NCG510006_Regional Office Historical File Pre 2018 (2)

N A % Michael F. Easley; Governor
William G. Ross Jr., Secretary
UJ North Carolina Department of Environment and Natural Resources
.0
`C Alan W. Klimek, F.E. Director
Division of Water Quality
. �UEPt
r J
February* 23, 2006
Mr. William H. ,Hall ) ',,
Environmental Business Manager
BP Products North America, Inc.
501 Westlake Boulevard, Suite 20.111C
Houston, TX 7707
W4 TER QUALITY Re: Name/Ownership Change
C � (� ;
CG51OOO6
Paw Creek remediation
Mecklenburg County
Dear Mr. Hall
e are in receipt of your correspondence regarding the above reference permit. I am returning your check 5935 in
the amount of $ 0.00 dated February 6, 2O06. At this time no fees are pending. The annual fee wilt be billed
separately at a later date.
If you have any additional questions or concerns pertaining to the subject permit, please contact me at (19) 733-503,
extension 520.
Sincerely,
Frances Candelaria
Point Source Branch
Enclosure
cc: CENTRAL FILES
���e. • c►na1 feeWater uality= '
PIES Unit
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 < Phone [phone] Customer Service
Internet: w.ncwatewdity ora Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax (91 ) 733-2496 1-877- 23-674
An Equal Opportunity/Affffnative Aclion Employer — 50% Re d110% Post Consumer Paper

tij't I- `11
AMA
Or A ;k
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Michael F. Easley, Governor William G. Ross, Jr., Secretary
A f
Alan W. Kfirnek, r�,E,, D"irector
March 2, 2005
Ms. Barbara Castleberry, Environmental Coordinator
TransMontaigne Terminaling, Inc.
200 Mansell Court East, Suite 600
Roswell, Georgia 30076
SUBJECT: Compliance Evaluation Inspection
TransMontaigme GWRS
Southeast Terminal, 7401 Old Mt. Holly Rd.
NPDES Permit No. NCG5 10000
Certificate of Coverage No. NC510006
Mecklenburg County, NC
Dear Ms. Castleberry:
On February 16, 2005, Mr. David Rimer of the Mecklenburg County Water Quality
Program (MCWQP) conducted an inspection at the subject facility. This inspection was
conducted as part of a cooperative working agreement between Mecklenburg County and the
Division of Water Quality. The enclosed report should be self-explanatory.
If you have any questions concenring this report or any other matters, please do not
hesitate to call Mr. Richard Bridge an or me at this Office.
Sincerely,
IR All
D. Rex Gleason, P.E.
Surface Water Protection Regional Supervisor
Enclosure
cc: Rusty Rozzelle, MCWQP
DRG/djr
File: WQ TransMontaigneS10006,205,doc
Mooresville Regional Office One
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 Carolina
Phone: [phone] / Fax [phone] / Internet: h2o.enr.state.ne.us
An Equal Opportunity/Affirmative Action Employer - 50% Recyded/10% Post Consumer Paper

United States Environmental Protection Agency, Washington, DC 20460
Form Approved 7-1
Am% NPDES Compliance Inspection Repoli OMB No, 2040-0003 03
AGA
North Carolina Department of Environment and Natural Resources
Approval Expires
Division of Water Quality, Mooresville Regional Office CDENR 7/31/85
Section A. National
Transaction Code t tPDES Permit No. YR/N'1O/DAY Inspection Type
Inspector Facility Type
N 5 NC510006 05/02/16 C
C 2
Remarks.
Inspector: lenburi Count Water iialit
Inspection Work Days Facility Self-I'vIonitoring Evaluation Rating III QA
...........Reserved.......;....
.6 3 N N
Section B: Facility Data
Name and Location of Facility Inspected- Entry'rime:
Permit Effective Date:
TransMontaigne GWRS 2:00 PM
October 1, 2001
Southeast Terminal Exit Time:
7401 Old Mt. Holly Rd. 110PM
Permit Expiration Date:
Mecklenburg County, NC Date:
September 30, 2006
May 28, 2004
NO ame(s) of n-Site Representatives ------- Title(s) -- — ---- P_honeNo(s).
Mr, Keith Lewis, ORC, [phone]
Name and Address of Responsible Official: Title:
Ms. Barbara Castleberry Environmental Coordinator
TransMontaigne Phone No.
200 Mansell Court East, Suite 600
Contacted?
[phone]
Roswell, Georgia 30076
No
Section C:
Areas Evaluated Durin gr, Inspection'
�Pennh�ZFla ­wMeasurement Z Operations& Maintenance
1:1 Sewer Overflow
Records/Reports Ej Self -Monitoring Program El Sludge Handling/Disposal
El Pollution Prevention
Facility Site Review El Compliance Schedules El Pretreatment Program
EJ Multimedia
Effluent/Receivi er
Other-.
Section D: Summary of Findings/Comments
All areas are rated satisfactory finless otherwise indicated. See attached sheets) for summary,
Signature(s) of Inspector(s):
Agency/Office/Telephone-,
Date:
David Ri
MCWQP/[phone]
February 21, 2005
Signature of Reviewer:
Agency/Office
Date:
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

GENERAL:
The facility was last inspected on May 28, 2004 by the Mecklenburg County Water
Quality Program MCWQP . A Compliance Evaluation Inspection Report was issued on June
22, 200 .
PERMIT:
The NPDES treatment works for the subject facility consist of a groundwater remediation
system with two oil/water separators in series, an air stripping` system, two particulate filters in
series, two carbon filters in series, and a holding tank.
The facility operates under General Permit No. NCG5 0000 Certificate of Coverage No.
NC510006. The permit becae effective on October 1, 2001 and expires on September 30,
2006. The permit authorizes the discharge of treated petroleum contaminated groundwater.
The permit properly describes the facility and appears adequate for the wastewater.
RECORDS/REPORTS:
The facility is not required to submit Discharge Monitoring Reports lDMs wider the
terms of the current permit. The system has not been operated since June 2000 and there are no
laboratory analytical reports for the current review period, The Operator in Responsible Charge
(O C) indicated that the system is shut down while the permittee considers more effective/
efficient methods oftreatment.
FACILITY SITE REVIEW:
The facility is engaged in fuel oil, gasoline, and kerosene storage and distribution. The
groundwater remediation system has not been operational/discharging since June 2000.
FLOW MEASUREMENT:
There has been no flow since June 2000.
LABORATORY:
No laboratory analyses were performed during the past twelve months since there has
been no flow.

C
EFFLUENT/RECEIVING WATERS:
The facility is permitted to discharge to an unnamed tributary to Paw Creel, which is
classified C waters within the Catawba River Basin.
The groundwater remediation system was not operational and the facility was not
discharging at the time of the inspection.
SELF -MONITORING PROGRAM:
o laboratory analytical reports or DMRs were available for the current review period
from January 2004 through December 2004, as there was no flow.
OPERATIONS S MAINTENANCE:
The facility and site appeared well maintained,

aware of the incident and had been in contact with appropriate persons. She sent
a letter to the company in August 2004 which included a requirement for additional
cleanup efforts® UESA was cc'd.
I Of 1 10/6/2004 8:38 AM

z
;,�>IDJULP
a., ENGINEERING, INC.
f
3
April 30, 20(}4
r. John Uteck
Connestoga Rovers & Associates
4215-I StuartAndrew BoulevardTar":;
�� � �
Charlotte, North Carolina 28217 M
Via. electronic mail - JUteck raworld. v
Dear Mr. Uteck:
In response to your request on April 27, 2004, Shield Engineering, Inc. is submitting the
attached Cleanup Report documenting cleanup activities to date. Shield had tentatively
coordinated additional excavation activities for Monday, May 3, 2004 to address affected
soils identified in our March 22, 2004 assessment,
Curtis Oil would like to complete additional cleanup activities as soon as possible.
Please review the attached information and contact Shield as soon as possible so we can
complete the cleanup. I am out of the office this week, but can be reached at (74) 562-
7949. Thank you for your assistance.
Respectfully Submitted;
Shield Engineering, Inc.
V- 4L�
Gil Rowland
Emergency Response Manager
Attachments
c: Connie Campbell [,RZ F. C IFE. 1 IVI F. 101]
Inn
'301 Taggart Creek Road
$harlotte, NC 28208
www,shieldengineering.com
(0s
Telephone 704.394,6913
Fax [phone]

Heating till Release Cleanup Report
Southeast Ter iaa ransMuntaigne
7401 Old Mt. Holly Road
Charlotte, North Carolina
for.
Curtis Oil Company
by:
Shield Engineering, Inc.
4301 Taggart Creek Road
Charlotte, North Carolina 28208
Gil Rowland
Emergency Response Manager
James Wellons
Emergency Response Manager
U-1
ENOINEE IN ,IN -

)uth ast Terminal/TransMontaigne
101 told Mt. Holly Road
larlotte, North Carolina
Heating Oil Release (12/17/03)
April 30, 200
Page i
Table of Contents
Page
Introduction......:.
Impact of Release .......
Regional and Site Geology and Hydrogeology
Remedial Action..
Post Excavation Assessment ...
!""fnwnlwaainsae .mne�'1?�nnarssveeare.-l.s#in»�
TABLES
Table 1:
Summary of Analytical Results - Soil Samples
FIGURES
Figure 1:
Site Location Map
Figure 2:
Approximate Flaw Path Map
Figure 3:
Site Map
APPENDICES
Appendix A:
Laboratory Analytical Report
Appendix :
Soil Disposal Documentation

Southeast Ten
7401 Old W
Heating Oil Release (12/17/03)
April 30,2004
Pa e I
EXECUTIVE SUMMARY
Facij!!y !!!LoIT.!Lon. Southeast Terininal/TransMontaigiie
7401 Old Mt. Holly Road
Charlotte, North Carolina
Cause of Release: Piping beneath a tanker was damaged by a bollard as a
driver was leaving the product loading area.
e anti mnurrt of
Release: Approximately 300 gallons of dyed heating oil was
released.
incident, Abatement and
CleaR!!�Dales.* The spill occurred on December 17, 2003. Ed Wallace
Construction (Ed Wallace) responded and constructed three
underflow dams to contain runoff, Ed Wallace also
contracted Haz-Mat to recover product using vacuum
trucks. On January 7 through 9, 2004, Ed Wallace returned
to the site and excavated 12.56 tons of petroleum -affected
soils.
Recoyffor!y, Approximately 182 gallons of heating oil and 7,500 gallow,
of wastewater were recovered using vacuum trucks. Soil
excavation activities resulted in the removal of 12.56 tow
of petroleum affected soil.
Anal tical Results: Six post -excavation soil samples were collected on March
22, 2004. The analytical report indicates that
concentrations of diesel -range organics (RC)) total
petroleum hydrocarbons (TPH) are above 40 milligrams
per kilogram (mg/kg) in five of the confirmatory soil
samples. Concentrations of DRO were below 40 ppm in
Area "A" located near the loading rack.
No detectable concentrations of EPA Method 625
constituents were reported in groundwater samples
collected from monitoring wells PMW-3, PMW-6, PMW-
9, and PMW- 10.

Southeast Terminal/TransMontaigne Heating fail Release: (1 /17/03)'s
7401 Cold Mt. Holly Road April 28, 2004
Charlotte, North Carolina Page 2+
Introduction
On December 17, 2003, approximately 300 gallons of dyed heating oil was released at the
Southeast Te inal/TransMontaine (SE Terminal) facility. Figure 1 illustrates the location of
the SE Terminal.
Based on conversations with SE Terminal personnel, piping on a Curtis Oil Company tanker was
damaged by a bollard while exiting the loading area. The dyed heating ;oil spilled onto a
concrete driveway to the crest of the loading area, Due to heavy rains at the time of the release,
some of the product flowed into a storm drain to the west of the incident area. The heating oil
followed a series of Glitches and storm drains until it reached a stream located on the southern
portion of'the property. Figure 2 illustrates the approximate flow path of the heating oil.
ReleaseImpact of
The heating oil was ;released onto a concrete parking area/driveway to the west of the fuel
loading rack. Figure 3 illustrates the approximate locations of the affected soil areas described
below:
Area "A," a gravel area to the north of the incident location,
loom low area to the west of the SE Terminal office building.
AlkloW linear ditch, trendingnorth/south, lined with cobble -sued stone (rip rap for erasion
control purposes),
NoWa linear ditch to the south of a chain -link fence (directly south of Area "C")..
In addition to the soil areas described above, a stream located to the south of the bulk petroleum
storage areas was reportedly affected by the release. However, monthly sampling of the stream
by SE Terminal personnel has not indicated an impact to the stream as a result of this incident.

Southeast Te inaltTransMontaigne ;heating Oil Release (12/17/03)
7401 Gild Mt. Holly Road April 28, 2004
Charlotte, North arolin page 3
Regional and Site Geology and Hydrogeology
The spill occurred in the Charlotte Belt of North Carolina's Piedmont Physiographic Province.
The topography of the Piedmont Province generally consists of low, well-rounded hills and long
rolling generally northeast -trending ridges. The Piedmont Province has been divided into five
parallel belts: from east to west, the Carolina Slate Belt, Charlotte, King's Mountain, Inner
Piedmont, and Brevard Belts. These belts represent the major litho -tectonic features of the
Piedmont Province. Based on the Geologic Map of North Carolina (Brown et al., 1985), the
Charlotte Belt consists of ancient igneous and metamorphic rocks of early Paleozoic to Mesozoic
age.
characteristic feature of the region is the reolith, which consists of residual soil, and sarolite
that typically covers the bedrock. The regolih is generally composed of an unconsolidated or
semi -consolidated mixture of clay and fragmental material ranging in grain size from silt to
boulders. The texture of the soil zone has been so modified by the intensity of chemical
weathering and biologic activity that any textural resemblance to the parent bedrock has been
destroyed. The saprolite is a clay -rich, residual material derived from in -place chemical
weathering of bedrock that retains some of the textural features, such as relic quartz veins and
dikes.
In this geologic setting, the aquifer for groundwater supply includes two components: soil and
underlying rock. The boundary between soil and rock: is not sharply defined. A transitional zone
termed "partially weathered rock" (PWR) is normally found overlying the parent bedrock. PWR
is defined for engineering purposes as residual or saprolitic material with standard ;penetration
resistance in excess of 100 blows per foot. Weathering is facilitated by fractures, joints, and by
the; presence of less resistant rock types. Consequently, the profile of the PWR and hard rock
may be irregular and erratic, even over short horizontal distances. Also, it is not unusual to find
lenses and boulders of hard rock and zones of PWR within the soil mantle well above the general
bedrock level (Sowers, 1954).

tl
Road
rnlara"
Heating Oil
Al
The virgin soils encountered in this area are the residual products of in -place chemical
weathering of the underlying rock. In areas not altered by erosion or disturbed by the activities
of man, the typical residual soil profile consists of near surface clayey sails and underlying sandy
silts and silts.
Local precipitation is the sources of practically all of the groundwater in the site vicinity. The
upland slopes e.g., ridges and hilltops) are recharge areas, whereas rivers, streams, and creep
beds represent discharge areas for groundwater. A portion of the precipitation infiltrates into the
ground and moves under the influence of gravity to the water table. After the water reaches the
water table, the direction of movement is generally parallel to the hydraulic gradient. Thus, the
movement of groundwater will be approximately in the direction of the topographic slope when
in a region of similar lithology and will move in the path of least resistance in areas with varying
lithologies and sediments. The movement of groundwater results in discharge to streams, lakes,
or springs where the ground water intersects topographic lows occupied by these water bodies.
Remedialcti
Immediately after the incident, SE Terminal personnel contacted Ed Wallace Construction to
initiate abatement activities: Three underflow dams were constructed in the flow path of the
release, and absorbent booms and pads were used to contain and collect heating oil. Ha -Mat
was also mobilized on the day of the incident to recover product from the underflow dam areas
and stream. Approximately 182 gallons of heating oil and 7,500 gallons of wastewater were
recovered using vacuum trucks. Recovered liquids were placed in an on -site oil/water separator.
Shield Engineering, Inc. was contacted on December 23, 2003, regarding the Curtis Oil
Company release. Mr. Gil Rowland of Shield met with Mr. Jim 'Sligh of SE Terminal and. Mr.
Ed Wallace on December 31, 2003 to discuss the scope of work for removal of soils affected by
the -Curtis Oil release. Mr. Sligh directed Ed Wallace to remove wails in Areas " " and "C" that
were visibly stained or exhibited petroleum odor. During this meeting Mr. Sligh indicated that
confirmatory samples were not necessary after soil excavation.

Southeast Tertninal/TransMontai ne Heating;Oil Release (12/17/03)
7401 Old Mt. Holly Road April 28, 2004
C'l aml lte, North Carolina Pape 5
On January 7 through 9, 2004, Ed Wallace mobilized to the site and excavated soils in Areas `*B">
cl "C". Approximately 12- 6 Mans of soil was excavated and transported to Soil Technologies
of Lattimore, NC for disposal. The excavated areas were backlilled with gravel (Area "B") or rip
rap (Area "C" ). Disposal documentation is included as Appendix A.
Post Excavation ss s
On February 4 2004, Mr. Jim Sligh contacted Shield and requested collection and analysis o
confirmatory soil samples from four areas (Areas "A" through "I ") and collection of
groundwater samples from existing groundwater monitoring wells. Mr. Sligh indicated this
request was made by' P Coil Company and/or their consultant, Connestoga Rovers & Associates
(C ). Shield contacted Mr. John. Utek of CRA and; requested historical data for the site. After
review of the historical data, Shield _ submitted a letter describing the proposed sampling
activities. After receiving comments from CRA and revising the proposed scope of work, Shield
collected soil and water samples from the site on March 22, 2004.
Soil samples were collected from in -situ soils rasing a decontaminated stainless -steel hand auger.
A portion of each soil sample was placed in a new, air -tight, plastic bag and after approximately
15 minutes, the head pace of each sample was field -screened with a TVA-1000 Organic Vapor
Analyzer. A separate portion of each sample was also placed in a new laboratory -supplied
container and placed on ice. Soil samples from each excavated area exhibiting the highest field -
screening; results were delivered under chain -of -custody control to Test America, Inc. o
Nashville, Tennessee for analysis. In addition, the soil `samples from Areas "B" and "C"
exhibiting the next highest field -screening results were also submitted for analysis. A total of six
soil samples (A- , 1 -1, 1 -2, C-1 C- , and 1 -2) were submitted. for I?RO-TPI1analysis.
summary of analytical results of snail samples is presented in Table 1. Refer to Appendix B for
laboratory analytical results. Soil sample locations and results are depicted on Figure 3.
Shield collected groundwater samples from four monitoring wells (P W-3, PMW-6, P W-q

Southeast Tenninal/TransMontaigne Heating Oil Release (12/17/03)
7401 Old Mt. Holly Road April 28, 2004
Charlotte, North Carolina Page
and PMW-101) located near the on -site stream that was reportedly affected by the release, Shield
personnel gauged groundwater depth and monitoring well depth to calculate well volumes in
each of the referenced wells. Shield personnel attempted to purge at =least three well volumes
from each well prior to sample collection. Three well volumes were purged from PMW-3 prior
to sampling. However, monitoring wells PMW-6, PMW-9, and PMW-10 were purged dry two
times each prior to sampling due to slow groundwater recharge. The groundwater samples were
placed in new, laboratory -supplied containers, placed on ice, and delivered under chain -of -
custody control to Test America for analysis of semi -volatile organics using EPA Method 625.
No detectable concentrations of requested method constituents were reported in any of the
sampled monitoring wells. Refer to Appendix B for laboratory analytical results. Monitoring
well locations are depicted on Figure 3.
Conclusions and Recommendations
Conclusions
• Concentrations of DRO-TPH were reported above 40 mg/kg in Areas "B", "C", and "D".
Concentrations of DRO were below 40 ppm in Area "A" located near the loading rack.
• No detectable concentrations of EPA Method 625 constituents were reported in groundwater
samples collected from monitoring wells PMW-3, PMW-6, PMW-9, and PMW-10.
Recommendations
4 3

c- 1 (0-0.5) C-2 (o.o.5) C-3 (o-o.5) .- C-4 - (o-o.5
_w� ­­ l_.________' TPH DRO NR
TPN DRO _iPH-6ko TPH DRO NR FID 22.85
FID 15 FID FID 23.66
K
18
TA TREE LINE
FENCE LINE
A-4 (0-0.5) ATANK D-3 (o-o.5) -2 (o-0.5) 117 _H­
TPH DRO NR 'ftikO NR
FID T49 ASPHALT--, TPH DRO NR FID 148
FID 1.04
PMW03
A-5 (0-CL5)
TPH DRIO NR PMW09
FID 6,61 COVERED PMW06
LOADIN
RA
GATE
TANK
TPH DRO 13 # 112
FID 912 D- 1 (o.o.5)
>_ ASPHALT— .,--,\
— — D-2
0q # TPH DRO NR (005
FID 454 TPH DRO (&Pmwlo
A-1 (o-o.5) # # FID
TPH D R 0 NR
FID 1.32 #
TANK
TANK TANK
TJAN
ill 1 5 TANK TANK
113 109
TPH DRO
FID 1372 oo5
W TPH DRO _B-3
uj FID 72.59 B-4 (0-0.5)
TPH DRO NR
LEGEND:
FID 14.99 TPH DRO NR
PIPE FID M64
MULTIPLE PIPE
6 FENCE LINE
TREE LINE
vt
4301 TAGGART CREEK ROAD
GROUNDWATER MONITORING WELL
Au"TION cm4ARLo-,,TTEw"`c 28208
+ SOIL BORING LOCATION 704 144,6913
ppm PARTS PER MILLION
mg/kg MILLIGRAMS PER KILOGRAM
SITE MAP
NR ANALYSES NOT REQUESTED
SAMPLE ID SAMPLE DEPTH (r'EET)
TOTAL PETROLEUM HYDROCARBONStAnsp SE TERMINAL tTRANS MONTAIGNE)
cr DIESELMMI 14GE ORGCS -- — ---- mglkg 7401 OL MT. HOLLY ROAD
FLAME IONIZATION DETECTOR rlD 6,41 pp,
PHIC SCALE CHARLOTTE, NORTH CAROLINA
GRAACTION A 4a32OW
0 NOTES: I- SOIL SAMPLES COLLECTED ON 03/22/04. 0 50 loo
F- DATE 04/29/04 DRAWN BY: DE
2- SITE MAP BASED ON CONESTOGA-ROVERS Et ASSOCIATES FIGURE 3.
3- ALL LOCATIONS ARE APPROXIMATE. SCALE: 1 in, - 100ft,
SCALE: APPROXIMATE FIGURE:
I L__j

Table I
Summary of Analytical Results
- Soil Samples
SE Terminal (TransMontaigne)
7401 Old Mt. Holly Road, Charlotte, Mecklenburg County, North Carolina
Marc 04
Analytical
TPH 8015/3550
15A NCAC 2L.01 15 (m) (Action Level) ------ >
40
Sample ID/Sample Sample Interval
OVA
Location (feet)
pin)
(mg/kg)
A -I 045
132
NR
A-2 0-0.5
1,04
NR
A-3 045
9.12
13-
A-4 0-0.5
7A9
NR
A-5 045
6.61
NR
0-0.5
597
1130
--B-I
B-2 0-0.5
72.59
82.2
B-3 0-0.5
1499
NR
0-0.5
19,64
NR
C-1 0-0.5
115
530
C-2 0-0.5
98.82
54.7
C-3 0-0.5
23.66
NR
C-4 045
2185
NR
D-1 0-0.5
454
NR
D-2 045
796
888
3 0.5
148
-NR
Notes:
OVA = Organic Vapor Analyzer
ppm = parts per million
TPH = Total petroleum hydrocarbons,
mg/kg = milligrams per kilogram
15A. NCAC 2L.01 15 (m) (Action Level) = NCDENR Statute rule for maximum allowable
concentrations for soil,
NR = Analyses not requested.
Concentrations in bold face type exceeded Action Levels,
K/Action1200WEVIC/Curtis Oil Co,[Table for soil samples

TestAmerica
ANALYTICAL TESTING CORPORATION
29I60 flos,irw CREIGIVION DkICk; " NASHFil,GL, T6\\i S,,EE 3720.1 :..:
800-765-0980 67a-726-,3404 FA\
ANA.LrYTICA.L, REPORT
SHIELD ENGINEERING, INC. 2138
Lab Number: 04-A42964
GIL ROWLAND
Sample ID: B-2
4301 TAGGART CREEK RD.
Sample Type: Soil
CHARLOTTE, NC 8208-5483
Site ID:
Date Collected: 3/22/04
Project: 403.2080-0:1
Time Collected: 11:15
Project Name: EC-CURTIS OIL CO
Date Received: 3/24,/04
Sampler: DH/ML
Time Received: 9:20
Page: 1_
Report
Pil Analysis Analysis
Analyse Result Units Lin:.t-
Factor Date Time :analyst Method Bauch
-GENERAL CHEMISTRY PARAMETERS*
% Dry Weight 52,6 %
1 3/ 24/04 10 40 B.Plett CLP 1493
*ORGANIC: PARAMETERS*
TPH (Diesel Range) 82.2 mg/:kg 4.E7
1 S/26/04 16:46 M.Jarrrett. 802 5B :4340
Simple Extraction Data
Fat/Val
Parameter Extracted Extract Vcl Date Time
Analyst Method
FPh/DRO 25.2 am 1.0 ml 3-j25/04
K. Turner 3550
Surrogate o Recovery
Target Range
TPH Hi Starr„ c-Ter phenyl 62.
35. 135.
Sample report continue
www testa mericainc.com
TestAmerica Analytical Testing Corporation I TestAmerica Drilling Corporation I TestAmerica Air Emission Corporation

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Fos6 rR C.hr i�;in'o\ Dkil F: - N %sul m r, `I t C" vsto t' 37201
ANALYTICAL REPORT
Laboratory Number: 04,-A42964
Sample ID: B-2
Project: 4032080-01
Page
LABORATORY COMMENTS:
ND - Not detected at the report limit.
B Anal to was detected in the method blank.
J = Estimated Value below Report ;Limit.
E = Estimated Value above the calibration limit of the instrument.
# = Recovery outside Laboratory historical or method prescribed limits.
All reported results for metals or Organic analyses have been corrected for dry weight.
End of Sample Report.
www.testamericainc.com
TestAmerica Analytical Testing Corporation I TestAmerica Drilling Corporation [ TestAme'rica Air Emission" Corporation

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Vr SUR tlut,16111'ON Dklvt', . Il x,nrtt t,t1, 'I'll,, NISZSI iE 374204 -
800-76 -t)980 615-726-3404 Fv,
A.LYTXC.".AL REPORT
SHIELD ENGINEERING, INC. 2138
Lab Number: 04--A4 965
GIL ROWLAND
,Sample ID: C-1
4301 TAGGART CREEK RIB.
Sample Type: Sail
CHARLOTTE, NC 8268-548<3
Site ID:
Date Collected: 3/2 /04
Project: 4032080-01
Time Collected: -12 a 20
Project Name: EMC-CURTIS OIL COmate
Received: 3/24/04
Sampler: Doi/ML
Time Received: 9 : 2
Page: 1
Report
Dil Analysis Analysis
A alyte Resuwt Units Limit
Factor Date Time Analyst Method batch
-GENERAL CHEMISTRY PARAMETERS*
%:Dry Weight 78,3 $
13/24/04 10:4.0 H,Plett CLP.. :1493
*ORGANIC PAR'AMEMERS-
TPH #Diesel Range? 530 mg,/kg 25
5 3/27/04 9:55 M.Jarrett 8015b 4340
Sample Extraction DaWa
wt/Vol.
Parameter Extracted Extract Vol Date Time
Analyst Method
E:PH/ 9RC 25,5 gm... 1,0 nil 3/25/09....
K. Turner 3550
Surrogate % Recovery
Tame." Ranat
TPH Hi 5urr., o-Terphenyl 90,
35, - 135,
Sample report continued ,
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TestAmerica
ANALYTICAL TESTING CORPORATION
2960 FosUitt Cvr; wroN, 1)ME - NASHNILLE- TENN SSEA", 3720
800-765-9980 - 61 a-729-3404 L:ty
ANALYTICAL ' REPORT
Laboratory Number: 04-A42965
Sample ID: C-1
Project._ 4032080-01
Rage 2
LABORATORY COMMENTS
NIA = Not detected at the report limit.
B = Anal to was detected in the method blank.
J =`Estimated Value below Report Limit.'
E = Estimated Value above the calibration limit of the instrument.
## =-Recovery outside Laboratory historical of method prescribed limits.
All reported results for metals or Organic analyses have been corrected for dry weight.
End of Sample Report.
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ANALYTICAL TESTING CORPORATION
2960 ! osi R Ctnt, rtwrwv 1)t,nta •
ti twtt4ir,st.. 1'r; r sr.t 37204
800-761-0980 615-720-:1404
Fvx
ANALYTICA.L, REPORT
SHIELD ENGINEERING, INC. 2138
Lake Number: 04-A42965
GIL ROWLAND
Sample III: C-2
4301 TAGGART CREEK RD.
Sample Type: Soil
CHARLOTTE, NC 28208-5483
Site ID:
Date Collected: 3/22/04
Project: 4032080-01
Time Collected: 12:28
Project Name: E tC-CUR'TIS COIL CO
Date Received: 3/24/04
Sampler: DH/ML
Time Received: 9: 2
Rage: 1
:.Report
Dil Analysis Analysis
Analyte Result Units Limit-
Factor Date Time analyst Method Batch
-GENERAL CHEMISTRY PARAMETERS*
% C`=y Weight '79,0 %
1 3/24/04 10:40 Ei.?,'UE'.%C CLk' 1493
-ORGANIC PARAMETERS*
TPH (Diesel Range) 54,7 me/kg 5.13
1 3/26/04 17:30 M,Jarrett 8015 4340
Sample ExtractionData
wt/vol
Parameter Extracted Extract Vol 'Late Time
Analyst Merhod
EPH/DRC 29.7 cm 1,0 :r:1 3/25/04
K. Turner 3550
Surrogate t Recovery
Target Range
TEE tit Surr., o-Terphenyl 75,
35. - 135.
Sample report cortirnaed
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TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Fosnii. CKimm,roN Dktt; -11 kisrta.r, J'cv\v,,,siX 3720,4
800-765-0980 - 615-726-3404 FA\
ANALYTICAL REPORT
Laboratory Number: 04-A42966
Sample ID: C-2
Project: 4032080-01
Page 2
LABORATORY COMMENTS:
ND = Not detected at the report limit.
B =Analyte was detected in the method blank.
J Estimated Value below Report Limit.
E Estimated Value above the calibration limit of the instrument.
# Recovery outside Laboratory historical or method prescribed limits.
All reported results for metals or organic analyses have been corrected for dry weight.
End of Sample Report.
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TestAmerica
ANALYTICAL TESTING CORPORATION
- 29F60 Frls'rric C.kr<l';ciar,w i)hiib,` • %' t s[I@'{P Lu;, 3 7'-1t1 4
800-765-0980 61,5426-3404 tryv
ANALYTXCAL REPORT
SHIELD ENGINEERING, INC. 2138 Lab Number: 04-A42967
GII. ROWLAND Sample ID: E-2
4301 TAGGARI` CREEK RD. Sample Type Soil
CHARLOTTE, NC 28208-5483 Site III.
Date Collected: 3/22/04
Project. 4032080-01 Time Collected: 13.55
Project Name: EMC-CURTIS OIL CO Date Received: 3/24/04
Sampler: SOH/MI Time Received: 9:20
Page: 1
Report = ail Anal=sig Analysis
Analyte Rest:lt Units Limit.: Factor mate Time Analyst: Method Batch
* GFNERAL CHEMISTRY PAPAMETERSn
u:: Dry Weight 49 0 b l 3/24/04 !C:40 B.Plett CLP 1493
*ORGANIC PARAMETERS*
TPH ;Diese: Range) 888 mg/kg 54.7 10 3,/27/04 1017 M.Jarre`t: 8015B 4340
Sample Extraction Data
Wt/V0l
Parameter Extracted Extract Vol Dave Time Analyst Method
EPE/DkC 24,7 gm:.. 1.0 m]. 3/ 5/04 K, Turner 35L0.
LABORATORY COMMENTS:
ND = Not detected at the report limit.
E Analyte was detected in the method blank.
J = Estimated value below Report Limit.
E = Estimated Value above the calibration limit of the instrument.
Recovery outside Laboratory historical or method prescribed limits.
All reported results for metals or Organic analyses have been corrected for dry weight.
The TRPH-Diesel surrogate was diluted out due to sample matrix.
End of Sample Report.
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Testl�merica
ANALYTICAL TESTING CORPORATION
'' t96 1 Fos'tkR ft[tFAt,it`Id % MR * N\ SltkK) E, TENNESSE' , 37204
800-705-0980 • 615- i 26-:3404 3; ii
PROJECT QUALITY CONTROL DATA
Iroject Number: 4032080-01
Irojec e: EMC-CURTI;S OI.L, CO
Page: ;1
''aboratory Receipt Date: 3124104
Matrix Spike Recovery
Note: If Blank is referenced as the sample spiked, insufficient volirne was received for
the defined
analytical batch
for -.
MS,/MSD analysis on an true sample matrix, Labotatory:.reagent water was
used for QC purposes.
Analvte Un:its orig. val. MS vat Spike Conic
Recovery
Target Range Q.C. Batch
Spike Sample
—EX'rRACTABLEE PARAMETERS-
2,4-Vichiorobenzene mg/l 0,0100 0,0310 0.0500
62
20 -
124 6398
BLANK"
N-11itrosod,_n-propyl.amine mg, -< 0.01CtC 0.3: 70 0.9500
94
1 '-
230 6398
:BLANK
1,2,4-Trichlorobenzene Mg,r/l < O,0100 0.0350 0.050
70
44 -
142 5398
BLANK
4-Chloro-3-methylphenol me3/l < 0,0100 0.0390 0,0500
1?8
22 -
147 6398
BLANK
Acenaphthene mg/1 - O.Dloo 0.0400 0.0500
se
47 -
145 6398
BLANK
2,4-dinitrotoluene mg/1 < 0.0100 0,0440 0.0500
88
39 -
139 6398
BLANK
Byrene mg/ < 0,0100 0.0360 0.0500
72
52 -
115 6398
BLANK
2-C.lorophenol mg/ < 0.0100 0,0240 0,0500
48
23 _
234 6398
BLANK
4-Nitrophenol mg/l < 0-,0100 < 0,0100 0,0500
N/A
1 -
132 6398
BLANK
Sesntachiorophenol Mg/2 < O.CCloo 0,0110 0.0500
22
14 -
176 6398
BLANK
Matrix Spike Dilpii4 at.e
Analyte units Orig. Val: Suplirate- R?D
Limit
2.C, Batch'
Laboratory Control Data
Analytte units Known Gal, Analyzed Val Recovery
Target
Range Q.C.
Batch
k roject QC. continued . `.
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TestAmerica
ANALYTICAL TESTING CORPORATION
2960 llosuf"'R Ckc1 (;Irru,% Dk1tr * NiSIRHJ,F. fENN1NSEC :3720.4
800-765-4980
(115-726-340411tt
PROJECT QUALITY CONTROL DATA
Iroject Number: 40320 -tit
Iroje Name: EMC-CURTXS OIL
CO
Page: 2
`'abvra ory Receipt mate: 3124104
Laboratory Control Datra
Analyte um is
Known Val,
Analyzed Val
% Recovery" Target Range
Q.C. Batch
w*UST PARAMETERS*
TPH Miesel Range) itg/kg
40,0
40.3
101
48 .- 135
4340
**EXTRACTABLE PARAMETERS**
Acenaphthene mgtl
0,0500
0,0440
88
47 - 145
6398
Acenaphthylene Mg/l
0,0500"
0,0416
E2
33 - 145
6398
Ant;hracene. nta,"l
0.0500
0,0450
90
27 - 133
6398
Berzidine mcp;t„
0,0500
< 0 0?00
N/A
3C - 155
6398
Benzo W anthracene ma/l
0,0500
0.0370
74
33 -- 143
6398
Benizota)pyrene Mq/1
0,0500
0..0360
?2
17:- 163
6398
Benzo (b) fluoranthene Mg/1
110500
0.0440
88
24 - 159
6398
Benzo(q,h, )perylene Mg/l
0.0500
0.0470
94
1 ;. 219
6398
Benzofk)fluoranthene mg/1
0.0500
0,0410
82
11 :- 162
6398
4-Bromopheny{lphenyiet.her mg/i
0.0500
0 0430
86
53 127
6398
Butyibenzylphthalate Mg/1
0.0502
0,04€70
80
I - 152
6398
4-Chloro-3-methylphenol :. mgfl
0.0500
0:0370
74
22 - 147
6396
bis{2-Chioroethoxy)metha7e n,g/]
0.0500.
0:0490
98
33 - 184
6398
bis";2-Chloroethyl)ether ingi`l
0 0500
0.061,10
122
12 - 158
6398
bis(2-Chloroisopropyl)ether ma/l
0.0500
0.0420
84
36 166
6398
2-Chloronaphthalene mg/1
0.0500
0,0410
62
50 - 118
6398
4-Chloroph+ny"lphenylether T"a/l
0.0500
0,0450
90
25 158
6398
Chrysene Mg/1
0.0500
0,0360
72
17 .- 168
6398
1!benz(a,h)anthracene tncg/1
0.0500
0:0500
100
1 - 227
G398
1,2.Dichlorobenzene cng/1
-.:0,0500
0,0360
72
32 -.129
6396
1,3-Dzchlorobenzene mg/1
0,0500
010330
66
10 - 172
6398
1,4-Dich16robenze e raq/ .
0.0500 .
0.0220...
-64
20 - 124...
6398
3,31-Dichlorobenzldane mg/!.
0,0500
010150
30
10 _ 262
6398
Diethylphthalate rgil
0,0500
0.0450
90
1 - 114
6398
Dimethylpnthalate mg/1
010500
0.0460
92
1 -- 112
6396
2,4-dinitrotoluene mq/'l
0.0500
0,0490
98
39 - 339
6398
2,6-D3nitrotoluene r4,`1
0.050E
0.0520
104
50 - 158
6398
Di-n-octylphthalate Tng/i
0,0500
C.0620
124
4 - 346
6398
vro1ject QC continued"
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TestAmerico Analytical Testing Corporation
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Corporotion

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 i osnk 0,,ritord % Dtot : a l lw{(Ft t.t l.. 1rr;Nvr.ssi;c 37204
tat 0-765-t)980
. 615-726-3404 111
PROJECT QUA.L XTY CONTROL DATA
"roject Number: 40320 1-0
roject Name: EMC-CURT a OXL,
CO
Page:
ra.bora ca. y Receipt Date. 3124104
Laboratory Control Data
Ana yte units
Known Val.
Analyzed Val
% Recovery-
"Baser Range
p.C. Batch
1,2-1liphenylhydsazine mg:/1
0.0500
0,0450
90
38 - 11..1
6396
Flucranthene nig/l
0,0500
00500
1.00
26 - 137
6398
Fluorene rng/1
0.0500
0,0450
90
59 - 121
6398
14ex chiorobenzene n1g/"'
0.0500
0.0510
102
1 -152
6398
Hexachlorobutadiene n1g/1
010500
0,0410
82
24 _ 116
6398
Hexachlorocyclopentadiene Tnq/1
0.DS00
0,0360
72
11 84
6398
Hexachloro thane mg./I
0,0500
0,0320
64
40 w 113
6398
inCieno(1,2 3-cd}pyrena Mg/1
0.0500:.
0,0480
96
1 _:.171
6398
isophorone Mg/:1
0,0500
OI 0440
fib
21 .: 196
6398
Naphthalene mg 1.
0.0500
0,0390
78
2'_ :33
6398
Nitrobenzene Mg/1
010500"
0,0460
92
35 - 160
6398
N-nitrosodl-n-prapylamine mg,F1
0,0500
0 0480
96
1 -=230
6398
h_n trosod pheny=l mine ma,''l
0,0500
0,0350
0
5,3 :: ;29
6399
N-nitrosodimethylamine rn/1
0.05D
0;0260
52
20 - 92
6398
Ph nanthrene mg/1
0.0500
0.0470
94
54 120
6398
Ryr-ene mg/1
0.0500,
0,0380
76
52 - 115
6398
Bis(2-ethy1hexy1)phtha1aTe Ing/1
0,0530
0.0460
92
8 - 258
6398
1,2,4-` richlorobk'.nzene m1 /3,
0.0500
01 0380
76
44 -.. 142
6398
2,4 6-Trichlorophenol mg;11
0.0500
010170
34 #
37 - 1.44
6398
2-Chiorophenol ing/1
0,0500
0.0260
56
23 - 134
6398
2,4-Dichlorophenol ukgfl
0.0500
0,0300
Go
39 - 135
6398
2,4-Dimethylphenol ma;e1.
00500
< 0.010'0
N/A
32 - 119
6398
2,4-ili.ns.trophenol mg/1
0.0500
0.012;
24
1 _:i91
6398
2_Methyl-4;:6-dini trophenol mg,"I
O0500
0.0140
28
1-..:38i
6398
2-N tronheaol nrg"1
0,0500
0.03310
62
29 - 182
6398
4-Nitrophencol mgll
C.0500
c 0.0100
N/A
1 - 132
6398
Pentachlorophenol Mg/1
0.0500
0.0i90
38
14 176
6298
Phenol Dgil
'0,0500
0.0180
36
5 - 11,2
61-98
Project CSC continued .
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ainc.com
TestAmerica=Analytical Te0inr0 Corporation
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{Drilling Corporation i TestAmerico
Air Emission Corporation

29n0Fotvrr<x t,6ut(«roof 6)wii itstszftff:, Tft ,-'ESsct":372 4
PROJECT QUALITY ITY CONTROL
DATA
Iroject Number: 0 32 0
-
Iroject Name: E C-CUR ''.Z5 OILS CO
Page: 4
*, .bora. t .ry° Receipt Date:
3124104
Dupi.-Ca es
Analyte units
Orig. Val,
Duplicate
RFD
Limit Q.C. Batch Sample Dup'd"
Blank
Data
Analyse
Blank Value
Units
Q.C. Batch
Date Analyzed
Time Analyzed
---------
--UST PARAMETERS—
TPR tDiesel Range:)
ma/kg
4340
3/26/04
1,4:13
, *EXTRACTABLE PFiPAMETERB*
Acenaphthere
<: 001D0
mg,/1
6398
3/30/04
1€::11
Acenaphthylene
0.0100
mg/]
C398
3/30/04
16:11
Anthracene
< 0.0100
mg/l
6398
3/30/04
1611
Benzidine
< 0,0100
rng,'1
6398
3/30/04
16: W i
Benzo(e anthracene
< 0.0100
mg/l
6398
3/30/04
16:1.e
Benzea)pyrene
< 0.01DO
mg,17:
6398
3/30/04
16.21
Benzokb)fluoranthene
< 0,0100
ing"11
6398
3/30/04
16:17
Benzotg,h, iperyl ne
< 00100
nag/i
6398
3i30/04
16:1:
BenzoWflacranthene
< 0.0100
mg/1
6398
+/'30/04
16tll
4-Bromophenyiphenylether
< 0,010E
nrg/l
6398
3/30/04
16= 11
Butylbenzylphthalat-e
< 0.0100
ingA'l
� 6398
3/30/04
I6:1`1
4-Chloro-3-methy? henol.
< 0.0100
cng,/l
6398
3/30104
1611
bisx2-Chloroethoxy)metnane
€ 0.0100
mg/1
6398
3/30/04
18s11
biF$(2-Ch1oroethyl)ether
< C?MOO
Mg/1
6398
3/30/04 _
16ill
bis(2-Chl0rolsopr-opy`)ether
e 00200
mg/1
6398
3/30/04
16:11
2-Chloronaphthalene
< 0,0100
mg/1
6398
3/30/04
16:11
-Cnloropnenol
< 00100
mg/1
C398
3/30/04
16:11
Project QC continued
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ANALYTICAL TESTING CORPORATION
2960 FritIER t;ttr.€€ru>i€as 1lrarai \tsrtr^ut,r, `i't.i,r°4,r.t. 37204
PROJECT QUALITY CONTROL DATA
Iroject Number: 4032080-01
rojec Name: E 'C-C'UR2'.:LS
OIL CO
Page:
;aboratory Receipt Date:
3124104
Bank
Data
Analyte Blank value
Uanits
Q.C. Bach
Analysis Date
Analysis Tirne
4-ChloropPenylphenylether
<.:.0,0100
mg/1
6398
3/30/04
16:11
Chrysene
c'0,0100
mg/l
6398
3/30/04
16s11
Drnenzta,hlanthra,cene
< 0,0100
me/1
6398
3/30,/04
26.11
1,2-Dichlorobenzehe
< 0,0100
mg/1
6398
3/30/04
16:11
1,3-Dichlorobenzene
<.:0,0100
rrg/l
6398
3/30/04
1611
1,4-Dichlorobenzene
< 0,0100;
Mg/l
6398
3;/30/04
16:11
3,31-richlorobenzidine
< 0.0100
mg/1
6398
3,/30/04
16:11
2,4-Dichlorophenol
< 0.0100
nrg/.l
6398
3/30/04
16:11
Die hylphthalate
< 0,0100
nig/1
6398
3/30/04
16;11
2,4-Dimethyl henol
< 0.0100
mg/1
6398
3/30/04
16:11
Dirrthylphthalate
< 0.02,00
mg/1
6398
3/30/04
1 :1]
Di-n-butylphChalate
< 0.0100
Mg/1
6398
3/30/04
16:11
2,4-D nitrophen^l
< O.0100
mg/1
6398
3/30/04
16;11
2,4-dinitrbtoluene
< 0.0100
Mg/1 :
6398
3/30/04.
1611
.2,6-banitrotoluene
< 0,0100
mg/1
6398
3/30/0
16:11
Di-n-ectylphtha..'ate
<:;0,01 00::
mg/l
:: 6398
3/30/04
16:11
1,2=D;pheny1hydraz:ne
< O.0100
mg/l
6398
3/30/04
16:1.1
3lucrantheae
< 0,0100
Mg/1
6398
3/30/04
18:11
8lu rene
< O0100
mg/l
6398
3/30/04
16+ 11
HexachIorobenzene`
< O} 0100^
mg/1
6398
3/30/04
16:11.
r".exachlorobutadiene
< 0,0100
Mg/1 "
6398
3/30/04
1'exachlorocyclopentadiene
, 00300
mg/i
6398
3/30/04
16:11
Hexachloroethane
c 0.0100
mg/1
6398
3/30/04
16:12
lndeno(1,2,3-cd)pyrene
c 0.0200
mg/l
6398
3/30/04
16:11
1sophorone
<..0,0100
mg/l
6398
3/30/04
16; 11
2-Methyl-4,6-•dinitrophenol
< 0.0100
mg/1
633,98
3/30/04
16:11
Naphthalene
< 0.0100..
nrg/1
6398
3/30/04
16.11
Nitrobenzene
<; 0,010
Mg/rl
6398
3/30/04
1E;11
2-N trophenol
< 0,0100
m9/l
6398
3/30/04
36:11
4-PNiCrophenol
< 0,0100
Ma/1
6.398
3/30/04
16M
N-nitrosods-n-propylamine
< 0.0200
mg.il
6398
3;/30✓04
:11
Project QC continued ; .
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TestArnerrca Analytical Testing Corporation
I
TestArnerica Drilling Corporation
I TestAmerica Air Emission Corporation

Testl-�merica
ANALYTICAL TESTING CORPORATION
CRI,i dl!rw, 1) I is • NA:rIM LE,
TEANE';.SET ;37204
800-765-0980 615-726-,1404 FAX
"
PROJECT QUALXTY CONTROL DATA
';reject Number: 403. f7- 01
'.r t j ec Name: HMC- CURT S CAI% Co
Page:
7$abc ra tory Receipt Date: 3124104
Blank Data
And.7yte Blank Value Uni. s Q.C. Batch
Anaiysi,s Date
Analysis Tune
N-nit.roscdi„when} attune < 0,0100 mg/1 6398
3/30/04
1611
N-nitrosodime:thylamine < 0.0100 Mg/1 6398
3/30/04
16M
Pentac:hlorcpherncl: < 0,0100" mq/ 6398
3/30/04
16:11
Phenanthrene < O.0100 Mg/l 6398
3/30/04
16:11
Phenol < 0,0100 m5/1 6398
3/30/04
16:11
P}rrene < 0,0100 n1g/1 6398
3/SO/04
16:11
B3s42-e1,hy1hexy1)p.._ha are < C.0100 tng/l 6398
3/30/04-
16: 1
2,4-Trichlorobenzene < 0,0100 Mq/I 6398
3/30/04
16:11
2,4,6-Trschicrophenal < O7 0100 mg,fI 6398
3/30/04,
16;11
End of Report for Project 338'775
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4
Y M1R.
368775
Projed Manager: �' � �+ &t 'UG C State
Telephone Number: 5q1-- bIL3 Fax: Report To:
Sarnp4err (P t } ? r 1 � �; nor i To:
Sampler Signature: �° ducat
Metre Preservation # of rosin
ter �t�r
St n a very
Rush (sur h rna pp) xs x trtt
n'_ s L vei
Date tlda.
''Fax Results, Y #
„� ;.
t
,a t
SAMPLE s REMARKS a
'
s
k
4
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Bottles Supplied y Test Ame6cw aRotd i
't0hod r,Rf f3,hipm-..n'V
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TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Fosrr,'R Ctri(mr o-, Dki\ i, - N �sm 37204
IL
800-76,53-0980 - 615-726-3404 10,"
4/ 1/04 CASE NARRATIVE
APR 720-442
�S'HIELD
ENGINESING,
SHIELD ENGINEERING, INC, 2138
1INC
GIL ROWLAND
4301 TAGGART CREEK RD.
CHARLOTTE, NC 28208-5483
This report includes the analytical certificates of analysis for all
samples listed below. These samples relate to your project identified
below-.
Project Name: EMC-CURTIS OIL CC
Project Number: 4032080-01.
Laboratory Project Number: 368775,
An executed copy of the n of custody, the project quality
control data, and the sample receipt form are also included as an
addendum to this report. Any CC recoveries outside laboratory
control limits are flagged individually with an 4. Sample specific
comments and quality control statements are included in the Laboratory
notes section of the analytical report for each sample report, if you
have any questions relating to this analytical report, please contact
your Laboratory Project manager at 1-800-765-0980. Any opinions, if
expressed, are outside the scope of the Laboratory's accredidation,
Pone I
Sample identification Lab Number Collection rate
- --------------------- -------- — ---------------
P!sW-3 04-A42958 31122/04
PMW-6 04-A42959 3/22/04
PMW-9 04-A42960 3/22/04
PMW-10 04-A42961 3/22/04
A-3 04-A42962 3/22/04
B-i 04-A42963 3/22/04
B-2 04-A42964 3/22/04
C— 04-A42965 a/22/04
C-2 04-A4296f, 3/22/04
D-2 04-A42967 3/22/04
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Page2
Sample Identification Lab Number Collection Date
These results relate only to the items tested.:
This report shall a
ced except i 11 and with
permission of the
Report Approved; By: eport Date: 4/ 2/04
Johnny A. Mitchell, operations Manager Gail A. Lage, QA/QC
Michael H, Dunn, M.S., Technical Director Glenn L. Norton, QA/QC
Pamela A. Langford, Technical: Sery Kelly S. Comstock, QA/Qc
Eric S. Smith, QA/QC Roxanne L: Cannot, QA/QC
Laboratory Certification Number: 387
zis material is intended only for the use of the individual(s) or- entity "to whom it is addressed,
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TestAmerica
ANALYTICAL TESTING CORPORATION
2960 7`os'rrR Lit i norioN ftir r: `
Ntsi3v
r` 3.7204
800-765-0980
615-726-3404
FAt
ANALYTICAL REPORT
SHIELD ENGINEERING, INC.
2138
Lab Number:
04-A42958
GIL ROWLAND
Sample ID: PW-3
4301 TAGGART CREEK RD.
Sample Type:
Water
CHARLOTTE, NC 28208-5483
Site ID:
Date Collected:
3/22/04
Project: 4032080-01
Time Collected:
16:00
Project Name: EMC-CURTIS
OIL CO
Date Received: 3/24/04
Sampler: DH/ML
Time Received:
9:20
Page: 1
Report
Dil
Analysis Analysis
.Analyte ". Result
Units
Limit
Factor Date rime
Ana;yst Method
Batch
*.-BXTRACTABL.E ORGANICS*
Acenaphthene ND
Ug/1
i0.0
1
3/30/04 28:03
R. Beard 625
6398
Acenaphthylene ND
ug/l
10.0
1
3/30/04 18:03
R. -Beard 625
6i98
Anthracene ND
ugtl
10.0
_
3/33j04 18:03
R. Beard 625
6398
Benzidine ND
ug/l
10.0
1
3/30/04 18:03
R. Beard 625
6396
Benzo(a)anthlacene ND
ug/1
10.0
?
3/30/04 18:03
R. Beard 625
6398
9enzo(a)pyrene ND
Ug/l
10.0
1
e3/30/04 18:03
R, Beard 625
6398
Benzo(b)fluoranthene ND
ug/l
1 .0
1
3/30/04 1 P 3
R. Beard 625
6398
Benzo(g,h,i)perylene VD
ug/l
10.0
1
3/30/04 18:03
R. Beard 625
6398
Benzo (k) fluoranthene ND
ug/l
10,0
1
3/30/04 12;03
R, Beard s25
6398
4:-Bromophenylphenylether -ND
ug1.1
i0.0
1
3./30/04 18:03....
R. Beard 625
6398
butyaberzylphthalate.: ND
ug;/:I
10.0
i
3../30/04:..18;03..
R. Beard 625
6398
4-Chloro:-3-methjlphenol ND
ug/l
10.0'
i.. ..
3/'30/04. 18;03
R. Beard 625
639.8
bis(2-Chloroethoxy)methane NI)
Ug/il
10,6
1.
3`30/04 18:03 ..
Rt Beard 62S
6396
bis(2-Chloroethyl)ethex ND
ug11
10.0
1
3/30/04" 18:03
R. Beard.. 625
6338
bis(2-Chhlorossopropyl)ether ND
ug/.1
10.0
1
3/30/04: 18:03.
R. Beard 625
63698
2-Chloronaphthalene ND
ug/l
10.0
1
3/.30/04 lEz03
R. Beard 625
6398
2-Chlorophenol _Nil
ug//.l
10,0
d,
3/30/04 16:03
R, Beard 625
6398
4.:-Chlorophenylphenylether ND
ug/
70...0
1
3./30/04.: 18:03
R. Beard 625
6398
Chrysene ND
ug/1
10.0
1
3/30/04 18:03-
R. Beard 625
6398
Dibenz(a,h)anthracene ND
ug/l
10,0
i
3/30/04 18;03 -
R, Beard 625
6398
1,2-Dicilorobenzene ND
ug/l
10.0
1
3/:10/04 16:03
R. Beard 625
6398
1,3-Dichlorobenzene ND
uql
10.0
1
3/301/04. 18:03
R, Beard 625
6398
Sample report continued ,
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ANALYTICAL TESTING CORPORATION
2460 Fosii§K CktAcirro% ]kilo,,
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04 P'Ne
ANALYTXCAL
REPORT
Laboratory Number:
04-A42958
Sample ID: PMW-3
Project.
4032080-01
Page 2
Report
Drl
Analysis
;Analy8a.s
Analyte
Result
Units
Limit
Factor Date
Time
Analyst
::.Method
Batch
1,4-Dichlorobenzene
ND
ug/l
14.0
1
3/30/04
18:03
R.
Beard
625
6398
3,3'-D4chlorobenzidine
ND
ug/`l
10.0
1
3/30/04
18:03 :
R.
Beard
625
6398
2,4-Dschlorophenol
ND
ug/l
10.0
1
3/30/04
18:03
R.
Beard
-625
6398
Diethylphthala e
ND
ug/l
10.0
1
3/30/04
18:03
R.
Beard
625
6398
2,4-Dimethylphen..c,l
ND
-agll
10.0
1
3/30/04-.
18:03
R.
Beard
.625
6398
Drmethylphthalate
ND
ug/1
10.0
1
3/30/04
' 18:03
R.
Beard
625
6398
Di-n-butylphthalate
ND
ug/l
10.0
1
3/30/04
18:03
R.
Beard
625
6398
2,4-Dinitrophenol
ND
ug/.i
10.0
1
3/30/04.
16:03
R.
Beard
625
6398
2,4-dsnitrotoluene
:ND
ug/i
: 10.0
1
3/30/04
-18;03
R.
Beard
625
6398
2,6-Dinitrotoluene
'TR)
ug/1
10.0
1
3/30/04
18:03
R.
Beard
.625
6398
Di -n-cctylphthalate
:ND
ug/:l
100
1
3/30/04
18:03
R.
Beard
::625
6398
1,2-Dipheny.hydrazine
ND
ug/1
10.0
1
3/30/04
18:03
R.
Heard
625
6398
Fluoranthene
ND
ua/l
10.0
1
3/30/04
=8:03
R.
Beard
625
6398
£luorene
ND
ug//l
10.0
1
3./30/04
18:03
R.
Beard
625
6398
fexachlorobenzene
ND
ug/1
lo.o
1
3/30/04
18:03"
R.
Beard
625
6398
Hexacirlorobutadiene
ND
ug/1
i0.0
1
3/30/04,
18:03
R.
Beard
625
6398
Hexachiorocyclopentadzene
ND
ug/1
10.0
1
3/30/04
18.03
R.
Beard
625
6398
Hexachlor©ethane
ND
ug/:1
10.0
1
3/30/04
:.18;03
R.
Beard
62S
6398
1ndeno(1,2,3-cd)pyrene.
ND
ug/l
10.0
1
3/30/04
3E:03.....
R.
Beard
625
6398
lsophorone
Nl
ug/1
10A
1
3/30/04
18:03
R.
Beard
625
6398
2 Methyl-4,6-din trophenol
ND
ug/l
". 10.0
1
3f30/04
= 18:0-1
R.
Beard
625
6398
Naphthalene
ND
ug/l
10.0
1
3/30/04
18:03
R.
Beard
625
6398
Nitrobenzene
ND
ucr/:1
-11r.0
1
3/30/04
18:03 :.
R.
Beard
625
6398
2-Nstrophenol
ND
ug/l
10:0
1
3/30/04
18:03
R.
Beard
625
E398
4-Nitrophenol
ND
ug/:1
10: 0
1
3/30/04
18:03...
R.
Beard
625
6398
N-nitresddi-n-propylamine
ND
ug/l
10.0
1
3/30/04
18:03
R.
Heard
625
6398
N-nilrosodiphenylamine
ND
ug/..1.
10.0
1
3/30/04.
18:03
R.
Beard
62.5
6398
N.-nitrosc,dameth}Flaming
Nn
u9/1
10.0
1
3/30/04-
18:03
R.
Beard
625
6398
Pentachlcrophendl
ND
ug/7
10.0
1
3/30/04
18:03
R.
Beard
625
6398
Phenanthrene
ND
ug/1
10.0
1
3/30/04,
18:03
R.
Beard
625
6398
Phenol
ND
ug/l
10.0
1
3/30/04
18:03
R.
Beard
625
6398
P,yrene
ND
ug/l
i0.0
1
3.j30/04.
18:03...
R,
Beard
625
6398
Bis(2-ethylhexyl)phthalate
ND
ug/l
1010
1
3/30/04
18:03
R.
Beard
625
6398
1',2,4-Trichlorobenzene
ND
ug/i
10.0
1.
3/30/04
18:03.
R.
Beard
625
6398
2 4,6 Trichlorophenol
ND
ug/1
10.0
l
3f''30f04.
8:03
R,
Beard
(5
6398
Sample report continued . . -.
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0
Testj-'..merica
ANALYTICAL TESTING CORPORATION
2960 Fosrtj. Cknnt;wro% lkiti37201
800-765-0980 - 615-726-3404 FAX
ANALYTICAL REPORT
Laboratory Number: 04-A42958
Sample ID: PMW-3
Project: 4032080-01
Page 3
------------------------------- ----------------- - ---------- ---------------------------- ---------------------------------------
Sample Extractlon Data
Wt/Vol
Parameter. Extracted Extract Vol Date Time Analyst method
----------------- ------- ------------ -------- ---------- ---------
625 1000 ml 1. M! 3/25/04 K. Turner 625
Surrouate Recovery Target Range
------------- ---------- ------------
surr-N.4trober.zene-d5 84. 12. - 135.
surr-2-Fluorobiphenyl 82. 14. - 132.
surr-Terphenyl d14 80, 11, - 1-42.
surr-Phenol. d5 39, 5. 79.
surr-2-Fluoronhenol 42. 5- 99,
surr-2,4,6-Tr,-bromophenol 61, 155,
LABORATORY COMMENTS:
ND = Not detected at the report limit.
B =Analyte, was detected in the method blank.
J = Estimated Value below Report Limit.
E = Estimated Value above the calibration limit of the instrument.
# = Recovery outside Laboratory historical or method prescribed limits.
No TIC's detected by GC/MS method 625.
End of Sample Report.
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TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Fws,ir't4 ( wh L,..
• NASHVIrE , .tr;,v'ES,,rf 37204
800-705-0980 *'
615-726-3404
Fiv
ANAL '''TXCAL
REPORT
SHIELD ENGINEERING, INC.
2138
Lab Number:-04-A42959
GIZ ROWLAND
Sample ID:
MW-
4301 TAGGART CREED RD.
Sample Type:
Water
CHARLOTTE, NC 28208-5483
Site ID,
Date Collected:
3/22/04
Project: 4032080-01
Time Collected:
1 :15
Project Name: EMC-CURTIS
OIL CO
Date Received:
3/24/04
Sampler: DH/ML
Time Received:
9: 0
Page: 1
Report"
Dil:
Analysis Analysis
Analyte Result
units
Limit
Factor Date Time
Analyst Method
Batch
-EXTRACTABLE ORGANICS"
Acenaphthene ND
ug/:l
10.0
1
3/30/04 19:40
R. Beard 625
6398
Acenaphthylene ND
ug//a
10.0
i
3t'30/04 18:40
R. Beard 625
6398
Anthracene ND
ua/1
10.0
1
3/30/04 18:40:
R. Beard 625
6398
Benzidine ND
ug/1
1L'.0
1
3/30/04: 18.40
R. .Heard 625
6398
Blenzo(a)anthracene ND
ugjtl
10,0
1
3/30/04 18:40
R. Beard 625
6398
Benzo(a)nyrene ND
ag/l
10.0
1
3t30,/04 18:40..
R. Beard 625
6398
Bes't..zo(b)fluoranthene, ND
uci`1
20,0
1
3/30/04 18:40
R. Beard 625
6398
Benzo(g,h,i)perylene ND
uq/l
20.0
1
3/30/04.. 18:40
R. Beard 625
6398
Benzo(k)fluoranthene ND
ug/i
1C.0
1
3/30/04 ..8.40
R. Beard 625
6398
4..Bromophenylpnenyleth.er ND
uq_1:1
i0.0
1
3/30/04 18:40:
R. Beard 625
€398
Bctylbenzylphthalate '. "ND
ug/1
10.0
1
3r30/04 18:40...
R. Board 625
6398
4-Chloro:-3-methylphenol :ND
ug/l
10..0
1
3/30/04 18:40
R. Beard 625
6398
b s(2-Chloroethoxy)methane ND
ua./.l.
111_0
7
3;/30/04 18:40'.
R. Beard 62.5
6398
b.s(2-Chloroethyl)ether ND..
ug/l
10.0
i.
3/30/04 18:40 :.
R. Beard 625
6398
bis(2-Chloroisopropyl)ether ND
ug/l
i0.0
1
3'30/04, 18:40
R. Beard 625
6398
2-Chloronaphthalene ND
ug/l
10,0
1
3/30/04 18:48
R. Beard 625
6398
2-Chloro-chenol ND
ug/'l
10.0
1
3/30/04 18:40
R. Beard 625
6398
4-Chlorophenylphenylet er ND
ug/l
10.0
1
3/30/04 18:40
R. Beard 625
6398
Chrysene ND
Ila/l
10.0
1
3'`30/04 18:40
R. Beard 625
6398
D benz(a,hyanchracene NDug/1
10.0
1
3/30/04 18:40
R. Beard 625
6398
1,2-Dichlorobenzene ND
ug/l
10.0
1
3/30/04 18:40
R. Beard 625
6398
1.3 Dichlcrobenzene.. ND
ug/l
10,0
1
3/30/04 78:40
R. Beard 625
6a9e
Sample report continued . .
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ANALYTICAL TESTING CORPORATION
2960 Fos i i : K C
R E 16 1 I'Vo N 1) R k
- N A S I i i I t, 1, 1, TE V\ 1,'S ,, 1,,, 1;
3 7 2 () 4
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F,\x
ANALYTICAL
REPORT
Laboratory Number:
04-A42959
Sample ID: PMW-6
Project:
4032080-01
Page 2
Report
Dil
Analysis
Analysis
Analyte
Result
Units
Limit
Factor Date
Time
Analyst
Method
Batch
------------------------
1,4-Dichlorobenzene
-----------
ND
------
ug/1
------
100
------
1
--------
3/30/04
18:40
----------
R.
Beard
---------
625
6398
3,31-Dichlorobenzidine
ND
Uq/1
10.0
2,
3/30/04
2 8 : 4 0
R.
Beard
625
6398
2,4-Dichlorophenol
ND
ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
Diethylphthalate
ND
ug/l
10.0
I
3/30/04
18:40
R.
Beard
625
6398
2,4-Dimethylphenol
ND
ug/l
10,0
1
3/30/04
18:40
R.
Beard
625
6398
Dimethylphthalate
ND
uq/1
10,0
1
3/30/04
18:40
R.
Beard
625
6398
Di-n-butylphthalate
ND
ug/1
10.0
1
31/30/04
18:40::.R.
Beard
625
6398
2.4-Dinitrophenol
ND
Ug/1
10,0
1
3/30/04
18:40
R.
Beard
625
6398
2,41-dinitrotoluene
ND
ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
2,6-Dinitrotoluene
ND
Ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
Di-n-octylphthalate
ND
Ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
1,2-Diphenylhydrazine
ND
ug/1
10,0
2
3/30/04
18:40
R.
Beard
625
6398
Fluoranthene
ND
Ug/1
1010
1
3/30/04
18:40
R.
Beard
625
6398
Fluorene
ND
Ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
Hexachlorobenzene
ND
uq/1
10,0
1
3/30/04
18:40
R.
Beard
625
6398
Hexachlorobutadiene
ND
Uq/1
10.0
1
3/30/04
18:40
R.
Beard
62-55
6396
Hexachlorocycaopentadiene
ND
Ug/1
10,0
1
3/30/04
18:40
R.
Beard
625
6298
Hexachloroethane
ND
ug/i
10.0
1
3/30/04
18:40
R.
Beard
625
6398
1ndeno(1,2,3-cd)pyrene
ND
ug/a
10 Q
1
3/30/04
18:40
R.
Beard
625
6398
Tsophorone
ND
Ug/l
10.0
1
3/30/04
18:40
R.
Beard
625
6398
.2-Methyl--4,6-dinitrophencl
ND
Ug/1
10,0
1
3/30/04
18:40
R.
Beard
625
6398
Naphthalene
ND
Ug/1
1o.0
1
3/30/04
3.8:40
R.
Beard
625
6398
Nitrobenzene
ND
Uq11
10.0
1
3/30/04
18:40
R.
Beard
C25
6398
2-Nitrophenol
ND
Ug/1
10,0
1
3/30/04
18:40
R.
Beard
625
6298
4-Nitrophenol
ND
Ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
N-nitrosodi-n-propylamine
ND
ug/1
10.0
2
3/30/04
18:40
R.
Beard
625
6398
N-nitrosodiphenylamine
ND
Ug/1
10.0
1,
3/30/04
18:40
R.
Beard
625
f,398
N-nitrosodimethylamine
NI)
ug/l
10,0
1
3/30/04
18:40
R.
Beard
625
6398
Pentachlorophenol
ND
Ug/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
Phenanthrene
ND
ug/1
10.0
1
3/30/04
18t40
R.
Beard
625
6398
Phenol
ND
u9/1
10.0
1
3/30/04
18:40
R.
Beard
625
6398
pyrene
ND
Ug/i
10.0
1
3/30/04
18,40
R.
Beard
625
6398
Bis(2-ethylhexyl)phthalate
ND
Uq/1
i0.0
1
3/20/04
18 : 4 0
R
Beard
625
6398
1,2,4-Trichlorobenzene
NI)
ug/l
10:0
1
3/30/04
18z40
R
Beard
625
6398
2,4,6-Tr"'chlorophenol
ND
ug/1
10,0
1
3/30/04
18:40
R
Beard
625
6398
Sample report continued
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TestAmerica Analytical Testing Corporation
I TestAmerica
Drilling
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Air Emission
Corporation

Testl �mer ica
ANALYTICAL TESTING CORPORATION
2960 Fosr,r:k, Dki�r - V\snn,i,t_ 37204
800-765-0980
615-726-3404 FAX
ANALYTICAL REPORT
Laboratory Number: 04-A42959
Sample ID: PMW-6
Project: 4032080-01
Page 3
------------ I -------- --------------------
Sample Extraction Data
------------ ---------- - ------------------ --------------------------
Wt/Vol
Parameter Extracted Extract Vol. Date Time
---------------- --------- ----------- --------
Analyst Method
---------- ------
625 1000 ml
1, ml 3/2S/04
K. Turner 625
Surrogate
-------------
% Recovery
----------
Target Range
------------
su-r-Nitrobenzene-d5
85,
12. 135.
surr-2-Fluorobiphenyl
90,
14, 132,
surr-Terphenyl di-4
Bi.
12., 142,
surr-Phenol d5
14,
5, 79,
surr-2-Fluorophenol
12,
5. 99.
surr-2,4,6-Tribromaphenol
4S.
7, 155.
LABORATORY COMMENTS:
ND = Not detected at
the report limit.
B = Analyte was detected in the method
blank.
J Estimated Value
below Report Limit.
E = Estimated Value
above the calibration
limit of the instrument
# = Recovery outside Laboratory historical or method prescribed limits.
No TIC's detected by GC/MS method 625.
End of Sample Report.
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Tesu'�merica
ANALYTICAL TESTING CORPORATION
2960 Fo rt;u Cvt;i(arir,,,, [iw • ti 4frtrr.r.r., I"t si,r 3720
ANALYTICAL
REPORT
SHIELD ;ENGINEERING,
INC.
2138
Lab Number:
04 -A4 2 9 0
GIL ROWLAND
Sample ID: PMW- 9
4301 TAGGART CREEK
RD.
Sample Type:
Water
CHARLOTTE, NC 28 08- 483
Site ID:
Date Collected:
3/22/04
Project. 4032080-01
Time Collected:
1 :20
Project Name: EMC-CURTIS
OIL CO
Hate Received:
3/'24/04
Sampler: DH/ML
Time Received:
9:20'
Page.: 1
Report
DIl
Analysis Analysis
Ana'yte
Result
Un9ts
%.unit
Factor
Date T;me
Analyst method
Hatch
*EXTRAC7'ABLE ?R+DANSCS"
Acenaphthene
ND
ug/l
i0.0
1
3/31/04 15:05
R. beard 625
6398
Acenaphthy]ene
ND
ug/l
1010
1
3/31/04 _:05
R. Beard 625
6398
Anthracene
ND
u 1
gl
a0.
1
*(3Itf04 15:05
R. bearrx 625
639
R,.erzwdire
ND
Uq/2
10.0
1
3I31/09 15;L5
R. Beard 625
6398
3enzo(a)ant.hrace.ne
ND
u9/1
10.0
1
3/31"04 5: 05
R, Beard 625
6398
Henze (a)pyrene
ND
ug/7
10, 0
1
3/31/04 E : 05
R, Beard 625
6?98
5tenzo(b) fluoranthene
ND
ug/l
t1.0
:.
3/ 31 /04 5. C5
R. Beard 625
6398
benco(g,h_i)perylene
ND
ug/1
i0lo
1
3/ '/L4
R. beard 625
6398
Benzo tkt:L-," oranthene
ND
U"q/.1
10,0
1.
� ..
J �.'.1' (}L y_.: i�J
R. Beard Aj:2 ?'
8
s�°iv 96
4-Bromopnenylphenylei:ter
.ND
ug/!
1.1,0
1
3./31/C4... ;5!05
R,, Beard 625
6398
9utylbenzy1phth lal.e
ND
ug/l
io7 o
1
2`,/04 .1e .05
R, Beard 625
6396
4-Chloro-3-methylphenol,
STD
Ug/1
1
37/04 15 L
3/.
R. Beard 625
6398
bas". Ch oroerhuxy^ methane
ND
"la/1
10,0
l
3/31/04 15
R. Heard 625
6398
bws(2 Chloroethl?)e
NND
:_,�� rR'"
- U 0
�
3 .! wt 1Dy... ,.�:,',5
-
R. b`e3T"d c�5
6a98
his(2-Ch1oroiscprczpy1):ether
ND
ug/1
10,0
1
3/31/04 25:05
R. beard 625
6398
2-Chloronaphthalene
ND
Ug/1
30,0
1
3'31,'04 15:05
R. Beard 625
6398
2-Chloro henol
ND
ug/l
1,0:0
i
3/31/04 15:05
R. beard 625
6398
4-Chlorophenylphenylether
ND
ug/l
10.0
1
3/31/04 15:C5
R. Beard 625
6398
Chrysene
NB
ug/1
c)l 00
1
3/3.1/04 1,= 05
R. beard 625
6398
DibLnz (o:,h) anthracene
ND
ug/1
1.0.0
1
3/3=/04. 15.05
R. beard 6:25
6398
1,2-Dichlorobenzene
ND
ug/l.
14.0
1
3/31/04 15:05
R. Sward 625
6398
11,3-Dichlorobenzene
ND
ug/1
10.0
1
3/31/04 6:05
R. Beard 625
6398
Sample report continued
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Air Emission Corporation

TestA,merica
ANALYTICAL TESTING CORPORATION
2960 FosrrP, 0a,,w1!'io,,\ Dokti
- Vksijvio,iL,
3720
800-765-0980
1
(315-726-3401 FAX
ANALYTICAL REPORT
Laboratory
Number:
04-A42960
Sample ID:
PMW-9
Project:
4032080-01
Page 2
Report
Dil
Analysis
Analysis
Analyte
-----------------
Result
---------
Units
- - ------
Limit
Factor Date
Time
Analyst
Method
Batch
4 - Di chlorobenzene
ND
ug/l
100
------
1
--------
3/31/04
---
15:05
---
R.
Beard
- ---------
625
-----
6398
3,3—Dichlorobenzidine
ND
cg/l
1-0,0
1
3/31/04
15:05
R.
Beard
625
6398
2,4-Dichlorophenol
ND
Ug/l
10,0
1
3/.11/04
15:05
R,
Beard
625
6398
Dierhylphthalate
ND
Ug/l
10.0
i
3/31/04
15:05
R.
Beard
625
6398
2.4-Dimethylphenol
ND
Ug/l
io.o
1
3/32/04
15:05
R.
Beard
625
6398
Dimethylphthalate
ND
ug/1
ic,o
3/31/04
15;05
R,
Beard
625
6398
D-4-n-butylphthalate
ND
tg/l
i0,0
1
3/31/04
15:05
R.
Beard
625
6398
2,4-DiniLrophenoi
ND
Ug/i
i0.0
i
3/31/04
15:05
R.
Beard
625
6398
2,4-diriltrotoluene,
ND
ug/i
10.0
1
3/31/04
15:05
R.
Beard
625
6398
2,6-Dinitrotoluene
ND
Uq/1
1010
1
3/31/04
15:05
R.
Beard
625
6396
ld-n-oatylphthalaLe
ND
JLT/I
10.0
1
3/31/04
15:05
R.
Beard
625
6398
!,2-Diphenylhydrazine
ND
Ug/1
10.0
1
3/31/04
15:05
R.
Beard
625
6398
Fluoranthene
ND
ug/1
1010
1
3/31/04
15:05
R.
Beard
625
6-198
Fluorene
ND
Ug/1
10.0
1
3/31/04
15:05
R,
Beard
625
6398
Hexachlorobenzene
ND
uq/1
10.0
I
3/3I/04
15:05
R.
Beard
625
6398
Hexachlorobutadiene
ND
uq/l
io,o
1
3/31/04
15:0S
R.
Beard
625
6398
Hexachlorocyclopent-ad-liene
ND
ug"!
10.0
1
3/31/04
15:05
R.
Beard
625
6398
Hexachlorcathane
ND
Ua/1
10,0
1
3/31/04
15.05
R.
Beard
625
6398
7ndenof1,2,3-cd)pyrene
DID
ug/l
10.0
1
3/311'/04
15:05
R.
Beard
625
6398
Isophor-one
ND
Ug/1
1010
1
3/31/04
15:05
R.
Beard
625
6398
2-Methyl-4,6-dinitrophano,
ND
ug/l
10.0
1
3/31/04
15:05
R.
Beard
625
6398
Naphtualene
ND
Ug/1
10 0
i
3 ' 131/04
35:05
R.
Beard
625
6398
N-,trobenzene
NID
uq/1
10.0
1
3/3311/04
25:05
R.
Beard
625
6398
2 -Nitrophenol
ND
Ug/1
10.6.
1
3/31/04
15:05
R.
Beard
626
6398
4-Nitropheno1
ND
.kg/1
1
3/31/04
15:05
R.
Beard
625
6398
N-nitrosodi-n-propylam,.ne
ND
Ug/l
1D.0
1
3/31/04
1505
R.
Beard
625
6398
N-ni trosodipheryl amine
ND
uq/1
io,o
1
3/31/04
15:05
R.
Beard
625
6398
N-ni-Irosodimethylamine
ND
1,19/1
10,0
1
3/31/04
15:05
R.
Beard
625
6298
Pentachloropheno!
ND
ug"ll
io,o
1
3/31/04
15:05
R.
Beard
625
6398
Phenanthrene
ND
Ug/l
i0,0
1
3/31/04
15:05
R.
Beard
625
6398
Phenol
ND
Ug/l
io'D
i
3/31-/04
15_05
R.
Beard
625
6398
Pyrene
ND
10.0
1
3/31/04
15:05
R.
Beard
625
Bis(2-ethy1hexyl)phthalate
ND
Ug/l
20.0
1
3/31/04
15:05
R.
Beard
625
6398
1,2,4-Trichlorobanzene
ND
uq/1
10.0
1
3/31/04...15:05
R.
Beard
625
6398
2,4.6-Trichlorophenal
ND
ug/l
10,0
1
3/31/04
15:05
R.
Beard
625
6398
Sample report continued
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TestAmerica Analytical Testing Corpolation
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Emission
Corporation

Testi�merica
ANALYTICAL TESTING: CORPORATION
2960 Foci ir. Ghnttn#ro'% i mt; • Vasmmu,. Ir:3vt.ssr.r 37209
800-765-0980 - 615-726-3404 FAx
ANALYTICAL REPORT
Laboratory Number: 04-A42960
Sample I7: PMW-
roject. 4032080-01
Page
Sample Extraction Data
Wt/'Vol
Parameter Extracted Extract Vol Date Time Analyst Method
625 1000 ml' 1. nil 3/25/04 K. Turner 625
Surrogate r Recovery Target range
Burr-Nitrcrbenzene-d.5 66. 12. - 135.
suer-2-177uorobiphenyl 6824. - 132.
surr-Terphenyl c'14 8, 11, 142.
Burr -Phenol d5 20. 5" - 75.
surr-2-F'uo.-ophenol 15. 5. - 99.
suer-2,4',6-Tribromophenol. 29. 7, - 155.
LABORATORY CO NTE ;
ND - Not detected at the report limit.
B ='Analyte was detected in the method blank.
J = Estimated Value below Report Limit..
B = Estimated Value above the calibration limit of the instrument.
## = Recovery outside Laboratory historical or method prescribed limits.
No 'SIC' s', detected by CC/MS method 625.
End of Sample Report,
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Test rnerica>Analytical Testing Corporation l TestArnerica Drilling Corporation I TestArnerica Air Emission. Corporation

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 I`oi irik Cr,,v t;tf w. Dwi t'
* 37204
ANALYTICAL
REPORT
SHIELD ENGINEERING, INC.
2138
Lab Number:
04-A429 1
GIL., ROWLAND
Sample ID: FMW-10
4301 TAGGART CREEK RD.
Sample e:
Water
CHARLOTTE, NC 28208- 483
Site ID:
Late Collected:
2/04
Project: 4032080-01
Time Collected:
16.25
Project Name: EMC-CURTIS
COIL COmate
Received:
3 24/04
Sampler. DH/ML
Time Received:
9:20'
Page: 1
Report"
Dil
Analysis Ana.iy5is
A> -:La Result:
------------
Unt .ts
Limit
Factor
Dave Time
Analyst Method
Batch.
-EXTRACTABLE ORGANICS'
Acenaphthene ND
Ug/1
1010
2
3/30/04 19.54
R. Beard 625
6398
Acenaphthylene ND
ug/l
10.0
1
3/30/04 19:54
Ra Beard 625
6398
Anthracene ED
uq,'!
10.0
1
3/30/04 19.54
R. Beard 625
6398
enzadine 10
ug"l
100
1
3/30/04 19: 4
RBeard 625
C398
Benz_'la)anthracene ED
Ug/I
10,0 ..
1
1'.30/04 19:54 ..
R. Beard 625
6398
Benzo(aipy'rene ,. ND
ug/1.
100
1
3.1.30/04..1.9:54
R. Beard 625
6398
Benzctb?fluoran^hene ND
rig/1
i0.0
1
3/30/04 -19i54
R. Beard 625
6398
Renzo(g,h,i)perl,lene ND
ug/1
oGo
1
3/30/04 .9:54
R. Beard 625
6398
enzo (k; T luuraothene Nil
"19/.1
i0.0
1
3� 30/04 .:19:54
IZ, Beard 625
6398
4:-Bromophenylphenylether ED
lag/.1
10.0 ...
1
:3/30/04 :1.9:54
s3, Beard 625
E398
Butylhenzy1phthalate ND
Uc3/1
10,0
3/30/04 19:54
R, Beard 625
6398
4'-Chioro<-3-merhylphenol ND
uq/1.
10.4
3730r Ci4 :7:il4:..
R. Beard 625
6395
b .s(2-Chloroethrxy)methane ND
ug/l
30.0
1
3/30/04 '15.:,4
Rc Beard 625
6398
b1s(2-Chloroethyl)ether ND
ugll
10.0
1
3/3C,/04 19:54
R. Beard 625
6398
b S(2-Ch?Fcro sogropy,I)ether ND
ug,61
1.0.0
1.
3/30/04 19:54
R. Beard 625
6398
`'-Chlcroraphthalene ND
1wg/l
i0.0
1
3/30/04 19:54
R. Beard 625
6398
2-Chlorophenol NE)
u9/l.
10,0
1
3'30/04 19:54
R. Beard 625
6398
4-Chloro henylphenyletxer ND
ug/1
10.0
1,
3/ 0/04 19:54 -
12. Beard 625
6398
Chrysene; ND
U9/1
10,0
1
3r3n,104 19.54
R. Beard 625
6398
D benz(a,n)anthracene Nb
U9/1
1.0.0
1
3/30/04 19:54
R. Beard 625
6398
1 2-Dlchlcrcbmenzene ND
ug';'l
it.6
1
3/30/04 19:54
R. Beard 625
6398.
_.,
' 3-Dichlorobenz.ene ND
U �'1
g,
10,0
r
:1 9 , 54
31.,3�� C74 �._ �:?
"S Be
S.. �.a.Y`d 6uS
a
6?„r3
Sample report continued ,
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TestAmeriea Analytical Testing Corporation
I TestArnerica Drilling Corporation i TeskAmer ca Air Emission Corporation

Testj,.�merica
ANALYTICAL TESTING CORPORATION
- 29.60 ['"it49 FR CW1,I6II`TON fkiu • Nvsn%i1!f. t'ENAESSV1 3720-1
800-765-0980 - 61 a_726-3 0.4 F%x
ANNALYTXCAL REPORT
Laboratory Number:
04-,A.42961
Sample III.
PMW-10
Project:
4 3208
--01
Page
Reports
Dil
Analysis
Analysis
Analyt.e
Result
Units
Limit
Factor Date
Time
Analyst
Method
Sat.ch
1,4-Dichl.urobenzene:
LID
ug/.1
10.0
1
3/30/04
19:5*1....
R, Beard
625
6398
3;,3' D hl�arobenzidine
ND
ug/1
10,0
1
3.'30/04
19:54
R. Beard
625
6398
2,4-Dichloropheno!
ND
ug/1
10»0
1
3/30/04
19:54
R. Beard
625
6398
D:ethylphthaiate
ND
ug/1
10,0
1
3;/30/04
19.54
R. Beard
625
6398
2,4-Dimethylphenol
ND
ug/:1
16.6
1
3/30/04
19.54
R» Beard
625
(1398
Dimethylphthalate
ND
ug/1
100
].
3/30/04
19.54
R» Beard
625
6398
Di-n-butylphthalate
ND
ug/1
107 0
1
3/30/04
-19;54
R. Beard
625
6398
2.4-Dinacroohenol
ND
Ug/1
1010
1
1/30/04
19:54
R. Beard
625
6398
2,4-dini`trctoluene
ND
ug/l
1010
1
3/30/04
19:54
R, Heard
625
639+5
2,6-Dinitrotoluene
ND
ui/1
10,0
1
3/30/04
19c54
R, Beard
625
6398
Di-n-crtylphtna'late
:ND
ua/1
10,0
i
3/30/04..
15:54
R. Beard
F,25
6398
1,2-Diphenylhydrazine
ND
n9/;1
10.0
7
3/30/04
i9.54
R. Beard
625
6398
xluoranthene
ND
Ug/1
10,0
1
3;30/04
19:54
R. Beard
625
6398
Fluorene
ND
119/1
10.0
1
3/30/04
:: 19:54 :
R. Beard
625
6398
Bexachloroberzdne
ND
1;g11
107 0
1
3/30/04
19:54
R. Beard
625
6398
H'exaehlorobutadiene
ND
ug/1
10.0
1
3`30/04
19.54
R. Beard
625
6398
Pexachlorocy lopen adiene
N;:
Ug/l
10.0
1
3/30/04
19:54
R. Beard
625
(398
H:exachloroethane
lei`
ug/3
10,0
1
3/30/04
i9:54
R, Beard
625
6398
lndenot ,2,3-cd)pyrene
ND
ug/1
l2.0
i
3/30/04
19:54
R. Beard
625
6398
Ssophorone
ND
ugfl
10,0
1
3/30/04
193 5.4
R, Beard
625
6398
2:Methyl:-4,6-diritrophenol
ND
cagf..I
10.0
1
3,/30/04
. 19:54
R. Beard
625
6398
Naphthalene
ND
ug:/1
10. 0
1
3/30/04
19:54
R. Beard
625
6398;
Nitrobenzene
IUD
uc/2
100
1
3/-,0,104 :.
19:54
R. Beard
625
6398
2-Nitrophenci
ND
ug/l'..
10,0
1
3/30/04
1954
R. Beard
62s
6398
4-Nitrop.henol
ND
ug/1
20.0
1
3/30/04
-19:54
R. Beard
625
6398
N-nitrrsodi-n.-propylamine
ND :
ug/1
2010.
i
3/30/04
19:54.
R. Beard
625
6398
N-nitresodiphenyl.emirs
ND
Ug/1
:.ta».C°
1: -
3d30/04
1S�:54
R. Beard
625
6398
N:-nitrosodimethylamine-..
ND -
ug:l
10.0
1
3/30/04:.:19:54
R. Beard
6625
6398
Pentachl5rophenol
TAD
Ug/1
"1.0.0
1
3/30/04
19:54..
R. Beard
6.25
6398
Phenanthiene
ND
ug/l
3i.
1
3/36,/04
:9:54:
R» Beard
625
6398
Phenol
ND
gig/'l
10,0
1
3/30/04
19:54
R. Beard
625
6398
Pyr'ene
ND
ug/1
.i3,1
1..
3/30/04
29:54":
R, Beard
625
6398
Bis(2-ethy1hexyl)phthalate
ND
uq/,l
10,0
1
3/30/04
19.54
R. Beard
625
6398
2;2,4-Trachlorobenzene
ND
ug/2
10.0.
1
3/30/04
19:54'
R, Beard
625
6398
2,4,6-Trichlorophenol
ND
Ueg l
i0,tt
l
3/30/04
29:54-
R. Beard
625
639,8
Sample report- continued ,
www.testomericainc.com
TestArnerica Analytical Testing Corporation
! TestArmerica Drilling
Corporation 1 TesiAmerica
Air Emission Corporation

29(�() FOSIER CREBMWN DRM: -
800-765-0980 - 61
ANALYTICAL REPORT
Laboratory Number: 04-A42962
Sample ID: PMW-10
Project: 4032080-01
Page 3
---------------------------
e Extract -ion Data
--.—
--------------- - ------- ------- ------
Wt/Vol
eter Extracted Extract Vol
Date
Time
- -----
Analyst Method
---------- ---
1000 M1 I. M1
3/25/04
K, Turner 625
rogat--e
< Recovery
Target Range
r-Nl'trobenzene-d5
67,.
12, 1-35,
r-2-F2uorobiphenyl
69,
14132,
r-Terphenyl d14
65.
71, 142
r-Phenol d5
13.
51
r-2-Fluorophenol
14,
5: 99,
r-2,4,6-Tribromophenol
44,
7, 155,
LABORATORY CO, ENTS:
ND = Not detected at the
report
limit.
B Analyte was detected
in the
method
blank.
J = Estimated Value below
Report
Limit.
# = Recovery outside Laboratory historical or method prescribed limits.
No TIC's detected by GC MS method 625.
id of Sample Report.
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TestAmerica Anolytical Testing Corporation I TestArrierica Drilling Corporation 1 'restAmerico Air Emission Corporation

Testi�merica
ANALYTICAL TESTING CORPORATION "
._ 2960 llos'lvp, is l.ri,#ilta\ ii3iti6s`. * 4filitlL4.i„ `P�:��F.,atd. 37203.
800- 65-0980 615-726-3404 F\x
ANALYTICAL REPORT
SHIELD ENGINEERING, INC. 2138
Lab Number: 94-A42 62
GIL ROWLAND
Sample ID A - 3
4301 TA GART CREEK RD.
Sample 'Type: Soil
CHARLOTTE, NC 2829 - 483
Site ID:
Date Collected: 3/22/04
Project. 4032080-01
Time Collected: '10:12
Project Name: E C-CURTIS OIZ. CO
Date Received: 3/24/04
Sampler. EN/ML
Time Received: 9:20
Page: 1.:
Report
Lit Analysis Pnalyss.s
Analy*e Result Units Limit
Factor Date Time AnalystMethod Batch
-GENERAL CHEMISTRY PARAMETERS*
Dry Weight 78,4
1 3/24 04 1040 S.R1ett CLP 1493
*ORGANIC PARAMETERS*
T:PH IEate,sel :Range) Sl mg/kg 5,06
I 3/26/04 15.02 M.Ja..rret. 8015.H 4340
SaCCiple Extraction Data
wt /vol
Parameter Extracted Fxt:.act Vol Late Time
Analyst Method
E` HIEPC 25.2 mn I . a m1 3:I25/04
F , r T
xr: net 3550'
Surrogate % Recovery
ia3"uct Range
TPH Hi Surr., o-Terphenyl 97,
35, - 13E.
Sample report continued . .
WWW.iestC9me
icoi c.corn
TestAmericss Analytical Testing Corporation' I TestAmerica Drilling
Corporation 1 Test,Amer ca Air Emission Corporotion

TestAmeriaca
ANALYTICAL TESTING CORPORATION
2960 Fosriik CRi,:w1rro\ Dwr.- -
800-765-0980 - 61
ANALYTICAL REPORT
LABORATORY COMMENTS:
ND = Not detected at the report limit,
B =Analyte was detected in the method b]
J Estimated Value below Report Limit.
E = Estimated Value above the calibratior
# = Recovery outside Laboratory historicz
i,i, Tr Nm,;,,si,,r :37204
3404 FiN
raboratory Number: 04-A,42962
Ample Its: A-3
Iroject: 4032080-01
,age 2
tit of the instrument.
method prescribed limits.
The TRPH-Diesel MS/MSD were not reported due to the matrix of the sample spiked.
End of Sample Report.
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TestArnerico Analytical Testing Corporation I TestArnerico Drilling Corporation I TesfAmerico Air Emission Corporation

TestAmerica
A tALYTtCAE TESTING CORPOPATCCS
2960 fees vk, 37201
800-765-0980 is 15-726-3 0 i Fi
ANALYTICAL REPORT
SHIELD ENGINEERING, INC. 2138
Lab Number: 04-A42963
GIL ROWLAND
Sample ID: B-1
01 TAGG.ART CREEK RTC.
Sample Type: Soil
CHARLOTTE, NC 82 - 46Site
ID:
Date Collected:' 3/2 /04
Project: 032080-01
Time Collected: 11. m 1
Project Name: EMC-CURTIS OIL CO
Late Received: 3,24/04
Sampler. DH/ML
Time Received: 9.20
Page
:Report
Dil Analysis Asia'yswa
Analyze Result Units Lindt
Factor Date: Time Analyst Method batch
- ENERAL: CHEMISTRY PARAMETERS-
$: Dry Weight 83.9 a
I 3/t4/04 10 40 _.,;sett ClIp :1493
*ORGAN-TC PARAMETERS^
TPH (Diesel Range) 1130 mg/kg 47.1
att / 7/04 9:33 M.iarrett 8015R 4340
Sample Extraction --Da--a
ist/vol
Parameter Extracted Extract. Vol Date Time Analyst Method
EPHIDR„ 25.3 gm.. 1.0 m`i 3;.;E5/04:. R,
Turner 3550
LABORATORY COMMENTS:
ND = Not detected at the report limit.
R _ Analyte was detected: in the method blank.
J Estimated Value below Report Limit.
E =-Estimated Value above the calibration
limit of the instrument.
4 = Recovery outside Laboratory historical
or method prescribed limits.
All reported results for metals or Organic
analyses have been corrected for dry weight.
The TRR -Dies l surrogate was diluted out
due to sample matrix.
End of Sample Report.
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TestAmericss Analytical Testing Corporation I TestAmerica Drilling Corporation I TestArnerica Air Emission Corporation

A011&
*501 L
TECHNOLOGIES, INC.
January 31, 2004
Certificate of Acceptance
Soil Technologies, Inc. (STI), a it remediation fkcility located in
Lattimore, No Carolina. Accepted the following amount of Non -hazardous, Petroleum
Contaminated Soil on the following Date(s):
Amount of Soi I : 12.56 Tons
Date(s) Received: January 7, 2004
Type of Contamination: Gas / Diesel
STI Job Number: 711
The Soil was rectivod from the following location:
Curtis Oil Company
7401 Old W Holly Road
Charlote, NC
The it will be processed and remediated in compliance with all
applicable rules and rcgluation seA forth by:
1) NORTH CAROLINA DEPARTMENT OF ENVIRONMENT,
AND NATURAL RESOURCES (NCDENR)
2) THE FACILITY PERMIT
3) THE STATE AUTHORITIES
4) AND ANY LOCAL LAWS AND ORDINANCES
947 CrQ*dcr PjA4
Sholby, NC 28150
Offioe/Fax [phone]
Mobile [phone]
N�cxtrl Mo 150* 156669* 1
EmAW

SOIL
Site A ddress, 947 Crowder Road
Shelby, North, Carolina 28150
TECHNOLOGIES, INC.Mailing Address, past Oh�ce Box 62
Lattimore, North Carolina
280 -006
Phone [phone] 'Office i Fax [phone]
CONTAMINATED SOIL
PETROLEUM CONTAMINATED SOI L. MANIFEST
S.T.E. Job Ala. �
Manifest No. �
Type of Contamination �i tn6Q, Cause of Release
Contractor Information'.
Teipht�ne N i
Generator Information* 'a N--s
C
Telephone No,
Transporter Information!
Telephone No.
READ REVERSE BEFORE tt
06 t il
Driver's Signature � Truck Rln
"Driver's sIgnature acknowledges that driver s read the terms arlI and/taons can the verse side of this pace and thar the
driver fully understands and agrees to be bound by therrrM
Date,Ti me Weighed:
Weigh Master Signature -
Gross Weigh Tare Weight &
Net Weight 2. L> quiv.Tons
Inspected & Acce ed y: SOIL TE' NOLOGIES, INC,
Cite:
NOTICE TO TRUCKER:
TRUCKS ILL. NOT BE PERMITTEDT FACILITY
WITHOUT A MANIFEST
White and Yellow copies of this form must be left at SOIL TECHNOLOGIES, INC.
White -Billing Green -Generator Canary -Trucker

,A %" Achael F. v r } William G. Ross Jr
, Secretary
North Carolina D'eparunent ofEnvironment and Natural Resources
l W, Klimek,
—� ie T', E. Director
IF —
Division of Water Quality
ColH. Sullins, DeputyDirector
Division of Water Quality
June 22, 2004
xrxx. a,..ae.a a„�axa. axy, karuarxuaxvxxex a....axe;saxcasa„a'
TransMontaigne Terininaling, Inc.
1AAVf44-0-1
,a.0 vv
Roswell, Georgia 30076
SUBJECT- Compliance l�Yxalu " ti�art lr6pection
TransMontaigne GWRS
Southeast Terminal, 7401 Old Mt. Holly Rd.
ICES Permit No. ? C G51 000
Certificate of Coverage No NC510006
Mecklenburg County, C
Dear r'l. Castleberry:
On May 28, 2004, Mr. David Rimer of the Mecklenburg County Water Quality Program
MCt'4 QP) conducted an inspection at the subject facility. inspection conducted a part
of a cooperative working agreement between Mecklenburg County d the Division of Water
Quality. The enclosed report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not
hesitate to call.. Mr. Richard Bridgeman or me at this Office.
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Enclosure ` K
cc: Rusty Rozzelle, MC WQP
G/dir
Fite: WCQ TmnsMontailme5l0006.504.doc
ruin
[phone] usservice
1-8 7-6 3-6 4

United Mates Environmental Protection Agency, Washington, DC -20460
Form Approved
Y NPI.DES Compliance Inspection Report , « OMB No. 2040-0003
North Carolina Department of Environment and.. Natural Resources
,Approval Expires
*, Division of Water Quality, Mooresville Regional Office CDE R. 7/31/85
Section A: National Data stem +Colin
Transaction Code NPDES Permit No. 1 O/DAY Inspection Type
Inspector Facility I ype
N 5 N 5100 6 04115128
C 2
Remarks:
Inspector: Mecklenburg Go-tyWater ualzty'
Inspection Work Days Facility Self-TNIonitoring Evaluation Rating BI QA
........... Reserved ............ €
4 3 N N
Section B: Facility Data
Name and Location of Facility Inspected: Entry Time:
Permit Effective mate:
TransMontacgne GWRS 1:30 PM
October 1, 2001
Southeast Terminal Exit Time:
7401 Old NIt. Holly Rd. 2:20 Pivl
Permit Expiration Date:
Mecklenburg County, NC Date:
September 30, 2406
Ma IQ 1AAA
Na e(s) of On -Site Representatives Title(s)-Phone No(s):
Mr. Keith Lewis, OR , (704) 39Pa3 371
E
! Name and Address of Responsible Official: Title:
Ms; Barbara Castleberry Environmental Coordinator
TraTrnsMontign
Mansell Court East, Suite 6{l Phone No.
Geonzia 30076 (r 0) 518-a671
o
:!C!outacted?Roswell,
Section C:
Areas :Evaluated ;Dunn Ins eetion
Pe t` Flowrleas < einent C Aerations &Maintenance
Sewer t3uerflow
j Z ecords/Reports Z Sell" -Monitoring Program [I Sludge Handling/Disposal
IEl
El Pollution Prevention
Facility;Site Review ] Compliance Schedules El Pretreatment Program
El Multimedia
Z Effluent/Receiving Waters Z Laborato 0 Stormwater
[-1 Other:
Section D: Summary of Findings/Comments
Signature(s) of
David Rimer
Signature of R{
EPA Form 3560-:
d satisfactory unless otherwise indicated. See: attached sheet(s) for summary.
n pector(s): Agency/Office/Telephone: Date:
MCWQPf(704) 336-5500 June 3, 2004
(fewer: : Agency/Office Date:
(Revised - ) Previous Editions are Obsolete

GENERAJU
The facility was last inspected on March 20, 2004 by the Mecklenburg County Water
Quality Program (MCWt P). A Compliance Evaluation Inspection Report was issued. on April
1 , 2003.
PERMIT:
The NPDES treatment works for the subject facility consist of a groundwater remediation
system with two oil/water separators in series, an air stripping system, two particulate filters in
series, two carbon filters in series, and a holding tank.
The facility operates under General Pe it No. NCG51 0000, Certificate of Coverage No.
NC510006. The permit became effective on October 1, 2001 and expires on September 30,
2006. The permit authorizes the discharge of treated petroleum contaminated groundwater.
The permit properly describes the facility and appears adequate for the wastewater.
The facility is not required to submit Discharge Monitoring Deports (D?v1 s) under the
terms of .the current permit. _ As the system not been operating since June 2000, there are no
laboratory analytical reports for the current review period. The Operator in Responsible Charge
(O1C) indicated that the system is shut down while the pernuttee considers more effective/
efficient methods of treatment.
FACILITY SITE "VIEW:
The facility is engaged in fuel oil, gasoline, and kerosene storage and distribution, The
groundwater remediation system has not been operational/discharging since June 2000.
FLOW MEASUREMENT:
There has been no flaw since June 2000.
LABORATORY:
No laboratory analyses were performed during the past twelve months since there has
been no flow.

EFFLUENT/RECEIVING WATERS:
The facility is permitted to discharge to an unnamed tributary to Paw Creek, which is
classified C waters within the Catawba River Basin.
The groundwater rernediation system was not operational and the facility was not
discharging at the time of the inspection.
SELF -MONITORING PROGRAM:
o laboratory analytical reports or DMRs were available for the current review
period from May 2003 through.. April 2004, as there was no flow.
OPERATIONS & MAINTENANCE:
The facility and site appeared well maintained.

VWN A
"'C' J�Q2'(VD'? Michael F rasley, G rnor
William G. Ross, Jr.,Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
April 15, 2003
Ms. Barbara Castleberry
TransMors taigne Terminaling, Inc.
200 Mansell Court East, Suite 600
Roswell, Georgia 30076
SUBJECT: Compliance Evaluation Inspection
TransMontaigne GWRS
Southeast Terminal, 7401 Old Mt. Holly Rd.
NPDES Permit No. NCG5 10000
Certificate of Coverage No. NC510006
Mecklenburg County, NC
Dear Ms. Castleberry:
In ')AAA Mr David Rimer of the Mecklent ura County Water Quality
hesitate to call Mr. Richard Bridgeman or me at this Office.
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Enclosure
cc: Rusty Rozzelle, MCWQP
dj r
File: WQ TransMontaigne 510006.303.doc
Mooresville Regional Office, 919 North Main street, Mooresville, NC 28115
)NE [phone] Customer Service
(704", C-63-6040 1800 623-7748

110 " United Stags Environmental Protection Agency, Washington, DC; 20460
i7ES Compliance Inspection Report
" nivision of water duality, ,Mooresville Regional Office + 7/31/85
Section Ai rNational llafa §ptem Colin'
Transaction Code NPllES Permit No. MO/DAY Inspection Type Inspector Facility Type
N 5 l~C510006 03/03/20 C C 2
Remarks.
Ins ector: Mecklenburg County Water Quality
inspection Work Days Facility Self Monitoring Evaluation Rating Ill QA ....Reserved............
.5 3 N N
:: aw
}
Name and Location of Facility Inspected. Entry Time. Permit Effective Bate.
TransMontaigne GWRS2.15 PM October 1, 2001
Southeast Terminal Exit Timert
7401 Old Mt, Dolly Rd. 3.00 P Per 't E�piratia n Bate.
Mecklenburg County, NC state. September 30, 2006
March20, 2003
Name(s) of On -Site Representatives Titles) Phone No(s)
Mr. Keith Lewis, ORC, (704) 39 -3371
Name and Address of Responsible Official. Title:
Ms. Barbara Castleberry Enviromnental'Coordiator
TransMontaigne Atone No. Contacte,d*?
200 Mansell Court East, Suite 600 (770) 518- 671 No
.Roswell, Georgia 30076
„" a � ° .`a `.s,. a "ras ' s t m y, 1 1s ail ''4" a,. *Ma , �. r ' '"y,a /'Y s a< "p p�. a ,y .
,'di a�d"` 'aaa t a b a on L,+s �+' .z r" a
reas' Ali[8 ed i ilri[1„ »Iit {?CtiiJlil
Permit
. Flow Measurement Operations i Maintenancett Sewer Overflow
Records/Reports Self-MonitoringSelf-Monitoring Program Sludge Handling Disposal El Pollution Prevention
Facility Site Review E] Compliance Schedules 0 Pretreatment Program El Multimedia.
Effluent/Receiving; Waters Laboratory 0 Stor water E3 Other.
0.Y 17kr+�ti� uFc:lgsCQ
aai,
All areas are rated satisfactory unless otherwise indicated. See attached sheet(s) for scnnsx�ary.
Signature(s) of lnspector(s). Agency/Office/Telephone: late.
David Rimer MCWC P/(704) 336-5 00 March. 28, 2003
Signature of Reviewer: Agency/Office slate:
. W
EPA Form 3 60-3 (Revised 3-85) Previous Editions are Obsolete

The facility was last inspected on December
Report was issued on January 15, 2002.
PERMIT:
�O S PORTS:
001 by Mr. D. Will Autry of the
A Compliance Evaluation Inspection
ty consist of a ro' dwater remediation
nethods of treatment.
fie terminal manager maintains clear, organized records and reports.
rY SITE
process.
FLOWMEASUREMENT:
There has been no flow since June 2000.

LABORATORY:
Analysis of effluent samples is performed by Test America. Te
evaluated under this inspection.
EFFLUENT/RECEMNG "ATE
,,-Lazo cc
The
discharging
The facility and sib
on.
[:
qE:
-ed well maintained.

Michael F. Easley
Governor
William G. Ross, Jr.,Secretary
North Carolina Department of Environment and Natural Resources
5 Gregory J. Thorpe, Ph.D., Acting Director
Division of Water Quality
January 15, 2002
Ms. Barbara Castleberry
TransMontaigne
200 Mansell Court East, Suite 600
Roswell, Georgia 30076
SUBJECT: Compliance Evaluation Inspection
TransMontaigne GWRS
Southeast Terminal, 7401 Old Mt. Holly Rd.
NPDES Permit No. NCG5 10000
Certificate of Coverage No. NC510006
Mecklenburg County, NC
Dear Ms. Castleberry:
On December 18, 2001, Mr. D. Will Autry of the Mecklenburg County Department of
Environinental Protection (MCDEP) conducted an inspection at the subject facility. This
inspection was conducted as part of a cooperative working agreement between Mecklenburg
County and the Division of Water Quality. The enclosed report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not
hesitate to call Mr. Richard Bridgeman or me at this Office.
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Enclosure
cc: Rusty Rozzelle, MCDEP
DWA
File: WQ TransMontaigne 510006.doc
Customer Service Mooresville Regional Office, 919 North Main Street, Mooresville, No 28115 PHONE [phone]
1 800 623-7748 FAX [phone]

N
MENOMINEE
But
777777777--
1� In
HOftjm.!gow-
1�1111111 11111�11 1%
#...
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

GENERAL:
The facility was last inspected on April 11 2001 by Mr. Derrick Harris of the
Mecklenburg County Department of Environmental Protection (MCDEP). A Compliance
Evaluation Inspection Report was issued on April 25, 2001.
PERMIT:
The NPDES treatment works for the subject facility consist of a groundwater remediation
system with two call/water separators in series, an air stripping system, o particulate filters in
series, two carbon filters in series, and a holding tank.
The facility operates under General Permit No. NCG51 10000, Certificate of Coverage No.
NCS 10006. The permit became effective on October 1, 2001 and expires can September 30,
2006. Prior to October I, 2001, the facility was covered under General Permit No. NCi510000,
Certificate of Coverage No. NC510006, which was effective from October 1, 1996 to September
30, 2001. The permit authorizes the discharge of'treated petroleum contaminated groundwater.
The permit properly describes the facility and appears adequate for the wastewater.
RECORDS/REPORTS:
The facility is not required to submit Discharge Monitoring Reports (T MR.$) under the
terms of the current permit. As the system has not been operating since June 2000, there were no
laboratory analytical reports for the current review period. The Operator in Responsible Charge
( ) indicated that the system is shut down while the permittee considers more effective/
efficient methods oftreatment.
The terminal manager ager maintains clear, organized records and reports.
FACILITY SITEREVIEW:
The facility is engaged in fuel oil, gasoline, and kerosene storage and distribution.. The
groundwater remediation system has not been operational/discharging since June 2000. The
terminal manager indicated that a consultant is in the process of reviewing the current treatment
process.
FLOW MEASUREMENT:
There has been no flow since June 2000.
LABORATORY:
Analysis of effluent samples is performed by Test America. Test America was not
evaluated under this inspection.

G
EFFLUENDRECEIVING WATERS:
The facility is permitted to discharge to an unnamed tributary to Paw Creek, which is'a
Class C water in the Catawba River Basin.
The groundwater remediation system was not operational and the facility was not
discharging at the time of the inspection.
SELF -MONITORING PROGRAM:
I-uuv inrougn November zuui, as there was no now,
OPERATIONS & MAINTENANCE:
The facility and site appeared well maintained.

State of North Carolina
Department of Environment IT
and NatNatu rat Resources LT.IWA
Division of Water Quality A&4
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary soft
A. Preston Howard, Jr., P.Eam Director
NCDENrl
May 5, 1998
Mr. Alan Seese
BP Oil Company
Environmental Remediation Management AAY,
2555 Westside Parkway, Suite 30
C.S. #1600
Alpharetta, Georgia 3 9951
$.
mv
Subject. GW Interceptor Trench
Louis Dreyfus Energy -S.E. Terminals #4762
COC # NCG510006
Mecklenburg County
Dear Mr. S se:
This letter is in response to your March 6 , 1998 letter requesting approval of expansion
plans for the groundwater rernediation system t the subject facility. The Division has determined
that the addition of the ;groundwater interceptor trench, as outlined in submitted documentation, is
acceptable under the terms `and conditions of NPDES Wastewater Discharge General Permit
NC 51 000 and is hereby approved.
Please note that this letter does not relieve the Permittee from responsibility for compliance
with any other applicable federal, state, or local law, rule, standard, ordinance, order; judgment, or
decree.
If you have any questions, please feel free to contact Darren England at 919) 733-5083,
ext. 545.
Sincerely,
A. Preston Howard, Jr,, P. E.
cc: Mr. Jim Sligh - Louis Dreyfus Energy
Central Files
Mcldenburg Ccr ty Health l�ep eat
Stormwater and General Permits "ts Unit
P.O. Box 29535, Raleigh, North Carolina 7626-0535 Telephone [phone] FAX [phone]
n Equal opportunity Affirmative Action Employer 50% recycledt 100/o post-consu er paper

JF!crom 7onfirmation of the COC concentrations in the water and vapor effluent, transfer of liquids
_1 4
fthe interceptor trench will resume. If the laboratory analytical results demonstrate the
system is not functioning properly, adjustments will be made to the system, and the
previously outlined start-up procedure will be repeated.
'If you have any questions or comments, please do not hesitate to contact the
undersigned at [phone] or at our new address shown above.
P-' (777b) 4
Respectfully Submitted,
Alan C. Seese
Contract Engineer
On Behalf of Environmental Remediation Management
encl.- Table 1 Summary of Treatment System Influent/Effluent
Concentrations
Figure 1 Site Plan
cc w/ encl.; Jim Sligh - Louis Dreyfus Energy
cc w/o encl. - Susan Sharp - BP Atlanta
Houston Johnson - BP Atlanta
John Uteck - G&E Engineering
S
kb, 51`
r/

" x� ✓L'f?X-�4-. "C,°h'`,�.% `°. .tea.. NWpkj..,.
UNKNOWN
x*.,a I w uc-17° * O ABANDONED WELL LOCATION
RECOVERY WELL LOCATION
esa_xe 1k MONITOR WELL LOCATION
t r CS IIM7.vE_*
.a..
�w_Ss I r z w-d , wr ;14 GEOTECHNICAL IL BORING
¢ $ SOIL BORING
AW-x i I ' v«- O E III DEEP MONITORING WELL LOCATION
E x . FIRE HYDRANT
VRU VAPOR RECOVERY UNIT
»..,..✓'° Itw-, wr*s .�'-_. Taw * _..�""'at�.
w-35 b i W 45 "-50
a5F ABOVEGROUND STORAGE TANK
ww_an s 4".rsnx auaFaEC naen
.ra_xa
UST UNDERGROUND STORAGE TANK
-fir i`
t�s I ; 4{ NnPl. NON—AOUEOUS P14ASE L:IOUIDS
} 7
t w I DPV s D E VACUUM EXTRACTION SYSTEM
W.-3* Stt r kit M t„ I
Vcu VAPOR CONl8USnON UNIT
-2s uv a O/W SEP UNDERGROUND OIL/WATER SEPARATOR
PIPELINE
OVERHEAD ELECTRIC LINE
OVERHEAD TELEPHONE LINE
fi w PROPERTY LINE
CHAIN LINK FENCE
k: ar
TOP/BOTTOM OF SLOPEfBERMED AREA
fk=k `r
t :r ABOVEGROUND/UNDERGROUND DPVES
RECOVERY LINES (APPROXIMATELOCATION)
NAFL RECOVERY TRENCH
{ i E ta.ax 44: it 4) PROPERTY LINE BOUNDARIES RELATIVE TO THE SITE FEATURES
ARE APPROMMATE.
i 2) MONITOR WELL uw-48. Yw-28, ES--t« PU -4e AND Ptsww2 ARE
;r i •:.�tDENTWXD IN TWO LOCATIONS
3) MONITOR LOCATIONS ARE )OMATE. ACTUAL LOCATORS
i NAPE NOT BEEN FIELD VERIFIED.
t y 4) UTILITY LOCATIONS ARE APPROMMATE. ON-STE UTILITIES ARE NOT
SHOWN ON THIS FIGURE.
"W, %
0 feet 150
w.a. SCALE
G&E ENGINEERING'
iat/ r-2 ■
mak
RE' 1} A T. CONSULTANTS. INC.. MONITOR WELL LOCATIONS, DATED- OT I28 Y �iii.+6'�kVTT CONSULTANTS
wk WAY
) TERRA VAC, OVE TREATMENTA, FIGURE 3..
3) SPATGO ENVIRONMENTAL, GENERAL GROUNDWATER TABLE DN JUNE 21. 19
aDANO.
N)A MENTAL SERVI6:ES. INC„ SAMPLING LOCATIONS, DATED- D?fO ) =1 {)
SCALE
SITE PLAN 4e
DRAWING o. REV.
F
RViSICII FIG./SIT.

SUMMARY OF TREAT?
S(
CHARLOTTE
TABLE I
TENT SYSTEM INFLUENTIEFFLUENT CONCENTRATIONS
WTHEAST TERMINAL SITE NO, 4762
7401 OLD MOUNT HOLLY ROAD
MECKLENBURG COUNTY, NORTH CAROLINA
ww
BENZO(B)
,-FLUORANTHgNE
BENZO(io
E
D BE

C&E ENGINEERING
NOTES:
1) The summation of all the PAH compounds cannot exceed 0.0311 pg&
2) pg/t a Micrograms per liter.
3) Liquid phase'carbon titter; ET O-A U TE MX200-1_.
4) Vapor phase carbon filter; CET t7-AQU TEC MX200-V.
5) PQL - EPA Method Practical Quantftation Limit,
6) Ibslyr - Pounds per year.
7) lbsld y - Pounds per day.
8) NL - Not fisted.
BP OIL COMPANY T1 24898-04
SOUTHEAST TERMINAL SITE NO, 4762 PACE 2 OF 2 MARCH 1998

+► +► SP OIL say Oil Company
2655 Wastside Parkway, Suite 300
. .;,., C. S.1600
Alpharetta, Georgia 30004-9961
April 23, 1998 N A Y 199GR
[phone]
via Airborne Express
a m
u,
Ms. Jeanette Powell
North Carolina Department of Environment and +Natural Resources
Division of Water Quality
Water Quality Section APR199
2728 Capital Boulevard
Raleigh, North Carolina 27604 p�11 1T SOURCE BRAN N
Re. NPDES Certificate of Coverage No. NCG510006
Terminal No. 4762
Southeast Terminals - Paw Creek
741 Old Mount Holly Road
Paw Creels, Mecklenburg Counter, North Carolina
NC Groundwater Incident No. 15618
Dear Ms. Powell.
viments were prepared by G&E Engineering.
described in a letter from BP to the Division of Water Quality dated March 06, 1998.
The attached documents have been included, at your request, to facilitate the review of
referenced permit modification.

IF-r
If you have any questions or comments, please do not hesitate to contact the undersigned at
(770) 41-; 4 8 or at our new address shown above,
Respectfully Submitted,
Alan C Seese
Contract Engineer
On Behalf of Environmental Remediation Management
encl.: Construction Specifications - Groundwater Interceptor Trench
prepared by G&E Engineering and dated February 1998
Table 8 taken from Corrective Action Plan prepared by G&E Engineering and
dated November 1997
cc w/o encl. Jim Sl gh - Louis Dreyfus: Energy
Susan Sharp - BP" Atlanta
Houston Johnson - BP Atlanta
John Check - G&E Engineering
Gil Butler - DENR Mooresville Regional Office

PA1140 it
AL
r X-i) G&E ENGINEERING
ENVIRONMENTAL CONSULTANTS
7- 1" 0 VWX P-- 1 4105-C STUART ANDREW BOULEVARD - CHARLOTTE, NC 28217 [phone] FAX [phone]
CORRECTIVE ACTION PLAN
SOUTHEAST TERMINAL SITE NO. 4762
7401 OLD MOUNT HOLLY ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
NCDENR GROUNDWATER INCIDENT NO. 15618
NCDENR PRIORITY RANKING 10013
PREPARED FOR
BP OIL COMPANY
2555 WESTSIDE PARKWAY, SUITE 300
ALPHARETTA, GEORGIA 30004
(ATLANTA, GEORGIA)
[phone]
NOVEMBER 1997
Prepared By: G&E Engineering/CRA Engineering, Inc.
"k�
Brian D. Webster, C MM
Regiona Manager.'"
es W. Hayman, PE, PG, CPG Date
NC Licensed Engineer No. 17956
NC Licensed Geologist No. 1471
A Division of CRA" c,oftmporw
AMERICAN CONSULTING ENGINEERS COUNCIL

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1)
Data obtained from CSA Addendum --Tank 111 P112 and Tank 117C118 Areas, COM Environmental Services, Inc., July 1, 4997,
2)
Data obtained from Report of Invstroatrons Addendum, CBM Environmental Services, Inc., November 26,1996,
3)
Data obtained from Comprehensive Srte Assessment Addendum; BM Environmental Services, Inc., April 11,1997.
4)
Data obtained from 1996 Annual Remedration S stem date Re ort, SME, Inc., March 1997.
)
Data obtained from 195 Annual Remediation System iJ date Report, SM&E, Inc., September 1996.
6)
Data obtained from 1994 4th Quarter Report, M&E, Inc., March 23,1996.
7)
Data obtained from Comprehensive Site Assessment Addendum; CBM Environmental Services, Inc., March 25,1994.
8)
The less than sign (<) indicates that the parameter was not detected. The number following the Ne' sign is the detection limit for the analysis of the sample:
g)
BDL - Below detection limit.
10)
Total STEX is expressed as the summation of benzene, toluene, ethylbenzene, and total xytenes without regard for significant flu
11)
Vg/L - Micrograms per liter,
12)
ND - No data available.
13)
' - Not analyzed for parameter.
14)
NIA - Not applicable.
15)
NL - No groundwater action level listed. However, in accordance with North Carolina Administrative Code, Title 15A, Subchapter 2L, Section .0200, parameters for which no action level is specified
cannot be present at any detectable concentration.
16)
Only the constituent parameters detected by the various methods are presented herein.
98
SP'IDIL COMPANY
PAGE 19 OF 1 ND BER 1997
SOU TERMINAL SITE NO.
SOUTHEAST

•�
G&E ENGINEERING
ENVIRONMENTAL CONSULTANTS
4105-C STUART A DREW BOULEVARD . CHARLOTTE, MC 28217 [phone] FAX [phone]
A `
CONSTRUCTION SPECIFICATIONS e�
A�
GROUNDWATER INTERCEPTOR TRENCH
SOUTHEAST TERMINAL. SITE NO.47"62
7401 OLD MOULT HOLLY ROAD
CHARLOTTE, MECKL.ENBURG COUNTY, NORTH CAROL.INA
PREPARE! FOR
BP COIL. COMPANY
2555 WE TSIDE PARKWAY, SUITE 300
ALPHARETTA, GEORGIA 30004
(ATLANTA, GEORGIA
[phone]
FEBRUARY 1998
Prepared By: G&E Engineering/ORA Engineering, Inc.
n B. Uteck, EIT
Project Manager
>E, PG, CPG Data,
w No. 17956
t No. 1471
Division
AMERICAN

G&E ENGINEERING
TABLE OF CONTENTS
PAGE/NO.
SECTION I GENERAL CONDITIONS
1.1
Site Location ................. _ .............. ....... ............... ................
1
1.2
Site Description ... __ ............ ...... __ .......... .......... ....... _ .............. ......
1
1.3
Facility Operating Hours .. ........................................................ .............
1
1.4
Description of Interceptor Trench Recovery .... ___ ............... ........... _...
1
1.5
Connection to Existing Treatment Equipment ..... ..............
2
SECTION 2 TECHNICAL SPECIFICATIONS
2.1
Documents . ............................................................................ ...........
4
22
Base Bid Requirements .................. _ ....... ................. ...........................
4
2.3
Permits and Inspections ....... _ ...... ......... ................ ....... .......
4
2A
Coordination of Work/Protection of Existing Facilities ............. .............
5
2.5
Utilities . ........... _._ ...... - ............ ........ ........ _ ......... ..........
5
2.6
Interceptor Trench and Sump .. ....... ...... _ ......
5
2.6.1 Removal of Existing Crushed Rock ........ __ ............. __ ............
5
2.62 Disposal of Excavated Soils ....... ........ ___ ... _ ...... _ ..... ...........
6
2.6.3 Geotextile Drainage Layer .. ....... ___ ........ ......... _ ...............
6
2.6A PVC Membrane . _ _ . - . ... ................. ..................
7
Z6.5 Interceptor Trench ....... ...... ............ ..................
7
2.6.6 Interceptor Trench Sump ... ............... ___ ...........................
8
2.6.7 Crushed Stone . ..................... .......... ................... .......
8
2.6.8 Installation ..... ........ ........ ........... ............. ­ ...........
8
2.7
Recovery Pump, Service Lines, Service Trench,
and Service Line Supports ... ........ ....... ...... ........
9
2.7.1 Interceptor Trench Sump Pump ...... _ .... __ ...... ...........
9
2.7.2 Flow Totalizer ........ ............. ........... .................... ...... _ .......
9
2.7.3 Discharge Pipe .................................. ............. ......................
10
2.7A Electrical Conduit ...... ..... _ ...... ................. .........
10
2.7.5 Piping, Fittings, and Valves . ... __ ... - ........ ............ ..............
10
2.7.6 Piping Supports ....... ____ .......... ..... ___ ........... ........
10
2.77 Service Trench ........ ................ ........ ...... ..........
10
2.8
Treatment System ........... _ ....... ......... .......... .................. ..........
11
2.8.1 Connection to Existing Treatment System... .... .........................
11
2.8.2 Influent Sampling Port ................ ............. __ .... ...
11
2.83 Emergency Trips and Controllers .. ........ .......... ................... __
11
2.9
Electric Service ............... ....... _ ......... ............... ..............................
12
2.10
System Check -Out ........ ......... ............. .... __ ... .......... .....
12
2.11
Operational Start -Up ...... ......... _ ......... ...... _ ..................
13
2.12
Documentation ....... ...................................
13
BP OIL COMPANY
24898-04
SOUTHEAST TERMINAL SITE G. 4762 i FEBRUARY1998

G&E ENGINEERING
TABLE E OF CONTENTS
(CONTINUED)
PAGETN4.
FIGURES
U.S.G.S. Topographic Map ............. ......... .................. .....................:....,...;.. 1
ExistingSite Plan........................................................................................
Trench -Drain System Plan............................................................._ ...... _ 3
Existing D 'VES Enclosures and Layout' ..................................................... 4
Existing DPVES Process Schematic ...... ...................... ...:.... __......... ...........
Proposed Additions to Existing DPVES Enclosures and Layout ................... 6
Proposed Additions to Existing DPVES Process Schematic .........................
Trench -Drain Collection System Details...... ....... .............................................. 8
Equipment Layout Plan and Details ... ............................ :....... .......... ............. 9
InterconnectDetails ...............................................:................................... 10
Detail .............................. ___ ....... 11
Controller Schedule...........`...................................................................... 12
OWNER - Furnished Site Plans
BP OIL COMPANY :24 8-04
SOUTHEAST TERMINAL SITE NO. 4762 FEBRUARY 1998

&E'ENGINEERING
SECTION 1
GENERAL CONDITIONS
1.1 Site Location. The site is located at 7401 told Mount Holly Road in Charlotte, North
Carolina, approximately 6.5 miles northwest of the city's center. The specific area is
referred to as Paw Creek. The site location is shown on the USGS topographic map
presented on Figure 1.
1.2 Site d s ri t M. The site is an active bulk
control office building, miscellaneous storage an
tanks, aboveground storage tanks (ASTs), under
bulk dispensing loading rack, associated pro
remediaton system. The bulk storage tanks are
and/or excavated areas with earthen cut -bar
conditions is resented on Figure 2 he facility
.. I 11M.1. .
piping,groundw
r�r � r r �.»rr�r •- rr�r -..
(BP) and Louis Dreyfus Energy Corporation (LCIEC), hereafter referred to as "OWNER".
1.3 FacilibLOperatin' Hours. The regular operating hours of the terminal are from 0700-
to 1700-hrs., Monday through Friday. CONTRACTOR shall request approval from the
terminal manager a minimum of 24-hours in advance of any required activities occurring
outside of the regular operating hours of the terminal.
1.4Qescri tion of Interce `tor Trench Recovg . A slope drain and interceptor itrench will
be 'installed along the base of the cut -bank slope north of Tank No. 112 and along the
immediately adjacent cut: -bank and/or dike slopes to the east and west (collectively
referred to hereinafter as the "cut -bank") as shown on Figure 3. The interceptor trench will
capture light non -aqueous phase liquid (LNAPL) and associated groundwater (containing
dissolved hydrocarbons) seeping from the slope bank. Based upon available data, the
LNPL. source is from a historical diesel fuel release.
BP COIL COMPANY 2498-04
SOUTHEAST TERMINAL SITE NO. 4762 1 FEB U ` 1998

G&E ENGINEERING
over the interceptor trench to exclude precipitation from directly entering the trench and
sump. Following installation of these materials, the crushed rock layer shall be replaced
on the slope.
1.5 Connection to lxistini Treatment E u merit. The existing treatment equipment is
located in the northwestern portion of the site. This system recovers liquids and soil
vapors from recovery wells in the northwestern portion of the site. The existing
groundwater treatment system consists of three oil/water separators piped in series, a
transfer tank, and a low -profile air -stripper. Effluent vapors from the air -stripper are piped
to an air dryer and a vapor -phase carbon filter prior to discharge to the atmosphere under
appropriate permits. Effluent water from the air -stripper is first piped to two particle filters,
piped in parallel, and then to two liquid -phase carbon filters, piped in parallel, prior to
discharge under a NPDES General Permit. The equipment layout and a process
schematic of the existing treatment system are shown on Figures 4 and 5.
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO. 4762 2 FEBRUARY1998

G&E ENGINEERING
ump shall discharge to the first oil/water separator of the
it system. Based on the estimated average flow rate of
ombined total flow rate into the existing treatment system
i 1. The equipment layout and a process schematic of the
g treatment system are shown on Figures 6 and 7.
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO. 4762 3 FEBRUARY 1998

G&E ENGINEERING
SECTION 2
TECHNICAL SPECIFICATIONS
2.1 Documents. The design specifications for the remediation equipment are referenced
on Figures 3 through 12; the drawings presented on the figures are considered a part of
these technical specifications. If the specifications as stated herein conflict with any item
in the drawings, the specifications shall prevail.
2.2 Base Bid Requirements. All BIDDERS shall attend an on -site pre -bid meeting with
BP/LDEC, Failure to attend the pre -bid meeting will result in rejection of the bid.
CONTRACTOR shall attend an on -site pre -construction meeting with OWNER.
CONTRACTOR shall verify all dimensions and conditions prior to commencing work.
CONTRACTOR shall attend a 4-hour, on -site safety meeting prior to engaging
construction activities.
CONTRACTOR shall clearly mark all construction areas with barricades, cones, plates or
other approved safety markers to restrict access and provide a safe work environment for
the contractor and facility employees.
CONTRACTOR shall provide only new materials for all stages of construction.
CONTRACTOR shall warrant all materials and construction for a period of one year.
CONTRACTOR shall correct all idefects at no expense to the OWNER.
CONTRACTOR shall obtain written approval from OWNER prior to commencing any
work that results in a modification of the contract cost.
2.3 Permits and lap ,petions. OWNER will modify/obtain the existing NPDES Permit and
Air Quality Permit. CONTRACTOR shall obtain all other permits and inspections required
for the work. All necessary construction permits and inspections shall be obtained and
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO. 4762 4 FEBRUARY 1998

G&E E:NGI LEERING
paid for by the CONTRACTOR, including local and/or building permits for electrical,
mechanical, and civil construction, unless otherwise specified. All national, state, county,
and local plumbing and electrical codes must be adhered to.
2.4 Coordination of 11 ork/Protection of Existina Facilities. CONTRACTOR shall protect all
existing site structures from damage or degradation,and except for the construction
specified herein, shall have no negative effect on site cleanliness or appearance.
CONTRACTOR shall protect the integrity of all on -site monitor wells (see ';Figure 2).
CONTRACTOR shall repair anti/or replace any monitor wells damaged during on -site
activities,
2.5 Utilities. CONTRACTOR .shall confirm the location` of all aboveground and
underground utilities from OWNER -furnished site plans, utility company records, and
overt physical evidence (see Figure 2). CONTRACTOR shall provide for the protection of
aboveground and underground 'utilities during the construction activities'. If utilities must
be temporarily severed or relocated to facilitate construction, the CONTRACTOR shell be
responsible to notify all affected parties, secure appropriate permission or permits,
replace or repair the affected utilities, and secure necessary inspections.'CONTRACTOR
shall be responsible for damage to underground utilities and any releases from the
damage of product transfer lines.
2.6 Interce torTrenh and Sump. The interception trench and sump details are shown on
Figures d through 10.
. .1 Removal of Existing Crushed 'Rock. The existing crushed rock on the cut -
bank and dike slope shall be removed prior to installation of the geotextile drainage
layer and the impervious membrane, and shall be stack piled on -site for
subsequent reuse.
BP OIL COMPANY 24 96-04
SOUTHEAST TERMINAL SITE NO. 4762 5 FEBRUARY`I996

G&E ENGINEERING
2.6.2 Disr)osal of Excavated Soils. CONTRACTOR shall stock pile all excavated
soil on plastic sheeting in an area designated by OWNER. OWNER will sample
and classify the soils to be disposed. CONTRACTOR shall provide North Carolina
certifications of the proposed thermal treatment facility to OWNER and request
pre -approval for off -site disposal. CONTRACTOR shall load and manifest the
excavated soils to the approved off -site thermal treatment facility. CONTRACTOR
shall provide copies of all manifests and documentation to OWNER within of one
week following final construction approval.
2.6.3 Geotextile Drainage Layer. The geotextile drainage layer shall function as a
drainage layer allowing transport of seeped liquids to the interceptor trench.
The geotextile layer shall be a three-dimensional geonet structure of entangled
core polymer extrusions of black high density polyethylene (HDPE) mono laments
melt -bonded at their intersections, forming a stable net of suitable weight and
configuration. The geonet shall be crush -resistant, pliable, resilient, water -
permeable, and highly resistant to chemicals and environmental degradation. One
side of the geonet shall be heat bonded to a non -woven polypropylene geotextile
fabric, free of oil, grease, and other foreign materials, to prevent migration of soils
into the core of the geonet.
The geotextile drainage layer shall be EnkanetTm Type 4010 as manufactured by
AKZO Industries Systems Company, P.O. Box 7249, Asheville, North Carolina
28802, [phone] or approved equal.
Installation of the geotextile, including seaming, shall be done in accordance with
the recommendations of the manufacturer, and handled in such a manner as to
ensure it is not damaged. Care shall be taken to ensure that stones, mud, and dirt
are not entrapped in the geotextile during placement. The geotextile shall be
placed with the filter -fabric backing on the bottom (i.e., the filter fabric backing shall
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO, 4762 6 FEBRUARY 1998

G&E ENGINEERING
be in direct contact With the exposed soil on the cut -bank and dike slopes) and
shall cover the entire cut -bank and dike slope as shown on Figures 3 and 9.
2.6.4 PVC Membrane. The PVC membrane shall function as an impervious layer
to line the interceptor trench and prevent precipitation and surface water runoff
from entering the trench.
The impervious membrane shall be manufactured of PVC in combination with
resins, pigments, carbon black, and plasticizers, specifically compounded to
remain flexible. The membrane material shall be so produced as to be free of
holes, contaminants, defects, blisters, undispersed raw materials, edge
irregularities, or any sign of contamination by foreign matter.
The membrane shall be ribbed or textured, 30 mil PVC, and shall be Oxy Flex, as
manufactured by OxyChem Vinyls Division, Armond Hammer Boulevard, Box 699,
Pottstown, Pennsylvania 19464, [phone] or approved equal.
Installation of the membrane, including seaming, shall be done in accordance with
the recommendations of the manufacturer, and handled in such a manner as to
ensure it is not damaged. Seaming shall be accomplished by solvent welding. The
membrane shall be installed as shown on the drawings so as to line the interceptor
trench, cover the geotextile drainage layer, and anchor at the top of the cut -bank
slope.
2.6.5 Interceptor Trench. The interceptor trench shall be constructed as shown on
the drawings. The side of the trench adjacent to the cut -bank or the trench shall be
lined with the impervious membrane. A 6-inch diameter, Schedule 40, slotted, PVC
pipe shall be installed along the entire length of the trench and sloped to allow
gravity flow of intercepted liquids to the sump. The upslope ends of the slotted pipe
shall be fitted with a cleanout plug which penetrates the PVC membrane and is
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO. 4762 7 FEBRUARY 1998

G&E ENGINEERING
accessible from the surface. The trench shall be backfilled with fine gravel as
shown on the drawings.
2.6.6 Intlerce tor Trench Sump. The interceptor trench collection sump shall be
constructed as shown on the drawings. The sump shall be lined with the
impervious membrane. A 16-inch diameter, schedule 40, slotted, PVC riser pipe
shall be installed in the sump. The 6-inch diameter perforated pipe extending the
length of the trench shall be connected to the riser pipe. The sump surrounding the
riser shall be backfilled with fine gravel.
2.6.7 Crushed Stone. Coarse, angular crushed stone, matching the existing
surrounding crushed stone surfacing, shall be placed over the PVC membrane to
the minimum depth shown on the drawings. Stone shall be placed starting at the
bottom of the slope and progressing to the top. CONTRACTOR shall exercise care
in placing stone to prevent puncture of the membrane.
2.6.8 Installation. Clearing the cut -bank and installation of the geotextile drainage
layer, PVC membrane, and trenching will encounter at -grade piping (i.e., piping
supported several inches above grade) and piping support pads. The existing
crushed stone shall be removed from beneath all at -grade piping within the area to
be covered by membrane. Excavation for the interceptor trench and collection
sump shall be extended beneath piping but shall not intercept the descending 1:1
load plane slope beneath any piping support pad. The geotextile drainage layer
shall be placed on the soil beneath piping and shall be cut to fit around piping
support pads. PVC membrane shall likewise be placed under piping, but shall
cover pipe support pads with only the minimum possible opening for penetration of
the pipe support riser. Crushed stone shall be placed under piping and over pipe
support pads.
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO. 4762 8 FEBRUARY 1998

G&E ENGINEERING
2.7 Recove Pum ` Service Lines Service Trench and Service Line Supports. The
interceptor trench sump pump and all associated service lines shall be installed as
specified hereinafter and as shown on the drawings.
2.7.1 lnterce for Trench' Sum Pum . The intercepter trench sump pump P-1)
shall be installed in the interceptor trenchsump. Pump P-1 shall be a Grundfos
Redi-FloTm Model 5E3 electric submersible pump capable of pumping LNAPL a
manufactured by Crundfos Pumps Corporation, 2555 Clovis Avenue, Clovis,
California 53612, (209) ; 2-8000 or approved equal. A check valve shall be
installed on the discharge side of the pump to prevent liquids from>backflowing into
the sump.
The estimated maximum total dynamic heart (static lift plus friction loss) of
approximately 30.5 feet was computed from the sump pump to the first oiltwater
separator for a 2-inch diameter, schedule 40, galvanized steel pipe.
Level control for pump P-1 shall be provided by an integral pressure switch or float
switch. A low low level switch shall be provided to prevent the pump from running
dry. The pump controls shall function as specified on the drawings.
2.7.2 Flow Totalizer. The flow totalizer shall be installed as shown on the drawings
and shall be capable of cumulative recording of the flaw rate accurately over a
range of 1 to 16 gpm from pump P-1. (NOTE: Although the average seepage flow
rate was estimated to be 0.16 gpm "slugs" of captured liquid will be periodically
plumped to the treatment system as the interceptor trench sump fills with liquid.
Therefore, the flow totalizer is sized to match the performance specifications of the
pump.)
BP OIL COMPANY 248 8-04
SOUTHEAST TERMINAL SITE NO. 4762 9 FE RUARY 1998

G&E EiNGINEERING
2.7.3 Discharge Pipe. The discharge pipe from the interceptor trench sump pump
to the oilAAtater separator located within the existing treatment system enclosure
shall be constructed of 2-inch diameter, schedule 40, galvanized steel pipe.
2.7.4 Electrical Conduit. Above -grade electrical conduit shall be constructed of3/4-
inch diameter, rigid, galvanized steel pipe and shall comply with local codes and
the NEC. Below -grade electrical conduit shall be constructed of 3/4-inch diameter,
rigid, PVC pipe and shall comply with local codes and the NEC. Transitions
between rigid galvanized conduit and rigid PVC conduit shall be made below
grade, water -tight, and shall comply with the local codes and the NEC.
2.7.5 Pi in Filtinas, and Valves. All aboveground and underground piping,
fittings, and valves shall be Schedule 40 constructed of the materials and in the
nominal sizes as specified herein or shown on the drawings and shall be airtwater
tight. All aboveground piping shall be equipped with low -point drains to allow
drainage of the system during freezing conditions.
2.7.6 Piping Supports. The piping supports shall consist of cast -in -place concrete
footings with structural steel supports in the dimensions as shown on the drawings.
The supports shall be installed 8 feet or less apart. Concrete shall consist of
Portland cement, aggregate, and water and shall have a minimum 28-day
compressive strength of 3,000 pounds per square inch (psi).
2.7.7 Service Trench. The service trench shall follow the routes, and shall be
constructed as shown on the drawings. All valves and fittings shall be air/water
tight and shall be as shown on the drawings.
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE NO3 4762 10 FEBRUARY 1998

GCE ENGINEERING
2.8 Treatment Svstem. The LN PL recovery system shall be connected to the existing
treatment system as shown on the drawings.
2.8.1 Connection to Existing_j[pptMqft_5ystem. The discharge pipe from the
interceptor trench sump pump shall be connected to the existing groundwater
treatment system so that the recovered fluids from the trench are discharged to the
first oil/water separator.
The existing air -stripper blower shall be equipped with a differential pressure
switch (DPS-) as shown on the drawings to provide emergency shut down of
pump P-1 if air flow is interrupted.
The existing transfer tank shall be equipped with a high level switch M.-2) as
shown can the drawings to provide emergency shut clown of pump P-1 if a high
level in the transfer tank is detected.
2.8.2 Influent Sampling Part. An influent sampling port shall be installed on the line
connecting the interceptor trench sump pimp and the first oil/water separator a
shown on the drawings and shall be located within the ; treatment equipment
enclosure.
2.8.3 EmeWencv Trips and Controllers. Emergency trips and controllers shall
provide operation of the system in accordance with the controller schedule and
shall be positioned as shown on the drawings. Controllers and emergency trips
may be electrical float switch or pressure sensor type devices, conductivity
controllers shall not be used. Controllers and emergency trips shall provide
operation of the system in accordance with the control schedule as shown on the
drawings.
BP OIL COMPANY 24898-0
SOUTHEAST TERMINAL SITE NO. 4762 11 FEBRUARY" 1998

G&E GNGINEERING
2.9 Electric Service. CONTRACTOR shall provide a new electrical control panel (ECP)
incorporating all controllers specified herein. CONTRACTOR shall mount the new ECP in
the location shown can the figures. The new ECP shall comply with the National Electrical
Manufacturer's Association (NEMA) standards, in accordance with the National Electric
Cade (NEC) Article 00, and shall be suitable for outdoor locations. Single-phase, 230
volt; 30 amp minimum electric service shall be supplied to the new ECP. Electric service
and control wiring shall be supplied to the interceptor trench sump pump from the new
EC. All components in the new ECP shall be Underwriters Laboratories (U.L.):listed and
include individual circuit breakers (i.e.,separate from any other equipment), International
Electric Code (IEC) design full' -voltage magnetic starters complete with single phase
overload protection, manual reset and adjustable overloads, 11 OV control circuit start/stop
buttons/switches, and terminal strips for external connections. The new ECP shall be
labeled "Electrical Control Panel" on the exterior face of the door and shall have a
"Danger = Nigh Voltage" sign mounted on the exterior face of the door. Each component,
terminal strip, and wire end within the new ECP shall be clearly labeled. All electrical
wiring and circuit schematics shall be included in the manufacturer's specificationsand
manuals. All electrical components and connections shall be explosion -proof. All electric
service, wiring, and components shall comply with the NEC. All electric service shall meet
local codes, and the requirements of local codes shall prevail.
2.10 System Check -Out. The CONTRACTOR shall, in the presence of the OWNER or its
agent, demonstrate that all mechanical elements of the system operate within' the
specified rates and capacities; and demonstrate the operating range and effective
operation of each controller. All piping shall be pressure tested at 75 psi. Specifically, the
check-out shall demonstrate operation of -
Mechanical Equipment.
• Pump; P-1 delivery of recovered groundwater/LNAPL. from the interceptor
trench sump to the first oiltwwater separator.
• Flow totalizer.
BP OIL COMPANY 2489E -0
SOUTHEAST TERMINAL SITE NO. 4r 2 12 FEBRUARY1998

&E EiNGINEERING
• Controllers.
• Level controllers (tLL-1, LL-1,-HL-1, and HL-2).
• Differential pressure switch (DPS-1).
2.11 Operational Start -Up CONTRACTOR shall be on -call and readily available during
the initial 48 hours of operation and testing. Acceptance of the system by OWNER will
follow the initial 48-hour testing period.
2.12 Documentation. CONTRACTOR shall furnish to OWNER manufacturer's
specifications, instruction manuals, data sheets, and warranty details for all commercially
acquired equipment (e.g., pumps, flow totalizer, controller components, PVC membrane).
CONTRACTOR CTOR shall furnish specifications for all service lines (e.g., electrical wiring,
controller wiring, and fluid discharge pipes). CONTRACTOR shall provide a complete set
of legible scaled redline drawings to OWNER. CONTRACTOR shall furnish as -built
construction details and shall furnish cross -sectional details of the service trench to the
treatment equipment enclosure. CONTRACTOR shall provide a complete set of
construction photographs to OWNER. CONTRACTOR shall provide all required
documentation a maximum of one weep following final construction approval.
BP OIL COMPANY 24898-04
SOUTHEAST TERMINAL SITE No. 4762 13FEBRUARY '1998

. . .. ......
t
f N
9
--IISITE
lu lormNARLOTTE
7/ 7"), NOT TO SCALE
....... PUBLIC POTA13LE WATER WELL
1100
PRIVATE POTABLE WATER WELL
Jt
PUBLIC POTABLE WATER
IL STORAGE RESERVOIR
/x
0 feet 2000
SCALE
G&E ENGINEERING
A Division of COMPANY
_J '1w ENVIRONMESITAL CONSULTANTS
RE: U.S.G.S. 7.5 MINUTE SERIES OUADRANGLE MAP, MOUNTAIN ISLAND LAKE, NORTH WOLINA, 1993.
DESIGNED BY:
DRAWN By,, L.D. MAYE2S 10/27/97 BP OIL COMPANY SOUTHEAST TERMINAL SITE No. 4762 U.&G.S. TOPOGRAPHIC 24898-00—Bil 0
DRAWING No, REV,
MAP
CHECKED By: ATLANTA, GEORGIA 7401 OLD MOUNT HOLLY ROAD
CHARLOTTE, NORTH CAROLINA 1
—C�ATE NO. REVISION APPROVED Client Project Locotion FIG./SHEET No,

--------------
1
0 EXISTING
UST P-5
UW--8 1
OVERHEAD PIPE RACK----*--)
-
r
o
OLD INTERCEPTOR
t TRENCH
*am I low on
S-3I c
T- r _ �- �- MONITOR WELL LOCATION
(SUMP) ~' ,� AT -GRADE PIPING' yy VRU VAPOR RECOVERY UNIT
U-7 NaPL NON -AQUEOUS PHASE LIQUIDS
U - .. �' APPROXIMATE LOCATION OF NAPL SEEPAGE
— -- 76
TOP/BOTTOM OF SLOPE/BERMED AREA
✓° - i l I l i l t I l i r t i t 1 r r AREA OF SLOPE DRAIN AND
CJ- -- - "" `" "" "` r t l i t I I I r 1 l r i l l t 1 l I r l i t l l I► l l *r INTERCEPTOR- TRENCH -- APPROXIMATE LOCATION OF TOP OF BERM SLOPE
— �;itttlll{11IIt ttlitllillltliittlrll ,r
CORRUGATED DRAIN r
A EXISTING UNDERGROUND PIPING
{
AREA OF SLOPE DRAIN AND INTERCEPTOR TRENCH
•-- — �. _..,..� �. -_.. � � � �" -----� � - - T84 - - GROUND SURFACE. ELEVATION CONTOUR, FT
AV -
}till 1l 11I11111111111111 tltitt'ttitilFr/
rf
_ L.P.
I I I I r I, IT COLLECTION SUMP ► t t r I 1- i uT
111 1
j ��'V _ `Ta ll�rl�rtirr
.;� t0 6" DIA SLOTTED I I {
pp I PVC PIPE gg 1) MONITOR WELL LOCATIONS ARE APPROXIMATE.
( I t 2) CONTOUR LINE ELEVATION$ RELATIVE TO DPEW-2 TOP -OF -CASING
CIOELEVATION OF 781,18 FT MEAN SEA LEVEL.
' /° \ "" j ` 3) SECTIONS A -A" ANC} B--W ARE SHOWN ON FIGURE 8.
Q.. t ` ,t w ` � N.. I
P�; I'�\III11IIt 1F"
O feet 15
1
SCALE
EXISTING ABOVEGROUND PIPING 3 11 AT --GRADE PIPING
G&E ENGINEERING
TANK 1 1 Givilan at -ANC
ENVIRONMENTAL CONSULTANTS
SCALE
DESIGNED BY. SOUTHEAST TERMINAL IT o. T T - aB s-Da-B1 O
DRAWN BY.. LIFTS 2f16l9 BP O 1 COMPANY
CHECKED sY. , �' ATLA TA, GE RGIA ` 7401 OLC MO HOLLY ROAD' Y DRAWING Na. REV_
CHARLOTTE, NORTH CAROLIA
DATE NO. REVISION �y APPROVED B Client Project Location FIG./SHEET No.

EXISTING
ELECTRICAL
'
CONTROL PANEL
Fr_
DISCHARGE
PUMP
EXISTING
TREATMENT
OIL/WATER
BLOWER EOUIPMENT
SEPARATOR
ENCLOSURE
LIQUID- (PLAN VIEW)
PHASE
el
LOW -PROFILE CARBON
FILTER
'_jPAnTICLEI
FILTER
AIR STRIPPER
DISCHARGE IN
ACCORDANCE
WITH EXISTING
OIL/WATER
-- "`---�--�el
WOES PERMIT
SEPARATOR
LIQUID -
PARTICLE
PHASE
CARBON
FILTER
TRANSFER TANK FILTER
OIL/WATER
SEPARATOR
-
TRANSFER
PUMP
EI�iEJM
IL
VAPOR -
PHASE
FLUID/VAPOR FLOW DIRECTION
CARBON
FILTER
EXISTING
ELECTRICAL
CONTROL PANEL
AIR DRYER VENT TO
ATMOSPHERE
FLUID:
TRANSFER
PUMP
BLOWER
EXISTING
VAPOR
DISCHARGE
ROTARY -LOSE,
PROPANE TO
STACK
DRY -VACUUM
BURNER
PUMP ENCLOSURE
( VIEW)
NOT TO SCALE
AIR/WATER
THERMAL CATALYTIC OXIDIZER
SEPARATOR
of
ev
RECOVERED
FLUID/VAPOR
ENVIRONMENTAL CONSULTANTS
FROM EXISTING
RECOVERY WELLS
NOT TO SCALE
rTE
DESIGNED BY.
L
8P
OIL [ TERMINAL 4762
COMPANY
SCALE
EXISTING 2' 8-04-814
DRAWBY,
B
.
7401 OLD MOUNT HOLLY ROAD
ENCLOSURES AND DRAWING No. REV.
CHECKED BY _
ATLANTA. GEORGIA
NORTH AROLINA
CHARLOTTE10
LAYOUT
NO,
REMSi
BY
ROVED B :
Client
Project Location
I'll,„
FIG./SHEET No.

VENT TO
ATMOSPHERE
E
DPVES DUAL —PHASE VACUUM
EXTRACTION SYSTEM
MANUAL
AMBIENT LIGHT NON —AQUEOUS
AIR INTAKE LNAPL PHASE LIQUIDS`
BLOWER FM FLOW METER
PROPANE TO PRESSURE RELIEF VALVE
1 I BURNER
ROTARY -LE, THROTTLE VALVE
THERMAL
DRY-VACUUMPUMP CATALYTIC BALL VALVE
010DIZER
VACUUM
RELIEF
RECOVERED VENT TO
FLUID/VAPOR VENT TO VENT TO ATMOSPHERE
FROI FM ATMOSPHERE ATMOSPHERE
RECpVERY WElLS
VENT TO AIR
ATMOSPHERE DRYER"
I I
I% I
t I
I I VENT TO
I I ATMOSPHERE
I< I
I I
t
IVAPOR-PHASE
tl I CARBON FILTER
I BLOWER
# r
AIR/WA R O WATER
I SEPARATOR OIL/WATER, SEPARATOR INFLUENT EFFLUENT -ILL
DISCHARGE IN
TYPICAL EXISTING TRANSFER SEPARATOR SAMPLING SAMPLING ACCORDANCE
RECOVERY WELL PORT PORT No. T WITH EXISTING
FATER LOW —PROFILE AREFFLUENT POES PERMIT
F+TIICLE
S ARATR TRANSFER AIR STRIPPER PART! FILTER
TR SFERPUMP DISCHARGE FILTER L110 --- -PHASE SAMPLING
TAW PUMP CARBON CARBON PORT No
FILTER FILTER
NOT TO SCALE
A " n Of • CRMcl a a v
ENVIRONMENTALCONSULTANTS
NOT TO SCALE
DESIGNED BY. SCALE
DRAWNBY. LI BP OIL O SOUTHEAST TERMINAL IT o. 47EXISTINGas s-oa—Bi3 0
CHECKED BY ATLANTA, G RGIA 74C 1 OLD MOUNT HOLLY ROAD I DRAWING, No. REV.
ival CHARLOTTE, NORTH CAROLINA
MATE NO. REVISI BY PROVED BY: Client Prefect Locetlert I'til lgwrgr ktn

EXISTING
ELECTRICAL
CONTROL PANEL
DISCHARGE
PUMP
FM
BLOWER
TREATMENT
EQUIPMENT
OIL/WATER (D ENCLOSURE
SEPARATOR OPS-1 LIQUID- (PLAN VIEW)
PHASE
LOW -PROFILE CARBON
PAR TIECRLE FILTER
IL TICLI FIL TER AIR STRIPPER
DISCHARGE IN
ACCORDANCE
— — - --------- ----------- OIL/WAIER
WITH EXISTING SEPARATOR
NPDES PERMIT
LIQUID -
PHASE
PARTICLE) CARBON
FILTER TRANSFER TANK FILTER
-foo- OIL/WATER ti
SEPARATOR TRANSFER
PUMP
VAPOR -
PHASE
FLUID/VAPOR FLOW DIRECTION
CARBON\
— — — — — — — — — — FLOW METER
'7-
��Z_z_ zzzz-4z
IN DPS-1 DIFFERENTIAL PRESSURE SWITCH
ELECTRICAL
CONTROL PANEL
AIR DRYEP VENT TO
L ATMOSPHERE
L — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — -- 3/4" DIA RIGID GALVANIZED
STEEL CONDUIT FOR PUMP POWER
L - — — — — — — ®. — — — — — — — — — — — — — — — — — — — — — — — — -- 3/4- DIA RIGID GALVANIZED FROM PROPOSED TRENCH -DRAIN
STEEL CONDUIT FOR CONTROL WIRES COLLECTION SUMP PUMP
2' DIA SCH 40 GALVANIZED
kSTEEL DISCHARGE PIPE FOR
RECOVERED FLUIDS
TRANSFER
PUMP
BLOWER
-------- --- j
PROPANE TO DISCHARGE
ROTARY LOBE STACI,
OR Y' VACUUM BURNER
PUMP ENCLOSUPE
(PLAN VIEW) NOT TO SCALE
AIR/WATER
THERMAL CATALiTIC OXIDIZER GaE ENECIONES ROHN uAw&
SEPARATOR A Dm" Of
nN
r77TTT77TrTTTTTTT7-rt ENVIRONMENTAL CONSULTANTS
FRtaM
RECOVERY WELLS NOT TO SCALE
SCALE
DESIGNED BY: PROPOSED ADDITIONS TO 24898-04-SI9 0
--I DRAWN BY: I I Ta OLARK 11/101w BP OIL COMPANY SOUTHEAST TERMINAL SITE No. 4762 EXISTING DPVES DRAWING No, REV.
CHECKED BY- ATLANTA, GEORGIA 7401 OLD MOUNT HOLLY ROAD
CHARLOTTE, NORTH CAROLING ENCLOSURES AND LAYOUT 6
k�Q�ATE NO. REVISION BY APPROVED 8
Client Protect Locotion FIG. /SHEET No.

.. .................. . . ....... .
VENT TO
ATMOSPHERE
DPVES DUAL —PHASE VACUUM
MANUAEXTRACTION SYSTEM
L
AMBIEN T
AIR INTAKE LNAPL LIGHT NON —AQUEOUS
SLOWER PHASE LIQUIDS
FLOW METER
N PRESSURE RELIEF VALVE/CHECK VALVE
]BURNER
VENT TO
ROTARY -LOSE, AIMCISPHERE
THROTTLE VALVE
DRY -VACUUM THERMAL
PUMP CATALYTIC BALL VALVE
OXIDIZER AIR
Z 1R DRYER
0.
FM VACUUM
INFLUENT
I I SAMPLING 7
IF RECOVERED PORT
-PHASE
FtUID/VAPOP VENT TO VFNT TO VAPOR
FROM EX[SDNG (FM AIMOSFHFP' ATMOSPHERE CARBON FILTER
REt.OVER r WELL
VENI TO TO PROPOSED
AIMOSPHERE
SUMP Pump
CONTROLS
VENT 10
A FM PHERE
TO PROPOSED
r SUMP PUMP CONTROLS
It
HL-1 Di` CHARCE IN
0 -_-"I I L-2 ACCOPEANCE
II t t
SLOWER WITH ExlDING
NPDES PEPMI T
SUMP
LL-I
—PROPOSED 011a ATER
LLL-I AIR/WATER SEPARATOR FIFFLUENT
SEPARATOR SAMPLIN6, SAMPLING
PUMP INFLUENT
I I OIL/WATER
,XISTING SEPARATOR PORT POR T No I
TYPICAL F LOW -PROFILE
RECOVERY WELL PUMP OIL/WATER TRANSFER AtIR STRIPPER PARTICLE PARTICLE TFIFLUELIT
SEPARATOR TRIAI SFER PUNIP DISCHARGE FILTER FILTER LIQUID-PHIASE LIQUIP�PHAt,5E SAMPL&I'G,
PROPOSED 'rANK PUMP CARBON CAR.80* ,4 FORT No ?
TRENCH -DRAIN FILTER FILTE4
COLLECTION SUMP
NOT TO SCALE
jtjWM G&E ENG""INEERING
A Division of SME"Po'
ENVIRONMENTAL CONSULTANTS
BP OIL COM
ATLANTA, GE,
EM 0 client

36' r 24" x 24"
STEEL PROTECTIVE ACCESS
VAULT WITH LIFTING HANDLES
PRESSURE 16"0 PVC
GAUGE WITH REMOVABLE
6" THICK CAP
3,000 PSI
CONCRETE CRUSHED ROCK
ELECTRICAJUNCTION
OXES
L "
.: da . .�
OWN
6"MIN
STAINLESS STEEL
EYEBOLT FOR
SUPPORT CABLE
" QUICK CONNECT "
COMPRESSION FITTING
I (SLOPE TO MATCH
EXISTING) BALL
VALVE PITLESS AFDAPTOR
1.5 TO LEVEL
COARSE ANGULAR CRUSHED
CONTROLS STAINLESS STEEL ROCK(MATCH EXISTING SUPPORT CABLE
SURFACE ROCK) 18" LONG GRADE HOSE
71
I'0 PVC
DRAIN PUMP
30 MIL PVC, RIBBED OR TEXTURED MEMBRANE POWER
/GRAVEL
-FILLED
ERCEPTOR
6 GEOTEX71LE DRAINAGE LAYER PER
MAX /GRAVEL•- DETAIL A-1 ED
1' SUMP 16" DIA SLOTTED PVC
FILTER FABRIC'
(BACKING ON DRAINAGE TEXTILE
6" DIA SLOTTED PUG PIPE
tj Q FINE GRAVEL (ASTM #8)
.-+ tt 6", DIA SLOTTED PVC PIPE
o ° (NOTE 1)
1 6" DIA SLOTTED PVC PIPE 0 0
(NOTE 1) 30 MIL PVC, RIBBED OR ° 0 000
TEXTURED MEMBRANE n 0
t3 1-i%2'
C} 0°
0 0 0�
TYPICAL TRENCH DETAIL A - A' °
NOT TO SCALE SUBMERSIBLE SUMP PUMP SUSPENDED
IN PVC SLOTTED RISER APPROXIMATELY
6" FROM THE BOTTOM t
COLLECTION SUMP DETAIL -B' NOT TO SCALE
NOT TO SCALE
ND
ffi�'-
1,) SLOPE BOTTOM OF TRENCH AND SLOTTED PVC'
PIPE TOWARDS THE COLLECTION SUMP AT 1j" PER
1OO
2.) ALL ELECTRICAL FITTINGS AND CONNECTIONS SHALL
COMPLY WITH THE NATIONAL ELECTRICAL CODE, ARTICLE 500,
3.) ADDITIONAL WIRE SHALL BE INSTALLED TO PROVIDE it A DlvWm of ` GRA"caa��tY
SUFFICIENT SLACK TO ENABLE PUMP REMOVAL.:. ENVIRONMENTAL CONSULTANTS
NOT TO SCALE
SCALE ;
DESIGNED BY: M. LIFE 2/ 7/98 E3 P OILCOMPANY SOUTHEAST TERMINAL IT a. COLLECTION � DRAIN8 8-00 Bt S O
DRAWN BY, SYSTEM DRAWING No, REV.
CHECKED BY: a- ATLANTA, GEORGIA 7401 OLD MOUNT HOLLY ROAD
CHARLOTTE, NORTH CAROLINA DETAILS
DATE NO. REVISION BY APPROVED BY: DATE Project Location FIG./SHEET No.

...........
"OF
A.
'4
v
t
J
PROPOSED AREA OF
7
A
A
TRENCH DRAIN COLLECTION
SYSTEM
J
W
VlA
Lr"
0 ABANDONED WELL LOCATION
EXISTING DPVES
RECOVERY WELL LOCATION
5 EQUIPMENT AREA
rg�' —PROPOSED NAPL
t 'w 9 9 z MONITOR WELL LOCATION
COLLECTION SUMP
A
SOIL BORING
218
0 TYPE III DEEP MONITORING WELL LOCATION
Iz. VRU VAPOR RECOVERY UNIT
xA.
LIST UNDERGROUND STORAGE TANK
Y
NAPL NON —AQUEOUS PHASE LIQUIDS
14
DPVES DUAL PHASE VACUUM EXTRACTION SYSTEM
j""
EXISTING PIPELINE
J
PROPERTY LINE
CHAIN LINK FENCE
TOP/BOTTOM OF SLOPE/BERMED AREA
•Tw
EXISTING ABOVEGROUND UNDERGROUND DPVES
k
RECOVERY LINES (APPROXIMATE LOCATION)
D . .... EXISTING NAPL RECOVERY TRENCH
EXISTING CRUSHED
ROCK SURFACE NEW ABOVEGROUND PIPING
NEW UNDERGROUND PIPING
EX" O
COMPACTED
SAND
COMPACTED
REPLACE CRUSHED ROCK SURFACE
D TO MATCH EXISTING
PROPERTY LINE BOUNDARIES RELATIVE TO THE SITE FEATURES
ARE APPROXIMATE.
r TO MA
D TCH EXISTING
2' DIA SCH 40 GALVANIZED
STEEL DISCHARGE PIPE
FOR RECOVERED FLUID
24" MIN
GALVANIZED
I
3/4- DIA RIGID GALVANIZED
T PUMP
P
STEEL CONDUIT FOR PUMP I
POWER AND CONTROLLER WIRE 0 f eet 80
SECTION D-D'
t7l SEC
COMPACTED SAND SCALE
BACKFILL
18- MIN----]
( 1" G&E ENGINEERING"
UNDERGROUND PIPING DETAIL v so A 1xvislo" of I 1 1* CarCLAP Y z ENVIRONMENTAL CONSULTANTS
NOT TO SCALE
1 #1=80'
L
DESIGNED BY: 24898-04-8211 b
DRAWN BY.' M LIFE 2/18/98 BP OIL COMPANY SOUTHEAST TERMINAL SITE No. 4762 EQUIPMENT LAYOUT DRAWING No.
CHECKED B ATLANTA, GEORGIA 7401 OLD MOUNT HOLLY ROAD PLAN AND DETAILS
CHARLOTTE, NORTH CAROLINA
pp 0, 9
By DESIGNEDBY:
BY:
IDATE NO� REVISION BY&-'_ Client Project Locotion FIG,/SHEET No.

2" DIA SCH 40 GALVANIZED
STEEL EFFLUENT DISCHARGE PIPE
FOR RECOVERED FLUIDS
3/4" OIA RIGID GALVANIZED STEEL CONDUIT
FOR PUMP POWER
3/4- DIA RIGID GALVANIZED STEEL CONDUIT FOR
EXISTING TREATMENT CONTROL WIRES
SYSTEM ENCLOSURE
✓— -- - ----------
+ + + + +
PROPOSED AREA: OF TRENCH DRAIN
COLLECTION SYSTEM (SEE FIGURE 3
RR/
°'>/,f FOR TRENCH LAYOUT)
7T-1i" / ` '/ ` ;
L�— �__J J
PROPOSED" NAPL COLLECTION SUMP
SEE FIGURE 9 SEE FIGURE 9 fx
r
FOR PIPE TRENCH " :FOR UNDERGROUND
ROUTING PIPING DETAILS j
TANK #11
NOT TO SCALE
n Of '' RlCr. aAaa�
ENVIRONMENTAL CONSULTANTS
NOT TO SCALE
SCALE
DESIGNED, MKLb=E 2/16t98 BP OIL COMPANY SOUTHEAST EAST TERMINAL SITE o. 4762 INTERCONNECT 4898-04-018 Q
CHECKED BY: �* �' ATLANTA, _GEORGIA 7401 OLD MOUNT HOLLY ROAD DETAILS —DRAWING No. I REV.
CHARLOTTE, NORTH CAROLINA10
DATE NO. REVISION DY APPROVED BY. Client Project Locotlon FIG./SHEET No.

12," MIN.
2" GALVANIZED --\ —2--
PIPE —2'-
3/4- RIGID GALVANIZED
CONDUIT
2" STEEL PIPE,—,,
PAINTED WHITE 2* x 4" x 1/4" T END PLATE;
�LD TO EACH SIDE OF HORIZONTAL
SUPPORT; PAINTED WHITE
12" MIN.
EXISTING
CRUSHED ROCK
SURFACE
—2'- 0' SQ—
—— CONCRETE COLLAR
CENTERED
EXISTING
' CRUSHED ROCK
CONCRETE (TYP) SURFACE
2- A IN, FOOTING
T
8' MIN.
J-
2-
(TYP
d
6" CLEAN OUT \\—2-#4 f-S"
L2'0 MIN,---� 6,0 TYP. x 4 SIDESLG.
PVC PIPE
SECTION C-C'
45*
BEND
c CLEAN OUT DETAIL
rNOT TO SCALE tt
EXISTING CRUSHED PVC MEMBRANE
ROCK SURFACE
—L�
f
G&E ENGINEERING c A DiwWon of - CRX'compmy
ABOVEGROUND PIPE SUPPORT DETAIL/ 2
I -------- ENVIRONMENTAL CONSULTANTS
NOT TO SCALE s t1
NOT TO SCALE
SCALE
DESIGNED BY: SOUTHEAST TERMINAL SITE No. 4762 24898-04-B221 0
DRAWN BY: M� LIFE 2/24198 BP OIL COMPANY DRAWING Na. REV,
CHECKED 8 ATLANTA, GEORGIA 7401 OLD MOUNT HOLLY ROAD DETAILS
APPROVED CHARLOTTE, NORTH CAROLINA
DATE NO. REMSION BY Client Project Location_ FIG./SHEET No

`•
CONtOOLLER
•SH
•
S OFF SUMP Pwp �FLOO LEVEL TO 2OX OF SUMP CAPACITY
11 11 itlkltCH TO 1t I ylRESTART l IM VI I I
EXISTING
I• -,
NOT TO SCALE
-
ENGINEERING
A 4O#L '.X°CN4P4NY
ENVIRONMENTAL CONSULTANTS
of Date
Date
O 248rawing o. BP 01L COMPANY
�@V� Na, Drawing Na.
SOUTHEAST TERMINAL SITE No. 4762
CONTROLLER
MKI
ATLA TA, GEORGIA
JBU j4i�
7401 OLEO MOUNT HOLLY ROAD
CHARLOTTE, NORTH CAROLINA
SCHEDULE
Crown by
Checked By Appra d By Client
Project Location I
I Fig No.