WQ0002702_Regional Office Historical File Pre 2018 (5)

AL "E , INC.
Corporate Office Sales and Manufacturin-
2042 Buie Philadelphus Road 8135 Red Road
Red Springs, NC 28377 Rockwell, NC 28138
Tel
Tel. [phone] . 704-279-7908 Boo-46
Fax 7o4-z79--841884i8
Fax [phone] [e-mail]
[e-mail]
May 13, 2011
Mr. Andrew Pitner
Regional Environmental Supervisor
NCDENR Division of Water Quality
Mooresville Regional Office
610 East Center Ave.
Suite 301
Mooresville, NC 28115
Re: NOV-2011-PC-0293
Dear Mr. Pitner:
I have your letter of May 2, 2011 which was received on May 3, 2011.
Condition 10- We found one instance in the logs where on April 21, Trent Tidwell wrote
in the log 22 inches. He did this only because Peggy Finley said that it was 22 inches.
He measured the distance after she left and found 24 inches which is not a violation.
Condition 12- We have tried to establish a vegetative cover and have spent a great deal of
time and money to do this. We have had a great deal of problems getting this done. We
cannot make something grow there. We are going to continue trying.
Condition 28- I cannot find the logs that say there is a violation and therefore as far as I
am concerned there was no violation.
Condition III.5- We are not aware of the discrepancies. I believe the site life is up to date
and is 10 years. DELTA may think 6 years. I am at a loss to understand how this could
possibly be a NOV. To the best of our knowledge we have been in complete compliance
after I fired Jason Desiato.
Best regards,
CHEM, INC.
Randall F. Andrews,
President
ams

Aja
C
North Carolina Department of Environment and
Beverly Eaves Perdue
Governor
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Alchem, Inc.
2042 Buie Phildelphus Rd.
Red Springs, North Carolina 28377
Attention: Randall Andrews
Dear Mr. Andrews:
Coleen H. Sullins
Division of Water Quality
Natural Resources
Dee Freeman
Secretary
RE: Inspection Report
Notice of Violation (NOV) and
Notice of Intent (NOI) to Enforce
NOV-201 1 -PC-0293
Non -Discharge Permit Nos.
WQ0002702 and WQ0016338
Recycle System, Monofill
Rowan County, N.C.
May 2, 2011
Chapter 143, North Carolina General Statutes, authorizes and directs the Environmental Management
Commission of the Department of Environment and Natural Resources to protect and preserve the water
and air resouces of the State. The Division of Water Quality (division) has the delegated authority to
enforce adopted pollution control rules. This letter is a standard notification and is intended to advise you
of the legal requirements under the law.
On February 28, 2011, staff of the Mooresville Regional Office, Aquifer Protection Section (Ellen Huffman
and Peggy Finley) conducted an inspection of the Alchem facility in Rockwell. Ms. Huffman and Ms.
Finley appreciated the time that your staff took in assisting them during the inspection. One purpose of
the visit was to determine if the violations/deficiencies identified during the April 2010 inspections had
been corrected. While several issues have been dealt with, the inspection revealed that the facility was
still in violation of conditions of the subject permits:
WQ0002702, Condition 10 requires at least two feet of freeboard in all three lagoons.
Freeboard measurements for lagoon #1 were recorded in the facility log as follows:
April 22 22 inches June 10 20 inches
May 12 20 inches October 20 inches
WQ0002702, Condition 12 requires that a protective vegetative cover be maintained on all earthen
lagoon embankments.
The earthen embankments were observed to still be essentially devoid of vegetaion.
WQ0002702, Condition #28 requires the permittee to report noncompliance.
Facility logs indicate inadequate freeboard on a number of occasions and no reports were filed.
One
NorthCarohi
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office Phone: [phone] Fax: [phone] J//l
610 East Center Avenue, Suite 301, Mooresville, NC 28115 Internet: www.ncwaterquality.org �/ Y a�uj,� k,

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t
w- .
AJchem, Inc.
Page Two
WQ0016338, Condition 111.5 requires that a report, providing the required information, be
submitted annually to the Division.
The 2010 Annual Report was deficient in the following areas:
1. There were discrepancies between the facility log and the annual report regarding freeboard
measurements.
2. The site life estimate that was included in the annual report is outdated; it stated that the
remaining site life was 10 years. In 2009, Delta Enviromental calculated the site life to be 6
years. In addition, staff has observed what appear to be noticeable changes in the size of the fill
area over the last few inspections.
Failure to comply with conditions in a permit may result in a recommendation of enforcement action, to
the Director of the Division of Water Quality who may issue a civil penalty assessment of not more that
twenty-five thousand ($25,000) dollars against any "person" who violates or fails to act in accordance
with the terms, conditions, or requirements of a permit under authority of G.S. 143-215.6A. Please note
that each day a violation continues may be considered a separate violation, subject to additional civil
penalties.
As a result of the violations described in this Notice this office is considering a recommendation for a
civil penalty assessment to the Director of the Division. If you wish to present an explanation for the
violations cited, or if you believe there are other factors that should be considered, please send such
information to me in writing within ten (10) days following receipt of this letter. Your response will be
reviewed, and, if an enforcement action is still deemed appropriate, it will be forwarded to the Director
and included for consideration.
Should you have any questions, please call me at 704/235-2180 or contact me via email at:
andrew. pitner@ncdenr.
Sincerely,
t4,
, 11 � \\�
Andrew H. Pitner, P.G.
Environmental Program Supervisor
Enclosure: Inspection Report
Cc: Trent Tidwell, Alchem, Inc., 8135 Red Rd., Rockwell 28138
Ed Hardee, Central Office
MRO file
MAF/alchem insp & NOVNOI 2-28-11

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Beverly Eaves Purdue, Governor
Dee Freeman, Secretary
Coleen H. Sullins, Director
00
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
. Recycle/Reuse/Reclamation System
GENERAL INFORMATION
Owner: Randall Andrews County: Rowan Project Name: Alchem, Inc.
Permit No. WQ0002702 Issuance Date: Dec. 28, 2004 Expiration Date: Nov. 30, 2009
Note: Session Law 2009-406 extended this permit to 91-30-2012
Permit No. WQ0016338 Issuance Date: Dec. 28, 2006 Expiration Date: Nov. 30, 2011
Note: Session Law 2009-406 extended this permit to 11-30-2014.
Permittee Contact: Trent Tidwell, Operations Mqr. Telephone No. 704/279-7908
Reason for Inspection
ROUTINE COMPLAINT X FOLLOW-UP OTHER
Type of Inspection
Reuse System (golf course) X Recycle System
Inspection Summary: (additional comments may be included on attached pages)
Many improvements have been made to record keeping but some deficineicies still exist.
The site manager stated that ALCHEM is no longer producing alum. The permittee may want to
consider requesting a permit modification for permit WQ0002702 (Industrial recycle) to reflect these
changes to the recycle system and modify permit WQ00016338 (Bauxite residuals monofil) to
suspend spent bauxite sampling.
A protective vegetative cover is still deficient on the earthen berms of the lagoons as well as the site in
general.
Is a follow-up inspection necessary X yes _no
Inspector (s): Peggy Finley, Environmental Specialist; Ellen huffman, Environmental Specialist
Tel. No. 704/663-1699 Fax No. 704/663-6040
Date of Inspection: 2/28/11

Permit # WQ0002702 & WQ0016338 Page 2
Y-yes N-no N/A- not applicable N/E- not evaluated
Treatment
N Are treatment facilities consistent with those outlined in the current permit.
N Do all treatment units appear to be operational? If no, note below.
Comment: Alum production has apparently ceased. The piping for the mixer and the mixer itself has
been removed from the reactor. There was very little bauxite ore observed in the storage area. Spent
bauxite is present in all three lagoons. The permittee may want to consider a permit modification for
permit WO0002702 (Industrial recycle) to reflect these changes to the recycle system and modify
permit WQ00016338 (Bauxite residuals monofil) to suspend spent bauxite sampling.
Residuals Storage Lagoons (for spent bauxite)
(check any/all that apply)
Y Influent structure free of obstructions
N/A Baffles/curtains (in need of repair)
Y Freeboard minimum 2 feet
N Evidence of overflow
Y Unusual color
N Foam (are antifoam agents used)
N/A Excessive solids buildup (from bottom)
N/A Effluent structure (free of obstructions, easily accessible)
Comment: The wastewater in lagoon #3 appears to have a mustard color. Mr. Tidwell stated that this
was from adding lime. Despite efforts to establish a vegetative cover on the outer walls of the lagoons
as noted in the last inspection, they remain effectively devoid of such vegetation for erosion control.
Lagoon #1 Lagoon #2
.,
14

Permit # WQ0002702 & WQ0016333 Page 3
Residuals
Mr. Tidwell stated that, except for transfers of the slurry from one lagoon to another, residuals have
not been removed from the basins. The residuals analysis data was not available at the time of the
inspection. Reportedly, it was in the possession of Mr. Andrews.
Transport of Residuals
It was stated that no residuals have been removed from the lagoons last year or this year (January 1,
2010, to the present).
Residuals Fill Area and Storrs -water Basin
As noted in previous inspections, most of the fill area has been graded and appears to meet berm
level. A report from Delta (2009) stated that site -life has been reduced from 9.5 years to 6 years. It is
unclear why site life has been reduced. A revised site -life calculation is in order. As noted during the
last inspection, a very large amount of what appears to be fill dirt is still being stored on top of the
monofill area.
Other Site Conditions
Vegetative cover on the lagoon earthen berms and areas where runoff needs to be controlled has
been an ongoing problem and is still deficient throughout the entire ALCHEM site.
Compliance Monitoring
Groundwater monitoring required by permit WQ0002702 is currently being conducted on a triannual
schedule as part of continuing groundwater investigation for 2L violations. GW-59 reports have been
submitted in a timely manner by John Reuscher with Antea Group (formerly Delta).
Recordkeeping
Y Is the permit available upon request?
Y Are operational logs present? Y* Complete?
NE Is the operation and maintenance manual present? Complete?
N Has DWQ received any complaints regarding the facility in the last 12 months?
Comment: * Operational logs were complete but available only for activities through December 2010.
The annual report was due March 1, 2011. An extension was granted and the report was received on
March 31. Inconsistencies and deficiencies were noted in the report. The laboratory results for the
required semi-annual spent bauxite sampling were incomplete.

'i
Reporting Noncompliance
Several instances of noncompliance were uncovered that were not reported to the regional office as
required by the permits:
1. Lagoon freeboard — at least four instances of freeboard measured less than two feet were
recorded during 2010;
2. Vegetative cover on lagoon berms and bare areas continues to be deficient.
s r { ; I ZtpostaClass Mail
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UNITED STATES POSTAL SERVICE y i +; Sit No_. G-10
• Sender: Please print your name, address, andZlPt4.in''ikiis-box' .y+
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DENR DWQ Aquifer Prolec110il �; 4
610 E. Center Ave., Ste. 301
Mooresville NC 28115 i`. '•t. L
I CEATIRED MAIL,, RECEIPT
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Certified Fee \
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(Endorsement Required)
I a Total Postag
m Randall Andrews
Sent To
Ir Alchem, Inc.
I o �ffeB�'`0 2042 Buie Philadelp hus Rd.
or PO Box No.
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r` ciry sreie ziF Red Springs NC 28377

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NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor
Certified Mail
Return Receipt Requested
Mr. Randall Andrews
Alchem Incorporated
2042 Buie Philadelphus Rd.
Red Springs, NC 28377
and
Alchem Incorporated
8135 Red Road
Rockwell, NC 28138
Dear Mr. Andrews:
Director, Division of Water Quality
Subject: Information Request
WQ0002702, WQ0016338
Recycle System, Monofill
Rockwell, Rowan County
Secretary
November 3, 2010
We have received information that Alchem may have plans to sell or may have sold the alum
production part of the business or the Rockwell operation in whole; please verify this information. Know that
changes in Alchem's production operations may directly affect DWQ-permitted activities. Permits that Alchem
holds will be affected if there is a change in ownership or Permittee. Further, other conditions must be met if
Alchem plans to cease alum production.
Please address the above as soon as possible, but no later than within 15 business days of receipt of
this letter. Your cooperation in this regard is appreciated. Should you have any questions, feel free to contact
me at 704/235-2180 or via email at: Andrew. Pitner(a)ncdenr.gov.
Sincerely,
&1
Andrew H. Pitner, P.G.
Environmental Program Supervisor
Cc: MRO-APS Files
DWQ-APS Land Application Unit, Raleigh
Anita LeVeaux, Attorney General's Office, Environmental Division
Division of Water Quality f Aquifer Protection Section / Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 ' One
Phone: [phone] t Fax: [phone] t Customer Service: 1-877-623-6748 North yC,arollina
Internet: www.ncwaterqualfty.org �%tKrQ6`y
An Equal Opportunity , Affirmative A-tion Employer f�

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ALCHEM, INC.
Corporate Office
2042 Buie Philadelphus Road
Red Springs, NC 28377
Tel. [phone]— 800-522-2944
Fax [phone]
[e-mail]
June 30, 2011
Mr. Andrew Pitner
Regional Environmental Supervisor
NCDENR Division of Water Quality
Mooresville Regional Office
610 East Center Ave.
Suite 301
Mooresville, NC 28115
Dear Mr. Pitner:
Sales and Manufacturing
8135 Red Road
Rockwell, NC 28138
Tel. [phone] — 800-462-2586
Fax [phone]
[e-mail]
We have cleaned up the remaining sand at Vernon Sechrist's house in Thomasville.
Vernon took this material to the Davidson County Landfill. I am enclosing two scale
tickets.
Best regards,
ALCHEM, INC.
�44�
Randall F. Andrews,
President
ams

06/29/2011 15:41 3362422287
LANDFILL SCALEHOUSE
PAGE 02
LOP R€EA9 LAWILL
P 0 WX 1087 - 118 W 4:EITTEH ST
LEXINGTO N NC 27293-1087
Naigf d: JMIE
Dup"it. Eii.V 0
RILL To: 10M
ALMM INS
Vehicle ID:
Rehrm: SAND
Origin: 166 FANNIE P(ILLUM RD TVIL
DATE IN* 05/0912O11 TIME IN: 00:28:31
DATE OUT: 06/0912011 TIM, MT: OS:5O
I?1SM TICKET Wow 03-204249
MAWAL URM WT. 53420 LB
VAUL TART: WT. 2m LB
NET 91QHT 24020 W
Otu Dmriptico Aft
12.01 fV-MRCIAL 432.36
MT CHM ARMT: 432.36
r
LUFF MAD LWILJ
P D Box 107 - 116 w GETTER ST
L£XIMTOM NC 27293-10$7
WgWt ELLY B
BILL Tb: 10-91
AL M im
Vahlole M M1OO1
DATE 1M. 06f 1012911 Tip IN; 07-.30:16
WAIL £11iT: ' 8/10JI011 THE i i : 07,30
ThMn TIMET fir: 03-204347
rAva mm 0. 511PD L13
STORED TARE :PT. 3D220 LB
NET ME1W, 20MO L9
sty Dawri-ptim AWMt
10.45 DS*- ~RCIAL 3E6.20
WET *ME AWW, 315.2O
J, :�n - �lllzl a

Huffman, Ellen
From: Huffman, Ellen
Sent: Wednesday, April 27, 2011 1:56 PM
To: aRANDON-MCiORE',
Cc: Andrews, Rand0l -P.itner }Andrew, Huffman -_Ellen.'
Subject: extension Fannie Pullam site
Brandon,
We (MRO) received your letter dated April 15, 2011 requesting a 90 day extension for the Fannie Pullam site cleanup
(NOV-2010-PC-0940 dated August 11, 2010). Please note that the original deadline for this clean up was November 1,
2010. We gave Mr. Andrews a 90 day extension on November 24, 2011 with a new deadline of January 28, 2011.
Our office believes that Mr. Andrews has had sufficient time to complete this clean up. Mr. Andrews needs to finish this
clean up asap. Our consideration of any civil penalties associated with this violation will include the level of response
demonstrated by Alchem.
Sincerely,
Ellen Huffman
Ellen Huffman
Environmental Specialist II
North Carolina Dept. of Environment & Natural Resources
Aquifer Protection
610 East Center Avenue
Mooresville, NC 28115
Ph:704.663.1699 Fax:[phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties.

•
PARAGON
Environmental Consultants, Inc.
April 15, 2011
Andrew H. Pitner
Mooresville Regional Office - NCDENR
610 E. Center Avenue - Suite 301
Mooresville, NC 28115
Reference: Soil Remediation
Alchem Site
165 Fannie Pullum Road
Thomasville, NC
Dear Mr. Pitner:
r
_-•-.,_­ - t-
Paragon Environmental Consultants, Inc. on behalf of Alchem, Inc. would like to request
an extension for the completion of the soil remediation project at the above referenced
facility. Alchem is obtaining bids from several soil excavation contractors to perform the
removal of the sandy material that has been previously disposed at the project site. This
work is going to require a specialized plan by the selected contractor as soil must be
gathered within the treeline at this site and then transported to the upper portion of the site
in order to be loaded into a truck for off -site disposal. This may require hand -excavation
or a small excavator which can access tight confines in some areas of the property, so it
may take a few weeks to award the contract to the selected remediation company.
A meeting between Paragon and a representative of Alchem was conducted at the facility
on Thursday, April 14 in which the directives of NCDENR agents were fully explained to
the responsible parry. We believe that an extension of 90 days should allow sufficient
time to complete the required cleanup at 165 Fannie Pullum Road in Thomasville, NC.
Please contact our office at [phone] if you have any questions regarding
these activities.
Sincerely,
Brandon Moore, L.G.
Paragon Environmental Consultants, Inc.
L11-1058 .
P.O. Box 157 • Thomasville, NC
Business Ph: [phone] • Fax

Huffman, Ellen
From:
Pitner, Andrew
Sent:
Monday, March 07, 2011 1:44 PM
To:
BRANDON MOORE
Cc:
Huffman, Ellen; Randall Andrews
Subject:
RE: Alchem site in Thomasville
Hi Brandon,
We'd be happy to come out to take a look at the site together after y'all have taken a stab at removing the remainder of
Alchem's material. We're not sure how long the removal may take this time around, but perhaps you can let us know
ahead of time when it is happening and, if schedules allow, we could come up that afternoon as things wrap up or
something like that.
Please note that we specifically required that the work and final report be overseen/signed/sealed by a PG/PE to provide
confidence that the work is done properly and completely. Final DWQ response to the dumping at this location would
only come after the cleanup is fully documented, submitted, and reviewed.
Andrew
From: BRANDON MOORE [mailto:[e-mail]]
Sent: Monday, March 07, 2011 12:58 PM
To: Pitner, Andrew
Subject: Alchem site in Thomasville
mr. pitner,
would it be possible to have Ellen Huffman or another rep from NCDENR on -site during our soil removal activities or soon
after to verify the proper removal of all material
Mr. Randall Andrews has asked that we make this request to you prior to scheduling the field activities for this project
brandon moore
paragon env.

Pitner, Andrew
From: Randall Andrews [[e-mail]]
Sent: Friday, February 11, 2011 3:20 PM
To: [e-mail]
BRANDON AT PARAGON IS TAKING SOME VACATION NEXT WK. HE SAID HE WILL CALL YOU UPON HIS RETURN. I AM
GOING TO TAKE A PICTURE OF VERNON IN HIS DUMP TRUCK THAT HE USED TO CARRY THR SAND TO THE LANDFILL. HE
DID NOT CREATE A B/L. HE OWNS THIS TRUCK AND IT IS PARKED AT HIS HOUSE. THANKS.
RANDALL ANDREWS
INDUSTRIAL & AG CHEMICALS, INC.
2042 BUIE PHILADELPHUS RD
RED SPRINGS, NC 28377
PHONE: [phone] EXT.23 FAX: [phone]

PARAGON
Environmental Consultants, Inc.
January 4, 2011
Andrew H. Pitner
Mooresville Regional Office - NCDENR
610 E. Center Avenue - Suite 301
Mooresville, NC 28115
�Ct�t
JAN - 5 2011'
Reference: Sdil Remediation Assessment
Alchem Site -165 Fannie Pullum Road - Thomasville, NC
Dear Mr. Pitner:
Please find enclosed a summary of the soil remediation and sampling activities at
the above referenced location. The soil removal was performed by IAC Services,
Inc. of Red Springs, NC with supervision provided by Paragon Environmental
Consultants, Inc. of Thomasville, NC. The site activities consisted of the
excavation and disposal of twenty-eight truck loads (average load of
approximately 13 tons) of material and the collection of seven confirmatory
samples and one "background" sample in native soils at the facility. The soils
which were removed from 165 Fannie Pullum Road were transported to the
Davidson County Landfill in Lexington, NC for disposal. Attachment A contains
copies of the disposal tickets for each of the loads of soil excavated from the
subject site. Samples were collected from native soils underneath the excavated
material at depths of approximately 18 inches below land surface following the
soil removal. The seven in -situ soil samples were submitted to Meritech, Inc. for
analyses according to RCRA metals and for pH. Only Arsenic was detected
above the lowest NCDENR standard; however, Arsenic was also present in the
"background" sample labeled as BG. With the "background" Arsenic
concentration of 8.59 mg/kg subtracted from the in -situ sample results, all of the
Arsenic levels would also be below the NCDENR standard of 4.4 mg/kg. The
other RCRA metals were below the state's lowest standard for each analyzed
metal. The pH results ranged from 3.9 to 6.1 which are similar to the
"background" level of 4.3 for pH. Table 1 summarizes the laboratory analytical
results for metals and pH. Attachment B contains copies of the laboratory
analytical reports and the chain -of -custody records for the soil samples obtained
at 165 Fannie Pullum Road in Thomasville, NC.
Paragon, on behalf of Alchem, Inc., is requesting a notice of No Further Action
for this facility since all soil concentrations are below the state's standards (with
Arsenic being corrected for the "background" level) and the pH levels are no
more acidic than the surrounding native soils. Please contact our office at (336)
669-6037 if you ha,,�jeA tions regarding these activities.
Sincerely, 0�0
m
o (-
Brandon Moores < r=
Paragon Envits, Inc.
cc: Randall AC.
°1g®a¢a aeeeea�
P.O. Box 157 • Thomasville, NC 27361-0157
Business Ph: [phone] • Fax: [phone]

TABLE 1
Summary of Soil Laboratory Analytical Results
Alchem Site
Thomasville, North Carolina
All results in milligrams per kilogram (mg/kg) except for pH.
BDL= Below Detection Limits X10-1058

Attachment A
SOIL DISPOSAL TICKETS

LOPP ROAD LANDFILL
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
P 0 BOX 1067 - 116
W CENTER ST
LEXINGTON NC 27293-1087
LEXINGTON NC 27293-1067
i
Weighed: ELLY B
i Weighed: JAMIE
BILL TO; 0
BILL TO: 0
CASH CUSTOMER
CASH CUSTOMER
Vehicle ID:
Vehicle ID:
Reference: SAND
I
Reference: SAND
_
Origin: ALCHEM
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 13:18:57
DATE IN: 12/14/2010 TIME
IN: 14:35:11
DATE OUT: 12/14/2010 TIME OUT: 13:18
i
DATE OUT: 12/14/2010 TIME
OUT: 14:35
INBOUND PICKET Number: 03-189213
j
INBOUND 'TICKET Number: 03-189227
MANUAL GROSS WT. 56640 LB
MANUAL GROSS WT.
57320 LB
MANUAL TARE WT. 30220 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT 26420 LB
NET WEIGHT
27100 LB
f
QtY Description Amount
Qty Description
Amount
13.21 MSW-COMMERCIAL 475.56
13.55 MSW-COMMERCIAL
487.80
NEI' CASH AMOUNT: 475.56
NET CASH AMOUNT:
487.80
AMT. TENDERED: 475.56
AMT. TENDERED:
487.80
CHANGE AMOUNT: 0.00
CHANGE AMOUNT:
0.00
CHECK # BC7777
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 15:31:33
DATE OUT: 12/14/2010 TIME OUT: 15:31
INBOUND. TICKET Number: 03-189238
MANUAL GROSS WT. 55520 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 25300 LB
Qty Description
12.65 MSW-COMMERCIAL
NET CASH AMOUNT:
AMT. TENDERED:
CHANGE AMOUNT:
CHECK # BC7777
Amount
455.40
455.40
455.40
0.00
7& r,,20

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: 8/ALCHEM
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME
IN: 10:20:45
DATE OUT: 12/11/2010 TIME
i
OUT: 10:20
INBOUND TICKET Number:
i
03-188993
MANUAL GROSS WT.
51160 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
20940 LB
Qty Description
Amount
10.47 MSW-COMMERCIAL
376.92
NET CASH AMOUNT:
376.92
AMT. TENDERED:
376.92
CHANGE AMOUNT:
0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed. KIM G
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: 8/ALCHEM
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME
IN: 12:43:50
DATE OUT: 12/11/2010 TIME
OUT: 12:43
INBOUND TICKET Number: 03-189032
MANUAL GROSS WT.
59880 LB
MANUAL TARE WT.
.30220 LB
NET WEIGHT
29660 LB
Qty Description
Amount
14.83 MSW-COMMERCIAL
533.88
NET CASH AMOUNT:
533.88
AMT. TENDERED:
633.88
CHANGE AMOUNT:
0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293--1067
Weighed: KIM G
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: B/ALCHEM
Origin: SAND
DATE IN: 12/11/2010 TIME IN: 13:44:18
DATE OUT: 12/11/2010 TIME OUT: 13:44
INBOUND TICKET Number: 03-189047
MANUAL GROSS WT. 60480 LB
MANUAL TARE WT.' 30220 LB
NET WEIGHT 30260 LB
Oty Description Amount
15.13 MSW-COMMERCIAL 544.68
NET CASH AMOUNT: 544.68
AMT. TENDERED: 544.68
CHANGE AMOUNT: -0.00
CHECK # BC7777
J;d F G V

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 0
CASH CUSTOMER
Vehicle
ID:
Reference: B/SAND
I
Origin:
ALCHEM
DATE IN:
12/14/2010 TIME
IN: 09:47:59
DATE OUT: 12/14/2010 TIME
OUT: 09:47
INBOUND
TICKET Number:
03-169176
MANUAL GROSS WT.
56640 LB
MANUAL TARE WT.
30220 LB
i
NET WEIGHT
26420 LB
Qty
Description
Amount
13.21
MSW-COMMERCIAL
475.56
NET CASH AMOUNT:
475.56
AMT, TENDERED:
475.56
CHANGE AMOUNT:
0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 10:54:23
DATE OUT: 12/14/2010 TIME OUT: 10:54
INBOUND TICKET Number: 03•-189190
MANUAL GROSS WT. 56760 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 26540 LB
Qty Description Amount
13.27 MSW-COMMERCIAL 477.72
NET CASH AMOUNT: 477.72
AMT. TENDERED: 477.72
CHANGE AMOUNT: 0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL'TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 12:22:49
DATE OUT: 12/14/2010 TIME OUT: 12:22
INBOUND TICKET Number: 03-189207
MANUAL GROSS WT. 51680 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 21460 LB
Qty Description Amount
10.73 MSW-COMMERCIAL 386.28
NET CASH AMOUNT: 386.28
AMT. TENDERED: 386.28
CHANGE,AMOUMT: 0.00
CHECK # BC7777
-� � �,)-z

LOPP ROAD LANDFILL.
LOPP ROAD LANDFILL
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116
W CENTER ST
P 0 BOX 1067 - 116
W CENTER ST
P 0 BOX 1067 - 116
W CENTER ST
LEXINGTON NC 27293-1067
LEXINGTON NC 27293-1067
LEXINGTON NC 27293-1067
Weighed: KIM G
Weighed: ELLY B
Weighed: KIM G
BILL TO: 0
BILL T0: 0
BILL TO: 0
CASH CUSTOMER
CASH CUSTOMER
CASH CUSTOMER
Vehicle ID:
Vehicle ID:
Vehicle ID:
Reference: 8/ALCHEM
Reference: 8/TRK 01
Reference: 8/ALCHEM
Origin: SAND PO#120910
Origin: 165 FANNIE PUL.LUM
RD
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME
IN: 07:45:55
DATE IN: 12/10/2010 TIME
IN: 13:30:45
DATE IN: 12/11/2010 TIME
IN: 11:19:11
DATE OUT: 12/11/2010 TIME
OUT: 07:45
DATE OUT: 12/10/2016 TIME
OUT: 13:30
DATE OUT: 12/1112010 TIME
OUT: 11:19
L
INBOUND TICKET Number: 03-188973
INBOUND 'TICKET Number: 03-188937
INBOUND TICKET Number: 03-189012
MANUAL GROSS WT.
71840 LB
MANUAL GROSS WT,
49500 LB
MANUAL GROSS WT.
56820 LB
MANUAL TARE WT.
30220 LB
MANUAL TARE WT.
30220 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
41620 LB
NET WEIGHT
19280 LB
NET WEIGHT
26600 LB
Qty Description
Amount
Qty. Description
Amount
Qty Description
Amount`
20.81 MSW-COMMERCIAL
749.16
9.64 MSW-COMMERCIAL
347.04
13.30 MSW-COMMERCIAL
478.80
NET CASH AMOUNT:
749.16
NET CASH AMOUNT:
347.04
NET CASH AMOUNT:
478.80
AMT. TENDERED:
749.16
AMT. TENDERED:
347.04
AMT. TENDERED:
478.80
CHANGE AMOUNT:
0.00
CHANGE AMOUNT:
0.00
CHANGE AMOUNT:
0.00
CHECK # BC7777
CHECK # BC7777
CHECK # BC7777
X
X
�_

LOPP ROAD LANDFILL
P 0 BOX 1067 -- 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: JAMIE
BILL. TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: DIRT
Origin: ALCHEM
DATE IN: 12/10/2010 TIME IN: 15:41:38
DATE OUT: 12/10/2010 TIME OUT: 15:41
INBOUND TICKET Number: 03-188964
MANUAL GROSS WT. 57240 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 27020 LB
Qty Description Amount
13.51 MSW-COMMERCIAL. 486.36
NET CASH AMOUNT: 486.36
AMT. TENDERED: 486.36
CHANGE AMOUNT: 0.00
CHECK # BC7777
X
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: ELLY B
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: DIRT/01
Origin: 165 FANNIE PULLMAN RD
DATE IN: 12/10/2010 TIME IN: 14:33:11
DATE OUT: 12/10/2010 TIME OUT: 14:33
INBOUND TICKET Number: 03-188950
MANUAL GROSS WT. 60300 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 30080 LB
Q�y Description Amount
'15.04 MSW-COMMERCIAL 541.44
NET CASH AMOUNT: 541.44
AMT. TENDERED: 541.44
CHANGE AMOUNT: 0.00
CHECK # BC7777
r
X
5'7/6-3

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/17/2010 TIME IN: 14:01:16
DATE OUT: 12/17/2010 TIME OUT: 14:01
INBOUND TICKET Number: 03-189414
MANUAL GROSS WT. 57860 LB
MANUAL TARE WT, 30220 LB
NET WEIGHT 27640 LB
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
DATE IN: 12/18/2010 TIME IN: 12:13:17
DATE OUT: 12/16/2010 TIME OUT: 12:13
INBOUND TICKET Number: 03-189472
MANUAL GROSS WT. 57280 LB
STORED TARE WT. 30226 ALB
NET WEIGHT 27060 LB
Qty Description Amount Qty Description Amount
13.82 MSW-COMMERCIAL 497.52 13.53 MSW-COMMERCIAL 487.08
NET CASH AMOUNT: 497.52 NET CHARGE AMOUNT: 487.0E
AMT. TENDERED: 497.52
CHANGE AMOUNT: 0.00
CHECK # BC7777
qo 0

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
I
DATE IN: 12/18/2010 TIME IN: 08:43:14
i DATE OUT: 12/18/2010 TIME OUT: 08:43
INBOUND TICKET Number: 03,-189432
MANUAL GROSS WT. 57480 LB
STORED TARE WT. 30220 LB
i
NET WEIGHT 27260 LB
Oty Description Amount
13.63 MSW-COMMERCIAL 490.68
NET CHARGE AMOUNT: 490.68
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
DATE IN: 12/18/2010 TIME IN: 09:45:32
DATE OUT: 12/18/2010 TIME OUT: 09:45
INBOUND TICKET Number: 03-189442
MANUAL GROSS WT. 57880 LB
STORED TARE WT. 30220 LB
NET WEIGHT 27460 LB
Oty Description Amount
13.73 MSW-COMMERCIAL 494.28
NET CHARGE AMOUNT: 494.28
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference; SAND
DATE IN: 12/17/2010 TIME IN: 11:14:24
DATE OUT: 12/17/2010 TIME OUT: 11:14
INBOUND TICKET Number: 03-189378
MANUAL GROSS WT.. 57520 LB
STORED TARE WT. 30220 LB
NET WEIGHT 27300 LB
Oty Description Amount
13.65 MSW-COMMERCIAL 491.40
NET CHARGE AMOUNT: 491.40

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 1061
iALCHEM INC
Vehicle ID: 1061001
iReference: SAND
DATE IN: 12/17/2010 TIME IN: 10:14:47
DATE OUT: 12/17/2010 TIME OUT: 10:14
i
INBOUND TICKET Number: 03-189366
MANUAL GROSS WT. 53880 LB
STORED TARE WT. 30220 LB
NET WEIGHT 23660 LB
i
aty Description Amount
11.83 MSW-COMMERCIAL 425.88
NET CHARGE AMOUNT: 425.88
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle
ID:
Reference: 8/SAND
Origin:
SAND
DATE IN:
12/15/2010 TIME
IN: 08:09:50
DATE OUT: 12/15/2010 TIME
OUT: 08:09
INBOUND
TICKET Number:
03-189246
MANUAL GROSS WT.
55720 LB
MANUAL. TARE WT.
30220 LB
NET WEIGHT
25500 LB
Oty
Description
Amount
12.75
MSW-COMMERCIAL
459.00
NET CHARGE AMOUNT:
459.00
X
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: B/SAND
Origin: SAND
DATE IN: 12/15/2010 TIME IN: 09:49:05
DATE OUT: 12/15/2010 TIME OUT: 09:49
INBOUND TICKET Number: 03-189255
MANUAL GROSS WT. 57840 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 27620 LB
Oty Description Amount
13.81 MSW-COMMERCIAL 497.16
NET CHARGE AMOUNT: 497.16

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 2.7293-1067
Weighed: KIM G -
BILL TO: 1061
ALCHEM INC
I Vehicle ID:
Reference: 8/SAND
Origin: SAND
DATE IN: 12/15/2010 TIME IN: 10:50:45
DATE OUT: 12/15/2010 TIME OUT: 10:50
INBOUND TICKET Number: 03-189265
MANUAL GROSS WT. 54080 LB
MANUAL TARE WT. 3022.0 LB
NET WEIGHT. 23860 LB
Qty Description Amount
11.93 MSW-COMMERCIAL 429.48
NET CHARGE AMOUNT: 429.48
LOPP ROAD LANDFILL.
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1087
Weighed: Sherri
BILL.TO: 1061
ALCHEM INC
Vehicle ID:
Reference: CONT. SAND
Origin: . CONTAMINATED SAND
DATE IN: 12/15/2010 TIME IN: 13:54:22
i DATE OUT: 12/15/2010 TIME OUT: 13:54
INBOUND TICKET Number: 03-189301
i
MANUAL GROSS WT. 56280 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 26060 L.B
Qty Description Amount
13.03 MSW-COMMERCIAL 469.08
NET CHARGE. AMOUNT: 469.08
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: 8/SAND
DATE IN: 12/15/2010 TIME IN: 12:40:07
DATE OUT: 12/15/2010 TIME OUT: 12:40
INBOUND TICKET Number: 03-1892B6
MANUAL GROSS WT. 66200 LB
MANUAL TARE WT. 30220 L.B
NET WEIGHT 25980 LB
Qty Description Amount
12.99 MSW-COMMERCIAL 467.64
NET CHARGE AMOUNT: 467.64

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116
W CENTER ST
LEXINGTON NO 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
i
Vehicle ID:
j Reference. 8/SAND
i
Origin: SAND
DATE IN: 12/15/2010 TIME
IN: 14:56:03
DATE OUT: 12/15/2010 TIME
OUT: 14:56
INBOUND TICKET Number: 03-1B9307
I
I
MANUAL GROSS WT.
51620 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
i
21400 LB
Qty Description
Amount
10.70 MSW-COMMERCIAL
385.20
NET CHARGE AMOUNT:
385.20
LOPP ROAD LANDFILL.
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: JAMIE
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/15/2010 TIME
IN: 15:52:36
DATE OUT: 12/15/2010 TIME
OUT: 15:52
INBOUND TICKET Number: 03-189313
MANUAL GROSS WT.
58740 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
28520 LB
Qty ...Description
Amount
14.26 MSW-COMMERCIAL
513.36
NET CHARGE AMOUNT:
513.36
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: ELLY B
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
DATE IN: 12/17/2010 TIME IN: 09:12:03
DATE OUT: 12/17/2010 TIME OUT: 09:12
INBOUND TICKET Number. 03-189358
MANUAL GROSS WT, 57240 LB
STORED TARE WT. 30220 LB
NET WEIGHT 27020 LB
Qty Description Amount
13.51 MSW-COMMERCIAL 486.36
NET CHARGE AMOUNT: 486.36
X
1 4/

Attachment B
SOIL ANALYTICAL RESULTS

: Meritech, Inc.
Environmental Laboratory
' Laboratory Certification No.165
Contact: Mr. Brandon Moore Report Date: 12/21/10
Client: Paragon Environmental Consultants Date Sample Rcvd: 12/13/10
PO# P-1058A
Project # Alchem Project
Meritech Work Order #
12131009 Sample: SS-1
12/13/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Barium, total
24.2 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 0.116 mg/kg
12/14/10
0.116 mg/kg
EPA 200.7
Chromium, total
56.7 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Lead, total
1.92 mg/kg
12/14/10
5.79 mg/kg
EPA 200.7
Mercury, total
< 0.0119 mg/kg
12/15/10
0.0119 mg/kg
EPA 200.7
Selenium, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Silver, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
pH
4.3 S.U.
12/13/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12131010
Sample: SS-2
12/13/10
Parameters
Result
Analysis Date Reporting Limit
Method
Arsenic, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Barium, total
12.0 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 0.16 mg/kg
12/14/10
0.160 mg/kg
EPA 200.7
Chromium, total
14.8 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Lead, total
2.23 mg/kg
12/14/10
5.79 mg/kg
EPA 200.7
Mercury, total
< 0.0115 mg/kg
12/15/10
0.0115 mg/kg
EPA 200.7
Selenium, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Silver, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
pH
5.0 S.U.
12/13/10
1.0-14.0 S.U.
SM 4500 S D
I hereby certify that I have reviewed and approve these data.
- n/z��
aboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#
Phone:
Client: PA men m*um, nx Fax: % % `� %:; i 5
PCAddress:
MER/TEe" LJ INC.
,:
ENVIRONMENTAL LABORATORIES
P.O. Box157
Tho�3M�"9-6037361 Email:
ice �+ 4
e A Division of Water Technology and Controls, Inc.
Project # �' �� / :� e c
P. O. # { 4,
Phone: [phone]
Turn Around Time*
642 Tamco Rd. Fax: 1=336-342-1522
*RUSH work must have prior approval.
Reidsville, NC 27320 Email: [e-mail]
Web Site:.www.merltech-labs.ciorn
f Std (10 days) 3 5 Day 24-48 Hr
Attention: %
a °7 o' �_ , //o �,- e
Sample Sampling Dates &Times
FeKsonTaktrti Sarri" Si nature : '�- 1/� - . Required Lab Use
^' !ti- Method Only
i_Ocation/lD # START END
Date Time Date Time
Comp? #of 200.8/200.7 pH OK?
Grab? conts. Tests Required
C120K?
_ Pl/
,.P%
J
^
�Jr S.�t�/e.Z
..`:. 5 5
% {
/�
'
f/- //r � f�/
cal �"`•'Q. ot.
.
L.
15 i_(.: -._ 5
Compositor #
***Dechlorination-(<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples. must be done in the field prior to preservation.***
Comments:
Jug #
Method of shipment:
Are these results for regulatory purposes?
Report results in
❑ _UPS-:x,a
YES ❑ NO ❑
mg/L ❑ mg/Kg ❑ µg/L ❑
On Ice? i � "'
/
,..
Temperature On Receipt �
p p
❑ Fed EX
Relm p}shed by Date Time
/
--Received by ` _ / Date i Time
Relin ished b
qt� Y E% Date Time
Received by Date Time
Hand Delivery
❑ Other
i
'
Relinquished by Date Time
Received at labbyDate Time

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Pg1of3
Contact: Mr. Brandon Moore Report Date: 12/29/10
Client: Paragon Environmental Consultants Date Sample Rcvd: 12/20/10
PO# P-1058B
Project # Alchem Project
Meritech Work Order #
12201045 Sample: SS-3
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
11.2 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
54.6 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.37 mg/kg
12/23/10
1.37 mg/kg
EPA 200.7
Chromium, total
45.9 pig/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 6.86 mg/kg
12/23/10
6.86 mg/kg
EPA 200.7
Mercury, total
0.0549 mg/kg
12/29/10
0.0010 mg/kg
EPA 200.7
Selenium, total
< 6.86 mg/kg
12/23/10
6.86 mg/kg
EPA 200.7
Silver, total
< 3.43 mg/kg
12/23/10
3.43 mg/kg
EPA 200.7
pH
4.3 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12201046 Sample: SS-4
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
6.90 mg/kg
12./23/10
1.00 mg/kg
EPA 200.7
Barium, total
34.6 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.31 mg/kg
12/23/10
1.31 mg/kg
EPA 200.7
Chromium, total
32.3 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 6.57 mg/kg
12/23/10
6.57 mg/kg
EPA 200.7
Mercury, total
0.0263 mg/kg
12/29/10
0.0010 mg/kg
EPA 200.7
Selenium, total
< 6:57 mg/kg
12/23/10
6.57 mg/kg
EPA 200.7
Silver, total
< 3.29 mg/kg
12/23/10
3.29 mg/kg
EPA 200.7
pH
3.0 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
642 Tamco Road, Reidsville,. North Carolina 27320
tel.(336)342=4748 fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Pg2of3
Contact: Mr. Brandon Moore Report Date: 12/29/10
Client: Paragon Environmental Consultants Date Sample Rcvd: 12/20/10
PO# P-1058B
Project # Alchem Project
Meritech Work Order #
12201047
Sample: SS-5
12/18/10
Parameters
Result
Analysis Date Reporting Limit
Method
Arsenic, total
9.63 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
29.2 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.20 mg/kg
12/23/10
1.20 mg/kg
EPA 200.7
Chromium, total
65.7 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 5.98 mg/kg
12/23/10
5.98 mg/kg
EPA 200.7
Mercury, total
< 0.0120 mg/kg
12/29/10
0.0120 mg/kg
EPA 200.7
Selenium, total
< 5.98 mg/kg
12/23/10
5.98 mg/kg
EPA 200.7
Silver, total
< 2.99 mg/kg
12/23/10
2.99 mg/kg
EPA 200.7
pH
5.2 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12201048 Sample: SS-6
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
16.5 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
20.3 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.18 mg/kg
12/23/10
1.18 mg/kg
EPA 200.7
Chromium, total
63.8 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 5.88 mg/kg
12/23/10
5,88 mg/kg
EPA 200.7
Mercury, total
< 0.0118 mg/kg
12/29/10
0.0.118 mg/kg
EPA 200.7
Selenium, total
< 5.88 mg/kg
12/23/10
5.88 mg/kg
EPA 200.7
Silver, total
< 2.94 mg/kg
12/23/10
2.94 mg/kg
EPA 200.7
pH
5.6 S U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
es
Pg3 of
Contact: Mr. Brandon Moore Report Date: 12/29/10
Client: Paragon Environmental Consultants Date Sample Rcvd: 12/20/10
PO# P-1058B
Project # Alchem Project
Meritech Work Order #
12201049 Sample: SS-7
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
10.3 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
24.4 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.18 mg/kg
12/23/10
1.18 mg/kg
EPA 200.7
Chromium, total
44.6 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 5.92 mg/kg
12/23/10
5.92 mg/kg
EPA 200.7
Mercury, total
< 0.0118 mg/kg
12/29/10
0.0118 mg/kg
EPA 200.7
Selenium, total
< 5.92 mg/kg
12/23/10
5.92 mg/kg
EPA 200.7
Silver, total
< 2.96 mg/kg
12/23/10
2.96 mg/kg
EPA 200.7
pH
6.1 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order # 12201050 Sample: BG 12/18/10
Parameters Result Analvsis Date Reportine Limit Method
Arsenic, total
8.59 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
45.0 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.27 mg/kg
12/23/10
1.27 mg/kg
EPA 200.7
Chromium, total
15:1 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 6;36 mg/kg
12/23/10
6.36 mg/kg
EPA 200.7
Mercury, total
< 0.0127 mg/kg
12/29/10
0.0127 mg/kg
EPA 200.7
Selenium, total
< 6.36 mg/kg
12/23/10
6.36 mg/kg
EPA 200.7
Silver, total
< 3.18 mg/kg
12/23/10
3.18 mg/kg
EPA 200.7
pH
4.3 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
I herebycertify that I have reviewed and approve these data.
IY rr .
Laboratory Representative
642 Tameo Road; Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
'
Client: � 13
NPDES1t L
Fax Phone:336 y%�' %70 9
MERI TECH, INC. C.
w E '
e ENVIRONMENTAL LABORATORIES
Address:
En�� coo seditntt, mr-
p,p, Box 157
`"°,3;�166 603 "�'
Email:
Project # /G /a�jec�
p A Division of Water Technology and Controls, Inc.
r
P-/D s8
- ` Phone: [phone]
642 Tamco Rd. Fax: [phone]
P. o. # ,6
Turn Around Time*
Reidsville, NC 27320 Email: [e-mail]
*RUSH work must have prior approval.
Web Site: www.meritech-labs.com
a�
Attention: �' oll /Sa
Std (10 days) 3 - 5 Day 24 48 Hr
Fpl Sampling Dates & Times
Person Takin Sam e Si nature :
Required Lab Use
Locatl4 START END
_ _ "_F Date Time Date Time
Comp?
Grab?
# of
cants. Tests Required
Method Only
200.8 / 200.7 PH OK?
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Compositor #
***Deck'ri ation (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation.***
Jug #
Comments:
Method
of Shipment:
Are these results for regulatory purposes?
YES [J
Report results in
On Ice?
L
UPS
NO
mg/L
mg/Kg, µg/L
Temperature On Receipt :
❑ Fed Ex
Relinquished by
Date
Time Receiv b
Date Time
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fv

'ILE,
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Colleen H. Sullins Dee Freeman
Governor Director, Division of Water Quality Secretary
February 8, 2011
Certified Mail
Return Receipt Requested
Mr. Randall Andrews
Alchem Incorporated
2042 Buie Philadelphus Rd.
Red Springs, NC 28377
and
Alchem Incorporated
8135 Red Road
Rockwell, NC 28138
Subject: Review of Soil Remediation Assessment Report
ALCHEM Site 165 Fannie Pullam Road
Thomasville, Davidson County, NC
For NOV-2010-PC-0940
Permits WQ0002702, WQ0016338
Recycle System, Monofill
Rockwell, Rowan County
Dear Mr. Andrews:
We received the report from Paragon Environmental Consultants, Inc. for the subject site on January 5,
2011. The report has been reviewed and placed on file at the Mooresville Regional Office (MRO). Based on our
review of the report, it did not include information requested in the subject Notice of Violation to document the
cleanup of the Fannie Pullam site and additional information will need to be submitted.
Please note that a site visit on January 25, 2011, by MRO staff concluded that the cleanup is incomplete.
The following items will need to be addressed in another report:
• A pile of Alchem material was missed directly behind the on -site home; it appears to have been used
as a loading ramp. Other areas of the site also had noticeable amounts of Alchem's spent bauxite
dispersed throughout (see attached photos).
• There was no assessment/discussion of potential damages to soil, groundwater and/or surface
water. Are pH levels consistent with mapped soils? Was any lime applied? Were areas re -seeded?
• No photos of before and after clean up were submitted with the report.
• No map was provided identifying the extent of the cleanup. No map was submitted indicating the
locations of the confirmatory soil samples and the background sample location.
• No list of companies or persons hired for the clean-up activity was provided (i.e. trucking company,
etc.), and no load transportation documentation (trucking/hauling bills) was provided.
A report documenting the remaining cleanup as well as the above items is due in this office no later than
March 11, 2011.
Division of Water Quality I Aquifer Protection Section I Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 One
Phone: [phone] Fax: [phone] Customer Service:1-877-623-6748 North,Carohiia
Internet: www.navaterquality.org 1+�"�
An Equal Opportunity 1 Affirmative Action Employer !� d %1,��U6

Alchem clean-up_report response
February 8, 2011
Should you have any questions, feel free to contact me at 704/235-2180 or via email at:
Andrew. Pitner(cDncdenr.gov.
Sin erely,
Andrew H. i ner, P.G.
Environmental Program Supervisor
Attachment
Cc: Brandon Moore, Paragon Environmental Consultants, Inc.
MRO-APS Files
DWQ-APS Land Application Unit, Raleigh
Anita LeVeaux, Attorney General's Office, Environmental Division

I"
FILE
MCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen.H. Sullins Dee Freeman
Governor Director, Division of Water Quality Secretary
November 24, 2010
Certified Mail
Return Receipt Requested
Mr. Randall Andrews
Alchem Incorporated
2042 Buie Philadelphus Rd.
Red Springs, NC 28377
and
Alchem Incorporated
8135 Red Road
Rockwell, NC 28138
Subject: Extension Request
NOV-2010-PC-0940
WQ0002702, W00016338
Recycle System, Monofill
Rockwell, Rowan County
Dear Mr. Andrews:
We received your signed response letters on November 7, 2010. The letters contained the basic information
on your plan to address the dumping that we had requested be submitted in August. Though your letters arrived as
unsigned attachments by email before the cleanup deadline of November 1, 2010, which was established in the
subject NOV, it is our current understanding that cleanup activities have yet to occur. The Division of Water Quality
is troubled by the continued apparent lack of concern demonstrated by Alchem's slow response.
One of your letters requests an extension of 90 days to complete the cleanup work and to submit the final
report assessing any environmental damages that may have resulted from the dumping conducted by Alchem. As a
result of extenuating circumstances outlined in your correspondence, an extension will be granted and the work will
have to be completed with all analysis and reporting outlined in the subject NOV to be submitted to this office no
later than January 28, 2011. Please note that failure to comply in the manner and time specified may result in the
assessment of additional civil penalties.
Should you have any questions, feel free to contact me at 704/235-2180 or via email at:
Andrew. Pitner�ncdenraov.
Sincerely,
Andrew H. Pitner, P.G.
Environmental Program Supervisor
Cc: MRO-APS Files
DWQ-APS Land Application Unit, Raleigh
Anita LeVeaux, Attorney General's Office, Environmental Division
Division of Water Quality / Aquifer Protection Section I Mooresville Regional Office T�TOne
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 NorthCarolina
Phone: [phone] Fax: [phone] Customer Service: 1-877-623-6748 Ndful"allY
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer

ALCHEM, INC.
r Corporate Office
2042 Buie Philadelphus Road
Red Springs, NC 28377
Tel. 9io-843-2121 — 8o0-522-2944
Fax 9io-843-5789
[e-mail]
October 27, 2010
Mr. Andrew Pitner
Regional Environmental Supervisor
NCDENR Division of Water Quality
Mooresville Regional Office
610 East Center Ave.
Suite 301
Mooresville, NC 28115
NOV-2010-PC-0940
Permit #: WQ0002702, WQ0016338
Dear Mr. Pitner:
Sales and Manufacturing
8135 Red Road
Rockwell, NC 28138
Tel. [phone]o8 — 800-462-2586
Fax [phone]
[e-mail]
vi
NOV - 8 2010
I went by to see Vernon Sechrist in Thomasville again. I have decided to ask Vernon to
dig the sand out and transport it to the Davidson County Landfill. Vernon has a front end
loader and a dump truck. At some point we will need to bring in our track hoe to dig the
material out of the ground. Until we get into this we will not know how much is there.
Vernon said that he does not know how many trucks delivered the sand. Vernon was told
by Robert Wolcott and Greg Gallimore that there was nothing wrong with the sand. He
was conned by Robert Wolcott just like me. Vernon is going into the hospital in
Salisbury today for back surgery. I would like to ask for a 90 day extension from you to
complete this work. It took much longer than I had believed to get everything approved
by the Davidson County Landfill and driving to Thomasville to work with Vernon on
how we are going to accomplish all of this. I had never heard of Vernon until I received
your letter.
Best regards,
ALCHEM, INC.
Randall F. Andrews,
President
F001.'1

ALCHEM, INC.
+ Corporate Office
2042 Buie Philadelphus Road
Red Springs, NC 28377
Tel. 9io-843-2121 — 800-522-2944
Fax 9io-843-5789
[e-mail]
October 27, 2010
Mr. Andrew Pitner
Regional Environmental Supervisor
NCDENR Division of Water Quality
Mooresville Regional Office
610 East Center Ave.
Suite 301
Mooresville, NC 28115
NOV-2010-PC-0940
Permit #: WQ0002702, WQ0016338
Dear Mr. Pitner:
Sales and Manufacturing
8135 Red Road
Rockwell, NC 28138
Tel. [phone] — 800-462-2586
Fax [phone]
[e-mail]
This is a formal response to your letter about the sand at Thomasville. I have not been
able to determine how much is there. I cannot find any records that show it was trucked
to Thomasville. An employee thought that he knew who trucked it. I asked him to ask
that person how many truckloads were transported. The answer I got back was that Jason
Desiato and Robert Wolcott are both low-lifes and this man hoped that the next thing he
heard or saw of them was their obituary in the newspaper.
I am guessing that there is 100-150 tons. When we dig it out and take it to the landfill we
will know. You have asked that we do some soil sampling after that and get the PG to
look at this and give us his opinion. After that is done we will lime and fertilize and seed
the area and do the best we can to restore it. I hope this is 11-Lat you needi will call you
shortly about this.
Best regards,
ALCHEM, INC.
Randall F. Andrews,
President
ams

Huffman, Ellen
From: LeVeaux, Anita [[e-mail]]
Sent: Monday, November 01, 2010 9:55 AM
To: Huffman, Ellen
Subject: RE: It's official randall sold
Interesting. What next???
-----Original Message -----
From: Huffman, Ellen[mailto:[e-mail]]
Sent: Monday, November 01, 2010 9:49 AM
To: LeVeaux, Anita
Cc: Pitner, Andrew; Finley, Peggy
Subject: FW: It's official randall sold
I got this text msg from Bob Wolcott.
-----Original Message -----
From: [e-mail] [mailto:[e-mail]]
Sent: Monday, November 01, 2010 9:46 AM
To: Huffman, Ellen
Subject: FWD: It's official randall sold
FWD: It's official randall sold all remain alum accts to gen chem for 750k. deal went down
yesterday. Gen chem is a Nj based co With plants in Hopewell va and catawba sc. Don't know if
property and eQuipment went with it.
C
N
E
f
E
O
U
C
CU
a
1

"W
Huffman, Ellen
From: Pitner, Andrew
Sent: Wednesday, October 27, 2010 3:51 PM
To: Huffman, Ellen; Finley, Peggy
Subject: FW: I MG00980-20100622-1625.jpg
Attachments: IMG00980-20100622-1625.jpg
At least he waited until the afternoon to share the F-bomb from Bob from June....
-----Original Message -----
From: RANDALL ANDREWS [mailto:[e-mail]]
� Sent: Wednesday; October 27;_ 2®16 _3:45_ PMI
To: Pitner, Andrew
Subject: FW: IMG00980-20100622-1625.jpg
PART OF THE REASON I HAVE SO MUCH TROUBLE FINDING OUT ANYTHING IS I AM DEALING WITH A NUT
CASE. THIS CAME FROM ROBERT6. I DO NOT KNOW EXACTLE WHAT IT MEANS BUT I ASSUME THAT IT IS A
THREAT.
-----Original Message -----
From: [e-mail] [mailto:[e-mail]]
�Sent:_Tuesday, Tune 22, 2016 4:57 P
To: [e-mail]
Subject: IMG00980-20100622-1625.jpg
Embezzlement. FUCK YoU I MADE U FUCKIN MILLiONS. Naw ask your self how much of soloman do I
really have randall? Your going to be really suprised my friend !!!
Sent from my Verizon Wireless B1ackBerry
1

Huffman, Ellen
From: Pitner, Andrew
Sent: Wednesday, October 27, 2010 3:52 PM
To: Huffman, Ellen; Finley, Peggy
Subject: FW: IMG00982-20100622-1626.jpg
Attachments: IMG00982-20100622-1626.jpg
And another...
-----Original Message -----
From: RANDALL ANDREWS [mailto:[e-mail]]
Sent : We.dnes_day_,_Octo�r 27, 2010 3 :47 PM
To: Pitner, Andrew
Subject: FW: IMG00982-20100622-1626.jpg
MORE WORK FROM ROBERT. AGAIN I REALLY CAN NOT TELL WHAT IT MEANS. I ASSUME ROBERT WILL PUT ME
IN JAIL FOR 10-15 YEARS IF I CONTINUE WORKING WITH SGT.
OWENS AT ROWAN COUNTY SHERIFF. RANDALL.
-----Original Message -----
From: [e-mail] [mailto:[e-mail]]
S_ent_: T_ u�esday, Ju_ ne 22-, 2910 4: 55TPM-
To: [e-mail]
Subject: IMG00982-20100622-1626.jpg
I'll let the state and feds handle you. You just had to keep coming! So I will do 1 year you
and julia will do 10-15 I told you I will not loose you attack my wife my kids my brother, my
dad, everything they know sand mines, off shore account, erline calvin trent charlie tim Sent
from my Verizon Wireless B1ackBerry
1

FT
INITIAL ABATEMENT REPORT '3i # � i
s'a U JUL 1 8 2011 ;
ALCHEM SITEu��a
165 FANNIE PULLAM ROAD -
THOMASVILLE, NORTH CAROLINA
JULY 159 2011
RESPONSIBLE PARTY:
Alchem, Inc.
2042 Buie Philadephus Road
Red Springs, NC 28377
Phone Number: [phone]
PROPERTY OWNER:
Vernon Sechrist
165 Fannie Pullam Road
Thomasville, NC 27360
Phone Number Not Available
CONSULTANT:
Paragon Environmental Consultants, Inc.
P. O. Box 157
Thomasville, NC 27361-0157
Phone Number: [phone]
The Soil Contamination Report for this site has been prepared by Paragon Environmental
Consultants, Inc. under the direct supervision of a licensed geologist. All activities
performed on this project were conducted under my direct supervision:
CAR .°11
�� ' ENg
1•
SEAL
1666
F0L0G\5•'� �v
Brandon Moore, L.G.
North Carolina License #1666

A
PARAGON
I X Environmental Consultants, Inc.
July 15, 2011
Randall Andrews
Alchem, Inc.
2042 Blue Philadelphus Road
Red Springs, NC 28377
Reference: Initial Abatement Report
Alchem Property
165 Fannie Pullam Road
Thomasville, North Carolina
Dear Mr. Andrews:
In accordance with a correspondence dated February 8, 2011 from the Mooresville
Regional Office of NCDENR, contained herein is an Initial Abatement Report for the
above referenced facility. These activities have been conducted following the
unauthorized surface disposal of bauxite material from Alchem's facility in Rockwell,
NC. The soil remediation consisted of the excavation and disposal of approximately 285
cubic yards of bauxite material and confirmatory sampling of in -situ soils and surface
water.
Mr. Andrews, if you have questions regarding this report please contact our office.
Sincerely,
Brandon Moore, L.G.
Paragon Environmental Consultants, Inc.
;cc Andrew II''P�tner, P GM- P�[ooresvifie Regioiii o_fMA-1.1w1CD�EIdR
RII-1058
P.O. Box 157 • Thomasville, NC 27361-0157
Business Ph: [phone] • Fax: [phone]

TABLE OF CONTENTS
Section
B. Site History
1. Introduction..........
2. Scope of Services.
Page
................................................... 1
.......:........................................... 1
C. Site Investigation
1. Excavation and Sample Collection ................................ 1
2. Soil Disposal.................................................................. 2
3. Conclusions and Recommendations .............................. 3
D. Figures
Figure 1: Project Location
Figure 2: Site Layout and Soil Sample Locations
E. Tables
Table 1: Summary of Soil Laboratory Analytical Results
Table 2: Summary of Water Laboratory Analytical Results
F. Appendices
Appendix A: Soil Analytical Results
Appendix B: Water Analytical Results
Appendix C: Soil Disposal Weight Tickets

INITIAL ABATEMENT REPORT
Alchem Site
65 Fannie Pullum Road
Thomasville, North Carolina
B. Site History
1. Introduction
In August of 2010 a N.O:V. was issued to Alchem notifying them that some bauxite
material had been transported and disposed in an improper location behind a residence
located at 165 Fannie Pullum Road in Thomasville, NC. The location of the project site
is illustrated in Figure 1. The North Carolina Department of the Environment and
Natural Resources (NCDENR) directed Alchem to remove their material and transport it
to a Subtitle D landfill. Following receipt of the NCDENR notification, Paragon
Environmental Consultants, Inc. was contracted by Alchem, Inc. to supervise the soil
remediation activities and conduct confirmatory soil sampling and laboratory analyses in
the subject area of the property at 165 Fannie Pullum Road. Contained herein is a
summary of activities which were completed at the project site.
2. Scope of Services
This Initial Abatement Report contains documentation concerning the following activities
which have been conducted at this facility:
o Excavation of bauxite soil performed by IAC Services, Inc. of Red Springs, NC
and Alchem, Inc. of Rockwell, NC
Transportation of contaminated soil by IAC Services, Inc. and Vernon Sechrist,
property owner, to the Lopp Road Landfill in Lexington, NC for final disposal
o Collection of samples from in -situ soils and collection of a surface water sample
by Paragon Environmental
o Laboratory analyses of samples conducted by Meritech, Inc. of Reidsville, NC
C. Site Investigation
Excavation and Sample Collection
The soil removal was performed by both IAC Services, Inc. of Red Springs, NC and
Alchem personnel from Rockwell, NC with supervision provided by Paragon
Environmental Consultants, Inc. of Thomasville, NC. Between December 13 and 17,
2010 approximately 269 cubic yards (372.52 tons) of bauxite material were removed
from the upper tier in the primary disposal area.
Page - 1

Following a site inspection by agents from the NCDENR, another 16 cubic yards (22.46
tons) of soil were removed from the subject site on June 9 and 10, 2011. The majority of
the material removed in June of 2011 was excavated from the lower tier within the tree
line which was where surface runoff had washed the bauxite down the slope and into the
wooded area.
Following the soil excavation at the subject site, Paragon collected seven confirmatory
samples and one "background" sample from the in -situ soils at the facility. Samples were
collected from native soils underneath the excavated material at depths of approximately
18 inches below land surface following the soil removal. The seven in -situ soil samples
were submitted to Meritech, Inc. for analyses according to RCRA metals and for pH.
Only Arsenic was detected above the lowest NCDENR standard; however, Arsenic was
also present in the "background" sample labeled as BG. With the "background" Arsenic
concentration of 8.59 mg/kg subtracted from the in -situ sample results, all of the Arsenic
levels would also be below the NCDENR standard of 4.4 mg/kg. The other RCRA
metals were below the state's lowest standard for each analyzed metal. The pH results
ranged from 3.9 to 6.1 which are similar to or even more neutral than the "background"
level of 4.3 for pH. Figure 2 illustrates the locations of the soil samples, and Table 1
summarizes the soil laboratory analytical results for metals and pH. Appendix A contains
copies of the laboratory analytical reports and the chain -of -custody records for the soil
samples obtained at 165 Fannie Pullum Road in Thomasville, NC.
One water sample was also obtained as directed by NCDENR from a surface water
collection area immediately below the main soil remediation location. This water sample
was obtained on April 11, 2011 and was immediately submitted to Meritech, Inc. for
analyses for RCRA metals and for pH. The water sample showed a pH of 6.2 which is
essentially neutral with regards to acidity. Several metals were detected in the surface
water sample at concentrations below the state's action levels. Figure 2 depicts the
location of this sample, and the analytical results for the water sample are summarized in
Table 2. Appendix B contains a copy of the laboratory analytical report and the chain -of -
custody record for the water sample from 165 Fannie Pullum Road.
2. Soil Disposal
A total of approximately 285 cubic yards (394.98 tons) of bauxite material were removed
during the site remediation activities at the Alchem site in Thomasville, NC. All of the
excavated material was transported by Vernon Sechrist and by IAC Services, Inc. to the
Lopp Road Landfill in Lexington, NC for proper disposal as directed by the NCDENR.
Copies of the soil disposal weight tickets from the landfill documenting each load of soil
are contained as Appendix C.
Page - 2

3. Conclusions and Recommendations
3. A Conclusions
The soil remediation activities at the Alchem site at 165 Fannie Pullum Road in
Thomasville, NC have been completed. From a review of all information gathered during
this removal project, Paragon Environmental Consultants, Inc. makes the following
conclusions:
Laboratory results for sampling of in -situ soils and of surface water were below
the NCDENR action levels for RCRA metals. No significant impact to pH has
occurred based on the sample results when compared to the "background" pH
level reported for the subject site.
A total of 394.98 tons of bauxite were removed from 165 Fannie Pullum Road in
Thomasville, NC during this soil remediation project. All of the excavated
material was transported to the Lopp Road Landfill in Lexington, NC for proper
disposal.
3. B. Recommendations
Based upon a review of all information gathered during the Initial Abatement activities,
Paragon makes the following recommendations:
o A notice of No Further Action should be issued for this facility since all soil
concentrations are below the state's standards (with Arsenic being corrected for
the "background" level) and the pH levels are no more acidic than the surrounding
native soils.
A copy of this report should be forwarded to the following address:
Mooresville Regional Office of NCDENR — Aquifer Protection
610 E. Center Avenue — Suite 301
Mooresville, NC 28115
3. C. Limitations
This report has been prepared for the exclusive use of Alchem, Inc. for the specific
application to the referenced site located in Davidson County, North Carolina. The
assessment was conducted based on the scope of work and level of effort desired by the
client. Our findings have been developed in accordance with generally accepted
standards in the practice of soil remediation projects, available information, and our
professional judgment. No other warranty is expressed or implied.
The data presented in this report are indicative of conditions that existed at the precise
locations sampled and at the time the samples were collected. Additionally, the data
obtained from the samples would be interpreted as meaningful with respect to the
parameters indicated in the laboratory reports. No additional information can be logically
inferred from this data.
Page - 3

FIGURES

-n
0
C
m
N
5CALE: 1'=30' 1 TITLE: PROJECT: CLIENT: PARAGON
DATE: 7/BM SITE LAYOUT AND SOIL RE MEDIATION ALCHEM, INC. I ENVIRONMENTAL
OWN. BY. KBM SOIL SAMPLE LOCATIONS 165 FANNIE PULLAM ROAD RED SPRINGS. NC I CONSULTANTS, INC.
DWG. NO. LII-1058 THOMASVILLE, NC THOMASVILLE. NORTH CAROL INA

TABLES

TABLE I
Summary of Soil Laboratory Analytical Results
Alchem Site
Thomasville, North Carolina
Constituent
SS-1
SS-2 SS-3 SS-4 Lowest NCDENR Standard
Date
WIT METTI
Arsenic
1211312010
BDL
1211312010
BDL
1211812010
11.2
1211812010
6.9
4.4
Barium
24.2
12
54.6
34.6
580
Cadmium
BDL
BDL
BDL
BDL
14
Chromium
56.7
14.8
45.9
32.2
23,000
Lead
1.92
2.23
BDL
BDL
270
Mercury
BDL
BDL
0.0549
0.0263
11
Selenium
BDL
BDL
BDL
BDL
78
Silver
BDL
BDL
BDL
BDL
78
pH
4.3
5
4.3
3.9
NSE
Constituent SS-5 -' I SS-6 SS-7 BG Lowest NCDENR Standard
Date
1211312010
1211812010
1211812010
1211812010
IS
Arsenic
9.63
10.5
10.3
8.59
4.4
Barium
29.2
20.3
24.4
45
580
Cadmium
BDL
BDL
BDL
BDL
14
Chromium
65.7
63.8
44.6
15.1
23,000
Lead
BDL
BDL
BDL
BDL
270
Mercury
BDL
BDL
BDL
BDL
11
Selenium
BDL
BDL
BDL
BDL
78
Silver
BDL
BDL
BDL
BDL
78
5.2
5.6
6.1
4.3
NSE
All results in milligrams per kilogram (mg/kg) except for pH.
BDL= Below Detection Limits
XIO-1058

TABLE 2
Summary of Water Laboratory Analytical Results
Alchem Site
Thomasville, North Carolina
Constituent WS-1
Lowest NCDENR Standard
Date
411112011
g{
101 PM
Arsenic
0.016
10
Barium
0.144
700
Cadmium
BDL
2
Chromium
0.037
10
Lead
BDL
15
Mercury
BDL
1
Selenium
0.023
20
Silver
BDL
20
H
6.2
NSE
All results in milligrams per liter (mg/L) except for pH.
BDL= Below Detection Limits Xi 1-1058

APPENDIX A
SOIL. ANALYTICAL RESULTS

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
a
Contact:' Mr. Brandon Moore Report Date: 12/21/10
Client: Paragon Environmental Consultants Date Sample Rcvd: 12/13/10
PO# P-1058A
Project # Alchem Project .
Meritech Work Order # 12131009 Sample: SS-1 12/13/10
Parameters Result Analysis Date Reporting Limit Method
Arsenic, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Barium, total
24.2 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 0.116 mg/kg
12/14/10
0.116 mg/kg
EPA 200.7
Chromium, total
56.7 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Lead, total
11.92 mg/kg
12/14/10
5.79 mg/kg
EPA 200.7
Mercury, total
< 0.0119 mg/kg
12/15/10
0.0119 mg/kg
EPA 200.7
Selenium, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Silver, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
pH
4.3 S.U.
12/13/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12131010
Sample: SS-2
12/13/10
Parameters
Result
Analysis Date Reporting_ Limit
Method
Arsenic, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Barium, total
12.0 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 0.16 mg/kg
12/14/10
0.160 mg/kg
EPA 200.7
Chromium, total
14.8 mg/kg
12/14/10
0.500 mg/kg
EPA 200.7
Lead, total
2.23 mg/kg
12/14/10
5.79 mg/kg
EPA 200.7
Mercury, total
< 0.0115 mg/kg
12/15/10
0.0115 mg/kg
EPA 200.7
Selenium, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
Silver, total
< 1.16 mg/kg
12/14/10
1.16 mg/kg
EPA 200.7
pH
5.0 S.U.
12/13/10
1.0-14.0 S.U.
SM 4500 S D
I hereby certify that 1 have reviewed and approve these data.
aboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#
Phone:
MERI TECM INC.-Client:
ENVIRONMENTAL LABORATORIES
A Division of Water Technology and Controls, Inc.
Phone: [phone]
PA Fax: =fi•' l'
P.O. Box Ite, Inc.
Thomasville NC 27361 Email:
Address: �336�`���037 Project If
P. o. # I
Turn Around Time*
642 Tamco Rd. Fax: [phone]
*RUSH work must have prior approval.
Reidsville, NC 27320 Erriail: [e-mail]
Web Site: www.meritech-labs.com
, Sid (10 days) 3 - 5 Day 24 - 48 Hr
Attention:
Sample Sampling Dates & Times
Required Lab Use
Person kina Sam Signature: = �?-r t, `, .. d-- Method only
Comp?
Grab?
# of
Conts.
Tests Required
200.8 / 200.7
pH OK
?
START END
Location/I D # Time Date Time
Date
JJ t.,
Compositor # .
***Dechlorination.(<0.5
ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservatiorl.***
Comments:
Jug #
Method of Shipment:
❑ .UPs ;th
Are these results for regulatory purposes?
YES ❑ NO ❑
Report results in
mg/L ❑ mg/Kg ❑ µg/L ❑
On Ice? ' '.i`'
Temperature On Receipt r`
Relinquished by Date Tlme
Received by ., Date Time
//2
❑ Fed Ex
Hand Delivery
❑ Other
Relinquished by -Y: '� Date Time
Received by Date Time
Relinquished by - Date Time
-
Received at lab by. Date Time
_.ill' -,a �C'..-i:C 'Y`�(_�. _���...._�1=_.._�—�-•�.��_:.-._:�,.•a.__._�....t-_.�-_•- �.,

Meritech, Inc.
w Environmental Laboratory
Laboratory Certification No.165
Contact: Mr. Brandon Moore
Client: Paragon Environmental Consultants
Pg1of3
Report Date: 12/29/10
Date Sample Rcvd: 12/20/10
PO# P-1058B
Project # Alchem Project
Meritech Work Order #
12201045 Sample: SS-3
12/18/10
Parameters
Result
Analysis Date
Reporting_Limit
Method
Arsenic, total
11.2 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
54.6 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.37 mg/kg
12/23/10
1.37 mg/kg
EPA 200.7
Chromium, total
45.9 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 6.86 mg/kg
12/23/10
6.86 mg/kg
EPA 200.7
Mercury, total
0.0549 mg/kg
12/29/10
0.0010 mg/kg
EPA 200.7
Selenium, total
< 6.86 mg/kg
12/23/10
6.86 mg/kg
EPA 200.7
Silver, total
< 3.43 mg/kg
12/23/10
3.43 mg/kg
EPA 200.7
pH
4.3 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12201046 Sample: SS-4
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
6.90 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
34.6 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.31 mg/kg
12/23/10
1.31 mg/kg
EPA 200.7
Chromium, total
32.3 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 6.57 mg/kg
12/23/10
6.57 mg/kg
EPA 200.7
Mercury, total
0.0263 mg/kg
12/29/10
0.0010 mg/kg
EPA 200.7
Selenium, total
< 6.57 mg/kg
12/23/10
6.57 mg/kg
EPA 200.7
Silver, total
< 3.29 mg/kg
12/23/10
3.29 mg/kg
EPA 200.7
pH
3.0 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
642 Tamco Road, Reidsville, North Carolina 27320
tel.(336)342=4748 fax.[phone] ;>

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Mr. Brandon Moore
Client: Paragon Environmental Consultants
Pg 2 of 3
Report Date: 12/29/10
Date Sample Rcvd: 12/20/10
PO# P-1058B
Project # Alchem Project
Meritech Work Order #
12201047 Sample: SS-5
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
9.63 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
29.2 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.20 mg/kg
12/23/10
1.20 mg/kg
EPA 20.0.7
Chromium, total
65.7 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 5.98 mg/kg
12/23/10
5.98 mg/kg
EPA 200.7
Mercury, total
< 0.0120 mg/kg
12/29/10
0.0120 mg/kg
EPA 200.7
Selenium, total
< 5.98 mg/kg
12/23/10
5.98 mg/kg
EPA 200.7
Silver, total
< 2.99 mg/kg
12/23/10
2.99 mg/kg
EPA 200.7
pH
5.2 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12201048
Sample: SS-6
12/18/10
Parameters
Result
Analysis Date Reporting Limit
Method
Arsenic, total
10.S mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
20.3 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.18 mg/kg
12/23/10
1.18 mg/kg
EPA 200.7
Chromium, total
63.8 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 5.88 mg/kg
12/23/10
5.88 mg/kg
EPA 200.7
Mercury, total
< 0.0118 mg/kg
12/29/10
0.0118 mg/kg
EPA 200.7
Selenium, total
< 5.88 mg/kg
12/23/10
5.88 mg/kg
EPA 200.7
Silver, total
< 2.94 mg/kg
12/23/10
2.94 mg/kg
EPA 200.7
pH
5.6 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.(B6)342-1522

Meritel h, Inc.
Environmental Laboratory
Laboratory Certification No.165
Pg 3 of 3
Contact: Mr. Brandon Moore Report Date: 12/29/10
Client: Paragon Environmental Consultants Date Sample Rcvd: 12/20/10
PO# P-1058B
Project # Alchem Project
Meritech Work Order #
12201049 Sample: SS-7
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
10.3 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
24.4 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.18 mg/kg
12/23/10
1.18 mg/kg
EPA 200.7
Chromium, total
44.6 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 5.92 mg/kg
12/23/10
5.92 mg/kg
EPA 200.7
Mercury, total
< 0.0118 mg/kg
12/29/10
0.0118 mg/kg
EPA 200.7
Selenium, total
< 5.92 mg/kg
12/23/10
5.92 mg/kg
EPA 200.7
Silver, total
< 2.96 mg/kg
12/23/10
2.96 mg/kg
EPA 200.7
pH
6.1 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
Meritech Work Order #
12201050 Sample: BG
12/18/10
Parameters
Result
Analysis Date
Reporting Limit
Method
Arsenic, total
8.59 mg/kg
12/23/10
1.00 mg/kg
EPA 200.7
Barium, total
45.0 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Cadmium, total
< 1.27-mg/kg
12/23/10
. 1.27 mg/kg
EPA 200.7
Chromium, total
15.1 mg/kg
12/23/10
0.500 mg/kg
EPA 200.7
Lead, total
< 6.36 mg/kg
12/23/10
.6.36 mg/kg
EPA 200.7
Mercury, total
< 0.0127 mg/kg
12/29/10
0.0127 mg/kg
EPA 200.7
Selenium, total
< 6.36 mg/kg
12/23/10
6.36 mg/kg
EPA 200.7
Silver, total
< 3.18 mg/kg
12/23/10
3.18 mg/kg
EPA 200.7
pH
4.3 S.U.
12/21/10
1.0-14.0 S.U.
SM 4500 S D
I hereby certify that have reviewed and approve these data. cJ�
Laboratory Representative
642 Tameo Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chairs of Custody Record (COC)
Cilerlt.
�
NPDES#
Fax:Phone:36 y76-7708
MERI TECI� INC.
tIN
_
ENVIRONMENTAL LABORATORIES
EnvfriMm®nPcal ConsWtmfNFt, !na
P.O. Box 157
Thomasville, NC2736t
Address: l336►669-6037
Email:
Project# /g/Ck,* 116e-C7'L
A Division of Water Technology and Controls, Inc.
Phone: [phone]
642 Tamco Rd. Fax: [phone]
P. o. #
Turn Around Time*
*RUSH work must have prior approval.
Reidsville, NC 27320 Email: [e-mail]
Web Site: www.meritech-labs.com
Attention:
—&0 0/1
Std (10 days) 3 - 5 Day 24 - 48 Hr
Sample Sampling Dates &Times
�� g
�-OCation/ID START END
Person Takin Sam e Si nature :
Comp? kof
Required Lab Use
Method Only
i
Time Date lime
Grab?
C;t'Tests Required
200.8/200.7 pH OK?
vTFDate _
e�
#'I�sq3� 2-/�-/o l!'3�q�, a.
,:roil 1:114
G
.
%�CR��e
C12 OK?
Compositor #
***®ech' ri ation (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation.***
Jug #
Comments:
Are these results for regulatory purposes?
�
Report results in
On Ice?
Method of Shipment:
❑ UPS
YES NO ij
mg/L ❑
mg/Kg µg/L
mperature On Receipt
Teipt ——
❑ Fed Ex
Relinquished by
Date
/Z-Zo-/a
Time Receiv b
Date Time
Hand Delivery
Relinq '
e �
Date
Time eceived b
Date Time
❑ Other
Reli h y G
Date
Time tjocetved at by J
ate /Time.,

APPENDIX B
WATER ANALYTICAL RESULTS

Meritech, Inc.
Environmental Laboratory
• Laboratory Certification No.165
i
Contact: Mr. Brandon Moore
Report Date:
4/25/11
Client: Paragon Environmental Consultants
Date Sample Rcvd:
4/11/11
PO# P-1058C
Project # Alchem Project
Meritech Work Order #
04111123 Sample: WS-1
4/11/11
Parameters
Result
Analysis Date
Reporting_ Limit
Method
Arsenic, total
0.016 mg/L
4/15/11
0.010 mg/L
EPA 200.7
Barium, total
0.144 mg/L
4/15/11
0.500 mg/L
EPA 200.7
Cadmium, total
< 0.002 mg/L
4/15/11
0.002 mg/L
EPA 200.7
Chromium, total
0.037 mg/L
4/15/11
0.005 mg/L
EPA 200.7
Lead, total
< 0.010 mg/L
4/15/11
0.010 mg/L
EPA 200.7
Mercury, total
< 0.0002 mg/L
4/15/11
0.0002 mg/L
EPA 200.7
Selenium, total
0.023 mg/L
4/15/11
0.010 mg/L
EPA 200.7
Silver, total
< 0.005 mg/L
4/15/11
0.005 mg/L
EPA 200.7
pH
6.2 S.U.
4/11/11
1.0-14.0 S.U.
SM 4500 S D
I hereby certify that I have reviewed and approve these data.
L a h o rat—ory--k ep rese n ta tive
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#
INC.ne:
M RI T" �'1-7 l V
k
Client:
PQThornasvHk
Fax: `
rx
ENVIRONMENTAL LABORATORIES
P.O. Box li7
NC 27361
AddrPZ�ess: (336)66�1-6037
Email:
A Division of Water Technology and Controls, Inc.
Project#
�-
Turn Around Time*
Phone: [phone]
642 Tamco Rd. Fax:. [phone]
*RUSH work must have prior approval.
Reidsville NC 27320 Email: [e-mail]
%'
y! %
Std (10 days)
3 - 5 Day
24 - 48 Hr
Web Site: www.meritech-labs.com
Attention: `f '°) 'J 0l;
Sample
p
Sampling Dat s & Times
P g _
i"
-Person .Sam a Si nature): .>, .n�- _� -_:, _ _..--..
Required
Method
Lab Use
Only
STARTj®END
Comp?
Grab?
#of
Conts.
Tests Required
q
20Qi8/200.7
pH OK?
Location/ID #
Date_
Time
Date
Time
C12 OK?
'W,, .,))j [�
{�J'
iq
�l
1 /
/I y/�r.� �a#r f(/icy /
•i
.'ylt1lt� • f
/ f
! <. ' L�•T�i�!';7
_�
/` F,r ///�J/ `j `- -J XII��,
7
.—f
***Decnlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation. **
Compositor
Jug #
Comments:
Are these results for regulatory purposes? Report results in 4 i
Method of Shipment:
❑ UPS
On Ice? Temperatur�On eceipt -i
YES NO ❑ mg/L mg/Kg ❑ µg/L ❑
❑ Fed Ex
Relinquished by . �( l �� Date Time Received by / / Date Time
r
a{ Hand Delivery_
Relinquished by ,.. / Date Time
Received by Date Time
❑ Other
, I. t .. {'i 7_
Relinquished by Date Time
Received at lab by Date Time

APPENDIX C
SOIL DISPOSAL WEIGHT TICKETS

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1087
Weighed: ELLY B
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME
IN: 13:18:57
DATE OUT: 12/14/2010 TIME
OUT: 13:18
INBOUND TICKET Number: 03-189213
MANUAL GROSS WT.
56640 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
26420 LB
QtY Description
Amount
13.21 MSW-COMMERCIAL
475.56
NET CASH AMOUNT:
475.56
AMT. TENDERED:
475.56
CHANGE AMOUNT:
0.00
CHECK # BC7777
LOPP ROAD LANDFILL
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116
W CENTER ST
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
LEXINGTON NC 27293-1067
Weighed: JAMIE
Weighed: JAMIE
BILL TO:
BILL TO: 0
C
CASH CUSTOMER
CASH CUSTOMER
-
Vehicle ID:
Vehicle ID:
Reference: SAND
Reference: SAND
Origin: ALCHEM
Origin: ALCHEM
DATE IN: 12/14/2010 TIME
IN: 14:35:11
DATE IN: 12/14/2010 TIME IN: 15:31:33
DATE OUT: 12/14/2010 TIME
OUT: 14:35
DATE OUT: 12/14/2010 TIME OUT: 15:31
INBOUND 'PICKET Number: 03-189227
INBOUND TICKET Number: 03-189238
MANUAL GROSS WT.
57320 LB
MANUAL GROSS WT. 55520 LB -
MANUAL TARE WT.
30220 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT
27100 LB
i NET WEIGHT 25300 LB
Qty Description
Amount
Qty Description Amount
13.55 MSW-COMMERCIAL
487.80
; 12.65 MSW-COMMERCIAL 455.40
NET CASH AMOUNT:
487.80
NET CASH AMOUNT: 455.40
AMT. TENDERED:
487.80
AMT. TENDERED: 455.40
CHANGE AMOUNT:
0.00
CHANGE AMOUNT: 0.00
CHECK # BC7777
CHECK # BC7777'

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: B/ALCHEM
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME IN: 10:20:45
DATE OUT: 12/11/2010 TIME OUT: 10:20
INBOUND TICKET Number; 03-188993
MANUAL GROSS WT. 51160 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 20940 LR
Qty Description
Amount
10.47 MSW-COMMERCIAL
376.92
NET CASH AMOUNT:
i
376.92
AMT. TENDERED:
376.92
i CHANGE AMOUNT;
0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: 8/ALCHEM
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME
IN: 12:43:50
DATE OUT: 12/11/2010 TIME
OUT:.12:43
INBOUND TICKET Number; 03-189032
MANUAL GROSS WT.
59880 LB
MANUAL TARE WT.
.30220 LB
NET WEIGHT
29660 LB
Qty Description
Amount
14.83 MSW-COMMERCIAL
633.88
NET CASH AMOUNT:
533.88
AMT. TENDERED:
533.88
CHANGE AMOUNT:
0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM 0
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: B/ALCHEM
Origin: SAND
DATE IN; 12/11/2010 TIME IN: 13:44:18
DATE -OUT: 12/11/2010 TIME OUT: 13:44
INBOUND TICKET Number: 03-189047
MANUAL GROSS WT.
60480 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
30260 LB
Oty Description
Amount .
15.13 MSW-COMMERCIAL
544.68
NET LASH AMOUNT:
544.68
AMT. TENDERED:
544.68
CHANGE AMOUNT:
-0.00
CHECK # BC7777

LOPP ROAD LANDFILL I LOPP ROAD LANDFILL LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST i P 0 BOX 1067 - 116 W CENTER ST P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067 LEXINGTON NC 27293-1067 LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: B/SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 09:47:69
DATE OUT: 12/14/2010 TIME OUT: 09:47
I
INBOUND TICKET Number: 03-189176
MANUAL GROSS WT. 56640 LB
f MANUAL TARE WT. 30220 LB
NET WEIGHT 26420 LB
Oty Description Amount
13.21 MSW-COMMERCIAL 475.56
NET CASH AMOUNT: 475.56
AMT. TENDERED: 475.56
CHANGE AMOUNT: 0.00
CHECK # BC7777
Weighed: JAMIE
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 10:54:23
DATE OUT: 12/14/2010 TIME OUT: 10:54
INBOUND TICKET Number: 03•-189190
MANUAL GROSS WT. 56760 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 26540 LB
Oty Description Amount
13.27 MSW-COMMERCIAL 477.72
NET CASH AMOUNT: 477.72
AMT. TENDERED: 477.72
CHANGE AMOUNT: 0.00
CHECK # BC7777
X
Weighed: ELLY B
BILL '.TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/14/2010 TIME IN: 12:22:49
DATE OUT: 12/14/2010 TIME OUT: 12:22
INBOUND TICKET Number: 03-189207
MANUAL GROSS WT. 51680 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 21460 LB
Oty Description Amount
10.73 MSW-COMMERCIAL 386.28
NET CASH AMOUNT: 386.28
AMT. TENDERED: 386.28
CHANGE,AMOUNT: 0.00
CHECK # BC7777

LOPP ROAD LANDFILL
P 0 BOX 1067 -.116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 0
CASH CUSTOMER
IVehicle ID:
Reference: 8/ALCHEM
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME IN: 11:19:11
DATE OUT: 12/11/2010 TIME OUT: 11:19
INBOUND TICKET Number: 03-189012
MANUAL GROSS WT. 56820 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 26600 LB
Qty Description Amount
13.30 MSW-COMMERCIAL 478.80
NET CASH AMOUNT: 478.80
AMT. TENDERED: 478.80
CHANGE AMOUNT: 0.00
CHECK # BC7777
LOPP ROAD LANDFILL
'P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM 0
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: 8/ALCHEM
Origin: SAND PO#120910
DATE IN: 12/11/2010 TIME IN: 07:45:55
DATE OUT: 12/11/2010 TIME OUT: 07:45
INBOUND TICKET Number: 03-188973
MANUAL GROSS WT. 71840 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 41620 LB
4
Qty Description Amount
20.81 MSW-COMMERCIAL 749.16
NET CASH AMOUNT: 749.18
-AMT. TENDERED: 749.16
CHANGE AMOUNT: 0.00
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 0
CASH CUSTOMER
j Vehicle ID:
Reference: 8/TRK 01
Origin: 165 FANNIE PULLUM RD
DATE IN: 12/10/2010 TIME IN: 13:30:45
DATE OUT: 12/10/2016. TIME OUT: 13:30
INBOUND TICKET Number: 03-188937
MANUAL GROSS WT. 49500 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 19280 LB
i
Qty. Description Amount
9.64 MSW-COMMERCIAL 347.04
NET CASH AMOUNT: 347.04
AMT. TENDERED:. 347.04
CHANGE AMOUNT: 0.00
CHECK # BC7777
X-4

LOPP ROAD LANDFILL
P 0 BOX 1067 •- 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: JAMIE
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: DIRT
Origin: ALCHEM
DATE IN: 12/10/2010 TIME IN: 15:41:38
DATE OUT: 12/10/2010 TIME OUT: 15:41
INBOUND TICKET Number: 03-188964
MANUAL GROSS WT. 57240 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 27020 LB
Oty Description Amount
13.51 MSW-COMMERCIAL 486.36
NET CASH AMOUNT: 486.36
1
AMT. TENDERED: 486.36
CHANGE AMOUNT: 0.00
CHECK # BC7777
Xt�
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: ELLY B
BILL TO:. 0
CASH CUSTOMER
Vehicle ID:
i
Reference: DIRT/01
Origin: 165 FANNIE PULLMAN RD
DATE IN: 12/10/2010 TIME IN: 14:33:11
DATE OUT: 12/10/2010 TIME OUT: 14:33
INBOUND TICKET Number: 03-188950
MANUAL GROSS WT. 60300. LB
MANUAL TARE WT, 30220 LB
NET WEIGHT 30080 LB
Qty Description Amount
15.04 MSW-COMMERCIAL 541.44
NET CASH AMOUNT: 541.44
AMT. TENDERED: 541.44
CHANGE AMOUNT: 0.00
CHECK # BC7777
c
X_

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 0
CASH CUSTOMER
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/17/2010 TIME IN: 14:01:16
DATE OUT: 12/17/2010 TIME OUT: 14:01
INBOUND TICKET Number: 03-189414
MANUAL GROSS WT. 57860 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 27640 LB
Oty Description
13.82 MSW-COMMERCIAL
NET CASH'AMOUNT:
AMT. TENDERED:
CHANGE AMOUNT:
CHECK # BC7777
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
i BILL T0: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
i
DATE IN: 12/18/2010 TIME IN: 12:13:17
DATE OUT: 12/18/2010 TIME OUT: 12:13
INBOUND TICKET Number: 03-189472
MANUAL GROSS WT. 57280.,LB
STORED TARE WT. 30226 aLB
NET WEIi3HT 27060 LB
Amount j Oty Description
497.52 I 13.53 MSW-COMMERCIAL
497.52 NET CHARGE AMOUNT:
497.52
0.00
Amount
487.08
487.08

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE.
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
i DATE IN: 12/18/2010 TIME IN: 08:43:14
DATE OUT: 12/18/2010 TIME OUT: 08:43
INBOUND TICKET Number: 03-189432
MANUAL GROSS WT. 57480 LB
STORED TARE WT. 30220 LB
NET WEIGHT 27260 LB
Oty Description Amount
13.63 MSW-COMMERCIAL 490.68
NET CHARGE AMOUNT: 490.68
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
-LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
DATE IN: 12/18/2010 TIME IN: 09:45:32
DATE OUT: 12/18/2010 TIME OUT: 09:45
INBOUND TICKET Number: 03-189442
MANUAL GROSS WT. 57680 LB
STORED TARE WT. 30220 LB
NET WEIGHT 27460 LB
Oty Description Amount
13.73 MSW-COMMERCIAL 494.28
NET CHARGE AMOUNT: 494.28
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116
W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
i
DATE IN: 12/17/2010 TIME
IN: 11:14:24
DATE OUT: 12/17/2010 TIME
OUT: 11:14
INBOUND TICKET Number: 03-189378
MANUAL GROSS WT..
57520 LB
STORED TARE WT.
30220 LB
NET WEIGHT
27300 LB
Oty Description
Amount
13.65 MSW-COMMERCIAL
491.40
NET CHARGE AMOUNT:
49.1.40

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILL TO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
DATE IN: 12/17/2010 TIME IN: 10:14:47
DATE OUT: 12/17/2010 TIME OUT: 10:14
i
INBOUND TICKET Number: 03-189366
MANUAL GROSS WT. 53880 LB
STORED TARE WT. 30220 LB
j NET WEIGHT 23660 LB
I
Oty Description Amount
11.83 MSW-COMMERCIAL 425.88
NET CHARGE AMOUNT: 425.88
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: 8/SAND
Origin: SAND
DATE IN: 12/15/2010 TIME IN: 08:09:50
DATE OUT: 12/15/2010 TIME OUT: 08:09
.,INBOUND TICKET Number: 03-189246
MANUAL GROSS WT. 55720 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 25500 LB
Oty Description Amount
12.75 MSW-COMMERCIAL 459.00
NET CHARGE AMOUNT: 459.00
X
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: 8/SAND
i Origin: SAND
DATE IN: 12/15/2010 TIME IN: 09:49:05
DATE OUT: 12/15/2010 TIME OUT: 09:49
INBOUND TICKET Number: 03-189255
MANUAL GROSS WT. 57840 LB
i MANUAL TARE WT. 30220 LB
NET WEIGHT 27620 LB
Oty Description Amount
13.81 MSW-COMMERCIAL 497:16
NET CHARGE AMOUNT: 497.16

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
1 Vehicle ID:
Reference: 8/SAND
Origin: SAND
DATE IN: 12/15/2010 TIME IN: 10:50:45
DATE OUT: 12/15/2010 TIME OUT: 10:50
INBOUND TICKET Number: 03-189265
i
MANUAL GROSS WT. 54080 LB
MANUAL TARE WT. 30220 LB {
NET WEIGHT. 23860 LB
Oty Description Amount
11.93 MSW-COMMERCIAL 429.48
NET CHARGE AMOUNT: 429.48
LOPP ROAD LANDFILL.
.P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: Sherri
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: CONT. SAND
Origin: . CONTAMINATED SAND
DATE IN: 12/15/2010 TIME IN: 13:54:22
DATE OUT: 12/15/2010 TIME OUT: 13:54
INBOUND TICKET Number: 03-189301
MANUAL GROSS WT. 56280 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 26060 LB
Oty - Description Amount
13.03 MSW-COMMERCIAL 469.08
NET CHARGE AMOUNT: 469.08
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NO 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: 8/SAND
DATE IN: 12/15/2010 TIME IN: 12:40:07
DATE OUT: 12/15/2010 TIME OUT: 12:40
INBOUND TICKET Number: 03-189286
MANUAL GROSS WT. 56200 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 25980 LB
Oty Description Amount
12.99 MSW-COMMERCIAL 467.64
NET CHARGE AMOUNT: 467.64

LOPP ROAD LANDFILL
P 0 BOX 1067 - 116
W CENTER ST
LEXINGTON NC 27293-1067
Weighed: KIM G
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: WAND
Origin: SAND
DATE IN: 12/15/2010 TIME
IN: 14:66:03
DATE OUT: 12/15/2010 TIME
I
OUT: 14:56
INBOUND TICKET Number: 03-189307
I
MANUAL GROSS WT,
51620 LB
MANUAL TARE WT.
30220 LB
NET WEIGHT
i
21400 LB
0ty Description
Amount
10.70 MSW-COMMERCIAL
385.20
NET CHARGE AMOUNT:
385.20
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: JAMIE
BILL TO: 1061
ALCHEM INC
Vehicle ID:
Reference: SAND
Origin: ALCHEM
DATE IN: 12/15/2010 TIME IN: 15:52:36
DATE OUT: 12/15/2010 TIME OUT: 15:52
INBOUND TICKET Number: 03-189313
MANUAL GROSS WT. 58740 LB
MANUAL TARE WT. 30220 LB
NET WEIGHT 28520 LB
Oty Description Amount
14.26 MSW-COMMERCIAL 513.36
NET CHARGE AMOUNT: 513.36
LOPP ROAD LANDFILL
P 0 BOX 1067 - 116 W CENTER ST
LEXINGTON NC 27293-1067
Weighed: ELLY B
BILLTO: 1061
ALCHEM INC
Vehicle ID: 1061001
Reference: SAND
i DATE IN: 12/17/2010 TIME
IN: 09:12:03
DATE OUT: 12/17/2010 TIME
OUT: 09:12
INBOUND TICKET Number:
03-189358
MANUAL GROSS WT.
57240 LB
STORED TARE WT.
30220 LB
NET WEIGHT
27020 LB
Oty Description
Amount
13.51 MSW-COMMERCIAL
486.36
NET CHARGE AMOUNT:
486.36
X

06/29/2011 15:41 3362422287 LANDFILL SCALEHOUSE PAGE 02
LOP RM U ILL LU F ROAD MSFILL
P A W 1087 118 W CWH ST- F D 5OX lW7 - 176 rr E-VffER ST
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Origin: M EAMIE ML14 RD TYIL DATE 'sK: OB/10IM11 TRE PR: 07:30:15
DATE IN: 03/0912011 TIME IN: 08*28:31 DAR Wf; t S/10RD11 THE ice: 07:?i
DATE OUT: 06/09/2011 TIM OIJT: 08:.50
[REM TIMT ;lu4sr: 03-204347
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12.01 W-MORCIAL 432.38
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MT CRAM ANW., 42.38
'cam X �

Comorate Office Sales and Manufacturing
2042 Buie Philadelphus Road 8135 Red Road
Red Springs, NC 28377 Rockwell, NC 28138
Tel. [phone] — 800-522-2944 Tel. [phone]o8 — 800-462-2586
Fax [phone]
[e-mail]
Fax 3-5789 [e-mail]
[e-mail]
August 23, 2010
Mr. Andrew Pitner
Regional Environmental Supervisor
NCDENR Division of Water Quality
Mooresville Regional Office
610 East Center Ave.
Suite 301
Mooresville, NC 28115
NOV-2010-PC-0940
Permit #: WQ0002702, WQ0016338
Dear Mr. Pitner:
I went to the location in Thomasville, NC. That has the sand. The man's name is Vernon
Sechrist. Robert Wolcott told Mr. Sechrist that the sand was fine to use. 1, nor anyone
else at ALCHEM told Robert Wolcott to do this. I had no knowledge of it and Mr.
Sechrist was unaware of a problem.
Robert Wolcott, Denise Wolcott, and Jason Desiato stole $500,000.00 from ALCHEM.
Robert then threatened that he . would reveal problems if I went to the Sheriff's
Department. I did not know what problems he was talking about and.I am not going to
be intimidated by him.
I am going to immediately get someone to help me with this. I am going to see about
finding a land fill in the area. I will do what I can to see who took this sand to
Thomasville, and try to determine how much is there. I should be able to get back in
touch with you within 10-15 days with a much more concrete plan about what is to
happen.
Best regards,
ALCHEM, INC.
Randall F. Andrews,
President
ams

NC®ENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director, Division of Water Quality Secretary
August 11, 2010
Certified Mail
Return Receipt Requested
Mr. Randall Andrews, Registered Agent
Alchem Incorporated
2042 Buie Philadelphus Rd.
Red Springs, NC 28377
and
Alchem Incorporated
8135 Red Road
Rockwell, NC 28138
Subject: Notice of Violation (NOV) and
Notice of Intent (NOI) to Enforce
NOV-2010-PC-0940
W00002702, WQ0016338
Recycle System, Monofill
Rockwell, Rowan County
Dear Mr. Andrews:
Chapter 143, North Carolina General Statutes, authorizes and directs the Environmental Management
Commission of the Department of Environment and Natural Resources to protect and preserve the water and
air resources of the State. The Division of Water Quality (Division) has the delegated authority to enforce
adopted pollution control rules. This letter is a standard notification and is intended to advise you of the legal
requirements under North Carolina law.
On April 4, 2010, staff from the Mooresville Regional Office, of the Division's Aquifer Protection Section
(Ellen Huffman, Andrew Pitner) investigated a complaint regarding a dump site located at 165 Fannie Pullam
Road, Thomasville, Davidson County, NC. Samples taken from the dump site physically and chemically
matched Alchem spent bauxite residuals and the material was found in substantial quantity among other debris
at the location. As a result of these findings, Alchem is in violation of conditions of the subject permits and the
November 27, 2007, Settlement Agreement. Specific violations are discussed below:
Permit WQ0016338, Condition 1.3 - the facilities should be effectively maintained and operated as a
non -discharge system to prevent the discharge of any wastes resulting from the operation of this
program.
Permit WQ0002702, Condition 6 — The residuals generated from these treatment facilities must be
disposed of in accordance with General Statute 143-215.1 and in a.manner approved by the Division.
Division of Water Quality / Aquifer Protection Section / Mooresville Regional Office One
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115 NorthCarolina
Phone: [phone] Fax: [phone] Customer Service: 1-877-623-6748
Internet: www.ncwaterquality.org / �/�lq���
An Equal Opportunity 1 Affirmative Action Employer YY

'V„^ ',,..
Alchem NOV/NG1
August 11, 2010
The aforementioned location is not an appropriately permitted facility for disposal and the
Division did not approve the manner of disposal or the location.
In order to correct this violation, you shall immediately cease disposal of residuals at locations that are
not permitted for disposal. You must also remove the spent bauxite residuals from their present location in
Davidson County and dispose of them in a Subtitle D landfill. Any future plans for using the residuals in such
processes must be submitted and approved in writing by the Division prior to off -site transport. Alchem is not
permitted to give away spent bauxite for fill or any other use without prior approval from the Division.
You are required to document the cleanup and proper final disposal of the material and to submit a
report assessing any damage to the soil and/or surface water and groundwater at the unapproved disposal site
in Davidson County. The clean up and assessment report shall be prepared by a North Carolina Licensed
Geologist or Professional Engineer. Clean up documentation shall include (but is not limited to) the following:
photos of the dumpsite before and after, names of any companies hired to clean up the site, documentation of
all loads transported, documentation of final disposal (such as landfill tipping charges/manifests), and any
necessary testing of the material, soils and water. This report shall be submitted no later than October 31,
2010.
You are required to respond to this notice by submitting a plan for removal and proper disposal of the
residuals dumped in Davidson County to the Division's Aquifer Protection Section of the Mooresville Regional
Office within 10 days following receipt of this notice. The plan shall identify the approximate amount of material
that will be sent to a Subtitle D landfill and the name and location of that facility.
Pending further investigation, the Division reserves the right to issue additional notices of violation and
recommendations for enforcement. As the permit holder and generator of these residuals, it is Alchem's
responsibility to ensure that they are handled properly and disposed of within the conditions of your permit and
applicable laws. The material shall not be given away to be used as fill.
Failure to comply with conditions in a permit may result in a recommendation of enforcement action to
the Director of the Division of Water Quality who may issue a civil penalty assessment of not more that twenty-
five thousand ($25,000) dollars against any "person" who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit under authority of G.S. 143-215.6A. Please note that each day a
violation continues may be considered a separate violation, subject to additional civil penalties.
As a result of the violations described in this Notice this office is considering a recommendation for a
civil penalty assessment to the Director of the Division. If you wish to present an explanation for the violations
cited, or if you believe there are other factors that should be considered, please send such information to me in
writing within ten (10) days following receipt of this letter. Your response will be reviewed, and, if an
enforcement action is still deemed appropriate, it will be forwarded to the Director and included for
consideration.
Should you have any questions, feel free to contact me at 704/235-2180 or via email at:
Andrew. Pitner(a.ncdenr.gov.
Sincerely,
Andrew H. Pitner, P.G.
Environmental Program Supervisor
Cc: Jackie Turner, property owner, 65 Fannie Pullum Road, Thomasville, NC 27360
MRO=APS-Files—= --•
WSRO- Hugh Jernigan
DWQ-APS Land Application Unit, Raleigh
Anita LeVeaux, Attorney General's Office, Environmental Division

2010 ALCHEM Fannie Pullam dump site time -line
Also known as dump site #2
April 10, 2010 — MRO investigates dumping complaint at 165 Fannie Pullam Road, Thomasville, NC.
Samples taken physically and chemically match ALCHEM spent bauxite.
August 11, 2010 — MRO issues NOV-2010-PC-0940 for WQ0002702 and WQ0016338 for dumping.
August 23, 2010 — letter via email and unsigned from Mr. Andrews stating "no knowledge" and blaming
Mr. Wolcott. Letter also states that he would get help to clean it up.
October 27, 2011— email from Mr. Andrews included an attached text message from Mr. Wolcott dated
4 months prior (June 22, 2010). Mr Andrews states that he is having trouble "finding anything out"
because he is dealing with nutcases. Mr. Andrews portrays the old text message as a recent threat
toward himself.
November 7, 2010 — received letter from Mr. Andrews requesting an extension for clean up. The
deadline for clean up was November 1, 2010.
November 8, 2010 — received two letters from Mr. Andrews both are dated October 27, 2010. One letter
is "a formal response" about the sand in Thomasville. Mr. Andrews states that he cannot find any
records that show sand was taken to Thomasville but, after talking to employees, he is guessing 100-150
tons were dumped. The other letter states that he went to see the land owner, Vernon Sechrest, again.
Mr. Andrews has decided to have Vernon remove the "sand" and transport it to the Davidson County
landfill. Letter also asks for a 90 day extension. Also states that he has never heard of Vernon until after
he received our letter.
November 24, 2010 —A new deadline of January 28, 2011 was given by MRO.
January 5, 2011— Soil remediation report was received from Paragon.
February 8, 2011— MRO sends letter of review of the Assessment report with a list of deficient and /or
missing data including no pH, no report of lime applied, no re -seeding, no photos, no map recording
points where samples were taken, no transportation documentation. A site visit on January 25, 2011
showed incomplete clean up. A deadline of March 24th is given to send the missing data.
February 11, 2011— email from Mr. Andrews stating that Brandon (Paragon) is taking some vacation.
March 7, 2011— email from Brandon requesting a visit from MRO to evaluate what else needs to be
cleaned up at the site. MRO responded with an email that we would be happy to look at the site after
they attempt to remove the remainder of the material.
April 15, 2011— letter from Brandon (Paragon) requesting an extension of 90 days to complete the clean
up.
April 27, 2011— email to Paragon in response to extension request. "Mr. Andrews needs to finish this
clean up asap. Our consideration of any civil penalties associated with this violation will include the level
of response demonstrated by ALCHEM."
May 4, 2011— follow up phone call requesting when report would be submitted.

7009 2250
0004
3265 69012
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UNITED STATES
0 Sender: Please print your name, add
NCDENR
AQLJIFIEP, PROTECTION SECTION
610 EAST'CENTER AVE
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SUITE 301
a cis
MOORESVILLE NC 28' 115
I . . . . . . . . .

cB
County:
DAVIDSON
Sample ID:
AB57812
River Basin
F V'pAT
�O R
Q
PO Number #
10G0231
Report To
MROAP
GP
Date Received:
05/0512010
r?
r
Time Received:
08:25
Collector:
A PITNER
p
_?
Labworks LoginlD
SMATHIS
Region:
MRO
Report Generated:
612/10
Sample Matrix:
SOILISEDIMENT
Date Reported:
06/02/2010
Loc. Type:
SOILISEDIMENT
Emergency Yes/No
VisitlD
COC Yes/No
YES
Loc. Descr.: TURNER
V
Location ID:
MROAPNLC
Collect Date: 05104/2010
Collect Time: 12:15
Sample Depth
CAS #
LAB
Analyte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
0.9
Units
C
Method
Reference
Analysis
Date
5/5/10
Validated by
SMATHIS
WET
pH in Soil
3 OfJ4
f,>f
pH Units
SW846/9045D
5/6/10
CGREEN
MET
7440-22-4
Ag in solid samples by ICPMS
0.2
0.20 U
mg/Kg
EPA 200.8
5/26/10
ESTAFFORDI
- ._7429-9005__
Akin _solid samples by LCP_W-.-� `�_� -
- = 5----
------`30000:4
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440-38-2
Arsenic solid samples by ICPMS
0.2
0.45 J3
mg/Kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-38-3
Barium in solid samples by ICP
1
67
mg/Kg
EPA 200.7
5125/10
ESTAFFORDI
7440-43-9
Cadmium in solids samples by ICPMS
0.2
0.20 U
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-70-2
Calcium in solid samples by ICP
10
350
mg/Kg
EPA 200.7
5125/10
ESTAFFORDI
744047-3
Cr in solids samples by ICPMS
0.2
22
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-50-8
Cu solid samples by ICPMS
0.2
2.8
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7439-97-6
Hg 245.5 solid
0.02
0.04
mg/Kg
EPA 245.5
5/11/10
ESTAFFORDI
7439-92-1
Lead in solids samples by ICPMS
0.2
19
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
7439-95-4
Mg in solid samples by ICP
10
54
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7439-96-5
Mn solid samples by ICPMS
0.2
3.2
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
7440-02-0
Nickel in solids samples by ICPMS
0.2
1.5
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
Percent Dry Solids
73.6
%
EPA 200.2
5/11/10
ESTAFFORDI
778249-2
Selenium in solids samples by ICPMS
0.2
0.34 J3
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-09-7
Sodium in solid samples by ICP
10
150
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440-66-6
Zinc in solids samples by ICPMS
0.2
y
mg/kg
EPA 200.8
5/25110
ESTAFFORDI
`A UI er P
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of?he qualifiercodes refer to hEtp efportS+.Lncc9rnr.nr<yw_c?hv_.1I:+hslAhin`cltee:,hnssis?#Da?;j quaLrier CnAes _;htt,Erlipq„talnc57m&og Loae yEgi" ws?afiinfgn r;h� _sist>
Page 1 of 1

f
A �-
GROUNDWATER FIELD/LAB FORM
SAMPLE TYPE
County _�?c>1��—___— —__ ❑ Water
04 Soil
North Carolina
k00111101" Department of Environment and Natural Resources
DIVISION OF WATER QUALITY-GROUNDWAfTER SECTION
SAMPLE PRIORITY 10 & 0 23 1 A�61
0—Routine Lab Number--__ o_—(((JJJ—
❑ Emeraencv \', i -�- c'
Quad No------ — Serial No.—__--__-- V v Date Received_ ,.2�Time-
Lat.—�' Long.— CCs,�S —_ ❑Other Rec'd By: *v.
From:6,Courier; and Del.,
Chain of Custody Other: —Report To: ARO, FRO, MRO�DataRRO, WaRO, WiRO, Data Entr_---- Ck:_--_--__
WSRO, Kinston FO, Fed. Trust, Central Off., Other:---- _— Reported:—_ _-- — —
Shipped by: Bus, Court Hn�d Deal., ther:—__—_ __ _ ___ Purpose:
Collector(s): R _ ` �_r_J 'N���'r` Date _y_(9 Time \2— pL, Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust
FIELD ANALYSES - roe—ivc %- (crcleone)
Owner----- - - — ------
pH 400_--- � --------- Spec. Cond.94—= at 25°C Location or Site __ L %�----_—__—__
____--____—__--_— Description of sampling point -
Appearance
Temp.lo — — °C Odor____ -� P P P --
Appearance— CL±A�3L��_ �� �"�� t'- Iis -TW -fi ! cgLNISampling Method— !V\,Crs�t� � �t-Z- 6)Y1��_— Sample Interval-_-
(Pumo. bailer. e1c.1
Field Analysis By:— �_T_�►��21_���i`�'`�a�i _--_ Remarks—_-- -- __---_— -- -----
_ (Pumping time, air temp., etc.)
Ag-Silver 46566
uglL
AI -Aluminum 46557
ug/L
As -Arsenic 46551 .
ug/L
Ba-Barium 46558
ug/L
Ca -Calcium 46552
mg/L
Cd-Cadmium 46559
ug/L
Cr-Chromium 46559
ug/L
Cu-copper46562
ug/L
Fe -Iron 46563
ug/L
Hg-Mercury 71900
ug/L
K-Potassium 46555
mg/L
Mg -Magnesium 46554
mg/L
Mn-Manganese 46565
ug/L
Na-Sodium 46556
mg/L
Ni-Nickel
ug/L
Pb-Lead 46564
ug/L
Se -Selenium
ug/L
Zn-Zinc 46567
ug1L
Lab Comme
GW-54 V. 12/87 For Dissolved Analysis -submit filtered sample and write'DIS' in block.

County:
DAVIDSON
Sample ID:
AB57813
River Basin
F V'dArFRQ
PO Number#
10G0232
�Q
Date Received:
Report To'
MROAP
�O.
05105/2010
f
Time Received:
08:25
Collector:
A PITNER
p
Labworks LoginlD
SMATHIS
Region:
MRO
Report Generated:
6/2/10
Sample Matrix:
SOIUSEDIMENT
Date Reported:
06/02/2010
Loc. Type:
SOIUSEDIMENT
Emergency Yes/No
VisitlD
t0/
COC Yes/No
YES
Loc. Descr.: TURNER
Location ID:
MROAPNLC
Collect Date: 05104/2010
Collect Time: 12:15
Sample Depth
CAS #
LAB
Analyte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
0.9
Units
C
Method
Reference
Analysis
Date
5/5/10
Validated by
SMATHIS
WET
pH in Soil
3.5 J4
pH Units
SW846/9045D
5/6/10
CGREEN
MET
7440-22-4
Ag in solid samples by ICPMS
0.2
0.20 U
mg/Kg
EPA 200.8.
5/26/10
ESTAFFORDI
7429-90-5
AI in solid samples by ICP
5
30000
mg/Kg
EPA 200.7
5125/10
ESTAFFORDI
7440-38-2
Arsenic solid samples by ICPMS
0.2
0.51 J3
mg/Kg
EPA200.8
5/26/10
ESTAFFORDI
7440-38-3
Barium in solid samples by ICP
1
62
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440-43-9
Cadmium in solids samples by ICPMS
0.2
0.20 U
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-70-2
Calcium in solid samples by ICP
10
160
mg/Kg
EPA 200.7
5125110
ESTAFFORDI
7440-47-3
Cr in solids samples by ICPMS
0.2
23
mg/kg
EPA 200.8
5/26110
ESTAFFORDI
7440-50-8
Cu solid samples by ICPMS
0.2
2.9
mg/kg
EPA 200.8
5126/10
ESTAFFORDI
7439-97-6
Hg 245.5 solid
0.02
0.09
mg/Kg
EPA245.5
5111/10
ESTAFFORDI
7439-92-1
Lead in solids samples by ICPMS
0.2
19
mg/kg
EPA200.8
5/25/10
ESTAFFORDI
7439-95-4
Mg in solid samples by ICP
10
130
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7439-96-5
Mn solid samples by ICPMS
0.2
7.8
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
7440-02-0
Nickel in solids samples by ICPMS
0.2
1.5
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
Percent Dry Solids
69.7
%
EPA 200.2
5111110
ESTAFFORD1
7782-49-2
Selenium in solids samples by ICPMS
0.2
0.41 J3
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-09-7
Sodium in solid samples by ICP
10
130
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440-66-6
Zinc in solids samples by ICPMS
0.2
2.6
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
0 JUN - 4 2010
NC
dWQ - Agyifer Protection
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Fora detailed description of the qualifier codes refer to htlp ±crtal_nrslenno:ctnvah.N/ rq !;,bsUf�nfatecAassist#[lata gua�ifer CMrs<htl�;/iportal.rccenr.grgN+ehwo/!ab/staffinraifechassist>
Page 1 of 1

+Q North Carolina
0
GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
rEAME SAMPLE PRIORITY 16 G-
County_✓`�J 1�_SoF�; _ Routine Lab NumberSerial No._ ❑ EmeraencvDate Received_°Time:_DQuad No__ ---
Lat. E=�Ps Long. C�,�5 __ Rec'd By: From:Bus Ourier. nd Del.,
of Custody Other: klm
Report To: ARO, FRO, CMF6)RRO, WaRO, WiRO, Data Entry B :_ _ Ck:
Data
WSRO, Kinston FO, Fed. Trust, Central Off., Other:—_— Reported: —
Shipped by: Bus,�_C
ouri , H nd Del .,�'ther:—______ _ _ —_--_. Purpose: ^�
Collector(s): i��'^_ Date_: Time�� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust Other:'
FIELD ANALYSES c� (circle one)
Aii'ElOwner_T�'�-�
pH 400_____ .-- __-----__ Spec. Cond.94__—at 250C Location or Site— — —
Temp.to°C Odor___—___— Description of samplin pointA-Q--iA
—
v�� wNr1lsH -sty, co.Ocgam Iln Method__ 1Atic=1 st=Z_ �-�Y2 Sample Interval L__t�c�' j
Appearance_�YLi�L , P g
IPumo. bailer. elc.1
Field Analysis By:_ C' Tom__�_���`�v — _ Remarks — __ —
r� n T� n V A n i A 1 V C C C (Pumping time, air temp., etc.)
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal 31616 /100ml
Coliform: MF Total 31504 /100mi
TOC 680 mg/L
Turbidity 76 NTU
Residue, Suspended 530 mg/L
pH 403 units
Alkalinity to pH .5410 mg/L
Alkalinity to pH 8.3 415 mg/L
Carbonate 445 mg/L
Bicarbonate 440 mg/L
Carbon dioxide 405 mg/L
Chloride 940 mg/L
Chromium: Hex 1032 ug/L
Color: True 80 Cu
Cyanide 720 mg/L
Lab
Diss. Solids 70300 mg/L
Fluoride 951 mg/L
Hardness: Total 900 mg/L
Hardness (non-carb 902 mg/L
Phenols 32730 ug/I
Specific Cond. 95 uMhos/cm
Sulfate 945 mg/L
Sulfide 745 mg/L
Oil and Grease mg/L
NH, as N 610 mg/L
TKN as N 625 mg/L
Noe+ NO3 as N 630 mg/L
P: Total as P 665 mg/L
GW-54 REV. 12187 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
Ag-Silver 46566 ug/L
AI -Aluminum 46557 ug/L
As -Arsenic 46551 ug/L
Ba-Barium 46558 ug/L
✓
Ca -Calcium 46552 mg/L
I ✓
Cd-Cadmium 46559 ug/L
Cr-Chromium 46559 ug/L
Cu-Copper46562 ug/L
Fe -Iron 46563 ug/L
Hg-Mercury 71900 ug/L
K-Potassium 46555 mg/L
Mg -Magnesium 46554 mg/L
Mn-Manganese 46565 ug/L
Na-Sodium 46556 mg/L
Ni-Nickel ug/L
Pb-Lead 46564 ug/L
Se -Selenium ug/L
Zn-Zinc 46567 ug/L
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile Organics (VOA bottle)
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival:

.F
Report to: ?'11, R t?
NC DENR/DWQ LABORATORY (check one):
GROUNDWATER SECTION
CHAIN OF CUSTODY (COC) RECORD
[y CENTRAL [ [ ARO [ I WaRO
Page ' of
For Investigation of: ALC tkv- lv\
Incident No.
Sample collector (print name)
and GW-54 forms completed by: T/`A, A
1
,J Sample collector's signature: 1r
Field storage conditions and location (when applicable):
Lab Use Only
LAB NO.
SAMPLE ID
QUAD. NO.
LOCATION
DATE
SAMPLED
TIME
SAMPLED
NUMBER
OF
CONTAINERS
�.iJSt'.L
t �ivc� y L&Ui,-*lvVk
2—
1-
F\titi�q t %-LAM �4JiIX�{v CO.
(signature):
Date
Time
Received by (signature):
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one): tare C Hand -delivered Federal Express . UPS
Other:
Security Type and Conditions:
Seal
Broken by:
INTRALABORATORY CHAIN OF CUSTODY - Lab Use Onlv
LAB NUMBERS
FROM THROUGH
NUMBER
BOTTLES
ANALYSES
REQUESTED
RELINQUISHED
BY:
RECEIVED
BY:
DATE
TIME
QA\Forms\Sample Receiving\COC form GW 4/10/Oldbs

t
North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
'--_— — —IF17
PLE TYPE ^A RoutiPeIORITY Lab Number
County_��\ I �_S(3f� aterr/ \1
O)Su
Quad No------- Serial No.------ -- oil tmeroencv Date Received_--__--_Time:—J
Lat.— Long.— Long.— Cs1�S -- ❑ Other Rec'd By: From:Bus, Courier; Hand Del.,
Q��
Chain of Custody Other:— — —___— --
Report To: ARO, FRO, RRRO, WaRO, WiRO, Data Entry By — — Ck:---__—
Data
WSRO, Kinston FO, Fed. Trust, Central Off., Other:— Reported: ---
Shipped by: Bus, Court H nd Del.,�ther:—_—_— __ __ ___ Purpose: —'�
Colleclor(s): ��__ ��_�v,'� "a` ^ Date_ _�J_tU Time�� �`? Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust Other:' ------
—__
FIELD ANALYSESOwnerL�'Z (circle one) _---_
— _--
pH ,�___— _ Spec. Cond.94— at 25°C Location or Site -vr �— s.�L— J�� t Kk;Li
Temp.lo _ C Odor________--_— Description of samplin point_—_F
Appearance—rCL ��3L�_S_Sf �`1 ��`���is� " �h Cv�Ot�amplingMethod_AV�AC�t �� ����5 .•—L�Y2 � Sample Interval—`✓_(�_"
Field Analysis B P T��- V F9� Aeu — _ Remarks ------
(Pumping
bale`. et`'� — ------
Y Y --- —1 ���—
(Pumping time, air temp., etc.)
LABORATORY ANALYSES
SOD 310
mg/L
COD High 340
mg/L
COD Low 335
mg/L
6
Coliform: MF FecalE31504
1100ml
Coliform: MF Total
/100mlTOC
680
mg/LTurbidity
76
NTUResidue,
Suspend0
mg/L
pH 403
units
Alkalinity to pH 4.5 410
mg/L
Alkalinity to pH 8.3415
mg/L
Carbonate 445
mg/L
Bicarbonate 440
mg/L
Carbon dioxide 405
mg/L
Chloride 940
mg/L
Chromium: Hex 1032
ug/L
Color: True 80
CU
Cyanide 720
mg/L
Lab Comme
Diss: Solids 70300
mg/L
Fluoride 951
mg/L
Hardness: Total 900
mg/L
Hardness (non-carb 902
mg/L
Phenols 32730
ug/I
Specific Cond. 95
uMhos/cm
Sulfate 945
mg/L
Sulfide 745
mg/L
Oil and Grease
mg/L
NH, as N 610
mg/L
TKN as N 625
mg/L
NO,+ NO, as N 630
mglL
P: Total as P 665
mg/L
GW-54 REV. 12/87 For Dissolved Analysis -submit filtered sample and write `DIS" in block.
Ag-Silver 46566
AI -Aluminum 46557
As -Arsenic 46551 .
Ba-Barium 46558
Ca -Calcium 46552
Cd-Cadmium 46559
Cr-Chromium 46559
Cu-Copper46562
Fe -Iron 46563
Hg-Mercury 71900
K-Potassium 46555
Mg -Magnesium 46554
Mn-Manganese 46565
Na-Sodium 46556
ckel
Pb-Lead 46564
Se -Selenium
Zn-Zinc 46567
u

North Carolina
GROUNDWATER FIELDIAB FORM DIVISDepartment Environment and Natural Resources
ION OF WATER QUALITY -GROUNDWATER SECTION
FSAMPLE TYPE SAMPLE PRIORITY
1 Routine Lab Number
County_ ^,-✓A`i) psC3%4-- ter ❑ Emeraencv Date Received__—_—_Time:—__Quad No—_--- Serial No.-- -----
er Rec'd By: From:Bus, Courier; Hand Del.,
Lat.— F'�,Long. G,N5
Chain of Custody Other:-- ----__----
Report To: ARO, FRO, MRO 'RRO, WaRO, WiRO, Data Entry By: _ — Ck:
Data
WSRO, Kinston FO, Fed. Trust, Central Off., Other:-- __ Reported:— __-- -
Shipped by: Bus, Cour' -, H nd Del., then._—_____—_ __-- _—_. Purpose:
_J�` 1� Date �� : lCJ Time_ 15�� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust Other: -------- —__
COIIeCiOr(S): ��' _— (circle one)
Owner—
------
FIELD ANALYSES Tv1v: __-----_--
—_--__
H 400__ _—_—__ Spec. Cond.94—= _ at 25°C Location or Site /v,�l
Temp.lo °C Odor_--__ --_ __ s __— Description of samplin point_— �_ -----
v"�� w H r cisN - 3(y�� F C��O9ampling Method �T� —1 vc_7 - �') — Sample Interval_
Appearance—� Y2 t fl�L 5- y fPumo. beKr. etc.l -- — ---
Field Analysis By: �_r"�—i_�1�`tc—^j--
(Pumping time, air temp., etc.)
BOD 310
COD High 340
COD Low 335
Coliform: MF Fecal 31616
Coliform: MF Total 31504
TOC 680
Turbidity 76
Residue, Suspended 530
l� pH 403
Alkalinity to pH 4.5 410
Alkalinity to pH 8.3 415
Carbonate 445
Bicarbonate 440
Carbon dioxide 405
Chloride 940
Chromium: Hex 1032
Color: True 80
Cyanide 720
Lab Comments
mg/L
mg/L
mg/L
/100ml
1100ml
mg/L
NTU
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ug1L
CU
mg/L
GW-54 REV. 12/87 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
Ag-Silver 46566
AI -Aluminum 46557
As -Arsenic 46551 .
Ba-Barium 46558
Ca -Calcium 46552
Cd-Cadmium 46559
I
omium 46559pper46562 46563rcury 71900ssium 46555gnesium 46554anganese 46565dium 46556kelad 46564leniumnc 46567
IL
ma/L
u

-MwDaVidson County Map Output Page
Page 1 of 2
Davidson County GIS
Scale: 1 in. = 608 ft.
Parcel Number: 0502400000035 Land Units:
Pin Id : 6784-03-04-4475 Deed Book:
CANAANLAND FREEWILL BAPTIST
Owner: 117 FANNIE PULLUM RD Deed Date:
THOMASVILLE NC 273600000
Property Address: 000117 FANNIE PULLUM RD Account Number:
Township: Conrad Hill Exempt Code:
Building Value: $116,820 Other Building Value:
1 AC
1367 Pg: 1684
12/03/2002
000009064558
1
$3,390
http://webgis. co.davidson.nc.uslservleticom. esri. esrimap.Esrimap?ServiceName=davidson... 7/22/2010

_;Davidson County Map Output Page
Page 2 of 2
Land Value: $22,300 Market Value: $142,510
Assessed Value: $142,510 Deferred Value: $0
Legal Description 1 : L35 BK1367-1684 Legal Description 2: NOAHTOWN RD
Additional Attributes
At point :1680601,744452
Fire Service Districts
Sq.Miles 16.86
Name FAIRGROVE FD
Townships
Sq. Miles 41.3
Name CONRAD HILL
County Zoning Districts
Zone RA-3
Soil Types
DSL Name BaD
Soil Name BADIN
Type CHAN N ERY-SILT-LOAM
Percent SI 8-15
Hydric
Municipal Boundary
No Features found.
The information contained on this map does not replace information that may be obtained by
consulting the official source of the information. In no event shall Davidson County, NC or the
consultants of Davidson County, NC be liable for any damages, direct or consequential, from the use
of the information contained on this map.
http://webgis.co.davidson.nc.uslservleticom. esri. esrimap.Esrimap?ServiceName=davidson... 7/22/2010

Davidson County Map Output Page
Page 1 of 2
Davidson County GIS
Fannie Pullam site
Scale: 1 in. = 608 ft.
Parcel Number :
0502400000036
Land Units:
5.79 AC
Pin Id :
6784-03-04-2351
Deed Book:
1073 Pg: 852
TURNER JACKIE
Owner:
165 FANNIE PULLUM ROAD Deed Date:
04/01/1998
THOMASVILLE NC
273600000
Property Address:
000165 FANNIE PULLUM RD Account Number:
000009036662
Township:
Conrad Hill
Exempt Code:
Building Value:
$90,490 Other Building Value:
$6,630
Land Value:
$31,240 Market Value:
$128,360
http://webgis.co.davidson.nc.us/servlet/com.esri.esrimap.EsAl
rimap. ervi e Ia[me=davidson... 7/22/2010

Davidson County Map Output Page
7 r
Page 2 of 2
Assessed Value: $128,360 Deferred Value: $0
Legal Description 1 : L36 BK1073-852 Legal Description 2: NOAHTOWN RD
Additional Attributes
At point :1680273,744369
Fire Service Districts
Sq.Miles 16.86
Name FAIRGROVE FD
Townships
Sq. Miles 41.3
Name CONRAD HILL
County Zoning Districts
Zone RA-3
Soil Types
DSL Name BaD
Soil Name BADIN
Type CHAN N ERY-SI LT -LOAM
Percent SI 8-15
Hydric
Municipal Boundary
No Features found.
The information contained on this map does not replace information that may be obtained by
consulting the official source of the information. In no event shall Davidson County, NC or the
consultants of Davidson County, NC be liable for any damages, direct or consequential, from the use
of the information contained on this ma .
http://webgis.co.davidson.nc.uslservleticom.esri.esrimap.Esrimap?ServiceName=davidson... 7/22/2010

Thomasville, NC - Google Maps
Page 1 of 1
Google- maps
aps Address Thomasville, NC Get Google Maps on your phone
1 Text the word "GMAPS" to 46645 3
/�'��' IK
http://maps.google.comlmaps?f=q&source=s_q&hl=en&geocode=&q=Thomasville,+NC&s... 5/3/2010

�19,� 4,;� — ip
s
i
Weatherford®
--n) N ne-P 1 (T 9 q N 9 1- 1

Report to: �A O GROUNDWATER SECTION Page � of �
CHAIN OF CUSTODY (COC) RECORD
NC DENR/DWQ LABORATORY (check one): IR CENTRAL [I ARO [ I WaRO
For Investigation of: ALc t},_)„\
Incident No.
Sample collector (print name) P TAMk,
and GW-54 forms completed by:
Sample collector's signature:
Field storage conditions and location (when applicable):
Lab Use Only
LAB NO.
SAMPLE ID
QUAD. NO.
LOCATION
DATE
SAMPLED
TIME
SAMPLED
NUMBER
OF
CONTAINERS
t-kN N-1 L&Lt.At4A , Q, � Co,
wiEsr S1w 6� C-Xi-u-,Ml.FA
S- -�I
/a: 1r, ,Y
2
MAY m 7
2010
�NCDFJTIZVIRU
otection
(signature):
Date
Time
b si r ):
Re v 14V,
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Relinquished by (signature):
Date
Time
Received by (signature):
Date
Time
Method of Shipment (circle one): ate C Hand -delivered Federal Express UPS
Other:
Security Type and Conditions:
Set
B enb:
TNTRALARORATORY CHAIN OF CUSTODY - Lah Ilse Only
LAB NUMBERS
FROM THROUGH
NUMBER
BOTTLES
ANALYSES
REQUESTED
RELINQUISHED
BY:
RECEIVED
BY
DATE
TIME
ill
g
Cs��LLN
0
QA\Fonns\Sample Receiving\COC form GW 4/10/01dbs

County:
DAVIDSON
Sample ID:
AB57813
River Basin
F U'.iATF
�4 9p
PO Number#
Received:
10G0232
05105/2010
Report To'
MROAP
O.
Date
Time Received:
08:25
Collector:
A PITNER
O Y
Labworks LoginlD
SMATHIS
Region:
MRO
Report Generated:
6/2/10
Sample Matrix:
SOIUSEDIMENT
Date Reported:
06/02/2010
Loc. Type:
SOIUSEDIMENT
/
Emergency Yes/No
VisitlD
COC Yes/No
YES
Loc. Descr.: TURNER
(�
Location ID:
MROAPNLC
Collect Date: 0510412010
Collect Time: 12:15
Sample Depth
CAS #
LAB
AnalYte Name
Sample temperature at receipt by lab
PQL
Result/
Qualifier
0.9
Units
°C
Ivletnoa
Reference
Finalysls
Date
515/10
Validated by
SMATHIS
WET
pH=in Soil' j'
ew,.r�=355 14" "'
PH Units
SW846/9045D
5/6/10
CGREEN
MET
7440-22-4
Ag in solid samples by ICPMS
0.2
0.20 U
mg/Kg
EPA 200.8
5126/10
ESTAFFORD1
7429-90-5
CAltl❑sOlid_Sarnples-lby ICP----`'
5
30000-" 'x-
mg/Kg
EPA 200.7
5125/10
ESTAFFORD1
7440-38-2
Arsenic solid samples by ICPMS
0.2
0.51 J3
mg/Kg
EPA 200.8
5/26/10
ESTAFFORD1
7440-38-3
Barium in solid samples by ICP
1
62
mg/Kg
EPA 20D.7
5125110
ESTAFFORD1
7440-43-9
Cadmium in solids samples by ICPMS
0.2
0.20 U
mg/kg
EPA 200.8
5/26/10
ESTAFFORD1
7440-70-2
Calcium in solid samples by ICP
10
160
mg/Kg
EPA 200.7
5125/10
ESTAFFORD1
744047-3
Cr in solids samples by ICPMS
0.2
23
mg/kg
EPA 200.8
5/26/10
ESTAFFORD1
7440-50-8
Cu solid samples by ICPMS
0.2
2.9
mg/kg
EPA 200.8
5126110
ESTAFFORD1
7439-97-6
Hg 245.5 solid
0.02
0.09
mg/Kg
EPA 245.5
5/11/10
ESTAFFORD1
7439-92-1
Lead in solids samples by ICPMS
0.2
19
mg/kg
EPA 200.8
5/25/10
ESTAFFORD1
7439-95-4
Mg in solid samples by ICP
10
130
mg/Kg
EPA 200.7
5/25/10
ESTAFFORD1
7439-96-5
Mn solid samples by ICPMS
0.2
7.8
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
7440-02-0
Nickel in solids samples by ICPMS
0.2
1.5
mg/kg
EPA 200.8
5/26110
ESTAFFORD1
Percent Dry Solids
69.7
%
EPA 200.2
5/11110
ESTAFFORD1
7782-49-2
Selenium in solids samples by ICPMS
0.2
0.41 J3
mg/kg
EPA 200.8
5/26/10
ESTAFFORD1
7440-09-7
Sodium in solid samples by ICP
10
130
mg/Kg
EPA 200.7
5/25/1D
ESTAFFORD1
7440-66-6
Zinc in solids samples by ICPMS
0.2
2.6
mg/kg
EPA 200.8
5/25/10
ESTAFFORD1
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Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
For a detailed description of the qualifier codes refer lo'rttp_!!pertal,.nrALrr ��r%.yeoivt;i la[?;%st�5ink.!techassist#Da!a Q�faf(pr_Crdes,jhtt ai.r;gR;il,n dgrtr oicfM�zh_wq. aC.=laRnfJ_echassist
Page 1 of 1

GROUNDWATER FIELD/LAB FORM
SAMPLE TYPE
�
Count --- Water
y—J°�_SoF� ❑
IA Soil
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
J,/
Routine
/
1 c) G- V X3 2,
Lab Number
❑ Emeraencv
Date Received
Quad No--__--__ Serial No.—_---_
❑ Other Rec'd By: From:Bus ourier, nd Del.,
Lat. - Long.— Cs,�S
Chain of Custody Other: _—__—__—
Report To: ARO, FRO, MRO�RRO, WaRO, WiRO, Data Entry B --__— Ck:
Data
WSRO, Kinston FO, Fed. Trust, Central Off., Other:-- Reported:-__ —__---_ — —
Shipped by: Bus, Couri , H nd Del., ther:--__—_ ---_. Purpose:
Collector(s): 1__ OiAE �`' to Date j �_( Time �� �� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust(Other:'-_____-_--
_�� — --* (circle one)
FIELD ANALYSES Owner T�ti� =-- 1
H aoo____— --_—__ Spec. Cond.94—_— __at 25°C Location or Site _-r��`�-------------
P _ _ __ Description of sampling point
Temp.to— -- °C Odor------- -- _-- Pp - r
Appearance—r2t� Co\_O�ampling Method— �c�'A7 Sample Interval-- ___ +'' J
(Pumo. bailer, elc.1
Field Analysis By:— C' �_T�_-1��a^°�_ — _ Remarks---_-- ------- —
(Pumping time, air temp., etc.)
n n -ATr" MV A nI AI VCGC _
La
Boo 310
COD High 340
COD Low 335
Coliform: MF Fecal 31616
Coliform: MF Total 31504
TOC 680
Turbidity 76
Residue, Suspended 530
b
pl-I 403
Alkalinity to pH 4.5 410
Alkalinity to pH 8.3 415
Carbonate 445
Bicarbonate 440
Carbon dioxide 405
Chloride 940
Chromium: Hex 1032
Color: True 80
Cyanide 720
Comments _
GW-54 REV. 12/87
1 J
■
Y
mg/L
mg/L
mg/L
/100ml
/100ml
mg/L
NTU
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
CU
mg/L
For Dissolved Analysis -submit filtered sample and write "DIS" in block.
Ag-Silver 46566
AI -Aluminum 46557
As -Arsenic 46551
Ba-Barium 46558
Ca -Calcium 46552
Cd-Cadmium 46559
'Cr-Chromium 46559
Cu-Copper
Fe -Iron 46563
Hg-Mercury 71900
K-Potassium 46555
Mg -Magnesium 46554
Mn-Manganese 46565
Na-Sodium 46556
Ni-Nickel
Pb-Lead 46564
Se -Selenium
Zn-Zinc 46567
ug/L
ug/L
ug/L
ug/L
mg/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/I
mg/I
ug/L
mg/
ug/L
ug/t
ugh
ua/I

County:
DAVIDSON
Sample ID:
AB57812
River Basin
A
�QF.
PO Number #
10G0231
05/05/2010
Report To
MROAP
O
Date Received:
j
C
Time Received:
08:25
Collector:
A PITNER
O
Labworks LoginlD
SMATHIS
Region:
MRO
Report Generated:
6/2/10
Sample Matrix:
SOIUSEDIMENT
Date Reported:
06/02/2010
Loc. Type:
SOIUSEDIMENT
Emergency Yes/No
VisitlD
COC Yes/No
YES
�j
Loc. Descr.: TURNER
0
Location ID:
MROAPNLC
Collect Date: 05104/2010
Collect Time: 12:15
Sample Depth
CAS #
LAB
Analyte Name
Sample temperature at receipt by lab
PQL
Result/Units
Qualifier
0.9
°C
Metnod
Reference
Analysis
Date
515/10
Validated by
SMATHIS
WET
-pH In Soil _: ' "'`
- - 3.5 �4 +
pH Units
SW846/9045D
5/6/10
CGREEN
MET
7440-22-4
Ag in solid samples by ICPMS
0.2
0.20 U
mg/Kg
EPA 200.8
5126/10
ESTAFFORDI
7429-90-5
Al in -solid sam_plesby ICP _ _ - �-
-----5-- -
-__ 30Q0:0r
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440-38-2
Arsenic solid samples by ICPMS
0.2
0.45 J3
mg/Kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-38-3
Barium in solid samples by ICP
1
67
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440A3-9
Cadmium in solids samples by ICPMS
0.2
0.20 U
mg/kg
EPA 200.8
5126/10
ESTAFFORDI
7440-70-2
Calcium in solid samples by ICP
10
350
mg/Kg
EPA 200.7
5/25110
ESTAFFORD1
7440-47-3
Cr in solids samples by ICPMS
0.2
22
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-50-8
Cu solid samples by ICPMS
0.2
2.8
mg/kg
EPA 200.8
5/26110
ESTAFFORDI
7439-97-6
Hg 245.5 solid
0.02
0.04
mg/Kg
EPA 245.5
5/11/10
ESTAFFORDI
7439-92-1
Lead in solids samples by ICPMS
0.2
19
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
7439-95-4
Mg in solid samples by ICP
10
54
mg/Kg
EPA 200.7
5125/10
ESTAFFORDI
7439-96-5
Mn solid samples by ICPMS
0.2
3.2
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
7440-02-0
Nickel in solids samples by ICPMS
0.2
1.5
mgfkg
EPA 200.8
5/26/10
ESTAFFORDI
Percent Dry Solids
73.6
%
EPA 200.2
5/11110
ESTAFFORDI
7782A9-2
Selenium in solids samples by ICPMS
0.2
0.34 J3
mg/kg
EPA 200.8
5/26/10
ESTAFFORDI
7440-09-7
Sodium in solid samples by ICP
10
150
mg/Kg
EPA 200.7
5/25/10
ESTAFFORDI
7440-66-6
Zinc in solids samples by ICPMS
0.2
1.7
mg/kg
EPA 200.8
5/25/10
ESTAFFORDI
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
of the qualifier codes refer to htt r.%1 fUn21�¢tier,[ortY�?ov_!Z''..gechassist#DB'.a Quil'.rper_Cr^I^s::httfr%itx;7atnc6rnr.nrq;�nr6/wq!j;fC�tila_ffin[�{echascist>
Fora tlelalletldescription Q L... k_..__ .. __. _._..__......__ .. -_..__- -._..--
Page 1 of 1

North Carolina
GROUNDWATER FIELD/LAB FORM Department ofEnviUALITtGROU and NaturalResources
DIVISION OF WATER (QUALITY-GROUNDW ER SECTION
_ SAMPLE TYPE SA PLE PRIORITY JB G � 51 i h
County I h.S�jN� _— ❑ Water Routine / Lab Number
y--=------------ J � ,
Soil Emeraencv v v Date Received 5_�,S` I" Time"
Quad No— ------ -- Serial No.-- ---------
--- ❑ Other Rec'd By*VV_
From:B Courier, and Del.,
Long. r,
-GAS -- yviChain of Custody Othe—Report To: ARO, FRO, RO�RRO, WaRO, WiRO, Data Ent _---_ Ck:_--_—__—
Data
WSRO, Kinston FO, Fed. Trust, Central Off., Other:—_—_---- Reported:—_— --_— _----
Shipped by: Bus, Couri , H nd Del., Cher:—__—_—_ _— --_—_. Purpose: ______—_—
Collector s : t1 _ t �s �'!f'_at� Date ,= Time�� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust Other:
— _� . � r Tyy e' -!y � — (circle one)
FIELD ANALYSES Owner-- ___ -------
pH 400-----_=---------- Spec. Cond.s4— at 25°C Location or Site _-- u` �——��i�d�'-_ ---------------
T e m p .1o_—__—
°C Odor_____________—__—___— Description of samplin poini___F__—
Appearance—r 2�"AL�—i_5"_�� `�—`Cp�O -Sampling Met
hod 1�� c L" ��Y�t Sample Interval_=v''1�1
(Pumo. bailer. etc.)
Field Analysis By: ---
(Pumping time, air temp., etc.)
LABORATORY ANALYSES
- ----- — i A silver 46566 „ten
BOD 310
COD High 340
COD Low 335
Coliform: MF Fecal 31616
Coliform: MF Total 31504
TOC 680
Turbidity 76
Residue, Suspended 530
t/ pH 403
All to pH 4.5 410
=dioxide
pH 6.3 415
445
440
xide 4050 Hex 1032
Color: True 80
Cyanide 720
Lab Comments
GW-54 REV. 12/87
r
J
mg/L
mg/L
mg/L
/100ml
/100ml
mg/L
NTU
mg/L
units
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
CU
mg/L
For Dissolved Analysis -submit filtered sample and write •DIS' in block.
9-
'Al-Aluminum v
AI -Aluminum 46557
As -Arsenic 46S51 .
Ba-Barium 46558
Ca -Calcium 46552
I
mium 46559
omium 46559pper46562 46563rcury 71900ssium 46555agnesium 46554anganese 46565dium 46556kelad 46564lenium
Zn-Zinc 46567
uo/L
u
mg/L
ug/L