL Reporting Detection Limit S Spike Recovery outside accepted reco Original Page 23 of 30 Summit Envirpnmental Technologies, Itta sm"11-3310 Win St. EtiYIROEC. C oho a F r4narytfeal Labar�Farses u 8 alls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Websfte: htn7,y1W nv..aettek com Client: Synagro Project: OXFORD Sample ID: LCS-R121667 Client 10: LCSS Analyte !`lashpoint (140T) QC SUMMARY REPORT WO#: 20121.123 29-Dec-20 BatchED: R121667 SaMPType: LCS TestCode: FlashPt_S(10 Units: °F Prep Date: RunNo: 121667 Batch ID.-R12166T iestNo: SW1010 Analysis Date: 12/22/2020 SegNo: 3129396 Result PQL 5PK value 5PK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 139 140.8 0 98.7 98 102 2 Qualifiers: B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area .response P Second column confirmation exceeds RL Reporting Detection Limit H Holding times for preparation or anal, MC Value is below Minimum Compound PL Permit Limit S Spike Recovery outside accepted reco Original Page 24 of 30 u MW Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT ENVIRO?IIJENTgL T$CMUOI,C . Cuyahoga Falls, Ohio 44223 ��at;" ' ;aboretaries TEL: (330) 253-8.211 FAX.- (330) 253-4489 WO#: 20121123 Website: hM:IAw ,settekeom 29-Dec-20 Client: Synagro Project: OXFORD BatchID: R121675 Sample ID: MB-R121675 SampType: MBLK TestCode: Sulflde,React Units: mg/Kg Prep Date: RunNo: 121675 Client ID: PBS Batch 10: R121675 TestNo: SW9034 Analysis Date: 12/2112020 SegNo: 3129617 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive ND 25.0 Sample ID: LCS-R121675 SampType: LCS TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 121675 Client ID: LCSS Batch ID: R121675 TestNo: SW9034 Analysis Date: 12/21/2020 SegNo: 3129618 Analyte Result PQL SPK value SPK Ref Val %REC Lowl.imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 3020 25.0 3080 0 98.1 85 115 Sample ID: 20121170-OOIAMS SampType: MS TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 121675 Client ID: BatchQC Batch ID: R121675 TestNo: SW9034 Analysis Date: 12/21/2020 SegNo: 3129629 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 2980 25.0 3080 0 96.8 80 120 Sample ID: 20121170-001AMSD SampType: MSD TestCode: Sulfide,React Units: mglKg Prep Date: RunNo: 121675 Client ID: BatchOC Batch ID: R121675 TestNo: SW9034 Analysis Date: 12/21/2020 SegNo: 3129630 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 2860 25.0 3080 0 92.9 80 120 2980 4.11 30 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times For preparation or analN J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Orr -final R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 25 of 30 SummiSummit t Environmental Technologies, Inc. 3310 Win St. SUMMARY SUMMARY1SUMMARY REPORT ENVIRONMENTALTEGHNOLOGIES. : . Cuyahoga Falls, Ohio44223 tl patytical l.,aporatar r,,s TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 20121123 Website: http://wv n .senek.com 29-Dec-20 Client: Synagro Project: OXFORD BatchID: R121675 Sample ID: 20121170-001AMSD SampType: MSD TestCode: Sulfide,React Units: mg/Kg Client ID: SatchOC Batch 1D: R121675 TestNo: SW9034 Analyte Result PQL SPK value SPK Ref Val Qualifiers: B Analyte detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits Prep Date: Analysis Date: 12121/2020 %REC Lowl-imit HighLimit RPD Ref Val RunNo: 121675 SegNo: 3129630 %RPD RPDLimit Qual E Value above quantitation range H Bolding times for preparation or anall M Manual Integration used to determine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Permit Limit RL Reporting Detection Limit S Spike Recovery outside accepted reco Original Page 26 of 30 Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT 7ZG:;.%CoL - Cuyahoga Falls, Ohio44223 ., Anadyticc! L5^.n'a WO#: 20121123 TEL (330) 253-8211 F.4X {334) 253 4489 Website: h""11Wwrv.seaek.c0m 29-Der-20 Client: Synae o Project: OXFORD BatchED: R121688 nple ID: Blank SampType: MBLK TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 121688 !nt ID: PBS Batch ID: R121688 TestNo: SW9014 Analysis Date: 12/21/2020 SegNo: 3129958 Ilyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua Cyanide, Reactive ND 0.500 Sample ID: LCS SampType: LCS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 121688 Client ID: LCSS Batch ID: R121688 TestNo: SW9014 Analysis Date: 12/21/2020 SegNo: 3129959 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 9.43 0.500 10.00 0 94.3 85 115 Sample ID: RLCheck SampType: RLC TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo, 121688 Client ID: Batch= Batch ID: R121688 TestNo: SW9014 Analysis Date: 12/2112020 SegNo: 3129961 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Cyanide, Reactive 0.528 0.500 0.5000 0 106 65 135 Sample ID: 20121170-001AMS SampType: MS TestCode: Cyanide,Rea Units: mg1Kg Prep Date: RunNo: 121688 Client ID: Batch= Batch ID: R121688 TestNo: SW9014 Analysis Date: 12/21/2020 SegNo: 3129973 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive 8.71 0.472 10.00 0 87.1 75 125 Qualiifiers: B Analyte detected in the associated Method Blank 7 Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits E Value above quantitation range H Holding times for preparation or anah M Manual lnteg ation used to determine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Permit Limit RL Reporting Detection Limit S Spine Recovery outside accepted reco Original Page 27 of 30 summnSr<mmitEnvironmenIalTechnologies. Inc. SUMMARY REPORT - 3310 Win St. QC SU EN+flM0NMEN-rAL.rECHH0L0G�sS. *,^ Cuyahoga Falls, Ohio44223 Ar7alytical4hbarafarles 7E'L. (330) 253-8211 F.4X.• (330) 253-4489 WO#: 20121123 Website: http,-11w-w.settekco7n 29-Dec-20 Client: Synagr4 Project: OXFORD BatchID: R121688 Sample ID: 20121170-OOIAMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 121688 Client ID: BatchQC Batch 10: R121688 TestNo: SW9014 Analysis Date: 12/21/2020 SegNo: 3129973 Analyte Result PQL SPK value ' SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDL]mit Qua] Sample ID: 20121170-001AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 121688 Client ID: BatchQC Batch ID: R121688 TestNo: SW9014 Analysis Date: 12/21/2020 SegNo: 3129974 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Cyanide, Reactive 9.41 0.500 10.00 0 94.1 75 125 8.706 7.78 10 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anab .1 Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 28 of 30 0'--OACOC339 Rcv.63 8SV R" MI / T EN"ROMMENTAL A-°alYsU Request / Chain of caswdy TECNNOWaorrr.. 1lUt:. 3270 VV� c lwou revs onro •�r.3 Refer to Tams sw Caadf6ews P'mlm ldrl Mmcbs 11t www.'evelLCom ��n�Sy�a+Ad¢rese '^ ?CPOProJcct 54cct Addtcp • R y- w�ryry..yyyy��1'7V�� Slsle NL lip �O � 1e r{y.•.�' 97 ZIP �� •t ,n l`ir�Y CcbC[Pe 1�/pn �r r 1� �V �C LAPS1� k" 1.V• Qpote Yweper .,7°., a._ �'�' n .• Ell Add m A6 ) vM M to s.�q m � t , 3 •0�e � ` .Y a °1pled s.i5ijnorr� bw kjA '4'LtN Q 'u^7/Acns614tWo Rtgp[rzmeny; ' : Qo ! OWaYAP PCc rD tPA ❑ O YA C5o p r -J > o watLrc mey , w. OY fT �RCE :01i1iO iiiT tryCR Othw i•AlT04n1 (Liza Uw PrDZr f P " A 1 9 •w.. .: _ E I?i a 4L *-. '9nmlk?bfutm�tIOQ .Date 'f1ai A rA o ', P QX��p L (_L - Izo I12-do Date r c1Tm'ivc Dates 1 0181R419 P.G. I or: S$i FarSammttFsvlroemracalTccAnc AzWyticat,Panmetm and Methods Requested n c yrj a o U It Summit bt: Dste 17mc Carrt& t voltune provided to run QC;to FS ❑NO Cao1m3 �NO CD RwbRcgtic2ted:_Day(s) RtcdvwTemp.: ptLCrCoetainer IV 210 Nmt be npproved b, Lab JiumQer cC 0 �� �O ❑1fEL•1'F.D w Page 1 of 1 ' ' i � SirnurrirGavirorurreafaf Teclurologies, Irrc. V 3310 Win Si. VIVIRON04ENrAt. TECIiNO1..Otii' S, :;1: Crry'al,oga rails, Oltfo 44223 - n+,aryr;car I nhnr,�trrrfPsTEL: Sample Log -In Check List (330) 253-82I1 FAX- (330) 253-4489 Websfre: hyp: /jvrvrs,.settekconr Client Name: SYN-NC-27028 Work Order Number: 20121123 - - - - - - - RcptNo: 1 Logged by: Christina N. Jager 12118/2020 10:20:00 AM C. Completed By: Christina N. Jager 12/18/2020 12:58:46 PM ti Reviewed By: Jennifer Woolf 12/18/2020 2:05:46 PM - - Chain of Custod 1. Is Chain of Custody complete? Yes No ❑ Not Present ❑ 2. Row was the sample delivered? FedEx Lop In 3, Coolers are present? Yes V No ❑ NA ❑ 4, Shipping container/cooler in good condition? Yes No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present U No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes No ❑ NA ❑ 6. Were all samples received at a temperature of >01 C to 6.0*C Yes No ❑ NA ❑ 7, Sample(s) in proper container(s)? 8. Sufficient sample volume for indicated test(s)? g. Are samples (except VOA and ONG) property preserved? 10. Was preservative added to bottles? 11. Is the headspace in the VOA vials less than 114 inch or 6 mm? 12. Were any sample containers received broken? 13. Does paperwork match bottle labels? (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? 15. Is it clear what analyses were requested? 16. Were all holding times able to be met? (If no, notify customer for authorization.) Special Handling 17f a iGable) 17 Was client t•f d Yes Yes Yes Yes ❑ Yes ❑ Yes ❑ Yes Yes Yes Yes No ❑ No ❑ No ❑ No 0 No ❑ No No ❑ No ❑ No ❑ No ❑ NA ❑ No VOA Vials 0 - no i Ee of all discrepancies vath [his order? Yes ❑ - - - No ❑ NA 0 Person Notified: - - - Date: �-- - - --- -- . By Whom: - - - - Via: ❑ eMatl Phone ❑ Fax ❑ In Person Regarding: �� . -- - - - - - ---- -- - Ctient- 18, Additional remarks: - - - - - - - Cooler Information Cooler No Ternp °C Condition1Seal intact _Seal No Seal Date Si7!l� L6 Good Not Present ---- J Panes qn of qn State of North Carolina Department of Environmental Quality Division of Water Resources LAND APPLICATION SITE CERTIFICATION Dlvlslon of Water Resources INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application, Unless otherwise noted the A licant shall submit one or! inal and two co !es of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non-DischyL a —Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or othe r type on forni)in (FORM accordance RLAP 06-16 or FORM. SDR 06- �) not submit this certification for review without a corresponding pp Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation fisted below. A. Land Application Site Certification (FORM: LASC 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-1form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments) to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit the requested information for all land application sites. ® For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. 13. Land Application Site Information: ®his residuals !and application program must be provided in table i, The The status of the land application site with respect to t status categories and their corresponding codes are as follows:. Transferred {T} 4 Deleted (D) ♦ New (N) ♦ Renewed (R) ♦ Modified (M) Attach the following in accordance with each status code: Page I of 3 INSTRUCTIONS FOR FORM: LASC 06-16 l� FOR. �l * This item may be required for land application site with a status code "W', please contact the Division if you need assistant in determining attachment requirements. Crop Type should include the most likely crop types for the life of the permit. (five years). Predominant Soils Series Name must be either the name of the soil indicated in Attachment "B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ® For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ® New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. Acceptable methods for determining location coordinates (i.e., latitude and longitude) acid their corresponding codes are as follows: • Address Matching (ADD) • Digital or Raw Photo Extraction (EX 1) • Aerial Photography with Ground Control (AER) • Geodetic Quality GPS Survey (GEO) • Cadastral Survey (SUR) • LORAN-C Navigation Device (LOR) • Conversion from Coordinate Plane (CP) • Navigation Quality GPS (GPS) • Conversion from Township -Section -Range (TSR) • Remote Sensing (RS) • Conversion from Universal Trans Mere (UTM) • Zip Code Centroid (ZIP) • Map Interpretation by Digital or Manual Extraction (MAP) C. Waterbody and Classifications Information: (new sites only) ❑ Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ❑ Surface water body classifications information may be found at: htt:Ilde .nc. ov/about/divisions/water- resources/ llanninp,/classification-standards/classifications ❑ Any questions concerning the Waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: lift :llde .nc, ov/contact/re ional-offices ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USG topographical map (an 8.5 x 1I-irich sheet showhig tine project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream Maine" as the Waterbody name. 3. Open the link htt ://de .tic. ov/abouUdivisions/water-resources/ lannin classification-standards/classifications. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project information. ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper Iocation descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of tiie waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the namc of the identified waterbody (from General Directions) on tiie list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15A NCAC 02B 91QHi). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Arens Hiwassee River Basin Little Tennesse River Basin And Savannah River Drainage Area French Broad River Basin Watauga River Basin Broad River Basin New River Basin Catawba River Basin Yadkin -Pee Dee River Basin Lumber River Basin Roanoke River Basin Chowan River Basin Tar -Pamlico River Basin Pasouotank River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." Streams entering Tennessee will be classified "B." Streams entering the State of Tennessee are classified "C." Streams entering South Carolina are classified "C." Streams entering the State of Tennessee are classified "C." Streams entering South Carolina are classified "C." Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Streams entering South Carolina are classified "C Sw." Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Streams entering Virginia are classified "C." All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "SC." All drainate canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: City Of Oxford Land application sites currently certified: 510.7 net acres and Total to be certified: 364.2 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Predominant Soil Series NamO Mapping Unit Status Site/Field Landowner(s) Lessee(s) or Operator(s) Net Acres County Crop(s) Code' ID or Rep. Slope' D C-GR-2-2 Morton, James Thomas 38.4 Granville Fescue VaB - Vance D NC-GR-2-3 Morton, James Thomas 36.9 Granville Fescue CaB - Cecil D NC-GR-2-4 Morton, James Thomas 23.1 Granville Fescue CaB — Cecil D NC-GR-2-5 Morton, James Thomas 9.9 Granville Fescue CaB - Cecil D NC-GR-3-1 Wiliford, John C. 39.2 Granville Fescue LmB - Lignum R NC-GR-1-1 Thorp, Henry N 46.1 Granville Fescue Geb - Georgeville R NC-GR-4-1 Denny. Edward B. & Denny. Toni H 12.1 Granville Fescue GeB - Georgeville R NC-GR-4-2 Denny, Toni H 8.5 Granville Fescue GeB — Georgeville R C-GR-4-3 Denny, Edward B. & Denny. Toni H 52.5 Granville Fescue GeB — Georgeville R NC-GR-13-1 Morton, Herbert P. 11.7 Granville Fescue GeB — Georgeville R NC-GR-13-2 Morton, Herbert P. 13.2 Granville Fescue Geb -- Georgeville R NC-GR-13-3 Morton, Herbert P 8.5 Granville Fescue Geb — Georgeville R NC-GR-13-4A Morton, Herbert P. 10.1 Granville Fescue GeB — Georgeville R NC-GR-13-4B Morton, Herbert P. 7.6 Granville Fescue GeB — Georgeville R NC-GR-13-5 Morton, Herbert P. 4.2 Granville Fescue EnB — Enon R NC-GR-13-6 Morton, Herbert P. 4,7 Granville Fescue EnB — Enon R NC-GR-13-7 Morton, Herbert P. 19.2 Granville Fescue EnB — Enon R NC-GR-13-8 Morton, Herbert P. 7.8 Granville Fescue EnB — Enon R NC-GR-13-9 Morton, Herbert P. 19.7 Granville Fescue EnB — Enon R NC-GR-60-1 Red Hill Plantation LLC Isley, Steven J. 43.3 Granville Fescue IrB — Iredell R NC-GR-60-2 Red Hill Plantation LLC Isley, Steven J. 31.9 Granville Fescue LmB — Lignum R NC-GR-60-3 Red Hill Plantation LLC Isley, Steven J. 16.2 Granville Fescue EnB — Enon P FORM: LAI 06-16 Page e 1 LAND APPLICATION SITE CERTIFICATION R NC-GR-60-4 Red Hill Plantation LLC Isley, Steven J. 11.9 Granville Fescue EnB -- Enon R NC-GR-60-5 Red Hill Plantation LLC Isley, Steven J. 11.7 Granville Fescue EnB — Enon R NC-GR-60-6 Red Hill Plantation LLC Isley, Steven J. 7.2 Granville Fescue EnB —Enon R NC-GR-60-7 Red Hill Plantation LLC Isley, Steven J. 16.1 Granville Fescue EnB - Enon a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) • D (Deleted) b Soil Series Name (i.e. Applinb, Cecil, etc.) ° Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the trapping unit is CeB2) H. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction Q: Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed Class ° NAD 83 ADD Nearest Second ° ' it ° ' ff NAD 83 ADD Nearest Second ° ' FF ° ' " NAD 83 ADD Nearest Second °ri ° it NAD 83 ADD Nearest Second ° ° F,NAD 83 ADD Nearest Second ° '11NAD 83 ADD Nearest Second ° ° ' ff NAD 83 ADD Nearest Second ° ' ff ° ' " NAD 83 ADD Nearest Second Note: Please keep the site information (I.) and waterbody information (II.) of the same field on the same page. P FORM: LA'-'" 06-16 ane 2 L� SITE SUMMARY City of Oxford (WQ#0011244) Site ID: NC-GR-1 Owners Name: Henry N. Thorpe Address: 5676 Old Roxboro Rd. Oxford. N.C. 27565 Phone: (919) 693-5679 home (919) 482-5712 mobile Operator: Same Granville Co. Estimated RYE -based Latitude & Applicable Annual Predominant Longitude c:.. i.e.. Anne fl. M&I RAN I imitc (WArt.0 S01I SP. rIAS [D.M.81 36,19.36 N 1 46.1 Fescue(pasture) 158 Georgeville(GeB) 78,44.28 W Fescue ha 211 TOTAL 46.1 Notes: uate: 01/15121 State of North Carolina 11WR Department of Environmental Quality Division of Water Resources Division of Water Resources ISA NCAC 02T.1100—LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supporting documentation For more ih fornhation, visit lite Water Quality Perutittihtg Sectioht's Non -Discharge Permitting Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class S residuals (may include water hteatment plant or other type residuals) hi accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): Qf Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) fonn. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attaclunents to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. [� Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: City Of Oxford hereinafter referred to as the Permittee, to land apply residuals from the following facility0es) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease Land Use or Intended Use of Crops Residuals Source o tional (optional) Special note (no-tilllover-seed/ (yes/no) Cropping Patterns pasture) NC-GR-1-1 N FESCUE (PASTURE) Animal Food City Of Oxford WWTP The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 0 6- 16 Pagel of 3 1. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with tie terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section Il) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDPNR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transrer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at time land application site(s). 6. The Pcrmittec has provided the landowner or his representative with information and data concerning (lie residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. Tile Permittec will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the sail p1 I of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of tie soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or iris representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on tie land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time ror the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. II. RESTRICTIONS: 1. Appropriate measures must be taken by (lie Permittee and/or the landowner or his representative to control public access to the land application sitc(s) during active use and for the 12-month period following it residuals land application event. Such controls may include tiie posting of signs that indicate the activities being conducted at (lie land application site(s). 2. Animals shall not he grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the hired shall not be harvested fora 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into tlhe soil. 6. Food crops with harvested pails below the surface of time land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turrgrown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. I ll. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105 h allows the compliance boundary to be placed closer to tie waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ER A re -defined compliance boundary is needed for field(s) ID: GR-I-I (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. W.ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application progranm and transferred into the new nroRrain: (Name of the new program) FORM: IAA 06- l6 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application sitc(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application sites) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant pennission to the Pennittee to land apply residuals to the land application site(s) as specified herein. j Landowner name: HEj" ! V . Address: 5616 0L-0 I OX(30" City: 0 V-0 o State: d V, Zip: 2 7565- Phone: �� 561 E-mail address: A114 Signature: _Date: NORTH CAROLINA, COUNTY I, the undersigned Notary Public do hereby certify that KI m N. r fy personally appeared before nie this day and acknowledged the due execution of the forgoing instrulnent/-'` WITNESS my hand and official seal this the rli?t!`�m for. day of Aov, 20 Z s NOTARY ' Signature and seal: W (.Of)C-LAN n PUBLIC ; Z i ti i qbL My commission expires: l b! I ��i�N /+ny Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Signature: L RNT-1- Date: I I I ti V2 FORM: LOA 06-1 G Page 3 of 3 U' r �aju�ys� a a _ -- CO Uj co Old R0 or Ra co late Rd 1304 5�R1 ay a ale Rd 1 " o0 Cc � Cl) n a � a a SfafsRa s@ U a f De n d co Joe �rz`�fl Rd Sfd� f _ � o f ¢ Bo ante d'o 7 G Q� D Far Rd b L n v = 0 Q d 1�� w fate - QQ f- Rd 11m late Rd 116 Lue Averette caco 4 d a f � Rd!/ri / a r o Ch � � atOj \` d, t D (all locitiotls approximate) I inch = 7,500 feet r -ate v l , �1 ir; �'i xy •��, , � ftr EMI" �., ' /I J r .l^# - 'I'r tit�rtf!�•! /rt 5��l, Sid !' � J � ' • l/(; ! , , '• 1`y rf R Yr , tl oA,r, f t111 �� t r• r ! i i 1 inch = 660 feet Legend (all locations approximate) -' -"- Stream ApplicationArea O SoilDescription The compliance boundary is established at -- Drain ❑ OnSiteHouse Unsuitable either 250 feet from the residuals application / area or 50 feet within the property boundary, Pond ❑ OffSiteHouse ® OffSiteHouse Qhffi &er is closest to the application area. The review boundary is established midway x e x - Fence Outbuilding between the compliance boundary and the perimeter of the residuals application area. ® PropertyLine "0, Well Feet ^ r2 01 0 230 460 920 1,380 1,840 n - TOPO hie Mal ' ' 11 ,' •, ` ' �4•" ! �•! `� { l ' �I � Y~� • l Is �X OU 46 ..., r- i �d C�N tr 01 (all locations approximate) 9 inch = 1,000 feet CUMULATIVE METAL LOADING 3SIAC) AS OF 12/31/2020 The cumulative metals for this report come from HISTORY records (i.e, the monthly monitoring process has been completed for the State and County where the Fields are located) In cases where a trace metal lab result was Not Reported to Synagro or tracking of metal loading was Not Required the loading on the report is displayed as "NR" FIELDID Last Date Applied AS CD CR CU PB HG MO MI SE NG-GR-00001-0-0001- 10/25/2019 0.22574 0.08935 2.81374 19.20267 1.62887 0.03217 0.54794 0.90362 0.67726 110..110476 Report OatelTime: 1/15/2021 2:20:07 PM page 1 of 1 • J•YT 1} ■ J _ L • Jim.■. NO _ rr �. f •�• •.r Li rl.: r F r IN ti_ r 0 •J ■ ■ ■ �7 _ } 1• •_ No NO 0 ■• ■ i• ..• ■ 4 ■ r— r • • 7r 1 No No . }1 • ■ ti • ■ 1 .• L■ • No ■� - •. •.. •--• ■� -■. 1 NO� • • ■ 1 ■ . • . . . ■ ■ Mis NO 0 .. .1 ■ NO 1 1 PENN 7M0 0 __ 7 ■ L ■ _ I.N. .. _ .• •• NNE..i 1 •_ ■ �._ ram. • r... .T ti f_■ r r• r• 110 ••�. Site ID: Owners Name: Address: Phone: Operator: Estimated Applicable Pialria Aerac SITE SUMMARY City of Oxford (WQ1l0011244) N C-G R-4 Edward B. Denny Toni H. Denny 6633 Old Roxboro Rd. 6633 Old Roxboro Rd. Oxford, N.C. 27565 Oxford, N.C. 27565 (919) 6904259 mobile (919) 693-6601 home (919) 693-4131 farm office Same Granville Co. RYE based Annual Crmiki PAN Limits ❑blaclvri Edward B. Denny Latitude R Predominant Longitude Soil Series (D.M.S) 36.21.41 N 1 12.1 Fescue(Hay) 211 Georgeville(GeB) 78.46.46 W fescue Pasture 158 36.21.49 N 2 8.5 Fescue(Hay) 211 Georgeville(GeB) 78.46.33 W Fescue Pasture 158 36.21.59 N 3 52.5 Fescue(Hay) 211 Georgeville(GeB) 78,46.32 W Fescue Pasture 158 TOTAL 73.1 Notes: 6-i` -1 DW I Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of tine required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and sunporti_ue documentation For more information, visit the lVater Quality Permitting Section's Not -Discharge Perrnifligg Unit. General -- This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in. accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): Submit tine completed and appropriately executed Laud Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. Wn Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. [ A copy of the completed and appropriately executed agreement must be provided to the Iandowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: City Of hereinafter referred to as the Permittee, to land apply residuals from tine following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-GR-4-1 N fescue (Pasture) Animal Food City Of Oxford WWTP NC-GR-4-2 N Fescue (Pasture) Animal Food City Of Oxford WWTP NC-GR-4-3 N Fescue (Pasture) Animal Food City Of Oxford WWTP The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall he renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Pagel of 3 I, STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another pennitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terns and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) arc met, 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application sitc(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives fill details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of tine residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application sitc(s). 11. The landowner or his representative will inform the Permittee of ally revisions or modifications to the intended use and cropping patterns for time land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods, 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, (lie landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to tine land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by tine permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. II, RESTRICTIONS: L Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for tine 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops ►with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not he harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of tile [and shall not be harvested for a 20-month period following a residuals lard application event when the residuals remain on tine land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. 'Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. IILALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 1 5A NCAC 02L ,0107(d) prohibits water supply wells within the compliance boundary. however, 15A NCAC 02T .0 105h allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ( A re -defined compliance boundary is needed for field(s) ID: GR-4-1, GR-4-3 (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ 'I'lte [and application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other' legal delegation, to make decisions regarding the use of the land application sites) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other pennitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: Address: 6 J 00 � o! orao City: © k State: (V G Zip: 2 755 Phone: (7 5 6 E-mail address: O Signature: Date: _ 21 NORTH CAROLINA, CYfl4WILLE COUNTY r! /� I, the undersigned Notary Public do hereby certify that 7 v ^r t fN. )0emi }� personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the ! ,C7if day of `1l�NU Z1 ,�``�%,`G�p 11 AI 20 Signature and seal: AN 7 `Z My commission expires: /6 /z4 _ Na 03L\G ' Lessee's/Operator's Certification: %g2lgNCE GOJ.•`' I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: �pw FivN�' Address: O QLp City: 0)(FO V F State: (, Zip: S65 Phone: 6 rq 3' 560 f E-mail address: A4 Signahrre: Date: Perroittee's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: A.I L, Signature: Date: 111 %1 Z1 FORM: LOA 06-16 Paee 3 of 3 0) s I s ?. Ib �h15 a � m J�Henry F rtf Sta o tic �yt. Walnut Grove Rd Z a 1�2 tiL _ y L Shams Ro ySlo�R� ,�� rye. S o`9lf n � i9fi' �a 73 `aeRd 1 a - a (�°� fdf� o n K tia r 0/d l30 `ale or R a 5 y fate Rd 7304 s,J a. stal�cy / J a a De n d U � u Q Bo1 a,rie �d 4 W a1143 sta fiCl7� IN �A e°Pi a� Rd er�y a ti J Far Rd a LO h r o- � U Q fate Rd 115, 10 (10 ¢d afe Rd y 55 (all locations approximate) vi awk y Map) 4 D a [ate Rci � ti w Rd d p�CP w 3 a � m O a fate Rd 9i6 y CO m L or� a v eekRd C) �- 7snn t- F { -77 Legend 1 ir;'ch = 660 feet (all locations approximate) Stream � ApplicationArea � Well The compliance boundary Is established at '— "— Drain ■ OnSiteHouse O SoilDescription either 250 feet from the residuals application area or 50 feet within the property boundary, Pond Church Unsuitable whichever Is closest to the application area. The review boundary Is established midway x — x - Fence ® OffSiteHouse Outbuilding between the compliance boundary and the perimeter of the residuals application area. i' PropertyLine VC -CAR-04 Feet 0 230 460 920 1,380 1,840 T© jog ra� uhk d_ftq) 01f LA ,. 1 1 � .` ON r 1 S � (all locations approximate) I inch = 1,000 feet CUMULATIVE METAL LOADING i-BS/AC) AS OF 12/31/2020 The cumulative metals for this report come from HISTORY records (i.e. the monthly monitoring process has been completed for the State and County where the Fields are located) In cases where a trace metal lab result was Not Reported to Synagro or tracking of metal loading was Not Required the loading on the report is displayed as "NR" FIELDID Last Date Applied AS CD CR CU PS HG MO Ni SE ZN NG-GR-00004-0-0002- 06/24/2019 0.23275 0.07387 2.15159 14.21356 0.77922 0.02334 0.27919 0.77749 0.28766 57.90515 NC-GR-00004-0-0003- 06/18/2019 0.17476 0.05537 1.69752 11.47207 0.60180 0.01747 0.21331 0.58071 0.26934 47.59523 Report Date/Time: 1/15/2021 2:21:41 PM Page 1 of 1 SITE SUMMARY City of Oxford (WQ#00112") Site ID: NC-GR-13 Owners Name: Herbert Morton, Jr. Address: PO Box 1564 Oxford, NC 27565 Phone: (919) 693-8727 Work (919) 616-2224 Mobile Operator: Same Granvllie County Estimated RYE -based Lalltude & Applicable Annual Predominant Longitude Fields Acres Cronlsl PANT Limits flhf H rl Soil -0—iac rn " at 1 11.7 Orchard Grass(Hay) 169 Georgeville (GeB) 36.28.12 N Orchard Grass(Pasture) 126 78.31.43 w 2 13.2 Orchard Grass(Hay) 169 Georgeville (GeB) 36.28.12 N Orchard Grass Pasture 126 78.32,02 W 3 8.5 Orchard Grass(Hay) 169 Georgeville (GeB) 36.28.17 N Orchard Grass(Pasture) 126 78.31.34 W 4A 10.1 Fescue (Hay) 211 Georgeville (GeB) 36.28.49 N Fescue Pasture 168 78.30.34 W 4B 7.6 Orchard Grass(Hay) 169 Georgeville (GeB) 36,28.59 N Orchard Grass(Pasture) 126 78.30.38 W 5 4.2 Soybeans 130 Enon (EnB) 36.21.26 N Com Grain 114 78.33.25 W 6 47 Soybeans 130 Enon (EnB) 36,31,20 N Corn Grain 114 78,33.19 W 7 19.2 Soybeans 130 Enon (EnB) 36-31.25 N Com Grain 114 78.33.10 W 8 7.8 Soybeans 130 Enon (EnB) 36,31.13 N Corn Grain 114 78,33.03 W 9 19.7 Soybeans 130 Enon (EnB) 36.31.15 N Corn Grain 114 78.32.55 W TOTAL 106.7 Notes Date: 01/15/21 6 f'- )3 State of North Carolina Department of Environmental Quality DWR Division of Water Resources 15A NCAC 02T .1100 — LANDOWNER AGREEMENT Division of Water Resources FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the A licaut shall submit one original and two copies of the HOPHS2110H and supportima documentation For more information, visit the 11'ater Quality Permitting Section's Non -Discharge Permilling Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with l SA NCAC 02T . l 100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed , below. A. Land Owner Agreement (FORM: LOA 06-16): Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as file attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessceloperator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: City Of Oxford hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following bind application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Special note Leese Land Use or Residuals Source n Special n seed! Sitelrield ID Intended Use of Crops o tional (yes/no) Cropping Patterns (optional) posture) NC-GR-13-1,2,3 N rescue (Hay) Animal Food City Of Oxford WWTP NC-GR-13-4A N rescue (Pasture) Animal Food City Of Oxford WW'TP NC-GR-13-4B N rescue (Pasture) Animal Food City Of Oxford WWTP NC-GR-13-5,6,7,8,9 N Row Crop Animal Food City Of Oxford WWTP The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page t of I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for tine site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section it) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-16I7. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with iufornnation and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by tine Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. if die soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil PH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application sitc(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to tine land application site(s) at any reasonable time for the purpose of detennining compliance with tine permit; establish monitoring facilities oil or near the land application site(s) as required by the permit; copy any records that must be kept tinder the terms and conditions of tine permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. J. RF,STRICTIONS: I. Appropriate measures must betaken by the Permittee and/or the landowner or his representative to control public access to the land application sites) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at tine land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period followhng a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuaWsoil mixture and are totally above the land surface shall not be harvested for a 14-ninth period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested fora 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals ]and application event when the residuals remain on the land surface for less (ban four months prior to incorporation into tine soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals Iand application event. IILALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105fh1 allows tine compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at tine newly -established compliance boundary. Please mark one of the following; [ A re -defined compliance boundary is needed for field(s) ID: GR-13-4A, GR-13-4B, GR-13-5, GR-I3-6 (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to file application package) ❑ A re -defined compliance boundary is not needed for this site. iV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted tinder another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the fields) be removed from the previously permitted residuals land application program and transferred into the new aroaram: (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of tine land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of Field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: E l f "r OR*41I Address: CO. 0�( r City: r-`/ State: Phone: q 1 ci - 6q-nnai[ Signature: Zip: 2 756 S Date: 0 \r I I r NORTH CAROLINA, t�kl:; COUNTY I, the undersigned Notary Public do hereby certify that {- personally appeared before me this day and acknowledged the due execution of [lie forgoing instrument. WITNESS my hand and official seal this the �T ��.�`GO�PE����''%,� day of �ahN 4 fty 2o 24 �.���� Gomm. Signature and seal: v _ NOTARY ' U' 1 ' My commission expires: - 2q Lessee's/Operator's Certification: 1 I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: State: Phone: E-mail Signature: Permittee's Certification: Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: A m i_ `—tom Signature: Date: 1 y a FORM: LOA 06-16 Page 3 of 3 I %/10IAII-rk/ nAA" GRAPHIC SCALE I" = 4,000' 4,000 0 4,000' The compliance boundary is established either 250 R from the residuals application area or 50 feet within nI ,n the property boundary, Milchever is closest to the application area. The review boundary is established ' C-G R" 13 midway behveen the compliance boundary and the perimeter of the residuals application area, All locations are approximate. Fields ®9 K.. (fl I LEGEND APPLICATION MAP APPLICATION AREA UNSUITABLE AREA --- — — — — — PRIVATE ROAD WATER — — — STREAM ® ONSITE HOUSE — DRAIN . OFFSITE HOUSE - FENCE OUTBUILDING PROPERTY LINE 0 WELL. The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway behveen the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1" = 660' ssaa ssa NC-GR-13 Fields 1-3 b C4, LEGEND APPLICATION MAP APPLICATION AREA UNSUITABLE AREA — — — — — — PRIVATE ROAD WATER — — — — STREAM ONSITE HOUSE — DRAIN OFFSITE HOUSE FENCE OUTBUILDING PROPERTY LINE 0 WELL The compliance boundary is established either 250 ft From the residuals application area or 50 feet v ilhin in the property boundary, whichever is closest to the application area. The revievi boundary is established midway behmen the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1" = 660' 660' 0 660' NC-GR-13 Fields 4A & 413 LEGEND APPLICATION AREA — — — — — — PRIVATE ROAD — — — — STREAM DRAIN FENCE PROPERTY LINE APPLICATION MAP 0 0 UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimetarof the residuals application area. All locations are approximate. GRAPHIC SCALE 1" = 660' BY o sw NC-GR-13 Fields 5-9 Vi TOPOGRAPHIC MAP GRAPHIC SCALE 1" = 800' 800, o aoo The compliance boundary is established either 250 ft from the residuals application area or 50 feet v ithin N C-GR-13 in the property boundary, whichever is closest to the application area. The review boundary is established f� midway beftwen the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1-3 U/ T®POrRAPHIr MAD GRAPHIC SCALE V, = 800, 8Q0' 0 800, The connpliance boundary is established either 250 ft from the residuals application area or 50 feet vilhin in the property boundary, whichever is closest to the application area. The review boundary is established midway behveen the compliance boundary and the perimeter of the residuals application area, All locations are approximato. NC-GR-1 3 Fields 4A & 4B TOPOGRAPHIC MAP GRAPHIC SCALE 1" = 1,000' -he compliance boundary is established either 250 ft from the residuals application area or 50 feet UAW N —Cj R' 3 ,he property boundary, ivWchever is closest to the application area. The review boundary is established midway behveen the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 5-9 SOIL SURVEY GRAPHIC SCALE 1" = 800' aW o 800' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-G R-1 3 in the property boundary, whichever is closest to the application area. The review boundary is established midway behveen the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1 _3 SOIL SURVEY GRAPHIC SCALE 1" = 800' aao o sao, The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-GR-1 3 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals applicaVon area. All locations are approximate. Fields 1-3 SOIL SURVEY L '.} GRAPHIC SCALE 1"=1,000' s ooa a1,00v The compliance boundary is established either 250 ft from the residuals application area or 50 feetwithin N C-G R-13 in the property boundary, whichever is closest to the application area, The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 5-9 CUMULATIVE METAL LOADING .BSIAC) AS OF 12/31/2020 The cumulative metals for this report come from HISTORY records (i.e. the monthly monitoring process has been completed for the State and County where the Fields are located) In cases where a trace metal lab result was Not Reported to Synagro or tracking of metal loading was Not Required the loading on the report is displayed as "NR" FIELDID Last Date Applied AS CD CR CU PB HG MO Ni SE ZN NC-GR-00013-0-0001- 09/10/2019 0.15020 0.10561 4.05255 22.30469 2.72820 0,04532 0.69755 1.26027 1.06743 85.24394 NC-GR-00013-0-0002- 09/09/2019 0.16470 0.11240 3.87927 22.89766 2.85104 0.04565 0.66944 1.21372 1.10033 83.21916 NC-GR-00013-0-0003- 09/09/2019 0.10364 0.07314 2.68203 15.64930 1.79412 D.02939 0.49590 0.82064 0.69879 53.14864 NC-GR-00013-0-0004-A 10/03/2006 0.02622 0,02833 0.75350 5.04637 0.82300 0.00705 0.22283 0.25500 0.24815 8.14216 NC-GR-00013-0-0004-B 08/30/2019 0.10733 0.05499 1.65135 10.31123 0.72554 0.02352 0.20609 0.52305 0.14234 52.23852 Report DatelTime: 1115/2021 2:22:06 PM Page 1 of 1 SITE SUMMARY City of Oxford (WQ#0011244) Site ID: NG-GR-60 Owners Name: Dr. Robert Cerwin Address: 4520 Townsville Rd. Bullock, NC 27507 Phone: (919) 690-8500 Operator: Steven Isley (Jake) Address: 4520 Townsville Rd. Bullock, NG 27507 Phone: (919) 690-8600 (919) 691-0007 Mobile Granville County Estimated RYE -based Latitude & Applicable Annual Predominant Longitude 1 43.3 Fescue(Hay) Fescue Pasture 121 90 Ired ell (IfB) 36.31.57 N 78,31.49 W 2 31.9 Fescue(Hay) Fescue Pasture 190 142 Llgnum (LmB) 36.31.11 N 78.31.36 W 3 16.2 Fescue(Hay) Fescue Pasture 194 145 Enon (EnB) 36.31.25 N 78.31.50 W 4 11.9 Fescue(Hay) Fescue Pasture 194 145 Enon (EnB) 36.31.37 N 78.31.58 W 5 11.7 Fescue(Hay) Fescue Pasture 194 145 Enon (EnB) 36.31.59 N 78.30.39 W 6 7.2 Fescue(Hay) Fescue(Pasture 194 145 Enon (EnB) 36.31.22 N 78.30.30 W 7 16A Fescue(Hay) Fescue Pasture 194 145 Enon (EnB) 36.31.28 N 78.31.36 W TOTALS 138.3 Notes: hate: 01115/21 -v) DWR Mvislon of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permittiyg Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. Qj Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. [ A copy of the completed and appropriately executed agreement must he provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: City Of hereinafter referred to as the Permittee, to land apply residuals from the following facility(ics) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-GR-60-1,5,6 Yes Fescue (Hay) Animal Food City Of Oxford W1YTP NC-GR-60-2,3,4,7 Yes Fescue (Pasture) Animal Food City Of Oxford VWTP The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. 'his Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Pagel of 3 1. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the sitc(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. 'fhe landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 1I) are net. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. S. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives frill details of the residuals applied at tine land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to cornmeneenient of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application sitc(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pl-I of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the perimitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). t 1. Tile landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application sitc(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months alter termination of, this Agreement. It. RESTRICTIONS: I . Appropriate measures inust be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested fora 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. IMALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) l5A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h)allows the complianee boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards call be met at the newly-establislied compliance boundary. Please mark one of the following; ® A re -defined compliance boundary is needed for field(s) ID; GR-60-1, GR-60-7 (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site, IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted tinder another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program: (Name of the new program) FORM: LOA 06-16 Page 2 of Landowner's Certification: I certiry that I ani a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application sites) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein, Landowner name: Address: eOA- CEWIN twN S%iILLT-- City: U e L State: Iq L , I1 Zip: 2^J S V .-7 Phone: �� ! �' E-mail address: NI h r Signature:l \� Date: NORTH CAROLINA, L C COUNTY 1, the undersigned Notary Public do hereby certify that _900ow µc personally appeared before me this day and acknowledged the due execution of the forgoing instrument. t ZTi+ WITNESS my hand and official seal this the I - day of Signature and seal -5(N►AQ W, puto i My commission expires: Lessee's/Operator's Certification: 01WO .11161 70 Lt O ;tie, :���°�•� .�-��_ I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: 57-eVyi S 15(-Err Address: _ Is H�;gO T lim3ol -a: R el City: TJ ,ttLoCIG State: [ V �- Zip: 27507 Phone: nnoll E-mail address: P( 4 Signature: Date: Permittee's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: w\••t L Signature: Date: I I I 1 I ,L1 FORM: LOA 06-I6 Page 3 of 3 I-V ______-___________________lHap ll 50, DIMS V/if � Sta `� Na Davis c a Fields r 1r_T R 1346 1-4s 7 �" Rd a �_. t 4 erberi F 1 ei Rd a� Milo �r e R j a arrow �i � late R� 143 f �`�� � yMfI—,811 �wa�e ��- - U) �— s w = CI Rce t� 4 a r, St to Rd 1 : 73 t vallCP Burnside R rl/ 4/ry ti } ate n CI°9 14 _Gela RR' cry S`,CLIP w� m 4 - S'c5' ry State Rd 1425 0 t' e Mountain Rd —� h d 4 9 JJt13 I Rd 73 CL DaLY t' 77 ^ �r�` - 1 inch7,500 feet r e-60 (all locations approximate) = or, m �r ' l.ir II ,,', ® • ': - s C� •��' x ; , /� . � S 1. .j, At. If 11 Legond 1 inch = 660 feet Stream ® PropedyL.ine 0 Outbuilding Unsuitable (all locations approximate) The compliance boundary Is established at Drain ApplicationArea ')S�, Well either 250 feet from the residuals application �i area or 50 feet within the property boundary, ® whichever Is closest to the application area. Pond OffSIteHQIISe SQilDescription 7ho review boundary is established midway between the compliance boundary and the x — x - Fence ❑ OnSiteHQuse perimeter of the residuals application area. Feet Fields 29 L/by, 9 7 0 230 460 920 1,380 1,840 ram- f - Apiudivc'Yore Ara- a Ma 7 _ � __ fir• 7. i' " •r A. ✓` } �'( � � - - - � t. ' r j f `}��' - r�rl •_ � _tom"�}� Legend i inch = 660 feet (ati locations approximate) —�� Otain PropetlyLine ® OnSiteHouse Unsuitable '®r, The compliance boundary is established at Pond/a �IicafiortArea RochOuteto either 250 feet from the residuals application p! 11}� p area or50 feet within the property boundary, whichever is closest to the application area. x e x Fence ■ OffSfteHouse O SoilDescription The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. Feet f rd `V- ci o °fields 5_6 0 230 460 920 1,380 1,840 % F—r r I I i IC"ON-64 (all locations approximate) 9 inch = 1,000 feet CUMULATIVE METAL LOADING, �LBSIAC) AS OF 12/31/2020 The cumulative metals for this report come from HISTORY records (i.e, the monthly monitoring process has been completed for the State and County where the Fields are located) In cases where a trace metal lab result was Not Reported to Synagro or tracking of metal loading was Not Required the loading on the report is displayed as "NR" FIELDID Last Date Applied AS CD CR CU PB HG MID Ni SE ZN NC-GR-00060-0-0001- 08/19/2019 0.22911 0.07296 2.95949 18.99403 2.19290 0.05311 0.37751 0.97128 0.86310 77.33477 NC-GR-00060-0-0002- NC-GR-00060-0-0003- NC-GR-00060-0-0004- NC-GR-00060-0-0005- NC-GR-00060-0-0006- 05/18/2020 08/27/2019 08/29/2019 11/10/2020 11/10/2020 0.43348 0.18359 0,16288 0.31081 0.29161 0.12676 0.06248 0.06071 0.08933 0,07832 3.73713 2.77813 2.67168 3.09996 2.56465 22.77083 14.58155 -13.88330 22.85506 19.47350 3.00170 1,44431 0.94352 1.59855 1.33857 0.06408 0.03474 0.03969 0.05726 0.04541 0.56040 0.28106 0.25274 0.47495 0.41365 1.31640 0.94101 0.77080 1.07768 0.93590 0.57524 0.23912 0.23998 0.48943 0.42221 109.77140 83.82434 66,94525 101.02049 85,98112 NC-GR-00060-0-0007- 11/06/2019 0.02122 0.00424 0.23770 1.98221 0.10866 0.00155 0.04415 0.05433 0.02122 6.15459 Report DatefTime: 1/15/2021 2:22:43 PM Page 1 of 1