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HomeMy WebLinkAboutWQ0023306_Residual Annual Report 2020_20210126Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No If not an application what is the submittal type?* r Annual Report r Residual Annual Report r Additional Information r Other Annual Report Year* 2020 Permit Number (IR)* WQ0023306 Applicant/Permittee Mark Stephens Email Notifications Does this need review by the hydrogeologist?* 0 Yes r No Regional Office Washington CO Reviewer Admin Reviewer Submittal Form Project Contact Information Rease provide inforration on the person to be contacted by N B Staff Name * Tony Hawkins Email Address* ha\M<inst@nev,bernnc.gov electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ .................................................................................................................................................. . Application/Document Type* r New (Fee Req ui red) r Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 2526397555 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0023306 Has Current Existing permt number Applicant/Permittee Address* PO Box 1129 New Bern, NC 28563 Facility Name * City of New Bern DCAR Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Bc.) 2020 report.pdf 6.04MB Upload only 1 FLFdocurrent (less than 250 fvB). Miltiple documents rust be corrbined into one FDFfile unless file is larger than upload limit. * V By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature f� '%r'ClICd�'.�%Cd Submission Date 1/26/2021 NEW BERN NORTH CAROLINA Department of Public Utilities 307 Glenburnie Dr./ P.O. Box 1129 New Bern, NC 28563 January 28, 2021 NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1636 Reference: 2020 Land Application Annual Report City of New Bern CLASS A RESIDUALS Permit Number WQ0023306 The City of New Bern is submitting all monitoring and reporting requirements as specified in the above referenced permit for its land application program for Sewage SIudge. There are three copies included. The City has managed and compiled the submitted data. The City produced approximately 2974 dried tons of sludge during 2020, which met the Class A Sewage Sludge criteria. The city hauled to the Craven County Solid Waste Management Authority to be used for ground cover. The report includes form ACF, form DMSDF, form RSSF, form MFLSF, Lab Sheets, form PVRF 2T. If any further inforination is required, please contact Tony Hawkins at (252) 639-7555. Sincerely, Toi1y Zwkins Treatment Plants Manager Enclosures cc: File Everything comes together here. ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0023306 County: Craven Year: 2020 Facility Name (as shown on permit): City of New Bem Land Application Operator: Tony Hawkins Phone.: (252) 639-7555 Land application of residuals as allowed by the permit occurred during the past calendar year? ❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary. Total number of application fields in thepermit: 1 Total number of fields utilized for land application 'during the year: 1 Total amount of dry tons applied during the year for all application sites: 2,953 Total number of acres utilizes for land application during the year: Craven county land field Part B - Annual Compiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. 21 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permif were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. I 1 I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and re.m.ediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Tony Hawkins Plant Manager Permittee Name and Title k or print) 1-12-z1 Signature of Permittee Date Signature of Prreparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0023306 FACILITY NAME: City of New Bern PHONE: (252) 639-7555 COUNTY: Craven OPERATOR: Tony Hawkins FACILITY TYPE (please check one): v❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes v❑ No ❑ lo If No skip parts A, B, C and certify form below Part A* • Part B*: Month ,Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) intended use(s) January land field 30 lime 168 198 February land field 35 lime 196 231 March land field 35 lime 196 231 April land field 35 lime 188 223 May land field 32 lime 89 121 June land field 36 lime 275 311 July land field 36 lime 224 260 August land field 36 lime 265 301 September Iand field 35 lime 188 223 October land field 36 tirne 269 304 November land field 35 lime 230 262 December land field 36 lime 273 309 Total from FORM DMSDF (sup) Totals: Annual (dry tons): 417 2560 2974 0 Amendment(s) used: 417 BuMn Agent(s) used: lime If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Sapp)p Part C: Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No lo if No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -J,.n � -� L j-22-2-1 ignature of Permittee Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM DMSDF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0023306 Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analvsis Data City of New Bern 23306 City of New Bern Laboratory: 1) 2) 3) 4) 5) Environment 1 Parameter (mg/kg) Ceiling Conc. Limit Sample or Composite Date 1114 3110 418 5112 614 - 718 815 9110 1018 11116 Percent Solids (%) NA 55.55 42.23 54.96 43.36 38.22 Arsenic 75 <2.5 4.9 4.4 <2.5 <2.5 3.3 2.7 <2.5 2.5 <2.5 Cadmium 85 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.72 <0.5 Copper 4,300 62 78 60 52 55 103 87 86 189 82 Chromium NA 7 9 8 8 6 9 8 7 15 7 Lead 840 3.6 3.8 3.2 2.9 3.1 6.3 5.1 5.5 8.3 3.8 Mercury 57 0.09 0.08 0.32 0.09 0.12 - 0.21 0.32 0.11 0.26 0.14 Molybdenum 75 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 6 <5.0 Nickel 420 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 12 <5.0 ,Selenium 100 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Zinc 7,500 155 184 161 127 125 239 215 193 416 1 181 Total Phosphorus NA c7771 c12000 c7937 c4467 c5898 e12080 e15920 c9731 c19450 c15000 TKN NA e14950 c25560 c12340 c11310 e11490 c23530 c20580 c15510 e29330 e20770 Ammonia -Nitrogen NA e12.89 c33.99 c57.48 c21.93 c35.74 c61.68 e73.89 c47.72 c147.2 c47.93 Nitrate and Nitrite NA el95.4 c5798 c79.29 c49.84 c606.6 c79.59 c626.1 c55.68 c19.90 c52.92 " For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Preparer * - *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of New Bern Total Dry Tons Applied (Annual): Permit #: WQ0023306 Cation Exchange Capacity (non 503 only): Operator: Tony Hawkins Owner: City of New Bern Predominant Soil Series: Acres Used: n/a Acres Permitted: Site #: land field Field #: 2974.00 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 1/14/21 2 3/10/21 3 418121 r5/12/21 5 614121 6 718121 7 815121 8 9/10/21 9 1018121 10 11/16/21 11 12 % Solids 55.55 42.23 54.96 43.36 38.22 Arsenic <2.5 4.9 4A <2.5 1 <2.5 3.3 2.7 1 <2.5 2.5 <2.5 Cadmium <0.05 <0.5 1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.72 <0.5 Copper 62 78 60 52 55 103 87 86 189 82 Chromium 7 9 8 8 6 9 8 7 15 7 Lead 3.6 3.8 3.2 2.8 3.1 6.3 5.1 5.5 8.3 3.8 Mercury 0.09 0.08 0.32 0.09 0.12 0.21 0.32 0.11 0.26 0.14 Molyb- denum <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Nickel <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 Selenium <5.0 1 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Zinc 155 184 161 127 125 239 1 215 193 416 181 Total Phos- horus 0771 02000 c7937 c4467 c5898 c12080 c15920 c9731 c19450 c15000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 11 L2]3 4 5 6j L7 8 9 10 11 12 y DT/Ac./ ° App. P Event Arsenic ###### 0.000 0.000 ###### ###### 0.000 0.000 ###### 0.000 ###### 0.000 0.000 ###### Cadmium ###### ###### ###### ###### ###### ###### ###### ###### 0.000 ###### 0.000 0.000 ###### Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- ###### ###### ###### ###### ###### ### ## ###### ###### #4944## ##### 0.000 0.000 ###### denum Nickel ###### ###### ###### ###### ###### ###### 94#444 ###### ###### ###### 0.000 0.000 #49444 Selenium ###### ###### ###### ###### ###### ###### ###### ###### ###### ######1 0.000 0.000 ###### Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 Total Phos- ###### ###### ###### ###### ###### ###### ###### 9#4944 ###### ###### 0.000 0.000 ###### horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" J Sign tore of Land Applier Date DENR FORM MFLSF (1212006) MEAUTOR05w % hvwpumbA 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN .NC 28563 Drinking Water rD: 37713 waste Water ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 01/14/20 DATE REPORTED : 01/17/20 REVIEWED BY: Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-I+C#5 Date Analyst Code Total Solids, % 55,55 50,71 56.59 53.85 54.09 01/14/20 MAR 2540G-11 Fecal Coliform (MPH /gram Solids G 1.8 C 1.8 C 1.8 C 1.8 C 1.8 01/14/20 MAR 9221E-06 Enw, _ Drinking water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 01/14/20 DATE REPORTED : 01/17/20 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % 55.86 47.98 01/14/20 MAR 254OG-11 Fecal Coliform (MPN), /gram Solids G 1.8 C 1.8 01/14/20 MAR 9221E-06 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Silver (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Cyanide (dry weight), mg/kg TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt,), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Holding Analysis Method Basin (RA) Date Analyst Code 2338 02/03/20 LFJ EPA200.7 <2.5 02/04/20 MTM 3113B-04 402156 01/31/20 LFJ EPA200.7 <0.5 01/30/20 MTM 3113E-04 62 02/03/20 LFJ EPA200.7 7 01/31/20 LFJ EPA200.7 3.6 01/29/20 MTM 3113B-04 3785 02/03/20 LFJ EPA200.7 0.09 01/16/20 MTM EPA7471B < 5.0 02/03/20 LFJ EPA200.7 1959 02/03/20 LFJ EPA200.7 <5,0 02/05/20 MTM 3113E-04 <2.5 01/31/20 LFJ EPA200.7 650 02/03/20 LFJ EPA200.7 155 02/03/20 LFJ EPA200.7 17.2 01/21/20 SEJ 4500CNE-11 c 14950 01/17/20 TLT1 351.2 R2-93 c 12.89 01/15/20 TLH 350,1 RZ-93 c 7771 01/17/20 BLD 365.4-74 c 185.4 01/1.5/20 BLD 353.2 R2-93 6167 01/23/20 SEJ <5.0 01/31/20 LFJ EPA200.7 Drinking Water ID: 17715 Wastewater I➢! la PHONE �252) 756-6208 FAX (252) 756-0633 SD#: 214 DATE COLLECTED: 01/14/20 DATE REPORTED : 02/14/20 REVIEWED BY:- c Uncertified data. ➢WR doea not offer ncn-aqueous certification for thin analytical procedure. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. Box 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mglkg Calcium (dry wt. basis), mg/lig Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt, basis), mglkg Potassium (dry wt. basis), mglkg Selenium (dry wt. basis), mglkg Silver (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mglkg Total Cyanide (dry weight), mg/kg TKN (dry wt.), mglkg Ammonia Nitrogen (dry wt.),mglkg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Holding Analysis Method Basin (RA) Date Analyst Code 2372 02/28/20 LFJ EPA200.7 G 2.5 02/28/20 MTM 311313-04 278355 02/29/20 LFJ EPA200.7 0.5 02/26/20 MTM 3113B-04 102 02/26/20 LFJ EPA200.7 11 02/29/20 LFJ EPA200.7 5.6 02125/20 MTM 3113B-04 3713 02/28/20 LFJ EPA200.7 0.25 02/27/20 MTM EPA7471B 5 02/29/20 LFJ EPA200.7 3771 02/29/20 LFJ EPA200.7 G 5.0 03/03/20 MTM 3113E-04 G 2.5 02/26/20 LFJ EPA200.7 < 1250 02/29/20 LFJ EPA200.7 235 02/29/20 LFJ EPA200.7 54.4 02/14/20 SEJ 450OCNE-11 c 27380 02/11/20 TLH 351.2 112-93 c 118.9 02111 /20 AKS 350.1 R2-93 c 10970 02f10/20 DTL 365.4-74 c 53.96 02/11/20 BLD 353.2 112-93 6167 02/10/20 SEJ 6 02/29/20 LFJ EPA200.7 Drinking water ID: 37715 Waatewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 02/05/20 DATE REPORTED : 03/10/20 REVIEWED BY: ;�e_ c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 03/10/20 DATE REPORTED : 03/13/20 REVIEWED BY: Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Bashi-FC#5 Date Analyst Code Total Solids, % 42.23 45.24 48.75 44.12 41.44 03/10/20 KDS 2540G-11 Fecal Coliform (MPH /gram Solids < 1.8 < 1.8 < 1.8 < 1.8 < 1.8 03/10/20 KDS 9221E-06 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID# : 214 A DATE COLLECTED: 03/10/20 DATE REPORTED : 03/13/20 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analvst Code Total Solids, % 48.05 46.85 03/10/20 KDS 2540G-11 Fecal Colfform (MPH /gram Solids <1.8 <1.8 03/10/20 KDS 9221E-06 ERAmmugid Ala JECOTPuMd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mglkg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt, basis), mglkg Silver (dry wt. basis), mglkg Sodium (dry wt. basis), mglkg Zinc (dry wt. basis), mg/kg Total Cyanide (dry weight), mg/kg TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mglkg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Holding Analysis Method Basin (RA) Date Analyst Code 2072 03/18/20 LFJ EPA200.7 4.9 03/31/20 MTM[ 3113B-04 314504 03/18/20 LFJ EPA200.7 < 0.5 03/20/20 MTM 3113B-04 78 03/18/20 LFJ EPA200.7 9 03/18/20 LFJ EPA200.7 3.8 03/18/20 MTM[ 3113B-04 3642 03/18/20 LFJ EPA200.7 0.08 03/23/2Q MTM EPA7471B <5.0 03/18/20 LFJ EPA200.7 ~ 3176 03/18/20 LFJ EPA200.7 <5.0 04/01/20 MTM 311313-04 <2.5 03/18/20 LFJ EPA200.7 <1250 03/18/20 LFJ EPA200.7 184 03/18/20 LFJ EPA200.7 19.6 03/17/20 SEJ 450OCNE-11 c 25560 03/13/20 AKS 351.2 R2-93 c 33.99 0342120 TLH 350.1 112-93 c 12000 03/13/20 BLD 365.4-74 c 57.98 03/12/20 BLD 353.2 R2-93 10285 03/16/20 SEJ <5.0 03/18/20 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 03/10/20 DATE REPORTED : 04/03/20 RE'Vl ,v3L°Fi BY: c uncertified data. DWR does net offer non -aqueous certification for this analytical procedure. Em'OnERM % hmpumbd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Silver (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Cyanide (dry weight), mg/kg TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Holding Analysis Method Basin (RA) Date Analyst Code 1944 04/21/20 LP.) EPA200.7 4.4 04/22/20 NITM 3113B-04 370866 04/21/20 LFJ EPA200.7 <0.5 04/17/20 MTM 31I3B-04 60 04/21/20 LFJ EPA200.7 8 04/21/20 LFJ EPA200.7 3.2 04/20/20 MTM 3113B-04 3739 04/21/20 LFJ EPA200.7 0.32 04/16/20 MTM EPA7471B <5.0 04/21/20 LF.J EPA200.7 ' 3005 04/21/20 LFJ EPA200.7 <5.0 05/01/20 MTM 3113E-04 C2.5 04/21/20 LFJ EPA200.7 < 1250 04/21/20 LFJ EPA200.7 161 04/21/20 LFJ EPA200.7 31.06 04/21/20 SEJ 450OCNE-11 c I2340 04/14/20 TLH 351.2 R2-93 c 57.48 04/15/20 TLH 350.1 112-93 c 7937 04/14/20 AKSI 365.4-74 c 79.29 04/17/20 AKS 353.2 R2-93 5021 04/20/20 SEJ <5.0 04/21/20 LFJ EPA200.7 I 2D#: 214 _PKIF_ s- N �_ -- PHONE (252) 756-6208 FAX (252) 756-0633 DATE COLLECTED: 04/08/20 DATE REPORTED : 05/07/20 REVIEWED BY. ;4 c Uncertified data. DWR does not offer non -aqueous certification for thin analytical procedure. EIMIT(MIMUM % hwpormfto Drinking Water ID: 37715 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mglkg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mglkg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mglkg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt, basis), mg/kg Silver (dry wt. basis), mg/lig Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Cyanide (dry weight), mg/kg TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt:),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Holding Analysis Method Basin (RA) Date Analyst Code 1716 05/22/20 LFJ EPA200,7 <2.5 05/26/20 MTM 3113E-04 388584 05/22/20 LFJ EPA200.7 <0.5 05/22/20 MTM 3113E-04 52 05/22/20 LFJ EPA200.7 5 05/22/20 LFJ EPA200.7 2.8 05/28/20 MTM 3113E-04 3382 05/22/20 LFJ EPA200.7 0,09 05/28/20 MTM EPA7471B <5.0 05/22/20 LFJ EPA200.7 2417 05122/2Q LFJ EPA200.7 <5.0 05/29/20 MTM 3113E-04 < 2.5 05/76/20 LFJ EPA200.7 < 1250 05/22/20 LFJ EPA200.7 127 05/22/20 LFJ EPA200.7 19.81 05/19/20 SEJ 450OCNE-11 c 11310 05/15/20 TLH 351.2 R2-93 c 21.03 05/14/20 TLH 350.1 R2-93 c 4467 05114/20 DTL 365.4-74 c 49.84 05/14/20 DTL 353.2 R2-93 4576 05/18/20 SEJ < 5.0 05/22/20 LFJ EPA200.7 ID#: 214 DATE COLLECTED: 05/12/20 DATE REPORTED : 06/01/20 REVIEWED BY: c Uncertified data, DWR does not offer non -aqueous certification for this analytical procedure. Epw'OTOR M % hmpTOA Drinking Water ID! 37715 waatewat.er ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 05/12/20 DATE REPORTED : 05/15/20 RtVIEWED BY: _ Holding Holding Holding Holding Holdntg Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, %n 54.96 48.15 48,03 52.55 50.52 05/12/20 JMS 254OG-11 Fecal Coliform (MPH /gram Solids < 1.8 < 1.8 < 1.8 < 1.8 < 1.8 05/12/20 JMS 9221E-06 GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking Water Tn: 37715 Waatewater ;zT IQ PRUNE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 05/12/20 DATE REPORTED : 05/15/20 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % 54.59 59.12 05/12/20 JMS 2540G11 Fecal CoIiform (MPH /gram Solids <1.8 <1.8 05/12/20 JMS 9221E-06 Em'UnIMEW 1, hmpombd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWK2NS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt, basis), mglkg 1968 06/15/20 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 06/17/20 MTM 3113E-04 Calcium (dry wt. basis), mglkg 399925 06/15/20 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg <0.5 06/01/50 MTM 3113B-04 Copper (dry wt. basis), mglkg 55 06/15/20 LFJ EPA200.7 Chromium, T,(dry wt. basis),mg/kg 6 06/15/20 LFJ EPA200.7 Lead (dry weight basis), mg/kg 3.1 06/16/20 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 3661 06/15/20 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.12 06/23/20, MTM EPA7471B Nickel (dry wt. basis), mg/kg <5.0 06/15/20 LFJ EPA200.7 ' Potassium (dry wt. basis), mg/kg 2282 06/15/20 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 06/12/20 MTM 3113E-04 Silver (dry wt. basis), mg/kg <2.5 06/15/20 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg < 1250 06/15/20 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 125 06/15/20 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 31,12 06/11/20 KDS 4500CNE-II TKN (dry wt.), mg/kg c 11490 06/10r20 TLH 351.2 R2-93 Ammonia Nitrogen (dry wt,),mg/kg c 35.74 06/08/20 TCW 350.1 R2-93 Phosphorus, T. (dry wt.), mglkg c 5898 06/10/20 DTL 365,4-74 Nitrate -Nitrite (dry wt.), mg/kg c 606.6 06/05/20 TLH 353,2 R2-93 Plant Available Nitrogen, mg/kg 5206 06/14/20 SEJ Molybdenum (dry wt. basis), mg/kg <5.0 06/15/20 LFJ EPA200.7 - PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 06/04/20 DATE REPORTED : 06/25/20 REVIEWED BY: c t2ncertified data. DWR doee not offer non-aqueouo certification for this analytical procedure. EMATORUN&W % kw TOW Drinking water ID: 37715 Wastewater ID: 10 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN rNC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 2941 07/21/20 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 3.3 07/24/20 MTM 3113E-04 Calcium (dry wt. basis), mg/kg 303542 07/21/20 LFJ EPA200.7 Cadmium (dry wt. basis), mglkg <0.5 07/23/20 MTM 3113E-04 Copper (dry wt. basis), mg/kg 103 07/21/20 LFJ EPA200.7 Chromium, T.(dry wt, basis),mg/kg 9 07/21/20 LFJ EPA200.7 Lead (dry weight basis), mg/kg 6.3 07/221Z0 MTM 3113E-04 Magnesium (dry wt. basis), mg/kg 4182 07/21/20 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0,21 07/20/20 MTM EPA7471B Nickel (dry wt. basis), mg/kg <5,0 07/21/20 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 3231 07/21/20 LFJ EPA200.7 Selenium (dry wt, basis), mg/kg <5.0 07/30/20 MTM 3113B-04 Silver (dry wt. basis), mg/kg <2.5 07/21/20 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 07/21/20 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 239 07/21/20 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 26.0 07/10/20 KDS 4500CNE-11 TKN (dry wt.), mg/kg c 23530 07/10/20 TM 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 61.68 07/13/20 TCW 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 12080 07/10/20 TCW 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 79.59 07/10/20 TLH 353.2 112-93 Plant Available Nitrogen, mg/kg 9498 07/14/20 SE1 Molybdenum (dry wt. basis), mg/kg 5 07/21/20 LFJ EPA200.7 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 07/08/20 DATE REPORTED : 08/05/20 �f REVIEWED BY: l a Uncertified data. DWR does not offer non -aqueous Certification for thin analytical procedure. 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt, basis), mg/kg 2271 08/27/20 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 2.7 08/26/20 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 296264 08/27/20 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg <0.5 08/27/20 MTM 3113E-04 Copper (dry wt. basis), mg/kg 87 08/27/20 LF.I EPA200.7 Chromium, T.(dry wt. basis),mglkg 8 08/31/20 LFJ F,PA200.7 Lead (dry weight basis), mg/kg 5.1 08/27/20 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 3429 08/27/20 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.32 08/18/20. MTM EPA7471 B Nickel (dry wt. basis), mg/kg <10 08/27/20 LFJ EPA200.7 Potassium (dry wt. basis), mglkg 2395 08/27/20 LF.1 EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 09/01/20 MTM 3113E-04 Silver (dry wt. basis), inglkg <2.5 08/31/20 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 08/27/20 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 215 08/31/20 LFJ EPA200.7 Total Cyanide (dry weight), niglkg 30.4 08/17/20 S> .I 4500CNE-11 THIV (dry wt.), mg/kg c 20580 08/14/20 TCW 351.2 112-93 Ammonia Nitrogen (dry wt.),mg/kg c 73.89 08/12/20 TLET 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 15920 08/14/20 TLH 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 626.1 08/10/20 TLH 353.2 R2-93 Plant Available Nitrogen, mg/kg 8865 08/17/20 SET Molybdenum (dry wt. basis), mglkg <5.0 08/31/20 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater In: 10 PHONE (252) 756-620c FAX (252) 756-0633 IT)# : 214 DATE COLLECTED: 08/05/20 DATE REPORTED : 09/14/20 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. 144 OAKMON T DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWXINS P.O. BOX 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mglkg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mglkg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mglkg Selenium (dry wt. basis), mg/kg Silver (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt, basis), mg/kg Total Cyanide (dry weight), mg/kg TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mglkg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mglkg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Bolding Analysis Method Basin (RA) Date Analyst Code 2309 10/06/20 LFJ EPA200.7 <2.5 09/23/20 MTM 3113B-04 316937 09/23/20 LFJ EPA200.7 <0.5 09/25/20 MTM 3113B-04 86 10/06/20 LFJ EPA200.7 7 09/23/20 LFJ EPA200.7 5.5 09/25/20 MTM 3113B-04 4267 10/06/20 LFJ EPA200.7 0.11 09/24/20 MTM EPA7471B <5.0 09/23/20 LFJ EPA200.7 2346 09/23/20 LFJ EPA200.7 *5.0 10/01/20 MTM 311311-04 < 2.5 09/23/20 LFJ EPA200.7 < 1250 10/06/20 LFJ EPA200.7 193 10/06/20 LFJ EPA200.7 40.44 09/16/20 KDS 450OCNE-11 c 15510 09/18/20 TL11 351.2 112-93 c 47.72 09/16/20 DTL 350.1 112-93 c 9731 0911W20 KES 365.4-74 c 55.68 09/16/20 DTL 353.2 R2-93 6264 09/22/20 SEJ < 5.0 10/06/20 LFJ EPA200.7 Drinking water ID: 37715 wastewater ID: 10 PHONE (252) 756-620b FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 09/10/20 DATE REPORTED : 10/14/20 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. 114 OAKMONT DRIVE GREENVILLE, N,C. 27858 CITY OF NEW BERN (BI050LIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking Water ID: 37715 Wastewater ID: 10 �'HUNL {262) 766-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 09/10/20 DATE REPORTED : 09/15/20 / 4 REVIEWED BY: 1-1-/ — Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 BasurFC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % 43.36 48.63 47.02 47.66 43.84 09/10/20 JMS 2540G-11 Fecal Coliform (MPH /gram Solids < 1.8 < i .8 < 1.8 < 1.8 < 1.8 09/10/20 JMS 9221E-06 n 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWYINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking Water ID: 37715 Wastewater ID: 10 EHUNE (252) 5ti-62U8 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 09/10/20 DATE REPORTED : 09/15/20 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % 49.17 46.99 09/10/20 dMS 254OG-11 Fecal Coliform WN), /gram Solids <1.8 <1.8 09/10/20 .1MS 9221E-06 1 Enw,umflonq % joupTsUd 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mglkg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mglkg Lead (dry weight basis), mg/lig Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Silver (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mgllig Total Cyanide (dry weight), mg/kg TIC-N (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Holding Analysis Method Basin (RA) Date Analyst Code 3967 10/20/20 LFJ EPA200.7 2.5 10/20/20 MTM 311313-04 209578 10/20/20 LFJ EPA200.7 0.72 10/20/20 MTM 3113B-04 189 10/20/20 LF.J EPA200.7 15 10/20/20 LFJ EPA200.7 8.3 10/19/20 MTM 3I1313-04 5579 10/20/20 LFJ EPA200.7 0.26 10/14/20 MTM EPA7471 B 12 10/20/20 LFJ EPA200.7 4387 10/20/20 LFJ EPA200.7 <5.0 10/21/20 MTlbl 31138-04 2.5 10/20/20 LFJ EPA200.7 < 1250 t0/20120 LFJ EPA200.7 416 10/20/20 LFJ EPA200.7 36.04 10/12/20 SFJ 450OCNE-11 c 29330 10/13/20 TLH 351.2 R2-93 c 147.2 10/14/20 DTL 350.1 112-93 c 19450 10/ 13/20 DTL 365.4-74 c 19.90 10/14/20 TLH 353.2 R2-93 11767 10/15/20 SEJ 6 10/20/20 LFJ EPA200.7 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 10/08/20 DATE REPORTED : 10/26/20 REVIEWED BY. .i i c Uncertified data. ➢WR does not offer non -aqueous certification for this analytical. procedure. 114 UAKMUN I DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking water In: 37715 Wastewater ID: 1D PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 11/16/20 DATE REPORTED : 11/19/20 REVIEWED BY: Holding Holding Analysis Method PARAMETERS Basin-FC#6 Basin-FC#7 Date Analyst Code Total Solids, % 31.93 36.03 11/16/20 KDS 254OG-11 Fecal Coliform (MPN), /gram Solids <1.8 <1.8 11/16/20 KDS 9221E-06 ���flQo��c��� �lfl D�c�oQpoQa�c�d T 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (262) 756-62U8 FAX (252) 756-0633 ID#: 214 A DATE COLLECTED: 11/16/20 DATE REPORTED : 11/19/20 REVIEWED BY: Holding Holding Holding Holding Holding Analysis Method PARAMETERS Basin-FC#1 Basin-FC#2 Basin-FC#3 Basin-FC#4 Basin-FC#5 Date Analyst Code Total Solids, % 38,22 34.16 34.13 35.34 35.81 11/16/20 KDS 254OG-11 Fecal Coliform (MPN), /gram Solids <1.8 <I.8 <1.8 <1.8 <1.8 11/16/20 KDS 9221E-06 C��a�Qo��c��� Ala D�c�oQpo�a��d 114 OAKMOfv i UHIVE GREENVILLE, N.C. 27858 CITY OF NEW BERN (BIOSOLIDS) ATTN: TONY HAWKINS P.O. BOX 1129 NEW BERN ,NC 28563 Holding Analysis Method PARAMETERS Basin (RA) Date Analyst Code Aluminum, (dry wt. basis), mg/kg 2499 12/07/20 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 12/09/20 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 370044 12/07/20 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg <0.5 12/10/20 MTM 3113E-04 Copper (dry wt. basis), mg/kg 82 12/07/20 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 7 12/07/20 LFJ EPA200.7 Lead (dry weight basis), mg/kg 3.8 12/08/20 MTM 3113B-04 Magnesium (dry wt. basis), mglkg 3994 12/07/20 LFJ EPA200.7 Mercury (dry wt, basis), mglkg 0.14 12/09/29 MTM EPA7471B Nickel (dry wt. basis), mg/kg <5.0 12/07/20 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 2571 12/07/20 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 12/04/20 MTM 3113B-04 Silver (dry wt. basis), mg/kg < 2.5 12/07/20 LFJ EPA200.7 Sodium (dry wt. basis), mg/kg <1250 12/07/20 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 181 12/07/20 LFJ EPA200.7 Total Cyanide (dry weight), mg/kg 20.42 11/19/20 SEJ 450OCNE-11 TKN (dry wt.), mg/kg c 20770 11/20/20 TLF1 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 47.93 11/18/20 TLH 350.1 122-93 Phosphorus, T. (dry wt.), mg/kg c 15000 11/20/20 KES 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 52.92 11/17/20 DTL 353.2 R2-93 Plant Available Nitrogen, mg/kg 8366 11/24/20 SEJ Molybdenum (dry wt. basis), mg/kg < 5.0 12/07/20 LFJ EPA200.7 Drinking Water In: 37715 Wastewater ID: 10 t-HL) vL j2 i2) 5b-0206 FAX (252) 756-0633 ID#: 214 DATE COLLECTED: 11/16/20 DATE REPORTED : 12/17/20 REVIEWED BY: c Uncertified data. nwx does not offer non -aqueous certification for this analytical procedure. j IIE:.fesWt'S Sot bi-th. herelia art. (7rovidc;d I3ti S(3S Nwt(lA,l?larl £? Inc. Technicat :R.O.ort. for Environment 1, Inc City of New Bern (Biosoilds)-, New Bern, NC 214A SGS Job Number: FA77622 Sampling Date: 08/05/20 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environinentliuc.com TTN: Deedee Woolard Total number of pages in report e-Heirdcgpy 2, 0 'Pest results contained within this data package meet the requirements /Norm Farmer ofthe National Environmental Laboratory Accreditation Program Technical Director andior state specific certification progrtuns as applicable Client Service contact: Jean Dent -Smith 407-425--6700 Certifications: FL(F83510), LA(0305I), KS(E-10327), IL(20W63), NC(573), Ni(0L.002), NY(12022), SC{96038001) DnD RLAP(ANA13 L2229), AZ(AZ0806), CA(2937), Tx(TM47044M), PA(68-0i73), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the wsitten approval of SGS. Test results relate only to samples analyzed SGS North America Inc. • 4405 Vineland Road • Suite C-15 Orlando. FL 37811 • te1: 407-425-6760 • Paz: 407-425-0707 ,Cis 0,0 ily tttiytiz..I .. ;f7 ��rundi Ga'i �1. t uoa�c to You Fd ,s anEi 1 4#'l4 wr tt is tlacurr3ent, €'1 L,r i..hun< < �x ,c u. sr -vYou btu'; at: A 7te.'iebti' �t�:13it��rC1 tu,Y 15 dl; ht.h..1 ins f=iiS.hS.f.,usvarleri'$r�; -,.. 'E 5-'UM PA77622 FJ SGS North America 1ric. Sample Summary Environment 1, Inc Jab No: FA77622 City of New Bern (Biosoiids); New Bern, NC Project No: 214A ample Collected. Matrix Client dumber Date Time By Received Cude Type Sample ID �s �repq cgriial5 ie5iiis re}�rtecl a� l�Ipt eletedterl rleTill" vwlzl ahe� Organics ND — Not detected above the MDL FA77622 1 08/05/20 10:20 LS 08/08/20 SO Soil EOLDING BASIN (RA) FA77622-IL 08/05/20 10:20 LS 08/08/20 SCE Soil I40LDINIW N.(RA. Soil samples reported on a dry weight basis unless otherwise indicated on result page. GS 3a#t4 _... FA77622 �. I Summary of Hits .lob Number: FA77622 Account: Environment 1, Inc Project, City of Now Beat (Biosoilds); New Bern, NC Collected: 08/05/20 Lab Sample ID Client Sample ID Result/ Analyte Qual R]L MDL Units Method ]FA77622-1 HOLDING BASIN (RA) Corrosivity as pH 12. Iguitabiiity (Flashpoint) > 200 FA77622-IL HOLDING BASIN (RA) No hits reported in this sample. Page 1 of 1 is Su SW846 CHA.P7 Deg. F SW846 1010A MOD 4of14 GS FA77622 Summary of Hits Job Number: FA77622 Account: Environment 1, Inc Project: City of Now Bern (Biosoilds); New Bern, NC Collected: 08/05/20 Lab Sample ID Client Sample ID Result/ Analyte Qua] RL MDL Units Nfethod FA77622-I HOLDING BASIN (RA) Corrosivity as pH Ignitability (Flashpcint) a 200. FA77622-1I, HOLDING BASIN (RA) No hits reported in this sample. Page 1 of 1 su SW846 CU.AP7 Deg, F SW846 1010A MOD 4 of 14 rarrezz SGS North America Inc, Report of Analysis Client Sample ID: HOLDING BASIN (RA) Lab Sample ID- FA77622-1 Date Sampled: 08/05/20 Matrix: SO - Soil bate Received: 08/08/20 Percent Solids: 26,8 Project: City of New Bern (Biosoilds); New Bern, NC General Chemistry Analyte Corrosivity as pH Cyanide Reactivity Cyanide reactivity Ignitability (Flashpoint) Solids, Percent Sulfide Reactivity RL = Deporting Limit Page 1 of 1 Result RL Units DF Analyzed By Method 12.4 su 1 08/14/20 14:00 jB SW846 CHAP7 <:1 5 1.5 mg/kg 1 08/14/20 10:14 AC SW846 CHAP7 <' { 5.6 tng/kg 1 08/14/20 10:14 AC SW845 CHAP7 7200 Deb. F 1 08/12/20 08:30 cs SW846 101oAMOD 26.8 '. " '' % 1 08/14/20 15 :31 AC SM19 254OG 190 mg/kg 1 08/14!20 15:14 JC SW846 CHAP7 S n f4 FA77622 SGS North America Inc. Report of Analysis 'lient Sample 1D: HOLDING BASfN (RA) ,ab Sample ID: FA77622-IL Date Sampled: 09/05/20 latrix: SO - Soil Date Received: 08/09/20 llethod: SW846 8260E SW846 1311 Percent Solids: 26.9 'roject: City of New Bern (Siosoilds), New Bern, NC Page l of 1 File 1D DF Analyzed By Prep Date Prep Batch Analytical -Batch Ran #1 P73473 ,D 10 08/12/20 17:29 SO 08/11 /20 12;10 OPS i498 VP2922 Run #2 Purge Volume #1 5.0 ml #2 VOA'iCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND..::. `: D018 0.50 0.010 75-93-3 2-Butanone (MEK) N1 l-.: ':i D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 O.010 108-90-7 Chlorobenzene ND D021 100 0.010 67-60-3 Chloroform N1? D022 6.0 0.010 106-46-7 1,4-Dichlorobenzene N17 D027 7.5 0.010 107-06-2 1.,2-Dichloroethane ND :.. D028 0.50 0.010 75-35-4 1,I-Dichloroethylene N D ". D029 0.70 0.010 127-18-4 Tetrachlomethylene ND `.' D039 0.70 0.010 79-01-6 Trichioroethylene ND D040 0.50 0,010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofiuoromethane 1070/,;'' 17060-07-0 1,2-Dichloroethatie-D4 106%: 79-125% 2037-26-5 Toluene-D8 103%n 85-1120/0 460-00-4 4-Bromo}luorobenzene 1°08% :: 83-118% (a) Sample was treated with an anti -foaming agent. NIDL Units Q 0.0031 mg/1 0.020 mg/l 0.0036 mg/l 0,0020 mg/I 0.0030 mgll 0.0026 mg/1 0,0031 mg/I 0,0032 mg/1 0,0022 mg/1 0.0035 mg/1 0,0041 mg/l ND = Not detected MDR, = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank F = Indicates value exceeds calibration range N = indicates presumptive evidence of a compound 11 7ofi4 FA?7622 i SGS North America Inc. Deport of Analysis ;lient Sample ID: HOLDING BASIN (RA) ,ab Sample ID: FA77622-1L Date Sampled: 08/05/20 Ilatrix: SO - Soil Date Received: 09/08/20 2ethod. SW846 8270D SW846 3510C Percent Solids: 26.8 'roject: City of New Bern (Siosoilds), New Bern, NIC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 61706535.D 1 08/12/20 19:46 MV 08/12/20 08:30 OP81525 S6F252 Run #2 Initial 'Volume Final Volume un #1 100 ml 1.0 all un #2 ABN TCLP List CAS No. Compound Result HW# MCL RL 95-48-7 2-Methylphenol N17:.':.: D023 200 0.050 3&4-Methyiphenol ND _ D024 200 0.050 87-86-5 Pentachlorophenol a ND:; D037 100 0.25 95-95-4 2,4,5-Trichlorophenol ND D041 400 0,050 88-06-2 2,4,6-Trichlorephenol ND:;:.D042 2.0 0.050 106-46-,7 1,4-Dichlorobenzene ND `.' D027 7.5 0.050 121-14-2 2,4-Dinitrotoluene ND = D030 0.13 0.050 118-74-1 Hexachlorobenzenc ND ',': D032 0.13 0,050 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 67-72-1 Hexacbloroethane ND D034 3.0 0.050 98-95-3 Nitrobenzene ND D036 2.0 0.050 110-86-1 Pyridine ND D038 5.0 9-10 CAS No. Surrogate Recoveries Run# 1 Run## 2 Limits 367-12-4 2-Flnarapheno] 34%':;; :, 14-67% 4165-62-2 Phenol-65 23°l0"';' 10-50% 1I8-79-6 2,4,6-Tribromopbenol 74% 33-118% 4165 60-0 Nitrobenzene-d5 74%:.` ::. 42-108% 321-60-$ 2 Fluorobiphenyl 781/.,. 40-106% 1718-51-0 `herphenyl-d14 77/6 39-121% (a) Associated BS recovery outside control limits. Within limits in tns/msd. TCLP Leachate method SW846 1313 MDL Units Q 0.0056 mg/l 0,0098 mg/1 0,050 mg/l 0.0074 mg/1 0,0075 mg/l 0.0050 mg/1 0.0081 mg/1 0.0069 mg/1 0.0050 mg/l 0.016 mg/l 0.0093 mg/l 0.020 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL — Maximum Contamination Level (40 CFR 261 7/l/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IN, 8of14 SGS- - FA77622 m_ A SGS North America Inc. Report of Analysis Pago I of 1� Client Sample ID: HOLDING BASIN (RA) Lab Sample ID: FA77622-lL Date Sampled. 08/05/20 Matrix: SO - Soil Date Received: 08/08120 ;Method: SW846 8151A SW846 3510C Percent Solids: 26.8 Project: City of New Bern (Biosoilds); New Bern, SIC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC069719.D 1 08/13/20 20:58 JA 08/12/20 13:15 OPS1527 GCC1704 Run #2 Initial Volume 'Final Volume Run#1 10.0m1 5.0MI Run #2 Herbicide TCLP List CAS No. Compound 94-75-7 2,4-D 93-72-1 2,4,5-TP (Silvex) CAS No- Surrogate Recoveries 19719-28-9 2,4-IDCAA TCLP Leachate method SW846 1311 Result HW# MCL RL NIDL Units Q ND :.°;:':''' D016 I0 0.050 0.C17 mg/1 ND . ": ;'. .; DO17 1.0 0.0050 0.0013 mg/l Run# 1 Run# 2 Limits 92% .' 39-135% ND = NTot detected MDL — Method Detection Limit J Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1111) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9cog14 x ��rrszz SGS North America Inc. Report of Analysis 'Bent Sample ll): HOLDING BASIN (RA) ,ab Sample ID: FA77622-IL Date Sampled: 08/05/20 'Iatrix: SO - Soil Date Received: 08/09/20 mthod: SW846 8081E SW846 3510C Percent Solids: 26.8 'roject: City of New Bern (Biosoilds); New Bern, NC Page l of I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run 41 KK98442.D I 08/12/20 22:50 WH 08/12/20 10:15 OP81526 CYKK3143 Run #2 Initial Volume Final Volume -un #1 100 ml 5.0 m1 _un #2 Pesticide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result llW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindanc) 107 D013 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane ND D020 0.030 0.0010 0,00038 mg/l 72-20-8 Endrin N!) D012 0.020 0,00020 0.000021 mg/l 76-44-8 Heptachlor D031 0,00800,00010 0.000026 rng/l 1024-57-3 Heptachlor epoxide NI) D031 0.0080 0.00010 0.000020 rng/l 72-43-5 Methoxychlor IND : :: ` : ° D0M 10 0.00020 0,000050 mg/1 8001-35-2 Toxaphenc ND D015 0.50 0.0050 0.0021 mg/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 877-09-8 Tctrachloro-m-xylene 115%, 42-127% 2051-24-3 Decachlorohiphenyl 38°io' .'-' 27-127% (a) Associated CCV outside of control limits high, sample was ND, Associated BS outside of control limits high, sample was ND. (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detectiou Limit r = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 T l f 11) 13 = Indicates aualyte found in associated method blank E — Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 'tit of 14 .y I�,arr6as SOS North America Inc. Deport of Analysis Page 1 of 1 '.lien( Sample ID: HOLDING BASIN (RA) ,ab Sample ID: FA77622-IL Date Sampled: 08/0.5/20 rlatrix: SO - Soil Date Received: 08/08/20 Percent Solids: 26.8 Tojeet: City of New Bern (Biosoilds), New Bern, NC 0- Metals Analysis, TCLP Leachate SW846 1311 Analyse Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic O:iQ D004 5.0 0.1c mg/1 1 08/18/20 08/18/20 DM SWB466010C2 SIN84631)1CA4 Barium <2 0 D005 100 2.0 mgll 1 08/18/20 08/18/20 DM SW846 6010C 2 SW84-6301CA 4 Cadmium <a.(35D D006 1.0 0.050 mg/I 1 08/18/20 08/18/20 Du SW846 6010C 2 SW846 301CA 4 Chromium <'0:10: ' .' D007 5.0 0.10 mg/l 1 08/18/20 08/18/20 DM SW846 6020C 2 SW8463010A4 Lead <0:[}50:': DD08 5.0 0.050 rng/l 1 08118,120 08/18/20 DM SW846 6010C 2 SW8463010A 4 Mercury < 0.0050 D009 0.20 0.0050 mg/l I 08/I4120 08/14/20 7C SW846 7470A 1 SW846 7470A 3 Selenium <0.10 . ° ° DO10 1.0 0.10 mg/l 1 08/18/20 08/18/20 DM SW846 6010C 2 SW846 3010A 4 Silver <0 10 DOI1 5.0 0.10 mg/l 1 08/18/20 08/18/2C L)m SW846 6010C 2 sw846 3010a 4 (1) Instrument QC Batch: MA16976 (2) Instrument QC Batch: MA16982 (3) Prep QC Batch: MP37679 (4) Prep QC Batch: MP37690 ILL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) 11 ai 14 FA776� ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of New Bern WWTP Name: City of New Bern WWTP Monitoring Period: From 1/1/2020 WQ Permit Number: NPDES Number: To 12/31/2020 WQ0023306 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt_ A (time/temp)❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs 1 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestior_ ❑ `. `. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample Type a ytica Tech - ni ue Minimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN <1.8 1.8 <1.8 MPN 7 bi monthI3 grab n/a CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ' ❑ Alt. 3 (30-day, bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable)❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed 0 CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tony Hawkins / Manager Preparer Name and Title (type or p nt) Sign tune of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12I2006)