Loading...
HomeMy WebLinkAboutWQ0011260_Residual Annual Report 2020_20210129Initial Review Reviewer Williams, Kendall Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0011260 Applicant/Permittee Town of Old Fort WWTP Email Notifications Does this need review by the hydrogeologist?* r Yes r No Regional Office Asheville CO Reviewer Admin Reviewer KendalI.Williams@ncdenr.gov Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other .......................................................... electronic surece, aner correspondence. _ - Name * Anthony West Email Address* twestmarion@aol.com Project Information ........ ......... .......................................................................................................................................... Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 18286684561 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 IT Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0011260 Fbs Current Existing perm number Applicant/Permittee Address* 38 Catawba Ave, Old Fort NC 28762 Facility Name * Town of Old Fort WWTP Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Rc.) sludge repo rt202O.pdf 2.93MB Upload only 1 FLFdocurrent (less than 250 fv8). Miltiple documents rust be combined into one FDFfile unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 1/29/2021 go-wn of 0(d �rt — FOUNDED IN 1870 — 38 CATAWBA AVENUE OLD FORT, NORTH CAROLINA 28762 Office of the Mayor January 29, 2021 NC Department of Environmental Quality Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh NC 27699-1617 Subject: Town of Old Fort Annual Bioresiduals report, (calendar year 2020) To Whom It May Concern: The Town of Old Fort operates a 1.2 MGD wastewater treatment plant (NPDES # NC0021229). The Town restarted its Pretreatment Program for Hillman Beer in April 2020. The Town has a bioresidual management permit, # WQ0011260, to process class A bioresiduals to be sold or given away to the public. The process consists of a 0.075 MG sludge holding tank, a 0.7 meter belt press and an RDP lime pasteurization process with a covered storage pad. The solids are mixed with quicklime to raise the pH up to 12 or higher after two hours and 11.5 or greater after 22 hours to satisfy the vector attraction reduction requirement, and heat the solids to 70 degrees Celsius or greater to satisfy the PFRP requirement. The pH is tested immediately as the final product begins to be discharged from the pasteurization vessel, after two hours, and again after 22 more hours. The temperature is monitored at the pasteurization vessel inlet and outlet every thirty minutes. In April 2020, the Town of Old Fort distributed 48.64 dry tons of bioresiduals that had been produced in 2019. These residuals were given to a farmer for use on a corn field for animals. These residuals were sampled for metals and nutrients in December 2019, and fecal coliform in March 2020. In all of 2020 the Town of Old Fort WWTP produced 27.1 dry tons of bioresiduals (14.13 tons of dry sludge + 12.97 tons of lime), which were sampled for metals, nutrients, reactivity, corrosivity, ignitability and toxicity characteristic leaching procedure (TCLP) on December 31, 2020. These bioresiduals will be sampled for fecal coliform in February/ March 2020 and land applied shortly thereafter. As always, untested biosolids are stored apart from those previously analyzed. "Colonial America's Western Outpost Until 1756" The result for Total Phosphorus from the December 17, 2019 analysis was 24900 mg/kg, much higher than previous results that were always less than 2000 mg/kg. Another sample was submitted from the remaining bioresiduals composite on January 21, 2020. Its result was 1850 mg/kg — more in line with previous results. We have no limit on Total Phosphorus; it only affects the application rate when land applying. After speaking with Mikal Willmer of Asheville Regional Office, DWR, I was advised to use the second result for land application rate planning. Enclosed with this narrative are copies of the operational logs and laboratory analyses of the bioresiduals. If you have any questions or require further information, please contact me at 828-668-4561. Sincerely, Anthony West Town of Old Fort WWTP ORC Land Application / Biosolids ORC 3 8 Catawba Ave Old Fort, NC 28762 CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0011260 FACILITY NAME: PHONE:828-668-4561 COUNTY: FACILITY TYPE (please check one): TOWN OF OLD FORT WWTP - YEAR 2020 MCDOWELL OPERATOR: TONY WEST ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) p Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes 0 No ❑ -► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January OLD FORT WWTP 1.19 1.22 2.41 February NCO021229 0.85 0.92 1.78 March " April 0.99 1.07 2.06 DARRELL SHERLIN 48.64 SILAGE May 1.02 1.14 2.15 June 1.8 1.97 3.77 July 0.82 0.89 1.71 August 0.96 1.03 1.98 September 0.96 1.14 2.09 October 1.86 2.38 4.24 November December 2.53 2.39 4.91 Total from FORM DMSDF (sup) Totals: Annual (dry tons): 12.98 14.15 27.1 48.64 Amendments used: I LIME Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (SuppA0 -� Part C: Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No --► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / 7:T7,, 1/29/2021 Signature of Permittee Date **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Signature of Preparer** (if different from Permittee) 1 /29/2021 Date DENR FORM DMSDF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0011260 Facility Name: TOWN OF OLD FORT WWTP -YEAR 2019 Residual Source WQ # or NCO021229 NPDES #: WWTP Name: TOWN OF OLD FORT WWTP Residual Analysis Data Laboratory: 1) WATERTECH LABS 2) RESEARCH & ANALYTICAL 3) ENVIRONMENTAL TESTING 4) 5) Parameter (mg/kg) Conc. Limit m a Sample or Composite Date 12/31/20 1/21/20 12/17/19 12/27/18 12/19/17 12/27/16 Percent Solids (%) NA 45.4 submitt& 46 57.5 48.3 45.8 Arsenic 75 < 3.9 2nd 3.45 2.13 < 1.99 < 2.18 Cadmium 85 1.2 sample < 0.217 0.177 0.213 < 0.218 Copper 4,300 210 for TP 179 138 166 137 Chromium NA analysis Lead 840 13.8 15 6.77 11.1 9.36 Mercury 57 0.21 0.133 0.246 0.127 Molybdenum 75 11.4 12.2 9.7 10.3 10.4 Nickel 420 6.3 6.36 6.14 4.73 6.07 Selenium 100 < 1.6 < 2.17 < 1.72 < 1.99 < 2.18 Zinc 7,500 225 192 166 140 126 Total Phosphorus NA 167 1850 24900 1180 1780 1230 TKN NA 9090 17500 6190 7650 12700 Ammonia -Nitrogen NA 467 751 1500 1250 4840 Nitrate and Nitrite NA 67.7 88.1 72.4 1 122 70.3 For surtace disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * 1 /29/2021 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0011260 Facility Name: TOWN OF OLD FORT WWTP-YEAR 2019 Residual Source NPDES # or WQ#: WWTP Name: Residual Analysis Data NCO021229 TOWN OF OLD FORT WWTP Laboratory: 1) WATERTECH LABS 2) RESEARCH & ANALYTICAL 3) ENVIRONMENTAL TESTING S. 4) 5) Parameter (mg/kg) Sample or Composite Date 12/31/20 12/17/19 12/27/18 12/19/17 12/27/16 Aluminum 7490 5130 2820 3410 3000 Calcium 350000 359000 385000 397000 327000 Magnesium 2730 2850 2530 2600 2600 pH 12.10 12.31 12.07 12.70 11.78 P.A.N. 2890 5490 2230 2670 4850 Potassium 878 622 444 496 656 Sodium < 775 208 224 171 318 S.A.R. 0.095 0.099 0.074 0.152 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * 1 /29/2021 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: TOWN OF OLD FORT WWTP WQ Permit Number: WQ0011260 WWTP Name: TOWN OF OLD FORT WWTP NPDES Number: NCO021229 Monitoring Period: From l/1/2020 To 12/31/2020 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑ Alt.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs 0 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization 0 Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number ot Excee- ences Frequency of Anal sis Y Sample Type Analytical Tech-ni ue q Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN < 79 0 < 140 MPN/g 0 7/YEAR GRAB SM9221 E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization 0 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." TONY WEST / ORC Preparer Name and Title (type or print) Signature of reparer* TONY WEST / ORC Land Applier Name and Title (if applicable)(type or print) 1/29/2021 �1 1/29/2021 Date Signature of L d Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ceAnalytical s www.pacelabs.com J Pace Analytical Services, LLC 106 Short St. Kernersvilie, NC 27284 336-996-2841 ANALYTICAL RESULTS Project: TOWN OF OLD FORT SLUDGE Pace Project No.: 92514430 Sample: TOWN OF OLD FORT Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid SLUDGE Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A Leachate Method/Date: 1311; 01/08/21 15:20 Initial pH: 11.71; Final pH: 12.02 Pace National - Mt. Juliet 2,4,5-TP (S[Ivex) ND mg/L 0.00200 1 01/13/21 19:16 01/14/21 14:33 93-72-1 2,4-D ND mg/L 0.00200 1 01/13/21 19:16 01/14/21 14:33 94-75-7 Surrogates 2,4-DCAA (S) 87.0 % 14.0-158 1 01/13/21 19:16 01/14/21 14:33 19719-28-9 8081 TCLP Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311; 01/06/21 15:25 Initial pH: 5.13; Final pH: 5 Pace Analytical Services - Charlotte gamma-BHC (Lindane) ND ug/L 0.50 1 01/08/21 06:49 01/11/21 07:46 58-89-9 M1 Chlordane (Technical) ND ug/L 3.0 1 01/08/21 06:49 01/11/21 07:46 57-74-9 Endrin ND ug/L 0.50 1 01/08/21 06:49 01/11/21 07:46 72-20-8 M1 Heptachlor ND ug/L 0.50 1 01/08/21 06:49 01/11/21 07:46 76-44-8 Heptachlor epoxide ND ug/L 0.50 1 01/08/21 06:49 01/11/2107:46 1024-57-3 M1 Methoxychlor ND ug/L 1000 1 01108/2106:49 01/11/21 07:46 72-43-5 Toxaphene ND ug/L 3.0 1 01108/2106:49 01/11/21 07:46 8001-35-2 Surrogates Decachlorobiphenyi (S) 128 % 10-154 1 01/08/21 06:49 01/11/21 07:46 2051-24-3 Tetrachloro-m-xylene (S) 50 % 10-184 1 01/08/21 06:49 01/11/21 07:46 877-09-8 8082 TCLP PCBs RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311; 01/06/21 15:25 Initial pH: 5.13; Final pH: 5 Pace Analytical Services - Charlotte PCB-1016 (Aroclor 1016) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 1000 1 01/08/21 06:49 01/11/21 14:51 11096-82-5 Surrogates Decachlorobiphenyl (S) 124 % 10-181 1 01/08/21 06:49 01/11/21 14:51 2051-24-3 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050B Pace Analytical Services -Asheville Aluminum 7490 mg/kg 15.5 1 01/06/2111:05 01/07/2118:41 7429-90-5 BC Arsenic ND mg/kg 3.9 1 01/06/2111:05 01/07/2118:41 7440-38-2 Cadmium 1.2 mg/kg 0.16 1 01/06/2111:05 01/07/2118:41 7440-43-9 Calcium 350000 mg/kg 1940 50 01/06/2111:05 01/08/2118:10 7440-70-2 Copper 210 mg/kg 7.8 1 01/06/2111:05 01/07/2118:41 7440-50-8 Lead 13.8 mg/kg 1.6 1 01/06/2111:05 01/07/2118:41 7439-92-1 Magnesium 2730 mg/kg 15.5 1 01/06/2111:05 01/07/2118:41 7439-95-4 Molybdenum 11.4 mg/kg 7.8 1 01/06/2111:05 01/07/2118:41 7439-98-7 Nickel 6.3 mg/kg 0.78 1 01/06/2111:05 01/07/2118:41 7440-02-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/18/2021 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 41 ,�acvrba.Analj cal www.pacolabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 Project: TOWN OF OLD FORT SLUDGE Pace Project No.: 92514430 Sample: TOWN OF OLD FORT SLUDGE Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050B Pace Analytical Services -Asheville Potassium 878 mg/kg 775 1 01106/2111:05 01/07/2118:41 7440-09-7 Selenium ND mg/kg 1.6 1 01/06/2111:05 01/07/2118:41 7782-49-2 Sodium ND mg/kg 775 1 01/06/2111:05 01/07/2118:41 7440-23-5 Zinc 225 mg/kg 1.6 1 01/06/2111:05 01/07/2118:41 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 01/06/21 15:17 Initial pH: 5.58; Final pH: 2 Pace Analytical Services -Asheville Arsenic ND mg/L 0.050 1 01/07/2123:25 01/08/2116:24 7440-38-2 Barium ND mg/L 0.25 1 01/07/2123:25 01/08/2116:24 7440-39-3 Cadmium ND mg/L 0.0050 1 01/07/2123:25 01/0812116:24 7440-43-9 Chromium ND mg/L 0.050 1 01/07/2123:25 01/08/2116:24 7440-47-3 Lead ND mg/L 0.025 1 01/07/2123:25 01/08/2116:24 7439-92-1 Selenium ND mg/L 0.10 1 01/07/2123:25 01/0812116:24 7782-49-2 Silver ND mg/L 0.025 1 01/07/2123:25 01/0812116:24 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A Leachate Method/Date: EPA 1311; 01/06/21 15:17 Initial pH: 5.58; Final pH: 2 Pace Analytical Services -Asheville Mercury ND mg/L 0.00020 1 01110/2114:42 01/1112112:02 7439-97-6 8270E TCLP RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311; 01/06/21 15:25 Initial pH: 5.13; Final pH: 5 Pace Analytical Services - Charlotte 1,4-Dichlorobenzene ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 106-46-7 2,4-Dinitrotoluene ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 121-14-2 Hexachloro-1,3-butadiene ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 87-68-3 Hexachforobenzene ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 118-74-1 Hexachloroethane ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/L 50.0 1 01/08/21 08:01 01/08/21 16:10 15831-10-4 Nitrobenzene ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 98-95-3 Pentachlorophenol ND ug/L 100 1 01/08/2108:01 01/08/21 16:10 87-86-5 Pyridine ND ug/L 50.0 1 01/0812108:01 01/08/21 16:10 110-86-1 2,4,5-Tdchlorophenol ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 95-95-4 2,4,6-Tdchlorophenol ND ug/L 50.0 1 01/08/2108:01 01/08/21 16:10 88-06-2 Surrogates Nitrobenzene-d5 (S) 91 % 10-144 1 01/08/21 08:01 01/08/21 16:10 4165-60-0 2-Fluorobiphenyl (S) 82 % 10-130 1 01/08/2108:01 01/08/21 16:10 321-60-8 Terphenyl-d14 (S) 165 % 34-163 1 01/08/2108:01 01/08/21 16:10 1718-51-0 S3 Phenol-d6 (S) 23 % 10-130 1 01/08/21 08:01 01/08/21 16:10 13127-88-3 2-Fluorophenol (S) 30 % 10-130 1 01/08/21 08:01 01/08/21 16:10 367-12-4 2,4,6-Tribromophenol (S) 50 % 10-144 1 01/08/21 08:01 01/08/21 16:10 118-79-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /18/2021 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 41 Pace Analytical Services, LLC 106 Short St. Kemersville, NC 27284 336-996-2841 ,�axftlXical www.pacelabscom ANALYTICAL RESULTS Project: TOWN OF OLD FORT SLUDGE Pace Project No.: 92514430 Sample: TOWN OF OLD FORT SLUDGE Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV TCLP Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311; 01/13/21 12:52 Pace Analytical Services - Charlotte Benzene 2-Butanone (MEK) ND ug/L 100 20 ND 01/1412113:59 71-43-2 Carbon tetrachloride ug/L 200 20 ND ug/L 100 01/14/21 13:59 78-93-3 Chiorobenzene 20 ND ug/L 100 01/14/21 13:59 56-23-5 Chloroform 20 ND ug/L 100 01/14/21 13:59 108-90-7 1,4-Dichlorobenzene 20 ND ug/L 100 01/14/21 13:59 67-66-3 1,2-Dichloroethane 20 ND ug/L 01/14/21 13:59 106-46-7 1,1-Dichloroethene 100 20 ND ug/L 100 01/14/21 13:59 107-06-2 Tetrachloroethene 20 ND ug/L 100 20 01/14/21 13:59 75-35-4 Trichloroethene ND ug/L 100 20 01/14/21 13:59 127-18-4 Vinyl chloride ND ug/L 100 20 01/14/21 13:59 79-01-6 M1 Surrogates 01/14/21 13:59 75-01-4 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 102 % 70-130 20 01/14/21 13:59 17060-07-0 4-Bromofluorobenzene (S) 100 % 67-135 20 97 % 01/14/21 13:59 2037-26-5 70-130 20 01/14/21 13:59 460-00-4 254OG Total Percent Solids Analytical Method: SM 254OG-2011 Pace Analytical Services - Charlotte Total Solids 45.4 % 0.10 1 01/04/21 18:05 Percent Moisture Analytical Method: ASTM D2974-87 Pace Analytical Services - Charlotte Percent Moisture 54.6 % 0.10 1 01/04/21 18:00 Wet Chemistry D93/1010A Analytical Method: D93/1010A Pace National - Mt. Juliet Ignitability DNI at 170 deg F 1 01/06/21 15:35 01/06/21 15:35 9045 pH Soil Analytical Method: EPA9045D Pace Analytical Services -Asheville pH at 25 Degrees C 12.1 Std. Units 0.10 1 01/11/21 16:10 E,H3 Plant Available Nitrogen Analytical Method: SM 271 OB-2011 Pace Analytical Services - Asheville Plant Available Nitrogen 2890 mg/kg 0.12 1 01/14/21 13:25 N2 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod. Pace Analytical Services -Asheville Nitrogen, Ammonia 467 mg/kg 19.7 1 01/12/21 09:14 01/12/21 15:05 7664-41-7 R1 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 9090 mg/kg 524 5 01/07/21 15:19 01/08/21 05:36 7727-37-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/18/2021 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 41 ceAnalXical www.pacelabs.com I Pace Analytical Services, LLC 106 Short St. Kemersviile, NC 27284 336-996-2841 ANALYTICAL RESULTS Project: TOWN OF OLD FORT SLUDGE Pace Project No.: 92514430 Sample: TOWN OF OLD FORT SLUDGE Lab ID: 92514430001 Collected: 12/31/20 08:00 Received: 12/31/20 12:15 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. ---- pQua[ 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Meth 3.2 Re v 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 Nitrogen, Nitrate 67.7 mg/kg 8.5 1 12/31/20 18:27 12/31/20 19:35 Nitrogen, Nitrite 67.7 mg/kg 8.5 1 12/31/20 18:27 12/31/20 19:35 14797-55-8 ND mg/kg 8.5 1 12/31/20 18:27 12/31/20 19:35 14797-65-0 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 167 mg/kg 4.4 2 01/12/2116:32 01/13/2117:55 7723-14-0 M1,R1 733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2 Pace Analytical Services - Greensburg Cyanide, Reactive ND mg/kg 2.2 1 01/07/21 18:06 01/07/21 18:49 734S Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2 Pace Analytical Services - Greensburg Sulfide, Reactive ND mg/kg 22.0 1 01/07/21 18:06 01/07/21 18:10 Date: 01/18/2021 10:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 41 Environmental Testing Solutions, Inc. Project name: Old Fort WWTP Collection date: 23-Mar-20 Date received: 23-Mar-20 Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828)350-9368 Project number: 200323.500 Sample identification: Sludge Grab - 5 Sample number: 197736 Parameter Method Result RL Units Date Analyst y Footnotes %TS Analyzed Mulitple Tube Fermentation Procedure SM 2540 G SM 9221-E 48 0.10 % 23-Mar-20 KEK <86 86 MPN 23 Mar 20 KEK Sample identification: Sludge Grab - 6 Sample number: 197737 Parameter Method Result RL Units Date Analyst Footnotes %TS Analyzed Mulitple Tube Fermentation Procedure SM 2540 G SM 9221-E 44 0.10 % 23-Mar-20 KEK <79 79 MPN 23 Mar 20 KEK Sample identification: Sludge Grab - 7 Sample number: 197738 Parameter Method Result RL Units Date Analyst Footnotes %TS Analyzed Mulitple Tube Fermentation Procedure SM 2540 G SM 9221-E 47 0.10 % 23-Mar-20 KEK <85 85 MPN 23 Mar 20 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: 03 -R& ao Data reviewed by: Kelley E. Keenan Signature: tA NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. i i Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Old Fort WWTP Collection date: Date received: 16-Mar-20 16-Mar-20 PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 200316.500 Sample identification: Sludge Grab - 1 Sample number: 197542 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 52 0.10 % 16-Mar-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E <94 94 MPN 16-Mar-20 KEK Sample identification: Sludge Grab - 2 Sample number: 197573 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 78 0.10 % 16-Mar-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E <140 140 MPN 16-Mar-20 KEK Sample identification: Sludge Grab - 3 Sample number: 197544 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 54 0.10 % 16-Mar-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E <97 97 MPN 16-Mar-20 KEK Sample identification: Sludge Grab - 4 Sample number: 197545 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 52 0.10 - % 16-M.-20 KEK Mulitple Tube Fermentation Procedure SM 9221-E <94 94 MPN 16-Mar-20 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: Data reviewed by: Signature: 7tW� Kelley E. Keenan /k- NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. a g 3 TOWN OF OLD FORT WASTEWATER TIREATMENT P�AJIT ��r � .�'LAID APIPLICATION OF BIOSOLIDS ClAk7v � n� � �� ? 2Y �� method: SW846 9040 C FINAL PRODUCT PH pH VALUES ARE IN STANDARD UNITS. YEAR_ CALIBRATION DATE, TIME COLLECTED DATE/TIM ANALYZED TEMP *C PH St. UNI TEMP CORR TRUE PH, S.0 TIME CAL. BUFFERS QC 10.0 OP. INIT. 10.0 12.45 /2, �3 ta,u3 /2 i 06-� /o,o i /2, Y o, Vim' 12 S4 I �. S-c/ „ ; 7z✓ j-- 2", p&ws 1/2 . _O,o3 ! a .5- Z- 0"') lD,a i 1.2 kc. Iv,d "-1kj -a-5 vs�/' 2-3 a (4 l . S6 .-v,v* /2. 07� `f.9�1 %23 U�,s 7- 3 i(J/ o23 j2,11- -0-0 1:2.5-Z- i �� � < <; 9-2-4 om .2 12,1v2 -J�Ob iA S u�i0,00 /2.CZ 10.10 i2- 37 t-U,u2- 42.11 v 06 1 lo,c) I 1,2 2 leg<l iO3S s' i2.36- U l.2• 36 lb -22 09 ,S id u lZ .4 c) �0,v3 !z. 37 d i5 i0,.v► 12, sv /0,04, a-N 09-15 /a•-U &-2� .Z l;j. �G/ i7,0(4 ) 2� y'� • ,;-6- 10,01 /2 S Z 10,10 -�!8 a,s iU xg- l0/,5- au 1 12. 4 _u,0, /2.4Z 1; 1 08`1 it/ --201 0 2. H 1-2- t4 S d Rdu /0•v� iZ• � k )1�,1 [ � . /2- 3 t��3✓ 12-3 os-&M Z2 )2.579 -0,09 /2.(4 Gl �- /0,0 ( 1.1.4<­ )0111 -5Q n -3 0� � ; is ia3s � v /.Z•�!� Q�l� J a . 35 i� k1 �� i 20 Ia. 2- --04 -1 jZ, 3 7 - 12 Oc- i , JZ i2-, d d Sao j2-1 v Use_?o a j 1 a. Ll -0,17- 2, 3 045� JD i o 1 12 :4(, lo, t VV U9-11U -10 0,0► l�•tiS i4,l1 Unless otherwise indicated, pH meter is calibrated the same day as the sample is analyzed. TEMP. CORR. = Temperature correction to 25 deg. C. 706 7•vJ 7,00 7.00 .. yvv �. vv iJ 7,0L) ;, -7:.vd TOWN OF OLD FORT WASTEWATER TREATMENT Ki PT LAND APPLICATION OF 1310SOLiDS OAR7'0'j P -7 zglsl�� FINAL PRODUCT PH YEAR: 2U 2 method: SW846 9040 C pH VALUES ARE IN STANDARD UNITS. CALIRRATION DATE, TIME COLLECTED DATErrIME ANALYZED TEMP *C PH St. UNII TEMP CORR TRUE PH, S.0 TIME CAL. BUFFERS QC 10.0 OP. INIT. 10.0 12.451 -0, 12.614 ,sU to=v i 1.2-9� /Mlo NIS aJ i;?, 6,ti ,7 -0, ►Z 12. G-i�- o8vU lv,v /v=f► ok) 2-1 I;j. -N ._V=a i�. D 4��o 1�-0 !2 4� >D,o.g -6 U7rs .--7 6 2 / , 79 - ,v5 -2L) 0-74;�- i ),Cll 1-2ti0 /d,dk Rj jaoi oi;o-v- y-1 0517" S 2 I .ta 7 -0:0 i2 . 1�;- `i-I G7.�cg y•-i lO057 2-1 ia.L i -0,12 L - �,� �- z OLS- 20 1-2, 2 i o6at j ; o,O n .4 - 1&0 , 5-& -2(o );2 i i -043 1.) ��2s l .c�1 IZ,y's 1D S- 73-0 7-! o ;?L tz, s Z !J )Z -(' -� 757i -"7 7S 1 /2•6 3 •-001 i.2, sLf Gc o o I fa•4b J0109 08'1 o 6 -10 0 � zo 2 9- 12. a 0, 09 >a .5 0&3 0 14;o < 12,gt , i0,v3 6--1 -26, /Z.yi' +v=03 12,(;-1 -, •, , , , & 10 09'10 (a-ll Odle) f 42.ti v /oZ 9 p�vu ) 101 2•tf( )0,vY 'n4IJ -/ 07s o c� -r vgo�� a la c� l� D� f S- 70 • c� i 1�. �19 / , 6-1 07s7) -1q ogvU ay l 12.y6 /O•r�'� Q.� 1'a. y 9Gl Z� /a,a 1 iz.0 -23 o?L+{ 7-�-K v?57) -�?- /,).Ll 0-7M 10.01 I2.SL Unless other%Wse indicated, pH meter is calibrated the same day as the sample is analyzed. TEMP. CORR. = Temperature correction to 25 deg. C. 7-oo -7. v1 -700 "==Wrmml ip. 0 ft IS MEAStNtm is lsftLa Ifts 2&. / 2 - 3-3k-o S c6,R6 FRM oun ET7HBMON*7MTO DID, ANY PROS tom` OWNER;= Mm Iumnrom ` 8 HISYCLED TIMM LYM PROCM GAL / / -2 5 UME 0 GTART 0 i � TC�i'Al !]ii wr � 2 3 0,f - `� SOUD3 FI�OY �,T E!►ID= ! `j l- TOTAL r TATAI. VOA„ 95 OWDS OF FlMAL M00LICT: `-J . � + UME 4 MXaUW. jM TOMS q , k Z L/ O MINDAFTIER /2,3N Ia.- 7 Jl70AATE o.31 I2- - 7 5 12-3 - ad i2-3 P. OF Ste- .z v a v - G� y - � - ROOM o LW OF W-UDW R BB T ®� 8Y � Do" OF DIGESTER 9EFCM 10 ANYPR0DtCrlwr#M&-nW ammmearART11 * Bft L � TCYrAL rAL- 1,17S o UME Q WART'SUMQE TOTAL MW vff Ly& 7 � AL x � BELT a T�% seS OF � PROMM L13,DAMAS+LW* �D�, IN T+ (4-57 L._ , I MRtWAF7ER �- 07� ff M2 MRS AFTER 24 HR& /2.4( Z �_ ,r 't =� s'a+Z� :t ., -13t - c. -, - i It' • t- ,.?ti.. j_ a- M i ICE-22--Z6 i /` v IBRECVC Eil $�l 7�rAl - / Z 7 S'C7 � erIIIII-rr• � 3=,LffAL rxt�r wr � 2 -7�7 p � / TOTAL V SOLM OF LW FBrFAL pr OVISDAFTER FJI�ATE Cp .z 3 AFTER 24 HW u�3 - -zz- �v -�2- 2 ia. 3 v P. OF /v fcJ Z2-Zo �� MOTAM �a - 7i?Z�`C co t U d 4 3 O, AFrM BELT PRESS MetB� WA M M W BY W�A a=.F''T7�OF M 9'-'a 3 - -z () Aw� m 2 dvwa 1-1 roT�"MOENDc -7sv TOTA-11OUAIE (?F BhF AL per: ,� - 0-43-zo 5mi:-7 covailoG, ...�, rt��� Arq=f--titpp A Y Em TQ ■tag■ F+�cra �rVW '� 7 Mtit.� ��START 3 7 IBr4L-VCLmD7wjoM LOW. 7 TOTAL - 1' -o %SOLIDS � r7 a7u _ &-=x TONAL DRYwT TOTAL 1OF VOLUME+ L3& f MIN TOM MWWAFTER Pot ...,.. AMR 2 HR3 AFTER 24 HR$- iz. Z- 't4 7 213 - �U CW OLD FAG.UY ATOM Loa 4" � � �� Tb MCHq� CEmm %/ALGA • /Z UMEQaTAIRT.; a Z' L a 7 �'" T�'A1. trwr '7 7 (a 0 5 % SOLOS BMa mr► L L8fi � Co 4 �( Oa 9s- 2- 7 �TA1.11� BIOR g + ¢ B OF FMAL PRODUCT S3� ( — /2. �i AFTER 24 HRH I .y ��77-DL --xD as (o ► �-- 2,0 TOWN CWCWFCWOKMUMotmuA AFMI . Avm- ..s ■ 10... I IPAIE FROM OUTLET TAM re � LFUTLt r THERMONErm ANY ACT MW 'Dr MRECYCL�-�. . �, n�ouc� � � END: TOT14L GAL• 7 �AFtT- Z 9Li1FRM st� TarAL m-LWEOy �T PF� T'Ai , sauvs oFFWPLI PAMEDAFnER 0 � S- o.�I _.'. -F I I if . - �• r. �� rr? r� T Tti VEi. Wyv -- -TWFROM -� . qac rfium WG& f TtEmMOMEMouTLET-n 2 % M MGMM STi4R; � # iC SGTER T�TJ�. i AL: fflalocom 3 S7V uNM 0 arm SUJDWMTALMYWr 210a TOTAL % WUDS OF FWL P TOTAL � • I •9 v � OF BtORESl UftS + � + � 1N Tore '""""-� aW-M AF ER 2 Hft AFTER 2A HRH � / ;z 1 , 5 I r�q tD 2s►c _ ,. r ., ,2 �' •:r• �-•�r �( :riM Wit: �y��: ., •+ : 'i:•_ _�•� �':• rr �.�. i I' is i. • 1 -- - - -ii c'7i TOWN OF OLD FORT WWTP BIOSOLIDS DISTRIBUTION INSPECTION 2020 APRIL 1, 2020 12:00 pm Greenlee Rd, Old Fort NC; Darrell Sherlin 40 acre field — flat, easy to drive around; Stay ten feet from property lines. April 23, 2020 09:00 am Greenlee Rd, Old Fort NC Field appeared to be in good shape, residuals within boundaries. 084 0016 TOWN OF OILD FOES T BIORESiD A s VIVCM11260 DELIVERY LOG YEAR: DATE DELIVER;' FIELD USED IBEGM END LOCATION IFOR j{J4r NER 'fMIL€ACE IMILEAGE � 3-75- I I , Dt� i / j fr f f ' f j i i t i I i 1 I [ I i I , I � f i I j I I � I i 1 3 � � t i f ( I f f , Li - l - -,)- o TOM OR OLD FORT PAm.rry �mvwwm e i nrs TIM --- .....� • • •,�••�„� � erc e u c�n�T THERAA L � � �,+/ � fw 7O Oil[ 1 ANy PAR[3� --- � uMEQ aTART: t -6 I2,, W-WW TOTAL MY Wr 2 t 3 Y ) - v 7 % soup UALSisay-_- � o ,; �r � TAM1L7%mOF PREP FINAL �:. TOTw.vW+ W, IN T S 3 2 AFTER U. PROS p f{ AFM 2 Hft AFMR 24 H R& BOATE day :lQNTEI.L 4 -1 - U P. "+C OF y-� y ' - z - z _ OF WM BELT PRM R ESSfQ IS gy F��, TH OF STB BEA E 2-6--ac-) or,)r- 1)3o 71ME FROM OUTE - - .. OUTLET " h I..To T-L21Ai RSST►: It T99%'07M=MLMM)CWL UFA J@ sTARrL1l `�Q1/ OEM 1 �� j Z-mMLxWT0TAL MYWr W& f N o. 9 Z % �� BST - � 96 S�Jp� OF .TOTAt. l.B& 'i 710R'H! VOLUME OF WORE S + UM E + � PM 9-: AFT -ass u AFM2 FM RFU R24 HRS MKLTE c cuemrm 10 :JGATEANgL _ F. -C OF WA63m. " " cal v�"v - _ _ �o fillTF 1� - 7 Wr � �T� RUN. BY �G DEBM OF � � TdIlY1i1 of ouD reiD y gI FAYww-wAnow LOS Lima � � �AE7� 7� �i a I �'L�IU vu#1LT "�RMpvEi'� ��&J �� � :� OrARr r. 1$'��uW� TER E "* TOTAL • t S 7 SO uAE Q START.- (.� r � TCYrAL DRY wr L,B 2 q U 3 i 1 Z 22 UME �.T H►t[}�`1`.�' _L6 _ —TOTAL LB& � ! � 1 �I TOTAL 1� � • S 96 SOLUX OF FDIAL � =AFTER r=s orLl MESg Rom! - .,.......� .016x- 1 rn yr DER BEFORE