WQ0039053_Residual Annual Report 2020_20210113

Initial Review
Reviewer Williams, Kendall
Is this submittal an application? (Excluding additional information.)*
r Yes r No
If not an application what is the submittal type?* r Annual Report
r Residual Annual Report
r Additional Information
r Other
Annual Report Year* 2020
Permit Number (IR)* WQ0039053
Applicant/Permittee Vaughn Stevenson
Email Notifications
Does this need review by the hydrogeologist?* r Yes r No
Regional Office Mooresville
CO Reviewer
Admin Reviewer [e-mail]

Submittal Form
Project Contact Information
Rease provide information on the person to be contacted by N B Staff regarding electronic receipt, another correspondence. ittal, confirmation of iptd othd
.......................................................... ronc su_ -
Name * Martin Mabe
Email Address*
[e-mail]
Project Information
........ ......... ....................................................................................................................................... .
Application/Document Type* r New (Fee Req ui red)
r Modification - Major (Fee Required)
r Renewal with Major Modification (Fee
Required)
r Annual Report
r Additional Information
r Other
Phone Number*
336-312-1396
O Modification - Minor
C Renewal
C GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
IT Residual Annual Report
r Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* r Wastewater Irrigation r High -Rate Infiltration
r Other Wastewater r Reclaimed Water
r Closed -Loop Recycle r Residuals
r Single -Family Residence Wastewater r Other
Irrigation
Permit Number:* WQ0039053
Fbs Current Existing pernit number
Applicant/Permittee Address* 530 Wood lawn Street, Belmont, NC 28012
Facility Name * Bio-Nomic Services, Inc.
Please provide comments/notes on your current submittal below.
Bio-Nomic Services, Inc. DCAR WQ0039053 - 2020 Annual Report
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form Engineering Rans, Specifications, Calculations, Bc.)
2020 Annual Report WQ0039053.pdf 21.58MB
Upload only 1 FLFdocurrent (less than 250 fvB). Miltiple documents rust be contained into one FDFfile unless file is larger than
upload limit.
* V By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order
and made payable to the North Carolina Department of Environmental Quality
(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
01V1a41!!;-1KMme
Submission Date 1/13/2021

2020 ANNUAL REPORT
LAND APPLICATION PROGRAM
BIO-NOMIC SERVICES, INC.
PERMIT #WQ0039053
Prepared For:
Bio-Nomic Services
530 Woodlawn St
Belmont, NC 28012
Compiled By:
Willcox & Mabe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
January 2021

willcox&mate
SOIL SOLUTIONS
January 13, 2021
NCDEQ-DWR Non -Discharge Branch
512 North Salisbury Street
9th Floor, Office #942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: 2020 LAND APPLICATION ANNUAL REPORT
Bio-Nomic Services, Inc.
Permit No. WQ0039053
WMSS Project No. 15-18 Ph: 09
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Bio-Nomic Services,
Inc. (Bio-Nomics) for the above referenced permit. WMSS compiled this report using data
gathered during the compliance year by Bio Nomics. This data includes: 1) Class A Annual
Distribution and Marketing / Surface Disposal Certification and Summary Form(s) (DMSDF),
2) Annual Residual Sampling Summary Forms) (ARSS), 3) Annual Pathogen and Vector
Attraction Reduction Form (2T) if required, and 4) Analytical Data.
Bio Nomics distributed a total of 2,566.07 Dry Tons of residual solids during the 2020
calendar year.
If there is any further information required or questions regarding this annual report please do
not hesitate to contact the Bio-Nomic Services, Inc. or WMSS for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
WMSS Projects1201511 5-18 Blo-Nomicsftase 09 - BNS Class A Permil12020 Annual Reporl12020 ANNUAL REPORT.docx
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road/ Summerfield, NC 273581 Rob 336.339.9128 or
Martin 336.312.13961www.willcoxmabesoil.com

Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
NC PERMIT # WQ0039053
Vaughn "Buck" Stevenson, Vice President
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
2020 Greenville Utilities WTP (NC0082139) Dry Tons 1,380,71
2020 Lake Rhodhiss WTP (NC0044164) Dry Tons 1,185.36
2020 Total Dry Tons 2,566.07
Total Dry Metric Tons 2,327.43

TABLE OF CONTENTS
SECTION NO. TITLE
I GUTSIA-1
II RSSF
III PVRF (2T)
IV Analytical Data

DMSDF

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039053 FACILITY NAME: Bio-Nomic Services, Inc.
PHONE: [phone] COUNTY: Gaston OPERATOR: Vaughn Stevenson - Vice President
FACILITY TYPE (please check one). ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
E Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes DYo ❑ --> If No skip parts A. B. C and certify form below
Part A*•
Part B*
Month
Sources(s) s) ( include NPDES # if
applicable)
Volume(dry tons)
Reci ient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
Lake Rhodhiss WTP NCO044164
845.73
845.73
Robert Snodgrass
845.73
Fertilizer
August
Lake Rhodhiss WTP NCO044164
339.63
339.63
Robert Snodgrass
339.63
Fertilizer
September
October
November
December
Total from FORM DMSDF (sup)l
0
0
0
0
Totals: Annual (dry tons):
0
1185.36
I18536
1185.36
Amendment(s) used: I
BulkingAgent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)l 0
Facility was compliant during the past calendar year with all conditions of the land application permit (including p Yes
but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"1. certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
f� 13,-;2 1
Signature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer"
(if different from Permittee)
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039053 FACILITY NAME: Bio-Nomic Services, Inc.
PHONE: [phone] COUNTY: Gaston OPERATOR: Vaughn Stevenson - Vice President
FACILITY TYPE (please check one): © Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
a Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar ear? Yes ENO ❑ —p- If No skip parts A, B, C and certify form below
Part A*•
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Reci lent Information
AmendmenU
Bulking A ent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
Greenville Utilities WTP NCO082139
183.96
183.96
City of Greenville
183.96
M . ay
Greenville Utilities WTP NCO082139
113.53
113.53
City of Greenville
113.53
June
Greenville Utilities WTP NCO082139
239.06
239.06
City of Greenville
239.06
July
Greenville Utilities WTP NCO082139
274.52
274.52
City of Greenville
274,52
August
Greenville Utilities WTP NCO082139
229.37
229.37
City of Greenville
229.37
September
Greenville Utilities WTP NCO082139
340.27
340.27
City of Greenville
340.27
October
November
December
Total from FORM DMSDF (sup)
0
0
0
0
Totals: Annual (dry tons):
0
1380.71
1380.71
1380.71
Amendment(s) used:
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)l 0
Facility was compliant during the past calendar year with all conditions of the land application permit (including 0 Yes
but not limited to items I-3 below) issued by the Division of Water Resources: ❑ No '> If No, Explain in Narritive
I. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I -certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
7/ `i -1/
Signature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Permittee)
Date
DENR FORM DMSDF (12/2006)

RSSF

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0039053 Laboratory: 1)
Facility Name: Bio-Nomic Services, Inc. 2)
Residual Source WQ # or NPDES NCO082139 3)
#: 4)
WWTP Name: Lake Rhodhiss WTP 5)
Residual Annlvsis Data
Waypoint Analytical
Parameter
(mg/kg)
Ceiling
Cone. Limit
m k a
Sample or Composite Date
8/17/20
8/17/20
8/17/20
8/17/20
8/17/20
8/17/20
Percent Solids (%)
33
35.2
32.5
36.7
37.6
35.8
Arsenic
8.36
7.87
7.97
7.22
6.626
6.4
Cadmium
0.303
0.327
1 0.326
0.313
0.38
0.279
Copper
37.3
35.2
36.9
32.2
33
30.7
Lead
34.2 1
35.8
32.3
31.9
44.1
33.5
Mercury
0.0575
0.0505
0.418
0.0509
0.0529
0.0553
Molybdenum
1.89
1.66
1.7
1.54
I.57
1.57
Nickel
19.7
19.2
20.4
19.8
17.7
17.7
Selenium
Zinc
1.52
203
1.42
272
1.54
256
1.36
208
1.33
197
1.4
213
TKN
Ammonia- Nitrogen
Nitrate and Nitrite
Total Phosphorus
6640
1200
40.6
1890
5600
736 1
60
1740
6860
892
196
1780
6380
872
1830
I600
5880
973
107
1610
5390
520
21.7
1460
rVL surinca LMPV 11 tacIJILICs the cemng concentranon timus ustea in tnis Torm are not applicable. Keterence the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
�- 47-a!
Date
DENR FORM RSSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or NPDES
WQ0039053
Bio-Nomic Services, Inc.
NCO082139
WWTP Name: Greenville Utilities WTP
Residual Analysis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Cone. Limit
m k a
Sample or Composite Date
3/16/20
4/27/20
7/23/20
9/11/20
Percent Solids (%)
2.32
20.3
15.20
16.3
Arsenic
0.50
12.60
11.60
16.10
Cadmium
0.10
0.49
0.66
0.61
Copper
3.20
265.00
338.00
319.00
Lead
0.41
24.10
14.20
23.10
Mercury
0.016
0.372
0.459
0.313
Molybdenum
0.25
2.17
1.74
1.53
Nickel
0.25
14.50
I2.80
13.60
Selenium
0.50
2.46
5.26
4.93
Zinc
1.40
61.10
58.20
58.80
TKN
659
11900
11900
13200
Ammonia- Nitrogen
167
626
329
307
Nitrate and Nitrite
4.73
44.50
152.00
36.10
Total Phosphorus
33.9
2820
2480
3260
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting
false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T _1102 (26)
DENR FORM RSSF (12/2006)

PVRF 2T

Lake Rhodhiss WTP and Greenville Utilities WTP is not required by permit to perform Pathogen
Reduction or Vector Attraction Reduction Monitoring, therefore no PVRF 2T Form has been included
in this report.

ANALYTICAL DATA

Greenville Utilities WTP is an ongoing annual dredge and dewatering project at the alum lagoon at the
respective plant. The project actually began in April of 2020 and finished in September 2020. The
sampling frequency is quarterly (or 4 times per year) which is determined by the amount of dry tons
distributed in 2020. Four sets of nutrient and metal analyses were performed during 2020 to satisfy the
permit condition outlined in Attachment A. One TCLP analysis has also been included.
Initial calculations for the alum lagoon cleanout at Lake Rhodhiss WTP indicated that a bi-monthly (or
6 times per year) sampling frequency should be considered based upon an anticipated 2,000 dry tons.
This project was performed in accordance with a lagoon cleanout at the facility. The residual solids
were mechanically removed from the lagoons and stockpiled on site prior to land application activities
beginning. The project only lasted for approximately two months. Six composite nutrient and metal
analyses were collected from the stockpile on the same day. However, due to the amount of residuals
that were land applied (1,185.36 DT's), only four analyses are required by permit. WMSS, PLLC and
Bio-Nomic Services, Inc. elected to use all six nutrient and metal analyses that were collected during the
two month window of actual land application activities from the stockpiles to best represent the actual
material being land applied. One TCLP analysis has also been included.

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lake Rhodhiss WTP
33.00 % Solids
5.8 pH
Permit No. WQ0039053
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
0.664
6,640.000
13,280
Phosphorus
0.189
1,890.000
3.780
Potassium
0.162
1,620.000
3.240
PAN (injected)*
0.233
3,869.500
7.739
PAN (surface)*
0.173
3,77T000
7.554
Ammonia Nitrogen
0.120
1,200.000
2.400
Calcium
0.142
1,420.000
2.840
Calcium Carbonate E .
5.400
54,000,000
108.000
Magnesium
0.211
2,110.000
4.220
Sodium
0.008
75.800
0.152
Sulfur
---
3480.000
6.960
Nitrate N / Nitrite N
---
40.600
0.081
Barium
Chloride
---
---
---
---
---
---
SAR
0.17
Iron
---
---
---
Ceiling Concen.
(M tK )
Aluminum
---
11,200.00
22.400
Arsenic
---
8.36
0.017
75
Cadmium
---
0.303
0,001
85
Chromium
---
82.700
0,165
---
Copper
---
37.30
0.075
4,300
Lead
---
34.20
0.068
840
Mercury
---
0,0575
0.000
57
Molybdenum
---
1.89
0,004
75
Nickel
---
19.70
0,039
420
Selenium
---
1.52
0.003
100
Zinc
---
203.00
0.406
7,500
Waypoint# 20-232-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or ¢ detection limits are listed as detection limits
for calculation purposes.
♦ E t
wiIlcox&mabe
Prepared By; SO I L SO LUT I ON S

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lake Rhodhiss WTP Permit No. WQ0039053
35.20 % Solids
5.8 pH
Parameter
%
Mg/Kg Dry Weight
x 10,000
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
0.560
5,600.000
11.200
Phosphorus
0.174
1,740.000
3.480
Potassium
0.165
t,650.000
3.300
PAN injected)*
0.177
3,869.500
7.739
PAN surface)*
0.140
3,777.000
7.554
Ammonia Nitrogen
0.074
736.000
1.472
Calcium
0.135
1,350.000
2.700
Calcium Carbonate E _
5.000
50,000.000
100.000
Magnesium
0.220
2,200.000
4.400
Sodium
0.007
71.000
O.I42
Sulfur
---
3750.000
7.500
Nitrate N / Nitrite N
---
60.200
0.120
Barium
---
---
---
SAR
0.16
Chloride
---
---
Iron
---
---
---
Ceiling Concen.
(M /K )
Aluminum
---
105,000.00
210.000
Arsenic
--
7.87
0.016
75
Cadmium
---
0.327
0,001
85
Chromium
---
75.600
0,151
--
Copper
---
35.20
0.070
4,300
Lead
---
35.80
0.072
840
Mercury
--
0.0505
0.000
57
Molybdenum
---
1.66
0.003
75
Nickel
---
19.20
0.038
420
Selenium
---
1.42
0.003
100
Zinc
---
272.00
0.544
7,500
Waypoint4 20-232-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or ¢ detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: S 0 1 L S O L U T I O N S

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lake Rhodhiss WTP Permit No. WQ0039053
32.50 % Solids
5.9 pH
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
0.686
6,860.000
13.720
Phosphorus
0.178
1,780.000
3.560
Potassium
0.169
1,690.000
3.380
PAN (injected)*
0.228
3,869.500
7.739
PAN (surface)*
0,184
3,777.000
7.554
Ammonia Nitrogen
0.089
892.000
1.784
Calcium
0.101
1,010.000
2.020
Calcium Carbonate E .
5.400
54,000.000
108.000
Magnesium
0.204
2,040.000
4.080
Sodium
0.008
76.900
0.154
Sulfur
---
3170.000
6.340
Nitrate N /Nitrite N
---
196.000
0.392
Barium
---
---
SAR
0.18
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
M /K )
Aluminum
---
104,000.00
208,000
Arsenic
---
7.97
0,016
75
Cadmium
---
0.326
0.001
85
Chromium
---
78.800
0.158
---
Copper
---
36.90
0.074
4,300
Lead
---
32.30
0.065
840
Mercury
---
0.4180
0.001
57
Molybdenum
---
1.70
0.003
75
Nickel
--- 1
20.40
0.041
420
Selenium
---
1.54
0.003
1 100
Zinc
---
256.00
0.512
7,500
Waypoint# 20-232-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(FKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application;
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.
41
willcox&mabe
Prepared By: SOI L SOLUTIONS

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lake Rhodhiss WTP Permit No. WQ0039053
36.70 % Solids
6.1 pH
Parameter
%
JMg/Kg Dry Weight
(% x 10,0001
Pounds/Dry Ton
(MgLKg (Mg/Kgx 0.002)
Nitrogen (TKN)
0.638
6,380.000
12.760
Phosphorus
0.160
1,600.000
3.200
Potassium
0.154
1,540.000
3.080
PAN injected)*
0.380
3,869.500
7.739
PAN surface)*
0.337
3,777,000
7.554
Ammonia Nitrogen
0.087
872,000
1.744
Calcium
0.169
1,690.000
3.380
Calcium Carbonate E .
5.100
51,000.000
102.000
Magnesium
0.223
2,230.000
4.460
Sodium
0.007
68.100
0.136
Sulfur
---
2940.000
5.880
Nitrate N / Nitrite N
---
1,830.000
3.660
Barium
---
---
--
SAR
0.15
Chloride
---
---
Iron
---
---
---
Ceiling Concen.
(mg/Kg)
Aluminum
---
91,300.00
182.600
Arsenic
---
7.22
0.014
75
Cadmium
---
0.313
0.001
85
Chromium
---
67.800
0.136
--
Copper
---
32.20
0.064
4,300
Lead
--
31.90
0.064
840
Mercury
---
0,0509
0.000
57
Molybdenum
---
1.54
0.003
75
Nickel
---
19.80
0.040
420
Selenium
---
1.36 1
0.003
100
Zinc
--
208.00
0.416
7,500
Waypoint4 20-232-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application.
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or a detection limits are listed as detection limits
for calculation purposes.
t � e
�1
willcox&me be
Prepared By: S O I L S 0 L U T 1 0 N S

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lace Rhodhiss WTP Permit No. WQ0039053
37.60 % Solids
7 pH
Parameter
11
%
lMg/KgDryWeight
(% x 10,000)
Pounds/Dry Ton
__(Mg/KM x 0.002)
Nitrogen (TKN)
0.588
5,880.000
11.760
Phosphorus
0.161
1,610.000
3.220
Potassium
0.152
1,520.000
3.040
PAN (injected)*
0.206
3,869.500
7.739
PAN (surface)*
0.157
3,777.000
7.554
Ammonia Nitrogen
0.097
973.000
1.946
Calcium
0.222
2,220.000
4.440
Calcium Carbonate E .
4.500
45,000.000
90.000
Magnesium
0.233
2,330.000
4.660
Sodium
0.007
66.500
0.133
Sulfur
---
2740.000
5.480
Nitrate N / Nitrite N
---
I07.000
0.214
Barium
Chloride
---
---
---
---
---
---
SAR
0.14
Iron
---
---
---
Ceiling Concen.
(Mg/Kg)
Aluminum
---
90,400.00
180.800
Arsenic
---
6.63
0.013
75
Cadmium
---
0.380
0.001
85
Chromium
---
67.300
0.135
-
Copper
---
33.00
0.066
4,300
Lead
---
44.10
0.088
840
Mercury
---
0.0529
0.000
57
Molybdenum
---
1.57
0.003
75
Nickel
---
17.70
0.035
420
Selenium
---
1.33
0.003
100
Zinc
---
197.00
0.394
7,500
Waypointff 20-232-0006
'Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
• E
Willcox&mabe
Prepared By: SOIL SOLUTIONS

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 17, 2020
Lake Rhodhiss WTP Permit No. WQ0039053
35.80 % Solids
6.2 pH
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(M x 0.0021
Nitrogen (TKN)
0.539
5,390.000
10.780
Phosphorus
0.146
1,460.000
2.920
Potassium
0.150
1,500.000
3.000
PAN (injected)*
0.152
3,869.500
7.739
PAN surface)*
0.126
3,777.000
7.554
Ammonia Nitrogen
0.052
520.000
1.040
Calcium
0.181
1,810.000
3.620
Calcium Carbonate E .
7.600
76,000.000
152.000
Magnesium
0.204
2,040.000
4.080
Sodium
0.007
69.800
0.140
Sulfur
---
2850.000
5.700
Nitrate N / Nitrite N
---
21.700
0.043
Barium
---
---
---
SAR
0.16
Chloride
---
---
---
Iron
---
---
---
Ceiling Concen.
M IK )
Aluminum
---
84,100.00
168.200
Arsenic
---
6.40
0.013
75
Cadmium
---
0.279
0.001
85
Chromium
---
62.000
0.124
---
Copper
---
30.70
0.061
4,300
Lead
---
33.50
0.067
840
Mercury
---
0.0553
0.000
57
Molybdenum
---
1.57
0.003
75
Nickel
---
17.70
0.035
420
Selenium
---
1.40
0.003
100
Zinc
---
213.00
0.426
7,500
waypoint# 20-232-0006
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection Iimits are listed as detection limits
for calculation purposes.
Willcox&mabe
Prepared By: SOIL SOLUTIONS

r
Waypoint 7621 Whitepine Road, Richmond, VA23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-232-0006
Client Project Description: Lencit-2
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
73416
1
Solids
08/17/2020 06:00
08/19/2020
73416
1
Solids
08/17/2020 06:00
08/19/2020
AOAC 955.01
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
4500NO3F-2011
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
9045D
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SM-254OG
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
6010D
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SW-7471B
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SM-4500-NH3C
WP MTN
73416
1
Solids
08/17/2020 06:00
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73417
2
Solids
08/17/2020 06.15
08/19/2020
73417
2
Solids
08/17/2020 06:15
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
SM-4500-NH3C
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
SM-2540G
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
4500NO3F-2011
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
AOAC 955.01
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
SW-7471B
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
9045D
WP MTN
73417
2
Solids
08/17/2020 06:15
08/19/2020
6010D
WP MTN
73418
3
Solids
08/17/2020 0630
08/19/2020
73418
3
Solids
08/17/2020 06:30
08/19/2020
6010D
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
9045D
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
4500NO3F-2011
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
SM-254OG
WP MTN
73418
3
Solids
08/17/2020 0630
08/19/2020
SW-7471B
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
SM-4500-NH3C
WP MTN
73418
3
Solids
08/17/2020 06:30
08/19/2020
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 19

e
r
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-232-0006
Client Project Description: Lencit-2
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
73419
4
Solids
08/17/2020 06:40
08/19/2020
73419
4
Solids
08/17/2020 06:40
08/19/2020
SM-4500-NH3C
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
SM-2540G
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
AOAC 955.01
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
9045D
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
SW-7471B
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
6010D
WP MTN
73419
4
Solids
08/17/2020 06:40
08/19/2020
4500NO3F-2011
WP MTN
73419
4
Solids
08/17/2020 06.40
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
73420
5
Solids
08/17/2020 06:50
08/19/2020
9045D
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SW-7471B
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
6010D
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
4500NO3F-2011
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SM-4500-NH3C
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
SM-2540G
WP MTN
73420
5
Solids
08/17/2020 06:50
08/19/2020
AOAC 955.01
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
73421
6
Solids
08/17/2020 07:00
08/19/2020
9045D
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
SW-7471B
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
6010D
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
4500NO3F-2011
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
SM-4500-NH3C-TKN
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
SM-4500-NH3C
WP MTN
73421
6
Solids
08/17/2020 07:00
08/19/2020
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page-3 of 19

(D
Waypoint 7621 Whitepine Road, Richmond, VA23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-232-0006
Client Project Description: Lencit-2
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
73421 6 Solids 08/17/2020 07:00 08/19/2020 AOAC 955.01 WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 19

(2)
Way
•
PAo� nt-.,
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 °
Fax [phone]
NALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report
Date : 08/27/2020
530 Woodlawn St
Information :
Received : 08/19/2020
Belmont, NC 28012
Report Number: 20-232-0006
REPORiOPANALYSIS
Pauric Mc Groary Ph.D., CPAAgronomist
Lab No : 73416
Matrix:
Solids
Sample ID : 1
Sampled:
8/17/2020
6:00
Test
Results
units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
67.0
%
0.010
1
08/24/2014:00
FMM
SM-254OG
Calcium Carbonate Equivalent 5.4
% - dry
0.1
1
08/26/20 09:44
DXT
AOAC 955.01
Test
Results
Units
MQL
DF
Date ! Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
1200
mg/Kg - dry
179
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
40.6
mg/Kg - dry
14.0
1
08/26/20 14:36
ZBD
4500NO3F-2011
Organic N
5420
mg/Kg - dry
758
1
08/26/20 11:00
CALCULATION
pH
5.8
SM.
1
08/24/2012:57
ADM
9045D
Total Solids
33.0
0.010
1
08/24/20 14:00
FMM
SM-2540G
Total Volatile Solids
24.2
0.010
1
06/24/2014:00
FMM
SM-2540G
Total Kjeldahl Nitrogen
6640
mg/Kg - dry
758
1
08/26/20 11:00
JPJ iM-4500-NH3C-TKP
Phosphorus
1890
mg/Kg - dry
15.2
1
08/24/20 22:45
TJS
6010D
Aluminum
11200
mg/Kg - dry
15.2
1
08/25/20 19:31
]ADS
6010D
Arsenic
8.36
mg/Kg - dry
1.52
1
08/24/20 22:45
TJS
6010D
Calcium
1420
mg/Kg - dry
152
1
08/25/20 19:26
DADS
6010D
Cadmium
<0.303
mg/Kg - dry
0.303
1
08/24/20 22:45
TJS
6010D
Chromium
82.7
mg/Kg - dry
0.757
1
08/24/20 22:45
TJS
6010D
Copper
37.3
mg/Kg - dry
1.52
1
08/24/20 22:45
TJS
6010D
Iron
30300
mg/Kg - dry
30.3
1
08/24/20 22:45
]ADS
6010D
Lead
34.2
mg/Kg - dry
0.909
1
08/24/20 22:45
TJS
6010D
Qualifiers/ DF
Dilution Factor
L Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 19

(D
Waypoint,
7621 Whitepine
Road, Richmond, VA23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information :
Received : 08/19/2020
Belmont , NC 28012
17QI' Dw
Report Number :20-232-OOD6
REPDRTD>CANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73416
Matrix: Solids
Sample ID : i
Sampled: 8/17/2020 6:00
Test
Results
Units
MOL
DF
Date / Time By Analytical
Analyzed Method
Magnesium
2110
mg/Kg - dry
15.2
1
08/25/20 19:26 DADS 6010D
Manganese
906
mg/Kg - dry
1.52
1
08/24/20 22:45 TJS 6010D
Mercury 0.0575
mg/Kg - dry
0.0454
1
08/24/20 13:48 DDB SW-74718
Molybdenum
1.89
mg/Kg - dry
0.757
1
08/25/20 19:26 ]ADS 6010D
Nickel
19.7
mg/Kg - dry
0.757
1
08/25/20 19.26 ]ADS 6010D
Potassium
1620
mg/Kg - dry
30.3
1
08/24/20 22:45 TJS 6010D
Selenium
<1.52
mg/Kg - dry
1.52
1
08/24/20 22:45 TJS 6010D
Sodium
<75.8
mg/Kg - dry
75.8
1
08/24/20 22:45 TJS 6010D
Zinc
203
mg/Kg - dry
3.79
1
08/24/20 22:45 TJS 6010D
Sulfur
3480
mg/Kg - dry
30.3
1
08/24/20 22:45 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 6 of 19

a
Waypoint,'
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn 5t
Information:
Received: 08/19/2020
Belmont, NC 28012
i
19 QD IV
Report Number: 20-232-0006
REPORT OFANACYSIS Pauric Mc Groary Ph.D„ CPAAgronomist
Lab No : 73417
Matrix: Solids
Sample ID: 2
Sampled: 8/17/2020 6:15
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Moisture
64.8
%
0.010 1 08/2412014:00 FMM SM-2540G
Calcium Carbonate Equivalent
5.0
% - dry
0.1 1 08/26/20 09:44 DKT AOAC 955.01
Test
Results
Units
MQL DF Date 1 Time By Analytical
Analyzed Method
Ammonia Nitrogen
736
mg/Kg - dry
164
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
60.2
mg/Kg - dry
14.2
1
08/26/20 14:36
ZBD
4500NO3F-2011
Organic N
4860
mg/Kg - dry
710
1
08/26/20 11:00
CALCULATION
pH
5.8
S.U.
1
08124/2012:57
ADM
9045D
Total Solids
35.2
%
0.010
1
08/24/20 14:00
FMM
SM-2540G
Total Volatile Solids
23.0
%
0.010
1
08/24/20 14:00
FMM
SM-2540G
Total Kjeldahl Nitrogen
5600
mg/Kg - dry
710
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1740
mg/Kg - dry
14.2
1
08/24/20 22:50
TJS
6010D
Aluminum
105000
mg/Kg - dry
142
10
08/25/20 19:42
]ADS
6010D
Arsenic
7.87
mg/Kg - dry
1.42
1
08/24/20 22:50
TJS
6010D
Calcium
1350
mg/Kg - dry
142
1
O8/25/20 19:37
]ADS
6010D
Cadmium
0.327
mg/Kg - dry
0.284
1
O6/24/20 22:50
TJS
6010D
Chromium
75.6
mg/Kg - dry
0.710
1
O8/24120 22:50
TJS
6010D
Copper
35.2
mg/Kg - dry
1.42
1
08/24/20 22:50
T]S
6010D
Iron
36100
mg/Kg - dry
284
10
08/25/20 19:42
]ADS
6010D
Lead
35.8
mg/Kg - dry
0.852
1
08/24/20 22:50
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 7 of 19

(D
s
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °
Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information :
Received : 08/19/2020
Belmont, NC 28012
Report Number : 20-232-0006
REPORTOFANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73417
Matrix: Solids
Sample ID : 2
Sampled: 8/17/2020 6:15
Test
Results
Units
MOL
DF
Date / Time By Analytical
Analyzed Method
Magnesium
2200
mg/Kg - dry
14.2
1
08/25/20 19:37 ]ADS 6010D
Manganese
994
mg/Kg - dry
1.42
1
08/24/20 22:50 TJS 6010D
Mercury 0.0505
mg/Kg - dry
0.0420
1
08/24/20 13:49 DDB SW-7471B
Molybdenum
1.66
mg/Kg - dry
0.710
1
08/25/20 19:37 ]ADS 6010D
Nickel
19.2
mg/Kg - dry
0.710
1
08/25/20 19:37 ]ADS 6010D
Potassium
1650
mg/Kg - dry
28.4
1
08/24/20 22:50 TJS 6010D
Selenium
<1,42
mg/Kg - dry
1.42
1
08/24/20 22:50 TJS 6010D
Sodium
<71.0
mg/Kg - dry
71.0
1
08/24/20 22:50 TJS 6010D
Zinc
272
mg/Kg - dry
3.55
1
08/24/20 22:50 TJS 6010D
Sulfur
3750
mg/Kg - dry
28.4
1
08/24/20 22:50 TJS 60101D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 8,of 19

Waypoint-
(2)
ANALYTICAL
45671
Bio-Nomic Service Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Report Number: 20-232-0006
Lab No : 73418
Sample ID : 3
Project Lencit-2
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT 0FANALYSIS
Report Date: 08/27/2020
Received: 08/19/2020
i kD W
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/17/2020 6:30
Test
Results
Units
MQL
DF Date I Time
Analyzed
By
Analytical
Method
Moisture
67.5
%
0.010
1 08/24/2014:00
FMM
SM-254OG
Calcium Carbonate Equivalent
5.4
% -dry
0.1
1 08/26/20 09:44
DXT
AOAC 955.01
Test
Results
Units
MQL
DF Date 1 Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
892
mg/Kg - dry
181
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+ N itrite-N
196
mg/Kg - dry
14.5
1
08/26/20 14:37
ZBD
4500NO3F-2011
Organic N
5970
mg/Kg - dry
769
1
08/26/20 11:00
CALCULATION
pH
5.9
S.U.
1
08/24/2012:57
ADM
9045D
Total Solids
32.5
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Volatile Solids
23.8
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Kjeldahl Nitrogen
6860
mg/Kg - dry
769
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1780
mg/Kg - dry
15.4
1
08/24/20 22:56
TJS
GD10D
Aluminum
104000
mg/Kg - dry
154
10
08/25/20 19:53
]ADS
6010D
Arsenic
7.97
mg/Kg - dry
1.54
1
08/24/20 22:56
TJS
6D10D
Calcium
1010
mg/Kg - dry
154
1
08/25/20 19:47
]ADS
6010D
Cadmium
0.326
mg/Kg - dry
0.308
1
08/24/20 22:56
TJS
6010D
Chromium
78.8
mg/Kg - dry
0.769
1
08/24/20 22:56
TJS
6010D
Copper
36.9
mg/Kg - dry
1.54
1
08/24/20 22:56
TJS
6010D
Iron
35100
mg/Kg - dry
308
10
08/25/20 19:53
JADS
6010D
Lead
32.3
mg/Kg - dry
0.923
1
08/24/20 22:56
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quaniitation Limit
Page 9 of 19

0
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °
Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information:
Received : 08/19/2020
Belmont, NC 28012
Pauric Mc Groary Ph.D., CPA
Report Number: 20-232-0006
REPOR T OF A NA L YSIS
Agronomist
Lab No: 73418
Matrix: Solids
Sample ID : 3
Sampled: 8/17/2020 6:30
Test
Results
Units
MOL
DF
Date I Time By Analytical
Analyzed Method
Magnesium
2040
mg/Kg - dry
15.4
1
08/25/20 19:47 ]ADS 6010D
Manganese
914
mg/Kg - dry
1.54
1
08/24/20 22:56 TJS 6010D
Mercury
0.418
mg/Kg - dry
0.0470
1
08/24/20 13:50 DDB SW-7471B
Molybdenum
1.70
mg/Kg - dry
0.769
1
08/25/20 19:47 JADS 6010D
Nickel
20.4
mg/Kg - dry
0.769
1
08/25/20 19:47 ]ADS 6010D
Potassium
1690
mg/Kg - dry
30.8
1
08/24/20 22:56 T]S 6010D
Selenium
<1.54
mg/Kg - dry
1.54
1
08/24/20 22:56 TJS 6010D
Sodium
<76.9
mg/Kg - dry
76.9
1
08/24/20 22:56 TJS 6010D
Zinc
256
mg/Kg - dry
3.85
1
08/24/20 22:56 TJS 6010D
Sulfur
3170
mg/Kg - dry
30.8
1
08/24/20 22:56 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 10 of 19

0
•
Waypoint.
7621 Whi#spine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Service Inc
Project
Lencit 2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information :
Received : 08/19/2020
Belmont, NC 28012
Pauric Mc Groary Ph.D., CPAAgronomist
Report Number: 20-232-0006
REPORT OFAN,4LYSIS
Lab No : 73419
Matrix: Solids
Sample ID : 4
Sampled: 8/17/2020 6:40
Test
Results
Units
MQL DF Date I Time By Analytical
Analyzed Method
Moisture
63.3
%
0.010 1 08/24/20 14:00 FMM SM-2540G
Calcium Carbonate Equivalent
5.1
% - dry
0.1 1 08/26/20 09:44 DXT AOAC 955.01
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
872
mg/Kg - dry
162
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
1830
mg/Kg - dry
13.6
1
08/26/20 14.37
ZBD
4500NO3F-2011
Organic N
5500
mg/Kg - dry
681
1
08/26/20 11:00
CALCULATION
pH
6.1
S.U.
1
08/24/2012:57
ADM
9045D
Total Solids
36.7
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Volatile Solids
22.9
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Kjeldahl Nitrogen
6380
mg/Kg - dry
681
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1600
mg/Kg - dry
13.6
1
08/24/20 23:01
TJS
6010D
Aluminum
91300
mg/Kg - dry
136
10
08/25/20 20:14
]ADS
6010D
Arsenic
7.22
mg/Kg - dry
1.36
1
08/24/20 23:01
TJS
6010D
Calcium
1690
mg/Kg - dry
136
1
08/25/20 20:08
]ADS
6010D
Cadmium
0.313
mg/Kg - dry
0.272
1
08/24/20 23:01
TJS
6010D
Chromium
67.8
mg/Kg - dry
0.681
1
08/24/20 23:01
TJS
6010D
Capper
32.2
mg/Kg - dry
1.36
1
08/24/20 23:01
TJS
6010D
Iron
27200
mg/Kg - dry
27.2
1
08/24/20 23:01
]ADS
6010D
Lead
31.9
mg/Kg - dry
0,817
1
08/24/20 23:01
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 11 of 19

0
Waypoint.
7621 Whitepine
Road, Richmond, VA 23237
Main 804-743-9401 °
Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information :
Received: 08/19/2020
Belmont, NC 28012
L
Report Number ; 20-232-0006
REPORT OFANQLYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73419
Matrix: Solids
Sample ID: 4
Sampled: 8/17/2020 6:40
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Magnesium
2230
mg/Kg - dry
13.6
1
08/25/20 20:08 )ADS 6010D
Manganese
812
mg/Kg - dry
1.36
1
08/24/20 23:01 TJS 6010D
Mercury 0.0509
mg/Kg - dry
0.0381
1
08/24/20 13:52 DDB SW-7471B
Molybdenum
1.54
mg/Kg - dry
0.681
1
08/26/20 17:31 ]ADS 6010D
Nickel
19.8
mg/Kg - dry
0.681
1
08/25/20 20:08 ]ADS 6010D
Potassium
1540
mg/Kg - dry
27.2
1
08/24/20 23:01 TJS 6010D
Selenium
<1.36
mg/Kg - dry
1.36
1
08/24/20 23:01 TJS 6010D
Sodium
<68.1
mg/Kg - dry
68.1
1
08/24/20 23:01 TJS 6010D
Zinc
208
mg/Kg - dry
3.41
1
08/24/20 23.01 TJS 6010D
Sulfur
2940
mg/Kg - dry
27.2
1
08/24/20 23:01 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 12 of 19

s
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.corn
45671
Bio-Nomic Servics Inc
Project
Lendt-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information :
Received : 08/19/2020
Belmont, NC 28012?awf�
i
Report Number: 20-232-0006
REPOR T OF A NA L YSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73420
Matrix: Solids
Sample ID : 5
Sampled: 8/17/2020 6:50
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Moisture
62.4
%
0.010 1 08/24/20 14:00 FMM SM-254OG
Calcium Carbonate Equivalent
4.5
% - dry
0A 1 08/26/20 09:44 DXT AOAC 955.01
Test
Results
Units
MQL DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
973
mg/Kg - dry
155
1
08/26/20 15:30
JPJ
SM-4500-611-13C
Nitrate+ N itrite-N
107
mg/Kg - dry
12.7
1
08/26/20 14:38
ZBD
4500NO3F-2011
Organic N
4890
mg/Kg - dry
665
1
08/26/20 11:00
CALCULATION
pH
7.0
S.U.
1
08/24/2012:57
ADM
9045D
Total Solids
37.6
%
0.010
1
08/24/20 14:00
FMM
SM-2540G
Total Volatile Solids
20.1
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Kjeldahl Nitrogen
5580
mg/Kg - dry
665
1
08/26/20 11:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
1610
mg/Kg - dry
13.3
1
08/24/20 23:07
TJS
6010D
Aluminum
90400
mg/Kg - dry
133
10
08/25/20 20:25
JADS
6010D
Arsenic
6.62
mg/Kg - dry
1.33
1
08/24/20 23:07
TJS
6010D
Calcium
2220
mg/Kg - dry
133
1
08/25/20 20:19
JADS
6010D
Cadmium
0.380
mg/Kg - dry
0.266
1
08/24/20 23:07
TJS
6010D
Chromium
67.3
mg/Kg - dry
0.664
1
08/24/20 23:07
TJS
6010D
Copper
33.0
mg/Kg - dry
1.33
1
08/24/20 23:07
TJS
6010D
Iron
26500
mg/Kg - dry
26.6
1
08/24/20 23.07
]ADS
6010D
Lead
44.1
mg/Kg - dry
0.797
1
08/24/20 23:07
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 13 of 19

7621 (2) Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax [phone]
45671 ANALYTICAL www.waypointanalytical.com
Bio-Nomic Servics Inc Project Lencit-2
Joel Coert Report Date : 08/27/2020
530 Woodlawn St Information : Received: 08/19/2020
Belmont , NC 28012 pJ i
awiL !" ��BW
Report Number: 20-232-0006 REPORT pPANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73420 Matrix: Solids
Sample ID: 5 Sampled: 8/17/2020 6:50
Test Results Units MQL DF Date lTime By Analytical
Analyzed Method
Magnesium
2330
mg/Kg - dry
13.3
1
08/25/20 20:19 ]ADS
6010D
Manganese
750
mg/Kg - dry
1.33
1
08/24/20 23:07
TJS
6010D
Mercury
0.0529
mg/Kg - dry
0.0401
1
08/24/20 13:56
DDB
SW-7471B
Molybdenum
1.57
mg/Kg - dry
0.664
1
08/26/20 17:36
)ADS
6010D
Nickel
17.7
mg/Kg - dry
0.664
1
08/25/20 20:19
)ADS
6010D
Potassium
1520
mg/Kg - dry
26.6
1
08/24/20 23:07
T)S
6010D
Selenium
<1.33
mg/Kg - dry
1.33
1
08/24/20 23:07
T]S
6010D
Sodium
<66.5
mg/Kg - dry
66.5
1
08/24/20 23:07
T]S
6010D
Zinc
i97
mg/Kg - dry
3.32
1
08/24/20 23:07
TIS
6010D
Sulfur
2740
mg/Kg - dry
26.6
1
08/24/20 23:07
TJS
6010❑
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 14 of 19

(2)
Waypoint.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www,waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date : 08/27/2020
530 Woodlawn St
Information :
Received: 08/19/2020
Belmont , NC 28012
Pauric Mc Groary Ph.D., CPA
Report Number: 20-232-0006
REPORT OFANALYSIS
Agronomist
Lab No : 73421
Matrix: Solids
Sample ID : 6
Sampled: 8/17/2020 7:00
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Moisture
64.2
%
0.010 1 08/24/20 14:00 FMM SM-2540G
Calcium Carbonate Equivalent
7.6
% - dry
0.1 1 08/26/20 09,44 DXT AOAC 955.01
Test
Results
Units
MQL DF Date /Time By Analytical
Analyzed Method
Ammonia Nitrogen
520
mg/Kg - dry
166
1
08/26/20 15:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
21.7
mg/Kg - dry
12.8
1
08/26/20 14:39
ZBD
4500NO3F-2011
Organic N
4860
mg/Kg - dry
698
1
08/26/20 11.00
CALCULATION
pH
6.2
S.U.
1
08/24/2012:57
ADM
9045D
Total Solids
35.8
%
0.010
1
08/24/20 14:00
FMM
SM-254OG
Total Volatile Solids
21.9
%
0.010
1
08/24/20 14:00
FMM
5M-2540G
Total Kjeldahl Nitrogen
5390
mg/Kg - dry
698
1
08/26/20 11:00
JPJ iM-4500-NH3C-TKP
Phosphorus
1460
mg/Kg - dry
14.0
1
08/24/20 23:12
TJS
6010D
Aluminum
84100
mg/Kg - dry
140
10
08/25/20 20:35
]ADS
6010D
Arsenic
6.40
mg/Kg - dry
1.40
1
08/24/20 23:12
TJS
6010D
Calcium
1810
mg/K9 - dry
140
1
08/25/20 20:30
DADS
6010D
Cadmium
<0279
mg/Kg - dry
0.279
1
08/24/20 23:12
TJS
6010D
Chromium
62.0
mg/K9 - dry
0.698
1
08/24/20 23:12
TJS
6010D
Copper
30.7
mg/Kg - dry
1.40
1
08/24/20 23:12
TJS
6010❑
Iron
26300
mg/Kg - dry
27.9
1
08/24/20 23:12
]ADS
6010D
Lead
33.5
mg/Kg - dry
0.837
1
08/24/20 23:12
TJS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quandtation Limit
Page 15 of 19

•
e
�' ��
Way
P
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYiI CAL
www.waypointanalyticaLcom
45671
Bio-Nomic Servics Inc
Project
Lencit-2
Joel Coert
Report Date: 08/2712020
530 Woodlawn St
Information :
Received: 08/19/2020
Belmont , NC 28012
Report Number: 20-232-0006
REPORT OFANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73421
Matrix: Solids
Sample ID : 6
Sampled: 8/17/2020 7:00
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Magnesium
2040
mg/Kg - dry
14.0
1
08/25/20 20:30 ]ADS 6010D
Manganese
1010
mg/Kg - dry
1.40
1
08/24/20 23:12 TJS 6010D
Mercury 0.0553
mg/Kg - dry
0.0418
1
08/24/20 13:57 DDB SW-7471B
Molybdenum
1.57
mg/Kg - dry
0.698
1
08/26/20 17:42 ]ADS 6010D
Nickel
17.7
mg/Kg - dry
0.698
1
08/25/20 20:30 ]ADS 6010D
Potassium
1500
mg/Kg - dry
27.9
1
08/24/20 23:12 TJS 6010D
Selenium
<1.40
mg/Kg - dry
1.40
1
08/24/20 23:12 TJS 60101D
Sodium
<69.8
mg/Kg - dry
69.8
1
08/24/20 23:12 TJS 6010D
Zinc
213
mg/Kg - dry
3.49
1
08/24/20 23:12 TJS 6010D
Sulfur
2850
mg/Kg - dry
27,9
1
08/24/20 23:12 TJS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 16 of 19

Waypoint..Q)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Again 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 20-232-0006
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
• Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
[_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: jBrandi Watson Date & Time: 08/19/2020 11:04:19
Page 17 of 19-

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eurofins
ANALYTICAL REPORT
Eurofins TestAmerica, Pittsburgh
301 Alpha Drive
RIDC Park
Pittsburgh, PA 15238
Tel: [phone]
Laboratory Job ID: 180-106162-1
Client Project/Site: Lenoir WTP
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Mr. Joel Coert
4--� 4�0��
Authorized for release by.
61412020 2.51:12 PM
Ken Hayes, Project Manager II
[phone]
ken.hayes @ testamericainc.com
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
PA Lab ID: 02-00416
0

Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Table of Contents
Laboratory Job 10: 180-106162-1
CoverPage .............................................. 1
Table of Contents ......................................... 2
Case Narrative ........................................... 3
Definitions/Glossary ....................................... 4
Certification Summary ...................................... 5
Sample Summary ......................................... 6
Method Summary ......................................... 7
Lab Chronicle ............................................ 8
Client Sample Results ...................................... 10
QC Sample Results ........................................ 12
QC Association Summary ................................... 24
Chain of Custody .......................................... 28
Receipt Checklists ......................................... 30
Page 2 of 30
Eurofins TestAmerica, Pittsburgh
&PS0320

Case Narrative
Client: Bio-Nomics Services., Inc.
ProjecttSite: Lenoir WTP
Job iD: 180-106162-1
Laboratory: Eurofins TestAmerica, Pittsburgh
Narrative
Job Narrative
180-106162-1
Job 1D: 180-106162-1
--_
..r
Receipt
The sample was received on 5/23/2020 9:30 AM; the sample arrived in good condition, properly preserved, and where required, on ice.
The temperature of the cooler at receipt time was 2.8°C
Receipt Exceptions
The Field Sampler was not listed on the Chain of Custody.
GC/MS VOA
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Herbicides
Method 8151A: insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with preparation batch 180-316683 and 180-316961.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PCBs
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Pesticides
Method 8081 B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSDIDUP) associated with preparation batch 180-316683 and 180-316951.
Method 8081 B: The Tetrachloro-m-xylene andfor DCB Decachlorobiphenyl (Surr) surrogate recovery for the following samples was
outside acceptance limits (high biased) on the primary or confirmation column due.: (LB 180-316683/1-E) and (LCS 180-31695112-A).
The recovery is within acceptance limits on the other column, indicating that the extraction process was in control. All associated samples
are ND.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 601OD: The low level initial calibration verification (ICVL) associated with prep batch 316941 recovered above the method 6010D
upper control limit for arsenic. The sample associated with this ICVL was non -detect for the affected analyte; therefore, the data have been
reported. The associated sample is impacted: LENOIR WTP (180-106162-1).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method 9014: The following sample was found to contain Sulfide: LENOIR WTP (180-106162-1). The sulfide was treated and removed
prior to distillation. All samples assumed to have sulfide and were treated with 100 uL of bismuth nitrate solution.
Method 9034_Calc: The following sample(s) was received outside of holding time: <&commaMerge&>.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAmerica, Pittsburggh
Page 3 of 30 6/4/2020

Definitions/Glossary
Client: Bio-Nomics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Qualifiers
GUMS Semi VOA
Qualifier Qualifier Description j
LCS or LCSD is outside acceptance limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC Semi VOA
Qualifier Qualifier Description
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
X Surrogate recovery exceeds control limits
Metals
Qualifier Qualifier Description
" ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.
F1 MS and/or MSD recovery exceeds control limits.
F2 MS/MSD RPD exceeds control limits
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
_Glossary --
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoVIDOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
MIL Minimum Level (Dioxin)
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Eurofins TestAmerica, Pittsburgh
Page 4 of 30 6/4/2020

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc.
Job ID: 180-106162-1
ProjectlSite: Lenoir WTP
Laboratory: Eurofins TestAmerica, Pittsburgh
Unless otherwise noted, all analytes for this laboratory were covered under each accreditationlcertification below.
Authority Program Identification Number
Expiration Date
North Carolina (WWISW) State 434
01-01-21
The following analytes are included in this report, but the laboratory is
not certified by the governing authority.
This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
EPA 10206 Sludge Ignitability
j EPA 9014 9010C Sludge Cyanide, Total
i South Carolina State 89014
04-30-20 "
The following analytes are included in this report, but the laboratory is not certified by the governing authority.
This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
EPA 1020B Sludge Ignitability
EPA 8151A 8151A Sludge 2,4-D
EPA 8151A 8151A Sludge Silvex (2,4,5-TP)
' AccreditationlCertification renewal pending - accreditation/certification considered valid.
Eurofins TestAmerica, Pittsburgh
Page 5 of 30 6/4/2020

Sample Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Job ID: 180-106162-1
Lab Sample ID Client Sample ID Matrix Collected Received Asset IE)
180-106162-1 LENOIR WTP Sludge 05/22120 09:00 05/23/20 09:30
Eurofins TestArnerica, Pittsburgh
Page 6 of 30 6/4/2020

Method Summary
Client: Bio-Nomics Services_, Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method
Method Description
Protocol
Laboratory
EPA 8260D
Volatile Organic Compounds by GCIMS
SW646
TAL PIT
EPA 8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PIT
EPA 8081E
Organochlorine Pesticides (GC)
SW646
TAL PIT
EPA 8082A
Polychlorinated Biphenyis (PCBs) by Gas Chromatography
SWB46
TAL PIT
EPA 8151A
Herbicides (GC)
SW846
TAL PIT
EPA 6010D
Metals (ICP)
SW846
TAL PIT
EPA 7470A
Mercury (CVAA)
SW846
TAL PIT
EPA 1020B
I nitabili Small Scale Closed-Cu Method
9 tY, p
SW846
TAL PIT
EPA 9014
Cyanide
SW846
TAL PIT
EPA 9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL PIT
EPA 9045D
pH
SW846
TAL PIT
3010A
Preparation, Total Metals
SW846
TAL PIT
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL PIT
3541
Automated Soxhlet Extraction
SW846
TAL PIT
5030C
Purge and Trap
SW846
TAL PIT
7470A
Preparation, Mercury
SW846
TAL PIT
8151A
Extraction (Herbicides)
SW846
TAL PIT
9010C
Cyanide, Distillation
SW646
TAL PIT
9030E
Sulfide, Distillation (Acid Soluble and Insoluble)
SWB46
TAL PIT
EPA 1311
TCLP Extraction
SW846
TAL PIT
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, PhysicallChemical Methods"% Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PIT = Eurofins TestAmerica, Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
Burofins TestAlnerica, Pittsburgh
Page 7 of 30 6/4/2020

Lab Chronicle
Client: Bio-Nomics Services., Inc.
Jab ID: 180-106162-1
Project/Site: Lenoir WTP
Client Sample ID: LENOIR WTP
Lab Sample ID: 180-106162-1
Date Collected: 05/22/20 09:00
Matrix: Sludge
Date Received: 05/23/20 09:30
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
TCLP Leach EPA 1311
25.00 g
500 mL
316691
05/27/20 22:00
JAS
TAL PIT
TCLP Analysis EPA 8260D
1
0.125 mL
5 mL
316868
05/29/20 11:25
KLG
TAL PIT
Instrument ID: C14HP9
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27/20 22:00
JAS
TAL PIT
TCLP Prep 3510C
200 mL
10.0 mL
316950
05/29/20 15:00
CBY
TAL PIT
TCLP Analysis EPA 8270E
1
1 mL
1 mL
317153
06/02/20 12:23
VVP
TAL PlT
Instrument ID: CH732
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27/20 22:00
JAS
TAL PIT
TCLP Prep 3510C
100 mL
40.0 mL
316951
05/29/20 15:00
CBY
TAL PIT
TCLP Analysis EPA 8081E
1
317106
06/01/20 19:39
DFE
TAL PIT
Instrument ID: CHGC15
Total/NA Prep 3541
15.4 g
20.0 mL
316603
05/27/20 10:01
CDH
TAL PIT
Total/NA Analysis EPA 80M
1
316711
05/28/20 16:59
JMO
TAL PIT
Instrument ID: CHGC8
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27/20 22:00
JAS
TAL PIT
TCLP Prep 8151A
100 mL
10.0 mL
316961
05/29/20 17:20
CBY
TAL PIT
TCLP Analysis EPA 8151A
20
317040
06/01/20 12:03
JMO
TAL PIT
Instrument ID: CGC1
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27/20 22:00
JAS
TAL PIT
TCLP Prep 3010A
f
5 mL
50 mL
316941
05/29/20 15:21
JL
TAL PIT
TCLP Analysis EPA 6010D
1
317142
06101/20 11:43
RJG
TAL PIT
Instrument ID: C
TCLP Leach EPA 1311
100.00 g
2000 mL
316683
05/27/20 22:00
JAS
TAL PIT
TCLP Prep 7470A
50 mL
50 mL
316915
05/29/20 15:10
NAM
TAL PIT
TCLP Analysis EPA 7470A
1
316982
05/29/20 18:40
NAM
TAL PIT
Instrument ID: HGZ
Total/NA Analysis EPA 1020E
1
316583
05/27/20 08:18
AVS
TAL PIT
Instrument ID: NOEQUIP
Total/NA Prep 9010C
0,23 g
10 mL
317066
06/01/20 12:00
CMR
TAL PIT
Total/NA Analysis EPA 9014
1
317144
06/01/20 14:05
CMR
TAL PIT
Instrument ID: SEAL2
TotallNA Prep 90305
5.06 g
50 mL
316574
05/27/20 09:00
CMR
TAL PIT
TotallNA Analysis EPA 9034
1
316625
05/27/20 12:00
CMR
TAL PIT
Instrument ID: NOEQUIP
Total/NA Analysis EPA 9045D
1
20.37 g
20 mL
316790
05/29/20 15:30
PMH
TAL PIT
Instrument ID: NOEQUIP
Laboratory References:
TAL PIT = Eurofins TestAmerica, Pittsburgh, 301 Alpha Drive, RI DC Park, Pittsburgh, PA
15238, TEL [phone]
Eurofins TestAmerica, Pittsburgh
Page 8 of 30 6/4/2020

Lab Chronicle
Client: Bio-Nomics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Analyst References:
Lab: TAL PIT
Batch Type: Leach
JAS = Jeremy Stundon
Batch Type: Prep
CBY = Charles Yushinski
CDH = Christopher Hayburn
CMR = Carl Reagle
JL = James Lyu
NAM = Nicole Marfisi
Batch Type: Analysis
AVS = Abbey Smith
CMR = Carl Reagle
DFE = David Eppinger
JMO = John Oravec
KLG = Kathy Gordon
NAM = Nicole Masi
PMH = Paloma Hoelzie
RJG = Rob Good
WP = Vincent Piccolino
Eurofins TestAmerica, Pittsburgh
0
Page 9 of 30 6/4/2020

Client Sample Results
Client: Bio-Nomics Services., Inc.
Job ID: 180-106162-1
ProjectlSite: Lenoir WTP
Client Sample ID: LENOIR
WTP
Lab Sample ID: 180-106162-1
Date Collected: 05122/20 09:00
Matrix: Sludge
Date Received: 05123/20 09:30
Method: EPA 8260D - Volatile Organic Compounds
by GC/MS - TCLP
Analyte
Result Qualifier
RL MDL
Unit
D Prepared Analyzed
Dil Fac
Benzene
ND
0.200
mg1L
0512912011:25
1
2-Butanone (MEK)
ND
0.200
mglL
05/29/20 11:25
1
Carbon tetrachloride
ND
0.200
mg1L
05/29/20 11:25
1
Chlorobenzene
ND
0.200
mg1L
0512912011:25
1
Chloroform
ND
0.200
mg1L
05/2912011:25
1
1,2-Dichioroethane
ND
0.200
mg/L
05/29/20 11:25
1
1,1-Dichloroelhene
ND
0.200
mg/L
05/29/20 11:25
1
Tetrachloroethene
ND
0.200
mg/L
0512912011:25
1
Trichloroethene
ND
0.200
mg1L
05/29/20 11:25
1
Vinyl chloride
ND
0.200
mg1L
05/29/20 11:25
1
1,4-Dichlorobenzene
ND
0.200
mg1L
0512912011:25
1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Di! Fac
4-8ramafluorobenzene (Burr)
73
54 - 125
05/29/201 1:25
1
Dibromofluoromethane (Surr)
115
55-150
0512912011:25
1
1, 2-Dichloroethane-d4 (Surr)
i71
53 - f 50
05/29/20 11:25
1
Toluene-f8 (Surr)
86
63 - 127
05/29/20 11:25
1
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
2,4,5-Trichlorophenol
ND
0.0500
mg/L
05/29/20 15:00
0610212012:23
1
2,4,6-Trichlorophenol
ND
0.0500
mg1L
05/29/20 15:00
06/02/2012:23
1
2,4-Dinitrotoluene
ND
0.0500
mglL
05129/2015:00
06102120 12:23
1
2-Methylphenol
ND
0,0500
mg1L
05129/2015:00
0610212012:23
1
Methylphenol, 3 E 4
ND
0.0500
mglL
05/29/20 15:00
06/02/20 12:23
1
Hexachlorobenzene
NO
0.0500
mg/L
05/29/20 15:00
0610212012:23
1
Hexachlorobutadiene
ND
0.0500
mg1L
05/2912015:00
06/0212012:23
1
Hexachloroethane
ND
0.0500
mg1L
0512912015:00
06/02/2012:23
1
Nitrobenzene
ND
0.0500
mg/L
05/2912015:00
06/02/2012:23
1
Pentachlorophenol
ND
0.250
mg/L
05/2912015:00
0610212012:23
1
Pyridine
ND
0.100
mg1L
05129/2015:00
06/02/2012:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromopheno! (Surr)
29
24 - 113
05/29/20 15:00
06/02120 12:23
1
2-Fluorobiphenyl
70
55-107
05129120 15.00
06/02/20 12:23
1
2-Fluorophenol (Surr)
69
60- 108
05/29/20 15:00
06/02/20 12:23
1
Nitrobenzene-d5 (Surr)
65
62 - 115
05/29/20 15.00
06102120 12:23
1
Phenol-d5 (Surr)
57
52 - 107
05/29/20 15:00
06102120 12:23
1
7'erphenyl-d 14 (Surr)
72
44 -116
05/29/20 15:00
06102120 12:23
1
Method: EPA 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chlordane (technical)
ND
0.00500
mg/L
05/29/20 15:00
06/01/20 19:39
1
Endrin
ND
0.000500
mg1L
05/29/20 15:00
06101/2019:39
1
gamma-BHC (Lindane)
ND
0.000500
mg1L
05/29/20 15:00
06/01/20 19:39
1
Heptachlor
ND
0.000500
mg1L
05/2912015:00
0610112019:39
1
Heptachlor epoxide
ND
0.000500
mg1L
05/29/20 15:00
06/01/20 19:39
1
Methoxychlor
ND
0,000500
mg/L
0512912015:00
0610112019.39
1
Toxaphene
ND
0.0400
mglL
05129/2015:00
0610112019:39
1
Eurofins TestAmerica, Pittsburgh
Page 10 of 30 6/4/2020

Client Sample Results
Client: Bio-Nomics Services., Inc.
Job ID: 180-106162-1
ProjectlSite: Lenoir WTP
Client Sample ID: LENOIR
WTP
Lab Sample
ID: 180-106162-1
Date Collected: 05/22120 09:00
Matrix: Sludge
Date Received: 05/23/20 09:30
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
D11 Fac
DCB Decachlorobiphenyl (Surr)
114
58 -115
05129120 15:00
06101120 19:39
1
DCB Decachlorobiphenyl (Surr)
101
58-115
05129120 15:00
06/01/20 19:39
1
Tetrachloro-m-xylene
100
43-118
05/29/20 15:00
06/01/20 19:39
1
Tetrachloro-m-xylene
114
43-118
05/29/20 15:00
06/0i/20 19:39
1
Method: EPA 8082A - Polychlorinated
Biphenyls (PCBs)
by Gas
Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016
NO
16.2
ug/Kg
05127/2010:01
0512812016:59
1
PCB-1221
ND
16.2
ug1Kg
05/27/2010:01
0512812016:59
1
PCB-1232
ND
16.2
ug1Kg
0512712010:01
05128/2016:59
1
PCB-1242
ND
16.2
ug/Kg
05/27/2010:01
05/2812016:59
1
PCB-1248
ND
16.2
uglKg
05/2712010:01
05/2812016:59
1
PCB-1254
ND
16.2
ug/Kg
05/2712010:01
05/28/2016:59
1
PCB-1260
ND
16.2
ug/Kg
05127120 10:01
05/28/2016:59
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m xylene (Sun-)
86
51-112
05127120 10:01
05/28/20 16.59
1
Tetrachloro-m-xylene (Surr)
84
51-112
05127120 10:01
05126120 16:59
1
DCB Decachlorobiphenyl (Surr)
86
61-132
05127120 10:01
05/2820 16:59
1
DCB Decachlorobiphenyl (Surr)
87
61-132
05127120 10:01
05/28/20 16:59
1
Method: EPA 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
2,4-D
ND
0.0400
mg1L
05129120 17:20
06101/2012:03
20
Silvex (2,4,5-TP)
ND
0,0100
mg1L
05/29/20 17:20
06/01/20 12:03
20
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4-Dichlorophenylacetic acid
29
23-122
05129120 17:20
0610112 112:03
20
2,4-Dichlorophenylacetic acid
39
23-122
05129/20 17:20
06101120 12:03
20
Method: EPA 6010D - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
Silver
N❑
0.500
mg1L
05/29/2015:21
06/01/2011:43
1
Barium
ND
2.00
mglL
05/29/2015:21
0610112011:43
1
Cadmium
ND
0.500
mg/L
05129/2015:21
0610112011:43
1
Chromium
ND
0.500
mg/L
0512912015:21
06101/2011:43
1
Lead
ND
0.500
mg1L
0512912015:21
06/01/2011:43
1
Selenium
ND
0.500
mg1L
0512912015:21
0610112011:43
1
Arsenic
ND "
0.500
mg1L
0512912015:21
06/0112011:43
1
Method: EPA 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
Mercury
ND
0.000200
mg/L
05/291201510
05/29/2018:40
1
General Chemistry
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed
Dil Fac
Cyanide, Total
ND
0,435
mg/Kg
06/01/20 12:00
06/01/20 14:05
1
Sulfide
56.0
29.6
mg/Kg
05/27/20 09:00
05/27/20 12:00
1
Analyte
Result Qualifier
RL
RL Unit
D
Prepared
Analyzed
Dil Fac
Ignitability
>140
Degrees F
05/27/20 08:18
1
PH
6.3 HF
0.1
SU
05129/2015:30
1
Eurofins TestAmerica, Pittsburgh
Page 11 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Method: EPA 826OD - Volatile Organic Compounds by GCIMS
Lab Sample ID: LCS 180-316868/3
Matrix: Solid
Analysis Batch: 316868
Job ID: 180-106162-1
Client Sample ID: Lab Control Sample
Prep Type: TotallNA
Spike LCS
LCS
%Rec.
Analyte
Added Result
Qualifier
Unit
D %Rec
Limits
Benzene
0,0100 0.01033
mg/1-
_ 103
72.118
2-Butanone (MEK)
0.0100 0.01176
mglL
118
33-133
Carbon tetrachloride
0.0100 0.009665
mglL
97
69-137
Chlorobenzene
0.0100 0.01069
mg1L
107
77 -122
Chloroform
0.0100 0.009641
mgiL
96
78.119
1,2-Dichloroethane
0.0100 0.01008
mglL
101
62-129
1,1-bichloreethene
0.0100 0,008952
mglL
90
60-131
Tetrachloroethene
0.0100 0.01105
mg1L
110
75 -125
Trichloroethene
0.0100 0.009349
mg1L
93
76 -120
Vinyl chloride
0.0100 0.008684
mglL
87
52 -130
1,4-Dichlorobenzene
0.0100 0.01133
mg1L
113
76 -119
LCS LCS
Surrogate
%Recovery Qualifer
Limits
f4-8romofluorobenzene (Surr)
103
54 -125
Dibromofluoromethane (Surr)
93
55- 150
1,2-Dichloroethane-d4 (Surr)
91
53- 150
Toluene-d8 (Surr)
93
63.127
Lab Sample ID: LB 180-316691/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 316868
LB LB
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed Dil Fac
Benzene
ND
0.0500
mg1L
05/29120 08:55 1
2-Butanone (MEK)
ND
0.0500
mg1L
05/29120 08:55 1
Carbon tetrachloride
ND
0.0500
mg1L
05/29/20 08:55 1
Chlorobenzene
ND
0.0500
mglL
05/29/20 08:55 1
Chloroform
ND
0.0500
mglL
05/29/20 08:55 1
1,2-Dichloroethane
ND
0.0500
mglL
05/29/20 08:55 1
1,1-Dichloroethene
ND
0.0500
mglL
05/29/20 W55 1
Tetrachloroethene
ND
0,0500
mglL
05/29/20 08:55 1
Trichloroethene
ND
0.0500
mglL
05/29/20 08:55 1
Vinyl chloride
ND
0.0500
mglL
05/29/20 08:55 1
1,4-Dichlorobenzene
ND
0.0500
mglL
05/29/20 08:55 1
LB LB
Surrogate
%Recovery Qualirier
Limits
Prepared
Analyzed Dil Fac
4-Sromofluorobenzene (Surr)
81
54 -125
05/29/20 08.55 1
Dibromofluoromethane (Surr)
111
55-150
05/29/20 08:55 1
1,2-Dichloroethane-d4 (Surr)
121
53-150
05/29/20 08:55 1
Toluene -dB (Surr)
69
63- 127
05129120 08:55 1
Lab Sample ID: 180-105839-A-13-B MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 316868
Sample Sample
Spike MS
Ms
%Rec.
Analyte
Result Qualifier
Added Result
Qualifier
Unit
D %Rec
Limits
Benzene
N❑
0.400 0.3558
mglL
89
72.118
2-Butanone (MEK)
ND
0.400 0.3283
mglL
82
33-133
Eurofins TestAmerica, Pittsburgh
Page 12 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Job ID: 180-106162-1
Method: EPA 8260D Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: 180-105839-A-13-B MS Client Sample ID: Matrix Spike
Matrix: Solid Prep Type: TCLP
Analysis Batch: 316868
Sample Sample
Spike
MS MS
%Rec,
Anafyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Carbon tetrachloride
NO
0.400
0.3682
mg/L
92
69-137
Chlorobenzene
ND
0.400
0,4116
mg1L
103
77-122
Chloroform
NO
0,400
0.4231
mg1L
106
78-119
1,2-Dichloroethane
NO
0,400
0.3949
mg1L
99
62-129
1,1-Dichloroethene
ND
0.400
0.3457
mg1L
86
60-131
Tetrachloroethene
ND
0.400
0.4141
mg1L
104
75 - 125
Trichloroethene
NO
0.400
0.3306
mglL
83
76 -120
Vinyl chloride
NO
0.400
0.3336
mglL
83
52 -130
1,4-Dichlorobenzene
NO
0.400
0.4232
mgll-
106
76 -119
MS MS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene(Surr)
113
54-125
Dibromofluommethane (Surr)
88
55-150
1, 2-Dichloroethan"4 (Surr)
93
53 -150
Toluene-d8 (Surr)
96
63 -127
Lab Sample ID: 180.105839-A-13-C MSD
Matrix: Solid
Analysis Batch: 316868
Client Sample ID: Matrix Spike Duplicate
Prep Type: TCLP
Sample Sample
Spike
MSD MSD
%Rec.
RPD
Anafyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Benzene
NO
0.40D
0.3195
mg1L
80
72-118
11
20
2-Butanone (MEK)
NO
0.400
0.2914
mg1L
73
33-133
12
35
Carbon tetrachloride
NO
0.400
0.3254
mglL
81
69 -137
12
20
Chlorobenzene
NO
0,400
0.3943
mg1L
99
77.122
4
20
Chloroform
NO
0,400
0.3906
mg1L
98
78_119
8
20
1,2-Dichloroethane
NO
0.400
0.3303
mglL
83
62-129
18
20
1,1-Dichloroethene
NO
0.400
0,2943
mg1L
74
60-131
16
35
Tetrachloroethene
NO
0.400
0.4046
mglL
101
75 -125
2
20
Trichloroethene
NO
0.4DD
0,3630
mglL
91
76 -120
9
20
Vinyl chloride
NO
0.400
0.2839
mg1L
71
52 -130
16
21
1,4-Dichlorobenzene
NO
0.400
0.4107
mglL
103
76 -119
3
20
MSD MSD
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
98
54 _ 125
Dibromofluoromethane (Surr)
83
55 -150
1, 2-Dichloroethane-d4 (Surr)
82
53 -150
Toluene-d8 (Surr)
91
63 -127
Method: EPA 8270E - Semivolatile Organic Compounds (GCIMS)
Lab Sample ID: MB 180-31695011-A
Matrix: Solid
Analysis Batch: 317153
MB MB
Anafyte
Result Qualifier RL
2,4,5-Trichlorophenol
NO 0.0500
2,4,6-Trichlorophenol
NO 0.0500
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316950
MDL Unit D Prepared Analyzed Oil Fac
mglL 05/29/20 15:00 06/02/20 08:55 1
mg)L 05/29/20 15:00 06/02/20 08:55 1
Eurofins TestAmerica, Pittsburgh
Page 13 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA 8270E - Semivolatlle Organic Compounds (GC1MS)
(Continued)
Lab Sample ID: MB 180-316950/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317153
Prep Batch: 316950
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
2,4-Dinitrotoluene
ND
0.0500
mg1L
05/29/20 15:00
06/02/20 08:55 1
2-Methylphenol
ND
0.0500
mg/L
05/29/20 15;00
06/02120 08:55 1
Methylphenol, 3 & 4
ND
0.0500
mg/L
05/29/20 15:00
06/02120 08:55 1
Hexachlarobenzene
ND
0.0500
mg/L
05t29120 15:00
06/02/20 08:55 1
Hexachlorobutadiene
ND
0.0500
mg/L
05/29/20 15:00
06/02120 08:55 1
Hexachloroethane
ND
0.0500
mg1L
05/29/20 15:00
06/02/20 08:55 1
Nitrobenzene
ND
0.0500
mg1L
05/29/20 15:00
06/02/20 08:55 1
Pentachlorophenol
ND
0.250
mg/L
05/29/20 15:00
06/02/20 08:55 1
Pyridine
ND
0.100
mg1L
05/29120 15:00
06/02/20 08:55 1
MB MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed Qil Fac
2, 4, 6-Tribromophenol (Surr)
68
24 -113
05/29/20 15:00
06102120 08:55 1
2-Fluorobiphenyl
70
55-107
05129/20 15:00
06/02/20 08:55 1
2-Fluoropheno! (Surr)
73
60- 108
05129120 15:00
06/02/20 08:55 1
Nitrobenzene-d5 (Surr)
65
62 -115
05/29/20 15,00
06/02/20 06:55 1
Phenol-d5 (Surr)
66
52-107
05/29/20 15.00
06102120 08:55 1
Terphenyl-04 (Surr)
73
44-116
05129120 15.00
06102120 08:55 1
Lab Sample ID: LCS 180-316950/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317153
Prep Batch: 316950
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2,4,5-Trichlorophenol
0,250
0.2139
mglL
86
54 -100
2,4,6-Trichlorophenol
0.250
0,2709
mg/L
108
56 -100
2,4-Dinitrotoluene
0.250
0,2183
mg1L
87
42 -100
2-Methylphenof
0.250
0.2089
mgiL
84
60 -101
Methylphenol, 3 & 4
0,500
0.4550
mg1L
91
62-106
Hexachlorobenzene
0.250
0.1838
mg/L
74
37-100
Hexachlorobutadiene
0.250
0.3074
mgiL
123
50-103
Hexachlaroethane
0.250
0.2387
mg/L
95
59-104
Nitrobenzene
0.250
0.2240
mg1L
90
58 -113
Pentachlorophenol
0.250
0.1011 1
mg/L
40
18 -100
Pyridine
0.250
0.2791
mg/L
112
54 -119
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
2, 4, 6-Tribromophenol (Surr) 106
24 -113
2-Fluorobiphenyl 102
55 -107
2-Fluoropheno! (Surr) 105
60 -108
Nitrobenzene-d5 (Surr) 94
62 -115
Phenol-d5 (Surr) 95
52 -107
Terphenyl{114 (Surr) 110
44-116
Eurofins TestAmerica, Pittsburgh
Page 14 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc-
Project/Site. Lenoir VVTP
Job ID: 180-106162-1
Method: EPA 8270E - Semivolatile Organic Compounds (GC/MS) (Continued]
Lab Sample ID: LCSD 184-31695013-A Client Sample ID: Lab Control Sample Dup
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 317153 Prep Batch: 316950
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier
Unit
❑ %Rec
Limits RPD
Limit
2,4,5-Trichloraphenol
0.250
0,2131
mg1L
85
54 -100 0
16
2,4,6-Trichlorophenol
0.250
0.2507
mg1L
100
56 -100 8
15
2,4-Dinitrotoluene
0.250
0.2072
mg1L
83
42 -100 5
17
2-Methylphenol
0.250
0.1843
mglL
74
60 -101 13
15
Methylphenol, 3 & 4
0.500
0.4245
mglL
85
62 -106 7
15
1 Hexachlorobenzene
0.250
0,1782
mglL
71
37 -100 3
15
Hexachlorobutadiene
0.250
0.2813
mglL
113
50-103 9
15
Hexachloroethane
0.250
0.2245
mglL
90
59 -104 6
16
Nitrobenzene
0.250
0.2142
mg/L
86
56-113 4
15
iPentachlorophenol
0.250
0.09624 J
mglL
38
18 -100 5
16
Pyridine
0.250
0.2758
mglL
110
54-119 1
16
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
98
24- 113
2-Fluorobiphenyl
95
55 -107
2-Fluorophenol (Surr)
102
60 -108
Nitrobenzene-d5 (Surr)
86
62 -115
Phenol-d5 (Surr)
92
52 -107
Terpheny!414 (Surr)
102
44 -116
Lab Sample ID: LB 180-316683/1-D
Client Sample ID: Method
Blank
Matrix: Solid
Prep Type:
TCLP
Analysis Batch: 317153
Prep Batch: 316950
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
2,4,5-Trichlorophenol
ND
0.0500
mg/L
05/2912015:00
06/02/2010:06
1
2,4,6-Trichlorophenol
ND
0.0500
mg1L
05/29/2015:00
06/02/2010:06
1
2,4-Dinitrotoluene
ND
0.0500
mg/L
05129/2015:00
06102120 10:06
1
2-Methylphenol
ND
0.0500
mglL
05/29/2015:00
06/02/2010:06
1
Methylphenol, 3 & 4
ND
0.0500
mglL
05/29/20 15:00
06/02/20 10:06
1
Hexachlorobenzene
ND
0.0500
mg1L
0512912015:00
06102120 10:06
1
Hexachlorobutadiene
ND
0.0500
mglL
05129/2015;00
06/0212010:06
1
Hexachloroethane
ND
0.0500
mglL
05129/2015:00
06102120 10:06
1
Nitrobenzene
ND
0.0500
mglL
05129/2015:00
06/0212010:06
1
Pentachlorophenol
N❑
0.250
mglL
05129/2015:00
06/02/2010:06
1
Pyridine
ND
0.100
mglL
05/2912015:00
06/02/2010:06
1
LS LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol(Surr)
67
24-113
0512912015:00
06/02/2010:06
1
2-Fluorobiphenyl
69
55-107
05129120 15:00
06/02/20 10:06
1
2-Fluorophenof (Surr)
72
60-108
05/29/20 15:00
06102120 10:06
1
Nitrobenzene-d5 (Surr)
64
62 -115
05/29/20 15:00
06102120 1006
1
Phenol-d5 (Surr)
65
52-107
05/29/20 15:00
06/02/20 10:06
1
Terphenyl-d14 (Surr)
70
44-116
05/29/20 15:00
06/02/20 1006
1
Eurofins TestAmerica, Pittsburgh
Page 15 of 30 6/4/2020

QC Sample Results
Client: Bio-NOmiCS Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA 8081E Organochlorine Pesticides {GCJ
Lab Sample la: MB 180-316951/1-A
Matrix: Solid
Analysis Batch: 317106
MB MB
Analyte
Result Qualifier
Chlordane (technical)
ND
Endrin
ND
gamma-BHC (Lindane)
ND
Heptachlor
ND
I Heptachlor epoxide
ND
Methoxychlor
ND
Toxaphene
ND
Ma MS
Surrogate %Recovery Qualifier
DCB Decachlorobiphenyl (Surr) 11 i
DCB Decachlorobiphenyl (Surf) 106
Tetrachloro-m-xylene 101
Tetrachloro-m xylene 116
Lab Sample ID: LCS 180-31695112-A
Matrix: Solid
j Analysis Batch: 317106
Analyte
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Client Sample ID: Method Blank
Prep Type: TotallNA
Prep Batch: 316951
RL
MDL Unit
D Prepared
Analyzed Oil Fac
0.00501)
mg1L
05129/2015:00
06101/2018:06 1
0,000500
mg/L
05/2912015:00
06/01/2018:06 1
0.000500
mg1L
05/2912015:00
0610112018:06 1
0.000500
mg1L
05/29/2015:00
06101/2018:06 1
0.000500
mg/L
0512912015:00
(1610112018:06 1
0.000500
mg/L
05129/2015:00
0610112018:06 1
0.0400
mg1L
05129/2015:00
0610112018:06 1
Limits
Prepared
Analyzed D11 Fac ;
58-115
05/29/20 55,00
06/0112018:06 1 - --
58 -115
05129120 15: 00
06101120 18,06 1
43-118
05/29/20 15:00
06101120 18,06 1
43 - 118
05129120 15:00
06101120 18: 06 1
Client Sample ID:
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316951
Spike LCS
LCS
%Rec.
Added Result
Qualifier
Unit
D %Rec
Limits
Q0100 0.01056
mg1L
106
37 -150
0.0100 0,01113
mg/L
111
50-137
0.0100 0.01099
mg/L
110
49 -135
0,0100 0.01155
mg/L
116
49.133
0.0100 0,009171
mg/L
92
45-150
LCS LCS
Surrogate %Recovery Qualifier Limits
DCB Decachlorobiphenyl (Surr) 119 X 58 -115
DCB Decachlorobiphenyl (Surr) 109 58 -115
Tetrachloro-m-xylene 104 43 -118
Tetrachlorc-m-xylene 121 X 43-118
Lab Sample ID: LCSD 180-316951/3-A
Matrix: Solid
Analysis Batch: 317106
Client Sample ID: Lab Control Sample Dup
Spike
LCSD LCSD
Analyte
Added
Result Qualifier
Endrin
0.0100
0.01026
gamma-BHC (Lindane)
0.0100
0.01127
Heptachlor
0.0104
0.01117
Heptachlor epoxide
0.0100
0.01157
Methoxychlor
0.0100
0A08714
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl (Surr)
110
58-115
DCB Decachlorobiphenyl (Surr)
102
58 -115
Tetrachloro-m xylene
104
43 -118
Tetrachloro-m-xylene
116
43 -118
Prep Type: Total/NA
Prep Batch: 316951
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
mg/L
103
37 -150
3
15
mg/L
113
50 -137
1
18
mg/L
112
49 -135
2
22
mg/L
116
49 -133
0
15
mg/L
87
45 -150
5
17
Eurofins TestAmerica, Pittsburgh
Page 16 of 30
6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA 8081 B Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LB 180-316683/1-E
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 317106
Prep Batch: 316951
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Chlordane (technical)
ND
0.00500
mglL
05/29/20 15:00
06/01/20 1&52 1
Endrin
ND
0.000500
mglL
0512912015:00
06101/2018:52 1
gamma-BHC (Lindane)
ND
0,000500
mglL
05/29/20 15:00
06/01/20 18:52 1
Heptachlor
ND
0.000500
mglL
05129/2015:00
0610112018:52 1
Heptachlor epoxide
ND
0.000500
mglL
05/29/20 15:00
06/01/20 18:52 1
Methoxychlor
ND
0.000500
mglL
0512912015:00
06/01/2018:52 1
Toxaphene
ND
0.0400
mglL
05/2912015:00
06/01/2018:52 1
I
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Di1 Fac i
DCB Decachlorobiphenyl (Surr)
119 X
58 -115
05/29/20 15:00
06,101120 18:52 1
DCB Decachlorobiphenyl (Surr)
110
58-115
05129120 15:00
0610i120 18:52 1
Tetrachloro-m-xylene
106
43-118
05/29/20 15:00
06101M 18:52 1
Tetrachloro-m-xylene
118
43-118
OW9120 15:00
06/01/20 18:52 1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
FLab Sample la: MB 180-316603/1-A
Client Sample
ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 316711
Prep Batch: 316603
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
PCB-1016
ND
16.7
uglKg
05/2712010:01
05/2812016:22 1
PCB-1221
ND
16.7
uglKg
05/2712010:01
05128/2016:22 1
PCB-1232
ND
16.7
uglKg
05/2712010:01
06/28/2016:22 1
PCB-1242
ND
16.7
ug1Kg
05/27/2010:01
05/2812016:22 1
PGB 1248
ND
16.7
ug1Kg
05/27/20 10:01
05/20/20 16:22 1
PCB-1254
ND
16.7
ug1Kg
05/27/2010:01
05128/2016:22 1
PCB-1260
ND
16.7
uglKg
0512712010:01
0512812016:22 1
MB me
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
Tetrachloro-m-xylene (Surr)
100
51-112
05127120 10:01
05126120 16:22 1
Tetrachloro-m-xylene (Surr)
97
51-112
05127120 10:01
05/28/20 16:22 1
DCB Decachlorobiphenyl (Surr)
96
61-132
05127120 10:01
05/28/20 16:22 1
DCB Decachlorobiphenyl (Surr)
94
61-132
05127120 10:01
0512WO 16:22 1
Lab Sample ID: LCS 180-316603/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 316711
Prep Batch: 316603
Spike
LCS LCS
%Roc.
Analyte
Added
Result Qualifier Unit
D %Rec
Limits
PCB-1016
1330
1224 ug1Kg
_ 92
48 -1 22
PCB-1260
1330
1162 ug1Kg
87
47-127
LCS LCS
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene (Surr)
101
51-112
Tetrachloro-m-xylene (Surr)
96
51- 112
DCB Decachlorobiphenyl (Surr)
98
61-132
DCB Decachlorobiphenyl (Surr)
97
61_ 132
Eurofns TestAmerica, Pittsburgh
Page 17 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA 8082A` Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: 180-106162-1 MS
Client Sample ID: LENOIR WTP
Matrix: Sludge
Prep Type: Total/NA
Analysis Batch: 316711
Prep Batch: 316603
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
PCB-1016 ND
1320
1103 uglKg
84 48 -122
PCB-1260 ND
1320
1017 uglKg
77 47-127
MS MS
Surrogate %Recovery Qualifier
Tetrach10ro-m-xylene (Sun•) 85
Tetrachloro-m-xylene (Surf) 83
DCB Decachlorobipheny! (Surr) 79
DCB Decachlorobipheny! (Surr) 60
Lab Sample ID: 180-106162-1 MSD
Matrix: Sludge
Analysis Batch: 316711
Sample Sample
Analyte Result Qualifier
Limits
51-112
51-112
61-132
61-132
Spike
Added
MSD MSD
Result Qualifier
PCB-1016
ND
1310
1056
PCB-1260
ND
1310
1022
MSD MSD
Surrogate
%Recovery Qualifier
Limits
Tetmchloro-m xylene (Surr)
82
51-112
Tetrachloro-m xylene (Surr)
80
51-112
DCB Decachlorobipheny! (Surr)
84
61-132
DCB Decachlorobipheny! (Surr)
83
61-132
Method: EPA 8151A -Herbicides (GC)
Lab Sample ID: MB 180-316961/1-A
Matrix: Solid
Analysis Batch: 317040
MB MB
Analyte
Result Qualifier
RL
MDL Unit
2,4-D
ND
0,0400
mglL
Silvex (2,4,5-TP)
ND
0,0100
mglL
MB MB
Surrogate
%Recovery Qualifier
Limits
2,4-Dichlorophenylacetic acid
75 p
23-122
2, 4-Dichlorophenylacetic acid
114
23 -122
Lab Sample ID: LCS 180-31696112-A
Matrix: Solid
Analysis Batch: 317040
Spike
LCS LCS
Analyte
Added
Result Qualifier
2,4-D
0.200
0.04237
Silvex (2,4,5-TP)
0.0500
0.01989
LCS LCS
Surrogate
%Recovery Qualifier
Limits
2,4-Dlchlorophenylacefic acid
36
23_ 122
w
Client Sample ID: LENOIR WTP
Prep Type: Total/NA
Prep Batch: 316603
%Rec. RPD
Unit
D %Rec Limits RPD Limit
uglKg
81 46 -122 4 40
ug1Kg
713 47-127 0 40
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316961
D Prepared Analyzed Dil Fac
0512912017:20 06101/2019:37 20
0512912017:20 0610112019:37 20
Prepared Analyzed Dil Fac
05/29/20 f 7:20 06101120 19:37 20
05/29/2017.20 0610112019:37 20
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316961
%Rec.
Unit D %Rec Limits
mglL 21 19 -127
mglL 40 24 -128
Eurofins TestAmerica, Pittsburgh
Page 18 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCS 180-316961/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 317040 Prep Batch: 316961
LCS LCS
Surrogate %Recovery Qualifier
Limits
2, 4-Dichlorophenylacetic acid 47
23 -122
Lab Sample ID: LCSD 180-316961/3-A
Client Sample ID: Lab
Control Sample Duip
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317040
Prep Batch: 316961
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
2,4-D
0,200
0A4372
mg1L
22
19-127 3 35
Silvex (2,4,5-TP)
0.0500
0.02054
mglL
41
24-128 3 35
LCSD LCSD
Surrogate %Recovery QualiFer
Limits
2,4-Dichlorophenylacefic acid 37
23 -122
2,4-Dichlorophenylaceiic acid 48
23-122
Lab Sample ID: LB 180-31668311-F
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 317040
Prep Batch: 316961
LB LB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
2,4-D ND
0.0400
mglL
05/2912017:20
06/0112013:19 20
Silvex (2,4,5-TP) ND
0.0100
mg1L
05/29/20 17:20
06/01/20 13:19 20
LS LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4-Urchlorophenylacefic acid 25
23-122
05/29/20 17:20
0610120 13:19 20
2,4-Dichlorophenyfaceiic acid 33
23-122
0512920 17:20
06101120 13,19 20
Method: EPA 6010D - Metals (ICP)
Lab Sample ID: MB 180-31694111-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317142
Prep Batch: 316941
MB M8
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Silver ND
0.0500
mglL
05/2912015:21
06/01/2010:46 1
Barium ND
0.200
mg1L
0512912015:21
06/01/2010:46 1
Cadmium ND
0.0500
mglL
0512912015:21
06/01/2010:46 1
Chromium NO
0.0500
mg1L
05/29/2015:21
06101/2010:46 1
Lead ND
0.0500
mg1L
05/29/2015:21
06/01/2010:46 1
Selenium ND
0.0500
mg1L
0512912015:21
06101/2010:46 1
Arsenic ND ^
0.0500
mg1L
05/2912015:21
06/01/2010:46 1
Lab Sample ID: LCS 180-316941/2-A
CIient
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total1NA
Analysis Batch: 317142
Prep Batch: 316941
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Silver
0.250
0.2457
mgiL
98
80-120
Barium
1.00
0.9948
mglL
99
80-120
Eurofins TestAmerica, Pittsburgh
Page 19 of 30 6/4/2020

QC Sample Results
Client: Bio-Namics Services., Inc. Job ID: 180-106162-1
Project/Site: Lenoir WTP
Method: EPA fi01—OD - Metals (ICP) (Continued]
_ .....
Lab Sample ID: LCS 180-316941/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total1NA
Analysis Batch: 317142 Prep Batch: 316941
Spike
LCS LCS
Analyte
Added
Result Qualifier
Cadmium
0.500
0,4961
Chromium
0.500
0.4918
j Lead
0.500
0.4933
Selenium
1.00
0,9703
Arsenic
1.00
1.034 A
Lab Sample ID: LB 180-316683/1-C
Matrix: Solid
Analysis Batch: 317142
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
Silver
ND
0.500
mg/L
Barium
ND
2.00
mg1L
Cadmium
NO
0.500
mg1L
Chromium
ND
0.500
mg1L
Lead
NO
0.500
mg1L
Selenium
NO
0.500
mg/L
Arsenic
NO ^
0.500
mg/L
Lab Sample ID: 180-106201-A-1-L
MS
Matrix: Solid
Analysis Batch: 317142
Sample
Sample
Spike
MS MS
Analyte
Result
Qualifier
Added
Result Qualifier
Silver
ND
Fi
1.00
NO F1
Barium
3.03
F1 F2
50.0
27.10 F1
Cadmium
NO
1.00
0.9592
Chromium
NO
5.00
4.688
Lead
NO
F1 F2
5.00
3.606 F1
Selenium
NO
1.00
0.8567
Arsenic
ND
A
5.00
4.920 A
Lab Sample ID: 180-106201-A-1-M MSD
Matrix: Solid
Analysis Batch: 317142
Sample Sample
Analyte
Result Qualifier
Silver
NO F1
Barium
3.03 F1 F2
Cadmium
ND
Chromium
ND
Lead
NO F1 F2
Selenium
ND
Arsenic
NO A
Spike
MSD MSD
Added
Result Qualifier
1.00
ND F1
50.0
18.40 F1 F2
1.00
0.9834
5.00
4.836
5.00
2.630 F1 F2
1.00
0.8581
5.00
5.053 A
%Rec.
Unit
D %Rec
Limits
mg/L
_ 99
80.120
mg/L
98
80 -120
mg/L
99
80 -120
mg1L
97
80 -120
mglL
103
80-120
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 316941
D Prepared
Analyzed
Oil Fac
05/29/20 15:21
06/01 /20 10:56
1
05/29/20 15:21
06/01 /20 10:56
1
05/29/20 15:21
06/01120 10:56
1
05/29/20 15:21
06/01/20 10:56
1
05/29/20 15:21
06/01120 10:56
1
05/29/20 15:21
06/01/20 10:56
1
05/29/20 15:21
06101 /20 10:56
1
Client Sample ID: Matrix Spike
Prep Type: TCLP
Prep Batch: 316941
%Rec.
Unit
D %Rec
Limits
mg/L
25
75.125
mg/L
48
75 _ 125
mg1L
96
75 -125
mg/L
94
75.125
mg1L
72
75.125
mg/L
82
75 -125
mg/L
98
75 -125
Client Sample ID: Matrix Spike Duplicate
Prep Type: TCLP
Prep Batch: 316941
%Rec. RPD
Unit
D %Rec
Limits RPD Limit
mg/L
28
75.125 10 20
mg1L
31
75 -125 38 20
mg1L
98
75.125 2 20
mg1L
97
75 -125 3 20
mg/L
53
75 -125 31 20
mg/L
82
75 -125 0 20
mg/L
101
75.125 3 20
Eurofns TestAmerica, Pittsburgh
Page 20 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Method: EPA 7470A - Mercury (CVAA)
Lab Sample ID: MB 180-31691511-A
Matrix: Solid
Analysis Batch: 316982
Job ID: 180-106162-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 316915
MP MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Mercury ND 0.000200 mg/L 05129/2015:10 0512912018:31 1
Lab Sample ID: LCS 180-316916/2-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total1NA
Analysis Batch: 316982 Prep Batch: 316915
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Mercury 0.00250 0.002498 mg/L 100 80-120
Lab Sample ID: LB 180-316683/1-B
Matrix: Solid
Analysis Batch: 316982
LB LB
Analyte Result Qualifier RL
Mercury ND 0.000200
Lab Sample ID: 180-106201-A-1-1 MS
Matrix: Solid
Analysis Batch: 316982
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 316915
MDL Unit D Prepared Analyzed Dil Fac
mglL 0512912015:10 0512912018:33 1
Client Sample ID: Matrix Spike
Prep Type: TCLP
Prep Batch: 316915
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec Limits
Mercury ND
0.00500
OA04666
mglL
93 75-125
Lab Sample ID: 180-106201-A-1-J MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 316982
Prep Batch: 316915
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec Limits RPD Limit
Mercury ND
6.00500
0.004784
mg1L
96 75- 225 2 20
Method: EPA 1020B - Ignitability, Small Scale Closed -Cup Method
Lab Sample ID: 680.181927-A-6 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 316583
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit
D RPD Limit
Ignitability >140
>140
Degrees F
NC 20
Method: EPA 9014 - Cyanide
Lab Sample ID: MB 180-317066/4-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 317144
Prep Batch: 317066
MB M13
Analyte Result Qualifier
RL MDL Unit
D
Prepared Analyzed Dil Fac
Cyanide, Total ND
0.500 mg/Kg
06/01/20 12:00 06/01/20 13:48 1
Eurofins TestAmerica, Pittsburgh
Page 21 of 30 6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Method: EPA 9014 - Cyanide (Continued)
Lab Sample ID: HLCS 180-317066/2-A
Matrix: Solid
Analysis Batch: 317144
Analyte
Cyanide, Total
Lab Sample ID: LCS 180-317066/3-A
Matrix: Solid
Analysis Batch: 317144
Analyte
Cyanide, Total
Lab Sample ID: LLCS 180-317066/1-A
Matrix: Solid
Analysis Batch: 317144
Analyte
Cyanide, Total
Lab Sample ID: 180-105925-B-1-W MS
Matrix: Solid
Analysis Batch: 317144
Sample Sample
Analyte Result Qualifier
Cyanide, Total N❑
Spike
Added
0.250
Job ID: 180-106162-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 317066
HLCS HLCS %Rec.
Result Qualifier Unit D %Rec Limits
0.2504 mg/Kg 100 90 -110
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 317066
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
23.1 20.13 mglKg 87 25. 150
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 317066
Spike LLCS LLCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.0500 0.05220 mg1Kg 104 90 -110
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 317066
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
4.00 3,468 i gg Kg 87 75 - 225
Lab Sample ID: 180-105925-B-1-X MSD
Matrix: Solid
Analysis Batch: 317144
Sample Sample Spike MSD MSD
Analyte Result Qualifier Added Result Qualifier
Cyanide, Total ND 3.92 3.206
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 317066
%Rec. RPD
Unit D %Rec Limits RPD Limit
mg1Kg 82 75 -125 8 20
-_. —
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 180-31657411-A
Matrix: Solid
Analysis Batch: 316625
MB MB
Analyte Result Qualifier
Sulfide ND
Lab Sample ID: LCS 180-316574/2-A
Matrix: Solid
Analysis Batch: 316625
Analyte
Sulfide
Client Sample ID: Method Blank
Prep Type: TotaI1NA
Prep Batch: 316574
RL MDL Unit D Prepared Analyzed Dil Fac
30.0 mg/Kg _ 05/27/20 09:00 05/27/20 12:00 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 316574
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
172 161.2 mg/Kg 94 85 -115
Eurofins TestAmerica, Pittsburgh
Page 22 of 30
6/4/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 180-106162-1
ProjecttSite: Lenoir WTP
Method: EPA 9034 - Sulfide Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 180-105766-A-1-D MS
Matrix: Solid
Analysis Batch: 316625
Sample Sample
Analyte
Result Qualifier
Sulfide
ND
Lab Sample ID: 180-105766-A-1-E
MSD
Matrix: Solid
Analysis Batch: 316625
Sample Sample
Analyte
Result Qualifier
Sulfide
ND
Method: EPA 9045D - pH
Lab Sample ID: LCS 180-31679011
Matrix: Solid
Analysis Batch: 316790
Analyte
pH
Lab Sample ID: 180-105906-A-1 DU
Matrix: Solid
Analysis Batch: 316790
Analyte
Sample Sample
Result Qualifier
8.6
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch:316574
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
171 146.3 mg/Kg 85 75-125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 316574
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
174 147.0 mgMg 85 75- 225 1 20
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS
%Rec.
Added Result Qualifier
Unit
D %Rec Limits
7.00 7.0
5U
100 99 _ 101
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU
RPD
Result Qualifier
Unit
D RPD Limit
&6
SU
0.3 2
Eurofins TestAmerica, Pittsburgh
Page 23 of 30
6/4/2020

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
GC/MS VOA
Leach Batch: 316691
Job ID: 180-106162-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
160-106162-1
LENOIR WTP
TCLP
Sludge
EPA 1311
LB 180-316691/1-A
Method Blank
TCLP
Solid
EPA 1311
180-105839-A-13-B MS
Matrix Spike
TCLP
Solid
EPA 1311
180-105839-A-13-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Analysis Batch: 316868
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 8260D
316691
LB 18D-31669111-A
Method Blank
TCLP
Solid
EPA 8260D
316691
LCS 180-316868/3
Lab Control Sample
Total/NA
Solid
EPA 8260D
180-105839-A-13-B MS
Matrix Spike
TCLP
Solid
EPA 8260D
316691
180-105639-A-13-C MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 8260D
316691
GC/MS Semi VOA
Leach Batch: 316683
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 1311
LB 180-316663/1-D
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 316950
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
3510C
316683
LB 180-316683/1-D
Method Blank
TCLP
Solid
3510C
316683
MB 180-316950/1-A
Method Blank
Total/NA
Solid
3510C
LCS 180-316950/2-A
Lab Control Sample
Total/NA
Solid
3510C
LCSD 180-31695013-A
Lab Control Sample Dup
TotaI1NA
Solid
3510C
Analysis Batch: 317153
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 8270E
316950
LB 180-316683/1-D
Method Blank
TCLP
Solid
EPA 8270E
316950
MB 180-31695011-A
Method Blank
Total/NA
Solid
EPA 8270E
316950
LCS 180-31695012-A
Lab Control Sample
Total/NA
Solid
EPA 8270E
316950
LCSD 180-316950/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8270E
316950
-.-..........
GC Semi VOA
.,.... .-
Prep Batch: 316603
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
3541
MB 180-31660311-A
Method Blank
Total/NA
Solid
3541
LCS 180-316603/2-A
Lab Control Sample
Total/NA
Solid
3541
180-106162-1 MS
LENOIR WTP
TotaUNA
Sludge
3541
180-106162-1 MSD
LENOIR WTP
Total/NA
Sludge
3541
Leach Batch: 316683
Lab Sample ID
Client Sample 1D
Prep Type
Matrix
Method
Prep Batch
184-106162-1
LENOIR WTP
TCLP
Sludge
EPA 1311
LB 180-31668311-E
Method Blank
TCLP
Solid
EPA 1311
LB 180-316683/1-F
Method Blank
TCLP
Solid
EPA 1311
Eurofins TestAmerica, Pittsburgh
Page 24 of 30 6/4/2020

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
GC Semi VOA
Job ID: 180-106162-1
Analysis Batch: 316711
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
EPA 8082A
316603
MB 180-316603/1-A
Method Blank
TotaWNA
Solid
EPA 8082A
316603
LCS 180-316603/2-A
Lab Control Sample
Total/NA
Solid
EPA 6062A
316603
180-106162-1 MS
LENOIR WTP
Total/NA
Sludge
EPA 8082A
316603
180-106162-1 MSD
LENOIR WTP
TotaIINA
Sludge
EPA 8082A
316603
Prep Batch: 316951
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
3510C 316683
LB 180-31666311-E
Method Blank
TCLP
Solid
3510C 316683
MB 180-31695111-A
Method Blank
Total/NA
Solid
3510C
LCS 180-31695112-A
Lab Control Sample
TotalfNA
Solid
3510C
LCSD 180-316951/3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Prep Batch: 316961
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
8151A 316683
LB 180-31668311-F
Method Blank
TCLP
Solid
8151A 316683
ME 180-316961/1-A
Method Blank
Total/NA
Solid
8151A
LCS 180-316961/2-A
Lab Control Sample
Total/NA
Solid
8151A
LCSD 180-316961/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
Analysis Batch: 317040
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 8151A
316961
LB 180-316683/1-F
Method Blank
TCLP
Solid
EPA 8151A
316961
ME 180-31696111-A
Method Blank
Total/NA
Solid
EPA 6151A
316961
LCS 180-31696112-A
Lab Control Sample
Total/NA
Solid
EPA 8151A
316961
LCSD 180-316961/3-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8151A
316961
Analysis Batch: 317106
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 8081E
316951
LB 180-31668311-E
Method Blank
TCLP
Solid
EPA 8081E
316951
ME 180-31695111-A
Method Blank
Total/NA
Solid
EPA 8081E
316951
LCS 180-316951/2-A
Lab Control Sample
Total/NA
Solid
EPA 8081B
316951
LCSD 180-31695113-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8081 B
316951
Metals
Leach Batch: 316683
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
1180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 1311
LB 180-316683/1-6
Method Blank
TCLP
Solid
EPA 1311
LB 180-316683/1-C
Method Blank
TCLP
Solid
EPA 1311
160-106201-A-1-I MS
Matrix Spike
TCLP
Solid
EPA 1311
180-106201-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
180-106201-A-1-L MS
Matrix Spike
TCLP
Solid
EPA 1311
180-106201-A-1-M MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 1311
Eurofins TestAmerica, Pittsburgh
Page 25 of 30 6/4/2020

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
Metals
Prep Batch: 316915
Lab Sample ID Client Sample ID
Prep Type
-
Matrix
Job ID: 180-106162-1
--
.-......—
Method Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
7470A
316683
LB 180-316663/1-B
Method Blank
TCLP
Solid
7470A
316683
MB 180-31691511-A
Method Blank
Total/NA
Solid
7470A
LCS 180-31691512-A
Lab Control Sample
Total[NA
Solid
7470A
180-106201-A-1-1 MS
Matrix Spike
TCLP
Solid
7470A
316683
180-106201-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
7470A
316683
Prep Batch: 316941
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
3010A
316683
LB 180-31668311-C
Method Blank
TCLP
Solid
3010A
316683
MB 180-316941/1-A
Method Blank
Total/NA
Solid
3010A
LCS 180-316941/2-A
Lab Control Sample
Tot2UNA
Solid
3010A
180-106201-A-1-L MS
Matrix Spike
TCLP
Solid
3010A
316683
180-106201-A-1-M MSD
Matrix Spike Duplicate
TCLP
Solid
3010A
316683
Analysis Batch: 316982
Lab Sample I❑
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR UVTP
TCLP
Sludge
EPA 7470A
316915
LB 180-31668311-B
Method Blank
TCLP
Solid
EPA 7470A
316915
MB 180-316915/1-A
Method Blank
TotallNA
Solid
EPA 7470A
316915
LCS 180-31691512-A
Lab Control Sample
Total/NA
Solid
EPA 7470A
316915
180-106201-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 7470A
316915
180-106201-A-1-J MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 7470A
316915
Analysis Batch: 317142
Lab Sample ID
Client Sample I❑
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
TCLP
Sludge
EPA 6010D
316941
LB 180-31668311-C
Method Blank
TCLP
Solid
EPA 601 OD
316941
MB 180-316941/1-A
Method Blank
Total/NA
Solid
EPA 6010D
316941
LCS 180-316941/2-A
Lab Control Sample
Total/NA
Solid
EPA 6010D
316941
180-106201-A-1-L MS
Matrix Spike
TCLP
Solid
EPA 6010D
316941
180-106201-A-1-M MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 601OD
316941
General Chemistry
Prep Batch: 316574
Lab Sample [❑
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-106162-1
LENOIR WTP
TotalINA
Sludge
9030B
MB 180-316574/1-A
Method Blank
Total/NA
Solid
9030B
LCS 180-31657412-A
Lab Control Sample
Total/NA
Solid
9030E
180-105766-A-1-D MS
Matrix Spike
Total/NA
Solid
9030E
180-105766-A-1-E MSD
Matrix Spike Duplicate
Total/NA
Solid
90308
Analysis Batch: 316583
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
EPA 1020E
680-181927-A-6 DU
Duplicate
Total/NA
Solid
EPA 1020B
Eurofins TestAmerica, Pittsburgh
Page 26 of 30 6/4/2020

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Lenoir WTP
General Chemistry
Job ID: 180-106162-1
Analysis Batch: 316625
�........_
................. --
Lab Sample ID
Client Sample la
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
EPA 90 44
316574
MB 180-31657411-A
Method Blank
Total/NA
Solid
EPA 9034
316574
LCS 180-31657412-A
Lab Control Sample
Total/NA
Solid
EPA 9034
316574
180-105766-A-1-D MS
Matrix Spike
Total/NA
Solid
EPA 9034
316574
180-105766-A-1-E MS❑
Matrix Spike Duplicate
Total/NA
Solid
EPA 9034
316574
Analysis Batch: 316790
Lab Sample 1D
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
EPA 9045D
LCS 180-31679011
Lab Control Sample
TotallNA
Solid
EPA 9045D
180-105906-A-1 DU
Duplicate
Total/NA
Solid
EPA 9045D
Prep Batch: 317066
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
9010C
MB 180-31706614-A
Method Blank
TotaVNA
Solid
9010C
HLCS 180-317066/2-A
Lab Control Sample
Total/NA
Solid
9010C
LCS 180-31706613-A
Lab Control Sample
Total/NA
Solid
9010C
LLCS 180-317066/1-A
Lab Control Sample
Total/NA
Solid
9010C
180-1 05925-B-1 -W MS
Matrix Spike
Total/NA
Solid
9010C
180-1 05925-B-1 -X MSD
Matrix Spike Duplicate
Total/NA
Solid
9010C
Analysis Batch: 317144
Lab Sample 10
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
180-106162-1
LENOIR WTP
Total/NA
Sludge
EPA 90 44
317066
MB 180-31706614-A
Method Blank
Total/NA
Solid
EPA 9014
317066
HLCS 180-31706612-A
Lab Control Sample
Total/NA
Solid
EPA 9014
317066
LCS 180-317066/3-A
Lab Control Sample
TotaUNA
Solid
EPA 9014
317066
LLCS 180-31706611-A
Lab Control Sample
Total/NA
Solid
EPA 9014
317066
180-105925-B-1-W MS
Matrix Spike
Total/NA
Solid
EPA 9014
317066
180-105925-B-1-X MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9014
317066
Euroftns TestAmerica, Pittsburgh
Page 27 of 30 6/4/2020

Pittsburgh TestAmedca
301 Alpha Drive h rloite 22 Chain
Custody
I + ` y Record
L� 41,��R ��l. u'SL�U•1 7HE LEnf]ER IN ENVIRONMENTAL TESTING
Pilisburgh, PA 15238
Mow 412.963.7059 fax [phone]
W....a■....... r _t____.__:__
Client COntaet
`'telinquished
Project Manager. VAuglm Stevenson
Site Contact:
Date: 5/22/211
CDC No:
Bio-Nomie Services
Tel/Fax:
Cab Contact: Ken Mayes
Carrier: Fedex
I of I COCs
530 Woodlawn Street
rq
5
e
v
F
U
f
16
FL-
0,
F
a
CL
E
C
a
h
a
x
t
Belmont, NC 28012
Calendar ( C ) or Work Days (W)
704-529-0000
TAT ifdifferentfmniBelow
2 weeks
0 I week
O 2 days
0 I day
SDG No.
Project Name: Lenoir WTP
State: NC
P O# 53348
Sample Identification
Sample
Date
Sample
'rime
Sample
'Type
Matrix
Nuf
Cunt
Sample Specific Notes:
I.enior WTP
5/22/2020
900
`sludge
*sludge
X
X
X
X
X
x
X
X
"Use Alternate Matrix; Sludec
180-1 D6162 Ghain of Cusivdy
Preservation llseM I= lee, 2=11C1; 3=112SO4: 4=11NO3; S=NaOII; 6= Other
Possible Hazard Identification Sample Disposal (A fee may be assessed if samples are retained tonger than i month)
Nw,-H¢nrd = Flammable =Skirl irritant Poison B � Unknown E Return To Client Disposal By Lab Archive For Months
Special InstructionslQC Requirements & Comments: *Alternate. Matrix: Shift
Relinquished by: Company: DateTrime: [Zee ii ed'hy: Company: Date ime: y
�...,
4elinquished by J
` lv 1
Company:
Dale I'il :
� ace
Received by:
c c cc t� �.�
Comps
i�l
Datefl'ime:
o
by:
Company:
Datcfrin e:
Received by:
Company:
Daterrime: ��

�� ..PNVA (704j'392-1164
601VIilwf S—W DATE
1138-9 QUEEN CfTyDRlVE CAD. 5096,iN a
CHMLMM NC 2.8208' 1
' BILL THIRD PhRTy '
TO ., j
X y PLE REC
a
�,E TAME-RICq z.
3a'fALPNA DRJ
t Rl p aR� r t
t � �
¢t fsBURGH RA 152388
rr YYY: REF
4
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ll� flf Ipoll 1110tu!!l��f1�� I�IfIu: �y
3 ' '
r �sAruAY
PRfb
98 05 R�TY AVER
1 f a
icorrecfed temp °C
ermorneter ID
r7
Initials I
k ±l'TaiY"R-0Gt a%diva 7/26/13

Login Sample Receipt Checklist
Client: Bio-Nomics Services., Inc.
Login Number: 106162
List Number: 1
Creator: Watson, Debbie
Question
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody sea[, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, Incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4"),
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Job Number: 180-106162-1
List Source: Eurofins TestAmerica, Pittsburgh
Answer Comment
NIA
True
True
True
True
True
True
True
True
True
False
True
True
True
True
True
True
True
True
True
True
True
Tru e
NIA
Eurofins TestAmerica, Pittsburgh
Page 30 of 30 6/4/2020

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 16, 2020
Greenville Utility Commision 91 Permit No. WQ0039053
2.32 % Solids
6.3 pH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg (Mg/Kgx 0.002)
Nitrogen (TKN)
0.066
659.000
L318
Phosphorus
0.003
33,900
0.068
Potassium
0,002
22.900
0.046
PAN injected)*
0.027
270.130
0.540
PAN surface)*
0.019
186.630
0.373
Ammonia Nitrogen
0.017
167.000
0.334
Calcium
0.003
28.300
0.057
Calcium Carbonate E .
40.200
58,000.000
116.000
Ma nesium
0.002
16.900
0.034
Sodium
0.003
25.000
0.050
Sulfur
---
128.000
0.256
Nitrate N / Nitrite N
---
4.730
0.009
Barium
---
---
---
SAR
0.14
Chloride
---
---
---
Iron
---
523.000
1.046
Ceiling Concen.
(Mg/Kg)
Aluminum
---
2,240.00
4.480
Arsenic
---
0.50
0.001
75
Cadmium
---
0,100
0.000
85
Chromium
---
0,527
0.001
-
Copper
---
3.20
0.006
4,300
Lead
---
0.41
0.001
840
Mercury
---
0.0155
0.000
57
Molybdenum
---
0.25
0.001
75
Nickel
---
0.25
0.001
420
Selenium
---
0.50
0.00I
100
Zinc
---
1.40
0.003
7,500
Waypoint Analytical 20-077-0008
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
n�
willcox&mabe
Prepared By: SOIL SOLUTIONS

Waypoint(2)
ANALYTICAL
3/26/2020
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 20-077-0008
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 3/17/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
?, & ieC.r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-077-0008
Client Project Description: GUC
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70804
GUC #1
Solids
03/16/2020
03/17/2020
70804
GUC #1
Solids
03/16/2020
03/17/2020
SM-254OG
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
SW-7471B
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
SM-4500-NH3C-TKN
WP MTN
70604
GUC #1
Solids
03/16/2020
03/17/2020
4500NO3F-2011
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
6010D
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
SM-4500-NH3C
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
9045D
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
9056A
WP MTN
70804
GUC #1
Solids
03/16/2020
03/17/2020
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

e
•
Way � � ��
7621 Whitepine
Road, Richmond,
VA 23237
PA
Main 804-743-9401 °
Fax $04-271-6446
NALYT[CAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Joel Coert
Project
GUC
Report Date : 03/26/2020
530 Woodlawn St
Information :
Received : 03/17/2020
Belmont , NC 28012
Report Number: 20-077-0008
RE'PORTOFANALYSI.S
Pauric McGroary
Agronomist
Lab No : 70804
Matrix:
Solids
Sample ID : GUC #i
Sampled:
3/16/2020 0:00
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Moisture
97.7
%
0.010
1
03/23/2013:54
CJR SM-2540G
Calcium Carbonate Equivalent
5.8
% - dry
0.1
1
03/20/20 10:59
DXT AOAC 955.01
Test
Results
Units
MOIL
DF
Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
167
mg/Kg
100
1
03/25/20 13:00
JPJ SM-4500-NH3C
Chloride
12.9
mg/Kg
4.00
1
03/24/2015:55
CCR 9056A
Nitrate+Nitrite-N
<4.73
mg/K9
4.73
1
03/24/2014:30
ZBD 4500NO3F-2011
Organic N
492
mg/Kg
250
1
03/25/20 11:00
CALCULATION
pH
6.3
S.U.
1
03/24/20 05:59
JSL 9045D
Total Solids
2.32
%
0.010
1
03/23/20 13:54
CJR SM-2544G
Total Volatile Solids
44.8
%
0,010
1
03/23/20 13:54
CJR SM-254OG
Total Kjeldahl Nitrogen
659
mg/Kg
250
1
03/25/20 11:00
JPJ iM-4500-NH3C-TKi'
Phosphorus
33.9
mg/Kg
5.00
1
03/19/20 18:58
KKM 6010D
Aluminum
2240
mg/Kg
5.00
1
03/19/2018:58
KKM 6010D
Arsenic
<0.500
mg/Kg
0.500
1
03/19/2018:58
KKM 6010D
Calcium
28.3
mg/Kg
25.0
1
03/19/2018:58
KKM 6010D
Cadmium
<0.100
mg/Kg
0.100
1
03/19/2018:58
KKM 6010D
Chromium
0.527
mg/Kg
0.250
1
03/19/2018:58
KKM 6010D
Copper
3.20 B
mg/Kg
0.250
1
03/20/20 12:54
KKM 6010D
Iron
523
mg/Kg
5.00
1
03/19/2018:58
KKM 6010D
Qualifiers/ B Analyte detected in blank
DF Dilution Factor
Definitions L Limit Exceeded
MQL Method
Quantitation Limit
Page 3 of 7

Waypdlont,(2)
ANALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC 28012
Report Number: 20-077-0008
Lab No : 70804
Sample ID : GUC #1
Project CUC
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanatybcal.com
REPORTOFANALYSIS
Report Date : 03/26/2020
Received : 03/17/2020
POW=G m` (fa"r
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 3/16/2020 0:00
Test
Results
Units
MOL
DF
Date / Time
Analyzed
8y
Analytical
Method
Lead
0.405
mg/Kg
0.300
1
03/19/2018:58
KKM
6010D
Magnesium
16.8
mg/Kg
5.00
1
03/19/2018:58
KKM
6010D
Manganese
11.6
mg/Kg
0.500
1
03/19/2018:58
KKM
6010D
Mercury
<0.0155
mg/Kg
0.0155
1
03120/2012:50
KKM
SW-7471B
Molybdenum
<0.250
mg/Kg
0.250
1
03/19/2018:58
KKM
6010D
Nickel
<0.250
mg/Kg
0.250
1
03/19/2018:58
KKM
6010D
Potassium
22.9
mg/Kg
5.00
1
03/19/2018:58
KKM
6010D
Selenium
<0.500
mg/Kg
0.500
1
03/19/2018:58
KKM
6010D
Sodium
<25.0
mg/Kg
25.0
1
03/19/2018.58
KKM
6010D
Zinc
1.40
mg/Kg
1.25
1
03/19/2018:58
KKM
6010D
Sulfur
128
mg/Kg
5.00
1
03/19/2018:58
KKM
6010D
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions
Page 4-of 7

(2)
WayPAoint
NALYTICAL
Client: Bio-Nomic Servics Inc
Project: GUC
Lab Report Number: 20-077-0008
Date: 3/25/2020
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 " Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 70804 (GUC#1)
Analyte: Copper
QC Batch No: L4835301L483018
Target analyte(s) was identified in the method blank associated with this project. Per laboratory protocol any
associated affected sample result is flagged "B" to indicate that it was detected in the method blank.
Page 5 of 7

Waypoin(Dt.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Sio-Nomic Servics inc
Report Number: 20-077-0008
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
! '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
I♦ Yes
0 No
CDC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
• Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
F_ High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
[_ Low concentration EnCore samplers (48 hr)
F_ Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0 Yes 0 No
Signature: jBrandi Watson Date & Time: 03/17/2020 14:24:54
Page 6 of 7

WASTEWATER SAMPLE TRANSMITTAL FORM/CHAIN OF CUSTODY
Waypoint Analytical
7621 Whircpiec Road Richmond VA 23237 Tcl: 804443.9401 Fax: H04-271-6446 Email: supportva@waypoinaaanlytical,com
Customer information
[, ] Submitted By Charge To Copy To
t`f �' ed
'roject
Sample ID
I Ck
Lab Humber
(Lab Use
Only)
t N 7'�011
Phone:
Collection Information
"oa — AL26c?I2__ I
f
Fax: E-mail: ' oar r L`! ��t ld1L . w vpx
Sam le Information
Container Informatfon Please Write in Desired Tests
Type
Data
Time
ofu hies
Type
Volume
'v
; l
1
^
I
{
g�-
^ Grab
—Composite
Glass
Plastic
— oz
�Fint
✓
�/ ql
A—=
Grab
Composite
_ Glass—
Plastic
oz
—pinl
1
Grab
_ Composite
_Glass
Plastic
,-- oz
--mint
t
Grab
Glass
— oz
Composite
_ Plastic
-----pint
isphorus(total, orthar), Poatsslum, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
tganose, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Load,
tnium, Silver, Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
mical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease {EPA),
Phenol, Solids (Dissolved, Suspended, Total, Volatile)
A
Account it
Page 7 of 7

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 27, 2020
Greenville Utility Commision #2 Permit No. WQ0039053
20.30 % Solids
5.4 W
Parameter
%
Mg/Kg Dry Weight
x 10,000)
Pounds/Dry Ton
(M x 0.002)
Nitrogen (TKN)
1.190
11,900.000
23.800
Phosphorus
0.282
2,820.000
5.640
Potassium
0.079
793.000
1.586
PAN (injected)*
0,293
2,925.300
5.851
PAN (surface)*
0.261
2,612.300
5.225
Ammonia Nitrogen
0.063
626.000
1.252
Calcium
0.186
1,860.000
3.720
Calcium Carbonate E .
40.200
82,000.000
164.000
Magnesium
0.103
1,030.000
2.060
Sodium
0.021
211.000
0.422
Sulfur
---
4,830.000
9.660
Nitrate N / Nitrite N
---
44.500
0.089
Barium
Chloride
---
---
---
---
---
SAR
0.44
Iron
---
30800.000
61.600
Ceiling Concept.
(Mg/kg)
Aluminum
---
129,000.00
258,000
Arsenic
---
12.60
0.025
75
Cadmium
---
0.493
0.001
85
Chromium
---
46.100
0.092
---
Copper
---
265.00
0.530
4,300
Lead
---
24.10
0.048
840
Mercury
---
0.3720
0.001
57
Molybdenum
---
2.17
0.004
75
Nickel
---
14.50
0.029
420
Selenium
---
2.46
0.005
100
Zinc
---
61.10
0.122
7,500
waypoint Analytical 20-119-0005
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
♦ E a
willeox&mabe
Prepared By: SOIL_ SOLUTIONS

Waypointe)
ANALYTICAL
5/6/2020
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 20-119-0005
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/28/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
4• r6"7'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of G.

(2)
e
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-119-0005
Client Project Description: GLIC
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
71184
GUC #2
Solids
04/27/2020 14:00
04/28/2020
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
AOAC 955.01
WP MTN
Page 2 of 6

i
Waypoint,
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401
° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Joel Coert
Project
GUC
Report Date : 05/06/2020
530 Woodlawn St
Information :
Received : 04/28/2020
Belmont, NC 28012
nI
Report Number: 20-219-0005
REPORT OFANALYSXS
Pauric McGroary
Agronomist
Lab No: 71184
Matrix:
Solids
Sample ID : GUC #2
Sampled:
4/27/2020 14:00
Test
Results
Units
MQL
DF
Date 1 Time
By Analytical
Analyzed
Method
Moisture
79.7
%
0.010
1
04/29/20 17:09
CJR SM-2540G
Calcium Carbonate Equivalent 8.2
% - dry
0.1
1
05/05/20 12:18
DXT AOAC 955.01
Test
Results
Units
MQL
DF
Date I Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
626
mg/Kg - dry
493
1
05/05/20 11:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
44.5
mg/Kg - dry
22.6
1
04/30/20 14:33
ZBD 4500NO3F-2011
Organic N
11300
mg/Kg - dry
1230
1
05/04/20 10:00
CALCULATION
pH
5.4
S.U.
1
05/05/20 06:32
JSL 9045D
Total Solids
20.3
%
0.010
1
04/29/20 17:09
CIR SM-254OG
Total Volatile Solids
35.0
%
0.010
1
04/29/20 17:09
CJR SM-254OG
Total Kjeldahl Nitrogen
11900
mg/Kg - dry
1230
1
05/04/20 10:00
JPJ iM-4500-NH3C-T0
Phosphorus
2820
mg/Kg - dry
24.6
1
04/30/20 17:31
KKM 6010D
Aluminum
129000
mg/Kg - dry
246
10
05/01/20 12:43
TJS 6010D
Arsenic
12.6
mg/K9 - dry
2.46
1
04/30/20 17:31
TJS 6010D
Calcium
1860
mg/Kg - dry
246
1
05/01/20 12:38
TJS 6010D
Cadmium
<0.493
mg/Kg - dry
0.493
1
04/30/20 17:31
KKM 6010D
Chromium
46.1
mg/Kg - dry
1.23
1
04/30/20 17:31
KKM 6010D
Copper
265
mg/Kg - dry
2,46
1
04/30/20 17:31
KKM 6010D
Iron
30800
mg/Kg - dry
49.3
1
04/30/20 17:31
TJS 6010D
Lead
24.1
mg/Kg - dry
1.48
1
04/30/20 17:31
KKM 6010D
Qualifiers/ DF
Dilution Factor
L Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page-3 of 6

WayPAointy
NALYTICAL
45671
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont , NC 28012
Report Number:20-119-0005
Lab No : 71184
Sample ID : GUC #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project GUC
Information .
REPORT OFANALYSIS
Report Date : 05/06/2020
Received : 04/28/2020
Pow'. Iff (fewr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 4/ 27/ 2020 14:00
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Magnesium
1030
mg/Kg - dry
24.6
1
04/30/20 17:31
KKM
6010D
Manganese
640
mg/Kg - dry
2.46
1
04/30/20 17:31
KKM
6010D
Mercury
0.372
mg/Kg - dry
0.0783
1
04/30/20 16:31
DDB
SW-7471B
Molybdenum
2.17
mg/Kg - dry
1.23
1
04/30/20 17:31
KKM
6010D
Nickel
14.5
mg/Kg - dry
1.23
1
04/30/20 17:31
KKM
60101)
Potassium
793
mg/Kg - dry
49.3
1
04/30/20 17:31
KKM
6010D
Selenium
t2,46
mg/Kg - dry
2.46
1
04/30/20 17:31
KKM
6010D
Sodium
211
mg/Kg - dry
123
1
04/30/20 17:31
KKM
6010D
Zinc
61.1
mg/Kg - dry
6.16
1
04/30/20 17:31
KKM
6010D
Sulfur
4830
mg/Kg - dry
49.3
1
04/30/20 17:31
KKM
6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 6

Waypoint..(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number: 20-119-0005
Shipping Method
i] Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other :
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
i
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
C) No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: 16randi Watson I Date & Time: 04/28/2020 13:31:50
Page 5 of 6

WASTEWA vl/CHAIN OF CUSTODY AccounE #
Ifllll!ff111!!fll!!!Ilffl!!IIIIIIIlIIIIlfIl!!IIINIIIIIIIIIIIIN 042819
0 0
5
45671
7621 Whitcpine Roar Bio-Norsk scrv:cs Inc 13.2s.sd supportva©waypointanalytical.com
GUC
Sub
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
GUC Phone: [phone] Fax:
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
E-mail: —N11@1011-rmaoesad com 7
Sample Information
Lab Number
Collection Information
Container Information
Sample ID
(tab Use
Only)
Type Date Time
Number
of Bottles Type Volume
TKN
NH4-N K
NO3-N
ue
�No
k' Grab
22i/� p f�w't
_ °Z
r
•
Composite
/ v
x I'fastic —pint
X X
n qt
— Grab
Glass — 0z
Composite
— Plastic pint
t
— Grab
Glass — oZ
Composite
_
Plastic —pint
t
_ Grab
Glass — Oz
Composite
Plastic —pint
Time
Copy To
Please Write in Desired Tests
pf. yr Hg, 1 Ne, Zn, CaCO3
cd. ca, Ni, XTS, Gr,Mg Org-N
cu.Pb I PH. So
Date
©©N
Test Available 0 7 I Sped
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, iron, Aluminum, C Icss A
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
110

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual 'Type: Wastewater Treatment Plant
Date Sampled: July 23, 2020
Greenville Utility Commision #3 Permit No. WQ0039053
15.20 % Solids
6 pH
Parameter
%
Mg/Kg Dry Weight
°!o x 10,000)
PaundslDry Ton
(MgfKg x 0.002)
Nitrogen (TKN)
1.190
11,900.000
23.900
Phosphorus
0.248
2,480.000
4.960
Potassium
0.051
512.000
1.024
PAN (injected)*
0.280
2,795.200
5.590
PAN (surface)*
0.263
2,630.700
5.261
Ammonia Nitrogen
0.033
329.000
0.658
Calcium
0.188
1,880.000
3.760
Calcium Carbonate E .
7.700
77,000.000
154.000
Magnesium
0.061
614.000
1.228
Sodium
0.021
208.000
0.416
Sulfur
---
5,750.000
11.500
Nitrate N I Nitrite N
---
152.000
0.304
Barium
Chloride
---
---
---
___
.._
_..
SAR
0.41
Iron
---
30900.000
61.800
Ceiling Concen.
(Mg/Kg)
Aluminum
--
143,000.00
286.000
Arsenic
--
I L60
0.023
75
Cadmium
---
0.658
0.001
85
Chromium
---
48.600
0.097
--
Copper
---
338.00
0.676
4,300
Lead
---
N.20
0.028
840
Mercury
---
0.4590
0.001
57
Molybdenum
---
1.74
0.003
75
Nickel
---
12.80
0.026
420
Selenium
---
5.26
0.011
100
Zinc
--
58.20
0.116
7,500
Waypoint Analytical 20-209-0001
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes.
willcox&mabe
Prepared By: SO] L SOLUTIONS

Waypoint_(Z)
ANALYTICAL
siai2020
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 20-209-0001
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
!Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/27/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NEIAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 3 of-6

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint'
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 20-209-0001
Client Project Description: GUC
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
73168
GUC #3
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
07/23/2020
08.45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
07/23/2020
08:45
07/27/2020
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
AOAC 955.01
WP MTN
Page 2 of 6

(2)
Way
i
�� ��
7621 Whitepine Road, Richmond, VA 23237
v
P
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
GUI
Joel Coert
Report Date : 08/04/2020
530 Woodlawn St
Information :
Received: 07/27/2020
Belmont , NC 26012
P�4 i�c
Report Number: 20-209-0001
REPORTOFANAL PSIS
Pauric McGroary
Agronomist
Lab No: 73168
Matrix:
Solids
Sample ID: GUC #3
Sampled:
7/23/2020 8:45
Test
Results
Units
MQL
DF
Date I Time
By Analytical
Analyzed
Method
Moisture
84.8
%
0.010
1
07/29/20 16:53
FMM SM-2540G
Calcium Carbonate Equivalent 7.7
% - dry
0.1
1
07/29/20 12:37
DXT AOAC 955.01
Test
Results
Units
MQL
DF
Date 1 Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
329
mg/Kg - dry
164
1
08/03/20 09:00
JPJ SM-4500-NH3C
Nitrate+Nitrite-N
152
mg/Kg - dry
32.9
1
08/03/20 14:49
ZBD 4500NO3F-2011
Organic N
11600
mg/Kg - dry
1640
1
08/03/20 07:00
CALCULATION
pH
6.0
S.U.
1
08/03/2017:12
ADM 9045D
Total Solids
15.2
%
0.010
1
07/29/20 16:53
FMM 5M-254OG
Total Volatile Solids
44.0
%
0.010
1
07/29/20 16:53
FMM SM-254OG
Total Kjeldahl Nitrogen
11900
mg/Kg - dry
1640
1
08/03/20 07:00
JPJ iM-4500-NH3C-TKP
Phosphorus
2480
mg/Kg - dry
32.9
1
07/30/20 00:32
JTR 6010D
Aluminum
143000
mg/Kg - dry
329
10
07/30/20 19:00
KKM 6010D
Arsenic
11.6
mg/Kg - dry
3.29
1
07/30/20 00:32
JTR 6010D
Calcium
1880
mg/Kg - dry
329
1
08/01/20 11:33
KKM 6010D
Cadmium
<0.658
mg/Kg - dry
0.658
1
07/30/20 00:32
JTR 6010D
Chromlum
48.6
mg/Kg - dry
1.64
1
07/30/20 00:32
JTR 6010D
Copper
338
mg/Kg - dry
3.29
1
07/30/20 00:32
JTR 6010D
Iron
30900
mg/Kg - dry
65.8
1
07/30/20 00:32
KKM 6010D
Lead
14.2
mg/Kg - dry
1.97
1
07/30/20 00:32
JTR 6010D
Qualifiers/ DF
Dilution Factor
L Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 6

(2)
7621 Whiteptne Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
45671
Bio-Nomic Servics Inc Project GUC
Joel Coert Report Date; 08/04/2020
530 Woodlawn St Information : Received : 07/27/2020
Belmont , NC 28012
Report Number: 20-209-OODI REPORTOF.4NALYSIS Pauric McGroaryAgronomist
Lab No: 73168 Matrix: Solids
Sample ID. GUC #3 Sampled: 7/23/2020 8:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Magnesium
614
mg/Kg - dry
32.9
1
07/30/20 00:32
JTR
6010D
Manganese
684
mg/Kg - dry
3.29
1
07/30/20 00:32
JTR
6010D
Mercury
0.459
mg/Kg - dry
0.0973
1
07/30/20 11:15
DDB
SW-7471B
Molybdenum
1.74
mg/Kg - dry
1.64
1
07/30/20 00:32
JTR
6010D
Nickel
12.8
mg/Kg - dry
1.64
1
07/30/20 00:32
JTR
6010D
Potassium
512
mg/Kg - dry
65.8
1
07/30/20 00:32
JTR
6010D
Selenium
5.26
mg/Kg - dry
3.29
1
07/30/20 00:32
JTR
6010D
Sodium
208
mg/Kg - dry
164
1
07/30/20 00:32
JTR
6010D
Zinc
58.2
mg/Kg - dry
8.22
1
07/30/20 00:32
JTR
6010D
Sulfur
5750
mg/Kg - dry
65.8
1
07/30/20 00:32
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

Waypoint(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waVpointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Servics Inc
Report Number. 20-209-0001
Shipping Method
i♦ Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
F 1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
• Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F High concentration pre -weighed (methanol -14 d) r- Low cone pre -weighed vials (Sod Sis -14 d)
Special precautions or instructions included? 0 Yes 40 No
Comments:
Signature: Brandi Watson Date & Time: 7/27/2020 09:59:12
Page 5 of 6

WASTEWATER SAMPLE TRANSMITTAL FORMICHAIN OF CUSTODY
Waypoint Analytical
7621 Whitcpine Road Richmond VA 23237 Tel: [phone] Fax, 804-271-6446 Email: supportvaC3a waypointanalyticat.com
Submitted By
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
GUC Phone:[phone]
Customer Information
Charge To
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
Account #
45671
20-20"001
1IIIIII1111111111111111111111111Jill III III IIIII IIIIIIllll11111111 n i7 2020
Bio-Nurnic Servics Inc 09:50:31
GUC
Fax: IE-mail: martin@%ilfcaxmabesell.coml
uSteVenSan@btu Aamjc,caRl
Sample ID
Lab Number
(Lab Use
Only)
Collection Information
Sample Information
Container Information
Please Write in Desired Tests
Type
Date
Time
Number
of Bottles
Type
Volume
NH4-N
p
K
C, rv,
Gd, Ga,
NI,
N1, %T
Cr.Na, g
Cr,Mg
CaC4
prg-N
NO3-N
Cu py
so
pH, Se
G �
x Grab
C)
�`
g �s Atk
_ oz
Composite
L`'
k
Pllasiic
---Pint
X
X
X
X
X
X
CZ qt
Grab
Glass
O2
Composite
_
Plastic
Pint
t
Grab
Glass
— Oz
— Composite
Plastic
—Pint
—
k
— Grab
Glass
— Oz
Composite
_
Plastic
---Pint
Relinquished By: (SignatuE!!2 I (SignatureDate I Time I Received By: (Signature) Date Time
I^LO
Test Available Special Instructions or
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen. I ft
Phosphorus(total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Nickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (BPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
as
44
0
to
m
to
ro
w

BIO-NOMIC SERVICES, INC.
LAND APPLICATION PROGRAM
CLASS A EQ RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: September 11, 2020
Greenville Utility Commision #4 Permit No. WQ0039053
16.30 % Solids
1; 1) .,u
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton
(Mg/Kg(Mg/Kg x 0.002)
Nitrogen (TKN)
1.320
13,200.000
26.400
Phosphorus
0.326
3,260.000
6.520
Potassium
0.055
549.000
1.098
PAN (injected)*
0.292
2,921,700
5.843
PAN (surface)*
0.277
2,768.200
5.536
Ammonia Nitrogen
0.031
307.000
0.614
Calcium
0.187
1,870.000
3.740
Calcium Carbonate E .
5.200
52,000.000
104.000
Magnesium
0.065
650.000
1.300
Sodium
0.027
267.000
0.534
Sulfur
---
5,440.000
10.880
Nitrate N / Nitrite N
---
36.100
0.072
Barium
...
---
Chloride
---
_--
___ I!
Iron
---
32,800.00
65.600
Aluminum
---
152,000.00
304.000
Arsenic
---
16.10
0.032
Cadmium
---
0.613
0.001
Chromium
---
50.100
0.100
Copper
---
319,00
0.638
Lead
---
23,10
0.046
Mercury
---
0.3130
0.001
Molybdenum
---
1.53
0.003
Nickel
---
13.60
0.027
Selenium
---
4.93
0.010
Zinc
---
58.80
0.118
r
I
Waypoint Analytical 20-258-0003
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
SAR
0.55
Ceiling Concen.
Surface Application:
(Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits
for calculation purposes,
s�
willcox&mabe
Prepared By: SOI L SOLUTIONS
75
85
840
57
75
420
100
7,501

Waypoint(D
ANALYTICAL
9/22/2020
Bio-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 20-258-0003
Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010Fax [phone]
www.waypointanalytical.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/14/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
.064W 0 yc".
Pauric McGroary
Agronomist
(�Qo c✓y/
e
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Waypoint(2)
ANALYTICAL
Report Number: 20-258-0003
Client Project Description: GUC
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
SM-2540G
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
SW-7471B
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
SM-4500-NH3C-TKN
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
4500NO3F-2011
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
60101)
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
SM-4500-NH3C
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
9045D
WP MTN
73629
GUC No 2
Solids
09/11/2020 11:22
09/14/2020
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

(2)
Waypoint
7621 Whitepine Road, Richmond,
VA 23237
Main $04-743-9401 °
Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic Servics Inc
Project
GUC
Joel Coert
Report
Date : 09/22/2020
530 Woodlawn St
Information :
Received: 09/14/2020
Belmont , NC 28012
�AW� is
i
kD w
Report Number: 20-258-0003
REPORT OF ANAL PSIS
Pauric
Mc Groary Ph.D., CPA
Agronomist
Lab No: 73629
Matrix:
Solids
Sample ID : GUC No 2
Sampled:
9/11/2020
11:22
Test
Results
Units
MOL
DF
Date I Time
By
Analytical
Analyzed
Method
Moisture
83.7
%
0.010
1
09/17/20 16:56
FMM
SM-2540G
Calcium Carbonate Equivalent
5.2
% - dry
0.1
1
09/17/20 13:10
DXT
AOAC 955.01
Test
Results
Units
MQL
DF
Date I Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
307
mg/Kg - dry
153
1
09/20/20 13:30
JP3
SM-4500-NH3C
Nitrate+Nitrite-N
36.1
mg/Kg - dry
29.6
1
09/16/20 13:57
ZBD
4500NO3F-2011
Organic N
12900
mg/Kg - dry
1530
1
09/20/20 13:00
CALCULATION
pH
6.2
S.U.
1
09116/2015:50
ADM
9045D
Total Solids
16.3
%
0.010
1
09/17/20 16:56
FMM
SM-2540G
Total Volatile Solids
42.7
%
0.010
1
09/17/20 16:56
FMM
SM-2540G
Total Kjeldahl Nitrogen
13200
mg/Kg - dry
1530
1
09/20/20 13:00
JPJ M-4500-NH3C-TKt
Phosphorus
3260
mg/Kg - dry
30.7
1
09/18/20 03:09
JARS
6010D
Aluminum
152000
mg/Kg - dry
307
10
09/18/20 18:04
]ADS
6010D
Arsenic
16.1
mg/Kg - dry
3.07
1
09/18/20 03:09
]ADS
6010D
Calcium
1870
mg/Kg - dry
307
1
09/18/20 03:09
]ADS
6010D
Cadmium
<0.613
mg/Kg - dry
0.613
1
09/18/20 03:09
]ADS
6010D
Chromium
50.1
mg/Kg - dry
1.53
1
09/18/20 03:09
JARS
6010D
Copper
319
mg/Kg - dry
3.07
1
09/18/20 03:09
JADS
6010D
Iron
32800
mg/Kg - dry
61.3
1
09/18/20 03:09
]ADS
6010D
Lead
23.1
mg/Kg - dry
1.84
1
09/18/20 03:09
]ADS
6010D
Qualifiers/ DF
Dilution Factor
L Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 6

(2)
•
Waypoint.
762x Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 °
Fax [phone]
ANALYTICAL
www.waypointanalytical.com
45671
Bio-Nomic 5ervics Inc
Project
GUC
Joel Coert
Report Date : 09/22/2020
530 Woodlawn St
Information :
Received : 09/14/2020
Belmont, NC 28012
`
Report Number: 20-258-0003
REPORT OFANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 73629
Matrix: Solids
Sample ID : GUC No 2
Sampled: 9/11/2020 11:22
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Magnesium
650
mg/Kg - dry
30.7
1
09/18/20 03:09 ]ADS 6010D
Manganese
822
mg/Kg - dry
3.07
1
09/18/20 03.09 ]ADS 6010D
Mercury
0.313
mg/Kg - dry
0.0858
1
09/17/20 12:00 DDB SW-7471B
Molybdenum
<1.53
mg/Kg - dry
1.53
1
09/18/20 03.09 ]ADS 6010D
Nickel
13.6
mg/Kg - dry
1.53
1
09/18/20 03:09 ]ADS 6010D
Potassium
549
mg/Kg - dry
61.3
1
09/18/20 03:09 ]ADS 6010D
Selenium
4.93
mg/Kg - dry
3.07
1
09/18/20 03:09 ]ADS 6010D
Sodium
267
mg/Kg - dry
153
1
09/18/20 03:09 ]ADS 6010D
Zinc
58.8
mg/Kg - dry
7.67
1
09/18/20 03:09 ]ADS 6010D
Sulfur
5440
mg/Kg - dry
61.3
1
09/18/20 03:09 3ADS 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

ANALYTICAL
Waypoint.,(D
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 45671
Customer Name: Bio-Nomic Setvics Inc
Report Number: 20-258-0003
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer 0:
^
Shipping container/cooler uncompromised?
4D Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
0 Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
• Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC property completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
NIA
Trip Blanks received with VOAs
0 Yes
0 No
NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
NIA
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: jBrandi Watson Date & Time: 09/14/2020 13:49:26
Page 5 of 6

WASTEWATER SAMI
7621 Whitepine Road Richmond VA 232",
2G-25"003
I�111l11111FIN111111111110111111111111111111111111111111111145571 20
GUC 13.47 37
Submitted By
Bic-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
GUC Phone: [phone] Fax:
)F CUSTODY
lanalytical.com
Charge To Copy To
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, NC 28012
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Sample information
Lab Number
Collection Information
Container Infomation
Please Write in Desired Tests
Sample ID
(Lab Use
Only)
Type Date Time
Number
T e Volume
of Bottles
TKNHg,
NH4-N P
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Test Available
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen,
Phosphorus (total, orthor), Poatssium, Sulfate -Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,
Manganese, Copper, Zinc, Arsenic, Barium, Cadmium, Chromium, Cobalt, Molybdenum, Mercury, Lead,
Selenium, Silver. Mickel. Acidity (Total), Alkalinity (Total), Biochemical Oxygen Demand (5 days), Boron,
Chemical Oxygen Demand, Chloride, Conductance (Specific), Hexavalent Chromium, Oil and Grease (EPA),
pH, Phenol, Solids (Dissolved, Suspended, Total, Volatile)
Date Time
- M40 M W
Instructions or Remarks
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45671
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eurofins
ANALYTICAL REPORT
Eurofins TestAmerica, Chicago
2417 Bond Street
University Park, IL 60484
Tel: [phone]
Laboratory Job ID: 500-179338-1
Client Project/Site: Greenville Utility Water Plant
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Vaughn Stevenson
Authorized for release by.
313012020 3.20:03 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNl requirements for accredited
parameters, exceptions aro noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Laboratory Job IQ: 500-179338-1
Cr�,l
Table of Contents
Cover Page .............................................. 1
Table of Contents ......................................... 2
Case Narrative ........................................... 3
Detection Summary ........................................ 4
Method Summary ......................................... 5
Sample Summary ......................................... 6
Client Sample Results ...................................... 7
Definitions ............................................... 9
QC Association ........................................... 10
Surrogate Summary ....................................... 13
QC Sample Results ........................................ 17
Chronicle ................................................ 26
Certification Summary ...................................... 27
Chain of Custody .......................................... 28
Receipt Checklists ......................................... 29
Eurotins TestAmerica, Chicago
Page 2 of 29 3/30/2020

Case Narrative
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Job ID: 500-179338-1
Laboratory: Eurofins TestAmerica, Chicago
Narrative
Job Narrative
500-179338-1
Comments
No additional comments.
Job ID: 500-179338-1
Receipt
The samples were received on 3/14/2020 12:10 PM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperature of the cooler at receipt was 1.80 C.
GClMS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC/MS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
Method 8081 B: DCB Decachlorobiphenyl Surrogate recovery for the following samples were outside the upper control limit: Greenville
Utility (500-179338-2) and (MB 500-535163/1-A). This samples did not contain any target analytes; therefore, re -extraction and/or
re -analysis was not performed.
Method 8082k The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation batch
500-535414 and analytical batch 500-535496 recovered outside control limits for the following analytes: PCB-1016 and PCB-1260;
however, %recovery was within control limits for both the LCS and LCSD.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page,
General Chemistry
No analytical or quality issues were noted, other than those described in the DefinitionslGlossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
9 Eurofins TestAmeric 3/ Q/2Q20
Page 3of29

Detection Summary
Client: Bio-Nomics Services., Inc.
Job ID: 500-179338-1
ProjecttSite: Greenville utility Water Plant
Client Sample ID: Greenville Utility
_
Lab Sample ID: 500-179338-2
Analyte Result Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
Flashpoint >176
99.0
Degrees F
1 _ 1010A Total/NA f
Sulfide 37.6
5.00
mg/L
1 9034 Total/NA
pH 5.56 HF
0.200
SU
1 9040C Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Chicago
Page 4 of 29 3/30/2020

Method Summary
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Protocol
Laboratory
Method
Method Description
8260D
Volatile Organic Compounds by GClMS
SW846
TAL CHI
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL CHI
8081 B
Organochlorine Pesticides (GC)
SW846
TAL CHI
8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
SW846
TAL CHI
8151A
Herbicides (GC)
SW846
TAL CHI
6010D
Metals (ICP)
SWB46
TAL CHI
7470A
Mercury (CVAA)
SW846
TAL CHI
1010A
Ignitability, Pensky-Martens Closed -Cup Method
SW846
TAL CHI
9014
Cyanide
SW846
TAL CHI
9034
Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAIL CHI
9040C
pH
SW846
TAL CHI
1311
TCLP Extraction
SW846
TAL CHI
3010A
Preparation, Total Metals
SW846
TAL CHI
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL CHI
5030B
Purge and Trap
SW846
TAL CHI
7470A
Preparation, Mercury
SW846
TAL CHI
8151A
Extraction (Herbicides)
SW846
TAL CHI
9010B
Cyanide, Distillation
SW846
TAL CHI
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CHI = Eurofins Test4merica, Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
Eurofins TestAmerica, Chicago
Page 5 of 29 3/30/2020

Sample Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Lab Sample ID Client Sample ID Matrix
500-179338-2 Greenville Utility Sludge
Job ID: 500-179338-1
Collected Received Asset ID
03/12/20 00:00 03/14/20 12:10
Eurofins TestAmerica, Chicago
Page 6 of 29 3/30/2020

Client Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
-- ....... ..
Client Sample ID: Greenville Utility Lab Sample ID: 500-479338-2
Date Collected: 03/12/20 00:00 Matrix: Sludge
Date Received: 03/14/20 12:10
Method: 8260D -Volatile Organic Compounds by GC/MS - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
1,1-❑ichloroethene
ND
20.0
ug/L
0312612017:09
20
1,2-Dichloroethane
ND
20.0
ug/L
03/2612017:09
20
2-Butanons (MEK)
ND
100
ug/L
03/26/20 17:09
20
Benzene
ND
20.0
ug/L
03/26/20 17:09
20 { 4"
Carbon tetrachloride
ND
20.0
ug/L
03/26/20 17:09
20
Chlorobenzene
ND
20.0
ug/L
03126/2017:09
20
Chloroform
ND
40.0
ug/L
0312612017:09
20
Tetrachloroethene
ND
20,0
ug1L
03126/2017:09
20
Trichloroethene
ND
20.0
ug/L
03126/2017:09
20
Vinyl chloride
ND
20.0
ug1L
03/26/20 17:09
20
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
1,2-Dichloroethane-d4(Surr)
104
75-126
03126/2017,09
20
4-Bromofluorobenzene (Surr)
92
72 -124
0312&/20 17:09
20
Dibromolluoromethene (Surr)
97
75- 120
0312612017:09
20
Toluen"S (Surr)
91
75-120
03/26/20 17,09
20
Method: 8270E - Semivolatile Organic Compounds (GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dichlorobenzene
ND
20.0
ugR
03/24/20 08:12
03/24/20 17:21
1
2,4,5-Trichlorophenol
ND
100
ug1L
03/24/20 08:12
03/24120 17:21
1
2,4,6-Trichlorophenol
ND
50.0
ug/L
03/24/20 08:12
03/24120 17:21
1
2,4-Dinitrotoluene
ND
10.0
ug1L
03/24/20 08:12
03/24/20 17:21
1
Hexachlorobenzene
ND
5.00
ug/L
03/24/20 08:12
03/24/20 17:21
1
Hexachlorobutadiene
ND
50.0
ug/L
03/24/20 08:12
03/24/20 17:21
1
Hexachloroethane
ND
50.0
ug1L
03/24/20 08:12
03/24/20 17:21
1
Cresols
ND
20.0
ug/L
03/24/20 08:12
03/24/20 17:21
1
Nitrobenzene
ND
10.0
ug/L
03/24/20 08:12
03/24/20 17:21
1
Pentachlorophenol
ND
200
ug/L
03/24/20 08:12
03/24/20 17:21
1
Pyridine
ND
200
ug/L
03/24/20 08:12
03/24/20 17:21
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
D11 Fac
2, 4, 6-Tribromophenol (Surr)
68
40 _ 145
03124120 08:12
03/24/20 17:21
1
2-Fluorobiphenyl
80
34 - 110
03124120 08:12
03/24/20 17.21
1
2-Fluorophenol (Surr)
47
27-110
03124120 06:12
03/24/20 17,21
1
Nitrobenzene d5 (Surr)
70
36 -120
03124120 08:12
03124120 17:21
1
Phenol-d5 (Surr)
29
20-100
03124120 08:12
03124120 17:21
1
Terphenyl di4 (Surr)
96
40-145
03124120 08:12
03124120 17:21
1
Method: 8081 B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chlordane (technical)
ND
10.0
ug/L
03/24/20 09:29
03/24/20 21:31
1
Endrin
ND
5.00
ug/L
03/24/20 09:29
03/24/20 21:31
1
Heptachlor
NO
4.00
ug/L
03/24/20 09:29
03/24/20 21:31
1
Heptachlor epoxide
ND
4.00
ug/L
03/24/20 09:29
03/24/20 21:31
1
gamma-BHC (Lindane)
ND
5.00
ug/L
03/24/20 09:29
03/24120 21:31
1
Methoxychlor
ND
10.0
ug/L
03/24/20 09:29
03/24/20 21;31
1
Toxaphene
ND
50.0
ug/L
03/24/20 09:29
03/24/20 21:31
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
140 X
30-130
03124120 09:P9
ON 4/20 21:31
1
Eurofins TestAmerica, Chicago
Page 7 of 29 3/30/2020

Client Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Client Sample ID: Greenville Utility
Date Collected: 03/12/20 00:00
Date Received: 03/14/20 12:10
Method: 8081 B - Organochlorine Pesticides (GC) - TCLP (Continued)
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene 1 f0 30-120
Job ID: 500-179338-1
Lab Sample ID: 500-179338-2
Matrix: Sludge
Prepared Analyzed Dil Fac
03124120 09:29 03/24/20 21:31 1
Method: 3082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
PCB-1016 ND 9
5.00
ug1L
0312512 118:08
03/26/20 09:31
1
PCB-1221 ND
5.00
ug/L
03/25/20 18:08
03/26/20 09:31
1
PCB-1232 ND
5.00
ug/L
03/25/20 18:08
03/26/20 09:31
1
PCB-1242 ND
5.00
ug/L
03/25/20 18:08
03/26120 09:31
1
PCB-1248 ND
5.00
ug1L
03125/20 18:08
03/26120 09:31
1
PCB-1254 N❑
5.00
ug1L
03/25/20 18:08
03/26/20 09:31
1
PCB-1260 ND *1
5.00
ug1L
03/25/20 18:08
03/26/20 09:31
1
Surrogate %Recovery Qualifer
Limits
Prepared
Analyzed
ail Fac
Tetrachloro-m-xylene 93
30-120
03125120 18.08
03/26/20 09:31
1
DC8 Decachlorobiphenyl 83
30 -140
03125QO 18:08
03128120 09:31
1
Method: 8151A - Herbicides (GC) - TCLP
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
j 2,4-D ND
0.100
mglL
03/23120001
0312412013:i0
1
Silvex (2,4,5-TP) N❑
0.100
mg1L
03/23/20 09:51
03/24/20 13:10
1
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Oil Fac
DCAA 67
25-130
03123120 09:51
03/24120 13:10
1
Method: 6010D - Metals (ICP) - TCLP
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Arsenic ND
D.0500
mg1L
0312212D 16:15
03/23/20 09:26
1
Barium ND
0.500
mg/L
03/22120 16:15
03/23/20 09:26
1
Cadmium ND
0.00500
mg1L
03/22/20 16:15
03/23/20 09:26
1
Chromium ND
0.0250
mg1L
03/22/20 16:15
03/23/20 09:26
1
Lead ND
0.0500
mg/L
03/22/20 16:15
03/23/20 09:26
1
Selenium ND
0.0500
mg/L
03/22/20 16:15
03/23/20 D9:26
1
Silver ND
0.0250
mg1L
03/22/20 16:15
03123/20 09:26
1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury ND
0.200
ug1L
03/23/ 00 07:50
03/23/20 12:04
1
General Chemistry
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
DO Fac
Flashpoint >176
99.0
Degrees F
03/27/20 08:27
1
Cyanide, Total ND
0.0100
mg/L
03/23/20 09:00
03/23120 13:13
1
Sulfide 37.6
5.00
mg1L
03117/2012:37
1
pH 5.56 HF
0.200
SU
03/3012010:22
1
Eurofins TestAmerica, Chicago
Page 8 of 29 3/30/2020

Definitions/Glossary
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Qualifiers
GC Semi VOA
Qualifier Qualifier Description
't LCSILCSD RPD exceeds control limits.
X Surrogate recovery exceeds control limits
Metals
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary —
Abbreviation These commonly used abbreviations may or may not be present In this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDlDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DDDIDOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Eurofins TestAmerica, Chicago
Page 9 of 29 3/30/2020

QC Association Summary
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
GC/MS VOA _ _ .__......
teach Batch: 535216
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
1311
LB 500-535216/1-A
Method Blank
TCLP
Water
1311
Analysis Batch: 535461
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
8260D
535216
j LB 500-535216/1-A
Method Blank
TCLP
Water
8260D
535216
MB 500-53546116
Method Blank
Total/NA
Water
8260D
LCS 500-53546114
Lab Control Sample
TotallNA
Water
8260D
GCIMS Semi VOA
Leach Batch: 534637
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
1311
LB 500-53463711-E
Method Blank
TCLP
Water
1311
500-179338-E-2-F MS
500-179338-E-2-F MS
TCLP
Sludge
1311
Prep Batch: 535134
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
3510C
534637
LB 500-53463711-E
Method Blank
TCLP
Water
3510C
534637
MB 500-535134/1-A
LCS 500-535134/2-A
Method Blank
Total/NA
Water
3510C
Lab Control Sample
Total/NA
Water
3510C
500-179338-E-2-F MS
500-179338-E-2-F MS
TCLP
Sludge
3510C
534637
Analysis Batch: 535155
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
6270E
535134
LB 500-53463711-E
Method Blank
TCLP
Water
8270E
535134
MB 500-53513411-A
Method Blank
Total/NA
Water
8270E
535134
LCS 500-535134/2-A
Lab Control Sample
Total/NA
Water
8270E
535134
500-179338-E-2-F MS
500-179338-E-2-F MS
TCLP
Sludge
8270E
535134
GC Semi VOA
Leach Batch: 534637
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
1311
LB 500-53463711-D
Method Blank
TCLP
Water
1311
LB 500-53463711-F
Method Blank
TCLP
Water
1311
Prep Batch: 534960
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
8151A
534637
LB 500-53463711-D
Method Blank
TCLP
Water
8151A
534637
MB 500-534960/1-A
Method Blank
Total/NA
Water
8151A
LCS 500-53496012-A
Lab Control Sample
TotallNA
Water
8151A
Analysis Batch: 535129
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
5D0-179338-2
Greenville Utility
TCLP
Sludge
8151A
534960
Eurofins TestAmerica, Chicago
Page 10 of 29 3/30/2020

QC Association Summary
Client: Bio-Nomics Services_, Inc.
Project/Site: Greenville Utility Water Plant
Job ID: 500-179338-1
... ... .__ . ... _.
GC Semi VOA (Continued)
Analysis Batch: 535129 (Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LB 500-53463711-D
Method Blank
TCLP
Water
8151A
534960
MB 500-53496011-A
Method Blank
Total/NA
Water
8151A
534960
LCS 500-53496012-A
Lab Control Sample
Total[NA
Water
8151A
534960
Prep Batch: 535163
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
3510C 534637
LB 500-534637/1-F
Method Blank
TCLP
Water
3510C 534637
MB 500-53516311-A
Method Blank
TotaUNA
Water
3510C
LCS 500-53516312-A
Lab Control Sample
Total/NA
Water
3510C �.
LCS 500-53516313-A
Lab Control Sample
Total/NA
Water
3510C
Analysis Batch: 535231
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
8081 B
535163
LB 500-53463711-F
Method Blank
TCLP
Water
8081 B
535163
MB 500-535163/1-A
Method Blank
Total/NA
Water
8081B
535163
LCS 500-535163/2-A
Lab Control Sample
Total/NA
Water
8081 B
535163
LCS 500-535163/3-A
Lab Control Sample
TotaUNA
Water
8061 B
535163
Prep Batch: 535414
Lab Sample ID
Client Sample 1D
Prep Type
Matrix
Method Prep Batch
500-179338.2
Greenville Utility
TotalINA
Sludge
3510C
MB 500-53541411-A
Method Blank
Total/NA
Water
3510C
LCS 500-535414l2 A
Lab Control Sample
Total/NA
Water
3510C
LCSD 500-535414/3-A
Lab Control Sample Dup
Total/NA
Water
3510C
Analysis Batch: 535496
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
8082A
535414
MB 500-535414/1-A
Method Blank
Total/NA
Water
8082A
535414
LCS 500-53541412-A
Lab Control Sample
Total/NA
Water
BD82A
535414
LCSD 500-535414/3-A
Lab Control Sample Dup
Total[NA
Water
8482A
535414
Metals
Leach Batch: 534637
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
1311
LB 500-534637/1-B
Method Blank
TCLP
Water
1311
LB 500-534637/1-C
Method Blank
TCLP
Water
1311
Prep Batch: 534857
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
3010A
534637
LB 500-534637/1-B
Method Blank
TCLP
Water
3010A
534637
LCS 500-53485712-A
Lab Control Sample
TotallNA
Water
3010A
Prep Batch: 534911
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
7470A
534637
Eurofins TestAmerica, Chicago
Page 11 of 29 3/30/2020

QC Association Summary
Client: Bio-Nomics Services., Inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Metals (Continued)
Prep Batch: 534911 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
LB 500-534637/1-C Method Blank
TCLP
Water
7470A 534637
MB 500-534911/12-A Method Blank
Total/NA
Water
7470A
LCS 500-534911114-A Lab Control Sample
Total/NA
Water
7470A
Analysis Batch: 534991
Lab Sample ID
500-179338-2
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Greenville Utility
TCLP
Sludge
7470A
534911
LB 500-534637/1-C
Method Blank
TCLP
Water
7470A
534911
MB 500-534911/12-A
Method Blank
Total/NA
Water
7470A
534911
LCS 500-534911/14-A
Lab Control Sample
Total/NA
Water
7470A
534911
Analysis Batch: 535002
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
TCLP
Sludge
6010D
534857
LB 500-534637/1-B
Method Blank
TCLP
Water
6010D
534857
LCS 500-534857/2-A
Lab Control Sample
Total/NA
Water
6010D
534857
General Chemistry
Analysis Batch: 534269
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
9034
MB 500-534269/1
Method Blank
Total/NA
Water
9034
LCS 500-53426912
Lab Control Sample
Total/NA
Water
9034
Prep Batch: 534916
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
9010B
MB 500-53491611-A
Method Blank
Total/NA
Water
9010E
LCS 500-53491612-A
Lab Control Sample
Total/NA
Water
9010E
500-179338-2 MS
Greenville Utility
Totaf/NA
Sludge
9010B
500-179338-2 MSD
Greenville Utility
Total/NA
Sludge
9010B
Analysis Batch: 535016
Lab Sample I❑
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
9014
534916
MB 500-534916/1-A
Method Blank
Total/NA
Water
9014
534916
LCS 500-53491612-A
Lab Control Sample
Total/NA
Water
9014
534916
500-179338-2 MS
Greenville Utility
Total/NA
Sludge
9014
534916
500-179338-2 MSD
Greenville Utility
Tota11NA
Sludge
9014
534916
Analysis Batch: 535749
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
1010A
Analysis Batch: 535938
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
500-179338-2
Greenville Utility
Total/NA
Sludge
9040C
LCS 500-53593815
Lab Control Sample
TotallNA
Water
9040C
LCSD 500-53593816
Lab Control Sample Dup
TotallNA
Water
9040C
500 179338-2 DU
Greenville Utility
Total/NA
Sludge
9040C
Euroffns TestAmerica, Chicago
0
Page 12 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Sludge Prep Type_TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCA BFB DBFM TOL
Lab Sample ID Client Sample iD (75-126) (72-124) (75420) (75-120)
500-179338-2 Greenville Utility 104 92 97 91
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Water
Pren Tine- Tntal/NA
Percent Surrogate Recovery (Acceptance Limits)
DCA
BFB
DBFM
TOL
Lab Sample ID Client Sample ID (75-126)
(72-124)
(75-120)
(75-120)
LCS 500-53546114 Lah Control Sample 101
91
96
95
MB 500-53546116 Method Blank 103
96
95
94
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Method: 82606- Volatile Organic Compounds by GC/MS
Matrix: Water
DCA
Lab Sample ID Client Sample ID (75-126)
LB 500-53521611-A Method Blank 101
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
i BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
Prep Tvpe: TCLP
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM TOL
(72-124) (75-120) (75-120)
93 94 94
Method: 8270E - Semivolatile Organic Compounds (GCIMS)
Matrix: Sludge
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
NBZ
PHL
TPHL
Lab Sample ID Client Sample ID (40-145)
(34-110)
(27-110)
(36-120)
(20-100)
(40-145)
500-179338-2 Greenville Utility 68
80
47
70
29
96
500-179338-E-2-F MS 500-179338-E-2-F MS 80
85
51
86
35
88
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d 14 (Surr)
Eurofins TestAmerica, Chicago
Page 13 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nomics Services., Inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TBP FBP 2FP
NBZ PHL TPHL
Lab Sample ID Client Sample ID
(40-145) (34-110) (27-110)
(36-120) (20-100) (40-145)
LCS 500-53513412-A Lab Control Sample
85 98 62
99 41 98
MB 500-535134/1-A Method Blank
71 84 63
75 33 105
Surrogate Legend
TBP = 2,4,6-Tnbromophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GCIMS) --
Matrix: Water Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TBP FBP 2FP NBZ PHL TPHL
Lab Sample ID Client Sample ID (40-146) (34-110) (27-110) (36-120) (20-100) (40-145)
LB 500-534637/1-E Method Blank 73 86 56 75 30 101
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Sludge
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCX1
Lab Sample ID Client Sample ID (30-130) (30-120)
500-179338-2 Greenville Utility 140 X 110 —
Surrogate Legend
DCBP = DCS Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Water
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP1
TCX1
Lab Sample ID
Client Sample ID
(30-130)
(30-120)
LCS 500-53516312-A
Lab Control Sample
125
103
LCS 500-53516313-A
Lab Control Sample
99
79
MB 500-53516311-A
Method Blank
131 X
106
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Eurofins TestAmerica, Chicago
Page 14 of 29
3/30/2020

Surrogate Summary
Client: Bio-Nomics Services., Inc. Jab ID: 500-179338-1
Project/Site: Greenville_ Utility Water Plant _
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Water Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1 TCX1
Lab Sample ID Client Sample ID (30430) (30-120)
500-179552-6-1-M MS Matrix Spike 60 70
LB 500-53463711-F Method Blank 112 92
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Matrix: Sludge _. _.. - _____......... _. Prep-.Type:Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TCX1 DCBP1 e�
Lab Sample ID Client Sample ID (30-120) (30-140)
500-179338-2 Greenville Utility 93 83
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
-- _._.. .... _ .....- -- - - -- _. .......
Method: 8082A - Polych�lori_nated Biphenyls {PCBs) by Gas Chromatography
Matrix: Water Prep Tvpe: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TCX1
DCBP1
Lab Sample ID
Client Sample ID
(30-120)
(30-140)
LCS 500-53541412-A
Lab Control Sample
82
100
LCSD 500-53541413-A
Lab Control Sample Dup
59
74
MB 500-53541411-A
Method Blank
68
95
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCBP = DCB Decachlorobiphenyl
Method: 8151A - Herbicides (GC)
Matrix: Sludge _ Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
Lab Sample ID
500-179338-2
DCPAAI
Client Sample ID (26-130)
Greenville Utility 67
Surrogate Legend
DCPAA = DCAA
_.. -- . .. ...............
—..... _.._ _.._............._..-- ---- -. -----
Method: 8151A - Herbicides (GC)
Matrix: Water Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCPAAI
Lab Sample ID Client Sample ID (25-130)
LCS 500-534960/2-A Lab Control Sample 67
MB 500-53496011-A Method Blank 70
Surrogate Legend
Eurofins TestAmerica, Chicago
Page 15 of 29 3/30/2020

Surrogate Summary
Client: Bio-Nomics Services., Inc.
ProjectlSite. Greenville Utility Water Plant
DCPAA = DCAA
Method: 8151A - Herbicides (GC)
Matrix: Water
DCPAAI
Lab Sample ID Client Sample ID (25-130)
500-179553-B-1-F W3 Matrix Spike 65
LB 500-534637/1-D Method Blank 65
Surrogate Legend
DCPAA = DCAA
Job ID: 500-179338-1
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
Eurofins TestAmerica, Chicago
Page 16 of 29
3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Job ID: 500-179338-1
Method: 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: MB 500-535461/6 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 535461
MB MB
Analyte
Result Qualifier
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
2-Butanone (MEK)
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
MS MB
Surrogate
%Recovery Qualifier
j 1,2-Dichloroethane-d4 (Surr)
103
4-Bromofluorobenzene (Surr)
96
Dibromofluoromethane (Surr)
95
Toluene-d8 (Surr)
94
Lab Sample ID: LCS 500-53546114
Matrix: Water
Analysis Batch: 535461
RL
MDL Unit
D Prepared Analyzed
oil Fac
1.00
uglL
031261201D:20
1
1.00
ug/L
0312612010:20
1
5.00
ug1L
0312612010:20
1
1.00
ug1L
03/26/2010:20
1
1.00
ug1L
03/26/2010:20
1
1.00
uglL
03126/2010:20
1
2.00
ug1L
03126/2010:20
1
1.00
uglL
03/2612010:20
1
1.00
uglL
03/26/2010:20
1
1.00
uglL
03/2612010:20
1
Limits
Prepared Analyzed
DU Fac
75-126
03/26/20 10:20
1
72-124
03/26/20 10:20
1
75- 120
03/26/2010:20
1
75-120
03126120 10:20
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
50.0
41.89
uglL
84
67-122
1,2-Dichloroethane
50.0
46.94
ug1L
94
68 -127
2-Butanone(MEK)
50.0
47.50
ug1L
95
46-144
Benzene
50.0
44,22
ug1L
88
70-120
Carbon tetrachloride
50.0
48.11
uglL
96
59-133
Chlorobenzene
50.0
44.02
uglL
88
70- 120
Chloroform
50.0
43,17
ug1L
86
70-120
Tetrachloroethene
50.0
48.77
uglL
98
70 -128
Trichloroethene
50,0
46.28
uglL
93
70 -125
Vinyl chloride
50.0
40.62
uglL
81
64 -126
LCS LCS
Surrogate
%Recovery Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
101
75-126
4-Bromofluorobenzene (Surr)
91
72 -124
Dibromotluoromethane (Surr)
96
75-120
Toluene -dB (Surr)
95
75 -120
Lab Sample ID: LB 500-535216/1-A
Matrix: Water
Analysis Batch: 535461
Client Sample ID: Method Blank
Prep Type: TCLP
LB LS
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
1,1-Dichloroethene
ND
20.0
ug1L
03126/2010:47
20
1,2-Dichloroethane
ND
20.0
uglL
03/26/20 10:47
20
2-Butanone (MEK)
ND
100
ug1L
03/26/20 10:47
20
Benzene
ND
20.0
ug1L
0312612010:47
20
Eurofins TestAmerica, Chicago
Page 17 of 29
3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: -82GOD - Volatile Organic Compounds by GC1MS (Continued)
— .... -.............----- ........
Lab Sample ID: LB 500-53521611-A Client Sample ID: Method Blank
Matrix: Water Prep Type: TCLP
Analysis Batch: 535461
LB LB
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Dil Fac
Carbon tetrachloride
ND
20.0
ug1L
03/26/20 10:47
20
Chlorobenzene
ND
20.0
uglL
03/26/2010:47
20
Chloroform
N❑
40.0
uglL
03/26/2010:47
20
Tetrachloroethene
NO
20.0
uglL
03/2612010:47
20
Trichloroethene
NO
20.0
uglL
03126/2010:47
20
Vinyl chloride
NO
20.0
uglL
03/26120 10:47
20
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Di! Fac
1,2-Dichloroethane-d4 (Surr)
101
75- 126
03/26/20 10:47
20
4-6romofluorobenzene (Surr)
93
72 -124
03/26/20 10:47
20
Dibromolluoromethane (Surr)
94
75 -120
03/2G/20 10:47
20
Toluene-d8 (Surr)
94
75-120
03126120 10:47
20
Method: 8270E - Semivolatile Organic Compounds (GCIMS)
Lab Sample ID: MB 500-535134/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535155
Prep Batch:
535134
MB MB
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Oil Fac
1,4-Dichlorobenzene
2,4,5-Trichlorophenoi
NO
NO
2.00
ug1L
03/24/20 08:12
03/24/20 16:22
1
10.0
ug1L
03/24/20 08:12
03/24/20 16:22
1
2,4,6-Trichlorophenol
NO
5.00
ug1L
03/24/20 08:12
03/24/20 16:22
1
2,4-Dinitrotoluene
ND
1.00
ug1L
03/24/20 08:12
03/24/20 16:22
1
Hexachlorobenzene
ND
0.500
ug/L
03/24/200&12
03124120 16:22
1
Hexachlorobutadiene
ND
5.00
ug1L
03/24/20 08:12
03/24120 16:22
1
Hexachloreethane
NO
5,00
uglL
03/24/20 08:12
03/24/20 16:22
1
Cresols
NO
2.00
ug1L
03/24/20 08:12
03/24/20 15:22
1
Nitrobenzene
NO
1.00
uglL
03/24/20 06:12
03124/20 16:22
1
Pentachlorophenol
NO
20.0
uglL
03/24/20 08:12
03/24120 16:22
1
Pyridine
NO
20.0
ug1L
03/24/20 08:12
03/24/20 16:22
1
MB Ala
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
71
40- 145
03/24/20 08:12
03124120 16:22
1
2-Fluorobiphenyl
84
34 - 110
03124120 08:12
03124120 16:22
1
2-Fluorophenol (Surr)
63
27-110
03124120 08:12
03124120 16:22
1
Nitrobenzene-d5 (Surr)
75
36-120
03124120 06:12
03124120 16:22
1
Phenol-0 (Surr)
33
20-100
03/24/20 08: f2
03124120 16:22
1
Terphenyl-d14 (Surr)
105
40-145
03124120 08:12
03124120 16:22
1
Lab Sample ID: LCS 500-535134/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535155
Prep Batch: 535134
Spike LCS LCS
%Rec.
Analyte
Added Result Qualifier
Unit
D %Rec
Limits
1,4-Dichlorobenzene
40.0 32.05
ug1L
A 80
23- 110
2,4,5-Trichlorophenol
40.0 37.70
ug1L
94
63-124
2,4,6-Trichlorophenol
40.0 37.20
ug1L
93
62 -121
Eurofins TestAmerica, Chicago
Page 18 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method: 8270E - Semivolatile Organic Compounds (GC/MS} (Continued)
Lab Sample ID: LCS 500-535134/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535155
Prep Batch; 535134
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2,4-Dinitrotoluene
40.0
35.45
ug1L
89
63 -129
Hexachlorobenzene
40.0
41.44
ug/L
104
61 -126
Hexachlorobutadiene
40.0
26.18
ug1L
65
20 -100
Hexachloroethane
40.0
27.07
ug/L
68
20 -100
Cresols
80.0
64.74
ug/L
81
Nitrobenzene
40.0
38.46
ug/L
96
54-121
Pentachlorophenol
80.0
74.30
ug/L
93
42-148
Pyridine
60.0
39,42
ug1L
49
15-110
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4,6-Tnbromopheno! (Surf)
85
40 -145
2-Fluorobiphenyl
98
34 -110
2-Fluorophenol (Surr)
62
27-110
Nitrobenzene-d5 (Surr)
99
36-120
Phenol-d5 (Surr)
41
20-100
Terphenyl-d14 (Surr)
98
40-145
Lab Sample ID: LB 500-534637/1-E
Client Sample ID: Method Blank
Matrix: Water
Prep Type: TCLP
Analysis Batch: 535155
Prep Batch: $35134
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D
Prepared
Analyzed Dil Fac
1,4-Dichlorobenzene
ND
20.0
ug/L
03/24/20 08:12
03/24/20 15:22 1
2,4,5-Trichlorophenol
ND
100
ug1L
03/24/20 08:12
03/24/20 15:22 1
2,4,6-Trichlorophenol
ND
50.0
ug1L
03/24/20 08:12
03/24/20 15:22 1
2,4-Dinitrotoluene
ND
10.0
ug/L
03/24/20 08:12
03/24/20 15:22 1
Hexachlorobenzene
ND
5.00
ug1L
03/24/20 08:12
03/24/20 15:22 1
Hexachlorobutadiene
ND
50.0
ug/L
03/24/20 08:12
03/24/20 15:22 1
Hexachloroethane
ND
50.0
ug1L
03/24/20 08:12
03/24120 15:22 1
Cresols
ND
20.0
ug1L
03/24/20 08:12
03/24120 15:22 1
Nitrobenzene
ND
10.0
ug/L
03/24/20 W12
03/24/20 15:22 1
Pentachlorophenol
ND
200
uglL
03/24/20 08:12
03/24/20 15:22 1
Pyridine
ND
200
ug/L
03/24/20 08:12
03/24/20 15:22 1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed B11 Fac
2,4,6-Tnbromopheno1(Surr)
73
40- 145
03124120 08:12
03124120 15.22 1
2-Fluorobiphenyl
86
34 -110
03124120 08.12
03124120 15:22 1
2-Fluorophenol (Surr)
56
27-110
03124120 08.12
03124120 15:22 1
Nitrobenzened5 (Surr)
75
36 -120
03124120 08:12
03124120 15:22 1
Phenol-d5 (Surr)
30
20- 100
03/24/20 08:12
03124120 15:22 1
Terphenyl-04 (Surr)
101
40- 145
03124120 08:12
03/24/20 15:22 1
Lab Sample ID: 500-179338-E-2-F MS
Matrix: Sludge
Analysis Batch: 535155
Sample Sample
Analyte Result Qualifier
1,4-Dichlorobenzene ND
Client Sample ID: 500-179338-E-2-F MS
Prep Type: TCLP
Prep Batch: 535134
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
400 274.5 ug/L 69 23 -110
EuroFns TestAmerica, Chicago
Page 19 of 29
3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
-- -- - . ..... _... - - - —
Method: 8270E - Semivolatile Organic Compounds (GCIMS) (Continued)
Lab Sample ID: 500-179338-E-2-F MS Client Sample ID: 500-179338-E-2-F MS
Matrix: Sludge Prep Type: TCLP
Analysis Batch: 535155 Prep Batch: 535134
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
2,4,5-Trichlorophenol
ND
400
342.9
ug1L
86
63 - 124
2,4,6-Trichlorophenol
ND
400
338.0
ug/L
85
62 -121
2,4-Dinitrotoluene
ND
400
318.3
uglL
80
63-129
Hexachlorobenzene
ND
400
356.6
ug/L
89
61-126
Hexachiorobutadiene
ND
400
238.8
ug/L
60
20 -100
Hexachloroethane
ND
400
236.2
ug/L
59
20 -100
Cresols
ND
800
572.4
ug1L
72
Nitrobenzene
ND
400
330.0
ug1L
83
54 -121
Pentachlorophenol
ND
800
639.1
ug1L
80
42 -148
Pyridine
ND
800
341.2
uglL
43
15-110
MS MS
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
80
40-145
2-Fluorobiphenyl
85
34-110
2-Ffuorophenot (Surr)
51
27- 110
Nitrobenzene-d5 (Surr)
86
36-120
Phenol-d5 (Surr)
35
20-100
Terphenyl-dN (Surr)
88
40-145
-----
Method: 8081 B - Organochlorine Pesticides (GC)
Lab Sample ID: MB 500-53516311-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 635231
Prep Batch: 535163
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Eac
Chlordane (technical)
ND
0,100
ug/L
03124/20 09:29
03/24/20 20:09 1
Endrin
ND
0.0500
ug/L
03/24/20 09:29
03/24/20 20:09 1
Heptachlor
ND
0.0400
ug/L
03/24/20 09:29
03/24/20 20:09 1
Heptachlor epoxide
ND
0.0400
ug/L
03/24/20 09:29
03/24/20 20:09 1
gamma-BHC (Lindane)
ND
0.0500
ug/L
03/24/20 09:29
03/24/20 20:09 1
Methoxychlor
ND
0.100
ug1L
03/24/20 09:29
03/24/20 20:09 1
Toxaphene
ND
0.500
ug1L
03/24/20 09:29
03/24/20 20:09 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dif Fac
DCB Decachlorobiphenyl
131 X
30-130
03/24/20 09:29
03/24/20 20.09 1
Tefrachloro-m xyfene
106
30-120
03124120 09:29
OM4120 20:08 1
Lab Sample ID: LCS 500-535163/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 635231
Prep Batch: 535163
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Endrin
0.0996
0.1150
ug/L
115
60 -132
Heptachlor
0.0999
0.1024
ug/L
102
40 -120
Heptachlor epoxide
0.100
0.1107
ug/L
111
64 -120
gamma-BHC (Lindane)
0.0999 0.09340
ug/L
93
68 -120
Methoxychlor
1.00
1.086
ug1L
109
63 -135
Eurofins TestAmerica, Chicago
Page 20 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method 8081 B Organochlorine Pesticides (GC) (Continued)
..........._..._....._..- - ---
Lab Sample ID: LCS 500-535163/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 535231 Prep Batch: 535163
LCS LCS
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
125
30 -130
Tetrachloro-m-xylene
103
30-120
Lab Sample ID: LCS 500-53516313-A
Client Sample ID:
Lab Control! Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535231
Prep Batch: 535163
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec
Limits
Toxaphene
10.0
8.363
ug1L 84
50-150
LCS LCS
Surrogate
%Recovery Qualifier
Limits
DCB Decachlorobiphenyl
99
30-130
Tetrachloro-m-xylene
79
30 -120
Lab Sample ID: LB 500-534637/1-F
Client Sample ID: Method Blank
Matrix: Water
Prep Type: TCLP
Analysis Batch: 535231
Prep Batch: 535163
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Oil Fac
Chlordane (technical)
NO
10.0
ug/L
03/24/20 09:29
03/24120 21:11 1
Endrin
NO
5.00
uglL
03/24/20 09:29
03/24/20 21:11 1
Heptachlor
NO
4.00
ug/L
03/24/20 D9:29
03/24/20 21:11 1
Heptachlor epoxide
NO
4.00
ug/L
03/24/20 09:29
03/24/20 21:11 1
gamma-BHC (Undane)
NO
5.00
ug/L
03/24/20 09:29
03/24/20 21:11 1
MethoxychlDr
NO
10.0
ug1L
03/2412D 09:29
03/24/20 21:11 1
Toxaphene
NO
50.0
ug/L
03/24/20 09:29
D3124120 21:11 1
LB LS
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobipheny!
112
30- 130
03124120 09:29
03/24/20 21.11 1
Tetrachloro-m xylene
92
30- 120
03124120 09:29
03124120 21:11 1
Method 8082A - Polychlorinated
Biphenyls
(PCBs) by Gas Chromatography
Lab Sample ID: MB 500-535414/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535496
Prep Batch: 535414
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Oil Fac
PCB-1016
NO
0.500
ug/L
03/25/20 18:08
03/26/20 08:44 1
PCB-1221
NO
0.500
ug1L
03/25/20 18:D8
03/26/20 08:44 1
PCB-1232
NO
0.500
ug1L
03/25/20 18:08
03/26/20 08:44 1
PCB-1242
NO
0.500
uglL
03/25/20 18:08
03126/20 08:44 1
PCB-1248
NO
0.500
ug/L
03/25/20 18:08
03/26/20 08:44 1
PCB-1254
NO
0.500
ug/L
03/25/20 18:08
03/26/20 08:44 1
PCB-1260
NO
0.500
ug1L
03125/20 18:08
03/26/20 08:44 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
Tetrachloro-m-xylene
68
30-120
0312512016:08
03/26/2008:44 1
Eurofins TestAmerica, Chicago
Page 21 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
...
Method: 8082A - Polychlorinated Bi hen Is PCBs b Gas ChromatographyContinued
_..- -..... Y...... --....._. p - .._{- - y _..........._..t __......_......_.............. -
Lab Sample ID: MB 500-53541411-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535496
Prep Batch: 535414
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed DH Fac
DCB Decachlorobiphenyl 95
30 -140
03125120 16:08 03/26/20 08:44 1
Lab Sample ID: LCS 500-535414/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535496
Prep Batch: 535414
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
PCB-1016
5,00
4.485 uglL 90 56-120
PCB-1260
5.00
4.585 ugiL 92 53 -137
LCS LCS
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene 82
30 -120
DC8 Decachlorobiphenyl 100
30 -140
Lab Sample ID: LCSD 500-535414/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535496
Prep Batch: 535414
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
PC13-1016
5.00
3.488 '1 ug/L 70 56 -120 25 20
PCB-1260
5.00
3.519 '1 uglL 70 53 -137 26 20
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
Tetrachloro-m-xylene 59
30-120
DCB Decachlorobiphenyl 74
30-140
Method: 8151A - Herbicides (GC)
Lab Sample ID: MB 500-534960/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535129
Prep Batch: 534960
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed ❑il Fac
2,4-D ND
0.00100
mg1L 03/23/20 09:51 03/24/20 06:58 1
Silvex (2,4,5-TP) ND
0.00100
mglL 03/23/20 09:51 03/24/20 08:58 1
MB me
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
DCAA 70
25 - 130
03/23/20 09: S i 03/24/20 08: 58 1
Lab Sample ID: LCS 500.534960/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 535129
Prep Batch: 534960
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
2,4-D
0.0101 0.007576 mglL 75 30 - 115
Silvex (2,4,5-TP)
0.00250 0.001740
mglL 70 32 -115
Eurofins TestAmerica, Chicago
Page 22 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility Water Plant
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCS 500-53496012-A
Matrix: Water
Analysis Batch: 535129
LCS LCS
Surrogate %Recovery Qualifier Limits
DCAA 67 25-130
Lab Sample ID: LB 500-53463711-D
Matrix: Water
Analysis Batch: 535129
Analyte
Silvex (2,4,5-TP)
LB LB
Surrogate %Recovery Qualifier
DCAA 65
Method: fi010D -Metals (fCP)
Lab Sample ID: LCS 500-53485712-A
Matrix: Water
Analysis Batch: 535002
LB LB
Result Qualifier RL
ND 0.100
ND 0.100
Limits
25-130
Job ID: 500-179338-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534960
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 534960
MDL Unit D Prepared Analyzed Dil Fac
mglL u 03/23/20 09:51 03/24/20 1016 1
mgiL 03/23/20 09:51 03/24/20 10:16 1
Prepared Analyzed Dil Fac
03123120 0,9:51 OT N120 10.16 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534857
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Arsenic
0.100
0.1138
mg1L
114
80-120
Barium
0.500
0.4986 J
mglL
100
80-120
Cadmium
0.0500
0.05382
mg1L
108
80-120
Chromium
0.200
0.1921
mglL
96
80-120
Lead
0.100
0.09605
mg1L
96
BO -120
Selenium
0.100
0.1053
mg1L
105
80 -120
Silver
0,0500
0.05532
mg1L
111
80 -120
Lab Sample ID: LB 500-534637/1-B
Client Sample ID: Method Blank
Matrix: Water
Prep Type: TCLP
Analysis Batch: 535002
Prep Batch: 534857
LB LB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Arsenic
ND
0.0500
mg1L
03/22/20 16:15
03/23/20 08:53 1
Barium
ND
0.500
mg1L
03/22/20 16:15
03/23/20 08:53 1
Cadmium
ND
0.00500
mg1L
03/22/20 16:15
03/23/20 08:53 1
Chromium
ND
0.0250
mg1L
03/22/20 16:15
03/23/20 08:53 1
Lead
ND
0.0500
mg1L
03/22/20 16:15
03/23/20 08:53 1
Selenium
ND
0.0500
mg1L
03/22/20 16:15
0312312D 08:53 1
Silver
ND
0,0250
mgiL
03/22/20 16:15
03/23/20 08:53 1
Method: 7470A - Mercury (CVAA)
—
--
Lab Sample ID: MB 500-534911112-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 534991
Prep Batch: 534911
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Mercury
ND
0.200
uglL
03/23/20 07:50
03/23/20 11:27 1
Eurofins TestArnerica, Chicago
Page 23 of 29
3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Method 7470A - Mercury (CVAA) (Continued)
Lab Sample ID: LCS 500-534911/14-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 534991 Prep Batch: 534911
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Mercury 2.00 1.799 ug/L 90 80-120
Lab Sample ID: LB 500-53463711-C Client Sample ID: Method Blank
Matrix: Water Prep Type: TCLP
Analysis Batch: 534991 Prep Batch: 534911
LB LB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Mercury ND 0,200 ug/L 03/231 00 07:50 031231 00 11:40 1
Method: 9014 - Cyanide
Lab Sample ID: MB 500-53491611-A
Matrix: Water
Analysis Batch: 535016
MB MB
Analyte Result Qualifier
Cyanide, Total ND
Lab Sample ID: LCS 500-534916/2-A
Matrix: Water
Analysis Batch: 535016
Analyte
Cyanide, Total
Lab Sample ID: 500-179338-2 MS
Matrix: Sludge
Analysis Batch: 535016
Sample Sample
Analyte Result Qualifier
Cyanide, Total ND
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 534916
RL MDL Unit D Prepared Analyzed Dil Fac
0.0100 mg/L 03/23/20 09:00 03/23/20 13:12 1
Spike LCS LCS
Added Result Qualifier
0.100 0.1053
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 534916
%Rec.
Unit D %Rec Limits
mglL 105 85 -115
Client Sample ID: Greenville Utility
Prep Type: Total/NA
Prep Batch: 534916
Spike MS MS %Rec.
Added Result Qualifier Unit ❑ %Rec Limits
0.0400 0.03740 mg/L _ 94 75.125
Lab Sample ID: 500-179338-2 MSD Client Sample ID: Greenville Utility
Matrix: Sludge Prep Type: Total/NA
Analysis Batch: 535016 Prep Batch: 534916
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Cyanide, Total ND 0,0400 0.03810 mg1L 95 75 -125 2 20
Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 500-53426911 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 534269
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Sulfide ND 1.00 mglL 03/17/2011:19 1
Eurofins TestAmerica, Chicago
Page 24 of 29 3/30/2020

QC Sample Results
Client: Bio-Nomics Services., Inc. Job ID: 500-179338-1
ProjectlSite: Greenville Utility Water Plant
...... ...... -...-----
Method: 9034 Sulfide Acid soluble and Insoluble (Titrimetric) [Continued)
Lab Sample ID: LCS 500-53426912 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 534269
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Sulfide 3.95 3.823 mg/L 97 80.120
Method: 9040C - pH --
Lab Sample ID: 500-179338-2 DU Client Sample ID: Greenville Utility
Matrix: Sludge Prep Type: Total/NA
Analysis Batch: 535938
Sample Sample DU DU RPD
i Analyte Result Qualifier Result Qualifier Unit D RPD Limit
pH 5.56 HF 5.550 SU 0.2
Eurofins TestAmerica, Chicago
Page 25 of 29 3/30/2020

Lab Chronicle
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville Utility
Water Plant
Client Sample
ID: Greenville Utility
Date Collected: 03112/20 00:00
Date Received:
03/14120 12:10
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
1311
TCLP
Analysis
8260D
TCLP
Leach
1311
TCLP
Prep
3510C
TCLP
Analysis
8270E
TCLP
Leach
1311
TCLP
Prep
3510C
TCLP
Analysis
8081 B
Total/NA
Prep
3510C
TotalINA
Analysis
8082A
TCLP
Leach
1311
TCLP
Prep
8151A
TCLP
Analysis
8151A
TCLP
Leach
1311
TCLP
Prep
3010A
TCLP
Analysis
6010D
TCLP
Leach
1311
TCLP
Prep
7470A
TCLP
Analysis
7470A
Total/NA
Analysis
1010A
Total/NA
Prep
9010E
Total/NA
Analysis
9014
Total/NA
Analysis
9034
Total/NA
Analysis
9040C
Job ID: 500-179338-1
Lab Sample ID: 500-179338-2
Matrix: Sludge
Dilution
Batch
Prepared
Run Factor
Number
or Analyzed
Analyst
Lab
535216
03/24/20 12:23
BEC
TAIL CHI
20
535461
03/26/20 17:09
PMF
TAL CHI
534637
03/19/20 12:22
BEC
TAL CHI
535134
03/24/20 08:12
DAK
TAL CHI
1
535155
03124M 17:21
AJD
TAL CHI
534637
03/19/20 12:22
BEC
TAL CHI
535163
03/24/20 09:29
DAK
TAIL CHI
1
535231
03/24/20 21:31
PJ1
TAL CHI
535414
03/25/20 18:08
CIVIC
TAIL CHI
1
535496
03/26/20 09:31
BJH
TAL CHI
534637
03/19/20 12:22
BEC
TAL CHI
534960
03/23/20 09:51
DAK
TAL CHI
1
535129
03/24/20 13:10
JBJ
TAL CHI
534637
03/19/20 12:22
BEC
TAL CHI
534857
03/22/20 16:15
SIDE
TAL CHI
1
535002
03/23/20 09:26
JEF
TAL CHI
534637
03/19/20 12:22
BEC
TAIL CHI
534911
03/23/20 07:50
MJG
TAIL CHI
1
534991
03/23/20 12:04
MJG
TAL CHI
1
535749
MS
TAL CHI
(Start)
03/27/20 08:27
(End)
03/27/20 09:19
534916
03/23/20 09:00
MS
TAL CHI
1
535016
03/23/20 13:13
MS
TAL CHI
1
534269
CLB
TAL CHI
(Start)
031171201237
(End)
03/17/2012:41
1
535938
JJB
TAIL CHI
(Start) 03130/2010:22
(End) 03130/2010:25
Laboratory References:
TAL CHI = Eurofins TestAmerica, Chicago, 2417 Bond Street, University Park, IL 60484, TEL [phone]
Eurofins TestAmerica, Chicago
Page 26 of 29 3/30/2020

Accreditation/Certification Summary
Client: Bio-Nomics Services., Inc. Jab ID: 500-179338-1
Project/Site: Greenville Utility Water Plant
Laboratory: Eurofins TestAmerica, Chicago
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WWISW) State 291 12-31-20
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes far which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
8270E 3510C
Sludge
2,4-Dinitrotoluene
8270E 3510C
Sludge
Cresols
8270E 3510C
Sludge
Pyridine
9040C
Sludge
pH
South Carolina
State
77001003 04-30-20
The following analytes are included in this
report, but the laboratory is not
certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
82601)
Sludge
1,1-Dichloroethene
B260D
Sludge
1,2-Dichloroethane
82600
Sludge
2-Butanone (MEK)
8260D
Sludge
Benzene
8260D
8260D
Sludge
Sludge
Carbon tetrachloride
Chlorobenzene
8260D
Sludge
Chloroform
8260D
Sludge
Tetrachloroethene
8260D
Sludge
Trichloroethene
8260D
Sludge
Vinyl chloride
8270E 3510C
Sludge
1,4-Dichlorobenzene
8270E 3510C
Sludge
2,4,5-Tdchlorophenoi
8270E 3510C
Sludge
2,4,6-Trichlorophenol
8270E 3510C
Sludge
2,4-Dinitrotoluene
8270E 3510C
Sludge
Cresols
8270E 3510C
Sludge
Hexachlorobenzene
8270E 3510C
Sludge
Hexachlorobutadiene
8270E 3510C
Sludge
Hexachloroethane
8270E 3510C
Sludge
Nitrobenzene
8270E 3510C
Sludge
Pentachlorophenol
8270E 3510C
Sludge
Pyridine
9034
Sludge
Sulfide
Eurofins TestAmerica, Chicago
Page 27 of 29 3/30/2020

Chicago � �
241417 Bond Street t
Test merica
Char of Custody Record
University Park, 1L 60466
THE LEADER IN ENVIRONMENTAL TESTING
phone [phone] fax [phone]
TestAmerica Laboratories, Inc.
Client Contact
Project Manager: Vaughn Stevenson site Contact:
D
No:
Bio-Nornie Services
Tel/Fax:
Lab Contact: Ken Hayes
Carrier: Fedex
I of I COCs
530 Woodlawn Street
Belmont. NC 28012
Calendar( C ) or Work Days (W)
744-529-0000
TAT irdifferenl from Below
E
2 weeks
SDG No.
Project Name: Greenville Utility Water Plant
State: NC
I week
'=
30
2 days
S00.179,338
S� _ �Ai
P 4# 51996
I day
a U F
COC
0
Sample Sample
Sample
g P4 vyi ?
nor
Sample Identification
Date Time
Type
Matrix Cant EV H N f H F a
Sample Specific Notes:
Greenville utility
3/12/2020 IDOO
aqueous
aqueous X X X X X X X X
*Use Alternate Matrix: Sludge
Preservation used: 1= Ice, 2= HCI; 3= H2SO4; 4=HNO3; 5=Na0H; 6= Other
Porsible Art and Jdenr[frcmlon
©
Sample Disposal (A fee may be assessed if samples are retained longer than 7 month)
=
Non-Ha=ard Flammable Skin Irriram
Poison B
!Unknown
Return To Client
Disposal By Lab © Archive
For Months
Special Instructions/QC Requirements & Comments: *Alternate
Matrix: Sludge
Relinquished by:
Company:
Dare/Time: Re i d by:q`
Company:
Dai i e:
^
jv Jo
Rel" u hed ataby:kau.r
Company:
p y
D to ime: Rec d bY
�33b 5 lL &
Company:
-,�
Da elfi
l l{Z5
Relinquished by:
Company
Damq me, Received by:
Company.
Dateffime:
Page 28 of 29
�. 3/30/2020

Login Sample Receipt Checklist
Client: Bio-Nomics Services., Inc.
Login Number, 179338
List Number: 1
Creator: Buckley, Paula M
Question
Radioactivity wasn't checked or is <1= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol, for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Muitiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Job Number: 500-179338-1
List Source: Eurofins TestAmerica, Chicago
Answer Comment
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
NIA
True
True
NIA
1.8
Eurofins TestAmerica, Chicago
Page 29 of 29 3/30/2020