NC0046213_Regional Office Historical File Pre 2018 (3)

/I C IVE NCQEN ! R
WQROS
MOORFSV(I r HR-41m1AL. O FJCE. MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
RECEIVED
SEP 2 0 2019
CEN tiAL FILES
DWR SECTION
September 13, 201.9
Sent via Overnight Mail
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
Enclosed please find the August 2019 NPDES report, plus one copy, for the above -referenced.
permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at ErRisner@,MarathonPetroleum.com.
Sincerely,
\Jij
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NPDES PEFOTT NO.: NC0046213 PERMIT VERSION; 4.0 PERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal CLASS: PC-1 COUNTY: Mecklenburg
OWNER NAME: Mplx Terminals LLC ORC: Darryl Keith Thompson ORC CERT NUMBER: 1005fl7
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 08-2019 (August 2019) VERSION: LO
4
6
9
11
12
14
15
16
17
10
19
20
21
23
24
25
26
27
20
29
30
31
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
2400 cloth Irre 1400 clack
50050
See Permit
Recorder
FLOW
nod
0.001
1,139
C0530
Monthly
Grab
las-Cane
mg0
12.2
34030
Monthly
Grab
IEO%E#E
00156
Monthly
Grab
r314GRWE
mel
<S
32734
Monthly
Grab
PI1E9, 31t1
mgll.
< 0.02
00070
Monthly
Grab
0.175
Monday Average 1,11011:
Monthly Average:
17.105
30
12.2
12.2
12.2
0
0
esr♦ No Reporting Reason: ENFRUSE tt, No Flow-Reuse/Rccvcic; ENVWTHR No Visitation --Adverse Weather; NOFLOW - No Flow; HOLIDAY No Visitation --Holiday
20,1

NPDES PERMIT NO,: NC0t 46213
FACILITY NAME: Charlotte Terminal
OWNER NAME: MpIx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 0€t-20)9 (August 2019)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4„0
CLASS: PC-1
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 10
CONTACT PHONE #: [phone]
ORC/Certifier Signature: Darryl Rci n' s' hemp
By this signature, I certify that this report is
PERMIT STATUS: Act
COUNTY: Mecklenburg
ORC CERT NUMBER: 10
STATUS: Processed.
SUBMISSION .DATE: 09,1 1/201 at
09i 1 1 /2019
:dkthompsonCmarathonpetroleum.com Phone 4:9 S0-tr13-0495 Date
urate and complete to the best of my knowledge.
The pennittee shall report tc the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the envirotttnetkl.
Any information shall be prttvided orally within 24 hours froth the time the pennittee became aware of the circumstances. A written suthtnission shall also be
provided within 5 days of the time the pennittee becomes aware of the circumstances.
[f the facility is noncompliant, please attach a Iist of corrective actions being taken and a ti
the NPDES pen
Pe
table for improvements to be made as required by past ILE.& of
ure:••• Angela S Brown E-Mail.asbrown(a?marathonpetroleum.com Phone :419m 421-26i
9/11/2019
Date
Pcrmittee Address: 80351'a o nt Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance w ith a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who mana);ed the
system, or those persons directly responsible for gathering the information, the information submitted i , to the best duly knowledge and belief, trm,
accurate, and complete, I am aware that there are significant penalties for submitting false infonnation„ including the possibility c'f fine and imprisonment for
knowing violations.
LAB NAME: Pace A.
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES: J Qua 1ticri
:.0
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance maybe obtained by calling the NPDES Unit [phone] or by visiting http.i portal.nedenr,orglw°c:b:wq,rsw ips..npdcs/`forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
No FlowDischarge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered fur all of the parameters on hie DMR
for entire monitoring period.
•" ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC SG .0204,
••• Signature ofPermittee: if signed by other than the pennittee, then delegation of the signatory authority must be on file with ram. tote per ISA yCAC 2B
,0506(b)(2 KD).

F�
August 26, 2019
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
MPLX Ter , is c
A subsidiary of Marathon (ti R, V R
539 South Main Street
Findlay, 0H 45840
Tel: [phone]
WOR",T;;
MOORS IL f RE(,c N
Sent via ©vernijht Mail
Enclosed please find the July 2019 NPDES report, plus one copy, for the above -referenced permit.
Also included is the quarterly toxicity test. Please note that on July 8, a sample for FTHD24AC
WET (Parameter Code TAE6C) was taken and delivered to the lab that processes the bioassay
sample. The bioassay sample was not received within compliant temperature range at the Pace lab.
The sample was discarded. On July 24, FTHD24AC WET (Parameter Code TAE6C) was resampled
and reported in this DMR with the required concurrent sampling parameters.
If you have any questions or require additional information, I can be reached at 419-421-201.9 or by
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc, Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)
NC DENR -- Division of Water Resources
Water Sciences Section / Aquatic Toxicology Branch
1621 Mail Service Center
Raleigh, NC 27699-1623

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 07-2019 (July 2019)
0
1400 cleKk
2
4
7
9
10
11
14,
1$
411
17
19
20
21
22
14
2$
26
27
28
29
30
21
PERMIT VERSION: 4 0
CLASS:. PC-1
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
bt
ict
Hes 2400 clock
1105
t-
Ors
0,25
015
Y
a
Moothly Avcroge Limit
500$41 C11530
Sre Permit Monthly
Recorder Grab
FLOW TSS Coor
mgd mg11.
0,001 16.5
0,00 i
0,266
M"'hlY A.'"V' 0 089333 16 5
Omni Miannanv. 0,266
Doily Miolnx0tnt 0,001
16.5
16,5
34030
Monthly
Grab
BENZENE
34371
Quarterly
Grub
E1111214119
<
=, I
TACK
Quarterly
Grab
9T111114AC
percent
> 1(X)
100
100
I 00
12421 3409n
Quarterly Quarterly
Grab Grab
WIVE FFLALE
ug/I ug./1
< ,< I
<5 <
0
(1
00556
Monthly
Gtab
(111,GIRSE
inW1
<5
**** No Reporting Reason: ENFRUSE =No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY No Visitation — Holiday
32730
Monthly
Grah
*000/21,1011
= 0.02
< 0.02
0

N PDES PERMIT NO.: NC0046213 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal CLASS: PC-1 COUNTY: Mecklenburg
OWNER NAME: Mplx Terminals LI.0 ORC: Darryl Keith Thompson ORC CERT NUMBER: 1005070
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 07-2019 (July 2019) VERSION: 1 AI
ra
2
3
4
7
$
10
It
12
13
14
00
16
17
IS
19
20
21
2'3
24
25
26
27
29
29
30
31
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2400 cloak Hrn 2490 cloak
1105
0515
0900
41
fin
0,25
0.25
0.25
Y/B/N
Y
Y
34010
Quarterly
Grab
TOLUENE
Monthly Average Limit
Monthly Average:
0
Daily Maximum: 0
Dal2y131101/11111111 0
00070
Monthly
Grab
111111110T1
nlu
19.4
294
J9,4
194
01551
Quarterly
Grab
%YU:NC
ug/1
v4 1
3
"" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR No Visitation Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation —Holiday

NPDES PERMIT NO.: ',C004621 3
FACILITY NAME: Ch (ione Terminal
OWNER NAME: Mplx criminals LLC
GRADE: PC-1
eDMR PERIOD: 07-20 (Juiy2019
COMPLIANCE STATI ti: C
PERMIT VERSION:4.0 PERMIT STATUS: Acthc
CLASS: PC -I COUNTY: Mecklenburg
ORC: Darryl Keith Thompson ORC CERT NUMBER: 1005070
ORC HAS CHANGED: Nu
VERSION: 1.0 STATUS; Processed
CONTACT PHONE #:[phone] SUBMISSION DATE: 03'2112019
08/09120 19
ORC/Certifier Sivature: Darrgf'eith Thom s 'Ldk homps arathonpetroleum.com Phone 4:980-6 13-04 05 Date
By this sigriature, I eel fy that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the c ironment.
Any information shall Pc provided orally within 24 hours from the time the permitter became aware of the circumstances, A writi,:n submissioe ,halt also be
provided within 5 day of the time the pennittee becomes aware of the circumstances.
If the facility is noncoiapliant, please attach a list of corrective actions being taken and a timetable for improvements to be mads required by art 11E6 of
the NPDES permit,
08f2i2OI9
Permitte bmittL r Signature:*** Angela S Brown E-Maikasbrown(marattionpetroleum.com Phone ii.419-421 !9 Date
Permittee ddress: 80 5 Mourn Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalt) of law, that this document and all attachments were prepared under my direction or supervision in accord ATIec with a sy n designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who maiiiiged the
system, or those persoi is directly responsible for gathering the information, the information submitted is, to the hest of my knowlii,,Ige and belie. true,
accurate, and complete 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and im isonment for
knowing violations,
CERTIFIED LABORATORIES
LAB NAME: Pace Anal \ ((cal Services, 1.I.0
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES; 1 Quatfkn
PARAMETER CODES
Parameter Code iissistince may be obtained by calling the NPDES Unit [phone] or by visiting http://porial,ncdennorgwetowq/swp/ps/rpdes/fornis,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge 1 rom Site: Check this box if no discharge occurs and, as a result, there are no data to he entered for all of the parameters i the DMR
for entire monitoring period.
** ORC on Site?: OR( must visit facility and document visitation of facility as required per I5A NCAC 8G ,0204.
***Signature of Permittee: If signed by other than the perrnittee, then delegation of the signatory authority must be on file with the state per I5,1, NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 07-2019 (July 2019)
PERMIT VERSION: 4,0
CLASS: PC -I
ORC; Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 1,0
Report Comments:
Analytical report for ETFID24AC WET Testing (Parameter Code TAE6C) is being submitted with hardcopy DM R.
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
On July 8, a sample for FTHD24AC WET (Parameter Code TAE6C) was taken and delivered to the lab. The sample was not received within compliant temperature range at
Pace National lab, The sample was discarded, On K July 24, FTHD24AC WET (Parameter Code TAE6C) was resampled and reported in this DMR.

Effluent Toxicity Report For
Chronic Pass/Fail and Acute
C50 Date
PAce Hunters4 ratS:Q➢k W89C w
Facility charlotte TenninAlto.tfa11 a n NPDES#NC 0046213
Laboratory Performing Test Pace Nat icrnal
x
in Responsible horde
of LaborMbry Supervisor
Pipe # County Mecklenburg
Comments
Pace Nat .ona1 ID: l,1:i22185-01
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
s
a
1st sample
Control
D.O.
Treatment 2
e
n
d
2 3 4 5 6
7 8 9 10
2 3 4 5 6 7
a
1st sample
e
n
d
2nd sample
s
t e
a n
r d
2nd sample
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replic
0
12.5
25
0
50
75
OA
1©0
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
11 12 Chronic Test Results
Calculated t
Tabular t
% Reduction
10 11 12
%Mortality
Control
Treatment 2
Control CV
% control organisms
producing 3rd brood
er Test
Collection (Start) Date
Avg.Reprod.
Control
Treatment 2
PASS FA
Check One
Test Start Date
7 /25/19
(not applicable)
Sample 1 7 / 24 /19 Sample 2 / /
Sample Tvpe/Duration
Sample 1
Sample 2
0
Hardness mg
Spec.Cond.(pmhos
Chlorine(mg/t
Sample temp. at receip
Concentration
Mortality
LC50= a 1 0
95% Confidence Limits
Method of Determination
Moving Average 0 Probit
Spearman Karber © Other N/A
Organism Tested Pimephales promelas
Duration (hrs) 24 hrs
DWQ form AT-1 (3/87) rev. 11/95
start/end
pH
Note: Please
Complete This
Section Also
start/end
Contro
High
Conc.
D.Q.
1 of 10

Chart Devices Used in
, Therm©_KQet Walk-in Incubator.
Dickson (small chart)
Thermo Graph for
e
Ch1
Ch2
Cur.A Date : 07/18/2019 19:25'52
Cur,B Date : 07/30/2019 4:28'09
diff. A-3 : 11 09:02'17.000
07/'224/19
08/01/2019 16:21'21
07/30/
0:00'00 0:00
Intv1. Sample
2min. 8000
2min. 8000
Cur.B A High Low Avg. Unit
- _- 26.6 24.3 25.6 °C
26.7 24.3 25.6 °C
Data Range 07/18/2019 19:25'52-07/30/2019 4:28'09
Ca1c.Range 07/18/2019 22:37'50-07/30/2019 1:16'11
V

ace Analytical°
Nolion«? Cerrear re.Miry OW101,1tharZ
Pace (Huntersville) - Marathon West - Charlotte Terminal -
Client:
(Outfall 001)
NPDES #: NC0046213
Test Start Date: 1 671
Temperature (QC) - Pimephales promelas (fathead minnow)
Control
12.5
25
50
75
100
Date:
Day 1 (initiation)
°c
Oc
°c
c
°c
Date:
Time: Analyst:
M). 306
Day 2 (morning)
94 °c
Time: Analyst:
Day 2 (final)
t( °C
-14-1 -5 °c
" Measurement taken directly In test chamber
oc
Lab Sample #:
Thermometer Serial Number: 18050064
Control Water Carboy Used
7 /
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH(Temp/mV/ISE Meter
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chambers: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c - VWR Traceable Dual -Range Light Meter- Model 62344-944 (S/N 181399747)
Photoperiod: 16 hours light, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific Isotemp Oven, Model 655F
Mean Dry Weight Determined using Mettler Toledo Balance, ATM Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Shain W. Schmitt (SWS); Brandon Etheridge (BE); Adam Macomber (AM)
Amy Eggleston (AME); Melissa Holwerda (MM); Cody Medley (CM); Nadler Yakob (NY); Clarissa Moore (CGM);
Brittnie Boyd (BB); Joel Soto (JSV), Rachel Conradi (RC), Jessica Davis (JOD)
3 of 10

Analytical
tr ter fur Tearing & innovation
ACUTE TOXICITY TEST DATA - Pimephales promelas (fathead minnow)
Client Pace (Huntersville) - Marathon West - Charlotte Terminal -
(Outfall 001)
Begin
End
Effluent in Replicate
Percent (%) Position
A:
CONTROL
B:
A:
12.5
25
50
A:
75
B:
1©©
Checked By: Biologist:
)5V
Fish Cup EiatchIL.ot:
Time:
Time
Time
# OF LIVE Minnows
O hrs 24 hrs
10
10
10
10
10
10
10
10
10
10
10
10
5000X82944
IC
e been recorded on the
E
heck here to con
mperature benc
Brine Shrimp Lot:
NPDES # NC0046213
Test Duration:
Dilution Water:
pH (std, units)
O hrs 24 hrs
8313223
24 hours *end test +/
10% DMW
Dissolved Oxygen (mg/L) Conductivity (umhoslcm)
0 hrs 24 hrs 0 hrs 24 hrs
final
final
final
g, 2
final
final
final
I2►.a
final
final
Lir
final
final
1u
Data divided by a slash mark ( / ) indicates that a duplicate was run on that parameter. Temperature of water (minnow batch) at time of test initiation: 2. Z Z_ °C
Minnows were Lu days old at test initiation and were taken from ESC Lot # it,. , d ` , Minnows were last fed
Control
0
AlkalIIIttty
100% Effluent
(Preliminary©) Hardness
Analyst: p p
Date: j—lt"~6C1
Time:
Control
analyzed prior to
initiation by Wet
Lab using:
LACHAT
Hardness
hr from start time
Total Cl2
(mg1L)
Control
< ©.2
Total Ct2 (ing&)
100%anIo fl
prior to the test.

Dates
09/05/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/ 18
01/03/19
01/03/19
01/16/19
01/23/19
01/23/19
02/06/19
03/06/19
04/03/19
04/03/19
05/01/19
05/01/19
06/05/19
06/05/19
07/10/19
Control Chart for July 2019 Acute C. dubia Refrence Toxicant
CV% = 21.2
Valu+ s
0.6547
0.5535
0.7040
0.6373
0.5391
0.4531
0.8801
1.0710
0.5946
0.6830
0.5840
0.6156
0.6156
0.4830
0.6373
0.7436
0.7500
0.6338
0.5477
0.7071
Mean
0.6041
0.6374
0.6374
0.6177
0.5903
0.6317
0,6866
0.6764
0.6770
0,6686
0.6642
0.6604
0.6478
0,6471
0.6531
0.6588
0.6574
0,6516
0.6544
Date
-1 SD
!ceAnalytic
Na ttc>nsf Canter for Tasting R fnnOvait on [phone]
[phone] Fax
0,5325
0.5607
0.5747
0.5479
0.4985
0.4938
0.4855
0.4858
0.4974
0.4958
0.4988
0.5015
0.4879
0.4930
0.5023
0.5109
0,5138
0.5098
0.5158
-2 SO
0.4610
0.4839
0.5121
0.4781
0.4068
0.3559
0.2845
0.2953
0,3177
0.3231
0.3334
0.3426
0.3280
0.3389
0.3515
0.3630
0.3702
0.3680
0.3772
+1 SD
0.6757
0.7141
0.7000
0.6875
0.6820
0.7696
0.8877
0.8669
0.8567
0.8413
0.8296
0.8194
0.8077
0.8012
0,8039
0.8067
0.8010
0.7935
0.7930
12065 Lebanon Rd
Mt, Juliet, TN 37122
July 2019
Reference Toxicant Test
+2 5D
+1 SD
Mean
-1 SD
-2 SD
+2 SD
0.7472
0.7909
0.7627
0.7574
0.7738
0,9075
1.0887
1.0575
1,0364
1.0141
0.9950
0.9783
0.9675
0,9553
0,9547
0.9546
0.9446
0.9353
0,9316
5 of 10

Control Chart for July 2019 Chronic C. dubia Refrence Toxicant
CV% 31.1
0.54
0.49
0,44
0.39
0.34
0.2
0,24
0.19
0.14 =
0.09
Dates
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01/08/19
01/22/19
01/22/19
01/29/19
01/29/19
02/05/19
03/05/19
04/02/19
04/02/19
05/07/19
06/04/19
06/04/19
07/09/19
Values
0.2935
0.2994
0,3091
0.2133
0.3355
0.2369
0.3662
0.1269
0,4433
0,2852
0.3669
0.2759
0.3074
0.2578
0.2880
0.4115
0,1409
0.3408
0.3784
0,1108_
n
0,2965
0,3007
0.2788
0.2902
0.2813
0.2934
0,2726
0,2916
0.2909
0.2978
0.2960
0.2969
0.2941
0.2937
0,3011
0.2916
0.2944
0.2988
0.2894
Date
0.2923
0.2928
0.2347
0.2443
0.2348
0.2402
0.1959
0.2000
0.2045
0.2127
0.2146
0.2189
0.2184
0.2208
0.2247
0.2081
0.2125
0.2169
0.1993
ace Analytical
National Cantor for Testing & Inrrrn are r+
-2 SD
0.2881
0.2849
0.1905
0.1984
0,1884
0.1871
0.1191
0.1084
0.1182
0.1277
0.1332
0.1409
0.1428
0.1479
0.1484
0,1246
0.1307
0.1351
0.1093
+1 SO
0.3006
0.3085
0,3230
0.3360
0.3277
0.3466
0.3493
0.3832
0.3773
0.3829
0.3774
0.3749
0.3697
0.3666
0.3774
0.3751
0.3762
0.3806
0.3794
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
July 2019
Reference Toxicant Test
+2 SD
+1 SD
Mean
1 3D
2 SD
+2 SD
0.3048
0.3164
0.3671
0.3819
0.3742
0.3998
0.4261
0.4748
0.4637
0.4680
0.4588
0.4528
0.4454
0.4395
0.4537
0.4586
0,4580
0.4625
0.4695
6 of 10

Control Chart for July 2019 Acute Minnow Refrence Toxicant
CV% 16.8
1.7
Dates
09/05/18
09/27/18
09/27/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
02/06/19
03/06/19
04/03/19
05/01/19
05/01/19
06/05/19
06/05/19
07/10/19
Values
1.2000
0.7387
0.7387
0.8196
0.8196
0.7715
0.6375
0.7000
0.8785
0.9415
0,9094
0.8485
0.6000
0.8801
0.9524
0.8667
0.8647
0.7917
0.8196
0.6000
Mean
0.9694
0,8925
0.8743
0.8633
0.8480
0.8179
0.8032
0,8116
0,8246
0.8323
0.8336
0.8157
0.8203
0.8291
0.8314
0.8334
0.8311
0.8305
0.8189
Date
-1 SD
0.6432
0.6261
0.6538
0.6708
0.6718
0.6385
0.6319
0.6494
0.6662
0.6799
0.6883
0.6621
0.6718
0.6820
0,6890
0.6952
0.6967
0.6998
0,6818
ace Analytical
r r_ Th0
-2SD
0.3170
0.3598
0.4333
0.4783
0.4956
0.4590
0.4606
0.4872
0.5079
0.5275
0.5429
0.5086
0,5233
0.5348
0.5466
0.5571
0.5623
0.5692
0.5446
+1 SD
1.2955
1.1588
1,0947
1.0558
1.0242
0.9974
0.9745
0.9738
0.9829
0.9847
0.9790
0.9692
0.9688
0.9762
0,9739
0,9715
0,9654
0.9611
0.9561
12065 Lebanon Rd.
Mt, Juliet, TN 37122
[phone]
[phone] Fax
July 2019
Reference Toxicant Test
2 SD
1 SD
Mean
-1 SD
-2 SD
+2 SD
1.6217
1.4251
1.3152
1.2483
1.2005
1.1769
1.1458
1.1360
1.1412
1.1370
1.1244
1.1227
1.1173
1,1233
1.1163
1.1097
1.0998
1.0917
1.0933.
7 of 10

Control Chart for July 2019 Chronic Minnow Refrence Toxicant
DV%=10.1
0.7
0.65
0.6
0.55
0.5
0.45
0.4
0.35
0.3
Dates
03/06/18
04/03/18
05/01 /18
06/05/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01/08/19
01 /29/19
02/05/19
03/05/19
04/02/19
05/07/19
06/04/19
06/04/19
07/09/19
Values
0.4562
0.5069
0.4335
0.5210
0.4300
0.5491
0.4410
0.4705
0.4976
0.5790
0.6174
0.4553
0.4956
0.5462
0.5583
0.4570
0.5036
0.5190
0.4995
0.5320_
Mean
0.4816
0.4655
0.4794
0.4695
0.4828
0.4768
0.4760
0.4784
0.4885
0.5002
0.4965
0.4964
0.5000
0.5038
0.5009
0.5011
0.5021
0.5019
0.5034
Date
-1 SD
0,4457
0.4280
0.4380
0.4274
0.4331
0.4288
0.4315
0,4361
0.4375
0.4381
0.4359
0.4384
0.4427
0,4466.
0.4444
0.4463
0.4488
0.4502
0.4526_
aceAnalytica�
National Center for Thsting 8 1nnov io,i
-2 SD
0.4098
0.3904
0.3967
0.3854
0.3833
0.3807
0.3869
0,3938
0.3865
0.3761
0.3753
0.3804
0.3854
0.3894
0.3879
0.3916
0.3956
0.3984
0.4018
+1 SO
0.5174
0.5031
0.5208
0.5116
0.5325
0.5249
0.5206
0.5207
0.5395
0.5623
0.5570
0.5544
0.5572
0.5611
0.5574
0.5558
0.5553
0.5537
0.5543_
)65 Lebanon Rd
uliet, TN 37122
[phone]
[phone] Fax
July 2019
Reference Toxicant Test
+2 SD
- +1 SD
Mean
- -1 SD
-�-. -2 SD
+2 SO
0.5533
0.5407
0.5621
0.5537
0.5822
0.5729
0.5651
0.5630
0.5905
0.6243
0.6176
0.6124
0.6145
0.6183
0.6139
0.6105
0.6086
0.6055
0.6051
8 of 10

0
Chain of Custody
0 Samples were sent directly to the Subcontracting Laboratory.
rkorder: 92438389 Workorder N NC0046213 CLT WEST OASSAY
Angela Baioni
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100
F$untersville, NC 28078
Phone [phone]
L1TFALL DOl
Released By
Pace National
12065 Lebanon Rd
Mt Juliet, TN 37122
615-758-5858
cofiect
Datelliree
7124/2019 08,10
Lab 81
92438389001
Date/Time *alvd By
Custod Seal Y or gr;)
State Of Origin: IN
Cert. Needed: Yes Ei No
Rcehied Date: 7/24/2019 Re
'Ott rved
Daterrirne
Received on ice / or N
ceAnalytical
WM.V.P.A".01404, =WTI
ults Requested By: 7 2
ussted A at sis
Cernateete
LAB USE ONLY
***In order to maintain client confidentiality, locationlname of the sampling site, sampler's name and signature may not be provided on this COC document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
--k VV erine
0
9 40610 PM
Fhli-ALL-C-002rev,00 24March2009

National Center 1
Cooler Receipt F t
Cooler Received/0 ened On: 7
Received By: Riley Dempsey
Scnaure:
Receipt Check List
COC Se
Presen
COC Signed / Accurate?
n
ct?
Correct bottles user
Suffici
en volume sent?
If Applicable
VOA Zero headspace?
lion Correct t Checked?
Preery
0
X
9 Tem.era ure:
wA
NP
Yes

ARATNO
July 15, 2019.
NC DENR TDWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
CENT
RE. NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
L FILES
ECTION
P Ter
A aiiory of Marathon Pe
lna
539 South Main Street
Findlay, OH 45840
Tel: [phone]
1-1ECElvl'w't NC"
Sent via Overnight
S l(.11.0
NR/DW1
1NAin. Cal ICE
Enclosed please find the June 2019 NPDES report, plus one copy, for the above -referenced permit.
If you have any questions or require additional information I can be reached at 419-421-2019 or by
email at ErRisner'MarathonPetroleum.com.
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environnie
a
anual (Water: NPDES; NPDES D%`IRs)

-
NPDES PERMIT NO.: N00046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 06-2019 (June 2019)
COMPLIANCE STATUS: Co
ORC/Certifier Signature: Darryl K
PERMIT VERSION: 4
CLASS: PC-1
ORC: Daryl Keith Thompson
ORC HAS CHANGED: No
VERSION:LO
ACT PHOT #i 4194212{i19
ormpson E-Mail:dkt
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
SUBMISSION DATE: 07/10/2019
07/08/2019
Phone #:[phone] Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens publie Itealth or the environment,
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the tithe the pennittec becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part I1.E,6 of
the NPDES permit.
07/10/2019
Submitter ggnature.*** Angela S Brown E-Mait:[e-mail] Phone tt:419-421-2629 Date
Permit ee Address: 803 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best (Amy knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Pace Analytical Scrvics:s, LLC
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES: J Qualficri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http:/tportal,ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units oftmeasurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Cheek this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
ORC on. Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
*** Signature of Perrnittee: If signed by other than the pennittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D)•

NPDES PRMIT NO.: NC0046213 PERMIT VERSION: 4.0EC
FACILITY NAME: Charlotte Terminal CLASS: PC-1 JUN 1 4 2°1
OWNER NAME: Mplx Terminals LLC ORC: Darryl Keith Thompson
,.. Vt L. r 1L v
GRADE: PC-1 ORC HAS CHANGED: No a LCT ION
eDMR PERIOD: 05-2019 (May 2019) VERSION: 1,0
PERMIT STATUS: Active
COUNTY: Mecklenb
HECEIVEMCDENR/DWR
ORC CERT NUMBER: 1005070
STATUS: Processed
N
WQROS
MOORESVILLE REGIONAL OFFICE
SAMPLING L©CATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
a
oFLOW
mSee
50050
C0530
34030
00556
32730
00070
Permit
Monthly
Monthly
Monthly
Monthly
Monthly
Recorder
Gr b
Grab
Grab
Grab
Grab
TSS -Cunc
BENZENE
OIL-GRSF.
Fl1EN.TR
TURBIDTY
2400 clock
firs
2400 clock
Hrx
Y/B/N
mgd
mg/1
u8/1
mg/1
mg*/l
ntu
4
6
7
0
9
10
MO
0.25
Y
0,005
12,2
<I
<5
<0.02
19,1
r
r
13
0-615
0.25
Y
0.264
14
11920
0.25
Y
0.156
15
16
17
IN
19
20
21
22
23
24
25
26
27
20
29
30
31
1
Monthly Average [Halt:
30
Monthly Average:
0.141667
12.2
0
0
0
19,1
Dolly Maximum;
0.264
12,2
0
0
0
19,1
Dolly Minimum:
1,005
12.2
0
D
0
19,1
***4 No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW - No Flow; HOLIDAY = No Visitation - Holiday

NPDES 6RMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mp1x Terminals LLC
GRADE:PC-1
eDMR PERIOD: 05-2019 (May 2019)
COMPLIANCE STATU
PERMIT VERSION: 4A
CLASS: PC-1
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mecklenbur&
ORC CERT NUMBER: 1005070
STATUS: Processed
SUBMISSION DATE: 06/
06/03/2019
ORC/Certifier Signatuyl Keith Thomason E-Mail:dkthompsongmarathonpetrcteum.cotn Phone #:[phone] Date
By this signature, i certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances, A written submission shall also be
provided within 5 days ate time the permittee becomes aware of the circumstances,
If the facility is noncompliant, please attach a list of corrective actions being taken and a titre -table for improverxsents to be made as required by° part II.E.6 of
the NPDES pc
06/ 11 /2t119
Per ri^ itiee/Submi� signature:*** Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: 35 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachtnents were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who rn:tnagcd the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Pace Analytical Service
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES:
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
ORC. on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Pennittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per E SA NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0046213 PERMIT VERSION: 4.0 PERMIT STATUS: Active
i.
FACILITY NAME: Charlotte Terminal CLASS: PC-1 d J COUNTY: Mecklenburg
.w�
OWNER NAME: Mplx Terminals LLC ORC: Darryl Keith Thompson V �y ORC CERT NUMBER: 1005070
ORC HAS CHANGED: No MAI 2 3 ZD'a
VERSION: 1.0 EN ft'\L F1L..ES STATUS: Processed
DWR SECTION
GRADE: PC-1
eDMR PERIOD: 04-2019 (April 2019)
RECEIVEDFNCOENR/DWR
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NQ QRos
MOORESVILLE
REGIONAL
n
tx
g
yg
C°
U
p
x
50050
C0530
34030
34371
TAE6C
22417
34696
00556
3I730
See Permit
Monthly
Monthly
Quarterly
Quarterly
quarterly
Quarterly
Monthly
Monthly
Recorder
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
FLOW
'r8S•Cone
BENZENE
E9'HY"I.BF,N
4T1024AC
MTBE
NA PTHALE
014GR.SE
PI/EN. TR
2400 clock
lira
2400 clock
Bra
Y!H/N
mgd
mg/I
ug/I
u0/I
percent
ug/1
uy,%1
mg/I
me
2
4
8
1340
0.25
y
0.002
11.2
< 1
<I
.> 100
1.3
< 1
<4.8
<0.02
l0
1000
0.25
Y
0.302
22
12
13
14
15
1020
0,25
Y
0,205
16
17
I8
19
20
21
22
23
24
25
26
27
20
29
30
*
r
Mon 61v Average Limit,
30
Monthly Average:
O.169667
11.2
0
0
100
1,3
0
0
0
Daily Nle. mnma
0.302
11.2
0
0
100
1.3
0
0
0
Dole Minlmema
0,002
11,2
0
U
100
1.3
0
0
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR No Visitation - Adverse Weather„ NOFLOW = No Flow; HOLIDAY No Visitation - Holiday
OFFII

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 04-2019 (April 2019)
PERMIT VERSION: 4.
CLASS: PC-1.
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 1.
PERMIT STATUS: Active
COUNTY: Mecklenburg;
ORC CERT NUMBER: 1005070
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
r„1
'C
d
.g
n
p
34010
00070
01551
Quarterly
Monthly
Quarterly
Grab
Grab
Grab
TOLUENE
TIiRBIDTI"
XYLI;NE
24011 clack
firs
2400 dock
lira
bB/N
ug/I
ntu
ug^'I
4
7
11
1340
0.25
Y
< 1
11.3
< 1
10
1000
0.25
Y
11
12
13
14
15
1020
0.25
Y
16
17
IN
19
20
21.
22
23
24
25
26
I7
20
29
30
Man hly Average Limn:
1
Monthly Average:
0
11.3
0
Da0y Maalmum:
11.3
0
Daily Minimum,
0
113
0
***. No Reporting Reason: ENFRUSE - Nu Flow-Reuse/Recycle; ENVWTHR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation -- Holiday

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE; PC-i
eDMR PERIOD; t}4 019 (April 2019)
COMPLIAN
ORC./Certifier Signa
PERMIT VERSION; 4,0
CLASS: PC-1
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
PERMIT STATUS: Active
COUNTY: Mccklenbur$
ORC CERT NUMBER; 1005070
VERSION; 1.0 STATUS: Proccssc.i
ONTACT PHONE [phone]Ei19 SUBMISSION DATE: 0512ft12019
05/08/2019
ryl Keith Thompson E-Mail:dkthompson(c marathonpetroleum.com Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becotnes aware of the circumstances,
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part ELE.6 of
the NPDES permit.
Perntittee/Submitter fgnature:*** Angela
05/2t}/2i319
E-Mail:[e-mail] Phone 4:419-421-2629 Date
Permittee Address: 803 14tount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designer[
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge arid belief, true,
accurate, and complete. [ am aware that there arc significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Pttec Analytical Services„ LLC
CERTIFIED LAB #;
PERSON(s) COLLECTING SAMPLES:1 t ualficri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenr.org/web/'wq/swp/ps/npdes/form:.
FOOTNOTES
Use only units ofrn surr„*ment de*tignated in the reporting facility's NPDES permit for reporting data,
* No FIowfDischarge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
tier entire monitoring period,
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
*** Signature of Perrnittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
,0506(b)(2)(D)•

Effluent Toxicity Report Form- Chronic Pass/Fail and Acute LC50 Date 5-1-19
Pace Munteraw111e- Marathon Nest -
Facility Charlotte Terminal,'©utfall 001i NPDES#NC 0046213
Laboratory Performing Test Pace National
x
Signature Operato Responsible Charge
5-.209
Sighe a of Labor €5ry Supervisor
Pipe # County Mecklenburg
Comments .
Pace National ZD:
6 2-©1
MAIL ORIGINAL TO:
North Carolina Cerlodaphnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
a
1st sample
Control
D.O.
Treatment 2
e
n
d
1 2 3 4 5 6 7 8 9 10
1st
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh. North Carolina 27699-1621
11 12 Chronic Test Results
Calculated t
2 3 4 5 6 7 8 9 10 11 12
e
n
d
1st sample
2nd sample
$
t e
a n
r d
2nd sample
LC50/Acute Toxicity Test.
(Mortality expressed as %, combining replicates)
%
Q
12.5
0
yo
%
25
0
% %
5© 75
%
1©©
%
Tabular t
Reduction
itv
Control
Treatment 2
Control CV
% control organisms
producing 3rd brood
CompleteThis For Either Tes
Avg.Reprod.
Control
Treatment 2
PASS FA
Test 5tsrt Date
4 / 9 /19
Collection (Start) Date (not applicab
Sample 1 4/ 8 /19 Sample 2 / /
Sample Type/Duration
Sample 1
Sample 2
Grab
grab
N/A.
Comp.
Duration
N/A
Hardness(mg/i
Spec.Cond.(pmhos
Chiorine(mg/l
Sample temp. at receip
41.©
22
.4
NIA
N/A
N/A
%
0/
Concentration
Mortality
LC50= > 1©© %
95% Confidence Limits
%-
hod of Determination
Moving Average © Probit
Spearman Kerber
Other N/A
Organism Tested Pimephales promelas
Duration (hrs)24 hrs
DWQ form AT-1 (3/87) rev. 11/95
start/end
7.8
7.6
pH
8.9
7.6
Note: Please
Complete This
Section Also
Control
High
Conc.
start/end
8.6
8.9
8.8
7.8
1 of 10

ace Analytical
? Center for Testing K inrmwration
Pace (Huntersville) - Marathon - Charlotte
Client: Terminal (Outfall 001)
NPDES #: NC0046213
Test Start Date:
I
Temperature (" C) - Pimephales promelas (fathead minnow)
Control
6.25
12.5
25
50
100(PL)
Date: 44-1 - ( 1
Time: Analyst:
i S ' �s8
Day 1 (i itiati
on)
°c
Date: t1,.
Time: Analyst:
i0 fill. ii'
Day 2 (morning)
zq
°C
°C
°C
Time: Analyst:
Measurement taken directly in test chamber
Day 2 (final)
°C
Lab Sample #:
Thermometer Serial Number: 18050064
Control Water Carboy Used:
67040? !g
-t"tovr. wv55ed
Adt. ip AkAIkisi-ewOV
Alm 6- I - iq
Outfall
001
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH/TemplmV/ISE Meter
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Water Bath: Lindberg/Blue, Model WB1140A-1 (serial #S01M-580360-SM)
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chamber: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c - VWR Traceable Dual -Range Light Meter- Model 62344-944 (S/N 181399747)
Photoperiod: 16 hours tight, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific Isotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Brandon Etheridge (BE), Shain W.Schmitt (SWS), Nadiar Yakob (NY), Brittnie Boyd (BB),
Joel Soto (JSV), Meaghan Robinson (MLR), Amy Eggleston (AME), Melissa Mathis (MM), Adam Macomber (AM),
Cody Medley (CM), Clarissa Moore (CGM), Rachel Conrad' (RC)
©0

Tutavhr
NOON
Chart Devices Used in
Thermo-Kool Walk-in Incubator:
Dickson (small chart)
Idompimiseimppolumemp
Thermo Graph for Windows
50"06
Name Intv1. Sample Cur.A Cur.B A<->H High Low Avg. Unit.
Ch1 2min. 8000 -- ----- 25.9 24.3 25.1 °C
2 Ch2 2min. 8000 - --- -- -_ 25.9 24.3 25.1 °C
Ch1 2min. 8000 __-- -- --- - 25.8 24.3 25.0 °C
4 Ch2 2min. 8000 _- --_- --- 25.8 24.3 25.0 °C
Cur.A Date : 03/28/2019 17:19'53
Cure Date : 04/1.6/2019 6:25'08
diff. A-H : 18 13:05'15.000
Data Range 03/26/2019 17:19'53-04/16/2019 6:25'08
Calc.Range 03/26/2019 22:32'50-04/16/2019 1:12'11
0

NORTH CAROLINA ACUTE TOXICITY TEST DATA SHEET - Pimephales promelas (fathead minnow)
client Pace - Huntersville - Marathon - Charlotte Terminal (Outfall 001) NPDES # NC0046213
Begin
End
Time
Time
Effluent in Replicate # OF LIVE Minnows
Percent (%) Position 0 hrs 24 hrs
CL2
(mg/L) 10')/0 DMW
< 0.2 CONTROL
CL2
(m9/1-)
"Z7
12.5
25
50
75
100(PL)
A:
B:
B:
B:
Biologist
Time
10
10
10
10
10
10
10
10
10
10
10
10
UP
0
I
O
1()
10
/0
0
ID
0
tA5
t(12
2 3
*end test +/- 1 hr
from start time
pH (std. units)
0 hrs final
initial
initial
CC
initial
initial
-7,7
initial
--04;
Test Duration: 24 hours ESC Sample #:
Dilution Water: 10% DMW e../00024/Z - 01
Minnow final
vFir
Minnow final
Minnow final
Minnow final
Minnow final
1 Co
Minnow final
Initial Readings By:
(.9
2:2)
Di dyed Oxygen (mg/L)
0 hrs final
initial
initial
s
initial
initial
,(4
initial
Minnow final
Minnow final
79
Minnow final
Minnow final
Minnow final
7
Minnow final
7
Fn Readings By:
Data divided by a slash mark ( / ) indicates that a duplicate was run on that parameter. Temperature of water (minnow batch) at time of test initiation: /l1,9 °C
Minnows were days old at test Initiation and taken from ESC Lot # 01-101/9H 0 Minnows were last fed / 6
AtIvlinity
0
Control
LACHAT
37
100% Effluent
LACHAT
(Preliminary) Hard,.neAs
Analyst: c:11 got
Date:
Control
analyzed prior to
test initiation by
Wet Lab using:
LACHAT
Hardness
Conductivity
(umhos/cm)
initial
,
initial
initial
3-
initial
Sc)
iriital
cCS
Conductivity
(umhos/cm)
Final
c).3
Final
12-1.
Final
Final
t2.1-1,(D
06 prior to the test.
100% Efftuen
Final
analyzed in Wet
Lab via LACHAT

u
Dates
Control Chart for April 2019 Acute C. dubia Reference Toxicant
CV% = 21.9
1.2
1.
0.9
0.8
0.7
0.6
0,5
0,4
0,3
04/04/18
05/02/18
06/19/18
07/03/18
08/02/18
09/05/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
01/23/19
02/06/19
03/06/19
04/03/19
04/03/19
Values
0,4910
0.6156
0.7368
0.5835
0.6156
0,6547
0.5535
0,7040
0,6373
0,5391
0.4531
0.8801
1.0710
0.5946
0.6830
0.5840
0.6156
0.6156
0.4830
0.6373
Mean
0.5533
0.6145
0.6067
0.6085
0.6162
0.6072
0.6193
0.6213
0.6131
0.5986
0.6220
0.6566
0.6521
0.6542
0.6498
0.6478
0.6460
0.6374
0.6374
Date
-1 SD
0.4652
0.4916
0.5052
0.5205
0.5352
0.5296
0.5398
0.5467
0.5381
0.5126
0.5066
0.4901
0.4913
0.4990
0.4989
0.5014
0.5038
0.4942
0.4981
-2 SD
0.3771
0.3687
0.4036
0.4325
0.4543
0.4520
0.4602
0.4720
0.4630
0.4265
0.3911
0.3235
0.3305
0.3438
0.3479
0.3550
0.3616
0.3511
0.3587
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
April 2019
Reference Toxicant Test
0.6414
0.7374
0.7083
0.6965
0.6972
0.6849
0.6989
0.6960
0.6882
0.6846
0.7375
0.8231
0.8130
0.8094
0.8008
0.7942
0.7882
0.7806
0.7768
+2 SD
+1 SD
Mean
-1 SD
-2 SD
+2 SD
0.7295
0.8603
0.8098
0.7845
0.7781
0.7625
0.7785
0.7707
0.7632
0.7706
0.8529
0.9896
0.9738
0.9646
0.9517
0.9406
0.9305
0.9238
0.9162
5 of 10

Control Chart for April 2019 Chronic C. dubia Reference Toxicant
CV% 24
0.5
0.45
0.4
0.35
0,
0,25 -
0.2 -
0.15
Dates
04/03/18
05/01/18
06/05/18
06/19/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01 /08/ 19
01/22/19
01/22/19
01/29/19
01/29/19
02/05/19
03/05/19
04/02/19
04/02/19
Values
0,2819
0.2879
0.2093
0.2882
0.2935
0,2994
0.3091
0.2133
0.3355
0.2369
0.3662
0.1269
0.4433
0.2852
0.3669
0.2759
0.3074
0.2578
0.2880
0.4115
Mean
0,2849
0.2597
0.2668
0,2722
0.2767
0.2813
0.2728
0.2798
0.2755
0.2837
0.2707
0.2840
0.2840
0,2896
0,2887
0.2898
0.2880
0.2880
0.2942
Date
-1 SO
Analytical
0.2807
0.2159
0.2284
0.2368
0.2432
0,2484
0.2340
0.2379
0.2337
0.2356'
0.2062
0.2058
0.2090
0.2141
0.2158
0.2190
0.2189
0.2209.
0,2233
-2 SD
0.2764
0,1722
0.1899
0.2014
0.2096
0.2154
0.1951
0,1959
0.1919
0,1874
0.1417
0.1277
0.1339
0.1387
0,1428
0.1482
0.1499
0.1538
0.1523
+1 SD
0.2891
0.3035
0.3053
0,3075
0.3102
0.3143
0.3117
0.3217
0.3173
0.3319
0.3352
0.3621
0.3591
0.3650
0,3617
0.3606
0.3571
0.3552
0.3651
12065 Lebanon Rd
Mt. Juliet, TN 37122
(615) 773-754_{
[phone] Fax
April 2019
Reference Toxicant Test
+2 SD
D
Mean
SD
-2 SD
+2 SD
0.2934
0.3472
0.3437
0.3429
0.3438
0.3473
0,3506
0.3637
0.3591
0.3801
0.3997
0.4402
0.4342
0,4404
0.4346
0.4314
0.4262
0.4223
0.4361
6 of 10

Dates
05/16/18
06/19/18
07/03/18
07/26/18
08/02/18
09/05/18
09/27/18
09/27/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
02/06/19
03/06/19
04/03/19
Control Chart for April 2019 Acute Minnow Reference Toxicant
CV% = 17.2
Values
0.6817
0.8842
0.8196
0.6875
0.6657
1.2000
0.7387
0.7387
0.8196
0.8196
0,7715
0.6375
0.7000
0.8785
0.9415
0.9094
0.8485
0.6000
0.8801
0.9524
Mean
0.7830
0.7952
0,7683
0.7477
0,8231
0,8111
0.8020
0.8040
0.8055
0.8024
0.7887
0.7819
0.7888
0.7990
0.8059
0.8084
0.7968
0.8012
0.8087
Date
-1 SD
aceAnalytical
;, mill Center fur 7yut*rq R inrwvs lart
0.6398
0.6917
0.6681
0.6496
0.6187
0.6217
0.6249
0.6382
0,6491
0,6537
0.6391
0.6366
0.6468
0.6566
0.6656
0.6721
0.6558
0.6628
0.6699
-2 SD
0.4966
0.5883
0.5679
0.5515
0.4143
0.4324
0.4477
0.4724
0.4927
0.5050
0.4895
0.4912.
0.5048
0.5142
0.5253
0.5359
0.5148
0.5245
0.5310
+1 SD
0.9261
0.8986
0.8684
0,8459
1.0275
1.0004
0.9792
0.9698
0.9619
0.9512
0.9383
0.9272
0.9308
0.9413
0.9462
0.9446
0.9378
0.9395
0.9476
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
April 2019
Reference Toxicant Test
+2 SD
+1 SD
Mean
-1 SD
-2 SD
+2 SD
1.0693
1.0020
0.9686
0.9440
1.2320
1.1897
1,1563
1.1356
1.1183
1.0999
1.0879
1.0725
1.0727
1.0837
1,0865
1.0808
1.0788
1.0779
1.0864
7 of 10

Control Chart for April 2019 Chronic Reference Toxicant
CV/ a = 10
0.7
0.65
0.6
0.55
0,
0.4
0.4
0.35
0.3 .-
Dates
11/07/17
12/05/17
01/09/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01/08/19
01 /29/19
02/05/19
03/05/19
04/02/19
Values
0.4694
0.5379
0.4941
0.4800
0.4562
0.5069
0.4335
0.5210
0,4300
0.5491
0.4410
0.4705
0.4976
0.5790
0.6174
0.4553
0.4956
0.5462
0.5583
0.4570
0.5037
0.5005
0.4954
0.4875
0.4908
0.4826
0.4874
0.4810
0.4878
0.4836
0.4825
0.4836
0.4904
0.4989
0.4962
0.4961
0.4989
0.5021
0.4998_
Date
-1 SD
0.4552
0.4658
0.4652
0.4561
0.4616
0.4482
0.4528
0.4434
0.4464
0.4418
0.4425
0.4451
0.4455
0.4446
0.4426
0.4442
0,4472
0.4500
0.4481
-2 SD
0.4068
0.4311
0.4351
0.4247
0.4324
0,4139
0.4183
0.4059
0.4049
0.4000
0.4024
0.4066
0.4005
0.3903
0.3890
0.3924
0.3955
0.3979
0.3965_
+2 SO
+1 SD
Mean
-1 SO
-2 SD
+1 SD 1 +2 SD
12065 Lebanon Rd
Mt. Juliet, TN 3 7 `2 `
[phone]
[phone] Fax
Apra 2019
Reference Toxicant Test
0,5521
0.5352
0.5255
0.5189
0.5199
0.5169
0.5219
0.5186
0.5293
0.5253
0.5225
0.5222
0.5354
0.5532
0.5498
0.5480
0.5506
0.5541
0.5515
0.6005
0,5698
0.5556
0.5503
0.5491
0.5512
0.5565
0.5561
0.5707
0.5671
0.5625
0.5607
0.5803
0.6075
0.6034
0.5999
0.6024
0.6062
0.6031
8 of 10

Chain of Custody
Workorder: 92424508
Baioni
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: [e-mail]
Origin: NC
order
Pace National
12065Lebanon Rd
Mt Juliet, TN 37122
615-758-5858
PC
Te
NCOO46213
ults Requested y: 4/2 12019
g ¢i-A -C C )2rev. i } 24M r02009
rgr')t'r 1 of 1
Monday, April 08, 2 P'19 4:41:12 P`4

Armlytical
aCe Artaiyiiea$ - :tttYtt+
K1 Kinney Avenue, Suite
NC 280T`8
rnprxare I 'Return
ustoimw Sarnple lD
OUTFA
CHAIN -OF -CUSTODY Antytica
Chzafi-nf Costcs
vlile, NC
equest Document
A{..1tCka;UMFNT . Complr
Angela Baioni
9 CR kEracayAire ,, Ste. 100
Hunterswlifa, NC 28078
EntaEt Sra: angela.tradonlatr
County/City: Time Lone Collected;
PT MT Cr FT
y
'urnarnund pate Required,
5ame pay f 1 Nert paY K Yes ) No
Day 1 ) 4 Day) ) .5 pay
(t.x dite Crotm Apply)
id (51, , ©€i (01 W pa) PI A€r Aid), Tissue (Y51 Bioassay {L+, v
Comp / Collected (or
Niatrlx * Grab - Composite Start)
su t>r f eat arks 1 Si acaa8 C or,dttlons / P nhk Hazard
FALL 01Q - Collect a grab sample and ship ove
rt ttt arrive at late the following day, "'PI
°'pe of ece Used'
Packlm M terdal
sired by/Crmpany° (Signature] Moe/Time,
0
1, ihastes sU r ("y
L ther (0T
Comiprlsite End
Time
Re by/Company;
i U C LA*. AM(z Worisurd r/to
Mill. Lcsg.ln Number Here
ALL SHADED AREAS are for LAB USE ONLY
NT (a7,'a, is+rar,) : rzJ N/A
464 .Nan
t B Santp9e Terr laeraeure tnte,.
Tot p Slarr1 P °e[r e . Y ° NA
Ther€xt ldt
Cosaket 1 TentTa tiprsn eTralytaC
�ocsier 1 Therm Corr, Fart0 oC
Tate(. # CiaoSer1 Corrected Temp o
AcCtntsrfa: PA.CF Consrnents:
Ta+rplat,Clfg4 TrdA 11iarrk Received; Y NA
Pseio na PE;16 7 Ha +'4Re0H TSP O
M,4 Nancy McLain NrsnCcnfnrrtarace{ Page
T fT y T�i YES

ARATHO
APR 11 2019
CEN't i"ILFS
1"11R
April 8, 2019
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
MPLX Terminals tic
A subsidiary of Marathon Petrokrum Corporation
539 South Main Street
Findlay, OH 45840
Tel: 419,422.2121
RECEN'ElYNCDENRIDWR
VVQROS
MOOR e SV iLLE REGfONAL OFFICE
Sent via OverniRht Mail
Enclosed please find the March 2019 NPDES report, plus one copy, for the above -referenced
permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NPDES PERMIT" NO:: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mpla Terminals LLC
GRADE: PC-1
eDMR PERIOD: 03-201A (March 201A)
PERMIT VERSION: 4A}
CLASS: PC-1
ORC: D irs 1 Keith Thortig sc
ORC HAS CHANCED: No
VERSION: LO
PERMIT STATUS: Ac#i
COUNTY: Mecklenburg
ORC CERT NUMBER; 1005070
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
OS!!B .3273i
84
n.ay M10n0u 0.00I
i No Flow-ReusciRecycic; ENVWTHR w No Visitation Adverse Weather; NOFLOW iv No Flow; [3I7LII)AV i. No Visitation - Holiday

NPDES PERMIT NO.: NC0046213 PERMIT 'VERSION: 4,0
FACILITY NAME: Charlotte TermCLASS: PC-1
OWNER NAME Mph( Terminals LLC ORC: Darryl Keith Thompson
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD:03-2019 (March 2019) VERSION: 10
COMPLIANCE STATUSrmpllanI CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
SUBMISSION DATE: 04 /2 9
04 2019
ORC/Certifier Signa • e• Darryl Keith hompson E- ail:[e-mail] Phone #[phone] Date
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or t e environment.
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part ILE6 of
the NPDES permit.
0 4/04/2 019
Pc iltec/Subf ter Signature:*** Angela S Brown [e-mail] Phone #[phone] Date
Permittee Addres : 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of rny knowledge and belief, true,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAD NAME: Pace AnalyticalAnaIytiea1 Serviccs, LLC
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES: JQtnlfleri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenr.org/web/wq/swp/pshipdeWforms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period,
ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
,0506(b)(2XD).

ARA
March 21, 2019
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
RECEIVED
MAR 2 6 2019
CEN t m,aL FILES
DWR SECTION
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via overnight Mail
Enclosed please find the February 2019 NPDES report, plus one copy, for the above -referenced
permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NPDES PERMIT NO.: NC004621 a
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mpkx Terminals LLC
GRADE; PC.i
DMR PERIOD: Ci'2-2019 if**
PERMIT VFRSIONs4
CLASS: PC-1
PERMIT STATUS: Actit==c
COUNTY: Meeklenburr
ORC: Darryl Keith Thou p;n ORC CERT NUMBER: 11015070
ORC HAS CHANGE
VERSION: 1.0
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCI?LARGE NO.: 001 NO DISCHARGE*: NO
"" No Repo0inM Rcawn; ENFR(JSF' No Flow-ReuacfRccycic; ENVWTt
Advemi NOFI,OW w No Flow; HOLIDAY wNo ViairatIon • Holiday

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC'-1
eDMR PERi.OD: ()-2tt19 (1»ebn
COMPLIANCE STA
ORC/Certifier Signature: D
PERMIT VERSION:4.ii PERMIT STATUS: Active
CLASS: PC-1 COUNTY. Mecklenburg
ORC: Darryl Keith Thompson ORC CERT NUMBER: 1005070
ORC HAS CHANGED: No
VERSION: 1,0 STATUS: Processed
lONTACT PHONE #: [phone] SUBMISSION DATE: 03r15-'2019
03/07/2019
kthttmpson(ii?marathonpetrolcum.com Phone #:[phone]
this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the perniittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the permittcc becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part IhE.fi of
the NPDES permit.
P
03/15/20(9
* Angela S Brown E-Mail:asbrown*marathonpetroleum.com Phone #:[phone] Date
Permittee Address: 8035 Mount. Holly Rd Paw Creek NC 28130 Permit Expiration Date: 0613012020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted„ Based on my inquiry oldie person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete, I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME; Pace Analytical Sc
CERTIFIED LAB #:
PERSON(sl COLLECTING SAMPLES: J Qualfieri
PARAMETER CODES
Parameter Code assistance may be obtained. by calling the NPDES Unit (91.9) 807-6300 or by vi
n
ttp:lfportal,ncdenr.org/wcblwq wp/psrnpdes/forms.
FOOTNOTES
Use only units of measurement do ignated in the reporting facility's NPDES permit for reporting data,
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document vis
*** Signature of Permittee: If signed by other than the permittee, Iben delegation of the signatory authority must be on file with the state per 15A NC AC 2EI
.0506(b)(2XD),
equircd per 15A NCA.0 8G .0204.

March 21, 2019
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
Blanchard Terminal Company LLC
A subsidiary of Marathon PetroleumCorporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
RECEIVED
MAR 26 2019
CEN i r(HL FILES
DWR SECTION
RE: NPDES (DMR) Monthly Report
Blanchard Terminal Company LLC ("BTC")
Charlotte Terminal
NPDES Permit NC0021971
Sent via ©verniRht Mail
Enclosed please find the February 2019 NPDES reports for Outfalls 009 and 010, plus one copy,
for the above -referenced permit. Also included is the annual toxicity test.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)
NC DENR — Division of Water Resources
Water Sciences Section / Aquatic Toxicology Branch
1621 Mail Service Center
Raleigh, NC 27699-1623

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 02-2019 (February 2019)
2400 rusk
4
10
11
11
13
14
15
16
17
18
T9
20
21
22
23
PERMIT VERSION: 4,0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 2,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 009 NO DISCHARGE*: NO
2400 clock
50050
See Permit
Recorder
FLOW
mgd
0,188
0.172
0.233
50060
Monthly
Grob
C0530
Grab
CHLORINE T69Cone
< 2,5
34030
Quarterly
Grub
BENZENE
770151
Quarterly
ETHANOL
200
34371 TAESC
-Quarterly Arsntrally
Grab
ET'HYLBEN 11'11014AC
uyl pereen1
34606
Monthly
Grab
NAPTHALF.
ugd
00556
Monthly
Grab
O0L GREE
mg4
<5
25
26
17
28
0,205
Moo1bl0 Average THEE
Monthly Arrer50o» 0,1500
sally Mncimam:r
0.233
Bail Mloisnurta 0,001
0
0
0
0
0
100
100
0
••"w No Reporting Reason: ENFRUSE., No Flow-ReusetRceycle, ENVWTHR _ N3 Visitation-- Adverse Weather, NOFLO = No Flow; HOLIDAY -No Visitation- Holiday

NPDES PERMIT NO,: NC0021971 PERMIT VERSION: 4.0
FACILITY NAME: Charlotte Terminal CLASS: PCNC
OWNER NAME: Blanchard Terminal Company LLC ORC: Not Required
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 02-2019 (February 2019) VERSION: 2,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 009 NO DISCHARGE*: NO (Continue)
ate
Co,,, .sitt Sample Tune
'.,' 'I'ofaF Cam{+asd#e:'Cutle
a
q
34010
00070
81551
Quarterly
Monthly
Quarterly
Grab
Grab
Grab
'fnl.l"EN6
'fl'RBIIYfY
XY'1.r=nNE
2400 cluck
lln
Y/a(N
-
tall
nllt
ugtl
9
�
6
7
8
x, t
ii.5
< I
10
13
15
14
15
16
l7
18
19
20
21
11
23
24
25
I6
27
.
28
Monthly *0 0149et
21a11y 9l8368308:
Dolly Mlnlmnm:_
8.5
6.5
0
****'No Reporting Reason: ENERUSE = No How-Reuse/Recycle; ENVWTHR= No Visitation —Adverse. Weather; NOFLOW -^ No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0021971 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal CLASS: PCNC COUNTY: Mecklenburg
OWNER NAME: Blanchard Terminal Company LLC ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 02-2019 (February 2019) VERSION: 2,0
2400 clock
4
10
11
12
13
14
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 010 NO DISCHARGE*: NO
Bra
2440 clack
Hrs VAIN
50950
Sre Permit
Recorder
FLOW
mgd
0.01
50060 C0530
Monthly
Grab
CHLORINE: ASS. Cone
34030
Quarterly
Grub
RENzENE
ug/'I
<1
77044
quarterly.
Grab
ETHANOL
200
34371
quarterly
Grab
ETHVI.BEN
TAEOC
Annually
Grab
F FHD24AC
percent
y 100
34696
ly
Grab
NAPTHALE
ug/I
00556
Monthly
Grab
OIL-GHSE
mg/I
15
26
17
IP
10
20
21
0.359
22
'23
24
0.3722
25
26
27
20
Mouthlr* Average LIRA:
00outhly Averae..
Daily Moxlarnnrr
Daly al)nlmunH
0.568
0,3134
0.560
0,01 0.
0
0
100
100
r...NoReporting Reason; ENFRUSE=NoFlow-Reuac/Recycle; ENVWTHR- NoVisitation--.AdverseWeather; NOFLOW NoFlow; HOLIDAY=NoVisitation- Holiday

NPi ES PERMIT NO.: NC0021971 PERMIT VERSION: 4.0
CLASS: PCNC
OWNER NAME: Blanchard Terminal Company LLC ORC: Not Required
ORC HAS CHANGED: No
eDMR PERIOD: 02-2019 (February 2019) VERSION: 2M
FACILITY NAME: Charlotte Terminal
GRADE: PCNC
4
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 010 NO DISCHARGE*: NO (Continue)
2400 ektk
lira 2400 clock
11r
WHIN
34010
crab
00070
Monthly
"rtiRBIDfY
81531
Quatletly
Grab
XYLEI4E
ug'I
<1
10
13
14
15
16
17
I0
19
20
21
22
23
34
as
26
27
70
Monthly Average LOntt:
2
2
2
11
0
**** No Reporting Reason.: ENFRUSE _ No Flow-Reuse/Recycle; ENVWTF1R- No Visitation - Adverse Weather; N©FLOW =No Flow; HOLIDAY No Visitation - -Holiday

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 02-2019 (February 2019)
COMPLIANCE STATUS: Compliant
ORC/Certifie
Signature:
PERMIT VERSION: 4,0 PERMIT STATUS: Active
CLASS: PCNC COUNTY: Mecklenbur&
ORC: Not Required ORC CERT NUMBER; 995491
ORC HAS CHANGED: No
VERSION: 2.0 STATUS: Processed
CONTACT PHONE #: [phone] SUBMISSION DATE: 03/20/2019
n Risner E-Mail:errisne
a
03/20/2019
thonpetroleum.com Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken anda time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
Per ee!Sub
03/20/2019
Signature:*** Angela S Brown E-Mail:asbrownCamarathonpetroleum.eom Phone #:[phone] Date
Pcrmittee Address: 74t7`1 Old Mount Holly Rd Charlotte NC 28214 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and unprisonment for
knowing violations.
LAB NAME: Pace Analytical Services, LLC
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES. 3 Qualfieri
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Petmittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0021971 PERMIT VERSION: 4,0 PERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal CLASS: PCNC COUNTY: Mecklenburg
OWNER NAME: Blanchard. Tenninal Company LLC ORC: Not Required ORC CERT NUMBER: 995491
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 02-2019 (February 2019) VERSION: 2.0 STATUS: Processed
Outfall 009 - Effluent Comments:
Fire suppression water was not discharged, therefore monitoring was not required for TRC in accordance with footnote 5 in the permit.
The analytical report for Acute Toxicity (Parameter Code FTI-ID24AC) is beta subntitted with the hardcopy DMR.

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 02-2019 (February 2019)
Outfall 010 - Effluent Comments:
PERMIT VERSION: 4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 2,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
Fire suppression water was not discharged, therefore monitoring was not required for TRC in accordance with footnote 5 in the permit.
The analytaca1 report for Acute Toxicity (Parameter Code FTHD24AC) is being submitted with the hardcopy DMR.

Effluent Toxicity Report Form- Chronic Pass/Fail and Acute LC50 Date 2/22/201.9
Facil
#3Sax91* Y V111 - Hlancnarn
NPDES#NC 002
Laboratory Performing Test Pace Nat iona1
x
971
Signature of Operator in Responsible Ch
1+4
Signature of Laborai©ry Supervisor
Pipe #
Corn
y Meck
enburq
Comments
pace National 1L; L1068497-01
I
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10
# Young Produced
Adult (L )ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
1st sample
Control
D.O.
Treatment 2
2
1s
e t e
n a n
d r d
1st sample
4
6 7
2nd sample
s
t e
a n
r d
2nd sample
LC50/Acute Toxicity Test
(Mortality expressed as %, comb
© a/0
0
12,�
0
°1©
2 5 °10
0
50
0
n
5 0 %
0
eplicates)
100%
%
0
Environmental Sciences Branch
Div, of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
11 12 Chronic Test Results
Calculated t
10 11 12
crptete,Ttis For E
Tabular t
• Reduction
y
Control
Treatment 2
Control CV
• control organisms
producing 3rd brood
Avg.Reprod.
Control
Treatment 2
PASS FA
Check One
Test tartDat1
9
Collection (Start) Date (not applicable)
Sample 1 2/ 8 t 19 Sample 2 / /
°!o
°!0
Hardness(mgli;
Spec,Cond.(pmhos
Chlorine(mgll
Sample temp. at receip
Concentration
Mortality
LC50= > 100 %
95% Confidence Limits
Method of Determination
Moving Average El Probit 0
Spearman Karber 0 Other none neeed
Organism Tested Pimephales promelas
Duration (hrs)24 hrs
DWQform AT-1 (3/87) rev. 11/95
pH
Note: Please
Complete This
Section Also
start/end
Control
High
Conc.
D.O.
1 of 11

iceAnaIvticaI
National Cernen for ni,nfing ru n.Natioo
Pace - Huntersville - Blanchard Terminal -
Client:
Outfall 009
NPDES #: NC0021971
Test Start Date:
Temperature (QC) Pimephales promelas (fathead minnow)
Control
12.5
25
50
75
100
Date:
Time: Analyst:
t
Day (initiation)
,Q5
0
') 44.
Date: 2,
Time: Analyst:
Day 2 (morning)
L\y't( C
1 v..,
(., °C
c)c
oC
o
Time:,, Analyst:
Day 2 (final)
‘1, °C
Measurement taken directly in test chamber
S> °C
°C
Thermometer Serial Number: 18050064
Control Water Carboy Used:
Outfall
009
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH/Temp/mV/ISE Meter
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Water Bath: Lindberg/Blue, Model WB1140A-1 (serial #S01M-580360-SM)
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chamber: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c VWR Traceable Dual -Range Light Meter- Model 62344-944 (SIN 181399747)
Photoperiod: 16 hours light, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific Isotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Shain W. Schmitt (SWS); Brandon Etheridge (BE); Amy Eggleston (AME);
Adam Macomber (AM); Melissa Mathis (MM); Cody Medley (CM); Clarissa Moore (CGM); Nadiar Yakob (NY)
Jon Berry (JB); Matthew Lockhart (MIL); Brittnie Boyd (BB); Joel Soto (JSV)
2 of 11

Thermo Graph for
do
ch Name Intv1. Sample Cur.A Cur.13 A<_y
1 Ch1 2min. 8000
2 Ch2 2min. 8000
Ch1 2rzin. 81800
9 h? 2min. 8000
Cur.A Date : 01/24/2019 18:18'53
Cur,B Date : 02/12/2019 7:24'08
diff. A-6 : 18 13.05'15.000
h Low Avg„ Unit
4 24.1 24.9 °C
25.5 24.1 24.9 °C
25„6 24.0 24.9 °C
25.6 24.0 24.8 °C
Data Range 01/24/2019 18:18'53-02/12/2019 3:24'08
Calc.Range 01/24/2019 23:31'50-02/12/2019 2:11'11

NORTH CAROLINA - ACUTE TOXICITY TEST DATA SHEET - Pimephales promelas (fathead minnow)
Client Pace - Huntersville - Blanchard Terminal - Outfall 009
Begin 3vIS -11-1°1 Time
End -iOtCj Time
Effluent in
Percent (%)
C L2
(mg/L) Or% DMW
< 0.2 CONTROL
12.5
25
50
75
CL2
(mg/L) 1 00
0,00
Checked By:
Replicate # OF LIVE Minnows
Position 0 hrs 24 hrs
A: 10
B: 10
A: 10
B: 10
10
B: 10
10
10
10
BHE 10
10
10
Biologist: ,"et;
Time 12
IL.
a)
0)
ca>
En
E.?
16
(4 CD
C-c
(/)
_c
E
c
4= • 0)
0• 0)
a) Et2
O 0)
a)
: o
*end test +/- 1 hr
from start time
pH (std, units)
0 hrs final
initial
71 S
initial
initial
75
nitial
niti
init
7
Initial F..R9?t. dings By:
ftf‘j,
NPDES NC0021971
Test Duration; 24 hours ESC Sample #:
Dilution Water: 10% DMW tdA9ci1
ace
Minnow final
0,,
Minnow final
Minnow final
Minnow final
Minnow final
i.
,
I
Dissolved oxygen (mg/L)
0 hrs
initial
initial
CO
initial
initial
Conductivity
final (umhoslcm)
Minnow final
Minnow final
Minnow final
Minnow final
nnow
initial
initial
initial
initial
initial Minnow final nUaI
Final Readings By: smt •
P „') '
Data divided by a slash mark ( / ) indicates that a duplicate was run on that parameter. Temperature of water (minnow batch) at time of test initia ion:
Minnows were 5 days old at test initiation and taken from ESC Lot # 0 '.3, OL-1 1,9, i-k . Minnows were last fed / 9 / t d @ (rt : j prior to the test.
0% Effiuertt
Alkalinity
-Pt
0
Control
LACHAT
L r'S
mg/L
100% Effluent
LACHAT
mg/L.
(Preliminary) Hardness
Analyst: T5
Date: 1115/19
Time: i33t
Contro
analyzed prior to
test initiation by
Wet Lab using:
LACHAT
Hardness
Conductivity
(umhos/cm)
Final
Final
ic7
Final
Final
Final
analyzed in Wet Lab
via LACHAT

Control Chart for Acute C.dubia Reference Toxicant January 2019
CV% = 23.3
1.07 •
0.87
0.67
0.47
0.27
Dates
12/06/17
01/03/18
02/07/18
03/07/18
04/04/18
05/02/18
06/19/18
07/03/18
08/02/18
09/05/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
01 /23/19
Values
0.6830
0,3693
0.7071
0.6429
0.4910
0.6156
0.7368
0,5835
0.6156
0.6547
0,5535
0.7040
0.6373
0.5391
0,4531
0.8801
1.0710
0,5946
0,6830
0.5840
0.5262
0.5865
0.6006
0,5787
0,5848
0,6065
0.6037
0,6050
0,6100
0.6048
0.6131
0.6149
0.6095
0.5991
0.6167
0.6434
0.6407
0.6429
0.6400
date
-1 SO
ace Analyticar
t"v,: Ta t,;f,^+,C r+•r�tx.? "; rE
0.3043
0.3980
0.4441
0.4346
0,4551
0.4749
0.4815
0.4907
0,5010
0.5001
0,5092
0.5153
0.5116
0,4965
0,4952
0.4822
0,4839
0.4902
0.4908
-2 SD
0.0825
0.2096
0.2877
0.2905
0,3253
0,3433
0.3594
0.3763
0.3921
0.3954
0.4053
0.4156
0,4137
0,3939
0.3737
0.3210
0.3271
0.3375
0.3416
+1 SD
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
(615) 75,i-5859 Fax
January 2019
Reference Toxicant Test
0.7480
0.7749
0.7570
0.7227
0.7146
0.7382
0,7258
0.7193
0.7189
0.7095
0.7170
0.7146
0.7074
0.7017
0,7382
0.8046
0.7975
0.7956
0,7892
+2 SD
+1 SD
Ntean
-1 SD
-2 SD
+2 SD
0,9698
0.9634
0,9135
0,8668
0.8443
0.8698
0.8479
0,8336
0.8278
0.8143
0.8208
0.8143
0,8053
0.8043
0.8597
0,9658
0.9543
0.9483
0.9384
5of11

IC25 (Reproduction) KCI
Dates
Control Chart for January 2019 Chronic C. dubia Reference Toxicant
0.45
0.4
0.35
0,3
0.2
0.2
0,15
0,
12/05/17
01/10/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
06/19/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01/08/19
01/22/19
01/22/19
01/29/19
01/29/19
Values
0.2650
0.2944
0,3203
0.2956
0.2819
0,2879
0.2093
0.2882
0,2935
0.2994
0,3091
0.2133
0.3355
0,2369
0,3662
0,1269
0.4433
0.2852
0.3669
0,2759
Mean
0.2797
0,2932
0.2938
0.2914
0,2909
0, 2792.
0.2803
0,2818
0.2836
0,2859
0.2798
0.2841
0.2807
0.2864
0,2765
0,2863
0,2862
0,2905
0.2897
Date
0.2589
0.2656
0.2712
0.2711
0.2726
0.2442
0,2477
0,2510
0.2540
0.2568
0.2451
0.2474
0.2433
0.2441
0.2194
0.2178
0.2198
0.2233
0.2243
-2 SD
0.2381
0.2379
0.2486
0,2508
0.2544
0.2092
0,2152
0,2202
0,2244
0,2277
0.2103
0.2107
0,2059
0.2019
0,1623
0.1493
0,1533
0.1561
0,1588
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
January 2019
Reference Toxicant Test
+1 SD
0,3005
0,3209
0,3164
0,3117
0.3091
0,3142
0,3129
0.3126
0.3131
0.3150
0.3146
0,3208
0,3182
0.3287
0,3336
0,3548
0.3527
0.3577`
0.3552
2 D
SD
n
1 SD
SD
+2 SD
0.3213
0.3486
0.3391
0,3320
0.3273
0,3492
0.3455
0.3434
0.3427
0.3440
0,3493
0.3575
0.3556
0,3710
0,3906
0.4233
0.4191
0.4248
0,4207
6 of 11

Control Chart for Acute Minnow Reference Toxicant January 2019
CV% = 16.4
1,3
1.2
1.1
0.9
0.8
0.7
0.6
0,5
0.4 "
Dates
04/05/18
04/11/18
05/02/18
05/16/18
06/19/18
07/03/18
07/26/18
08/02/18
09/05/18
09/27/18
09/27/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
Values
0.6892
0.6892
0.7647
0,6817
0.8842
0.8196
0.6875
0.6657
1.2000
0.7387
0.7387
0.8196
0.8196
0.7715
0.6375
0.7000
0.8785
0,9415
0.9094
0.8485
Mean
0.6892
0,7144
0,7062
0,7418
0.7548
0.7452
0.7352
0.7869
0,7821
0.7781
0.7816
0.7845
0.7836
0.7738
0.7692
0,7756
0.7849
0.7914
0,7943
aceAnalytical
..
Date
-1 SD
0,6892
0,6708
0,6670
0.6553
0.6711
0.6647
0.6556
0-6150
0,6193
0.6231
0.6333
0,6422
0.6468
0,6367
0.6355
0.6435
0.6508
0.6580
0.6638
-2 SD
0,6892
0,6272
0,6279
0,5687
0.5875
0.5842
0.5760
0.4431
0,4565
0.4681
0.4851
0.4998
0.5100
0.4996
0,5017
0.5113
0.5167
0.5247
0,5334
12065 Lebanx n ;
Mt. Juliet, TN 3712.
[phone]
[phone] Fax
January 2019
Reference Toxicant Test
+1 SD
0.6892
0.7580
0.7454
0.8283
0.8384
0.8256
0.8149
0.9588
0.9448
0.9331
0.9298
0,9268
0.9204
0.9109
0.9030
0.9078
0.9189
0.9248
0.9247
+2 SD
+1 SO
Mean
-1 SD
-2 SD
2 5D
0.6892
0.8015
0.7845
0.9149
0.9221
0,9061
0.8945
1,1307
1.1076
1,0881
1.0781
1.0692
1.0572
1.0480
1.0367
1.0400
1.0530
1.0582
1.0552
7 of 11

Control Chartfor January 2019 Chronic Minnow Reference Toxicant
CV% = 1 1
0.75
0.7
0.65
0.55
0.5
0,45
0.4 -
0.35
0.3
Dates
09/12/17
10/10/17
10/10/17
11/07/17
12/05/17
01/09/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01/08/19
01 /29/ 19
Values
0.5547
0.5459
0,6094
0.4694
0.5379
0.4941
0.4800
0.4562
0.5069
0.4335
0.5210
0.4300
0.5491
0,4410
0.4705
0.4976
0.5790
0.6174
0.4553
0.4956
n
0.5503
0.5700
0.5449
0,5435
0,5352
0.5273
0.5185
0.5172
0.5088
0,5099
0.5033
0,5068
0,5021
0.5000
0,4998
0.5045
0.5108
0.5078
0.5072
ace,nalyfal
n1 ex,.ti-��;r t;u.,>zE4t f'a.xr 7aai:a+r,
Date
0,5441
0.5356
0,4872
0.4935
0.4862
0.4779
0.4663
0,4682
0.4556
0.4593
0.4498
0.4540,
0.4484
0.4476
0.4492
0.4519
0.4532
0.4505
0.4513
-2SD
0.5379
0.5012
0.4296
0.4435
0.4371
0.4285
0.4141
0.4192
0.4024
0,4087
0.3963
0.4012
0.3948
0,3953
0.3987
0.3993
0.3956
0.3931
0.3954
+1 SD
12065 Lebanon Rd
Nit, Juliet, TN 37122
[phone]
[phone] Fax
January 2019
Reference Toxicant Test
0.5565
0,6044
0,6025
0,5935
0.5843
0.5767
0.5706
0,5661
0.5620
0.5605
0.5567
0.5595
0.5557
0.5523
0.5504
0.5571
0.5683
0.5652
0.5631
2 SD
+1 SD
lean
SD
-2 SD
+2SD
0,5627
0.6388
0.6601
0,6434
0.6333
0.6261
0.6228
0.6151
0.6152
0.6111
0.6102
0.6123
0.6094
0.6047
0.6010
0,6097
0.6259
0.6226
0.6190
8 of 11

Work()
Raf,toi d» w1 To
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0 KinceyP e Sute;m
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2W277 q2
Transfers
T East NC4 21971
:12417115D01
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ResUlts Requewted By: &le2019
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CHA4N£ �UaTQDY Analytcai e$t Document
vino, NC
Ainge,.ta xr(t
N unters'vttk», NC UO7
'01.1ri ALL 009 VON
vib t n i i ip overnight t.D arri
ce National Lab the following day, **
TSP

Chief: C
'Coo i<visciivcsI/Or,,ineci Orr
flcept Check List
COC Seaf Present Intact?
COC Si,ened / Acc rt
Booies orrive intact?
Sufficient volume sent?
'If Appficable
VOA Zeici h ea d spa c
Pace Analytical National Center for Testirl
Cooler Receipt For
s-
-
t tut
nnovation
No
Preservation Correct / Checki?ci

E uen Toxicity Repart Form- Chronic Pas Fail and Acute LC50 Date 2/22/2019
Pacei.n
Facili ....1-1:...:111111111!111111111111%11iigift1t1:111!1!.1111111111111111i1..11111111.111:..1"..:1
boratory Pe
X
n
NPDES#NC 0 02 1 971
ing Test Pace National.
Signature of Operaor in Responsible Char
x
3 .
ture of Labobry Supervisor
Pipe #
County Mecklenburg
Comments
Lace .Natioqa. ID; L10684-01
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia ChroniQPas&Eajl Reproduction Toxicity Test
4 5 6 7 8 9 10
CONTROL ORGANISMS
# Young Produced
Adult (L )ive (0 )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
e
n
d
1st sample
Control
D.O.
Treatment 2
2
23 4 5 6 7
2nd sample
s s
t e t e
a n a n
r d r d
t t
1st sample 2nd sample
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates)
%
0
12.
0
0
2 5
5 0
0
°A
5 0
0
°
100'
0
%
0
Environmental Sciences Branch
Div. of Water Quality
N,C, DENR
1621 Mail Service Center
Raleigh, No!thCarolina 27699-1621
11 12 Chronic Test Results
Calculated t
10 11 12
Tabular t
% Reduction
%Mortality
Control
Treatment 2
Control CV
%cooboloroarilsols
modudriOrdbrood
Cornp1ete This For Either Test
Sample Type/Duration
Sample 1
Sample 2
A
Avg,Rppr9d.
Control
Treatment 2
PASS FA
Check One
Test Start Date
2 9 .9
(not applicable)
9 Sample 2 / /
Duration
Hardness(mg/1
Spec.Cond.(urrhos
Chlorine(mg/I
Sample temp. at receip
Concentration
Mortality
LC50= > 100 %
95% Confidence Limits
%-
Method of Determination
Moving Average Probit
Spearman Karber E Other noie neeed
Organism Tested Pimephales pro
s
Duration (hrs) 24 hrs
DWQ form AT -I (3/87) rev, 1 1/95
end
pH
*gawp
Wite4
Note: Please
Complete This
Section Also
start/end
High
Conc.
D.O.
1 of 11

race Analytical
National Conte, tor Tostinp & innovation
Pace - Huntersville - Blanchard Terminal -
Client:
Outfall 010
NPDES #: NC0021971
Test Start Date:
Temperature (uC) Pimephales promelas (fathead minn
—Date: 2„—
Control
12.5
25
50
75
100
Date: •41 -
Time: Analyst;
Day 1 (initiation)
c5 3
°c
oc
) 5 3
Time: Analyst:
Day 2(morning)
I °C
06
°c
°c
°c
°
Ti e: Analyst:
Day 2 (final)
Measurement taken directly in test chamber
°C
°c
Lab Sample #:
Thermometer Serial Number: 18050064
Control Water Carboy Used:
3-7 I
Outfall
010
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH/Temp/mV/ISE Meter
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Water Bath: Lindberg/Blue, Model WB1140A-1 (serial #S01M-580360-SM)
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chamber: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c - VWR Traceable Dual -Range Light Meter- Model 62344-944 (SIN 181399747)
Photoperiod: 16 hours light, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific lsotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Shain W. Schmitt (SWS); Brandon Etheridge (BE); Amy Eggleston (AME);
Adam Macomber (AM); Melissa Mathis (MM); Cody Medley (CM); Clarissa Moore (CGM); Nadiar Yakob (NY)
Jon Berry (JB); Matthew Lockhart (MIL); Brittnie Boyd (BB); Joel Soto (JSV)
2 of 11

aph for Windows Q2f1?d2 19 8:40'05
1 --C h l
2----Ch 2
3 Chl
4 Ch2
Cur-4 Date 01/24/2019 18:1.8'53
Cur.B Date : 02/12/2019 7:24'08
dir'E, A-B : 19 13:05'15.000
2min.
2min,
2m1n.
8000
8000
8000
8000
High Low Avg, Unit
25.4 24.1 24.9 °C
25.5 24,1 24.9 °C
25.6 24.0 24.9 °C
25.6 24,0 24,8 °C
Data Range 01/24/2019 18:18'53-02/12/2019 7:24'08
Ca1c,Ftange 01/24/2019 23:31'50-02/12/2019 2:11'11

NORTH
client Pace - Huntersville -
Begin
End
CL2
(mg/L)
< 0.2
CL2
(mgIL)
Effluent in
Percent (%)
10% DMW
CONTROL
12.5
25
50
75
100
Checked By:
Replicate
Position
B:
A: C4
B:
B:
CAROLINA - ACUTE
Blanchard Terminal
Biologist:
lime
NOS
Time
Time
# OF LIVE Minnows
0 hrs 24 hrs
10
10
10
10
10
10
10
10
10
10
10
10
TOXICITY TEST DATA SHEET - Punephales promelas (fathead minnow)
- Outfall 010 NPDES #: NC0021971
Test Duration: 24 hours
Dilution Water: 10% DMW
mperatures have been recorded on
heck here to confirm
*end test +/- 1 hr
from start time
pH
0 hrs
initial
initial
718
initial
7 (
initial
0
initial
Initial Readings By:
P'1L-
units)
finai
Minnow fin
Minnow final
Minnow final
Minnow final
1
Minnow final
Minnow final
ace Analytical
ESC Sample #:
L
Dissolved Oxygen (mg/L)
0 hrs
initia
0
initial
initial
initial
initial
0
final
Minnow fin
7
Minnow final
Minnow final
Minnow final
Minnow
Minnow final
7
Final Readings By:
Conductivity
(umhos/cm)
initial
initial
initial
initial
06,c
initial
?-14-1„s-
1.43
Data divided by a slash mark ( / ) indicates that a duplicate was run on that parameter. Temperature of water (minnow batch) at time of test initiation:
@ 45 prior to the test.
100% Effluent
Minnows were
Alkalinity
0
Control
days old at test initiation and taken from ESC Lot # 0,:kot-.1 C k ti Minnows were last fed
100% Effluent
LACHAT
9 0
mglL
LACHAT
10
g
mg/l
(Preliminary) Hardness
Analyst: __9S
Date:
Time: ja„5 8
Con
nalyzed prior to
est initiation by
t Lab using:
LACHAT
Hardne
9'1
Conductivity
(L-MOS/CM)
Final
Final
Final
Final
1„i 5
Final
analyzed in Wet Lab
via LACHAT

Control Chart for Acute C.dubia Reference Toxicant January 2019
CV% 23.3
1.07
0.87
J
0.67
J 0.47 -
Dates
12/06/17
01/03/18
02/07/18
03/07/18
04/04/18
05/02/18
06/19/18
07/03/18
08/02/18
09/05/18
10110/18
11/01/18_
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
01/23/19
Values
0.6830
0.3693
0.7071
0,6429
0,4910
0.6156
0.7368
0.5835
0.6156
0,6547
0,5535
0.7040
0.6373
0.5391
0.4531
0.8801
1.0710
0,5946
0.6830
0.5840
n
0.5262
0.5865
0.6006
0.5787
0.5848
0.6065
0.6037
0.6050
0,6100
0.6048
0.6131
0.6149
0.6095
0.5991
0.6167
0,6434
0.6407
0.6429
0.6400
date
-1 SD
0.3043
0.3980
0,4441
0.4346
0.4551
0.4749
0.4815
0.4907
0.5010
0.5001
0.5092
0.5153
0.5116
0.4965
0.4952
0.4822
0.4839
0.4902
0.4908
-2 SD
0.0825
0,2096
0.2877
0.2905
0.3253
0.3433
0.3594
0.3763
0.3921
0.3954
0,4053
0.4156
0.4137
0.3939
0.3737
0.3210
0.3271
0.3375
0,3416
ehanan Rd
TN 37122
[phone]
[phone] Fax
January 2019
Reference Toxicant Test
SD
0.7480
0.7749
0.7570
0,7227
0.7146
0.7382
0.7258
0.7193
0.7189
0.7095
0.7170
0.7146
0.7074
0,7017
0.7382
0.8046
0.7975
0.7956
0.7892_
+2 SO
+1 SD
Mean
-1 5D
-2 SD
+2
0.9698
0.9634
0.9135
0.8668
0.8443
0.8698
0,8479
0.8336
0,8278
0.8143
0,8208
0.8143
0,8053
0.8043
0,8597
0.9658
0,9543
0.9483,
0.9384
5of11

Control Chart for January 2019 Chronic C. dubia Reference Toxicant
0.45
0.4
0,35
0.3
0.25
0.2
0.15
0.1
Dates
12/05/17
01/10/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
06/19/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01/08/19
01/22/19
01/22/19
01/29/19
01/29/19
Values
0.2650
0,2944
0.3203
0.2956
0.2819
0.2879
0,2093
0.2882
0.2935
0.2994
0.3091
0,2133
0.3355
0,2369
0,3662
0.1269
0.4433
0.2852
0.3669
0,2759_
0.2797
0.2932
0.2938
0.2914
0.2909
0.2792
0.2803
0,2818
0.2836
0.2859
0,2798
0,2841
0.2807
0.2864
0.2765
0.2863
0,2862
0.2905
0 ,2897_
. ace Analyticall'
N;tfiorr411C4.rlier ra.s.r'r9
Date
-1 SO
0.2589
0.2656
0.2712
0.2711
0,2726
0.2442
0.2477
0.2510
0.2540
0.2568
0.2451
0.2474
0.2433
0.2441
0.2194
0.2178
0.2198
0.2233
0.2243
-2 SD
0.2381
0.2379
0.2486
0.2508
0.2544
0.2092
0.2152
0.2202
0.2244
0.2277
0.2103
0,2107
0,2059
0.2019
0.1623
0,1493
0.1533
0.1561
0.1588
12065 Lebanon Rd
Nit. ',Juliet, TN 37122
[phone]
[phone] Fax
January 2019
Reference Toxicant Test
+1 SO
0.3005
0,3209
0.3164
0,3117
0.3091
0,3142
0,3129
0 3126
0.3131
0.3150
0,3146
0.3208
0,3182
0.3287
0,3336
0.3548
0,3527
0.3577
0,3552
+2 SO
0,3213
0.3486
0,3391
0.3320
0,3273
0.3492
0.3455
0.3434
0.3427
0.3440
0.3493
0.3575
0.3556
0.3710
0.3906
0.4233
0.4191
0.4248
0.4207
6 of 11

Dates
04/05/18'
04/11/18
05/02/ 18
05/16/18
06/19/18
07/03/18
07/26/18
08/02/18
09/05/18
09/27/18
09/27/18
10/10/18
11/01/18
11/01/18
12/05/18
12/05/18
01/03/19
01/03/19
01/16/19
01/23/19
Control Chart for Acute Minnow Reference Toxicant January 2019
CV% = 16.4
Values
0.6892
0.6892
0.7647
0,6817
0.8842
0.8196
0.6875
0.6657
1.2000
0.7387
0.7387
0.8196
0.8196
0.7715
0.6375
0.7000
0.8785
0.9415
0.9094
0.8485
Mean
0.6892
0.7144
0.7062
0,7418
0,7548
0.7452
0,7352
0.7869
0.7821
0.7781
0.7816
0.7845
0,7836
0,7738
0,7692
0.7756
0.7849
0.7914
0,7943
Analy /cal =
Date
0.6892
0.6708
0,6670
0.6553
0.6711
0.6647
0.6556
0.6150
0.6193
0.6231
0.6333
0,6422
0.6468
0.6367
0.6355
0.6435
0.6508
0.6580
0,6638
•2 SD
0.6892
0.6272
0.6279
0.5687
0,5875
0,5842
0.5760
0,4431
0.4565
0.4681
0,4851
0,4998
0.5100
0,4996
0.5017
0.5113
0.5167
0,5247
0,5334
12065 Lebanon
Mt. Juliet. TN 37122
[phone]
[phone] Fax
January 2019
Reference Toxicant Test
+1 SD
0,6892
0,7580
0.7454
0.8283
0.8384
0.8256
0.8149
0.9588
0.9448
0.9331
0,9298
0.9268
0.9204
0,9109
0.9030
0.9078
0,9189
0.9248
0,9247
+2 SD
+1 SD
Mean
-1 SD
-2 SD
+2 SD
0.6892
0.8015
0.7845
0.9149
0.9221
0.9061
0.8945
1,1307
1.1076
1.0881
1.0781
1.0692
1.0572
1.0480
1.0367
1,0400
1.0530
1.0582
1.0552
7 of 11

Control Chartfor January 2019 Chronic Minnow Reference Toxicant
CV%
0.75
0,7
0.65
0.6
0.5.-
0.5
0,4
0,4
0,35 -
0,3
Dates
09/12/17
10/10/17
10/10/17
11/07/17
12/05/17
01/09/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
07/03/18
08/07/18
09/05/18
10/02/18
11/06/18
12/04/18
12/04/18
01 /08/ 19
01/29/19
Values
0.5547
0,5459
0.6094
0.4694
0,5379
0.4941
0,4800
0,4562
0.5069
0.4335
0,5210
0.4300
0.5491
0.4410
0.4705
0.4976
0,5790
0.6174
0,4553
0,4956
Mean
0.5503
0,5700
0.5449
0,5435
0.5352
0.5273
0,5185
0.5172
0.5088
0.5099
0.5033
0.5068
0.5021
0.5000
0.4998
0.5045
0.5108
0,5078
0.5072
'ln yt/ cf,
Date
-1 SO
0.5441
0.5356
0,4872
0.4935
0.4862
0.4779
0.4663
0.4682
0.4556
0.4593
0.4498
0,4540
0,4484
0,4476
0,4492
0.4519
0,4532
0.4505
0.4513
-2 SD
0.5379
0.5012
0.4296
0,4435
0.4371
0,4285
0.4141
'0.4192
0.4024
0.4087
0.3963
0.4012
0,3948
0.3953
0.3987
0,3993
0,3956
0.3931
0.3954
+1 SD
12065 Lebanon Rd
Nit. Juliet, TN 17122
[phone]
[phone].Fax
January 2019
Reference Toxicant Test
0,5565
0.6044
0.6025
0.5935
0.5843
0.5767
0,5706
0.5661
0.5620
0.5605
0.5567
0,5595
0.5557
0.5523
0.5504
0.5571
0,5683
0.5652
0.5631
+2 SD
D
Mean
-1 SD
-2 SD
+2 SD
0.5627
0,6388
0.6601
0.6434
0.6333
0.6261
0.6228
0.6151
0,6152
0,6111
0,6102
0.6123
0,6094
0.6047
0.6010
0,6097
0,6259
0,6226
0.6190
8©f11

C hJ
Ana
ody
7117
sx . NC -
Relc 4 e
rTempemmm o.R
NC0021 1
;
'Ciaternme \© 2d
toclv
Results Requested By: .
Y or2 \ Receiv § on Ice

m,p-m
» m;
y6AC6 « w !
adgcl-

N one Cantu for
Coc)I F For

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 01-2019 (January 2019)
oroportse Sample Time
PERMIT VERSION: 4.0
R-
CLASS: PC-1
FER 22 Z019
ORC: Darryl Keith Thompson
ORC HAS CHANGED: NoC,EIN ikJ4L FILES
LAN R SECTION
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
MiCEIVEDINCDENRIVAR
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*; Q
monp sv K) OF F IC E
09
Operator AVtiVid Time
Operator Time On Site
2400 cloak firs 2400 duck Has
4
6
9
60
11
12
13
14
15
16
17
18
20
21
22
24
25
26
27
28
29
30
31
WHIN
Monthly Average
Monthly Average,
Daily Maximum,
Minitmant
50050
Sec Permit
Recorder
FLOW
mgd
0,001
0,431
0.001
0.255
0.172
0.431
0.00 I
C0530
Monthly
Grub
TSS Cone
< 4.5
5.6
30
2 N
5,6
0
34030
Monthly
Grab
BENZENE
ug/1
< 1
0
0
34371
Quarterly
Grab
ETHVLBEN
tig/1
< 1
< I
141269) 22417
Quarterly Quarterly
Grab Grab
FT111114AC MTBE
remit ugil
09I
> 100 2.6
10f1 1,3
100 2.6
100
34696 00.556
Quarterly Monthly
Grab Grab
NAPTIIALE 011,0RSE
utill mg/1
< < 4.8
< I < 4,8
**** No Reporting Reason: .ENFRUSE = No Flow-Rouse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOELOW -= No FlowHOLIDAY = No Visitation — Holiday
32730
Monthly
Grab
PII
< 0.01
< 0,01

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 01-2019 (January 2019)
29
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Dan-yl Keith Thompson
ORC HAS CHANGED: No
VERSION: I 0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
5
490d9ek 1129 140000ek Nrs
Monthly Average Limit,.
0athly Aarragm
Daily Maximum
Daily 144itimaaa
34010
Quarterly
Grub
.VOLUENE
00070
(Monthly
ta
TURRIDTY
ntu
7.3
7.75
.2
7.
PI 51
Quarterly
Grab
KYLENE:
ug/I
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY - No Visitation — Holiday

NP
FACILITY NAME: Charloin: Terminal
OWNER NAME: btplx Ter:ninats LCC
GRADE: PC-1
eDMR PERIOD: 01-2019 (, anuary 2019)
COMPLIANC
0462!.
PERMIT VERSION: 4,0 PERMIT STATUS: Active
CLASS: PC-1 COUNTY: Mecklenbur&
ORC: Darryl Keith Thompson ORC CERT NUMBER; 1C
ORC HAS CHANGED: No
VERSION: 1,0 STATUS: Processed
CONTACT PHONE #: [phone]
ORC/Certifier Signet , : Darryl Keith Tliaampson E-I4fail:dkthompson(ii
By this signatt
SUBMISSION DATE: 02115 2019
02;06,2019
athonpetrolcum,com Phone #:980-613 t1495 Date
hat this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the enaironnient.
Any information shall be arovided orally within 24 hours from the time the permittee became aware of the circumstances, A written submisssirn shall ,ilso be
provided within 5 days of the time the permittee becomes aware of the circumstances.
lithe facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to he made as required by part li E,6 of
the NPDES permit.
Permitteelub
Permittee Address:
02ti
9
Signature:*** Angela S Brown E-1,stall:asbrown(marathonpetroleum.com Phone #;419-421-2629 Date
Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date; 06130/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordances<
to assure that qualified pe -sonnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons
:nt deigned
ale:1 he
system, or those persons cirectly responsible for gathering the information, the information submitted is, to the best of my knowledge and be ief, true,
accurate, and complete, I tm aware that there are significant penalties for submitting false information, including the possibility of fines and rmprisonrrsent for
knowing violations.
LAB NAME: Pace Analytic d Services, LLC
CERTIFIED
PERSON ) ct LLECrIN , SAMPLES:1 rluaUiar'l
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code as zstartcW: may be obtained by calling the NPDES Unit [phone] or by v
n
dear,org'webr"wglswpip,;?npdesrfornts.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
* No Flow, Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters <tit the'DMR
for entire monitoring peri.rd.
** ORC on Site?: ORC must visit facility and document visitati€m of facility as required per I5A NCAC 8G ,0204,
*** Signature of Permitte.; Tf signed by other than the pernittee, then delegation of the signatory authority must be on file with the state per 15 A NCAC 2B
,0506('b)(2)(D).

E
uent Toxici
Repo
For
Chronic Pass/Fail and Acute LC50 Date 1-24-2019
Pace 410rl erevtllle- Mara Citdri WQabt
Facility char}eet8.Tara,inail(°at:811 001! NPDES#NC ©04
Laboratory Performing Test Pace National
x
213
Sign
f Operator Responsible Charge
ure of Laboratory Superviso
Pipe #
County Mecklenburg
Comments
Pace. National ID: L10624-01
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10
# Young Produced
Adult (L) ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
t e
a
r d
1st sample
Control
D.O.
Treatment 2
2
1st sample
4
6
2nd sample
s
t e
a n
r d
2nd sample
7
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates)
0
12.5
0
25
0
5©
75
5
1©0
o/
Environmental Sciences Branch
Div, of Water Quality
N,C, DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
11 12 Chronic Test Results
Calculated t
Tabular t
% Reduction
10 11 12
ornt3lete This For E
Sample Type/Duration
Sample 1
mple 2
Grab
ality
Control
Treatment 2
Control CV
% control organisms
producing 3rd brood
Avg.iieprod.
Control
Treatment 2
PASS FAIL
Check One
Test Start Da
(not applicable)
Sample 2 / /
Duration
Hardness(mg/1)
Spec,Cond.(µmhos)
Chlorine(mg/l)
Sample temp. at receipt
Concentration
Mortality
©= > 100 °/d
95% Confidence Limits
%- °/d.
Method of Deter ation
Moving Average © Probit
Spearman Kerber © Other N/A
Organism Tested 'Pimephales promelas
Duration (hrs) 24 hrs
DWQ form AT-1 (3/87) rev. 11/95
pH
0,04 N/A
Note: Please
Complete This
Section Also
D.Q.
1 of 10

AnaleAnalvticaI
Atalith Utt Cent -or for rOslftv In,novi,than
Pace (Huntersville) - Marathon West - Charlotte Terminal -
Client:
(Outfall 001)
NPDES #: NC0046213
Test Start Date: - I 9
Temperature (°C) - Pimephafes promelas (fathead
Control
12.5
25
50
75
100
Date:
Time:
151
Qc
0
Date: &
Time: Analyst:
si
Day 2 (mornin
oc
2 Li °C
s °c_
0 c
innow)
Time: Analy t:
11-
Measurement taken directly in test chamber
Day 2
Lab Sample #:
Thermometer Serial Number:
e 2_3(-1U—e\
064
Control Water Carboy Used:
Aot (3 11
Instruments and Methods Used for Acute/Chronic Blomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH/Temp/mV/ISE Meter
pH/IWO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chambers: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c - VWR Traceable Dual -Range Light Meter- Model 62344-944 (SIN 181399747)
Photoperiod: 16 hours light, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific lsotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation, The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Shain W. Schmitt (SWS); Brandon Etheridge (BE); Adam Macomber (AM)
Amy Eggleston (AME); Melissa Holwerda (MM); Cody Medley (CM); Nadiar Yakob (NY); Clarissa Moore (CGM);
Matthew Lockhart (MIL); Brittnie Boyd (BB); Joel Soto (JSV)
2 of 1 0

DlariDevicesUlsedin
Thermo-Kool Waik-in Incubator:
Dickson (small chart)
AI
26.0
Thermo
r
a h for Windows
25,5
2.5*0
74,5
g
TUESDAY
NOON
01/22/2019 B5722
24.0'
23,5
01/12/19 01/14/19 01/16/19 01/19/19
010000 0:0000 0:000D 00000
01/20/15 01./22/
010000 0:0000
---*
Intv1. Sample Avg.
Ch1 2min. B000 ----- ----- 25.4 24.1 24.9
Ch2 2min. 8000 25.3 24.1 24.8
Cur.A Date : 01/10/2019 20:19'52
Cur.B Date : 01/22/2019 5:2209
diff. A-B : 11 09:0217.000
Data Range 01/10/2019 20:19'52-01/22/2019 5:2209
Ca1c.Range 01/10/2019 23:31'50-01/22/2019 2:10'11

ace Analytica
Centel' i,reve,ntj 10,ovitdor,
ACUTE TOXICITY TEST DATA - Pimephales promelas (fathead minnow)
Client Pace (Huntersville) - Marathon West - Charlotte Terminal - (Outfall
001)
Begin
End
H A
Effluent in Replicate
Percent (*Ix) Position
CONTROL
12.5
25
50
75
100
A:
B:
A: I
B:
B:
A:
B:
A:
B:
A: (D
B:
Checked By: Biologist:
Fish Cup Batch/Let:
Time J5 :
Time
# OF LIVE Minnows
0 hrs 24 hrs
10
10
10
10
10
10
10
10
10
10
10
10
.)
\c.
Time: 1.C):4S
6-1 ISWP
a)
E _c
4—
C 0
2 E
NPDES# NC0046213
Test Duration:
Dilution Water:
pH (std. units)
0 hrs 24 hrs
initial
7
initial
initial
initial
7i
Initial
3
Bi4ogist, 33.4.
final
7-7
final
final
final
final
7 • (1
ablogist
tke
ESC Sample #:
/ b 73 Li ° I
24 hours
*end test +
DMW
DIssoived Oxygen (mg/L) Conductivity (umhos/cm)
hrs 24 hrs 0 hrs 24 hrs
initial
initial
initial
initial
initial
1.5 :35
final
final
final
final
final
BlolcigisLA
I 1(0
initial
Initial
5.‘
nitial
initial
71-i
initial
f4A -5
15 35
final
151,7
final
37
final
final
final
[tc
Data divided by a slash mark ( / ) indicates that a duplicate was run on that parameter- Temperature of water (minnow batch) at time of test initiation: $C-/ 3 °c
Minnows were
Alafinity
0
COMM!
LACHAT
days old at test initiation and were taken from ESC Lot #01011°) '9 Minnows were last fed k C\ @ k
100% Effluent
LACHAT
(Preliminary) Hardness
Analyst: 51a.
Date:
Time:
analyzed prior to
at initiation by Wet Lab
using:
T
hr from start time
Total Cl2
(m9/1-)
Control
< 0.2
Total Cl2 (mg/L)
100% effluent
0 (,1
Biologist/0g
prior to the test

Control Chart for December 2018 Acute C.dubia Reference Toxicant
ne'
0,
(,5
os
:�� � f� +� ,A � �� .�
. ~. ~. .. ~~ ~. .~ _`� -
r w' a+�p "�� �
te
1UIO7/17
1025/17
10/2517
11/02/17
1102/17
1208/17
O1/03/ B
D2071G
O3/O7/18
V4/D4/18
85/O2/18
O(01S/18
07/03/1B
Q802/18
0905/18
101O/1&
1101/18
1101/18
12/05/1O
12/O5/18
Values
0.5196
M373
0,6830
0,4798
0,5402
0,6830
03693
0,7071
0,6429
OAg1O
0.6156
0.7368
05835
M150
0,6547
0,5535
0.7040
0.6373
0,5391
0,4531
Mean
0.5785
0,6133
0.5799
MT2O
0.5905
O.558Q
M774
U.5047
0.5753
0.5790
0.5921
0.5915
0,5932
MS73
0.5946
0,60,10
0.6030
0.5996
O.5g23
OAB52
0,5290
0,4840
8.4871
0.5020
0,4427
OA577
0.4706
0.4639
0.4725
0.4808
0.4849
0.4906
0,4971
14972
0,5030
0,5076
015058
0,4953
ke°
V.412O
8.4447
03882
0,4022
O.413@
03264
03380
0.3566
03522
0.3660
0.3695
0,3783
0,3880
0.3970
0.3998
OAO51
O.4122
0,4119
OM82
1SQ
OJ6617
0,6976
0,6758
D.8�5g
0,6789
8,0751
0,6971
0.6988
0.6869
o�O855
0,7034
0,6981
0.6958
O.OB74
0.6919
0,6989,
0.6984'
V.soo5
M8g4
l2OdjLebanon Rd
Mt, Juliet
(615)773-75 "
(dl5)58-5O59Fax
December
2018
���� ��
0�����M�������� ~���_���
U�������l���� ��`�~������� ����
Reference Toxicant Test
1+2 SD�
07449
0,7819
0.7717
0.7418
0,7674
0,7913
0.8168
0,8128
07984
0.7920
0.8148
0,8047
0,7984
0.7970
0.7893
O.786g
0.7938
0.7874
o^78d5

Control Chart for December 2018 Chronic C,dubia Reference Toxicani
IC25 (Reproduction) K
Dates Values
07K6/17
U8/01/17
O905/17
101U/17
1107n7
12/O5/17
O1/10/18
8200/18
D3X]G/18
D403l8
O501/18
O6/O5/18
0EV1S/18
87/n8/l8
0007718
O905/18
10D2/1B
11/O8/18
12/0*/18
1204/1V
0,3988
0,3209
0.3382
0.2255
U558
U55Q
U844
0.3203
0,2956
02819
02879
02093
01882
0,2935
O2894
0.3091
0,2133
03355
0,2369
�31662
Mean
03599
O.3528
03209
0.3078
0,3007
0.2998
8.3024
03016
0,2996
01986
0,2911
O2SQ8
0.2911
0.2916
O2827
0.2881
02907
0.2879
0,2918
'
'1SD
0,3048
0.3117
0490
0,2392
U30g
D2415
0,2479
0.2506
0.2511
0,2524
0.2401
0.2421
0.2442
02484
0.2486
O2414
01440
n.z*ns
Q2428
02497
0.2708
0.1772
0,1705
0,1730
0.1831
01934
0.1996
0.2026
U053
01DS1
0,1932
0.1973
0.2011
0,2048
0.1946
0,1974
0,1939
0.11938
+1SD_
O4149
03935
0,3927
03765
O.3O45
0.3581
0.3569
0,3526,
0,3481
0.3447
0,3421
0.3397
03380
03369
O.%3G7
0.3348
0,3374
0.3349
U408
lZO65Lebanon RJ
\Mt. Juliet, TN 37122
[phone]
(0l5)758'5859Fax
December
2018
���� ��
��8�A�����0����� ��0�,���
U������������� �~�,�°������� ����
Reference Toxicant Test
�eSD
0.4700
0,4645
QA452
0.4284
0,4165
0,4113
0,4037
0,3967
O.3SOg
0,3931
V.3G80
0.3849
0.3822
0.380§,
0.3815
0.3840
0.3819

Control Chart for December 2018 Acute Minnow Reference Toxicant
4
Ol03/18 07817
0207/18 0,6557 0,7287
8307/18 0,8196 O�7590
0404/1,8 0.7135 0,7476
04/05/18 0.8892 0J359
84/11/18 Q.8892 0.7202
05/02/18 0.7647 07334
05/16/18 0.8817 U.7269
001018 U842, V444
07103/18 U196 0.7518
07/26/18 0,6875 0,7461
0802/18 U657 0,7394
09/05/18 1,2000 0,7748
09/27/18 0.7387 07722
09/27/18 0,7387 03700
1010/18 D.8196 0.7731
11/01/18 0,8138 07758
1101/18 0.7715 03756
12/05/18 0,6375 0.7683
12/05/18 0.7000 0.7�49
V.G3AO
0,6770
O/67OS
O.GGU4
0,6656
O.G746
O�6690
0,6694
8.8773
0,6726
0.6656
0.@288
0,6316
0�G342:
O.G414
0,6478
O'6514
0.6435,
06425
�pe°
O�55D5
0�5858
O.§O82
016028
8.6O31
V.6159
0,6122
O.5944
0,6027
0,5992
0.5919
0.4829
OAG11
0.4985
0.5096
0.5198
0,5272
o�o1o7
0,5200
&D178 0�9069
0.8410 0,9230
0.8183 O.B830
0,8025 0.8891
0J887 0.8532
0.7921 83508
0.7843' 0.8418
0.8194' U944
0.8265 0,9012
0.8195 0.8929
U131 0,8808
0�0208 1�066
0,9128 t0534
K9057 1l)414
U048 1.0365
Q.8�281.0319
H898 1.0240
o.8e31 1/0179
0'8873 1,0098
|4'O0jLebanon Bd
[phone]
��������NLd�0� 2018
���� ��
�°�m�"����mmN����m ��������
Reference Toxicant Test

Control Char-t for December 2018 Chronic Minnow Reference Toxicant
cvm=n.1
0,75
Dates Values
~2 8
07/11/17 OA597
08/01/17 0A085
08/12/17 0.5547
10/1017 0.5459
1010/17 0.6094
11/07/17 04684
12/05/17 0'5378
0105/18 OA941
02/06/18 OA808
030018, 0'4562
0402/18 O�5069
0501/18 0,4335
06/05/18 0.5210
07/03/18 0.4300
08/07n8 0.5491
0905/18 UA410
1002/18 0.4705
11X0618 0,4976
1204/1e 0.57e0
0.4641
QA943
0.5072
0,5276
0,5179
0,5208
0.5175
O.5133
0.5076
0,5075
O.5014
0�5O29
UAg77
O�5V11
OA873
O.435@
0,4959'
V�5nV2,
0.5061,
OA578
O.4418
CA572
14647
0,4568
0.4645
0.4O45
14622
0,4561
0.4587
O.45O1
0,4535
O.4484
O.44S9
0,4457
0,4453
V.44G9
oA48O
0.4498
P +2
84517 0A703 0,4765
O.3893 O�5488 O�5993
0.4071' 0.5572 0\0873
U.4017 0.5900 0.6536
U2957 O�5791 U402
0.4081 0,5771 8/6334
0.4115 0.5704 U234
0,4111 U044 0.6155
0.4047 O�5580 0,6105
0.4099 0.5563 U052
0.3969 0.5526 U030
0.4042 0.5522/ 0'6015
0.3952 O�5489 0.6002
0-3908 0.5522 0.6034
0'3841' 0.54901 0.6005
0.3949 0.5462 UQOD
0.3980 0,5448 0.5837
8.3978 0,5515 0,6027
0.3934 _ 0,5624- O.G187
12065 Lebanon Rd
1\1t, Juliet, TN 37122
[phone]
December
2018
���� ��
����«�����@�N��= .��@-���
Refer������x�������~�� ~�����~�`����1� ~���x��
ence ����~8=~~=""� 0��c��

Chain of Custody
kc r er: 41443 r rla rder Name: Wet Terminal l° C'0
Le Anatytscal Charlotte
00 Kincey Ave. Suite 100
6Hunt©rsville, NC 28076
Phone[phone]
Email: an9eia.b ions labs,corn
NC
Cooler Temperature cnrrgeeel
i Psur d y, Ja1nu ,~y 17, 2019 'Lt)4:2 PM
M
ody Seal Y csr
Restrt earJerd
ace na � cal
H101

Anal
CHAIN-0 USTt, 6Y Analytical Requeso urnent
Gt es °Cx<vE4 {tV t5mia31*eh,
AmaiytiC'44 - #4#n#3t s5+ tktt NC nint�t
Art4eL4 Ef.ia�,i
9a00 KiriteyAwe„Sit, SOS
�i%artat�rxer"iler. f 2SR�i7at
CuvroivfCi1y; i411,`Z.„%,wtr.�oaiera�� �i
(044.4
0GITFd
Might

ReCENEDINCD
WOROS
OF oi;E
January 14, 2019
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
V [9'422 2
840
RECEI
JA►N182019
CENTRAL FILES
DWR SECTION
Sent via Overnight Mail
Enclosed please find the December 2018 NPDES report, plus one copy, for the above -referenced
permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
4
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NPDit PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC -I
eDMR PERIOD: 12-2018 (December 2018)
PERMIT VERSION: 4,
CLASS: PC-1
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 1,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
16
17
.18
14
20
21
22
03
24
25
26
27
28
20
30
31
I ;
6. 0
lirs
2400 dark
1505
1400
Operator Time Oa Site
0,25
0,25
ORC On Site?.
27/23/8
No Reporting Reason..
50050
See Permit
Recorder
FLOW
000 I
o.177
C0530
Monthly
Grab
Tss6022
-
4,7
34030 00556
Monthly Monthly
Grab Grab,
BENZENE MAMA
n36,11
<2 <5
32780
Monthly
Grab
5(41/3 Ta
mei!
00070
Monthly
Grab
TURKIDTV
ntu
(38
0910
t
0915
0.25
0.25
0.25
0,251
0,18.3
01 9
Monthly .ANTragELBEEE'
8100008 A..8#' 0,1604
Daily 6188660 68 W251
IL10). Minirrnm: o9
30
4 7
4.7
4,7
0
(1
**** No Reporting Reason: ENT -RUSE = No Flow-ReuseiRacyclei ENVWTEIR No Visitation — Adverse Weather; NOFLOW No Flow; HOLIDAY No Visitation -- Holiday
6,8
6.8
6,8

NPDES rE:Rmrr NO,: NC0046213
FACILITY NAME: Charlotte TenninaI
OWNER NAME: Mplx Terminals LK
GRADE: I)C-1
eDMR PERIOD: 12,-2018 (December 2018)
COMPI LANGE STATUS. Compliant
•
ttl•
ORCICertifier ''` ure; Darryl Keith Thompson E-Maii:dkthorripson@marathonPet
PERMIT VERSION: 4,.0
CLASS; PC-1
ORC: .Darryl Keith Thompson
ORC IU%S CHANGED: No
VERSION: 1,0
CONTACT PRONE 4194212019
By this signature, 1 certify that this reporl isa0curalc and complete to the best of my knowledge.
PERMIT STATUS: Active.
COUNTY: Meckleriburk
ORC CERT NUMBER.: 1005070
STATUS: Processed
SUBMISSION DATE: I 1120 I 9
The pennittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment,
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the lime the pennittee becomes aware of the circumstances.
lithe facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part 11-E,6 of
the NPDES permit,
01/1112019
Perin .ee, 'at :*** Angela S Brown [e-mail] Phone t1:419-421-2629 Dale
Permittec Address: 8035, Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06130/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those perwns directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Pace Analytical ;ervices, Inc,
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES: Qualfieri
PARAMETER CODES
Parameter Code assistance may be obtained by callin.g, the NPDES Unit (919.) 807-6300 or by visiting http://portal.nedenr,o
ip,ps/n
s,
FOOTNOTES
Use only units of measurement. designated in the reporting facility's NPDES permit fur reporting data,
* No FlowfDischarge From Site: Check this box 'if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period,
ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G ,0204,
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on fUe with the state per ISA NCAC 213
.0506(b)(2)(D).

FLED
ON
December 12, 2018
NC .DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corpor.tion
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via Overnight Mail
I ECEIVED/NClENR/DWR
UVOR3S
MOORESViLLE REGtONAL OFFICE;
Enclosed please find the November 2Q18 NPDES report, plus one copy, for the above -referenced
permit.
If you have any questions or require additional information, I can be reached at 419-421-201.9 or by
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

PERMIT NO,: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 11-2018 (November 2018)
2400 clock
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Darryl Keith Thompson
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
Br,
2400 stack
Warn
4
12
13
t4
1630
1130
1210
0,25
0,25
11.}25
Y
50050
mit
Recorder
)7LOW
rnd
11.001
0.101
0,149
15
1b
17
1530
0.25
Y
0,253
COS3O
Monthly
thab
5 0S - Gnnc
34030
Monthly
Grab
BENZENE
u0I
<2
00550
Monthly
Grab
Ott,-GRS)
<5
32730
Y
Grab
MEN, iR
<0.01
00070
Monthly
Grub
n;ABtDTY
aft
10
19
20
21
22
23
24
25
26
27
z4
30
1130
••"' No Reporting Reason: ENFRUSL = No Flo
'2,2trathly Averek*ac
Daily Mas(Mnum:
Daily Minimum:
0.1128
11.2.53
0001
50
7,9
79
7.9
0
0
0
0
0
se/Recycle; ENVWTHR,r No Visitation -- Adverse Weather; NOFLOW = No Flow; HOLIDAY No Visitation — Holiday
12.8
12,8

NPDES PERMIT NO.: NC0046213 PERMIT VERSION: 4,0 PERMIT STATUS: Active
PAC tun' NAME.: Charlotte Terminal CLASS: PC-1 COUNTY: Mecklenburti
OWNER NAME: Mplx Terminals LLC ORC: Darryl Keith Thompon ORC CERT NUMBER:, 1005070
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 11-201.8 (November 2018) VERSION: 1,0 STATUS: Processed
COMPLIANCE STATUS: Corsi CONTACT PHONE #: [phone] SUBMISSION DATE: 10/2018
ORC/Certifier Signature: Da
12/06/2015
Keith Thompson E-MaiLdkthompsor4„ainarathonpetroleurn„corn Phone #:[phone] Date
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge,
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens pubhe health or the environment,
Any information shall be provided orally within 24 hours from the time the nominee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table far improvements to be made as required by part II.E.6 of
the NPDES permit,
0
Pc n. Signature:*** Angela S Brown [e-mail] Phone #:[phone]
Permit:tee Address 015 Mounty Rd Paw Creek NC 28130Permit Expiration Date: 06;130/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABORATORIES
1A:13 NAME; Pace .rvices, Inc.
CERTIFIED LAB #:
PERSONN COLLECTING SAMPLES:. I Qoallteri
Date
PARAMETER CODES
.Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting hitp://portalmcdertr.org/wela/wq/swp/psinpdes/fonns,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
4 No Flow/Discharge From Site: Check this boxif no discharge occurs and, as a result, there are 11,0 data to be entered .for all of the parameters on the DMR
for entire monitoring, period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per I5A NCAC 86 .0204.
*** Signature of .Pertnittee: If signed, by other than the permittee, then delegation of the signatory authority must he on file with the state per 15A NCAC 2B
.0506(b)(2)(D),

NPDES PERMIT NO.: NC0046213
FACILITY NAME: C ha:acme Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC- I
cDMR PF,RIOD: 10-2018 (October 2018)
RECEIVED
PERMIT VERSION: 4,0 .3ERMST STATUS: Active
VED/NCDFNROWP
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
WQROS
CLASS: PC -I 3 E C 0 4 zoie •COUNTY; Meeldenbura
ORC: Darryl Keith Thompson ORC CERT NUMBER: ll. 5.07
---t EN. t-0:\E FILES
ORC HASCHANGED: No Di\i"ii: SECTION
VERSION: 1.0 STATUS: Processed
"'* No Ropoiling Reason: ENFRUSE.. No Flow.Riiuso/Rocycl< ENYWT1111,7 No Visitodon Adveriiie Wither, NDFLOW, No Plow: HOLIDAY - No Visitation - Holiday

NPDES PERMIT NO.: NCOO4(21 3
EACILrry NAAM Ual-tom Terminal
OWNER NAE Mpk Tectninkils LUC
GRADE: PC -I
c7011111 14411.0W 10-20 '20181
PERMUT VERSION: 4 (..1
CLASS: PC -I
OR(-: Darryl Tlwason
OKC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS; Activ(:.
COUNTY: Mec.klenburg
onc (-tin NUMBER: 1005070
STATUS:
SAMPLING LOCATION: EFFLUENT DISC A G NO.: 001 NO DISCHARGE*: NO (Continue)
No Reporirog Reason. ENTRANT, tt' No Flow-Reti$eltecyrtW ENNAVTIAR. Visitatturi - AI cese Weather, NiaTIOW No Flow, HOLIDAY a- No ViOation - Holiday'

NEVES PERMIT NO.: NC0046213 PERMEE VERSION: 4 0
FACILITY NAME: Charlotte Terminal CLASS: PC -
OWNER NAME: Mplx Terminals LTC ORC: Darryl Keith Thompon
GRADE; pC,-.1 ORC HAS CHANGED: No
rDMR PERIOD: 10-2018 (October 20111) VERSION: 1
COMPLIANCE STATUS: Compliant CON"' ACT PHONE #: [phone]
ORC/Certifier Signature: Darr,
(backup) Terry Pridgcn Email; tepridgengmarathonpetroleurn.com PC / I / 1004617
Primary ORC Thompson is out of office until 12-03-2018.
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
PERMff STATUS: Active
COUNTY: Meeklenbrirl
OR(' CE,RT NUMBER: 100,, 7
STATUS: Processed
SUBMISSION 'DATE:
26/2
11112/20 8
- E-Maikdkthompson©marathonpetroleum.com Phone #[phone] Date
The perm ittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment,
Any information shall be provided orally within 24 hours 1mm the time the permittee became aware of thc circumstances, A written submission shall also be
provided within 5 days of the time the NI -mince becomes aware of the circumstanee.s,
lithe facility,' is noncompliant; please attach a list of corrective actions being takenand a time -table for improvements to be matte as required by part I1E,6 of
the 'NPDES permit
126/201
eSubner Signature:*** Angela S Brown E-MaiLasbrowngmarathonpetrolcurn.com Phone 4!419-421-2629
Permittee Address: 8035 Mount Dolly Rd Paw Creek NC 28130 Permit 'Expiration Date: 06/3012020
I certify. under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the intbrwation submitted, Based on my inquiry or the person or persons who managed the
system, or those persons directly responsible for gathering the information. the information submitted is. to the best of my knowledge and belief true,
accurate, and complete, I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERT1 Ft ED LABORATORIES
LAB NAME: Pace Ana
ccwr Fl El) LAB #:
PERSON(s) COLLECTING SAMPLES: I Qua "len
Date
PARAMETER COD1?.S
Parameter Code assistance may he obtained by calling the NPDES Unit [phone] or by visiting hup://portaLnedenr.orgAvebiwq/swpipsin d s,
FOOTNOTES
Use only units of measurement designated in the reporting, facility's NPDES permit for reporting data,
* No Flow/Discharae From Site: Check this box if no discharge occurs and, as a result. there are no data to be entered for all of the parameters on the DMR
for entire monitoring period,
** ORC on Site?: ORC must visit facility and document visitation of Facility as required per 15A NCAC 8G .0204.
*** Signature of Permilice: If signed by other than the perminee. then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
,0506(b"}(2)(1))

pas ;iw,d :StLV,LS
Nq
OJ
V :Sl.1.V.LS 11181134
071:Nt)ISWAA
J tiV1IJ SVI1:YiO
1. 91!ay. 175 rO-:MAO
)d =SSV L)
A.nttia3d
1•34 :110V2V.)
'0141110I3d S31141,1

Effluent Toxicity Report Form- Chronic Pass/Fail and Acute LC50 Date 10-16-18
Pace Mun:ersvil,le- Marathon -
Facility charlotte Terminallnutfa11 00L1 NPDES#NC 0046213
Laboratory Performing Test ESC Lab Sciences
x
Signatu
perator in s onsibl a Charge
cie,
aborato u erv�s r
S
9
0
rY P
0
Pipe # County Mecklenburg
Comments
ESC Lab ID: L1031089-01
MAIL ORIGINAL TO:
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10
# Young Produced
Adult (L )ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
a
e
n
d
1st sample
Control
D.O.
Treatment 2
a
1st sample
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
11 12 Chronic Test Results
Calculated t
Tabular t
% Reduction
2 3 4 5 6 7 8 9 10 11 12
e
n
d
2nd sample
a
2nd sample
e
n
d
LC50/Acute Toxicity Test
(Mortally expressed as %, combining replicates)
0
Ok
5
6.25
0
12.5
25
0
50
5
100
/o
%Mortality
Control
Treatment 2
Control CV
% control organisms
producing 3rd brood
Complete This For Either Test
Avg.Reprod.
Control
Treatment 2
PASS FAI
Test Start Date
10/ 3 18
Collection (Start) Date (not. applicable)
Sample 1 10 / 2 /18 Sample 2 / /
Sample Type/Duration
Sample 1
Sample 2
Grab
grab
N/A
Comp.
Duration
N/A
%
Hardness(mg/I)
Spec.Cond.(pmhos)
Chlorine(mg/l)
Sample temp. at receipt
Concentration
Mortality
LC50= > 10 0
95% Confidence Limits
%-
Method of Determination
Moving Average © Probit
Spearman Karber EJ Other N/A
Organism Tested Pimephales promelas
Duration (hrs)24 hrs
DWQ form AT-1 (3/87) rev. 11/95
startfend
pH
49.2
99.2
63.9
0.11
1.0
N/A
N/A
N/A
Note, Please
Complete This
Section Also
start/end
Contro
High
Conc.
D.O.
1/10

Analytical
- National Center for Testing & Innovation
Pace - Huntersville - Marathon - Charlotte
Client:
Terminal (Outfall 001)
NPDES #: NC0046213
Test Start Date:
it)-3 )0
Temperature (uC) - Pimephales promelas (fathead minnow)
Control
6.25
12.5
25
50
100(PL)
Date:
Time: Analyst:
1'71)5 or
Day 1 (initiation)
2L1 °c
?L1-7 °c
2 9-4 °c
Date: LL- tif
Time: Analyst:Tio0 Anial2
ts.) :o
Day 2 (morning)
,k‘,°c
°c
Z_c_i °c
'C
Day 2 (final)
ac
2_4 oc
:ZtV1 °c
"" Measurement taken directly in test chamber
°C
Lab Sample
Thermometer Serial Number: 18050064
Control Water Carboy Used:
g \PM
Outfall
001
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH/Temp/mV/ISE Meter
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Water Bath: Lindberg/Blue, Model WB1140A-1 (serial #S01M-580360-SM)
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chamber: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c - VWR Traceable Dual -Range Light Meter- Model 62344-944 (S/N 181399747)
Photoperiod: 16 hours light, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific Isotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc„ serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
bench sheets in this report: Shain Schmitt (SWS), Brandon Etheridge (BE), Amy Eggleston (AME)
Adam Macomber (AM); Melissa Holwerda (MM); Cody Medley (CM); Nadiar Yakob (NY); Kristen Rodgers (KR)
Clarissa Moore (CGM); Matthew Lockhart (MIL)

E°c
26.0
24.5
Chart Devices Used in
Thermo-Kool Walk-in Incubator:
Dickson (small chart)
dV ©T (0
a -fig +o 10-4-1
Thermo Graph for Windows 10/09/2018 15:35'45
-71
10/03/18 10/0 5✓19 101 t17f 13 10/09/19
0:00'00 0:00'00 0:00'00 0:00'C70 0:00 00 0:00'00
ch Name
1 Ch1
2 Ch2
Cur.A Date : 09/27/2018 19:23'52
Cur.B Date : 10/09/2018 4:26'09
diff. A-B : 11 09:02'17.000
Intv1. Sample Cur.A Cur.B A<->B High Low Avg. Unit
2min. 8000 ----- ----- ----- 25.7 24.4 25.2 °C
2min. 8000 - ----- _---- 25.7 24.4 25.2 °C
Data Range 09/27/2018 19:23'52-10/09/2018 4:26'0^3 / 1 Calc.Range 09/27/2018 22:35'50-10/09/2018 1:14'1

NORTH CAROLINA - ACUTE TOXICITY TEST DATA SHEET - Pimephales promelas (fathead minnow)
Client Pace - Huntersville - Marathon - Charlotte Terminal (Outfall 001)
Begin
End
CL2
(mg/L)
< 0.2
CL2
(mg/L)
Effluent in
Percent (%)
10% DMW
CONTROL
6.25
12.5
25
50
100(PL)
Checked By:
(//,
Replicate
Position
A:
A: 2
B:
B:
A: u.
B:
B:
A: G
B:
Biologist:
Time
Time
Time
# OF LIVE Minnows
0 hrs 24 hrs
10
10
10
10
10
10
10
10
10
10
10
10
IT :3r
)0
( tYl
o
f4,
emperatures have been recorded on
Check here to confirm
a)
_c
*end test +/- 1 hr
from start time
pH (std, units)
0 hrs final
initial
g*
initial
0
initial
initial
initial
Initial Readings By: (Y1
NPDES #: NC0046213
Test Duration: 24 hours
Dilution Water: 10% DMW
Minnow final
77
Minnow final
Minnow final
7,
Minnow final
Minnow final
-7, 7
ESC Sample #:
Analyticar
t A, ha .14,,trq frtrig..o.
Dissolved Oxygen (mg/L)
0 hrs
initial
CH
initial
initial
initial
initial
initial
final
Minnow final
Minnow final
Minnow final
Minnow final
(-)
Minnow final
Final Readings By: (
Data divided by a slash mark ( / ) indicates that a duplicate was run on that parameter, Temperature of water (minnow batch) at time of test initiation:
Minnows were c2 days old at test initiation and taken from ESC Lot # ()/V /*I h Minnows were last fed
Control
ILACHAT
Alkali
100% Effluent
LACHAT
mg/L
(Preliminary) Hardness
Analyst: 14)(0
Date: 10-5-kt
Time: t
Contro
49ic mg
analyzed prior to
test initiation by
Wet Lab using:
LACHAT
Cit kVi
°c
Conductivity
(umhos/cm)
initial
cri
initial
initial
/0 / / )1 : o_s- prior to the test,
Hardness
100% Eff uent
initial
initial
analyzed in Wet
Lab via LACHAT

Control Chart for September 2018 Acute C.dubia Reference Toxicant
CV% = 16.5
0.9
9.
0,7
0.6
0
J 0.5
0.4
Dates
06/07/17
07/05/17
08/02/17
09/08/17
10/07/17
10/07/17
10/25/17
10/25/17
11/02/17
11/02/17
12/06/17
01/03/18
02/07/18
03/07/18
04/04/18
05/02/18
06/19/18
07/03/18
08/02/18
09/05/ 18
Values
0.4830
0.6164
0.5743
0.6515
0.4433
0.5196
0.6373
0.6830
0.4798
0.5402
0.6830
0.3693
0.7071
0.6429
0.4910
0.6156
0.7368
0,5835
0.6156
0.6547_
Mean
0.5497
0.5579
0.5813
0.5537
0.5480
0.5608
0.5761
0.5654
0.5628
0.5738
0.5567
0.5683
0.5736
0.5681
0.5711
0.5808
0,5810
0.5828
0.5864
Date
-1 SD
aceAnalytica
CFrr,rer fur Ppvrrtg & tcrmr,0!47,7
0.4554
0.4897
0.5086
0.4655
0,4679
0.4802
0.4899
0.4786
0.4807
0.4878
0.4557
0.4630
0,4705
0.4665
0.4722
0.4770
0.4802
0.4846
0,4894_
-2 SD
0.3610
0.4215
0.4358
0.3773
0.3878
0.3997
0.4037
0.3918
0.3985
0.4018
0.3547
0.3577
0.3674
0.3648
0.3733
0.3731
0.3794
0.3863
0.3925
+1 SD
0.6440
0.6261
0.6540
0.6419
0.6281
0.6413
0.6622
0.6521
0.6450
0.6597
0.6577
0.6736
0.6768
0.6698
0.6700
0.6847
0.6817
0,6810
0.6834_
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
September 2018
Reference Toxicant Test
+2 SO
1 S©
Mean
-1 SD
-2 SD
+2 SD
0.7384
0,6943
0.7268
0.7301
0.7082
0.7218
0.7484
0.7389
0.7272
0.7457
0.7587
0.7789
0.7799
0.7714
0.7689
0.7886
0.7825
0.7793
0.7803
5/10

~
Control Chart for September 2018 Chronic C,dubia Reference Toxicant
C4
O3/OD17
D4/0417
u5/O2/17
000G/17
O7/0O/17
U8/O1/17
D90517
101O/17
1107/17
1205/17
O1/10/18
Q20O18
O3/V@18
0403/18
O501/18
O6/05/18
06/19/18
V70318
U80718
09/O5/18
Values
0.3150
0.2329
O.3O93
01938
Q.3888
0.3209
03382
O.%255
0.2558
0.2650
0.2944
0.3203
02958
0,2819
0.2879
01093
0.2882
0.2935
0.2994
0.3091_
/
Mean
0.2740
0.3057
0,2778
03020
0,3051
0,3098
O.2QQ3
0.2945
0,2915
0.2918
0.2942
0,2943
01934
O.2830
0.2878
0,2878
O.%881
U.2887
�0.2QS7
'1 8D
keAnalytical -V
0.2159
O2871
0.1985
0.2146
U2O6
02371
0.2256
0.2240
Q.2245
02282
0,2329
0,2357
0.2370
0.2386
0.2312
0.2331
0.2350
02370
0,2392
+18D
0,1578
0.1684
0.1193
01272
0.1480
0.1643
0.1519
0.1536
0]574
01645
0.1717
0.170
0.1806
0.1843
0.1747
0.1783
0.1819
0.1853
0.1887
)206jLebanon Rx
(015)773'7549
�� �=�� ���� 2018
���� ��
�������NL���������� ����|U��
N�^���~�W������� ��*�����`������ ��^�N���
mn.��m�����mmm��� m����N����mw&. N��~��
03320
03744
0.3570
03894
0.3837
0.3826
03730
0.3649
0.3586
0.3554
0.3554
0.3529
0.3498
0.3474
0.3443
03426
U413
0.3404
0,3403
0.3901
0A431
OAJ62
0,4767
0.4622
8A554
0.4467
0.4353
0.4256
0,4190
0,4166
0.4115
V.4OG2
0.4O18
OAOQ9
0,3973
0.3944
0.3921
0.3908

~
~
Control Chart for September 2018 Acute Minnow Reference Toxicant
�
�
�
1025/17
1025/17
110217
110Z17
120tJ17
O1/03/18
0207/18
0307/18
O40418
0405/18
O4/11/18
U50218
O5/1U/18
O019/18
O703/1O
07/2018
O802/18
0g05/18
U027/18
U027/10
Values
U128
0.8858
O�S415
0.8785
0.8045
O�7S17
O�6657
0.8196
0.7135
0.6892
0,6892
0.7647
0.6817
0.8842
0.8196
0.6875
0.6657
1.2000
0.7387
0.7387.
Mean
0.8493
U8OO
0,8797
0.8646
0.8525
0.8258
0,8250
O.8128
0.8003
03902
0.7881
0.7799
03873
03895
O.7831
0.7762
03997
03965
03936
'1 SO
0.7977
0,8155
0.8269
0,8079
03937
0.7371
0.7429
0.7273
0.7109
0.6990
0.7008
O.GD13
0.6977
O.7O27
D.6&55
0.6867
0.6674
0.6672
0.6671
5"e Analj4ical *
03460
O751O
0.7742
0.7513
8.7348
0,6484
088D8
0.6419
0.6214
0.6078
0.6135
O.002O
UU82
U10O
0.6079
0.5973
0.5351
O.5878
0.5405
+1GD
0,9009
0,9446
0.9224
0.9213
0.9113
O.9145
0.9071
U98O
0.8897
O.8814
0,8753
O.8085
0.8769
0,8762
U.87O7
0.8657
0.9321
0.9259
0.S2O2
l2O65Lebanon Bd
(615)78'7549
(615)758`5859 Fax
September ���� 2018
���� ��
��o����NL��mmN����� ����|U��
�����A�U����� ���������U�� �����
m`���m��m��mm~~�� m��=�Nn���mmN. N��~p�^
0.9526
1.0091
0.9851
0.9780
O�D7U1
1,0031
V�98S3
0.9833
U.Q781
O�9726
V.QO2@
0.9571
0.9665
0.BO2Q
0.9583
0.9551
1,0644
1.0552
1.0468
7/l0

^
Control Chart for September 2O18Chronic Minnow Reference Toxicant
cvm=1VA
oG
007/17
O40417
05/1017
000G/17
D7/11/17
0801/17
09/12/17
101017
101CV17
1107/17
120517
D10Q18
O2/OO/18
V308/18
U403/18
0501/18
0O05/1G
O78]3/18
0G07/18
0905/18
Values
0�0O09
0.4926
O.5522
0.4925
O.45S7
0,4685
0.5547
O�545S
0,6094
0.4694
0.5379
0.4941
0.4800
0.4562
0�5O0S
0,4335
0.5210
0.4300
0,5491
OA41O
Mean
0.5468
0.5486
O.5340
0.5196
0.5111
0,5173
0,5209
0.5307
0,5246
O.5258
0.5232
O�518G
0.5153
O�5147
O.5O97
0.5103
0.5059
0.5081
O�5O48
'1SO
0.4702
0.4943
0.4821
0.4632
0.4585
0.4648
0.4712
O/4757
0.4692
0.4731
0,4721
OA6Q
0.4640
0,4653
0.4577
OA0OO
O.4535
0.4563
0.4521
0.3936
0.4401
OA297
0.4068
0.4019
0.4123
0.4216
0.4207
0,4138
0.4204
0.4210
0.4192
O/4128
0.4158
OAO58
0.4097
O.4O11
0.4044
0.3995
8.6233
O�6O28
0.5870
0.5760
0.5657
0.669@
0.5705
0.5857
O'58OO
D.5786
0.5742
0.5702
Q.5865
D�5642
O.5G18
Q.5GUG
0,5582
0'5OAO
0.5574
12065 Lebanon Rd
Ivk Juliet, TN 37122
[phone]
(6l5)758'5859Fax
September
p������
w�y����N���m���~�m�.m �����L��
N�"���~ ~
��«�N8��U�U��~�� ��m?�N����U�� ������
���"m��~~ m��°~�m���mwN^ 0��~wN.
O�6999
0,6570
0.6394
0,6324
U2O2
O.G223
0.6201
0.6407
0.6353
0.6312
0.6253
O�02D5
0,6178
0,6136
0.0135
0.6110
O.O1D6
0,6118
0J51O1

Chain of Custody
Workorder: 92401759
Rpt°t; Ini
Workorder Name: Tox ity NC0046213
Angela a onI
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: angeiaobaionir paceiabs-corn
State f Sarnpie Origin: NC
0
RAD S
A14F��

c/qN-O-CUTODY&nyticak RequestDocument
w2 a ( ,rrr
Ages
1011TIALLS1
wbemrant, chip we»we>H
,amerrr
ALL SHADED AREAS are for LAB USEONLY

NPDES PERAIT NO.: NC0046213 PERMIT VERSION: 4.0
RtzCEIVF
nERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mpl Terminals 1,1,C
GRADE: PC -I
eDMR PERIOD: 09-2018 (September 2018)
CLASS: PC-1 COUNTY: Meeklenbur
ORC: Darryl Keith Thompson OCT 2 5 2Qth ORC CERT NUMBER: 1005070
RECLIVEDINCOENRIDWR
ORC HAS CHANGED: No ll—ZN i'-<./AL, FrLES
VERSION: 1.0 DWR SECTION STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCIIARGE NO.: 001 NO DiscmA
,1(,)
24410 Omit
lth
Average Limn:
Monthly Average:
Daily Maximum:
Oath! nlinimorat
Sng.50 C0530 34440 005.56 34744
See Permit
0.189
0.612
oni1-11
BENZENE.
ona
Grab
0.11,6
lonthly
MIEN, TR
ltt
'OS
,a..(3,10NAL„ E
(11020
Groh
TURRIDTV
(1,5 0 0 4.4
*•*" No Ropootng Reason: ENFRUSE Flow-Reuse/Recycle ENVWTHR = No Visitation— Adverse Weather; NOFLOW = No Row; HOLIDAY =No Visitation IloOday

NPDES PERMIT NO.: NCO046.213 PERMIT vERSION:
FACILITY NAME: ChartoncIennina CLASS: PC-1
OWNER NAME: Ivipls 'Terminals TLC OR( Darryl Keith 'Thompson
GRADE: PC- ORC HAS CHANGED: No
eDNIR PERIOD: 00-20IS iSeitember 20) VERSION: 1,0
COMPLIANCE .F.LATUSi Com ant CONTACT POONE *: 4)42209
PERMIT STATUSi
COUNTY': Nlecidenburil
ORC CERT NUMBER: 1005070
STATUS: Processed
SUBMISSION DATE:
0202/2018
°RC/Certifier Sig tire: Darryl Keith 'Thompson E-Nlail,dkihompson@marathonnetroleum,eum Phone #,980-613-0495 Date
this signature, I certify that this report ceurate and complete to the hest of my knowledge,
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment
Any information shall he provided orally within 24 hours from the time the permittee became a Niqi re of the circumstances, A written submission shall t'ilso
provided within 5 days of the t imc the permittee becomes aware of the circumstances,
If the facility is noncornpliant, please attach a list of corrective actions being taken and a time -table tOr improvements to be made as required by part I1.E.6 of
the NPIThS permit,
10:211201 8
Per ;tceS oh er Si gna ture:+" A.ngela S BrOWn Es.MatEashrown@inarathonpetroloutracom Phone #:[phone] Date
Permittee Address: 8035 Mount Holly Rd 'Paw Creek NC 281,W Permit Expiration Date: 06/30 2020
I certify.% under penalty of law, that thi;s document and all attachments ‘+ere prepared under rny direction or supervision in accordance with a system qlesigned
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person 'or persons v0ho managcd the
system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of iny knowledge and belief, true.
accurate, and complete, I am aware that there are significant, penalties for submitting false information, including the possibility of fines and imprisonmen
knowing violations,
CERTIFIM 1 \ BORN ES
LAB NAME; Pace Analytical Strvit:tItt,
CERTIFIED LAB
PERSON(,) 'COLLE( r INC: SAM PI, ES: uhcw cotThy
PARAMETER CODES
Parameter Code. assistance may be obtained hy calling the 'NTDES Unit [phone] or by visiting, httinifportaLitcdent.org/webAvq/swprpsfitpties' forms,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit lot reporting data.
No Flo'.'Dichargc From Site: Check this hox if no digeharge OCCUTS and, as a result. there are no data to be entered for all oldie parameters on 10 DMR.
Mr entire monitoring, period.
" ORCon Sitet ORC must visit facility and document visitation of facility as required per 15A NC AC 8G ,0204,
""' Signature of Permittee: If signed by other tit 211 the permittee, then delegation or the signatory authoritymust be on file with the state per I 5A NCAC 214
,(15(6(0)(20),

NPDES PEI MtT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
PERMIT VERSION: 4.0
CLASS: PC-1
ORC:.Darryl Keith Thompson
ORC HAS CHANGED: No
eDMR PERIOD: 09-20I R (Septeasther 2018) VERSION: I,0
Outfall OO1 - Effluent Comments:
ss is being reported on 09/12/2018 due to a laboratory error for the 09/07/201 R samples collected,
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 1005070
STATUS: Processed

Risner, Erin E.
From; Nicole GasiomwsN«Nkohe.GasiorowsW@>paccabs.com^
Sent: Friday, September 14'20109:21 AM
To. Risner,Erin E.;]arnbeck'Bob
Cc; Angela 8aioni
Subject: (EXTERNAL] TSS Lab Error for Pace WO# 92398729 and Pace WO# 92398731
Good morning,
This email is to document the TSS volume loss due to a laboratory error for the 9/7/18 samples collected in association
with the following two WO#s:
92398729:CLTEast NC8OO2l971 K4mnthk/
SZ398731.[LTWest N[O046Z13Monthly
TSS was re -collected for both sites on9/12/l8.
|fyou have any questions atall, please let nneknow,
Thank you,
Nicole

NPDES P`E MtT N©.; NC0046213
FACIL1 NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals l„.LC
GRADE: PC-1
eDMR PERIOD: (i8.2018 (August 201E
PERMIT VERSJON.4.0 ERMIT STATUS: Active
E�EIVFp�
CLASS: PC-1 COUNTY: Mecklenburg
ORC: Darryl Keith Thompson S E P 24 Z Q t ORC CERT NUMBER: 1005070
ORC HAS CHANGED: No CENTRAL FILES
VERSION: 1.0 ©WR SECTION STATUS: Processed
SAMPLING L "'ATI©N: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
o Flow-Reuse/Recycle; ENVWTHR m No Yisilation- Adverse Weather, NOFLOW n No Flow; HOLIDAY vt, No Visitation- Ho!'

NPDES PERMIT NO.: NC0046213
FACILITYAME: Charlotte Temunat
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 0S-2018 (August 2018.1
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: PC -I COUNTY: Mecklenburg
ORC: Darryl Keith Thompson ORC CERT NUMBER: 1005070
ORC HAS CHANGED: No
VERSION: I.© STATUS: Processed
T PHONE k: 4194212019 SUBMISSION DATE: 09/18/2018
ORC/Certifier Signature: Darj/eith Thompson E-
:dkthomns+un
09/10/2018
tbonpetroleum.com Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittcc shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the enviranment,
Any information shall be provided orally within 24 hours front the time the permittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
e/Su
09
atsre:*** Angela S Brown E-Mail:asbrown@marathonpetroleum,com Phone #:[phone] Date
Permittee Address: 8035 Mount holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABO
LAB NAME Pace Anatytc Seavi s, isrc.
CERTIFIED LAB 0:
PERSON(s) COLLECTING SAMPLES:1 Qualfieri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box lino discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Perntittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 213
.0506(b)(2)(D).

NPI)N S PERMIT NO.. NIL 0046213
NAcILL1.y NAME: CharrletacTe
C)1" FR ti,�ME Adis 'fi
e©ISIR PER OD: 0
SAMPL,ING LOCATION: EFF
PERMIT VERSION: iRF(Fl\ED PERMIT s- AIIES:r�cli
CLASS: PC-1
VERSION:
04 Z016
a1. FILES
ECTION
Thnnir t>
COUNTY: Y: MecLlcnbur
ORC C°FRT NOSH:SF;R; )005,070
RECEIVED/NCDEN / WR
0 x
DISCHARGE NO.: 001 NO DISCHARGE*: NO (Ci9 Ige)
MOORESVILLE REGIONAL QFFICE

*IASPERMF\: /
FACILITY N ME 9.
OWNER N !
GRADE:
mwREE .c :mom o
7R R VERSt :
O S:
ORCR6 CHANGED: No
VERSION: ILI
RR9RSTATUS: woy
COUNTY: ±aw$
ccml>D:k% 1W070
S w Pr x cd
SAMPLING LOCATION: EFFLUENT DISCHARGE NOegnl NO DISCHARGE*: NO
v-Re a » wvwn»=vim

046213
Ts €nzrtals L.L.c
el)f•MR PER IC)ll:07-_(31 ul= 111Ki
COMPLIANCE STA`1C
I
ORC'C cr'tificr
PERMIT V'ERSIO'
CLASS: PC -I
ORC: t.)unryy1 Keith Thompson
ORC tIAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: 4 4:
Thompson E Maihdkthirrnpsonrri;
n
PERMIT STAT('S: lctixs
('OCE'[V >Ai�nrklcrnhurc
OR(: C:ERT S ' I lEH: 100507(i
-0495 Gate
The pent -Mice shall repo t to the Director or the, appropriataa Ra ioetttt t)ffice any ncrncrtrnpliatrrte that potennn ll, threatens public health or the et
Any infi)rmation shall be provided orally within 24 hours f ont ilia tune the 1?e ttaittee hectatate avant eaf the eire
provided within 5 days o: the tithe the pene nittee becomes aware of thcatcttt slancas.
I the fa oil it .' 3+.: no tli.ontt" i6ant, please attach a list of .cort"4etive: actions being t:i kkm nYtnkd n°l t96}tL'-table for t2Y'B"YY`l'3vernotts to be Made a.S. r4qu➢r
the NPDLS permit,
:'Su titiat Signature;"** Angela S f3roo•n E-Mail:ashrcrwn%cmarathonpetraleunt.com Phone #:4t9-421- ( 9 Date
Address: 8035 Muunt Holly°Rd Paw Creek N(. 2$130 Permit Expiration Date 06/30'2.(120
penalty r, t taw, that this document attd all attachments were prepared under in direction or supervision in accordancc:vatlt a s5° tnna tis stet±ad
10 assure that qualified psi sonnei properly gather and evaluate the information submitted, I3a ed on my inquiry of the person or persons who managed Mc
system. or those persons directly responsible for gathering the infarnialirm, the infurmation submitted is, to the hest of my knowledge and belief, true,
accurate„ and complete. 1 to a9,,arc that there itre signihci nt penalties for submitting Fafse sattt t ttatit rs, ittelttding the possibility of fines and imprisonment for
knobe°in
CAR NAME; Peicr Araly a=.tl Svrvice,. €nw.
CERTIFIED LA R 1:
PERSC)N(s) COLLECTI" SAMPLES: 1 Qualfie
Parameter Code ass
Use only eint
* Nu Flow/Discharge Pta.-an Site: Check this box it no discharge occurs and, as a result, there are no data to be entered for all of tile parameters on the t)1 1R
for entire monitoring per+erd.
p" ORC on Site's: ORC must visit fa
"** Signature orPcrni 1 . if
t)5O 1hi'2)(I)),
n
RIFE
NP'UES Unit (9 i 9) SO7 (300 or lv v isilitrg itetftotpctrlai,at�c tar.org ek °' �* r p'ps�'rtpd
FOOTNOTES
designated in the reporting facility's
dper I50Nt.-0.
n delegation of the signatory aaiher3ty' must he on tile
to per 15A.. NC'w\C" 213

IDES PERMIT .;Nt
,FACILITY\ NAME:
OWNER NAME: Ntzl
GRADE:: 1
mMRPLR im as<A am
Report Comments:
TSS excociirdr +>
PERMIT vERSION:
G
CLASS; PC ,
ORC: m,g hT 3z m
OR ASCHANGED; No
VERSION: 1,0
PERMIT STw
COUNT V Meckienhua,
C CERT NUMBER; ice i

&Po b .PERMNt.. 0046213
EA C 11,1TVNAME.: c e. 2r &
OWNER NAME: Nipla T t w1 y
GRADE: ,
mvk! PERIOD: O-0yw¥2m
Outran A - Effluent c mm.m:
yAm
PERMITVERSION: G
CLASS: 1
OR .D @ Keith 7 %
OR HAS CHANGED: No
VERSION:,»
PERMIT STATq:6c
CO 1 w: Mee(
ORC CERTNUMBE ! q
a

Effluent Toxicity Repo
Form- Chronic Pass Fail and Acute LC50 Date 7%20/18
Pace r.naiytical- Marathon -
Facilitycha-lor_re Terminal- west NPDES#NC 0046213
Laboratory Performing Test ESC . Lab. Sciences
x
Operator in Responsible Charge
Signature of Labors ory Supervisor
Pipe #
County Mecklenburg
Comments
ESC Lab ID: L1007_817-01
MAIL ORIGINAL TO:
North Carolina Ceriodaphrria Chronic Pass/Fail Reproduction Toxicity Test
2 3 4 5 6 7 8 9 10
CONTROL ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
Control
D.O.
Treatment 2
1
2
4
2nd sample
s
t e t e t e
a n a n a n
r d r d r d
t t t
1st sample 1st sample 2nd sample
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates)
0
0
100
d
7
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh. North Carolina 27699-1621
11 12 Chronic Test Results
Calculated t
Tabular t
% Reduction
Avg. Reprod.
10 11 12
Control
Treatment 2
PASS FAI
%Mortality
Control
Treatment 2
Control CV
% control organ ;ms
Producing 3rd b ood
Collection (Start) Date (not applicable)
Sample 1 7 1 9/ 18 Sample 2 / I
Sample Type/Duration
Sample 1
Sample 2
Grab
grab
N/A
Comp.
Duration
N/A
Hardness(mg/i)
Spec.Cond.(pmhos)
Chlorine(mg/l)
Sample temp, at receipt
Concentration
Mortality
LC50= > 10 0 %
95% Confidence Limits
Method of Determination
Moving Average © Probit
Spearman Kerber © Other N/A
Organism Tested Pimephales promelas
Duration {hrs124 hrs
DWQ form AT-1 (3/37) rev. 11/95
sta
nd
pH
48.5
247 92.'7
28
1.4
NIA
N/A
N/A
Note: Please
Complete This
Section Also
start/end
D.O.

ESC
.... w,".s.4.�
Client: Pace - Marathon - Charlotte Terminal - West (Outfall 001)
NPDES #: NC0046213
Test Start Date:
Temperature (uC) - Pimephales promelas (fathead minnow)
Control
100
Time A
143 "
Day 1 (initiation)
Date: T 11- t
T
Day 2 (moming)
0
Time: An Cyst:
" Measurement taken directly in test chamber
Day
S" °C
Lab Sample
Thermometer Serial Number: 18050064
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH: Beckman 390pH/Temp/mV/ISE Meter
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chambers: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50.100 ft-c - SPER Scientific Light Meter 840021/Universal Enterprises Model DLM2
Photoperiod. 16 hours Tight, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific Isotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Shain W. Schmitt (SWS); Brandon Etheridge (BE); Stacy Kennedy (SK);
Amy Eggleston (AME); Adam Macomber (AM); Melissa Holwerda (MM); Cody Medley (CM); Jon Berry (JO)
Nadiar Yakob (NY); Kristen Rodgers (KR); Clarissa Moore (CGM); Keith Hargis (KH), Paige Brazzel (PB)

DAY
oow
25.9
25.9
J
21.5
24,5
21,6
24.6
12100'00-07/17/2018
12:00'00-07/17/2018
Chart Devices Used in
Thermo-K©ot Walk-in Incubat©f
DiCkS©n (small chart)
c5E' 7-3-1 B -Eo 7-! 7-1
Gr
Ch1
•°Ch2
-Ohl
q_.., Ch2
Cur,A Date
Cur,° Date
dirt, a -a
07/03/2018 12:00'00
07/17/2019 21 07
13 13:21' 07, 000
intv1.
2min.
_2min,
2min, 25.5
2min, 0000 25.6
Data uange 07/03/2D15
Ca1c.Range ©7/03r2013
25.3
25.4 'C
25.4 'C
6:24'07
6:24'07

ES
•
Client Pace -
Begin
End
Effluen
Percent
ACUTE TOXICITY TEST DATA - Pimephales promelas (fathead minnow)
athon - Charlotte Terminal - West (Outfall 001)
n Replicate
Position
CONTROL
CI
100
kBy
A:
D:
C:
D:
Biologist:
Time:
nitial Readings for
Undiluted Sample (100% effluent)
# OF LIVE Minnows
ors 24 hrs
10
10
10
10
10
10
10
10
Data divided by a sl<
Minnows were
Alkalinity
Chlorine (mgfL)
NPDES # NC0046213
Test Duration:
Dilution Water:
pH (std. units)
0 hrs 24 hrs
initial
eioiogist N
pH
final
-777
final
24 hours *end tes
10% DMW
Dissolved Oxygen (mglL) Conductivity (umhoslcm)
0 hrs 24 hrs 0 hrs 24 hrs
inittal
Biobgist(,t\(
final
final
initial
2-1
®loIogisti cN
Dissolved Oxygen Conductivity (umhoslcm) Analyst
h mark ( / ) indicates that a duplicate was run on that parameter. Temperature of water (minnow batch) at time of test initiation: c2 1
days old at test initiation and were taken from ESC Lot ft 0 Te.-':,) 1 g L!! Minnows were last fed
(Preliminary) Hardness
Analyst: .-1‘36°
Date:.?/Ic/ I
Time; L.,' I c.)
on
analyzed priorto
t initiation by Wet Lab
using;
LACHAT
r@
Hardness
final
final
gi
Time
hr
Total Cl2
(mg/L)
Control
< ©.2
Total Cl2 (myJL)
100% effluent
prior to the test.

U
V
J
Dates
Control Chart for June 2018 Acute C. dubia Reference Toxicant
CV% = 17
0.9
0
0,7
0.
0.
0.4
0.3
03/02/17
04/06/17
05/03/17
06/07/17
07/05/17
08/02/17
09/08/17
10/07/17
10/07/17
10/25/17
10/25/17
11/02/17
11/02/17
12/06/17
01 /03/ 18
02/07/18
03/07/18
04/04/18
05/02/18
06/19/18
Values
0.5486
0,7071
0.5946
0.4830
0.6164
0,5743
0.6515
0.4433
0,5196
0.6373
0.6830
0.4798
0.5402
0.6830
0.3693
0.7071
0.6429
0.4910
0.6156
0.7368
Mean
0,6279
0,6168
0,5833
0.5899
0.5873,
0.5965
0.5774
0.5709
0.5776
0,5872
0.5782
0.5753
0.5830
0.5687
0.5774
0,5812
0.5762
0.5783
0.5862
*ES
Date
-1 SD
0.5158
0,5352
0.4890
0.5069
0.5128
0,5242
0,4913
0.4881
0.4967
0.5042
0,4932
0.4932
0.4991
0.4708
0.4767
0.4824
0.4 780
0.4825
0.4864
-2 SO.
0.4037
0.4537
0.3946
0.4238
0.4382
0.4520
0.4052
0.4054
0.4159
0.4211
0.4082
0.4112
0.4151
0.3729
0.3760
0.3836
0.3799
0.3866
0.3866
0.7399
0.6983
0.6777
0,6730
0.6619
0.6688
0.6634
0.6537
0.6584
0.6702
0,6632
0,6573
0.6669
0.6666
0.6781
0.6800
0.6744
0.6741,
0.6860•
12065 Lebanon Rd
Mt, Juliet, TN 37122
[phone]
[phone] Fax
June 2018
Reference Toxicant Test
+2 SD
1 SD
-2 SD
+2 SD
0.8520
0.7799
0.7721
0.7561
0.7365
0,7410
0.7495
0.7365
0.7392
0.7532
0.7482
0.7394
0,7508
0.7645
0.7788
0,7788
0.7726
0,7700
0.7858

Dates
02/07/17
02/21/17
02/21/17
03/07/17
04/04/17
05/02/17
06/06/17
07/06/17
08/01/17
09/05/ 17,
10/10/17
11/07/17
12/05/17
01/10/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
06/19/18
Control Chart for June 2018 C. dubia Reference Toxicant
Values
0.0655
0.2476
0,2590
0.3150
0.2329
0.3693
0.1938
0.3988
0.3209
0.3382
0.2255
0.2558
0.2650
0.2944
0.3203
0.2956
0,2819
0.2879
0.2093
0,2882
0.1566
0.1907
0.2218
0.2240
0.2482
0.2404
0.2602
0.2670
0.2741
0.2697
0.2685
0.2683
0.2701
0,2735
0.2749
0.2753
0,2760
0.2725
0.2732
*ES
.....nlxrrary a ..;
Date
0,0278
0,0821
0.1135
0.1301
0.1454
0,1444
0.1551
0.1666
0,1768
0,1762
0.1793
0.1829
0.1878
0,1931
0.1970
0.1998
0.2027
0.1997
0.2023
-2 SD
0,0000
0,0000
0.0052
0.0362
0.0426
0.0483
0.0500
0.0662
0.0795
0.0828
0.0901
0,0975
0.1054
0.1127
0.1191
0,1244
0,1295
0.1269
0.1314
12065 Lebanon Rai
Mt. Juliet, TN 37122
SD
[phone]
[phone] Fax
June 2018
Reference Toxicant Test
0.2853
0.2993
0,3300
0.3179
0.3510
0.3365
0.3653
0.3674
0.3714
0.3631
0.3577
0.3537
0.3525
0.3539
0.3527
0.3507
0.3492
0.3452
0.3442_
+2 SD
SD
1
•1 SD
-2 SO
+2 SD
0.4141
0.4079
0.4383
0.4118
0.4539
0.4326
0,4705
0,4677
0.4687
0.4566
0.4469
0.4390
0,4348
0.4343
0,4306
0.4261
0.4224
0.4180
0.4151

u
Dates
Control Chart for June 2018 Acute Minnows Reference Toxic n
CV%= 11,4
1,3
1.
1.
0,9
0.8
0.
0.6
0,
0.4
06/07/17
07/05/17
08/02/17
09/08/17
10/07/17
10/07/17
10/25/17
10/25/17
11/02/17
11/02/17
12/06/17
01 /03/18
02/07/18
03/07/18
04/04/18
04/05/18
04/11/18
05/02/18
05/16/18
06/19/18
Values
0.7135
0.9415
0.6657
0.7387
0.7647
0.7917
0.8128
0.8858
0.9415
0.8785
0.8045
0.7917
0.6657
0.8196
0.7135
0.6892
0.6892
0.7647
0,6817
0.8842
can
0.8275
0,7736
0.7649
0.7648
0.7693
0.7755
0.7893
0.8062
0.8134
0.8126
0.8109
0.7997
0.8011
0.7953
0,7887
0.7828
0.7818
0.7765
0.7819
*ES
Date
-1 SD
0.6663
0.6262
0.6433
0.6595
0.6745
0.6874
0.6989
0.7076
0.7177
0.7217
0.7240
0.7073
0,7122
0.7067
0.6990
0.6927
0.6943
0.6885
0.6929
-2 SD
0,5051
0.4788
0.5217
0,5542
0.5797
0.5993
0.6085
0,6090
0.6219
0.6309
0,6372
0.6149
0,6233
0,6180
0,6094
0.6026
0.6068
0.6004
0,6038
+1 SO_
0.9887
0,9210
0.8864
0.8701
0.8641
0.8636
0.8797
0.9048
0.9092
0.9035
0.8977
0.8921
0.8901
0.8839
0.8783
0.8729
0,8693
0.8646
0.8710
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
June 2018
Reference Toxicant Test
+2 SD
1 SD
Mean
SD
2 SD
+2 S13
1.1499
1.0683
1.0080
0.9754
0,9589
0.9517
0.9701
1.0035
1.0050
0.9944
0.9846
0.9845
0.9790
0.9726
0.9680
0.9630
0.9568
0.9527
0,9600

Dates
12/06/16
01/10/17
02/14/17
03/07/17
04/04/17
05/16/17
06/06/17
07/11/17
08/01117
09/12/17
10/10/17
10/10/17
11/07/17
12/05(17
01/09/18
02/06/18
03/06/18
04/03/18
05/01/18
06/05/18
Control Chart for June 2018 Chronic Minnow Reference Toxicant
CV% = 11.8
Values
0.5573
0.4545
0.6743
0.6009
0.4926
0.5522
0.4925
0.4597
0.4685
0.5547
0.5459
0.6094
0.4694
0,5379
0,4941
0.4800
0.4562
0.5069
0.4335
0.5210
Mean
0.5059
0.5620
0,5718
0.5559
0.5553
0.5463
0.5355
0.5281
0,5307
0.5321
0.5385
0.5332
0,5336
0.5309
0.5277
0.5235
0.5226
0.5179
0.5181
,konstati.Y. "
Date
-1 SD
0.4332
0.4521
0.4799
0.4688
0,4774
0.4714
0.4596
0.4537
0.4601
0.4649
0.4707
0.4655
0.4685
0.4674
0.4651
0.4604
0.4613
0.4549
0.4567
-2 SD
0.3605
0.3421
0.3880
0.3818
0.3995
0.3964
0,3838
0.3793
0.3894
0.3977
0.4029
0.3978
0.4034
0.4039
0.4024
0.3973
0.3999
0.3918
0.3954
+1 Sp
0.5786
0,6720
0.6636
0.6430
0.6332
0.6213
0,6114
0,6025
0.6014
0.5993
0.6064
0.6009
0.5986
0.5945
0.5904
0.5867
0,5840
0.5810
0.5794
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
June 2018
Reference Toxicant Test
+2 SD
+1 SD
Mean
-1 SD
-2 SD
+2 SD
0.6513
0.7820
0.7555
0.7301
0.7111
0.6963
0.6872
0.6769
0,6720
0.6665
0.6742
0.6687
0.6637
0.6580
0.6531
0.6498
0.6453
0.6440
0.6408

Tuan fnrs
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USE ONLY

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Receipt F

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Center for resting 8 trowel:Won
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uly 16, 2018
R
POR I
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1007817
Samples Received: 07/10/2018
Project Number: 92391074
Description: CLT West Monthly NC0046213
Report To:
Matthew Brainard
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values, This test report shall not be
reproduced, except In full, without Witten aPProval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided In laboratory standard operating procedures: 060302, 060303, and 060304,
'19P4r4P141419944.9,,,,,,
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12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenotional.com

TABLE OF CONTENTS
ONE LAB* NATIONWIDE,
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr Sample Results
OUTFALL 001 GRAB L1007817-01
Qc: Quality Control Summary
Wet Chemistry by Method 130.1
Wet Chemistry by Method 310.2
GI: Glossary of Terms
Al: Accreditations & Locations 9
Sc: Sample Chain of Custody 10
2
3
4
5
5
6
6
7
8
4
Cn
Sr
Qc
7
GI
AI
ACCOUNT:
Pace Analytical - Huntersyille NC
Page 17 of 26
PROJECT: SDG: DATE/TIME: PAGE:
92391074 L1007817 07/16/18 13:28 2 of 11

SAMPLE SUMMARY
ONE LAB. NATIONWIDE.
OUTFALL 001 GRAB L1007817-01 WW
Collected by Collected date/time Received dateftime
07/09/1816:25 07/10/18 08:45
Method
Aquatic Toxidty by Method 2000
Wet Chemistry by Method 130.1
Wet Chemistry by Method 310.2
Batch Dilution Preparation Analysis Analyst
date/time date/time
WG1137074 1 07/10/1814:42 07/1011814:42 SWS
WG1136126 1 07/11/18 09:15 07/11/18 09:15 KK
WG1135869 1 07/11/1811:03 07/11/1811:03 KK
Tc
4Cn
5
Sr
GI
Al
9
Sc
ACCOUNT:
Pace Analytical - Huntersvllle, NC
Page 18 of 26
PROJECT: SW: DATE/TIME:„ PAGE:
92391074 L1007817 0746/18 13:28 3 of 11

CASE NARRATIVE
ONE LAB. NATIONWIDE, AO
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All radiochemical sample results for
solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet
weight was requested by the client. All Method and Batch Quality Control are within established
criteria except where addressed in this case narrative, a non-conformance form or properly qualified
within the sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
Nancy McLain
Project Manager
Project Narrative
Please review all information in this report for accuracy and completeness, Contact our office within ten days if there are any
questions,
Chronic Test Methods are described in "Short Term Methods for Estimating the Chronic Toxicity of Effluent and Receiving Waters
to Freshwater Organisms" (EPA/600/4-89/001).
The Biomonitoring results in this report are only a summary of the tests performed. A detailed report will follow. The detailed
report (not this summary sheet) must be submitted to the appropriate regulatory agency,
2
Tc
3
Ss
6
Qc
7
GI
a
Al
9
Sc
ACCOUNT:
Pace Analytical - Huntersville, NC
Page 19 of 26
PROJECT: SOG: DATE/TIME: PAGE:
92391074 L1007817 07/16/18 13:28 4 of 11

OUTFALL 001 GRAB
Collected date/time: 07/09/18 16:25
SAMPLE RESULTS - 01
L1007817
ONE LAB. NATIONWIDE.
Aquatic Toxicity by Method 2000
Analyte
24 Hour LC50 - Minno
Result Qualifier Analysis Batch
96 date / time
>100 (PASS) 07/10/201814:42 WG1137074
Wet Chemistry by Method 130.1
Result Qualifier RDL Dilution Analysis
Analyte ug/l ug/ date / time
Hardness (colorimetric) as CaCO3 35500 30000 1 07/1V2018 09:15
Wet Chemistry by Method 310.2
Batch
WG1136126
Result Qualifier RDL Dilution Analysis
Analyte ug/I ug/I date / time
ALK 27800 20000 1 07/11/201811:03
WG1135869
3
Ss
4
Cn
Qc
7GI
a
Al
9
SC
ACCOUNT:
Pace Analytical - Huntersville, NC
Page 20 of 26
PROJECT: SDG: DATE/TIME: PAGE:
92391074 L1007817 07/16/1813,28 5 of 11

WG113612g
Wet Chemistry by Method 130.1
QUALITY CONTROL SU
L1©©7817-01
ARY
ONE LAB, NATIONWIDE,.
Method Blank (MB)
24630-1 07/11118 0
Analyte
Hardness (colorimetric) as
CaCO3
MB Result MB Qualifier MB MDL MB RDL
ug/I ug/I ug/I
3420 J 1430
30000
L1008033-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1008033-02 07/11/18 09:24 • (DUP) R3324630-7 07/11/18 09:24
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Hardness (colorimetric) as 60100 55900 1 7.24 20
CaCO3
L1007757-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1007757-01 07111/18 09:31 • (DUP) R3324630-8 07/11/18 09:32
I Original Result DUP Result Dilution DUP RPD DUP Qualifier ©mits RPD
Analyte ug/I ugil % %
Hardness (color#metric) as 477000 479000 5 0.523 20
CaCO3
Laboratory Con rol Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3324630-2 07/11/18 09:02 • (I_D) R3324630-3 07/11/18 09:03
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec, limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte z ug/I ug/I ug4 % % % % %
Hardness (colorimetric) as 150000 148000 148000 98.7 98.7 85.0-115 0.000 20
CaCO3
L1007826-.03 Original Sample (OS) • Matrix Spike ( S) * Matrix Spike Duplicate (MSD)
(OS) L1007826-03 07f/11/18 09:18 • (MS) R3324630-5 07/11/18 09:19 • {MSD) R3324630-6 07/11/18 09:21
Spike Amount Original Result MS Result
Analyte t ug/I ug/t ugll
Hardness (colorimetric) as
CeCO3
MSD Result
ug/I
150000 168000 230000 231000
ACCOUNT:
Pace Ar}alyticel - Huntersville, NC
MS Rec. MSD Rec, Dilution Rec, Limits MS Qualifier MSD Qualifier RPD RPD Limits
41.3 42.0 1 80.0-120 E J6 E_J6 0,434 20
Ss
4Cn
Sr
7
GI
Page 21 of 26
PROJECT: SDG: DATE/TIME: PAGE:
92391074 L1007817 07/16/1813:28 6 of 11
a
Al
Sc

WG113586
Wet Chemistry by ttethod 310,2
QUALITY CONTROL SUMMARY
1.1007817-01
ONE LAB, NATIONWIDE„
Method Blank (MB)
O7
Analyte
ALK
0:42
MB Result
ug/1
u
MB Qualifier MB MDL
ug/1
MB RDL
ug/I
20000
L1006655-01 ©rginal Sample (©S) • Duplicate (DUP)
(OS) L1006655-01 07111/1810:46 • (DUP) R3324687-4 07/11/18 10:47
original Result DUP Result Dilution DUP RPD DUP Qualifie
Analyte
ALK
ug/I ug/I
45300 43400
4.28
L1007826-01 ©r ginal Sample (OS) • Duplicate (DUP)
DUP RPD
Limits
20
(OS) L1007826-01 07/11/1811:06 • (DUP) R3324687-5 07/11/1811:07
I Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
ALK i 130000 129000 1 0,772 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3324687-2 07%11/18 10:43 • (LCSD) R3324687-3 07/11/18 10;44
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec, Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I % % % % %
ALK 200000 199000 200000 99,5 100 85.0-115 0.501 20
L1007826-03 Original Sample (©S) • Matrix Spike (MS) • Matrix Spike Dupli
D)
(OS) L1007826-03 07/11/18 11:09 • (MS) R3324687-6 07/11/18 1110 • (MSD) R3324687-7 07/11/18 11:11
Spike Amount original Result MS Result MSD Result MS Rec, MSD Rec, Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ugh % % % % %
ALK 100000 246000 315000 315000 69.0 69.0 1 80.0-120 E J6 E J6 0.000 20
4
Cn
5Sr
7GI
3
Al
Page 22 of 26
ACCOUNT: PROJECT; SDG: DATE/TIME: PAGE:
Pace An lyticel - Huntersville, NC 92391074 L1007817 07/16/18 13:28 7 of 11
Sc

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE,
MDL Method Detection Limit,
RDL Reported Detection Limit,
Rec. Recovery.
RPD Relative Percent Difference,
SDG Sample Delivery Group,
U Not detected at the Reporting Limit (or MDL where applicable).
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis, If a value different than 1 is used in this field, the
result reported has already been corrected for this factor,
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample, The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte,
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples, These analyses are not
being performed on your samples typically, but on laboratory generated material,
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform, This
Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples, These results are provided
Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
Analyte
Dilution
Quality Control
Summary (Qc)
Sample Summary (Ss)
Qualifier Description
E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J The identification of the analyte is acceptable„ the reported value is an estimate,
J6 The sample matrix Interfered with the ability to make any accurate determination: spike value is low.
z
Tc
3
SS
4
Cn
8
Al
Sc
Page 23 of 26
PROJECT: SDG DATE/TIME: PAGE:
92391074 L1007817 07/16/1813:28 8 of 11
ACCOUNT:
Pace Analytical - Huntersville, NC

ACCREDITATIONS & LOCATIONS
ONE LAB, NATIONWIDE,
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location, One phone call, one point of contact, one laboratory. No other lab Is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our Industry. The most significant benefit to our one location design is the design of our laboratory campus, The model Is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample Integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
• Not all certifications held by the laboratory are applicable to the results reported in the attached report,
"Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace NationaL
State Accreditations
Alabama
Alaska
Arizona
Arkansas
California
Colorado
Connecticut
Florida
Georgia
Georgia
Idaho
Illinois
Indiana
lows
Kansas
Kentucky1°
Kentucky 2
Louisiana
Louisiana
Maine
Maryland
Massachusetts
Michigan
sots
Montana
40660 Nebraska NE-OS-15-05
17-026 Nevada TN-03-2002.34
AZ0612 New Hampshire 2975
88-0469 New Jersey-NELAP TN002
2932 New Mexico' n/a
TN00003 New York 11742
PH-0197 North Carolina Env375
E87487 North Carolina' OW21704
NELAP North Carolina' 41
923 North Dakota R-140
TN00003 Ohio-VAP CL0069
200008 Oklahoma 9915
C-TN-01 Oregon TN200002
364 Pennsylvania 68-02979
E-10277 Rhode Island LA000356
90010 South Carolina 84004
16 South Dakota n/a
A130792 Tennessee " 2006
LA180010 Texas T 104704245.17-14
TN0002 Texas' LA80152
324 Utah TN00003
M-TN003 Vermont VT2006
9958 Virginia 460132
047-999-395 Washington C847
TN00003 West Virginia 233
340 Wisconsin 9980939910
CERT0086 Wyoming A2LA
Third Party Federal Accreditations
A2LA 1S017025 1461.01
A2LA - ISO 170255 1461.02
Canada 1461,01
EPA-Crypto TN00003
AIHA-LAP,LLC EMLAP 100789
DOD 1461,01
USDA P330-15-00234
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ' Chemical/Microbiological ' Mold ° Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies, rf you would like assistance from one of our support offices, please contact
our main office, Pace National performs all testing at our central laboratory.
Tc
4
n
7
GI
9
SC
ACCOUNT:
Pace Analytical - Huntersviile, NC
PROJECT:
92391074
SDG:
11007817
DATE/TIME:
07/16/1813:28
Page 24 of 26
PAGE:
9 of 11

Cooler Received/Opened Om 7
RIpt Check List
COC Seal Present / Inta
,CO fired Accur
ttlles save Meet?
C
r cb t ?
u lent atu a sent?

Prir NPDES PERMIT NO,: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mr)lx Terminals LIC
GRADE: PC-1
eDMR PERIOD: 06-2018 (June 2018)
44
4,
44 'I91
240 clerk
SAMPLING LOC,
Ilra 241711 aloe,
91
0
OR( On Siter'.
VON
PERMIT V'ERS ON: 4.0
CLASS: PC-1
RECEIV
PERMIT STATUS: Active
NTY: Mecklenburg
y Lee Swick
JUL 2 0 "ZU1!?RC CERT NUMBER: 991168
ORC: Terr
RECEIVED/NCIDENR/OWR
CEN I kAL F!L
DWR SECTI0T1 ATus: Processed
ORC HAS CHANGED: No
VERSION:
TION: EFFLUENT DISCHARGE NO.: 001 NO DIS
No Reporting Regyze..*
See Permit
FLOW
CO5311
Monthly
Grab
TSS = Cane
Monthly
Grab
8.T.NZLNE
130
00856
Nlonthly
Grab
011.4.6144E
,12740
Monthly
Grab
PIARN,TR
- GIONAL OFFICE
801170
Monlhly
Grab
181148114111
4
1525
7
9
141
12
44
44
.25
100
9,8
0,013
9,8
44,
44,
17
18
44
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21
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21
24
24
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47
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29
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Monthly Average,
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290110
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9.8
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9.8
448
Rally Mininnow
1000
9,8
0
0.013
Reposing Reason: ENFRLISE 33 No Elow-ReusetRecycle; ENVWTHR = No Visitation — Adverse Weather; is'OrLOW 33 No Flow; HOLIDAY 33 No Visitation — Holiday
9.8

NPDES PERMIT NO.: NC00462 1 3
FACILITY NAME:Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 06-2018 (June 2018)
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: Terry
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: 41
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991 168
STATUS: Processed
21278 SUBMISSION DATE; 07/13/2018
Swick [e-mail] Phone #:[phone]
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
07/10/2018
Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment,
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II,E.6 of
the NPDES permit.
Su
07/13/2018
ure: Angela S Brown E-Mail:asbrown@marathonpetroleum,eom Phone #:419-42I-2629 Date
Permittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the infonnation submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Pace AnaMe
CERTIFIED LAB #:
CERTIFIED LABORATORIES
PERSON(a) COLLECTING SAMPLES: J
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portalmcdenrorg/web/wq/swpips/npdes/forms,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility arid document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2XD).

PERMIT NO.: NC0046213
A LITV NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 05-2018 (May 2018)
2
3
4
5
6
7
9
10
11
12
13
14
15
16
17
—,„
PERMI"f STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: .
WY
STATUS: Processed
N, 'ENR/DWR
WQROS
MOORESVILLE REGIONAL OFFICE
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
1)
8
240 dock Ors 24110 'dock
0900
0800
peratm. Tine On Site
.25
.25
VAIN
v
30
PERMIT VERSION: 4.0.
R E-,
CLASS: PC-1
ORC: Terry Lee Swick JUN 2 8 ?.018
ORC HAS CHANGED: „
VERSION: 1.0 LVV2 CTiOf'i
500511
Site Permit
culttled
FLOW
0.006
0209
C0530
Mornitly
Grab
VS'S - Calle
mgil
16,7
34030
Monthly
Grab
BENZENE
< 2
00556
Moral-11y
Grab
011,GRSE.
mg.11
5
32730
Monthly
Grab
POEN, TR
tnr
< 0.01
00070
Monthly
Grab
T1321111AN
ntu
34.5
(0
19
20
21
22
23
25
26
27
20
29
30
31
0900
09,30
101.10
.25
.25
25
0,139
.32124
Monthly Average Limit*
Monthly Avougin
Daily Minimum
Daily Minimum:
0,11a5
1/.1 126
0.209
0,006
30
16,7
16.7
16,7
0
0
I)
0
0
0
0
**** No Reporting Reason: ENFRUSE No Flovv-ReuseRecyele; LiNVWTHR — No Visitation -- Adverse Weather, NOELOW No Flovv; HOLIDAY No Visitation - Holiday
34,5
34.5
34,5

MIT NO.: N1462d
FACILITY NAME: Charlotte Teraina)
OWNER. NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 05-2018 (A+lay 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: PC
ORC; Teny 1.ce Swick
ORC HAS CHANGED: Nat
VERSION: l .©
CONTACT PHONE N: 419421297
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: 06/21/2018
ORC/Certifier Signature: Terry L. Swick E-Mail:tlswick@marathonmctrolcunt,com Phone #:[phone]
By this signature,
eport is accurate and complete to the best of my knowledge.
6
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that poteattially t)treatens public health or the environ
Any information shall be provided orally within 24 hours from the time the permittee became aware attic circumstances, A written
provided within 5 days of the time the per mittee 'becomes aware of the circumstances.
lithe facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part tLE.6 of
the NPDES permit.
2018
Dale
omission shall also be
06/1/2018
/Submilr Signature:*** Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address:
Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
rd
system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly rcponsible for gathering the information,; the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Pace Ana
CERTIFIED LAB 0:
PERSON(s) COLLECTING SAMPLES: ) Q
PARAMETER CODES
ay be obtained by calling the 'NPDES Unit [phone] or by visiting http://portal,n
enr.org/web/wq/swp/psinpdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
*• ORC on Site?: ORC must visit facility and document visitation o facility as required per I5A NCAC 8G .0204,
*** Signature of Pennittee: If signed by other than the permitt
.0506(bX2)(D).
delegation of the signatory authority must be on file with the state per 15A NCAC 2B

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 04-2018 (April 2018)
PERMIT VERSION: 4.0
CLASS: PC -I
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
MAY 2
PERMIT STATUS: Active
Mecklenburg
ORC CERT NUMBER;„„
ocessed
ED/NCDENRJDWR
WQROS
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCIIARISIOViiMoNAL OFFICE
�
�y
e;
Fw
8
�
4
,�
�
p
c
�
a
50050
C0530
34030
34371
TA1,6C
22417
34696
09556
32730
See t'exrnit
i4funthiy
Monthly
Quarterly
Quarterly
Quarterly
ivf[sntktiy
Monthly
Calculated
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
FLOW
TSS - Carr
HEKLE5T:
ETUYLBE5
9T21D24AC
MBE
11AFTIiAL11
01241RSE
PIMEA,TR
2400 clock
Hrs
2400 clock
llrs
1011012
gpd
mgfl
A4y,+`1
nil
percent
ugil
u8/l
ntgll
Itl 3
4
7
10
II
12
.1500
_25
y
I0(0)
9.4
< I
s 100
a I
2 0,01
13
14
15
16
090£1
25
y
1,77000
17
18
19
28
21
22
23
34
25e
0930
.25
y
2280i)0
29
27
20
19
30
Monthly Average Limit:
JO
Monthly A verkael
135333.33333
44
0
0
I04)
0
U
0
0
Daily llaalm um:
228000
9,4
0
0
100
0
0
0
0
Daily Miuimmns
I000
9.4
Il
0
l(40
0
0
0
0
**** No Reporting Reason: ENFRUSE-=No Flow-ReuculRecycle; ENVWTHR No Visitation - -Adverse Weather; 'NOFLOW No Flow; HOLIDAY=, No Visitation-- Holiday

NPDES PERMIT" NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 04-2018 {April 2018)
4
7
1b
11
12
1S
14
13
16
17
1S
19
29
21
22
23
14
29
26
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2409 clock
Ws 2400 clack
1500
11900
0930
;25
25
.25
17111N
y
34919
Quarterly
Grab
TOLUENE
<1
00679
Monthly
Grab
T171101DTE
Mu
3.6
01551
Quarterly
Grab
owl
<t
27
2S
29
Monthly Average 66,4 t
Monthly Atorage:
0
3.6
0
Daily Minimum:
3.6
3.6
0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR No Visitati
Adverse Weather; NOFLOW ** No Flow; HOLIDAY No Visi
clliday

NPDES PERMIT NO.: N
FACILITY NAME: Charlene Terminal
OWNER NAME: Mp1x Terrain aIs LLC
GRADE: PC-1
eDMR PERIOBi:0472015 (April 2018)
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: Terry L.
PERMIT VERSION: d,0
CLASS: PC-1
ORC: Terry Lee Sw%k
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE t/t 419421 +97
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE:05/15/2018
k E-Mail:[e-mail] Phone if:704-392-1345
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any nonco
Date
y threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances,
lithe facility is noncompliant, please attach a list of corrective actions being taken and a titne•tab)e for tmprovernnis to be made as squired by part II.E.6 of
the NP1ES permit..
ture:*** Angela S Brown E-Mail:[e-mail] Phon
rmittee Address: 80.3S Mount }lolly Rd Paw Creek NC 28130 Permit Expiration Date: 06/3012020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in ace
05/15/2018
#:419-421-2629 Date
igned
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Pace Analytical Services Inc.
CERTIFIED LAtt k:
PERSON(*) COLLECTING SAMPLES:
Parameter Code assist
CERTIFIED LABORATORIES
PARAMETER. CODES
obtained by calling the NPDES Unit [phone] or by vi
ttp://portal.ncdenr.org/web/wq/s
p
fo
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to he entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC SG _0204.
***Signature of Perms tee: If signed by other than the permittee, then delegati
.0506(b)(2)(D).
he signatory authority must be on file with the state per I5A NCAC 2B

NPDES PER_MIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 04-2018 (April 2018)
Outfall 001 - Effluent Comments:
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.(
The analytical for Acute Toxicity (Parameter code FTHD24AC) is being submitted with the hardcopy DMR,
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed

Effluent Toxic
Repo
Form- Chronic Pass/Fail and Acute LC50 Date-4/18/1
Pace AnatytI caT= Marathon -
Facilityrhar]otte Terminal -.west NPDES#NC 0046213
Laboratory Performing Test ESC Lab Sciences
x
Signet a of ©p r in Res nsible Charge
��C-r7-i8
Signature of Laboratory Supervisor
Pipe #
County Mecklenburg
Comments
ESC Lab ID: L98S432-01
MAIL ORIGINAL TO:
North Carolina Ceriodaphrlia Chronic Pas Fail Reproduction Toxicity Test
CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10
# Young Produced
Adult (L )ive (D )ead
Effluent%
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L )ive (D )ead
Control
pH
Treatment 2
sample
Control
D.O.
Treatment 2
1st sample
2
4
1st sepie 2nd sample
s
e t e
a n
d r d
2nd sample
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replic
©%
100
tes
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleighl North Carolina 27699-1621
11 12
10 11 12
Chronic Test Results
Calculated t
Tabular t
% Reduction
%Mortality
Control
Treatment 2
Control CV
Complete This For Either Test
Avg.Reprod.
Control
Treatment 2
Test Start Date
4/ 13 / 18
Collection (Start) Date (not applicable)
sample.' 4 / li / 18 Sample 2 / /
Sample Type/Duration
Sample 1
Sample 2
Grab,
grab
N/A
Comp.
Duration
N✓A
Hardness(mg/1
Spec.Cond.(pmho
Chlorine(mg
Sample temp. at receipt
Concentration
Mortality
LC50= > 1©© %
95% Confidence Limits
ivtethod of Determination
Moving Average © Probit
Spearman Karber © Other N/A
Organism Tested Pimephal,es promelas
Duration (hrs) 24 hrs
DWQ form AT-1 (3/87) rev. 11/95
sta
nd
pH
A
Note: Please
Complete This
Section Also
start/end
ontro
High
Conc.
D.O.
1 of 11

»ESC
Client: Pace - Marathon - Charlotte Terminal - West
NPDES #: NC0046213
Test Start Date: -1
Temperature (°C) - Pimephales promelas (fathead minnow)
Control
100
©ate:
Time:
50
Analy
Day 1 (Initiation
•- Meese
oc
J °C
Ti
A
Day 2 (morning)
nt taken directly in test chamber
Day 2 (final)
°
Thermometer Serial Number: 18050064
Lab Sample #: L
Instruments and Methods Used for Acute/Chronic Biomonitoring Analysis
Dissolved Oxygen: YSI 5000 DO Meter/Probe (serial #01L0435)
pH; Beckman 390pH/Temp/mV/ISE Meter
pH/RDO/Conductivity: Thermo Scientific Orion VersaStar (serial #V 02105)
Temperature: Thermometers calibrated to NIST certified thermometer
Conductivity: Thermo Orion Model 150A+
Alkalinity: Lachat
Hardness (Wet Lab): Lachat
Total Residual Chlorine: Hach Pocket Colorimeter, Model #46770-00 (serial #971000112186)
Environmental Chambers: 25 degrees C + 1.0 degree - Thermo-Kool
Light Quality: Ambient Lab Illumination
Light Intensity: 50-100 ft-c - SPER Scientific Light Meter 840021/Universal Enterprises Model DLM2
Photoperiod: 16 hours light, 8 hours dark
Drying: Overnight at >60 degrees Celsius in a Fisher Scientific Isotemp Oven, Model 655F
Mean Dry Weight: Determined using Mettler Toledo Balance, AT261 Delta Range
Reference Weights (Set #1): Class 1, TREOMNER, Inc., serial number 85035
Reference Weights (Set #2): Class 1, TREOMNER, Inc., serial number 67812
EPA Acute Manual Edition and Date: EPA-821-02-012 October 2002, Fifth Edition
EPA Chronic Manual Edition and Date: EPA-821-R-02-013 October 2002, Fourth Edition
Tests are performed only by Assistant Biologists, Biologists, and Senior Biologists that have experience with
aquatic toxicity testing. Laboratory Technicians will not handle test organisms during a toxicity evaluation. The
following analysts have met Technical Training Qualifications and their initials (in parenthesis) can be found on the
benchsheets in this report: Shain W. Schmitt (SWS); Brandon Etheridge (BE); Stacy Kennedy (SK);
Amy Eggleston (AME); Adam Macomber (AM); Melissa Holwerda (MM); Cody Medley (CM); Jon Berry (JB)
Nadiar Yakob (NY); Kristen Rodgers (KR); Clarissa Moore (CGM); Keith Hargis (KH), Paige Brazzel (PB)
2of11

Thar..
Chl
Ch2
Cur.A pate : 04/08/2018 21:18'55
Cu.r.8 ©ate : 04/17/2013 13:39'47
dlff. A-B : 8 16:20'52.000
I-© 9 _17-Irk
Chart Devices Used in
Thermo-Kool Watk-in Incubator:
Dickson (small chart)
P
_min. 8000 -----
2min. 8000
Cu
2 43
gh c4 Avg, Uni
25,6 24.1 25„. °C
25:8 24.1 25,1 °C
Data Range 04/08/2018 21:13'55-04/17/2013 13:39'47
Ca1c.Range 04/08/2010 22:32'50-04/18/2018 1:11'1.1
3of11

Minnows were
Control
LAC HAT
AI l$ Hnity
0
ACUTE TOXICITY TEST DATA - Pimephales promelas (fathead minnow)
Client Pace - Marathon - Charlotte Te
Begin
End
Effluent in Replicate
Percent (%) Position
CONTROL
1©©
Checked By;
C:
D:
A:
Biologist:
Time:
0 hrs
10
10
10
10
10
10
10
10
Initial Readings for
Undiluted Sample (100% effluent)
Time
nal - West
u
# OF LIVE Minnows
24 hrs
12:i7
Chlorine (m9/L)
•pH (std. units)
0 hrs 24 hrs
pH
Initlat
initial
NPDES # NC0046213
Test Duration:
Dilution Water:
final
final
24 hours
10% DMW
end test +/- 1 hr from start time
Dissolved Oxygen (mglL) Conductivity (umhostcm)
0 hrs 24 hrs 0 hrs 24 hrs
initial
initial
final
final
Dissolved oxygen Conductivity (umhos/cm
initial
initial
Analyst
final
final
Time
Data divided by a slash mark (1) indicates that a duplicate was run an that parameter. Temperature of water (minnow batch) at time of test initiation: i. °C
. Minnows were last fed i / 3 / 1 @ 07 .37 prior to the test.
days old at test initiation and were taken from ESC Lot #
m&�
100% Effluent
LACHAT
2. 5
mglL
(Preliminary) Hardness
Analyst:
Date: 1 1 -
Time: 11,54
Total Cl2
(mglL)
Control
< ©.2
cud C12 (mg/L)
100% affluent
analyzed prior to
t initiation by Wet
LEA:
Hardnes

Control Chart for April 2018 (4-4-18) Acute C.dubia Reference Toxicant
Dates
01/04/17
02/16/17
03/02/17
04/06/17
05/03/17
06/07/17
07/05/17
08/02/17
09/08/17
10/07/17
10/07/17
10/25/17
10/25/17
11/02/17
11/02/17
12/06/17
01 /03/ 18
02/07/18
03/07/18
04/04/18
Values
0.6830
0.4579
0.5486
0.7071
0,5946
0.4830
0.6164
0.5743
0,6515
0.4433
©.5196
0.6373
0.6830
0.4798
0.5402
0.6830
0.3693
0.7071
0.6429.
0.4910_
Mean
*ES
A.„:371:CaEti7-
..00tor - $.
0.5705
0.5632
0.5992
0.5982
0.5790
0.5844
0.5831
0.5907
0.5760
0.5708
0.5764
0.5846
0.5771
0.5746
0.5814
0.5689
0,5766
0.5801
0.5756
"date"
-1 SD.
0,4113
0,4499
0.4820
0.4968
0.4768
0.4900
0.4956
0.5058
0.4833
0.4813
0.4889
0.4958
0.4873
0.4876
0.4930
0.4691
0.4744
0.4796
0.4758
-2 SD
0.2521
0.3367
0.3648
0.3953
0.3745
0.3956
0.4082
0.4208
0.3907
0.3918
0.4014
0.4069
0.3974
0.4005
0.4046
0.3692
0.3722
0.3792
0.3760
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
April 2018
Reference Toxicant Test
0.7296
0.6764
0.7163
0.6997
0.6813
0.6788
0.6706
0.6756
0.6686
0.6604
0.6639
0.6734
0.6669
0.6617
0.6698
0.6688
0.6788
0.6806
0.6754.
+ SD
+1 SD
Mean
-1 SD
-2 SD
+2 SO
0.8888
0.7897
0.8335
0.8012
0.7835
0.7732
0.7581
0.7606
0.7613
0.7499
0.7514
0.7623
0.7568
0.7488
0.7582
0.7686
0.7810
0.7810
0.7753
5 of 11

U10417
O1/11n7
O1/11/17
0207/17
O2/21/17
D2/21/17
83/0717
0404/17
0502/17
O00O17
070#/17
O801/17
0905/17
10U017
1107Y17
12/D5/17
O1/10V1O
02106118
0306/18
04/03/18
0.3010
03063
0.2401
0.2464
0.2485
0.258O
8.%549
U67O
0.2602
0.2728
0,2768
01815
0.2775
0.2761
0.2754
O.27M5r
0.2798
Control Chart for April 201WChronic C.dub|eReference Toxicant
Values
OA09
0.1921
0,3169
O�0855
0.2476
0,2590
0.3150
0,2329
03693
U.1Q3@
0,3988
0,3209
03382
01255
0.2558
0.2650
02944
O'82O3
0.2956
02819
*ES
SD
�
0.1470
0,1970
0.0962
01166
0.1323
0.1490
0.1536�
8.1854
01611
0.1699
0,1777
O1858
0,1837
0,1855
0.1879
0.1916
0.1960
(l1Q81
0.20,13
1-12 S D,
.
0.0000
OD878
010000
0,0000
0.0161
0,0400
O.85%3
0.0633
0,0620
O.O87O
0,0787
O.QR8V
0,0900
0.0950
0.1003
01068
D�1130
01183
01228
l2065Lebanon Rd
I\It, Juliet, TIN 37122
[phone]
(6l5)758-5059Fax
April
*�mN��"� ��
��������N �N����L��v
~ ~�=�"w ~~.�=�~��
Ni*����~�� -�~�N����
m���m��.~���~w�� mn���m��m�wwm. mesw.
0.4549
0,4155
0.3959
0.3701
0,3647
0.3670
03561
0.3697
0.3593
0.3757
0.3759
0.3779
0.3713
0.3666
03629
0.3614
0.3619
0.3605
O'%585
0�6088
0,5247
0.5457
(l5O58
OA808
0,4760
0.4574
0.4719
0.4584
0,4785
0.4749
OA742
0.4651
0.4572
0.4504
0.4462
0.4449
0,4413
0.4371

Control Chart for April 2018 (4-4-18) Acute Minnow Reference Toxicant
03/02/17
04/06/17
04/13/17
04/28/17
05/03/17
06/07/17
07/05/17
08/02/17
09/08/17
10/07/17
10/07/17
10/25/17
10/25/17
11/02/17
11/02/17
12/06/17
01/03/18
02/07/18
03/07/18
04/04/18
Values
0,7387
0.7647
0.6284
0,8024
0.6657
0.7135
0.9415
0.6657
0.7387
0.7647
0.7917
0.8128
0,8858
0.9415
0.8785
0.8045
0.7917
0.6657
0.8196
0.7135_
Mean
0.7517
0,7106
0.7335
0,7200
0.7189,
0.7507
0.7401
0.7399
0.7424
0,7469
0.7524
0.7626
0.7754
0.7823
0.7837
0.7841
0.7776
0.7798
0.7765
*ES
44.040.4' „ titkVA.*
date
..1 SD
0.7333
0,6382
0,6587
0.6484
0.6548
0.6482
0.6406
0.6468
0.6543
0.6620
0.6692
0.6748
0.6785
0.6851
0.6897
0.6931
0.6849
0.6892
0.6871
-2 SD
0.7149
0.5658
0.5839
0.5769
0.5908
0.5458
0.5411
0.5538
0.5662
0.5771
0.5861
0.5870
0.5815
0.5880
0.5956
0.6020
0.5923
0.5987
0,5977
+1 SD
12065 Lebanon Rd
Mt, Juliet, TN 37122
(615) '773-7549
[phone] Fax
April 2018
Reference Toxicant Test
0.7701
0,7830
0.8084
0.7915
0.7830
0.8532
0.8396
0.8330
0,8305
0,8318
0.8355
0,8504
0.8724
0.8794
0.8777
0.8752.
0.8702
0.8703
0.8658
+2 SD
+1 SO
Mean
-1 SD
-2 SO
+2 SO
0.7885
0.8553
0.8832
0.8631
0.8470
0.9556
0.9391
0,9261
0.9186
0.9167
0.9187
0.9382
0.9693
0.9766
0.9717
0.9662
0.9628
0.9609
0.9552
7 of 11

Control Chart for April 2018(4-5~ 8)Acuha0Ninnow Reference Toxicant
O40O/17
04/13/17
04/28/17
0503117
0607/17
0/05117
O80217
090@K17
10U7/17
10Q7Y17
1025/17
l0t25/17
1102/7
1102/17
13/00/17
O10J/8
O20718
03/07/1O
0404118
0405/18
U�7G47
0.0284
0,8024
O.OS57
01135
O.9415
0.6657
0.7387
0.7647
0.7917
0.8128
0.8858
0,9415
0.8785
UO45
0.7917
0,6657
0.8196
0,7135
D.O8&2
0,6965
03318
03153
0.7149
0.7527
03403
0.7401
07428
0.7477
0.7536
Q-764O
0.7782
0.7854
0,7867
03870
03799
8.7821
0.7785
*ES
0.6001
0,6403
00336
0.6441,
0.6406
0.6328
O.O40@
0.6494
0.6583
O.0065
0.GT32
0.8770
0,6854
0.6902
Q.G937
0.8848
0.6895
O.8871
O�5O38
Q.5487
0,5518
0.5734
0.5285
0.5253
0.5411
O�5550
0.5688
0.5794
0.5819
0,5776
0.5853
0.5936
0.6005
0.5899
0.5Q6&
0.5957
O.5017
-
l2O85Lebanon 86
%It, Juliet, TN 3712Z
(615)78-7549
(6l5)758-5859Fax
A �� w�u��4N ��
=
��U��� ~��U��
mn��m������°~*`� �����°�~=�~°~~ Test
0.7929
0.8234
0.7970
0.7857
0.BG40
OS477
0.8396
0.8362
0.8371
0.8407
U�8508
V�8708
0,8854
03832
U'88V2
8.8748
0,8747
0.8698
0,8661
0.8893
0.9149
0.8788
0.8565
0.9769
0.9552
0.9381
0.9297
0.9266
0.9278
0,9474
O.S788
0.9855
0.9797
0.9735
0.9098
0,9673
V.8612

en
C.)
Dates
10/05/16
11/01/16
12/06/16
01/10/17
02/14/17
03/07/17
04/04/17
05/16/17
06/06/17
07/11/17
08/01/17
09/12/17
10/10/17
10/10/17
11/07/17
12/05/17
01/09/18
02/06/18
03/06/18
04/03/18
Control Chart for April 2018 Chronic Minnow Reference Toxicant
Values
0.5498
0.5297
0,5573
0.4545
0.6743
0,6009
0.4926
0.5522
0.4925
0.4597
0.4685
0.5547
0.5459
0.6094
0.4694
0.5379
0,4941
0.4800
0.4562
0.5069
Mean
0.5398
0,5456
0.5228
0.5531
0.5611
0.5513
0,5514
0.5449
0.5364
0,5302
0.5322
0.5333
0.5387
0.5341
0.5343
0.5320
0.5291
0.5252
0.5243_
*ES
date
-1 w
0.5255
0.5313
0.4758
0,4741
0,4877
0 4795
0.4850
0.4797
0.4692
0.4633
0,4681
0.4717
0.4762
0,4712
0.4736
0.4724
0.4700
0 4654
0 4660
-2 SD
0.5113
0.5171
0.4288
0.3950
0.4144
0.4078
0.4185
0,4145
0,4021
0.3965
0.4039
0.4102
0.4137
0.4084
0.4129
0.4128
0.4109
0.4056
0.4076
12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
[phone] Fax
April 2018
Reference Toxicant Test
0.5540
0.5599
0.5698
0.6322
0.6344
0.6231
0.6179
0.6101
0.6035
0.5970
0.5964
0.5948
0.6012
0.5969
0.5951
0.5916
0.5882
0.5851
0.5827_
+2 SD
+1 SD
Mean
-1 SD
-2 SD
+2 SD
0.5682
0.5741
0.6169
0.7112
0.7078
0.6948
0.6843
0.6752
0.6706
0.6639
0.6605
0.6563
0.6638
0.6598
0.6558
0.6512
0,6473
0.6449
0.6411
9 of 11

Chain of Custody - .�.
Ave, Suite 100
Hurdc rsvifte, NC 28078
Phone [phone]
i5�n il: rr attr7ewbr°:aimardi
f {rc.r ttx�. Apt 12, 201 e 4.45 41 'M
CLT- West T €in
G109
ALL-C'-O 2rew.Q0 24March2,
LAB USE; ONLY

ESC 1 B SCIENCES
Cooler Form
,wd On: 41
ecetpt Check list
COC Seal Present / I, tct
NP
Yes No
COC Signed / Accurat
Bottles arrive intact?
!Correct battles used?
Sufficient volume sent?
If Applicable
VOA Zero hedspace
Prese' ion Correct C:fte k d

Laboratory receiving samples:
Asheville © Ede
Courier:
C Commercial
Client Name:
Document Name:
Sample Condition Upon Recelpt(SCUtil
Document No.:
F-CAR-05-033-Rev.06
Hunte rsvlll
Project
Ex ©UPS
3Pace
Custody Seal Present? CYes
Pecking Material: ©Bubble Wrap
Thermomete
lR Gun ID: 92T036
Cooler Temp ('C):s Correctton
Cooler Temp Corrected (C):
USDA Regulated Soil ([N/A, water sample)
Old samples original 'in a quarantine zone within the United States: CA, NY, or 5C (check maps)?
IJYes [No
CUSPS
°`©¢Cher:
Seals Intact? ©Yes
Bubble Bags
Type of Ice:
actor: Add/Subtract ('C) +0.1
Other
©Blue
Document Revised; February 7, 2018
Page 1 of 2
Issuing Authority;
Pace Carolinas Quality Office
nal+YhO rnei.nks.uq
'pp#:92380666
II�IIVIIII 11111111
etate/Inelals Person Examining Contents:
ONone
biological Tissue Frozen?
©Yes CNo ©N/A
Temp should be above freezing to 6'C
©Sarnpies out of temp criteria. Samples on ice, cooling process
has begun
old samples originate from a foreign source (Intern ovally,
Including Hawaii and Puerto Rico)? QYes No
Chain of Custody Present?
lea
Short Hald Time Analysis (472 hrj?
Rush Turn Around Time Requested?
lent Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Inta ct?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CDC?
D/Analysis Matrix:
Headspace in VOA Vials>5-6mm)7
Trip Blank Present?
Trip Blank Custody Seals Present?
CDMMENTS/SAMPLE DISCREPANCY
2es ONO ©N/A
Yes no' QN/A
Qtr CIN
I]Yes
©N/A
/A
Yet ©No aN`A
(g©No DN/A
Yes ©No ©N/A
[ Sres (INo
©Y. l jNo N/A
Yes ©No ©N/A
©Yes © °.. I 4
ores
©Yes ©No JN/A
1.
2.
4.
5.
6.
7.
10.
11.
Field Data Required? ©Yes ©No
Lot ID of split containers:
CLIENT N©TifICATIQN/RESCiLUTtON
Person contacted: Date/Time:
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Page 2 of 16

l Plastic Unpreserved (N/A)
Plastk Unpreserved IN/A)
Plastic Unpreserved (N/A)
iastic H2SO4 (pH < 2) (CI-)
plastic HNO3 (pH c 2)
ZN Acetate & NaOH (>9)
aOH (pH > 12) ICI•)
Glass Jar Unpreserved
AG1U-1 titer Amber Unpreserved (N/A) (CI-)
00000000000
AG1H-1 rrter Amber Ha (pH < 2)
AG3U-250 mL Amber Unpreserved tN/A)
AG1Sl titer Amber HZSt 4 (pH <2)
1163S-250 ml Amber H2504 (pH < 2)
AG3A(t1G3A)-250 mL Amber NH4CI (N/A)(CI-)
DG9N-40 mL VOA HCI (N/A)
VG9T-40 ml VOA Na25203 (N/A)
VG9U-40 ml VOA Unp (N/A)
DG9P-40 nil VOA H3PO4 (N/A)
VOAK (6 vials per kit)-5035 kit (N/A)
V/GK (3 vlab per kit)-VPH/Gas kit (N/A)
SPST-125 mi. Sterile Plastic (N/A — lab)
SPZT-250 ml Sterile Plastic (N/A — lab)
AGOU-100 mL Amber Unpreserved vials (N/A)
VSGU-20 mL Sdntikation vials (N/A)
aG9U-40 mt Amber Unpreserved vials (N/A)
1

Section A
Required Client Information:
Address:
Email To:
Phone;
Requested Due Date/TAT:
Section D
Required Diem Irlom anion
Fax:
SAMPLE ID
(A-Z, 0-9 / ; )
Semen lOs MUST BE UNIQUE
Section B
Required Pro)oct Information:
Report To:
Copy To:
CHAIN -OF -CUSTODY / Analytical Request Document
The Chairwf-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
7' rr Sw ► c
Purchase Orde. No,:
Project Name; Wes'
Project Number.
Matrix Codes
MATRIX (COOL
Drinking Water OW
Water WT
Waste Water WW
Product P
Soil/Sold SL
Oil OL
Wipe WP
Air AR
Tissue TS
Other OT
©
w
0 Q-
© r
r
COLLECTED
COMPOSITE
START
DATE
TIME
rT MP0.5ITE
ENO/GRAB
DATE
T
Section C
Invoice Information:
Attention:
Company Name:
Address:
Pace Profile 9:
Preservatives
z
z
4.
5
9
7
9
ADDITIONAL CCNAMEMTS,
ORIGINAL
D 8Y t AFFILWTION
I
DATE
AND SIGNATURE
PRWT Name of SAMPLER.
SIGNATURE of SAMPLER:
ACC
CT- 1 • 'Important Nolo: By sicpun9 tha form you are accepting Paces NET 30 day payment leer* and agreeing to isle Ole/gee or 1.s% per month any invoices not paid vegan 30 d
Requested
Page:
REGULATORY AGENCY
of
2229553
r NPDES r GROUND WATER r DRINKING WATppE,,R
r UST r RCRA OTHER S f+4+
ale Filtered (rm)
obVe
Pace Prolect No/ Lab I.D.
ctl
Y
DATE Signed
(MRI/DDfYY}:
A
3.0
SAMPLE CONDITIONS
F-ALL-Q-020rev,07, 15-May-2007

Chain of Custody
Workorder: 92380666
Workorder Name:
Matthew Brainard
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: [e-mail]
State of Sample Origin: NC
3
4
Marathon CLT- West Terminal
4/1 1201814:45 92380666001 ' Water
P.O.
(5
r TN
Results Requested By: 4/19/20
Cooler Temperature on Receipt °C I Custody Seal Y or N 1 Received on I+ce Y or N
8
LAB USE ONLY
Samples Intact Y or N
ursday, April 12, 2018 4:46:49 PM
FMT-ALL-C-002rev.00 24March2009
Page 1 of 1

ESC
*ESC A
niW.almY Popp MWWa'
CA
April 19, 2018
Pace Analytical - Huntersville, NC
Sample Delivery Group:
Samples Received:
Project Number:
Description:
Site:
Report To:
PER
L985432
04/13/2018
92380666
Pace - Marathon Charlotte 001
NC0046213
Matt Brainard
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
Results relate only to the items testei! or c
reproduced, except in full, without written
performed per guidance provided in labor
y
Nancy McLain
Technical Service Representative
d and acre reported as9't%upded values -This test report shall not be
{ of the laboratory. Where appllcabte, sampling conducted by ESC i5
and,rd operating procedures: 060302, 060303, and 060304,
12065 Lebanon Rd Mount Juliet. TN 37122 615-758-5858 800-767-5859 www.esc

TABLE OF CONTENTS
ONE LAB, NATIONWIDE,
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
OUTFALL 001 L985432-01
Qc: Quality Control Summary
Wet Chemistry by Method 130.1
Wet Chemistry by Method 310.2
GI: Glossary of Terms
Al: Accreditations & Locations 9
Sc: Sample Chain of Custody 10
1
2
3
4
5
5
6
6
7
8
4
Cn
Sr
GI
AI

OUTFALL 001 L985432-01 WW
Method
Aquatic Toxicity by Method 2000
Wet Chemistry by Method 130.1
Wet Chemistry by Method 310.2
Collected by
Collected date/time
04112/1814:46
vtcd
04/13/18 08:45
Dilution Preparation Analysis Analyst
dateflime date/times
WG1099244 1 04/13/181108 04113/1813:08 AMP
WG1098860 1 04/17/18 08:08 04/17/18 08:08 44
WG1098692 1 04/17/1812:06 04/17./1812:06 KK
Batch
4
Cn
Sr
7GI
AI
9
Se

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All radiochemical sample results for
solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet
weight was requested by the client, All Method and Batch Quality Control are within established
criteria except where addressed in this case narrative, a non-conformance form or properly qualified
within the sample results, By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data,
bk4,,L
Nancy McLain
Technical Service Representative
Project Narrative
Please review all information in this report for accuracy and completeness. Contact our office within ten days if there are any
questions.
Chronic Test Methods are described in 'Short Term Methods for Estimating the Chronic Toxicity of Effluent and Receiving Waters
to Freshwater Organisms" (EPA/600/4-89/001).
The Biomonitoring results in this report are only a summary of the tests performed. A detailed report will follow. The detailed
report (not this summary sheet) must be submitted to the appropriate regulatory agency.
z
Tc
Ss
Qc
7GI
AI
Sc

Aquatic Toxicity by Method 2000
Result
Wet Chemistry by Method 130,1
Qualifier
Analysis
date / time
04/13/2018 13:08
ch
4
Analyte
Hardness (colo6rnetric) as CaCO3
Result
ug/I
31500
Wet Chemistry by Method 310,2
Qualifier RDL
ug/I
30000
Dilution Analysis
date / time
04/17/2018
Batch
860
Anal
ALK
Result
ug/I
25200
Qualifier
RDL
ug/I
20000
Dilution
Analysis
date / time
04/17/201812:06
B
h
WG1O9
92
Tc
u
Ch
Qc
7
GI
Al
a
Sc

Method Blank (MB)
(MB) R3302327-1 04/17/18 07:47
MB Result
Analyte ug/I
Hardness(colorimeftric)es 3960
CaCO3
MB Qualifier MB MDL
ug1
MB RDL
ug/I
1430 30000
L984266-03 Original Sample (OS) • Duplicate (DUP)
(OS) L984266-03 04/17/13 07:54 • (DUP) R3302327-4 04/17/18 07:55
Analyte
Hardness
CaCO3
caber))
c)
Original Result DUP Result
ugil
164000 160000
ug/I
Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
2.47 20
L985076-03 Original Sample (OS) • Duplicate (DUP)
(OS) L985076-03 04/17/18 08:05 • (DUP) R3302327µ7 04/17/18 08:07
Analyte
Hardness (colori
CaCO3
ric) as
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
ugil ug/l 4b
67800 60400 1 11.5
20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3302327-2 04/17/18 07:48 • (LCSD) R3302327-3 04/17/18 07:49
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD
Analyte ugil ugll ug/I `Y % `%
Hardness (c©larimt.tnc),gas 150000 164000 166000 109 111 85.0-115 1.21
CaCO3
L985072-03 Original Sample (OS) • Matrix Spike (MS
rix Spike Duplicate (MSD)
/,
RPD Limits
20
(05) L985072-03 04/17/18 08:00 • (MS) R3302327-5 04/17/18 08:01 • (MSD)
Spike Amount Original Result MS Result
Analyte ug/I ug/I ugfl
Hardness (calorimetric) .as 150000 55000
CaCO3
2327-6 04/17/18 08:02
MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
ug/I,
203000 205000 98.7 100 1 80.0-120
RPD Limits
0.980 20
4
Cn
7
GI
a
Al
Sc

Analyte
ALK
Method Blank (MB)
(MB) 93302422-1 04/17/18 11:40
MB Result
ug/I
MB Qualifier MB MDL MB RDL
ug/I
0 ..
20000
L984241-02 Original Sample (OS) • Duplicate (DUP)
(OS) 0984241-02 04/17/18 11:49 • (DUP) 93302422-4 04/17/18 1L52
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ugil
ALK 198000 197000 1 0.506 20
L985718-02 Original Sample (OS) • Duplicate (DUP)
(OS) 0985718-02 04/17/18 12:08 • (DUP) 93302422-7 04/17/18 12:09
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I ^„
ALK 42600 43000 0,935_., 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) 93302422-2 04/17/18 11:41 • (LCSD) 93302422-3 04/17/18 11:42
Spike Amount LCS Result LCSD Result
Analyte ug/I ug/l ug/I
ALK 20000(1 184000 177000 92.0
LCS Rec,
°6
LCSD Rec.
Rec. Limits
eft)
0
LCS Qu
L984266-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
LCSD Qualifier RPD
RPD Limits
Z0_
(OS) L984266-02 04/17/18 11:59 • (MS) 93302422-5 04/17/18 12:00 • (MSD) 93302422-6 04/17/18 12:01
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits
Analyte ug/l ug/l ug/I ug/I % "4
ALK 100000 124000 203000 203000 70 0 79,0
1 80,0-120
ier
MSD Qualifier RPD RPD Limits
J6 0.000
20
Page 0
PAGE:
5432{34Jt f1 13 9 ' 7of 11
4
Cn
7
GI
LAI
Sc

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical
intended as a comprehensive explanation, and if you have additional questions please contact your pr
Abbreviations and Definitions
uEts from the Laboratory. This is not
et representative.
MDL
RISE.
Rec,
SDG
El
Analyte
Limits
Qualifier
Case Narrative (Cn)
Gul#ty" Cyr.
Sutntt ry at)
Sample Chain of
Custody (Sc)
Sample Summary (Ss)
Qualifier
Method Detection Limit.
Reported Detection Limit„
Recovery,
l efati e ?ercent Dt efen e.
Sample Delivery Group.
Not detected at the Reporting Limit or WI. where appicable).
The name of the particular compound or analysis performed, Some Analyse
reported,
nd Methods will have multiple analytes
pte ntay be
etl for thi ;
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
itte sitar+ spiked Sample in the peep(betch used tel deterrrrine the Relative Percent Difference (RPD) from rt quality controt
sample: fhe drtglnai ample may not Fie inctu'tfecl'wiftitrt`the reported SDG.:
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
T:
tofui
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process, If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Th(s sec ttpft orthe'repo t irttdi ttte results taf the abo tort'+ to ut gontrdl anal ses required by procedure or
to assi pies. These analyses are not
+tides
n your sampled typlcalFy; but on ti
This is the document created in the field when your samples were initially collected_ This is used to verify the time and
date of collection, the person collecting the samples„ and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis*
This section of y er report wtll provide the,resuits of al
provided
ectton fear
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Description
B
J
The same analyte is found in the associated blank.
Thaianalyte.. iancent€at, s the upper krn t.e the e for can r nge of the instrument tabllsht
c ibrat-On tC AL)i. i . .
The identification of the analyte is acceptable; the reported value is an estimate.
lire salrtple matrix tntGrfefed with the ability to make any.ac ur todeter atom spike val
Cp
4
Cn
Qc
Al

ACCRE©ITATIONS & LOCATIONS
ONE LAW, NATIONWIDE,
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location, 0ne phone call, one point of contact, one laboratory. No other lab
is as accessible or prepared to handle your needs throughout the country. 0ur capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. 0ur focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
' Not all certifications held by the laboratory are applicable to the results reported in the attached report.
"Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences.
State Accreditations
Alabama 40660 Nebraska NE-0S-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey—NELAP TN002
California 2932 New Mexico' n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida .. ... .. .. .-.E87487 .... North Carolina ....... ...... DW21704
Georgia NELAP North Carolina' 41
Georgia' 923 North Dakota R-140
Idaho TN00003 0hio—VAP CL0069
Illinois 200008 0klahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356
Kentucky' 90010 South Carolina 84004
Kentucky 16 South Dakota n/a
Louisiana A130792 Tennessee 1° 2006
Louisiana LA180010 Texas T 104704245.17.14
Maine TN0002 Texas LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Third Party Federal Accreditations
A2LA — 150 17025 1461.01
A2LA—15017025 1461,02
Canada 1461.01
EPA—Crypto
TN00003
AIHA-LAP,LLC EELAP 100789
DOD 1461.01
USDA P330-15.00234
Drinking Water a Underground Storage Tanks ' Aquatic Toxicity ° Chemical/Microbiological 5 Mold ` Wastewater n/a Accreditation not applicable
Our Locations
ESC Lab Sciences has sixty-four client support centers that provide sar
contact our main office. ESC Lab Sciences performs all testing at our c
pickup and/or the delivery of sampling supplies, If you would like assistance from one of our support offices, please
I laboratory.
Cp
2Tc
Ss
Cn
5
Sr
Qc
7
GI
Sc

Hunte
Phone(?
Email m#
Cooler7em
2#+ 4:

Receiveded fly: K kej
COC :Seat`;
Battles arrive intact?
Correct bed
Page 16 of 16

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Tenninal
OWNER NAME: Mplx Terminals LLC,
GRADE: PC-1
eDM'R PERIOD: 03-2018 (March 2018)
2400 e1ock
4
6
7
10
PERMIT VERSION: 4,0
CLASS: PC-1 RECEIVED
ORC: Terry Lee Swick
ORC HAS CHANGED: No MAY d 3 Z018
VERSION: 1.0 CEN C kML FILES
DWR SECTION
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
RECEIVEOINCDENR/DWR
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE
MOORESVILLE RE
11rs
2400 010ek
1540
0900
Hrs
0,25
0.25
WO"'
Y
>y
50050
See Permit
Calculated
FLOW
mad
U211S`
(/0030
Monthly
Grab
'1;S'S - £]aur
ntgil
15,2
34030
Monthly
C3•3tz
BENZENE
00956
Monthly
C71L,)HSE
32730
Monthly
Grab
1711EN, 'tR
< 0.01
00070
Monthly
Grab
Tviumyrk
nth.
10.3
11
12
13
08011
0,25
0.102
14
15
17
111
19
20
21
0730
0.25
0 226
23
24
25
26
27
20
25
30
31
Monthly Aorrakr Limit:
Monthly Average:
Daily 01021,72m0
naily Minimum:
0.1345
0.226
11.002
10
6.2
6.2
'.2
0
0
0
**** No Reporting Reason: ENFRLSENo Flow-Reuse/Recycle: ENVWTIIR-- No Visitation—Adversc Weathcrt NOEL©W - No Flow; HOLIDAY ' No Visitation - Holiday
10.3
10.3
10.3

NPDES PERMIT NO.: NC0446213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mp14 Terminals LLC
GRADE: PC-1
eDMR PERIOD: 03-20
COMPLIANCE STATUS; Compliant
ORC/Certifier Signature: Terry
By this signature, I certify that this
is aceu
PERMIT VERSION:4,0
CLASS: PC -I
ORC: Terry Lee Swick
ORC HAS CHANGED: No
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
VERSION: 1,0 STATUS: Processed
CONTACT PHONE #: [phone] SUBMISSION DATE:
018
iek E-Mail:[e-mail] Phone #:[phone]
and
0
of`my knowledge.
04/09/2018
Date
The permittee shall report to (he Director or the appropriate Regional Offtcu arty noncompliance that potentially threatens public health or the environment_
Any information shall be provided orally within 24 hours from the iirlt t e ernittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances,
lithe facility is noncompliant, please attach a list of corrective actions being taken and a timeµtabk for improvements to be made as required by part 11.E.6 of
the NPDES permit.
Prmittee2S ub
04//2018
Signature:*** Angela S Brown E•Mail:asbr©wnrnarathonpetroleum.com Phone #:419-4I-2629 Date
Permittee Address: R03 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/200
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervisitttt in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best (Amy knowledge and belief, true,
accurate, and complete.' am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations„
LAB NAME: Pace Analytical Services Inc.
CERTIFIED LAB #:
PERSON(s) COLLECTING AMPLE&
Parameter Code assistance
CERTIFIED LABORATORIES
PARAMI:1'ER CODES
e obtained by calling the NPDES Unit [phone] or by visiting http://portalwncdenr.org/weblwq/swp/ps/npdes/fornis.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document viattation of acility as required par l5A NCAC 80 .0204..
*** Signature of Penntttee: If signed by other than the permitter, then delegation of the signatory authority must be on file with the state per I5A NCAC 2B
.0506(bX2)(D)•

ONeilv
NPDES PER If NO.: N0004621.3 PERMIT VERSION: 4,0
FACILITY 1%A.ME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC -I
eDMR PERIOD: 02-2018 (February 2018)
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0 GE Na R/ L H LES
REC .
MAR 1 3 C11S
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
RECEIVED/NC 3ENR!1)
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO D
3
ONAL, OFF?CE
H
G
G
2
500511
C0530
00556
32730
161070
34030
See Permit
Monthly
Monthly
Monthly
Monthly
Calculated
Grab
Grab
Grab
Grab
Grab
0YdI5v
"ISti-looc
014CNSB
Plle79,"1`21
T1.:1I91019
BEsZ.kNO;
2400 clock
ors
2400 dock
Ilre
V/11/79
mgd
mgil
mg/I
mg.'I
nlu
t1gJt
(
J
10
11
12
1100
.25
y
0.(102
8.0
'= 5
<0.01
12.1
c 2
13
1(I11I
:25
y
t7.tt25
.
14
15
Iti
17
10
19
20
21
21
23
24
25
2d
27
'28
Monthly Average I.Imll:
30
i
MOaad,A.era$et
0.095
8.8
(1
0
12,1
(I
Daily Madnmme
of FS
0,8
0
0
12.1
0
Daily Minimum:.00
3.R
(1
i3
12.1
i1
**** No Reporting Reason: ENFRUSE • No Flow-Rcusc,/Recycle, ENV V1I-IA=No Visitadnn - -Adverse Weather; NOFLOW No Flow; HOLIDAY = No Visitation -Holiday

NPDES PFAMIT NO.: NC00462 13
FACILIT NAME: Charlotte Terminal
OWNER NAME: Mpi* Terminals LLC
GRADE: PC -I
eDM Ft PERIOD 02 2018 Fcbruary 2018)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0 PERMIT STATUS: Active
CLASS: PC-1 COUNTY: Mecklenburg
ORC: Terry Ler Swick ORC CERT NUMBER: 9
ORC HAS CHANGED: No
VERSION: 1.0 STATUS: Processed
CONTACT PHONE #: [phone]
SUBMISSION DATE: 03/08/2918
03/07/2018
ORC/Certifier Signature: Terry L. Swick [e-mail] Phone #:704-392-I345 Date
By this sign
ify thai tlus eport is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list ofcorrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
03/08/2018
ermittee ubmi Signature:*** Angela S Brown E-Mail:asbrown®marathonpetroleum.com Phone #:[phone] Date
Permitice Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certifY, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the inforrnation submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and eomplete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Pace Analytical Ine
CERTIFIED LAB #:
PERSON(s) coLLEcn G S P eri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portalmcdenr.org/web/wq/swp/ps/npdes/fomis.
FOOTNOTES
Use only units of measurement designated in the reporting theility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box lino discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 86 .0204.
*** Signature of Perrnittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2XD).

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC -I
eDMR PERIOD: 01-2018 (January 2018)
2400 clotk
2
3
4
6
9
10
11
12
13
PERMIT STATUS: Active
r"). COUNTY: Mecklenburg
ORC CERT NUMBER: 9911AECEIVEDINCUENRIDWR
FE,H 1 ZOZ
cE,,A"vt,-(AL F;iLes STATUS: Processed
0\1\1 'LOTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHA
Total Contizasitt
RC Site?..
2400 clock 1163 3/066
1530 0.25
Wag Reason"'
08
0
PERMIT VERSION: 4 0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANCED: No
VERSION: I M
5005 A
See Permit
Calculated
C0530
Monthly
Grab
34030
_Monthly
Grab
34371 "MEM:
Quarterly Quarterly
Grab Crab
22417
Quarterly
Grab
34696
Quarterly
Grab
00556
M.ontb.ly
Grab
WO A S
REG W,) 1„ 0 FE FIC
32730
Monthly
Grab
FLOW
rogd
0,002
3"SS - Coot
2.5
ug/1
ETHYLREN 6,111024AC
ug/1 percent
1 100
131111E
ug/I
< 1
NAPTIIALE
ugil
< I
011,GRSE
Ing/1
< 5
POEN, TR
1187
< 0,01
14
15
17
IS
19
20
21
22
23
24
20
26
27
28
29
10
31
WOO 0,25
Monthly Average Limn:
Monday Averago:
Daily Mashannv
0,357
0,1795
0,357
30
0
0
100
100
0
0
0
0
D0I1y /3116103666
0.0()2
(1
I 00
0
**** No Reporting Reason; ENFRUSE No Flow-Reuse/Recycle; ENVWTHR.., No Visitation — Adverse Weather; NOELOW = No Flow; HOLIDAY No Visitation — Holiday
0

NPDES PERMIT NO.: NC0046213 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal CLASS: PC-1 COUNTY: Mecklenburg
OWNER NAME: Mplx Terminals LLC ORC: Terry Lee Swick ORC CERT NUMBER: 991 168
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 01-2018 (January 2018) VERSION: 1.0
STATUS: Processed
SAMPLING L©CATI©N: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
c°a
p
i
341110
00070
01551
Quancrly
Monthly
y
Grab
Grab
Grab
vorvIENE
TIABInYY
XYLENti
2400 clock
Mt
2400 clock
flrr,
Y'r$/N
ug/I
ntu
uyl
fi
1530
0.25
y
< 1
8.4
< I
10
I
12
1.3
14
15
In
17
IS
19
20
21
2I
23
24
25
2M1
27
I0
29
3B
31
11)00
0.25
y
Monthly A.crnhe. Limll.
Monthly A.en¢c
0
8.4
0
Daily Mnnlmnnu
0
N.4
0
Dulls Minimum:
(1
8.4
0
****NoReporting Reason; ENFRUSE==NoFlow-Reuse/Recycle; ENVWTHR-NoVisitation--AdverseWeather; NOFLOW No Flow; HOLIDAY — NoVisitation— Holiday

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMRPERIOD:0 .201 (January2018)
COMPLIANCE STATUS; Compliant
ORC/Certifier Sign
ur
fy that this
Terry
u
PERMIT VERSION: 4,0
CLASS: PC•1
ORC: Terry Lee Swick
ORC HAS CHANGED:
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
VERSION: 1,0 STATICS: Pr
CONTACT PHONE #: [phone] SUBMISSION ©A
02114/20 i 8
Swiek E-Mail:[e-mail] Phone #:[phone] Date
0
my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that poterttialty threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
lithe facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part IlE,6 of
the NPDES pennit.
Permitter Address:
02/ t 4/2018
Signature:*** Angela S Brown 1 -Mail:asbrown®marathonpetroleum.com Phone #:[phone] Date
Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true,
accurate, and complete. i am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Pace Analytical Services Inc.
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES: J Qualfieri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portaLncdenr.org/w
s/npdes/fortns.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per ISA NCAC 80 .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per ISA NCAC 213
,0506(bx2)(D).

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 01-2018 (January 2018)
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1 0
Outfall 001 - Effluent Comments:
Analysis for Acute Toxicity was subcontracted to ETT Environmental Inc (Certified Lab #02
submitted with hardcopy DMR,
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
The analytical report for Acute Toxicity (Parmeter Code TAE6CO is being

P o, Est l t4f. n ill 4 Crofts -flan C
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2090
Client: MARATHON OIL
Facility: CHARLOTTE TERMINAL WEST 001
NPDES #: NC0046213
Test Reviewed and Approved By:
Test Date: 09-Jan-18
Laboratory Ill #: T50717 AD
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E871319
Florida Dept, of Health. Included results pertain only to provided samples.
Page 1 of 4
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022 Page 6 of 9

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Date 16-Jan-18
Facility: Marathon West/Paw Creek
Laboratory Performing Test:
ETT Environmental, Inc.
Signature of Operator in Responsible Charge
X
Signature of Laboratory Supervisor
NPDES# NC0046213
Pipe # 001 County. Mecklenburg
Comments
MAIL ORIGINAL TO
North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
# Young Produced
Adult (L)Ive (D)ead
Effluent
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L)Ive (D)ead
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
2
2
4
10
10
11
11
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
12
12
Chronic Test Results
Calculated t=
Critical Value=
% Reduction=
% Mortality
Control
Avg, Reprod.
Control
Treatment 2
Treatment 2
Control CV
%8rd Brood
PASS FAIL
X
start end
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates)
6,25
0
12.5,
0
NA% NA%
Organism Tested
25
{
50
0
1st sample
start end
1st sample
100
0
Method of Dete
Moving Average
Spearman Kerber
ination
Probit
Other
Pimephales promelas
2nd sample
start
2nd so
Concentration
Mortality
Complete This for Either Teat
Collection part) Date
.Sample 1 08Jen•18
Test Start Dale
09-Jan-18
Sample 2 NA
Sample Tvpe (Duration(
Sample 1
Sample 2
Grab Comp Duration
Hardness (mg/L)
Spec. Cond. (pmhos)
Chlorine (mg1L)
Sample Temp. et receipt (°C)
1st 2nd
Tox Tox
Dilution Sample Sample
192
59
<0.05
0.1
start/end start/end
8.0
8.3
7.4
7.4
Co
High Canc.
7.8
10.3
8.1
8.5
pH D.O.
DEM Form AT-1
Page 2 of 4
Page 7 of 9

24 Hour Acute Toxicity Test
Test Method: EPA 821 R-02-012 ; Method 2000 Plmephales promeles
Chen
Sample ID: West/Pa Creek
Lab 1D#: T50717 AD
Start Date: 01/09/18
End Date: 01/10/18
Time: 02:50 PM
Time: 03:21 PM
MORTALITY DATA
Conc.
Rep.
Initial It
Organi9FSY9
Cumulative Mortality
211. an hr ahn 46 br
Final
M nruaty
. Control
A
10
0
0%
B
10
0�
C
D
6.3%
A
10�
0
0%
B
10
0
C
D
12.5%
A
10
0
0%
B
10
0
C
D
25.0%
A
10
0
0%
B
10
0
C
D
50.0%
A
10
0
0%
B
10
0
C
D
100.0%
A
10
0
0%
B
10
0
C
D
Al
B
C
D
Set By: FJ
Ended By: AM
Page 3 of 4
Page 8 of 9

P© 16414, Grearsv tie, SC 296tt366 7414
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
W W W.ETTEN VIRONMENTAL.CDM
Client
l CSIi
State:
(Composite only)
AMPLE ID ? c,
Special It structions:
Sample Custody Transfer Record.
(Grab or Composite)
Date Time Relin t `_ _. BY 10
CCIPPOSITE S MPLfAG PROCEDURES
Ctilposite samples must be collected over a 24 hour period.
Tito Proportional: 1 sample each hour for 24 hours. Equal volul
orminimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES permit.
Sign, and Print below
the dotted line
CININ OF CUSTODY RECORD
d Oraaniz
1Paae
Chemical Analysis & other
Secure
Sample
TEMPERATURE MONJTORING PROCEDURES
Sample temperature during collection and transport rues be between
0"0 and 6.1:1 °C. Samples must not be frozen. Use water ice in sealed bags.
HOLD TIME PROCEDURE.S
For toxicity resting the sample must first used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection,

4
[phone], [phone] Faz:[phone]
Slipping Address: 4 Craftsman Ct, Greer, SC 29650
W W W.CTTCNV IfONMCNtAL,CQM
'Client:
SAMP
D t?
(Composite only)
Composite Sinn fixate Time
►Sample Custody Transfer Record
Date Time
"/ag/l
(Grob or Composite)
Relinctt By I0
E©URES
ted over a 24 hour period.
c Proportional: 1 sample each hour for 24 hours. Equal v
minimum 1 sample every 4 hours over 24 hours.
Proportional: As per instructions in INIPDES permit.
Program
Sign, and Print below
the dotted line
OF CUSTODY RECORD
Containers
Preservative
I -H2SO4
2". HCL
3.HNO3
4-Hoeft
s° Zoile
6. (Mier
Nowt
Teat Oreants.
Parameters
Z 6`003,
herniae! Analysis & Other
6)ved By / Organization
TE,MPEURE MON/TORIN PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
Secure
DU
xicity testing fate sarrtple must first used within 36 hours
pie collection (completion oa`composite sample).
Sample may not be used after 72 hours from sample collection.
Receipt
Temp 'C
Sample
Preserved?

Chain of Custody
korder:
2369039
Report / Invoice To
Workorder P ati e:
Matthew Brainard
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: [e-mail]
6tre_r SC a.0 A5°
State of Sample Origin: NC
ha to
Subcontract To
NC004613 Qu
Sample ID
Outfall € 01 Grab
/8/2018 15:15
Cooler Tem . erature on Recei it '+
0'
P.O.
v rvEvlA-h\
Lab ID
92369039001
Matrix
D te/Time Received By
Custod Seal Y or N
Preserved Containers
Results Requested y: 1/1 rig i18
Received on Ice Y or N
LAB USE ONLY
g)anday, January 08, 2018 4:35:06 PM
FMT-ALL-C-002rev,00 24Marci12009

Laboratory receiving samples:
Asheville © Eden©
Courier:
© Commercial
Custody Sul Present?
Packing Matertait
Thermometer:
„al Gunn):
Correction Factor
ubble t+ftrap
Tetnp
Project #:
Document Revised: August 4, 2017
Page 1of2,
Issuing Authority:
Pace Quality Office
Raleigh© Mechanicsville©
WO#�92369039
11.11111 III
Date/Initlats Person Examining Contents:
© Other
©slue ©None
S
Document Name:
Condition Upon Receipt(SCUR)
Document No.:
F•CAR•CS-033-itev.o4
Greenwood
Huntersvi'
Seals Intact? ©Yes— No
©Bubble Bags
T of
cted (C): , Temp should be above freezing to VC
©samples out of temp criteria, Samples on ice, cooling process
has begun
Biological Tissue Frozen?
©Yes ©No ?JNTA
USDA Regulated SoilfiA, watersamte)
Did samples originate in a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a fore
Yes
Chain of Custody Present?
s Ar
d within Hold Time?
Id Tithe Analysts (<72 hr.)?
Rush Turn Around Time Rerguested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Disso
Iysis: Samples Field Fii
Sample labels Match COC?
d?
-Includes Date,Time/ID/Analysis Mat
Headspace in VOA Vials i>5•6mm)
Trip Blank Present?
Trip Blank Custody Sealy Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
es _ONO ©N/A
©Yes
[jN/A
A
/A 4.
©N/A
'IJY ©No ON/A 6.
;litres ©N© CNLA
No pNA
Ejres ©r o
N
©yes ©No
(*fives (:)No
©N/A
including Hawaii and Puerto Rico)?
Date/Time:
Comments/Disc►ey
ce
ancy:
Field Data Required? Dyes ©No
Lot ID of split containers,
Project. Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Note; Whenever there is a discrepancy affecting North CaroHnd cornpliance samples, a copy of this form will be sent to the North Carolina DENNR Certification Office (Le.
Out of hotd, incorrect preservative, out of temp, incorrect containers
Page 2 of 9

iter Plastic Unpreseiw d (U,,
U-1 liter Amber Unpreserved (PtfA) (+C
0

NPOES PELaMIT NO.: NC#It}46
FACIL.I'I'Y NAME: Charlotte I'ermine!
OWNER NAME: MEIx Terminals LLC
GRADE: PC -I.
eDMR PERIOD: 12 2OI7 (L?cce7nber 2
7
PERMIT VERSIOi: 4.tt
CLASS: PC -I
ORC: Te2vY 1
ORC HAS CHANGED: No
VERSION: 1.0
RECE IVEDERMITSTATUS: A
JAN 23 2013
CENT t AL FILES
DWR SECTION
COUNTY: Mccklenburq
ORC CERT NUMBER:„,!!_6
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: NI NO DISC
C0430
Recorder
FLOW
NAL OFFICE
99970
, 34930
TSS,C.or
810alh1y
Gab
01L-GRSE
TILRNItITY
mgil
025
4,R
12
13
li
15
17
19
20
24
23
26
27
IN
39
30
32429thly Arrow ©. 116
4,R
a.o 4,8 0 0
***. No Reporting. Reason: ENFRUSI: -: No Flow-Reuse/Recycle: ENV WTHR Q No Vi911itio11 - Adverse Weather: NOFL.OW No Flow, HOLIDAY s. No Visitation - Holiday

NPT3sr„ PAMIT NO.: NC0046213
/FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals Lie
GRADE: PC-1
eDMR PERIOD: 12.2017 (December 2017)
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: Terry L.
By this signature, I certify that this report is
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lpe Swick
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mccklcnburli
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: 01/15120
ick E-Mail:[e-mail] Phone #:[phone]
and complete to the best of my knowledge.
01/1tl/20
Date
The pennittce shall report to the Director or the appropriate Regional Office any noncompliance that potentially tftreatetts public health or the environment.
Any information shall be provided orally within 24 hours from the time the pennittce became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the pennittce becomes aware of the circumstances,
if the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for i
the NPDES permit,
Pc nitteefSubmitter
g
vements to be made as required by part ILE.6 of
01 /1/2018
Angela S Brown E-Mail:asbrown@marathonpetroleum,com Phone #:[phone] Date
Permit tee Address: 8035 rottnt Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or su
tatOn I
ce
ystem designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that therearesignificant penalties for submitting false infonnation, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABORATORIES
LAB NAM Analytical Services, inc
CERTIFIED LA.B #:
PERSON(s) COLLECTING SAMPLES: 1 Qu#I6cri
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http:/7portal,ncdenr,org/web/wq/sw
FOOTNOTES
Use only units of measurement dcsitatcd in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From. Site: Cheek this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC: on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G ,0204,
""* Signature of Permitter: 1f signed by other than the pennittce, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
,0506(b)(2)(D),

MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Math Street
Findlay, OH 45840
Tel: [phone]
January 18, 2018
Sent via Overnight Mail
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
Enclosed please find the December NPDES report, plus one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NODES PERMIT NO.: NC0046213 PERMIT VERSI
FACILITY NAME: CharlotteTermirtal CLASS: PC -I
OWNER NAME: Mplx Terminals LLC ORC: Terry Lee Swick
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 11-2017 (November 2017) VERSION: 1.0
4.0
ATUS: Active
kleuburr
T NUMBER: 99116E
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
•*•• No Reporting Reason: ENFRUSE m No Flow-Reuse/Recycle; ENVWTHR = No Visitation -- Adverse Weather; NOFLOW No Flow; HOLIDAY No Visit
Holiday

PDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eOMR PERIOD: 11-2017 (November 2
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4
CLASS: PC-1
ORC: Tcrry Lac Swic1
ORC HAS CHANGE
VERSION: 1,0
CONTACT PHONE #: 419421
No
9
PERMIT STATUS: Active
COUNTY; Meeklcnburia
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: l2/12/2017
ORC/Certifier Signature: Terry Swick E-Mail;t1swick@ marathonmetroleum.com Phone
By this signature, i certify that this report is accurate and complete to the best of my knowledge.
The permiitee shall report to the Director or the appropriate Regional Office any noncompliance that pate
Any information shall be provided orally within 24 hours from the time the permittee became aware of th
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part i1.E.6 of
the NPDES permi
:704-392-1345
0
7
Date
ially threatens public health or the environment.
irnumstances. A written submission shall also be
2/2017
Pere/ 'rnitter mature.*** Angela S Brown [e-mail] Phone #i:419-421-2629 Date
Permittee Address: 8035 ' stunt Holly Rd Paw Creek NC 28130 Permit. Expiration Date: 06/30/2020
i certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Paco Analytal Services, Inc,
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES:1 Q
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.orgtweb/wq/swplps/npdes/forms.
Use only uni
e
FOOTNOTES
ent designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR.
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 28
.0506(b)(2)(D).

RMIT N
FACILITY NAME: Cha
OWNER NAME: Nip 1x Ter
GRADE: IC-1
eDMR PERIOD: 1i}- 017 (C)cica#x r 17)
PERMIT VEitS1@N:4
CLASS: PC -I
ORC: Terry Leo Swick
ORC HAS CHANGE!): No
VERSION: 1,0
PERMIT STATUS: Active
COUNTY: M ckh oburg
OR( CERT NUMBER: 991148 „
S"I"ATU s': Process cd
SAMPLING LOCA 1ON: EFFLUENT DI C A. GE NO.: 001 NO DISCHARGE*: NO
**" No Roporung Reason: l:Nhttll'F, No Flow-Reuse/Recydo; I,NVW 'HIt No Vi i anon - Adrer3e Weather: s"s'OFLt3W No Flow, HOL PAY No Visitaiioee- Holiday

NPDES PERMIT NO.: NC4t546'
FACILITY NAME: Chariotte Tomlin'
OWNER NAME: Mplx Terminals Li,.E.
GRADE: PC,1
eDMR PERIOD: 10-2W7 (October 2U17)
PERMIT VERSION:4.0 PERMIT STATUS Active
CLASS: PC-1 COUNTY: Mcckicnbur
ORC: Tory Lcc Swick ORC CERT NUMBER: 99116
ORC HAS CHANGED: No
VERSION: 1,0
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCBARGE NO.: 001 NO DISCHARGE*: NO (Continue)
THIt ry No V i#1ri # - Adverae Weather, NO IOW • No Flow', 'HOLIDAY No Visi'tution- Holiday

Nl'l)E S PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC:
Cl AI)E:PC-1
eDMR PERIOD: 10.2t)17 (October 2017)
COMPLIANCE STATUS: Cornpliant
ORC/Certifier
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Spa=ick
ORC HAS CHANGED': No
VERSION: I.0
CONTACT PHONE #: 4194
PERMIT STATUS: Activc
COUNTY: Mccklcnbtrrr
ORC CERT NIIMBER:')91
STATUS: Processed
SUBMMiSSSION DATE: 11'14/2017
ick E-Mail:tlswick@_utarathontrsetroleunt.com Phone tl;704-392-1345
By this signature, I certify that this report is accurate and complete to the best of m knowled
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the en
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall alp be
provide! within 5 days of the time the perniittee becomes'aware of the circumstances.
If the facility is noncompliant, please attach a list of corTectivc actions being taken and a time -table for improvements to be made as required by part 11,E,6 of
the NPDES permit.
7
Date
4f2017
a S Brown E-Mail:asbrown(%marathonpctroleum.com Phone T.419-421-2629 Date
Penrtitt Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: (*/3012020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supers,°isitra in accordance with a system do igrted
to assure that qualified personnel properly gather and evaluate the information submitted.. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete, 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Pace Anal tic:a? Services, lsrc.
CERTIFIED LAB 4:
PERSON(%) COLLECTING SAMPLES: J Qualtieri
Parameter Code as
CERTIFIED LABORATORIES
PARAMETER CODES
may be obtained by calling the NPDES [Unit [phone] or by vis
ng http:/I
rtal.nedenr.arglwebfwq'swplps npdeslforms.
FOOTNOTES
Use only units of measurement designated in the reporting faciliiy`s NPDES pernit for reporting data,
* No Flow/'Discharge From Site: Check this box if no discharge occurs and, Its a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
* * ORC on Site'?: ORC must visit facility and document visitation of fiacility as required per i 5A NCAC t1G .0204.
*** Signature of Pernittee: Tf signed by other than the petmittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
„0506(b,)(2)(D).

NPDES PERMIT NO.; NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mpix Terminals LLC
GRADE: PC-1
eDMR PERIOD: 10-2017 (October 2017)
Report Comments;
Analysis for Acute Toxici
submitted with hardcopy
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lae Swick
ORC HAS CHANGED: No
VERSION: 1,0 STATUS: ProceSSed
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 9
al l ab 11022 The analvisaal report tier Aerate Toxicity (Parameter C:esdc TAE6C is bernii

ARATHO
November 16, 2017
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
**Enclosed: Signed hardcopy of eDMR submitta
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via Overnight Mail
RE VED
Nov 1i 7 ?O17
CENTRAL FILES
DWR SECTION
Enclosed please find the October NPDES report, plus one copy, for the above -referenced permit.
Also included is the quarterly toxicity test.
If you have any questions or require additional information, 1 can be reached at 419-421-2019 or by
email at ErRisnergMarathon.Petroleum.com.
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual
NPDES; NPDES DMRs)
NC DENR — Division of Water Resources
Water Sciences Section / Aquatic Toxicology Branch
1621 Mail Service Center
Raleigh, NC 27699-'1.623

(664) 677 42 , rAx (64) 077-6936
P.O. Box 16414, Greenville, $C 29606
4 Craftsman Court, Greer, SG 29650
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON PETROLEUM
Facility: CHARLO'1`1L TERMINAL WEST
NPDES #: NC0046213
Test Reviewed and Approved By:
4/
Test Date: 12-Oct-17
Laboratory ID #: T50202 AD
Robert W. Kelley, Ph.D. Farbad Rostampour
QA/QC Officer
Certification #E87819
Test results presented m this report conform to all requirements of
NELAC, conducted under NELAC Certification limber E87819
Florida Dept of Health. Included results pertain only to provided samples,
Page 1 of 4
Laboratory Director
SCDHEC Certification #23104
NCDENR certification # 022
Page 17 of 20

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
irate 16-Oct-17
Facility: Marathon West/Paw Creek NPDES# NC0046213
ory Performing Test:
ETT Environmental, Inc.
Signature of Operator In Responsible Charge
X
Signature of Laboratory Supervisor
Pipe # 001
Comments
eolclenburg
MAIL ORIGINAL TO
North Carplina Ceriodaohnla Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
# Young Produced
Adult (L)ive (D)ead
Effluent %
TREATMENT 2 ORGANISMS
it Yotmg Poduced
Adult (L)ive (D)ead
pH
Control
Treatment 2
MO.
Control
Treatment 2
LC50/Acute Toxicity Test
2
1st sample
4
4
Method of Determination
Moving Averaga Probit
SpeamtenKerber •. er
6
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mall Service Center
Raleigh, North Carolina 27699-1621
10
10
11
11
Hardness (mg/L)
Spec. Cond. (Nmhos)
Chlorine (mg/L)
rrpie Tamp. at receipt ('C)
12
4
7
pH
8.a j 6.9
D.O.
Page 18 of 20
Page 2 of 4

48 Hour Acute Toxicity Test
lient: Marathon
'Start Date: 10/12/17
nd Date: 10/14/17
Conn.
Rep,
Control
6.3%
12.5%
25.0%
50.0%
100.0%
A
D
A
A
D
A
D
D
A
MORTALITY DATA
to is N
organinns
10
10
10
10
10
10
10
10
10
Cumulative Mortality
34 bt
Test Method: EPA 821 R-02-012 : Method 2000 Pimephales promalas
?3* %A
Final
bCWiaiity
0%
0%
0%
Set By. AM
Ended By. AM
Lab 1D#: T56202 AD
Page 3 of 4
Page 19 of 20

ET'
x 16414, GRC8NV11,4E, SC 2 -7414
(884) 077-19942, 10CIM/ 891-2825 F4,0(88.4)877 6938
SHIRRING APOR6581 4 CRAFTSMAN CT, rEIREER SC 2985O
WWW,ETTENVIRONM ENTAL. COM
Client:
i VH44 Ater4on Peatrete,km co .
Facility: oviv toitt -RC rittrIef
State: NPDES 14:
0
SAMPLE ID
11Agitt4- oo)
Special Instructions:
(Composite only)
Composite Start Date Time
Sample Custody Transfer Record
Date Time
ZO5
itc),
Do
r Composite)
Semple Collection Onto Time
to to It;
' quished By / Organization
C POSITE SAMPLING PROCEDURES
Caposite samples must be collected over a 24 hour period.
Tie Proportional: 1 sample each hour for 24 hours. Equal volu
aril minimum 1 sample every 4 hours over 24 hours.
FleX4/ Proportional: As per instructions in NPDES permit,
Co
by
CHAIN OF CUSTODY RECORD
Program
•
Containers Preservative
1=/-12S0-4
2. Ha.
3.IINO3
4.Na011
5. ZnAr
"151gl's
cr,
Pararneters
1Vhole Effluent Toxicity
Acute 'Chronic
C.)
e.
Received By / Organizton
TEMPERATURE MONITORING PROCEDURES
Samplc temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
Test Organisms
.41100,-
2
Chemical Analysis & Other
PROCEDURESD TIME
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Samp!e may not be used after 72 hours from sample collection.
Secure
Area
Receipt
Temp °C
5094
Sample
Preserved?

i1PDE PERMIT NO.: NC0EP362 13
•'I ACILITV NAME; Charlotte Term nal
OWNER NAME: M six "Pcraxttatts S L
GRADE: PC-1
eDMR PERIOD: 09•201 (e tcxnl r
7
CLASS: PC-t
ORC: Terry 1_cc Swick ,
ORC HAS C:I1A.NCED: No
VERSION:1,0 ENTt
C`"
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 99116£
STATUS: Proecssct3
SAMPLING LOCATION: EFFLUENT DISCDARGE NO.: 001 NO DISC
irAa
Sec Permit
Recorder
0
VWTHR _ No Visiia ion - Adverse W ather: NOFLOW..r- NO Flora: HOLIDAY. No Visitation Holiday

NPR P PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals
GRADE: PC-1
eDMR PERIOD: 09-2017 (September 2201 7)
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: Terry
By this sina
The permittc
Any informaton shall he provided o
provided within 5 days of the time the perrnittee becomes aware of the c,lreumstances.
If the facility. is noncompliant, please attach a list of corrective actions being taken and a time -
the NPDES permit.
Permitiee
PERMIT VERSIONa 4 0
CLASS: PC-!.
ORC: Terry t.ce Swick
ORC HAS CHANGED: No
VERSION; 1,0
CONTACT PHONE #: [phone]
Swick )-Ivfail.tls
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS.
SUBMISSION DATE: 10123/2017
ck >marathonmetroleum,corn Phone #:[phone]
hat this report is accurate and complete to the best of my knowledge.
eport to the Director or the approp
Date
'fie e any noncompliance that potentially threatens public health or the environment.
within 24 hours from the time the perm became aware of the circumstances, A written submission shall also be
to be made as required by part Il.lu,6 of
2t117
Signature:*'** Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Perrnittee Address: 8(i3 " +count Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I` certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
toassurethat qualified personnel properly gather and evaluate the infunnation submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete, I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
(w1$l 1VlF„ED LABORATORIES
LAB NAME: Pace Analytic/ tl Services, Inc.
CERTIFIED LAI3 #:
PERSON(s) COLLECTING CTING SAMPLI:Sr 3 Qu
PARAMETER CODES
gay he obtained by calling the'NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdestforms.
FOOTNOTES
Use only units of nteasthre ent designated in the reporting faeility`s'NPDES permit for retorting data
* No Flow/Discharge Frorn Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period,
�* ORC on Site?: ORC must visit fatality and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the pcnnittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(bX2)(0).

Nt'D ;S P1 MIT NO. CO046213
FACILITY NAME: Ctmrloit; Terminal
OWNER NAME: Mplx Terminals LLC
MADE; PC-1
eDMR PERIOD:08-2017
PERMIT VERSIO
CLASS; PC-1
ORC: Terry Lee Swiek
ORC HAS CHANGED:
VERSION: 1,0
4,
RECEIVED
SEP 29Z017
'CENTRAL FILES
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.:
PERMIT STATUS: Active
COUNTY; Mcekienbu
ORC CERT NUMBER; 99
STATUS; Process
NO DISCHARGE*: NO
•" No Reporting -Reason: ENFRUSF No Flow-Reut;oRccycle: ENV W 1 HR =No Visitation •- Adverse Weather; NOF LOW - No How; HOLIDAY No Visitation Holiday

NPI)ES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Tcrmina6
OWNER NAME: Mplx Terminals L,LC
GRADE: PC-1
eUM R PERIOD; 0-t)17 (August 2017)
COMPLIANCE STATUS. Compliant
ORCiCertificr Signature: Terry
PERMIT VERSION: 4,0
CLASS: PC-1
ORC; Terry Lee Sws`ck
ORC HAS CHANGED: No
VERSION: I0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: 0912.5/2017
09/20/2017
iek E-Mail:[e-mail] Phone 4:704-392-1.345 Date
urate and complete to the best of my knowledge,
The pemtittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment,
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the pennittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for i presvernents to be made as required by putt fl 1L6 of
the NPDES penult.
09/25/2017
ubmitt Signature:*** Angela S Brown E-Mail:asbrownramart€th€>npetroleum.com Phone 4:419-421-2629 Date
ee Address. £l Mount, Holly Rd Paw Creek NC-28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
ter a sure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true„
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABORATOR[FS
LAB NAME:
CERTIFIED LAB 4:
PERSON(s) COLLECTIN
PARAMETER COTES
Parameter Code assistance may be obtained by calling the NPDES unit [phone] or by visiting httpa/portal.ncdenr.org/wch/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of tnea rerntsnt designated in the reponing facility`s NPDES permit for reporting data.
* No F1ow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for ail of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must a rt f luty and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permitter, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

Blanchard Terminal Company LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
September 27, 2017
Sent via Overn
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
Blanchard Terminal Company LLC
Charlotte Terminal
NPDES Permit NC0021971
**Enclosed: Signed hardcopy of eDMR submittal*
Enclosed please find the August NPDES reports for Outfalls 009
above -referenced permit.
If you have any questions or require additional information, I can
email at ErRisnergMarathonPetroleum.com.
Sincerely,
Erin Risner
Analytical. Processor
ail
and 010, plus one copy, for the
be reached at 419-421-2019 or by
Enclosure
cc: -Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

'NPDES PERMIT NO.: NC0021971 PERMIT VERSION: 4.0
FACILITY NAME: Charlotte Terminal (outfall 009) CLASS: PCNC
OWNER NAME: Blanchard Terminal Company L_LC ORC: Not Required
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-20I7 ('August 2017) VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCIIARGE NO.: 009 NO DISCHARGE*: NO
2400 cock II
2400 onerk
Orr
4`1RfN
50050
5000 C0830
34030
77004
34371 TAEMC
34696
0055.6
Recorder
000W
rn�d
Monthly Monthly
Grab Grab
CHLORINE TSS Corra
u l nr JI
Quarterly
Grab
u iI
Quarterly Quarterly Annually
Grab Grab etrab
ETHANO1. 0T'r0Yt00N F"1`ND24
ug/1
ug11 percent
Monthly
Grab
NA±'i'}IA1
Monthly
Crab
0rl.0RSE
2
Od403
It 76
)LOSS
9
39 9.4
le
12
13
`14
15
16
17
18
0,23
(r.076
0.074
19
2n
21
23
24
25
0.099
26
27
28
29
30
31
**** No Reporting Reason
Monthly Average timid
Monthly Average:
0.101857
pail)- Msarrnu m
Dully Minimum;
0.23
39
9,4
9,4
}
Il
t).00l3 39 9,4
NFRUSE = No Flow-Reuhu'Recyclei E NVWTHR -'No Visitation — Adverse Weather; NOFLOW =No Flow; HOLIDAY = No Visitation- Holiday
0

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard. Terminal Company IT_C
GRADE: PCNC
eDMR PERIOD: O8-2017 (August 2017)
PERMIT VERSION: 4.0
CLASS; PCNC
ORC: Not. Required
ORC HAS CHANGED; No
VERSION; 1,0
PERMIT STATUS: Active
COUNTY: Mccklcnbur
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 009 NO DISCHARGE*: NO (Continue)
****No Reporting Reason; ENFRUSE = No Flow-Rcusc!Recyclec; ENV WTNR = No Vision(
Adverse Weather; NOFLOW No Flow; HOLIDAY o Visitation — Fioliday

INPDES PERMIT NO.: NC0021971 PERMIT VERSION: 4.0
FACILITY NAME: Charlotte Terminal (t rrtfall 009) CLASS: PCNC
OWNER NAME: Blanchard Terminal Company LLC ORC: Not Required
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2017 (August 2017) VERSION: 1,0
4
7
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 010 NO DISCHARGE*: NO
2400 clank nets 2400 dock
YiBI
50050
Recorder
FLOW
mhd
90060 C0030
Monthly
Groh GiOh
CHLORINE 1`±1S-Cann
rny'I
34030
1100'!00'1?.
77004
Quxnerly
Grab
ETHANOL
34371
Quarterly
Grab
flitYLBEN
u0rl
faEtiC
Grab
FI111024.01
percent
34696 00556
Monthly
Grab
NA74114117 01L—Gu0E:
9
10
12
13
14
15
10
0,037
< 2.6
<5
0.453
W359>
17
19
20
21
22
23
24
(1.132
as
27
28
29
30
31
01uu1Ul7• Avnrxget
Daily Maximum:
0.24525
14453
31 0
31
Daily Mlnln, nn
00
37 3l tl
k'"' No Repotting, Reason: I;NFRUSO 0, No Flow-Reuse/Recycle; ONVWTI IR y= N. Visitation-- Adverse Weather; NQF`i.C1W NoF1ow', HOLIDAY =° No Visitati
aliday

`NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outrall 009)
OWNER NAME: Blanchard Terminal Company TLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION:4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS:
SAMPLING L©CATI©iN: EFFLUENT DISCHARGE NO.: 010 NO DISCHARGE*: NO (Continue)
2400 clock 1113 2406 ¢lock
Firs
Y(1.10Iti
34010
90070
81551
Quarterly
Grab
"1'00011136
ugl
Monthly
Grab
1131DIDTY
1110
()uarterly
Grab
ugi l
3
4
4
8
9
10
12
13
14
15
16
17
18
19
21
22
23
24
25
1.4
26
27
28
29
30
31
Aver0g
111961919 Average:
1)4tty 1319Y160986
Daily M10106166
1.4
I.4
1.4
""'" No Reporting Reason: ENFRUSE — No How-RcusciRecycle: ENVWTHR No Visitation - Adverse Weather: NOFLOW No Flaw, HOLIDAY = No Visitation-Holiduy

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard Terminal Company L.LC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2t117)
COMPLIANCE STATUS: Com
ORC/Certifier Signature: Erin R
PERMIT VERSION: 4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
()RC CERT NUMBER: 995491
STATUS: Processed
CONTACT PHONE #: [phone] SUBMISSION DATE: 09/25/2017
09
4/2017
ner E-Mail:errisncr(ulmarathonpetroleum.com Phone ' #:419-421-2019 Date
By this signature, I certify that this report is accurate and complete to the be of my knowledge.
The perm
shall report. to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment,
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES pennit.
Perm
09/25/2017
Signature:*** Angela S Brown 'E-Mail:a.sbrownEmarathonpetroleum.com Phone #:[phone] Date
Permittee Address: 7401 Old Mount Holly Rd Charlotte NC 28214 Permit Expiration Date: 06/30</2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision rn accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. 1 ant aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Pace Analytical Services, Inc.
CERTIFIED LAB #:
PERSONts) COLLECTING SAMPLES: J Qua Hier:
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http:/ portal.ncdenr.orglweb/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR.
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per I.5A NC:,AC: 8G .0204,
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 1 5A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0021971 PERMIT" VERSION: 4.0
FACILITY NAME: Charlotte Terminal (outfall 009) CLASS: PCNC
OWNER NAME: Blanchard Terminal Company LLC ORC: Not Required
GRADE: PCNC ORC HAS CHANGED: No
eDMR PERIOD: 08-2017 (August 2017) VERSION: 1.0
Outfall 009 - Effluent Comments:
Total Residual Chlorine was inadvertently tested in August and is bein
ted, Hydrostatic
s
as not d
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
d from Ou

• NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outran 009)
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
Outfali 010 - Effluent Comments:
PERMIT VERSION: 4,0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 1.0
Fire suppression water was discharged, therefore Total Residual Chlorine (TRC) is being reported.
PERMIT STATUS: Active
COUNTY: Mecklenburg,
ORC CERT NUMBER: 995491
STATUS: Processed

Blanchard Terminal Company LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: 419.422,2121
September 27, 2017
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
Blanchard Terminal Company LLC
Charlotte Terminal
NPDES Permit NC0021971
**Enclosed: Signed hardcopy of eDMR submittal*
Sent via Overnight Mail
Enclosed please find the August NPDES reports for Outfalls 009
above -referenced permit.
If you have any questions or require additional information, I can
email at [e-mail].
Sincerely,
Erin Risner
Analytical Processor
and 010, plus one copy, for the
be reached at 419-421-2019 or by
Enclosure
cc: -Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
2400 olock
PERMIT VERSION: 4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 009 NO DISCHARGE*: NO
nrs
2400 cloth
11rs
TAM
50050 50060
See Permit Monthly
FLOW
mgd
Grab
CHLORINE
ug/1
CO530
Monthly
Grab
TSS• Cnnc
mg/1
34030
Quarterly
Grab
ug/1
77004
Quarterly
Grab
ETHANOL
34371
Quancrly
Grab
ETIIYLIIEM1
ug/1
TAE6C
34696 00596
Annually Monthly Monthly
Grab Grab
Grab
MT11024AC NAFTIIALE 011.GRSE
percent ug/1
3
4
6
0,003 39
9,4
<5
7
9
0,176
0,055
10
It
12
13
14
15
0.23
16
17
0.076
0,074
is
19
20
21
23
24
26
27
0.099
2a
29
30
31
Moutbly Average Lint:
Monthly Average:
3.05 Maximum:
Unity Minimum:
No Reporting Reason: ENFRUSE = No Flow-Reuse/R
0.101857 39
0.23 39
39
9.4
9A
9.4
a
0
0 0
yele; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: I.
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING L©CATI©N: EFFLUENT DISCHARGE NO.: 009 NO DISCHARGE*: NO (Continue)
34010
u
t,t
0001
ab
T
111011
2400 clock
40
0
0
31.2
4
24
30
A
Monthly Average:
Doily Minimum: 1 1.2
"" No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation — Holiday

IYPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Tenminal {outfall 009)
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED; No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING L©CATI©N: EFFLUENT DISCHARGE NO.: 010 NO DISCHARGE*: NO
Sa03a
See Permit
Recorder
VI -ow
0.359
0.132
Monthly Average L
Mantaty Ave
50060
Monthly
Grab
CHLORINE
COS36
Monthly
36030
Quarterly
BENZENE
343,t
Quarterly
Grab
E1IIYLBEN
1 AE6C
Annually
Grab
VTHn24AC
percent
'A ALE
"• No Reporting Reason: ENFRUSE = No Flow-Reusc/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW _ No Flow; HOLIDAY = No Visitation — Holiday
Monthly
Grab
©IL-GRSE

N'PDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard Tenninal Company LLC
GRADE: PCNC
cDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4,0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGE
VERSION: 1,0
No
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 010 NO DISCHARGE*: NO (Continue)
2444 clock 11r2
2400 clock Hrs
34010
Quarterly
Grab
00070
Month!
Grab
n1u
91551
Grab
X3l,I43`E
3
7
10
11
12
13
14
L4
1,4
16
17
19
19
20
21
23
23
24
25
26
27
29
29
31
Monthly Average Limit
Monthly Avcritge:
Daily Maximum.
Daily Miroimaxn1
**** No Reporting Reason: ENFRUSE==No Flow•Rcusd
y
1,4
1.4
1.4
ENVWTHR No Visitation - Adverse Weather, NOFLOW No Flow; HOLIDAY = No Visitation - Holiday

NPDES PERMIT NO.: NC0021971 PERMIT VERSION: 4.0
FACILITY NAME: Charlotte Terminal (e utfall 009) CLASS: PCNC
OWNER NAME: Blanchard Terminal Company LLC ORC: Not Required
GRADE: PCNC ORC HAS CHANGED: N
eDMR PERIOD: 08-2017 (August 2017) VERSION: I.0
COMPLIANCE STATUS: Compl
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
SUBMISSION DATE: 09/25/2017
09/14/2017
ORC/Certifier Signature: Erin Risher E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part ILE.6 of
the NPDES permit.
Permittee/Sub
09/25/2017
Signature:*** Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: 7401 Old Mount Holly Rd Charlotte NC 28214 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Pace Analytical Services, Inc.
CERTIFIED LAB #:
PERSON(s) COLLECTING SAMPLES: J Qua Hied
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
PERMIT VERSION: 4.0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGE
VERSION: 1,0
No
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed
Outfall 009 - Effluent Comments:
Total Residual Chlorine was inadvertently tested in August and is being reported. Hydrostatic test water was not discharged from Outfall 009,

NPDES PERMIT NO.: NC0021971
FACILITY NAME: Charlotte Terminal (outfall 009)
OWNER NAME: Blanchard Terminal Company LLC
GRADE: PCNC
eDMR PERIOD: 08-2017 (August 2017)
Outfall 010 - Effluent Comments:
PERMIT VERSION: 4,0
CLASS: PCNC
ORC: Not Required
ORC HAS CHANGED: No
VERSION: 1.0
Fire suppression water was discharged, therefore Total Residual Chlorine (TRC) is being reported.
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 995491
STATUS: Processed

3
ARATft0
August 23, 2017
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
ECEIVED
AUG252017
CENTR !- FILE,
D'A/13 SECTION
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: 419.422,2121
Sent via Overnight Mail
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
**Enclosed: Signed hardcopy of eDMR submittal*'
Enclosed please find the July NPDES report, plus one copy, for the above -referenced permit. Also
included is the quarterly toxicity test.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at ErRisner a,MarathonPetroleum.com.
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)
NC DENR — Division of Water Resources
Water Sciences Section / Aquatic Toxicology Branch
1621 Mail Service Center
Raleigh, NC 27699-1623

NPDESPERMIT NO.: NC0046213
FACILITY NAME: Charlotte Tenninal
OWNER NAME: MpllxTerminals LLC
GRADE: PC-1 ' Jc' +"0.-44
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4.Ci
CLASS: PC-1
ORC: Terry Lec Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERTNUMBER: 9911C ,"rl. e, ,t
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHA
50050
t'0030
3403k
4,
TAE6C
4
34696 00356
YOZ: Pomot Mo
Record
us
Q
b
ly Qh arte
y
hob Grab
4AC
NAVERA E 011.GRSE
4t
6 ttr. v/nrn
nr
u
Pa
u
4
0 0.25 Y.
0,156
16
< 0.5
00
<10
4, 5
0.25 Y
04
7
4
9
A
30
Dully Maximum. 0 156
16
0
0
0
0 0
(Lily Minimum; 0,
104
16
0
0 0
"•"• No Reporting Reason: ENFRUSE - No Flow-Reuse/Recycle; ENVWTHR ==
Visitation —Adverse Weather; NOFLOW-No Flow; HOLIDAY—NoVisitation-Holiday

NPDES„PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
cDMR PERIOD: 07-2017 (July 2017)
4
7
10
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SAMPLING L©CATI©N: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2400 clock
2400 Noek
1107
ors YA1/N
0.25
0.25 Y
34010
Quarterly
Grab
TOLUENE
ubll
<1
Monthly
Grab
TI%U0115TY
81551
Grab
XYLENO
not ug/1
19
3
13
14
15
17
le
19
20
21
22
23
24
25
26
27
28
29
30
31
Monthlyy Average Y,inxit:
Monthly Average:
Pally Maximum:
Unity Mlntmums
0
0
19 0
19 0
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR w No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY == No Visitation
loliday

NPDES PERMIT NO.: NC00462 I
FACILIiV NAME: Charlotte Terminal
'OWNER NAME: Mplx Terminals LLC
GRADE: PC-,1
OMR PERIOD: 07-2017 (July 20171
COMPLIANCE STATUS: Complial
ORC/Certifier Signature: Terry
PERMIT VERSION: 4 0
CLASS: PC -I
ORC: Tcny Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processcx1
SUBMISSION DATE: 08/21/2017
Swick E-Mail:[e-mail] Phone #:[phone]
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
08/15/2017
Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list ofcorrective actions being taken and a time -table for improvements to be made as required by part 11E6 of
the NPDES permit.
08 2 2017
Permittee/Submi Signature:*** Angela S Brown E-Mail:[e-mail] Phone #[phone] Date
Permittee Address 5 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the inforrnation submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penaltks for submitting false information, iluding the possibility of fines and imprisonment for
knowing violations.
LAB NAME:Ptism Laborstorics1n.
CERTIFIED LAB #: 402
PERSON(s) COLLECTING SAMPLES;
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenr,org/welativq/swp/ps/npdcs/forms.
FOOTNOTES
Use only units ofmeasurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge Fmm Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC SG .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(bX2XD),

NPDES,,PERMIT NO,: NC0046213 PERMIT VERSION: 4.0 PERMIT STATUS: Active
FACILITY NAME: Charlotte Terminal CLASS: PC-1 COUNTY: Mecklenburg
OWNER NAME: Mplx Terminals L.LC ORC: Terry Lee Swick ORC CERT NUMBER: 991168
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 07-2017 (July 2017) VERSION: 1,0 STATUS: Processed
Report Comments:
Analysis for Acute Toxicity was subcontracted to ETT Environtnental, Inc, (Certified Lab #022), The analytical report for Acute Toxicity (Parameter Code TAE6C os being
submitted with hardcopy of DMR.

(C&4) 077'43: i2 . rA). (864) 0
RO Box 1 E414, Greenv tip, St 2960e,
4 Craftsman Cs trl, Greer, 5C 298.50
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON PETROLEUM
Facility: WEST
Prism Sample I➢: 001 Outfall
Test Reviewed and Approved I3y:
Robert W, Kelley, Ph.i..
QA/QC Officer
Test Date: 07-Jul-1.7
Laboratory ID #: T49555
Farhad Rostampour
Laboratory Director
Certification #E87819 t 'IbIWII l.. Certification #23104
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Honda Dept. of Health. Included results pertain only to provided samples.
Page 1 of 4
NCDENR Certification # 022

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Facility; MARATHON WEST
Te
Signature of Operator in Respeolsiible Charge
/
X
Signature of Laboratory Supervisor
MAIL ORIGINAL TO
c
NTROL ORGANISMS
# Young Produced
Adult (L)ive (D)ead
Effluent %
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L)ivo (D)eed
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
LC501Acute Toxicity Test
LC50=
05% Confidence Limits
NA % NA o,
d
2
2
4
4
Method of Determination
Moving Average Probit
Spearman Kerber Other
NPDES# NC
7
7
8
Date 11-Jut-17
Pipe # 001 County: Mecklenburg
Comments
10
10
11
11
Collection (Steil Date
Sample 1 06-Jul-17
Sample 1
Sample 2
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
12
12
Grab Comp Duration
X
s
Hardness (mg/L)
Spec, Condi(urnhos)
Chlorine (mg/L)
Sample Temll at receiptiCJ
start/and
7.6
7,2
pH
7.6
7.5
Chronic Test Results
Calculated t=
Critical Value=
Reduction=
% Mortality
Control
Treatment 2
Control CV
% 3rd Brood
Control
High Conc.,
Avg., Reprod.
Control
Treatment 2
PASS
FAIL
1st 2nd
ox r04
Sample Sample
start/and
7,8
6,7
D.O.
7.3
7.6
Page 2 of 4

n
S
07/07/t7
Ti
24 Hour Acute Toxicity Test
Test Method. EPA 821 R-02.012 Method 20E10 Pimephales pr
2:45
nd Date: 07/0$/I7
Fathead Minnows
Time; 02
Test Vessel
500 mL plastic cup
N
TEST ORGANISMS
for Ceriodaphnics'dubia
Date Removed:
Pimephafes promelas
Mysid©psis bahi
Between:
Test Solution Volume
200 mL
holding vessel
and:
Source: ABS 7/6/ 17 fays old: 5
Source: Days old:
Test Or
Conc,
Control
6.3%
12.5%
25.0%
50.0%
100.0%
A
13
B
A
B
ed by. JC Ti
MORTALITY DATA
11000,1
araanicine
10
10
10
10
10
10
10
10
10
Cumulative Mortality
0
24he Ali to- 72br 9t br
0
0
0
0
C
A
B
C
10
10
0
Final
Moliutty
0%
0%
pie ID: MARAT
Set By: JC
Ended By: FJ
Incubator
#1
Transfer Volume
0.5 mL
hrli$hf/6hr
Dilution Weter
Soft Synth 140H)
Comments:
ORGANISMS HATCHED 7/2/17 B/W 1000-1130MDT
SSF 7/7/17A
Page 3 of 4
Page 10of11 I

(Composite only)
Compullo Sind Dail Time
(Ore
Sample C
or Composite)
atindoa Due
Sign, and Print below
die dotted line
Collarled by
C
rog
0 0
Ca
©:.. CUSTODY RECORD
ntnl
ers
P res
1-H15o4
1-}ICL
3-HNn3
44440H
6- Mar
7� Iaha
Teal
Tent
Oro.
iample Cunto
Dote TI
#7-c —r7 (l
t7
Transfer Record
Relinquished By / Organization
d By / Organization
Analysis 8.0
Secure
Area
Receipt
Temp °C
Sample
Prose
:©MPOSITE
:omposile samp
Ime Proportion
vat minimum
1'rop©rt
G
©CEDURES
looted over a 24 hour period.
each hour for 24 hours. Equal volul
hours over 24 hours.
ions in NPDES permit.
TEMPE7MrURE MONITORING PROCEDURES
Sample 4empelature during collection and transport must be between
0.0 and.6.0i°C. Samples must not be frozen. Use water fee in sealed hags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

t• NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mph( Terminals LLC
GRADE: PC-1
eDMR PERIOD:06-2017 (June2CJJ7)
“"' No Re
PERMIT VERSION: 4,0
CLASS; PC -I
ORC:Tcr. LccS*vlck
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Act e
COUNTY: Mecklcnburj
ORC CERT NUMBER: i91168
STATUS: Processed
SAMPLING LOCATION: EFFLUEN' ' ©ISCIIARGE NO.: 001 NO DISCHARGE*: NO
rting
ason� GNFRUSF T No Flow ReuseiRccycle: ENVWTNR- No Visit
Adverse Weather; NVI LOW No Flow; HOLIDAY No Viiitati
d

p
r/ NPDES PERMIT NO.: NC0046213
FACILITY NAME: Chariot e Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
VERSIO
C•I
ORC: Terry Lee Swiek
ORC HAS CHANGED: No
eDMR PERIOD: t1t'i-2ii17 (June Ct1) VERSION: IA)
CONTACT PHONE #: [phone]
COMPLIANCE STATUS: Corn
PERMIT STATUS: Active
COUNTY: Mecktenburg
ORC CERTNUMBER: 99116
STATUS: Processed
SUBMISSION DATE: 07(18/2017
7/06/2017
ORC/Certifier Signature: Terry L.. Swick E-Mail:[e-mail] Phone #:704-392-i345 Date
By this s gt tune, 1 certify that this report is accurate and complete to the best of my knowledge.
The pertttittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the c
rtment,
Any information shall he provided orally within 24 hours from the time the permittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part11.E.6 of
the NPDES permit.
07/1Sf(-017
Permittee/Submitter( rgnature:*** Angela S Brown E-Mail:asbrownq,marathonpetroleum.com Phone #:[phone]
Permittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Prism Laboratories, Inc.
CERTIFIED LAB: 402
PERSON(9) COLLECTING SAMPLES: Scott Miller
Parameter Code as
CERTIFIED LABORATORIES
PARAMETER. CODES
obtaincd by calling the NPDES Unit [phone] or by visit
Use only units of measurement designated in the rep
ing faci
FOOTNOTES
's NPDES permit for reporting data,
„ncdenr.org/web/wq/swp/ps/npdes' o
Date
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
`• ORC on Site?: ORC must visit facility and document visitation of facs'lrty as required per 15A NCAC 8G .0204.
" * Signature of Permittee, If signed by other than the perrniuee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(bX2)(D).

8ThO
July 19, 2017
NC DENR / DWR.
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail. Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
**Enclosed: Signed hardcopy of eDMR submittal*
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via ©vernijzht Mail
Enclosed please find the June NPDES report, plus one copy, for the above -referenced peiinit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Scerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

SAMP
PERMIT VERSION: 4.0
CLASS:PC-, -RECEIVED
ORC: Terry Lee Swirl
ORC HAS CHANGE
VERSION: 1 0
JUN 1 6 2017
Jta
CENTRAL FILES
DWR SECTION
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER:I1f
NG LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISC
""` No Reporting Reason. ENFRUS%Inre-ReusefRe.ycIe3 ENVWTUR Nu Visit©tit r •- _ 3 arse tVcasktcr, NOFLOW No Fkw. HOLIDAY — No Visitation —

E: PC-
46213 PERMIT VERSION: 4.0
: Charlotte Terminal CLASS: IT -I
E: Mplx Terminals LLC ORC: Terry LeetSwiek
ORC HAS CHANGED: No
R PERIOD: 05-2017 (May 2017)
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: —
VERSION: 1,0
CONTACT PHONE #: 4194
PERMIT STATUS: Ate '3,
COUNTY: Mecklenburg
ORC CERT NUMBER: 991'16/1
STATUS: Processed
SUBMISSION DATE.: 06/12/2017
k E-Mall:tiswickgmarathonmetroleum,com Phone
By this signature, t certify that this report is accurate and complete to the best of my knowledge.
06/0 7
4:704-392-1345 Date
The permit -tee shall report to the Director or the appropriate Regional Office any mmeompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the perminee became aware of the circumstances. A written submission shall also he
provided within 5 days of the time the perrnittee becomes aware of the circumstances,
If the facility is noneornpliant, please attach a Est of corrective actions being taken and a time -table for improvements to be made as required by part 11,F,.6 of
the NPDES permit.
06/12/20 7
Permittee/Submit Signature:*** Angela S Brown E-Mail:asbrownmarathonpetroleum.com Phone [phone] Date
Permittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the infonnation, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete, 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABORATORIES
LAR NAME: Prism Laboratories, Inc.
CERTIFIED LAB 4: 402
PERSON(s) COLLECTING SAMPLES: Sc
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal,ne,denrorgAvebfwq/sv ps n estfonns.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
*No How/Discharge From Site: Cheek this box if no discharge occurs and, as a result, there are no data to he entered fbr all of the parameters on the DMR
for entire monitoring period:
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
*** Signature of Pennittee: signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2I3
.0506(b)(2)(D).

NPDES PERMIT NO.'. NC0046213
FACILITY NAME: Charlotte Terminal
OWNER 'NAME: MAIN Terminals IA:
GRADE: PC-1
eDMR PERIOD: 0420t7 1_,LNLpril 3017)
fl
4
IS
RMIT STATUS: Actiye
PERMIT VERSION: 4.0
CLASS: PC-1 COUNTY: N..inckicniajl RECEVEDINCOPNRIEWR
MAY 2 3 Z°17 ORC CERT NUMBER: 99116K
ORC:`Teriy Lee Swick
MNY 3 f.b
ORC
"" CHANG": No CENTRAL FILES
VERSION: L2 DWR SECTIONSTATus:
sed
WQROS
MOORESM REC4(WAI r",c' '—
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: NI NO DISCHARGE*: NO E
Ontk
Stattatty
DA 57
(LI I 1
C09.0
MonLMv
Grob
Com
4onthlo
OfiCrl
tiTHVIAIIM
QuAttr,h,
Gran
mosztnar
Quartet
Groh
Month I y
• ••• No Reporting Reason] ENFRUSE No Flow-ReosotRonyclet ENVWTHR No Visitation — A.dverst Weather, NO171...OW -No Flow; HOLIDAY No Viiitation - Holiday
Month
Grsb
MEN:1U

NPDES PERMIT NO.; NC004621,
FACILITY NAME; Charlotte Terminal
OWNER NAME: Mpb Terminals LIC
GRADE:pc:1.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION; 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 99116
STATUS: Processed
SAMPLING LOCATION: EFFLUENT »ISCBARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Quartepy,
lotogat
tarred
(.1
MENE
•••• No Reporting Reamt: ENFRUSE No Flow-Rowe/Recycle: ENVWTHR No Visitation - Adverse Weather: NOFLOW No Flow, HOLIDAY No Visitation — I loliday

NPDES PERMIT NO.: NC004621.3
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mjilx Terminals LLC
GRADE: pC-1
eDMR PERIOD: 04-2017 (April 2017)
COMPLIANCE STATUS: Compliant
OR.C/Certifier Signature: Terry
PERMIT VERSION: 4,0
CLASS: PC -I
ORC: Terry Lee .Swick
ORC HAS CHANGED: No
VERSION: LO
CONTACT PHONE 9: 4194019
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: 03/19
201 7
ick [e-mail] Phone #704-392-I345 Date
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge.
The perrnittee shall repot/ to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the pennittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the pennittee becomes aware of thc circumstances,
If the facility is noncompliant, please attach a list of corrective actions being taken and a tiane-table for improvements to be made as required by part II.E.6 of
the NPDES permit.
Permittee/Submi
Permittee Address.
05/19/2017
ignature:*** Angela S Brown [e-mail] Phone #:[phone] Date
5 Mount Bony Rd Pasv Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on any inquiry of the person or persons who managed thc
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, mac,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Prism Laboratories,
CERTIFIED LAB 41402
PERSONW COLLECTING SAMPLES: David Morris
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Cheek this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period,
** ORC on Site? ORC must visit facility and document visitation of facility as required per 15A NCAC 8G ,0204.
*** Signature of Perrnattee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per I5A NCAC 213
.0506(b)(2)(D).

NPDES PERMIT NO,: NC0046213
FACILITY NAME: Chariotae Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: f14,2ft17 (April ?C}17)
Outfall 001 - Effluent Comments:
Analysis for Acute Toxicitty was subcontracted
submitted with hardcopy of OMR.
On April 24, there
0,102 MOD was discharged
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
,te discharges due to incomi
022
0, 0,034
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: V)1161
STATUS: Procv'seri
cute. Toxic' {Para
d, at 0110
bei
discharged, and at 13:00,

Y
CA
April 17, 2017
R
Pace Analytical - Huntersville NC
Sample Delivery Group: L901963
Samples Received: 04/12/2017
Project. Number: 92336728
Description: West Oak Toxicity
Report To:
POR
Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By:
Jimmy Hunt
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures; 060302, 060303, and 060304,

TABLE OF CONTENTS
ar;?: NATiONWVE It*
1Cp: Cover Page
2TcsToble of Contents
3Ss: Sample Summary
4Cn: Case Narrative
sSa Sample Resutts
OUTFALL 001 1901963-01
%I: Glossary of Terms
Accreditations & Locations
aSc: Chain of Custody
3
4
5
6
7
8
4Cn
6
GI
Sc
ACCOUNT:
Pace Analytical - Huntersville NC
Page 4 of 12
PROJECT: SDG; DATE/TIME : PAGE:
92336728 L901963 04/17/17 17:07 2 of 10

SAMPLE SUMMARY
Aquatic Toxicity by Method 2000
WG970659
Dilution Preparation Anafysis
date/time date/time
1 04/12/1714:10 04112/1714:10
Analyst
SWS
4
Cn
6
GI
Sc
ACCOUNT:
Pace Analytical - Huntersville NC
Page 5 of 12
PROJECT: S©G: DATE/TIME: PAGE:
92336728 L901963 04/17/1717:07 3 of 10

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ)
values reported for environmental samples have been corrected for the dilution factor used in the
analysis. All Method and Batch Quality Control are within established criteria except where addressed
in this case narrative, a non-conformance form or properly qualified within the sample results. By my
digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the
laboratory as having the potential to affect the quality of the data have been identified by the
laboratory, and no information or data have been knowingly withheld that would affect the quality of the
data.
Jimmy Hunt
Technical Service Representative
Project Narrative
Please review all information in this report for accuracy and completeness. Contact our office within ten days if there are any
questions.
Chronic Test Methods are described in "Short Term Methods for Estimating the Chronic Toxicity of Effluent and Receiving Waters
to Freshwater organisms" (EPA/600/4-89/001).
The Biomonitoring results in this report are only a summary of the tests performed. A detailed report will follow, The detailed
report (not this summary sheet) must be submitted to the appropriate regulatory agency.
s
GI
6
SC
ACCOUNT:
Pace Analytical - Huntersville NC
Page 6 of 12
PROJECT: SDG: DATE/TIME: PAGE:
92336728 L901963 04/17/17 17:07 4 of 10

OUTPALL 001
Collected date/time: 04/11/17 07:30
SAMPLE RESULTS - 01
1901963
itti1 11(>NVNIDE 40!
AqUatiiC TOY. iCify bit/ ?.1100
Result
Analyte
24 Hour LC50 - Minnow
Qualifier Analysis
date / time
04/12/201714:10
Batch
WG970659
4
Cn
6G1
Sc
ACCOUNT:
Pace Analytical -Huntersville NC
Page 7 of 12
PROJECT: SDG: DATE/TIME: PAGE:
92336728 L901963 04/17/17 17:07 5 of 10

GLOSSARY OF TERMS
Abbreviations and Definitions
SDG
Sample Delivery Group.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
4
Qn
e
Sc
ACCOUNT:
Pace Analytical - Huntersville NC
Page 8 of 12
PROJECT: SDG: DATE/TIME: PAGE:
92336728 L901963 04/17/1717:07 6 of 10

ACCREDITATIONS & LOCATIONS
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory, No other
lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the
network laboratories in our industry. The most significant benefit to our "one location" design is the design of our laboratory campus. The model is conducive to accelerated productivity,
decreasing turnaround time, and preventing cross contamination, thus protecting sample integrity, our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
• Not all certifications held by the laboratory are applicable to the results reported in the attached report.
State ALl., lk';'l111,rt ttu1r;
Alabama 40660
Alaska UST-080
Arizona AZ0612
Arkansas 88.0469
California 01157CA
Colorado TN00003
Conneticut PH-0197
Florida E87487
Georgia NELAP
Georgia' 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky' 90010
Kentucky 1 16
Louisiana A130792
Maine TN0002
Maryland 324
Massachusetts M-TN003
Michigan 9958
Minnesota 047-999.395
Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-05-15-05
Third d Party & Fedora
A2LA — 15017025 1461,01
A2LA — ISO 170255 1461.02
Canada 1461.01
EPA—Crypto TN00003
Nevada
New Hampshire
New Jersey—NELAP
New Mexico
New York
North Carolina
North Carolina'
North Carolina'
North Dakota
Ohio—VAP
Oklahoma
Oregon
Pennsylvania
Rhode Island
South Carolina
South Dakota
Tennessee 14
Texas
Texas s
Utah
Vermont
Virginia
Washington
West Virginia
Wisconsin
Wyoming
AIHA-LAP,LLC 100789
DOD 1461,01
USDA S-67674
Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity ` Chemical/Microbiological s Mold """ Accreditation not applicable
t
cations
TN-03-2002.34
2975
TN002
TN00003
11742
Env375
DW21704
41
R-140
CL0069
9915
TN200002
68-02979
221
84004
n/a
2006
T 104704245-07-TX
LA80152
6157585858
VT2006
109
C1915
233
9980939910
A2LA
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies, If you would like assistance from one of our support offices, please
contact our main office, ESC Lab Sciences performs all testing at our central laboratory,
4
Cn
5
G1
Sc
ACCOUNT;
Pace Analytical - Huntersville NC
PROJECT:
92336728
SDG:
L901963
Page 9 of 12
DATE/TIM E; PAGE:
04/17/1717:07 7 of 10

Chain of Custody
itr z er: 2� 2#3 1 i rk d c N 1 l Toxic'
Kevin Godwin
Pace Analytical Charlotte
9800 Kinccey Ave. Suite 100
Hun a sv lIe, NC 28079
Phone [phone]
Email: kevin.godavi,'
Tuesday, Ali 11, 2017 ;3; A
G2Qg
x
4120
Page 1 of
Page 10 of 12

SAMPLE ID
cr.. C?wIK*01 va+ 6e,.
S,muM ids aunt es u.e*.a
CHAIN -OF -CUSTODY / Analytical Request Document
The Chinn-od-C usterdy is a LE.{3AL. DOCUMENT AM re want feelds must be completed accuratery.
Section C
Page 11 of 12

Sufficient volume sent?
f able
VOA Zero headsrace?
Pry ate Corry.:
Page 12 of 12

PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 03-2017 (March 2017)
m
2490 clock
4
6
9
10
11
12
13
14
IS
)8
17
20
19
20
21
22
23
25
22
27
29
29
30
31
VED/NCOENROWR
STATUS: Processed
WORM
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCMARGFALNQuoNAL OFFICE
I Composite Time
tlr
.111t
2400 dock
1615
0930
peretor Time Os Site
0,25
0.25
0
WIVN
Y
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
511050 e0530
Sc Permit Monthly
Recorder Grab
stow Tss Cone'
mgd nzgil
0.002 7.8
0,143
Monthly Average Limit
MfmthErage:
0,0725
Daily /11.1mum: 0 143
Daily Minimum 0 002
30
7.8
7,8
7,8
90.536
Monthly
Crab
OIL-611SE
mg/I
,c 5
0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: .
32731
Monthly
Grab
FlIEN, TO
or 1
, 0,05
0
00070
Monthly
Grab
1211111113TY
16
16
16
16
*.** No Reporting Reason: ENFRUSE No Flow-Reuse/Recycle; ENVWTHR = No Visitation — Adverse Weather; NOFLOW = No Flow; HOLIDAY No Visitation — Holiday
34020
Grab
BENZENE,
0
0

DES PERMIT NO.: NCl/04,2:3
FACILITY NAME: C,Sto:lotfo'fmningil
OWNER NANIE: Mr13 Tormmu L.LC
GRADE: 1'0 1
cOAIR PERIOD: 02-201.7 :Mir: 20171
COMPLIANCE STATES: Compliato
PERMIT VERSION: 4,0
'CLASS: PC-
ORC: Terry LSwk
ORC HAS CBANGEB:
VERSION: 1 „O
CONTACT PRONE 4: 4 1.942: ZOT9
PERMIT SiATES: AI:,:e
COUNTY: Mcci:lentosil
ORC CLWf NUMBER; 99110
STATUS: PrOCCSSed
SUBMISSION DATE: 044'1102017
411
ORCiCertifier Signature; Terry 4. Strict( marathonmetrolcitm..com Phone it:704-392.1345 Date
By this signature. I certify that this report is accurate and complete to the best of my knowtedgc.
The pennittec shall report to I Director or the .appropriate Regional Office any noncompliance that potentially threatens public health or the environsnent.
Any information shall be provided 'orally within ?A hours from the time the permittec became avvare of the cireumstaricesi A written submission shall also he.
provided within 5 days of the time the permitwe becomes aware of the circumstances,
If the facility is noncompliant, please attach a list of eorrective actions being taken and a time -table for improvements to he made a3 rt.‘xptirted by pan 1 1I0 of
the NPDES permit,
04118!20 7
Perrnitte.ei;iibirn: rnattire:**• Angela S Brown E-Mailtasbrown(kmarathonpetro cam,corn Phone rti419-471-2629 Date
Permitter Address: .1.135 Mount Holly Rd Paw Creek NC 2itt 130 Permit Expiration Date: 06i'30)2020
certify. under penalty of loss', that this document and al: attachments WeN prepared under my dircetion or supersision in accordance with a system designed'
to assure that qualified personnel properly gather ind011Ittate the information submitted, Based on iny inquiry: of the person or persons who managed the
sy•stein, or those persons directly responsible for gathering the. information, he information iobinitted is, to the hest of my knowledge and belief. true,
accurate, and .complcse. 1 um aware that there are significant penalties for submitting false. information, including the pos.sibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Prisln 1„;,lboralortcs. nc
CERTIFIED LAB 4: 402
PERSONts) COLLECTING SAMPLES:
PARAMETER CODES
Pariuncter Code assistance may be obtained ycatling the NPDES Unit [phone] or by visiting httptii'portaltici,lenr.orgi'webzwq'swpipsiiindesiforms.
HXYINOTtiS
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flo'sqDschare From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parufficterN on the D\IR
for entire monitoring period.
()RC on Site?: ORC must isit facility and document visitation of facility as. required per I 5A NCAC G 0204,
*** Signature of Permittee: If signed by her than the pennittre, then delegation of the signatory authority must be on file with the stow per 1.5A NCAC 2B
T)506(b)(2XD).

April 19, 2017
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
RECEIVE(
APR 2 0 2017
CENTRAL FILES
DWR SECTION
3
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via OverniRht Mail
Enclosed please find the MarchNPDES report, plus one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at ERRisnergMarathonPetroleum.com.
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

RECE VEL)
MAR 2 8 2Q17
A 0
CENTRAL FILES
DWR SECTION
March 23, 2017
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via Overnik
.tc,-7.IVEDINCOENRIDWR
WOROS
MOORESVRIE REGKNAL OFFICE
Enclosed please find the February NPDES report, plus one copy, for the above -referenced permit.
Also included is the quarterly toxicity test.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail],.
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

ERMIT NO.; NCM)46213
AGILITY NAME: Charlotte Term
OWNER NAME: Mpla Term}
GRADE; PC-1
eDMR PERIOD 02-20 17 (February 2017)
PERMIT VERSION: 4w0
CLASS: PC•1
ORC: Terry
ORC HAS CHANGED No
VERSION: 1,0
PERMIT STATUS; Aci vc
COUNTY: Mccklenbur
ORC CERT NUMBER; 9
STATUS; Processed
am. t..
"ez.,a>.
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGES': NO
it
IA
.CO530 bik5 k ,1173e
ly Al o hly
TSS=C.'temc Cit3rC:h1. Ptt
2
.♦.. No Reporting Reason' ENFRI
9,4
9.A
Recycle; I?.NV WTHR v No Visitation Adverse 1'deather; NO I,O W .0 No Flow; HOLIDAY w No Visitation - Holiday

PERMIT NO.: NC0046213
ITY NAME: Charlotte Terminal
R NAME; Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD; 02-2017 (February
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: Terry
By this signature, I certify that this rep
PERMIT VERSION: 4,0
CLASS: PC-!
ORC: Terry Lee ick
ORC HAS CHANGED: No
VERSION; 1,0
CONTACT PHONE it: 41942 2019
u
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC cERT NUMBER: 991168
STATUS: Processcd
SUBMISSION DATE:
03 7
Swick E-Mail:[e-mail] Phone #:[phone] Date
d
e best y knowledge.
The permittee port to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall he provided orally within 24 hours from the time the permittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part ILE.6 of
the NPDES permit.
03/21/2017
Perm u Signature:"* Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Permittec Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date; 06/30/2020
I certitY, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: Prism Laboratories, Inc.
CERTIFIED LAB it: 402
PERSON(s) COLLECTING SAMPLES:
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http.//portal.ncdenr. )!,/ • q)/wq/swpips/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state A NCAC 213
.0506(b)(2XD).

POLS PERMIT NO.: NC0046211
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 01-2017 (January 2017)
09
.91
91
PERMIT VERSION: 4,0
CLASS: PC-1
V E LINTY: Mecklenburg
ANGED: No
ORC:R E E Terry 'Lee Swick IC CERT NUMBER: 991168
ORC HAS CH
VERSION: 1.0
PERMIT STATUS: Active
R ECENEDINCDEN R 'DWR
FEB 1 6 2017
S:TATUS: Processed
CENTRAL FILES
DWR SECTION
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DIS
ratW 'now Ou Su
ORC 011 Site?**
240 dock lire 2400 data 114-3 3713(0
3
4
5
7
a
9
10
12
13
14
15
08
17
111
19
20
21
22
23
24
25
26
27
28
29
30
31
No Reporting Rtaion*"
50450
See Punta
Recorder
FLOW
rued
c0534
Monthly,
Grab
'EFS Cour
34030
tvlonthly
Grab
BENZENE
ug.4
34371
Quarterly
Grab
ETU VLBEN
TAE6C
Quarterly
Grab
FEII024AC
percent
12417
Quarterly
Oran
MTBE
34696
Quarterly
Grab
94920010
69999
00556
Monthly
Grab
011.44aRSE
OFFfCE
92730
MontBly,,
(Ran
PHEW, 114
1410 0,25 O. F4
1345 0.25 Y 0,239
153 0 1129 V 0.234
Menthta Average Lintift
Monthly Averng.
0,220333
WOW MAXIMUM 0,234
Dully Minimum, 01 84
5,4
30
5 4
< 0.5
< 1
100
100
0
< 1 ()
19
< 0-)15
5.4
5.4
1(41
I 00
0
(1
0
••*" No Reporting, Reason: ENERLISE= No Flow-Reuse/Recycle; ENVWTHR No ‘Isitation — Adverse Weather; NOFLOW = No Flosv; HOLIDAY — No Visitation > Holiday
0

PERMIT NO.; NC0046213
FACILITY NAME: Charlotte Terminal
OWNIZR NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 01-2017 (January 2017)
3
4
6
7
11
10
12
13
14
15
46
11
I it
ID
20
21
22
23
24
25
211
27
20
211
31
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue
240 intk
11
11
Operator Arrivat Time
11
firs 2400 51058 Sirs
1410 0.25
1345 1115
1530 0.25
ORC Ou Site”
WIIIN
11
No Reporting Reason**.*
Monthly Average Limit:
34010
Qum:It:fly
Grab
TOLUENE
<
Monthly Away: 0
Daily- Maximum: 0
Daily Pillniontin: 0
Monthly
Grah
2.45111DT5
1181
8.7
8.7
8.7
8.7
82551
Quarterly
Grab
XYLENE.
11
0
0
."•• No Reporting Reason: ENPRUSE = No Flow-ReuseRecyclet ENVWTHR = No Visitation — Adverse Weather; NOELOW = No Flow; HOLIDAY =No Visitation - Holiday

Nprm7;s; PERMIT NO.: NCOt1462
FACII1TY NAME: Charlott,„! Tctpita
OWNER NAME: Mr:.‘ TVIII1i14{1.S
GRAPE: PC-1
eDNIR PI:At 101): 1 7 OtTuaty 2017)
COMPLIAN S S: Compliant
VERSION
C I..A SS: NI:
()RC; 'Ferry I.e5Sk
ORCI-IAS CHANCED: :so
VERSION
C()NTACT PH()'
PERMIT STATUS: Active
COUNTY: Mk...alenbur
ORC CERT NUMBER: 4 6.
STAflIS
Pro,:es,st*A1
SUBMISSION DATE:022'
02108 2017
ORCiCertifier Signature: Terry 1... Sw;ck Ila Phone :[phone] Date
thhs signature, I eerily that this rcp accurate 3 to the best of my knowledge.
The pennitice shall report to the Direetor or the apprepriate Regional (J17fice any noncoinpliatirc that poicntia4 threatens public healthor the environment.
Any informatim shall be provided orally within 24 hours from the time the permitter became swam of the circumstances. A written !aibinission shU also be
provided within 5 days of the lime the permutes beecines aware of the cire;=stances.
Ifthe facility is nonconipliant, please attach a list of correetiVe actions being taken and a nine -table for tinprovements to be i'id lS reotitred by part 11,E,6 of
ih NPDES permit.
0 2, 1 0!2.0 I 7
Pcrinitiee,`Stibiti er Signature,' AuttrItt S Brown E-NItitl:asbrciwwconarailionpettoletimcoin Phone it:419-42.1-2629 Date
Permittee NO15 Mount Ilolly Rti Paw Creek NC 2N130 Perini kspitation Date: 06'30'2020
1 e-ertify, under penally or law. shot this document and all attachments were premired under tay direction or supervioon n accordance with a system designett
to assure that quh1ed personoel properly gather and evaltiate the in formation siibmittrit Bused on MX inquiry of the person or persons V,ho managed
system. or those persons directly responsible for gathering the information, the information submitted is., to the best of iny knowledge and belief, true,
accurate, and complete, 1 am arx'are that there arc siplificant pentilties for submitting false information, iiieluding Ole possibility of lines and impri,soninent for
knowing violations,
(TRTIFIFD LABORATORlES
LAB NAME': t'r111 T:lbsITatorics.
CERTIFIED LAR 4t:' 402.
P ER SON ) COI LECH \G SAMPLES:: David Morns
PA RA ktf.i71,,R CODLS
Parameter ode assistance may be obtained by calling the PDES Unit (919) K07.6300 tri by visiting http,.,"-portatnedenr„org.'welVvvqlswp?psitipties.(forms.
FOOT',N'OT
Use only units of ineasorcmcni designated. in the rep:lrting facility's NPDES permit for reporting data.
*No Flov/Discharge From Site:. (..'herk this bofi 1 discharge (recurs and, as a result, there arc no data to be entered for ail of the parameters on the DNIR
for entire monitoring period,
ORC. on Site`.!: ORC most '. so facility and document visitation of facility as requrd per I 5A NCAC ((G *0204,
* • Signature of Periniv,ce., 1f signed by oilier than the pcninttee, then delegation of die signatory authority zmist be on 11:e with the stare per ISA NCA(' .213
.0506tbi(2)(1

PDES PERMIT NO.: INC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 01-2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
Report Comments:
Analysis for Acute Toxicity was subcontracted to ETT Enviro cntal, rtified Lab 22 The analytical report for Acute Toxicity (Parameter Code TAE6C0 is being
submitted with hardcopy of DMR.

won
r, (X Box 16414 Gfee),elle, EX: 296O6
61746642) . r AX 064) 677-6636
4 Craftsman i3fit, '30 29e50
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: PAW CREEK
NPDES NC0046213
Prism Sample ID: Pond
Test Date: 064a0-17
Laboratory ID #: T48348
Test Reviewed and Approved By:
Robert W. Kelley, PILD,
QA/QC Officer
C rfification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept of Health, Included results pertain only to provided samples,
Page 1 of 4
Forbad Rostampoor
Laboratory Director
SCDHEC Certification #23304
NCD.ENR Certification # 022

Facflx y MA
Effluent Toxicity Report Form - Chronic Psss/Fall end Acute LC50
ON PAW CREEK
ng Test'
TO
Control
Treatment 2
SWAcarte T
?ace 2 of
tt;t'+c.A xl Pipe # f
PH

or, MARATHON
t Date. iil106/17
hie
ST R
48 Hour Acute Toxicity Test
Test Lfielhae EPA 821 R-02-072 ; Meth€id 2000 PIma.heles
e: 03:30 PM
Toot Scdutton V
200 to L
oldln v
Ceriodaphns`a clu
Date Removed:
Pimephales promelas
Source;
and:
0 HATCHays old:
MORTALITY DATA
t1N Cuondativo Mortality
�t hr Y2 Rr na 151
22.0%
45.0%
60,0%
90,0%
100,0%
0%
0%
0%
0%
0%
Set 13y:
star Vo
0,5 mL
.t 1tf lirdark.
Soft Synth(40H)
Page 3 of 4

V.
FAL
PO 0o1(i41,nrM11, & 2g8074l4
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 2985D
Www„crTiCNvIRONFOr.e.rrAt..Cqt.
Client:
Facility:
State:
SAMPLEID
KPDES
, (Compo9ite oniy)
Coonpaalia Start Dior Time
Sample Custody Transfer Record
(Grob or COmpo5ba)
Sr,, la Called!. Doe Time
Sign, and Print belo
the dotted line
Collected by
CHAIN Or CUSTODY RECORD
Containers
r rev:motive
I-62804
1- HCL
3-HNO3
4-tio011
Zrukc
0 r
h u le EMecot Toxicity
Acute Chronic
Parameters
Toot Pr animas
Pe
TthU Analysis
Secure Receipt
Date Time Relin wished By / Or anization Received B /Oanto Area Terno °C
0S/2'S S4MPLINGfl?OCEDURES T&PZAUREMONtfOJUNOPROCEDU.
posile samples must be collected over a 24 hour period. Smp1e lenlpernture during collection and transport must be between
pordonal: 1 sample each hour for 24 hours. Equal Yalu 0.0 oed 6.OE°C. Samples must not be frozen. Use water ice In sealed bags.
at minimum, I sample every 4 hours ever 24 hours.
v Pro ' tab A rinurutionu in PDES ermit,
Sample
Preserved?
TIMEPROCEDURSS
icily testing 0 be used within 3h hours
ofsample collection (completion o co posite sample).
Sample may not be used atter 72 hours from sample collection.

„ES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC.
GRADE: PC-1
eDMR PERIOD: 12-2016 (December 2016)
2440 clock
3
4
6
9
le
11
;
12
13
14
15
16
17
46
19
20
21
22
23
24
29
26
27
211
29
34
31
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
RECEIVEDERMITSTATUS:Active
COUNTY: Mecklenburg
JAN 2 4 2017 ORC cERT NumBERMMEIVEDiNCDENRIDWR
CENTRAL FILES
MR SECTION STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISM
HD 240 61646
1510
1530
11
0
FIrs
0_25
0.25
0.25
ORC On Site'**
Y11455
7461041, Average Limit:
Monthly Averag.
06119 Maximum
Daily 141606664_
50050
See Permit,
Recorder
FLOW
0.001
0.143
0,16
(1,1(11333
0,16
0.001
C0.530
Monthly
Grab
T5F- Font
mel
9.5
30
9.5
9,5
9.5
04556
Monthly
Grab
011-4,1RSE
< 5
0
0
32734
Monthly
Grab
mg/1
0
04070
Monthly
Grab
TURBIDLY
ntu
17
17
17
17
”" No Reporting Reason: ENERUSE - No Flow-Reuse/Recycle; FNVWTIIR No Visitation Adverse Weather; NOFLOW - No Flow; HOLIDAY No Visitation — Holiday
ONAL. OFFICE
34430
Calculated
DENZ6.516.
0
0.5

DES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mpbt "Terminals LLC
GRADE: PC-1
eDMR PERIOD; 12-2016 (Decembor 2016)
COMPLIANCE STATUS: Compliant
ORC/Cer
PERMIT VERSION: 40
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: LO
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS; Processed
SUBMISSION DATE: 01/17/2017
01/12/2 0 1 7
Signature: Terry E. Swick E-Mail:t1swick '„marathonmetroleum.com Phone #:[phone] Date
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the pennittee be -comes aware of the circumstances,
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part 11E6 of
the NPDES permit.
01/17/2017
Permittee/Sub er Signature:*** Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABORATORIES
LAB NAME: Prism Laboratories, Inc.
CERTIFIED LAB #: 402
PERSON(s) COLLECTING SAMPLES: Scott Miller
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncdenrorg/web/wq/swp/ps/npdes/forms,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
* No Flow/Discharge From Site: Check this box ifno discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per I 5A NCAC 2.B
,0506(b)(2)(D),

PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: l 1-2016 {November 2016)
2400 clock
4
9
10
12
13
14
15
16
17
1$
20
22
23
25
26
27
20
20
3ti
'••' No Repo
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 99
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*
2400 cluck 'firs WHIN
1415 0.25
50050
See Pernne
Recorder
FLOW
4
Monthly Averegr 1,110111
Monthly Aucrugcv
holly M8xinr0m:
L1aily. Minimum:
Inge'
0.115
0,115
(1.115
C0030
Monthly
Grab
TSS- Cour
30
0
00556
Monthly
1511.-GRSE
n
0
0
❑: ENFRUSE = No Flow-Reuse/Recycle; ENVWTHR = No Visitation- Adverse Weather, NOFLO
32730
Monthly
Grab
MIEN, TR.
rel
<005
(1
0
00070
Moodily
3I0f 0
Grab Grab
TV11111i5TY BENZENE
ntu ugl
8.6
8.6 0
14,6
No Flow; HOLIDAY No Visitation - Holiday

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charkme Ten-1.011a!
OWNER NAME: Mplx Terminals. LAX
GRADE: PC-1
eDMR PERIOD: 11-2016 (Novembr2
comvuAr4cE STATUS: Compliant
PERMIT VERSION: 40 PERMIT STATUS: Active
CLASS: PC! COUNTY: MeekUnhurt'.
ORC: Terry Lee Swick ORC CERT NUMBER: 99)168
ORC HAS CHANGED: No
VERSION LO STATUS: Processed
CONTACT PHONE #: [phone] SUBMISSION DATE: 12/16/2016
12/16/20 6
ORC/Certifier Signature: 'ferry — Swiek E-Mail:ttswick,@marathonmetroleurn.com Phone W:704-392-1.345 Date
By this signature. I certify that this port is accurate and complete to the best of iny knowledge:
The pennittee shall report to the Director or the appropriate Regional Office any noncompliance that potntially threatens public health or the environment:
Any infommtion shall be provided orally within 24 hours from the time the permittee became aware of the circumstances, A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances,
lithe facility is noncompliant, please attach a list olcorrective actions being taken and a time -table for improvements to be made as required by part ILE:6 of
the NPDES permit.
12/16/2016
Permittee/Submi Signature:** Angela S Brown E-Maikasbrown@marathonpetrolcum,com Phone #:419-42I -2629 Date
Permittee Address: 35 MountHolly Rd Paw Creek NC 28130 Permit Expiration Date: 06/3012020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry ofthe person or persons who managed the
system, or those persons directly responsible tbr gathering the information, the information submitted is, to the best of nty knowledge and belief, true,
accurate, and complete. .1 ant aware that there are significant penalties for submitting false information., including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME; Prism Laboratories, Inc.
CERTIFIED LAB #: 402
PERSON(s) COLLECTING SAMPLES: Scott Miller
PARAMETER CODES
Parameter Code assistance may he obtained by calling the NPDES 'Unit [phone] or by visiting http://portal.nedermorgAmeb/wq/swpipsinpdestforms:
FOOTNOTES
Use only units of measurement designated in ibe reporting facility's NPDES permit for reporting data,
• No Flow/Discharge From Site: Check this box if no discharge occurs and, as a. result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per I 5A NCAC 8G ..0204:
*** Signature of Pennittee; if signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 1.5,A NCAC 2B
,0506(b)(2)(D):

3
ARAT 0
December 21, 2016
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via Overnikht Mail
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617 RECEIVED
RE: NPDES (DMR) Monthly Report DEC 28 2016
MPLX Terminals LLC
Charlotte Terminal CENTRAL FILES
8035 Mt. Holly Road DWR SECTION
Charlotte, NC 28214
NPDES Permit Number NC0046213
**Enclosed: Signed hardcopy of eDMR submittal**
Enclosed please find the November NPDES report, plus one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at ERRisner(i4MarathonPetroleum.com.
Sincerely,
Erin Risner
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

NPUFS PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME; Mplx Tenninals LLC
GRADE: PC-1
eDMR PERIOD: 10-2016 (October 2016)
zoo clock
4
6
9
10
11
12
13
14
15
16
17
IR
19
21
22
23
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE* t
Hrs
2400 clock firs
1520
945
viem
50050
See Permit
Recorder
FLOW
mad
Y 0.003
(1306
C0530 34030 34371
Monthly
Grab
mg/I
25
ily Quarterly
Grab Grab
one BENZENE ETHYLBEN
ua/i1
<0.5
TAE6C
Quarterly
Groh
24AC
percent
> I(10
22417
Quarterly
Groh
MTBE
<5
34696
Quarterly
NAPTHALE
< 10
00556 32730
Monthly Monthly
Grab
Grab
OIL-GRSE PHEN, TR
< 0,05
24
25
26
27
28
29
30
31
1100
0J)04
Monthly Average Limit;
Monthly Average:
Daily Maximum: 0.306
Doily Minimum: 0,003
30
0
0 0
(1 0
11
100
IOU
0
****NoReporting Reason: ENFRUSE=NoFlow-Rcusc/R.ecyelc; EvVWTHR= No Visitation- Adverse Weather; NOFLOW- NoFlow; HOLIDAY NoVisitation-- Holiday
0

TSPERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Tertnitutls LLC
GRADE: PC -I
eDMR PERIOD: 10-2016 (October 2016)
4
6
9
I0
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Teny Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
2400 clock II7s
2400 clock
1520
945
1100
Ors
0.25
0,25
0.25
Ylll/N
Monthly Average Limit:
Monthly Average:
34010
Quarterly
Grab
TOLUENE
ug/I
<I
**** No Reporting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENVWT
R
00070
htonthly
Grab
TUR9ODTY
81551
Lluanerly
Grab
XYLENE
<3
0
0
Adverse Weather; NOFLO W � No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0046
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRA DE: F!C.- I
eDMR PERIOD: !O-2016(Octth.r2Q1
COMPLIANCE...fool
ORC/Certifier Sig
PERMIT VERSION: 4,0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
CONTACT PHONE 0: 70439,21345
ure: Terry L. Swiek
PERM Fr STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: 6
11/29/2016
arathonmetroleum.com Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the hest of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment,
Any information shall be provided orally within 24 hours from the time the pemiittce became aware ofthe circumstances, A written submission shall also be
provided within 5 days of the time the pennittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
the NPDES permit.
29/2016
Perm ittee/Subn Signature:** Angela S Brown E-Mail:[e-mail] Phone #:[phone] Date
Permittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to thc hest of tny knowledge and belief, true,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAO NAME; Prisrn Labo toftds,
CERTIFIED LAB #: 4
PERSON(a) COLLECTING SAMPLES: Scott Miller
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting futp://portal,ncdenrorgAvehAvq/swp/ps/npdes/fomis.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box ifno discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
*** Signature of Permittee: If signed by other than the Rermittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D),

NPDES PERMIT NO.: NCO046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 10-2016 (October2016)
PERMIT VERSION: 4.()
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: LO
Outfall 001 - Effluent Comments:
Analysis for Acute Toxicity was subcontcracted to ETT Environmental, [nc, (Certified Lab #022). The analydca
submitted with hardcopy of DM:R,
P
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
Acute Toxicity (Parameter Code TAE6C) is being

P,Q, Box 16414, Greenville. $C 29606
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: PAW CREEK
Prism Sample ID: 001 ©utfall
Teat Date: e6-oat-16
Laboratory ID#: T47838 AD
Tert Reviewed and Approved By:
t
Robert W. Kelley, Ph.D. Fulled Rostampour
QA/QC Officer Laboratory Director
I= Certification #E87819
Teat r suhr presented in flab report conibrm to all requirements of
NELAC, conducted under NELAC Certification Number 887819
Florida Dept of Health. Included result, pertain only to provided samples,
SCDHEC certification #23104
NCDENR Certification # 022
Page 1 of 4
Page 9 of 12

Iuent Toxicity
actit MARATHON PAW CREEK
La.. at o oTest:
t st
Rt nature co pe. t+ In (asp ns trli
Paeefl sli end Acute I.C6© Date
P©nbu
ETT Environmental, Inc.
aboratory Supervisor''
MAIL ORIGINAL TO
Borth Carolina Coria lh
CONTROL ORGANISMS
p Young Produced
Effluent %
TREATMENT 2 ORGANISMS
pH
Control
Treatment 2
D.O.
Control
Treatment 2
lal wimple
sleet end
tel sample
Or r anlsm Tested
Pass/Fall Rearoduction
2
2
tat aampie
Marl end
lsl wimple
4
4
2nd sample
elan end
2nd sample
Method of Determination
Average Problt
Karber Other
Page 2 of 4
x
v Tpst
Environmental 8olencss Branch
Div. of Water Quality
N.C. DENR
1821 Mall Service Center
Raleigh, North trckltna 27889-^tt
10 11 12
►Chront Teat Resu
Cetculated t=
Critical Value=
ductlon=
7.6
7.2
0.0.
6

MAAATTION
rt;
Date: 10/06/16
Date: 10/07/16
Coca,
Control
22.0%
45.0%
60.0%
90.0%
100.0%
A
A
D
Time:
Time:
Ted Vessel
MORTALITY DATA
ogodamil
I
10
10
10
Cuiu1 dv;Mortality
s*rx xrar
0
0
48 Hour Acute Toxicity Test
Ted Method: EPA 821 R-02.012 . Method 2000 Ptmephsteo penal*.
ID: PAW CREEK
12:50 PM
12:14 PM
Test BoIuton Volume
0
A
B
10
10
0
A
13
C
A
10
10
10
10
0`
0
D
0%
0%
0%
5%
Set By: JC
Ended By: JC
Page 3 of 4
Tranvia Volume
Lab 1D#: T47838 AD
Dilution Wita

(Coe x sire m1Y)
SAMPLE ID
op aiKV\c5t
co
•
(Grab or Composite)
Sign, and Print below
the dottrel tine
cur by
Program
Care CUSTODY RECORD
Containers Preservative
Parameters
Whale/HI Ti
Ten Orianbms
Chemical
0
nr
nple Custody Transfer co
Babe . Time clencu
COMPOSITE SAMI2LIN0 PROCEDURES
Composite samples must be collected over a 24 door period.
Time Proportional: 1 sample etch hourlbr 24 hours. Equal rota
or at minimum l sample every 4 hours aver 24 doors.
Flowkropoctioneh As per inatroctons in NPDES permit
Wed By / ©t4,aniz,tian
TEkPER,4TURE MONITORING PRoCEOWS
Sample temperltu a during collection and transport must be between
0.0 and 6.0 C. Samples must not be fres= Use water ice in sealed bags.
Secure
Area
Receipt
Temp °C
Sample
Preserved?

A
December 6, 201.6
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Teiininals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: 419,422.2121
RECEIVED
DEC 072016
CENTRAL FILES
DWR SECTION
Sent via ©vernieht Mail
Enclosed please find the October NPDES report, plus one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
Dawn Benjamin
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)
NC DENR — Division of Water Resources
Water Sciences Section / Aquatic Toxicology Branch
1623 Mail Service Center
Raleigh, NC 27699-1623

`NO.: NC0046213 PERMIT VERSION:4.0
"Y NAME: Charlotte Terminal CLASS: PC -I
OWNER NAME: Mplx Terminals LLC ORC: Terry Lee Swick
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 09-2016 (September 2016) VERSION: 10
PERMIT STATUS: Active
COUNTY: Mecklenbur*
ORC CERT NUMBER: 99
STATUS: Processed
SAMPLING L©CATION: EFFLUENT DISCHARGE NO.: 001 NO DISCjA
. N $
g
d
6
E B
t7 f»
�"^
F
•t
c
O
F
i`vz
4
V
*
ai
50050
C0530
34030
00556
32730
00070
See Permit
Monthly
Monthly
Monthly
Monthly
Recorder
Grab
Calculated
Grab
Grab
Grab
FLOW
TSS - Coot
BENZENE
OIL-GRSE
PHEN,TR
TURBIUTY
2400 clack
Hro
24011 clock
Sirs
Y!B/N
mgd
nrg(I
ug/I
mell
nrg/l
ntu
4
6
1510
0,25
Y
0.001
13
<0.5
<5
<0,05
15`
7
9
10
11
12
13
14
I5
16
17
18
19
20
21
22
23
24
25
26
1000
0,25
Y
0.457
27
620
0.25
Y
0.501
28
29
925
0.25
Y
0.057
30
Monthly Average Limit:
30
Monthly Avcroget
0.254
13
0
0
0
18
Daily Maximum:
0.50I
13
0
0
0
IB
Daily b13Utmumr
0,00)
13
(1
0
0
18
4*** No Repotting Reason: ENFRUSE = No Flow-Reuse/Recycle; ENV W7"FIR = No Visitation - Adverse Weather; NOFLOW = No Flow; HOLIDAY = No Visitation - Holiday

PDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER. NAME; Mplx Terminals LIC
(;RADE pC-1
eDMR PERIOD: 09-2016 1Septembe 6)
COMPLiANCE: Compliant
ORC/Certifier Signature: Terry
PERMIT VERSION; 4 0
CLASS; PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE N; 7043921345
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 9916
STATUS: Processed
SUBMISSION DATE: 10/28
0 0
6
ck E-Mail:[e-mail] Phone 4:704-392-1345 Date
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time thc permittee became awarc of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part 11.E.6 of
the NPDES permit.
10/28/2016
Permittec/Submittcr S a ure:**• Angela S Brown E-Maikasbrown©marathonpetroleum.com Phone 4:419-421-2629 Date
Permittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty °flaw, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the infomiation, the infomiation submitted is, to the best of my knowledge and belief, trIle,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME; Prism Laboratories, Inc.
CERTIFIED LAB fri; 402
PERSON(s)CoLLECTING SAMPLES: Scott Miller
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nederirorgfweb/wq/swp/ps/npdes/fonns,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box lino discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and docutnent visitation of facility as required per I 5A NCAC 8G .0204.
*** Signature of Permince: If signed by other than the permittee, then delegation of the signatory authority must be on tile with the state per 1 5A NCAC 2B
.0506(b)(2)(D),

November 4, 2016
NC DENR / DWR
Information Processing Unit
Attn: Central Files / eDMR
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) Monthly Report
MPLX Terminals LLC
Charlotte Terminal
8035 Mt. Holly Road
Charlotte, NC 28214
NPDES Permit Number NC0046213
Enclosed please find th
MPLX Terminals LLC
A subsidiary of Marathon Petroleum Corporation
539 South Main Street
Findlay, OH 45840
Tel: [phone]
Sent via Overnight Mail
RECEIVED
NOV 09 2U16
CENTRAL FILES
DWR SECTION
us one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or by
email at [e-mail].
Sincerely,
(t)
Dawn Benjamin
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)

PERMIT NO.: NC0046213
'AMITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 08-2016 (August 2016)
4
6
7
9
10
11
12
13
14
15
16
17
18
19
20
21
22
24
26
28
29
30
PERMIT VERSION: 4J0 PERMIT STATUS: Active
CLASS; PC-1 COUNTY: Mecklenburg
ORC: Terry Lee Swick ORC CERT NUMBER. 9
ORC HAS CHANGED: No
VERSION: 1.0
STATUS: Processed
E DIN COEN ROW R
or: 1 Wok
Lon v
r4
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCIIARGE-ti NEVON!Ni. Orr ICE
tfi
2400 clock tars
rator Arrival Time
2400 clock
1500
7110
9211
1352
1319
Operator Time Ott Site
Hrs
0.25
0,25
0.25
0.25
0,25
ORC �n Site?"
Y
Ttlonthly Average Limit:
50050
See Permit
Recorder
FLOW
mgd
_0.01
0,02
0,072
0,076
Monthly Average: 0516
Daily Maximum:200
Daily Minimum: 001
C0530
Monthly
Grab
TSS Conc
4,3
4.3
43
34030
Grab
BENZENE
ugl
, 0,5
0
00556
Monthly
Grab
OIL-GRSE
< 5
0
32730 0007U
Monthly Monthly
Grab Grab
PHEN, TR TURBIDTY
5101 ntu
<0.05 5.2
RECE
1VED
CT 04 /OIh
CEN RAI:FILES
DWR SECTION
52
0 5,2
*III" No Reporting Reason: ENFRLISE No Flow-Reuse/Recycle; ENVWTEIR = No Visitation — Adverse Weather; NOFLOW No Flow; HOLIDAY = No Visitation — Holiday
5.2

NJDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME; Mph.: Terminals LTC
GRADE: PC-1
eDMR PERIOD: 0a-2016 (August 2016)
COMPLIANCE: Compliant
PERMIT VERSION: 4J0 pERma STATUS: Active
CLASS: PC-1 COUNTY: Mecklenburg
ORC: Terry Lee Swick OMCCERTNIJMI8IiR:991168
ORC HAS CHANGED: No
VERSION: 1,0 STATUS: Processed
CONTACT PRONE th 704392134,5 SUBMISSION DATE; 7/2016
9 6/2016
ORC/Ccrtifier Signature: Terry L. Swick E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I. certify that this report is accurate and complete to the best of my knowledge.
The pertnittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environtnent.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also he
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part 1LE,6 of
the NPDES permit.
09 2 2016
Permittee/Subn .:*** Angela S Brown [e-mail] Phone N:419-421-2629
Pennittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Perini' Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false inform.ation, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Prism Laboratories, Inc,.
CERTIFIED 1ABtt: 402
PERSON(s) COLLECTING SAMPLES: David Morris
Date
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting lutp://portal.nedenrorg/web/wq/swpips/npdestfonns.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit fur reporting data.
• No Flow/Discharge From Site: Cheek this box lino discharge occurs and, as a result, there arc no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC must visit facility and document visitation of facility as required per I5A NCAC 8(3 .0204.
*** Signature of Pennittee: If signed by other than the permittce, then delegation of the signatory authority must be on file with the state per I5A NCAC 2B
.0506(b)(2)(D).

ES PERMIT NO.: NC0046213 PERMIT VERSION: 4.0
FACILITY NAME: Charlotte Terminal CLASS: PC -I
OWNER NAME: Mplx Tern -in -Ws LLC ORC: Terry Lee Swick
GRADE: PC-1 ORC HAS CHANGED: No
VERSION: 1,0
eDMR PERIOD: 07-2016 (.1341y 2016)
6
g
2400 clock
4
10
13
14
17
IN
19
20
22
23
24
25
27
28
29
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER:
VED/N CD EN RID WR
STATUS; Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHN
II, 2400 cluck
730
rater Time On Site
flra
0.25
0,25
RC On Site'••
NIB/ N..'
50050
*E• See Permit
.27 Recorder
g
`2. X FLOW
mgd
0.00 I
0 024
•
Monthly Average Limit:
Monthly Average: 0,4,25
Daily Maximum« 04424
Daily Minimum: 0.001
C0530
Monthly
Crab
TSS Cone
ing/1
9
30
9
9
9
34030
Monthly
Grab
BENZENE
u.g/1
0.5
0
34371
Quarterly
Grub
ETHYL BEN
ug/l
< 1
TA E6C
Quarterly
Grab
FT1-1924AC
> 100
100
100
100
22417
Quarterly
_Grab
MT BE
5
0
0
SEP -r 2c16
VAOROS
ceiNVREGIONAL. OFFICE
34696 00556 32730
Quarterly Monthly Monthly
Grab
Grab Grab
NAPTHALE 01143R.SE PHEN, TR
ugI
mg/3 mg/1
<10 <5
75377/' intri=„ EVE
AUG 2 6 2016
(..ENFIL.FS
Tif,Drq
**" No Reporting Reason; ENFRUSE = No Flow-Reuse/Recycle; ENVWIFIR - No Visitation -,Adverse Weather; NOFLOW = No Flow; HOLIDAY' =No Visitation -- Holiday
a.05
0

ES PERMIT NO,: NC0046213 PERMIT VERSION: 4,0
FACILITY NAME: Charlotte Terminal CLASS: PC-1
OWNER NAME: Mplx Terminals LLC ORC: Terry Lee Swick
GRADE: PC-1 ORC HAS CHANGED: No
eDMR PERIOD: 07-2016 (July 2016) VERSION: LO
4
9
10
33
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
5 a
perat©r Arrival Time
2400 dock lirs 2400 clock
730
13
14
15
16
17
18
20
21
22
23
.24
25
26
27
29
29
31
ratar Time Ott Site
Hrs
0,25
0.25
C On Site?"
'OWN
Y
34010
Quarte!ly
Grab
z TOLUENE
<
Monthly Average Limit:
Monthly Awltget
Dully 'Maximum: 0
Dully Minimum:
00070
Monthly
Grab
TURBIDTY
9,3
9.3
9.3
9.3
81551
quarterly
Grab
NYLENE
<3
0
•"* No Reporting Reason: ENFRUSE = No FlowReuse/Reeyele; ENVWTFIR - No Visitation — Adverse Weather; NOFLOW No Flow; HOLIDAY No Visitation -- Holiday

S PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
eDMR PERIOD: 07-2016 (July 2016)
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
STATUS: Processed
Outfall 001 - Effluent Comments:
Analysis for Acute Toxicity was subcontracted to ETT Environmental, Inc. (Certified Lab #022), The anaytical reporttor Acute Toxicity (Parameter Code TAE6C) is being
submitted with hardcopy of DMR.

NPDES PERMIT NO,: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC-1
e0MR PERIOD: 07-2016 (July 2016)
COMPLIANCE: Cernpliant
PERMIT VERSION: 4.0
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
CONTACT PHONE it:7043921345
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 9.
STATUS: Processed
SUBMISSION DATE:
ORC/Certifier Signature: Terry L Swick E-Mail:[e-mail] Phone ft704-392-1345 Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittce shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances,. A written submission shall also be
provided within 5 days of the time the pennittee becomes aware of the circumstances,
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part 11,E.6 of
the NPDES permit.
0 I 6
Permittee/S Signature:*** Angela S Brown E-Mail:asbrown@marathonpetroleurn,com Phone #:[phone] Date
Permittee Address., 8035 Mount [lolly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Prism Laboratories, Inc.
CERTIFIED LAB 0: 402
PERSON(s) cou,Ecrolc SAMPLES: Scott Miller
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portahncdenr.org/web/wq/swp/ps/npdes/fomis„
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES pennit for reporting data,
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period„
** ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G ,0204,
*** Signature of Permittee: If signed by other than the perrnittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D)„

PO Box 14414, Gr vlie„ SC 29606
(660 877.6442 . FAX [phone]
4 Craftsman Court, Grp, SC 29650
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: PAW CREEK
Prism Sample ID: 001
Test Date: 06-Ju1-16
Laboratory ID#: T47279 AD
Test Reviewed and Approved By;
ad- 474
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC officer Laboratory Director
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
SCDHEC Certification #23104
NCDENR Certification # 022
Page 1 of 4
Page 8 of 11

Effluent Toxicity Report Fo
Fi lit : MARATHON PA k CREEK 00
X
Signature of 0
X
Signature of
orato
pe
is
- Chronic Pa
harge
Fe
dA
LC50
Comments
©ate
Coun
11.Iu1-1 e
nbur
MAIL ORIGINAL TO
North CproIJna Carlo gtpohnia.CI rot3ic Pass/F 1&E Reproduction Toxicity Test
CONTROL ORGANISMS
Produced
Effluent %
TREATMENT 2 GRGANISMS
Young Produced
pH
Control
Treatment 2
start end
D.O.
Control
Treatment 2
2
start and
1st sample
4
4
start and
LC50/Acute Toxic ity+ Test
DE i4t Form AT-1
Page 2 of 4
10 11
10
11
Environmental Solomon Branch
01v, or Water Quality
NwC. DENR
1621 Mall Service Canter
Ralalghr North Carolina 27666-11
pH
ttorllo Test Results
t:alculated t=
Critical Value=
12 Reduction=
.a�
12
T
1st 2nd
Tox Tox
not frozen
D.O.

48 Hour Acute Toxicity Test
Tost Mathodc EPA 821 R-02-012,Method 2000 Plmephales premakes;
A n4614 fA11V C1
07/06/16
Time: 1600
Thine: 04:42 PM
Test Vessel
Test Solution Volume
DAY
T
Cum
Control
22.0%
45,0%
60.0%
90.0%
100.0%
Rep.
A
13
A
T
MORTALITY DATA
Weal M
organism.
10
10
10
Cumulative
0
le Iv aabY 72 br 9a er
0
0
A
c
A
c
10
10
10
10
10
0
0
0
x
A
10
10
0
O
c
D
Finn!
M axiality
0%
0°
Oars
0%
Sample ID: 001
Set By; AM
Ended By JC
Incubator
Transfer Volume
Lab II #; T47279 AD
Page 3 of 4
Page 10 of 11

4
7414
[phone], (BOO) 891-2325 Fanc(884) 877 8938
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
W WW.6TTCNVIRONMENTA4.C©M
(Composite only)
Composite Sian Data Time
(©reb or Composite)
Sample Collection neta Time
a 24 hour period.
r 24 hours. Equal volur
4 hours over 24 hours
soma in NPDES permit.
Con
tni
F CUSTODY RECORD
ners
ram
Sign, and Print below
the dotted line
eeloci by
Pres
eu
te
realc
u
est
rgo
nisei
Parameters
I4CtSO4
>.o-IN0
4.NaOH
i=Atk
rw otter
cvne-
d By / Organization
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
Chemical Analysis & Other
Secure
Area
• Receipt
Temp °C
l 1771
HOLD TIME PROCEDURES
For toxicity testing the sarnple must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.
Sample
reserved?

ES PERMIT NO.: NC0046213 PERMIT VERSION: 4.0
FACILITY AVIE: Charlotte Terminal CLASS: PC-1
OWNER NAME: Mplx Terminals LLC ORC: Terry Lee Swick.
GRADE: PC -I ORC HAS CHANGED: No
eDMR PERIOD: 06-2016 (June 2016) VERSION: 10
4
13
14
IS
16
(0
20
21
22
23
24
26
27
29
30
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 99116
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
atilt Composite Time
..2400 ulock Ors
Operator Arrival Time
pera tor Time On Site
2400 clock Ws
1(130 0 25
C 0i Site.*
YIBIN
Monthly Awrage Lima:
50050 C0530
See Permit
Recorder
FLOW
Monthly
Grab
TSS t, Cone
mud eng/I
0,001 26
hlunthly Awelimgei 03001
Dolly Maximum:
Dolly Minimum: (11011
30
20
26
26
34030
Grab
BENZENE
< 0,5
00556
Monthly
Grab
011,,GRSE
rog,i1
<5
0
RE
32730
Monthly
;Grab
MEN, TR
O 0(
-itt 0,05
00070
Monthly
Grob,
TURBIDLY
010
5,2
CEiVED
CEN
DWR
TRAL FILES
SEC
0
TJON
"*. No Reporting R2000r1: ENERUSE - No FlowiRcusii/Reqcle; ENVWIFIR - No Visitation - Adverse Viicather; NOELOW - No Flowi HOLIDAY - No Visitation Holiday
RECEIVED/NCDENR/DWR
AV 01 2U16
WOROS
MOORESVILLE REGIONAL OFFICE
5.2
5.2
5.2

PERM(' NO.: NC:(!t}46213
FACILITY NAME; Chark
OWNER NAME:
[:RAVE: PC-1
cf»IK PERiOD: 06-2016 (June 2t316)
COMPLIANCE: Compliant
ina
:Certifier Signature:
By this sig
The permit
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circutn
provided within 5 days of the time the peranittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list ofcorrective actions being taken and a
the NPDES perm it,
u
is
PERM rr VERSION: 4.i?
(:LASS: PC-1
ORC: "terry Lee Sick
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE k: 7043v32t345
PERMIT STAT Active
COUNTY: Mecklenburg
ORC CER`r NUMBER: 991168
STA'rldS; Processed
SUHMIS tON DATE: 07/2it2tit6
07/21/2016
wick(a;rnarathonmetrolcum.cotn Phone 4:704-392-1345 Date
to the hest of
1 to the T)ire("tor or the appropriate Regional Office any noncompliance that potentia
s public health or the enyirc>ntncnt.
s. A written submission shall also be
eats to he made as required hyF part ILE.6 of
07/21/2016
PcrmitteeISuh ticr Signature:*** Angela S Brown h-ivMail:ashrownri?martthrstspetroleum:com Phone 4r:419-421-26.29 Date
Pcrmittee Address: 8035 Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my lit ction or supervision itt a€ eortisttt with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on toyr inquity of the person or persons who managed the
system, or those persons directly responsihlc for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for
knowing violations.
D LABt)RATORI1aS
LAB NAME; Pris
CERTIFIED LAB
PERSON(s) COLLECTING SAMPLES: ♦)avid ISatorns
PARAMETER CODES
Parameter Code assistance may he obtained by calling the NPDES Unit [phone] or by visiting http:/Iportal.ncdcnr.orglvv°
Use only units of measurement desi
FOOTNOTES
1acihty' NPDES permit for report'
ti
/npdelfonms.
* No How/Discharge From Site: Check this box ifno discharge occurs and, as a result, there are no data to he entered for all oldie parameters on Lk DMR
for entire monitoring period.
** ORC on Site?: ORC mull visit facilsiy and document visitation cif f ilit as required. per 15A NCAC 8G ,0204.
*** Signature of Pcrmittee; If sign
,0506(h)(2)(D).
by other than the permittee, then delegation of the signatory authority must he on file with the state per 15A NCAC 2f3

OWNER NAME: NIT/Ix Terminals L„I..0
GRADE: PC-1
cDMR PERIOD: OS- 61Mov 2016)
PERMIT VERSION: 3,0
CLASS: PC.-1
ORC: Terry Lee Svviek
ORC I-IAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC (.:ERT NUMBER: 99
STA
`US: Pr
SAMPLING LOCATION: EFFLUENT[' DISCHARGE NO.: 001 NO DISCHAI
2400 clock Fin 2400 clock Hrs
50050
See Per
Recorder
FI,OW
C0530 34010
00556
Monthly
00070
32730
Grab Grab
SS -Cone BENZENE
mg11 ug 1
Crab
C)1L-GRSE TURB
nlu
3
4
1400
)2
030
0,25
4
8
9
10
RECE
'ED
12
I3
14
15
CENTr
FLES
'T1ON
16
180.
19
22
23
24
25
26
1050
730
025
0,25
0 25
40104
Y 0.001
Y 0.033
27
28
29
311
Alonddv Averegr
,10
Monthly .Average 000333
Daily 131itximum: 0,033
Drily Minimum: 0 001
18 0
18 0
0
I8 0
*••* No Reporting Reason: fa.NFR1.3SE -- No Flow -Reuse Recyele', ENV \ THR = No \'islration ... t\elvers V a6lrer; NC)FI Ov No Floes° Fi t.,it)A1` = No Visitvi©n - Holiday

T NO.: NC0046213
IF,: Charlotte Terminal
NER TAME: Mplx Terminals ITC
GRADE: pC-1
eDMR PERIOD: 05-2016 (May 2016)
COMPLIANCE: Compliant
ORC/Certifier Signature: Terry
PERMIT VERSION: 41)
CLASS: PC-1
ORC: Terry Lee Sick
()RC HAS CHANGED:No
VERSION: 1,0
CONTACT PHONE tf: 7043921345
,v )
PERMIT STATUS: Active
COUNTY: Mecklenhuru,
()RC CERT NUMBER: 991168
STATUS: Processed
SUBMISSION DATE: 06/28/2016
Swick E-Mailllswick@marathonmetroleum,com .Phone 4:704-392-1345
By this signature. 1 certify that this report is accurate and complete to the best of my knowledge.
0 2 20 6
Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall he provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also he
provided within 5 days of the time the permittec becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to he tirade as required by pari 11E6 of
the 'NPDES permit.
06/ -016
Permittee/Su Signature:*** Angela S Brown E-Mail:[e-mail] Phone 14:419-421-2629
Permittee Address: 8(135 Mount Holly Rd NW Creek NC 28130 Permit Expiration Date: 06/30/2020
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the hest of my knowledge and belief. true,
accurate, and complete:1am aware that there are significant penalties for submitting false information, including the possibility of lines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: }'rlsrn Laboratories, lne,
CERTIFIED LAB SI: 4,02
PERSON(s) COLLECTING SAMPLES: Scott Miller
Date
PARAMETER CODES
Parameter Code assistance may he obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedenrorgiwch/wq/swp/psinpd&forins,
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC 11111Si visit facility and document visitation of facility as required per I 5A NCAC 8O .0204.
*** Signature of Permittee: If signed by other than the pennittec, then delegation (Attie signatory authority must be on file with the state per I5A NCAC 213
A/506(b)(2)(D),

NPDES PER.MIT 00.i NC0046213
FACILITY NAME: Charlotte 'Terminal
PERNIET VERSION:4.0
CLASS: PC-1
OWNER kME: Mplx Terminals LLC ORC: Terry 1 Swink
GRADE: PC-1 ORC HAS CHANGED; No
eDMR PERIOD: 04-2016 (Apri) 2016) VERSION: 10
PERMIT STATUS: Active
COUNTY: Mecklenburg
ORC CERT NUMBER: 991168
RECEDVEDINCIDENRIDWR
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: OW NO DISCHARGE*: 7'i4C)S
MOORESVILE F,',EFF1ONA,L OFFICE
24( 0 c or
Monthly Average Limits
Monthly Average':
Doily hlaximunit
Sae emit
FLOW
0.0075
E0530 12
TSS,, Cone
0.014 I
Dully Nlintrournt uot I 5'
0'HFrOl S
3400 346%
BENZENE
rosier
SAPTHALE
34(110
uarterni
Grab
TOLUENE
34371
ETHYLBEN
Quarterly
Grab
XYLENE
"" No Reporting Reason; ENFR No Flow-Reuse/Reeyele; ENVWTHR = No Visitation — Advcrs2 Weather; SO) LOW = No Flow; HOLIDAY = No Visitation Holiday
RECEIVED
JUN 0 k ZI.11b
CENTRAL ALES
DWR SECTION

PDES PERM rr NC0046213
rAciLrry NAME: Charlotte 'Terminal
OWNER NAME: Mplx Terminals LL,C,
GRADE: PC -I
eDNIR PERIOD: 04-2016 (April 2016)
PERMIT VERSION: 40
CLASS: PC-1
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: LO
PERMIT STATUS Active
COUNTY: Mecklenburg
ORC CERT!NUMBER: 991168
STATUS: Processed
SAN PLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
Monthly A swag(' Unlit:.
Daily rrr
11". No Reporting Reason: ENTRUST No Flow-Regse/RevyckL ENVW"TOR = No Visitation — Adverse Wcather; NOELOW No Flow; HOLIDAY = No Visitation — Holiday

NPDES PERMIT NO.: NC0046213
FACILITY NAME: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE: PC.1
eDMR PERIOD: 04-2016 (April 2016)
PERMIT VERSION: 4.0
CLASS: PC -I
ORC: Terry Lee Swick
ORC HAS CHANGED: No
VERSION: 1,0
PERMIT STATUS: Active
COUNTY: Mecklenburg
OR( CERT NUMBER: 991168
STATUS: Processed
Outfall 001 - Effluent Comments:
Analysis for Acute Foxicity was subcontracted to Ell Environmental, Inc. ((ertified L,ab 4022). The analytical report for Acute Toxicity (Parameter Code TAE6C) is being
submitted with hardcopy ofDN4R,

NPDES PERMIT NO,: NC00462 13
FACILITY NAN.' E: Charlotte Terminal
OWNER NAME: Mplx Terminals LLC
GRADE; PC -I
e03IR PERIOD: 04-20 I (5 (April 2016)
COMPEIANCE Compliant
PERMIT VERSION:4.0
CLASS; PC
ORC: Terry Leo Swick
ORC HAS CHANGED: No
VERSION: 1.:0
CONTACT PHONE #: [phone]
PERAWF STATUS: Active
COIJNEY: Mccklenbii%
ORC CERT NUMBER*. 991168
STATUS: Processed
MAIM ISM ON DATE: 05/2612016
0
26 2016
ORC/Certifier Signature: Terry L. S ick E-Mail:t1swick(a),marathonmetroleuncorn Phone #:[phone] Date
By this signature, 1 certify that this cport m accurate and complete to the best of my k.nowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time. the perrnittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to he made as required by part ILE.6 of
the NPDES permit.
Pc rm nte eISub in
Perrnittee Address: 80
05/26/2016
Signature:*** Angela S Brown E-Maikasbrown@matathonpetroleurn,com Phone 4:419-42.1-2629 Date
Mount Holly Rd Paw Creek NC 28130 Permit Expiration Date: 06/30/2020
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations,
CERTIFIED LABORATORIES
LAB NAME: Prism Laboratories, Inc.
CERTIFIED LAB #: 402
PERSON(s) COLLECTING SAMPLES: Scott Miller
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http/portal.ncdenrorgiweb/wq/swp/psinixies/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
** ORC on Site?: ORC mast visit facility and document visitation of facility as required per 15A NCAC SG .0204,
*** Signature of Permirtee; If signed by other than the perminee, then delegation of the signatory, authority must be on file with the state per I5A NCAC 213
.0506(b)(2)(D).

[phone] FAX [phone]
FOE Ecox e414, Greemtite, SC 29606
4 Craftsmao Court, Greer, SC 29650
Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: WEST
Prism Sample ID: 001 Outfall
Test Date: 14-Apr-16
Laboratory DO: T46847 AD
Test Reviewed and Approved By
44.7'
Robert W. Kelley, Ph.D. Farhad Rostampour
QNQC Officer Laboratory Director
17t
Certification #E87819 SCDHEC Certification #23104
Test results presented in this report contbrm to all requirements of
NELAC, conducted under NELAC Certification Number E87B19
Florida Dept. of Health, Included results pertain only to provided samples.
rsTCDENR certification # 022
Page 1 of 4
Page 9 of 12

Effluent Toxicity Report Form - Chronic Pas
MAIL ORIGINAL TO
s Fail and Acute LC50
POES4 NC ply 1
North Caroiltra eriodephnio.Chronic Pass/Fail Reproduction To c ity Test
CONTROL ORGANISMS
tl You
Adult (L)ilye (C7)ead
Effluent %
TREATMENT 2 ORGANISMS
#Young Produced
Adult (L
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
start end
1st sample
2
2
1st sample
start end
4
4
2nd sample
start end
2nd sample
LC50/Acute Toxicity Test
ortailty expressed as
0
/
LC5©
biding replicates)
12.5 25 50 1 00
0 0 0 0 0
Method of Determination
lUovirag Average Protlit
Spearman KaOther
Or atfi ftl Tested Pimephal pramelas
County: Mecklenburg
Environmental Sciences Branch
eiv. of Water Quellty
N.C. ©ENR
1821 Mall Service Center
Raleigh, North CaroIIna
7 8 9 10 11 12
i
10 11 12
Complete Thle for Erther Test
Satllole Type (Duration)
Sample 2
Sample Te
Chronic Test
Calculated t7-•
Critical Value=
`% Reduction=
Treetrnertt 2
Control CV
% 3rd Brood
621
Avg. Reprod,
Treat
PASS FAIL
Test Start Date
14-Apr.16
2 NA
Comp Duration 1st 2nd
Hardness (m/L)
Spec, Cond. patios)
Chlorine (mgfL)
at reeoipt (°C)
star
7.7
7.8
7.7
7.7
Tox Tox
7.4
.7
D.O.
DEM Form AT-1
Page 2 of 4

24 Hour Acute Toxicity Test
Test Method: EPA 821 R..02-012 ; Method 2000 Pimephales romelas;
MARATHON
Start Date, 04/14/16
End Date: 04/15/16
FatheariMinhows
Time:
Time:
Test Vessel
500 mL Plastic cuP
1230
12:20 1'M
Test Solution Volume
200 ml
Sample
Set By: AM
.Ended By: JC
Incubator
#1
Transfer Volume
0,5 ML
0 : !Neonates from common lioldInd vessel !Light: 50 -100 16 hr light / 8 lu datk-
TEST OR
1:01',.C.0.49(10PMfa*I.1141
. „
Between:
promelas
MySiddfisis,1;aht,
e:
and:
AFC Age: 5 DAY
Age:
1
Com
Control
6.3%
12.5%
25.0%
50.0%
100,0%
Rep,
D
A
173
A
13
D
13
MORTALITY DATA
'111.
tioninistes
10
10
10
10
10
10
CumuIativ Mortality
24
0
0
0
72 la
94 1.
D
A
373
A
D
A
10
0
10
10
Final
0%
0%
0%
0%
0%
Lab 11.)#: 146847 Al)
Dilution Water
Surface (40H)
Comments: NC
-31-16
" • „
1111111113111
11111111111101rill
Page 3 of 4
Page
of 12

x
7414
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Cl, Greer, SC 29650
www.ETTEN VinONH cNTAI.onm
4
(Composite only) (Grab
AA PLEI➢
'Custody Transfer Record
Time Relinquished I3y / Or
r Composite)
Sign, and Print below
the dotted line
Collected by
OF CUSTODY RECORD
rogram Containers
Parameters
Whole Effluent Toxicity
Chronic Test 0 : nnisms
ceived By / Oruanization
COMPOSI7",S S4MPUt' G PROCEDUIU.iS
Composite samples mus be collected over a 24 hour pe
Time Proportional, 1 sample each hourfor 24 hours. Et
or'x# nriniirtum # sample every 4 hours over 24 hours.
Proportional: As per instructions in NPDES perm
v
1 AaPRR 4TUA MoNfmItm!a PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags,
eul Analysts & Cr
Receipt'
Temp °C
HOLD i`#A PROCEDURES
Eor toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

QA
April 28, 2016
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NPDES (DMR) MONTHLY REPORT
MARATHON PETROLEUM COMPANY LP
CHARLOTTE TERMINAL
8035 MT. HOLLY ROAD
CHARLOTTE, NC 28214
NPDES PERMIT NUM`
Enclosed please find the
Terminal, Transport & Rail
Marathon Petroleum Company LP
539 South Main Street
Findlay, OH 45840
Tel: [phone]
4
Sent via Overnight Mail
Fc`FIvE
MAY -22016
DWR SECTION
INFORMATION PROCESSING UNIT
i)VVR ScEION
0 ATION PROCESSING UNIT
plus one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or
by email at [e-mail].
Sincerely,
Dawn Benjamin
Analytical Processor
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES; NPDES DMRs)
KH
MAY O5Z016

ENT
RMIT NO. NC0046213 DISCHARGE NO.
ITT NAME Marathon Petroleum Company LP
'ERATOR IN RESPONSIBLE CHARGE (ORC) ert
z.RT1FIEQ LABORATORIES (1 (1)
1ECK BOX IF ORC HAS CHANGEQ
ORIGINAL ani ONE COPY to'
tn: CENTRAL FILES
VISION OF WATER QUALITY
.17 MAIL SERVICE CENTER
OH,
2
2
22
2
AV
MAXIMUM
MINIMUM
Terry Swick - C
Prism Laboratorre
001 Month tvtaroh Year 2016
CLASS County Mecklenburg
991168 GRADE PC1 PHONE [phone]
tC (2)
PERSON(S) COLLECTING SAMPLES
IGNATURE IiFF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
Miner
MONTHLY REQUIREMENTS
50050 , C05 o } t€ 556 32730 340
YIN MGD
Comp. (C)?Grab(G)
Monthly Average Limit
Daily Maximum Unlit 45.0
0.029
0.0
0.029
0.0
)WO Form MR-1 (01/00)
:.harlotte
30
5© o
QUARTIRLY RE
401t 4 437

Facility Status: (Please check one ofthe fo|�wing)
V All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
iant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respectUuequipment, operation, maintenance,
etc,and otime table for improvements hrbemade.
^| certify, under penalty of law, that this document and all attachments were prepared under mydirection msupervision inaccordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. |amaware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539S, MAIN ST, F|NDLAY, OH 45840
Permittee Address
Marathon Petroleum Company LP
By� W1PC |nvesbnentLUC. its General Partner
By: TimothyJ, AwdL Deputy Assistant Secretary
Permittee (Please print orVe
419-421-4422
Phone Number
June 3O.2O2O
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site ath2o,encstabs.no,us/wqs and linking to the Unit's information pages, ,
Use only units designated intheneporbngfanhty'spennitfornapnrhngdata.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)

ENT
RMIT NO. NC0046213 DISCHARGE NO, 001 Month February Year 2016
ITY NAME Marathon Petroleum Company LP CLASS County Mecklenburg
PERATOR IN RESPONSIBLE CHARGE (ORC) N/A GRADE N/A PHONE N/A
CERTIFIED LABORATORIES (1 (1) Prism Laboratories, Inc. (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
Monthly Average Limit 30.0
David Morris
N/A
RE % F0I
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DATE,;
MOORESViiI r
ONTHLY REQUIREMENTS QUARTERLY REQUIREMENT
Daily Maximum Limit 45.0 50.0
DWQ Form MR-1 (01/00)
Charlotte

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Co 'ant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made.
All monitoring data and sampling frequencies do NOT meet permit requirements.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S. MAIN ST., FINDLAY, OH 45840
Permittee Address
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: Timothy J, Aydt, Deputy Assistant Secretary
Permittee (Please pri;f. or type)
Signature . Per it ee**
419-421-4422
June 30, 2020
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o,enr.state.nc.us/wqs and linking to the Units information pages.
Use only units designated in the reporting facility's permit for reporting data.
* ©RC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

NC0046213 DISCHARGE NO, 001 Month January Year 2016
Marathon Petroleum Company LP CLASS County Mecklenburg
R IN RESPONSIBLE CHARGE (ORC)
FIED LABORATORIES (1 (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
025
AVERAGE
MINIMUM
Monthly Average Limit 300
Daily Maximum Limit 45.0 50.0
N/A GRADE N/A PHONE N/A
Prism Laboratories, Inc, (2) R Fc:p v ;LT, n R
PERSON(S) COLLECTING SAMPLES Scott Miller
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CH 7SViLLE PEE:AIWA_ OF,
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
MONTHLY REQUIREMENTS
DWQ Form MR-1 (01/00)
Charlotte
<1.0
FEB I
UARTERLY REQUIREMENTS
<10
.0
ugA
44:14pW'.4
<3.0
AvW-VOK,
V.41**,,Vo4
V010-e-g,
tiggitte(
4.itattit,
>100%
gtf0A1.74,7?

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Compliant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc,, and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S. MAIN ST., FINDLAY, OH 45840
Permittee Address
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: Timothy J. Aydt, Deputy Assistant Secretary
Permittee (Please prjt o.a' e
2/11/2©16
Signature of P- mi e Date
419-421-4422
June 30, 2020
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Unit's information pages.
Use only units designated in the reporting facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
" If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D)•

(Eat) 977.E 42 , FAX (864) R77.6438
P 0, Box, "I 414. Greenv lte. G
4 Craftsman Curt, Graer, SC 29650
Pimephales promelas 24 Hour Acute De
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: PAW CREEK
Test Date: 21-Jan-16
Laboratory ID#: T46372 Al)
Test Reviewed and Approved By:
ive Test
Robert W. Kelley, Ph.D. Farhad Rostampour
QA/QC Officer Laboratory Director
Certification #E87819
Test resuls presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E878I9
Florida Dept. of Health. Included results pertain only to provided samples,
SCC Ce
0
NCDENR Certification # 022
Page 1 of 4

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Date 22-Jan-16
Facilit : MARATHON PAW CREEK
X
Signature of Operato in Respot sibiC,harge
X
Signature of Laboratory Supervisor
Pipe #
Comments
Count Mecklenbur
MAIL ORIGINAL TO
North Carolina Ceriodaohnia Chronic Pass/Fail Reproduction Toxicity Test
CONTROL ORGANISMS
# Young Produced
Adult (L)Ne (D)ead
Effluent %
TREATMENT 2 ORGANISMS
# Young P
Adult (L)Ne (D)ead
pH
Control
Treatment 2
D O°
Control
Treatment 2
1st sample
start end
1st sample
2
2
lst sample
start end
1st sample
4
4
6
2nd sample
stall end
2nd sample
LC50/Acute Toxicity Test
(Mortality expressed as %, combining replicates)
22
45
60
LC50_ >lea °/t
95% Confidence Limits
NA eke
.e►
Organism Tested
90
10©
Method o
Moving Average
Spearman Kerber
ination
Probit
Other
Pimephales promelas
7
Concentration
Mortality
8
10
10
11
11
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699.1621
Complete This for Either Test
Collection (Start) Date
Sample 1 20-Jan-16
Sample Tyoe (Durations
12
12
Grab Comp Duration
Sample1 X
Semple 2 X
Hardness (mg/L)
Spec, Cond. (pmhos)
Chlorine (mg/L)
Sample Temp. at receipt (°C)
pH
nd
Chronic Test Results
Calculated t=
Critical Value=
% Reduction=
Control
Treatment 2
Control CV
Avg. Reprod.
Control
Treatment 2
PASS FAIL
Test Start Date
21-Jan-16
Sample 2 NA
Dilution
201
Control
1st 2nd
Tox Tox
Sample Sample
54
0.05
0.2
d
High Conc.
7.9 ( 7.6
8.81 7.8
D.O.
DEM Form AT-1
Page 2 of 4

24 Hour Acute Toxicity Test
Fathead Min
Test Method: EPA 821 R-02-012 ; Method 2000 Plmophales promeias
S©p ,
!a
promelas
Mysirlapsta Bahia
Test Vessel
Test Solution Volume
200 mL
'Neonatal from common holding vessel
Between;
Cone.
Control
22.0%
45,0%
60.0%
90.0%
100,0%
Rap,
A
D
A
Source: ABS
fi
e
and:
DAY:
MORTALITY DATA
la tlela
orQeaiems
10
10
10
10
10
10
Cumulative Mortality
0
0
0
0
0
18 it iht
4
D
A
D
13
10"
10
10
10
0
0
0
Final
artatity
0%
0%
Sample ID: PAW CREEK
Sct 13y: JC
Ended By: AM
Incubator
#1
Transfer Volume
'Light: 50 -100 ft-c. 16a;
0.5 mL
Lab ID#: T46372 AD
40H)
Co
ORGANISMS HATCHED ON 1-16-16
NC H2O 1-21-16
Page 3 of 4

O
ET
0 Box 16414, fat aartt€e, C 7414
[phone], [phone] Fax[phone]
Shipping Address: 4 Cre0sman Ct, Greer, SC 24850
W W W.CTTCNVIRONMCNTA4.COM
Client:Afi
._{ k0/-1
COF CUSTODY RECORD
Facility: 'pox / 7,steAc.
State: NPDES #:
SAMPLE ID
CIPLV.
(7)c'
(Composite only)
Compasit* Start Dal
(Crab or Composite)
Sample Cotkcdaa Data Time
MPOSITE SAMPLING PROCEDURES
mposite samples must be collected over a 24 hour period.
Ate Proportional: 1 sample each hour for 24 hours. Equal volut
Nat minimum ( sample every 4 hours over 24 hours.
,w Proportional: As per instructions in NPDESpermit.
1(J30
Program
Sign, and Print below
the dotted line
Collected by
,14
U
Containers
s w
I.H2504
2e HCL
3.02403
1�S©H
ZMS
6.. Other
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags.
Parameters
\Yholc Effluent Toxicity
r
Chronic Teat Organisms
r
Chemical Anaiys
Other
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection,

ENT
RMIT NO.
ITY NAME
NC0046213 DISCHARGE NO.
Marathon Petroleum Company LP
ERATOR IN RESPONSIBLE CHARGE (ORC)
CERTIFIED LABORATORIES (1 (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
001 Month December
CLASS County
N/A GRADE N/A PHONE
Prism Laboratories, Inc. (2)
PERSON(S) COLLECTING SAMPLES David Morris
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
Year 2015
Mecklenburg
N/A
RECENE0iNgThr:KR/OVVR
FEE 2 2016
WOW)
A4001-cbblAw REG
ONTHLY REQUIREMENTS
1105
AVERAGE
MINIMUM
0.001
0.025
0.021
Monthly Average Limit 30.0
Daily Maximum Limit 45.0 500
DWQ Form MR-1 (01/00)
Charlotte
50
UARTERLY R
,".
UIREMENTS
RASM
FILEs
1.1400.4
ziAlf40,11.%
:,;,„Ogy,f,rik0

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Noncomplian
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made,
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
539 S. MAIN ST., FINDLAY, OH 45840
Permittee Address
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: Timothy J. Aydt, Deputy Assistant Secretary
ermittee (Please prim«r»e)
Signature of P; i
419-421-4422
June 30, 2020
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr.state.nc.us/wgs and linking to the Unit's information pages.
Use only units designated in the reporting facility's permit for reporting data,
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

UENT
ERMIT NO.
ITY NAME
NC0046213 DISCHARGE NO. 001 Month November Year 2015
Marathon Petroleum Company LP CLASS County
Mecklenburg
OPERATOR IN RESPONSIBLE CHARGE (ORC) N/A GRADE N/A PHONE N/A
CERTIFIED LABORATORIES (1 (1) Prism Laboratories, Inc. (2)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699.1617
HRS HRS YIN MGD
12
PERSON(S) COLLECTING SAMPLES David Morris
N/A
RECEwsvi:DtNCorNR/DWR
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE WO
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS MOOR,ESViLLE REGI
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE. ()EC
ONTHLY REQUIREMENTS €QUARTERLY REOUIRNTS
20
22
24
2
2
0 1110 0.2
0.022
AVERAGE
0.024-
MINIMU
0.008
Monthly Average Limit
Daily Maximo
DWQ Form MR-1 (01/00)
Charlotte
30.0
45.0 50.0

Fir Facility Status: (Please check one ofthe following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Compliant
Noncompliant
If the facility is noncomp|ian1, please comment on corrective actions being taken in respect to equipmerd, operation, maintenance.
etc., and a time table for improvements to be made.
^| oertify, under penalty oflaw, that this document and all attachments were prepared under mydirection or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based nnmy
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best ofmy knowledge and bo|ief, true, apuunutn, and complete, | am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
Marathon Petroleum Company LP
By: K4PCInvestment LLC.its General Partner
By: Timothy J. Aydt, Deputy Assistant Secretary
11/1OC2O15
Signature ofPr rnh1e
419-421-4422
Permittee Address
Phone Number
Permit Exp, Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.en r. state, nc. us/wqs and linking to the Unit's information pages.
Use only units designated indhereporhngfon|ity'spennbforreporbngUata.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G 0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)

EFFLUENT
NPDES PERMIT NO. NC0046213 DISCHARGE NO, 001 Month October Year 2015
FP,CILITY NAME Marathon Petroleum Company LP CLASS County Mecklenburg
OPERATOR IN RESPONSIBLE CHARGE (ORC) N/A GRADE N/A PHONE N/A
CERTIFIED LABORATORIES (1 (1) Prism Laboratories, Inc. (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Scott Miller PFC.FIVPD/NCDFNR/DWR
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
AVERAGE
MINIMUM
Gornp fAti (G)
Monthly Average Limit
Daily Maximum Limit
DWQ Form MR-1 (01/00)
Charlotte
DEC — 1 2015
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATfi
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS MOORESVILLE FN&QFFCE
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
NOV 2 5 206
MONTHLY REQUIREMENTS UARTERLY REQUIREMENTS
45,0 50.0
7
N.541fi.
11134.4A(
Ofilltk
IL
MAtiWi'M
AgRiitOttinigksw.
44,4910:01,,!"
railiOtt
Itifitt10011'401,,,R.

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
'ant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S. MAIN ST,, FINDLAY, OH 45840
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: Angela S. Brown, Deputy Assistant Secretary
rmittee (Please print or type)
l�
11/10/2015
Signatur f Permittee** Date
419-421-2629
June 30, 2020
Permittee Address
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr,state.nc,us/wqs and linking to the Units information pages.
Use only units designated in the reporting facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 26.0506(b)
(2) (D).

Pimephales promelas 24 Hour Acute Definitive Test
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: PAW CREEK
Prism Sample ID: 001 Outfall
Test Date: 62-Oct-I5
Laboratory lD#: T45833 AD
Test Reviewed and Approved By:
Robert W. Kelley, Ph.D,
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted wider NELAC Certi&cation Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
Page 1 of 4
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 922

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50
Fa ils : MA ATHON PAW CREEK
Signature of 0
X
ib
Signature of Laboratory Supervisor
Charge
Date
Floe # coun : Mecklenbure
Comments Insufficent test organisms in purchased batch
to set a reference toxicant test. Discussed with
Cindy Moore of ATU. Monitor and Report only.
Review of reference toxicant data from test
organism supplier indicated sensitivity in range.
Reporting of test results approved. RWK.
MAIL ORIGINAL TO
North Carolina Ceriodaohnia Chronic Pass/Fall Reproduction Toxicity Test
CONTROL ORGANISMS
*Young Produced
Adult (L)lve (D)ead
Effluent
4
7
10
11
Environmental Sciences Branch
Div. of Water Quality
N.C. DENR
1621 Mall Service Center
Raleigh, North Carolina 27699.1621
12
TREATMENT 2 ORGANISMS
# Young Produced
Adult (L)ive (D)ead
pH
Control
Treatment 2
D.O.
Control
Treatment 2
1st sample
start end
1st sample
2
1st sample
start end
1st sample
4
8
2nd sample
start end
2nd sample
LC50/Acute Toxicity Teat
(Mortality expressed as %, combining replieatee)
0
0
12.5.
0
25
0
50
0
s*
90
•
0
100
LC50 = >100% Method o
95% Confidence Limits
Moving Average
Determination
Probit
�% Spearman Kerber lOther
Or anism Tested Pimephales promelas
Lncentratlon
Merteilty
NA
DEM Form AT-1
Page 2 of 4
10
11
Complete This for Either Test
12
Chronic Test Results
Calculated t=
Critical Value=
% Reduction=
Control
Avg. Reprod.
Control
Treatment 2
S.ollectton f ) Date
Sample 1 01-Oct-15
Sample Typa (Du i . )
Sample 1
Sample 2
Sample Temp. at receipt (°C)
pH
Control CV
% 3rd Brood
Treatment 2
PASS FAIL
Test Start Date
02-Oct-15
Sample 2
7.
7.4
High
8.0 / 6.5
D.D.

rtent MARATHON
tart Date: 10/02/15
Date: 10/03/15
Cone,
Control
12.5%
25,0%
50,0%
90.0%
100.0%
48 Hour Acute Toxicity Test
Test Method: EPA 821 R-02-012 : Method 2000 PMnephalea promMar
Time: 1130
Time: 11:09 AM
Test Vessel
MORTALITY DATA
IoaYl a
oraaniw.
10
Cumulative Mortality
24 kr 44 kr 22 kr
Teat sotwwn Volume
v
A 10
10
C
D
10
10
C
T3
A 10
10
C
0
10
10
13
A 10
B 10
C
A
0
DAY:
M walk/
0%
0
0%
0%
0%
ample ID: PAW CREEK
Set By: JC
Ended By: JC
Incubator
TO
Page 3 of 4
Transfer Volume
Lab T134: T45833 AD
D 80 NOT ROUGH 1 XTRA;OR
REF
Tt3C. s
Page 10 of 11

Oct. 2. 2015 8:34AM Prism Labs No.0351
SUBCONTRACT ORDER
Prism Laboratories, Inc.
5100018
$ENDING LABORATORY:
Priam Laboratories, Inc.
P. O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
Pax: 704-525-0409
Project Manila: Cara C. Rusmisoll
RECEIVING LABORATORY:
ETT Environmental, Inc
P.O. Box 16414
Greenville, SC 29606-7414
Phone :[phone]
Fax: [phone]
Due
Sample ID: 5100018-02
Acute Twucity Definitive, Fat 1
Containers Swppl/ed:
Expires
SampledrlW0111516100
10/03/15 16:00
Redd tut ©.©°C
Page I of 1
Page4of4

7FFLUENT
2ERMITDE NO.
CILITY NAME
NC0046213 DISCHARGE NO.
00 1
Marathon Petroleum Company LP CLASS
Month September Year 2015
County
Mecklenburg
OPERATOR IN RESPONSIBLE CHARGE (ORC) N/A
GRADE N/A PHONE
CERTIFIED LABORATORIES (1 (1) Prism Laboratories, Inc (2)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
2
6
18
,V
22
24
26
28
30
-
• '
HR
tUR
N.51P44,
PERSON(S) COLLECTING SAMPLES
N/A
Scott Miller
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
N 4
Nel.RIWPMAWARAVinagMtni*W
Ant-14V4r,aWriTOM:4**INA
dvkqe,,,,,,twAmm,,ezesm,,,,,*.‘art*ORW.
r4„4.
VAWAVAA`
I -,
twanum-voiNVON Kommt
WrAtotO 44V-WhoviaRMAituft
34111014, „7"Sig,"„tit
Wsr,e,07,4,103,W;
W*165k**1044,41ASHitatight
0414110
4*.ialgtnG5kkeVilqa*.VORA,4.,,,;,444
INS
AVERAGE
'W,Vtg*Komv,
4v'M
gv.Z-V4A'.k
MINIMUM
Monthly Av
m%R.MN..mAm*.
,Int-AXg.A44h2Wtatt,,,.'41..3.>ft V„,W
,55,5Wili*51:0119,7,,A,:ttn5t1,0MCNOMAViel55.
V •
4
Mratq)''YWRRMgitPPtXate*t*
,,,,ovt..m.plArse4A11.11,,MANZAMS.144'
41,414:11,M41*-A4,.aig,mmos.,
244g4144401
tnfnegftwat titseve*
10,t5,550*;,45:13,5545WM, 4MWM,
145,10avt*,,IWookaiognomvtA,
„.„
Oft-444561 AVV*444,z,
**WealktiaZ,0 V-f„.--Keittic941
,',i4,4%Anatift4tiltt4.44.e
ailtaCW:4001:401900.
Artatifrii***WARV*stlidigNOZ-a.,
rienaiNtlit,94),'11104,0
qmoggi
".14140
44.3.4)40$-
,
1,t,g4.4.,411#4.4
;;;Afeliti4,,IW
UARTERLY REQUIRE
ug./1
U *
11*
U
.44,• ' c., \WEntlfali
NOVV*404. 'MOM" 1 -4,
faigarAt40044
PWW,G,
NatZlitit
. . ,
alikaSESVY'4,4500
fintRieglailigenalgtalMill
tSatgitiESANigeIVSISNMVII
iuu
14.82-11
*Amu* 42,4*".;'*14,-,VW040,4.,44ft4.14,VAM
Ai,g4frntitf,U:'tpaM* 0,14,M***04AN,Wita*AWa.,,,,,,W.WN*1.,
itintrititiARIESWItit titlf,MA
f4.54M.54,1V55Ntlit
Vg5,18744.:**,&055,AM,
1M,m M • ••
• " M..WAAVOtlAtmlitp,,,4,444',401M
ktMOU'AO ••• ,
m,Mmf,,'Mt,MNe' ZKI,VM,kki,M4 , • . •
W.,,,t*A4..,0.0mA05,,X,4erAVOMINA,. VW' 140^#4,V,M,A,>. 41, 4.44iv VMti,,,',:latse`AMMI*NNzteRWM410,kitr
1-04**PAVOttft *Ma .CAAN''W46't tigt*-VM V*1.4,;,,W.,30-;;AtiV*My4.,et
0.130
l',W.Aka*Atal4ADONWAiai*,,:,AMAZAP,, ,/04,WrAvt4,..;
'',VateVOWitri4,4X04407:%'.:,06MItibitaiNtiginitigt,g .14604rIONIV: Vganaiit,IlttgAii#"*Akitiedsl"
0.002
13Alt.A.WAV.M4,Z4A0MM'T-..1,,,ra Mlf..M0; XXV., ARA „Mataff
, 1W,V, 401 n'w
aao Limit 30.0
Daily Maximum Limit
DWQ Form MR-1 (01/00)
Charlotte
45.0 50.0

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S. MAIN ST., FINDLAY, OH 45840
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: Angela S. Brown, Deputy Assistant Secretary
ermittee (Please print or type)
Signatu1of Permittee**
419-421-2629
June 30, 2020
Permittee Address
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Unit's information pages.
Use only units designated in the reporting facility's permit for reporting data.
*©RC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D)•

EFFLUENT
NPDES PF,AMIT NO. NC0046213 DISCHARGE NO. 001 Month August Year 2015
Mecklenburg
FACl/IY NAME Marathon Petroleum Company LP CLASS County
OPERATOR IN RESPONSIBLE CHARGE (ORC) N/A GRADE N/A PHONE N/A
CERTIFIED LABORATORIES (1 (1) Prism Laboratories, Inc. (2)
nccEIVED/NCDP4RiDWR
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES David Morris
A
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
HRS HRS YIN
2
OCT 1 3 2015
2 2013 N/A WQROS
(SIGNATURE OF OPERATOR IN RESPONSWOMKEt REOIONA
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
MONTHLY REQUIREMENTS
MGD mg/I
NTU
mg/I
QUARTERLY REQUIREMENTS
ug/I 9/1 ug/I ug/I ug/I ug/I ug/I
ANNUAL
0
12
14'°915 025 Y" 0.218 10
15
16
17
19
20 930 0.25 Y 0.235
71-40:Aiii;§,z1
0.095,
22
24
2
28
30
AVE
GE
0.182
MAXIMUM 0.235
0,095
MINIMUM
Monthly Limit
DWQ Form MR-1 (01/00)
Charlotte
45,0
50.0

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
pliant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations"
539 . MAIN ST., FINDLAY, OH 45840
Permittee Address
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: Angela S. Brown, Deputy Assistant Secretary
ermittee (Please print or type)
9/18/2015
Signatur rf Permittee** Date
419-422-2121
June 30, 2015
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Unit's information pages.
Use only units designated in the reporting facility's per
0
eporting data.
*©RC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

O.
E
NC0046213 DISCHARGE NO. 001 Month July
Marathon Petroleum Company LP CLASS County
Year 2015
Mecklenburg
R IN RESPONSIBLE CHARGE (ORC)
TIFIED LABORATORIES (1 (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
6
10
12
14
16
18
20
22
23
24
26
28
30
HR
Y/N
AVERAGE
MAXIMUM
MINIMUM
CI A
N/A GRADE N/A PHONE
Prism Laboratories, Inc. (2)
PERSON(S) COLLECTING SAMPLES Scott Miller
N/A
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
ONTHLY REQUIRE
MGD
ENT
NTU
mg/I
QUARTERLY REQUIREMENTS
u
<0, 0
ELC
2 ,;Li 2015
RECEIVED/NCDENR/DWR
SE," 2 2015
ANNUAL
„.A.10,1,4 Mtak,3,151:11t;iiiigifie
mft-ipt,
Monthly Limit
DWQ Form MR-1 (01/00)
Charlotte
45.0
50.0

Facility Status: (Please check one nfthe following)
Vilmonitoringdataondsamp|ingfrequanoieameetpermitnoquiremonts
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
ant
Noncompliant
If the facility is nuncomp|iant, please comment on corrective actions being taken in respect to equipment, operahon, maintenance,
etc,and atime table for improvements hobemade.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based onmy
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. |amaware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations,"
Marathon Petroleum Company LP
By: W1PCInvestment LLC.its General Partner
By� Angela S. Brown, Deputy Assistant Secretary
ittee (Please print or type)
419-422-2121
Permittee Address
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o,enr.state.nc.us/wqs and linking to the Unit's information pages.
Use only units designated inthe reporting fao|ity'opemnkharneonrtingdabe
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G �0204-
**°|fsignodbyctherthonthepennittee.de|egodonofsignatoryouthodtymustbeonfi|eviththesbohaper15ANCAC28.QSO0(b)

Attn. CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER\
RALEIGH, NC 27699-1617
T
NO. NC0046213 DISCHARGE NO.
001 Month June Year 2015
NAME Marathon Petroleum Company LP CLASS County
TOR IN RESPONSIBLE CHARGE (ORC) N/A
Mecklenburg
GRADE N/A PHONE N/A
TIFIED LABORATORIES (1 (1) Prism Laboratories, Inc. (2)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
\.rWi
A
fRSS (S) COLLECTING SAMPLES
Scott Miller
N/A
RECEIVED/NCDENR/DWR
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE. WQROS
MOORESVILLE REGIONAL OFFICE
DAT,AUG122015
Monthly Limit
MONTHLY REQUIREMENTS
CO 30
45.0 50.0
QUARTERLY
EQUI
MENTS
ANNUAL
DVVQ Form MR-1 (01/00)
Charlotte

Facility Status-, (Please check one ofthe following)
VAII monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Compliant
Noncompliant
If the facility is nonoomp|imnt, p|eema comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc,and atime table for improvements 8obomade.
^| nertify, under penalty oflaw, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted, Based nnmy
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, Vzthe best ofmyknowledge and belief, true, accurate, and complete. |omaware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539G.MAIN ST,F|NDLAY.QH 45840
Permittee Address
Marathon Petroleum Company LP
By: yWPCInvestment LUC.its General Partner
By: Angela S, Brown, Deputy Assistant Secretary
ittee (Please print or type)
419-422'2121
Phone Number
June 30.2O1S
Permit Exp, Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web s,ite at h2o,enr. state. nc. us/wqs and linking to the Unit's information, pages,
Use only units designated indhoneporUngfau|ity'opennithorreoortingdota.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G �0204�
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)

ATOR IN RESPONSIBLE CHARGE (ORC) N/A
RTIFIED LABORATORIES (1 (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
10
12
3
14
NT
T NO. NC0046213 DISCHARGE NO. 001 Month May Year 2015
Y NAME Marathon Petroleum Company LP CLASS County Mecklenburg
N/A
GRADE N/A PHONE
Prism Laboratories, Inc. (2)
PERSON(S) COLLECTING SAMPLES David Morris
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DATE
UARTERLY REQUIREMENTS ANNUAL
6
20
22
24
26
28
0
AVERAGE
MINIMUM
Monthly
DWQ Form MR-1 (01/00)
Charlotte
45.0
50.0
VED/NCDEN
JUL 22 2015
WQROS
MOORESVILLE REGIONAL OFFICE

PPIPFacility Status: (Please check one of the following)
Fr,
AM monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
iant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S, MAIN ST., FINDLAY, OH 45840
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: T. J. Aydt, Deputy Assistant Secretary
Permittee (Please print or type)
6/24/2015
Signature o ermi . ee** Date
419-422-2121
June 30, 2015
Permittee Address Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Unit's information pages.
Use only units designated in the reporting facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8G +0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

EFFLUENT
NPDES PERMIT NO, NC0046213 DISCHARGE NO, 001 Month April
Year 2015
Mecklenburg
FACILITY NA'.....;i Marathon Petroleum Company LP CLASS County
OPERA -MR IN RESPONSIBLE CHARGE (ORC) N/A
GRADE N/A PHONE
CERTIFIED LABORATORIES (1, (1) Prism Laboratories, Inc, (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
10
12
13
14
N/A
JuN 0
N/A
Z015
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Rif
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS MOORESVILLE
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
MONTHLY REQUIREMENTS
HRS HRS YIN MGD mfI NTU
16 935 0.25 Y 0,133
22
3
4
26
8
30
AVERAGE 0257
AXIMt --
MINIMUM
Monthly Limit
DWQ Form MR-1 ((moo)
Charlotte
0.001
45.0 50.0
UARTER Y REQUIREMENTS
MAY 2 I " 01
ANNUAL
igttdit8
adtaAP:Ww-V.
.440.119"
MtL
j4.5.:*KRItaii:511191411t8,914
inttflgatit

Facility Status: (Please check one of the following)
monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
iant
Noncomplian
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made,
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S. MAIN ST., FINDLAY, OH 45840
Permittee Address
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: T. J. Aydt, Deputy Assistant Secretary
ermittee (Plea - � in type)
5/20/2015
Signature o ert, "ittee" Date
419-422-2121
Phone Number
June 30, 2015
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visitin
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Unit's information pages,
Use only units designated in the reporting facility's permit for reporting data.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

May 22, 2015.
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED/NCDENR/DWR
JUN 01 2U15
WQROS
MOORESVILLE REGIONAL OFFICE
RE: NPDES (DMR) MONTHLY REPORT
MARATHON PETROLEUM COMPANY LP
CHARLOTTE TERMINAL
8035 MT. HOLLY ROAD
CHARLOTTE, NC 28214
NPDES PERMIT NUMBER NC0046213
Enclosed please find the
Terminal, Transport & Rail
Marathon Petroleum Company LP
539 South Main Street
Findlay, OH 45840-3229
Tel: [phone]
Sent via Overnight Mail
RE E VED
MAY 22015
CENTRAL FILES
DVVR SECTION
plus one copy, for the above -referenced permit.
If you have any questions or require additional information, I can be reached at 419-421-2019 or
by email at [e-mail].
Sincerely,
Dawn Benjamin
Analytical Processor
C) A
Enclosure
cc: Posted to electronic Environmental Manual (Water; NPDES: NPDES DMRs)

Month March
Year 2015
EFFLUENT
P'^DEPERMIT NO. NC0046213 DISCHARGE NO, 001
rPCILITY NAME Marathon Petroleum Company LP CLASS
OPERATOR IN RESPONSIBLE CHARGE (ORC)
CERTIFIED LABORATORIES (1 (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
N/A
Prism Laboratories, Inc. (2)
PERSON(S) COLLECTING SAMPLES
GRADE
County
N/A PHONE
Scott Miller
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
Mecklenburg
N/A
RECEIVED/NCDENR/DWR
MAY 5 2015
WQROS
MOoRPRE RE°I
ONTHLY REQUIREMENTS
QUARTERLY REQUIREMENTS
ANNUAL
©
k.`.
4
NI,S I-!RS
150 0.25
`i ...
c
MGD
5tiq'3`}`'�
® 0.002 4.7 9.5
�`^',`\.\�?\glgy`�ti5.,t1Z
�'^^,,,,yy�\ {'`i"*5:'Y�L�}?x`,°�\�t},p
�t�v'�y,�7�'eFo
�4`' Y ,'„ i�'1�\�}i tiy��5
`.'4%\,q: ° �``�. A.':.: \\`Z.',
�a
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al
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fit`• ., ���$\}\\i
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tt
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,4`".?"ki`'Lty
V
��'
.g�am\iSS1,
Mantttl Limit
�}at',��jz}� y cn;t:�,�i
�.� 3p �\,!!�hj "`3�{�Y3 ";1"',3g`5'��D 5��5}
4, F \t4`*{
..
g,z. .4.\�x etz' k':}',`m.,.
L..�m �2;n�`v"SaR.l�a*
0.21
k 5�` &'
�1V.i ��
0.002
�"�`��, 1®�\`02.. �. \i 'a.�Szti
45.0 50.0
4' kx,2�.,`•y?T ?, t, s tF.#aF:.
�`}?��t�\�jz;,Ft �i}�}�Foi `7?';:'�u,{1t ititrry, .v59Fi�Y�3s h:"v
1`; ^t �ati1 +,,{ :t ?,# ^.. >.., ¢.i ttt\trti
,`v5'3�� t r�:>tl i. ..,;"'.'{.R.,.�{�s
lls"„z\,t}\'?`F\�;eh14I'I.:.zF:l■'
:R;xt�`,\} lt:�,{ty
t+`t'%��41`1�1.`C�\�?t`�,raa�:
``1`{`{cX.�:1''9+.'b{fijt
f'l} ° is �'� is};ti tti�v�:t, �.ti .,' `"�:$`\ '. \� °'
Y.t,{f:.'>•\7l 4`iq�`.q's?:�, rta, �� �F� ��tl.. �' 1
tlit }' 15ftt3t•, t```�s 4; $y�'1tt .'t`,�`?j�x:..`Ce'x'F St'\X S���;,�
,E ,,y�if� t�_e". a�e'� a•..t s�.
`:.}� .}T"� stN!`���� lk
.'..�F,:@e
�\����`•a"iA a.
>`°'.`�'4??i
tt
t..s..;,t� 4g`u.
DWQ Form MR-1 (01/00)
Charlotte

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
iant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S. MAIN ST., FINDLAY, OH 45840
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: T. J. Aydt, Deputy Assistant Secretary
Permittee (Please print or
Signature of Peitte
419-422-2121
June 30, 2015
Permittee Address
Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Units information pages.
Use only units designated in the reporting facility's permit for reporting data.
* ©RC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

NT
T NO. NC0046213 DISCHARGE NO.
NAME Marathon Petroleum Company LP
001 Month February
CLASS County
Year 2015
Mecklenburg
ERATOR IN RESPONSIBLE CHARGE (ORC)
CERTIFIED LABORATORIES (1 (1)
CHECK BOX IF ORC HAS CHANGED
N/A GRADE N/A PHONE
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
20
22
0.088
28
Prism Laboratories, Inc. (2)
N/A
PF�1(SLLECTING SAMPLES David Morris
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
Y REQUIREMENTS
UARTERLY REUtREMEN
RECEIVED/I11C01DWR
DATE
APR 7 Z015
WQROS
Monthly Limit
DWQ Form MR-1 (01/00)
Charlotte
45.0
50.0

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
"ant
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
etc., and a time table for improvements to be made,
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
539 S, MAIN ST., FINDLAY, OH 45840
Marathon Petroleum Company LP
By: MPC Investment LLC, its General Partner
By: T. J. Aydt, Deputy Assistant Secretary
ermittee (Please
Signature of P
419-422-2121
June 30, 2015
Permittee Address Phone Number
Permit Exp. Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by vi
the Water Quality Section's web site at h2o.enr.state.nc.us/wqs and linking to the Unit's information pages.
n
Use only units designated in the reporting facility"s permit for reporting data.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506(b)
(2) (D).

Monthly Limit
DWQ Form MR-1 (01/00)
Charlotte
0 NC0046213 DISCHARGE NO,
E Marathon Petroleum Company LP
OR IN RESPONSIBLE CHARGE (ORC) N/A
TIFIED LABORATORIES (1: (1) Prism Laboratories, Inc, (2)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
Attn: CENTRAL. FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27899-1617
H RS
001 Month January Year 2015
CLASS County Mecklenburg
GRADE N/A PHONE
N/A
PERSON(S) COLLECTING SAMPLES David Morris
N/A
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
MONTHLY REQUIREMENTS
000
QUARTERLY REQUIREMENTS
ELC
7.kP. 27i115
DAZE_
rteuEIVED/NCDENR/DWR
MAR 9 2015
• NUAL
$0
u
0 04
ue u •/1 u•ll
tatAtift
4IttnitSP
10
12
830 0.25
u-41.704 gpio.
Y 0,270
800
0,25
0.286
14
-ammt-M,
ViOavitti
16
Zilarge '''*r<145
18
itzttAso
20
t:f tkig,
22
titi150 aliS4-467
24
A N4,4:442
;,:4,„"ftw41-'3,4*It-0 i-WPOINO
26
28
30
AVERAGE
0.204
UM
MINIMUM 0.002
.104014y 0
45.0
50.0
.5\

Facility Status* (Please check one of the following)
VAllmorfltoringdabaandmsmpUngfm»quenoiesmeetpermbrequ|rements
All monitoring data and sampling frequencies do NOT meet permit requirements.
Co
iand
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance,
ahc,and gtime table for improvements hobemade.
^| uertify, under penalty of law, that this document and all attachments were prepared under mydirection or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based onmy
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. |emaware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing x\o|m\innu.^
Marathon Petroleum Company LP
By: K8PCInvestment LUC.its General Partner
By: TJAydt, Deputy Assistant Secretary
Permittee (Please print or
Ai
Signature o
419-422-2121
2/13/2015
June 3O.2O15
Permittee Address Phone Number
Permit Exp, Date
Parameter Code assistance may obtained by calling thePoint Source Compliance/Enforcement Unit at [phone] or by visiting
the Water Quality 8ecdon'sw,eb site ath2o.encstate.no.unkmonand linking to the Unit'sinfonnmdon pages.
Use only units designated in the reporting facility's permit for reporting data.
~ORCmust visit facility and document visitation of facility as required per 15ANCAC8G�02O4�
If signedbvotherUhanUlepemndbee.de|eoodonofsi natoryaudhodtymustbaonfi|ewiththeabahsper15ANCAC2B4O5OG(b)

(664) 77 42.
77.6938
PO, Box 1 E414, Greenv I C29686
4 Craftsman Caw, Gr?er, C 2965E
Pimephales promelas 24 Hour Acute Pass/Fail Test
EPA-821-R-02-012 Method 2000
Client: MARATHON
Facility: PAW CREEK
Prism Sample ID: 001
Test Date: 06-Jan-15
Laboratory ID#: T44441 APF
Test Reviewed and Approved By:
W
Robert W, Kelley, Ph,D.
QA)QC Officer
Certification #E8781.9
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida. Dept, of Health Included results pertain only to provided samples,
Page 1 of 4
Forbad Rostampour
Laboratory Director
SCDI IC Certification #23104
11 C D EN R Certification # 022
Page 6 of 9

t Aetic Toxtcl Re; r at Forf
MAIL OR G NA TO:
Treatment 2
Concentration
Tested
- Acute Pass/Fait Date:
Ina Acute PslFl To lei Te
Pipe # 001 County
Environmental Sciences Branch
Div. of Water Quality
N,C. DENR
1621 Mali Service Center
Raleigh, North Carolina 27699.1621
, ©rgar isrtt Tested:
Pi
Contr
Treatrne
Treatmen
Replicate
B C
n controad
Calculated Student's t
Tabular Student's t
(ONE TAILED)
,94
4,
the absolute value of the calculated t is less than or equal
the absolute value of the tabular t, check PASS
If the absolute value of the calculated t is greater than the
absolute value of the tabular t, check FAIL,.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control, check FAIL.
start end
PASS
FAIL
AT-2 (8/91)
v
Page 2 of 4

nd Date'. 01107/15
Fathead Minnows
48 hour Acute Toxicity Test
Test Mottxxt: EwPA 821 R-02-012 ; tutethod 2000 Pi
Time. 15
Test Vessel
500 mL plastic cup
Rundomixati©o pattern per SOP
TEST ORGANISMS
for Ceriodaphnia dubs
Date Removed:
Pimephales promelas
Mysidopsis bahia
Test Solution Volume
200 mL
dud By: JC
Incubator
#1
Transfer Volume
0.5 mL
(Neonates from common holding vessel 'Light. 50 -100 ft-c. 16 Itt light / g hr dark
Between:
Source;
and;
0 Age: 7 DAY
Age;
lrg
Conc,
Control
90,0%
d
Ti
MORTALITY DATA
Mittel*
10
10
10
A 10
10
C 10
Cumulative Mortality
0
isk 4 Lr flu 0&»
0
0
0
D 10
A
C
A
D
A
A
Final
0%
0%
Dilution Water
Surface (4011)
Comments;
NC H2O BATCH 1-6-15
Page 3 of 4
Page 8 of 9

P© Box 16414, Grennuittn, SC 2960$ 7414
[phone], (BOO) 891-2325 Fax[phone]
Shipping Address: 4 Cransman Ct, Greer, SC 29550
WWW-LI; aNVIR©NM AL.GGM
Client:
Facility:
State;
(Grab or Composite)
SAMPLE lid C5 'Cornpesntc5en tnate T#ma Samnnn Ca
ample Custody Transfer Record
Dnte Time Relin tz'tshed
Containers
Sign, and Print below
the dotted line
Collected try,
UST DY C
Presen,o the
1=H2504
2. HCL
3=1NO3
•I NaOH
3=ZN1c
d $ F t Organization
Param eters
Receipt
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours. Equal volun
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportional: As per instructions in NPDES13ermit.
5 EMPER4TURE MONITOJUNCr PROCEDURES
Satrnple temperature during cion and transport must be between
0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bags,
HOLD TIME PROCEDURES
For toxicity testins the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.