NCG500208_Regional Office Historical File Pre 2018

State of North Carolina IqT41
Department of Environment,
Health and Natural Resource;; w
Divisionof Water Quality lit r
AM
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.., Director July 2,17
John W. Anderson JUL li'' 1 19
`l~illett Chemical, Inc.
P.O. Box 579
Pineville, NC 28134
... dti .i rl"V
Subject:.Certificate of Coverage No, NCG500208
Renewal of General Permit
"Tillett Cherrdcal, Inc.
Mecklenburg County
Dear Pe ittee. '
In accordance with your application for renewal of the subject Certificate of Coverage, the Division is forwarding
the enclosed General Permit. This renewal is valid until July 31, 2002. This permit is issued pursuant to the
requirements of North Carolina General Statute 143-215 .1 and the Memorandum of Agreement between Forth
Carolina and the U.S. Environmental Protection Agency dated December 6,1983. if any parts, measurement
frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to request
an individual permit by submitting an individual permit application. Unless such demand is made, this certificate
of coverage shall be final and binding.
The Certificate of Coverage for your facility is not transferable except after notice to the Division. Use the enclosed
Permit Name/Ownership e form to notify the Division if you sell or otherwise transfer ownership of the
subject facility. The Division may require modification or revocation and reissuance of the Certificate of Coverage. '
If your facility ceases discharge of wastewater before the expiration date of this permit, contact the Regional
Office listed below at (7 4) 66 -16 9Once discharge from your facility has ceased, this pe t may be rescinded.
This permit does not affect the legal requirements to obtain other permits which may be required by the Division of
Water Quality, the Division of Land Resources, Coastal Area Management Act or any other Federal or Local
govermnental permit that may`be required.
If you have any questions concerning this permit, please contact the NPDES Group at the address below.
Sincerely,
cc: Central Files fvpl� A. Preston Howard, Jr., P.E.
NPD S File`
Facility Assessment Unit
P.O. Box 29535 Raleigh, North Carolina 2 -0535 (919) 7 -5083 FAX [phone] p&e*dem.ehnr.state.nc.us
n Equal Opportunity Affirmative Action Employer 0% recycled 110% post -consumer paper

STATE OF NORTH CAROLINA
DEPARTMENT OF
CERTI
TO DISCHARGE NON-0
BLOWDOWN, CONDENSATE,
HYDROELECTRIC Of
NAIMNAL RQUIMANI DISCHARGE
C-xj-.L IL A
1:3�00
0. NC G500208
ATi N SYSIEM
and regulations promulgated and adopted by the No Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Tillett Chemical, Inc.
is hereby authorized to discharge
non -contact cooling water, condensate and other similar wastewaters
from a facility located at
Tillett Chemical, Inc.
316 College Street
Pineville
lei ecIdenburg County
to receiving waters designated as subbasin 30834 in the Catawba River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth
in Parts 1, 11, 111 and IV of General Permit No. NCG500000 as attached.
This certificate of coverage shall become effective August 1, 1997.
This certificate of coverage shall remain in effect for the duration of the General Permit.
Signed this day July 24, 1997.
A. Preston Howard, Jr., P.E., Director
Am
of Water Quality
By Authority of the Environmental Management Commission

•. nv
r: o1.•R
!DDMMUNITY
Mate of North Carolina
CJepartment of Environment, 3 99
W*A
Health and Natural Resources ru ,
Division of Environmental Manag
fllii
James B. Hunt, Jr., Govermr
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
September 30,193
P 2 8 1993
TILLETT CHEMICAL INC
P.C. BOX 579,316 COLLEGE ST.
PINEVILLE NC 28134 Subject: TILLETr CHEMICAL INC
Certificate of Coverage NCG500208
General Permit NCG50000
Formerly NP ES Permit NCO048607
Mecklenburg County
Dear Per itteex
e Division of Environmental Management has recently evaluated all existing individual permits for potential
coverage under general permits currently issued by the Division.. 15A N.C.A.C. 2H.0127 allows the Division to
evaluate groups of permits having similar discharge activities for coverage under general permits and issue
coverage where the Division finds control of the discharges more appropriate in is manner. The Division has
determined that the subject discharge qualifies for such coverage. Therefore, the Division is hereby issuing the
subject Certificate of Coverage under the state-NPDES general permit no. NCG500000 which shall void NPDES
Permit NC0048607. This Certificate of Coverage is issued pursuant to the requirements of North Carolina and the
US Environmental Protection Agency Memorandum of Agreement dated December 6,1983 and as subsequently
ended:
If any parts, measurement frequencies or sampling requirements contained in this general permit are unacceptable to
you., you have the right to submit an individual permit application, associated processing fee and letter requesting
coverage under an individual permit. Unless such demand is made, this decision shall be final and binding. Please
take notice this Certificate of Coverage is not transferable. Part II, EA. addresses the requirements to be followed
in case of change of ownership or control of this discharge.
In the event that the facilities fail to perform satisfactorily, including the creation of nuisance conditions, the
Permittee shall tape inunediate corrective action, including those as may be required by this Division, such as the
construction of additional or replacement wastewater treatment or disposal facilities. Construction of any
wastewater treatment facilities will require issuance of an Authorization to Construct from this Division.
Failure to abide by the requirements contained in this Certificate of Coverage and respective general permit may
subject the Permittee to an enforcement action by the Division of Environmental Management in accordance with
North Carolina General Statute 143-215.6A to 14-215.6C. Please note that the general permit does require
monitoring in accordance with federal law. The monitoring data is not required to be submitted to the Division
unless specifically requested, however, the permittee is required to maintain all records for a period of at least
three (3) years.
Post Office Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity ° ative Action Employer 5WIo recycled -101/6 post -consumer paper

JOHN W. ANDERSON
TILLET17 CHEMICAL INC
Certificate of Coverage, No. NCG500208
e issuance of this Certificate of Coverage is an administrative action initiated by the Division of
Environmental Management and therefore, no fees are due at this time. In accordance with current rules, there
are no annual administrative and compliance monitoring fees for coverage under general permits. The only fee
you will be responsible for is a renewal fee at the time of renewal. The current permit expires ,July 31,1997.
This coverage will remain valid through the duration of the attached general permit. The Division will be
responsible for the reissuance of the general permit and at such time, you will be notified of the procedures to
follow to continue coverage under the reissued permit. Unless you fail to follow the procedures for continued
coverage, you will continue to be permitted to discharge in accordance with the attached general permit.
e issuance of this Certificate of Coverage does not preclude the Permittee from complying with any and all
statutes, rules, regulations, or ordinances which may be required by the Division of Environmental Management
or permits required by the Division of Land Resources, the Coastal Area Management Act or any Federal or
Local other governmental permit that may be required.
If you have any questions or steed additional information regarding this matter, please contact either the
Mooresville Regional Office, Water Quality Section at telephone 'number (704) 6 3-1699, or a review engineer i
the NPDES Groin in the Central Office at telephone number 919/733-5083.
cc. Mooresville Regional Office S' erely,
Central Files
A. Preston Howar r., P.E.

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL AGEMENT
GENERAL PERMIT NO. NCG500000
CERTIFICATE OF COVERAGE No. NCG50020
TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER BLOWDOWN,
CONDENSATE D SIMILIAR WASTEWATERS UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North. Carolina General Statute 143-21.1, other lawful standards and regulatior
promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water
Pollution Control Act, as amended,
TILLETT CHEMICAL INC
is heresy authorized to discharge non -contact cooling water, cooling tower and bailer blowdown wastewater from a
facility located at -
TILLETT CHEMICAL INC
Mecklenburg o ty
to receiving waters designated as the UT SUGAR CREEK/CATAWBA RIVER BASIN
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts L II, III ar
IV of General Permit No. NCG500000 as attached.
This certificate of coverage shall become effective November 1, 1993.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day, September 30,1993.
9A. Preston Howar , Jr., P.E.,Director
Division of Environmental Management
By Authority of the Environmental Management Commission

Permit No. NCO(
STATE OF NORTH CAROLINA
DIVISION OF ENVIRONMENTAL MANAGEMENT
P E R M I T
pgiS
To Discharge Wastewater Under the NATIONAL
POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215. 1,
other lawful standards, and regulations promulqated and adopted by the North
Carolina Environmental Management Commission, and the Federal Water Pollution
Control Act, as amended,
TILLETT CHEMICAL COMPANY
is hereby authorized to discharge wastewater from a facility located At
Pineville
on College Street
Me(klenburg County
to receiving waters designated as an unnamed tributary to Sugar Creek in the Catawba
River Basin.
Ala A. A- AA
1, 1987
29, 1992
,is day Of February 25, 1987
R. PAUL WILMS, DIRECTOR
DIVISION OF ENVIRONMENT
BY AUTHORITY OF THE ENN
MANAGEMENT COMMISSION

Tillett Chem
VIER SHEET
any
f IIII„ :011 UI II bCI[I# ,.a tI#L.F'U. l:::i VW
C" waters in the Catawba ',Riven Basin.

— .-.. ..:. .. ......i r ax an we. s:+s R� M .A. AO.Fi J.#A':,►7: xR. 67
During ,the period beginning on the effective dateof the permit and lasting until expiration,
the permittee is authorized to discharge from outfall(s) serial number(s) 001.
Such discharges shall be limited and monitored by the permittee as specified below:'
Effluent Characteristics Dischar a Limitations Monitoring Requirements
kg day`(lbs/day)' Other Units (Specify) Measurement Sample *Sample
Daily Avg. Daily Max. Daily Avg. Daily Max. Frequency 'Type Location
Flog Monthly Instantaneous E
temperature * ** Monthly Grab E,U,D
kesidual Chlorine *'** ** Monthly Grab E
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER
*Sample locations: E Effluer.
**The temperature of the effluet
receiving stream of more than
'he permittee sh
the temperature of the
— 4-4. u=u&F—L uL a j.v - ex eea
a
>ly;if chlorine is
added to the
cooling water.
Fri ation from the
Division of
Environmental Management prior
coaling wager (See
Part III of
this Permit)
0 standard units near ,greater than 9.0 standard units and shall be
»�
.t by grab samples
ra m
'loating solids or
visible foam
in other than trace amounts.
e''
0
cra ,

Part l
Permit I
;CHEDULE OF COMPLIANCE
folllowing schedule:
requirement.
14

C. MONITORING AND REPORTING
1. Representative Sampling
Samplescollected and measurements taken as required herein
shall be characteristic, of the volume and nature of the
permitted discharge. Samples collected at a frequency less
than daily shall be taken on day and time that is
characteristic of the discharge over the entire period which
the sample represents.
. Reporting
U^ n 4 4• ^ a _ _ —....».. 1 A. ,,,. ... 9,, a.......... w...� � .,.._ .....� � L ..... _......... _ _ .. ._ ..,_ .,..,._. r. L. t :. a
r
N
Lnitions
Act or "the Act": Th
t
Copies or it eser ana aii otner
be submitted to the following
meat
ederal Water Pollution Control
ter Act, as' amended, 1.C.C.
wl et. seq.
The "daily average" discharge means the total: diseharcre
W_ j+v aa,.sa,a.%-1 4aa %A"M L:Ly C&V=xL Caw 4&.M.A6wit+R 3.l ?BF .k..: lJ M.. :3. dki.M.lEC:4A
the summation of all the :measured daily discharges by
weight divided by the number of days sampled during the
calendar month when the measurements were made.
c. The "daily maximum" discharge means the total discharge
by weight during any calendar 'day.
I

d. DEM, or Division: means the Division of Environmental
Management, Department of Natural Resources and Community
Development.
e. EMC: used herein means the North Carolina Environmental
Management Commission.
f. Flow, M3/day (MGD): The flow limit expressed in this
permit is the 24 hour average flow, averaged monthly. It is
determined as the arithmetic mean of the total daily flows
recorded during the calendar month.
g. Arithmetic Mean: The arithmetic mean of any set of
values is the summation of the individuals values divided by
the number of individual values.
h. Geometric Mean: The geometric mean of any set of values
is the Nth root of the product of the individual values
where N is equal to the number of individual values. The
geometric mean is equivalent to the antilog of the
arithmetic mean of the logarithms of the individual values.
For purposes ofi calculating the geometric mean, values of
zero (0) shall be considered to be one (1).
i. Composite Sample: These samples consist of grab samples
collected at equal intervals and combined proportional to
flow, a sample continuously collected proportionally to
flow, or equal volumes taken at varying time intervals. If a
composite sample is obtained from grab samples, the
following requirements apply. The intervals between influent
grab samples shall be no greater than hourly. Intervals
between effluent grab samples shall be no greater than
hourly except where the detention time of the wastewater in
the facility is greater than 24 hours, in which case, the
interval between grab samples shall be no greater in number
of hours than the detention time in number of days;
provided, however, in no case may the time between effluent
grab samples be greater than six hours nor the number of
grab samples less than four during any discharge period of
24 hours or less.
j. Grab Sample: Grab samples are individual samples
collected over a period of time not exceeding 15 minutes:
the grab sample can be taken manually.
1 6

. Test Procedures
I cxj. « zaa..La sLAcuu vL u-cenzion snaxi ire extended during the
course of any unresolved litigation or if requested by the
Division ' of Environmental Management or the Regional
Administrator of the Environmental Protection Agency.

II GENERAL CONDITIONS
MANAGEMENT REQUIREMENTS
. Change in Discharge
All discharges authorized herein shall be nnnsi tof with
any pollut<
or at a 1
a violati(
expansions,
which will
of pollutar
application
effluent l
the AEM of
may be mop
previously
. Noncompliance
The permit
central of
division as
hours or on
first kn awle
. Any
facility
punts
characte
sludge
w ..
. . .
Wilk

Persons reporting such occurrences by telephone shall also
filea written report in letter form within 15 days
following first knowledge of the occurrence.
3. Facilities Operation
The permittee shall at all times maintain in good working
order and operate as efficiently as possible all treatment
or control facilities or systems installed or used by the
permittee to achieve compliance with the terms and
conditions of this permit.
4. Adverse Impact`
The permittee shall take all reasonable steps to minimize
any adverse impact to navigable waters resulting' from
noncompliance with any effluent limitations specified in
this permit including such accelerated or additional
monitoring as necessary to determine the nature and impact
of the noncomplying discharge.
. Bypassing
Any diversion from or bypass of facilities is prohibited,
except M where unavoidable to prevent loss of life or
severe property damage,', or (ii) where' excessive storm
drainage or runoff would damage any facilities necessary for
compliance with the effluent limitations and prohibitions of
this permit. All: permittees who have such sewer bypasses or
overflows of this discharge shall submit, not later than six
months from the date of issuance of this permit, detailed
data or engineering estimates which identify:
a. The location of each sewer system bypass or
overflow.-
. The frequency, duration and quantity; of flow from
each sewer system bypass or overflow.
The permittee shall report by telephone to either the
central office or appropriate regional office of the
division as soon as possible but in no case more than 24
hours or on the next working day following the occurrence or
.first' knowledge of the occurrence of any diversion from o
bypass of facilities,
19

6. Removed Substances
Solids, sludges, filter backwash, or other pollutants
removed in the course of treatment or control of wastewaters
shall be disposed of in accordance with 'NCCS' 143-21 .1 and
in a manner such as to prevent .any pollutant from such
materials from entering waters of the State or navigable
waters of the United .States.
7. Fewer Failures
The permittee is responsible for maintaining adequate
safeguards to prevent the discharge of untreated or
inadequately treated wastes during electrical power failures
either by means of alternate power sources, standby
generators or retention of inadequately, treated effluent`.
8. (inshore or Offshore Construction
This permit does not authorize or approve the construction
of any onshore or offshore physical structures or facilities
or the undertaking of any work in any navigable waters*
B. RESPONSIBILITIES
. Right of Entry
The permittee shall allow the Director of the Division of
Environmental Management, the Regional Administrator, and/or+
their; authorized representatives, upon the presentations of
credentials:
a. To enter upon the pe ittee's premises where an
effluent source is located or in which any records are;
required to be kept under the terms and conditions of
this permit; and
b. At reasonable times to have access to and copy any
records required to be kept under the terms and
conditions of this permit; to inspect any monitoring
equipment or monitoring method required in this permit,
and to sample any discharge: of pollutants.
Q
x

"ransfer of Ownership or Control
This permit is not transferable, In the event of any
charge _in control or ownership of facilities from which the
+ • • • to - . ;: .. _ _ �, .... � .. ——
Knowingly making any; false statement -on -any -such' -report -may
result in the imposition of criminal penalties as provided
for in NCGS 143-215.1( ) (2) or in Section 309 of the
Federal Act.
4. Permit Modification
After notice and opportunity for a hearings pursuant to NCGS
143-2I5.1(b) (2) and NCGS 14-215.1(e) respectively, this
permit may be modified, suspended, or revoked in whole or in
part during :its term for cause including, but not limited
to, the following.
a. Violation of anyterms or conditions' of this permit,-
b. Obtaining this permit by misrepresentation or failure
to disclose fully all relevant facts: or
c. A change in any condition that requires either a`
temporary or permanent reduction or elimination of the
authorized discharge.
11

. Toxic Pollutants
Notwithstanding Part II, -4 above, if a toxic effluent
standard or prohibition (including any schedule of
compliance specified in such effluent standard or
prohibition) is established under Section 307(a) of the Act
for a toxic pollutant which is preset in the discharge, if
such standard or rohibition is more stringent than any
limitation for suci pollutant in this permit, this permit
shall be revised or modified in accordance with the toxic
effluent standard prohibition and the permittee so notified.
. Civil and Criminal Liability
Except as provided in permit conditions on "Bypassing" (Part
I1, - and "lower Failures" (Part II, A- ), nothing in
this permit shall be construed to relieve the permittee from
any responsibilities, liabilities, or penalties for
noncompliance pursuant to NCCB' 143-153, 43-215.6 o
Section 309 of the Federal Act,; 33 USC 1319. Furthermore,
the permittee is responsible for consequential damages, such
as fish kills, even though the responsibility for effective
compliance may be temporarily suspended.
. oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the
institution of any legal action or relieve the permittee
from any responsibilities, liabilities, or penalties to
which the permittee is or may be subject to under NCGS
143 225.7,5 et seq. or Section ;311 of the Federal Act, 33 USC
1321. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the
responsibility for effective 'compliance may be temporarily
suspended.
8. Property Rights
The issuance of this permit' does not convey any property
rights in either real or personal property, or any exclusive
privileges, nor does it authorize any injury to private
property or any invasion of personal :rights, nor any
infringement of Federal, State or local: laws or regulations.
1 12

Severability
The provisions of this permit are severable. and if an
UU�.. 9WA6 eAA %.,�.. a z1tt-.L Lo any circumstance is held
nvalid, the application of such provision to other
circumstances, and the remainder of this permit shall not be
affected thereby.
10. Expiration of Permit
Permittee is not authorized to discharge after the
expiration date. In order to receive authorization to
discharge beyond the expiration date, the permittee shall:
submit such information, forms, and fees as are required b
the agency authorized to issue permits no later than 180
days prior to the expiration date. Any discharge without
permit after the expiration will subject the permittee to
enforcement procedures as provided in NCGS-143-215.6, and 33
USC 1251 et seq.
1

I OTHER REQUIREMENTS
- - � -v cz T-ei _ °one compliance o
permitted facility with the current groundwater
P
Reopener
.iit shall be modified or
.-->. e-r ♦ as ,jw s as&f \'&t W. L L.d.i RC %,-Ltlan
Water Act, if the effluent guideline or water 'quality standard
so issued or approved:
1. contains different conditions or is otherwise more
stringent than any effluent limitation in the permit; or
. controls any pollutant not limited in the permit.
1 14

F. Toxicity Repener
Part III Continued
Permit No. NC>O048607
This permit shall be modified, or revoked and reissued to
incorporate toxicity liritatlons and monitoring, requirements in the
event toxicity testing or other studies conducted on the effluent
or receiving stream indicate that detrimental effects may be
expected in the receiving stream; as a result of this discharge;.
G. The permittee shall' not use any biocides except these: approved in
conjunction with the permit application. The permittee shall
notify the Director in writing not later than ninety (90) days
prior to instituting use of any additional biocide used in cooling
systems which may be toxic to aquatic life other than those
previously 'reported 'to the Division of Environmental Management.
Such notification shall include completion of Biocide Wor%shee't
Form 101 and a map locating the discharge point and receiving.
stream.

t4q
lff
* r NATURAL
a'I�ESOIJIRCES AMD
Y..tr>trrt"
'1992
State of North Carolina REQUAL LiffiCE
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor A. Preston Howard Jr. PE
William W. Cobey, Jr., Secretary Acting Director
September 14, 192
r. John W. Anderson
Tillett Chemical, Inc.
P.C. Sox 579
Pineville, NC 28134
Subject: NPDES Permit No. NCO048607
Tillett Chemical Inc.
Mecklenburg County
Dear Mr. Anderson;
In March 2, 1992 the Division of Environmental Management issued NPDES Permit No..
NCO148607 to Tillett Chemical, Inc. A -review of the permit file has indicated that an error'
was inadvertently made in the permit. Accordingly, we are forwarding herewith modifications to
the subject permit to correct the error. These: permit modifications include the addition of a
statement saying that monitoring requirements for Total Residual Chlorine only apply if
chlorine is added by the permittee to the cooling water. The upstream monitoring for
temperature mint remain to insure that the discharge is not increasing the temperature of the
receiving stream.
Please find enclosed an amended effluent page which should be inserted into your permit. The
old page should be discarded. All ether terms and conditions contained in the original permit
remain unchanged and in full effect. These permit modifications are issued pursuant to the
requirements of North Carolina General Statutes 14-15.1 and the Memorandum of Agreement
between North Carolina and the U. S. Environmental Protection Agency.
If any parts, measurement frequencies or sampling requirements contained in this
permit are `unacceptable to you, you have the right to an adjudicatory hearing upon written
request within thirty :30) days following receipt of this letter. This request must be in the
farm of a written petition, conforming to Chapter 150B of the North Carolina general Statutes,
and filed with the Office e of Administrative Hearings, Post Office drawer 27447, , Raleigh, forth
Carolina 27611-47. Unless such demand is made, this decision shall be final and binding.
Pollution Prevention Pays
P.O. Box 27,687, Raleigh, North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affmative Action Employer

If you have any questions concerning these permit modifications, please contact Mr. Randy
Kepler at telephone number 19/733-5583.
Sincerely yours,
'A. Preston Howard Jr., P
Acting Director
. Mr. Jim Patrick ,PA
Central Flle
Permits and Engineering

A� (). EFFLUENT LIMrrATIONS AND MONITORING REQUIREMENTS FINAL Permit No. NCO04860
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial number till,. Such discharges shall be limited and monitored by the permittee as specified below:
affluent _ Characlerlsup. 12 har slim Mgnitoringent�
Y
Units (sgjgffy MeasuremepiSa 1e *
U^n. Avcr, va naillu, Uaw. f u�
Flow Monthly Instantaneous
Temperature Monthly Grab E,D
Total Residual Chlorine*** Monthly Grab E
SHALLTHERE BE NO CHROMIUM, C, OR COPPER DED TO THE COOLING WATER.
SampleLocations: E - Effluent, U - tips , D - Downstream
* The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than .°C: and in
no case cause the ambient water temperature to exceed 32.0'C .
Monitoring requirements only apply if chlorine is added to the cooling water:
e permittee shall obtain authorization from the Division of Environmental Management prior to utilizing any biocide in the cooling water (See
Part III of this Permit).
The pH shall not be less than 6.0 standard units nor greater than . standard units andshall be monitored monthly at the effluent by grab
sample
There shall he no discharge of floating solids or visible foam in other than trace amounts.

RESotrRets Nit
t
State of North Carolina 4 =UE WAML Off ICE
Department of Environment, Health and Natural Resources
Division of Environmental ement
Sit North SatisburY SRaleigh, North Carolina 27611
James G. Martin, Governor George T'.'Eve Ph.D
Will' W. Cebey, 3., SecretaryDirector
March1992'
John W. Anderson
P. O. Box 579
316 College Street
Pineville, NC 28134
Subject; NPDES Permit No. NCO048607
Tillet Chemical Inc.
Dear , Anderson
Mecklenburg County
In accordance with your application for discharge permit received on November 4, 1991, we
e forwarding herewith the subject state - NPDES permit. 'Ibis permit is issued pursuant to the
requirements of North Carolina. General Statute 143-215 .1 and the Memorandum of Agreement
between North Carolina and the US Environmental Protectinn a `enc da
If any parts, mei
unacceptable to you,
thirty ` 0) days follo
petition, conforming
Office of Administral
-7447. Unless such dt
permit are
tst within With the
na is maae, tots decision shall be final and binding.
Jis nertnit is not tr sfe ble. P' II, .4. addresses the requirements to
be followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirements to obtain other permits which may be
required by the Division of Environmental :Management' or permits required by the Division of
Land Resources, Coastal Area I agement Act or any other Federal or Local governmental permit
that may be requ"
If you have any questions concerning this permit, please contact Mr. Randy Kepler at
telephone number 919/733-5083
Sin008
ce t J�ed by
Doh for
George T. Everett
cc: Mr. Jim Patrick, EPA
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 9I -7 3-7015
An Equal oppornmity Affmnative Action Employer'

Permit No. NCO048607
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
TO DISCHARGE V�
Kt EQLLUIANI DIN'
In compliance with the provision of North Carol:
'
is hereby authorized to discharge wastewater from a faci
316 College
Pineva
Mecklenburg
d Inc.
ty located at
treet
bunty
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in
This permit shall become effective April 1, 1992
This permit and the authorization to discharge shall expire at midnight on August 31, 1996
Division of Environmental,
By Authority of the Envin
uiagement

Permit No. NCO048607
rCOVERSBEET
ac.
. Continue to discharge non contact cooling water from one outfall located at Tillett Chemical,
Inc., 316 College Street, Pineville, Mecklenburg County (See Part III of this Permit), and
2. Discharge from said treatment works at the location specified on the attached map into an
unnamed tributary to Sugar Creek which is classified Mass C waters in the Catawba River
Basin.

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A. 0. EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL Permit No. NCO048607
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial 'number 001. Such discharges shall be limited and monitored by the permittee as specified below:
Effluent CharactqrIllip Discharge Limitations
UnIts (spSSIfy M20112ring Reaulrements
I Measurement Sa pie *giamizl
Mon. AMg. Pajjy__J&n Mon. Avo. Ra ily Max, Ereguency iY-P—e Loqallm
Flow Monthly Instantaneous E
Temperature Monthly Grab E,U,D
Total Residual Chlorine Monthly Grab E
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.
*Sample Locations: E - Effluent, U - Upstream, D - Downstream
** The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than 2.8 degrees
C and in no case cause the ambient water temperature to exceed 32 degrees C.
The permittee shall obtain authorization fi-om the Division of Environmental Management prior to utilizing any biocide in the cooling water (See
Part III of this Permit).
The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored monthly at the effluent by grab
sample..
There shall be no discharge of floating solids or visible foam in other than trace amounts.

existing facilities at o of
PART I
with Final Effluent Limitations ' specified for discharges in
schedule:
t Final Effluent Limitations by the effective date of the
le the operation and maintenance necessary to operate the
cency.

Part II
Page I of 14
PART ii
STANDARDO i ONS FOR DES PERMITS
1.
The Director of the Division of Environmental Management.
2. M gr Dhision
Means the Division of Environmental Management, Department of Environment, Health
d Natural Resources.
.
Used herein means the hire Carolina Environmental Management Commission.
. act °'the Act' -
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended,
33 USC '1251, et. seq.
5.
a. The "monthly average discharge" is defined as the total mass of all "ly discharges
sampled and/or measured during a calendar month on which daily discharges are
lit.
re" is defined as the total mass of all daill
of pollutant calculated from it is the "ma)
identified a "wily " in Part I of
ie permit.4

flaw at the treatment system, or
(3) a single, continuous sample collected over a 24 hour period proportional
to the rate of flow.
In accordance with (1) above, the time interval between influent grab samples shall be
no greater than once per hour, and the time interval between effluent grab samples shall
be no greater than once per hour except at wastewater treatment systems having a
detention time of greater than hours. In such cases, effluent grab samples may be
collected at time intervals evenly spaced over the 24 hour period which are equal in
number of hours to the detention time of the system in number of days. However, in
no case may the time interval between effluent grab samples be greater than six (6)
hours nor the number of samples less than four ( during a 24 hour sampling period.
» Grab Sample: Grab samples are individual samples collected over a period of time not
exceeding 15minutes; the grab sample can be takenrn a y.
. Calculation cif M s
a Arithmetic Mean: Ile arithmetic mean of any set of values is the summation of the
individual values divided by the number of individual values.

Pan I[[
Page 4 of 1
b. GeometricMean: The geometric mean of any set of values is the Nth root of the
product of the individual values where N is equal to the number of individual values.
The geometric mean is equivalent to the antilog of the arithmetic mean of the logarithms
of the individual values. For purposes of calculating the geometric mean, values of
zero (0) shall be considered to be one (1),
c. Weighted by Flow Value: Weighted by flow value means the summation of each
concentration " es its respective flow divided by the summation of the respective _
flows.
10. Calm Uav
calendar day is defined as the period from midnight of one day until midnight of the next
day. However, for purposes of this permit, any consecutive 24-hour period that
reasonably represents the calendar day may be used for sampling.
1L o,sance
Ahazardous substance means any substance designated under 40 CFR Part 116 pursuant
to Section 31 of the Clean Water Act
12. Toxic Pollutant
toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean ter
Act.
SECTION
I. Duty to mole
The DerTnittee roust comply with all conditions of this permit. Any permit noncompliance
, i i . i • '
i y* R i uii
i-
i 1OW&IMMIM• i r'
t • i o•I R R• a
NO . %,@FW—
at any person who violates a per
IM,
criminal penalties of $5,000 to $50,000 per day of violation, or imprisonment` for not
more than 3 years, or both. Also, any person who violates a pennit condition may be
assessed an administrative penalty not to exceed $10,000 per violation with the
maximum amount not to exceed $125,000. [Ref. Section 309 of the Federal Act 33
U.S.C. 1319 and 40 CFR 122.41 (a)

Part II
Page 5 of 1
. Under state law, a daily -civil penalty of not more than ten thousand dollars ($10, )
per violation may be assessed against any person who violates or fails to act in
accordance with the terms, conditions, or requirements of a permit. [Ref. North
Carolina General Statutes § 14-215.6 (a)]
. trot^
The permittee shall take all reasonable steps to minimize or prevent any discharge in
violation of this permit which has a reasonable likelihoodof adversely; affecting human
health or the environment.
3,l Liability
Except as provided in permit conditions on "Bypassing" (Part 11, CA.) and "Power
Failures" (Part H, C.7.), nothing in this permit shall be construed to relieve the permittee
from any responsibilities, liabilities, or penalties for noncompliance pursuant suant to NCGS
1 3- 15.3,143-215.6 or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the
permittee is responsible for consequential damages, such as fish kills,even though the
responsibility for effective compliance may be temporarily suspended.
4. "mil s Ttabtlity
Nothing in this permit shall be construed to preclude the institution of any legal action or
relieve the permittee from any responsibilities, liabilities, or penalties to which the permittee
is or may be subject to under NCS 143-215. et seq. or Section 311 of the Federal Act,
33 USG 1321. Furthermore, the permittee is responsible for consequential damages, such
as fish kills, even though the responsibility for effective compliance may be temporarily
suspended.
. Prsrtv RiLrhts
e issuance of this permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or
any invasion of personal rights, nor any infringement of Federal, State or local laws or
regulations.
6. whore or h► ns coon
This permit does not authorize or approve the construction of any onshore or offshore
physical structures or facilities or the undertaking of any work in any navigable waters.
7 "`
W.
e provisions of this permit are severable, and if any provision of this permit, or the
application of any provision of this permit to any circumstances, is held invalid, the
application of such provision to other circumstances, and the remainder of this permit, shall
not be affected thereby.

Part 11
Page
8. Iu lion
e permittee shall furnish to the Permiti Issuing Authority, within a reasonable time, any
information which the Permit Issuing Authority may request to determine whether cause
exists for modifying, revoking and reissuing, or terminating this permit or to determine
compliance with this permit. The permittee shallalso furnish to the Permit Issuing
Authority upon request, copies of records required to be kept by this permit.
9.
If the permittee wishes to continue an activity regulated y this permit after the expiration
to of this permit, the permittee must apply for and obtain a new permit
10. F °an of P "t
e permittee is not authorized to discharge after the expiration date. In order to receive
automatic authorization to discharge beyond the expiration date, the permittee shall submit
such information, forms, and fees as are required by the agency authorized to issue permits
no later than 180 days prior to the expiration date. Any discharge that has not requested
renewal at least 180 days prior to expiration, or any discharge that does not have a permit
after the expiration and has not requested renewal at least 180 days prior to expiration, will
subject the pe' "ttee to enforcement procedures as provided in NCGS' 143-215.6 and 33
USC 1251 et. s
11.Si gag= RQUinrlum=
All applications, reports, or information submitted to the Permit Issuing' Authority shall be
signed and certified"
a. All permit applications shall be signed as follows:
(1) For a corporation. by a responsible corporate officer" For the purpose of this
Section, a responsible corporate officer means: (a) a president, secretary, treasurer
or vice president of the corporation in charge of a principal business function, or
any other person who performs similar polio or decision making functions for the
corporation, or (b) the manager of one or more manufacturing production or
operating facilities employing more than 250 persons or having gross annual sales
r expenditures exceeding 25 million (in second quarter 1980 dollars), if authority to
sign documents has been assigned or delegated to the manager in accordance with
corporate procedures.
(2) For a partnership or sole proprietorship. by a general partner or the proprietor,
respectively; or
(3) For a municipality, Mate, Federal, or Mather public agency. by either a principal
executive officer or ranking elected official..
b. All reports required by the permit and other information requested by the Permit Issuing
Authority shall be signed by a person described above or by a duly'; authorized
representative of that person. A person is a duly authorized representative only if:
0) Ile authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility
for the overall operation of the regulated facility or activity, such as the position of
plant manager, operator of a well or well field, superintendent, a position of

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Part 11
Page 8 of 14
. per Qp=�Qn and Mainlo=
e permittee shall at all times properly operate and maintain all facilities and systems of
treatment and control (and related appurtenances) which are installed or used by the
permittee to achieve compliance with the conditions of this permit. Proper operation and
maintenance also includes adequate laboratory controls and appropriate quality assurance
procedures. This provision requires the operation of back-up or auxiliary facilities or
similar ilar systems which are installed by a permittee only when the operation is necessary to
achieve compliance `ith the conditions of the permit.
3.
t shall not be a defense for a permittee in an enforcement action that it would have been
necessary to halt or reduce the permitted activity in order to maintain compliance ce the
condition of this permit.
4.n of Tram nt Facilities
a. Definitions
(I) "Bypass" means the known diversion of waste streams from any portion of a
treatment facility including the collection system, which is not a designed or
established or operating made for the facility.
) "Severe property age" means substantial physical damage to property, damage
to the treatment facilities which causes them to become inoperable, or substantial
d Dermanent loss of natural resources which can reasonably be expected to occur
in the absence of a bypass. Severe property damaged s not mean economJ
caused by delays in production.
b. Bypass not exceeding limitations.
The permittee may allow any bypass ` to occur which does not cause effluent limit
to be exceeded, but only if it also is for essential maintenance to assure efl
operation. These bypasses are not subject to the provisions of Paragraphs c. t
this section.
c. Notice
(1) Anticipated bypass. If the permittee knows in advance of the need for a byl
shall submit prior notice, if possible at least ten days before the date of the b
including an evaluation of the anticipated quality and affect of the bypass.
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated t
as required in Part I, E. 6. of this permit. (24-hournotice).
d. Prohibition of Bypass
(I Bypass is prohibited and the Permit Issuing Authority may take enforcement aci
against a permittee for bypass, finless:
() Bypass was unavoidable to prevent loss of life, personal injury or se`
property damage;

Part 11
Page 9 of 14
(b) There were no feasible alternatives to the bypass, such as the use of auxiliary
treatment facilities, retention of untreated wastes or maintenance during normal
periods of equipment downtime. This condition is not satisfied if adequate
backup equipment should have been installed in the exercise of reasonable
engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance;
(c) The permittee submitted notices as required under Paragraph c. of this section.
(2) The Permit Issuing Authority may approve an anticipated bypass, after considering
its adverse affects, i the Permit Issuing Authority determines that it .t the
three conditions listed above in Paragraph d. (1) of this section.
.Il
a. Definition.
"Upset " means an exceptional incident in which there is unintentional and
temporary noncompliance with technology based permit effluent limitations because of
factors beyond the reasonable control of the permittee. An upset does not include
noncompliance to the extent caused by operational' error, improperly designed treatment
facilities, inadequate treatment facilities, lack of preventive maintenance, or careless or
improper operation.
b. Effect of an upset.
An upset' constitutes an affirmatives defense to an action brought for
noncompliance with such technology based permit effluent limitations if the
requirements of paragraph c. of this condition are met. No Bete nation made during
administrative review of claims that noncompliance was caused by upset, and before an
action for noncompliance, is final administrative ` action subject to judicial review.
c. Conditions necessary for a demonstration of upset.
A permittee who wishes to establish the affirmative defense of upset shall demonstrate,
through properly signed, contemporaneous operating lags, or other relevant evidence
that:
(a) An upset occurred d that the permittee can identify the cause(s) of the upset;
(b) The permittee facility was at the time being properly operated-, and
(c) The permittee submitted notice of the upset as required in Part , E. 6. ) ) of
this permit.
t.
(d) The permittee complied with any remedial measures required under Part II, B. 2. of
this permit.
d. Burden of proof.
In any enforcement proceeding the permittee seeking to establish the occurrence of an
upset has the burden of proof.

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pan Il
Page 12 of 14
g. InsWr.1jQLi and En
The permittee shall allow the 'Director, or authorized representative, upon the
presentation of credentials and other documents as may be required by law, to;
a. Enter upon the in 's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the
conditions of this e t
c. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance
or as otherwise ise authorized by the Clean Water Act, any substances or parameters at any
location.
SECTION E. REPORTING REOUIREN4ENTS
1, Chance in Discharae
All discharges authorized herein shall be consistent with the terms and conditions of this
permit. The discharge of any pollutant identified in this permit more frequently than at a
level in excess of that authorized shall constitute a violation of the permit.
2" Rlanud Chanees
e permittee shall give notice to the Director as soon as possible of any planned physical
alterations or additions to the permitted facility. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for
dete °ning whether a facility is a new source in 40 CFR Part 122.29;(b); o
b e alteration or addition could significantly change the nature or increase the quantity
of pollutants discharged. This notification applies to pollutants which 'are subject
neither to effluent limitations in the permit, nor to notification requirements under 40
CFR Part 12.42 a) (1).
. ei lJoncornlai ce'`
The permittee shall give advance notice to the Director of any planned changes in the
pe `tted facility or activity which'may result in noncompliance with permit requirements.
TrAnefor
except after notice to the Director.
incorporate such either requ

Part II
Page 13 of 14
5. lytonitorin
Monitoring results shall be reported at the intervals specified elsewhere in this permit
.= Monitoring results must be reported on a Discharge Monitoring Report ) (See
Part H. D. 2. of this permit).
. If the permittee monitors any pollutant more frequently than required by the permit,
using test procedures specified in Part H, D. 4. of this permit, the results of this
monitoring shall included in the calculation and reporting of the data submitted'in the
D
c. Calculations for all limitations which require averaging of measurements shall utilize
arithmetic mean unless otherwise specified ifi y the Director in the permit.
6. TT. nt: r ur Reno a
a The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment. Any information shall
be provided orally within 24 hours from the time the permittee became aware of the
circumstances. A written submission shallalso be provided within 5 days of the time
the permittee becomes aware of the circumstances. The written submission shall
contain a description of the noncompliance, and its cause, the period f noncompliance,
including enact dates and tunes, and if the noncompliance has not been corrected, the
anticipated' time it is expected to continue; and steps taken or planned to reduce,
eliminate, and prevent reoccurrence of the noncompliance.
b. The following shall be included as information which must be reported within 24 hours
under this paragraph.
(A) Any unanticipated bypass which exceeds any effluent limitation in the permit.
(B) Any upset which exceeds any effluent limitation in the permit.
(C) Violation of a maximum daily discharge limitation for any of the pollutants listed by
the Director in the permit to be reported within 24 hours.
c. The Director may waive the written report on a case -by -case basis for reports under
paragraph b. above of this condition if the oral' report has been received `thin 24
hours.
7. ` cr &-ngg=liance
;e permittee shall report all instances of noncompliance not reported under Part H. E. 5
d 6. of this permit at the time monitoring reports are submitted. The reports shall contain
the information listed in Part H. E. 6. of this pernift.
. Other lnf "on
Where the permittee becomes aware that it failed to submit any relevant facts in a permit
application, or submitted incorrect information in a permit application or in any report to the
Director, it shall promptly submit such facts or information.

maintained uncler this permit, inclucung monitoring reports or reports of co po nce or
noncompliance shall, upon conviction, be punished by a fine of not more than 1 , per
violation, or by imprisonment for not more than o years per violation, or by bath.

A. C_QnStMcdQB
No constructioi
capacity or to cl
Plans and Spec-,
and written app
B Qmundwateur
The permittee
Management, ci
of this NPDES
C. Changes in This!
The permittee
believe:
a. That any a(
PART 111
OTHER REQUIREMENTS
of wastewater treatment facilities or additions to add to the plant's treatment
inge the type of process utilized at the treatment plant shall be begun until Final
ications have been submitted to the Division of Environmental Management
)val and Authorization to Construct has been issued.
Qnj rind
call, upon written notice from the Director of the Division of Environmental
nduct groundwater monitoring as may be required to determine the compliance
)ermitted facility with the current groundwater standards.
igrgeS Toxic Substa=
call notify the Permit Issuing Authority as soon as it knows or has reason to
ivity has occurred or will occur which would result in the discharge, on a
r A-+
discharge will exceed the highest of the following "notification levels";
(1) One hundred n-Acrograms per liter (100 ug/1);
(2) Two hundred micrograms per liter (200 ug/1) for acrolein and acrylonittile; five hundred
micrograms per liter (500 ug/1) for 2.4-dinitrophenol and for
2-methyl-4.6-dinitrophenol; and one milligram per liter (I mg/1) for antimony;
(3) Five (5) times the maximum concentration value reported for that pollutant in the permit
application.
b. That any activity has occurred or will occur which would result in any discharge, on a
non -routine or infrequent basis, of a toxic pollutant which is not limited in the permit, if
that discharge will exceed the highest of the following "notification levels";
(1) Five hundred micrograms per liter (500 ug/1);
(2) One milligrain per liter (I mg/1) for antimony;
(3) Ten (10) times the maximum concentration value reported for that pollutant in the perniit
application.

Part TlI Permit No. NCO04 607
D. Toxicity Condition
E. Biocide Condition
The permittee shall not use any biocides except these approved in conjunction with the permit
application. The permittee shall notify the Director in writing not later than ninety (0) days prier
to instituting use of any additional biocide used in cooling systems which may be toxic to aquatic
life other than those; previously reported to the Division of Environmental Management. Such
notification shall include completion of Biocide Worksheet Form 101 and a map locating the
discharge point and receiving stream.

PART N
ANNUAL ADMINISTERING AND COMPLIANCEMONITORING QU
A. The permittee must pay the annual administering and compliance monitoring fee within 30
(thirty) days after being billed by the Division. Failure to pay the fee in a timely manner in
accordance with 15A NCAC 2H .0105(b)(4) may cause this Division to initiate action to
revoke the permit.

Too, Permits and Engineering Unit
Water Quality Section
Date: December 3, 1991
NPDES STAFF REPORT AND RECOMMENDATIONS
County: Mecklenburg
Permit No.: NCO048607
MRCS No.: 91254
PART I GENERAL INFORMATION
1. Facility and Address; 'illett Chemical, Inc*
Past Office Box 579
36 College Street
Pineville, NC 28134
2. Date of Investigation: November 21, 1991
3. Report Prepared by: W. Allen Hardy, Environmental Engineer i
4. Persons Contacted and 'telephone NumbersT. Ritchie Crump,
[phone]
5.' Directions to Site: From the intersection of Church Street
and Highway 51 in Pineville travel north can Church Street one
block to the junction of College Street. 'burn left on College
Street and travel approximately 50 yards to the plant
entrance.
6. Discharge Poi t(s), List for all discharge points:
Latitude: 35" 05, 101,
Longitude. 80 53' 27''"
Attach a USGS map extract and indicate treatment facility
site and discharge point on map.
UGS Quad No. G1'5SW USS Quad Names Fort Dill, NC
7. Size (land available for expansion .and upgrading): There is
limited land available for expansion and upgrading.,
8.' Topography (relationship to flood plain included).- The
topography is relatively flat.' The site is not in or near a'
flood plain
9. Location of nearest dwellings The nearest dwelling is
approximately 300 feet from the discharge location.
10. Receiving stream or affected surface waters; Unnamed
tributary to Sugar Creek

i
Page Two
a. Classification:
b. River Basin and Bubba in No. Catawba 03-48-3
C. describe receiving stream features and pertinent
downstream uses.- The receiving stream is a dry ditch
which meanders through residential yards and stormwrater
pipes (i.e. culverts) to Sugar Creek. There are no known
pertinent downstream uses other than those typical of
Class C waters.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. Type of wastewater: 0% Domestic
100% Industrial
at Volume of Wastewater: MCD (Design Capacity)
b. Types and quantities of industrial wastewater: * Flow is
intermittent depending on production. Supply well water
or water from a storage pond are used for the cooling
process.'
C. Prevalent toxic constituents in wastewater: N/A
d. Pretreatment Program (POTWs only).- N/A
in development approved
should be required not needed
. Production rates (industrial discharges only) in pounds per
day: N/A
a. Highest month in past 12 months: lbsday
b. Highest year in the past 5 years: lbs/day
3 Description of industrial process (for industries only) and
applicable CFR Part and Subpart: The principal process is the
production of carboxymethylated starch. CFR, Part 414; Subpart
G-Bulk Organic Chemicals
4. Type of treatment (specify whetherproposed or existing):
There is no formal treatment prior to discharge,.
5 Sludge handling and disposal scheme*- /A
6. 'treatment plant classification (attach completed rating
sheet): No rating sheet completed as there are no treatment
facilities.
7. SIC Code(s)» 2869
Wastewater Codes)»
Primary: 14
Secondary:
Main Treatment Unit Code. 00000

Page Three
I PART III - OTHER PERTINENT INFORMATION
1.' Is this facility being constructed with Construction Grant
Funds (municipals only)? No
2. special monitoring requests: No
. Additional effluent limits requests.- No
4. Other- No
PART I - EVALUATION AND RECOMMENDATIONS
The applicant, Tillett'Chemical, Inc., has requested: the
renewal of'the ,permit which allows the discharge of non -contact
cooling water produced from a condenser. The plant manager stated
that no biocides or additives ,are presently being used in the
cooling wafer process. There were no noticeable problems in the
receiving stream caused by the discharge.
Pending review and approval by the 'Technical Review Group it
is recommended that the permit be renewed.
17-
Signature of Reportivreparer
m
Water Quality egional Supervisor
Date

lesodsj{�
0ea
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OTC• Co') 1T44 nnnrien e

RESOUPCLS AND
r }
DIV
I10R OF ENVlNNNENAI MAMGE#Eq
State of North Carolina MOORESVIUE REGIOUL WICE
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street. Raleigh, North Carolina 27604
.Tames G. Martin, Governor George T. Everett,Ph.D.
William W. Cobey, Jr. Secretary Director
November 6, 1991
r. JOHN W. ANI ERSON
PINEVILLE, NORTH CAROL NA 28134
Subject: Application No. NCO04 60
TiLLE CHEMICAL, INC'..
Sear Mr. A ERSON:
The Division's Pe its and En2ineerin2 Unit acknowledizes receipt of your permit application and
regional Supervisor for this project prior to final action by the Division.
you have any questions, please ont ' (919) 733-50 3.
Sincerely,
Pu.pDale Over ash, P.E.
ervisor, NP ES permits Group
ice
Pollution Prevention Pays
P.0, Sox 29535, Raleigh; North Carolina 27626-0535 Telephony 919-7 3-5083
An Equal Opportunity Affirmative Action Employer

F
C O INA DEPT. OF NA, L SOURCES A GO NI DEVELOPMEN'1:ON OF ENL'IRO ENTAL NAG ENT, P.O. BOX 27687, LEIGH, NC 27611
OLLUTANT DISCHARGE ELIMINATION SYSTEM APPLICATION NumaLR
APPLICATION FOR PERMIT T1 DISCHARGE SHORT FORM C FORAGENCY
USE DATE RECEIVED
To b filed only by persons engaged in manufacturing and -mining
YEAR MD. DAY
Do not attempt to complete this farm before reading accompanying instructions
Please print or, type
1. NA ,-address, location, and telephone number of facility producing discharge
A. I Name TILLETT CHEMICAL, INC.
8. Mailing 'address P . 0. Box 579 316 College Street
1. Street address
2, City
Plnev'lle, . State N. ,
4. County f ec en urg S. LIP 28134
C. Location:
1. street 316 College Street
Pinevi1 e,
2. City 3. County Mecklenburg
4._ State North Carolina
D. Telephone No 704 889-7226
vn�
Area
Code
2. SIG
{Leave blank}
3. Number of employees 25
CMrl
If all your waste is discharged into a publicly owned waste treatment facility
and to the best of your knowledge you are not required to obtain a discharge
Permit, proceed to item 4. Otherwise proceed directly to item 5.
4. if you meet the condition stated above, check here p and supply the information
asked for below, After completing these items, please complete the date, title;
and signature blocks below and return this form to the proper reviewing office;
without completing the remainder of the form.
A. Name of organization responsible for receiving waste
S. Facility; receiving waste.-
1. Name
2. Street address
3. City 4. County
. State 6. ZIP
S.)b Principal product, 0 raw material (Check one)
`6> Principal process CarboxynLthylated starch
7. Maximum amount of principal product, produced or raw material consumed per (Checkone)
Amount
Saris 1-99 100-195 00-499 -999 1000- 5000• 10,000» 50,000
499 9999 49.999 or more
{1j (2) (3) (4) ,; (5) (5) (7) (8)
A. Day
R. Monti
r . Year EH
PREVIOUS EDITION MAY 8t USED UNTIL SUPPLY IS EXHAUSTED

° ± DEPT.5 7
sotUrtc AND
COMMUNITY, 1)EVr_,LoptfENr
1 rv��
4JI,
Mate of North Carolina
� 'De a e t ofEnvironment, Health, and. Natural R � ��c� i A0,4GEMENT
Division of Environmental Management
LE REGIONAL OFFICE
512 North Salisbury Street • Raleigh, North Carolina 27604
James G. Martin, 'Governor George T: Everett, Ph.D.
William W. Cobey, Jr., Secretary Director
November 7,1991
hn W. Anderson, President Subject: N DES Permit Application
ll tt Chemical Inc. N DES Permit No.NCO048607
o. Box 579
neille„ NC 81�k Tllett Chemical, Inc.'
'ar Anderson
Mecklenburg County
y
pis is to acknowledge receipt, of the following documents on November 4, 199 :
Application Form
Engineering Proposal (for proposed control facilities),
Request for permit renewal,
Application Processing Fee of $200.00,
Engineering Economics Alternatives Analysis,
Local Government Signoff,
Source Reduction and Recycling,
. ,lnterba in Transfer,
. Other ,
to items checked below are needed before review can. begin:
Application Form
Engineering proposal , (seeattachment) ,
Application Processing Fee of
. Delegation of Authority (see attached)
Biocide Sheet (see attached)
Engineering Economics Alternatives Analysist
Local Government Signoff,
Source Reduction and Recycling,
lntrbasin 'transfer,
Other
REGIONALOFFICES
Asheville Fayetteville Mooresville Raleigh Washington Wilmington Winston-Salem
704/251-6208 919/486-1541 704/663-1 r 9 919/733- 314 919/946-6481 919/395-3900 919/896-7007
Pollution Prevention pays
P.O. Box 29535, Raleigh, North Carolina 27626-05 5 Telephone [phone]
An Equal' Opportunity Affirmative Action Employer

Lcation is not made complete within thirty ( Q) days, it will be
you and may be resubmitted when complete.
ition has been assigned to Randy ;Kepler
--omments recommendations, questions or other information necessary for the
review of the application.
r am, by copy of this letter, requesting that our Regional Office
e
5ugervisor prepare a staff report and recommendations regarding this
iischarce. if you have any questions regarding this applications,
alease contact the review person listed above.
incerly,
M. gale C?vercash, P
CC. Mooresville Regional Office

NPI ES WASTE LOAD ALLOCATION
Modeler Date Rec.
PER NO.: NCO048607
PE ,E NA T llett Chemical Inc.
Drainage Ara (ni)
Avg. Streaniflow (cfs):
�
NA Iillett Chemical, Inc.
30C2 (cfs)FACIL
7Q0 (cfs)Wintr 7C1I (cfs)
Facility Status: Ex stir
Toxicity Limits: IWC
% Acute/Chronic
permit status: Renewal
Major Minor �
Ina treazn Monitonng:
No.: 001
parametersPipe
Location
Upstream
Design Capacity:
1>ci�y i�strc'iala�2
Location
Domestic (% of Flaw):
Industrial (% of Flow): 100 %
Effluent
Summer Minter
Characteristics
Comments:
BOD5 (m )
Ncn contact c ltn water
NIA -N m)
D.O. ( )
RECEIVING STREAM: an unnamed tributary to Su cr CTeck
TSS (ing/1)
�(/
glass: , C"
Fw Cool. 0 l)
Sub -Basin: 3-08- 4
Reference USGS Quad « Gl5S
(please{att{acla)
pH ( U)
County, Mec.11enb
Regional Office: Mooresville Regional Office
Previous Exp. bate: 2/29/ 2 Treatment Plant Class.
Classification chanores within three miles:
no c n e.
Requested b Randy Kepler
Date. 11%i/1
p..
dl �t4J*
Date:
L4Id dA1X:Vntr3 w.
Comments:
Prepared by:
Reviewed by.
Date:

State of P
I-tT"t-T-tt (if Environment
Division of Env
512 North Salisbury Stn�et
Mar6n, Governor
W. Cobey, Jr, Secretary
IN 0 c- rr
)IIN W. ANDERSON
30X 579
il,L,I,E, NORTH CAROLINA 2 8134
Mr. ANDERSON:
laterials received on Novembe
Please refer to this number
nng.
- C, I I
n 's regional offlc�
Tional �)Upei-Visul lul ulla plup,�-,L J�
I
m
0)
i Carolina
-1- -A
eztt
aolina 27604
Director
er 6, 11991
,,ou have, any questions, please contact Randy Kepler at [phone].
sincc—e,ly,
#J)4. Dale Overcash, P,1"
Supevisor, NPI)ES Permits Group
T Ntional ofl-lcc looresvillc, 1�cI '
P,0, [lox 2953�, Ril,�igh, Caroli'M 27',,26-0535 919-731-5083
An r'

NPDES FACILITY AND PERMIT DATA
UPDATE OPTION TRXID ' 5NU KEY NCO048607
REGION
PERSONA, DATA FACILITY APPLYING FOR PERMIT COTT2iT�> MFCT{LENBtJRG Q3
FACILITY N E> TILLETT CHEMICAL INC
ADDRESS: MAILING (REQUIRED) LOCATION (REQUIRED)
STREET: P.O, BOX 579, 316 COLLEGE ST. STREET: P.O BOX579, 316 COLLEGE ST
CITY: PINEVILLE ST NC ZIP 28134 CITY: P NEVIL,LE ST NC SIP 28134
TELEPHONE [phone] DATE FEE PAID: 04/29/86 OUi4T: 100.00
STATE CONTACT> BRIDGES PERSON IN CHANGE HUGH M. TILLETT
1=PROPOSED, 2= IS T ,; =CLOSED 2 1= A OR, 2—MINOR 2 1=MU , 2=NON-- UN
LAT. 3.505110 LONG: 08053280 N=NEW, M=MOI IFICATION, R=RE'ISSUE> R
DATE APP RCVD 04/29/86 WAS`S'ELOAD REQS 04/29/86
DATE STAFF REP REQS 0 /01/86 WAST LOAD RCVD 04/29/86
DATE STAFF REP RCVD 09/1,8/86 SCH TO ISSUE 1.2/01/86
BATE TO P NOTICE 10/1'7/86 DATE DRAFT PREPARED 09/30/86
LATE O`i" Ada COM REQS / / DATE DENIED
DATE OT AG COM RCVD / % DATE RETURNED
DATE TO EPA / / DATE ISSUED 02/ 5/87 ASSIGN/CHANGE PLFglIT
m re nArn» 02/ 9/92
=(>IVM:xVI,/—it ati tt- t. —...___ ..
3P'76) 9 = (GP13, 34, 30, 52) 0= (NOFEE) ] IS C 1.4 CONBI-7--
PERMIT BECOMES EFFECTIVE, 0 / 01 / 87
SITTER DATA FOR UPDATE ***

Permit No. NCO04I
STATE OF NORTH CAROLINA
4%RTMENT OF NATURAL RESOURCES & COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
-P E R M I T
amended,
TILLETT CIS
rued to discharge wa
F
on C(
Me(klei
'CAM PAN Y
y
A"i
t forth in Part 1, It, and III hereof.
This permit shall become effective
This permit and the authorization to discharge shall expire at midnight
Signed this day of
R. PAUL WILMS, DIRECTOR
DIVISION OF ENVIRONMENTAL M
BY AUTHORITY OF THE ENVIROt
MANAGEMENT COMMISSION
&11

Permit No. NCO
SUPPLEMENT TO PERMIT COVER SHEET
Tillett Chemical Company
reby authorized to;
nn--cont,a t cooling water l
Permit) into are unnamea'raLJU'-c11 y
Class` 4,Clm waters in the Catawba River Basin.

Such discharges shall be limited and monitored by they Kermittee as apt
Effluent Characteristic
Discharge
Ljmitatl
kg/day ;(lbs/day)
Otherunits
(Specify)
Daily Avg. Daily Max.
Daily Avg. °
Daily Max, I
Alta
�
s'empernture
Residual Chlorine
THERE SHALL BE NO CHROMIUM, ZINC,,
ample locations: f - Effluent, t
"The temperature of the effluent at
receiving stream of more than .8
***Monitoring requirements only appl
y
such as not to cause an inc
n no case cause the ambient
or. i. e its added to the cools.
from ;the Division of Envi.roi
ci.fied below:
Monitorins Requ.1jesnat
€easuremexnt Sample pl
req ency Type Location
4onthly Instantaneous
font ply Crab B,U,D
ionthly Grab
we in the temperature of the
wer temperature to exceed 321C .
Eater.
xtal Management prior
ait) .
wand rd units and shall be td �

Part III
Permit N(
xicity Repener
e modified, or revoked ad reissue
is permit shall b n
g re
corporate toxicity limitations and monitorinqui
ther studies conducted on
eat toxicity test" or 0 that detrimettal effects
receiving stream indicate this
'pected in the receiving stream as a result of viocides except these
"'--D
systems wnacu "j --
previouslY rePortedlol
For, 101 and a map locating rut;
stream.

Dante: September 15, 1986
County: Mecklenburg
NT DES Permit No. NC 0048607 � ;r �►; a�� �,r�y ��� �
i'ARI I - GENERAL 1NFor�MAT10N SE y( ter.:
1. Facility and Address: Tillet:t Chemical, Inc.
316 College Street
post office Box 579
Pineville, `>:oath Carolina 28134
Date of Investigation: on: September 15, l 93Es
3. Report Prepared By: Michael L. Parker, , nvironment & Engineer4.
erson Contacted: Mr. Thigh M. `T`il sett # telephone number (704) 889-7 "226
5. Directions to Site. From the junction of Church Street and Highway 51 in
he sown of Pineville in southern _eckle..bur ; County, travel north on
Church Street; one block to the junction of College Street, `turn left and
travel approximately 50 yards. °.C:i let_tChemical cal in at the end of College
Street.
'
6, Dis harge Point - Latitude: 80' 5� :5r'
Longitude: 35*0513011
Attach ach a USGS >.=aap Extract and indicate treatment atment plant site and discharge
_point can map.I
_ . Sl:wc (l.axaci available for c=r;paaaaa.crt.
eaad upgrading):
Thdre is limiter a.i,any
area available for any future expansion,
C Topogt:apby (relationship t;cs flood Main included): not
located in or ne.aar a flood plain 'area.
c Location of Nearest tJrei.la.ar;: None witrsw.t 500 feet of & Qc.T ar8aa` pc ix t
Area is heavily industrialized.
10. Receiving Sta`oam or Affected Surfaze Waters: Is'rrnasaed tributary to Sugar
reak
C Lassif is s t ion: C,
River 1 Basin YiILCI ;riibTi i s Lll No.: CatnKa
330834
{'ess
{ ( 1,ia1t pertinent downstream e m rtµxes
Describe receiving a� a��si���y X4 t c . 4 er
Discharge enters aa'drain prior LO w_._"'r'Ilia; unnamed tributary to Sugar
t'rt'a'ia
o flow observed in tributnrY. No other dischargers in
immediate area.
Yvpu of Wastewater: tt Domosric,

came of Wastewater: *MGD
es and quantities Of industrial wastewater: *Flow is intermittan
ending upon productionsupply well from whih water is drawn is
able of producing 150 gw.
valenz toxic constituents in wastewater: All information concern
;acides, biocides, etc. has been forwarded to Raleigh by the Compa
Areatment Program (POTWs only) : N/A
iion Rates (industrial discharges only) in Pounds: N/A
)tior wf' industrial Process (for industries only) and Applicable,
7t an! Subpart: N/A'
E Treaniient (specify whether proposed or existing) : An existing
acility being constructed wi
A
vni:oring requests: II/A
r generated at
;onstruction Grants Funds Nut
nical is non -contact cooling
aus types of chemicals processed by the Company - ine cou&Tu,
t come into contact with the product. A cooling basin is pri
alps brie j the temperature down to ran acceptable level.
nding re7-aw and approval of biocidal information, additiona
Mont s fcr toxic s may be necessary at this facility -
is reccn-,',endid that the NPDES Permit be renewad.
Signature of 1Z,,port preparer
T ypurv,-

COMMUNITY DEVELOPMENTNORTH CA�CII,INA' '<. E OF NATURAL 'RESOURCES LEIGH, NC 27611
DIVISION OF;ENVjpoNMFNTAi NAG ENi, P.O�3'l 27 T,
NATIONAL POLLUTANT DISCHARGE ELIMINATIONSYSTEM APPLICATION NUMP
APPLICATION FOR ERMITTO ISltAE SHORT FORM C AGENCY DATE RECEIVED
USE
to be filed only by persons engaged in manufacturing and mining YEAR hlC1: DAY
Elsa not att ript to complete this form before reading accompanying instructions
Please print or type
1. N ,-address, location, and telephone number of facility producing discharge
TILLETT CHEMICAL, INC.
A. hame
S. Mailing address P . 0. BOX 67 � 1 College Street
1. Street address N
Pi neV 11 e 3. State
2. City t� e rr 2lP 2 1 S4
4, County;
C, Locations
1. street' 16 College "�.tn�:e%
Pi nevi e; 3. County MeckleC1bu
2. City
.;state
North Carolina
. Telephone r c 88 04 — 7 2 6
1-5
Area
Code
2. SIC.
(Leave blank)
3. Number of es,plcyees r
If all your waste is discharged into a publicly owned waste treatment facility M
are not required
and o the best of your knowledge you to obtain a discharge
permit, proceed, to item 4. Other,4ise proceed directly to 'item
4. If you meet the Condition stated above, check here Z and Supply the information
asked for bolo After completing these items, Please complete the date, title,
and signature blocks below and return this form to the propel' reviewit9 office
without COnVIeting the remainder of the for'n.
A, Name of Organization responsible for receiving wast(=
B.`Facility receiving waste:
1; Name
2, Street address
3, Crty=
4. County
S;, State 6. ZIP
S. Principal product, craw.material (Check one)--.
'. Principal process
n1et3 fated starc.r,
7, KaximuRn anxtunt of principal product produced or ra'. material consumed per (Check one)
Amount
basis 1-99 100-199 00-499 500-999 1000- 5000- 10,Ot1Q- 50,000
4999 9999 49,999 or mre
X
P �ant,
tea t�._w
Pci yr *US FiY'++-.��• a. ,u: '+ CarUSE LNTU SUP '...Y 9S CvwAUST er,

nxin, im ArtjrHlnt tit prlriclIto I prtiiliiat pr(otleait it rew rnatrrt.i! roair.iaa+�<I, t'oiwietr=<j
ttr*n f, aticvr, is rr,aasured in (Lne,i. 01W) bushels C Ca harre square feet
A. S pounds Bi 0 tons ' . l Lt. Ca E . t rsq
F.0 gallons G.C)pieces or units H$Clother, specify
a) Cheek here if discharge occurs all year CX, or
;b) Check the munth(s1 discharge occurs
l,GlJanu January, 2.C7February 3.0Marcn 4,oApril 5.Camay 6.0June
12,C1 Decmbl
7.0 July 8.0 August g : 0 septent,er to.0 October 11.0 Noverrbev r
;c} Check hcYw rnany days per week 1.01 2. -3 3.tt 4-5 4.o 6-7
Types of waste water discharged to surface waters only (cheek as applicable) yo1 treated before
F low, 981jorts'per operating clay discharging -Aperc it)
Discharge Vr p.l- 9s 1000'4999 50 C1-9999 10,000- 50,000- Hrrrte 0 1- 30- 65- 9 -
operating day 49,999 or more 29.9 64,9 949 100
(1) (2) (3) (4) (5)` (6} (9) (10)
Sanitary, daily
average
Coc,7intl: water, ett. h
daily average
process water,
daily average;
Haxir im! per ocivrat-
ing day for total
discharge (a11 t lies)
l f ar t f tt three tyt>es c f waste tretow as applicable.
ident) `ied in ttern 10, either treated or untreated,
are d';schar�ged to ;,;laces tither Char. surface water°,, rlaeek
Average flow, gallons per ol>erating day
waste water is 1 -4999 000-9999 10,-49,99S 50,Cit10 or
more
dischergaid to: (3) (4
Municipal sewer sys,ten',
underground well
Evaporation laq,)rn Or pond
Outer, Sheet..*'
7. number of separate discharge points: IiU
A, tj 1 8.1 2-3 C-.0 4-5 D. CJ b or huJre
3. Marie of receiving water or waters M
1 , Does ;your discharge contain or is it passible for your discharge to contain
One or moreof the fol)Owing subst"Ces d as a result of your operations,
activities, or processes: a nia, cyanide; aluminum, beryllium, ca iunt,
chroeni urn, cooper, lead, mercury, nickel, selenium, zinc, Phenols, oil and
grease, and chlorine (residual). A.0yes : g�Uno lication and
F certify that 1 am familiar with the information CCptatn"d in the apP
that to the best of my knowledge and belief such information is true, comOlete, and
accurate. Prr s1d°lit
John W. Anderson
Pr`nted a of Person Signing Title s '# �i ".
Cc., , 1 ,°
Sign ta
Gate Application Signedrt f licant ma
1 arc'l ina General Statute' 1 3- 15 , b 2 pride that: person knowingly
lication) record, report,
False statement repre entaticrt etc certification it any 21 or ulatitalaa Of
Cher document files or required o be maintained under Article who falsifies, tampers
rolimertal Management Commission implementing that Article,to I>e
nowly renders inaccurate and recording o monitoringfdthece or method nviroomenta required ent t
ted or maintained under Article 21;or regulation
s oevent n that Article, shall b guilty o a misdemeanor #aucrn� h�b�e�b ... Section 100
00, or -by ittipr lsonment tacit to exceed sip months, or by
T11 t ; a $ 1 fit: CiC i m" YE' i'ha., !' , )00 0 _ prisoiine'r;". not mor � years, C7'

STATE OF Ni
Permit No. NCO048607
TN CAROL INA
Tillett Chennit
Tillett Chem:
316 College
Pinevil
Mecklenburg
A s i
C.
Dcated at.
crc.
.t
in accordance c with effluent limitations, monitoring requirements, and other conditions set forth i
Parts 1, lI, and III hereof.
This permit shall become effective
This permit and the authorization to discharge shall expire t midnight can August 31, 1996
Signed this day
w ,'i
George T. Everett, Director
Division of Environmental Management
By Authority of the Environmental Management Commission

Permit No. N 86t
SUPPLEMENT PERMIT COVER SBEET
Tllett Chemical Inc.
y authorized t:
Inc., .f ib Uoile8e Street, Pineville,;Mecklenburg County (See Part M of this Pert.
Basin.

ram--
�
Y
as RM his!
t
Y'
A:
ID I
141i / i \ )'
t t fort
a
twill
14,
os y,� I# it
f�„ ItI
� ` �•" ^`4 � �tS;
1 40,
yyo
hl
Z \ T a}t •k� N �1.'f "+,. u.+3 i'. k. vp �' � t �/t �.
co,133A CM,
?.; q.. " 't9 t i U j f(p p[il'/ r f �•` �'lz 1 •� `;if..
��`. V r {4t?.tt�,�'F� � �`;Z..�, t `'� �t`;1 i 1 i€' �1 ���'"r>.."`..J/� f..�".�': '`"`�..� { "v` ��;,-�� d^.°+..u'""� � " ► ,".fit
9$�c
1
l' 9 a , j 1
Yl1J&ZO.�G
��-

. k; ) rJ ,U.IN l LJIVJ I 1 A I 1UNS AIND MONYFORING REQUIREMENTSFINAL Permit No. NCO048607
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial number 001. Such discharges shall be limited and monitored by the permittee, as specified below:
Effluent Ca I ©Ichar Itaticm Maltc�►lrrernent
Uri is LWmAyl Measurement Sarn le
Flow on A DA FrequencyLequency IY220 Igcotlon
Temperature Monthly Instantaneous
rn� ,� � Monthly grab ,U,C
Total Residual Chlorine Monthly Grab
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.
*Sample,Locations: E - Effluent, U - Upstream, D - Downstream
** The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than 2.8 degrees
C and in no ease cause the ambient water temperature to exceed 32 degrees C.
The permittee, shall obtain authorization from the Division of Environmental Management prior to utilizing any biocide in the cooling water (See
Part III of this Permit).
The pH shall not be less than 6.0 standard units nor greater than ►.0 standard units and shall be monitored monthly at the effluent by grab
sample..
There shall be no discharge of floating solids or visible foam in other than trace amounts.

Cl
oicity Reopenr Condition
Permit No; NCO048607
receiving itivain indicate that detrimental e6cts maj be expected in the receiving stream
as a result
of this discharge.
E. Biocide Condition
--- a,._ --I .�.„...,...�,«..��,..,.,. w...:....,,,t..w »w..r++. -- XA".T 16J GLJxA.AV vw
life other than those previously reported to the Division of Environmental 'Management. Such
notification shall include completion of Biocide Worksheet Form 101 and a map locating the
discharge point and receiving stream.

r 1
rF
State of North Carolina
Department of Environment, Health, and Natural Resources
Mooresville Regional Office
James G. ' Martin, Governor Albert F. Fulton, Regional Manager
William W. Cobey Jr.,` Secretary DIVISION OF ENVIRONMENTAL MANAGEMENT
March 14, 1992
Mr. John W. Anderson
Tillett Chemical, Inc.
Post Office Box 579
Pineville, North Carolina 28134
Subject. NPEES Permit No. NCO0486 '7
Tillett Chemical, Inc.
Mecklenburg County, NC
Dear Mr. Anderson:
our records indicate that NPDES Permit No. NCO04 60 7 :was
issued on March 2, 1992'for the discharge of wastewater to the
surface waters of the State from your facility. The purpose of
this letter is to advise you of the importance of the Permit and
the liabilities in the event of failure to comply with the terms
and conditions of the Permit. If you have not already done so',
it is suggested that you thoroughly react the Permit. Of
particular importance is Page 4.
Page 4 sets forth the effluent limitations and monitoring
requirements for your discharge(s). Your discharge(s) must not
exceed, any of the limitations set forth. The section headed
"Monitoring Requirements" describes the measurement frequencies,
sample types and sampling locations. Upon commencement of your
discharge (car operation), you mint initiate the required
monitoring. The monitoring results must be entered on the
reporting form: furnished to you; by this ;Agency. If you have not
received these forms, they should be arriving shortly. If you
fail to receive the forms, please contact this office as quickly
as possible`. I have enclosed, a sample of the "Effluent"
reporting farm (DEM Form -l), talus instructions for completing
the form. It is imperative that all applicable parts be
completed, and the original and one copy be submitted as
required..
The remaining Parts of the Permit set forth definitions,
general conditions and special conditions applicable to the
operation of wastewater treatment facilities and/or discharges.
The conditions include special reporting requirements in the
919 North Main Street, Mooresville, NC. . 28115 . Telephone 7 -1699 • FAX 663
An Equal Opportunity Affirmative Action Employer

the Permit ana con--du-L�
if you have any questions or need clarification. We look forward
to providing any assistance
Sincerely,
u
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
Enclosure
DRG : se

PV
Permit No. NCO048607
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
PEffi&T
TO DISCHARGE WASTEWATER UNDER THE
!2,
NATIONALEI � EQLLUTANT ''' � '" "" I 113NE ELIMINATION SYaJ—EM
)mpliance with the provision of North Caroiina General Statute 143-215.1,
r lawful standards and regulations promulgated and adopted by the North Carolina Environmental
agement Commission, and the Federal Water Pollution Control Act, as amended,
Tillett Chemical Inc.
reby authorized to discharge wastewater from a facility located at
Tillett Chemical, Inc.
316 College Street
Pineville
Mecklenburg County
ceiving waters designated as an unnamed tributary to Suger Creek in the Catawba River Basin
-cordance with effluent limitations, monitoring requirements, and other conditions set forth in
s 1, H, and 111 hereof
permit shall become effective
permit and the authorization to discharge shall expire at midnight on August 31, 1996
ied this day
oV,
George T. Everett, Director
Division of Environmental Management
By Authority of the Environmental Management Commission

Permit No NC'.O048607
SUPPLEMENT TO PERMIT COVER SHEET
Tilled Chemical Inc.
authorized to:
. Discharge from said treatment works at the location specified can the attached map into an
Basin

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A. (). EFFLUENT LIMITATIONS AND MONITORING ORING REQUIREMENTS l=°lNAL Permit No. NCO048607
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial number 001. Such discharges shall be limited and monitored by the permittee as specified below:
Effluent Characteristics l lschar im'fatIons Monitorinc Reaulre tints
Lbs/da Units s ecif Measurement Sam a�,,1 *Sam 1e
Man. Aver. 2lly Max Mean. A ball' Max Frequency Lyp e Location
Flow Monthly Instantaneous F
Temperature Monthly GrabE,U,D
Total Residual Chlorine Monthly Grate
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE COOLING WATER.
*Sample Locations: E - Effluent, 1. i - Upstream, D - Downstream
The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than 2.8 degrees
C and in no case cause the ambient water temperature to exceed 32 degrees C.
The permittee shall obtain authorization from the Division of Environmental Management prier to utilizing any biocide in the cooling water (See
Part III of this Permit).
The pH shall not be less than .0 standard units near greater than 9.0 standard units and shall be monitored monthly at the effluent by grab
sample..
There shall be no discharge of floating solids or visible foam in other than trace amounts.

PPartlH Permit No. NCO048607
D. Toxicity Reopener Condition
This permit shall be modified, or revoked and reissued to incorporate toxicity limitations and
monitoring requirements in the event toxicity testing or ether studies conducted on the effluent or
receiving stream indicate that detrimental effects may be erected in the receiving stream as a result
of this discharge.
F. Biocide Condition..
The permittee shall not use any biocides, except those approved in conjunction with the permit
application. The permittee shall notify the Director in writing not later than ninety days prior
to instituting use of any additional biocide used in cooling systems which may be toxic to aquatic
life other than those previously reported to the Division of Environmental Management. Such;
notification shalt include completion of 'Biocide Worksheet Forin 101 and a map locating the
discharge point and receivingstream,

Date: September 15, 1986
NPDES STAFF REPORT AND RECO�NuENDATIONS
County: Mecklenburg
NPDES Permit No. NC 0048607
ART I - GENERAL INFORMATION
Facility and Address: Tillett Chemical:, Inc.
316 College Street
Post Office Box 579
Pineville, North Carolina 2513
Date of Investigations September 15, 1956
Report Prepared By Michael L. Parker, Environmental Engineer I
Person Contacted: Mr. Hugh M. Tillett,;telephone number (70) 889-7226
irections to ;Site: From the function of Church Street and Highway 51 in
°ae Town of Pineville in southern Mecklenburg County, travel north on
°aurch Street one block to the junction' of College Street. Turn left and
ravel, approximately 50 yards. Tillett Chemical is at the end of College
:reef.
Ls harge Point - Latitudes 80°53'' 5"
Longitudes 5*05'30"
.tach a USGS Map Extract and indicate treatment plant site and discharge
Sint on map.
'GS Quad No.: G 15 SW
.e (land available for expansion`and upgrading): There is limited if any
ea available for .any future expansion.
po raphy (relationship to flood plain included):' Relatively flat, net
sated in or near a flood plain area.
cation of NearestDwelling: None within 500 .feet of the discharge paint,'
ea is heavily industrialised.
ce ving Stream or Affected Surface Waters: Unnamed tributary to Sugar
eek
Classifications C
River Basin and Subbasin No.: Catawba 030834
Describe receiving stream features and pertinent downstream uses.
Discharge enters a drain prior to entering unnamed tributary to Sugar
Creek. No flow observed in tributary. Na other dischargers in
immediate area.
C -- DESCRIPTION OF DISCHARGE AND TREATMENT WORK
►e of Wastewaters 0 Domestic
100% Industrial Cooling Water

Page Two
a. Volume of Wastewater: iGD
b.Types and quantities of 'industrial wastewater: *Flow is intermittant
depending upon production. Supply well from which water is drawn is
capable of producing lit) gpm.`
c. Prevalent toxic constituents in wastewater: All information concerning
alg cider, biocides, etc. has been forwarded to Raleigh by the Company.
. Pretreatment Program (POT s only); N/A;
Production Rates (industrial discharges only) in Pounds: N/A
Description of Industrial Process (for industries only) and Applicable
CFR Part and Subpart: N/A
Type of Treatment (specify whether proposed or existing). An existing cooling
basin is the only treatment provided prior to discharge.
Sludge Handling and Disposal Scheme: /A
Treatment Plant Classification: /A
kR.T III -- OTHER PERTINENT INFORMATION
Is this facility being constructed with Construction Grants Funds (municipals
only)? N/A
Special monitoring requests: N/A
Additional effluent limits requests: N/A
Other: Other: N/A
i T ICE ` - EVALUATION AND RECOMMENDATIONS
The wastewater generated. at Tillett Chemical is non -contact cooling water
1ch is passed through water jackets which are used in the heat extrapolation
various types of chemicals processed by the Company. The cooling :water'
es not cows into cont-act with the product. A cooling basin is present can. -site
.ch helps bring the temperature down to an acceptable level..
Pending review and approval of biocidal information, additional monitoring
quirements for to ics may be necessary at this facility.
It is recommended that the NPDES Permit be renewed.
Signature of Report Proparer
Quali eg Supervisor

State of North' Carolina
Department of Natural Resources and Community Development
Mooresville RegionalOffice
James G. Martin, Governor Albert E Hilton, Regional Manager
S. Thomas lodes, Secretary
DIVISION C1 ENVIRONMENTAL MANAGEMENT
March 4, 1987
r. Hugh M. Tillett
Tillett Chemical, Inc.
Past Office ,Sox 579
Pineville,` North Carolina 28134
Subject. NPDES Permit No. NC 0048607
Tillett Chemical
Mecklenburg County, NC
Dear Mr. Tillett:
r records indicate that``NPDES Permit No. NC 0048607 was issued, on
February 25, 1987 for the 'discharge of wastewater to the surface waters of the
State from your facility. The purpose of this letter is to advise you of the
importance of the Permit and the liabilities in the event of failure to comply
with the terms and conditions of the Permit. If you have not already done so,
it is suggested that you thoroughly read. the Permit. Of particular importance
is Page 1-3.
]Page -3 sets forth the effluent limitations and monitoring requirements
for your discharge. Your discharge must not exceed any of the limitations set
forth section headed "Monitoring Requirements" describes the measurement
frequencies, sample types and sampling locations. Upon commencement of your

Mr. Hugh M. Tillett
Page Two
March 4, 1987
ioned previously, the purpose
ce of your PDES Permit. Ple&
arification. We look forward to providing any assistance.
Sincerely,
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
closure
F: se

d i N .� NC
STATE OF
P
C"L.r�rLa�tataa�.c ar.a.,ac,�az�aa
t l Management Commission, and '!
it
hcl'
waters
Sugar Creek In
ROLINA
COMMUNITY DEVELOPMENT
MANAGEMENT
er the NATIONAL
NATION SYSTEM
I cal Company
-rom a facilitylocated a
ill
rg County
Ltions set forth in Parts I, II, and III hereof.
This i t shall become mI t. SEP 9 S 199
This Permit and the authorization to discharge shall expire at
AUC 3 1 1986
Signed this day of
SEP 0 8 1981 Original SiRned by
.s P. BENTON, JR.
? 1f P-ljo—b-Cmrt —r. K;Ims —,Dir�ecto�
Division of En1 1 Ma

Page of
Permit No. NC
SUPPLEMENT TO PERMIT COVER SHEET
Tillett Chemical Company
is hereby authorized to'
Sugar Creek which is classified Class I;%

P
S
Effluent Fra a t I
l l
I t l rements
Kg l ay)
Other Units
(Specify) Meas ant
Sample
Sample
l gig. Daily Max.
Daly g,_
daily Maxb
�pCo—ca—tion
Flow
Weekly
Instantaneous
Temperature
Monthly
Grab
*SampleLocations-
I -Influent, E-Effluent, G pst a r,
I nstraa r
**All stream samples shall
be grab samples.
***The,temperature
shall be such as to not cause a temperature in the receiving
stream of 50F° above
ambient stream
water
temperature and in
no case shall exceed 900F.

Part 1
Pemi t No. NC
SCHEDULE OF COMPLIANCE
1. The ittee shall achieve compl
specified for discharges in accov
NOT AP
actions taken, and the probability of meeting the next schedulei
14

PART I
Permit No. NC
Act used herein means the Federal Water Pollution Control Act, As amended.
DEM used herein means the Division of Environmental Management of the
Department of Natural Resources and Community Development
"EMC" used herein means the North Carolina' Environmental Management
Commission
C. MONITORING AND REPORTING
1. Representative Sampling
Samples and measurements taken as required herein shall be representative
of the volume and nature of the monitored discharge.
. Reporting
Monitoring results obtained during the previous month(s) shall b
summarized for each month and reported on a Monthly Monitoring Report
Form C M No MR 1.0, 1.1, and l.) postmarked nc.later than the 45th
day following the completed reporting period. The first report is due on
NOVI 5 1981 . The CDEM may require reporting of additional monitoring
results by written notification. Signed copies of these, and all other
reports' required herein, shall be submitted to the following address:
Division of Environmental Management
Water Quality Section
Post Office Box 27667
Raleigh, North Carolina 27611
. Definitions
a. The "daily average discharge means the total discharge by weight
during a`calendar month divided by the number of days in the month
that the production or commercial 'facility was operating. Where less
than daily sampling is required by this permit, the daily average
discharge shall be`determined by the summation of all the measured
daily discharges by weight divided by the number of days sample
during the calendar month when the measurements were de.
b.: The "daily maximum' discharge means the total discharge by weight
during any calendar day.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to The FM
regulations published pursuant to N. C. G. S. 13215. 3 at seq.# The
Water and Air Quality Reporting Act, Section 304g, 13 dSC 1314, of the
Federal Water Pollution Control Act, As Amended, andRegulation 40 CFR 1.
. Recording Results
For each measurement or sample taken pursuant to the requirements of
this permit, the permittee shall record the following information:
15

PART I
Permit No. 1C
a. The exact place, date, and time of sampling;
b. The dates the analyses were performed
c. The per son who performed the analyses;
d. The analytical techniques or methods used; and
e. The results of all required analyses
6, Additional Monitoring by Permittee
If the peritte monitors any pollutant at the location(s) designated
herein more frequently than required by this permit, using approved'
analytical methods as specified above, the results of such monitoring
shall be included in the calculation and reporting of the values required
in the Monthly Monitoring Report Porn (DE1 MR 1.0, 1.1, 1.4)
Such increased monitoring frequency shall'also 'be indicated. The DEM
may require more frequent monitoring or the monitoring of other ollu-
tuts not required in this permit by written notification
. Records Retention
All records and information resulting from the monitoring activities
required by this permit including all records of analyses performed and
calibration and maintenance of instrumentation and recordings from
continuous monitoring instrumentation shall be retained by the perm ttee
for a minimum of three () years, or banger if requested by the State
Division of Environmental Management or the Regional Administrator of
the Environmental Protection Agency.;

PART I I
Pemi t N. NC
Notification
eration
IG COWITWU OT 'Lnis permiT..
(ct
noncomplying discharge.
issing
diversion from or bypass of facilities necessary to mainta-
i the terms and conditions of this mit is prohibited, ex(
I

PART i
Permit No.
lures
1 G1C I
lt! t"ClI- 1, d g
stru tion
11 I " SA,;j K:e LA Y A V I w4 %± 4 + .

PART II
Permit No. NC
ONSIBILITIES
Right of Entry
rship or Control
i1 Act.
ration
--
'uspended, or revoked in whole or in part during its terry
di, but not limited to the following:
n of any terms or conditions of this it
ng this pemit by misrepresentation or failure to disclos
01 relevant facts; or
le in any condition that requires either a temporary or
,nt reduction or elimination of the authorized discharge.

PAT I i
Pemit No. NC
Toxic Pollutants
fled.
Liability
SC 1319.
is Substance Lia

PART III
Permit No. NC
S. Previous Permits
All previous Stag water quality permits issued to this facility,
whether for construction or operation or discharge, are hereby revoed
by issuance of this permit. The conditions, requirements, terms, and
provisions of this permit authorizing discharge under the National
Pollutant Cichare Climnaion system goys s discharges from this
facility.
C. Construction
No construction of wastewater treatment facilities or additions thereto
shall be begun until Final Plans and Specifications have been submitted
to the Division of Environmental Management and written approval and
Authorization to Construct has been issued. If no objections to Final
Plans and Specifications has been made by the D M after 30 days following
receipt of the plans or issuance of this permit, whichever is fatter, the
plans may be considered approved anconstruction authorized.
D. Certified Operator
Pursuant to Chapter 90A of North Carolina General Statutes, the permittee
shall employ a certified wastewater treatment plant operator in responsible
charge of the wastewater treatment facilities. Such operator must hold a
certification of the gradeequivalent `to the classification assigned to
the wastewater treatment facilities.'
15 & 1 1

Permit No. - NC
STATE OF NORTH CAROLINA
DEPARTMENT -.OF NATURAL RESOURCES & COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
E R M I T
To Discharge Wastewater Under the NATIONAL
POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143- 15.1,
other lawful standards and regulations promulgated and adopted by the North Carolina
Environmental Management Commission, and the Federal Water Pollution Control Act, as
amended,
is hereby authorized to discharge wastewater from a -facility located at
Pineville
Mecklenburg County
to receiving waters
Sr Creek in the Catawba River Basin
in accordance with effluent limitations, monitoring requirements, and other
conditions set forth in Parts I, II, and III hereof.
This permit shall become effective
This permit and the authorization to discharge shall expire at midnight
on
Signed this day of
Robert F. Helms, Director
Division of Environmental Management
By Authority of the Environmental
Management Commission
M1 & i

F1 f I V s W I %A
It IV I I I UW # �is -j V­
tla' ... -- -r—­­
Effluent Characteristics DijSha �
imitat es
Mon i jorin uir nts
Kg ay (lbs/day)
Other Units
(Specify)
Measurement
Sample * Samp
Daiii Avg. ail Max.
Daily A v g �-
wily
�Max
_�u�ency
L7—
=,ype - ocat
Flow
',Weekly
Instantaneous I 0V
Temperature
Monthly
Grab E
*Sample Locations:
I -Influent, E-Effluent, U-Upstream,
D-Downstream
"All strearyi
samples shall be grab samples.
***The temperature
shall be such as to not cause a temperature in the receiving stream
of 5OF above
ambient stream water
temperature and in
no case shall exceed 900F.
A.
t+

704/881
,,, (j jtCAND
LDE1yEL<)pjxrNT
1a
t
W
T. Adkins
M a rr r
e, North Carolina
d k i n s :
appreciate ur assistance.
S
Hu
SO
Enclosure
zal, Inc.
EEC"
lin
981
ral
n t
ort Form " as our
i s har qe. This water
rel,y,
rJ. Tillptt

r .1
CAROLINA DEPT. OF NATURAL RESOURCES AND C0101UNTTY DEVELOPNENT
ON OF ENTAL MANACFNtNT, P.O. BED' 27687* T>T IGH r NC 7 611
)OLLUTANf DISCHARGEELIMINATION SYSTEM APPLICATION NUMBER
)N FOR PERMIT TO DISCHARGE - SHORT FORM C FOR
AGENCY
USE ;ATE RECEIVED
My by persons engaged in manufacturing and mining �
YEAR Mo. DAY
A to complete this form before reading accompanying instructions
Please print or type
ess, location, and telephone number of facility producing discharge
Inle Tillett Chemical —
Wing address 16 College Street
1, Street address_
w pity P n v 1 stag North Carolina
A, County M e c k 1 en61r . ZIP 28134
cation:
1. Street M s
Em City 3. County
4. State
rile hone o 704 88 722 ,
p to
Area ttEal it t
Code 7,t T° a ap`ittiTf.
WAY 4
ve blank)
employees 35
waste is discharged into a publicly oweed waste treatment f<acilit a
est of your knowledge you are not required to obtain a discharge Dun
ed to item 4; Otherwise proceed directly to item S.
,et area condition stated above, check hereii and supply the iric6rroation
below. Af er,co pleting these items, please complete the date, tide,
tare blocks blown and return dais" for°rar to the proper 'reviewing office
:ompleting the remainder~ of the fora,
lame of organization responsible for receiving waste
cili y receiving waste:
1, Name
. Street address
3.'City , County
. State n, ZIP
ra product, Draw atwiteea'aal (Check erne)
r-oce s Closed system batch processing
rant of principal product produced or raw material consumed per, (Check one)
Amount
is 1-99 100-199 00-4 9 500-999 1000 5000- 10,000- 50,000
€7; a 9999 49,999 by, ar*res
(1) (2) (d)- (4) 5) (f'i) (7) 8)