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HomeMy WebLinkAboutNCG510277_Regional Office Historical File Pre 2018 (2)PPPan rk7rr,1MWichael From: Weaver, Charles Sent: Thursday, May 27, 2010 2:00 PM To: Bowser, Daniel P c: Taraban, Ron; Parker, Michael Subject: F: expired wastewater permit for BofA property at 401 North Tryon Street [21 Attachments: i ac e001.pnp, irmape002.Jpp; it d e003.Jp Dan thanks for the information, and for getting it to me so promptly. I'll make this CoC Inactive in BIM . Or From: Bowser, Daniel P Seat: Thursday, May 27, 2010 12:32 PM To: Weaver, Charms c: Taraban, Ron Subject: expired wastewater permit for BofA property at 401 North Tryon Street Charles, No further environmental work was noted in the file beyond S&ME involvement. See below . Dan Bowser Hydrogeologist ".C4�01r' onit Carolina Depiadmentof Environment and Natural Resources (0) a-217 dan.bowser@ncdenr.gov E-MAIL CORRESPONDENCE TO AND FROM THIS ADDRESS MAYBE SUBJECT TO THE NORTH CAROLINA PUBLiG R"coR es L.AW AND MAYBE DISCLOSED TO THIRD PARTIES. From: Al Quarles [mailto:AQuarles ads einc. om] Seat: Thursday, May 27 2010 12:21 PM To. Bowser, Daniel P Subject. RE: expired wastewater permit for`BofA property at 401 North Tryon Street Dart, S&ME has not worked on this site for many years. As we recall, the NPD S discharge permit was obtained for a subgrade parking deck dewatering system whore groundwater was impacted with petroleum products from UST releases. It was not part of a groundwater corrective action remediation system. We were not involved with the project during or after construction of the new building, however, we believe that the system, , was never activated since groundwater levels dropped after construction and dewatering was not necessary. The permit may have been renewed in the event that t P_ Pppppdewatering (and treatment and discharge of water) became necessary. the person to contact to find out more details. Thanks, Al Quarles, P.G. Senior Hydrogeologist -S&ME ENGINEERING INTEGRITY, S&ME, Inc. 9751 Southern Pine Boulevard Charlotte NC 282731M21 Ph: 704-523-4726, ext. 11657 Fax: 704-565-4929 Mobile: 803-984-6764 AgRarlesftsmeinc.corn I-A-1 P^M The building manager would be This electronic message and its attachments are forwarded to you for convenience and "for information only." The message may represent a summary with limitations, conditions and further explanations omitted in the interest of brevity and time constraints. The contents of this electronic message and any attachments may be preliminary and incomplete, subject to review and revision. If this electronic transmittal contains Findings, Conclusions or Recommendations, S&ME, Inc. will submit a follow-up hard copy via mail or overnight delivery for your records, and this hard copy will serve as the final record. In the event of conflict between electronic and hard copy documents, the hard copy will govern. This electronic message and any attachments transmitted with it are the property of S&ME, Inc, and may contain information that is confidential or otherwise protected from disclosure. The information this electronic message contains is intended solely for the use of the one to whom it is addressed, and any other recipient should delete this electronic message and destroy all copies. VER 4, Rev 1 — 031207 From: Bowser, Daniel P [mailto:dan.bowser@ncdenr,gov] Sent: Thursday, May 27, 2010 11:47 AM To: Al Quarles Subject: FW: expired wastewater permit for BofA property at 401 North Tryon Street Importance: High Al, Looking at the file it appears that nothing has been done at the site since the late 90s, this is intermediate, any work would be non -directed, as such can I assume that the system has been shut down, to satisfy Charles Weaver? See attached/below. Thanks Dan Bowser Hydrogeologist U North Carolina 0epartinsent, of Environment and Nattiral Resources (704) 235-2172 dan.bowser@ncdenr.gov E-mAiL CORRESPONDENCE TO AND FROM THIS ADDRESS MAYBE SUBJEC T"ro'rHE NORTH CAROLINA Joust to REcORDS LAWAND mAYBr DiscLosED To TRtRD PARTms, 2 PPPFPP' From: Taraban Ron Sent: Thursday, May 27, 2010 10:32 AM To: Bowser, Daniel P Subject: : expired wastewater permit for BofA property at 401 North Tryon Street Importance: High Rory Taraban - Ron.Taraban@ncdenr.gov North Carolina Department of Environment & Natural Resources Division of Waste Management 610 East Center Avenue, Smite 310 Mooresville, NC 25115 Ph; 70-63-1699 Fax. 70-663-600 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. From: Weaver, Charles Sent: Thursday, May 27, 2010 9.57 AM To: suzanne.fountain@bankofamerica.com Cc Taralan, Ron Subject. expired wastewaterpermit for BofA property at 401 North Tryon Strut Importance: High Ms. Fountain.' In 1995, Bank of America acquired a permit to discharge wastewater from its property at 401 North Tryon Street: The wastewater was from a system to remediate contaminated groundwater at the site. RofA was issued Certificate of Coverage NC 510277 under general Permit NCG510000 on /30/19 5. N G5102 7 was renewed by BofA in 1997 and 2001. A renewal notice was sent in February 2006; no response to the notice was received. A Notice of Violation was sent via Certified Mail to Mr. Lincoln Harris of RofA in June 2006; records from the LISPS show it was received on June 8, 2006 by Cynthia Leonard. No response to the NOV was ever received by the Division. NC 5102 7 expired on 9/30/ 006. Any discharge from the system after 9/30/2006 is ILLEGAL. Your name was included in Division records as a contact for this facility. Please let me know if RofA is still using the system, or when the system was shut down. If the system is still in operation, complete and return the attached renewal form IMMEDIATELY. There are also several unpaid annual fees to be resolved. O If the system has been shut dawn, I will pursue resolution with our inspectors in the NC DEIR Mooresville Regional Office. Thanks for your assistance with this matter: Charles H. Weaver NPDES Unit 3 +. NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. l a ; Jr., Secretary Alan W. #, Director June 5, 200 CERTIFIED MAIL);°,. RETURN RECEIPT REQUESTED Lincoln Harris Bank of America 525 North Tryon St, Suite 218 Charlotte,NC 2820 Subject. Notice of Violation Failure to Submit Permit Renewal Application Certificateof Coverage NCG510277 Transamerica Square site Mecklenburg County Dear Per ittee: NPDES General Permit NCG510000, under which the subject facility is covered, expires on September 30 2006. North Carolina. Administrative Code (15A NCAC 2H.0105(e)) requires that an application for permit renewal be filed at least 180 days prior to expiration of the current hermit. To satisfy this requirement, your renewal package should have been sent to the Division postmarked no later than ,April 3 2006 The Division has not received a renewal request for the subject CoC. This is a violation of your permit at fart 11. S. 10, which states "Any permittee that has not requested renewal at least 180 days prior to expiration..`. will subject the per ittee to enforcement procedures as provided in NCGS 143-215.+6 and 33 USC 1251 et. seq.". To prevent an assessment of civil penalties you must submit a completed permit application (see enclosed forms) no later than. Jame 19. 2006. If the system is inactive clue to lack of trust fund payments, but the'remediation equipment is still on site, the CoC should be renewed. If all remediation discharge from this facility has ceased and you wish to rescind this COG [or if you have any other questions], contact Charles Weaver of my staff. Mr. Weaver's telephone number, fax number and e-mail address are listed at the bottom of this page. Sincerely, �7 Alan W. Klimek, P.E. c: Central riles LIII+File 117 Mail Service Center, Raleigh, North Carolina 27699-1617 919 73-5983, extension 511 (fax) 919 733-0719 VISIT US ON THE INTERNET @ http://h2o,enr.state,ne.us/NPDES e-mail- charles.Weav r@ncmail.net A74LA. NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross, Jr., Secretary Alan W. Klimek, P.E., Director February 10, 2006 Lincoln Harris Bank of America 525 North Tryon St, Suite 218 Charlotte, NC 28202 Subject: NPDES Permit NCG510000 renewal Certificate of Coverage (CoC) NCG510277 Transamerica Square site Mecklenburg County Dear Permittee: The facility listed above is covered under NPDES permit NCG510000 for discharge of remerhated groundwater. NCG51 0000 expires on September 30, 2006. Federal (40 CFR 122.41) and North Carolina (15A NCAC 2H.0105(e)) regulations require that permit renewal applications must be filed at least 180 days prior to expiration of the current permit. If you have already mailed your renewal request, you may disregard this notice. To satisfy this requirement, the Division must receive your renewal request postmarked no later than Apdl & 2006. Failure to request renewal by this date may result in a civil assessment of at least $500.00. Larger penalties may be assessed depending upon the delinquency of the request. If any discharge from the remediation system will occur after September 30, 2006, your CoC must be renewed. Discharge of wastewater without a valid permit would violate North Carolina General Statute 143- 215.1; unpermitted discharges of wastewater may be assessed civil penalties of up to $25,000 per day. If you have halted remediation activity due to lack of trust fund money, but your site ranking from the Aquifer Protection Section requires future remediation & discharge, your CoC must be renewed. If all discharge has ceased at your facility and you wish to rescind this CoC [or if you have other questions], contact me at the telephone number or e-mail address listed below. Sincerely, Charles H. Weaver, Jr. NPDES Unit F E 7 cc: Central Files OM "M WOMMMOM"M NPDES File 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 One 512 North Salisbury Street, Raleigh, North Carolina 27604 NofffiCarohna Phone: 919 733-5083, extension 511 / FAX 919 733-0719 / charles.weaver@ncmail.net ;Vaturally An Equal Opportunity/Affinnative Action Employer— 50% Recycled/10% Post Consumer Paper J Ii LME ' F lary 1, 1997 ?ENNR North Main Street resvxlle, NC 23115 ition 1r. Rex Gleason :rend; NPDES Monitoring Report - Fourth Quarter 1996 General Permit NCG51 000 Certificate of Coverage NCG510277 Netionsl3enk; 401 North Tryon Street Charlotte, Mecklenburg County, North Caroline ME Project 1354-95-296F A Mr. Gleason- parting period'. NPDES Monitoring Report - Fourth Quarter 1996 S&ME Project 135 -95- 96F Transamerica - Monitoring/Sampling January 13, 1997 If you have any questions, please contact us at (7 4) 523-4725. Sincerely, SIZE=,Inc. �/ Al Quarles, L.G. Project Manager , Dane A. Herne, P.E. Environmental Manager c; Mr. Kent Polen, NetionsBank Ms. Ann Lofton, MCDEP Mr. Allen Schiff, NCDEHNR Mr. Tom Causey, The Harris Croup A,.A - s\ pds12 .rpt _2 TABLE 1. WATER TREATMENT SYSTEM DISCHARGE FLOW TRANSA ERICA SQUARE 401 NORTH TRYON STREET CHARLOTTE, NORTH CAROLINA FLOW CUMMULATIUE ELAPSED AVERAGE DATE METER FLOW TIME FLOW (gal) (gal) (day)glam} 7/1/96 213,570 213570 7/ /96 231,917 231,917 7 1.82 7/1/6 243,871 243871 7, 1.19 7/22/96 271,750 271750 7 2.77 7/29196 290,128 290,128 7 1.82 8/5/6 307,535 307,535 7 1.73 8/12/96 321,925 321,925 7 1.43 8/19/96 352,229 352,229 7 3.01 8/26/96 361,948 361948 7 0.96 8/ 0/ 6 380,238 380,238 4 3.18 9/4/96 392,120 392,120 5 1.65 916/96 396, 569 396,569 2 1.54 TABLE Ila. WATERTREATMENT SYSTEM SAMPLE ANALYSIS TRANSAMERICA SQUARE 401 NORTH T YON STREET CHARLOTTE, NORTH CAROLINA PARAMETER Units JUL AUGSEP Permit e 11 i CIA' �i All concentration In ugll (ppb) IAA = Not Applicable T = Not Tested ,August Lead Effluent sampled can August 15, 1996 rest\gprodate\environ\project\1 9 \ -29 t\npdes3 6.wb2 TABLE Ilb. WATER TREATMENT SYSTEM SAMPLE ANALYSIS TRANSAMERICA SQUARE 401 NORTH TRYON STREET CHARLOTTE, NORTH CAROLINA :R Units OCT NOV DEC Permit 1996 1996 1996 Average Limit -LUEIYT t Mon -Ave Daily -Max. Bd 10/3/96 11 /21 /96 12/5/ C /l NT NT NT NA NA NA ie ug/l NT NT NT NA NA NA ug/l NT NT NT NA NA NA ug/l NT NT NT NA NA NA ug/l NT NT NT NA NA NA ug/l NT NT NT NA NA NA u/l NT NT NT NA NA NA FLUENT L-d 10/3/96 11 /1 /6 12/5/96 /1 1.0 <1.0 <1.0 0 71.4 142.E 1 /l <1.0 1.0 <10 0 NA NA ug/l <1.0 <1.0 1.0 0 11 22 ug/l <1.0 <1.0 <1.0 0 NA NA ug/l 0 0 0 0 NA NA ug/l 71 6A 20 32 NA NA IIM/1 1A e-r A 179 gn All concentrations in ug11(ppb) NA = Not Applicable NT = Not Tested Cared\ prod t lenv ronlprojecti19 5195-2 6ftnpd s495,wb2 AUG;PRI 1( Pace Anayt C:P_Analvtinal Hung Tel: 7 75-909 Fax: 7 7 -90 1 August 08, 1996 Mr. Bill McGuinness SME 951 Southern Pine Boulevard Charlotte, NC 28241 RE. PACE Project No. 6676.513 Client Reference: Nations Bank 354-9-9E Dear Mr, McGuinness: Enclosed is the report of laboratory analyses for samples received July 26, 1996. Footnotes are given at the end of the report. f ,you have any questions concerning'this report, please feel free o contact us. Sincerely, Wt�,4 . U V1zc-e Kelly H. Wallace' Project Manager Enclosures REPORTP LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the, written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 800 Kinc y Avenue, Suite 100 " Hunteesville, 28078 Tel: 7 7 -90 2 Fax: 7 75-901 S&ME August 08, 1996 9751 Southern Pine Boulevard PACE Project Number: 6607265i13 Charlotte, NC -28241 Attn: Mr. Bill McGuinness Client Reference, Nations Bank 15-9-296E PACE Sample Number: 92 0643372 Date Collected: 07/26/96 Date Received: 07/26/96 Client Sample ID: Influent Parameter Units PRL Water METHOD DATE ANALYZED ORGANIC ANALYSIS PURGEABLE AROMATICS; 602 Methyl-t--butyl ether u/L 200 4500 08/06/96' Isopropyl ether ug/L 50 ND 0806/96 Benzene ug/L 50 470 08/06/96 Toluene ug/L 50 480 08/06/96 Chlorobenene u/Li 5o ND 08/06/96 Ethylbenzene ug/L 5o NO 8/06/96 ylenes, (total) ug/L 50 420 08/06/96 1,-Dichlorobenzene u/L 50 ND 08/06/96 1,2--Dichlorobenzene ug/L 5o ND 08/06/96 1,4--Dichlorobenzene u/L 5o ND 08/06/96 w Pace! Analytical Services, Inc. r 9800 Kincey Avenue, Suite 100 Huntersville,,NC 2 075 Tel.704-875-9092 Fax: 7 7 - 0 1 Mr. Bill McGuinness August 08, 1996 Page 2 PACE Project Number: 660726513 Client Reference. Nations Bank 1354-95-296E PACE Sample Number: 92 0643380 Date Collected. 07/26/96 DateReceived: 07/26/96 Client Sample 1D: Stripper Parameter Units PILL Effluent METHOD DATE ANALYZED ORGANIC ANALYSIS PUPGEABLE AROMATICS 602 Methyl-t-butyl ether /L 100 2200 08/06/96 Isopropyl ether u/L 1.0 ND 08/06/96 Benzene ug/L 1.0 21 08/06/96 Toluene u/L 1.0 21 08/06/96 horobenzene ug/L 1.0 ND 08/06/96. Ethylbenzene ug/L 1.0 1.0 08/06/96 ylne, (total,) ug/L 1.0 23 08/06/96 1,3-Dichlorobenzene ug/L 1.0 ND 08/06/6 1,2-Dichlorobenzene ug/L 1.0 NO 08/06/96 1,4-Dichlrobenzene u/L 1.0 ND 0/06/96 Pace Analytical Servic 9800 Kincey Avenue; St Pane n a lvt1 na Huntersville, NC PA Da Da Cl P Tel: 7 7 9092 Fax: 704-875-9091 McGuinness August 08, 1996 PACE Project Number: 660726513 Reference: Nations Bank 1354-9-6E ample Number: 92 0643399' all ected: 07/26/96 acei'ved: 07/696 Sample ID: Final ter Units PRL Effluent METHOD DATE ANALYZED 41C 'ANALYSIS )UAL PARAMETERS m /L 0.005 NO 239.2 08/01/96 ANALYSIS 3LE AROMATICS 60 -t-butyl ether' ug/L_' 10 320 08/06/96 ayl ether u/L 1.0' ND 08/06/96 a ug/L` 1.0 NO 08/06/96; a ug/L 1.0 ND 08/06/96 aenzene u9/L 1.0 ND 08/06/96 anzne a/L. 1.0 ND 08/06/96 , ('total) g/L 1.0 NO 08/06/96 whlorobenzene ug/L 1.0 ND 08/06/96 :hldrebenzene ug/L; 1.0 ND 08/06/96 :hlorObenzene ug/L 1.0 ND 08/06/96 Jata have been reviewed and are approved for release. I'Ec � ?t S. Harding Laboratory Operations REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Paste Analytical Services, Inc. 9800 Kinoey Avenue, Suite 100 ' Huntersville, NC 28078 Tel* 7 7 2 Fax: 704-875-9091 Mr. Bill McGuinness FOOTNOTES August 08, 1996 Page; 4 for pages 1 through 3 PACE Project Number: 660726513 Client Reference: Nations Bank 154-95-296E NO Not detected at or above the P L. PRE PACE Reporting Limit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, , except in full, without the written consent of Face Analytical Services, Inc. Pace .Analytical Services, Inc. 9800 I ncey Avenue, Suf#e 100 ■ ace Huntersville, NC 28078 Tel: 7 75-90 Fax: 704-878-9091 Mr. Ball McGuinness QUALITY CONTROL DATA August 08, 1996 Page 5 PACE Project Number: 660726513 Client Reference: Nations Bank 1-95--6 Lead Batch. 92 48915 Samples. 92 0643399 METHOD BLANK: Method Parameter Units PRL Blank. Lead mg/L 0.005 WD— SPIKE AND SPIKE DUPLICATE: Spike Spike Dupl Parameter Units PRL 92064138$ gSike Recv Recv RPD Lea m /L .005 t}.NO DeD OO 10 �4° LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE: Reference Dupl Parameter Units PRL Value Recv Recv RPD ea -mg/ - O.005 _ Q.Q2 1 100 4% im, Face Analytical Services, Inc. 9800 Vincey Avenue; Suite 100 xtical Fluntersville,NC 28078 Tel: 75 Fax: 7 75-901 Mr. Bill McGuinness QUALITY CONTROL DATA August 08, 1996 Page ' 6 PACE Project Number: 660726513 Client Reference: Nations Bank 1354-95-296E PURGEABLE AROMATICS Batch: 92 49131 Samples; 92 0643372,; 92 0643380, 92 0643399 METHOD BLANK: Method Parameter Units PRL Blank Met y - -butyl ether ug/L 1.0 N Isopropyl ether /L 1.0 NO Benzene ug/L 1.0 NO Toluene ug/L 1.0 NO Chlorobenzene ug/L 1.0 NO Ethylbenzone ug/L 1.0 NO Xylenes, (total) a /L 1.0 NO 1,3-Oichlorobenzene g/L 1.0 NO 1,2-Oichlrobenzene u/L 1.0, Nil 1,4-Cichlorobenzene ug/L 1.0 NO LABORATORY CONTROL SAMPLE. Reference Parameter Units PRL Value Recv Met yf--t-butyl ether ug/L 1.0 20 12 Isopropyl ether ug/L 1.0 20 100% Benzene ug/L 1.0 `` 20 100 Toluene ug/L 1.0 20 100 Chlorobenene ug/L 1.0 20 90 Ethylbenzone /L 1.0 20 105 Xyle es, (total) g/L 1.0 40 103 1,3-Dichlorobenzene ug/L 1.0 20 100 1,-Oichlorobenzene ug/L, 1.0 20 105 1,4- is l roben ene` ug/L 1.0 20 95 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Ser 9900 Kincey Avenue,'i Hntersville t Tel: 7Q Fax: 70 r. Bill McGuinness FOOTNOTES August 08, 1996 Page 7 for pages 5 through 6 FACE Project Numhe Client Reference: Nations Bank. 1 54- - 96E ND Net detected at or above the PRL. PRL RACE Reporting Limit RPD Relative Percent Difference REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, lthout the written consent of Pace Analytical Services, Inc. P^Am A"A-M11&jF+"2 329809 AA 3A M AM I I-,v ILE -al CHAIN -OF -CUSTODY RECORD Analytical Request Client B2�grt TO: Pace Che nt No. 4 k P.O. # Billinq Reference N. 4g4L, "Ieqtested Due Date: Sampled B (PRINT): PRESERVATIVES ANALYSES REQUEST 777 SAMPLE DESCRIPTION TIME MATRIX PACE NO. MEN= :�►� dr"1a tiP`� Pace An 9800 Kinc4 t August 1, 1996 Mr. Bill McGuinness S&ME 751 Southern Pine Boulevard Charlotte, ;MC 28241 roc. r)nr t' n- 4--* xa.. CCAOAC cnn va s—x.. — awe waa+,.m . .a.v wa:-s .✓ xr vac,. Dear Mr. McGuinness. Enclosed is the report of labortor August 05, '1996. Footnotes are given at the end of Tel, 704-875-909, Fax: 794-875-909, Banff rt. o contact us. Sincerely, bellyh �' llace Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Face Analytical Services, Inc. l i 9800 Kincey Avenue, Suite 100 Fluntersvlle, NC 28078 Tel: 704-875-909 Fax, 704-875-9091 S&ME August 1, 1996 9751 Southern Pine Boulevard PACE Project Number. 660805502 Charlotte, NC 28241 Attn: Mr. Bill McGuinness Client Reference: 1354-95-298E/Nations Bank PACE Sample Number, 92 0648498 Date Collected. 08/05/96 Date Received. 08/05/96 Influent Parameter Units PRL METHOD DATE ANALYZED INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Lead mg/L 0.050 0.25 239.2 08/08/96 ORGANIC ANALYSIS INDIVIDUAL PARAMETERS Isopropyl ether ug/L 20 NO 11 602 08/09/96 Methyl-t-butyl ether u/L 50 1800 602 08/09/96 PURGABLE'AROMATICS 602 Benzene ug/L 20 130 08/09/96 Toluene ug/L 20 180 08/09/96 Chlorobenzene ug/L 20 ND 08/09/96i Ethylbenz ne ug/L 20 NO 08/09/96' Xylenes, (total;) ug/L 20 170 08/09/96 1, - ichlorobenzene ug/L 20 ND 08/09/96 1,2-D3chlorobenzene ug/L 20 ND 08/09/96 1,4-Dichlorobenzene ug/L 20 ND 08/09/96` Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 untersville, NC 28078 Tel: 704-87 -9092 Fax: 704-875-9091 Mr. Bill McGuinness August 19, 1996 Page 2 PACE Project Number: 660805502 Client Reference: 1354-95-298E/Nations Bank PACE Sample Number: 92 0648501 Date Collected: 08/05/96 Date Received. 08/05/96 Client Sample ID: Effluent Parameter Units PRL METHOD DATE ANALYZED ORGANIC ANALYSTS INDIVIDUAL PARAMETERS Isopropyl ether u/L 1.0 ND 602 08/09/96 Methyl-t-Butyl ether /L 10 340 602 08/09/96 PURGEABLE AROMATICS 602 Benzene ug/L 1.0 NO 08/09/96 Toluene /L; 1.0 ND 08/09/96 Chlo oben ene ug/L 1.0 ND 08/09/96 Ethylbenzene ug/L 1.0 NO 08/09/96 ylees, (total) u/L 1.0 ND 8/1/96 1,3--Dichlorobenzene ug/L 1.0 ND 08/09/96 1,2-ichlorobenzene ug/L 1.0 ND 08/09/96 1,4-Dichl robenzene ug/L 1.0 NO 08/09/96 These data have been reviewed and are approved for release. i ~& Margaret S. Harding Manager, Laboratory'Operations REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Puce Analytical Services, Inc. Pace Anal) 9800 Kincey Plum Tel; 704-875-9 92 Fax; 04-87 -9 91 Mr. Bill !McGuinness FOOTNOTES August 19, 1996 Page 3 for pages 1 through 2 PAGE Project Number: 6608055C Client Reference: 1354-95-296/Nations Bank 11 Sample was diluted due to the presence of elevated concentrations of target/non-target compounds. NC Not detected at or above the PRL# PRE. PACE Reporting Limit REPORT OF LABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Face Analytical Services, Inc. Pace Analyt 9800 incey aP_P_ Ann1v 'lln-ai Hunte Tel: 704-875-9092 Fax: 704-875-99 1 Mr. Bill McGuinness QUALITY CONTROL DATA August 19, 1996 Page 4 PACE Project Number: 660805502 Client Reference: 1354- 5- /Nations Bank Lead Batch: 92 4916 Samples. 92 0648498 METHOD BLAND: Method Parameter Units PRL Blank Lead-mg/L 0.005 NU — SPIKE AND SPIKE` DUPLICATE'. Spike Spike Dul Parameter Units' PRL 920680332 SS ike Recv Recv RPD Lea___ mg/ 0.005 N 0.0 0 9 ` 6` LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE. Reference Dupl Parameter' Units PRL Value Rec Rev RPD ea _ mg/ 0.005 0,0 0 9 11. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pane Analytical Services, Inc. Face Analytical Services, Inc. 9800 Kinsey Avenue, Suite 100 untersville, NC 28078 Tel: 704-875-9092 Fax: 794-875-9991 Mr. Bill McGuinness QUALITY CONTROL DATA August 19, 196 Page 5 PACE Project Number: 660805502 Client Reference: 1 -9 -298E/Nations Bank Isopropyl ether Batch: 92 49392 Samples: 92 0648498, 92 0648501 METHOD BLANK, Method Parameter Units PRL Blank sopropyT ether g/L 1—.0 ND LABORATORY CONTROL SAMPLE: Reference Parameter Units' P L Value Recv IsopropyT`'ether ug/L 1.0 0 9O Para Analytic 9800 Kincey Au Par- _ Analvti(' a I Hunter Tel: 704-875-9 92 Fax: 7 4-875-9091 Mr. Bill McGuinness QUALITY CONTROL DATA August 19, 16 Page,6 PACE Project Number: 660805502 Client Reference: 1354-95-298E/Nations Bank PLIABLE AROMATICS Batch: 92 49252 Samples: 92 0648498, 92 0648501 METHOD BLANK: Method Parameter Units PRL Blank INDIVIDUAL PARAMETERS Methyl-t-butyl ether /L 1.0 N PURGEABLE AROMATICS Benzene ug/L 1.0 N Toluene ug/L 1.0 NO Chloenzen ug/L 1.0 ND Ethylbenzene ug/L 1.0 ND Xylenes, (total) ug/L 1.0 NO 1,3-ilrobenene` ug/L 1.0 ND 1,-Dichlobezene ug/L 1.0 ND 1,4-Dichlorobenzene ug/L 1.0 NO LABORATORY CONTROL SAMPLE: Reference Parameter Units` PRL Value Recv INDIVIDUAL PARAMETERS Methyl-t-butyl ether ug/L 1.0 20 85 PURGEABLE'AROMATICS Benzene ug/L ' 1.0 20 100 Toluene ug/L 1.0 20 100% Chlorobenene ug/L 1.0 20 100 Ethybenzne u/L 1.0 20 105 Xylenes, (total) u /L 1.0 40 105 1, -Dichl robenzene ug%L 1.0 20 110 1,2- ichlorobenzene ug/L 1.0 20 11 % 1,4-ichlerobenzen ug/L 1.0 20 110 Pace Analytical Services, Inc. . ` 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 0 75- 0 2 Fax, 04-875-9091 r. Bill McGuinness FOOTNOTES August 19, 1996 Page 7 for pages 4 through 6 PACE Project Number: 660805502 Client Reference: 154-95-298E/Nati`ons Bank NO Not detected at or above the PRL* PRL PAGE Reporting Limit RPD Relative Percent Difference REPORT OF LABORATORY TORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. CHAIN -OF -CUSTODY RECORD Analytical Request Client Revort To- J !' Pace Client No. , . Address Pi VeA, Bill To: Pace Pro' ct Mang er P.O. #1 BIIIIn Referen � :. Pace Pro`ect No. Phone Pro eat P ame 1 No. -Requested Due [sate. Sampled By (PRINT): PRESERVATIVES ANAL 5ES w REQ REQUEST z Lu Sampler Signatury Cate Sampled Z Cr cu cc rCL • • • C7 C47 ` _REMARKS v ,?a .., ���.?. v eF r..., c :�.,....:,.a a • �_ „^.. v v '�L �, »f q', •..� t2 �:...` vv m, to �, sti o u ,r..:.' " .w..: e k r u .. � $ ,, t '. a' „av `i,k, 1 `: %, _: 'GYL Y', f, :r•',. .,y, .: \v SR rr&. e1? C ttY "'s""`d FR ': r ., 9,6. .... S'"c�e rot. ' .. .'93`i �. c .„ 'left. ... .......,. <..� S cam` .:`2 � '�. �, . r.. w, e.,, „ ,. k.. , a._e '�S .i„ ,. � e � .. s '� ��,; k i � , y� .�y ,.,". e i�a }IL � � „, )rnment tp .l n,,► Ae i Pace Analytical Services, Inc. ' 9800 Kincey Avenue, Suite 100 untersvill , NC 28078 Tel; 704-875-9092 Pax: 704-875-9091 August 15, 1996 r. Bill McGuinness ME 751 Southern Piste Boulevard Charlotte, NC 28241 RE: PAGE Project No. 660808.53 ClientReference: 135-95-296EjPB-U Analysis Hear Mr. McGuinness: Enclosed is the report of laboratory analyses for samples received August 0, '1996. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free` o contact us. Sincerely, Kelly H. all ace Project Manager Enclosures'` REPORT F LABORATORYALYI This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersy1fe, NC 28078 Tel: 704-87 -9092 Fax: 704-875-9091 S&ME August 15, 1996 9751 Southern Pine Boulevard PACE Project Number: 660808503 Charlotte, NC 28241 Attn: Mr. Bill McGuinness Client Reference: 13-95-296EPB-U Analysis PACE Sample Number: 92 0681312 Date Collected:08/07/96 Date Received: 08/08/96 Client Sample ID: Effluent nd Parameter Units PRL Carbon METHOD DATE ANALYZED INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Lead m/L 0.005 0.005 23.2 08/09/6 These data have been reviewed and are approved for release. } Margaret S. Harding Manager, Laboratory Operations REPORTTANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services; Inc. Pace Analytical Services, Inc. 9800 Kiney Avenue, Suite 100 Huntersville, NC 2878 Tel: 704-875-9 9 Fax: 704-875-9 91 Mr. Bill McGuinness FOOTNOTES August 15, 1996 Page 2 for page 1 PACE Project Number: 660808503 Client Reference: 1354-95-296E/PB-U Analysis PRL PACE Reporting Limit REPORT OF LABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. M 9800 Kincey Avenue, Suite 100 * . Huntersville, NC 28078 Tel. 704-875-9092 Fax: 704-8 5-9091 Mr. Bill McGuinness, QUALITY CONTROL DATA August 15, 1996 Page 3 PACE Project Number. 660808503 Client Reference: 135-95-296E/PB-U Analysis . Lead Batch: 92 49208 Samples. 92 0611 METHOD BLANK: Method Parameter Units PRL Blank LeaF mg/L 0.005 ND SPIKE AND SPIKE DUPLICATE. Spike Spike Dpl Parameter Units PRL 9061967 Sake Recv Recv RPD Lead-mg/L 0.005 ND 0.025 08 Q 1 44% 4 ZATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE. Reference neter Units PRL Value g/L 0.00 5 6 REPORTT ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Ser f r 7'JVV fVl1t Vy mra tuc, Huntersville, h Tel; 704-f Fax; 044 Mr. Bill McGuinness FOOTNOTES August 15, 1996 Page 4 for page 3 PAGE Project Number: Client Reference: 134-95-296E/P_N Analysis NO Not detected at or above the PL. PRL PACE Reporting Limit RPD Relative Percent Difference REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc, Pi, 332571. 2 SA 2 - W, 161 CHAIN -OF -CUSTODY RECORD Analytical Request ATo: 4f r s � Pace Client No. Client l . wAddress Pace Pre'ect Manaer Yt It ! a t P.t . k ! Billin Reteren a Pace Pro'ect No. � Pro ct Name 11 o. F � �'"` r 'Requested Due Crate: Phone T Sampled By (PRINT}; .� .�.•--, �"`~� a,. � F'F�BSI�RATIUS REQUEST w Sampler Signature Crate Sampled fJ `' ITEM SAMPLE DESCRIPTION TIME MATRIX PACE NO 0 z 0 REMARKS .„ :., ,...� a; o, ,y,,;,... a f l�r v A "z ,..tea}v,. ., , ... 4 „'".'t v� < . U' ", sY .. �:. 'usi�.�y, 3 4,. ,., a '� , �.'S .4 � , w. , ,\ ., .. ,, ; „ :,,. ,,,.. ., . .•..., , „, h: x *' Additional Comments 01, Pace 9800 Kir aiaLy Qa--- Tel: 704-875-9092 Fax: 704-875-9091 October 09, 1996 Mr. Bill McGuinness S&ME 9751 Southern Pine Boulevard Charlotte, NC 28241 RE: PACE Project No. 660925.506 Client Reference: 1354-95-296-E/Nations Bank Dear Mr. McGuinness: Enclosed is the report of laboratory analyses for samples received. September 25, 1996. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, C4 Kelly H. Wallace Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Tel: 1 9751 Southern Pine Boulevard PACE Project Numb Charlotte, NC 28241 Attn: Mr. Bill McGuinness Client Reference: 1354-95-296-E/Nations Bank PACE Sample Number: 92 0684567 Date Collected: 09/25/96 Date Received: 09/25/96 Client Sample ID: Effluent Parameter Units PRL METHOD D, INORGANIC ANALYSIS INDIVIDUAL PARAMETERS MIJ NIC ANALYSIS e data have been reviewed and are approved for release. &14- aret S. Harding ger, Laboratory Operations REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace i 9800 Kit Ica I Mr. Bill McGuinness FOOTNOTES October 09, 1996 Page 2 for page 1 PACE Project Num Client Reference: 1354-95-296-E/Nations Bank NO Not detected at or above the PRL. PRL PACE Reporting Limit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical 9800 Kincy Ave WL Huntersv TeL Fax:> Mr. Bill McGuinness QUALITY CONTROL DATA October 09, 1996` Page 3 PAGE Project Numt Client Reference: 1354-95-296-E/Nations Bank Lead Batch. 92 50888 Samples: 92 0684567 METHOD BLANK, Method Parameter UnitsPRL Blank Lea mg/L 00.005 NO SPIKE AND SPIKE DUPLICATE: Sp' Parameter Units PRL 920684508 S ik R Lea leg/L 0.005 ND 0.025 LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE:- Reference Parameter Units PRL Value R Lead g/L 0.005 0a025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Aralyki 800 Kincey As Hunter T Fa: r. Bill McGuinness QUALITY CONTROL DATA October 09, 199E Page 4 FACE Project Nur Client Reference: 1354-95-296-E/Nations Ban- PURGABLE AROMATICS Batch: 92 51222 Samples: 92 064567' METHOD BLANK: Method Parameter Units PRL Blank Met -t-butyl ether ug/L 1.0 ND - Benzene ug/L 1.0 ND Toluene ug/L 1.0 ND` Chl orobenene ug/L 1.0 ND' Ethybenene ug/L 1.0 ND Xylenes, (total) ug/L 1.0 NO 1,3--Dichl robenzene ug/L 1.0 ND 1,2-Dichlorobenzene ug/L 1.0 NO 1,4-Dichlorobenzene ug/L 1.0 NO LABORATORY CONTROL SAMPLE: Reference Parameter Units PRL Value I et Y— -t--butyl ether g/L 1.0 0 Benzene gL 1.0 20 Toluene g/L 1.0 20 hlorobenene ug/L 1.0 20 Ethylbenzene ug/L 1.0 20 ylees, (total) ug/L 1.0 40 1,-Dichlorobenzene' ug L 1.0 20 1,-Dichlorobenzene ug/L 1.0 20 1,4-Dichlorobenzene ug/L 1.0 20 REPORTLABORATORY ANALYSIS This report shall not be reproduced, except in full,, without the written consent of Pace Analytical Services; Inc. Pace Anal) 9800 Kincey Mr. Bill McGuinness FOOTNOTES October 09, 199E Page 5 for pages 3`through 4 PACE Project Nun Client Reference: 13`54-95-295-EJNations Bank NO Not detected at or above the PRE. PRL RACE Reporting Limit RPO Relative Percent Difference REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. .;- f Phon Samph 7 CHAIN -OF -CUSTODY RECORD ' Analytical Request Re cart To: t' pace Client No. ! t Bill To: Pace Project Manager, RO. #t Billing Refer n1ce t f Pace Project No. t Pr ioM M.— f kln RFMARK V "I " - ' q N U'U 1 1'9 9 6 Pace Analytical Service 9800 Kincey Avenue, Sui Am A ca Huntersville, NC Tel: 704-87! Fax: 704-87,1 October 17, 1996 Mr. Bill McGuinness S&ME 9751 Southern Pine Boulevard Charlotte, NC 28241 RE: PACE Project No. 661003.510 Client Reference: 1354-95-296-E/Nations Bank Dear Mr. McGuinness: Enclosed is the report of laboratory analyses for samples received October 03, 1996. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. incerely, Wa CVrJ Kelly H. Wallace Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9850 Kincey Avenue, Suite 100 Ica Huntersville, SIC 28978 Tel: 704-875-9092 Fax, 704-875-9091 S&ME October 17, 1996 9751'Southrn Pine Boulevard PAGE Project Number: 661003510 Charlotte, NC 28241 Attn: Mr. Bill McGuinness Client Reference: 134-95.296-E/Nations Bank. ; PACE Sample Number. 92 0691717 Date Collected: 10/03/96 Date Received: 10/03/96 Client Sample ID, Effluent Parameter_ Units PRL METHOD DATE ANALYZED INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Lead mg/L 0.05 ND 239.2 10/09/96' ORGANIC ANALYSIS PURABLE AROMATICS 602 Methyl-t-butyl ether ug/L 5.0 71 1015/6' Benzene u/L 1.0 ND 10/5/6 Toluene ug/L 1.0 NO 10/15/96 Chlorobenzen ug/L 1.0 NO 10/15/96 Ethylbenz ne ug/L 1.0 ND 10/15/96 lenes, (total) ug/L 1.0 NO 10/15/96 1,3-Dichlorobenzene ug/L 1.0 ND 10/15/96 1,2-Dichlorobenzene ug/L 1.0 ND 10/15/96 1,4-Dichlorobenzene ug/L 1.0 NO 10/15/96 These data have been reviewed and are approved for release. 6-If-Margaret S. Hard; Manager, Laboratory Operations REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Anal) 9800 Kincey y CIA3 Huni Mr. Bill McGuinness FOOTNOTES October 17, 19 Page 2 for page 1 PACE Project N Client Reference: 1354-95-296-E/Nations Bank ND Not detected at or above the PRL. PRL PACE Reporting Limit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, withni it tho writtian c-.nn.qP.nt tif P;4t,.p Anq1vtir.n1 1;A.rvir,.Aq Inr Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 A Huntersville, NC 28078 Ada Tel: 704-875-9092 Fax: 704-875-9091 Mr. Bill McGuinness QUALITY CONTROL DATA October 17, 1996 Page 3 PACE Project Number: 661003 Client Reference: 1354-95-296-E/Nations Bank Lead Batch: 92 51263 Samples: 92 0691717 METHOD BLANK: Method Parameter Units PRL Blank Ue-a-d ig —/L D—.005 N-D— SPIKE AND SPIKE DUPLICATE: Spike 920691717 Spike Dupl Parameter Units PRL Effluent Recy Recy Lead mg/L 0.005 N—D 0.0250 ITH -lTF% LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE: Reference Dupl Parameter Units PRL Value Recv Recv R E-e-a-d ig­/ -L U—.O 0 5 1-13% -1 F5-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Mr. Dnrin FUH E Sarr MET Par Pace Analytic 9800 Kincey Av nt--A Annlvtl(--.ql Hunter~ I ill McGuinness QUALITY CONTROL DATA October 17, 199( 4 PACE Project NuT t Reference: 1354-95-296-E/Nations Bank ABLE AROMATICS ch: 92 51471 es: 92 0691717 FIX-44mm Method eter Units PRL Blank —butyl ether u -g/ —L 1—.0 WD— ne ug/L 1.0 ND ne ug/L 1.0 ND obenzene ug/L 1.0 ND benzene ug/L 1.0 ND es, (total) ug/L 1.0 ND d chl orobenzene ug/L 1.0 ND d chl orobenzene ug/L 1.0 ND dchlorobenzene ug/L 1.0 ND ATORY CONTROL SAMPLE: Reference lieter Units PRL Value ,T--t-butyl ether ug/L 1.0 Zo one ug/L 1.0 20 me ug/L 1.0 20 ,obenzene ug/L 1.0 20 benzene ug/L 1.0 20 ies, (total) ug/L 1.0 40 )ichlorobenzene ug/L 1.0 20 )ichlorobenzene ug/L 1.0 20 )ichlorobenzene ug/L 1.0 20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace An 9800 Kinci f--P- Annlvtinal HL # ; 4 W.W.M. Mr. Bill McGuinness FOOTNOTES October 17, 1996 Page 5 for pages 3 through 4 PACE Project Number: 6 Client Reference: 1354-95-296-E/Nations Bank NO Not detected at or above the PRL. PRL PACE Reporting Limit RPD Relative Percent Difference REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc, COC4# �006853* [ytical Request Page TT�7Report To: U�C Invoice To. M Sample ID Date Time Matrix cc Please specity any special reporting requirements. 4 nquishe Date Time Received By Date Time Temperature Sampled By Airbill # cO # �ustody Record & Analyticat Request Page' of Date. Report To: Turnaround. 5A)b Number: A;219 Invoice To: �. Pace 9800 K r. - Itinal .. I Mr. Bill McGuinness SME Pi 0. Box 78 Charlotte, NC 28241-7668 RE: PACE Project No. 661121.518 Client Reference: Nations Bank Dear Mr. McGuinness: Enclosed is the report of laboratory analyses for samples received November 21, 1996. Footnotes are even at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, Kelly . Wallace Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Aria 9800 Kince, _ _ Analvtinal Hug Tel: 74 Fax: 701 S&ME December';0, 1996 Wn INDI Leaf Box 7668 PACE Project Number' tte, NC 2241-7668 Mr.Bill McGuinness Reference: Nations Bank' ample Number: 92 072944 ' olleeted:` 11/21/6 eceived: 11/21/6 Sample ID: Effluent ter Units PRL System METHOD DATI NIC ANALYSIS DUAL PARAMETERS mg/L 0.005 0.025 239.2 C ANALYSIS BLE AROMATICS 602 -t-butyl ether ug/L 1.0 6.4 e u/L 1.0 N e ug/L ; 1.0 ND benzene ug/L' 1.0 ND enzee ug/L 1.0 NO s, (total) ug/L 1.0 NO chloobenene ug/L 1.0 ND hlobnene ug/L 1.0 ND chloobenene ug/L 1.0 ND data have been reviewed and are approved for release. et S. Warding r, Laboratory Operations REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc, Pace i 800 Kh ,� n�1 oral i r. Bill McGuinness FOOTNOTES December 02, 1 Page 2 for page I PAGE Project Nu,, Client Reference: Nations Bank ND Not detected at or above the PRL. PRL PAGE Reporting Limit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services„ Inc. Pace Analytical 800 Kincey Avel Huntersv Tel:: Fax: r. Bill McGuinness QUALITY CONTROL DATA December 02, 1996 Page 3 RACE Project Numb( Client Reference: Nations Bank Lead Batch. 92 52836 Samples: 92 0726944 METHOD BLANK. Method Parameter Units PRL Blank Lead mg/L .005 NO SPIKE AND SPIKE DUPLICATE: pi4 Parameter Units PRL 9067 S ke Re( Lea g L 0.005' 0.00 0.020 o-( LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE: Reference' Parameter Units PRL Value Re( Lea g L O.00S 020 TOY REPORT OF LABORATORY ANY I This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace An 9899 Vince !P- Analvtlnal Hu r. Bill McGuinness QUALITY CONTROL DATA December 02, 1996 Page 4 PACE Project Numb Client Referenced Nations Bank PURGEABLE AROMATICS Batch: 92 52776 Samples: 92 0726944 METHOD BLANK Method Parameter Units PRL Blank Met ; -t--butyl ether u/L 1:0G NU Benzene ug/L 1.0 NO Toluene ug/L 1.0 ND Chlorubenzene ug/L 1.0 NO thylbenzene /L 1.0 ND Xylen s, (total) ug/L 1.0 ND 1,3-Dchlorobenzene /L 1.0 ND 1,2-Dchlorobenzene ' ug/L 1.0 ND 1,4-Dchlorobenzene ug/L 1.0 ND LABORATORY CONTROL SAMPLE: Re ce Parameter units RL Value Re et ,yT-i-butyl ether ug/L 1:0 20 Benzene /L 1.0 20 9 Toluene u/L 1.0 20 9 Chlorobenz ne u /L 1.0 20 Ethyl benzene ug/L 1.0 20 9 Xylen s, (total) ug/L 1.0 60 8 1,3-Dchlorobenzene ug/L 1.0 20 9' 1,2-Dchlorobenzene ug/L 1.0 20 9 1,-Dchlorobenzene /L 1.0 20 9' REPORT OF LABORATORY ANALYSIS This report shell not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace 98009 nalvtinal Tel: 704-875- Fax: 74-875- r. Bill McGuinness FOOTNOTES December02, 1996 Page 5 for pages 3 through 4` PACE Project Number: 66 Client Reference: Nations Bank, ND Not detected at or above the PRL. PRL PACE Reporting Limit PD Relative Percent Difference REPORT F LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services„ Inc. P11--, 357814. "I CHAIN -OF -CUSTODY C Analytical Request Client A Re ort To: ' � � Pace Client No. t� Address ! L✓ % RIll To ' ` + t . µ Pace Pro`ect Mena' er ~ Y Pace Pro'e I cI rP,O. #1 Billing Reference ;` 1 Phone d Pro eot Name t No. t `Requested Due Date: Sampled y (PRINT),. PRESERVATIVES ANALYSES LU REQUEST: {# Sa per Signature Date Sampled {°"' > �* ac , {{yy {�f " L i � � ITEM SAMKE �6WRI"4* TIME IA;ATRw7�P2E—:NO. 0 Z Z 0 .. ., v. ..,F7773.4 ,r .v .. . ...\\ ,., %N. .u. .+`.`t.. q\ ,v - w\� b �. ..., A... MR "Wit", 2 ,.:. „. .... , r. G. �an4':..�,:R. us7 va ,.,c.v'.as.��..;.,¢ L Additional Comments u 1 Pace Analytical Services, Inc. 9800 Kinc y Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 December 18, 1996 r. Bill McGuinness S&ME P. 0. Box 7668 Charlotte, ;NC 28241.7668 RE; PACE Project No. 661205.503 ClientReference: 135 --95- 96- Dear Mr. McGuinness: Enclosed is the report of laboratory analyses for samples received December 05, 1996. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free o contact us. Sincerely, 1 j WC�Q2a<-Q Kelly H. llace Project Manager Enclosures REPORT OF LABORATORY ALY 1 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services,. 9800 Kincey Avenue, Suite Huntersville, NC 2 Tel: 704-875- Fax; 704-87 -G SME December 1, 1996 P. O. Box 7668 PACE Project Number: 6 Charlotte, NC 28241-7668 Attn: Mr. Bill McGuinness Client Reference: 1354--95-296- PACE Sample Number: 92 0734602 Date Collected. 12/05/96 Date Received: 12/05/96 Client Sample ID: Effluent Parameter Units PRL System METHOD DATE INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Lead mg/L 0.005 ND 239.2 12 ORGANIC ANALYSES PURGEABLE AROMATICS 602 Methyl-t-butyl ether ug/L 1.0 20 1 Benzene u/L 1.0 NO 12 Toluene ug/L 1.0 ND 1 Chlorobenzene ug/L 1.0 ND 12 Ethylbenzene ug/L 1.0 ND 12 Xylenes, (total) g/L 1.0 ND 12 1,3-Dichlorobenzene ug/L 1.0; ND 12 1,2-Dichlorobenene ug/L 1.0 ND 12 1,4-Dichlorobenzene u/L 1.0 ND 12 These data have been reviewed and are approved for release. N Margaret S. Harding Manager, Laboratory ;Operations REPORTLABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analyti 9899 Kincey A Hunte e Mr. Bill McGuinness FOOTNOTES December 18, 1996 Fade 2 for page 1 PACE Project Number. Client Reference. 1354-95-26-F ND Not detected at or above the P. PRL PACE Reporting Limit REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc, Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Ic Huntersville, NC 28078 Tel: 704-875-9092 Fax; 70-875-9091 Mr. Bill McGuinness QUALITY CONTROL DATA December 18, 1996 Page 3 PACE Project Number: 661205503 Client Reference: 1354--95-296- Led Batch: 92 5359 Samples. 92 0734602 METHOD BLANK AND SAMPLE DUPLICATE: Duplicate Method of Parameter Units PRL Blank 92073 608 2 0738608 RPD U a _ Ong/L 0—.00 N U SPIKE AND SPIKE DUPLICATE: Spike Spike Dupl Parameter Units PRL 920738608 Spike Recv Re RPD Lead- mg/L 0.00Nil 0.020 TIN LABORATORY CONTROL SAMPLE. Reference Parameter Units PRL Value Rec lea 1g/L U.08 A.2U lfl REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services,;Inc. Pace Analytic< 9800 Kincey Avi Jf1n.qIvt*1 r- q I Hunters Tel: 70 -87 -90 2 Fax: 70-875-90 1 Mr. Bill McGuinness = QUALITY CONTROL DATA December 18, 1996 Page 4 PACE Project Number: 661205503 Client Reference: 13 4-95-296-F PURGEABLE AROMATICS' Batch: 92 53622 Samples: 92 0734602 METHOD BLANK: Method Parameter Units PRL Blank. Met , --t-butyl ether ug/L 1— ND Benzene ug/L 1.0 NO Toluene ug/L 1.0 NO Chlorobenzene /L 1.0 ND" Ethylbenzene g/L 1.0 ND lee, ('total) g/L 1.0 N 1,3-Dichlurobenzene /L 1.0 ND' 1, 2--Di chl urobelzene /L 1.0 ND 1,-Dichlorobenzene ug/L 1.0 ND SPIKE AND SPIKE DUPLICATE: 920734602 Spike Effluent Spike Dul Parameter Units PRL System S ike Recv Rev RPD et -t-butyl ether g/ 1.0 D 100 Benzene g/L 1.0 ND 20 95 90% 5% Toluene ug/L 1.0 ND 20 100 95% 5% Chlorobenzene g/L 1.0 ND`` 20 125% 125% Ethybenzne ug/L 1.0 ND 20 100 90% 1% lees, (total) ug/L 1.0 ND 40 105 9% 10% 1,3-Dichlorobenzene u L 1.0 NO 20 95% 95% 0% 1,2-0ichlerobenzene ug/L 1.0 ND 20 90% 95% 1, -ichlbrobe zene ug/L 1.0 ND 20 95% 5% % LABORATORY CONTROL SAMPLE: Reference Parameter Units PRL Value Recv Met y -t-butyl ether g/L 1.0 20 Benzene ug/L 1.0 20 95% Toluene ug/L 1.0 20 95% Chlorobenzene ug/L 1.0 20 15% Ethylbenene ug/L , 1.0 20 100 Xlees, (total) ug/L 1.0 40 100% REPORT OF LABORATORY ANALYSIS This report shall not be reproduced„ except in full;` without the written consent of Face Analytical Services, Inc. Face Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28078 Tel: 704-875-9092 Fax:704-875-9091 Mr. Bill McGuinness QUALITY CONTROL DATA December 18, 1996 Page 5 PACE Project Number. 66120550: Client Reference: 1354-95- 6- PURGEABLE AROMATICS Batch: 92 5362 Samples: 92 0734602 LABORATORY CONTROL SAMPLE: Reference Parameter Units PRL Value Rec c `Torobenzene ug,%L . t 2 D 1,2-D cbloroben e e jL 1.0 20 95 1,4-D chlorobenzene ug%L 1.0 20 1 G` REPORT OF LABORATORY ANALYSIS This report shall not be reproduced„ except in full, without the written consent of Pace Analytical Services, Inc, Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 ,a A Huntersville, NC 28078 A;;3 Ica Tel:-TO4-875-9092 Fax: 704-875-9091 Mr. Bill McGuinness FOOTNOTES December 18, 1996 Page 6 for pages 3 through 5 PACE Project Number: 6612055 Client Reference: 1354-95-296-F NC Na calculation due to value below detection limit. NO Not detected at or above the PRL. PRL PACE Reporting Limit RP D Relative Percent Difference REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc, Client '� t , , , • * *. * ••* fl •. • *� .. III N , • sDate Samp .* * • NOSAMPLE DESCRIPTION TIME MATRIX PACE NO. • r ►� es EI j tionai Comments State of North Carolina Department of Environment, Health and Natural Resources r Division of Environmental Management James B. Hunt, Jr., Governorgo do 11,1111=1 i�� Jonathan . owes, Secretary A. Preston Howard,Jr., P.E., Director NATURAL cacrn S August 30, 1995 SEP I 1995 r. Kent B. Poles . Environmental Analyst W t MARACERV Nations Bank 441 gum r' Environmental Services Department TX1 - 9 -51-0 901 Main Street Floor 51 Dallas, 'Texas 75202-3714 Subject: Certificate of Coverage Issuance General Permit 10000 Cert. of Coverage NCG510277 NationsBank 401 North Tryon Strut - Chariotte Mecklenburg County Dear Mr. Polenz: n accordance with your application for an NPDES discharge permit received June 28, 1995 by the Division, we are herewith forwarding the subject Certificate of Coverage under the state-NP ES general permit for groundwater remediation facilities and one set of final approved plans and specifications. .Authorization is hereby granted for the construction and operation of a ;31,000 GPD groundwater remediation system consisting of a 200 gallon oil/water separator with a 30 gallon product wn , a 275 gallon sump with a 0.5 hp tr sfe ;sump, a 3 tray aif stripper with a 300 cfm (minimum) btow,�r, a 0.5 hp transfer pump, dual particulate filters in parallel, and dual carbon adsorption units in series with discharge of treated wastewater into Little Sugar Creek. This Certificate of Coverage is issued pursuant to the requirements of North. Carolina and the US Environmental Protection Agency Memorandurn of Agreement dated December 6, 1983 and a�=° vnbsequently amended. f any parts, measn�,=,,'=nt frequencies or sampling requirements contained in this general permit are unacceptable to you y,-=c have the right to submit an individual permit application and letter requesting coverage under an indii(id-ial permit, unless such demand is made, this decision shall be final and binding. Please take notice 4his permit is not transferable. Part 11, EA. addresses the requirements to he followed in case of change of ownership or control of this discharge. The Authorization to Construct is issued in accordance with Part 111, Paragraph 2 of NPFS Permit No. NCG5 10000, and shall be subject to revocation uaiess the wastewater treatment facilities are constructed in accordance with the conditions and limitations stpecified in Pe it No. WOW In the event that the facilities fail to perform satisfactorily, including the creation of nuisance conditw° ns, the Permittee shall take immediate corrective action, including those as may be regdred by this Envision, such as the construction of additional or replacement wastewater treatment or disposal facilities.. P.O. Box 29535, lies;:, North Carolina_27C26- 535 Telephone 919-73 -5083 FAX 919-733-9919 n Equal opportunity Affirmative Action Employs: 0% recycled/ 10% past -consumer paper Permit No. 10000 COC NCG510277 Authorization to Construct NationsBank Page 2 , e Mooresville Regional Office, telephone number (704)663-1699, shalt be notified at least forty- eight (48) hours in advance of operation of the installed facilities so that an in -place inspection can be made. Such notification to the regional supervisor shall be made during the normal office hours from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. Upon completion of construction and prior to operation of this permitted facility, a certification must be received from a professional engineer certifying that the permitted facility has been installed in accordance with the NPDES Permit, the Certificate ofCoverage, this Authorization to Construct and the approved plans d specifications. bait the Certification to the Permits and Engineering Unit, P.O. Box 29535, Raleigh, NC 2762+ -0535. A copy of the approved plans d specifications shall be maintained on file by the Pennittee for the life of the facility. Failure to abide by the requirements contained in this Authorization to Construct may subject the Permittee to an enforcement action by the Division of Environmental Management in accordance with North Carolina General Statute 143-215.6A to 1 3- 1 . C The issuance of this permit does not preclude the Permittee from complying with any and all statutes; rules, regulations, or ordinances which may be required by the Division of Environmental Management or permits required by the Division of Land Resources, the Coastal Area Management :Act or y Federal or Local other governmental permit that may be requi f you have any questions or need additional information, please contact Dana Bolden, telephone number ;919/733-50 , extension 518. Sincerely; ..ul SS -Pled By .: "d A Goodrich A. Preston Howard, Jr., P.E. Central Files Permits and Enfrineering Unit "' ing d e ' ieabon Unit Facilities Assessment Unit William McGuinness, I.mG., S&ME Mooresville Regional Office, Groundwater STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HENATURAL RESOURCES DIVISION OF ENVIRONMENTAL MANAG GENERAL E M ERTI`I ATE OF" VRA 7"T TO DISCHARGE PETROLEUM CONTAMINATED GROLNDWATER AND SMMAR WASTEWATERS ER THE NATIONAL I' L T N I IIAR ELIMMINATI N SYSUM In compliance with the provision of North Carolina General Statute 143- 15.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental ental agement Commission, and the Federal Water Pollution Control Act, as amended, NationsBmk is hereby authorized to construct and operate or continue operation of a groundwater treatment system consisting of an oil/water separator, an air stripping system and carbon filtration for petroleum contaminated groundwater or similar waste streams with the discharge of treated wastewater from a facility located at 401 North 'Tryon Street Charlotte Mecklenburg County to receiving waters designated as Little Sugar Creek k in the Catawba River Basin in accordance with the effluent limitations, monitoring requirements; and other conditions set forth in Parts 1,11,111 and IV of General Permit No. NCG510000 as attached, This certificate of coverage shall become effective October 1, 1995, ; This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this the 29th day of August, 19 h; A. Preston Howard, Jr., P.E., Director Division of Environmental Management y Authority of the Environmental Management Commission ".` ry Yt4 l� "` � � /✓Y • yyy },, iet�'tu*4 t „ o. :CS rk1 ,[�^,',�" k �, r�� � � •''� .i^,`. '�e't y • r^. ;° Q't � t:�f �°t�r�,w, _ t • F r r" f e A t ;c.J High c rw 3 rcanr d it DIS GE POINT yvoc � { \ 0r 3 e700 { C` `.�� ,� ,r.':'�,.. ✓ �,�k It a`iT) sb' f F;d 1 eT j wow • D ow"a. ,► • RECEIVING WATER-- UT`T`E.: SUGAR CREEK STORMMTER DRAINAGESYSTM REF ES TOPOGRAPHIC MAP, EAST, CHARLOTTE, REV, 197E l.T.S. TREATED WATERDISCHARGE FIGURE 1111, CHECKED BY' � TO RECEIVING WATER DRAWN SY° 401 NORTH TRYCN STREET JHC CHARLOTTE, NORTH CAROLINA -jATE: 1_ENMRONMENTAL SERMCES JOB NO: _