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HomeMy WebLinkAboutWQ0002702_Regional Office Historical File Pre 2018 (22)ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wOlcOtt—r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3108 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH - - 4 1 _ 1�_ O ALiU l yes' (a 1 -iS�lo l 1 (D 3 - Ca,0 - QI — J ' ,—t —� -i - 10 W J-1 N 9-1 b. -t I f 1 ` 0 _ i ALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 Phone:704-279-7908 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 REACTION # I DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH n - L G a 7a C. . S- 6 0 (1 - --(D 11 O _ Z- /I - 2 - 09 9 OL- D ( L( c 5 1 ,9�2 r 79 0 7- to 10 11 - - I- 10 1( ALCHEM, INC ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 8135 RED RD ROCKWELL, NC 28138 Phone: 704-279-7908 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com PH SAMPLING POTte o G .a(I r�- ,1 �. Q6 6. os � r�7 NLALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 Phone: 704-279-7908 Fax: 704-279-8418 E-mail: wolcott—r@yahoo.com REACTION# DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH 0" o r I Y J 4s JC4' 0c) 10 Yj 7 S _01-2-S-fin 2.- 2-S - t j( co-20 c'; 02.- 5! 6- 10 (0 ALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3108 - 6109 Phone: 704-279-7908 Fax:704-279-8418 E-mail: wolcott_r@yahoo.com ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott—r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT I LAGOON # SAMPLING PORT PH LAGOON PH -t I- in i -Z _ G b a6 _ ISI-I5-Io Jo - 1 16. os. _ — (d ? 3 - 3-1- lo 11 Yds 2 ,!t 6.oc ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: Wolcott—r@yahoo.com ANNUAL RESIDUAL REPORT c cl Aca Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 ALCHEM, INC 813 5 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: ANNUAL RESIDUAL REPORT wolcott_r@yahoo.com Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3108 . 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # I SAMPLING PORT PH LAGOON PH i V f i 3/3/2008 20 TONS 6% 3 J 3/4/2008 I 20 TONS 6 % 3 1 y-� 1 ! t 3/5/2008 3/6/2008 I 20 TONS I 20 TONS I 6% 6% 3 3 i 3/7/2008 20 TONS 6% 3 Y 311012008 I 20 TONS 6%, 3 � ► � c"�o0 - ? 3/1 112008 I 20 TONS 6% 3 311212008 I 20 TONS I 6% 3 311312008 20 TONS 6% 3 3/1412008 I 20 TONS 6% 3 *G 3/1712008 I 20 TONS 6% I 3 3/18/2008 I 20 TONS 6% 3 1 ✓ �� 3/19/2008 I 20 TONS 6% 3 3 3/20/2008 20 TONS 6% I _ r' 5 3/21/2008 20 TONS I 6% I 3 p.�J _ tI i 1 "�� � � 3/2412008 I 3/25/2008 I 20 TONS 20 TONS 6% 6% 3 3 3 f _ C) 1 3/26/2008 I 20 TONS 6%aw I - ( (? }CG 3/27/2008 G 20 TONS 6% I 3 3/2812008 I 20 TONS 6; I 3 ALCHEM. INC L,Q .at i 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT LAGOON PH I PH 3131 /2008 20 TONS 6% 3 4/1/2008 20 TONS 6% 3 412/2008 20 TONS 6% 3 4/312008 20 TONS 6% 3 4/412008 20 TONS 6% 3 ' ?2 4/712008 20 TONS 6% 3 - 2 4/8/2008 I 20 TONS 6% 3 nT 4/912008 20 TONS 6% T 3 4/10/2008 20 TONS 6% 3 4/1 112008 20 TONS 6% 3 Q_ 4/14/2008 20 TONS 6% 3 4/15/2008 20 TONS 6% 3 4/16/2008 20 TONS 6% 3 r 411712008 I 20 TONS 6% I 3 4/1812008 20 TONS 6% 3 4/21/2008 20 TONS 6% 3 jj _ 4/22/2008 20 TONS 6% 3 () p ` C _ G { ,) L D 4123/2008 20 TONS 6% 3 I/ 4/24/2008 20 TONS I 6% 3 u kr-on % ', 4/2512008 20 TONS 6% 3 1, 1 ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 REACTION # DATE BAUXITE USED SLURRIED OUT LAGOON#! SAMPLING PORT PH LAGOON PH 4/28/2008 20 TONS 6% 3 T-G 42 4/2912008 20 TONS 6% 3 4/30/2008 20 TONS 6% 3 `+ q. `t 511/2008 20 TONS 6% 3 12T 5/2/2008 20 TONS 6Y 3 Q T ' , S/S12008 20 TONS 6% 3 a — 5/612008 20 TONS 6% 3 5/712008 20 TONS 6% 3 5/8/2008 20 TONS 6% 3 51912008 20 TONS 6% 3 �+ 5112/2008 20 TONS 6% 3 5/13/2008 20 TONS 6% 3 5/14/2008 20 TONS 6% 3 5/IS/2008 20 TONS 6% 3 ^NW05_L 5l1612008 20 TONS 6% 3 P 5/ 1912008 I 20 TONS 6% 3 rQ57_ 7 512012008 20 TONS 6% 3 5/21/2008 20 TONS 6% 3 5/22/2008 20 TONS 6% 3 rJ� , 5/2312008 20 TONS 6% 3 i ` AL HEM, INC j 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT I i 5/2612008 20 TONS 6 % 3 C7 , .D ( r S/27/2008 20 TONS 6% 3 T G (�- 5/2812008 20 TONS 6% 3 5/29/2008 20 TONS 6% 3 DOoa •T c�u � 5/30/2008 20 TONS 6% 3 � . ? y 612/2008 20 TONS 6% 3 6/3/2008 20 TONS 6% 3 614 - 6143 REACTOR DOWN 6116/2008 20 TONS 6% 3 T /- Co & 6/17/2008 20 TONS 6% 3 / 9 17 6/18/2008 20 TONS 6% 3 _ 7 �G Z 6119/2008 20 TONS 6% 3 / 6/2012008 20 TONS 6% I 6/2312008 20 TONS b% I 6/24/2008 20 TONS 6% I 6/2512008 20 TONS 6% I 6126/2008 20 TONS 6% I 6127/2008 20 TONS 6% I G Vl: 6/30/2008 20 TONS 6% I 7/1/2008 20 TONS 6% I AL HEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH 712/2008 20 TONS 6 % `( 7/3/2008 20 TONS 6 % I �^ F 1 718/2008 20 TONS 6% I 1� 719/2008 20 TONS 6% I JCo.i 7,1012108 20 TONS 6% I ij 711 112008 20 TONS 6% I 7/14/2008 20 TONS 6% I 711512008 20 TONS 6% I �l L3 7/16/2008 20 TONS 6% I 7/17120/8 20 TONS 6% I I 7/18/2008 20 TONS 6% I 7/21/2008 20 TONS 6% I O 7/22/2008 20 TONS 6% I 7/23/2008 20 TONS 6% I I J%} �cha 7/2412008 I 20 TONS 6% I U 712512008 20 TONS 6% I 712812008 20 TONS 6% I 7129/2008 20 TONS 6% I 7130/2008 20 TONS 6% I 7131/2008 20 TONS 6% I 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcot _r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dare: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT LAGOON PH PH V 81112008 20 TONS 6% 13 8/4/2008 20 TONS 6% I 8/S/2008 20 TONS 6% I 8/6/2008 20 TONS 6% I / V/ U 8/7/2008 I 20 TONS 6% I ' 818120087 20 TONS 6% I 811 112008 20 TONS 6% I �y } ( t 8/12/2008 20 TONS 6% I f 8/13/2008 20 TONS 6% I 8/14/2008 20 TONS 6% I 8/15/2008 20 TONS 6% I 8/18/2008 20 TONS 6% I i J 8/19/2008 20 TONS 6% 1 •ems"`' J � E 8/20l2008 20 TONS 6% I rn �t 8/21/2008 20 TONS 6% 1 � n v 8122/2008 20 TONS 6% I rri 8/25/2008 20 TONS 6% Q 8/26/2008 20 TONS 6% I 2, 8127/2008 20 TONS 6% I 1 V Z. 8/2812008 20 TONS 6% I ALCHEM, 1NC 813 5 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE I BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT LAGOON PH I PH 1 8129//2008 20 TONS 6 % 9/1/2008 20 TONS 6% 9/2/2008 20 TONS 6% I 9/3/2008 20 TONS 6% I fir �2 914/2008 20 TONS 6% i 91S12008 20 TONS 6% I 1Tv i� 918/2008 20 TONS 6% I 0 919/2008 20 TONS 6% I 9110/2008 20 TONS 6% I i OC'0 °• _ 9/1112009 20 TONS 6% I 9/12/2008 20 TONS 6% I y � 9/1512008 20 TONS 6% I 3 9/16/2008 20 TONS 6% I I 1 19 9/17/2008 20 TONS 6% I r7 . _ 911812008 20 TONS 6% I 1 J -71 9119/2008 20 TONS 6% I 9/2212008 20 TONS 6% I r C l 71 r 912312008 i 20 TONS 6% I 9/2412008 20 TONS 6% I 9/2512008 20 TONS 6% I 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3108 - 6109 Phone:704-279-7908 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH J� 9126/2008 20 TONS 6 % I r C (� c J� 9/29/2008 20 TONS 6 % I CC 9130/2008 20 TONS 6%fT- I 10/1/2008 20 TONS 6% I 10/2/2008 20 TONS 6% 1 10/3/2008 20 TONS 6% I 10/6/2008 20 TONS 6% I 10/7/2008 20 TONS 6% I I0/8/2008 I 20 TONS 6% I ea i 10/9/2008 20 TONS 6% I Q "-7 10/1012008 20 TONS 6% I 10/13/2008 20 TONS 6% I 10/14/2008 20 TONS 6% I 1011S/2008 20 TONS 6% I 10/16/2008 20 TONS 6% I 10/17/2008 20 TONS 6% I 10/20/2008 20 TONS 6% I J 10/21/2008 20 TONS 6% 1 i �'/ � / 10/22/2008 20 TONS 6% I 7.10 q % i 10/23/2008 20 TONS 6% I I ALCHEM, INC ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 8135 RED RD ROCKWELL, NC 28138 Phone:704-279-7908 Fax:704-279-8418 E-mail: wolcott_r@yahoo.com REACTION # DATE BAUXITE USED %SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH 2:) 10/24/2008 20 TONS 6 % I LLLL) 10/27/2008 20 TONS 6 % I 7.05 10128/2008 20 TONS 6% &000 1 b S 10/29/2008 20 TONS I 6% 1 10/30/2008 20 TONS 6% I ~G V ( I 10/31/2008 I 20 TONS 6% I I lLT(I�JL 4 r V I 11/3/2008 20 TONS 6% I 11/4/2008 20 TONS 6%O I 6.90 rrroI ��� 11/5/2008 20 TONS I 6% ` 11/6/2008 20 TONS 6% I n F � 11/7/2008 I 20 TONS 6% I I I/1012008 20 TONS I 6% I I 6.95 11/1 112008 I 20 TONS 6% I ;, '}(X t,) S i 5 I00 11� 1 1/12/2008 I 20 TONS 6% 1 0 I I/13/2008 20 TONS 6% 1 . 1 11/14/2008 20 TONS 6% 1 20 TONS 6%Y7!��6.89 PT-f() 11/1812008 20 TONS 6%�� /�-n �i/ I U191200817---T 20 TONS 6% !t( 0DC' j �� 11120/2008 20 TONS 6% 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH 1 1121/2008 20 TONS 6% 1 G O� 1 1/24/2008 20 TONS 6% 1 1 1125/2008 20 TONS 6% I 6.89 12/1/2008 20 TONS 6% 1 12/2/2008 20 TONS 6% 1 6.99 12/3/2008 20 TONS 6% I 11/412001 20 TONS 6% I 12/5/2008 20 TONS 6% I 12/8/2008 20 TONS 6% I 2 12/9/2008 20 TONS 6% I n • 12110/2008 20 TONS 6% I / 12111/2008 20 TONS 6% I 12/1212008 20 TONS 6% I nTv �o� � �. 12/15/2008 20 TONS 6% I 7.02 2TOw0 n 12116/2008 20 TONS 6% I 12/17/2008 20 TONS 6% I J J 12118/2008 20 TONS 6% I i 12/19/2008 20 TONS 6% I J 12/22/2008 20 TONS 6% I 12/2912008 20 TONS 6% I 6.89 County: ROWAN _ Sample ID: AB58147 River Basin Q 1!"" apF VlA7FgQ PO Number# 10G0245 Report To MROUST U O Date Received: 06/12/2010 G 2 r Time Received: 08:10 Collector. E HUFFMAN n rr ' t � Q i Labworks LoginlD SMATHIS Region: MRO J 'Clt Q Report Generated: 6/7/10 Sample Matrix: GROUNDWATER lam, O Cv �jj Date Reported: 06/07/2010 Loc. Type: MONITORING WELL Emergency Yes/No pVisitlD COC Yes/No YES G SM C Location ID: MROAPNLC o lect Date: 0511012010 Collect Time: 13:47 Sample Depth Result/ Method Analysis CAS # Analvte Name PQL Units Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.4 °C 5/12/10 SMATHIS MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.8 5/17/10 ESTAFFORDI 7429-90-5 Al by ICP 50 570000 ug/L EPA 200.7 5/27/10 ESTAFFORDI 7440-38-2 As by furnace 2 lop ug/L EPA 200.9 5/18/10 ESTAFFORDI 7440-38-3 Ba by ICP 10 20 ug/L EPA 200.7 5/27110 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 300 mg/L EPA 200.7 5/27110 ESTAFFORD1 7440-43-9 Cd by furnace 2 1.2 ug/L EPA 200.9 5/17/10 ESTAFFORDI 7440-47-3 Cr by ICPMS 10 340 ug/L EPA 200.8 5/17/10 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 300 ug/L EPA 200.8 5/17/10 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 5/20/10 ESTAFFORDI 7439-95-4 Mg by ICP 0.1 33 mg/L EPA 200.7 5/27/10 ESTAFFORDI 7439-96-5 Mn by ICP 10 6100 ug/L EPA 200.7 5127/10 ESTAFFORDI 7440-23-5 Na by ICP 0.1 26 mg/L EPA 200.7 5/27/10 ESTAFFORDI 7440-02-0 Ni by ICPMS 10 680 ug/L EPA 200.8 5/17/10 ESTAFFORDI 7439-92-1 Pb by ICPMS 10 11 ug/L EPA 200.8 5/17/10 ESTAFFORDI 7782-49-2 �Zn Se by ICPMS 5 5.0 U ug/L EPA 200.8 5/21/10 ESTAFFORDI 7440-6 1-6 by ICP 10 3900 ug/L EPA 200.7 5/27110 ESTAFFORDI Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed description of the qualifier codes referto hflpllnortal_nccfanr.q,�:\ve�.4v.p7; t±!staftin`c:iechassstDa'a Quaf•.fier Cedes<htln:!itartaLncdenr.art�M.eh�_v_ggab'staffinfo::echassist_> Page 1 of 1 ROUNDWATER FIELD/LAB FORM County_ Quad No---_—_- Serial No.-- _--- Lat.— Long. Report To: ARO, FRO, e RRO, WaRO, WiRO, WSRO, Kinston ncurii Trust, Central Off., Other:—__ Shipped by: Bus Hand Del., Other:—__ Collector(s):__�___— Date 3= i0 Jo)/U Ti FIELD ANALYSES Spec. Cond.94-- at 25eC pH 400------------- p — Temp.lo _ IC Odor—_-_ AppearanceL ' ��1/ iL/gtc!CC ll7l;�i"—cl Field Analysis By:—_— -- C nn MATnoV ANAI VCFC v Boo 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /loom] Coliform: MF Total 31504 /loom( TOC 680 mg/L Turbidity 76 NTU Residue, Suspended 530 mg/L pH 403 units Alkalinity to p5 mg/L Alkalinity to pH 8.3 415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 cu Cyanide 720 mg/L Lab Com GW-54 REV. 12/87 SAMPLEIYPE SAMPLE PRIORITY ❑ Water ❑ Routine ❑ Soil ❑ Emeraencv a 1 v� of Custody Purpose: `5/ PW4 Baseline, Complaint, nor A 1 r in rGni e ) A/ Location or Site /, Description of sampling Sampling Method-CL6 300 mglL mg/L al 900 mglL Ed n-carb 902 mg/L 0 ugh Specific Cond. 95 uMhoslcm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NOz + NO3 as N 630 mg/L P: Total as P 665 mg/L For Dissolved Analysis -submit filtered sample and write "DIS" in block. North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWAT R SECTION )o(- o a4 � � Lab Number _ --- _— — Date Recei e _ T Rec'd By, �/����,,,,,�� Fro :Bu , Courier I Other: __►__ Data Entry By: —_ Ck:-_—__— Data Reported:— ;ompliance, LUST, Pesticide Study, Federal Trust,Other: r (cirde one) Ag-Silver 46566 ug/L AI -Aluminum 46557 ug/L As -Arsenic 46551 ug/L Ba-Barium 46558 ug/L Ca -Calcium 46552 mg/L Cd-Cadmium 46559 ug/L Cr-Chromium 46559 ug/L Cu-Copper46562 ug/L Fe -Iron 46563 ug/L Hg-Mercury 71900 ug/L K-Potassium 46555 mg/L Mg -Magnesium 46554 mg/L Mn-Manganese 46565 ug/L Na-Sodium 46556 mg/L Ni-Nickel ug/L Pb-Lead 4564 ug/L Se -Se mum ug/L glLZn-Zinc 46567 u Sample Interval — air temp., etc.) Organochlorine Pesticides Organophosphorus Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolalile Organics TPH-Diesel Range Volatile Organics (VOA bottle) TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival: l� County: ROWAN Sample ID: AB58148 River Basin t] U u Q�/ArFip PO Number # 10G0257 Report To MROUST { Date Received: 0511212010 C r Time Received: 08:10 Collector: E HUFFMAN > tD < Labworks LoginlD SMATHIS Region: MRO b n� u -'" 1 ! Report Generated: 6l7/10 Sample Matrix: GROUNDWATER 'e-; 6 T'1 O Date Reported: 06/07/2010 Lac. Type: MONITORING WELL Emergency Yes/No j}i O Visit D % COC Yes/No YES ty >�. €� �rLoc„Des� M. INC Location ID: MROAPNLC -Fiat ate: 05110/2010 Collect Time: 13:47 Sample Depth �J CAS # AnalVte Name PQL Result/ Units Method Analysis Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 0.4 °C 5/12/10 SMATHIS MET 7440-22-4 Ag by ICPMS 5 5.0 U ug/L EPA 200.6 5/17110 ESTAFFORDI 7429-90-5 'Al by ICP 50 860000 ug/L EPA 200.7 5/27/10 ESTAFFORDI 7440-38-2 As by furnace 2 22 ug/L EPA 200.9 5/18/10 ESTAFFORDI 7440-38-3 Ba by ICP 10 110 ug/L EPA 200.7 5127/10 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 330 mg/L EPA 200.7 5127/10 ESTAFFORDI 7440-43-9 Cd by furnace 2 1.1 ug/L EPA 200.9 5/18/10 ESTAFFORDI 744047-3 Cr by ICPMS 10 560 ug/L EPA 200.8 5/17110 ESTAFFORDI 7440-50-8 Cu by ICPMS 2 330 ug/L EPA 200.8 5/17/10 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 5/20110 ESTAFFORDI 7439-95-4 Mg by ICP 0.1 31 mg/L EPA 200.7 5/27/10 ESTAFFORDI 7439-96-5 Mn by ICP 10 5800 ug/L EPA 200.7 5/27/10 ESTAFFORDI 7440-23-5 Nab y ICP 0.1 25 mg/L EPA 200.7 5/27/10 ESTAFFORDI 7440-02-0 Ni by ICPMS 10 660 ug/L EPA 200.8 5/17/10 ESTAFFORD1 7439-92-1 Pb by ICPMS 10 36 ug/L EPA 200.8 5/17/10 ESTAFFORDI 7782-49-2 Se by furnace 5 10 ug/L EPA 200.9 5/17/10 ESTAFFORD1 7440-66-6 Zn by ICPMS 10 4700 ug/L EPA 200.8 5/17/10 ESTAFFORDI Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to fta!!octljLnrierrorgAvebtiygh¢lstaffiric 9echass-.. wag'a 4uar CMe_<t:tln.(!UOAel.ncdenr_ertf,YwehMgcijj. affinfoieer, assisb Page 1 of 1 * Fi eiws�eej -mu�ft I vi L4 R__4 GROUNDWATER FIELD/LAB FORM Location code SAMPLE TYPE SAMPLE PRIORITY County fo Water ❑ Routine Quad No Serial No. El Soil ❑ Emergency Lat. Long. ❑ Other Chain of Custody Report To: ARO, FR MR RO, WaRO, WiRO, WSRO, Kinston FO, F rust, Central Off., Other: Shipped by: Bus, i Del., Other: Purpose: Collector(s): Date 5- lo-20toTime I ((T Pm Bas line FIELD ANALYSES Owner pH 40o Spec. Cond.9a at 25°C Location or Site Temp.°C Odor Description of sampling Appearance ,A ck, P, 4-viz Sampling Method Field Analysis By: Remarks I ARnPATnPY ANAI YSFR BOD 310 mg/L COD High 340 mg/L COD Low 335 mg1L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /looml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L pH 403 units Alkalinity to pH4.5410 mg1L Alkalinity to pH 8.3415 mg1L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon dioxide 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 Cu Cyanide 720 mg1L Lab Comments Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/l Specific Cond. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg1L NH, as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg1L P: Total as P 665 mg/L Nitrate (NO3 as N) 620 mg1L Nitrite (NO2 as N) 615 mg1L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION to �- 025�+ �� Lab Number � 61� q Date Receive Tirr Rec'd By: I�,, From:Bus, R Other: im J�� /l , Data Entry By: Date Reported: Complaint, Compliance, LUST, Pesticide Study, Federal Trust, the Sample Interval (Pumping time, air temp., etc.) Ag-Silver46566 u 1L AI -Aluminum 46557 u /L As -Arsenic 46551 ug/L IV Ba-Barium 46558 u /L Ca -Calcium 46552 mg/L Cd-Cadmium 46559 u /L Cr-Chromium 46559 ug/L u-Copper 46562 u /L ug/L Hg-Mercury 71900 u /L K-Potassium 46555 m IL Mg -Magnesium 46554 mg/L Mn-Manganese 46565 u /L Na-Sodium 46556 m /L Ni-Nickel u 1L Pb-Lead 46564 u 1L Se Selenium u /L Zn-Zinc 46567 u /L Organochlorine Pesticides Or ano hos horus Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): D County: ROWAN River Basin �, L Report To MROUST r Collector: E HUFFMAN s�r Region: MRO i ' r C ) Sample Matrix: GROUNDWATER -0— N Loc. Type: MONITORING WELL ii� C.,::) �iL Emergency Yes/No sIt COC Yes/No YES p Location ID: MROAPNLC CAS # Analyte Name LAB Sample temperature at receipt by lab MET 7440-22-4 Ag by furnace 7429-90-5 Al by ICP Collect Date: 05/10/2010 Result/ PQL — Qualifier 0.4 5 5.0 U 50 1400000 i t � Sample ID: AB58149 PO Number# 10G0258 Date Received: 06/12/2010 Time Received: 08:10 Labworks LoginlD SMATHIS Report Generated: 617/10 Date Reported: 06107/2010 �1 Collect Time: 13:47 Sample Depth Units Method Anal sis Validated by Reference Date °C 5/12/10 SMATHIS ug/L EPA 200.9 5119/10 ESTAFFORDI ug/L EPA 200.7 5/27/10 ESTAFFORDI 7440-38-2 As by furnace 2 36 ug/L EPA 200.9 5118/10 ESTAFFORDI 7440-38-3 Ba by ICP 10 1500 ug/L EPA 200.7 5/27/10 ESTAFFORDI 7440-70-2 Ca by ICP 0.1 290 mg/L EPA 200.7 5/27110 ESTAFFORDI 7440-43-9 Cd by furnace 2 1.2 ug/L EPA 200.9 5/17/10 ESTAFFORD1 7440-47-3 Cr by ICP 10 3100 ug/L EPA 200.7 5/27/10 ESTAFFORDI 7440-50-8 Cu by ICP 2 680 ug/L EPA 200.7 5/27110 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 16.3 ug/L EPA 245.1 5/20/10 ESTAFFORDI 7439-954 Mg by ICP 0.1 60 mg/L EPA 200.7 5/27/10 ESTAFFORDI 7439-96-5 Mn by ICP 10 7600 ug/L EPA 200.7 6/27/10 ESTAFFORDI 7440-23-5 Na by ICP 0.1 25 mg/L EPA 200.7 5/27/10 ESTAFFORDI 7440-02-0 Ni by ICP 10 630 ug/L EPA 200.7 5/27/10 ESTAFFORDI 7439-92-1 Pb by ICPMS 10 300 ug/L EPA 200.8 5118/10 ESTAFFORD1 7782-49-2 Se by furnace 5 6.4 ug/L EPA 200.9 5/17/10 ESTAFFORDI 7440-66-6 Zn by ICP 10 4500 ug/L EPA 200.7 5/27110 ESTAFFORDI Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908 For a detailed description o(the qualifier codes reterto ti vgal.nrdenr.orciAvah.M«ah?etaflin o_Yechassist#Data qualifier Crdes <httnataortal.nrAenr_umMah�lv<L�b�staffnfi?techassist> Page 1 of 1 J GROUNDWATER FIELD/LAB FORM Location code County 90 WA,-j Quad No Serial No Lat. Long._ OaL E TYPE Water Department of Environment and Natural Resources DIVISION OF WATER QUALITY -GROUNDWATER SECTION Lab Number Date Received] Rec'd By:.. From Other:_ _ 47P 6; Report To: ARO, FRO ll RO, WaRO, WiRO, III Ili Data Entry y: Ck: WSRO, Kinston FO rust, Central Off., Other: Date Reported: Shipped by: Bl. , Cour and Del., Other. Purpose: Collector(s): ��1 Date .S�lo aElo Time I' L- 1 PA Bas li e, Complain , Compliance, LUST, Pesticide Study, Federal Trust, FIELD ANALYSES Owner N (circle one) PH 400 Spec. Cond.94 at 25°C Location or Site r Temp.to °C 0 or Description of sampling point Appearance 1d., �� ( Sampling Method dpazz Cyr Sample Interval Field Analysis By: f) Remarks Mumo. bailer. a c. LAB 0 RATO RY ANALYS ES (Pumping time, air temp., etc.) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml TOC 680 mg/L Turbidity 76 NTU Residue, Total Suspended 530 mg/L pH 403 units Alkalinity to pH 4.5 410 mg/L Alkalinity to pH 8.3415 mg/L Carbonate 445 mg/L Bicarbonate 440 mg/L Carbon diobde 405 mg/L Chloride 940 mg/L Chromium: Hex 1032 ug/L Color: True 80 CU Cyanide 720 mg/L Lab Comm ❑ Soil ❑ Other Chain of Custody Diss. Solids 70300 mg/L Fluoride 951 mg/L Hardness: Total 900 mg/L Hardness (non-carb) 902 mg/L Phenols 32730 ug/I Specific Cord. 95 NMhos/cm Sulfate 945 mg/L Sulfide 745 mg/L Oil and Grease mg/L NH3 as N 610 mg/L TKN as N 625 mg/L NO2 + NO3 as N 630 mg/L P: Total as P 665 mg/L Nitrate (NO3as N) 620 mg/L Nitrite (NO2 as N) 615 mg/L GW-54 REV. 7/03 For Dissolved Analysis -submit filtered sample and write "DIS" in block. SAMPLE PRIORITY ❑ Routine ❑ Emergency Ag-Silver46566 ug/L AI -Aluminum 46557 u /L As -Arsenic 46551 u /L Ba-Barium 46558 u /L Ca -Calcium 46552 mg/L Cd-Cadmium 46559 u tL Cr-Chromium 46559 ug/L Cu-Copper 46562 u /L Fe -Iran 46563 u /L Hg-Mercury 71900 u /L K-Potassium 46555 m /L Mg -Magnesium 46554 m /L Mn-Manganese 46565 ug/L Na-Sodium 46556 m /L Ni-Nickel u /L Pb-Lead 46564 ug/L e-Selenium u /L Zn-Zinc 46567 u /L Or anochlod a Pesticides Or ano hos horus Pesticides Nitrogen Pesticides Acid Herbicides PCBs Semivolatile Organics TPH-Diesel Range Volatile Organics VOA bottle TPH-Gasoline Range TPH-BTEX Gasoline Range LAB USE ONLY Temperature on arrival (°C): 0 ALCHEM, INC. Corporate Office 2042 Buie Philadelphus Road Red Springs, NC 28377 Tel. 9io-843-2121— 800-522-2944 Fax 9io-843-5789 rfa@semr.net February 18, 2011 Mr. Andrew Pitner Regional Environmental Supervisor NCDENR Division of Water Quality Mooresville Regional Office 610 East Center Ave. Suite 301 Mooresville, NC 28115 Permit #: WQ0002702, WQ0016338 Dear Mr. Pitner: Sales and Manufacturing 8135 Red Road Rockwell, NC 28138 Tel. 704-279-79o8 — 800-462-2586 Fax 704-279-8418 wolcott_r@yahoo.com I would like to request a 15 day extension to submit our reporting requirements for our permits as well as submission of our monitoring well samples reports. We have had some employee problems arise that have delayed our reporting. Best regards, ALCHEM, INC. /1"Lo/ jj Randall F. Andrews, President 0 i �N v C1 ' �l��C'La- (, l�� �- -�4� f� �e i7'1`%�i _ � � .; �in � � ✓ i w(N� 1 `-� cam--- Huffman, Ellen From: Hardee, Ed F Sent: Thursda March 31,720�111:50PM To: Huffman, leg Subject: RE: ALCHEM Ellen, Below are the facilities I have as not submit ing an annual report in MRO. The ones in red have request in as noted. Alchem did request an extensio. , due t� oday WQ0000701 Tyson Poultry Inc W00002378 Town of Mooresville WQ0002616 City of Albemarle WQ0006860 Pilgrim's Pride Corporation WQ0006906 Town of Taylorsville WQ0016338 Alchem Incorporated WQ0032332 Water & Sewer Authority of Cabarrus County W00033960 Organic Plant Health LLC Ed Hardee Aquifer Protection Section Land Application Unit 1636 Mail Service Center Raleigh, NC 27699-1636 Phone (919) 715-6189 Fax (919) 715-0588 Harmony, NC Rendering Plant Residuals Land Application Program Requested to rescind permit Rocky River WWTP City of Albemarle Residuals Land Application Program (D) Extension Granted Marshville, NC Processing Facility Residuals Land Application Program Town of Taylorsville Residuals Land Application Program Extension Granted Alchem Incorporated Residuals Reuse Program Extension Granted Rocky River Regional Wastewater Treatment Plant Organic Plant Health DISCLAIMER: Per Executive Order No. 150, all e-mails sent to and from this account are subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Huffman, Ellen Sent: Thursday, March 31, 2011 1:22 PM To: Hardee, Ed Subject: ALCHEM Ed, Do you have a list of missing annual reports for MRO? If so, please send me a copy seeing one. Did they ask for an extension? Thanks! little old forgetful me;-) Ellen Huffman Environmental Specialist II North Carolina Dept. of Environment & Natural Resources Aquifer Protection 610 East Center Avenue Mooresville, NC 28115 Ph:704.663.1699 Fax:704.663.6040 Also, is ALCHEM on it? I don't recall 1 ALCHEM, INC 8235 RED -ROA � D CKWF�, NC 2823 MAR A 9 2010 704-279.7908 fax 70279-8r��0�' DM -,4 !:'. i'iotection 2009 ANNUAL MONITORING REPORT Permit No. W00016338 Bauxite Residuals Mono -fill Surface Disposal Program 1. Annual Residual Report 2. Residuals Analysis 3. TCLP Analysis 4. Quarterly Groundwater Monitoring 5. Lagoon Records, Application Activities Jason A. Desiato Chief Operating Officer .; 7 Annual Residual Report )- 4,5elpd / — � ,Q - / 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 �I? ( tr : E-mail: - ANNUAL RESIDUAL REPORT wolcott_r@yahoo.com ) � 'T `� Purpose NCDENR S'3 `0, _go SURFACE DIPOSAL PERMIT REQUIREMENT �� �. /�- �/Cl \fJ o }'`� � �i � % `f��}�l� '.� � IJL, �o I J Date: 3/08 - 6/09 REACTION # I DATE I BAUXITE USED I % SLURRIED OUT LAGOON # SAMPLING PORT PH I LAGOON PH f t C f 12130l2008 I� 20 TONS I 6% i _I__ Pf24.20D;9 D TCJ . 5. 6 I =. 0W2Q' 1/5/2009 20 TONS 6% I I h` (�/�`� J vV V 1/6/2009 a j I 20 TONS 6% 6.92 �( `v 7 C� 1f712009 I 20 TOMS 6% �t p 1/8/2009 +T t 1 I 20 TONS 6% I S�� r� �J 1LJ 119/2009 20 TONS 11�V I/12/2009 P,} ' 20 TONS I 6% I 1 I 6.89 I/13/2009 I 20 TONS 6% I 1 1/14/2009�/ I/15l2009 111612009 I 20 TONS 20 TONS 20 TONS I I 6% 6/ I 6%, I I I . I ! /') 1/19/2009 I 20 TONS 6% �. 'bc1/21/2 _ I120/2009 009 2D TONS I 20 TONS I � 6% I b, I I I I 689 l CODa 112212009 I 20 TONS 1�- '�-LXJ I 6% r I123/2009 I 20 TONS I 6% 1/26/2009 I 20 TONS I I �+ .. 1/27/2.009 I 20 TONS I 6% 9; 1/28/2009 20 TONS Rr onoDa 6% 1 I e 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERM17 REQUIREMENT Date: 3108 - 6109 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT LAGOON PH I I I PH �j-W 10�✓1�J 112912009 20 TONS 6% I 1 I� 6.75 ' �1.3 1/30/2009 20 TONS 6% I l,' 212/2009 20 TONS i 6% 1 y �� 2/3/2009 I 20 TONS 6%000a i I I ✓ J s 00(D a s u4/2009 i 20 TONS I b% I i n 2/5/2009 \ ( 20 TONS 6% 1 6.90 216/2009 20 TONS 6/ I I J 9 2/9/2009 I 20 TONS 6% 2/10/2009 20 TONS I 6% 1 I I 2/1 112009 20 TONS I 6% I I 6.96 � —moo �• I 2/12/2009 I 20 TONS 6% I I I -7 , L) q I �rO Z 2/13/2009 20 TONS I 6% i I 211612009 I 20 TONS 6% I 211712009 20 TONS I 6% i I I 7.10 I T 2/18/2009 i 20 TONS I 6% I I 4 2/19/2009 20 TONS I 6% I I � I I 2120/2009 20 TONS 6% I I nL 2/23/2009 20 TONS I 6% I I i 70 (( 2/24/2009 20 TON$ 6% 1 6.98 _ R i o i 2/2512009 I 20 TONq I 6% I v 0 (1) �r7 —7 ALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 Phone:704-279-7908 Fax:704-279-8418 E-mail: wolcott_r@yahoo.com REACTION # DATE I BAUXITE USED % SLURRIED OUT I LAGOON # I SAMPLING PORT I PH LAGOON PH 2/2612009 I 20 TONS 6% 1 2/27/2009 20 TONS I 6 q /� 7 312/2009 I 20 TONS I 6% 3/312009 I 31412009 20 TONS, I 20 TONS I 6% 6% 1 — 5 315/2009 I 20 TONS I 6% I I 7.12 nn 3/6/2009 I 20 TONS 6% C- 7 o 31912009 20 TONS 6% _ I 'OCt� ZGx� 3/10/2009 20 TONS I 6% I I 3/11/2009 20 TONS I 6% I I 6.87 - Z�1 3/12/2009 20 TON$ I 6% I _ L r _ 22 3113/2009 20 TONS 6% 3/16/2009 I 20 TONS I 6% I lL 1 3117/2009 20 TONS 6% I I _ ,I 311812009 311912009 3120/2009 312312009 3/2412009 I 20 TONS I 20 TONS 20 TONS I 20 TONS 20 TONS' I 6% I I I 6% 6% 6% i 6.89 7.zo r_ +' I _ fit( -G7cyo r 3/2512009 i 20 TONS I 6% 2 I ta=r' 1t'\ ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo_com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dale: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT I LAGOON # SAMPLING PORT LAGOON PH PH I 3/26/2009 20 TONS 6% I 2 - 2-L L 3/27/2009 20 TONS; 6% I 2 CC L4 3/30/2009 I 20 TONS 6% 2 3/31/2009 20 TONS I 6% 2 411/2009 20 TONS 6% I 2 I 7.10 I 4/212009 20 TONS I 6% 2 1 I �' 4/312009 I 20 TONS I 6% 2 1 416/2009 20 TONS I 6% I 2 T -OOQ 26ql i 4/7/2009 20 TONS, 6% I 2 418/2009 I 20 TONS I 6% 2 7.11 4/9/2009 20 TONS 6% I 2 �y Y _ L_ 1i 4110/2009 20 TONS 6% 2 I 411312009 I 20 TONS' 6% I 2 I I I �/ (�1 r j 4/14/2009 20 TONS- I 6% I 2 7.05 4/1S/2009 20 TONS- I 6% I 2 4/1612009 I 20 TONS 6% 2 4/17/2009 20 TONS • 6% 2 r I 4/20/2009 20 TONS 6% 2 I _ I I 4/21/2009 20 TONS I 6% I 2 412212009 I 20 TONS,, 6% 2 6.98 I �l I 0/1 ALCHEM, INC ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # I DATE 412312009 31 4124/2009 _00 2--' I:T r 4f2712009 4/28/2009 C— I 4/29/2009 5 l � 4/3012009 51112009 514/2009 5/5/2009 5/6/2009 5/712009 J 5/812009 , 511112009 G 7 _C av 01 s 511212009 5/13/2009 5114/2009 5115/2009 S11 W009 s 5/ 1912009 S/2012009 813 5 RED RD ROCKWELL, NC 28138 Phone:704-279-7908 Fax:704-279-8418 E-mail: wolcott_r@vahoo.com 0 BAUXITE USED % SLURRIED OUT I LAGOON # I SAMPLIPNG PORT I LAGOON PH 20 TONS I 6% I 2 20 TONS I 6% I 2 20 TONS I 6% i 2 20 TONS I 6% I 2 20 TONS I 6% I 2 20 TONS I 6% 2 I 20 TONS 6% G _ 20 TONS I 6% I 2 I I 20 TONS i 6% I 2 I 6.89 20 TONS I 6% 2 1 eeeQQQ 20 TONS I 6% I 2 20 TONS I 6% I 2 20 TONS i 6% 2 20 TONS I 6% 2 I �A �' 4 20 TONS I 6% 2 I 6.92 I I 20 TONS I 6% 2 20 TONS 6% I 2 20 TONS I I 6% 2 ° 20 TONS I 6% 2 20 TONS I 6% I 2 ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # I SAMPLING PORT I LAGOON PH I I I PH 5/21/2009 I 20 TONS 6% I 2 _ 5/22/2009 20 TONS I 6% I 2 5125/2009 I 20 TONS I 6% I 2 5/26/2009 20 TONS I 6% 2 5/27/2009 20 TONS I 6/ I 2 7.10 i - ccc) iici 512812009 I 20 TONS 6% I 2 p— L 512912009 I 20 TONS 6% 2 611/2009 20 TONS 6% I 2 I „ t — 3C-G 6/212009 I 20 TONS I 6% � z � — w i I 613/2009 20 TONS 6% 2 (a3e1 I 6/4/2009 20 TONS 6% 2 6.78 6/512009 20 TONS I 6% I 2 6/8/2009 I 20 TONS 6% I 2 P) T-cI 6 I 20 TONS 6% 2I j I 6/1012009 I 20 TONS 6% I 2 6111/2009 I 20 TONS I 6% I 2 6.89 M I�I (�- 6112/2009 I 20 TONS I 6% 2 6/1512009 I 20 TONS 6% 2 Y 7�(Q) Z� 6/16/2009 I 20 TONS I 6% I 2 6/1712009 20 TONS 6% 2 j -OC 2" M lrx i ALCHEM. INC ru. 8135 RED RD Phone: 704-279-7908 ROCKWELL. NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT I LAGOON PH I I PH 6/18/2009 20 TONS 6% I 2. ZZ �� 6/19/2009 20 TONS 6% I 2. I I rt7 _ 6/22/2009 20 TONS 6% 2, ^ZL 6/23/2009 20 TONS 6% 2' r�J�T' ��\ 1 % Z 6/2412009 I 20 TONS 6% I 2. -coux 2 I 6/25/2009 20 TONS 6% 2' 612612009 20 TONS 6% 2 _ I 6/29/2009 20 TONS' 6% I 2. f <l ? i 6/30/2009 I 20 TONS 6% 2 cz 1 i- t Lt j i� 2 m tom: m ALCHEM, INC ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # :92- SAMPLING PORT PH LAGOON PH C i ��I 1 f .3 07- � 11 gd5 z (�•�'o 0-7- - 1 . s S -Q q 0 h I lL s 1 1 J �,5 r 1 0 —IS— 07-2 `.� It �) a - c [ C o - 3i-0 It 1 M31 09 ki C� j I ID ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dare: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH co . IR � -r / ° ^,o- i- Gq rL , S- (', - C) d • (a 1 I . , c' >ct I I z 7 ��-�s-0h �U i I 5 I 7 U/S-o7J6q c0 cs3-o7—a( 3 r ��-_�,�z_ Cq I(��� yC cv-C I 0 G) 6F ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # �� SAMPLING PORT PH LAGOON PH V -Z-C -Oct it Jd' q _J � —09 -o`f 1 i (v ' 6.6 f Cl�-/1-)y A 5 3 qq 0S3-12-bq 1/ 6, J .so e.9 -13 -o # L - ? a S o 3 -01 _�� .. 2 G• 17 / D-l3-oK`.� o -/f-oy 54/ o f f- q v'd 1� 9 Icy /� s � -�-o rI�JS � �� I ��,G f �•�� S� n -/ -o �0 i 0 ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6109 REACTION # DATE I BAUXITE USED % SLURRIED OUT LAGOON # I SAMPLING PORT PH LAGOON PH 05-]7 O I l! Jji '" I `O c I V a e 67 ��-I -oq >l - I � �• G G ',-0 , G' G�1`� ' ,1;'9 II JA 6. �0 C R 2c c%rr� - -21cq 6� a 6 -9- -c 12 --7 l I I I I P ALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 Phone: 704-279-7908 Fax:704-279-8418 E-mail: Wolcott r(@.vahoo.com REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH -��-oy 1 J,) . -� 0y l �#� c • G . CG c,02 -21-37 J Goy W -20� L lO.��i� V 02 c( 5-2Z-09 n V�J• C 1 I.- Ofl 11 c> 6 1 C. / 0 i r ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMfT REQUIREMENT Dace: 3108 - 6109 REACTION # DATE BAUXITE USED Ill % SLURRIED OUT LAGOON # SAMPLING PORT I PH LAGOON PH ip -s ci i - os 9 i t k, 6�_CI -oc I If �o 1 l- i- —09 ! f dl_ d 0 - C't-c`i (' QS a / - 0 I I . 7, 0 �i C/- -cq //JA5 - c, - 4 I c 16, ' J I ALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 Phone:704-279-7908 Fax:704-279-8418 E-mail: WoIcott_r@yahoo.com REACTION # DATE BAUXITE USED 1 % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH o — r 9 -l0- 11 ds lS � zu 2 9 061- i1 -09 (l Y j S 9-6 -)I- 0 9 ii ,.d -1/ - .y I - �5 9_ 2-0q 11 # G,7 b dS I i 3c O- 3 01 -I (-Oq q_ 15 .-oq G a6 i- 9 a - t5-.oq'F u Yj5 0 Gq- is j t( `j ,� �� u6) . m m ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT DaEe: 3108 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT I PH LAGOON PH G l iycl S JC/ #-9 q.- �i- q 1 r -cw9 on 4.1r a �. _ L`, — C. ��) C 1 — c 142- / 0 .a 1� ALCHE V- , INC-- a 8135 RED RD ROCKWELL, NC 28138 ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMFT REQUIREMENT Date: 3/08 - 6109 Phone: 704-279-7908 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com REACTION # DATE I BAUXITE USED 1 % SLURRIED OUT I LAGOON # I SAMPLING PORT I PH LAGOON PH .ti5 �S 16 - 5 �•3 165 .- /, Q ��, oL. �- a - ,10cl I yj` 169 10 `` - i� YJ . --97-0q 123 0q '--f45 -0 q 9A C( -as_c q // l C ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL. NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3108 - 6/09 REACTION # DATE I BAUXITE USED % SLURRIED OUT I LAGOON # I SAMPLINiG PORT LAGOON PH _,O 1� yj 5 . 4+ O � J... - r t t V.4 G,a( 6.0< , o // .J'1 ; � � % G a I 16)-Ff :;-�,r _o yd cl i qq i(,--oI/ N �j fa., ,-c I `ljs CD �. it -cry 1( yJ D - Rb ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date 3I08 - 6109 REACTION # DATE I BAUXITE USED I % SLURRIED OUT I LAGOON # SAMPLING PORT I i LAGOON PH - 1:�-cjq /l Yj 5 �. d 6./7 aS gi QS 0 - I . 3.-oq tj Y r'--__07 e JS 2, . - 2_ i - CA Z 0 1- 2-1 - 091 1 ;I 6,42 16. 7 I ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott—r@yahoo.com ANNUAL RESIDUAL REPORT Purpose: NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # L I SAMPLING PORT PH LAGOON PH 2z 2- -2 J, 1 .22.3 t'io 2- 3 - Qq it 610 6 Ca.. ail - 0 1 11 c er, e 9)� L 2 -zin (11 2- s -9-q - 09 c A- 2 FOA, ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott—r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3108 - 6109 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH — —I J4 - J 1 I �[. — — �J 1 I � t 1. 9q:7 it-02, clI 1•�� C.30 ki CIS -o-09 1l 11 U,4 c 411 , 2 - l2- '- 2s 5� ! -o ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL. NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3108 - 6109 REACTION # I DATE I BAUXITE USED I % SLURRIED OUT I LAGOON # SAMPLING PORT I PH LAGOON PH lo G l _ 1 41- CI 9 ZY n, - _0.e y �� �: S �•S-� G j� b �J sj _per c- ` is CL �- -i9-09 6 - -i 3s �•� j (- _�q (( YJS �� 2 NO, ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 REACTION # DATE u BAUXITE USED N SLURRIED OUT LAGOON # I SAMPLING PORT PH LAGOON PH yj 2 _a5-0 J5 35 b.�G 5 11 - 3o- o I 11-;0-0q I s 1 l� 2 - o �= 1 3 L.1-a2-0a I /- -03-0�Z .b 1c 3 '-z/ 2 30 ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Dace: 3/08 - 6/09 REACTION # DATE BAUXITE USED ; SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH 219 G. 60 - 0 5 - 0 OS / --o - o q / Qds C 2 �S 306 1 -0 -o ll a- l0-0 /2-/0 -0� 311 7,e I 7i l -P- - -o 1 It- 0 9 3 - �Kc ALCHEM, INC 8135 RED RD Phone: 704-279-7908 ROCKWELL, NC 28138 Fax: 704-279-8418 E-mail: wolcott_r@yahoo.com ANNUAL RESIDUAL REPORT Purpose NCDENR SURFACE DIPOSAL PERMIT REQUIREMENT Date: 3/08 - 6/09 REACTION # DATE BAUXITE USED % SLURRIED OUT LAGOON # SAMPLING PORT PH LAGOON PH 1( J f q 32_5 —2,3,— - - -0 9 6 1 Y 2-- ` - v UR Al �Zfy s 2- - l[ v (� -'q� 3 - /C, Residuals Analysis 01/05/2uiu li-u'1 PAR Laboratories, Inc. LASORA7t7RlES, INC, www.parlabs.com AL' .�n: TR N _T%tti r_L nLc-�M INC R135 ?=7 R P.O. Box 411423 Charlotte, NC 28241.1483 Phone: (704) 535-8333 Fax: (7041 588.8335 NC CERT #20; SC CERT #99005 T-EPORT OF ?RG ,EC= NAM' DEC 09 SA`L ti ti,rF 5 scG3 SWFLE ID- F,ESI A S P,1A=`STS ' 7.. SAMPL.71 MATRIX- ' S Wt., 'd �.%'L /(;,OR TT.is.r� SAtiL�LED- C"-c DAT.-mREC.�.� _ - 1 2: J9/09 FOT SL C SLED RECETVED BY- D T"i„E RECE: 330 DE-IiT-F.ED iXl?E SAMPLE-- Gra� ?3QC 7 C ?' E1 MIDiARY RESULTS A\1AL1S1S ANALY-TS METH -OD ;r_E TIMa B3 RESULT UN.7.TS 1j° LTL SM 4 _ .�1'.1. y —D 12 / 3 / 0 �' 7 0 0 CN ST:GVFR, TC- i. E2l_ _J C t 2/31 /09 1030 C_ <^0. 10 ;ng/L - /� � � 1�t 1 Q 00a-;1''� icr7 iY C:r�t'f _-- ccS?�-C, T _ C, ^/��° 1v30 CT� <'D 0 mg 20C.7 "2/31/03 IC30 C_ r.8.4 7- L CAT,�yU'_f, T07'.= FT- a. 20C. , 1 7/'31 / 0 9 1030 CT 3, 040 mar/.L. - 0. 12/3' /09 1 030 C" 0.10 ^Ig/L rROMI:i'✓ - E=ti -0_.- 2!31/09 10?0 CT b.97 mG/L COPP=.P, TGTI'--- . ._ , , , 2/31 / 0 9 1 030 CT 7 .00 rnq/L MERCU!?,' , T07- 2 \. C. ma/L MACN.�_STUM, T'.'`.f.'P.:, 7-PA =0" 1LI3;/v9 103'C CT 74.6 Tq/r N,VCANESE, - :T=. =Fn OD_- 12/3'i09 '030 C= 0.954 -1J/L 50DI:aJ, =^v- ._ E3 Z%?_ % 12/31/09 1030 CT 212 mg 20C.- 12/31/O9 1030 CT 2.11 Tng/.T_ =i-CS_ 03 S, `(_,aL 7r 204. '31/09 1030 C= 9.°7 ~q/L L,r:AD, TOTA"• EFA 200 -7 1 2/31 /09 1030 CT :�.?8 .:.g/L EL�D:-UJ:, _ EPA 20'?. 2/3" /C9 030 C;: 0.7?2 ng/L ZINC, TC^:�T => N '0_.7 17!31109 103C CT 1 .74 T.q/ Cl WAB OF-CH'010E, Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 Report Summary Tuesday November 24, 2009 Report Number: L432444 Samples Received: 11 / 10 / 0 9 Client Project: TBL-20793 Description: 12065 Lebanon Rd. Mu. Juiiet' T'N 37122 (615) 758-585P 1-800-76-1-5859 Fax (615) 758-5859 T'ar. T.D. 62-0814289 Fst. 19-10 r The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. Tif you have any questions regarding this data package, please do not legit to�,R-ep-r—es-e-nf-a-t-i—ve Entire Report Reviewed By:• _— John ;% _a��ma Laboratory Certification Numbers i, A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-232�, CT - PH-0197, FL - E87487 GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375,DW9-1704, ND - R-140 NJ - TN002, Ni NELAP - TN002, SC - 84004, TN - 2006, VA - 00109, WV - 233 AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from Environmental Science Corp. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. 2 Samples Reported: 11/23/09 17:09 Revised: 11/24/09 10:36 Pace 1 0f 6 12065 Lebanon Rd. Mt, ,tuii.et, TN :37122 (615) 758-5858 1-800-767-5859 OESC F'ax (f•15) 758-5859 L•A-@ S•C•!•E•N•C•E•5 T a:c J.D. 62-0814283 Est. 1970 REPORT OF ANALYSIS Pam Hester November 24,2009 TBL Laboratory P.O. Box 589 Lumberton, NC 28359 ESC Sample # : L432444-01 6 Date Received November 10, 2009 Description Site ID 7N4. D SAN Project # TBL-20793 Collected By Collection Date 11/08/09 16:00 Parameter Dry Result Det. Limit Units Method Date_ Dil. Nitrate -Nitrite BDL 3.6 mg/kg 9056 11/18/09 1 Phosphate as P BDL 1.6 mg/kg 9056 1.1/18/09 1 Corrosivity BDL 0.0 9040C 11/19/09 1 Cyanide BDL 0.45 mg/kg 9012E 11/18/09 1 Ignitability BDL 0.00 Deg. F D93/1010A 11/19/09 i Ammonia Nitrogen BDL 9.1 mg/kg 350.1 11/17/09 1 PH 8.3 0.0 su 9045D 11/17/09 Reactive CN (SW846 7.3.3.2) BDL 0.230 mg/kg 9012B 11/18/09 1 Reactive Sulf.(SW846 7.3.4.1) BDL 45. mg/kg 9034/9030B 11/17/09 1 �j Sl..1 t,og� vKu 4' 36. mg/kg 351.2 11/18/09 1s Total Solids 100. 0.00 z 2540G 11/18/09 1 Mercury BDL 0.036 mg/kg 7471 11/17/09 1 171 jRu Ivnum 2T00'0 9.1 mg/kg 6010B 11/18/09 1 Arsenic BDL 3.6 mg/ka 6010B 11/19/09 2. Cadmium BDL 0.45 mg/kc 6010B 11/18/09 1 Calcium 20000 45. mg/kg 6010E 11/18/09 1 Chromium 22. 0.91 mg/kg 6010B 11/18/09 1 Copper BDL 1.8 mg/kg 6010B 11/18/09 1 Lead 15. 0.45 mg/kg 60106 11/18/09 1 Magnesium 110 9.1 mg/kg 6010B 11/18/09 1 Molybdenum 0.98 0.45 mg/kg 6010E ii/18/09 1 Nickel 3.6 1.8 mg/kg 6010B 11/18/09 1 Potassium 640 45. mg/kg 6010B 11/18/09 1 Selenium 4.0 1.8 mg/kg 6010B 11/18/09 1 Silver BDL 0.91 mg/kg 6010E 11/18/09 1 Sodium 140 45. mg/kg 60103 11/18/09 1 Zinc 3.1 2.7 mg/kg 6010E 11/18/09 1 Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted Reported: 11/23/09 17:09 Revised: 11/24/09 10:36 L432444-01 (PH) - 8.3@20.2c L432444-01 (IGNITABILITY) - Did Not Ignite @ 170 F Page 2 of 6 TCLP Analysis Pam Hester TBL Laboratory P_0. Box 589 Lumberton, NC 28359 Date Received November 10, 2009 Description Sample ID SAND Collected By Collection Date 11/08/09 16:00 Parameter REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 75P-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289, Est. 1970 November 24,2009 ESC Sample # : L432444-02 Site ID Project TBL-2.0793 Result Det. Limit Units Limit Method Date/Time By D "T1- - 1311 11/18/09 0730 MVE 1 Mercury BDL 0.0010 mg/1 0.20 7470A 11/18/09 1738 CLL 1 Arsenic BDL 0.050 mg/l 5.0 6010B 11/18/09 2120 ALT 1 Barium BDL 0.15 mg/1- 100 6010B 11/18/09 2120 ALT 1 Cadmium BDL 0.050 mg/1 1.0 6010B 11/18/09 2120 ALT 1 Chromium BDL 0.050 mg/1 5.0 6010E 11/18/09 2120 ALT 1 Lead BDL 0.050 mg/1 5.0 6010B 11/18/09 2120 ALT 1 Selenium BDL 0.050 mg/l 1.0 6010B 11/18/09 2120 ALT 1 Silver BDL 0.050 mg/1 5.0 6010B 11/18/09 2120 ALT 1 TCLP ZHE Extraction - 1311 11/19/09 0744 MVE 1 TCLP Volatiles Benzene BDL 0.050 mg/l 0.50 8260B 11/20/09 0947 1 Carbon tetrachloride BDL 0.050 mg/1 0.50 8260B 11/20/09 0947 1 Chlorobenzene BDL 0.050 mg/1 100 8260E 11/20/09 0947 1 Chloroform BDL 0.25 mg/1 6.0 8260B 11/20/09 0947 1 1,2-Dichloroethane BDL 0.050 mg/l 0.50 8260B 11/20/09 0947 1 1,1-Dichloroethene BDL 0.050 mg/l 0.70 8260B 11/20/09 0947 1 2-Butanone (MEK) BDL 0.50 mg/l 200 8260B 11/20/09 0947 1 Tetrachloroethene BDL 0.050 mg/l 0.70 8260B 11/20/09 0947 1 Trichloroethene BDL 0.050 mg/1 0.50 8260B 11/20/09 0947 1 Vinyl chloride BDL 0.050 mg/1 0.20 8260E 11/20/09 0947 1 Surrogate Recovery Toluene-d8 101. % Rec. 114. 8260B 11/20/09 0947 1 Dibromofluoromethane 103. % Rec. 125. 8260B 11/20/09 0947 1 a,a,a-Trifluorotoluene 104. % Rec. 114. 8260E 11/20/09 0947 1 4-Bromofluorobenzene 99.0 % Rec. 128. 8260B 11/20/09 0947 1 TCLP Pesticides Chlordane BDL 0.0050 mg/l 0.030 8081A 11/20/09 0357 CSU 1 Endrin BDL 0.0050 mg/l 0.020 8081A 11/20/09 0357 CSU 1 ' Heptachlor BDL 0.0050 mg/l 0.0080 8081A 11/20/09 0357 CSU 1 Lindane BDL 0.0050 mg/l 0.40 8081A 11/20/09 0357 CSU 1 Methoxychlor BDL 0.0050 mg/l 10. 8081A 11/20/09 0357 CSO 1 Toxaphene BDL 0.010 mg/l 0.50 8081A 11/20/09 0357 CSU 1 Decachlorobiphenyl 35.2 % Rec. 123. 8081A 11/20/09 0357 CSU 1 ' Tetrachloro-m-xvlene 35.7 % Rec. 114. 8081A 11/20/09 0357 CSU 1 TCLP Herbicides 2,4,5-TP (Silvex) BDL 0.0020 mg/1 1.0 8151A ll/19/09 1128 CBB 1 2,4-D BDL 0.0020 mg/1 10. 8151A 11/19/09 1128 CBS 1 Page 3 of 6 cmm 'YOU'R LAB OF CHOICE REPORT OF ANALYSIS Pam Hester TBL Laboratory P.O. Box 589 Lumberton, NC 28359 12065 Lebanon Rd. Mt. Ju,1et, TN 37122 (615) 758-5858 1.-800-767-5859 Fax (615) 756-5859 Tar. 1.D. 62-0814289 Est. i97U November 24,2009 ESC Sample n L432444-02 Date Received November 10, 2009 Description Site ID Sample ID SAND Project TBL-20793 Collected By Collection Date 11/08/09 16:00 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Surrogate Recovery 2,4-Dichlorophenyl Acetic Acid 84.2 % Rec. 8151A 11/19/09 1128 CBB 1 - TG ;P : er it Volatiles 4-Dichlorobenzene BDL 0.10 mg/l 7.5 8270C 11/19/09 1805 LSB 1 2,4-Dinitrotoluene BDL 0.10 mg/1 0.13 8270C 11/19/09 1805 LSB 1 Hexachlorobenzene BDL 0.10 mg/1 0.13 8270C 11/19/09 1805 LSB 1 Hexachloro-1,3-butadiene BDL 0.10 mg/l 0.50 8270C 11/19/09 1805 LSB 1 Hexachloroethane BDL 0.10 mg/1 3.0 8270C 11/19/09 1805 LSB 1 Nitrobenzene BDL 0.10 mg/1 2.0 8270C 11/19/09 180.5 LSB 1 Pyridine BDL 0.10 mg/1 5.0 8270C 11/19/09 1805 LSB 1 3&4-Methyl Phenol BDL 0.10 mg/1 400 8270C 11/19/09 1805 LSB 1 2-Methylphenol BDL 0.10 mg/1 200 8270C 11/19/09 1805 LSB 1 Pentachlorophenol BDL 0.10 mg/1 100 8270C 11/19/09 1805 LSB 1 2,4,5-Trichlorophenol BDL 0.10 mg/1 400 8270C 11/19/09 1805 LSB 1 2,4,6-Trichlorophenol BDL 0.10 mg/1 2.0 8270C 11/19/09 1805 LSB 1 Surrogate Recovery 2-Fluorophenol 28.8 % Rec. 87.0 8270C 11/19/09 1805 LSB 1 Phenol-d5 18.5 % Rec. 67.0 8270C 11/19/09 1805 LSB 1 Nitrobenzene-d5 44.5 % Rec. 120. 8270C 11/19/09 1805 LSB 1 2-Fluorobiphenyl 56.5 % Rec. 122. 8270C 11/19/09 1805 LSB 1 2,4",6-Tribromophenol 71.6 % Rec. 148. 8270C 11/19/09 1805 LSB 1 p-Terph.nyl-d14 62.7 % Rec. 149. 8270C 11/19/09 1805 LSB 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Limit - Maximum Contaminant Level as established by the US EPA Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 11/23/09 17:09 Revised: 11/24/09 10:36 Page 4 of 6 G Sample Work Number Group L432444-01 WG451131 Attachment A List of Analytes with QC Qualifiers Sample Type Analyte SAMP Arsenic Run ID Qualifier R1001128 0 Page 5 of. 6 LI U Attachment B Explanation of QC Qualifier Codes Qualifier Meaning (ESC) Sample diluted due to matrix interferences that impaired the ability to make an accurate analytical determination. The detection limit is elevated in order to reflect the necessary dilution. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. in addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA. or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unless qualified as 'R' (Rejected). Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction., and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 6 of 6 Summary of Remarks For Samples Printed 11/24/09 at 10:36:24 TSR Signing Reports: 151 R5 - Desired TAT Per Set -- MTLPREP-15, DISPOSAL-5, SHIPPING-30 - Report only to Pam Hester. Do not change Report TO: Sample: L432444-01 Account: TBLLAB Received: 11/10/09 09:00 Due Date: 11/19/09 00:00 RPT Date: 11/23/09 17:09 Sample: L432444-02 Account: TBLLAB Received: 11/10/09 09:00 Due Date: 11/19/09 00:00 RPT Date: 11/23/09 17:09 I 11 11 Quarterly Groundwater Monitoring L R ATORIES, INC. www.pariabs.com Shipping: 2217 Graham Park Drive Charlotte, NC 28273 CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North r•.,...i; n+ of e 1 Al of nrnl Rc nr CompanyName(billing) Comments/ Special Instructions Alchem, Inc. Address 8135 Red Road City, State & zip code Rockwell, NC 28138 Point of Contact & Telephone Number R#yiii }�'e (704) 279-7908 Page 1 of 3 Sample Taken - By: IS THIS FOR STATE or EPA REPORTING? YES V% NO *Sample type: DW WW GWMW - HW Soil other Sample Temp at time of sampling: °C Sample Temp upon receipt: °C ** Preserved: Yes z/ No Teflon Liner/ Zero Headspace: Yes _ No _ N/A _ Client Sample I.D. Set Up Collection nalyses (Sample Location / Number) Comp Grab Preserv. Date/TimP Date/Time ((Requested -re r-P 1tp`" -- MW-1 p>-' �-4,y c _�"_�y-Dci /v'C-c' TDS, COND, TSS, SO4 MW-1 HNO3 Al e�^r i 5. y 3 _1 " -c e MW-2 <41 C ;u . ;7 TDS, COND, TSS, SO4 MW-2 "V HNO3 Al MW-3 3 , =1 <41 C TDS, COND, TSS, SO4 MW-3 HNO3 Al <_- e; < 4°-C , as TDS, COND, TSS, SO4 C.v __R_NO3 Al i/ Kel rqulsnetl y %. uaie/ i ime PC6GCIVCU uy. va=c i i is �/'E'2,Y _ -�✓ _ .c t 3 `2 5 - (J 91 ` I o_ _ i/U fL .IJ / , ;� Relinquished by: Date/Time by: Date/Time * C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See Other Side 91 ., PAR CHAIN OF CUSTODY LABORATORIES, INC. PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parlabs.com Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 , Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custodv document for acceptance by PAR LahoratoriPs Inr. anti tha North �arollna ue arrment of tnvlronmental ano Natural Kesources. Company Name (billing) Alchem, Inc. Address 8135 Red Road City, State & zip code Rockwell, INC 28138 Point of Contact & Telephone Number Phyllis Drye (704) 279-7908 Sample Taken By: n Comments/ Special Instructions Page 2 of 3 , IS THIS FOR STATE or EPA REPORTING? Y S ✓ NO *Sample type: DW WW GWMW ,� HW Soil other Sample Temp at tim of sampling: °C Sample Temp upon receipt: °C ** Preserved: Yes No Teflon Liner/ Zero Headspace: Yes _ No _ N/A Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date/Time Collection Date/Time nalyses Requested Pt� �:(�) MW-4 T -��� ✓ <4' C -oD / y 2 " u-Oq TDS, COND, TSS, SO4 MW-4 HNO3 Al MW-5 � . L1. r <4* C 3 2L4- TDS, COND, TSS, SO4, MW-5 HNO3 Al P MW-6 p 1 3 <4* C -�4 p4 TDS, COND, TSS, SO4 MW-6 ✓ HNO3 Al MW-7 le �`l 7 /'C <4' C i :�IGJ TDS, COND, TSS, SO4 MW-7 HNO3 Al Imay. L2, �� oXl/ LJCIMI I II I IC 3 LS=off' � - !D Necelveu ay: uatei IIme111..'-JUIQ�L A���,(,�/ Relinquished by: Date/Time Received by: DatelTime * C=CompositeG=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See Other Side fjg�'8RTORIES, INC. www.parlabs.com CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North U; Company Alchem, Inc. I Address 8135 Red Road City, State & zip code Rockwell, NC 28138 Point of Contact & Telephone Number Phyllis Drye (704) 279-7908 Sample Taken By: Comments/ Soecial Instructions Page 3 of 3 IS THIS FOR STATE or EPA REPORTING? YES NO *Sample type: DW WW GWMW ;-" HW Soil other Sample Temp at time of sampling: °C Sample Temp upon receipt: °C "Preserved: Yes r/ No Teflon Liner/ Zero Headspace: Yes No _ N/A Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date/Time Collection Date/Time nalyses lRequested MW-8 t, 3 . <4* C i �.��; TDS, COND, TSS, SO4 MW-8 HNO3 Al °iMV4--9 - <41 C TDS, COND, TSS, SO4 -� HNO3 Al rcennquis� cy: /L uatel I Impe /Kecelved by: UatelTime /,�, .-1q—t../l u.� jib/`✓/ .� ''2� L� ( _I � /�J � �r ,r✓L{.1�i��_,c�1✓�/� �'7 •� ..;,, ,; .:' �_ `. v _ Relinquished by: Date/Time Received by: !, ' Date/Time * C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste '*See Other Side � 5 t=19 i4 PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert # 20; SC Cart « 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89632 SAMPLE ID- ALCHEM MW-1 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 1 of 8 ANALYSIS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL ANALYSIS METHOD DATE TIME BY THERM. 03/24/09 1000 TT EPA 150.1 03/24/09 1000 TT EPA 160.1 03/25/09 1430 BN EPA 160.2 03/30/09 0810 DJ EPA 120-1 03/25/09 1450 CT EPA 375.2. 04/01/09 1606 CT EPA 200.7. 04/01/09 1457 CT LABORATORY DIRECTOR SAMPLE MATRIX-- WW TIME SAMPLED- 1000 RECEIVED BY-- DJ TYPE SAMPLE- Grab RESULT UNITS 16 degrees C 4.82 units 398 mg/1., 13 mg/L 585 urn/cm 249 -,na L 1.02 -rig/L a LABORAWS.1 www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert r 20: SC Cent # 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89633 SAMPLE ID- ALCHEM MW-2 SAMPLE MATRIX- WW DATE SAMPLED- 03/24/09 TIME SAMPLED- 1015 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED RECEIVED BY- DJ TIME RECEIVED- 0910 DELIVERED BY- TT TYPE SAMPLE- Grab Page 2 of 8 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL THERM. 03/24/09 1015 TT EPA 150.1 03/24/09 1015 TT EPA 160.1 03/25/09 1430 BN EPA 160.2 03/30/09 0810 DJ EPA 120.1 03/25/09 1450 CT EPA 375.2 04/01/09 1606 CT EPA 200.7. 04/01/09 1457 CT LABORATORY DIRECTOR 15.8 degrees C 4.00 units 66.5 mg/L 76 mg/L 99.7 um/crn 14.2 mg/L 0.346 mg/L 11 I PAR Laboratories, Inc. I LABORATORIES. INC. www.parlabs.com 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; "Fax: 704-588-8335 NC Cert w 20: SC Cert k 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89634 SAMPLE ID- ALCHEM MW-3 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 3 of 8 ANALYSIS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL SAMPLE MATRIX- WW TIME SAMPLED- 1030 RECEIVED BY-- DJ TYPE SAMPLE- Grab ANALYSIS METHOD DATE TIME BY RESULT UNITS THERM. 03/24/09 1030 TT 16.8 degrees C EPA 150.1 03/24/09 1030 TT 3.24 units EPA 160.1 03/25/09 1430 BN 1,343 mg/L EPA 160.2 03/30/09 0810 DJ 228 mg/L EPA 120.1 03/25/09 1450 CT 2,030 um/crn EPA 375.2 04/01/09 1606 CT 1,270 mg/L EPA 200.7. 04/01/09 1457 CT 202 mg/L LABORATORY DIRECTOR j u PAR LABORATORIES, INC. www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert tt 20: SC Cert #i 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89638 SAMPLE ID- ALCHEM MW-4 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 7 of 8 ANALYSIS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL SAMPLE MATRIX- WW TIME SAMPLED- 1145 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS METHOD DATE TIME BY RESULT UNIT'S THERM. 03/24/09 1145 TT 17.1 degrees C EPA 150.1 03/24/09 1145 TT 3.22 units EPA 160.1 03/25/09 1430 BN 4,660 mq/L, EPA 160.2 03/30/09 0810 DJ 580 mg/L EPA 120.1 03/25/09 1450 CT 7,010 um/cm EPA 375.2 04/01/09 1606 CT 7,370 mg/L, EPA 200.7. 04/01/09 1457 CT 1,290 ma/L LABORATORY DIRECTOR 13 E ri PAR Laboratories, Inc. 2217 Graham Park Drive LABORATORIES, INC. PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert # 20: SC Cert # 99003 www.parlabs.com REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89637 SAMPLE ID- ALCHEM MW-5 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 6 of 8 ANALYSIS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL SAMPLE MATRIX- WW TIME SAMPLED- 1130 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS METHOD DATE TIME BY RESULT UNITS THERM. 03/24/09 1130 TT 17.1 degrees C EPA 150.1 03/24/09 1130 TT 4.23 units EPA 160.1 03/25/09 1430 BN 27.8 mg/L EPA 160.2 03/30/09 0810 DJ 7 mg/L EPA 120.1 03/25/09 1450 CT 41.9 um/cm EPA 375.2 04/01/09 1606 CT 1,570 mg/L EPA 200.7. 04/01/09 1457 CT 0.292 mg/L LABORATORY DIRECTOR 11 11 PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333: Fax: 704-588-8335 NC Cert # 20,,- SC Cart # 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89639 SAMPLE ID- ALCHEM MW-6 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 8 0f 8 ANALYSIS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL ANALYSIS METHOD DATE TIME BY THERM. 03/24/09 1200 TT EPA 150.1 03/24/09 1200 TT EPA 160.1 03/25/09 1430 BN EPA 160.2 03/30/09 0810 DJ EPA 120.1 03/25/09 1450 CT EPA 375.2 04/01/09 1606 CT EPA 200.7. 04/01/09 1457 CT LABORATORY DIRECTOR SAMPLE MATRIX- WW TIME SAMPLED- 1200 RECEIVED FAY- DJ TYPE SAMPLE-- Grab RESULT UNITS 11.8 degrees C 3.36 units 1,385 mg/L 86 mg/L 2,080 um/cm 2,238 rng/L 356 ma/L 11 11 11 PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert # 20: SC Cert # 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89636 SAMPLE ID- ALCHEM MW-7 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 5 of 8 SAMPLE MATRIX- WW TIME SAMPLED- 1115. RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FIELD TEMPERATURE THERM. 03/24/09 1115 TT 16.4 degrees C pH VALUE EPA 150.1 03/24/09 1115 TT 4.10 uniLs TOTAL DISSOLVED SOLIDS EPA 160.1 03/25/09 1430 BN 44.6 mg/L TOTAL SUSPENDED SOLIDS EPA 160.2 03/30/09 0810 DJ 24 mg/L CONDUCTIVITY EPA 120.1 03/25/09 1450 CT 66.4 um/cm SULFATE EPA 375.2 04/01/09 1606 CT 4.82 rng/L ALUMINUM, TOTAL EPA 200.7. 04/01/09 1457 CT 0.474 mg/L LABORATORY DIRECTOR 11 PAR LABORATORIES. INC. www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert ## 20; SC Cert # 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: MAR 09 DATE: 04/02/09 SAMPLE NUMBER- 89635 SAMPLE ID- ALCHEM MW-8 DATE SAMPLED- 03/24/09 DATE RECEIVED- 03/25/09 SAMPLER- NOT SPECIFIED TIME RECEIVED- 0910 DELIVERED BY- TT Page 4 of 8 ANALYSIS FIELD TEMPERATURE pH VALUE TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL, ANALYSIS METHOD DATE TIME BY THERM. 03/24/09 1100 TT EPA 150.1 03/24/09 1100 TT EPA 160.1 03/25/09 1430 BN EPA 160.2 03/30/09 0810 DJ EPA 120.1 03/25/09 1450 CT EPA 375.2 04/01/09 1606 CT EPA 200.7. 04/01/09 1457 CT LABORATORY DIRECTOR SAMPLE MATRIX- WW TIME SAMPLED- 1100 RECEIVED BY- DJ TYPE SAMPLE- Grab RESULT UNITS 12.5 degrees C 5.61 units 146 mg/i, 8 mg/L 220 um/cm 42.8 rng/L 0.424 mg/L 13 73 GV%-59A COMPUANCE REPORT FORM Perm t �� C��C� � � V (Submit one each monitoring period x•ith GN'-i4 forme ) 1 Enter date monitoring results were due. ( ) Will this monitoring report (GW-59 and GW-59A) YGS NO be submitted after the established due date? 2 1Was any required information missing on the GW-59 report forms? YES N( '. IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES( NQ identification plate, area overgrown, etc.)? /f the answer it "}es", contact the Regional Of ice.for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO if the answer to question 4 is "NO'; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? if the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 f rms for required wells to the address provided at the top of the current GW-59 form. I hereby ack edge tl a above in o ation was evaluated and the information submitted in this report (kio i ice port GW-59A) is true and complete to the best of my knowledge. 'gnat&r4 of Permittee (or Authorized Agent) I Da e (AV-59A 13/8i2003 ci IMNAIT Pr)DhA nNi VPl i nim PAPFR nNl Y ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM CILITY INFORMATION ` Please Print Clearly or Type cility Name: A I - I Ie rmit Name (if different): r, cov Address: �_s � NC County l Conlact Person: Qobe ( i W OI w� Telephone#: r c) L r%a "7 108 Well Location/Site Name: 5 o y \ No. of wells to be sampled: )EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES AVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (%19)733-3221 PERMIT Number: Expiration Date: A Z Non -Discharge Wa0000Z%0Z UIC NPDES Other PE OF PERMITTED OPERATION BEING MONITORED ® Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): KA VJ ` Date sample collected: 3'02 �%'O g Well Depth: {eft. Well Diameter: 2- in. Depth to Water Level:,q eft. below measuring point Screened Interval: 2 5 ft. to C/ 5 ft. Measuring Point is 2.5 r ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: t 'Lf gallons Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO FIELD ANALYSES: pH y SZ units Temp. °C It Spec. Cond. f Odor A/l/9 Appearance r If WELL WAS DRY at time of sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed: ',> - 1 -Qq � Laboratory Name: ?� \` LAW R �ITO R ��S Certification No. �y PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal 1100m1 Nitrate (NO3) as N mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total Me mg/I AI - Aluminum 0mg/I T^-t (�� c5� i S�'J2Y\� 2� �� � CJIS - (� Mg I L pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron `mg/1 (Specify test and method #. ATTACH LAB REPORT.) Sulfate j y 9 mg/I Hg - Mercury mg/I Report Attached? rA, Yes (1) ❑ No (0) Specific Conductance S55 µMhos K - Potassium mg/I VOC method # Total Ammonia mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): GW-59 Rev.1/2007 Influent Total VOCs: tmuent I oral vut-s: inyl� O SUBMIT FORM ON YELLQV PAPER ONLY GROUNDWATER QUALITY MONITORING: . . COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: c- Permit Name (if different): Facility Address: i 3 1PrxilJAiP_ NC 13F County pwG_D ItactPerson {�O'�e�� 1AL��COTelephone#:-7CA-Z%e1" II Location/Site Name: S (a n-) No. of wells to be sampled: )EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES AVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE OETITER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 . . PERMIT Number: Expiration Date Non -Discharge I�JQc��"a2OZ70-2- UIC NPDES Other 'PE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL SAMPLING INFORMAT__I.4.L1 II FIELD WELL ID NUMBER (from Permit): %(�\/.� 2 Dale sample collected: 3- 2 `.II! ANALYSES: Well Depth: Screened Well Diameter: 2 in. pH 7` units Screened Interval: ft. Depth to Water Level: ' 3" ft. below measuring point 1 Measuring Point is 2 . ft. above land surface Relative M.P. Elevation: ft Odor ftSpec. Cond. . gallons Appearance Volume of water pumped/bailed before sampling: •3 „3 Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO I ABORATORY INFORMATION G y 'PAQ LA�Q R 1 b21�_ '2 _ ' 1 Laboratory Name: Date sample analyzed: � a s - �.CX� PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/l Zn - Zinc /100 I Phosphorus: Total as P mg/I Temp. /618 eC µMhos Certification No. 0-0 mg/I mg/1 DRY at lime of sampling, check here: El Coliform: MF Total m (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): L �U •5 mg/l Al -Aluminum D 3 t i (D mg/I Tot cO SiA soended Dissolved Solids: Total units Ba - Barium mg/I pH (when analyzed) TOC mg/1 Ca - Calcium mg/1 Chloride mg/1 Cot - Cadmium mg/I Arsenic mg/1 Chromium: Total _mg/I ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils mg/I Cu - Copper _mg/I mg/l (Specify test and method #. ATTACH LAB REPORT.) Phenol -mg/1 Sulfate q , mg/I Fe - Iron Hg - Mercury mg/1 Report Attached? W Yes (1) ❑ No (0) c� (� '� µMhos K - Potassium — mg/l VOC method # Specific Conductance Total Ammonia mg/1 Magnesium Mg - g mg/I method # method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): GW-59 Rev.112007 Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM 1 ITY INFORMATION Please Print Clearly or Type a ity Name: I t^ h(2 1 Y-1C- iit Name (if different): /� p itv Address: lS 1_3 r) i � P A 9A _ NC SUBMIT FORM ON YELLOW PAPER ONLY County -� Ce k 01 � Telephonem act Person: Location/Site Name: 5 q M e� No. of wells to be sampled: )EPARTMENT OF ENVIRONMENT R NATURAL RESOURCES )IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-161i- Phone: (919) 733-3221 PERMIT Number: Expiration Date: Non-DischargkjQQQC0)--102 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL >AMPLING INFORMATION 2 m �' J Date sample collected: 3-A—I[A FIELD ANALYSES: CJ o WA' DRY at NELL ID NUMBER (from Permit): 2- in. pH 3 .Qunits Temp. C Nell Depth: 3 55 ft. Well Diameter: Screened Interval: �ft. to 35 ft. Spec. Cond. µMhos time of sampling, Depth to Water Level: &)' /O_ft. below measuring point check Measuring Point is �? y1ft. above land surface � Relative M.P. Elevation: ft. Odor A/A (� here: c Volume of water pumped/bailed before sampling: � " J gallons ` Appearance 1,0 ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION pp 3� a S - C8 Laboratory Name: Certification No. 020 Date sample analyzed: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb Lead mg/I COD mg/I Nitrite (NO2) as N mg/I - Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I mg/I Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 2- Tofa( SLkSOW4,PC &)]JS- d28 Mc, IL Total 3 13 mg/I Al - Aluminum 20 mg/l Dissolved Solids: pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper _ mg/I ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Phenol mg/I O mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Sulfate Specific Conductance 0 3a µMhos K - Potassium mg/I VOC method # Total Ammonia mg/l Mg - Magnesium mg/I method # method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.1/2007 GROUNCLW*AATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Clearly or Type SUBMIT FORM ON YEL OO61. PAPER ONLY Facility Name: Y v r r r) �- Permit Name (if different): Facility Address: i^. _ / 1 r .,n 1 ( NC Z'�—s 13P) County 1� Ov'3an act Person: Rovv r l W O COt I Telephone#: (y Y- Z 7 0(- 7 Q 0 Location/Site Name: No. of wells to be sampled: (from Permifl )EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES )IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 PERMIT Number: Expiration Date: Non -Discharge IA1(a(�000 2?(JZ UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL SAMPLING INFORMATION �i WELL ID NUMBER (from Permit): PAVJ " i Date sample collected: 3 "o9 4 -0 FIELD ANALYSES: / / e C H 1 ;a units Temp. 7. Well Depth: J� ft. Well Diameter: In. P �7• Depth to Water Level: g r 10 ft. below measuring point Screened Interval: x ft. toff. Spec. Cond. ftMhos Measuring Point is 2S ft. above land surface Relative M.P. Elevation: ft. Odor Volume of water um ed/bailed before sampling: gallons Appearance P P P g� _ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO I ABORA ORY INFORMATION Pa Q LI9'PSOR ATOR I ES Date sample analyzed:_= Laboratory Name: r-1 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb - Lead COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Zn - Zinc I Phos horus: Total as P mgll Certification No. 020 mg/I mg/I DRY at time of sampling, check here: El Coliform: MF Total (Note: Use MPN method for highly turbid samples) /100m P Orthophosphate mg/I _Otheer (Specify Compounds and Concentration Units): I S �O�m9 ��- Dissolved Solids: Total �� CP% D mg/I AlAluminum _ _ �f� _mg/I /a I & tk'si6 .Yy�Or/ T— " pH (when analyzed) units Ba - Barium _mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I mg/I ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils mg/1 Cu - Copper mg/I (Specify test and method##.. ATTACH LAB REPORT.) Phenol 3 "70 mg/I mg/I Fe - Iron Hg - Mercury mg/I Report Attached? 't�l Yes (1) ❑ No (0) Sulfate µMhos K - Potassium mg/I VOC method # Specific Conductance _��_ mg/I method # Total Ammonia Total) mg/I Mg - Magnesium mg/I ,method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Mn - Manganese TKN as N mg/l Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: m /L Effluent Total VOCs: mg/L VOC Removal%__ ��*�w�^��k�rt rmrririrrrTrrrnrr r i .n mr . r, a ���. 1i1T�3>F�] f.7/CD qr 11 •1r(`V V Signat o[-Pei tee (or Authorized AgenQ rdrmfttee (or Auth (ized Agent) Name and Title - Please pint or type GW-59 Rev.1/2007 ROUNDWATER QUALITY MONPrORING: OMPLIANCE REPORT FORM Please Print Clearly or Facility Name: -/--W Permit Name (if different): Facility Address: SS `2 NC SUBMIT FORM ON YE1 LOW PAPER ONLY County ontact Person: �r i o I C [) I Telephone#: / ()y'Z7Q-7� /ell Location/Site Name: S F'- M l� No. of wells to be sampled: $_ Orom Permit )EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES NVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1d1J Phone: (919) 733-3221 PERMIT Number: Expiration Date: 2� Non-Dischargk QOCXXZ2-1b2 U I C NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor El Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL FLING INFORMATION L ID NUMBER (from Permit): MvA - Date sample collected: �J-a 4 -0 Depth: _ .�� ft. Well Diameter: �in. to ft h to Water Level: �ft. below measuring point Screened Interval: 2$ ft. ft. Suring Point is _2.5 ft. above land surface Relative M.P. Elevation: ft• me of water pumped/bailed before sampling: _ -2 . I_,� ��_ _( gallons les for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑YES ❑ NO FIELD ANALYSES: pH L%�units Temp. 1_ 7.1 ec Spec. Cond. ftMhos Odor A/ Appearance C I ABORATORY INFORMATION �A� L�$�� �'f O rc(ES Date sample analyzed:_ �,S-Cb9l_ Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb _Lead COD mg/1 Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Zn - Zinc h Total as P mg/I Certification No. zo _ mg/I mg/I ,RY at me of check here: ❑ Coliform: MF Total /100ml Phosp Oros. (Note: Use MPN method for highly turbid samples) Orthophosphate 7 � /I mg/I Other (Specify Compounds and C Units): AI - Aluminum �. 291 mg/I qo` qA Stk&Vended So++oncentration dS— frtU I� 0` Dissolved Solids: Total mg mg/I pH (when analyzed) units Ba - Barium TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I T t I mg/I Arsenic mg/I Chromium. .. mg/I ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils mg/I Cu - Copper (Specify test and method #. ATTACH LAB REPORT.) Phenol mgll Fe - Iron mg/I mg/I Report Attached? �- Yes (1) ❑ No (0) Sulfate 4�10 mg/I Hg - Mercury method # Specific Conductance (� Ot ftMhos K - Potassium mg/I VOC # Total Ammonia mg/I Mg - Magnesium mg/I method method # (Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese mg/l /I , .method # TKN as N mg/I Ni - Nickel mg For Remediation Systems Only (Attach Lab Reports): Effluent Total VOCs: VOC Removal% Influent Total VOCs GW-59 Rev.112007 Id ROUNDVjlATER QUALITY MONITORING: - - OMPLIANCE REPORT FORM , Please Print Clearly or Type Facility Name: .4 1 C -h2 r—y-) Y1 C Permit Name (if different): dress: NC SUBMIT FORM ON YF1 LOlU PAPER ONLY County 1-110 tAI) ontact Person: �i�v r tn) o C.C7 1 ` Telephone#: r7 fit{-"arP -7`tab l(n� No. of wells to be sampled: F fell Location/Site Name: SC — (from Perm_ )EPARTMENT —OF ENVIRONMENT &NATURAL RESOURCES )IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SEM&ECENTER, RALEIGH, NC 27699-1617 Phone; (919) 733-3221 PERMIT Number: Expiration Date: I �' c�IJ ao() Non-Discharge(jC_YQQ2—' D2- UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Ie Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL MPLING INFORMATI9Sl n :LL ID NUMBER (from Permit): �} ��_ Date sample collected;. ell Depth:_ft. Well Diameter: ;?,_in. pth to Water Level: -Z.�6'g ft. below measuring point Screened Interval: ZA—ft. to ft. asuring Point is _?.. `j ft. above land surface Relative M.P. Elevation: H• lume of water pumped/bailed before sampling: _ ____ gallons moles for metals were collected_ unfiltered: DYES ❑ NO and field acidified: ❑YES ❑ NO FIELD ANALYSES: '� Q PH units Temp.—eC Spec. Cond. µMhos Odor Ala Appearance GIP Ck-I' AaQRATQIRY INFORMATION O T� LW nQ Ir6p t _ S ate sample analyzed: Laboratory Name: r'—�-� ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb -Lead Coliform: MF Fecal 1100ml Nitrate (NO3) as N mg/I Zn - Zinc I Phosphorus: Total as P mg/I Certification No. '�? 0_ mg/I mg/I RY at me of ampling, �J Coliform: MF Total I m P (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): 3SL 0 Dissolved Solids: Total 3 g S m 9/I AI -Aluminum m9/l pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I T t I mg/l Arsenic mg/I Chromium. o a Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils mg/I mg/I (Specify test and method #. ATTACH LAB REPORT.) Phenol Mgt] Sulfate d. �R mg"Hg Fe - Iron - Mercury mg/l Report Attached? Yes (1) ❑ No (0) # Specific Conductance 2 O ?) n µ Mhos K - Potassium mg/I VOC method Total Ammonia m9/I M Magnesium g - g mg/I method # method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , TKN as N mg/1 Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports) Perrhitlee (or Authorized Aqent) Name and i file GW-69 Rev.112007 or type Influent Total VOCs: Effluent Total VOCs: mg/L VOC Removal% GROUNDWATER QUALITY M041TORING: COMPLIANCE REPORT FORM or Type SUBMIT FORM ON YE1 L.OInL PAPER ONLY Facility Name: A I Gh e nn Sri Permit Name (if different): p p Facility Address: OcAu 12 l NC ?_$ 3 cQi County "FO W Cy�-N p Contact Person: '� lamer 1 W 0 Telephone#: %oq-off ? 9" 790 cD Well Location/Site Name: Z)a m4� No. of wells to be sampled: e Qrom Permit EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733.3221 PERMIT Number: Expiration Date: Non -Discharge LA/a yZ r%0 Z UIC NPDES Other PE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL 4MPLING INFORMATION[ —1 Permit): ��=! Date sample collected: 4' 9 vvHa FIELD ANALYSES: oC DRY at FELL ID NUMBER (from ) ft.µMhos Well Diameter: 2-in. pH y /O units Temp. time of tell Depth: epth to Water Level: �/ �„ft. below measuring point Screened Interval: ft. Spec. Cond. sampling, /i/ E check leasuring Point is a. s ft. above land surface ft. Relative M.P. Elevation: _ ft. Odor here: ❑ Appearance C/ea2 olume of water pumped/bailed before sampling: 3 9 allons am les for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO ABORATORY INFORMATION ^� _ Laboratory Name: �p ������ DES Certification No. ate sample analyzed: ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb mg/I COD mg/I Nitrite (NO2) as N mg/I -Lead mg/I Coliform: MF Fecal /loom) Nitrate (NO3) as N mg/I Zn - Zinc Coliform: MF Total /loom[ Phosphorus: Total as P mg/I Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate _mg/I O � % 4 � 5 Lopend Dissolved Solids: Total 44 . �0 mg/I Al - Aluminum . mg/I pH (when analyzed) units Ba - Barium mg/I _ TOC mg/I Ca - Calcium mg/I Chloride mg/I Cd - Cadmium mg/I Arsenic mg/l Chromium: Total mg/I mg/I ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils mg/I Cu - Copper mg/I (Specify test and method ## ATTACH LAB REPORT.) Phenol mg/I 4 $2- ing/l Fe - Iron Hg -Mercury m /I El. ort Attached? & Yes (1) No (0) Report p Sulfate r LO µMhos K - Potassium mg/I VOC method # Specific Conductance (o mg/I method # Total Ammonia m /I 9 Total) Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Mn - Manganese TKN as N mgll Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% G Permillee or Authorized Agent) Name and Title - ease printSignature gt'Aermitf-ee (or or type GW-59 Rev. 1/2007 ROUNDWATER QUALITY MONITORING: OMPLIANCt REPORT FORM Facility Name: Permit Name (if different): Facility Address: � I NC SUBMIT FORM ON YELLOW PAPER ONLY Print Clearly or Type 27c I ��"Fl) County ontact Person: �(� V� f" �� �o�'-� Telephone#: - 7q � /ell Location/Site Name: S0.1Y1 e No. of wells to be sampled: (from Permit)_ )EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES )IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733.3221 PERMIT Number: Expiration Date: Zoo Non -Discharged olr3(,) L UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED I&Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: mP ING INFORMATION :LL ID NUMBER (from Permit): WW J Date sample collected: :II Depth: 22 o ft. Well Diameter: in. pth to Water Level: ' 10'I ft. below measuring point Screened Interval:LGL-ft, to 7-0 ft. asuring Point is "Ic , 5 ft. above land surface Relative M.P. Elevation: n• lume of water pumped/bailed before sampling: i' . gallons m les for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO FIELD ANALYSES: pH 5-L(o Lunits Spec. Cond. Odor Appearance _ WELL Temp ��5 eC DRY at • µMhos time of sampling, BORATORY INFORMATION pA a L�r3d R ATOR 1 ES Certification No. �— :e sample analyzed: r3.Laboratory Name: a s-O09 RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/l Zn - Zinc mgll I Phos horus• Total as P mg/I a Coliform: MF Total /100m p (Note: Use MPN method (of highly turbid samples) Orthophosphate mg/I Other ((Specify Compounds an�dConcentration Units): r Dissolved Solids: Total yCe9 mg/I At - Aluminum _ mg/I Total t spend 5-2� 1 i i� �d.r pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium _mg/I Chloride mg/I Cd - Cadmium mg/I mg/I Chromium: Total mg/I Arsenic mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils mg/I (Specify test and method #. ATTACH LAB REPORT.) Phenol mg/I mg/I Fe - Iron Hg - Mercury mg/I Report Attached? 19 Yes (1) ❑ No (0) Sulfate ttMhos K - Potassium mg/I VOC method # Specific Conductance mg/I method # Total Ammonia Total) mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Mn - Manganese _ TKN as N mg/I Ni - Nickel mg/I - method # For Remediation Systems Only (Attach Lab Reports) GW-59 Rev.1/2007 mg/L VOC Removal% Influent Total VOCs: mg/L Effluent Total VOCs: PAR LABORATORIES, INC. www.parlabs.com Shipping: 2217 Graham Park Drive Charlotte, NC 28273 CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina De artment of Environmental and Natural Resources. Company Name (billing) Comments/ Special Instructions Alchem, Inc. Address 8135 Red Road City, State & zip code Rockwell, NC 28138 Point of Contact & Telephone Number Trent Tidwell (704) 279-7908 Page 1 of 3 Sample Taken By: IS THIS FOR STATE or EPA REPORTING? ES >� NO *Sample type: DW WW GWMW 4f HW Soil other Sample Temp at time of sampling:— °C Sample Temp upon receipt: D °C ** Preserved: Yes No Teflon Liner/ Zero Headspace: Yes — No _ N/A Client Sample I.D. (Sample Location /Number*) I Comp I ( Grab I Preserv. I Set Up Date/Time i Collection Date/Time (Requested Analyses I I 1740- I `-TDS. COND, TSS, SO4 MW-1 1 <41 C FMw-1 I JI HNO3 I i AI I f/ I I !?=pS� TDS, COND, TSS, SO4 MW-2 <40C M W-2 I I v/I HNO3 MW-3 I <41 c I I% .3�% I TDS, COND, TSS, SO4 - MW-3 I HNO3 I I I Al Stream �� � <4* I -- - TDS, COND, TSS, SO4 � Al E f j if I I I Stream HNO3 %_a .,. natPrrimP Relmqulsnea Dy:-- Relinquished by: Date/Time Received by: C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well Other Side 1' ; -0 )-L DatefTime ous Waste " See BAR CHAIN OF CUSTODY LABORATORIES, INC. PAR Laboratories, Inc Phone (704) 588-8333 [i Fax (704) 588-8335 www.parlabs.com Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina Department of Environmental and Natural Resources. :�ompany Name (billing) Comments/ Special Instructions Alchem, Inc. Address 8135 Red Road City, State & zip code Rockwell, NC 28138 Point of Contact & Telephone Number Trent Tidwell (704) 279-7908 Page � Pa 9 Sample Taken By: IS THIS FOR STATE or EPA REPORTING? YES NO *Sample type: DW WW GWMW HW Soil other Sample Temp at time of sampling: °C Sample Temp upon receipt: J °C ** Preserved: Yes No Teflon Liner/ Zero Headspace: Yes — No — N/A — Client Sample I.D. (Sample Location / Number) I Comp.I.Grab I.Rresenr. I I Set Up I DateR-rme Collection Date me (Requested Analyses MW_8 I :e <41C TDS, COND, TSS, SO4 MW-8 I HNO3 I I Al MW_g , < 40 C I TDS, COND, TSS, SO4 _ MW_9 I I I HNO3 ` Ai II I I I I I n�ro R"imo Y Uaie/ I IffIC by. Datei rime Received C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring other Side -1 .7 3-2 IX2 _D ous Waste — See I GW-59A CONIPLLA NCE REPORT FORM Permit # K u CO ) L U (Submu one each monitoring period wit* GW-59 fornm) 1 Enter date monitoring results were due. 0 " Will this monitoring report (GW-59 and GW-594) '''YES NO be submitted after the established due date. 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 9 or 2 is 'YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES E'O identification plate, area overgrown, etc)? If the answer is "Yes", contacr the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES 0 If the answer to question 4 is "NO', skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration (s) exceeding standards in the space provided below. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is `NO' skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO , If the answer is "YES"' a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? if the answer to question 7 is 'YES; describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permrttee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form. b J, K t.7—z...,•:.G'?.'Fa— k f-Yc_..n.�+:`J,.w Y-"'" .. � L heist cknornrl d eovertocmao ;w s�eva e n t eino�riiaftosubtt irth�s ,s ; mn repoitl `79.C2(j Signature of Perrnittee (or Authorized Agent) bate GW-59A 12/8/2003 L4BORAFORES.INC. www.parlabs. com PAR Laboratories, Inc_ 2217 Graham Park Drive PO Box 411483 Charlore, NC 28241-1483 Phone: 704-5880333: Fax: 700588/335 NC Cw # 20; SC Cert = 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: jUL 09 DATE. 0//21/09 SAMPLE NUMBER- , 2� SAMPLE TD- ALCHEM 91 t 9 DATE SAMPLED- 07/10/09 DATE RECEIVED- 07/ 1 3/ 09 SAMPLER- ,T --ME RECEIVED- 1230 DELIVERED BY- TT Page1 of 8 ANALYSIS TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL. ANALYSIS METHOD DATE TIME BY SAMPLE MATRIX- WW ME SAMPLED- 0800 RECEIVED BY- Di TYPE SAMPLE- Grab RES:L_ UNITS EPA 160.1 07/15/09 0850 BN 1,950 mg/. EPA_ 150.2 07/20/09 0810 DJ 5 mg/L EPA 120.1 07/15/09 1110 CT ?,9'0 um/cm EPA 375.2 07/15/09 1152 CT 1,158 mg/L EPA 200.7. 07/21/09 0847 CT 21.8 ng/L LABORATORY DIRECTOR 0 PAR �oamRaI. www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 282 1-1483 Phone: TGm@83;Fox: 70-qE835 NC G�# s G>#@9@ 2 PORT of ANALYSES Attn: TRENT TIDWELL ate !NC alas RED Roma ZOO w 1L, NC 28138- ? OJECT NA2S: JUL oe TE: 07,121/09 SAMPLENUMBER- 51256 S zsz :o- rlT c 3R -2 262E SAMPLED,- 07/10/09 DATE RECEIVED- 07/13/09 SAMPLER- 22 III RECEIVED- 1230 DELIVERED s7- 22 wage 2 of a ANALYSIS TOTAL DISSOLVED SOLIDS 2c2A7 SUSPENDED SOT7T- CONDUCTIVITY Soso I3 %£�,T M zwv , TO 7-,'A 7 ANALYSIS sago o s 2z S 212 : TRTXWW - 2:Z3 SAMPLED- Gels RECEIVED BY- of . ?VP7 s PLE- G«a2 2z32E2 Sx123 EPA leG.l 07/15Z09 ease 3N 2,890 Z1 EPA 160.2 07/20/09 0810 DJ 5e � /L EPA 12e_1 07Z11sZ:9 1110 CT4,340 um Zce EPP, 375.2 old 5/09 1152 CT 73_7 ZS EPA 200-7. e;Zy Zog 0847 C G.;93 :,-,g /L LABORATORY DTRECTO u 11 PA R LABORATORIES. WC. I www. parlabs. com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert = 20: SC Cert r 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138- PROJECT NAME: jUL 09 DATE. 07/21/09 SAMPLE NUMBER- 91297 SAMPLE ID- ALCLEM MW-3 DATE SAMPLED- 07/10/09 DATE RECEIVED- 07/13/09 SAMPLER- T TIME RECEIVED- 1230 DELIVERED BY- TT Page 3 of 8 ANALYSIS TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL SAMPLE l,_ATRIX-- iAw TIME SAMPLED- 0830 RECEIVED BY- DO TYPE SAMPLE- Grab ANALYSIS METHOD DATE TIME BY RESULT JNI-_ SPA 160.1 07/15/09 0850 BN 1,728 `,g/L EPA, 160.2 07/20/09 0810 DJ !65 mg/L EPA 120.1 07/15/09 1110 CT 2,600 um/= EPA_ 375. 2 07/15/09 1152 CT 1 , 1 92 :gig/L -EPA 200.7. 07/21/09 0847 CT 106 mg/L LABORATORY DIRECTOR 13 Ll L soRATORIES.INC. www.parlabs.com PAR Laboratories, inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 70A-588-8335 NC Certr 20: SC Cert a 99003 REPORT OF ANALYSES A tr. TRENT--DiNE-L AICHEi✓ 7 NC 8135 RED ROAD ROCKWELL, NC 28138- SAMPLE NUMBER- 91298 SANPLL ID- A.L.C"r_EM _NiW DATE SAMPLED- 07/10/09 DATE RECEIVED- 07/13/09 SAMPLER- TT TINE RECEIVED- 1230 DELIVERED 3Y- TT Page = o" 8 ANALYSIS TOTAL DTSSOLJED SOLIDS TOTAL. SUSPENDED SOT IDS CONDUCTIVITY SULFATE ALUMINUM, .TOTAT - PhOvECT NAy- L: JU- 09 DATE: 07/21/09 ANALYSIS METHOD DATE I M7 BY S -YMPLE VATRTX- WW TIME SAM='LED- 081_ 5 . RECEIVED BY- D17 TYPE SAIMPLE- Grab EPA 160.1 07/15/09 0850 BN 5,220 :gig/L EPA 160.2 07/20/09 0810 DJ 15' mg/L EPA 120.1 C7/15/09 1110 CT 7,840 m/c7, �PA _ 375.2 07/15/09 1152 CT 8,389 :,g/L EPA 200.7. 07/21/09 081_7 CT LABORATORY DIRECTOR s PAR LABORATORIES INC. www.parlabs.com RARLobOr fodeslnc. 2217 Graham Ro& Drive PO Box d1483 Choeo. ,N C 28241-1483 Rhone ? $ms8 3;Fc< 704 @8 y, , G;# s G!#m,so REPORT OF ANAT.VSss A:tn: TRENT 2: ELL 7N- 8135 RED ROAD SKI LL, yc 2e133- PR OJsc N. E: zoa e9 DATE: 07Z21Ze5 SAMPLE - §1299 SAMPLE 7D- TE s G - 07/10/09 DATE &Ec Iv S- :7Z131/:e s a2 R- TT 222E RECEIVED- 123c OZ2I 2 BY- TT ?age 5 Of a ANALYSTS TOTAL D! SSOT VED SOLIDS TOTALSUSPENDED sos:es NDOC2:7I27 SUT FA T s ALUMINUM, TOTAL ARC 2SI5 Ise D.A 2E _TM SAM, 22y MAT R i X - W-W TTV,7 SAMPLED- 0900 zecE:v - DQ 2y23 s � 21£- Grab asset? 23:23 EPA l6:.1 e2ZlsZe9 0850 140 mgZi EPA 160.2 e7'20/09 Gale S1 5 mgZi EPA 120.1 e2Z15Ze9 1110 C l,i;o Zzz EPA 375.2 07d 5Z25 11152 CT 27.5 mg/1 Elk 200.7. 07Z21/09 0841 e.<2: Z2 2A307,,ATCRY DTREc OR BY J E PAR LABORATORIES, Na www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cart = 20: SC Cart " 99003 REPORT OF ANALYSES Alto: TRENT TIDWELL ALCHEM INC 8135 RED ROAD ROCXWELL, NC. 28138- PROJECT NAME: jUL 09 DATE: 07/21 /09 SAN_ L= NUMBER- 91 300 SAMPLE ID- ALCHEM MW-5 DATE SAMPLED- 07/10/09 DATE RECEIVED- 07 / 1 3 i 09 SAMPLER- TT TIME RECEIVED- 1230 DELIVERED BY- TT Page 6 of 8 ANALYSIS TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL ANALYSIS METHOD DATE - IME BY SAMPLE MATRIX- Ww TIMr', SAMPLED- 0915 RECEIVED BY- Di TYPE SAMPLE- Grab RESULT UNITS EPA 160.1 07/15/09 0850 BN 2,520 mg/L EPA 160.2 07/20/09 0810 Di 23 mg/L EPA 120.1 07/15/09 1110 CT 3,930 um/cm EPA 375.2 07/15/09 i152 CT 2,555 :m/L EPA 200.7. 07/21/09 0847 CT 252 m.;%- LABORAT'ORJ DIRECTOR n LABORATORIES, INC. PAR www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert = 20: SC Cent '. 99000 REPORT 0!= ANALYSES Attn: TRENT T-DWELL ALCHEM INC 8135 RED ROAD ROCKWE, T NC 7.81 38- PROUECT NAME : L 0 ° DATE: 07i 21 /09 SAMPLE NUMBER— 91301 SAMPLE ID- ALCHEM Mrn'-7 DATE SAMPLED- 07/10/09 DATE RECEIVED- 07/13/09 SAMPLER- TT TIME RECEIVED- 1230 DELIVERED BY- T'T Page / of 8 ANALYSIS TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE ALUMINUM, TOTAL ANALYSIS METRO!; DATE TIME BY SAMPLE MATRIX- W'W' TIME SAMPLED- 0930 RECEIVED BY_ Di 7YPE SAMPLE- Grab RE SJi,7 Nr7.0 EPA 160.1 07/15/09 0850 BN 2,A90 ,,,,g/L EPA 160.2 07/20/09 0810 DJ; 17 :r:g/L EPA. 120_1 07/15/09 1110 CT 3,730 um/cm EPA 375. 2 07/1 5/ 09 1152 CT < 10 EPA 200.7. 07/121/09 084_7 CT 0.564_ Mg/7 LABORATORY DIRECTOR 0 r I PAR casoaaTOWS,W www. parlabs. com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert r 20: SC Cart n 99003 REPORT OF ANALYSES Attn: TRENT TIDWELL. ALCBEM INC 8135 RED ROAD .ROCKWELL, NC 28138- PROJECT NAME: JUL 09 DATE: 07/21/09 SAMPLE NUMBER- 91302 SAMPLE ID- A.LCrEM MW-S DATE SAMPLED- 07/10/09 DATE RECEIVED- 07/13/09 SAMPLER- ^_T ED- 1230 DELIVERED TIME RECEIVED- -' BY- - TT ?age 8 of 8 ANALYSIS TOTAL DISSOLVED SOLIDS TOTAL SUSPENDED SOLIDS CONDUCTIVITY SULFATE: ALUMINUM, TOTAL L ANALYSIS METHOD DATE TIME BY SAMPLE MATRIX- WW TIME SAMPLED- 0945 RECEIVED 3Y- D:, ' TAPE SAMPLE- Gran EPA 160.1 07/15/09 0850 BN 2,410 . g; EPA 40.2 07/20/09 0810 Di 59 mg/L EPA 120_1 07/i5/09 1110 CT 3,620 'um/cm EPA 375.2 07/15/09 1152 CT 99.2 mg/L EPA 200.7- 07/21/09 0847 CT p _90 mg/L LABORATORY DIRECTOR r. u u Lagoon Records Application Activities LAGOON RECORDS A L C H E M I N C DATE LAGOON I Q o� LAGOON II p S LAGOON III a — --- ---- - --- ---- NON -ACTIVE ACTIVE -------- --- NON -ACTIVE ACTIVE NON -ACTIVE ACTIVE FREEBOARD ) 6 FEET FREEBOARD_ FEET FREEBOARD �FEET APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS TO FILL_ FREEBOARD LEVEL 5ZS O _ APPROXIMATE CUBIC YDS TO FILL_ FREEBOARD LEVEL O APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVELtj OQ _ 175 X 110 X12 LAGOON SIZE FORMULA = L X W X 11 /27 120 X 135 X10 LAGOON SIZE FORMULA = L X W X H 127 175 X 175 X12 LAGOON SIZE FORMULA = L X W X H /27 **NOTE: ALL LAGOONS MUST MAINTAIN A 2 FOOT FREEBOARD** LAGOON RECORDS ALCHEM INC DATE Nov LAGOON 1 � LAGOON II LAGOON III U NON -ACTIVE ACTIVE NON -ACTIVE ACTIVE NON -ACTIVE ACTIVE FREEBOARD FEET FREEBOARD 3 FEET FREEBOARD FEET APPROXIMATE CUBIC YDS J APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS c) APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL J7On APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL ® APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL dl 006 175 X 110 X12 LAGOON SIZE FORMULA = L X W X H /27 120 X 135 X10 LAGOON SIZE FORMULA = L X W X H /27 175 X 175 X12 LAGOON SIZE FORMULA = L X W X H /27 *'"NOTE: ALL LAGOONS MUST MAINTAIN A 2 FOOT FREEBOARD" LAGOON RECORDS ALC H E M I N C DATE LAGOON I (1) �1 ,y S LAGOON II p1l L, �� LAGOON III NON -ACTIVE ACTIVE NON -ACTIVE ACTIVE NON -ACTIVE ACTIVE FREEBOARD �— FEET FREEBOARD 3 FEET FREEBOARD FEET APPROXIMATE CUBIC YDS -C APPROXIMATE CUBIC YDS LID, G APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL e° APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL Cs APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVELI 6- C) 175 X 110 X12 LAGOON SIZE FORMULA= LXWXH/27 120 X 135 X10 LAGOON SIZE FORMULA= LXWXH/27 175 X 175 X12 LAGOON SIZE FORMULA= LXWXH/27 "NOTE: ALL LAGOONS MUST MAINTAIN A 2 FOOT FREEBOARD" LAGOON RECORDS ALCHEM INC DATE C� LAGOON I Q a �,� LAGOON II LAGOON III NON -ACTIVE ACTIVE A:�: NON -ACTIVE ACTIVE NON -ACTIVE ACTIVE FREEBOARD 1 FEET FREEBOARD FEET FREEBOARD I:� FEET APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS APPROXIMATE CUBIC YDS TO FILL FREEBOARDLEVEL�jL APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL •i APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL �•: 175 X 110 X12 LAGOON SIZE FORMULA = L X W X H /27 120 X 135 X10 LAGOON SIZE FORMULA = L X W X H /27 175 X 175 X12 LAGOON SIZE FORMULA = L X W X H /27 **NOTE: ALL LAGOONS MUST MAINTAIN A 2 FOOT FREEBOARD** % - d� I � LAGOON RECORDS ALC H E M� I N C DATE LAGOON 1 (, ,3 LAGOON II g LAGOON III NON -ACTIVE ACTIVE NON -ACTIVE t ACTIVE NON -ACTIVE' ACTIVE FREEBOARD "�-� FEET FREEBOARD :3 FEET FREEBOARD la FEET APPROXIMATE CUBIC YDS �Soc) APPROXIMATE CUBIC YDS o� APPROXIMATE CUBIC YDS C) APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL S ®p APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL ® APPROXIMATE CUBIC YDS TO FILL FREEBOARD LEVEL f f, OUCH 175 X 110 X12 LAGOON SIZE FORMULA = L X W X H /27 120 X 135 X10 LAGOON SIZE FORMULA = L X W X H /27 175 X 175 X12 LAGOON SIZE FORMULA = L X W X H /27 "NOTE: ALL LAGOONS MUST MAINTAIN A 2 FOOT FREEBOARD" E. MG DcNR MR. DWQ -r� +sifer Protects`cirt. RESPONSE TO, NO-V-2008-SC-0134, MARCH 26, 2008 ATT: ELLEN HOFFMAN ALCHEM, INC 8135 RED ROAD ROCKWELL, NC 28138 March 24, 2008 RE: NOV-2008-SC-0134 Dear Ms. Hoffman, This letter is in response to your NOV dated February 21, 2008, that was based upon your inspection on January 29, 2008. Following please find my opinion and evaluation of Alchems` current situation in regards to the Settlement Agreement dated November 27, 2007 and the steps Alchem, Inc has taken to rectify some of the issues. Attached you will also find photos of the progress that has been made, receipts for expenditures, man hours, etc. Alchem's Environmental Progress Report PERMIT #WQ0002702 LAGOONS Lagoon #1: Since your last inspection, Alchem has been able to empty 70% of this lagoon, 50% of this is down to the GEO lined floor of the cell. (Please see supporting photos) Lagoon #2: Alchem has been able to create an 8 — 10 foot Freeboard around this lagoon, to achieve this we have stacked a pile of the material in the center of the lagoon for drying purposes to enable us to haul it off site. This appears to be the only way to achieve both of our goals i.e. empty the lagoon and be able to have an inspection done by a licensed NC PE. Lagoon #3: We have created some Freeboard around #3 but this lagoon will continue to receive Bauxite Residuals until we achieve emptying Lagoons 1 & 2, at that point we will be able to begin the neutralizing and wash process. At this point we will be able to attack this lagoon with the same aggressiveness we used on Lagoons 1 & 2. RECYCLE & WASH SYSTEM At this time I believe it is counter productive to neutralize and wash the Bauxite Residual without having an uncontaminated area to place the clean material. Once we achieve completely emptying Lagoon #1 we will then immediately start the neutralizing process. Our neutralization process will be accomplished by mixing the Bauxite Residuals and 10% Soda Ash Solution into the Alum Reactor (cleaned out of course), we have done several micro tests and have calculated the right formula to achieve a PH of 6.0 — 7.0 su on a continuing basis. Alchem has purchased approx. 10,000 gallons of 10% Soda Ash Solution and approx. 45 tons of Soda Ash Powder to produce its own solution once all is achieved as stated above. PH READINGS & MATERIAL REMOVAL— Alchem will continue to take PH readings, document tonnage removed from the site and where the material was transported to, just as you received during your last inspection, if this is acceptable. F rd, p WASTE LEVEL GUAGES The installation of the waste level gauges will begin as soon as each lagoon is cleaned, repaired and inspected by a licensed NC PE. VEGETATIVE COVER Alchem is in the process of removing all pine saplings and bushes from all earthen embankments, when this is achieved, we will use rolls of erosion control blankets, seed and fertilizer to stabilize Lagoon embankments from any further erosion. The projected completion date of this step, weather permitting, is no later then April 21, 2008. SUMMARY OF LAGOONS It is my opinion and assessment that from an Environmental & Business standpoint it would be counter productive to put good neutralized material with a PH of 6.0 — 7.Osu on top of a material with a PH of 3.0 — 4.Osu. I believe we share the same goals on this issue. Before Alchem begins neutralizing its residuals, which would not only help us environmentally, but also from a business stand point, giving us a clean recycled sellable product, instead of a large expense and burden. PERMIT #WQ0016338 STORMWATER BASIN At the time of your inspection storm water was ponded beyond the reinforced Hydraulic Engineered Bermed area. We have since pumped the water into tanks for use in product manufacturing. Though water still exists in our storm water pond, it is not beyond the reinforced area. As summer approaches it is my plan to finish the retention pond so that this overspill no longer happens. It is my plan that using the water in the manufacturing of product and the summer heat assisting in evaporating the excess water, that we should be able to control this area with some elevation changes and a more efficient pumping system. However please keep in mind that even after this work is completed, I can not honestly say this will NEVER HAPPEN again, due to the fact that we can not control the Forces of Nature or Acts of God. SEEPAGE You have stated in your NOV the reinforced area of our Berm has seepage, this is not true. I did see what looked to be seepage which was approx 200' beyond the engineered bermed area. Our reinforced area extends 230 linear feet north of the catch basin, your photo and the delineated line you used to show the reinforced berm was over 200' too long. The seepage from the un-reinforced area will be repaired by lowering the water levels to the reinforced area only and regrading the berm in that area. I believe we can accomplish this work no later than April 30, 2008, again weather permitting. RAIN RECORD As you explained to me during your last inspection, the DWQ uses rain gauges around the area to determine rainfall amounts and that you have used this method to determine how much storm water should be in our bermed area. Respectfully, it is my contention to get an accurate reading of the ponded water in our retention pond, you would have to use area rainfall records and calculate the total square footage of the area and also take into consideration the topography of the area to retrieve a true and accurate measurement of rainfall for this area. As I am not a PE, it would only seem logical to me to use the whole runoff surface area and not a straight downpour of rain just in the pond itself. I know we have discussed this issue on several different occasions and in no way am I trying to make this a point of argument. If I am wrong in my theory of calculating storm water runoff, I would please ask you to advise me as to what the correct calculation method is and what should be in our pond after a rainfall of/", 1 ", 2", etc atone time. FINAL SUMMARY As I am very aware of the Settlement Agreement dated November 27, 2007 and all that it entails, I can only tell you that Alchem will rectify all of the points/issues as requested in the above mentioned agreement at some point. I cannot honestly say that we will have 100% of all the issues completed by June 1, 2008; 1 say this due to the fact that I have only held my current position with FULL operational . control since December 21, 2007. As you are all aware, November 2007 when we met for the first time, Alchems' prior management was still on staff, which hampered my authority and complete control at that time. I am in no way making excuses for the delay in achieving the Settlement Agreement issues, but the truth of the matter is that prior management did have approx 1 '/ years to begin or complete all of the issues in a timely manner and instead CHOSE to "SWEEP IT UNDER THE CARPET". With all of this being said, I truly hope that you and your colleagues have seen a major difference 'in ALCHEM as a company. I feel that in a very short period of time we have made great strides in cleaning up the image and reputation of Alchem, Inc. I do however realize that Alchem still has a long way to go to achieve all of the neglected Environmental issues and all the other mismanaged business issues as a whole.-- i It is at this time that I would humbly request that NCDENR & Alchem, Inc irebuild our relationship based upon TRUST, an open line of honest communication and the visual/documented-progress- that -has _ been accomplished in a short though very expensive timeframe (please see attached expense documentation i.e. man hours, equipment rentals, before & after photos, etc). In closing I would like to request that NCDENR reconsider your decision to impose a civil penalty at this time due to all the visible work and documented expenses, I truly believe this would only add to the extreme financial burden that years of neglect, lack of management and complete disregard have already caused. At this time 100% of all revenues being generated by Alchem, Inc are being streamlined into labor, equipment rental, fuel and other additional expenses needed to come into compliance and survive as a company. Thank you for your time, attention and understanding during the complete restructuring of Alchem, Inc. Sincerely, ROBERT A. WOLCOTT CHIEF OPERATIONS OFFICER ALCHEM, INC 8135 RED RD ROCKWELL, NC 28138 OFFICE — 704-279-7908 FAX — 704-279-8418 PERSONAL CELL — 704-245-9689 (AFTER 6pnn) Enclosures: Photographs before & after to show progress Expenditures i.e. equipment, manpower, etc cc: Randall Andrews 3 SUPPORTING EXPENDITURE DOCUMENTS DIRECTLY RELATED TO CLEAN-UP EFFORTS EQUIPMENT RENTALS - $299162.02 FUEL — $259564.63 STONE - $159162.02 CONCRETE- $ 19920.76 DELTA ENGINEERING - $259140.72 ROUZER' S (HYDRAULIC/MOTOR OIL) - $19454.31 MAN HOURS- 12,851.11 = $192,758.58 (man hours calculated based on average of $14/hr rt & $21.00/hr ot) MISC - $19266.45 TOTAL $ 292942.9.49 Y' J� HEAVY -EC i l= RENT A SALES, Rented Machines to Alchem 2007 Rentals Ingersoll Rand SD70D 178867 12/6-12-28 $2500 a month 2008 Rentals CAT 322BL 1YS1470 1/14-1/23 $7500amonth Ingersoll Rand SD70D 178887 1/8 —1/11 $967 a weer X CAT 725 BIL0155 2127 $7500amonth Volvo EC290 V 13625 3/4 $7500 a month Komatsu PC30OLC-7 A86280 3/25 $7000 a month Volvo A25D 'V'13037 3/25 $7000 a month 6941 NC Highway 8 • Lexington, North Carolina 27292.336-367.5005 • Fax 336-357-7650 www.mayequip.com 10 Mdd 1N3WdInM AAV3H AVW T98EL9E9EE TT:9T 800Z/LZ/E0 Current 1-30 Days PE31ys Past 61-90 DueeDue 8,467.00 0.000 0.00 ME U El Over. 90. Days Past Due 77 Amount.Due 0.001. $8,467.00 ` H_EAVY-EQUIP RENTAL & SALES ®' P.O. Box 600090 Raleigh, North Carolina 27675-6090 Phone:336-357-5005 Fax:336-357-7650 Bill To: Alchem, Inc. 8135 Red Road Rockwell, NC 28138 , P.O. # Quant... Item Code 1 322 BL Invoice Date Invoice # 1 /14/2008 16642 Ship To: Rowan Co. 8135 Red Road Terms Due Date Sales.Rep Ship Via Rental Period Net 30 2/13/2008J-7 WT 1/14/2008 Common Carrier 01/14/08-02/10/08 Description Rental Rate Amount CAT Excavator (SN#1YS01470) # 2053 7,500.00 7,500.00T One Month Rental No Charge Freight North Carolina Sales Tax Exempt 0.0096 .0.00 Invoices not paid within terms are subject to finance charges of per month (annual rate of 18%). /44 Total $7,500.00 Payments/Credits $0.00 Balance Due $7,500.00 HEAVY -EQUIP RENTAL&SALES invoice. P.O. Box 600090, Raleigh, North Carolina 27675-6090 Phone:336-357-5005 Fax:336-357-7650 Date Invoice # F1/9/2008 16615 Bill To: Ship To: Alchem, Inc. r -Rowan County 8135 Red Road Rockwell, NC Rockwell, NC 28138 P.O. # Terms Due Date Sales Rep Ship Via Rental Period Net 30 2/8/2008 WT 1/8/2008 Common Carrier 01/08/08-02/04/08 Quant... Item Code Description Rental Rate'. Amount 1 SD 70 D Pro Pao Smooth Drum Roller ( SN#178887) # 895 2,600.00 21600.00T One Month Rental Delivery Charge Delivery Charge 50.00 50.0OT 1 Pick -Up Charge Pick -Up Charge 50.00 50.00T North Carolina Sales Tax Exempt 0.00% 0.06 J?o (4)D I co?' Invoices not paid within terms are subject to finance charges of 1.5% Total per month (annual rate of 18%). $2,700.00 Payments/Credits $0.00 Balance Due $2,700.00: HEAVY -EQUIP RENTAL & SALES P.O. Box 600090 Raleigh, North Carolina 27675-6090 Phone:336-357-5005 Fax:336-357-7650 Bill To: Alchem, Inc. 8135 Red Road Rockwell, NC 28138 Invoice Date Invoice # 3/4/2008 16908 Ship To: Rowan County . P.O. # Terms Due Date Sales Rep Ship Via Rental Period Net 30 4/3/2008 WT 3/4/2008 Common Carrier 03/04108-03/31/08 Quant... Item Code Description Rental Rate Amount 1 EC290 Volvo Longreach (SN#V13625) # 2103 7,500.00 7,500.00 One Month Rental 3 G�dkoiT �, s lrlol' Invoices not paid within terms are subject to finance charges of 1.5% Total per month (annual rate of 18%). $7,500.00 Payments/Credits $0.00 Balance Due $7,500.00 FIEAW EQUIP R '.. r RENTAL & SALES P.O. Box 600090 Raleigh, North Carolina 27675-6090 Phone:336-357-5005 Fax:336-357-7650 Bill To: Alchem, Inc. ' 8135 Red Road Rockwell, NC 28138 Invoice Date Invoice # 3/4/2008 1 16907 Ship To: -Rowan County P.O. # Terms Due Date Sales Rep Ship Via Rental Period Net 30 4/3/2008 WT 2/27/2008 Common Carrier 02/27/08-03/25/08 Quant... Item Code Description Rental Rate Amount 1 725 Cat Truck (SN#61 L00155) #7031-2 7,500.00 7,500.00 One Month Rental G.4- r SILL TO: ALCHEM, INC 8135 RED ROAD ROCKWELL NC 28138 SHIP TO: ALCHEM, INC 8135 RED ROAD ROCKWELL NC 28138 INVOICE INVOICE #: 23937 INVOICE -DATE: 01/02/2008 CONTRACT #: 15744 CUSTOMER: 2052 TEL:.70.4-279-.7.908 TERMS: ON RECEIPT PAGE: 1 JH THANK YOU FOR USING M&M EQUIPMENT -RENTAL; NE APPRECIATE YOUR BUSINESS!. --------------------------=-------- - =--= ------ _ PRODUCT fI.DESCRIPTION ---------'--------- DATE/TIME OUT BILLED THRU. STATUS 2102-10 BOBCAT 5175 WED DEC 05/2007 9:OOAM WEO JAN 0212008 9:OOAM.' RTD: TER OUT/IN: 251.6/257.6 METER USED: 0 INCLUDED: 0 OT:: RENTAL PERIOD: 4 WEEK(S) DAMAGE WAIVER TOT RENTALS: 1215.00 TOT SALES: 00 TOT SERVICES: 145.80 L Pil�1 7Y/V0" �y %� _-��... OTY UNIT PRICE AMOUNT 1 1215.00.. 1215.00 0 - 1.45.80 SUBTOTAL: 1360.80 STATE TAX 91.85 TOTAL: 1452.65 BALANCE DUE: 1452.65 / a� M & M EQUIPMENT. RENTAL j 8545 HIGHWAY 52 1 ROCKWELL, NC 28138. (704) 279-2558 i' ALCHEM, INC 8135 RED ROAD ROCKWELL.NC 28138 TO: ALCHEM, INC 8135 RED ROAD ROCKWELL NC 28138 INVOICE INVOICE #: 23959. INVOICE DATE: "01/07/2008 CONTRACT #: 15800 CUSTOMER: 2052 TEL: 704-279-7908 TERMS: ON RECEIPT PAGE: 1 JH IANK YOU FOR USING M&M EQUIPMENT RENTAL APPRECIATE -------------------------------------------------------------------------------------------------------------------------------- YOUR BUSINESS! PRODUCT 11 DESCRIPTION --------- ----------- DATE/TIME OUT ------------- BILLED THRU STATUS ----------- pTY UNIT PRICE AMOUNT "'"" 10 BOBCAT S175 WED JAN 0212008 ------ 9:OOAM MON JAN 0712008 9:OOAM. RTD: ------------- 1 450.00 ------ 450.00 R OUT/IN: 257-6/350.4 METER USED: 92.8 INCLUDED: 0 OT: 92.80 RENTAL PERIOD: 5 DAY(S) DAMAGE WAIVER 54.00 TOT RENTALS: 450.00 TOT SALES: .00 TOT SERVICES: 54.00 SUBTOTAL: 504.00 STATE TAX 34.02 TOTAL: 538.02 BALANCE DUE: 538.02 LOCATION #004 Page: 1 United' SALXSBURYSVNCLE2814 4 WEEK BILLING INVOICE MLN Rentals 704-6-80 to � 704-642 -1046 FAX ALCHEM INC 8135 RED ROAD ROCKWELL, NC 28138 C#: 704-279-7908 J#: 704-279-7908 4.1.987 1 MB 0.360 33055S11.p04 1 of 1 500 000987 a t �11�1��Il�llll��ll��l�ll�l�ll�lt�I�II�II1�111�11��11�1�11�1�1� �� ALCHEM INC s= S135 RED ROAD enm!em ROCKWELL NC 28138-8557 Customer.:.. 901405 Invoice.#... 714.99259-001 Invoice,date 2/22/08 Date:out..... 2/05/08 5:00 PM Billed thru. 3/04/08 Job Loc..... 8135 RED ROAD, ROCKWELL Job No...... 1 -.ALCHEM INC P.O. #.... Ordered By., JASON Written by.. CYCLE BILL Salesperson. 2113 Terms........ Net 30 Days PLEASE REMIT PAYMENT TO: UNITED RENTALS (NORTH AMERICA), INC. PO BOX 100711 ATLANTA, GA 30384-0711 Qty Equipment # MinDay Week 4 Week Amount 1 MINI EXCAVATOR 6000-6799# * 185:00 185.00 _ 550.00 1400.00 1400.00 1008927 Make: TAKEUCHI Model; TB125 Ser #: 12518133 HR OUT: 106.50 HR IN:" TOTAL: 106.50 W thumb 18" bucket SALES ITEMS: Qty Item number Stock class Unit Price Amount 1 ENV MCI EA 6.720 6.72 ENVIRONMENTAL CHARGE UM: (EA) EACH DELIVERY CHARGE 50.00 PICKUP CHARGE 50.00 Sub -total:- 1506.72 Rental protection:. 196.00 Tax: 101.72 BILLED FOR FOUR'WEEKS 2/05/08 THRU 3/04/08 05:00 PM Total: 1804.44 RENTAL PROTECTION ACCEPTED FOR YOUR CONVENIENCE, UNITED RENTALS IS NOW OFFERING A TOLL -FREE NUMBER TO CALL EQUIPMENT OFF RENT PLEASE CALL 800-UR-RENTS (800-877-3687) CUSTOMER CARE REPRESENTATIVES ARE AVAILABLE 24/7 TO SUPPLY YOU WITH A TERMINATION NUMBER IN ORDER TO CLOSE THIS CONTRACT. A CLEANING CHARGE WILL APPLY,TO ALL EQUIPMENT RETURNED WITH EXCESSIVE DIRT, CONCRETE, AND/OR PAINT'. CUSTOMER IS RESPONSIBLE FOR ALL DAMAGES INCLUDING TIRES. OEM THERE WILL BE AN ADDITIONAL CHARGE FOR MISSING KEYS AND A REFUELING CHARGE WILL BE APPLIED TO ALL EQUIPMENT NOT RETURNED FULL OF'FUEL. %t,) T�u not clue uv*1 ENVIRONMENTAL CHARGE: The items indicated above are subject to an environmental charge which Is designed to recover the company's direct and indirect expenses for the handling, managing and ,,sr of waste products, hazardous materials, and related administrative costs. This is not a government mandated charge. FUEL: Fuel charges do not include federal, state or local fuel excise taxes. OPTIONAL RENTAL PROTECTION PLAN: THE RENTAL PROTECTION PLAN IS NOT INSURANCE! Upon accepting the 0pptionel Rental Protection Plan, the Customer agrees to pay a charge equal to 1-4!,- of the rental charges on Equipment Customer wants covered by the Rental Protection Plan. In return, as set out on Ih6 back page, United agrees to waive to theft listed under The Rental Protection Plan provisions (n the -Terms and certain claims for accidental damage to such covered Equipment occuring during normal and careful use. Customer remains liable for all damages and loss due Cond tions on back page, including Customers negligence. Customer ACCe is Customer Declines EAD BEFORE SIGNINGUnited hereby leases to Customer the Equipment (as dented In the Terms and Conditions on the reverse side) and Customer hereby acapis, all TERMS AND CONDITIONS listed tn�s rental agreement, including the Terms and Conditions set forth on the reverse side, which the undersigned has read and understands. REMINDERS: (1) Rates do not Include fuel or delivery; (2) :bona) Rental Protection Plan charge is IAYl Qf the total rental charge for covered equlSmant; (3) Customer pays for all time the Equipment Is out, Including Saturdays, Sundays and Holiday(g) This oe 9 ocnerlcosts, including late charges.rsedes sit her Details ot purchase above as worders or e I as other obs and i In gglioa os andeespo responsibilities areof Custmcontal es ed in the In nts oTERMS ANDr forms; D CONDITIONS ON REVERSE. THE Customer assumes all risk and Is NDIVIDUAL SIGNINIs for all G BELOW AS OR ON BEHALF OF CUSTOMER: (1) AGREES TO ALL OF THE TERMS AND CONDITIONS ON THE REVERSE SIDE OF THIS RENTAL AGREEMENT, (2) ACKNOWLEDGES RECEIPT OF THE EQUIPMENT IN GOOD WORKING ORDER AND, (3) IS FULLY FAMILIAR WITH ITS OPERATION AND USE. X STOMER SIGNATURE DATE A LARGER FONT COPY OF THE TERMS AND CONDITIONS IS AVAILABLE UPON REQUEST. DATE U SALC o MAN E ;gip 1' 3, R c. r r• 1 ROUZER MOTOR PARTS. WIX `FILTERS CO. INC. 330 NORTH DEPOT ST. SALISBURY, N.C. 28144 PHONE 1-800-230-1569 OFFICE &PARTS DEPT. LOCAL 704-636-1041 MACHINE SHOP SERVICE ALL GOODS RETURNED MUST BE ACCOMPANIED BY•THIS INVOICE Conoco User: P 'Y'PC : i VL., Cust: 2750 (:r CHARGE INVOICE:335514 BUY (1) I HYD FLUID I 1 547. 50 1435. 00 43c. 0 0 f X (1) 76—UNAX—AW-1(0 A/R chla.r•Q 464.37 .. ...... . 4,,,,, `... 3 x N A 1. ,ti ._) • v V f— 1 435( r(:r GH:i ,.zss;LABOR tl­,,j 47.. 5.0 ..,". - A 35.00 2 7.37 TOTAL UNfS' ,TOATAXAB „TA%ABL=s RECEIVED BY: " x . 4/14.'7 _ ALL GOODS RETURNED MUST BE ACCOMPANIED BY THIS INVOICE - � Conoco WIX`FILTERS CO. INC. 'm 330 NORTH DEPOT ST. . 9 SALISBURY, N.C. 28144 OFFICE &PARTS DEPT. PHONE 1-800-230-1569 LOCAL 704-636-1041 MACHINE SHOP SERVICE ALL GOODS RETURNED MUST BE ACCOMPANIED BY THIS INVOICE i `'US er h z� U r m `k 'fi%A "� r^rA TI1 °'"dt. a' '*�' .�.."'atis m'�;.sunr s a,.+Ya:"+.F,. r AL+. HEIi , INI: - _� �Cu t: �. TvP �:.IVv ' OR AiUtiALL ANDREWS� " ` A �� 750 �`H I NVO , w t RGf MEo.133:, 1 E a RoCKWEL RD,t -• .� �70$ 427:� Q DESCRIPTION r, 8=23ANi 1 CON. 5 5GFLEET 1540 (1) ; b22.00 465.87 465.87 (1) GUARDOL OIL 5W40 � !' E.I L 0508 CLEANER 6..55 3.59. 21.54- �' BLA 1�—P8 (1) 6 07 3. 8/� (1) BLASTER PENS RANT 23.16 X SO H1310P (V53L 4w E r"1„ 1 . °> a a41� 0(7 , , (1) 10W HYU FLUID i $,A 17 6�0:34 t j A/R ch,are 6.09.45 15 570.91 795 72 . LABGR, *' ..... �,�, r GG" ` ` 570. g 1 -38. 54 . L r,,,. �T:13P ALL,., a NON%TA7(ABLE REC E _ Y: -a oFA)(ABLE x ., ® 609.4 ALL RETURNED UST B CCOMP.ANIED BY THIS INVOICE ""'Phone 704-633-0952;-'- .614: f ast Inure St: : Saris iary;11T 28 46 . _�/ So ld =To r F � j Address , :..city f •Customer No • T1ii5-PRODUCT lS�D'E®IESEC.' k a WONTP"- �#BL .- SE 3NL1G M Fr- ALTY.fOR -ly"/R'BLE USE =yx 1 ❑. co v r -ram.='•gy,f�s�t } -FUEL ❑ OIL DIESEL El -FUEL I 'SALES TAX im OTA xD17l x C-.CUSTOMERSIG ATURE - - •-DRIV SIFFORD'S.OIL CO. 6130 HWY. 152 EAST ROCKWELL, N. C. 28138 STEVE SIFFORD PHONE". 704-279-2125 INVOICE DATE 4i i NO. 4 10594 !j NAME ADDRESS I CITY * ❑ FU OIL ❑ KEROSENE * QUIPMENT FUEL ❑ DIESEL j * ❑ FARM FUEL ❑ GASOLINE * DYED DIESEL FUEL NONTAXABLE USE ONLY PENALTY FOR TAXABLE USE AMOUNT - AMOUNT 1 PAID TOTAL RECE+VED BY: DUE Gals. Reading - Start — — — - - - .0 i Gals. Reading - Finish — — — j Sales Sequence Number — - - '-• : -- 7 Price per Gallon - cents — .•_ ._ M ca,I Product Cost - Tax .._ ', r F , w t_' Total Price _ `i ' '. '3�, 4 SIFFORD'S OIL CO. :SIFFORD'S -- 6130 HWY. 152 EAST - ®IL CO.:. w. ROCKWELL, N. C. 28138 6130 �HWY 152 ,EAST': STEVE SIFFORD ' ,ROCKWELL, N C:' 28138 PHONE: 704-279-2125 STEVE:=SIFFORD 'PHONE: 704-279-2125 INVOICE Q ' DATE �12 NO. —� O 9 s r INVOICE l DATE _ �NO. -� .L 0 9. 4 NAME 1Z _ NAME n ADDRESS ADDRESS CITY . CITY PRODUCT CODE s * ❑ FUEL OIL KEROSENE PRODUCT CODE ❑ * O FUEL OIL Aka' FUEL ❑ -KEROSENE ❑ DIESEL` ❑ EQUIPMENT FUEL, * ❑ FARM FUEL ❑DIESEL ❑ GASOLINE ,k ❑ FARM -D DIESEL FUEL FUEL - GASOLINE I ITAXABLE USE ONLY * DYED DIESEL FUEL : { ­ALTY FOR TAXABLE USE NONTAXABLE USE.ONLY PENALTY FOR TAXABLE USE AMOUNT LJ. t AMOUNT AMOUNT �uV ll LSll11 r_ PAID 'AMOUNT ;- • CEIVED B TOTAL PAID DUE TOTAL RECEIVED BY: DUE C1 l- r, _ _ Gals. Reading --'Start - r _ f Gals. Reading -Finish _ :_ �, 0 Gals. Reading -Start Sales Sequence Number _ _ _ _ — Gals.• Reading - Finish Price per Gallon - cents = — — — �- Sales Sequence Number — — — — Product Cost — — �� r L 4 Price per Gallon - cents . ~ _ — -- 2 0 Tax i rProduct Cost : 2 y 5 h; 9 9, -Tax Total Price - �' �= -T _ 3 oa. - T t I Price R,� a :vim s�"5;�'��'�`'�.-.mac -�',• ..�;"k`„y' yy �;; .. 1 r._... ' SIFF®R®'S ®IL CO.. 6130 HWY, 152 EAST ROCKWELL, N. C. 28138 STEVE SIFFORD r .. PHONE: 704-279-2125 ( INVOICE ® - DATE ._ J(J NO. -� 1 0 J ®;1 NAME / C Pe !?� ADDRESS /� L✓`�u ADDRESS CITY ITY PRODUCT CODE PRODUCT CODE'' k ❑ FUEL OIL ❑ KEROSENE- ' * ❑- FUEL OIL ❑KEROSENE:" EQUIPMENT FUEL ❑ DIESEL EQUIPMENT FUEL ❑ DIESEL ❑ FARM FUEL ❑GASOLINE * 0 .FARM .-FUEL ❑GASOLINE it DYED DIESEL FUEL _ * DYED DIESEL -FUEL - NONTAXABLE USE ONLY NONTAXABLE USE ONLY PENALTY FOR TAXABLE USE PENALTY FOR TAXABLE USE _' e AMOUNT AMOUNT .AMOUNT PAID PAID AMOUNT PAID - TOTAL TOTAL RECEIVED BY: - DUE CEIVED BY DUE � 'tr II T t`I� AT T �,. Gals. Reading -Start `_ u Gals. Reading -Start:- , _ o >. Gals. Reading - Finish - _ _ _ -:.Gals. Reading- Fmish. _ I Sales Sequence Number - _ ry "j `' �` Sales Sequence,Number. p.4 1 J Price per Gallon - cents _ .�yq Price per Gallon -cents p c (?I Product Cost `, Li 4 .'Product Cost tiI .' Tax Total Price — 1 ; y `1 �� '" °` Tax Total Price , - f .' 2927 yL ,i... i !.I "d31%p,e.'Y`E.t •'ity. 3-. ..ib iy^`[ ..y .S '-',:d'a.3'ti.5+'�x.♦k'wi—n'r�Ads3jafl hje'e�n' SIFFORD.'S `OIL CO. 6130 HWY. 152 EAST ROCKWELL, N. C. 28138 STEVE SIFFORD PHONE: 704-279-2125 r7 _ Lf - INVOICE NO. 10645 DATE;-� ✓ NAME ADDRESS CITY PRODUCT CODE .. ❑ FUEL OIL ❑KEROSENE ' ` UIPMEN- T FUEL ❑ DIESEL'': * ❑ FARM FUEL . ❑ GASOLINE,,- * DYED DIESEL FUEL NONTAXABLE USE ONLY PENALTY FOR TAXABLE USE AMOUNT AMOUNT PAID TOTAL RECEIVED BY: DUE - ` 10aQt Uals h ading =' gtV1 147; i 1 i'1 E 12 v..4-7 Gals. Reading - Finish Sqtles Sequence Number — — — 9 6- , Price per Gallon - cents Product Cost — - — . -1 3, 0 Tax _ Total Price vvi iii cvvo -va:1;f I"A.-A 7U4+88B+2270 . ... ..... J... RU9SELL 1002 REMIT TO: J .: T . Russell & Sons; 1721, US,52 NORTH- - Albemarle-, NC; 280.01. 704-982=2225 Regular: Invoice BILL T0: 1037 ALCHEM, INCORPORATED SHIP TO: *SAME* 8135 RED ROAD ' ROCKWELL, NC 28-138 Invoice No. - 2663 Page-1 of_ -1 Transaction •Date-..02/01/08 Due Date Prof Number -'"''."Reference, Terms 02/02/08 Crusher Sales - an 08 Due Upon Receipt, Description U/M ;_Quantity Unit Price ` - Ext : ' Price . 1.2 Crushed Conc 1.3 Crushed Conc TONS TONS 40'.0000.' 11.0000 44.0.00..: 1 •4 Crushed Conc TONS 7.54.0000 154. 0000 11.0000 1,;.694.00 1.10 Crushed Conc TONS 110.0000 11.0000 11.0000 1', 69'4 .00 . 1.11 Crushed Conc 1 . 11 3" Rock TONS .• 132.0000 11..0000 1'r210.00 ;.,-1, 452. 00 1.14 Crushed Conc. TONS' 110.0000 000 12.0000 V`264.00, 1.17 3" Rock 'TONS. 44.0-000 11.0000 1,210.00 1.17, Crushed Conc TONS,',,. 66.0000 .000.0 11.0000 5.28.00 . 1.18 Crushed Conc 1.23* Crushed Conc TONS '. TONS 22.0000 11:0000 726.00 242..00 1.24 Crushed Conc TONS 22.0000' 110.00`00 11,0000 242.00- 1.25 3° Rock TONS 44.0000 11.0000 12.0000 1,21Q.00 - 1.25 Crushed Conc TONS . 220000 11.0000, 528..00 1.28 3." Rock 1..28 'Crushed Conc TONS TONS 22.0000 12..0000 .242.00 264.00.- 44.0000 11.0000 484.00' SUBTOTAL $12,430.00 Sales Tax $732.11. Freight 0.00 Other- Amounts , 0:'0'0 **Reprinted Invoice Invoice TOTAL $13,162.11 Net, Invoice ,,,TOTAL $T3, 162.11 008 09:12 FAX 70.4+986+2270 . � J T'RUSSELL wool REMIT TO. J. T. Russell &Sons., -Inc. .1,721 US52.-NORTH-... Albemarle, NC 28001 704-982-2225 Regular" Invoice BILL TO: 1037 ALCHEM, INCORPORATED SHIP' TO: *SAME* 8135 RED ROAD ROCKWELL, NC 28138 Invoice No: - 2717 .Due Date Proj Number: Reference 2.1 3" Rock 2.1 Crushed Conc 2.4 311 Rock 2:1,1 Crushed Conc 2.13 3" Rock 2.14 .3" Rock **Reprinted Invoice page :.I of z: ' #4,saction Date; - , 03/04/08.'. Terms TONS" TONS. 44.0000,, 22.0000 12.0000 ..; 5,28 : 00 TONS 44.0000 11. 00'00. '12.0000; .. TONS. 22.A000 . 11: 0000 1 ; „ 5,218:00., . . TONS.. TONS 44.0000 44.0000 . 12.0000 , . :`'528:00 12.0000 -528.00 Clndlerf>G N. Long Street, P.O. Box 139 Salisbury, North Carolina 28145-01-0139 Salisbury, 704/636.4713 Fax 704/636-2424 Chalddller�Coonccrete and BuildingSupplywww.chan�die�ridon�+crre+t�e.com ' 6':Z":3^+AMA 'bwA. •`M 'V'ir.lwli. , �.;74 f Lr' ',: ,6J �X �.?7.£,�'e� C:;r •!. HIP1 i'C�t1wNT • _L�.1 C 41 r J{DT 1:'ia 1 F�'7C t l.._ ; 11".thr N#:1- l0"t"k'# DESCRIPTION • _ 10 1'7i f # 3 ; )-iaL OCt CONC 13-1_OCK ; 0� ,. 4X 7 m' ;. Liw!_. li.i C. a i0 A 1 �� , G 31P Q to 3 .00 L1 it0.0ej 1�a D I - L CLAIMS AND RETURNED GOODS MUST BE ACCOMPANIED BY THIS BILL. 50 MM G i l 14M" M 3 WON DAYS ffii RE iment is due upon delivery of the goods and/or performance of the services described above and may be made within 30 days after date of this invoice without payment of a finance charge. A finance charge at the annual rate of 18 % (1112%) per month) Is payable any unpaid portion of the purchase price from the 31 st day after the date of the Invoice until the day on which the purchase price is paid. cn� ndler � C7r ndler Concrete and Building Supply �" —.r #. + I" }"si u 11 L�08. f,.nQ100 IJLL }?f�t`i- q�sr'f�l'�IRc��1 704--279_-79 8 . 400 N. Long Street, R"0,•Box 139 Salisbury, North Carolina 28145-0139 704/636-4713 Fax 7041636-2424' www.chandlerconcrete.com i} IVt /EtCIL►faPS ' 3f, wl3 -f€31•AE.. =i fsd5� �t3 Received By RI S P TRk: NT Cwus-r r,o « 1 C,7G:; 'I T1~ R119 p r1.►� 11 0 r at�t1 r7YL1 c . �J tyr e t:l 3 C 24 • DESCRIPTION • i ti3 t. %1 INTERLOCK CONC BL OCI-% �313}�c";'�'t•;� 72 . 13 DEI_. t+l70C.. A 10 ? x. 00 B� _,3 ' ,��. �f('f C.'' g i 10 I..I) 100. 00 y ' 11' • �O• CLAIMS AND RETURNED GOx' ODS MUST BE ACCOMPANIED BY THIS BILL. t WE KVH U�4 1 am eraGo 30,DAY9 air ME �y f101J 1iy1(J'�1111Yr4 - ^('�}!�y'}vy N,!.1 i U NCI-ROWd1P't ... ..'i�i}.1. Iq TOTAL, 41101 136 nent is due upon delivery of the goods and/or performance of the services described above and may be made within 30 days after late of this invoice without payment of a finance charge. A finance charge at the annual rate of 18% (1112%) per month) Is payable ny unpaid portion of the purchase price from the 31st day after the date of the Invoice until the day on which the purchase price Is paid. _s Received Rv 400 N. Long Street, P.O. Box 139r Chandlernc Salisbury, North Carolina 28145-0139 , , iHECKE+ Y HOWDELIVERED 704/636-4713 Fax 704/636-2424 TIME OU- Chandler Concrete and Building Supply www.chandierconcrete.com I P4 V C3 I ifs th f �, i_ f i.�t"f 07 !31-;1P JAS:ON t; 1 F,J 0le"jI t.`� ►:ti l P. t: tit-�T = • �J+ I � '�f �. ifr ra ., d ,!l)4--i_,'r' a :.,,j08 DESCRIPTIONUNITS PRICEMNIT • OX24 X36 ] '61 iC f 3O)tiE'4 )L 72 ] il1K7c� u 3 2 1 r , 550 rA fi • . �}J�2 i) 1 t� _ �,,,:,- t Fd. 00 LD ]. GiiLI, tjl�ri LL CLAIMS AND RETURNED GOODS MUST BE ACCOMPANIED BY THIS BILL. IVC'�'R�14df�1'i 38 P TOTAL //0. r ,fit { i' G; (16G �C7� f P17 ' TO PMTS GR 30 mys PMT RE 'ayment is due upon delivery of the goods and/or performance of the services described above and may be made within 30 days after ie date of this invoice without payment of a finance charge. A finance charge at the annual rate of 18 % (11/2%) per month) is payable - -Jd ,n e portion of the purchase price from the 31 st day after the date of the invoice until the day on which -the -purchase Rec prjce Is paid. ' w. , . eived By , N. Long Street, P.O. Box 139 Chandlernc lis -01 Salisbury, North Carolina 28145 0139CHECKED , Y HOW 704/636-4713 Fax 704/636-2424 ' DELIVERED TIME OUT Chandler Concrete and Building Supply www.chandierconc�rrete.com �:6v �!ti, i t✓il�t It r I_F' iIE111 '. i,. r'•'"�i:_1..�.. {'I I_r �!tli a - Ci l-i I �. i <i . +. _ 's !. a i. ].I,',�:!(;, 1�1i%n;'.tt:`.i [.il:�t_ '[:11=t'I'(� o ��i;r: �' 1.i�:.'✓ttrS DESCRIPTION• ci 1;J'i-J`I<QCK !:ONC BI-OCK 3! X6,,,s:(/ ].it`d�4 liST%!=(i.1:td( Fi!'It_f" 30' 2'4X t,. 1l4't70 0 g r.3 w 35. 1(h EA 17.50 GAF] 31`1. �} to 10. Of!) L:Z) oE -�-1� s-erg a� .L CLAIMS AND RETURNED GOODS MUST BE ACCOMPANIED BY THIS BILL. f<4 0r.Jt' HFII T€31`nL irl:�, 38 >Lii ' 31 CUSTOMER COPY yment is due upon delivery of the goods and/or performance of the services described above and may be made within 30 days after f' date of this invoice without payment of a finance charge. A finance charge at the annual rate of 18% (1112%) per month) Is payable any unpaid portion of the purchase price from the 31 st day after the date of the Invoice until the day nn which the n11rrh— —;-1. —1,4 Q N 00 Agri -Direct® PO Box 239 Micro, NC 27555 80034"169 or 919-2 ".15 Webslte* www.aad-suoolv.com AGRI SUPPLY "Since 1962" Invoice I -Pane Inv; 011ce" No.--`;" .3-5503300: K, gg. ifl Ship T4 Aldh6m.Inc , 8135'%Red.Rd. Rockwell NC 28138 "Operatdr.. I ".:`-Te ­V70 JASON "7 04 2791.7908 BEVERLY' Btfik tard . MOTOR FREIGHT Item # I Bin I Description UM, I QOR, I QBO--I',. GISH I Price. I Amount 12703 1806A SF2JL PE 2 5 tip PMESTAL. MOUNTED- Ex 0 , 44 �95 4 9 5 PUMP 12704 1806A SE3LL PE 32 5-HP PEDESTAL MOUNTED EA 2 0 169.95 339.90 PUMP 66650 2011B YCD-48 FOLDING CHAIR EA 8 0 66648 2019E YCZ-244Z 81 FOLDING TABLE' EA I 1 g 59.95 0.00 Comments: 12-28-07 ITEM#66648 W'l IS OA SHIPPIING FROM STORE#4 ON PRESOLD# 453198 0 too S mer"M 0. 6jPD jotal it qfld BSI Due .400j� I ... Customer# lnvc hm 100096 _07351Si R.t. Cod.: Item # Bin DescriptIon Ulm"Price Amount 12703 1806A SE2JL PH 2-5 HP'PEPESTAL-MOUN -EA- • '144.95 144.95 12704 1806A SE3LL PE 30 5 HP PEDHSTAL.MOUN EA 169.95 339 90 Refund or Credit In 66650 2011B YCD-48 FOLDING CHAIR EA 17.95 143.60 the form of the 66648 2019B YCZ-244Z 81.POLDzNo. TABLE rA 59`95. original payment? 0. 00-:.-�,".: Complete the order form on the T-15-3 reverse side Please check her. If You wish to order additional ftemsL: - ✓ ("form on reverse side) _WV1..QWJJVV VOVW HOW16.", "Alchem Inc. P1 8135 Red Rd. the' R0CkWe11*NC 26138 Return Codes: I. Damaged in Shipment SHIPTO:.. 2. Ordered wrong item 'AGRI. 3. Wrong Item' Shipped PIRECT(P 4. Did not like product 582 Lowell Mill Rd 5. Defective IIIII 6. Not shipped timely Selma, NC 27576 7. Listed wrong in catalog 5E0702101 P - Alchem - Stormwater Berm InvoIce •#: 1309033, Invoice Group: invoice Date: • 12/14/2007 Phase: 0010 - Existing Berm Evaluation Task: '*" - Default Rate Schedule Labor Class / Employee Name Hours Rate Amount ENGINEER SENIOR Ribblett, Gary C. 1.75 . 130.00 . 227.50 Total: ENGINEER SENIOR 1.7F 227.50 ENGINEER SENIOR Walls, Stephen A. 0.25 105.00 26.25 Total: ENGINEER SENIOR 0.25 _ 26.25 SCIENTIST STAFF Lindsay, Katherine Shaber 0.25 70.00. Total: SCIENTIST STAFF • 0.26 `... 17.50 17.50 PARAPROFESSIONAL Gallagher, Laura 0.50 50.00 ... Neal, Vicky M. 0.75 25.00 Total: PARAPROFESSIONAL 1.25 50.00 37.50 62.50 Total Labor 333.75 Unit Pricing Expenses - Rate Vendor/ Employee Name Doc Nbr Date_ ,• Units„-. •. Rate Amount DIRECT EQUIPMENT EXPENSE OVERNIGHT SHIPPING -EACH UP0337199 11/09/2007 1,00 20.000 Gallagher, Laura: overnight letter report 20.00 y Total Unit Pricing 20.00 Total Phase: 0010 - Existing Bernt:Evaluation Labor: 333.75 Expense: 20.00 Total : 353.75 Total Project: 5E0702101 P - Alchem - Stormwater Berm Labor : ' 333.75 Expense : ' 20.00 Total :. 353.75 I I o+h e r be l o r e Lei sandal l - can ei cop(es � ORti IN -Al L i , " TustainableStrafegies for-GlobalLeaders' ` Pa e 2 Q E_ 0 V E i k:'':. 9 of 2 �LLt�.r7.Y-=1� v� . MAN HOURS WORKED FROM 11/2007 - 3/2008 REGULAR HOURS WORKED-11,016.39 x $14.00 (AVG) _ $154,229.46 OVERTIME HOURS WORKED-1,834.72 x $21.00 (AVG) , =$38,529.12 TOTAL LABOR COST = $192,758.58 MAE 4Irk e . 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