NCG030499_2020 DMR with Lab Results_20210122

Anchor QEA of North Carolina, PLLC ANCHOR
231 Haywood Street�z Asheville, North Carolina 28801 QEAi
828.281.3350
January 21, 2021
Attn: DEMLR Stormwater
Asheville Regional Office
Division of Energy, Mineral, and Land Resources
North Carolina Department of Environmental Quality
2090 U.S. 70 Highway Swannanoa, North Carolina 28778-8211
Re: Stormwater Sample Analytical Results, Period 2 2020
Crane Resistoflex
Marion, North Carolina
General Permit No. NCG030499
To Whom It May Concern,
Anchor QEA of North Carolina, PLLC (Anchor QEA), is pleased to present the following stormwater
sample analytical results. On behalf of Crane Resistoflex, Anchor QEA collected two stormwater
samples on December 14, 2020, for the referenced facility covered by National Pollutant Discharge
Elimination System Stormwater General Permit No. NCG030000 (Stormwater General Permit). This
sampling event fulfills the compliance sampling requirement for Period 2 of 2020.
In the samples collected from sampling locations OF-001 and OF-002, all constituent concentrations
detected were below or within the acceptable ranges of the benchmark values specified in the
general permit. This letter provides background information and describes the methods, findings,
and conclusions regarding the stormwater sample collection and analysis.
Background
The most recent Stormwater General Permit for metal fabrication activities was issued by the North
Carolina Department of Environmental Quality with an effective date of November 1, 2018, and it will
expire at midnight on May 31, 2021. Sample collection and reporting protocol for this event followed
the current permit requirements.
The Stormwater General Permit indicates that the permittee shall complete analytical sampling on
a semiannual schedule, once during the first half of the year (January 1 to June 30; Period 1) and
once during the second half of the year (July 1 to December 31; Period 2), at a minimum, allowing
at least 60 days between sample collection dates.
The general location of the facility is indicated in Figure 1. The facility's two permitted outfalls and
sample locations are labeled OF-001 and OF-002, as identified in Figure 2.
Stormwater Sample Analytical Results, Period 2 2020.docx

January 21, 2021
Page 2
Methods
On December 14, 2020, Anchor QEA mobilized to the Crane Resistoflex facility to collect stormwater
samples during a measurable storm event of approximately 1.35 inches of rainfall'. There had not
been a measurable storm event in the 72 hours preceding this sampling event.
The stormwater samples were collected from two outfalls labeled OF-001 and OF-002 (Figure 2).
Samples were collected as indicated in the surface water sampling logs (Attachment 1) from the
approximate center of the discharge streams and were transferred to laboratory -supplied containers.
The containers were placed in a cooler on ice and delivered to Pace Analytical Services, Inc. (Pace), in
Asheville, North Carolina, for laboratory analyses. The pH measurement was obtained in the field by
placing a probe within the flow of the respective outfall. The pH measurement was recorded once
stabilization occurred. Anchor QEA's equipment documentation and instrument calibration data
sheet is included as Attachment 2.
Anchor QEA also performed a stormwater discharge outfall (SDO) qualitative monitoring event
during the stormwater analytical sampling event. The associated SDO qualitative monitoring reports
are included as Attachment 3.
Findings
The laboratory analytical results are summarized in the Semiannual Stormwater Discharge Monitoring
Report (Attachment 4). The samples contained concentrations lower than or within the range of the
specified benchmark values for all constituents analyzed by Pace.
The field measurements of pH for both OF-001 and OF-002 were within the acceptable benchmark
value range. The field measurement results are listed in the surface water sampling logs
(Attachment 1), and pH results are shown in Attachment 4. The Pace analytical report and chain -of -
custody form are included in Attachment 5.
Conclusions
The stormwater sample results for outfalls OF-001 and OF-002 showed concentrations below or
within the range of the benchmark values specified in the general permit for all constituents.
The next analytical monitoring of stormwater discharges will be performed during another
measurable storm event between January 1 and June 30, 2021, to satisfy the Period 1 of 2021
compliance period.
Rainfall depth was obtained from the Weather For You online database records for the MID_F4683 gauge station in Marion, North
Carolina. Available at: https://www.weatherforyou.com/

January 21, 2021
Page 3
If you would like additional information, please contact me at [phone], or contact Victoria
Boyer at [phone].
Sincerely,
rad::1
Robert Cork PE, MEng
Managing Engineer
cc: Victoria Boyer, Crane Resistoflex
Duplicate, Central Files
Attachments
Figure 1 Site Location Map
Figure 2 Stormwater Discharge Outfall Locations
Attachment 1 Surface Water Sampling Logs
Attachment 2 Equipment Documentation and Instrument Calibration Data Sheet
Attachment 3 Stormwater Discharge Outfall Qualitative Monitoring Reports
Attachment 4 Semiannual Stormwater Discharge Monitoring Report
Attachment 5 Laboratory Analytical Report and Chain -of -Custody Form

Figures

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Publish Date: 2021101112, 9:01 PM I User: cpatterson
Filepath: Q:\Jobs\Crane-Resistoflex-2062\Maps\AQ-Fig01-SiteLocationMap.mxd
kZANCHOR
QEA
Figure 1
Site Location Map
Stormwater Sample Analytical Results
Crane Resistoflex, Marion, North Carolina

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Attachment 1
Surface Water Sampling Logs

kZANCHOR
QEA 4-4-4—
Surface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name Crane Resr's fp f/ej(
Date. 1.21 lei"/21l.2-0
Protect Number G q 20 �2 -- O /. 0 f
Weather: 5U°f, Ra1llllt
m
Sapling Personnel: C • P
&fILc Yvn
Facility Permit #: /030 tL �Q
Ne6
Sample Name. OF— 00
Comments:
I
i
-
Sample Method: Grab Syringe
Fu 1, Bailer-Disp. Other.
Oxidation
Dissolved Specific Cond.
pH (S.U.) Reduction Turbidity
Time Temp l C) Oxygen (mg/L) (PS/cm)
report to 0.1 S.U. Potential (mV) (NTU) Comments
r.AP
� vl � CAP
d•
Samp'irg Cortainer Number of Containers Requested Analysis
_ - J00 AL a.,id��i c 2
TTCJ - S(XJ TTU - Parr%c Af
250 rr.L Plastic
--
12S mL Plastic
1 — C aA•`�
40 mi Glass 3
/ ry —yec r
1 L Glass ,✓/ f1zL -- -- 2
T PH- _ate I Co re4-re _ -
Q �e • l , L Pla.rtic ZSO.,c I
7 TTU- Ph en0 /
/4,—Fri
Vegetat:on_ e7ood Access Fa;l - S/e-e _J- n e
Sampling Personnel Signature: //' Date: 1: l tz 0--) U
Notes.
Samples are analyzed immediately upon collection
'C degrees Celsius
p9cm- micro-Stemen per tuba centimeter
mg/L milligrams per Iner
mV: millivolt
NTU nephelometric turbidity units
S U-- standard units
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity EPA Method 120.1, Rev- 1982
DO: SM 4500 O G-2011
pH SM 4500-H' B-2011
Page 1 of 1

ANCHOR
QEA
Surface Water Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name
Cf,911-n e Res;.rty -peX,
Hate /2 ' /4/ Zolo
Project Number-
0'7-2o P — 0!, 0 /
Weather. S 'F Ra'IA Sty'//
Sampling Personnel
C. pa-fltrs
Gpn Facility Permit a: NGo3o
Sample Name
QF — 002
Comments:
Pa th M q,, txAyl e d .
Sample Method: rab Syringe
Pump
Bailer-Disp Other.
Oxidation
Dissolved Specific Cond.
pH (S.U.)
Reduction Turbidity
Time Temp ('C)
Oxygen (mg/L) (PS/cm)
report to 0.1 S.U.
Potential (mV) (NTU) Comments
072-5
CAP
(} . Q p
G/�P
Sampling Container
Number of Containers
Requested Analysis
TTV - 5V6r- f TTU - Pcst/;c.'des
250 mL Plastic
3
/�
/ 4e-fii/s CCwr P6, ZI, �Qi`sJe% ACAIS/ T70 -Melt/s
_
12S mL Plast^c _
TTO - <f as i,WG
d0 mL Glass
7-TO - V o c -r
1 L Glass r/ His L
2
TPH C),/ f G ease
TSS Z Try - PA i�/101
vegetavon Goo d Access: �al/' i M �ySACC2 s'lv�,r 1sU��J�`Oe
Sampling Personnel Signature: Date: / -21 ! 4/20 2 O
Note
Samples are analyzed immediately upon collection
'C degrees Celsius
VS/cm micro-Siemen per cubic centimeter
mg/L miQigrams per liter
mJ millivolt
r4TU rrephebmetnc turbidity units
S U standard units
Method Reference.
Temperature. SM 2550 B-2010
Specific conductivity EPA Method 1201, Rev 1982
PO SM 4500 O G-2011
pHSM 4500-H' B-2011
Page 1 of 1

Attachment 2
Equipment Documentation and
Instrument Calibration Data Sheet

tzANCHOR
QEA
Equipment Documentation and Instrument Calibration Data Sheet
Anchor QEA of North Carolina, PLLC
231 Maywood Street
Asheville, North Carolina 28801
CALIBRATION DOCUMENTATION
Prefect Nacre �'it I,� � � � �[ Person Conducting Calibration C - Prx (ter. -an
Ptrtyect Number o 1;.1 ,U _ o / Date of Calibration. /2/ /f}/ 2-02-0
Neiect Lotcatton- „/V7Ari�bnq; �y/ vC Date of field Measurements %21 /L}f Z0 z U
Paziitt Pe7nita !vC `7030 419
KWIPMENT DOCUMENTATION
or meters tj cod to take measurements
Eciliuipmelli Bramd Serial Number Data of Use Rental Company
Select Turbid imet er Hach 21000 (sin 151006045207)
HF Soenific MitroTPW ts/n 100601045)
lnstrument Reading
(Hach 2106Q)
Instrument Reading
(HF Scientific MicroTPW)
10 NTU
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Caishrati:sn Lot Na. &
Expiration Date:
Cal
Cal
Caf
Cal
Ca(
Time
Time
Time
Ti
Time
Time
Calibration
Vetiftcatilo=
'Pre -Analysis
Check (10 NTU):
Meas
Time
"Pre -Analysis
Check (10 NTU):
Meas
Time
`Post -Analysis
Check (10 U):
Time
t-Anal sis Imeas
Time G¢ f
Check (10 NTU):
YSI Professional Plus Multiparameter Meter (s/n 188t04$62) / % Q1
Instrument Readings
Calibration Lot No.
& Expiration Date
Cal (V
mmHg
Temperature (Q
Time CAP
saturation)
DO (Site ol2,
If a ;:cable)'
mR1al (%).
Cal (`t)
mmH
Lure (1C)
Time i✓�
pH 7 s L
report M 0 7 Yu
IniUaL
6, qS
pHmV /�
— / p . 3
Cal
7- 01
pHmV
Time
0S If5
Y/
LJ• 2 �
PH o s u- ii�^,kcal
_ -1 L7 pH�,-7•
Cal ! 1 . o O
pHmV
Tim 547
0,2f -2Z
PH 10 reDcwrto01s-u
70- o1
I
PH-133 7
Cal/V• O1
PHnV
Time
V
V L 121
QC^ pH 7 S-U.
re7_? �r;5
Al`.,, Tlr .e
O-5sz
Meas-
-7.d2
Mid Day Ttme
0740
Check
6•�9
PM Time
Check
OSlz2
Spec Cond.
ps/cm
Ca!
Time
0-P
Meas
Mid Day Time
Check
PM Time
Cheek
Ns/cm
3E Recovery=
Cal
cure C
Time
signature: — Date: l / I � �QaV 7
IVoref
Rewswn 5 Ilflg= JW
1 LAffi'tanents Owl be calibrated tr accordance with the manufacturers operation manual
2 Soil ConducDwdy should be calibrated according to values representative of historic range
3 Omer of CAWraton q as follows SpeofK Conducttwty. pH 7, pH 4 pH 10, DO. OPP QC checks
4 'tM>ten perform" DO anaryses it multiple sample soles (i e. prolect/fa<dity locations) the DO probe must be calibrated at each sample site prior to analysts
5 OC Acceptable Panges pH ./ 01 S U and Specific Conductmty 10% of the true value If OC readings are out of range the instrument needs to be recalibrated
B " OC chedi must be performed prior to sampling and following completion of sampling, at a minimum
T 96 7tec;vt = (Value ObtaMed, jjS/cm - True value. pS/cm) x 100
McMod Reference Temp SM 2550 8-2010 1 Conductivity EPA Merhod 120 1 1 DO SM 4500 0 G-2071 j pH SM 4500 H+8 2077 1 Turbidity SM 2130 8 2017
Page 1 of 1

Attachment 3
Stormwater Discharge Outfal I Qualitative
Monitoring Reports

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit hItps://deg.nc.gov/about/divisions/energy-mineral-land-
resource s/energvv-mineral-land-permits/stormwater-permits/npde s-industrial-sw#tab-4
Permit No.: N/C/ 0 / 3 / 0 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 / 0 / 4 / 9 / 9 /
Facility Name:
County: McDowell
Crane Resistoflex
Phone No. [phone]
Inspector: Christian Patterson (Anchor QEA of North Carolina, PLLC)
Date of Inspection: 12.14.2020
Time of Inspection: 06:50
Total Event Precipitation (inches): 1.35
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. of-001
Receiving Stream:
Catawba River
Structure (pipe, ditch, etc.)
Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? © Yes No.
8. Is there an oil sheen in the stormwater discharge? OYes 0 No.
9. Is there evidence of erosion or deposition at the outfall? O Yes Q No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No indications of stormwater pollution were observed.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit hItps://deg.nc.gov/about/divisions/energy-mineral-land-
resource s/energvv-mineral-land-permits/stormwater-permits/npde s-industrial-sw#tab-4
Permit No.: N/C/ 0 / 3 / 0 / 0 / 0 / 0 / 0 / or Certificate of Coverage No.: N/C/G/ 0 / 3 / 0 / 4 / 9 / 9 /
Facility Name:
County: McDowell
Crane Resistoflex
Phone No. [phone]
Inspector: Christian Patterson (Anchor QEA of North Carolina, PLLC)
Date of Inspection: 12.14.2020
Time of Inspection: 07:25
Total Event Precipitation (inches): 1.35
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. of-002
Receiving Stream:
Catawba River
Structure (pipe, ditch, etc.)
Pipe
Describe the industrial activities that occur within the outfall drainage area: Metal fabrication
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: clear
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): None
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? () Yes No.
8. Is there an oil sheen in the stormwater discharge? ()Yes 0 No.
9. Is there evidence of erosion or deposition at the outfall? Q Yes Q No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No indications of stormwater pollution were observed.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

Attachment
Semiannual Stormwater Discharge
Monitoring Report

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitorin Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the ap
propriate DEMLR Regional Office.
Certificate of Coverage No. NCG03
Facility Name: Crane Resistoflex
Facility County: McDowell
Person Collecting Samples: Christian Patterson
Laboratory Name: Pace Analytical
Laboratory Cert. No.: 40
Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ,IN No
If so, which Tier (I, II, or III)?
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall 1
Outfall 2
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
C
C
N/A
Date Sample Collected MM/DD/YYYY
12/14/2020
12/14/2020
46529
24-Hour Rainfall in inches
1.35
1.35
00552
Non -Polar Oil & Grease in mg/L (15)
<5.0
<5.0
C0530
TSS in mg/L (100 or 50*'
7.6
2.5
00400
pH in standard units" ' �)
6.93
O
6.88
0
NCOIL
New Motor/Hydraulic Oil Usage in
gal/month
01119
Copper, total recoverable in mg/L
<0.005
<0.005
(0.010 FW, 0.005 SW)
1
01051
Lead, total recoverable in mg/ L
<0.005
<0.005
(0.075 FW, 0.220 SW)
0.0681
ND
l
01094
Zinc, total recoverable in mg/ L (0.126
FW, 0.095 SW)
0 .0355
78141
Total Toxic Organics (TTO) in mg/L(1)
ND
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of . All other water classifications have a benchmark of
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
Signature
Authorized Individual
Date

Attachment 5
Laboratory Analytical Report and
Chain -of -Custody Form

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
January 11, 2021
Mr. Christian Patterson
Anchor QEA
231 Haywood Street
Asheville, NC 28801
RE: Project: Crane Resistoflex
Pace Project No.: 92511537
Dear Mr. Patterson:
Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
C�e .-
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 41

Pace Analytical Services, LLC
aceAnalytical ®
Asheville,
Riverside NC 2880404
www.pacelahs.com [phone]
SAMPLE SUMMARY
Project:
Pace Project No.:
Crane Resistoflex
92511537
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92511537001
OF-001
Water
12/14/20 06:55
12/14/20 13:15
92511537002
OF-002
Water
12/14/20 07:25
12/14/20 13:15
92511537003
OF-001 TTO
Water
12/14/20 06:55
12/14/20 13:15
92511537004
OF-002 TTO
Water
12/14/20 07:25
12/14/20 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project: Crane Resistoflex
Pace Project No.: 92511537
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92511537001
OF-001
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
4
PASI-A
EPA 200.7 Rev 4.4 1994
SH1
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
92511537002
OF-002
EPA 1664B
CJM
1
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
4
PASI-A
EPA 200.7 Rev 4.4 1994
SH1
1
PASI-A
SM 254OD-2011
RED
1
PASI-A
92511537003
OF-001 TTO
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
DS
12
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
35
PASI-C
EPA420.4 Rev 1.0 1993
JKG
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
92511537004
OF-002 TTO
EPA 608.3
SEM
30
PASI-C
EPA 200.7 Rev 4.4 1994
DS
12
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
SAS
35
PASI-C
EPA420.4 Rev 1.0 1993
JKG
1
PASI-A
SM 4500-CN-E-2011
CJL
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 41

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[phone]
SUMMARY OF DETECTION
Project: Crane Resistoflex
Pace Project No.: 92511537
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 234013)
1700
ug/L
EPA 200.7 Rev 4.4 1994
Zinc
35.5
ug/L
EPA 200.7 Rev 4.4 1994
Zinc, Dissolved
32.5
ug/L
SM 254OD-2011
Total Suspended Solids
7.6
mg/L
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
Hardness, Total(SM 234013)
2030
ug/L
EPA 200.7 Rev 4.4 1994
Zinc
68.1
ug/L
EPA 200.7 Rev 4.4 1994
Zinc, Dissolved
68.0
ug/L
SM 2540D-2011
Total Suspended Solids
2.5
mg/L
92511537003
OF-001 TTO
EPA 200.7 Rev 4.4 1994
Antimony
3.2J
ug/L
EPA 200.7 Rev 4.4 1994
Zinc
34.6
ug/L
92511537004
OF-002 TTO
EPA 200.7 Rev 4.4 1994
Zinc
59.7
ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit Analyzed Qualifiers
662
12/19/20 00:20
10.0
12/19/20 00:20
10.0
12/16/2021:47 M1,R1
2.5
12/16/20 22:42
662
12/19/20 00:24
10.0
01/05/2118:19
10.0
01/05/2117:31
2.5
12/16/20 22:42
5.0 12/20/20 15:27
10.0 12/20/20 15:27
10.0 12/20/20 15:30
Page 5 of 41

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001
Parameters
1664 SGT-HEM, TPH
Total Petroleum Hydrocarbons
200.7 MET ICP
Copper
Lead
Hardness, Total(SM 234013)
Zinc
200.7 MET ICP, Dissolved
ANALYTICAL RESULTS
Lab ID: 92511537001 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Results Units PQL
MDL
DF
Prepared
Analyzed CAS No.
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
ND mg/L 5.0
5.0
1
12/18/2011:08
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
ND ug/L 5.0
4.3
1
12/17/20 02:09
12/19/20 00:20 7440-50-8
ND ug/L 5.0
4.5
1
12/17/20 02:09
12/19/20 00:20 7439-92-1
1700 ug/L 662
131
1
12/17/20 02:09
12/19/20 00:20
35.5 ug/L 10.0
9.5
1
12/17/20 02:09
12/19/20 00:20 7440-66-6
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Qual
Zinc, Dissolved 32.5 ug/L 10.0 2.5 1 12/15/20 09:43 12/16/20 21:47 7440-66-6 M1,R1
2540D Total Suspended Solids Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids 7.6 mg/L 2.5 2.5 1 12/16/20 22:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 41

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002
Lab ID: 92511537002 Collected:
12/14/20 07:25
Received: 12/14/20 13:15 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared Analyzed CAS No. Qual
1664 SGT-HEM, TPH
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Total Petroleum Hydrocarbons
ND mg/L 5.0
5.0
1
12/18/20 11:08
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Copper
ND ug/L 5.0
4.3
1
12/17/20 02:09 12/19/20 00:24 7440-50-8
Lead
ND ug/L 5.0
4.5
1
12/17/20 02:09 12/19/20 00:24 7439-92-1
Hardness, Total(SM 234013)
2030 ug/L 662
131
1
12/17/20 02:09 12/19/20 00:24
Zinc
68.1 ug/L 10.0
9.5
1
01/05/2113:03 01/05/2118:19 7440-66-6
200.7 MET ICP, Dissolved
Analytical Method: EPA 200.7 Rev 4.4
1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc, Dissolved
68.0 ug/L 10.0
2.5
1
01/05/21 15:20 01/05/21 17:31 7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
2.5 mg/L 2.5
2.5
1
12/16/20 22:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
alpha -Chlordane
gamma -Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
PCB, Total
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Selenium
Silver
Thallium
Analytical Method: EPA608.3 Preparation Method: EPA608.3
Pace Analytical Services - Charlotte
ND
ug/L
0.050
0.022
1
12/15/2014:51
12/17/2019:39
309-00-2
ND
ug/L
0.050
0.019
1
12/15/2014:51
12/17/2019:39
319-84-6
ND
ug/L
0.050
0.014
1
12/15/2014:51
12/17/2019:39
319-85-7
ND
ug/L
0.050
0.020
1
12/15/2014:51
12/17/2019:39
319-86-8
ND
ug/L
0.050
0.012
1
12/15/2014:51
12/17/2019:39
58-89-9
ND
ug/L
0.50
0.14
1
12/15/2014:51
12/17/2019:39
57-74-9
ND
ug/L
0.050
0.0090
1
12/15/2014:51
12/17/2019:39
5103-71-9
ND
ug/L
0.050
0.017
1
12/15/2014:51
12/17/2019:39
5103-74-2
ND
ug/L
0.050
0.0069
1
12/15/2014:51
12/17/2019:39
72-54-8
ND
ug/L
0.050
0.0064
1
12/15/2014:51
12/17/2019:39
72-55-9
ND
ug/L
0.050
0.018
1
12/15/2014:51
12/17/2019:39
50-29-3
ND
ug/L
0.050
0.0073
1
12/15/2014:51
12/17/2019:39
60-57-1
ND
ug/L
0.050
0.0094
1
12/15/2014:51
12/17/2019:39
959-98-8
ND
ug/L
0.050
0.0065
1
12/15/2014:51
12/17/2019:39
33213-65-9
ND
ug/L
0.050
0.0091
1
12/15/2014:51
12/17/2019:39
1031-07-8
ND
ug/L
0.050
0.0089
1
12/15/2014:51
12/17/2019:39
72-20-8
ND
ug/L
0.050
0.013
1
12/15/2014:51
12/17/2019:39
7421-93-4
ND
ug/L
0.050
0.016
1
12/15/2014:51
12/17/2019:39
76-44-8
ND
ug/L
0.050
0.0097
1
12/15/2014:51
12/17/2019:39
1024-57-3
ND
ug/L
0.50
0.22
1
12/15/2014:51
12/17/2019:39
12674-11-2
ND
ug/L
0.50
0.32
1
12/15/2014:51
12/17/2019:39
11104-28-2
ND
ug/L
0.50
0.21
1
12/15/2014:51
12/17/2019:39
11141-16-5
ND
ug/L
0.50
0.44
1
12/15/2014:51
12/17/2019:39
53469-21-9
ND
ug/L
0.50
0.34
1
12/15/2014:51
12/17/2019:39
12672-29-6
ND
ug/L
0.50
0.24
1
12/15/2014:51
12/17/2019:39
11097-69-1
ND
ug/L
0.50
0.30
1
12/15/2014:51
12/17/2019:39
11096-82-5
ND
ug/L
0.50
0.50
1
12/15/2014:51
12/17/2019:39
1336-36-3
ND
ug/L
0.50
0.19
1
12/15/2014:51
12/17/2019:39
8001-35-2
139
%
10-154
1
12/15/2014:51
12/17/2019:39
877-09-8
172
%
10-184
1
12/15/2014:51
12/17/2019:39
2051-24-3
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
3.2J
ug/L
5.0
3.0
1
12/17/20 02:09
12/20/20 15:27
7440-36-0
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:27
7440-38-2
ND
ug/L
1.0
0.70
1
12/17/20 02:09
12/20/20 15:27
7440-41-7
ND
ug/L
1.0
0.40
1
12/17/20 02:09
12/20/20 15:27
7440-43-9
ND
ug/L
5.0
3.7
1
12/17/20 02:09
12/20/20 15:27
7440-47-3
ND
ug/L
5.0
4.3
1
12/17/20 02:09
12/20/20 15:27
7440-50-8
ND
ug/L
5.0
4.5
1
12/17/20 02:09
12/20/20 15:27
7439-92-1
ND
ug/L
5.0
3.5
1
12/17/20 02:09
12/20/20 15:27
7440-02-0
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:27
7782-49-2
ND
ug/L
5.0
2.5
1
12/17/20 02:09
12/20/20 15:27
7440-22-4
ND
ug/L
10.0
8.1
1
12/17/20 02:09
12/20/20 15:27
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
M1
M1
M1
M1
M1
M1
Page 8 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO Lab ID: 92511537003 Collected: 12/14/20 06:55 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc
34.6
ug/L
10.0
9.5
1
12/17/20 02:09
12/20/20 15:27
7440-66-6
245.1 Mercury
Analytical Method: EPA245.1
Rev 3.0
1994 Preparation
Method: EPA245.1 Rev 3.0 1994
Pace Analytical Services - Asheville
Mercury
ND
ug/L
0.20
0.12
1
12/16/2012:20
12/17/2012:05
7439-97-6
625 RVE
Analytical Method: EPA625.1
Preparation
Method: EPA625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
83-32-9
Acenaphthylene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
208-96-8
Anthracene
ND
ug/L
5.0
2.3
1
12/15/20 17:36
12/17/20 04:16
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
2.7
1
12/15/20 17:36
12/17/20 04:16
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:16
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
2.6
1
12/15/20 17:36
12/17/20 04:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:16
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
2.7
1
12/15/20 17:36
12/17/20 04:16
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1.8
1
12/15/20 17:36
12/17/20 04:16
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
3.1
1
12/15/20 17:36
12/17/20 04:16
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
3.3
1
12/15/20 17:36
12/17/20 04:16
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1.8
1
12/15/20 17:36
12/17/20 04:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:16
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:16
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.2
1
12/15/20 17:36
12/17/20 04:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
7005-72-3
Chrysene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
3.0
1
12/15/20 17:36
12/17/20 04:16
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
8.1
1
12/15/20 17:36
12/17/20 04:16
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
120-83-2
Diethylphthalate
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:16
105-67-9
Dimethylphthalate
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:16
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
10.0
3.4
1
12/15/20 17:36
12/17/20 04:16
534-52-1
2,4-Di nitro phenol
ND
ug/L
50.0
26.0
1
12/15/20 17:36
12/17/20 04:16
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1.6
1
12/15/20 17:36
12/17/20 04:16
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:16
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
3.9
1
12/15/20 17:36
12/17/20 04:16
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
3.7
1
12/15/20 17:36
12/17/20 04:16
117-81-7
Fluoranthene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
206-44-0
Fluorene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1.8
1
12/15/20 17:36
12/17/20 04:16
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/15/20 17:36
12/17/20 04:16
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
2.9
1
12/15/20 17:36
12/17/20 04:16
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced,
except in
full,
Date: 01 /11 /2021 12:50 PM
without the written consent
of Pace
Analytical Services,
LLC.
Page 9 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO
Lab ID:
92511537003
Collected:
12/14/20 06:55
Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical
Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical
Services - Charlotte
Isophorone
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:16
78-59-1
Naphthalene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:16
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:16
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
88-75-5
4-Nitrophenol
ND
ug/L
10.0
6.6
1
12/15/20 17:36
12/17/20 04:16
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:16
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1.3
1
12/15/20 17:36
12/17/20 04:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
3.0
1
12/15/20 17:36
12/17/20 04:16
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1.2
1
12/15/20 17:36
12/17/20 04:16
108-60-1
Pentachlorophenol
ND
ug/L
10.0
3.8
1
12/15/20 17:36
12/17/20 04:16
87-86-5
Phenanthrene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:16
85-01-8
Phenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:16
108-95-2
Pyrene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:16
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:16
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.6
1
12/15/20 17:36
12/17/20 04:16
88-06-2
Surrogates
Nitrobenzene-d5 (S)
76
%
10-120
1
12/15/20 17:36
12/17/20 04:16
4165-60-0
2-Fluorobiphenyl (S)
47
%
15-120
1
12/15/20 17:36
12/17/20 04:16
321-60-8
Terphenyl-d14 (S)
105
%
11-131
1
12/15/20 17:36
12/17/20 04:16
1718-51-0
Phenol-d6 (S)
40
%
10-120
1
12/15/20 17:36
12/17/20 04:16
13127-88-3
2-Fluorophenol (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:16
367-12-4
2,4,6-Tribromophenol (S)
97
%
10-137
1
12/15/20 17:36
12/17/20 04:16
118-79-6
624 Volatile Organics Acrolein
Analytical
Method: EPA 624.1
Pace Analytical
Services - Charlotte
Acrolein
ND
ug/L
5.0
3.8
1
12/15/2019:01
107-02-8
Benzene
ND
ug/L
1.0
0.38
1
12/15/2019:01
71-43-2
Bromod ichloromethane
ND
ug/L
2.0
0.24
1
12/15/2019:01
75-27-4
Bromoform
ND
ug/L
2.0
0.40
1
12/15/2019:01
75-25-2
Bromomethane
ND
ug/L
2.0
1.2
1
12/15/2019:01
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
0.29
1
12/15/20 19:01
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.37
1
12/15/2019:01
108-90-7
Chloroethane
ND
ug/L
2.0
1.4
1
12/15/2019:01
75-00-3
Chloroform
ND
ug/L
2.0
0.58
1
12/15/2019:01
67-66-3
Chloromethane
ND
ug/L
2.0
0.73
1
12/15/2019:01
74-87-3
Dibromochloromethane
ND
ug/L
2.0
0.32
1
12/15/2019:01
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
0.24
1
12/15/2019:01
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
0.31
1
12/15/2019:01
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
0.41
1
12/15/2019:01
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
0.51
1
12/15/2019:01
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
0.34
1
12/15/2019:01
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
0.41
1
12/15/2019:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12/15/2019:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12/15/2019:01
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
0.27
1
12/15/2019:01
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-001 TTO
Lab ID: 92511537003 Collected:
12/14/20 06:55
Received: 12/14/20 13:15 Matrix: Water
Parameters
Results Units PQL
MDL
DF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics Acrolein
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND ug/L 2.0
0.33
1
12/15/20 19:01
10061-01-5
trans-1,3-Dichloropropene
ND ug/L 2.0
0.41
1
12/15/20 19:01
10061-02-6
Ethylbenzene
ND ug/L 1.0
0.28
1
12/15/20 19:01
100-41-4
Methylene Chloride
ND ug/L 2.0
0.24
1
12/15/20 19:01
75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L 2.0
0.34
1
12/15/20 19:01
79-34-5
Tetrachloroethene
ND ug/L 2.0
0.28
1
12/15/20 19:01
127-18-4
Toluene
ND ug/L 1.0
0.44
1
12/15/20 19:01
108-88-3
1,1,1-Trichloroethane
ND ug/L 2.0
0.35
1
12/15/20 19:01
71-55-6
1,1,2-Trichloroethane
ND ug/L 2.0
0.31
1
12/15/20 19:01
79-00-5
Trichloroethene
ND ug/L 2.0
0.36
1
12/15/20 19:01
79-01-6
Trich lo rofluoro methane
ND ug/L 2.0
0.28
1
12/15/20 19:01
75-69-4
Vinyl chloride
ND ug/L 2.0
0.72
1
12/15/20 19:01
75-01-4
Surrogates
4-Bromofluorobenzene (S)
94 % 70-130
1
12/15/20 19:01
460-00-4
Toluene-d8 (S)
97 % 70-130
1
12/15/20 19:01
2037-26-5
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
12/15/20 19:01
17060-07-0
420.4 Phenolics, Total
Analytical Method: EPA420.4 Rev 1.0
1993 Preparation
Method: EPA420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
Phenol
ND mg/L 0.020
0.0076
1
12/17/20 09:35 12/17/20 15:15
108-95-2
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E-2011 Preparation Method:
SM 4500-CN-E-2011
Pace Analytical Services - Asheville
Cyanide
ND mg/L 0.0080
0.0060
1
12/15/20 01:23 12/15/20 23:37
57-12-5 M1,R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
608 PCB Pest RVE
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
Chlordane (Technical)
alpha -Chlordane
gamma -Chlordane
4,4'-DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endosulfan I
Endosulfan 11
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
PCB, Total
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
200.7 MET ICP
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Copper
Lead
Nickel
Selenium
Silver
Thallium
Analytical Method: EPA608.3 Preparation Method: EPA608.3
Pace Analytical Services - Charlotte
ND
ug/L
0.050
0.022
1
12/15/20 14:51
12/17/20 20:37
309-00-2
ND
ug/L
0.050
0.019
1
12/15/20 14:51
12/17/20 20:37
319-84-6
ND
ug/L
0.050
0.014
1
12/15/20 14:51
12/17/20 20:37
319-85-7
ND
ug/L
0.050
0.020
1
12/15/20 14:51
12/17/20 20:37
319-86-8
ND
ug/L
0.050
0.012
1
12/15/20 14:51
12/17/20 20:37
58-89-9
ND
ug/L
0.50
0.14
1
12/15/20 14:51
12/17/20 20:37
57-74-9
ND
ug/L
0.050
0.0090
1
12/15/20 14:51
12/17/20 20:37
5103-71-9
ND
ug/L
0.050
0.017
1
12/15/20 14:51
12/17/20 20:37
5103-74-2
ND
ug/L
0.050
0.0069
1
12/15/20 14:51
12/17/20 20:37
72-54-8
ND
ug/L
0.050
0.0064
1
12/15/20 14:51
12/17/20 20:37
72-55-9
ND
ug/L
0.050
0.018
1
12/15/20 14:51
12/17/20 20:37
50-29-3
ND
ug/L
0.050
0.0073
1
12/15/20 14:51
12/17/20 20:37
60-57-1
ND
ug/L
0.050
0.0094
1
12/15/20 14:51
12/17/20 20:37
959-98-8
ND
ug/L
0.050
0.0065
1
12/15/20 14:51
12/17/20 20:37
33213-65-9
ND
ug/L
0.050
0.0091
1
12/15/20 14:51
12/17/20 20:37
1031-07-8
ND
ug/L
0.050
0.0089
1
12/15/20 14:51
12/17/20 20:37
72-20-8
ND
ug/L
0.050
0.013
1
12/15/20 14:51
12/17/20 20:37
7421-93-4
ND
ug/L
0.050
0.016
1
12/15/20 14:51
12/17/20 20:37
76-44-8
ND
ug/L
0.050
0.0097
1
12/15/20 14:51
12/17/20 20:37
1024-57-3
ND
ug/L
0.50
0.22
1
12/15/20 14:51
12/17/20 20:37
12674-11-2
ND
ug/L
0.50
0.32
1
12/15/20 14:51
12/17/20 20:37
11104-28-2
ND
ug/L
0.50
0.21
1
12/15/20 14:51
12/17/20 20:37
11141-16-5
ND
ug/L
0.50
0.44
1
12/15/20 14:51
12/17/20 20:37
53469-21-9
ND
ug/L
0.50
0.34
1
12/15/20 14:51
12/17/20 20:37
12672-29-6
ND
ug/L
0.50
0.24
1
12/15/20 14:51
12/17/20 20:37
11097-69-1
ND
ug/L
0.50
0.30
1
12/15/20 14:51
12/17/20 20:37
11096-82-5
ND
ug/L
0.50
0.50
1
12/15/20 14:51
12/17/20 20:37
1336-36-3
ND
ug/L
0.50
0.19
1
12/15/20 14:51
12/17/20 20:37
8001-35-2
209
%
10-154
1
12/15/20 14:51
12/17/20 20:37
877-09-8 S3
263
%
10-184
1
12/15/20 14:51
12/17/20 20:37
2051-24-3 S3
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
ND
ug/L
5.0
3.0
1
12/17/20 02:09
12/20/20 15:30
7440-36-0
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:30
7440-38-2
ND
ug/L
1.0
0.70
1
12/17/20 02:09
12/20/20 15:30
7440-41-7
ND
ug/L
1.0
0.40
1
12/17/20 02:09
12/20/20 15:30
7440-43-9
ND
ug/L
5.0
3.7
1
12/17/20 02:09
12/20/20 15:30
7440-47-3
ND
ug/L
5.0
4.3
1
12/17/20 02:09
12/20/20 15:30
7440-50-8
ND
ug/L
5.0
4.5
1
12/17/20 02:09
12/20/20 15:30
7439-92-1
ND
ug/L
5.0
3.5
1
12/17/20 02:09
12/20/20 15:30
7440-02-0
ND
ug/L
10.0
4.7
1
12/17/20 02:09
12/20/20 15:30
7782-49-2
ND
ug/L
5.0
2.5
1
12/17/20 02:09
12/20/20 15:30
7440-22-4
ND
ug/L
10.0
8.1
1
12/17/20 02:09
12/20/20 15:30
7440-28-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Zinc
59.7
ug/L
10.0
9.5
1
12/17/20 02:09
12/20/20 15:30
7440-66-6
245.1 Mercury
Analytical Method: EPA245.1
Rev 3.0
1994 Preparation
Method: EPA245.1 Rev 3.0 1994
Pace Analytical Services - Asheville
Mercury
ND
ug/L
0.20
0.12
1
12/16/2012:20
12/17/2012:07
7439-97-6
625 RVE
Analytical Method: EPA625.1
Preparation
Method: EPA625.1
Pace Analytical Services - Charlotte
Acenaphthene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
83-32-9
Acenaphthylene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
208-96-8
Anthracene
ND
ug/L
5.0
2.3
1
12/15/20 17:36
12/17/20 04:45
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
2.7
1
12/15/20 17:36
12/17/20 04:45
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:45
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
2.6
1
12/15/20 17:36
12/17/20 04:45
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:45
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
2.7
1
12/15/20 17:36
12/17/20 04:45
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1.8
1
12/15/20 17:36
12/17/20 04:45
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
3.1
1
12/15/20 17:36
12/17/20 04:45
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
3.3
1
12/15/20 17:36
12/17/20 04:45
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1.8
1
12/15/20 17:36
12/17/20 04:45
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:45
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:45
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1.2
1
12/15/20 17:36
12/17/20 04:45
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
7005-72-3
Chrysene
ND
ug/L
5.0
2.8
1
12/15/20 17:36
12/17/20 04:45
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
3.0
1
12/15/20 17:36
12/17/20 04:45
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
10.0
8.1
1
12/15/20 17:36
12/17/20 04:45
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
120-83-2
Diethylphthalate
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:45
105-67-9
Dimethylphthalate
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:45
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
10.0
3.4
1
12/15/20 17:36
12/17/20 04:45
534-52-1
2,4-Di nitro phenol
ND
ug/L
50.0
26.0
1
12/15/20 17:36
12/17/20 04:45
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1.6
1
12/15/20 17:36
12/17/20 04:45
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:45
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
3.9
1
12/15/20 17:36
12/17/20 04:45
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
3.7
1
12/15/20 17:36
12/17/20 04:45
117-81-7
Fluoranthene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
206-44-0
Fluorene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:45
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1.8
1
12/15/20 17:36
12/17/20 04:45
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1.6
1
12/15/20 17:36
12/17/20 04:45
77-47-4
Hexachloroethane
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
2.9
1
12/15/20 17:36
12/17/20 04:45
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced,
except in
full,
Date: 01 /11 /2021 12:50 PM
without the written consent
of Pace
Analytical Services,
LLC.
Page 13 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO
Lab ID:
92511537004
Collected:
12/14/20 07:25
Received: 12/14/20 13:15 Matrix: Water
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
625 RVE
Analytical
Method: EPA625.1 Preparation Method: EPA625.1
Pace Analytical
Services -
Charlotte
Isophorone
ND
ug/L
10.0
1.7
1
12/15/20 17:36
12/17/20 04:45
78-59-1
Naphthalene
ND
ug/L
5.0
2.1
1
12/15/20 17:36
12/17/20 04:45
91-20-3
Nitrobenzene
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:45
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
88-75-5
4-Nitrophenol
ND
ug/L
10.0
6.6
1
12/15/20 17:36
12/17/20 04:45
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1.9
1
12/15/20 17:36
12/17/20 04:45
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1.3
1
12/15/20 17:36
12/17/20 04:45
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
3.0
1
12/15/20 17:36
12/17/20 04:45
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1.2
1
12/15/20 17:36
12/17/20 04:45
108-60-1
Pentachlorophenol
ND
ug/L
10.0
3.8
1
12/15/20 17:36
12/17/20 04:45
87-86-5
Phenanthrene
ND
ug/L
5.0
2.0
1
12/15/20 17:36
12/17/20 04:45
85-01-8
Phenol
ND
ug/L
5.0
1.4
1
12/15/20 17:36
12/17/20 04:45
108-95-2
Pyrene
ND
ug/L
5.0
2.2
1
12/15/20 17:36
12/17/20 04:45
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1.7
1
12/15/20 17:36
12/17/20 04:45
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1.6
1
12/15/20 17:36
12/17/20 04:45
88-06-2
Surrogates
Nitrobenzene-d5 (S)
86
%
10-120
1
12/15/20 17:36
12/17/20 04:45
4165-60-0
2-Fluorobiphenyl (S)
52
%
15-120
1
12/15/20 17:36
12/17/20 04:45
321-60-8
Terphenyl-d14 (S)
121
%
11-131
1
12/15/20 17:36
12/17/20 04:45
1718-51-0
Phenol-d6 (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:45
13127-88-3
2-Fluorophenol (S)
49
%
10-120
1
12/15/20 17:36
12/17/20 04:45
367-12-4
2,4,6-Tribromophenol (S)
90
%
10-137
1
12/15/20 17:36
12/17/20 04:45
118-79-6
624 Volatile Organics Acrolein
Analytical
Method: EPA 624.1
Pace Analytical
Services -
Charlotte
Acrolein
ND
ug/L
5.0
3.8
1
12/15/2019:19
107-02-8
Benzene
ND
ug/L
1.0
0.38
1
12/15/2019:19
71-43-2
Bromod ichloromethane
ND
ug/L
2.0
0.24
1
12/15/2019:19
75-27-4
Bromoform
ND
ug/L
2.0
0.40
1
12/15/2019:19
75-25-2
Bromomethane
ND
ug/L
2.0
1.2
1
12/15/2019:19
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
0.29
1
12/15/20 19:19
56-23-5
Chlorobenzene
ND
ug/L
2.0
0.37
1
12/15/2019:19
108-90-7
Chloroethane
ND
ug/L
2.0
1.4
1
12/15/2019:19
75-00-3
Chloroform
ND
ug/L
2.0
0.58
1
12/15/2019:19
67-66-3
Chloromethane
ND
ug/L
2.0
0.73
1
12/15/2019:19
74-87-3
Dibromochloromethane
ND
ug/L
2.0
0.32
1
12/15/2019:19
124-48-1
1,2-Dichlorobenzene
ND
ug/L
2.0
0.24
1
12/15/2019:19
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
0.31
1
12/15/2019:19
541-73-1
1,4-Dichlorobenzene
ND
ug/L
2.0
0.41
1
12/15/2019:19
106-46-7
1,1-Dichloroethane
ND
ug/L
2.0
0.51
1
12/15/2019:19
75-34-3
1,2-Dichloroethane
ND
ug/L
2.0
0.34
1
12/15/2019:19
107-06-2 M1
1,1-Dichloroethene
ND
ug/L
2.0
0.41
1
12/15/2019:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12/15/2019:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
0.42
1
12/15/2019:19
156-60-5
1,2-Dichloropropane
ND
ug/L
2.0
0.27
1
12/15/2019:19
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Project: Crane Resistoflex
Pace Project No.: 92511537
Sample: OF-002 TTO
ANALYTICAL RESULTS
Lab ID: 92511537004 Collected: 12/14/20 07:25 Received: 12/14/20 13:15 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No
624 Volatile Organics Acrolein
Analytical Method: EPA 624.1
Pace Analytical Services - Charlotte
cis-1,3-Dichloropropene
ND ug/L 2.0
0.33
1
12/15/20 19:19
10061-01-5
trans-1,3-Dichloropropene
ND ug/L 2.0
0.41
1
12/15/20 19:19
10061-02-6
Ethylbenzene
ND ug/L 1.0
0.28
1
12/15/20 19:19
100-41-4
Methylene Chloride
ND ug/L 2.0
0.24
1
12/15/20 19:19
75-09-2
1,1,2,2-Tetrachloroethane
ND ug/L 2.0
0.34
1
12/15/20 19:19
79-34-5
Tetrachloroethene
ND ug/L 2.0
0.28
1
12/15/20 19:19
127-18-4
Toluene
ND ug/L 1.0
0.44
1
12/15/20 19:19
108-88-3
1,1,1-Trichloroethane
ND ug/L 2.0
0.35
1
12/15/20 19:19
71-55-6
1,1,2-Trichloroethane
ND ug/L 2.0
0.31
1
12/15/20 19:19
79-00-5
Trichloroethene
ND ug/L 2.0
0.36
1
12/15/20 19:19
79-01-6
Trich lo rofluoro methane
ND ug/L 2.0
0.28
1
12/15/20 19:19
75-69-4
Vinyl chloride
ND ug/L 2.0
0.72
1
12/15/20 19:19
75-01-4
Surrogates
4-Bromofluorobenzene (S)
93 % 70-130
1
12/15/20 19:19
460-00-4
Toluene-d8 (S)
98 % 70-130
1
12/15/20 19:19
2037-26-5
1,2-Dichloroethane-d4 (S)
90 % 70-130
1
12/15/20 19:19
17060-07-0
420.4 Phenolics, Total
Analytical Method: EPA420.4 Rev 1.0 1993 Preparation
Method: EPA420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
Phenol
ND mg/L 0.020
0.0076
1
12/17/20 09:35 12/17/20 15:16
108-95-2
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services - Asheville
Cyanide
ND mg/L 0.0080
0.0060
1
12/15/20 01:23 12/15/20 23:39
57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
Page 15 of 41

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
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QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 588138 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537001, 92511537002
METHOD BLANK: 3107878
Matrix:
Water
Associated Lab Samples: 92511537001, 92511537002
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Petroleum Hydrocarbons
mg/L
ND
5.0
5.0 12/18/20 11:08
LABORATORY CONTROL SAMPLE:
3107879
Spike
LCS LCS
% Rec
Parameter
Units
Cone.
Result % Rec
Limits Qualifiers
Total Petroleum Hydrocarbons
mg/L
20
15.6 78
64-132
MATRIX SPIKE SAMPLE: 3107880
35598602001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 5.01-1 20 11.7 54 64-132 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587409 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3104355 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury ug/L ND 0.20 0.12 12/17/2011:53
LABORATORY CONTROL SAMPLE: 3104356
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.2 87 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3104357 3104358
MS MSD
92509470001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2.3 2.4 91 95 70-130 4 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3104359 3104360
MS MSD
92511537003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 2.3 2.6 91 101 70-130 10 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587665 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537001, 92511537002, 92511537003, 92511537004
METHOD BLANK: 3105714
Matrix:
Water
Associated Lab Samples: 92511537001, 92511537002,
92511537003, 92511537004
Blank
Reporting
Parameter
Units
Result
Limit
Antimony
ug/L
ND
5.0
Arsenic
ug/L
ND
10.0
Beryllium
ug/L
ND
1.0
Cadmium
ug/L
ND
1.0
Chromium
ug/L
ND
5.0
Copper
ug/L
ND
5.0
Hardness, Total(SM 2340B)
ug/L
ND
662
Lead
ug/L
ND
5.0
Nickel
ug/L
ND
5.0
Selenium
ug/L
ND
10.0
Silver
ug/L
ND
5.0
Thallium
ug/L
ND
10.0
Zinc
ug/L
ND
10.0
LABORATORY CONTROL SAMPLE: 3105715
Parameter
Antimony
Arsenic
Beryllium
Cadmium
Chromium
Copper
Hardness, Total(SM 2340B)
Lead
Nickel
Selenium
Silver
Thallium
Zinc
MDL Analyzed
3.0
12/20/20 15:11
4.7
12/20/20 15:11
0.70
12/20/20 15:11
0.40
12/20/20 15:11
3.7
12/20/20 15:11
4.3
12/20/20 15:11
131
12/20/20 15:11
4.5
12/20/20 15:11
3.5
12/20/20 15:11
4.7
12/20/20 15:11
2.5
12/20/20 15:11
8.1
12/20/20 15:11
9.5
12/20/20 15:11
Qualifiers
Spike
LCS
LCS
% Rec
Units
Cone.
Result
% Rec
Limits Qualifiers
ug/L
500
483
97
85-115
ug/L
500
482
96
85-115
ug/L
500
489
98
85-115
ug/L
500
498
100
85-115
ug/L
500
499
100
85-115
ug/L
500
496
99
85-115
ug/L
33100
32500
98
85-115
ug/L
500
490
98
85-115
ug/L
500
497
99
85-115
ug/L
500
484
97
85-115
ug/L
250
246
98
85-115
ug/L
500
497
99
85-115
ug/L
500
498
100
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105716
3105717
MS
MSD
92511027001 Spike
Spike
MS
MSD
MS MSD % Rec
Max
Parameter Units Result Cone.
Cone.
Result
Result
% Rec % Rec Limits
RPD RPD Qual
Antimony ug/L 15.6 500
500
511
507
99 98 70-130
1 20
Arsenic ug/L ND 500
500
489
484
98 97 70-130
1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105716
3105717
MS
MSD
92511027001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Beryllium
ug/L
ND
500
500
498
492
100
98
70-130
1
20
Cadmium
ug/L
ND
500
500
492
485
98
97
70-130
1
20
Chromium
ug/L
ND
500
500
489
481
97
96
70-130
1
20
Copper
ug/L
7.6
500
500
518
514
102
101
70-130
1
20
Hardness, Total(SM 2340B)
ug/L
9800
33100
33100
43300
42700
101
100
70-130
1
20
Lead
ug/L
ND
500
500
481
473
96
95
70-130
2
20
Nickel
ug/L
ND
500
500
496
490
99
98
70-130
1
20
Selenium
ug/L
ND
500
500
504
507
101
101
70-130
1
20
Silver
ug/L
ND
250
250
253
253
101
101
70-130
0
20
Thallium
ug/L
ND
500
500
476
466
95
93
70-130
2
20
Zinc
ug/L
106
500
500
602
591
99
97
70-130
2
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105718
3105719
MS
MSD
92511033003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
23.8
500
500
511
518
97
99
70-130
1
20
Arsenic
ug/L
ND
500
500
502
508
100
101
70-130
1
20
Beryllium
ug/L
ND
500
500
503
508
101
102
70-130
1
20
Cadmium
ug/L
3.3
500
500
494
500
98
99
70-130
1
20
Chromium
ug/L
235
500
500
721
725
97
98
70-130
1
20
Copper
ug/L
327
500
500
866
871
108
109
70-130
1
20
Hardness, Total(SM 2340B)
ug/L
108000
33100
33100
140000
141000
97
100
70-130
1
20
Lead
ug/L
114
500
500
611
619
99
101
70-130
1
20
Nickel
ug/L
103
500
500
597
595
99
98
70-130
0
20
Selenium
ug/L
ND
500
500
495
499
99
100
70-130
1
20
Silver
ug/L
ND
250
250
255
257
102
103
70-130
1
20
Thallium
ug/L
ND
500
500
441
450
88
90
70-130
2
20
Zinc
ug/L
6290
500
500
6540
6640
50
70
70-130
2
20 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 590708 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537002
METHOD BLANK: 3118555
Matrix:
Water
Associated Lab Samples: 92511537002
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Zinc
ug/L
ND
10.0
9.5 01/05/2118:12
LABORATORY CONTROL SAMPLE:
3118556
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Zinc
ug/L
500
476 95
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118557 3118558
MS MSD
92511537002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Zinc ug/L 68.1 500 500 567 580 100 102 70-130 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 586977 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Dissolved
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537001
METHOD BLANK: 3102330
Associated Lab Samples: 92511537001
Parameter Units
Zinc, Dissolved ug/L
LABORATORY CONTROL SAMPLE: 3102331
Parameter Units
Zinc, Dissolved ug/L
Matrix: Water
Blank Reporting
Result Limit
ND 10.0
Spike LCS
Conc. Result
500 449
MDL Analyzed Qualifiers
2.5 12/16/20 21:40
LCS % Rec
% Rec Limits Qualifiers
90 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102332 3102333
MS MSD
92511537001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Zinc, Dissolved ug/L 32.5 500 500 62.3 470 6 88 70-130 153 20 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 590706 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Dissolved
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537002
METHOD BLANK: 3118545
Associated Lab Samples: 92511537002
Parameter Units
Zinc, Dissolved ug/L
LABORATORY CONTROL SAMPLE: 3118546
Parameter Units
Zinc, Dissolved ug/L
Matrix: Water
Blank Reporting
Result Limit
ND 10.0
Spike LCS
Conc. Result
500 472
MDL Analyzed Qualifiers
2.5 01/05/2117:11
LCS % Rec
% Rec Limits Qualifiers
94 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3118547 3118548
MS MSD
92511537002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Zinc, Dissolved ug/L 68.0 500 500 543 535 95 93 70-130 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587031 Analysis Method: EPA 624.1
QC Batch Method: EPA 624.1 Analysis Description: 624 MSV with Acrolein
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3102522
Associated Lab Samples: 92511537003, 92511537004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
0.35
12/15/20 11:41
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
0.34
12/15/20 11:41
1,1,2-Trichloroethane
ug/L
ND
2.0
0.31
12/15/20 11:41
1,1-Dichloroethane
ug/L
ND
2.0
0.51
12/15/20 11:41
1,1-Dichloroethene
ug/L
ND
2.0
0.41
12/15/20 11:41
1,2-Dichlorobenzene
ug/L
ND
2.0
0.24
12/15/20 11:41
1,2-Dichloroethane
ug/L
ND
2.0
0.34
12/15/20 11:41
1,2-Dichloropropane
ug/L
ND
2.0
0.27
12/15/20 11:41
1,3-Dichlorobenzene
ug/L
ND
2.0
0.31
12/15/20 11:41
1,4-Dichlorobenzene
ug/L
ND
2.0
0.41
12/15/20 11:41
Acrolein
ug/L
ND
5.0
3.8
12/15/20 11:41
Benzene
ug/L
ND
1.0
0.38
12/15/20 11:41
Bromod ichloromethane
ug/L
ND
2.0
0.24
12/15/20 11:41
Bromoform
ug/L
ND
2.0
0.40
12/15/20 11:41
Bromomethane
ug/L
ND
2.0
1.2
12/15/20 11:41
Carbon tetrachloride
ug/L
ND
2.0
0.29
12/15/20 11:41
Chlorobenzene
ug/L
ND
2.0
0.37
12/15/20 11:41
Chloroethane
ug/L
ND
2.0
1.4
12/15/20 11:41
Chloroform
ug/L
ND
2.0
0.58
12/15/20 11:41
Chloromethane
ug/L
ND
2.0
0.73
12/15/20 11:41
cis-1,2-Dichloroethene
ug/L
ND
2.0
0.42
12/15/20 11:41
cis-1,3-Dichloropropene
ug/L
ND
2.0
0.33
12/15/20 11:41
Dibromochloromethane
ug/L
ND
2.0
0.32
12/15/20 11:41
Ethylbenzene
ug/L
ND
1.0
0.28
12/15/20 11:41
Methylene Chloride
ug/L
ND
2.0
0.24
12/15/20 11:41
Tetrachloroethene
ug/L
ND
2.0
0.28
12/15/20 11:41
Toluene
ug/L
ND
1.0
0.44
12/15/20 11:41
trans-1,2-Dichloroethene
ug/L
ND
2.0
0.42
12/15/20 11:41
trans-1,3-Dichloropropene
ug/L
ND
2.0
0.41
12/15/20 11:41
Trichloroethene
ug/L
ND
2.0
0.36
12/15/20 11:41
Trich lo rofluoro methane
ug/L
ND
2.0
0.28
12/15/20 11:41
Vinyl chloride
ug/L
ND
2.0
0.72
12/15/20 11:41
1,2-Dichloroethane-d4 (S)
%
91
70-130
12/15/20 11:41
4-Bromofluorobenzene (S)
%
95
70-130
12/15/20 11:41
Toluene-d8 (S)
%
97
70-130
12/15/20 11:41
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE:
Parameter
3102523
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1-Trichloroethane
ug/L
20
16.2
81
70-130
1,1,2,2-Tetrachloroethane
ug/L
20
21.9
110
70-130
1,1,2-Trichloroethane
ug/L
20
17.8
89
70-130
1,1-Dichloroethane
ug/L
20
16.3
81
70-130
1,1-Dichloroethene
ug/L
20
16.0
80
70-132
1,2-Dichlorobenzene
ug/L
20
23.5
118
70-130
1,2-Dichloroethane
ug/L
20
15.1
76
70-130
1,2-Dichloropropane
ug/L
20
18.4
92
70-130
1,3-Dichlorobenzene
ug/L
20
23.5
118
70-130
1,4-Dichlorobenzene
ug/L
20
23.7
118
70-130
Acrolein
ug/L
100
106
106
60-140
Benzene
ug/L
20
18.1
91
70-130
Bromod ichloromethane
ug/L
20
16.9
85
70-130
Bromoform
ug/L
20
18.7
94
70-130
Bromomethane
ug/L
20
18.1
91
30-177
Carbon tetrachloride
ug/L
20
17.9
89
70-130
Chlorobenzene
ug/L
20
21.8
109
70-130
Chloroethane
ug/L
20
15.8
79
46-131
Chloroform
ug/L
20
15.5
78
70-130
Chloromethane
ug/L
20
14.8
74
49-130
cis-1,2-Dichloroethene
ug/L
20
15.3
77
70-130
cis-1,3-Dichloropropene
ug/L
20
18.6
93
70-130
Dibromochloromethane
ug/L
20
21.7
109
70-130
Ethylbenzene
ug/L
20
21.5
108
70-130
Methylene Chloride
ug/L
20
14.1
71
68-130
Tetrachloroethene
ug/L
20
22.1
110
70-130
Toluene
ug/L
20
18.1
90
70-130
trans-1,2-Dichloroethene
ug/L
20
16.3
82
70-130
trans-1,3-Dichloropropene
ug/L
20
18.0
90
70-130
Trichloroethene
ug/L
20
18.8
94
70-130
Trich lo rofluoro methane
ug/L
20
16.7
84
61-130
Vinyl chloride
ug/L
20
15.4
77
59-142
1,2-Dichloroethane-d4 (S)
%
87
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
94
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102524
3102525
MS
MSD
92511537004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,1,1-Trichloroethane
ug/L
ND
20
20
15.9
18.1
80
90
70-148
13
21
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
20.1
21.4
100
107
70-131
7
30
1,1,2-Trichloroethane
ug/L
ND
20
20
16.9
18.2
85
91
70-136
7
27
1,1-Dichloroethane
ug/L
ND
20
20
15.5
17.8
77
89
71-143
14
30
1,1-Dichloroethene
ug/L
ND
20
20
14.8
17.6
74
88
70-158
17
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102524
3102525
MS
MSD
92511537004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,2-Dichlorobenzene
ug/L
ND
20
20
21.5
24.1
107
121
70-133
12
30
1,2-Dichloroethane
ug/L
ND
20
20
13.9
16.3
70
81
72-137
15
29 M1
1,2-Dichloropropane
ug/L
ND
20
20
17.3
19.5
87
98
70-138
12
30
1,3-Dichlorobenzene
ug/L
ND
20
20
22.0
24.6
110
123
75-133
11
24
1,4-Dichlorobenzene
ug/L
ND
20
20
21.8
24.2
109
121
70-133
11
30
Acrolein
ug/L
ND
100
100
91.6
101
92
101
50-150
9
30
Benzene
ug/L
ND
20
20
17.5
19.5
88
97
75-125
11
30
Bromod ichloromethane
ug/L
ND
20
20
15.3
17.4
77
87
70-138
13
30
Bromoform
ug/L
ND
20
20
15.8
18.8
79
94
57-138
17
25
Bromomethane
ug/L
ND
20
20
16.0
17.8
80
89
10-200
10
35
Carbon tetrachloride
ug/L
ND
20
20
17.0
18.9
85
94
70-125
10
26
Chlorobenzene
ug/L
ND
20
20
21.0
23.3
105
117
82-137
10
29
Chloroethane
ug/L
ND
20
20
14.7
17.9
74
90
51-166
20
30
Chloroform
ug/L
ND
20
20
15.3
17.6
77
88
70-121
14
30
Chloromethane
ug/L
ND
20
20
13.6
16.0
68
80
24-161
16
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
14.6
17.1
73
85
67-148
16
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
17.4
19.5
87
98
70-142
11
30
Dibromochloromethane
ug/L
ND
20
20
19.4
22.4
97
112
69-133
14
30
Ethylbenzene
ug/L
ND
20
20
20.5
22.7
102
113
75-134
10
30
Methylene Chloride
ug/L
ND
20
20
13.0
14.9
65
75
64-148
14
30
Tetrachloroethene
ug/L
ND
20
20
21.2
23.7
106
119
70-133
11
23
Toluene
ug/L
ND
20
20
17.2
18.8
86
94
75-134
9
22
trans-1,2-Dichloroethene
ug/L
ND
20
20
14.8
17.7
74
89
70-143
18
27
trans-1,3-Dichloropropene
ug/L
ND
20
20
16.4
18.2
82
91
70-138
10
30
Trichloroethene
ug/L
ND
20
20
18.2
20.4
91
102
75-138
11
29
Trich lo rofluoro methane
ug/L
ND
20
20
14.7
18.4
74
92
61-154
22
30
Vinyl chloride
ug/L
ND
20
20
14.5
17.1
73
85
55-172
16
30
1,2-Dichloroethane-d4 (S)
%
85
93
70-130
4-Bromofluorobenzene (S)
%
93
98
70-130
Toluene-d8(S)
%
93
94
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587108 Analysis Method: EPA 608.3
QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3103046
Associated Lab Samples: 92511537003, 92511537004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
4,4'-DDD
ug/L
ND
0.050
0.0069
12/17/20 22:19
4,4'-DDE
ug/L
ND
0.050
0.0064
12/17/20 22:19
4,4'-DDT
ug/L
ND
0.050
0.018
12/17/20 22:19
Aldrin
ug/L
ND
0.050
0.022
12/17/20 22:19
alpha-BHC
ug/L
ND
0.050
0.019
12/17/20 22:19
alpha -Chlordane
ug/L
ND
0.050
0.0090
12/17/20 22:19
beta-BHC
ug/L
ND
0.050
0.014
12/17/20 22:19
Chlordane (Technical)
ug/L
ND
0.50
0.14
12/17/20 22:19
delta-BHC
ug/L
ND
0.050
0.020
12/17/20 22:19
Dieldrin
ug/L
ND
0.050
0.0073
12/17/20 22:19
Endosulfan I
ug/L
ND
0.050
0.0094
12/17/20 22:19
Endosulfan 11
ug/L
ND
0.050
0.0065
12/17/20 22:19
Endosulfan sulfate
ug/L
ND
0.050
0.0091
12/17/20 22:19
Endrin
ug/L
ND
0.050
0.0089
12/17/20 22:19
Endrin aldehyde
ug/L
ND
0.050
0.013
12/17/20 22:19
gamma-BHC (Lindane)
ug/L
ND
0.050
0.012
12/17/20 22:19
gamma -Chlordane
ug/L
ND
0.050
0.017
12/17/20 22:19
Heptachlor
ug/L
ND
0.050
0.016
12/17/20 22:19
Heptachlor epoxide
ug/L
ND
0.050
0.0097
12/17/20 22:19
PCB-1016 (Aroclor 1016)
ug/L
ND
0.50
0.22
12/17/20 22:19
PCB-1221 (Aroclor 1221)
ug/L
ND
0.50
0.32
12/17/20 22:19
PCB-1232 (Aroclor 1232)
ug/L
ND
0.50
0.21
12/17/20 22:19
PCB-1242 (Aroclor 1242)
ug/L
ND
0.50
0.44
12/17/20 22:19
PCB-1248 (Aroclor 1248)
ug/L
ND
0.50
0.34
12/17/20 22:19
PCB-1254 (Aroclor 1254)
ug/L
ND
0.50
0.24
12/17/20 22:19
PCB-1260 (Aroclor 1260)
ug/L
ND
0.50
0.30
12/17/20 22:19
Toxaphene
ug/L
ND
0.50
0.19
12/17/20 22:19
Decachlorobiphenyl (S)
%
231
10-184
12/17/20 22:19 S3
Tetrachloro-m-xylene (S)
%
133
10-154
12/17/20 22:19
LABORATORY CONTROL SAMPLE:
3103047
Spike LCS LCS
% Rec
Parameter
Units
Cone. Result % Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
5 4.4 89
50-137
PCB-1260 (Aroclor 1260)
ug/L
5 4.5 89
42-140
Decachlorobiphenyl (S)
%
209
10-184 SO
Tetrachloro-m-xylene (S)
%
117
10-154
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE:
Parameter
3103079
Units
Spike
Cone.
LCS
Result
4,4'-DDD
ug/L
0.25
0.28
4,4'-DDE
ug/L
0.25
0.26
4,4'-DDT
ug/L
0.25
0.33
Aldrin
ug/L
0.25
0.14
alpha-BHC
ug/L
0.25
0.30
alpha -Chlordane
ug/L
0.25
0.25
beta-BHC
ug/L
0.25
0.34
delta-BHC
ug/L
0.25
0.28
Dieldrin
ug/L
0.25
0.28
Endosulfan I
ug/L
0.25
0.27
Endosulfan 11
ug/L
0.25
0.30
Endosulfan sulfate
ug/L
0.25
0.34
Endrin
ug/L
0.25
0.27
Endrin aldehyde
ug/L
0.25
0.30
gamma-BHC (Lindane)
ug/L
0.25
0.31
gamma -Chlordane
ug/L
0.25
0.29
Heptachlor
ug/L
0.25
0.19
Heptachlor epoxide
ug/L
0.25
0.24
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
LCS
% Rec
% Rec
Limits Qualifiers
114
45-141
104
37-141
133
52-160
55
42-130
121
37-139
100
45-139
134
39-147
113
39-140
112
40-146
107
45-145
119
47-153
136
48-144
109
41-147
119
45-146
125
42-140
117
45-140
77
34-135
97
39-142
245
10-184 SO
154
10-154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103048
3103049
MS
MSD
92511537003 Spike
Spike MS MSD
MS
MSD
% Rec
Max
Parameter
Units Result Cone.
Cone. Result Result
% Rec
% Rec
Limits
RPD RPD Qual
PCB-1016 (Aroclor 1016)
ug/L ND 5
5 4.7 5.0
93
100
50-140
7 36
PCB-1260 (Aroclor 1260)
ug/L ND 5
5 5.2 5.6
104
112
42-140
7 38
Decachlorobiphenyl (S)
%
184
179
10-184
Tetrachloro-m-xylene (S)
%
129
125
10-154
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103080 3103081
MS
MSD
92511537003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
4,4'-DDD
ug/L
ND
0.25
0.25
0.40
0.37
159
146
36-141
9
39 M1
4,4'-DDE
ug/L
ND
0.25
0.25
0.37
0.37
146
147
31-145
1
35 M1
4,4'-DDT
ug/L
ND
0.25
0.25
0.36
0.36
145
143
25-160
1
42
Aldrin
ug/L
ND
0.25
0.25
0.21
0.26
86
105
42-140
21
35
alpha-BHC
ug/L
ND
0.25
0.25
0.29
0.30
117
120
37-140
3
36
alpha -Chlordane
ug/L
ND
0.25
0.25
0.34
0.34
136
135
45-140
1
35
beta-BHC
ug/L
ND
0.25
0.25
0.42
0.43
167
172
30-147
3
44 M1
delta-BHC
ug/L
ND
0.25
0.25
0.37
0.38
147
153
32-140
4
52 M1
Dieldrin
ug/L
ND
0.25
0.25
0.35
0.31
138
123
36-146
11
49
Endosulfan I
ug/L
ND
0.25
0.25
0.33
0.35
133
138
45-153
3
28
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103080
3103081
MS
MSD
92511537003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Endosulfan II
ug/L
ND
0.25
0.25
0.39
0.38
155
151
27-176
3
53
Endosulfan sulfate
ug/L
ND
0.25
0.25
0.39
0.38
157
154
31-144
2
38 M1
Endrin
ug/L
ND
0.25
0.25
0.37
0.36
147
143
30-147
3
48
Endrin aldehyde
ug/L
ND
0.25
0.25
0.32
0.33
127
130
16-177
3
30
gamma-BHC (Lindane)
ug/L
ND
0.25
0.25
0.33
0.34
130
137
32-140
5
39
gamma -Chlordane
ug/L
ND
0.25
0.25
0.40
0.39
161
155
45-140
4
35 M1
Heptachlor
ug/L
ND
0.25
0.25
0.26
0.31
102
122
34-140
17
43
Heptachlor epoxide
ug/L
ND
0.25
0.25
0.32
0.30
130
121
37-142
7
26
Decachlorobiphenyl (S)
%
232
289
10-184
SO
Tetrachloro-m-xylene (S)
%
127
222
10-154
SO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587125 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3103116
Associated Lab Samples: 92511537003, 92511537004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
1.7
12/16/20 10:45
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
1.2
12/16/20 10:45
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.6
12/16/20 10:45
2,4-Dichlorophenol
ug/L
ND
5.0
1.4
12/16/20 10:45
2,4-Dimethylphenol
ug/L
ND
10.0
1.7
12/16/20 10:45
2,4-Di nitro phenol
ug/L
ND
50.0
26.0
12/16/20 10:45
2,4-Dinitrotoluene
ug/L
ND
5.0
1.6
12/16/20 10:45
2,6-Dinitrotoluene
ug/L
ND
5.0
1.7
12/16/20 10:45
2-Chloronaphthalene
ug/L
ND
5.0
1.7
12/16/20 10:45
2-Chlorophenol
ug/L
ND
5.0
1.2
12/16/20 10:45
2-Nitrophenol
ug/L
ND
5.0
1.4
12/16/20 10:45
3,3'-Dichlorobenzidine
ug/L
ND
10.0
8.1
12/16/20 10:45
4,6-Dinitro-2-methyl phenol
ug/L
ND
10.0
3.4
12/16/20 10:45
4-Bromophenylphenyl ether
ug/L
ND
5.0
1.8
12/16/20 10:45
4-Chloro-3-methyl phenol
ug/L
ND
5.0
3.3
12/16/20 10:45
4-Chlorophenylphenyl ether
ug/L
ND
5.0
2.0
12/16/20 10:45
4-Nitrophenol
ug/L
ND
10.0
6.6
12/16/20 10:45
Acenaphthene
ug/L
ND
5.0
2.0
12/16/20 10:45
Acenaphthylene
ug/L
ND
5.0
2.0
12/16/20 10:45
Anthracene
ug/L
ND
5.0
2.3
12/16/20 10:45
Benzo(a)anthracene
ug/L
ND
5.0
2.7
12/16/20 10:45
Benzo(a)pyrene
ug/L
ND
5.0
2.8
12/16/20 10:45
Benzo(b)fluoranthene
ug/L
ND
5.0
2.6
12/16/20 10:45
Benzo(g,h,i)perylene
ug/L
ND
5.0
2.8
12/16/20 10:45
Benzo(k)fluoranthene
ug/L
ND
5.0
2.7
12/16/20 10:45
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
1.8
12/16/20 10:45
bis(2-Chloroethyl) ether
ug/L
ND
5.0
1.9
12/16/20 10:45
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
3.7
12/16/20 10:45
Butylbenzylphtha late
ug/L
ND
5.0
3.1
12/16/20 10:45
Chrysene
ug/L
ND
5.0
2.8
12/16/20 10:45
Di-n-butylphthalate
ug/L
ND
5.0
2.2
12/16/20 10:45
Di-n-octylphthalate
ug/L
ND
5.0
3.9
12/16/20 10:45
Dibenz(a,h)anthracene
ug/L
ND
5.0
3.0
12/16/20 10:45
Diethylphthalate
ug/L
ND
5.0
2.0
12/16/20 10:45
Dimethylphthalate
ug/L
ND
5.0
2.1
12/16/20 10:45
Fluoranthene
ug/L
ND
5.0
2.2
12/16/20 10:45
Fluorene
ug/L
ND
5.0
2.1
12/16/20 10:45
Hexachloro-1,3-butadiene
ug/L
ND
5.0
1.8
12/16/20 10:45
Hexachlorobenzene
ug/L
ND
5.0
2.2
12/16/20 10:45
Hexachlorocyclopentadiene
ug/L
ND
10.0
1.6
12/16/20 10:45
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
METHOD BLANK: 3103116
Associated Lab Samples: 92511537003, 92511537004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Hexachloroethane
ug/L
ND
5.0
1.4
12/16/20 10:45
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
2.9
12/16/20 10:45
Isophorone
ug/L
ND
10.0
1.7
12/16/20 10:45
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
1.3
12/16/20 10:45
N-Nitrosodimethylamine
ug/L
ND
5.0
1.9
12/16/20 10:45
N-Nitrosodiphenylamine
ug/L
ND
10.0
3.0
12/16/20 10:45
Naphthalene
ug/L
ND
5.0
2.1
12/16/20 10:45
Nitrobenzene
ug/L
ND
5.0
1.9
12/16/20 10:45
Pentachlorophenol
ug/L
ND
10.0
3.8
12/16/20 10:45
Phenanthrene
ug/L
ND
5.0
2.0
12/16/20 10:45
Phenol
ug/L
ND
5.0
1.4
12/16/20 10:45
Pyrene
ug/L
ND
5.0
2.2
12/16/20 10:45
2,4,6-Tribromophenol (S)
%
107
10-137
12/16/20 10:45
2-Fluorobiphenyl (S)
%
74
15-120
12/16/20 10:45
2-Fluorophenol (S)
%
63
10-120
12/16/20 10:45
Nitrobenzene-d5 (S)
%
109
10-120
12/16/20 10:45
Phenol-d6 (S)
%
56
10-120
12/16/20 10:45
Terphenyl-d14 (S)
%
125
11-131
12/16/20 10:45
LABORATORY CONTROL SAMPLE:
Parameter
3103117
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
24.9
50
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
35.9
72
36-166
2,4,6-Trichlorophenol
ug/L
50
44.6
89
37-144
2,4-Dichlorophenol
ug/L
50
41.0
82
1-191
2,4-Dimethylphenol
ug/L
50
41.3
83
32-119
2,4-Di nitro phenol
ug/L
250
282
113
1-181
2,4-Dinitrotoluene
ug/L
50
38.3
77
39-139
2,6-Dinitrotoluene
ug/L
50
46.5
93
50-158
2-Chloronaphthalene
ug/L
50
34.4
69
60-118
2-Chlorophenol
ug/L
50
38.8
78
23-134
2-Nitrophenol
ug/L
50
45.0
90
29-182
3,3'-Dichlorobenzidine
ug/L
100
88.5
89
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
143
143
1-181
4-Bromophenylphenyl ether
ug/L
50
42.5
85
53-127
4-Chloro-3-methyl phenol
ug/L
100
94.3
94
22-147
4-Chlorophenylphenyl ether
ug/L
50
38.2
76
25-158
4-Nitrophenol
ug/L
250
202
81
1-132
Acenaphthene
ug/L
50
36.6
73
47-145
Acenaphthylene
ug/L
50
36.8
74
33-145
Anthracene
ug/L
50
36.5
73
1-166
Benzo(a)anthracene
ug/L
50
41.2
82
33-143
Benzo(a)pyrene
ug/L
50
41.4
83
17-163
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
LABORATORY CONTROL SAMPLE:
Parameter
3103117
Units
Spike
Cone.
LCS
Result
1-CS
% Rec
% Rec
Limits
Benzo(b)fluoranthene
ug/L
50
40.9
82
24-159
Benzo(g,h,i)perylene
ug/L
50
44.2
88
1-219
Benzo(k)fluoranthene
ug/L
50
40.8
82
11-162
bis(2-Chloroethoxy)methane
ug/L
50
39.8
80
33-184
bis(2-Chloroethyl) ether
ug/L
50
36.4
73
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
49.3
99
8-158
Butylbenzylphthalate
ug/L
50
50.3
101
1-152
Chrysene
ug/L
50
40.6
81
17-168
Di-n-butylphthalate
ug/L
50
44.4
89
1-118
Di-n-octylphthalate
ug/L
50
54.5
109
4-146
Dibenz(a,h)anthracene
ug/L
50
45.4
91
1-227
Diethylphthalate
ug/L
50
41.1
82
1-114
Dimethylphthalate
ug/L
50
39.4
79
1-112
Fluoranthene
ug/L
50
42.1
84
26-137
Fluorene
ug/L
50
38.6
77
59-121
Hexachloro-1,3-butadiene
ug/L
50
20.9
42
24-116
Hexachlorobenzene
ug/L
50
38.2
76
1-152
Hexachlorocyclopentadiene
ug/L
50
25.5
51
25-150
Hexachloroethane
ug/L
50
21.4
43
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
45.6
91
1-171
Isophorone
ug/L
50
34.8
70
21-196
N-Nitroso-di-n-propylamine
ug/L
50
35.9
72
1-230
N-Nitrosodimethylamine
ug/L
50
45.8
92
25-150
N-Nitrosodiphenylamine
ug/L
50
40.6
81
25-150
Naphthalene
ug/L
50
28.9
58
21-133
Nitrobenzene
ug/L
50
36.8
74
35-180
Pentachlorophenol
ug/L
100
95.4
95
14-176
Phenanthrene
ug/L
50
40.7
81
54-120
Phenol
ug/L
50
32.5
65
5-112
Pyrene
ug/L
50
40.4
81
52-115
2,4,6-Tribromophenol (S)
%
110
10-137
2-Fluorobiphenyl (S)
%
67
15-120
2-Fluorophenol(S)
%
67
10-120
Nitrobenzene-d5 (S)
%
79
10-120
Phenol-d6 (S)
%
58
10-120
Terphenyl-d14 (S)
%
93
11-131
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103118
3103119
MS
MSD
92511577001 Spike
Spike MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result Cone.
Cone. Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
1,2,4-Trichlorobenzene
ug/L
ND 50
50 18.7
16.5
37
33
44-142
12 30 M1
2,2'-Oxybis(1-
ug/L
ND 50
50 46.8
42.8
94
86
36-166
9 30
chloropropane)
2,4,6-Trichlorophenol
ug/L
ND 50
50 54.2
33.7
108
67
37-144
47 30 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103118
MS
92511577001 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
3103119
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
2,4-Dichlorophenol
ug/L
ND
50
50
48.7
42.5
97
85
1-191
14
30
2,4-Dimethylphenol
ug/L
ND
50
50
47.7
38.2
95
76
32-119
22
30
2,4-Di nitro phenol
ug/L
ND
250
250
77.6
ND
31
7
1-181
30
2,4-Dinitrotoluene
ug/L
ND
50
50
44.1
39.1
88
78
39-139
12
30
2,6-Dinitrotoluene
ug/L
ND
50
50
59.9
56.1
120
112
50-158
7
30
2-Chloronaphthalene
ug/L
ND
50
50
33.3
30.2
67
60
60-118
10
30
2-Chlorophenol
ug/L
ND
50
50
46.0
40.7
92
81
23-134
12
30
2-Nitrophenol
ug/L
ND
50
50
54.1
48.5
108
97
29-182
11
30
3,3'-Dichlorobenzidine
ug/L
ND
100
100
108
108
108
108
1-262
0
30
4,6-Dinitro-2-methyl phenol
ug/L
ND
100
100
141
38.3
141
38
1-181
115
30 R1
4-Bromophenylphenyl ether
ug/L
ND
50
50
47.0
43.9
94
88
53-127
7
30
4-Chloro-3-methyl phenol
ug/L
ND
100
100
113
105
113
105
22-147
7
30
4-Chlorophenylphenyl ether
ug/L
ND
50
50
40.2
36.5
80
73
25-158
10
30
4-Nitrophenol
ug/L
ND
250
250
146
35.8
58
14
1-132
121
30 R1
Acenaphthene
ug/L
ND
50
50
39.5
34.7
79
69
47-145
13
30
Acenaphthylene
ug/L
ND
50
50
41.0
36.7
82
73
33-145
11
30
Anthracene
ug/L
ND
50
50
44.0
41.5
88
83
1-166
6
30
Benzo(a)anthracene
ug/L
ND
50
50
52.0
51.3
104
103
33-143
2
30
Benzo(a)pyrene
ug/L
ND
50
50
53.5
52.2
107
104
17-163
3
30
Benzo(b)fluoranthene
ug/L
ND
50
50
52.2
51.7
104
103
24-159
1
30
Benzo(g,h,i)perylene
ug/L
ND
50
50
55.2
55.3
110
111
1-219
0
30
Benzo(k)fluoranthene
ug/L
ND
50
50
53.1
52.5
106
105
11-162
1
30
bis(2-
ug/L
ND
50
50
48.5
46.6
97
93
33-184
4
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/L
ND
50
50
48.3
44.8
97
90
12-158
8
30
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
50
59.6
59.6
119
119
8-158
0
30
Butylbenzylphtha late
ug/L
ND
50
50
62.0
60.8
124
122
1-152
2
30
Chrysene
ug/L
ND
50
50
51.2
50.3
102
101
17-168
2
30
Di-n-butylphthalate
ug/L
ND
50
50
56.3
54.8
113
110
1-118
3
30
Di-n-octylphthalate
ug/L
ND
50
50
65.4
64.9
131
130
4-146
1
30
Dibenz(a,h)anthracene
ug/L
ND
50
50
56.9
57.1
114
114
1-227
0
30
Diethylphthalate
ug/L
ND
50
50
52.5
50.1
105
100
1-114
5
30
Dimethylphthalate
ug/L
ND
50
50
50.0
46.5
100
93
1-112
7
30
Fluoranthene
ug/L
ND
50
50
53.3
51.2
107
102
26-137
4
30
Fluorene
ug/L
ND
50
50
44.1
39.6
88
79
59-121
11
30
Hexachloro-1,3-butadiene
ug/L
ND
50
50
4.9J
4.OJ
10
8
24-116
30 M1
Hexachlorobenzene
ug/L
ND
50
50
43.8
41.1
88
82
1-152
6
30
Hexachlorocyclopentadiene
ug/L
ND
50
50
8.6J
7.1J
17
14
25-150
30 M1
Hexachloroethane
ug/L
ND
50
50
6.9
5.4
14
11
40-113
24
30 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
50
57.4
56.9
115
114
1-171
1
30
Isophorone
ug/L
ND
50
50
43.2
40.9
86
82
21-196
5
30
N-Nitroso-di-n-propylamine
ug/L
ND
50
50
44.4
42.6
89
85
1-230
4
30
N-Nitrosodimethylamine
ug/L
ND
50
50
48.1
46.1
96
92
25-150
4
30
N-Nitrosodiphenylamine
ug/L
ND
50
50
50.5
46.9
101
94
25-150
7
30
Naphthalene
ug/L
ND
50
50
31.3
28.4
63
57
21-133
10
30
Nitrobenzene
ug/L
ND
50
50
46.3
43.8
93
88
35-180
6
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3103118
MS
92511577001 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
3103119
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
Pentachlorophenol
ug/L
ND 100
100
122
49.3
122
49
14-176
85
30 R1
Phenanthrene
ug/L
ND 50
50
48.7
45.7
97
91
54-120
7
30
Phenol
ug/L
ND 50
50
33.8
31.0
68
62
5-112
9
30
Pyrene
ug/L
ND 50
50
49.3
48.7
99
97
52-115
1
30
2,4,6-Tribromophenol (S)
%
136
109
10-137
2-Fluorobiphenyl (S)
%
53
50
15-120
2-Fluorophenol (S)
%
65
53
10-120
Nitrobenzene-d5 (S)
%
90
89
10-120
Phenol-d6 (S)
%
55
55
10-120
Terphenyl-d14 (S)
%
115
115
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587549 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537001, 92511537002
METHOD BLANK: 3105210
Matrix:
Water
Associated Lab Samples: 92511537001, 92511537002
Blank
Reporting
Parameter
Units
Result
Limit
Total Suspended Solids
mg/L
ND
2.5
LABORATORY CONTROL SAMPLE:
3105211
Spike
LCS
Parameter
Units
Cone.
Result
Total Suspended Solids
mg/L
250
254
SAMPLE DUPLICATE: 3105691
92511268001
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg/L
348
388
SAMPLE DUPLICATE: 3105692
92511502001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 659 595
MDL Analyzed Qualifiers
2.5 12/16/20 22:28
LCS % Rec
% Rec Limits Qualifiers
102 90-110
Max
RPD RPD Qualifiers
11 25
Max
RPD RPD Qualifiers
10 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 587535 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3105108 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Phenol mg/L ND 0.020 0.0076 12/17/2014:45
LABORATORY CONTROL SAMPLE: 3105109
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phenol mg/L 0.05 0.047 93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105110 3105111
MS MSD
35596343001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Phenol mg/L 0.00761-1 0.05 0.05 0.055 0.040 97 67 90-110 32 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3105125 3105126
MS MSD
92511148001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Phenol mg/L ND 0.05 0.05 0.050 0.044 96 85 90-110 12 10 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 35 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Crane Resistoflex
Pace Project No.: 92511537
QC Batch: 586885 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92511537003, 92511537004
METHOD BLANK: 3102109 Matrix: Water
Associated Lab Samples: 92511537003, 92511537004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Cyanide mg/L ND 0.0080 0.0060 12/15/20 23:30
LABORATORY CONTROL SAMPLE: 3102110
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Cyanide mg/L 0.1 0.10 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102144 3102145
MS MSD
92511537003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.020 0.064 19 64 80-120 105 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3102146 3102147
MS MSD
92511537004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/L ND 0.1 0.1 0.091 0.084 91 84 80-120 7 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 41

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Project: Crane Resistoflex
Pace Project No.: 92511537
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /11 /2021 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 41

aceAnalytical
www.pacelahs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Crane Resistoflex
92511537
Analytical
Lab ID
Sample
ID
QC Batch Method
QC Batch
Analytical
Method
Batch
92511537001
OF-001
EPA 1664B
588138
92511537002
OF-002
EPA1664B
588138
92511537003
OF-001
TTO
EPA 608.3
587108
EPA 608.3
587726
92511537004
OF-002
TTO
EPA 608.3
587108
EPA 608.3
587726
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7
Rev 4.4 1994
587689
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7
Rev 4.4 1994
587689
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
590708
EPA 200.7
Rev 4.4 1994
590740
92511537003
OF-001
TTO
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7
Rev 4.4 1994
587689
92511537004
OF-002
TTO
EPA 200.7 Rev 4.4 1994
587665
EPA 200.7
Rev 4.4 1994
587689
92511537001
OF-001
EPA 200.7 Rev 4.4 1994
586977
EPA 200.7
Rev 4.4 1994
587006
92511537002
OF-002
EPA 200.7 Rev 4.4 1994
590706
EPA 200.7
Rev 4.4 1994
590776
92511537003
OF-001
TTO
EPA 245.1 Rev 3.0 1994
587409
EPA 245.1
Rev 3.0 1994
587457
92511537004
OF-002
TTO
EPA 245.1 Rev 3.0 1994
587409
EPA 245.1
Rev 3.0 1994
587457
92511537003
OF-001
TTO
EPA 625.1
587125
EPA 625.1
587394
92511537004
OF-002
TTO
EPA 625.1
587125
EPA 625.1
587394
92511537003
OF-001
TTO
EPA 624.1
587031
92511537004
OF-002
TTO
EPA 624.1
587031
92511537001
OF-001
SM 2540D-2011
587549
92511537002
OF-002
SM 254OD-2011
587549
92511537003
OF-001
TTO
EPA 420.4 Rev 1.0 1993
587535
EPA 420.4
Rev 1.0 1993
587822
92511537004
OF-002
TTO
EPA 420.4 Rev 1.0 1993
587535
EPA 420.4
Rev 1.0 1993
587822
92511537003
OF-001
TTO
SM 4500-CN-E-2011
586885
SM 4500-CN-E-2011
586939
92511537004
OF-002
TTO
SM 4500-CN-E-2011
586885
SM 4500-CN-E-2011
586939
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 38 of 41

Document Name: Document Revised: October 28, 2020
acemalytical- Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.D7 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ;' Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[]
Mechanicsville[] Atlanta❑ Kernersville❑
Sample Condition Client Name:
WQ# : 92511537
Upon Receipt — )
Vid ker �'
ProjectA
#:
Courier: ❑Fed Ex OUPS ❑USPS
f❑Client
❑ Commercial ❑Pace ❑Other:
92511537
Custody Seal Present? []Yes "gNo Seals Intact? ❑Yes ❑No
Person Examining Contents: %oi /QU
pate/Initials
Packing Material: El Bubble Wrap Bubble Bags ❑None ❑ Other
Biological Tissue Frozen?
❑Yes ❑No ffN/A
Thermomet
IR Gun ID: C D�Vet ❑Blue
/
❑None
Type of Ice:
Correction Factor:
Cooler Temp: �' R qAdd/Subtract (°C) n
Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): 5 , [
has begun
USDA Regulated $oil (� N/A, water sample)
Did samples originate ifi a quarantine zone within the United States: CA, NY, or SC (check maps)?
rlym 71Nn
Did sanip!es originate from a foreign source (internationally,
incluriimHawaii and Puerto Rico)? ❑Yes ] I}No
Comments/Discrepancy:
Chain of Custody Present?
yes
❑No
El N/A
1.
Samples Arrived within Hold Time?
ZYes
[-]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
No
❑NIA
4.
Sufficient Volume?
Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
4es
Zes
[-]No
[:]No
❑NIA
❑NIA
6.
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Yes
ONO
❑N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Yes
t '
[-]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
El Yes
jZr4o
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
x/ No
❑No
❑N/A
N/A
11.
r
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Lot ID of split containers:
Field Data Required? ❑Yes ❑No
,❑ r a /m
Project Manager SCURF Review: Date:
r' I�
Project Manager 5RF Review:
Date:
Page 39 of 41

*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coli€arm, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottles
Document Name: Document Revised: October 28, 2020
Sample Condition Upon Receipt(SCUR) Page 2 of 2
accAnalytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.07 Pace Carolinas Quality Office
Project # I W®# : 92511537
PM: LJp Due Date: 12/21/20
CLIENT: 93-ALTAMONT
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
Amount of Preservative
Lot k
adjusted
added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certitication Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 40 of 41

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TEMP in C
Received on
Ice
(YIN)
ust�
Sealed
Canter
(Y!N}
Samples
Intact
(YIN)
Z 6 o - % w m L I ITEM #
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SAMPLETEMP AT COLLECTION
# OF CONTAINERS
Unpreserved
N
ry
H2SO4
HNO3
HCI
NsOH
c'
y
Na2S203
Melhanol
Other
Analyses Test
YIN
TSS
Metals (Cu. Pb. Znj
Dissolved Melals - field filter
c
TPH OII and Grease
m
TTO Metals
a
TTO - Cyanide
a
m
TTO -Phenol
w
T
TTO-VOCa
TTO-SVCCs
a
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TTO- Pesticides
z
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Page 41 of 41