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HomeMy WebLinkAboutNC0085944_Complete File - Historical_20171231State of North Carolina Department of Environment, Health and Natural Resource Division of Water Quality ` x James B. Hunt, Jr., Governor Jonathan B. Hewes, Secretary . Preston Howard, Jr., P.E., Director Mr. Joe A. Began Manager of Environmental Affairs Fleet 'Transport Company, Inc. 1300 East 9tb Street Suite I 100 Cleveland, Ohio 44114 • 0 April 14, 199 T r " 97 v Subject: NPDES Permit Application Permit No. NCC944 Fleet Transport Company, Inc. Mecklenburg County "Ilk ; An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper State of North Carolina Department of Environment, IV" X.Y_ VA' Health and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary ED FE INJ F-4 A. Preston Howard, Jr., P.E., Director May 9, 1997 N, r. 1) 100 OF 'S & N,%TURAL M�,X)UTRCV Mr. Joe A. Began Manager of Environmental Affairs MAy 1, 4 1997 Fleet Transport Company, Inc. 1300 East 9th Street 00OF flu"Luv[ST'R lukAIRIAT Suite 1100 "[VUE MRAL IFINE Cleveland, Ohio 44114 Subject: Return of Permit Application Return Number 866 Fleet Transport Company, Inc. Mecklenburg County Dear Mr. Began: associated material received on September 17, 1996. A letter, dated April 14, 1997, was drafted and sent to your attention to outline the additional information required to complete the review of the subject application. Please be advised that the subject application is being returned because you failed to fulfill the obligations of the additional information request by the deadline of April 30, 1997. Should you have any questions regarding this application, please do not hesitate to contact Jeff Myhra at (919) 733-5083, extension 597. Sin erely, Preston Howard, Jr., E. cc: Central Files INIF001140", 0 0", Permits and Engineering Unit, Jeff Myhra Mr. Paul A. Banks, Banks Environmental Consultants, P.C. P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-7015 FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper SOC PRIORITY PROJECT: Yes No X To: Permits and Engineering Unit Water Quality Section Attention: Jeffrey Myhra Date: November 6, 1996 NPDES STAFF REPORT AND RECOMMENDATION County: Mecklenburg MRCS No. 96-181 Permit No. NCO085944 PART I GENERAL INFORMATION 1. Facility and Address: Fleet Transport Company 6712 Freedom Drive Charlotte, N.C. 28130 2. Date of Investigation: 10-30-96 3. Report Prepared By: Samar Bou-Ghazale, Env. Engineer: I 4. Persons Contacted and Telephone Number: Mr. Paul". Banks, Geologist with Banks Env. Consultants, P.C.; tel# (704) 334- 3967 5. Directions to Site: From the junction of 1-85 and Highway 27 in Charlotte, travel west on Highway 27 (Freedom Drive) approximately three (3) miles. The site is located on the right side of Hwy 27 approximately 300 feet north 'of the intersection with Little Rock Road (SR 1641). 6. Discharge Point(s). List for all discharge points: Latitude: 350 161 3611Longitude- 80* 481 55" Attach a U.S.G.S. map extract and indicate treatment facility site and discharge point on map. USGS Quad No.: F 15 SW USGS Quad Name: Mountain Island Lake 7. Site size and expansion are consistent with application? Yes X No If No, explain: 8. Topography (relationship to flood plain included) Sloping east toward an intermittent stream at the rate of 2 to 4%. The ppppp� F site is not locatedin a flood plain. . Location of nearest dwelling: Where are several businesses within` 00 feet of the site. A drinking water well is located at 6518 Freedom Drive approximately 600 feet from the site. A second drinking water well is located at 700 Windgate Road approximately 1:100 feet from the site. 10. Receiving stream or affected surface waters: Unnamed Tributary to Paw Creek. . Classifications C 34 b. River Basin and Subasin No.: Catawba; -ti8- C. inscribe receiving stream features and pertinent downstream uses: The receiving 'stream is a wet weather ditch. general "C" classification uses downstream. PART II -- DESCRIPTION OF DISCHARGE AND TREATMENT WORK 1.. a. Volume of wastewater to be permitted: 0.000144 D b. What is the current permitted capacity of the wastewater treatment facility? N/A C. Actual treatment capacity of the current facility (current design capacity)? N/A d.Date(s) and construction activitiesallowed by previous Authorizations to Construct issued in the previous two years: 'A e. Please provide a description of existing or substantially constructed wastewater treatment facilities: N/A f. Please provide a description: of proposed wastewater treatment facilities* The proposed`treatment facilities will consist of an oil/water separator, air stripper, and carbon adsorption. g. Possible toxic impacts to surface waters: Discharges of this nature have been shown to be toxic. h Pretreatment program (PC'Ws only): N/A . Residuals handling and utilization/disposal scheme: Generation of re idu is is not expected. XPDES Permit Staff Report Version 10/9 Page 2 A AM 1� 'AM 3. Treatment plant classificati( sheet): Proposed, no rating g.-' 4. SIC Code(s): 5171 Primary: 39 Secondary: 66 Main Treatment Unit Code: 560( PART III - OTHER PERTINENT INFORMAT'. 1. Is this facility being constri Funds or are any public moniea N/A. 2. Special monitoring or limit requests: Toxicity may need t the suspected toxic nature of 1 3. Important SOC, JOC or Complia indicate) N/A. A 'A 1 4- 4 ",m A rl;m I 'crc i C P'IrA I IlAt i M (attach completea n. ed with Construction tuna (including tc a discharge. e Schedule dates: Has the facility e regional perspective for each option evaluated. Spray irrigation: This option has been evalue permittee and found not to be a viable alternal limited space. Connection to regional Sewer System: The Charlotte exists at the site. No hazardous materials concern. Air quality permit for this site may be required by Mecklenburg County. PART IV - EVALUATION AND RECOMMENDATIONS Fleet Transport Company, is requesting NPDES Permit for the discharge of treated groundwater at the subject facility. NPDES Permit Staff Report Version 10/92 Page 3 It is recommended that the NPDES Permit be issued once 'tl above mentioned concerns regarding toxicity have been addresse< and comments from GW Section have been received. Signature of rot Preparer Date { ,.f Vatr salty 1 onalxa isor ate NP ES Permit Staff Report Version 10/92 Page 4 i Carolina Department of Environment, Health and Natural Resources ` j Division of Water Quality � !Al L4j* lot James P. Hunt, Jr., Governor Jonathan B. Howes, Secretary I A Preston Howard, Jr., P.E., Director 6 , l October 1, 1996 E_ ... tt 0 . Joe A. Began Environmental Affairs Manager. 1300 East 9th Street, Suite 1100 Cleveland, Cho 44114 Subject. I PDE Pen -zit Applicai Fleet Transport C:'ompai Mecklenburg County Lear . Eegatt: /VC a The Division of Water Quality acknowledges receipt of the following information • NNPDE Application for permit to discharge. 55 ,00 application fee.... The Division recognizes that the requirement to submit all applicable analytical results has beet ury conta elation: s raxe::titacr that ear:.A�'Tr�rf. ccrrllr..::T�'ritlrr-yl ff'rYe�*air�rrYicrar ware>r<.�r-r� ,a recommendations regarding this discharge, Your' ill be advised of any atnmendations, questions, or other information necessary for the application review. ae any questions regarding this application, please do not hesitate to contact me at 3, extension 597. OV4 era is Group NIVAINNONNOWermits and Engineering Unit Ord C. Whittlesey, RE. Environmental Consultants, I.C. Boy 1125 otte, NC 2220 535, Raleigh; North Carolina 7525-0535 Telephone 1-733-7015 FAX 91-733-07'1t Equal Opportunity Affirmative Action Employer 0% recycled/ 10% past -con urner papei %$;s OCT 4 1% i. Q NATIONAL POLLUTANT DISCHARGE ELIMINATION TION SYSTEM APPLICATION TI FOR DISCHARGE PERMIT Fleet Transport Company 6712 FreedomDrive Charlotte, North Carolina PREPARED BY Hank.sEnvirownental Consultants, P.O. Box 11252 Charlotte, North Carolina 28220 NPDES APPLICATION FOR DISCHARGE Fleet Transport Company 6712 Freedom Drive Charlotte, North Carolina July 30, 11 A PREPARED FOR �.04 Feet Transport Company, Inc. SEAL 1300 East th Street Suite 1100 r Cleveland, Ohio 44114 p ��� '' wskq. "',o C'' Paul A. Banks, RG, Date�Khirtlesey, RE, 1 1e Senior Geologist Profession Engineer Ranks .'nvironme ntaxl Consultants, R t": Sole Proprietor rietor r' Affiliate R0, Box 11252 Charlotte, North Carolina 220 Telephone (704) 334-3967 Fax 704) 4-3 6 Project No. 4.0 4,004 TABLE OF CONTENTS APPLICATION FOR DISCHARGE PERMIT SHORT FORM C-GW ................ i 1.0 REPORT OF ALTERNATIVES TO SURFACE WATER DISCHARGE ....... I LI General Information ..... ....... 1 I. Evaluation of Environmental Feasibility of Discharge Alternatives 1 1.11 Connection to Sewerage System .. 1 1.2.2 Subsurface Disposal System ....... I I . 2.3 Spray Irrigation System 2 L3 Proposed Discharge Alternative 2 1.4 Cost Estimation and Comparison 3 1.4.1 Subsurface Disposal System ...... ........ 3 2.0 PROPOSED REMEDIATION PROJECT ................................. 3 11 System Concept —,3 2.2 Treatment Methods 22 1 Soil/Free Product Treatment ............ 4 2.2.2 Groundwater Treatment.. 5 3.0 GROUNDWATER QUALITY ........................................... 5 REFERENCES TABLES Table 1: Summary of Groundwater Analytical Results FIGURES Figure 1: Site and Discharge Point Location Map Figure 2: Site Configuration Map Figure 3: Proposed Infiltration Gallery Figure 4. Remediation Configuration Map Figure 5: System Components Layout APPENDICES Appendix A: Infiltration Gallery Calculations Appendix B. Infiltration Gallery Cost Estimate Appendix C. Well Yield Estimate Calculations Appendix D: Laboratory Analytical Documentation Division of �nvtrunmenLai rianagernenL, P.u. oox NATIONAL POLLUTANT L)ISCHARGE ELIMINATION SYSTEM APPLICATION NUMBER 1AMIK-1 114111/ APPLICATION FOR PERMIT DISCHARGE SHORT FORM C—GW Date Received To be filed by persons engaged In groundwater ytar ftnth Day remediation projects, (DEM USE ONLY) be not attempt to complete this form before reading accompanying instructions. (Please print or type) 1. Name, address, location, and telephone number of facility producing discharge A. Name et Tram cri an Inc. B. Mailing address 1. street address 1300 East 9th Street,Sup. tee 1100 2. City Cleveland, 3. State Qhi!2 4 Zip 44114 C, Location: 1. Street 6712 Freedom Drive 2. City harlotte 3.5tate %Tnrtb Carnl J n;q 4. County mecki-an D. Telephone No. QD4L)- 394-1 312 E. Nature of business Tiaili-ds J:Lanspart 2. Facility contact A.Name mr. aaa 'Regan B. Title gnviron ental Cordinator C. Telephone No. (-21B - 664-Annn 3, The application is for (Ma new permit, E3permit renewal, [3 permit modification. rm SIC [= (if known). if application is for renewal or modification, please Indicate pe it number: NCOO 4 Product(s) recovered Diesel [Diesel fuel, leaded or unleaded fuel, solvents, etc] This application must also Include the following: A) A report of alternatives to surface water discharge as outlined by N.C. Permit and Engineering Unit's *6uidance for Evaluation of Wastewater Disposal Alternatives," [Required by 15ANCAC 211.0105 (0). (CHAPTER 1D) 8) An engineering proposal detailing the remediation Project. (Required by 15A NCAC 2H .0105 (01. (CHAPTER 2) C) A listing of any chemicals found In detectable amounts with the maximum observed concentration reported. The summary of analytical results containing this maximum value should also be submitted (i.e. the listing, not the graphical scan). The most recent sample must be no older than one year previous to the date of this application. (CHAPTER 3) For fuel remediation projects, volatile organic compounds should be scanned along with any suspected fuel additives. The following compounds should be included: benzene*, toluene*, ethylbenZene*, xylene*, lead, methyl tert-butylether (MTBE), dibromoethane (EDB), 1,2-dichloroethane, Isopropyl ether, naphthalene, phenol. An EPA approved method capable of detection levels to 1 ppb should be used to detect these compounds for solvents or unidentified products, an EPA Method 624/625 analysis should be provided, with the 10 largest peaks, not identified as one of the targeted compounds and not present in the procedural blank, identified and approximately quantitated. [As per the same guidance stipulated on NCDEM's Annual pollutant Analysis Monitoring (APAM) Requirement - Reporting Form A," Revised June 1990). If metals or pesticides are suspected to be present; these should e analyzed to the same detection level as presentedin the NC APAM. A) The removal efficiency of each compound detected for the proposed project should be provided, if known. Removal efficiency of each compound will be determined during startup test. S. Name of receiving wager Dry stream bed - tributarLr tc Paw tSreek IFLLure 1 Attach a USGS topographical reap with all discharge points clearly marked. . Is potential discharge directly to the receiving water? If not, state ID&ciLtcally. the discharge point. Di h e is tO a dry stream bed located alona eastern 2rop. boundary Mark clearly the pathway to the potential receiving water on the site map. [This includes tracing the pathway of the storm sewer to its discharge point, if a storm sewer is the only viable means of discharge.] (Figure 1 ) 7. Amount of treated groundwater to be discharged in gallons per operating day: 144 ga l/day B. Describe the duration and frequency of the discharge (continuous, intermittent, seasonal) including the months of discharge, number of days per week of discharge, volume treated (monthly average flow` in gallons per day). Discharge is ro °ected to be low flow continuous 7 days/week. A monthly average flaw may be 4320 gals. I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete, and accurate. J, rAA) PRINTED Name f e Pn Signing 'Title �w SIGNAT , RE f Applicant Cate Application Signed North Carolina General Statute 14-21 S,6 (b) (2) provides than Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan or other document files or required to be maintained under Article 21 or regulations of the Environmental management Commission implementing that Article, or who falsifies, tampers with or knowingly renders inaccurate any recording or monitoring device or method' required to be operated or maintained under Article 21 or regulations of the Environmental management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to exceed S 10,000, or by imprison- ment not to exceed six months, or by both. (1 S U.S.C, Section 1001 provides a punishment by a fine of not more than S 10,000 or imprisonment not more than 5 years, or both, for a similar offense.) 1.0 REPORT OF ALTERNATIVES TO StJRFACE WATER DISCHARGE The following chapter presents alternatives to surface water discharge as outlined in the "Guidance for Evaluation of Wastewater Disposal Alternatives", 1.1 General Information Facility Name. FleetTransportCompany, Inc. (Figure 1 ) County. Mecklenburg Facility Address. 6712 Freedom Drive Charlotte, North Carolina Report Preparer's Name . Paul A. Banks, P.G. Mr. Cliff C. Whittlesey, P.E. Licensed Geologist 1361 Professional Engineer 12000 Report Preparer's Mailing Address. P.O. Box 11252 Charlotte, North Carolina 28220 A detailed description of the proposed discharge facilities is provided in Chapter 2 of this report. 1.2 Evaluation of Environmental Feasibility of Discharge Alternatives 1.2_.l Connection Ig Sgn&L4g& Sewer service should be capable of an additional 240 gallons per day, which is a minimal additional flow. The connecting pipe would be a 4 inch diameter PVC pipe. Charlotte Mecklenburg Utility Department is not presently accepting any applications to discharge treated recovered groundwater to the county sewage system. Location of the sewer system to the property, sewer routes, slopes, etc. do not affect the co ty's position on this matter. 1 It has been determined that the zone of unsaturated soil to be considered for a subsurface disposal system is enon sandy loarn soil. This soil type has very slaw permeability. Based on the Mecklenburg g o ty soil survey, the ;permeability of this soil ranges from 0.06 to 0.2 inches per hour. An average of0.13 inches per hour was used for the design. Available water capacity` ranges between 0.15 and 0.2 inch per inch. An average of 0.175 inch per inch was used for design. The resulting loading rate is 0. 00 186 cu, ft. per hour per sq ft. of water flow (Appendix A). Page E Y Land size required based on loading rate: based on attached calculations, 15,000 sq ft of area is required for the initial field and a reserve area of 15,000 sq ft. is required. e site does neighbor residential property, less than 100 ft. from the required system location. The subsurface field may be located over 50 ft. from the property line. Reduction in recovered groundwater flow would reduce the amount of area needed for the absorptive system, but it would also greatly increase the time required to remediate the site. There is sufficient usable land on the project site to install a subsurface absorptive system. The calculations included in Appendix A determine that a total of 30,000 sq ft would be required for a subsurface disposal system with 100% reserve area. The area available for the field is presently a gavel parking lot. It is possible to install the system and it is possible it will work, but thereis the likelihood that the permeability is less than the design, which will cause the system to back up on a consistent basis, preventing the remediation system from operating. ;The subsurface disposal system is also costly, approximately $20,000 before consultant markup. It was found that no neighboring land is presently available to the site for purchase or lease. 1,21 Snrav Irrigation It has been determined that the zone of unsaturated soil to be considered for a spray irrigation system is enon sandy loam sail. This soil type has very slow permeability, and would not b suitable for consideration for the installation of a spray irrigation system. The required system size would make this choice uneconomical. The majority of the surface of the site is compacted crusher run and gravel, which has a very high runoff coefficient, A high runoff coefficient surface would not be acceptable for the installation of a spray irrigation system.. The buffer zone requirement of 400 ft. may not be complied with on this site for the installation of a. spray irrigation system. Reduction in recovered groundwater flow would reduce the amount of area needed for the spray irrigation system, but it would also greatly increase the time required to re el ate the site. There is insufficient usable land on the project site to install` a spray irrigation system. It was found that no neighboring land is presently available to the site for purchase or lease. 1.3 Proposed Discharge Alternative The alternatives discussed related to sewer and spray irrigation were not found to be feasible. Subsurface re -infiltration is feasible, but much more costly than discharge to surface waters. Discharge to the sewer system is the preferred course of action to take, but is not available per aL,e 2 the Charlotte Mecklenburg Utility Department, The proposed location of discharge at this site is a dry stream bed, not a flowing stream (Figures I and 3). 2.1 System Concept The proposed Phase I remediation of this site involves removal of free product and extraction of petroleum hydrocarbon vapor from the vadose zone (Figure 4), The vadose vapor extraction system will consist of 3 four -inch, 0.02" slotted PVC vapor extraction points installed vertically to a depth 15 feet below ground surface. The free product removal system will consist of one six-inch, 0.02" slotted PVC product removal point installed vertically to a depth 30 feet below ground surface, Vapor extraction will also be conducted from the six-inch free product recovery point. To promote vapor movement at depth and encourage biodegradation, two passive inlet wells will be also be installed to 15 feet below ground surface. Soil vapor extraction modified to include passive air injection is proposed over bioremediation and natural attenuation to more quickly remediate the unsaturated impacted portions of the site. To accommodate and account for heterogeneities in the subsurface and to promote natural indigenous biodegradation, passive ambient air injection wells are proposed in addition to vapor Page 2.2 Treatment Methods �! I III I U - IL 71_1 L, , I Vapor removed from the product recovery well and vapor extraction wells will be transported through two-inch PVC piping from each extraction point to the remediation system enclosure. Moisture contained in the vapor will be separated out and collected prior to treatment and discharge. Vapors will be appropriately treated to meet discharge concentration requirements set by the Mecklenburg County Environmental Protection Department. Proper treatment of the vapors will be determined using vapor concentration data obtained during the startup test Page 4 u conducted prig to continuous system operation. If required, -carbon vessels will be used in the up flow position to treat vapors. 2.2.2 Groundwater Treatment Groundwater remediation will be conducted via a vacuum enhanced pump and treat system. Groundwater will be removed from two six-inch diameter recovery wells specially designed and located to control and remove petroleum hydrocarbon impacted groundwater at the site (Figure 4). Groundwater removed from these recovery points will be treated within an above to achieve the required clean up level concentrations for each constituent identified during GSA activities at the site. Prier to implementing the groundwater remediation system, aquifer pump test data will be utilized to confirm estimated well yield and pumping cycle time calculations. For the purpose of creating the Phase 11 system design included in this report a 0.1 gal/min well yield estimation was used. This estimation was derived using the Theim equation, assuming a 10 foot drawdown and a saturated thickness of 50 feet (letter, 1988). The resulting yield was then doubled to account for the effects of vacuum applied to the well. Field estimate calculations are included as Appendix C. Banks Environmental tic pates that one groundwater recovery well will be located in the area ofgroundwater monitoring wells -4'and DW-1. In the event pump test data indicates adequate well yield, the proposed product recovery well may be converted into; a groundwater recovery well following removal of all free product from the area surrounding groundwater monitoring wells MW-6 and - . However, the proposed free product recovery well will not be advanced beyond 30 feet below ground surface in order to minimize vertical contaminant transport during the Phase 1 ` erred ation period. Groundwater will be removed from the recovery wells using a four inch diameter top loading automatic pneumatic atic total fluids recovery pump. Recovered groundwater will be transported below ground through, 3/4 inch diameter 160 psi rated HDPE tubing encased in I. 5 inch diameter 160 psi rated HDPE tubing serving as secondary containment. Groundwater will then enter a prior to e The oil water separator will be located outside the system` enclosure in order to minimize vapor accumulation within the system building. r r' fge tgur . 3.0 GROUNDWATER QUALITY Groundwater assessment at the subject site indicates the presence of petroleum based hydrocarbon constituents. Based on the concentrations of constituents found, the predominant fuel source is thought to be diesel, although constituents common to gasoline and solvent compounds have also been detected. Table I summarizes laboratory reported contaminant Page S' i concentrations for groundwater samples collected on May 20, 1996. Appendix D contains the laboratory analytical documentation corresponding to this sampling event. The groundwater samples were analyzed by EPA Methods 502,2 and 610. Sampling events conducted prior to May 20, 1996 included analysis of constituents by EPA Method 625, Results of the EPA Method 625 analyses indicated the presence of constituents which can also be analyzed by EPA Method610, Approval for 610 analysis in lieu of 625 was given by the North Carolina Department of Environment, Health and Natural Resources prior to the May 20, 1996 sampling event. The following constituents were identified in groundwater samples collected at the site on May 20, 1996: EPA 502.2 Constituents Benzene* Toluene Ethylbenezene Xylenes 1,3 - Dichlorobenzene 1,4 - Dichlorobenzene 1,2 - Dichlorobenzene Isopropylbenzene* n-Propylbenzene* 1,3,5 - Trimethylbenzene* 1,2,4 - Trimethylbenzene* s - Butylbenzene* 4-Isopropyltoluene* n-Butylbenzene* Naphthalene* EPA 610 Constituents Anthracene* Acenaphthene Fluorene Fluoranthene* Naphthalene* Phenanthrene Pyrene* constituents having concentrations greater than 2L Class GA Standards. i REFERENCES Fetter, C. W, 1988, Applied F ydr rgeolog (2nd. Edition): Merrill Publishing Company, 592 p. Page 'TABLE I SUMMARY OF GROUNDWATER ANALYTICAL RESULTS SAMPLED 5/20/96 FLEET TRANS PORT COMPANY ("HARLOTTE, NORTH CAROLINA Com)onent Name EPA 502.2 MW-1 MW-2 MW-4 MW-S MW-6 MW-7 MW-8 MW-10 MW-11 DW-1 21. Class GA Standard Benzesic BQL _ '74 - B )L. �_QL E_QL_ 130t, 28 B�, L " 'L BQL, I Toluene NL p �L-A 1.9 BQL ;B B Q 1, ffL,B 00 EtliN lbenzenc EQL,_ EQL 6,6 B 11 -±QL- L 1- 16 130 BOL, 1 B 1, 29 XN,lcncs BQL B_ �L _ I �) B 1�i B L B L 13 0 () L. 530 13 - Dichlorobenzenc BQL BQL BQL BOL BQL BQL BQL BQL 1 L2 8 )L B)L 620 IA - Dichlorobenzenc B Lw -BQL- B L B L B L B L B �)L L j4 BQL 75 1,2 - Dichlorobenzene B )L pQL __.fjQL POL L 1301, -B �2L 1-4 B OL 62o YQL _AQL_ 17 BOL _LQL B01, _LQ_ BOL _ I0 BC1. --.-Z�- B L NL ' L -A2L- 12 :=I BQL --,!iQL- BQL L I I BQ1. BQL NL 13.5-Trinicth5 lbenzenc - - --- B L --p(�x,_ 10 -- BOL BOL — B !iL -Q—_ -B-(-,) (2t, 9 L_ j�qL N1, I-- -' rinicilivibenzene BQL BQL 35 B01 L 2.2 1301w _A B I. 83 BQL BQL N1, s-Buo, lbenzen B 1. B L 7 BOO B:O:L:IQL Qi— 4.6 NL BQL BQL I BQL F3 H. 3.2 B01, Nt, B(,)L PQL 17 B X B L RQ1- BOL 20 BQL B X, NL BQL BQL 80 B)L 2 ' 19 BQL. BQL 100 3.7 BQL 21 I 41m �W.v I�Q� )L�qamcters B)L B L BOL B fM nnf - Inic EPA 614) 110 BO, L, 180 BQL BC L 63 BOL BOL 21 P-Q-L— --q-Q—L B 1. 3i BOL BQL B L B F. BE 1 NL —L --P�QL- --M—L L 11 B X )t �L 80 Fluorene BQL B2! --§-Q-- 6,5 BOL —9.5 12 --N -L- BQL ---!iqL- BOL --pQ -- 18 --T� -i� BQL - 280 Phonanthrenc !BIQI, )L B L 10 — B)L B L B 1, _B01. B 11 B 210 Fluoranthene Btl, J# BQL 5 BQL LA ABI 13 13 L B BQL NL IN rene )L EBQL B 1, 2.9 8.6 ES� B PQL _J�L)L BOL BQL NL ('ornpontnt Name RCWA Metals _QL Arsenic —NT —NT NT —NT _Nf- 50 . Barauaas NT —NT 190 —Wl� —NT —NT 230 ---2000 Cadmium NT NT NT NT —NT BOL NT N,r NT �L 5 Chromium NT NT NT NJ' NT BQL NT NT NT BQL io Lead N7' —NT NT ITT— —NT BQL NT NT NT Qt, 15 klcrcur� NT NT NT NT NT 0,4 NT NT NT _B() 0,7 H Sclenium NT NT NT NT NT 13 L �NNI�N T NT 50 I-INer E� NT NT NT NT NT 1301- NT N --Nt" 18 All results are shown in pg/L NL. = Not Listed NT = Not'rested BQL = Below Quantitation Limit f f 17 -.,\DISCHARGE POINT LOCATION Me LN�Oe t�o lz�11 If j N a iie r *j ind Z SITE LOCATION:*r� '7 8 VI �4 714 r d <1 14,1111 n n a m e FIGURE I SCALE Prol. No, Batiks Environmental Site and Discharge Point Location Map 1.5 2(9)0' Date, 7 1196 Consultants, P.C. Fleet Transport Compam Charlotte, North Carolina D,�kp, Fdo: NPI)ESI DC2 750 760 75 77 r 't 50' MIN, ' t INITIAL t MW-10 ,INFILTRATION , I 1 GALLERY MW 7 AREA ; INTERMITTENT STREAM BED M-9 4 t . t MW-11 l o O W- -- i i._--i PROPOSEDDISCHARGE POINT . •. MW MW- '. 4 k MW01 -8 RES `RVE APPROXIMATE TREE DINE D-1 AR MW-5 I ; Y t 4 � i OVERHEAD POWER LINE 0' MIN. LEGEND i GROUNDWATER MONITORING WELL 780 770 APPROXIMATE FENCE LINE 750 750 APPROXIMATE PROPERTY BOUNDARY t . I FIGURE tIPR XIM N 1 !tALF 'rtj, No,: 4.014tt4 Banks Environmentali a}1'ry Infiltration. ( 0 I130 60 100 200 .W�I�p}��d Consultants, P'. Fleet Transport Company l� bite. �7/23/96 Charlotte, North Carolina ) g;. File NPDES3 IBC 2 NU l H Mw-I()' 's4iGV`-7 FORMER UST PIT PASSIVE AIRP JEC"TION SYSTEM ENCU)SURE -"�,7pFr7:aimr.xi vnr>t��' MW-6 ,01 . 6"VAC'UUNI-1SSIS FREEGROT."N('rt�i.';t Et2i'E€t7DE-(1 �- Rt C'OVER4' L1k'RI:L mW1 vh PASSME AM INJECz i ). . .. ... ... - MW 41 � t~>l2tat`NI7WATER f>i';CHARGE i a\T m.a M-2 -R R)RMER Us r I'll 4" V,ld"CtR CXS'f ACTION WELLS. M4V-w i7 a 0 r�rcx LEGEND GROUNDWATER MONITORING WELL M PROPOSED FREE PRODUCT V 1POR RECOVERY VLT I,I„ 10 PROPOSED V'.VP0P RECOVFRY WELL PROPOSED PASSIVE AIR INIFCTIOIN' WELL is PR()Pt,1SF:[1 NMAL GROUNDWATER RECo ERY WFI POWER POLE OVERHEAD POWF.iR ti?t%. Environmental FICA (� R i I ORAPHIC SCALE i'rgj No -i 014 004 l medication t iimn Map 3° 0 is 30 w Date. 7 2496 r t t ► Fleet Tran p � � E=tE any Charlotte, �r — t _z' diva-InFeet) Utvg File NP)FS4JSC' FLEET TERMINAL FACILITY GV1f DISCHARGE VAPOR I - 3" ILIA. SCH. 40 PVC OUT AIR SUPPLY OUT VAPOR DISCHARGE, 4'"CIA SCH. { PVC, 12' TAt.L CONTINUOUS 3" DIA. SCH. 40 STEEL VENT FANi tI ;1 12' TALL VAPOR DISCHARGE ' Kl AIR FILTER t SAMPLE _ SURGE G PORT , 7.5 HP RECOVERED1 (DRC GURGLER DAT TANK) TANK SVES GX 200 } CARBON BLOWER GW AERATION - SHUT OFF , ; VESSELS "" ILIA. TANK ( VALVE !!— FLOAT ,' SAMPLE SCH 40 PORT T NSFER �.� 'SAMPLE SWITCH ' °rto STEEL ' ' 'PORT PUMP ' FORT NC �. VEL. PRESSURE SWITCH � � !SCREEN �r i G 200 � 112" C�#A. i YF' NC COOPER NIGH FLOAT FLOW' METER r SOLENOID; VALVES AIR REGULATOR SWITCH t AIR FILTER SAMPLE IN LINE CHECK HALVE SOLENOID VALVE. ,. GRAIN OPENING PORT VALVE SHUT OFF TO SUMP WITH VALVE 5 HP °r EEC) GAL HIGH FLOAT SWITCH NOT SHOWN: 4-3CI W FLUORESCENT TIMED LIGHT FIXTURES . CONTROL PANELS SOLENOID AIR VALVE COMPR. / 1"TALL THRESHOLD 8'X 20' REMEE IATION 4" FIBERGLASS FRESH AIR SUPPLY SYSTEM ENCLOSURE INSULATION - ' WIDE DOORS METER BASF TO AIR COMPRESSOR (MIN - ' WALL) WALLS AND CEILING DUPLEX OUTLET IGi U R . 5 Prgj, No,: 4,014.004 Banks En vironmental system Components Layout tltt t t ? , F le t 'Franspo Company an SCALE, i Gate: 7/24/9 Charlotte, North Carolina Dwg. File" NPDt: ;.D'2 sercttsezca 2 4-44 " ' OA -n 99 1 '?1 r Iz ere Aq paMoaqo p indwo --.ON Bulme'Cl 10- ,;�-'ON 19914E " jo i n OBI139foJd jjvii l 10 olej Project .S Project No. Subject Sheet No,of Drawing No. Computed by e"e t pate .a "' C�he ked b Gate A Pi 4.,1WAe-F/ '' caeca tl�r Z rf e �t' F. ,!5. EA 02898 7/13189 a sa-5,1 le Ile G/ ?t 0-4( rs ©-5�4 .. :VIC fy /* /",., „�' .� ,/"#...�.3 ...." ,�y ids' d"� /" "'..G.».fff$✓ aleC Aq pad ail ' a;e —Aq paindwoo 'ON Bulme'0 ,�f—ON 4994 Ioafgn 'ON 109fOi d 139 fOJ A1VtEf"'_.qI Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 luntersville, NC 28078 Tel: 7 4-87 -9092 Fax: 794-875-9091 June 04, 1996 Mr. Paul Banks Banks Environmental Consultants 1409 East Blvd. Suite 106C Charlotte,NC28203-5876 RE; PACE Project No. 66520.1 Client Reference: Fleet Dear Mr. Banks. Enclosed its the report of laboratory analyses for samples received May 20, 1996. Footnotes are given at the end of the report. If you have any questions concerning this report, please feel free to contact us. Sincerely, Kjs� 'k Kelly H. Wallace Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This repeat shall not b e, , ,;ced except in full„ without the written consent of Pa -'e Analytical Services, Inc. Pace Analytica9'Services Inc. 9800 Klncey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-09 Pax: 04-87-091 ns Environmental Consultants June 04, 1996 D9 East Blvd. PACE ProjectNumber: 660520512 ite 106C alotte, NC 28203-5876 tn: M. Paull Banks :E Sample Number;' 92 0601890 to Collected: 05/20/96 to Received. 05/20/96 idnt Sample ID: Mtn-11 rwameter Units ML METHOD DATE ANALYZED 3ANIC ANALYSIS LYNUCLEAR AROMATIC HYDROCARBONS 610 phthalene ug/L 2.5 ND 05/25/96 ephtlene ug/L 2.5 ND 05/25/96 e apht ene ug/L 2.5 ND 05/25/96 uorene` ug/L 2.5 NO 05/25/96 enanthrene u L 2.5 NO 05/25/96 thracene u/L 2.5 NO 05/25/96 udranthene ug/L 2.5 NO 05/25/96 rene u/L 2.5 NO 0/25/9 nz[a]anthra ene ug/L 2.5 NO 05/25/96 rysene' ug/L 2.5 ND 0/25/9 nzo[b]fluoranthene ug/L 2.5 NO 05/25/96 n o[k]fluoranthene ug/L 2.5 NO 05/25/9 nzo[apyrene ug/L 2.5 ND 055/96 b n [a,'h an hracene ug/L 2.5 NO 05/25/96 nzo[g,h,i]perylene ug/L 2.5 NO 05/25/96 deno[1,2,3-cd]pyrene ug/L 2.5 NO 05/25/96 to Extracted Date 05246 05/4/96 LATILEiORGANICS 502.2 chlorodi luoromethane g/L 1.0 NO 05/29/96 lorome have ug/L 1.0 NO 05/29/96 loroethene ('Vinyl' chloride)` ug/L 1.0 NO 05/29/96 oromethane ug/L 1.0 NO 05/29/96 ldroethane ug/L 1.0 NO 05/29/96 i hlerdfluoromethan ug/L 1.0 NO 05/29/96 1 Dichl'ureethene ug/L 1.0 ND 05/29/96 chloromethane ug/L 1.0 ND 05,/29/96 a-1,-Dichloroethene ug/L 1.0 ND 05/29/6 1-Dichloroethane ug/L 1.0 ND 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be , ° •7-,-ed except in full, ; without the written. consent : ° t' � e A naiyticsl Services, Inc, ,- Pace Analytical Services, Inc. 9809 Kincey Avenue, Suite100 Huntersville, NC 28078 Tel: 794-875-9992 Fax: 704-875-9091 1 Banks June 04, 1996 2 PACE Project Number: 660520512 Reference: Fleet" mple Number:: 92 0601890 11'ected. 05/09 ceived: 05/20/96 Sample 'ID: MW-11 er_ Units MDL METHOD DATE ANALYZED ANALYSIS E ORGANICS 502.2 -D'ichloroethene ug/L 1.0 ND 05/29/9 .hloropropane ug/L 1.0 ND 05/29/96 `o m ug/L 1.0 NO 05/29/96 clo'romethane ug/L 1.0 ND 05/29/96 1richloroethane a /L 1.0 ND 05/29/96 �hloro-I-propene ug/L 1.0 ND 05/29/96 tetrachloride g/L 1.0 ND 5/2/96 �hloroethane ug/L 1.0 ND 05/29/96 .ri'chloroethene u L 1.0 NO 05/29/96 .hloropr pane ug/L 1.0 ND 05/29/96 hloromethane u/L 1.0 ND 05/29/96 lmethane ug/L 1.0 ND 05/29/96 I-Dichloro-l-propene ug/L 1.0 ND 05/29/96 -Dichiloro-l-propene ug/L 1.0 ND 05/29/96 richloroethane ug/L 1.0 NO 05/29/96 :hlioropropane ug/L 1.0 ND 05/29/96 Iloroethene ug/L 1.0 ND 05/29/96 Ichlorolethane ug/L 1.0 ND 05/296 -Tetrachloroetane ug/L 1.0 ND 09/6 lrrn ug/L 1.0 ND 05/29/96 '-Tetrachloroethane ug/L 1.0 ND 05/29/96 "richloopropane ug/L 1.0 ND 029/6 bnzene ug/L 1.0 ND 05/29/96 "otoluene u/L 1.0 ND 05/29/96 `otoluene ug/L 1.0 NO 05/29/96 .hlorobenzene u /L 1.0 1.2 05/29/96 ,hlorobenzene ug/L 10 1.4 05,/29/96 .hlorobenzene u/L 1.0 1.4 05/29/96 Iromo-3-chloropropane ug/L 1.0 NO 05/29/96 richlorobenzene ug/L 1*0 ND 05/29/96 orobutadiene ug/L 1.0 ND 05/29/96 REPORTOF LABORATORY ANALYSIS This report shall not be reoroducecl except in full, without the written consent of Page Analytical Services, Inc. Face Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Hunter vi(le,1 28078 Tel: 704-875-9092 Fax: 704-875-9091 1 Banks June 04, 1996 ! PACE Project Number. 660520512 Werence. Fleet iple Number: 92 060190 lected: 05/20/96 :eived: 05/20/96 ;ample ID: MW-11 =.r Units MDL METHOD DATE ANALYZED ANALYSIS ORGANICS 502.2 ichlorobenzene a /L 1.0 NO 05/29/96 ug/L 1.0 NO 05/29/96 ug/L 1.0 NO 0/29/9 4 zene a /L 1.0 NO 05/29/96 tzene u/L 1.0 NO 0/29/96 ug/L 1.0 NO 05/29/96 ug/L 1.0 ND 05/29/96 rlbenzene ug/L 1.0 NO 05/29/96 [benzene ug/L 1.0 NO 0/29/96 -methylbenzene ug/L 1.0 NO 05/29/96 aenzene ug/L 1.0 NO 05,/29/96 ^methylbenzene g/L 1.0 NO 05/29/96 aenzene ug/L 1.0 NO 0/29/96 )pyltoluene ug/L 1.0 NO 05/29/96 )nzene ug/L 1.0 NO 05/99 Iene ug/L 1.0 3.7 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9840 Kincey Avenue, Suite 100 Nuntersville, NC 2 078 Tel: 704-875-9092 Pax: 704-875-9091 . 'Paul Banks June 04, 1996 lge 4 PACE Project Number: 660520512 lent Reference: Fleet ICE Sample Nurnberg 92 0601904 Ite Collected: 05/20/96 Lte Received. 05/20/96 lent Sample 'ID: MW- trameter knits ML METHOD DATE ANALYZED 4AIC ANALYSIS iLYNUCLEAR AROMATIC HYDROCARBONS 610- Iphthalene ug/L 2.5 NO 05/25/96 .enaphthylene ug/L 2.5 NO 05/25/96 wenaphthene ug/L 2.5 NO 05/25/96 uorne ug/L 2.5 NO 0/2/9 ienanthrene ug/L 2.5 NO 05/25/96 Ith'racene ug/L 2.5 NO 25/96 uo'rantbne ug/L 2.5 NO 052/9 Frene ug/L 2.5 NO 05/25/96 lnz[a]anthracene ug/L 2.5 NO 05/25/96 lrysene ug/L 2.5 NO 05/25/96 !nzo[b]fluoranthene /L 2.5 NO 05/25/96 pnzo[k]fluoranthene /L 2.5 NO 05/25/96 lnzo[a]pYrene< ug/L 2.5 ND 0/2/96 benz[a,h]anthracene u /L 2.5 NO 05/25/96 !nzo[g,h,, ]perylene a /L 2.5 NO 05/25/96 ldeno[1, ,3-c ]pyrene u /L 2.5 NO 05/25/96 Ite Extracted Date 052496 05/24/96 ILATILE ORGANICS 502.2 chlorodifluoromethane g/L 1.0 NO 05/29/96 iloromethane g/L 1.0 NO 0/9/96 iloroethene (Vinyl chloride) ug/L 1.0 NO 05/29/96 omomethane ug/L 1.0 NO 05/29/96 loroethane ug/L 1.0 IND 029/6 ,ichlorofluoromethane ug/L 1.0 NO 05/29/96 1- ichloroet ene ug/L 1.0 NO 05/29/96 chloromethane a /L 1.0 NO 05/29/96 ,an's-1,2-Dichloroethene ug/L 1.0 ND 05/29/96 1-Dichloroethane ug/L 1.0 NO 05/29/96 s-;1,2-Dichlorwoethene ug/L 1.0 NO 05/29/96 2-Dichloropropane ug/L 1.0 NO 05/29/96 loroform ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY RY ANALYSIS This report shall not c except in full, without the written consent :: , e .aiytical Services, Inc, Pace Analytical Services, Inc. 980-0 King ey Avenue, Suite 159 Huntersville, NC 28978 Tel: 704-875-9092 Fax: 704-875-9091 r. Paul Banks dune 04, 1996 Page 5 PACE Project Number: 660520512 Client Reference: Fleet' PACE Sample Number: 92 00104' Date Collected: 05/20/96 Date Received: ; 05/20/96 Client Sample ID: MIS--B Parameter Units MDL METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 Bromochlromethane ug/L 1.0 ND 05/29/96 1,1,1-Trichloroethane u/L 1.0 ND 05/29/96 1,1-Dichloro-1-propene ug/L. 1.0 ND 05/29/96 Carbon tetrachloride u/L 1.0 ND 0529/9 1,2-Dichloroethane u/L 1.0 ND 0529/96 1,1„2-Trichloreethene ug/L 1.0 ND 05/29/96 1,2-Dichldropropane ug/L 1.0 ND 05/29/96 Bromodichiloromethane ug/L 1.0 ND 05/29/96 Dib omomethane ug/L 1.0 NO 05/29/96 cis 1,-Dichloro-l-propene ug/L 1.0 ND 05/29/96 trans-1,3-Dichloro-l-propene ug/L 1.0 ND 05/29/96 1,1,2-Tri'chloroethane u/L 1.0 ND 05/29/9 1,-Dichloropr pane ug/L 1.0 NO 05/29/96 Tetrachloroethene g/L 1.0 ND 05/29/96 Dibromochloromethane ug/L. 1.0 ND 05/29/96 1,1,1,2-Tetrachloroethane ug/L 1'.0 ND 05/29/96 " Broofor /L 1.0 ND 0529/9 1,1,2,2--Tetrachlorothn ug/L 1.0 ND 05/29/9 1,2,3-Trichlorpropne ug/L 1.0 ND 05/29/96 Bromobenzene ug/L 1.0 ND 05/29/96 2-Cnlorotoluene ug/L 1.0 ND 0/29/96 4--Chlorotoluene ug/L 1.0 ND 05/29/96 1,3-Dichloroben e e a /L 1.0 ND 05/29/96 1,4-;Dichlorobenzene ug/L 1.0 'ND 05/29/96 1,-Dichldrobenzene ug/L 1.0 ND 05,/29/96 1,2-Dibromo-3-chloropropane ug/L 1.0 ND 05/29/96 1,2,4-Tri hlorobenzene ug/L 1.0 ND 05/29/96 Neclorebtaiene u/L 1.0 ND 05/29/96 1,2,3-Trichlorobenzene ug/L 1.0 ND 05/29/96 Benzene u/L 1.0 ND 05/29/96 Toluene ug/L 1.0 ND 05/29/96 ,.we reportThis i., be reproaxed except in full, *lths.:tn� consent& Pace Analyfical Services, Inc. Pace Analytical Services, l Inc, 9800 Klncey Avenue, Suite 100 Huntersville, NC 2 078 Tel: 7 4-875-9 92 Fax: 794-875-9991 Mr. Paul Banks June 04, 1996 Page 6 PACE Project Number: 660520512 Client Reference: Fleet PACE Sample Number. 92 0601904 Date Collected: 05/20/96 Date Received. 05/20/96 Client Sample;ID: MW-8 Parameter Units MDL METHOD DATE ANALYZED ORGANIC ANALYSTS VOLATILE ORGANICS 502.2 larobenzene ug/L 1.0 NO 05/29/96 Ethylben en ug/L 1.0 NO 05/29/96 Xylee ug/L 1.0 ND 05/29/96 Styrene ug/L 1.0 ND 05//6 Isupropylbenzene ug/L 1.0 NO 05/29/96 n-Prapylbenzene ug/L 1.0 NO 05/29/96 1,3,5-Trimethybenzene ug/L 1.0 ND 5/29/9 t-Butylbenzene ug/L 1.0 ND 0/29/96 1,,4-Trimethylbenzene ug/L 1.0 ND 05/9/96 -Butylbenzene ug/L 1.0 ND 05/29/96 4-Isaprop ltnluene u /L 1.0 ND 05/29/96 n-Bu ylbenzene ug/L 1.0 NO 05/29/96 Naphthalene ug/L 1.0 NO 05/29/96 This ys ept in full, withouta Pace Analyticai Services, Inc. 989f3 FCincey Avenue, quite 1l�ti Hunter~svi[C, 875 Tel: 04-�75-9�}9 Fax: 704-875-90 1 Mr. Paul Banks; June 04, 1996 Page 7 PACE Project Number: 660520512 Client Reference: Fleet PACE Sample Number: 92 0601912 Date Collected: 05/20/96 Date Received. <05/20/96 Client Sample ID. MW-5 Parameter units MDL METHOD DATE ANALYZED ORGANIC ANALYSIS POLYNUCLEAR AROMATIC HYDROCARBONS " 610 Naphthalene ug/L 2.5 NO 0/25/96 Acen phth lene u /L 2.5 NO 05/25/96 Acenaphthene ug/L 2.5 NO 05/25/96 Fluorene u/L 2.5 NO 05/25/96 Phenanthrene ug/L 2.5 NO 05/25/9' Anthracene ug/L 2.5 NO 05/25/96 Fluoranthene u/L 2.5 NO 0525/96 Pyrene u/L 2.5 NO 05/25/96 Benz[a]anthracene ug/L 2.5 NO 05/25/96 Chryene ug/L 2.5 NO 05/25/96 Benzo[b]f]uoranthene ug/L' 2.5' NO 05//96 Benzo[k]f uoranthene ug/L 2.5 NO 05,/25/96 Benze[a]pyrene ug/L 2.5 NO 05/25/96 Dibenz[a, ]anthracene ug/L 2.5 NO 05/25/96' Benzb[g,h,i]perylene a /L 2.5 NO 05/25/96 Indeno[1,2,-c]pyrene ug/L 2.5 ND 05/25/96 Date Extracted Date 052496 0//96 VOLATILE ORGANICS 50#2 Dichlorodifluorometh'ane ug/L 1.0 ND 05/29/96 Chloromethane ug/L 1.0 ND 05/29/96 Chloroeth ne (Vinyl chloride) ug/L 1.0 NO 05/29/96 Bromomethane ug/L 1.0 NO 05/29/9, Chloroethane ug/L 1.0' NO 05/29/96 Trichioro luoromethane ug/L 1.0 ND 05/29/96 1,1-Dichldroethene ug/L 1.0 NO 05/29/96 Dichl'oromethan ug/L 1.0 NO 05/29/96` trans-1,2-Dichloroethene u/L 1.0 NO 05/29/96` 1,1-Oichloroeth ne ug/L 1.0 NO 05/29/96 cis-1',2-Dichloroethen ug/L 1.0 ND 05/9/96 2,2-Dichloropropane ug/L 1.0 NO 05/29/96 Chloroform ug/L 1.0 NO 05/29/96 reportThis - repr uped, except Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 * Huntersville, NC 28078 Tel: 704-875-9092 Fax. 70 .875-9091 Ir. Paul Bans June 04, 1996 rage B PACE ProjectNumber: 660520512 Bent Reference: Fleet 'ACE Sample Number 92 0601912 'ate Collected* 05/20/96 ,ate Received:` 05/20/96 let Sample ID: MW-5 arameter' ,Units MDL METHOD DATE ANALYZED RGAIC ANALYSIS OLATILE ORGANICS 502. romochloromethane ug/L 1.0 NO 05/29/96 ,1,-Trichloroethane ug/L 1.0 ND 05/29/96 ,1-Dichloro-1-propene ug/L' 1.0 NO 05//6 arbor tetrachloride ug/L 1.0 ND 05/29/96 ,2-Dichloroethane u/L 1.0 ND 0/29/96 ,1,2-Trichloroethene ug/L 1.0 ND 0/29/6 ,2--Dichloropropane ug/L 1.0> ND 05/29/96 romodichloromethane ug/L 1.0 ND 05/29/96 ibromomethane' ug/L 1.0 ND 05/29/96 is-1,-Dchloro-l-propene ug/L 1.0 ND 0529/96 raps-1,3-Dichloro-l-propene g/L 1.0 ND 65/29/96 ,1,2a-Trichloroethane ug/L 1.0 ND 05/29/96 ,-Dichloropropane ug/L 1.0 ND 05/29/96 atrachloroethene ug/L 1.0 NO 05/29/96 ibromochloromethane ug/L 1.0 NO 05/29/96 ,1,1,-Tetrachloroethane ug/L 1.0 ND 05/29/96 romp orm ug/L 1.0 ND 05/29/96 11,2,2-Tetrachloroethane ug/L 1.0 ND 05/29/96 ,2,-Trihloropropane u/L 1.0 ND 05/29/96 romobenene ug/L< 1.0' NO 05/29/96, -Chlorotolu ne ug/L 1.0 NO 05/29/96; -Chlorotoluene ug/L' 1.0 ND 05/29/96 ,-Dichlorobenzene ug/L 1.0 ND 05/29/96 ,4-Dichlor^oben'zene ug/L 1.0 ND 05/29/96 ,-Dichlorobenzene u /L 1.0 ND 05/29/96 ,2-Dibromo--chloropropane ug/L 1.0 ND 05/29/96 ,2,4-Trichlorobenzene ug/L' 1.0 ND 05/29/96; �xachlorobutadiene ug/L 1.0 ND 05/29/96 ,2,3-Trlchlorobenzene ug/L 1.0 ND 05/29/96 !nzene u/L 1.0 ND 0//6 >luene ug/L 1.0 ND 05/29/96 REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. M Pace Analytical Services, #nc. 9S(}� k�rnceyy+�Ay venue, 1 CgityI �S�u+rtey' '��.ii llvr�J(�rll�t 4Y4`F ftt trJ Pax.704-875-9091 r. Paul Banks June 04, 1996 Page 9 PACE Project Number. 660520512 Client Reference. Fleet PACE Sample Number. 92 0601912 Cate Collected. 05/20/96 Date Received, 05/20/96 Client Sample ID. MW--5 Parameter Units MDL METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502..2 Chlercbenzene ug/. 1.0 ND 05/29/96 Ethylbenzene ug/L 1.0 ND 05/29/96 Xylenes ug/L 1.0 ND 05/29/96 Styrene ug/L 1.0 NO 05/29/96 Isupropylbenzene ug/L 1.0 ND 05/29/9 n-Prnpylbenzene u/L 1.0 -ND 05/29/96 1,3,5-Trimethylbenzene ug/L 1.0 ND 05/29/96 t-Butylbenzene ug/L 1.0 NO 05/29/96 1,2,4-Trimethylbenzene ug/L 1.0 ND 05/29/96 s--Butylbenzene ug/L 1.0 ND 0/2/96 { 4-Isopropyltnluene a /L 1.0 NO 05/29/96 n-Butylbenzene ug/L 1.0 ND 0/29/6 Naphthalene u/L 1.0 ND 0/29/6 This `6M F in full, without Pace Analytical Services, Inc. 9800 Kinsey Avenue, Suite 100 Jim 3119 Nuntersville, NC 2 078 Tel; 04-878-9092 Fax: 704-878- 091 1 Banks June 04, 1996 PACE Project Number: 660520512 Reference: Fleet mpe Number:- 92 0601920 llected 05/20/96 ceivd:, 05/20/96 Sample ID: M'W-1 er Units ML METHOD DATE ANALYZED ANALYSIS LEAR AROMATIC HYDROCARBONS 610 lene /L 2.5 NO 05/25/96 thylene ug/L 2.5 NO 05/25/96 there ug/L 2.5 NO 05/25/96 e u/L 2.5 ND 05/25/96 hrene ug/L 2.5 NO 05/25/96 ene ug/L 2.5 NO 05/25/96 there ug/L 2.5 NO 05/25/96 ug/L' 2.5 NO 05/25/96 anthracerie ug/L 2.5 NO 05/25/96 e ug/L 2.5 ND 05//96 )fluoranthene ug/L 2.5' NO 05/25/96 )f)uoranthene ug/L 2.5 NO 05/25/96 ]pyrene ug/L 2.5 NO 05/25/96 a,h)anthracenie ug/L 2.5 NO 05/25/96 ,h i)perylene ug/L 2.5 NO 05/25/96 1,2,3-cd pyrene ug/L 2.5 NO 05/25/96 trcted' Date 052496 05/24/96 w ORGANICS 502.2 )difluoromethane ug/L 1.0 NO 05/29/96 :thane ug/L` 1.0 NO 05/29/96 '.here (Vinyl chloride) ug/L 1.0 NO 05/29/9 '.hare ug/L 1.0 NO 05/29/96 Shane ug/L 1.0 NO 05/29/96 ,ofluoromethane u /L 1.0 NO 05/29/96 , lloroethene ug/L 1.0 NO 05/29/96 )methane ug/L 1.0 ND 05/29/6 ,2-Dichloroethene ug/L 1.0 NO 05/29/96 iloroethane ug/L 1.0 NO 05/29/96 -Dichloroethene a /L 1.0 NO 05/29/96 iloropropane ug/L 1.0 NO 05/29/96 Irm ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not b e ., u o W ced except in full, without the written consent of Pace z naiytical Services, Inc. Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 A 31 Oil, 69 Huntersville, NC 28078 Tel: 704-876-9092 Fax: 704-875-9091 Ir. Paul Banks June 04, 1996 'age 11 PACE Project Number: 660520512 :Bent Reference: Fleet 'ACE Sample Number- 92 0601920 )ate Collected: 05/20/96 )ate Received: 05/20/96 'Bent Sample ID: MW-1 larameter Units MDL METHOD DATE ANALYZED IRGANIC ANALYSIS 'OLATILE ORGANICS 502.2 tromochloromethane ug/L 1.0 NO 05/29/96 ,1,1-Trichloroethane ug/L 1.0 NO 05/29/96 ,1-Dichloro-l-propene ug/L 1.0 ND 05/29/96 arbors tetrachloride ug/L 1.0 ND 05/29/96 ,2-Dichloroethane ug/L 1.0 ND 05/29/96 ,1,2-Trichloroethene ug/L 1.0 NO 05/29/96 ,2-Dichloropropane ug/L 1.0 ND 05/29/96 romodichloromethane ug/L 1.0 NO 05/29/96 ,ibromomethane ug/L 1.0 ND 05/29/96 is-1,3-Dichloro-l-propene ug/L 1.0 ND 05/29/96 rans-1,3-Dichloro-l-propene ug/L 1.0 ND 05/29/96 ,1,2-Trichloroethane ug/L 1.0 ND 05/29/96 ,3-Dichloropropane ug/L 1.0 ND 05/29/96 etrachloroethene ug/L 1.0 ND 05/29/96 ibromochloromethane ug/L 1.0 ND 05/29/96 ,1,1,2-Tetrachloroethane ug/L 1.0 ND 05/29/96 romoform ug/L 1.0 ND 05/29/96 ,1,2,2-Tetrachloroethane ug/L 1.0 NO 05/29/96 ,2,3-Trichloropropane ug/L 1.0 ND 05/29/96 romobenzene ug/L 1.0 ND 05/29/96 -Chlorotoluene ug/L 1.0 NO 05/29/96 -Chlorotoluene ug/L 1.0 ND 05/29/96 ,3-Dichlorobenzene ug/L 1.0 ND 05/29/96 ,4-Dichlorobenzene ug/L 1.0 ND 05/29/96 ,2-Dichlorobenzene ug/L 1.0 ND 05/29/96 ,2-Dibromo-3-chloropropane ug/L 1.0 NO 05/29/96 ,2,4-Trichlorobenzene ug/L 1.0 ND 05/29/96 axachlorobutadiene ug/L 1.0 ND 05/29/96 ,2,3-Trichlorobenzene ug/L 1.0 NO 05/29/96 ?nzene ug/L 1.0 ND 05/29/96 )luene ug/L 1.0 ND 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not t)e -�c,ed except in full, without the written consent -1 - *�, e Araiyttcal Services, Inc. Pace Analytical Services, Inc. 9800 Kiney Avenue, Suite 100 Nuntersville, NC 28078 Tel; 704-875-9092 Fax: 704-875-9091 1 Barbs June 04, 1996 PACE Project Number: 660520512 leference: Fleet npe Number: 92 0601920' Elected: 05/20/96 :eived: 05/20/96 ;ample ID: MW-1 !r Units MOL METHOD DATE ANALYZED ANALYSIS ORGANICS 502.2 enzene u/L 1.0 NO 05/29/96 lzene ug/L 1.0 NO 0/9/96 ug/L 1.0 NO 05//6 °lbenzene u9/L ug/L 1.0 1.0 NO NO 05/9/96 0/29/96 benzene ug/L 1.0 NO 0529/96 nmethylbenzene ug/L 1.0, NO 05/29/96 ,enzene nmethylbenzene g/L ug/L 1.0 1.0 NO NO 05/29/96 05/9/6 enzene pyltvluene ug/L /L 1.0 1.0 NO NO 05/29/96 05/29/96 enzene u/L 1.0 NO 05/29/96 ene ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full, without the writtenconsentof Pace Analytical Services, Inc. Pace Analytical Services„ Inc. 9800 Kincey Avenue, Suite 100 Fluntersvilie, NC 28078 Tel: 704-87 - 092 Fax; 04-875- 091 �. Paul Banks June 04, 1996 ige 13 PACE Project Number: 660520512 lient Reference. Fleet kCE Sample Number. 92 0601939 ite Collected: 05/20/96 ►te Received: 05/20/96 lent Sample ID: MW- trameter Units MDL METHOD DATE ANALYZED tGANIC ANALYSIS )LYNUCLEAR AROMATIC HYDROCARBONS 610 1phthalene ug/L 2.5 ND 05/25/96 :enaphthylene ug/L 2.5 ND 05/25/96 .enaphthene ug/L 2.5 ND 05/25/96 uerene ug/L 2.5 ND 05/25/96 fenanthrene /L 2.5 ND 05/25/96 ithracene ug/L 2.5 NO 05/25/96 uoranthene ug/L 2.5 NO 05/25/96 ,rene ug/L 2.5 NO 05/25/96 nz[alanthracene ug/L 2.5 ND 05/25/96 ry ene ug/L 2.5 NO 05/25/96 nzo[b]fluoranthene u/L 2.5 ND 05/25/96 no[k]fluoranthene ug/L 2.5 ND 05/25/96 nzo[alpyrene' ug/L 2.5 ND 05/25/96 benz[a,h]anthracene ug/L 2.5 ND 05/25/96 nzo[9,h',ilperylene ug/L 2.5 ND 05/25/96 deno[1,2,3-cd]pyrene ug/L 2.5 ND 05/25/96 to Extracted Date 052496 05/24/96 LATILE ORGANICS 502.2 chlorod fluoromethane ug/L 1.0 NO 05/29/96 loromethane ug/L 1.0 ND 05/29/96 loroethene (Vinyl; chloride) a /L 1.0 NO 05/29/96 omomethane ug/L 1.0 NO 05/29/96 loroeth ne ug/L 1.0 NO 05/29/96 ichlorofluoromethane ug/L 1.0 NO 05/29/96 I-Dichloroethene ug/L 1*0 ND 05/29/96 chloromethane ug/L 1.0 ND 0/29/96 ns-1,2-Dichloroethene ug/L 1.0 ND 05/29/96 1-Dichluroethane /L 1.0 NO 05/29/96 -1,2-Dihloroethene ug/L 1.0 ND 0/29/96 -Dichloropropane ug/L 1.0 ND 05/29/9 loroform u /L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wriiien consent of Pace Analytical Services„ Inc. Pace Analytical Services, Inc. 9800 Kineey Avenue, Suite 100 Huntersville, NC 28078 Tel; 704-875-909 Fax: 704-87-9091 Paul Banks June 04, 1996 14PACE Project Number: 660520512 nt Reference. Fleet Sample Number: 92 0601939 Collected 05/20/96 Received.' 05/20/96 t Sample ID: - meter Units MDL METHOD DATE ANALYZED Klimfulaw TILE ORGANICS 502.2 chloromethane ug/L 1.0 NO 05/29/96 1-Trichloroethane ug/L 1.0 NO 05/29/96 )ichloro-1-propene u /L 1.0` NO 05/29/96 n tetrachloride ug/L 1.0 NO 05/29/96 )ichloroethane ug/L 1.0 NO 05/29/96 2-Trichloroethen ug/L 1.0 NO 05/29/96 Dichloropropane u/L 1.0 NO 05/2/6 Ddichoromethane ug/L 1.0 NO 0/29/96 Dmomethane ug/L' 1.0 NO 05/29/96 1,-Dichloro-l-propene u/L 1.0 ND 05/29/96 --1,-Dichloro---propene u/L 1.0 NO 05/29/96 2-Trichloroethane ug/L 1.0 NO 05/9/9 )ichlbropropane ug/L 1.0 NO 05/29/96 chlor°oethene ug/L 1}0 NO 05/29/96 mochloromethane ug/L 1.0 NO 05/29/96 1,2-Tetrachloroethane ug/L` 1.0; NO 05/29/96 )form ug/L 1.0 NO 05/29/96 2,-Tetrachloroethae ug/L 1.0 NO 05/29/6 3-Tri hloropropane ug/L 1.0 NO 05/29/96 )benzene ug/L 1.0 ND 05/29/96 [orotbluene u/L 1.0` NO 0/29/96 Corotluene ug/L 1.0 NO 05/29/96 )ichlorobenzene ug/L 1.0 NO 05/29/96 )ichlorobenzene ug/L 1.0 NO 05/29/96 )ichlorobenzene ug/L 1.0 NO 05/29/96 )ibromo---Chloroprop ne ug/L 1.0 NO 05/29/96 1-Trichlorobenzene ug/L 1.0 NO 05/29/96' hlorobutadiene' u/L 1.0 NO 05/29/96' -Tri hlorobenzene ug/L 1.0 NO 05/29/96 ?ne ug/L 1.0 NO 05/29/96 'ne ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be i. -ceu except in full; without the written consent , ° � 4 o _-aiyticai Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite100 Huntersville, NC 28078 Tel; 704-875-9092 Fax; 704-87 -9091 tl Banks June 04, 1996 .6' PACE Project Number. 660520512 Reference: Fleet im le Number.: 92 0601939 ►llected: 05/20/96 ,ceivd 05/2/96 Sample ID: -2 ,er Units M L METHOD DATE ANALYZED ANALYSIS ,E ORGANICS 502. lenzene ug/L 1.0 NO 05/29/96 tnzene ug/L 1.0 NO 05/29/96 ug/L 1.0 ND 05/29/96 ug/L 1.0 ND 05/29/96 fylbenzene ug/L 1.0 ND 05/29/96 ,lbenzene a/L. 1.0 ND 05/29/96 rimethylbenzene a /L 1.0 NO 05,/29/96 benzene ug/L 1.0 NO 05/29/96 ri'methylbenzene ug/L 1.0 ND 05/29/96 benzene u/L 1.0 ND 05/29/96 ,opyltuluene ug/L 1.0 NO 05/29/96 benzene ug/L 1.0 ND 0/29/96 lene ug/L 1.0 ND 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be ec ° `�,I iced except in full, without the written consent of =ace Analytical Services, Inc. RCRa Arsi Bar Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite '100 untersville, IBC 28078 Tel: 704-87 - 092 Fax: 704.875- 091 'aul Banks June 04, 1996 16 PACE Project Number: 660520512 it Reference: Fleet Sample Number. 92 0601947 Collected. 05/20/96 Received: 05/20/96 t Sample ID: DW-1 Teter Units MDL METHOD DATE ANALYZED ANIC ANALYSIS is mg/L 0.005 ND 05/23/96 m mg/L 0.010 0.2 05/28/96 um m /L 0.010 NO 05/28/96 ium mg/L, 0.010 NO 05/28/96 mg/L 0.005 ND 05/22/96 ry mg/L 0.0002 0.0007 05/23/96 ium mg/L 0.005 ND 0522/96 r mg/L 0.010 NO 05/28/96 11MUMMIMM UCLEAR AROMATIC HYDROCARBONS 610 hlee ug/L 2.5 NO 05/25/96 phthylene ug/L 2.5 NO 05/25/96 phthene u/L 2.5 ND 05/25/96 ene ug/L 2.5 ND 05/25/96 nthrene ug/L 2.5 ND 05/25/96 acen ug/L 2.5 ND 05/25/96 anthne ug/L. 2.5 ND 0/5/96 a]anthraene ug/L 2.5 NO 05/25/96 ene ug/L. 2.5 ND 05/25/96 [b]fluoranthene ug/L 2.5 NO 05/25/96 k]fluoranthene ug/L 2.5 NO 05/25/96 [a]pyrene ug/L 2.5 ND 05/25/96 z[a,h]anthracene ug/L 2.5 NO 05/25/96 [g,h,i]perylene ug/L 2.5 ND 02/96 oj1,2,3-cd]pyrene ug/'L 2.5 ND 05/25/96 Extracted Date 052496 024/96 ILE ORGANICS 502.2 orodfluoromethane ug/L 1.0 ND 05/29/96 omethne ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shell not ue -.: .��ced except in full, without the written consent : , a +,e Aralytical Services„ Inca . ul 'saoiAjaS le ijAjeu v aged jo guasuao uapm aqj Inogl!m 'ling ul gdaaXa 'paonp0jC1aj aq ICU jlegs podaa sigj 1 1 Y .L 1 J 3 96/6Z/90 ON 0°1 _ 1/6n auezuaq( 96/6Z/90 ON O` 1/6n au dujdoA0L43L 1-1 96/6Z/90 ON 0,1 1/6n 8ue44a0J0L43VJ40i- ` 96/6Z/90 ON 0*1 1/6n AOJ( 96/6Z/90 ON 0'1 1/6n 9uP41a0J0L4:M Ia1- ` 96/6Z/90 ON 0`T 1/6n aue41aw0J0 L430 ( 96/6Z/90 ON 0.T 1/6n au944a0,A0L4at 96/6Z/90 ON 0 ° T ` 1/6n auedudaiO MM 96/6Z/90 ON 0`T 1/6n auey .a0JOL11aP1_# 96/6Z/90 ON 0*1 1/6n auadojd-I-0J0L4DLO- =T_< 96/6Z/90 ON 0' T 1/6n auada,ad-T- 0JO H LO-C j 6/6Z/90 ON 0' T 1/6n aue6awom 96/6Z/90 ON 0"T 1/6n auey aw0, 0L4:)L ( 96/6Z/90 ON O ° 1 1/6n aueda.tdoaa L4:) L( 96/6Z/90 ON O°T I/6n au041a0J0L4al l_i 96/6Z/90 ON 0°T 1/6n aue44a0J0LVl( 96/6Z/90 ON 0" T 1/6n apPultl e 18 ut 96/6Z/90 ON O"T 1/6n; auadoad-T-0J0 LgaLT 96/6Z/90 ON 0 ` T 1/6n aue4480J0 LL{a LJj-1 96/6Z/90 ON 0°1 1/6n auR418w0J0L4a( 96/6Z/90 ON 0 ° T i/6n tj03.0 96/63/90 ON 0 ` 1 1/6n auedajd0.A0 Lqa L 96/6Z/90 ON 0' T 1/6n aua4100J 0 L4D W-Z ` 1 96/6Z/90 ON 0 ` 1 1/6n auetllauJLV LI 96/6Z/90 ON 0' T 1/6n< au84 a0J0LyaLO-Z=T_< 96/6Z/9O ON 0" T 1/6n auetiPwOJOI 96/6Z/90 ON O`T 1/6n 0ua4190 0L4:)t( 96/6Z/90 ON 0.1 1/6n 0uP4 au 0J0n LJ0J0 Lt 96/6Z/90 ON 0' T 1/6n au4004 96/6Z/9O ON 0'1 1/6n auP440 t 96/6Z/90 ON 0`1 1/6n (a l aL43 L utA) auatllaa Z' Z09 O Ntf'9 O 31I1 SISA1VNV 31L O3 AIVf -V 31VO OOHAW 10W SIM ual au T-MO :OI a LdweS 1t 96/OZ/90 :paLa30 96/O /SO aPa L Lu0 Lt61090 Z6 :jagwnN aldweS U :a uaua a� It ZTSoZS099 :jagwnN 1. aPOJd 30Vd LT 966T ` o aunt ueB Lnec M6-9L9-t0L:XeJ 606- L1 tOL :lal ME JN `9Ii1nsiaiun 00� apnS lai uanyAa ul}i 0086 'Out'sealluaS P11,41euV Wed Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 l untersville, NC 28078 Tel. 704-87-99 Fax: 04-875.9091 1 'Banks June 04, 1996 $ PACE ProjectNumber: 660520512 Reference: Fleet' mple Number: 92 0601947 l lected`: -05/20/96 ceived. 05/20/96 Sample ID: DW-I er Units MDL METHOD DATE ANALYZED ANALYSTS E ORGANICS 502.`2 otoluene ug/L 1.0 NO 05/29/96 otoluen a /L 1.0 NO 05/29/96 hlorobenzene ug/L 1.0 NO 05/29/96 hlorobenzene: ug/L 1.0 NO ` 05/29/96 hlorobenzene u/L 1.0 NO 05//9 romp--hloropropane ug/L 1.0 NO 0529/96 ri hlorobenzene a /L 1.0 NO 05/29/96 orobutadiene" u/L 1.0 NO 05/29/96 richlorobenzene ug/L 1.0 NO 05/29/96 u /L 1.0 NO 05/29/96 u /L 1.0 NO 05/29/96 en ene ug/L 1.0 NO 05/29/96 nzene a /L 1.0 NO 05/29/96 u/L 1.0 NO 05/29/96 ug/L 1.0 NO 05/29/96 ylbenzene ug/L 1.0 NO 05/29/96 lbenzene ug/L 1.0 NO 05/29/96 rimethylbenzene a /L 1.0 NO 05/29/96 benzene ug/L 1.0 NO 05/29/96 ri ethylbenz ne u /L 1.0 NO 05/29/96 benzene' ug/L 1.0 NO 05/29/96 opyltoluene ug/L 1.0 NO 05/29/96 benzene ug/L 1.0 NO 05/29/96 lene ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY RY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc, 95110 hCiricey Avenue, Smite 1C1t} Huntersv�l�e, 8i 1`el: 7Q4-875.Q9 Fax: 7 4-S75-9091 aul Banks June 04, 1996 19 PACE Project Number: 660520512 t Reference: Fleet Sample Number: 92 0601955 ellected`: 05/20/96 leceived: 05/20/96 t Sample -ID. MW- �ter Units MDL METHOD DATE ANALYZED WC ANALYSIS a_ - is m /L 0.005 ND 05/23/96 mg/L 0.010 0.19 05/28/96 .1m mg/L 0.010 NO 05/28/96 ium mg/L 0.010 NO 0/28/96 mg/L 0.005 NO 05/22/96 �y mg/L 0.0002 0.0004 05/23/96 ium mg/L 0.005 NO 05/22/96 m/L 0.10 NO 05/28/96 ICLEAR AROMATIC HYDROCARBONS 610 ialene u/L 2.5 NO 05/25/96 )hthylene ug/L 2.5 NO 05/25/96 )hthene ug/L 2.5 NO 05/25/96 one ug/L 2.5 NO 02/96 ithrene ug/L 2.5 NO 05/25/96 scene ug/L 2.5 NO 0525/96 anthene ug/L 2.5 NO 05/25/96 ug/. 2.5 NO 05/25/96 i]anhracene ug/L 2.5 NO 05/25/96 ?ne ug/[ 2.5 NO 05/25/96 [b]fluoranthene ug/L 2.5 NO 0//96 [k]fluoranthene ug/L 2.`5 NO 05/25/96 [a]pyrene ug/L 2.5 N0 0/25/96 t[a,h]anthracene ug/L 2.5 NO 05/25/9 [9,h,i]perylene ug/L 2.5 NO 05/25/96 )[1,2,3-cd]pyrene ug/L 2.5 ND 0/2/96 .xtracted Date 05246 05/24/96 [LE ORGANICS 502.2 )rodfluoromethane ug/L 1.0 ND 05/29/96 )methane' ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not ne wed except in full„ without the written consent ':,, Anaiyticai Services, Inc, Pace Analytical Services, Inc. 9800 Kincey avenue, Suite 199 Huntersville, NC 28078 Tel: 704-875-9092 Fax:794-875-9091 liul Banks dune 04, 1996 20 PACE Project Number: 660520512 w Reference: Fret ;ample Number: 92 0601955 1ollected: 05/20/96 heceived. 05/20/96 Sample ID: MW-7 =ter Units MDL METHOD DATE ANALYZED X ANALYSIS ILE ORGANICS 502.2 )ethene (Vinyl chloride) ug/L 1.0 NO 05/29/96 aethane ug/L 1.0 NO 05/29/96 )ethane ug 1.0 ND 05/29/96 forfluoomethane ug/L 1.0 ND 05/29/96 1chloroethene ug/L 1.0 ND 05/29/96 wog ethane g/L 1.0 ND 05/29/96 -1,2-Dichloroethene ug/L 1.0 NO 05/29/96 1chl'oroet ane ug/L 1#0 ND 05/29/96 ,-Dichloroethene ug/L 1.0 ND 05/29/96 ichloropropane ug/L 1.0 NO 0/29/6 )form ug/L 1.0 NO 02/96 :hloromethane ug/L 1.0 NO 05/29/96 -Trichloroethane u/L 1.0 ND 05/29/96 lchloro-l-propene ug/L 1.0 NO 052/6 i tetrachloride ug/L 1.0 ND 05/29/96 lchloroethane u /L 1.0 NO 05/29/96 -Trichloroethene /L 1.0 NO 05/29/96 lchloropropane g/L 1.0 NO 0/2/96 iichloromethane g/L 1.0 NO 05/29/96 aomethane u/L 1.0 NO 05/29/96 ,3-Dichloro-l-propene ug/L 1.0 NO 05/29/96 -1,3-Dichloro-l-propene ug/L 1.0 NO 05/29/96 -Trichloroethane ug/L 1.0 ND 05/29/96 lchloropropane ug/L 1.0 ND 05/29/96 whloroethene ug/L 1.0 ND 05/29/96 aochloromethane ug/L 1.0 NO 05/29/96 ,2-Tetrachloroethane ug/L 1.0 NO 05/29/96 ,orm ug/L 1.0 NO 05/29/96 ,2--1`etrachloroethane ug/L 1.0 NO 05/29/96 •Trichloropropane u /L 1.0 ND 05/29/96 )enene u/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be terc, ,« ced except in full, without the written consent of P,a :e Analytical Services, Inc Pace Analytical Services„ Inc. 9800 Kincey Avenue, suite 100 " Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 Paul Banks June 04, 1996 21 PACE Project Number. 660520512 ,it Reference: Fleet Sample Number: 92 0601955 Collected. 05/20/96 Received: 05/20/96 it Sample ' ID: MW-7 deter Units MDL METHOD DATE ANALYZED= 4IC ANALYSIS TILE ORGANICS 50.2 lorotolue e u /L 1.0 ND 05/29/96 iorooluene ug/L 1.0 NO 05,/29/96 )ichlorobenzene /L 1.0 ND 0/9/9 )ichlorobenzene ug/L 1.0 NO 05/29/96 )ichlorobenzene ug/L 1.0 NO 05/29/96 )ibremo- -chlo opro ane ug/L 1.0 ND 05/29/96 I-Trichloroben ene : ug/L 1.0 NO 05/29/96 :hlorobutadiene ug/L 1.0 ND 0/29/9 3-Trichlorobenzene ug/L 1.0 ND 05/29/96 ane ug/L 1.0 ND 05/29/96 ane ug/L 1.0 ND 05/29/96 rwobenzene ug/L 1.0 NO 05/29/96 iben ene g/L 1.0 NO 05/29/96 ies ug/L 1.0 NO 05/29/96 ane ug/L 1.0 NO 05/29/96 ropyl;benzene g/L 1.0 ND 05/29/96 )pyl enze e u /L 1.0 NO 05/29/96 5-Trimethylbenzene a /L 1.0 NO 05/29/96 tylbenzene ug/L 1.0 ND 05/29/96 I-Trimethylbenzene u/L 1.0 NO 05/29/96 tylbenzene ug/L 1.0 NO 05/29/9 )pro ltoluene a /L 1.0 NO 05/29/96 tylbenzene ug/L 1#0 ND 05/29/96 thalene ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY ANALYSIS This report small notce , -,iced except in full, without the written consent , �' Ace Araiytical Services, Inc, Pace Analytical Services, Inc. 9800 Klncey Avenue, Suite 100 l luntersville, NC 28078 Tel, 04-87-909 Fax704-875-9091 aul Banks June 04, 1996 22 - RACE Project Number. 660520512 t Reference: Fleet Sample Number. 92 0601963 Collected': 05/20/96 Received: 05/20/96 t Sample ID: MW-10 eter [hits MDL METHOD DATE ANALYZED IC ANALYSIS UCLEAR AROMATIC HYDROCARBONS 610 halene ug/L 2.5 63 05/25/96 phth,ylene ug/L 2.5 NO 05/25/96 phth ne ug/L 2.5 NO 05/25/96 ene ug/L 2.5 3.8 05/25/96 nthr ne ug/L 2.5 NO 05/25/96 acen u/L 2.5 ND 05/25/96 anthene ug/L 2.5 NO 05/25/96 e ug/L 2.5 NO 05/25/96 a]anhracene ug/L 2.5 ND 05/25/96 ene ug/L 2.5 ND 052/96 [b]fluoranthene ug/L 2.5 ND 05/25/96 [k]fluoranthene /L 2.5 ND 05//96 [a]pYrene g/L 2.5 ND 05/25/96 z[a,h]anthracene u/L 2.5 ND 052596 [g,h,i]per,ylen g/L 2.5 NO 05/25/96 o[1,2,3--cd]pyrene /L 2.5 NO 05/25/96 Extracted Date 052496 05/24/96 ILE ORGANICS 50. orod fluoromethane ug/L 1.0 NO 05/29/96 omethane ug/L 1.0 NO 05/29/96 oeth ne {Vinyl chloride} ug/L 1.0 NO 05/29/96 methane ug/L 1.0 NO 0/29/96 oethne ug/L 1.0 ND 529/96 loco luoremeth ne ug/L 1.0 NO 05/29/96 ichloroethene u/L 1.0 ND 0/2/96 oromethane ug/L 1.0 NO 0//96 -1,-Dichloroethene ug/L 1.0 NO 0/29/96 ichleroethane ug/L 1.0 ND 05/29/96 ,2-Dchloroethene - ug/L 1.0 ND 09/96 ichloroprepane` ug/L 1.0 ND 059/96 ofor ug/L 1.0 ND 0//9 REPORT OF LABORATORY ANALYSIS This report shall not be reotoduced, except in full, without the written consent of Pace analytical Services, Inc. Pace Analytical Services, Inc.` 9800 Kir cey Avenue, Suite 100 Huntersv lle, NC 28078 Tel: 704-875-909 Fax: 04-875-9091 . Paul Banks June 04, 1996 tge 23 PACE Project Number: 66052051 ient Reference: Fleet tCE Sample Number. 92 060196 ite Collected. 05/20/96 ite Received: 05/20/96 lent Sample ID: MW-10 xameter Units MIL METHOD DATE ANALYZED ,GANIC ANALYSIS ILATILE ORGANICS 502.2 "oochldromethane ug/L. 1.0 NO 05/29/96 1,1-Tri°chloroethane ug/L 1.0 NO 05/29/96 I-Oichloro-l-propene u /L. 1.0 NO 05/29/96 xbon tetrachloride u /L 1.0 NO 05/29/9 2-Oichloroethane ug/L 1.0 NO 05/29/96 1,2-Trichloroethene ug/L 1.0 NO 05/29/96 2-0ichloropropane u/L 1.0 NO 05/29/9 "omodichloromethane /L 1.0 ND 05/29/96 bromomethane ug/L 1.0 NO 05/29/96 s1,-Dichln'ro-l-propene u/L 1.0 NO 05/29/96 °ans-1,-Oichloro-l-propene ug/!. 1.0 NO 05/29/96 1,2-Trichlo oeth ne /L 1.0 NO 05/29/96 -Oichloropropane ug/L 1.0 NO 0529/96 ltrachloroethene ug/L 1.0 NO 05/29/96 bromochloromethane u/L 1.0 NO 05/29/96 1,1,-Tetrachloroethane ug/L 1.0 ND 05/29/96 "omoform ug/L. 1.0 NO 05/29/96 1,2,-Tetrachloroethane ug/L 1.0 NO 05/29/96 2,3-Trichloro ropane ug/L 1"0 NO 05/29/96 °omobenene ug/L 1.0 NO 05/29/96 `Chlorotoluene u/L 1.0 NO 05/29/96 'Chlorotolue e u /L 1.0 NO 05/29/96 -Oichlorobenzene ug/L 1.0 NO 05/29/96 4.0ichlorobenzene ug/L 1.0 NO 0/2/96 2- Dichloroben ene ug/L 1.0 NO 05/29/96 2--Dibromo-3-chloropropane, a /L 1.0 NO 05/29/96 2,4-Trichlorobelnzene ug/L 1.0 NO 5/29/96 I achlorobutadiene ug/L 1.0 NO 05/29/96 2,3-Trichlorobenz ne ug L 1.0 NO 05/29/96 m ene a /L 1.0 28 05/29/96 iluene u/L 1.0 1.9 05/29/6 REPORT RT OF TRY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace' Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 i:i A 'r+lcal V- Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 Paul Banks June 04, 1996 e 24 PACE Project Number: 660520512 ant Reference: Fleet E Sample Number: 92 0601963 a Collected: 05/20/96 a Received: 05/20/96 ant Sample ID: MW-10 ameter Units MDL METHOD DATE ANALYZED WC ANALYSIS MLE ORGANICS 502.2 Drobenzene ug/L 1.0 NO 05/29/96 ylbenzene ug/L 1.0 16 05/29/96 tines ug/L 10 130 05/29/96 rene ug/L 1.0 NO 05/29/96 propylbenzene ug/L 1.0 10 05/29/96 ropylbenzene ug/L 1.0 11 05/29/96 ,5-Trimethylbenzene ug/L 1.0 19 05/29/96 utylbenzene ug/L 1.0 NO 05/29/96 ,4-Trimethylbenzene ug/L 10 83 05/29/96 utylbenzene ug/L 1.0 4.6 05/29/96 sopropyltoluene ug/L 1.0 3.2 05/29/96 utylbenzene ug/L 1.0 20 05/29/96 hthalene ug/L 10 100 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not : i.,ced except in full, without the written consent -- e, -',,.aiyfical Services, Inc. Pace analytical Services, Inc, 9800 Kir cey Avenue, Suite 100 Huntersvilie, NC 2 078 Tel: 704-875-092 Fax. 704-875-091 . Paul 'Banks dune 04, 1996 age 25 FACE Project Number: 660520512 Bent Reference: Fleet ACE Sample Number.' 92 0601971' ate Collected`: 05/20/96 ate Received: 05/20/96 lint Sample ID: MW-4 arameter Units MDL METHOD DATE ANALYZED RGANIC ANALYSIS OLYNUCLR AROMATIC HYDROCARBONS 610 aphthal ene u / . 25 110 05/25/96 cenaphthylene ug/L 2.5 ND 05/25/96 cenaphthene u/L 2.5 ND 05/25/96 lurene u/L 2.5 6.5 05/25/96 henanthrene ug/L 2.5 10 05/25/96 nthracene u/L 2.5 ND 05/25/96 luoranth'ene ug/E 2.5 5.0 05/25/96 yrene ug/L 2.5 2.9 05/25/96 enz[a]anthraeene ug/L 2.5 NO 05/25/96 hrysene ug/L 2.5 ND 05/25/96 enzo[b]fluoranthene ug/L 2.5 NO 05/25/96 en o[k]fluoranthene ug/L 2.5 NO 05/25/96 enzo[a]pyrene u /L 2.5 NO 05/25/96 ibenz[a,h]anthrace e u /L 2.5 NO 05/25/96 en o[ ,',i]per len ug/L 2.5 ND 05/25/96 ndeno[1,`2,3-cd]pyrene ug/L 2.5 ND 05/25/96 ate Extracted Date 05246 052/96 OLTILE ORGANICS 502.2 ichlorodifluoromethane ug/L 1.0 ND 029/96 hleromethane ug/L 1.0 NO 05/29/96 hloroeth+ene (Vinyl chloride) ug/L 1.0 NO 05/29/96 ro ometh' ne ug/L 1.0 _ NO 05/29/96 hloroeth'ane u /L 1.0 NO 05/29/96 riehlorofluoromethalne u /L 1.0 NO 05/29/96 ,I-Dichloroethen ug/L 1.0 ND 05/96 ichloromethane ug L 1.0 ND 05/29/96 rans-1,2--Dichloroehene ug/L 10 ND 05/29/96 ,I-Dichlroethane u/L. 1.0 ND 0529/6 is-1, - ichloroeth n ug/L 1.0 ND 05/29/96 ,2-Dichloroprdpane ug/L 1.0 NO 0/9 hloroform ug/L 1.0 ND 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be � e used. except in full; without the written consent of r'a, e analytical Services, Inc, Pace Analytical Services, Inc. Jill 9800 Kincey Avenue, Suite 100 l�MIt'll Huntersville, NC 28078 54 Tell: 704-875-9092 Fax: 704-875-9091 Mr. Paul Banks June 04, 1996 Page 26 PACE Project Number: 660520512 Client Reference: Fleet PACEi Sample Number: 92 0601971 Date Collected: 05/20/96 Date Received: 05/20/96 Client Sample ID: MW-4 Parameter± Units MDL METHOD DATE ANALYZED DRGANIC ANALYSIS VOLATILE ORGANICS 502.2 Bromochloromethane ug/L 1.0 NO 05/29/96 1,1,1-Trichloroethane ug/L 1.0 NO 05/29/96 1,1-Dichloro-l-propene ug/L 1.0 NO 05/29/96 Carbon tetrachloride ug/L 1.0 NO 05/29/96 1,2-Dichloroethane ug/L 1.0 NO 05/29/96 1,1,2-Trichloroethene ug/L 1.0 NO 05/29/96 1,2-Dichloropropane ug/L 1.0 NO 05/29/96 Bromodichloromethane ug/L 1.0 NO 05/29/96 )ibromomethane ug/L 1.0 NO 05/29/96 :is-1,3-Dichloro-l-propene ug/L 1.0 ND 05/29/96 trans-1,3-Dichloro-l-propene ug/L 1.0 NO 05/29/96 1,1,2-Trichloroethane ug/L 1.0 NO 05/29/96 1,3-Dichloropropane ug/L 1.0 NO 05/29/96 Tetrachloroethene ug/L 1.0 NO 05/29/96 )ibromochloromethane ug/L 1.0 NO 05/29/96 1,1,1,2-Tetrachloroethane ug/L 1.0 NO 05/29/96 3romoform ug/L 1.0 NO 05/29/96 1,1,2,2-Tetrachloroethane ug/L 1.0 NO 05/29/96 1,2,3-Trichloropropane ug/L 1.0 NO 05/29/96 3romobenzene ug/L 1.0 NO 05/29/96 2-Chlorotoluene ug/L 1.0 NO 05/29/96 4-Chlorotoluene ug/L 1.0 NO 05/29/96 1,3-Dichlorobenzene ug/L 1.0 NO 05/29/96 1,4-Dichlorobenzene ug/L 1.0 NO 05/29/96 1,2-Dichlorobenzene ug/L 1.0 NO 05/29/96 1,2-Dibromo-3-chloropropane ug/L 1.0 NO 05/29/96 1,2,4-Trichlorobenzene ug/L 1.0 NO 05/29/96 iexach,lorobutadiene ug/L 1.0 NO 05/29/96 1,2,3-Trichlorobenzene ug/L 1.0 NO 05/29/96 3enzene ug/L 5.0 74 05/29/96 Toluene ug/L 1.01 NO 05/29/96 This r without the Para Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-87-092 Fax: 04-875-9091 aul Banks June 04, 1996 27 PACE Project Number: 66052051 t Reference: Fleet aamle Number. 92 0601971 :ollecte'. 05/20/96 lecived: 05/20/96 t Sample ID: MW-4 Ater Units MDL' METHOD DATE ANALYZED [C ANALYSIS [LE ORGANICS 502.2 )benzene ug/L. 1.0 NO 05/29/9 )en ene ug/L 1.0 6.6 05/29/96 �s ug/L 1.0 1.9 05/29/96 rle ug/L 1.0 NO 05/29/96 apylbenzene ug/L 1.0 17 05/29/96 )ylbenzene ug/L 1.0 12 05/29/96 -Trimeth lben ene ug/L 1.0 10 05/29/96 lrlbenzene ug/L 1.0 ND 05/29/96 -rimeth,lbenene ug/L 1.0 35 05/29/96 yIbenzen ug/L 1.0 7.0 05/29/96 aropyltnluene ug/L 1,0 4.6 05/29/96 lbnzene ug/L 1.0 17 0/29/96 ial ne ug/L. 5.0 80 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite ;100 Huntersvllle, NC 28078 Tel: 794-87 -909 Fax: 04-875-991 Mr. Paul Banks June 04, 1996 Page 28 PACE Project Number: 660520512 Client Reference: Fleet PACE Sample Number: 92 0601980 Date Collected`: 05/20/96 Date Received: 05/20,/96 Client Sample ID: -6 Parameter Units MDL METHOD DATE ANALYZED ORGANIC ANALYSIS POLYNUCLFAR AROMATIC HYDROCARBONS 610 Naphthalene ug/L 25; 180 05/25/96 Acenaphthylene ug/L 2.5 9.5 05/25/96 Acenaphthene ug NO 05/25/96 Fluorene g/L 2.5 12 05/25/96 Phenanthrene ug/L 2.5 NO 05/25/96 Anthracene ug/L 2.5 5.9 05/25/96 Fluoranthene ug/L 2.5 13 05/25/96 Pyrene ug/L 2.5 8.6 05/25/96 Ben[a)anthracene ug/L 2.5 NO 05/25/96 Chrysene ug/L 2.5 ND 05/25/96 Beno[bfluoranthene ug/L 2.5 NO 05/25/96 Benzo[kfluorenthene ug/L 2.5 ND 05/25/96 Beno[apyrene ug/L 2.5 ND 05/25/96 Dibn[a,h]anthracene ug/L 2.5 NO 05/2/96 Beno[g,h,i]perylene ug/L 2.5 NO 0/25/6 Ineno[1,,-c]pene u/: 2.5 ND 055/96 Date Extracted Date 05246 05/24/96 VOLATILE ORGANICS 502.2 Dichlorodifluoromethane ug/L 1.0 NO 05/29/96 Chleromethane ug/L 1.0 ND 05/29/96 Chloroethene (Vinyl chloride) ug/L 1.0 NO 05/29/96 Brotomethane u/L 1.0 NO 0/29/9 Chloroethane ug/L 1.0 NO 05/29/96 Triehlorofluoromethane ug/L 1.0 NO 05/29/96 1,1-Dichleroethene ug/L 1..0 'ND 09/96 Dichloromethane u/L 1.0 NO 05/29/9 trans-1,2'-Dichloroethene u/L 1.0 NO 05/29/96 1,1-Dichleroethane ug/L 1.0 NO 05/29/96 cis-1,-Dichlo oethene ug/L 1.0 NO 05/29/96 2,2-Dichloroprepane ug/L 1.0 NO 05/29/96 Chloroform ug/L 1.0 NO 05/29/96 withoutThis report shall not be reproduced, except in full, +1, of w Pace Analytical Services, Inc, ffi 9800 Kincey Avenue, Suite 100 il I Huntersville, NC 28078 caL ;tersville, Nc 28o78 Tel: 704-875-9092 Fax: 704-875-9091 Mr. Paul Banks June 04, 1996 Page 29 PACE Project Number: 660520512 Client Reference: Fleet PACE Sample Number: 92 0601980 Date Collected: 05/20/96 Date Received: 05/20/96 Client Sample ID: MW-6 Parameter Units MDL METHOD DATE ANALYZED VOLATILE ORGANICS 502.2 Bromochloromethane ug/L 1.0 NO 05/29/96 1,1,1-Trichloroethane ug/L 1.0 NO 05/29/96 1,1-Dichloro-l-propene ug/L 1.0 NO 05/29/96 Carbon tetrachloride ug/L 1.0 NO 05/29/96 1,2-Dichloroethane ug/L 1.0 NO 05/29/96 1,1,2-Trichloroethene ug/L 1.0 NO 05/29/96 1,2-Dichloropropane ug/L 1.0 ND 05/29/96 Bromodichloromethane ug/L 1.0 NO 05/29/96 Dibromomethane 1.0 NO 05/29/96 cis-1,3-Dichloro-l-propene ug/L 1.0 ND 05/29/96 trans-1,3-Dichloro-l-propene ug/L 1.0 NO 05/29/96 1,1,2-Trichloroethane ug/L 1.0 NO 05/29/96 1,3-Dichloropropane ug/L 1.0 ND 05/29/96 Tetrachloroethene ug/L 1.0 NO 05/29/96 Dibromochloromethane ug/L 1.0 ND 05/29/96 1,1,1,2-Tetrachloroethane ug/L 1.0 ND 05/29/96 Bromoform ug/L 1.0 NO 05/29/96 1,1,2,2-Tetrachloroethane ug/L 1.0 NO 05/29/96 1,2,3-Trichloropropane ug/L 1.0 NO 05/29/96 Bromobenzene ug/L 1.0 NO 05/29/96 2-Chlorotoluene ug/L 1.0 NO 05/29/96 4-Chlorotoluene ug/L 1.0 NO 05/29/96 1,3-Dichlorobenzene ug/L 1.0 NO 05/29/96 1,4-Dichlorobenzene ug/L 1.0 NO 05/29/96 1,2-Dichlorobenzene ug/L 1.0 ND 05/29/96 1,2-Dibromo-3-chloropropane ug/L 1.0 NO 05/29/96 1,2,4-Trichlorobenzene ug/L 1.0 NO 05/29/96 Hexachlorobutadiene ug/L 1.0 NO 05/29/96 1,2,3-Trichlorobenzene ug/L 1.0 NO 05/29/96 Benzene ug/L 1.0 NO 05/29/96 Toluene ug/L 1.0 NO 05/29/96 This report shall not in full, without the written consent I Services, Inc, Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 10 untersville, NC 28078 Tel. 704-875-9092 Fax: 704-875-9091 . Paul Banks June 04 1996 ge 30 PACE Project Number: 66O520512 aunt Reference: Fleet CESample Number: ` 92 0601980 to Collected. 05/20/96 to Received: 05/20/96 lent SampleID: MW-6 rameter Units MDL METHOD DATE ANALYZED; g ►_�.7�+� LATILE ORGANICS 502.2 lorobenzene u /L 1.0 NO 05/29/96 hylbenzene ug/L 1.0 ND 05/29/96 lees u/L 1.0 1.5 05/29/96 yrene ug/L 1.0 ND 05/29/96 opropyl enze e ug/L 1.0 NO 05/29/96 Propylbenzene ug/L 1.0 ND 05/29/96 ,-Trimethylbenzene ug/L 1.0 NO 05/29/96 u ylbenzene _ ug/L 1.0 ND 05/29/96 , Tri ethy benzene ug/L 1.0 2.2 05/29/96 Butylbenzene ug/L 1.0 ND 05/29/96 I oprop ltoluene ug/L 1.0 ND 05/29/96 Bu ylbenzene ug/L 1.0 NO 05/29/96 ph hale a ug/L 1.0 2.9 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be rec--,,,Juced.except in full, without the written consent of Page Anaiyt,c l Services, Inc. 1 U1 i of 11. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-909 Fax; 04-875-9091 Raul Banks dune 04, 1996 1 RACE Project Number: 66052051 t Reference: Fleet Sample Number: 92 0601998 Collected: 05/20/96 Received: 05/20/96 nt Sample ID: F deter~ Units MDL METHOD DATE ANALYZED CANIC ANALYSIS METALS nic mg/L 0.005 NO 05/23/96 um mg/L 0.010 NO 05/28/96 ium mg/L 0.010 NO 05/28/96 mium mg/L 0.010 NO 05/28/96 mg/L 0.005 ND 05/22/96 ury m/L 0.0002 0.0002 05/23/96 nium m /L 0.005 NO 05/22/96 er mg/L 0.010 ND 05/8/96 414EMM&W NUCLEAR AROMATIC HYDROCARBONS 610 thalene u/L 2.5 NO 05/30/96 aphthylene ug/L 2.5 NO 05/30/96 aphthene ug/L 2.5 NO 05/30/96 rene' g/L 2.5 ND 05/30/96 anthrene ug/L 2.5 NO 05/30/96 racene ug/L 2.5 ND 05/30/96 ranthene ug/L 2.5 ND 05/30/96 ne ug/L 2.5 NO 05/30/96 [aanthracene ug/L 2.5 ND 0/30/96 serve u/L 2.5 NO 05/30/96 o[b)fluoranthene ug/L 2.5 ND 05/30/96 o[k]fluoranthene ug/L 2.5 NO 05/30/96 o[a]pyrene ug/L 2.5 ND 05//96 nz[a,;h]anthracene ug/L 2.5 ND 05/30/96 o(g,h,ilperylene ug/L 2.5 NO 05/30/96 no[1,2,3-cdpyrene u/L 2.5 ND 0/30/96 Extracted Date 0246 05/24/96 TILE ORGANICS 502.2 lorodifluorome hane ug/L 1.0 ND 05/29/96 romethane ug/L 1.0 NO 05/29/96 REPORT OF LABORATORY RY ANALYSIS This report Shall not ce ' (-L. �,.4ced except in full, without the written consent "i .' j,.e -analytical Services, Inc. Face Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 An Huntersville, NC 28078 TeL 704-875-9092 704-875-9091 4r. Paul Banks June 04, 1996 )age 32 PACE Project `' Number: 660520512 ;Herat Reference: Fleet :ACE Sample Number: 92 0601998 )ate Collected': 05/20/96 )ate Received:'` 05/20/96 'Bent Sample ID: FB >ara eter Units MILL METHOD DATE ANALYZED )RGANIC ANALYSIS IOLATILE ORGANICS 502.2 `>hloroeth ne (Vinyl chloride)' a /L 1.0 N 05/29/96 3romomethane ug/L 1.0 NO 05/29/96 fhloroethne u/L 1.0 NO 05/29/96 Frichlorofluoromethane u /L 1.0 NO 05/29/96 1,1-pichloroethene u /L: 1.0 ND 05/29/96 )ichloromethane ug/L 1.0 NO 05/29/96 trans-1,2-Dich oroethene u /L 1.0 Nil 05/29/96 1,1-Dichloroethane ug/L 1.0 NO 05/29/96 :is-1,2-Dlchloroethne ug/i 1.0 ND 05/29/96 ?, 2-- ichl oro ropane ug/L 1.0 NO 05/29/96 hlo ofora u /L 1.0 2.205/29/96 3romochloometane u/L 1.0 ND 05/29/96 1,1,1-Tri hloroethane ug/L 1.0 ND 05/29/96 [,I-Dichloro--l-propene /L 1.0 NO 05/29/96 urban tetrachloride ug/L 1.0 ND 05/29/96 1,2-- ichloroethane ug/L 1.0 ND 05/29/96 1,1,2-Trichlor€aethene ug/L 1.0 NO 05/2/9 1,2- ichloropr pane ug/L 1.0 NO 05/29/96 3romodich prom thane ug/L 1.0 ND 05/29/9 )ibroibomethane` ug/L 1.0 NO 05'29/96 :is-,3-Dlchloro-l-propene u/L 1.0 ND 05/29/96 'ran-1,3-Dichloro-l-propene - ug/L 1.0 NO 05/29/96 1,1,-Trichloroethane ug/L 1.0 NO 05/29/96 1,-tlichloropropane u /L 1.0 NO 05/29/96 ietrachloroethene ug/L 1.0 NO 05/29/96 )ibromochloromethane u/L 1.0 NO 05/29/96 1,1,,2-Tetrachloroethane ug/L 1.0 NO 02/96 3ro o orm ug/L 1.0 ND 05/29/96 1,1,,2-Tetrachloroethane u/L 1.0 ND 05/29/96 1,2,-Trichloropropane u/L 1.0 ND 05/29/9 3romebenzene u/L 1.0 ND 05/29/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent' of Pace Analytical Services, Inc. Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28978 Tel: 704-87 -9092 Fax. 704-87 -9091 Mr. Paul Banks ,tune 04, 1996 Page 33 PACE Project Number: 660520512 Client Reference: Fleet PACE Sample Number: 92 0601998 Date Collected: 05/20/96 DateReceived: 05/20/96 Client Sample ID: EB Parameter Units MDL METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502. 2-Chlorotoluene ug/L 1.0 ND 05/29/96 4-Chlorotoluen ug/L 1.0 NO 05/29/96 1,-Dichloroben en a /L 1.0 ND 05/29/96 1,4-Drchloroenene /L 1.0 ND 29/96 1,2-Di hlorobe zene ug/L 1.0 ND 05/29/9 1,2-Drbroo--chloropropane u/L 1.0 ND 0/9/96 1,2,4-Trichlorobenzene u/L 1.0 ND 0/29/9 Hexachlorobutadiene u/L 1.0 ND 05/2/9 1,2,3-Trichlorobenzene g/L 1.0 ND 05/9/96 Benzene ug/L 1.0 ND 05/29/96 Toluene u/L 1.0 ND 0/29/6 Chlorobenzene u/L 1.0 ND 05/29/96 Etlbenene ug/L 1.0 ND 05/29/96 Xylenes a /L 1.0 ND 05/29/96 Styrene ug/L 1.0 ND 05/2/9 Isopropylbenzene ug/L 1.0 ND 05/29/96 n-Propylbenzene u/L 1.0 ND 05/29/96 1,3,5-Trimethlbenzene ug/L 1.0 ND 05/29/96 t-Butylbenzene ug/L 1.0 ND 05/29/96 1,2-Trrmethylbenzene ug/L 1.0 ND 052/6 s-Butylbenzene ug/L 1.0 ND 05/29/96 -Iopropyltoluene ug/L 1.0 ND 05/29/96 n-Butlbenzene ug/L 1.0 ND ` 05/29/9 Naphthalene ug/L 1.0 ND 05/29/96 : REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace AnalyticalServices, Inc. Pace Analytical 9800 Kincey Aven It' -A Analvtinal Huntersvill€ Tel: 704-875- ax: 04-87 -9 Mr. Paul Banks June 04 1996 Page 34 '' PACE Project Number: 6 Client Reference: Fleet RCRA Metals in Liquids Analytical Methods: Barium, Cadmium, Chromium, Lead, Silver - EPA 200. Arsenic, Selenium -- EPA 200.9 Mercury - EPA 245.1 Digestion Methods: Mercury - EPA 245.1 All Others - 20.2 These data have been reviewed and are approved for release. Margaret S. Harding Manager, Laboratory Operations REPORT OF LABORATORY ANALYSIS This report shall not b PL -.rt,, ced except in full, without the written consent -* * . e Anafyttcal Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 fiDaL Hu6mville,NC 28.078 Tel: 704-875-9092 Fax: 704-875-9091 Mr. Paul Banks FOOTNOTES June 04, 1996 Page 35 for pages I through 34 PACE Project Number: 660520512 Client Reference: Fleet MDL Method Detection Limit ND Not detected at or above the MDL. REPORT OF LABORATORY ANALYSIS This report shall not be ec,,w,l iced except in full, without the written consent of P a,-e Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 E:1 1!21 1111,11iW.W.I.i..ii Ical Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 Mr. Paul Banks QUALITY CONTROL DATA June 04, 1996 Page 36 PACE Project Number: 660520512 Client Reference: Fleet Arsenic Batch: 92 46718 Samples: 92 0601947, 92 0601955, 92 0601998 METHOD BLANK: Method Parameter Units MDL Blank Arsenic mg/L 0.005 -ND— SPIKE AND SPIKE DUPLICATE: Spike - 920601947 Spike Dupl Parameter Units MDL DW-1 §pike Rev Recv RPD rse i�§­/—L U-.-005 — 0.0 0 ME T64% � W LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE: Reference Dupl Parameter Units MOIL Value Rector Recv RPD T r—s —en-ir —c -g/ —L DUO 5 0.050 --94% -W REPORT OF LABORATORY ANALYSIS This report shall not be f—v ,,c.ced except in full, without the written consent w' ;41e Analytrcal Services, Inc, Pano Analvtlnal Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersviile, NC 2978 ® Tet 04-875-9092 Fax; 704-8 5- 091 Paul 'Banks QUALITY CONTROL DATA June 04, 1996 le 37 PACE Project Number: 660520 12 ient Reference: Fleet ►d itch: 92 4667 1ples. 92 0601947, 92 0601955, 92 0601998 FHOD BLANK: Method ,ameter Units MDL Blank ia mg/L 0.0C 0 5 - Ng --WE AND SPIKE DUPLICATE: Spike Spike Dupl ,ameter Units MDL 92060060 S ike Recv Rcv PD m9/ 0. 0t 5 N _ O 10 ` 0 3RATORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE. Reference Dupl ,meter Units MDL Value Reev Recv RD m/L 0.005 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace .Analytical Services, Inc: Pace Analytical Services, Inc, 9800 Kinsey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 Mr. Paul Banks QUALITY CONTROL DATA June 04, 1996 Page 38 PACE Project Number: 6►0520512 Client Reference: Fleet Mercury Batch: 92 46698 Samples: 92 0601947, 92 0601955, 92 0601998 METHOD BLANK AND SAMPLE DUPLICATE. Duplicate Method of Parameter Units MDL Blank 9205 6927 92 0596927 RPD Mercury mg L 002 N SPIKE: Spike Parameter Units MDL 920596927 Spike Recv Mercury mgJL 002 N LABORATORY CONTROL SAMPLE: Reference Parameter Units MDL Value Re v mercury mg/L 0.0002 This; report shall hot b pt in fulL with6onsern4teServices, inc. Pace Analytical Services, Inc. 9800 Kinsey Avenue* ulte 100 Huntersvlle, N� 2078 Fax: 704-87-091 it Banks QUALITY CONTROL DATA June 04, 1996 39 PACE ProjectNumber: 660520512 Reference: Fleet am 1: 92 46692 s:'92 0601947, 92 0601955, 92 0601998 BLANK:' Method ter Units MDL Blank im g/L .045 kND SPIKE DUPLICATE: Spike 920601947 Spike Dupl ter Units MDL D-1 Spike Rev Recv RPD JIM mg 1 L 0.000 Nib 0.0 8 iORY CONTROL SAMPLE AND CONTROL SAMPLE DUPLICATE: Reference Dupl ter Units MDL, Value Rev Recv RPD JIM mg/L 0.005 U.0 a 6 1 REPORT OF LABORATORY ANALYSIS This report shall not to o­ xi ced except in full, without the written consent + ;-'+:,e Anaiyticaf Services, Inc. Face Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 Huntersvill , NC 28078 Tel: 704-87-9092 Fax: 704-87 -9091 Banks QUALITY CONTROL DATA dune 04, 1996 PACE Project Number: 660520512 eferene: Fleet 1TY CONTROL 2 46811 2 0601947, 92 0601955, 92 0601998 LANK. Method r Units MDL Blank mg/L 10TU 5 NO mg/L 0.20 N mg/L 0.50; ND; mg/L, 0.010 ND m mg/L 0.010 ND mg/L 0.10 ND mg/Ln 0.010 ND mg/L 0.10 NO _mg/L 0.010 ND mg/L0.010 ND mg/L 0.010 ND mg/L 0.010 ND mg/L 0.10 NO m' mg/L 0.20' ND e mg/L 0.010 NO urn mg/L 0.05 ND mg/L 0.05 ND` m mg/L 1.0 ND mg/L 0.50 ND mg/L; 0.010 ND mg/L 0.20' NO mg/L` 0.50 NO mg/L ' 0.20' NO mg/L; 0.010 ND mg/L, 0.010 NO mg/L 0.010 NO REPORT OF LABORATORY ANALYSIS This report shall not be rec wx,.j ed except In full, without the written consent of Face analytical Services, Inc, Pace AnalyticalServices, Inc, 9800 Kincey Avenue, Suite 100 PAL Call Fluntersville, NC 29078 Tel: 704-875-09 Fax: 704-875-9091 Paul Banks QUALITY CONTROL DATA June 04, 1996 e 41 PACE Project Number: 660520512 ent Reference: Fleet QUALITY CONTROL atch: 92 4 811 Ales; 92 00194, 92 0601955, 92 0601998 E AND SPIKE DUPLICATE: Spike Spike Dpl ameter Units MDL 920603338 S ike Recv Rcv RPD �num_ mg/L .0 __ 0 1 4% 04% 0% Imony mg/L 0.20 ND 5.0 100% 101% 1% enic mg/L 0.0 ND 5.0 104 104% 0% ium mg/L 0.010 0.011 5.0 101% 101% 0% llium m/L' 0.10 ND 1.0 103% 103% 0% on m/L 0.10 ND 1.0 108% 108% 0% ium mg/L 0.00 ND 1.0 103% 103% 0% ium m/L 0.10 78 100 97% 98% 1% omim' mg/L 0.00 ND 1.0 100% 101% 1% all mg/L 0.010 ND 1.0 11% 102% 1% per m/L 0.010 ND 1.0 101% 101% 0% n mg/L; 0.010 1.1 50 101% 11% 0% mg/L; 0.10 ND 5.0 101% 11% 0% esiu mg/L 0.20 1.4 50 107% 107% 0% anese /L; 0.010 ND 1.0 104% 104% 0% ybdenum mg/L 0.05 ND 1.0 96% 97% 1% kel mg/L 0.05 ND 1.0 100% 100% 0% assium mg/L 1.0 1.2 100 109% 110% 1% enium /L' 0.50 ND 5.0 104% 104% 0% ver mg/L 0.010 ND 5.0 83% 84% 1% 1um mg/L 0.20 5.4 50 104% 104% 0% Ilium m/L 0.50 ND 5.0 106% 106% 0% anium mg/L" 0.010 ND 1.0 96% 97% 1% adium mg/L 0.010 ND 1.0 102% 103% 1% mg/L" 0.010 0.28 5.0 104% 104% 0% REPORT OF LABORATORY RY ANALYSIS This report shall not c ,!- ced except in full, without the written consent 41 � * -e L,,nafytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 untersville, NC 28078 Tel. 704-875-9092 Fax: 704-875-9091 Mr. Paul Banks QUALITY CONTROL DATA June 04, 1996 Pace 42 PACE ProjectNumber: 660520512 Client Reference: Fleet ICP QUALITY CONTROL Batch: 92 46811 Samples: 92 0601947, 92 0601955, 92 0601998 LABORATORY CONTROL SAMPLE AND CONTROL SAMPLE` DUPLICATE Reference Dupl Parameter' Units MDL Value Rev Recv RPD A uminum mg/L 0.05 'O 9- 9 °0% Antimony m/L; 0.20 5.0 9% 97% 0% Arsenic mg/L; 0.50 5.0 % 97% 0% Barium mg/L 0.010 5.0 95% 95% 0% Beryllium g/L 0.010 1.0 95% % 1% Boren mg/L 0.10 1.0 9% 96% 1% Cadmium mg/L 0.010 1.0 9% 9% 0% Calcium mg/L 0.10 100 91% 91% 0% ` Chromium mg/L 0.010 1.0 94% % 1% Cobalt m/L' 0.010 1.0 95% 5% 0% Copper mg/L 0.010 1.0 94% 5% 1% Iron m/L' 0.010 50 9% 95% 1% Lead m /L 0.10 5.0 94% 94% 0% Magnesium mg/L; 0.20 50 100% 100 0% Manganese mg/L; 0.010 1.0 97% 7% 0% Molybdenum m /L; 0.05 1.0 94% 94% 0% Nigel mg/L 0.05 1.0 9% 4% 1% Potassium mg/L 1.0 100 10`1% 102% 1% Selenium mg/L 0.50 5.0 96% 96% 0% Silver mg/L 0.010 5.0 95% 94% 1% Sodium mg/L 0.20 50 97% 98% 1% Thallium m /L; 0.50 5.0 9% 9% 0% Titanium mg/L 0.00 1.0 3% 9% 0% Vanadium mg/L 0.010 1.0 9% 96% 0% Zinc m/L 0.010 5.0 95% 96 1% REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Dace analytical Services, inc; Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 r. Paul Banks QUALITY CONTROL DATA June 04, 1996 age 43 PACE Project Number: 660520512 lient Reference: Fleet )LATILE ORGANICS Batch: 92 46927 amples: 92 0601980, 92 0601998 7-THOD BLANK: Method arameter Units MDL' Blank r- icfiT-or--o-difluoromethane -dg-/-L T-.O ND- floromethane ug/L 1.0 ND iloroethene (Vinyl chloride) ug/L 1.0 ND romomethane ug/L 1.0 ND floroethane ug/L 1.0 ND richlorofluoromethane ug/L 1.0 ND ,1-Dichloroethene ug/L 1.0 ND ichloromethane ug/L 1.0 ND rants-1,2-Dichloroethene ug/L 1.0 ND ,I-Dichloroethane ug/L 1.0 ND is-1,2-Dichloroethene ug/L 1.0 ND ,2-Dichloropropane ug/L 1.0 NO floroform ug/L 1.0 ND romochloromethane ug/L 1.0 ND ,1,1-Trichloroethane ug/L 1.0 ND ,I-Dichloro-l-propene ug/L 1.0 ND arbon tetrachloride ug/L 1.0 ND ,2-Dichloroethane ug/L 1.0 ND ,1,2-Trichloroethene ug/L 1.0 ND ,2-Dichloropropane ug/L 1.0 NO romodichloromethane ug/L 1.0 ND ibromomethane ug/L 1.0 ND is-1,3-Dichloro-l-propene ug/L 1.0 ND rans-1,3-Dichloro-l-propene ug/L 1.0 ND ,1,2-Trichloroethane ug/L 1.0 ND ,3-Dichloropropane ug/L 1.0 ND atrachloroethene ug/L 1.0 ND ibromochloromethane ug/L 1.0 ND ,1,1,2-Tetrachloroethane ug/L 1.0 ND romoform ug/L 1.0 ND ,1,2,2-Tetrachloroethane ug/L 1.0 ND ,2,3-Trichloropropane ug/L 1.0 ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the w6ften consent of Pace Analytical Services, Inc, Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 unterville, NC 28078 Tel. 704875-90 2 Fax: 704.875- 091 Paul Banks QUALITY CONTROL DATA dune 04, 1996 44 PACE Project Number: 660520512 nt Reference: Fleet I Method ameter Units MDL Blank Ito enzene ug/L 1.6 ND hlorotoluene ug/L; 1.0 ND hlorotoluene ug/L 1.0 ND -Dichlorobenzene ug/L 1.0 ND -Dichlorobenzene ug/Ls 1.0 ND -Dichlorobenzene ug/L 1.0 ND -Dibromo--chloropro ;ane g/L 1.0 ND ,4-ri'chlorobenene ug/L 1.0 ND achlorobutadiene ug/L 1.0 ND 3--Trichlorobenzene g/L 1.0 N ene ug/L 1.0 ND uene u/L 1.0 ND orobenzene /L 1>0 ND ylbenzene u/L 1.0 ND enes g/L 1.0 ND gene g/L 1.0 ND propylbenzene ug/L 1*0 ND roplenzene ug/L 1.0, ND -Trimethylbenzene ug/L 1.0 ND utylbenzene ug/L- 1.0 ND ,4-Tri'methylbenzene ug/L 1.0' ND utylbenzene u/L 1.0- ND sopropyltoluene ug/L 1.0 ND utylbenzene ug/L 1.0 ND hthalene u/L 1.0 ND REPORT OF LABORATORY ANALYSIS This report shall not be except in full, without the written consent -F ,k e Ana yt}cal services, Inc. ' Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersvllle, NC 28078 Tels 704-87 -9092 Fax: 704-875-9091 . Paul Banks QUALITY CONTROL DATA June 04, 1996 lge 45 PACE ProjectNumber: 660520512 ient Reference: Fleet u Reference xameter Units MDL Value Re v cfiToro ifluoromethane ug/L .0, 0 60% iloromethane ug/L 1.0 20 70% iloroethene (Vinyl chloride) a /L, 1.0 20 9 °omomethane ug/L 1.0 20 6 iloroethane a/L; 1.0 20 90% ichlorofluoromethane /L 1.0 20 85% 1--Dichloroethene ug/L 1.0 20 105% chlorothane ug/L- 1.0 20 16% R1 tans-1,-Dich'l6roethene ug/L 1.0 20 100% I-Dichloroethane ug/L 1.0 20 90% -1,2-Dichloroethene a/L' 1.0 20 6% -Dichloropropane ug/L 1.0 20 100% lloroform ug/L 1.0 20 % `omochloromethane ug/L 1.0 20 95% I,'I-Trichloroethane ug/L; 1.0 20 90% I-Dichloro-I-propene ug/L 1.10 20 95% lrbon tetrachloride ug/L 1.0 20 95% 2-Dichloroethane ' u/L: .1.0 20 9'5% 1,2--Trihloroethene ug/L 1.0 20 95% 2-Dichlropropane ug/L; 1.0 20 90 "o odichloromethane a /L 1.0 20 85% bromomethane ug/L 1.0 20 9% s- 1, -D'i chl oro--I-propene ug/ L 1.0 20 0% -an-1,3-Dichloro-l-propene ug/L 1.0 20 90% 1,2-Trichloroethane ug/L 1.0 20 90% 3-Dichloropropane /L 1*0 20 8% !trachloroethene ug/L 1:0 20 95% bromochloromethane ug/L 1.0 20 85% 1,1,2-Tetrachloroethane ug/L 1.0 20 105% -omoform ug/L 1.0 20 0% 1,2,2-Tetrachloroethane ug/L 1..0 20 5% REPORT OF LABORATORY ANALYSIS This report shall not be er°�mced except in full, without the written consentof Pvice Ana�ytical Services, Inc; Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 Paul Banks QUALITY CONTROL DATA June 04, 1996 le 46 PACE Project Number: 660520512 ient Reference: Fleet imp W. �*P L E Reference ,ameter Units MDL Value Rev F,3---T'richloropropane -dg—/ —L 1—.0 ---M— -85-%- )mobenzene ug/L 1.0 20 90% *hlorotoluene ug/L 1.0 20 95% 'hl orotol uene ug/L 1.0 20 100% 3-Dichlorobenzene ug/L 1.0 20 100% I-Dichlorobenzene ug/L 1.0 20 95% )-Dichlorobenzene ug/L 1.0 20 95% ;-Dibromo-3-chloropropane ug/L 1.0 20 75% ?.4-Trichlorobenzene ug/L 1.0 20 100% (achlorobutadiene ug/L 1.0 20 105% 3-Trichlorobenzene ug/L 1.0 20 90% ' izene ug/L 1.0 20 90% luene ug/L 1.0 20 90% lorobenzene ug/L 1.0 20 95% iyl benzene ug/L 1.0 20 90% lenes ug/L 1.0 60 90% (rene ug/L 1.0 20 100% )propylbenzene ug/L 1.0 20 90% )ropylbenzene ug/L 1.0 20 90% 1,5-Trimethylbenzene ug/L 1.0 20 90% lutylbenzene ug/L 1.0 20 95% ?4-Trimethylbenzene ug/L 1.0 20 95% iultylbenzene ug/L 1.0 20 95% [sopropyltoluene ug/L 1.0 20 90% )utylbenzene ug/L 1.0 20 95% )hthalene ug/L 1.0 20 75% REPORT OF LABORATORY ANALYSIS This report shall not be -L, ,, -ced except in full, without the written consent :* � ,i,e —aiytical Services, Inc. Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 Huntersvi#le, NC 28078 Tel: 704-875- 092 Fax; 704-875.9091 Ir. Paul 'Banks QUALITY CONTROL DATA June 04, 1996 )age 47 PACE Project Number. 660520512 .Bent Reference: Fleet' fOLATILE ORGANICS Batch. '92 46933 samples.`92 0601€390, 92`0601904, 92 0601912, 92 0601920, 92 0601939 92 0601947, 92 060155, 92 0601963,`92 0601971 Method Parameter Units ML Blank Mle Toro ifluoromethane ug/L Chlromethane ug/L 1.0 NO Chloroethene (Vinyl chloride) ug/L 1.0 NO Bromomethane ug/L 1.0 NO Chloroethane ug/L 1.0 NO Trichlorfluoroetane ug/L 1.0 NO 1,1-Dichloroethene ug/L 1.0 NO Dichloromethane u/L 1.0 NO trans-1,2-Dichloroethene u/L; 1.0 NO 1,1-Dichl'oroethane ug/L' 1.0 NO cis-1,2-Dichloroethene ug/L 1.0 ND 2,-Dichloropropane ug/L' 1.0 ND Chloroform u /L 1.0 NO Bro ochl rome h ne a /L 1.0 NO 1,1 1-Trlchloroethane a /L; 1.0 NO 1,1Dichloro--propene ug/L 1.0 NO Carbon tetrachloride u/L' 1.0 NO 1,2-Dichloroethane ug/L 1.0' NO 1,1 2-Trichloroethene ug/L 1.0' NO 1,2-Dichloropropane a /L 1.0 NO Bromodichloromethane ug/L 1.0' NO Dibromomethane ug/L 1.0 ND cis1,3-pichloro-1-propene ug/L 1.0 NO trans-1,-Diclorol-propene' u/L 1.0 ND 1,1,2-Trichlor°oeth ne a /L 1.0 N 1,-Dichloropropane ug/L 1.0 NO Tetachloroethene ug/L 1.0 NO Dibromochloromethane u L 1.0 NO 1,11,2-Tetrachlorpethane ug/L 1.0 NO Bromofor ug/L 1.0 NO 1,1,2,2-Tetra hloroethane ug/L 1.0 NO REPORT OF LABORATORY RY ANALYSIS This report shall not be reproduced. except In full, without the written consent of Pace Analytical Services, Inca Pace Analytical Services, Inc. . 9800 Kincey Avenue, Suite 100 A Ica Huntersville, N 28078 Tel; 7 4-87 -909 Fax. 704-875-9091 ! Banks QUALITY CONTROL DATA June 04 1996 3 PACE Project Number: 660520512 leference: Fleet ORGANICS 2 46933 92 0601890, 92 0601904, 92 0601912, 92 0601920, 2 0601939 2 0601947, 92 0601955, 92 0601963, 92 001971 3LANK: Method ?r' Units MDL Blank chloropropane ug/L' 1.0 izene ug/L 1.0 ND )toluene ug/L; 1.0 ND )toluene ug/L 1.0 ` ND florobenzene ug/L 1.0 NO rlorobenzene ug/L 1.0' ND florobenzene g/L 1.0 ND �omo--chloropropane ug/L 1.0 ND ,-ichlorobenzene u/L 1.0' ND )robuiene; ug/L 1.0 ND ^i hlorobenzene /L'; 1.0 ND u/L 1.0 ND u/L 1.0 ND ?nzene ug/L 1.0 ND izene ug/L 1.0 ND u/L 1.0 ` ND ug/L 1.0 ND (lbenzene ug/L' 1.0 ND Ibenen u/L 1.0 ND ,*imethylbenzen ug/L 1.0 ND )enzene u/L 1.0 ND ,'imethylbenzne ug/L 1.0 ND )enzene ug/L 1.0 NO )pyltoluene a/L, 1.0 ND aenene ug/L 1.0 ND Iene a /L 1.0 ND REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written'consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 +AM Huntersville, NC 28078 Tel: 704-87 -9 92 Fax: 794-875-9091 Banks QUALITY CONTROL DATA June 04, 1996 PACE Project ' Number: 660520512 ,e"erenee: Fleet ORGANICS 92 46933 2 0601890, 92 0601904, 92 0601912, 92 06 1920, 92 0601939 92 0601947, 92 0601955, 92 0601963, 92 0601971 lRY CONTROL SAMPLE: Reference r Units MDL Value Recv Ichloropropane ug/L 1.0 100 zene ug/L 1.0 20 95% ,toluene a /L 1.0 20 100% ,toluene ug/L 1.0 20 110% ilorobenzene ug/L 1.0 20 105% lorobenzene ug/L 1.0 20 100% ilorobeene ug/L 1.0 20 100% ,o o- - hloropropane ug/L 1.0 20 90% 1 hlorobenzene g/L 1.0 20 105% irobutadiene ug/L; 1.0 20 105% ,lhlorobenzene ug/L; 1.0 20 105 ug/L 1.0 20 95% ug/L 1.0 ' 20 95% m ene ug/L 1.0 20 95% izene g/L 1.0 20 95% ug/L 1.0 60 9 % ug/L 1.0 20 105% ,lbenzene ug/L 1.0 20 90% benzene ug/L 1.0 20 95% ,imeth lben ene a /L, 1.0 20 95% ienzene ug/L 1.0 20 9% imethylbenzene ug/L- 1.0 20 95% ienzene ug/L 1.0 20 95% ipyltoluene ug/L 1.0 20 9% ienzene u/L 1.0 20 95% ene ug/L 1.0 20 % REPORT OF LABORATORY ANALYSIS This report shall not be re,. .> e . except in full, without the written consent of P,.a:ee znalytkcal Services, Inc. Pace Analytical Services, Inc, 9800 Kincey Avenue, Suite 100 ok r full Huntersville, NC 28078 Tel: 704-875-9092 Fax: 704-875-9091 1 Banks FOOTNOTES June 04, 1996 1 for pages 36 through 50 PACE Project Number: 660520512 Zeference: Fleet Method Detection Limit No calculation due to value below detection limit. Not detected at or above the MDL. Recovery falls outside the quality control limit, however, this compound is not detected in the associated sample(s). Relative Percent Difference REPORT OF LABORATORY ANALYSIS This report shall not be -�v, -I-ced except in full, without the written consent �' �- * e 4naiyfical Services, Inc. Pace Analytical Services.; Inc. „ 9800 Kincey Avenue, Suite 100 Huntersv lie, NC 28078 Tel: 04-87-909 Fax; 704-875-091 QUALZTY CONTROL RUPORT.BY Min Op, CUSTODY S P T X 8 A C C U P A C Y DATA alyte Procedure SP SSR SA SII _.'73 SUL SLL F Det Date Ast SY S 1 Fluorenc Imenaphc 610««« 610 0 14.6__ 25 20«__ 20 132 43 05/25/96 rkp 96 0000000 Pl ante Fltxr tc 610 610 O 0 18.3 20 125 92 147 116 36 36 05/25/96 05/25/96 r p rkp 96 96 0000000 0000000 in crppyc Haphthso 610 0 13.9 14.4 20 20 70 72 124 116 43 36 05/25/96 O5/25/96 rkp rkp 96 96 0000000 Phnanthc 610 610 0 O 14 15:9 20 20 '70 80 145 67 05/25/96 rkp 96 0000000 0000000 2Menaphc 610 0 19.7 20 99 145 158 5o 48 05/25/96 O5/25/96 rkp rkp 96 96 0000000 he Acen phyc 610 610 0 0 14,8 15;9 20 20 74 146 40 05/25/96 rkp 96 0000000 OOQOOOO Anthracc Bnzaantc 610 0 15 s 20 80 80 146 155 55 61 05/25/96 055/25/96 rkp rkp 96 9,6 0000000 0000000 Bnza rc 610 610 0 0 15.9 15 20 20 80 75 139 113 40 41 05/25/96 05/25/96 rkp 96 0000000 13nzkfluc nzkliue 610 61O 0 0 16 14.9 20 80 133 37 O5/25/96 r r 96 96 0000000 0000000 Snzperyc Chrysenc 610 0 22.8 0 20 75 U4 121 115 36 61 05/25/96 05/25/96 rkp rkp 96 96 0000000 Pyrenec 610 610 0 0 21.4 11.6 20 20 107 151 49 05/25/96 rkp 96 0000000 0000000 i vppyc Naphthec 610 0 15.023 20 58 75 144 116 52 36 OS/25/96 OS/29/86 r t 56 9 0000000 Fh Chc 610 610 0 0 15,0517 15.8813 20 20 75 64 14a 145 67 50 O5/29/96 05/29/96 ge 96 OAO5 31 0005531 Fyzanec Sncbfluc 610 610 O 0 1S,88L3 16.8067 0 79 144 52- 05/29/96 90 96 0005531 0005531 antc 610 61O 0 O 23.8425 37.8161 20 20 20 84 119 189 133 11 116 37 61 * 36 * OS/29/96 05/29/96 96 96 0005531 0005531 Bnzkryc Hn kLiu 610 0 15.379 20 77 121 36 05/29/96 96; OOOS531 Fluorenc Flurantc 61O 610 0 0 15.5254 14.5127 20 20 78 73 131 124 43 43 05/29/96 09/29/96 96 96 0005531, 0005531 Chrysenc 610 0 22.1995 20 111 151 49 05/29/96 05/25/96 96 0005 31 Imenaphc phc 610 610 0 0 23.3758 16.042 20 20 117 80 147 14 36 40 05/29/96 05/29/96 96 96 0005531 0OOSS31 Mena pkc A np yc 610 610 0 0 18.8553 0 54 158 48 05 29/56 ec 96 OOOSS31 0005531 Anth acc 610 0 16.806 15.3481 20 20 84 77 146 255 55" 61 05/25/96 OS/29/96 gmh 96 0005531 gmh 96 000 531 REPORT LABO TORY ANAL1 This report shall not be . ed except in full, without the written consent of . 4,�a�ytical Services, Inc. Pace Analytical Services, Inc. 9890 Kincey Avenue, Suite 100 kuntersville, SIC 28978 Tel: 704-875-9092 Pax: 704-875-9091 QUALITY CONTROL REpopT BY Ct A.SFt OF; CLMSTODy twwww^.w wwwwww:w#wwww#wwwwww#wwa:ew+aw www#wWww#srww#wwww#s+,e##ww#wwwwry d.3 : a wwwwrS P I KS A=CCEMR A CY DACA Cont3nuContinuedc� rrw#wwww.r•w www#w.w wwwwaawwww#ww.ww#ww waaw wwwwwwwwwww+wwwwwxa r+www sew tir Zumber Ana yte Procedure ---- SR SSR SA 5pk&R UL SLL F Det .22742 Bnzaantc 610.. 0____ J .16:6353 20_ _. ___ _m Date Aar SY 9mpi 22742 Snzapyrc 610 0 83 1S,5443 20 78 139 40 113 05/29/96 96 _ 00O5S31 wwww#w,tt www,twww w,rw iewwwwwww#we,t ws, wwwwtw#wwwar,.a w,rvwwtsrw 41 OS/29/e6 96 0005531 Q. C. R: S, A C C V FA C Y Mw#wwwwwwew#wwww#w,a##w#w#'f4#wwwwwwwwwww D A T A . www#wwbwwwwwwwwww umber Analyze Procedure QCRS True Val QCRS Meaeured QCRS k Rec A7L 22686 Fluorene 610 20.OPQ 14. __ ----- _.. ALL _ F Dot hate Ast 22686 22606 1 naphc Dabnantc 61O 610 20.0 9.9 74,5 17i.S ISO 30 05/25/96 rkp 22686 22686 Flurantc 610 20.0 20«O 19.4 14.3 zSO 30 OS/25/96 OS/25/96 rkp rkp 22686 lndn Ftaph sc 610 15.8 79«0 150 O 05/25/96 rkp Z2686 22686 Phnanthc 610 20.0 20.0 18.0 17,5 90.0 ISO 150 30 30 OS/25/96 0 /2Sj9 rkp rkp 42686 2Menaphc Acenaphe 610 610 20,0 20.0 19.7 19.7 98.5 ISO 30 05/25/96 05/25/96 rkp 12686 12686 Acenptyc Anthracc 61.0 610 20.0 17.5 87.5 IISO SO ISO 30 OS/2SJ96 rkp rkp r2686' 2686 Snza�antc 610 20.0 20.0 1.9 16.3 ISO 30 3Q 05/25/96 Q /2 /9 rkp rkp ,2686 Bnzappyy e Bnzbi 610 20,0157 81.5 S1.5 1S0 30 05/25/96 rkp 2686 `2686 uc Bnzkf2uc 610 610 20.0 20.0 16.6 15.2 83.0 ISO 30 OSf25/96 0/2S/96 rkp rkp 2686' Bnzperyc Chrysenc 10 610 20.0 15.7 76.0 150 ISO 30 05/2S/96 rkp 2686 Pyronec 610 0.0 20.0 22.0 15.4 178 0.0 110. ISO 30 30 05/25/ 6 05/25/96 rkp rkp 263E 269S 2695' 1 aphc Mena phe Na Mc 610 610 610 20,0 20,0 21.5764 21.7401 77'9 107.9 195.E ISO 250 30 30 05/25/96 05/27/96 rkp rk In 20,0 19.1134 1ISO 0 05/27/96 rkp 2742 Na2742 p h ac 610 20.0 20.0 17. 19 17,5192 50 150 30 05/29/96 OS/29/96 r ;9 2742' 2742 Phnazethc Pyrenec 610 6100.0 20.0 15.9176 87.8 87.6 79`6 ISO ISO 30 OS/29/96 11,2218 56.1 ISO 30 30 05/29/'96 gmh 05/29/96 gmh REPORT 0F1.ABORATORYANALYSIS This report shall not be reproduced except in full, without the written consent of face Analytical Services, Inc. Pace Analytical Services, Inc, ' 9800 Kincey Avenue, Suite 100 Nuntersville, NC 28078 Tel. 704-875-9092 Fax: 704-87-091 QUALITY CONTROL REPORT BY CHAIN OF CUSTODY ^wwvrxx^awwrww,aw^,rw,aw.aww#,rrw*arrwm,awwwxr:awxxarww�a.www�,aw.twww,aawxxw.r,�d. C C U wrr,mwww+ww++,t,atwawwtrwww�^�arwwx.awe,awwwxwwwwx*wrwxwwr,�.rw,rw^auww,ra^,ar;:a R A C Y D'A T A continued<--_ ber -® Analyte Procedure QCRS 'rue Val QCRS Measured______ QCRS k Rec 742 ---------- Bnzbflue 61O 20.t7-----7--- ®4®76.8 ACL __ ALL F -_ Det Date Ast 742 742 anzp$ryc 610 Dibnantc 610 MO 21.7264 108,E 15O 30 05/29/96 742 742 BnzkPluc 610 Fluoreuc 20.0 34„3821 20.0 34.3821 171.9 ISO ISO 30 30 w 05/29/96 qmh 05/29/96 gmh 742 742 610 Fluorenc 610 Chrysenc 20,0 13,9115 20.0 14. 528fal '71.8 ISO 30i 05/29/96 05/29/96 gmh gmh 742 610 IMenaphc 610 20,0 20,720068.3 20.0 103.E ISO ISO 30 05/29/96 742 742 Acenaphc 610 2Menaphe 610 21.812 20.0 14.9727 20.0 17.5952 174.5 74.9 ISO ISO 30 3O 05/29/96gmh 05/29/96 gmh 05/29/96 F42 142 Acenpiayo 610 Anzaantc 610 20.0 16.i276 88.0 ISO 30 05/280.6 9/96qmh qmh 42' 1 �42 Bnzaantc 610 t9ttsapyro 610 20,0 14.4696 20.0 15.2549 72.3 70.3 ISO ISO 30 30 005/29/96 gmh 5/29/96 guth wwa,vwxxxwxwxwww,axxwwwaxxxwwwaxxwawwaxwxwwwxxwxwwxa. 20.0 14.1785 70.9 ISO 150 30 30 05/29/36 OS/29/96 qmh ^wx;awxxwxxrrw.awxw;aw P R$ C? S T O' I4 D A T A. awxwwwwxxwwxxwwxxww wwxxww,awxwwxiae er Proc Analyte ---- _ sample Result Dup Sample Result Dup RPD 86 610 -- --- ____ 14.6m µ 12.6 DLFL F SY Smpl# D$t Date Ast 86 86 IMenapnc 1M$sapksC 61O Dibnantc 610 25 21.1 18.3 14.7058 16,9197 38 40 96 004t&000 05j 5/96 xkp 86 86 Flurantc 62O Sndn c 610 15.95 13.9 12.2 24.4 12.5 13,7226 13.0269 38 90 96 96 96 ODOOOOO 05/25/96 0000000 05/25/96 0000000 rkp rkp 86'@7a 96 ht Phepr s c 61O 12,4 14.1263 12.1212 37 96 05/25/96 0000000 05/5/96 rkp rkp 96 96 2Menaphc 610 Acs�napple 61i7 IS's 13.8 19.7 16.9 14.1424 15.3005 42 28 96 96 000000#i O5/25/96 0000000 05/25/96 rkp rkp 96 96 Acenph Anthr'acc 14.a 12.9 13.9 13.7184 47 40 96 96 OOOOOOO 05/25/96 0000000 05/25/96 rkp 36 610 8na to 610 15.9 13.3 15.9 13.4228 17.8082 35 25 96 0000000 O5/2S/96 rkp rkp 36 Bnzapyrc 610 15 13 9 13.4228 14.2857 37 96 96 0000000 05/25/96 OOOOOOO 05/25/96 rkp 37 96 0000000 05/25/96 zkp rkp REP O F LABORATORY ANAS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, Inc. a ' 9800 Kincey Averse, Suite 100 Huntersvlile, NC 28078 Tel; 0-875-9092 Pax. 704-875-091 QUALITY - CONTROL PO T »BY CHAIN OF CUSTODY wawwrwwwwwawwwwaw,rrwtwr.w�r wwwww�rwww�rwwawwxw,a�wraww+r,tawrwr:rw,rw ww�.a P R 6 C 19 S 0 N D T A wwwwar:aww,r.wwarww,rw�wwzawrtwwa.wwww;uwt,w+r,mw++,s.�wwrwwwa.:.wm.ewwwwww.twww�w continued <c..w. Number Aaalyte ---Proc Sample Result Y?UpSample Result i7up RPS7 37S9L 22686 $nab6luc 61016.__ 13,8 F SY S 1 I1et Date AeC 22686 22686 Snxkfluc Ba 610 14.9 12.9 14.7651 143884 34 37 96 96 O000000 05/2 /96 rk- 22686 22686 C i8eno 610 21.4 20.2 18.7 12.0930 39 96 0000000 0000000 05/25/96 OS/25/96: rkp rk 22742 Pyrenec In c �c' 610 610 11.6 15,023 10.2 14.4738 12.8440 27 39 96 96 0000000 0000000 05/25/96 05/25/99 rkp 22742 Vaph 610 15.0517 14.4158 3.72379 4.31594 37 96 0005531 05/29/56 zrk 22742 2274 Phnanthc enec 610 61O 16,7725 a5.$813 16.6456 15.9706 %59468 41 28 96 96 0005531 0005531 05/29/96 05/29/96 qMh 2274 2 742 $nzb luc 610 16.8067 16.1765 560097 4.6093 39 96 00OSS31 05/29/96 gmh 22742 Snipe Dibnaa� 610 610 23.8425 37.8161 23.2499 2.94771 34 39 96 96 0005531 0005531 OS/29/96 gmh 22742 22742 Sra kfluc Fluorenc 610 610 15`.379 37.9252 14.8196 288085 3.70480 39 96 0005531 O5f29/96 05/29/96 gmh gelh 22742 F3urantc 610 15.5154 14.5127 14.9127 13.9699 7.96146 37 3 96 96 00O 531 0005531 OS/29/96 05/29/96 qfMh 22742 22742 Chrysenc 1Menaphc 610 610 22,1995 26.027 3,81216 15.8730 27 7 96 0005531 05/29/96 qMh gM 22742 Acenphc 61O 23.3798 16.042 23,8041 15.5134 1„79949 3.75029 40 96 96 0005531 00OS31 05/29/96 05/29/96 gish 22742 2274 2 =phc Acenphyc 610 610 18:BS53 16;806 19.5298 16.3 3.51438 40 47 96 96 00055 1 0005531 05/29/96 O5/29/96 gmh gmh 22742 Anthracc 610 153491 19 14,7567 2.86198 3.92894 39 96 0005531 OS/29/96 goth 22742 22742' $nsaantc $nra 610 610 16:6353 15.9927 3193894 25 37 96 Ci00 S31 05/29/96 gmh gmh 155443 15.1764 2.39512 37 96 0005531 05j9/96 qMh ww�rwar6araw,xytetyp w wwwxw,a w,o-wwerws+wwa;vww+awwrt,rwww+k�ww aw+aara�tw 96 000551 05/29/96 Thh MST H0 w was q4+r w•w wara,vwww!'wwf D $ LAN K DATA ww*w wA:.eM ww«w warww w wlarw•rewwiYr wYaw e<- ii4'w irwWa umber Analyte Proc Detection 'Lim Sl k Result it 2 PluIMenapnc 1D___ _78;._ _ per Date Ast 606 22686 22686 1Mersaphc DikxOantc 610 610 1 2 ' BDL U /L VG/L 05/ s/96 05/25/96 rim rkp 22696 Fiurantc 610 .2 .97 SSDLDL BDL CSD/L 05/25/96 rkp UG/L 05/2 /96 rkp • �;*. . 1 this report shall notexcept withouta Face Analytical Services, Inc. 9800 Kincey Avenue, Suite'100 •Aft AM Aft Huntersville, NC 28078 Tel: 704-875- 92 Fax: 704-875-9091 QUALiTy CONTROL REPORT,BY cnAIN OF CUSTODY wW*Www**w#w**ww##www k**#w*�9tWw'hY4***#5pw*A'94w*#'*#i}wtl¢a+Y#ww:H iy .W*##k*'k*t4##*p{ -> M S T H 0 D B L A N K D A T A continued ww*+rrww,rw#***wWwww#*i�r****t#:r.wW*.u*aa ww w�a�iawy„y**##ww*wwwwr,aW*►aw W+�*rr* Number Anal to Prot Detection Lim Blank Result Unit Der Date Ast 22686 22606 Indn c aph c 610 610 1,3 1 _ 5/_6 rk 2686 22686 1Phnanthc 2Menaphc 610 610 1.1 1.2 SOL SOL UG/L} UG/L 05/25/96 OS/25/96 rkp rkp 22686 22686 Acena he Ace27 Epp 610 1.l SOL UG/L UGfT. 05/25f96 05/25/96 rk rkp 22646 22686 Anthrracc Bnzaantc 61°' 610 ill 8 SOL UG/L U /L 05/25/96 05/25/96 rkp rkp 22686 22686 Bnza yrc ansti uc 610 610 i 84 BD SOL UG/L UG/L 05/25/96 05/25/96 rkp rkp 2268E 22686 Bnxkflue Snzkfluc 610 610 .8 6 SOL SOL UG/L UG/L 05/25/96 05/25/96 r rkp 22686 22686 Chrysene Manse 610 610 1.1 86 SOL SOL BD UG/L CTG/L 05/25/96 05/25/96 rkp rkp 2269 22695 1MnapYac 2Menaphe 6a0 610 2.5 1.2 8DLL SOL U05/7f96kp 2222695 742 NaphthBe uapddhnnLhec 610 61A 1 SOL SOL UG/L VGfi 05/27f96 05/27/96 rkp r pp 1'1 SOL UG/L OS/29/96 gm}i 22742 22742 ph the enscic 610 1,1 BDL UG/L UG/L 05/29/96 05/29/96 gmh 22742 22742 B Bnzperyc 61t01 610 .86 9'7 SOL UG/L UG/L 05/29/96 05/29/916 gmh 22742 22742 Dibaaante Snzkfluc 610 610 1.2 BDL SOL DG/L. GS/29/96 gmh gmh 22742 22742 Florenc Flurantc 610 610 ,8 .78 SOL UG/L UG/L 05/29/96 05/29/96 qmh Smh 22742' 22742 Chryeenc 1 naphc 610 610 .97 1.1 1 BDL L BSiD1S,' UG/L UGLL / 05/29/96 gmh gmh 22742 22742 22742 Acenapha 2Xenap h Acen;El 610 610 1.1 1.2 SDL SOL U /L UG/L 05/ 9/96 05/:29/96 05/29/96 gah qmh 22742 Anthracc 61t0i 91 UG/L 05/29f96gmh gah 22742' Snzaantc 610 .81 SOL' SOL UG/L 05/29/96 gmh 05/29/96 gmh Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 AmWical Hunter vill , NC 28078 Tel: 704-878-9092 Fax: 704-878-9091 QUAL17Y COUTROL REPORT HY CHAM OF CUSTODY twww>tiwwwvr^�yrrvrwwwrkaaarrwtkdre#wawprw.wwwwwOrwwwxkAw:W+4wYxwekwwwwwww#r4rc.wyewww 8 T H 0 A 8 L A M K D; A T A Continued e< �rwvywmwwwrmww.wwwxr,rwkarww,rwrr�awa^ewww.;twwwyrww:wttw.cye�s*w.rwwrwwwwwwrwvrwwwww.try fiber Analyte Peoc Detection Lim Blank Result Unit Det Date Ast >2"742 Snzapyrc 6itt_._____ .:__.__w®-__ HDL ttGiL--------- 05/29/56 rwwwwwwtxewwwwwwyrwwwwaMwwww.w wwwe,w w.;aawwww*�www awww t,ewwwitt 1. e,r ww,sw w`w w*aw,ayr.trw,ear«�a w ar0,wMawM,aE.wNwww,w.�,a y�** ther.. 2265 tples are dilutions, see qc 22686 for: spike data. tsers 22742 ao (9,h,i) oervlere matr m anis-a —.-A. ..si ciumAlziecs as estimates _r ORT OFI ABOR ATORY YSIS iil M R. This report shall not be rer .~.,M m except in full, without the. written consent of ,na:ytcal Services, Inc. Pace Analytical 1 9800 Kincey Aven !III A Huntersvill Tel. Fax: 51311111 QC "PORT S$ CHAIN opCUSTODY +r� �aAwN A� raxY.S Tw+rw � � �aQC COMMINTS T m w c�a aw Nul 22695 ;smples are dilutions, see qc# 22686 for spike ta. t er: 22742 erszc (g,h i) � zo ; peryjons matrix spike exceeds rho ., c; )0' 78 3 )1 ,u macrzx spike exceed the acceptance limit«. Trace %e ano c preision are in coratri�l. Dibenzo €a,hd qualified as estimates. REPORT OF I I TRY ANALYSIS This report shall not be reproduced except in full, without the written consent of Pace Analytical Services, Inc. sw" By (PhINT)' �N� L !J ------------------ - --------------- ----------------- Date SaftVlocl SAMPLE DESCRIPTION TIME MATRIX PACE IN COOLER NOS, BAILERS METHOD ITEM RELINOUISHED BY AFFILIATION ACCEPTED BY AFFILIATION DATE TIME OUT ATE RETURNED DATE NUMBER