HomeMy WebLinkAboutWQ0011260_Residual Annual Report 2020_20210129Initial Review
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0011260
Applicant/Permittee Town of Old Fort WWTP
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Asheville
CO Reviewer
Admin Reviewer KendalI.Williams@ncdenr.gov
Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other
.......................................................... electronic surece, aner correspondence.
_ -
Name * Anthony West
Email Address*
twestmarion@aol.com
Project Information
........ ......... ..........................................................................................................................................
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
18286684561
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0011260
Fbs Current Existing perm number
Applicant/Permittee Address* 38 Catawba Ave, Old Fort NC 28762
Facility Name * Town of Old Fort WWTP
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Rc.)
sludge repo rt202O.pdf 2.93MB
Upload only 1 FLFdocurrent (less than 250 fv8). Miltiple documents rust be combined into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 1/29/2021
go-wn of 0(d �rt
— FOUNDED IN 1870 —
38 CATAWBA AVENUE
OLD FORT, NORTH CAROLINA 28762 Office of the Mayor
January 29, 2021
NC Department of Environmental Quality
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh NC 27699-1617
Subject: Town of Old Fort Annual Bioresiduals report, (calendar year 2020)
To Whom It May Concern:
The Town of Old Fort operates a 1.2 MGD wastewater treatment plant (NPDES #
NC0021229). The Town restarted its Pretreatment Program for Hillman Beer in April
2020.
The Town has a bioresidual management permit, # WQ0011260, to process class A
bioresiduals to be sold or given away to the public. The process consists of a 0.075 MG
sludge holding tank, a 0.7 meter belt press and an RDP lime pasteurization process with a
covered storage pad.
The solids are mixed with quicklime to raise the pH up to 12 or higher after two hours
and 11.5 or greater after 22 hours to satisfy the vector attraction reduction requirement,
and heat the solids to 70 degrees Celsius or greater to satisfy the PFRP requirement. The
pH is tested immediately as the final product begins to be discharged from the
pasteurization vessel, after two hours, and again after 22 more hours. The temperature is
monitored at the pasteurization vessel inlet and outlet every thirty minutes.
In April 2020, the Town of Old Fort distributed 48.64 dry tons of bioresiduals that had
been produced in 2019. These residuals were given to a farmer for use on a corn field for
animals. These residuals were sampled for metals and nutrients in December 2019, and
fecal coliform in March 2020.
In all of 2020 the Town of Old Fort WWTP produced 27.1 dry tons of bioresiduals
(14.13 tons of dry sludge + 12.97 tons of lime), which were sampled for metals, nutrients,
reactivity, corrosivity, ignitability and toxicity characteristic leaching procedure (TCLP)
on December 31, 2020. These bioresiduals will be sampled for fecal coliform in
February/ March 2020 and land applied shortly thereafter. As always, untested biosolids
are stored apart from those previously analyzed.
"Colonial America's Western Outpost Until 1756"
The result for Total Phosphorus from the December 17, 2019 analysis was 24900 mg/kg,
much higher than previous results that were always less than 2000 mg/kg. Another
sample was submitted from the remaining bioresiduals composite on January 21, 2020.
Its result was 1850 mg/kg — more in line with previous results. We have no limit on
Total Phosphorus; it only affects the application rate when land applying. After speaking
with Mikal Willmer of Asheville Regional Office, DWR, I was advised to use the second
result for land application rate planning.
Enclosed with this narrative are copies of the operational logs and laboratory analyses of
the bioresiduals. If you have any questions or require further information, please contact
me at 828-668-4561.
Sincerely,
Anthony West
Town of Old Fort WWTP ORC
Land Application / Biosolids ORC
3 8 Catawba Ave
Old Fort, NC 28762
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0011260 FACILITY NAME:
PHONE:828-668-4561 COUNTY:
FACILITY TYPE (please check one):
TOWN OF OLD FORT WWTP - YEAR 2020
MCDOWELL OPERATOR:
TONY WEST
❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
p Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ -► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
OLD FORT WWTP
1.19
1.22
2.41
February
NCO021229
0.85
0.92
1.78
March
"
April
0.99
1.07
2.06
DARRELL SHERLIN
48.64
SILAGE
May
1.02
1.14
2.15
June
1.8
1.97
3.77
July
0.82
0.89
1.71
August
0.96
1.03
1.98
September
0.96
1.14
2.09
October
1.86
2.38
4.24
November
December
2.53
2.39
4.91
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
12.98
14.15
27.1
48.64
Amendments used: I LIME Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (SuppA0 -�
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No --► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/ 7:T7,, 1/29/2021
Signature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
1 /29/2021
Date
DENR FORM DMSDF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0011260
Facility Name: TOWN OF OLD FORT WWTP -YEAR 2019
Residual Source WQ # or NCO021229
NPDES #:
WWTP Name: TOWN OF OLD FORT WWTP
Residual Analysis Data
Laboratory: 1) WATERTECH LABS
2) RESEARCH & ANALYTICAL
3) ENVIRONMENTAL TESTING
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m a
Sample or Composite Date
12/31/20
1/21/20
12/17/19
12/27/18
12/19/17
12/27/16
Percent Solids (%)
NA
45.4
submitt&
46
57.5
48.3
45.8
Arsenic
75
< 3.9
2nd
3.45
2.13
< 1.99
< 2.18
Cadmium
85
1.2
sample
< 0.217
0.177
0.213
< 0.218
Copper
4,300
210
for TP
179
138
166
137
Chromium
NA
analysis
Lead
840
13.8
15
6.77
11.1
9.36
Mercury
57
0.21
0.133
0.246
0.127
Molybdenum
75
11.4
12.2
9.7
10.3
10.4
Nickel
420
6.3
6.36
6.14
4.73
6.07
Selenium
100
< 1.6
< 2.17
< 1.72
< 1.99
< 2.18
Zinc
7,500
225
192
166
140
126
Total Phosphorus
NA
167
1850
24900
1180
1780
1230
TKN
NA
9090
17500
6190
7650
12700
Ammonia -Nitrogen
NA
467
751
1500
1250
4840
Nitrate and Nitrite
NA
67.7
88.1
72.4
1 122
70.3
For surtace disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
1 /29/2021
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0011260
Facility Name: TOWN OF OLD FORT WWTP-YEAR 2019
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
NCO021229
TOWN OF OLD FORT WWTP
Laboratory: 1) WATERTECH LABS
2) RESEARCH & ANALYTICAL
3) ENVIRONMENTAL TESTING S.
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
12/31/20
12/17/19
12/27/18
12/19/17
12/27/16
Aluminum
7490
5130
2820
3410
3000
Calcium
350000
359000
385000
397000
327000
Magnesium
2730
2850
2530
2600
2600
pH
12.10
12.31
12.07
12.70
11.78
P.A.N.
2890
5490
2230
2670
4850
Potassium
878
622
444
496
656
Sodium
< 775
208
224
171
318
S.A.R.
0.095
0.099
0.074
0.152
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
1 /29/2021
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: TOWN OF OLD FORT WWTP WQ Permit Number: WQ0011260
WWTP Name: TOWN OF OLD FORT WWTP NPDES Number: NCO021229
Monitoring Period: From l/1/2020
To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs 0
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization 0
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number ot
Excee-
ences
Frequency
of Anal sis
Y
Sample
Type
Analytical
Tech-ni ue
q
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
< 79
0
< 140
MPN/g
0
7/YEAR
GRAB
SM9221 E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
TONY WEST / ORC
Preparer Name and Title (type or print)
Signature of reparer*
TONY WEST / ORC
Land Applier Name and Title (if applicable)(type or print)
1/29/2021 �1 1/29/2021
Date Signature of L d Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
ceAnalytical s
www.pacelabs.com
J
Pace Analytical Services, LLC
106 Short St.
Kernersvilie, NC 27284
336-996-2841
ANALYTICAL RESULTS
Project: TOWN OF OLD FORT SLUDGE
Pace Project No.: 92514430
Sample: TOWN OF OLD FORT Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid
SLUDGE
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
Chlorinated Herb. (GC) 8151A
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 01/08/21 15:20 Initial pH: 11.71; Final pH: 12.02
Pace National - Mt. Juliet
2,4,5-TP (S[Ivex)
ND mg/L
0.00200 1
01/13/21 19:16
01/14/21 14:33
93-72-1
2,4-D
ND mg/L
0.00200 1
01/13/21 19:16
01/14/21 14:33
94-75-7
Surrogates
2,4-DCAA (S)
87.0 %
14.0-158 1
01/13/21 19:16
01/14/21 14:33
19719-28-9
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 01/06/21
15:25 Initial pH: 5.13; Final pH: 5
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
ND ug/L
0.50 1
01/08/21 06:49
01/11/21 07:46
58-89-9
M1
Chlordane (Technical)
ND ug/L
3.0 1
01/08/21 06:49
01/11/21 07:46
57-74-9
Endrin
ND ug/L
0.50 1
01/08/21 06:49
01/11/21 07:46
72-20-8
M1
Heptachlor
ND ug/L
0.50 1
01/08/21 06:49
01/11/21 07:46
76-44-8
Heptachlor epoxide
ND ug/L
0.50 1
01/08/21 06:49
01/11/2107:46
1024-57-3
M1
Methoxychlor
ND ug/L
1000 1
01108/2106:49
01/11/21 07:46
72-43-5
Toxaphene
ND ug/L
3.0 1
01108/2106:49
01/11/21 07:46
8001-35-2
Surrogates
Decachlorobiphenyi (S)
128 %
10-154 1
01/08/21 06:49
01/11/21 07:46
2051-24-3
Tetrachloro-m-xylene (S)
50 %
10-184 1
01/08/21 06:49
01/11/21 07:46
877-09-8
8082 TCLP PCBs RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 01/06/21 15:25 Initial
pH: 5.13; Final
pH: 5
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
12674-11-2
PCB-1221 (Aroclor 1221)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
11104-28-2
PCB-1232 (Aroclor 1232)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
11141-16-5
PCB-1242 (Aroclor 1242)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
53469-21-9
PCB-1248 (Aroclor 1248)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
12672-29-6
PCB-1254 (Aroclor 1254)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
11097-69-1
PCB-1260 (Aroclor 1260)
ND ug/L
1000 1
01/08/21 06:49
01/11/21 14:51
11096-82-5
Surrogates
Decachlorobiphenyl (S)
124 %
10-181 1
01/08/21 06:49
01/11/21 14:51
2051-24-3
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Pace Analytical Services -Asheville
Aluminum
7490 mg/kg
15.5 1
01/06/2111:05
01/07/2118:41
7429-90-5
BC
Arsenic
ND mg/kg
3.9 1
01/06/2111:05
01/07/2118:41
7440-38-2
Cadmium
1.2 mg/kg
0.16 1
01/06/2111:05
01/07/2118:41
7440-43-9
Calcium
350000 mg/kg
1940 50
01/06/2111:05
01/08/2118:10
7440-70-2
Copper
210 mg/kg
7.8 1
01/06/2111:05
01/07/2118:41
7440-50-8
Lead
13.8 mg/kg
1.6 1
01/06/2111:05
01/07/2118:41
7439-92-1
Magnesium
2730 mg/kg
15.5 1
01/06/2111:05
01/07/2118:41
7439-95-4
Molybdenum
11.4 mg/kg
7.8 1
01/06/2111:05
01/07/2118:41
7439-98-7
Nickel
6.3 mg/kg
0.78 1
01/06/2111:05
01/07/2118:41
7440-02-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/18/2021 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 41
,�acvrba.Analj cal
www.pacolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
106 Short St.
Kemersville, NC 27284
336-996-2841
Project: TOWN OF OLD FORT SLUDGE
Pace Project No.: 92514430
Sample: TOWN OF OLD FORT
SLUDGE
Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Pace Analytical Services -Asheville
Potassium
878 mg/kg 775
1 01106/2111:05
01/07/2118:41
7440-09-7
Selenium
ND mg/kg 1.6
1 01/06/2111:05
01/07/2118:41
7782-49-2
Sodium
ND mg/kg 775
1 01/06/2111:05
01/07/2118:41
7440-23-5
Zinc
225 mg/kg 1.6
1 01/06/2111:05
01/07/2118:41
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 01/06/21 15:17 Initial pH: 5.58; Final
pH: 2
Pace Analytical Services -Asheville
Arsenic
ND mg/L 0.050
1 01/07/2123:25
01/08/2116:24
7440-38-2
Barium
ND mg/L 0.25
1 01/07/2123:25
01/08/2116:24
7440-39-3
Cadmium
ND mg/L 0.0050
1 01/07/2123:25
01/0812116:24
7440-43-9
Chromium
ND mg/L 0.050
1 01/07/2123:25
01/08/2116:24
7440-47-3
Lead
ND mg/L 0.025
1 01/07/2123:25
01/08/2116:24
7439-92-1
Selenium
ND mg/L 0.10
1 01/07/2123:25
01/0812116:24
7782-49-2
Silver
ND mg/L 0.025
1 01/07/2123:25
01/0812116:24
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 01/06/21 15:17
Initial pH: 5.58; Final
pH: 2
Pace Analytical Services -Asheville
Mercury
ND mg/L 0.00020
1 01110/2114:42
01/1112112:02
7439-97-6
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 01/06/21 15:25
Initial pH: 5.13; Final
pH: 5
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
106-46-7
2,4-Dinitrotoluene
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
121-14-2
Hexachloro-1,3-butadiene
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
87-68-3
Hexachforobenzene
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
118-74-1
Hexachloroethane
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
67-72-1
2-Methylphenol(o-Cresol)
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
95-48-7
3&4-Methylphenol(m&p Cresol)
ND ug/L 50.0
1 01/08/21 08:01
01/08/21 16:10
15831-10-4
Nitrobenzene
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
98-95-3
Pentachlorophenol
ND ug/L 100
1 01/08/2108:01
01/08/21 16:10
87-86-5
Pyridine
ND ug/L 50.0
1 01/0812108:01
01/08/21 16:10
110-86-1
2,4,5-Tdchlorophenol
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
95-95-4
2,4,6-Tdchlorophenol
ND ug/L 50.0
1 01/08/2108:01
01/08/21 16:10
88-06-2
Surrogates
Nitrobenzene-d5 (S)
91 % 10-144
1 01/08/21 08:01
01/08/21 16:10
4165-60-0
2-Fluorobiphenyl (S)
82 % 10-130
1 01/08/2108:01
01/08/21 16:10
321-60-8
Terphenyl-d14 (S)
165 % 34-163
1 01/08/2108:01
01/08/21 16:10
1718-51-0 S3
Phenol-d6 (S)
23 % 10-130
1 01/08/21 08:01
01/08/21 16:10
13127-88-3
2-Fluorophenol (S)
30 % 10-130
1 01/08/21 08:01
01/08/21 16:10
367-12-4
2,4,6-Tribromophenol (S)
50 % 10-144
1 01/08/21 08:01
01/08/21 16:10
118-79-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01
/18/2021 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 41
Pace Analytical Services, LLC
106 Short St.
Kemersville, NC 27284
336-996-2841
,�axftlXical
www.pacelabscom
ANALYTICAL RESULTS
Project: TOWN OF OLD FORT SLUDGE
Pace Project No.: 92514430
Sample: TOWN OF OLD FORT
SLUDGE
Lab ID: 92514430001 Collected: 12/31/20 08:00 Received:
12/31/20 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No.
Qual
8260D MSV TCLP
Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311; 01/13/21
12:52
Pace Analytical Services - Charlotte
Benzene
2-Butanone (MEK)
ND ug/L 100 20
ND
01/1412113:59
71-43-2
Carbon tetrachloride
ug/L 200 20
ND ug/L 100
01/14/21 13:59
78-93-3
Chiorobenzene
20
ND ug/L 100
01/14/21 13:59
56-23-5
Chloroform
20
ND ug/L 100
01/14/21 13:59
108-90-7
1,4-Dichlorobenzene
20
ND ug/L 100
01/14/21 13:59
67-66-3
1,2-Dichloroethane
20
ND ug/L
01/14/21 13:59
106-46-7
1,1-Dichloroethene
100 20
ND ug/L 100
01/14/21 13:59
107-06-2
Tetrachloroethene
20
ND ug/L 100 20
01/14/21 13:59
75-35-4
Trichloroethene
ND ug/L 100 20
01/14/21 13:59
127-18-4
Vinyl chloride
ND ug/L 100 20
01/14/21 13:59
79-01-6
M1
Surrogates
01/14/21 13:59
75-01-4
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
102 % 70-130 20
01/14/21 13:59
17060-07-0
4-Bromofluorobenzene (S)
100 % 67-135 20
97 %
01/14/21 13:59
2037-26-5
70-130 20
01/14/21 13:59
460-00-4
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Pace Analytical Services - Charlotte
Total Solids
45.4 % 0.10 1
01/04/21 18:05
Percent Moisture
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
54.6 % 0.10 1
01/04/21 18:00
Wet Chemistry D93/1010A
Analytical Method: D93/1010A
Pace National - Mt. Juliet
Ignitability
DNI at 170 deg F 1 01/06/21 15:35
01/06/21 15:35
9045 pH Soil
Analytical Method: EPA9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C
12.1 Std. Units 0.10 1
01/11/21 16:10
E,H3
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
Pace Analytical Services - Asheville
Plant Available Nitrogen
2890 mg/kg 0.12 1
01/14/21 13:25
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method:
EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
Nitrogen, Ammonia
467 mg/kg 19.7 1 01/12/21 09:14
01/12/21 15:05 7664-41-7
R1
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Kjeldahl, Total
9090 mg/kg 524 5 01/07/21 15:19
01/08/21 05:36 7727-37-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/18/2021 10:20 AM
without the written consent of Pace Analytical Services, LLC.
Page 7 of 41
ceAnalXical
www.pacelabs.com
I
Pace Analytical Services, LLC
106 Short St.
Kemersviile, NC 27284
336-996-2841
ANALYTICAL RESULTS
Project: TOWN OF OLD FORT SLUDGE
Pace Project No.: 92514430
Sample: TOWN OF OLD FORT
SLUDGE
Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. ---- pQua[
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Meth 3.2 Re
v 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
67.7 mg/kg 8.5 1 12/31/20 18:27 12/31/20 19:35
Nitrogen, Nitrite
67.7 mg/kg 8.5 1 12/31/20 18:27 12/31/20 19:35 14797-55-8
ND
mg/kg 8.5 1 12/31/20 18:27 12/31/20 19:35 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev
2.0 1993
Pace Analytical Services -Asheville
Phosphorus
167 mg/kg 4.4 2 01/12/2116:32 01/13/2117:55 7723-14-0 M1,R1
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
ND mg/kg 2.2 1 01/07/21 18:06 01/07/21 18:49
734S Reactive Sulfide
Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mg/kg 22.0 1 01/07/21 18:06 01/07/21 18:10
Date: 01/18/2021 10:20 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 41
Environmental Testing Solutions, Inc.
Project name: Old Fort WWTP
Collection date: 23-Mar-20
Date received: 23-Mar-20
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: (828) 350-9364
Fax: (828)350-9368
Project number: 200323.500
Sample identification: Sludge Grab - 5
Sample number:
197736
Parameter
Method
Result
RL
Units
Date Analyst
y
Footnotes
%TS
Analyzed
Mulitple Tube Fermentation Procedure
SM 2540 G
SM 9221-E
48
0.10
%
23-Mar-20 KEK
<86
86
MPN
23 Mar 20 KEK
Sample identification: Sludge Grab
- 6
Sample number:
197737
Parameter
Method
Result
RL
Units
Date Analyst
Footnotes
%TS
Analyzed
Mulitple Tube Fermentation Procedure
SM 2540 G
SM 9221-E
44
0.10
%
23-Mar-20 KEK
<79
79
MPN
23 Mar 20 KEK
Sample identification: Sludge Grab
- 7
Sample number:
197738
Parameter
Method
Result
RL
Units
Date Analyst
Footnotes
%TS
Analyzed
Mulitple Tube Fermentation Procedure
SM 2540 G
SM 9221-E
47
0.10
%
23-Mar-20 KEK
<85
85
MPN
23 Mar 20 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
Date reviewed: 03 -R& ao
Data reviewed by: Kelley E. Keenan
Signature: tA
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.
i
i
Environmental Testing Solutions, Inc. Certificate of Analysis
Project name: Old Fort WWTP
Collection date:
Date received:
16-Mar-20
16-Mar-20
PO Box 7565
Asheville, NC 28802
Phone: (828) 350-9364
Fax: (828) 350-9368
Project number: 200316.500
Sample identification: Sludge Grab - 1 Sample number:
197542
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 52 0.10 % 16-Mar-20 KEK
Mulitple Tube Fermentation Procedure SM 9221-E <94 94 MPN 16-Mar-20 KEK
Sample identification: Sludge Grab - 2 Sample number:
197573
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 78 0.10 % 16-Mar-20 KEK
Mulitple Tube Fermentation Procedure SM 9221-E <140 140 MPN 16-Mar-20 KEK
Sample identification: Sludge Grab - 3 Sample number:
197544
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 54 0.10 % 16-Mar-20 KEK
Mulitple Tube Fermentation Procedure SM 9221-E <97 97 MPN 16-Mar-20 KEK
Sample identification: Sludge Grab - 4 Sample number:
197545
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
%TS SM 2540 G 52 0.10 - % 16-M.-20 KEK
Mulitple Tube Fermentation Procedure SM 9221-E <94 94 MPN 16-Mar-20 KEK
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
Date reviewed:
Data reviewed by:
Signature:
7tW�
Kelley E. Keenan
/k-
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.
a g 3
TOWN OF OLD FORT WASTEWATER TIREATMENT P�AJIT ��r � .�'LAID APIPLICATION OF BIOSOLIDS ClAk7v � n� � �� ? 2Y ��
method: SW846 9040 C
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YEAR_
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YEAR: 2U 2
method: SW846 9040 C
pH VALUES ARE IN STANDARD UNITS.
CALIRRATION
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PH
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-- - - -ii c'7i
TOWN OF OLD FORT WWTP BIOSOLIDS DISTRIBUTION INSPECTION 2020
APRIL 1, 2020 12:00 pm
Greenlee Rd, Old Fort NC; Darrell Sherlin
40 acre field — flat, easy to drive around;
Stay ten feet from property lines.
April 23, 2020 09:00 am
Greenlee Rd, Old Fort NC
Field appeared to be in good shape, residuals within boundaries.
084
0016
TOWN OF OILD FOES T BIORESiD A s VIVCM11260
DELIVERY LOG
YEAR:
DATE DELIVER;' FIELD USED IBEGM END
LOCATION IFOR j{J4r NER 'fMIL€ACE IMILEAGE �
3-75-
I I
,
Dt� i
/ j
fr
f f
' f
j
i
i
t i
I i
1
I [ I
i I ,
I � f
i
I
j I
I � I
i 1
3 � �
t i f
( I f
f
,
Li - l - -,)- o
TOM OR OLD FORT PAm.rry �mvwwm e i nrs
TIM --- .....� • • •,�••�„� � erc e u c�n�T THERAA L � � �,+/
� fw 7O Oil[ 1
ANy PAR[3� --- �
uMEQ aTART: t -6 I2,, W-WW TOTAL MY Wr 2 t 3 Y ) - v 7
% soup UALSisay-_- � o ,; �r � TAM1L7%mOF
PREP FINAL �:.
TOTw.vW+ W, IN T S 3 2
AFTER
U. PROS p f{
AFM 2 Hft
AFMR 24 H R&
BOATE
day
:lQNTEI.L 4 -1 - U
P. "+C OF
y-�
y '
- z - z
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