NCG030329_LAB DATA_20200716

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3O 3 a 7
July 16, 2020
Honda Power Equipment Manufacturing, Inc.
Post Office Box 37
Swepsonville, North Carolina 27359
Attention: Mr. Brendan Conway
[e-mail] C
Reference: Stormwater Sampling Event—June 2020 RECFI\,ED
Honda Power Equipment JUL 2 7 2020
Swepsonville, Alamance County, North Carolina
CE S&ME Project No.4335-20-087 N ► �� �lE"
IA, ScC noN
Dear Mr. Conway:
S&ME, Inc. (S&ME) respectfully provides the attached information to detail and summarize the stormwater
sampling activities conducted on June 15, 2020 at the Honda Power Equipment Manufacturing facility located at
3721 South NC Highway 119 in Swepsonville, Alamance County, North Carolina.
The following information summarizes the activities of the stormwater sampling event:
• An intermittent rain event began at approximately 0530 (5:30 am) on Monday,June 15, 2020, and ended
at approximately 0900 (9:00 am) on Wednesday,June 17, 2020. The approximate total rainfall was 1.88
inches as measured at the Mebane, NC rain station.
• Stormwater sampling was conducted by Carl Hewett of S&ME and samples were collected at four outfalls:
HPE-01, HPE-02, HPE-03, and HPE-04. After collection, the stormwater samples were preserved on ice and
were delivered to Pace Analytical Services, Inc. in West Columbia, South Carolina for chemical testing.
• Copies of the Stormwater Monitoring Records are provided in Attachment A. The current analytical
results are summarized in a table in Attachment B. A copy of the laboratory analytical report is
presented in Attachment C.
S&ME appreciates the opportunity to provide our services on this project. Please contact us if you have any
questions or require additional information.
Sincerely,
S&ME, Inc.
edaattie t'0 IC
7
Carl Hewett Wayne Watterson, P.E.
Senior Reviewer Senior Engineer/Group Leader
S&ME,Inc.19751 Southern Pine Blvd.I Charlotte,NC 28273 I p 704.523.4726 I www.smeinc.com

ATTACHMENT A
Stormwater Monitoring Records

STORMWATER MONITORING RECORD
Sampling Summary
Site: Honda Power Equipment
3721 South NC Highway 119
Swepsonville, North Carolina
Monitoring Date: June 15, 2020
Storm Event:
Approximate Start: 0530 (5:30 am) on June 15, 2020
Approximate End: 0900 (9:00 am) on June 17, 2020
Approximate Storm Duration: 51.5 hours
Rainfall Amount: 1.88 inches
Sampling Information:
Sampled outfall HPE-01 at 1630 (4:30 pm) on June 15, 2020
Sampled outfall HPE-02 at 1500 (3:00 pm) on June 15, 2020
Sampled outfall HPE-03 at 1730 (5:30 pm) on June 15, 2020
Sampled outfall HPE-04 at 1600 (4:00 pm) on June 15, 2020
Analytical Testing:
Volatile organic compounds by EPA Method 624.4
Semi-volatile organic compounds by EPA Method 625
PCBs/Pesticides by EPA Method 608
Copper, Lead, Zinc by EPA Method 200.8
Total oil and grease by EPA Method 1664B
Total suspended solids (TSS) by SM 2543D-20
pH by SM 4500 H-B
Sampled By;
Carl Hewett of S&ME
Notes:
• Storm duration obtained from timeanddate.com weather overview for Mebane, North Carolina.
• Total rainfall obtained from the Community Collaborative Rain, Snow& Hail Network (CoCoRaHS)

STORMWATER MONITORING RECORD
Qualitative Observations
Site: Honda Power Equipment
3721 South NC Highway 119
Swepsonville, North Carolina
Monitoring Date: June 15, 2020
Outfall Location: HPE-01
Sample structure: Concrete basin
Discharge
Ratings Comments
Characteristic
Color 1
Odor none
Clarity 1
Floating Solids 1
Suspended Solids 1
Foam none
Oil Sheen none
Other obvious indicators of
none
stormwater pollution
Characteristic rating scale: 1 to 5 (1 = least or lowest; 5= most or heaviest)
Completed by: Cart H. Hkwelf Date: 6/1.5/2020

STORMWATER MONITORING RECORD
Qualitative Observations
Site: Honda Power Equipment
3721 South NC Highway 119
Swepsonville, North Carolina
Monitoring Date: June 15, 2020
Outfall Location: HPE-02
Sample structure: Stream
Discharge
Ratings Comments
Characteristic
Color 1
Odor none
Clarity 2
Floating Solids 2
Suspended Solids 1
Foam none
Oil Sheen none
Other obvious indicators of
none
stormwater pollution
Characteristic rating scale: 1 to 5 (1 = least or lowest; 5= most or heaviest)
Completed by: Girt H. He-weW- Date: 6/15/2020

STORMWATER MONITORING RECORD
Qualitative Observations
Site: Honda Power Equipment
3721 South NC Highway 119
Swepsonville, North Carolina
Monitoring Date: June 15, 2020
Outfall Location: HPE-03
Sample structure: Stream
Discharge
Ratings Comments
Characteristic
Color 1
Odor none
Clarity 2
Floating Solids 2
Suspended Solids 1
Foam none
Oil Sheen none
Other obvious indicators of
none
stormwater pollution
Characteristic rating scale: none, slight, minor, medium, heavy
Completed by: Cart H. Newell Date: 6/i /2020

STORMWATER MONITORING RECORD
Qualitative Observations
Site: Honda Power Equipment
3721 South NC Highway 119
Swepsonville, North Carolina
Monitoring Date: June 15, 2020
Outfall Location: HPE-04
Sample structure: Stream
Discharge
Ratings Comments
Characteristic
Color 2
Odor none
Clarity 2
Floating Solids 2
Suspended Solids 1
Foam none
Oil Sheen none
Other obvious indicators of
none
stormwater pollution
Characteristic rating scale: 1 to 5 (1 = least or lowest; 5= most or heaviest)
Completed by: Cart H. He a- Date: 6/15/2020

ATTACHMENT B
Table of Analytical Results

STORMWATER ANALYTICAL RESULTS TABLE
Honda Power Equipment
3721 South NC Highway 119
Swepsonville, North Carolina
Benchmark
HPE-01 HPE-02 HPE-03 HPE-04
Values
pH—lab measured 8.0 6.5 6.1 6.9 6 - 9
Total suspended solids
14 22 2.5 19 100
(TSS)
EPA Method 200.8(ug/L)
Copper < 5 < 5 < 5 < 5 10
Lead < 1 < 1 < 1 < 1 75
Zinc < 10 < 10 25 < 10 126
EPA Method 608(ug/L)
Target PCBs BDL BDL BDL BDL 1000
EPA Method 608 (ug/L)
Target Pesticides BDL BDL BDL BDL 1000
EPA Method 624.2(ug/L)
Trichloroethene BDL BDL BDL 2.2 1000
Other Target VOCs BDL BDL BDL BDL 1000
EPA Method 625(ug/L)
Target SVOCs BDL BDL BDL BDL 1000
EPA Method 1664 (ug/L)
Total Oil &Grease < 5 < 5 < 5.3 < 5 15
Notes:
• TSS and total oil and grease presented in milligrams per liter (mg/L).
• Other analytical data presented in micrograms per liter (ug/L).
• BDL = below laboratory limit of quantitation (the laboratory minimum detection
limits are below the applicable benchmarks)
• Stormwater samples collected on June 15, 2020 by S&ME personnel.

ATTACHMENT C
Laboratory Analytical Report

0
AnalYtical
Report of Analysis
S&ME, Inc.
9751 Southern Pine Blvd
Charlotte, NC 28273
Attention: Carl Hewett
Project Name: Honda Power Equipment
Project Number: 4335-20-087
Lot Number:VF16069
Date Completed:06/29/2020
Rigiej(1/44.----
06/30/2020 12:53 PM
Approved and released by:
Project Manager: Kelly M. Nance
Tay
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0 A WNWkvu N/w.
.„ ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 51

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
S&ME, Inc.
Lot Number: VF16069
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance
Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to
the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the samples in this report were performed after the method
recommended 15 minute holding time.
Pace Analytical Services,LLC(formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 51

PACE ANALYTICAL SERVICES, LLC
Sample Summary
S&ME, Inc.
Lot Number: VF16069
Sample Number Sample ID Matrix Date Sampled Date Received
001 HPE-1 Aqueous 06/15/20201630 06/16/2020
002 HPE-2 Aqueous 06/15/20201500 06/16/2020
003 HPE-3 Aqueous 06/15/20201730 06/16/2020
004 HPE-4 Aqueous 06/15/20201600 06/16/2020
(4 samples)
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 51

PACE ANALYTICAL SERVICES, LLC
Detection Summary
S&ME, Inc.
Lot Number: VF16069
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 HPE-1 Aqueous TSS SM 2540D- 14 mg/L 5
002 HPE-2 Aqueous TSS SM 2540D- 22 mg/L 11
003 HPE-3 Aqueous TSS SM 2540D- 2.5 mg/L 17
003 HPE-3 Aqueous Zinc 200.8 25 ug/L 22
004 HPE-4 Aqueous TSS SM 2540D- 19 mg/L 23
004 HPE-4 Aqueous Trichloroethene 624.1 2.2 ug/L 24
(6 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 51

....,I yt4uhI ......W._.
Client:S&ME,Inc. Laboratory ID:VF16069-001
Description:HPE-1 Matrix:Aqueous
Date Sampled:06/15/2020 1630
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (pH)SM 4500-H B-2011 1 06/17/2020 1749 SRB 57300
2 (TSS)SM 2540D-2011 1 06/21/2020 1639 MOM 57631
1 (SGT-HEM(n) 1664B 1 06/28/2020 0000 GLT 58335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
pH @ 18.4°C SM 4500-H B-20 8.0 su 1
TSS SM 2540D-2011 14 14 mg/L 2
SGT-HEM(non-polar material) 1664B ND 5.0 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 51

•V Ica anIV V■WfAi■UV VS ■..VS/M11Isa N' VV/�V.V
Client:S&ME,Inc. Laboratory ID:VF16069-001
Description:HPE-1 Matrix:Aqueous
Date Sampled:06/15/2020 1630
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 06/17/2020 0219 JTH 57177
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acrolein 107-02-8 624.1 ND 5.0 ug/L 1
Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1
Benzene 71-43-2 624.1 ND 1.0 ug/L 1
Bromodichloromethane 75-27-4 624.1 ND 1.0 ug/L 1
Bromoform 75-25-2 624.1 ND 1.0 ug/L 1
Bromomethane(Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1
Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L 1
Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L 1
Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1
2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1
Chloroform 67-66-3 624.1 ND 1.0 ug/L 1
Chloromethane(Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1
Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1
1,2-Dichlorobenzene 95-50-1 624.1 ND 1.0 ug/L 1
1,3-Dichlorobenzene 541-73-1 624.1 ND 1.0 ug/L 1
1,4-Dichlorobenzene 106-46-7 624.1 ND 1.0 ug/L 1
Dichlorodifluoromethane 75-71-8 624.1 ND 2.0 ug/L 1
1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1
1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1
1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1
cis-1,2-Dichloroethene 156-59-2 624.1 ND 1.0 ug/L 1
trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1
1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1
cis-1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1
trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1
Ethylbenzene 100-41-4 624.1 ND 1.0 ug/L 1
Methylene chloride 75-09-2 624.1 ND 1.0 ug/L 1
1,1,2,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1
Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1
Toluene 108-88-3 624.1 ND 1.0 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 624.1 ND 1.0 ug/L 1
1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1
1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1
Trichloroethene 79-01-6 624.1 ND 1.0 ug/L 1
Trichlorofluoromethane 75-69-4 624.1 ND 1.0 ug/L 1
Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 104 70-130
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 51

VV■fUIV Ut4L\JV vIywI•U VV.■Or.V M••MJ SO ••IVI.11.,1/
Client:S&ME, Inc. Laboratory ID:VF16069-001
Description:HPE-1 Matrix:Aqueous
Date Sampled:06/15/2020 1630
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/24/2020 2123 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 625.1 ND 1.6 ug/L 1
Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L 1
Anthracene 120-12-7 625.1 ND 1.6 ug/L 1
Benzidine 92-87-5 625.1 ND 8.0 ug/L 1
Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L 1
Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L 1
Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L 1
Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L 1
Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 1
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L 1
Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L 1
bis(2-Chloro-1-methylethyl)ether 108-60-1 625.1 ND 1.6 ug/L 1
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L 1
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L 1
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 1
2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 1
2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 1
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L 1
Chrysene 218-01-9 625.1 ND 1.6 ug/L 1
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 1
2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L 1
Diethylphthalate 84-66-2 625.1 ND 1.6 ug/L 1
Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1
2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L 1
Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug/L 1
2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1
2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1
2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1
Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1
1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 ug/L 1
Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1
Fluorene 86-73-7 625.1 ND 1.6 ug/L 1
Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L 1
Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1
Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1
Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L 1
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1
Isophorone 78-59-1 625.1 ND 1.6 ug/L 1
Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1
Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1
2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 51

VV•�h■•V Uf4LIIY VI t...“0 VV11.1r./VM110MJ N' VV/IVP
Client:S&ME,Inc. Laboratory ID:VF16069-001
Description:HPE-1 Matrix:Aqueous
Date Sampled:06/15/2020 1630
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/24/2020 2123 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 1
N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 1
N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1
N-Nitrosodiphenylamine(Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1
Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1
Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1
Phenol 108-95-2 625.1 ND 1.6 ug/L 1
Pyrene 129-00-0 625.1 ND 1.6 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1
2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 98 37-129
2-Fluorophenol 46 24-127
Nitrobenzene-d5 84 38-127
Phenol-d5 55 28-128
Terp henyl-d 14 104 10-148
2,4,6-Tribromophenol 94 41-144
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 8 of 51

VX WfA11 IVVI•■VII IX IV, X SS% SU IMVV Ifa11 UM ■ VrIV
Client:S&ME,Inc. Laboratory ID:VF16069-001
Description:HPE-1 Matrix:Aqueous
Date Sampled:06/15/2020 1630
Date Received:06/16/2020
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 1 06/19/2020 2239 DAL1 06/17/2020 1358 57236
2 608.3 3665A 608.3 1 06/19/2020 2048 DAL1 06/17/2020 1358 57236
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aldrin 309-00-2 608.3 ND 0.040 ug/L 1
Aroclor 1016 12674-11-2 608.3 ND 0.40 ug/L 2
Aroclor 1221 11104-28-2 608.3 ND 0.40 ug/L 2
Aroclor 1232 11141-16-5 608.3 ND 0.40 ug/L 2
Aroclor 1242 53469-21-9 608.3 ND 0.40 ug/L 2
Aroclor 1248 12672-29-6 608.3 ND 0.40 ug/L 2
Aroclor 1254 11097-69-1 608.3 ND 0.40 ug/L 2
Aroclor 1260 11096-82-5 608.3 ND 0.40 ug/L 2
gamma-BHC(Lindane) 58-89-9 608.3 ND 0.040 ug/L 1
alpha-BHC 319-84-6 608.3 ND 0.040 ug/L 1
beta-BHC 319-85-7 608.3 ND 0.040 ug/L 1
delta-BHC 319-86-8 608.3 ND 0.040 ug/L 1
Chlordane 57-74-9 608.3 ND 0.40 ug/L 1
4,4'-DDD 72-54-8 608.3 ND 0.040 ug/L 1
4,4'-DDE 72-55-9 608.3 ND 0.040 ug/L 1
4,4'-DDT 50-29-3 608.3 ND 0.040 ug/L 1
Dieldrin 60-57-1 608.3 ND 0.040 ug/L 1
Endosulfan I 959-98-8 608.3 ND 0.040 ug/L 1
Endosulfan II 33213-65-9 608.3 ND 0.040 ug/L 1
Endosulfan sulfate 1031-07-8 608.3 ND 0.040 ug/L 1
Endrin 72-20-8 608.3 ND 0.040 ug/L 1
Endrin aldehyde 7421-93-4 608.3 ND 0.040 ug/L 1
Heptachlor 76-44-8 608.3 ND 0.040 ug/L 1
Heptachlor epoxide 1024-57-3 608.3 ND 0.040 ug/L 1
Toxaphene 8001-35-2 608.3 ND 0.40 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q %Recovery Limits Q %Recovery Limits
Decachlorobiphenyl 49 20-131 44 20-131
Tetrachloro-m-xylene 66 30-132 92 30-132
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 51

Client:SBME,Inc. Laboratory ID:VF16069-001
Description:HPE-1 Matrix:Aqueous
Date Sampled:06/15/2020 1630
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 06/28/2020 2304 BPK 06/17/2020 1643 57262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Copper 7440-50-8 200.8 ND 5.0 ug/L 1
Lead 7439-92-1 200.8 ND 1.0 ug/L 1
Zinc 7440-66-6 200.8 ND 10 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 10 of 51

...v■yw...v ■.v..-...vLw.v
Client:S&ME,Inc. Laboratory ID:VF16069-002
Description:HPE-2 Matrix:Aqueous
Date Sampled:06/15/2020 1500
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (pH)SM 4500-H B-2011 1 06/17/2020 1755 SRB 57300
1 (TSS)SM 2540D-2011 1 06/18/2020 1837 MOM 57413
1 (SGT-HEM (n) 1664B 1 06/28/2020 0000 GLT 58335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
pH @ 17.8°C SM 4500-H B-20 6.5 su 1
TSS SM 2540D-2011 22 3.3 mg/L 1
SGT-HEM(non-polar material) 1664B ND 5.0 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 11 of 51

V V INtlIV V I W NIIIV V VI I.r%INI■NV N' VVI IN.,I,
Client:S&ME,Inc. Laboratory ID:VF16069-002
Description:HPE-2 Matrix:Aqueous
Date Sampled:06/15/2020 1500
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 06/17/2020 0243 JTH 57177
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acrolein 107-02-8 624.1 ND 5.0 ug/L 1
Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1
Benzene 71-43-2 624.1 ND 1.0 ug/L 1
Bromodichloromethane 75-27-4 624.1 ND 1.0 ug/L 1
Bromoform 75-25-2 624.1 ND 1.0 ug/L 1
Bromomethane(Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1
Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L 1
Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L 1
Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1
2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1
Chloroform 67-66-3 624.1 ND 1.0 ug/L ' 1
Chloromethane(Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1
Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1
1,2-Dichlorobenzene 95-50-1 624.1 ND 1.0 ug/L 1
1,3-Dichlorobenzene 541-73-1 624.1 ND 1.0 ug/L 1
1,4-Dichlorobenzene 106-46-7 624.1 ND 1.0 ug/L 1
Dichlorodifluoromethane 75-71-8 624.1 ND 2.0 ug/L 1
1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1
1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1
1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1
cis-1,2-Dichloroethene 156-59-2 624.1 ND 1.0 ug/L 1
trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1
1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1
cis-1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1
trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1
Ethylbenzene 100-41-4 624.1 ND 1.0 ug/L 1
Methylene chloride 75-09-2 624.1 ND 1.0 ug/L 1
1,1,2,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1
Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1
Toluene 108-88-3 624.1 ND 1.0 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 624.1 ND 1.0 ug/L 1
1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1
1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1
Trichloroethene 79-01-6 624.1 ND 1.0 ug/L 1
Trichlorofluoromethane 75-69-4 624.1 ND 1.0 ug/L 1
Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 103 70-130
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 12 of 51

VV II■I♦VIca LIIY V.ucw.IIV VVIII'dVMIIMJ M' VVI I■IV
Client:S&ME,Inc. Laboratory ID:VF16069-002
Description:HPE-2 Matrix:Aqueous
Date Sampled:06/15/2020 1500
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/24/2020 2148 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 625.1 ND 1.6 ug/L 1
Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L 1
Anthracene 120-12-7 625.1 ND 1.6 ug/L 1
Benzidine 92-87-5 625.1 ND 8.0 ug/L 1
Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L 1
Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L 1
Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L 1
Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L 1
Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 1
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L 1
Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L 1
bis(2-Chloro-1-methylethyl)ether 108-60-1 625.1 ND 1.6 ug/L 1
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L 1
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L 1
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 1
2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 1
2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 1
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L 1
Chrysene 218-01-9 625.1 ND 1.6 ug/L 1
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 1
2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L 1
Diethylphthalate 84-66-2 625.1 ND 1.6 ug/L 1
Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1
2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L 1
Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug/L 1
2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1
2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1
2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1
Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1
1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 ug/L 1
Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1
Fluorene 86-73-7 625.1 ND 1.6 ug/L 1
Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L 1
Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1
Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1
Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L 1
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1
Isophorone 78-59-1 625.1 ND 1.6 ug/L 1
Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1
Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1
2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 13 of 51

V VUhPI•V I{nt.I\. VU t4IhI •l t t•I IMV M' VV/UWIV
Client:S&ME,Inc. Laboratory ID:VF16069-002
Description:HPE-2 Matrix:Aqueous
Date Sampled:06/15/2020 1500
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/24/2020 2148 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 1
N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 1
N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1
N-Nitrosodiphenylamine(Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1
Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1
Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1
Phenol 108-95-2 625.1 ND 1.6 ug/L 1
Pyrene 129-00-0 625.1 ND 1.6 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1
2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
2-Fluorobiphenyl 93 37-129
2-Fluorophenol 51 24-127
Nitrobenzene-d5 82 38-127
Phenol-d5 55 28-128
Terphenyl-d14 118 10-148
2,4,6-Tribromophenol 95 41-144
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 14 of 51

V.V SAN■VV1■IVII.II IV, U YV L•V•MVV f4.It ■ VVJ
Client:S&ME,Inc. Laboratory ID:VF16069-002
Description:HPE-2 Matrix:Aqueous
Date Sampled:06/15/2020 1500
Date Received:06/16/2020
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 1 06/19/2020 2254 DAL1 06/17/2020 1358 57236
2 608.3 3665A 608.3 1 06/19/2020 2101 DAL1 06/17/2020 1358 57236
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aldrin 309-00-2 608.3 ND 0.040 ug/L 1
Aroclor 1016 12674-11-2 608.3 ND 0.40 ug/L 2
Aroclor 1221 11104-28-2 608.3 ND 0.40 ug/L 2
Aroclor 1232 11141-16-5 608.3 ND 0.40 ug/L 2
Aroclor 1242 53469-21-9 608.3 ND 0.40 ug/L 2
Aroclor 1248 12672-29-6 608.3 ND 0.40 ug/L 2
Aroclor 1254 11097-69-1 608.3 ND 0.40 ug/L 2
Aroclor 1260 11096-82-5 608.3 ND 0.40 ug/L 2
gamma-BHC(Lindane) 58-89-9 608.3 ND 0.040 ug/L 1
alpha-BHC 319-84-6 608.3 ND 0.040 ug/L 1
beta-BHC 319-85-7 608.3 ND 0.040 ug/L 1
delta-BHC 319-86-8 608.3 ND 0.040 ug/L 1
Chlordane 57-74-9 608.3 ND 0.40 ug/L 1
4,4'-DDD 72-54-8 608.3 ND 0.040 ug/L 1
4,4'-DDE 72-55-9 608.3 ND 0.040 ug/L 1
4,4'-DDT 50-29-3 608.3 ND 0.040 ug/L 1
Dieldrin 60-57-1 608.3 ND 0.040 ug/L 1
Endosulfan I 959-98-8 608.3 ND 0.040 ug/L 1
Endosulfan II 33213-65-9 608.3 ND 0.040 ug/L 1
Endosulfan sulfate 1031-07-8 608.3 ND 0.040 ug/L 1
Endrin 72-20-8 608.3 ND 0.040 ug/L 1
Endrin aldehyde 7421-93-4 608.3 ND 0.040 ug/L 1
Heptachlor 76-44-8 608.3 ND 0.040 ug/L 1
Heptachlor epoxide 1024-57-3 608.3 ND 0.040 ug/L 1
Toxaphene 8001-35-2 608.3 ND 0.40 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q %Recovery Limits Q %Recovery Limits
Decachlorobiphenyl 70 20-131 66 20-131
Tetrachloro-m-xylene 66 30-132 96 30-132
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 15 of 51

Client:S&ME,Inc. Laboratory ID:VF16069-002
Description:HPE-2 Matrix:Aqueous
Date Sampled:06/15/2020 1500
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 06/28/2020 2311 BPK 06/17/2020 1643 57262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Copper 7440-50-8 200.8 ND 5.0 ug/L 1
Lead 7439-92-1 200.8 ND 1.0 ug/L 1
Zinc 7440-66-6 200.8 ND 10 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 16 of 51

■..v.aWw...v ..v..-...a...uw
Client:S&ME, Inc. Laboratory ID:VF16069-003
Description:HPE-3 Matrix:Aqueous
Date Sampled:06/15/2020 1730
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (pH)SM 4500-H B-2011 1 06/17/2020 1757 SRB 57300
1 (TSS)SM 2540D-2011 1 06/18/2020 1837 MOM 57413
1 (SGT-HEM (n) 1664B 1 06/28/2020 0000 GLT 58335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
pH @ 17.5°C SM 4500-H B-20 6.1 su 1
TSS SM 2540D-2011 2.5 1.7 mg/L 1
SGT-HEM(non-polar material) 1664B ND 5.3 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 17 of 51

V I LIIY V■Will INS, IPI1JVS IIt4 M' ',VI■VUV
Client:S&ME,Inc. Laboratory ID:VF16069-003
Description:HPE-3 Matrix:Aqueous
Date Sampled:06/15/2020 1730
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 06/17/2020 0307 JTH 57177
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acrolein 107-02-8 624.1 ND 5.0 ug/L 1
Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1
Benzene 71-43-2 624.1 ND 1.0 ug/L 1
Bromodichloromethane 75-27-4 624.1 ND 1.0 ug/L 1
Bromoform 75-25-2 624.1 ND 1.0 ug/L 1
Bromomethane(Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1
Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L 1
Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L 1
Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1
2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1
Chloroform 67-66-3 624.1 ND 1.0 ug/L 1
Chloromethane(Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1
Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1
1,2-Dichlorobenzene 95-50-1 624.1 ND 1.0 ug/L 1
1,3-Dichlorobenzene 541-73-1 624.1 ND 1.0 ug/L 1
1,4-Dichlorobenzene 106-46-7 624.1 ND 1.0 ug/L 1
Dichlorodifluoromethane 75-71-8 624.1 ND 2.0 ug/L 1
1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1
1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1
1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1
cis-1,2-Dichloroethene 156-59-2 624.1 ND 1.0 uglL 1
trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1
1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1
cis-1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1
trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1
Ethylbenzene 100-41-4 624.1 ND 1.0 ug/L 1
Methylene chloride 75-09-2 624.1 ND 1.0 ug/L 1
1,1,2,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1
Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1
Toluene 108-88-3 624.1 ND 1.0 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 624.1 ND 1.0 ug/L 1
1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1
1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1
Trichloroethene 79-01-6 624.1 ND 1.0 ug/L 1
Trichlorofluoromethane 75-69-4 624.1 ND 1.0 ug/L 1
Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 103 70-130
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 18 of 51

V LilSI■•V 11NLI11V VI W.L41 IIV VV.10r./VM••MV M' VWI P•IV
Client:S&ME,Inc. Laboratory ID:VF16069-003
Description:HPE-3 Matrix:Aqueous
Date Sampled:06/15/2020 1730
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/24/2020 2213 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 625.1 ND 1.6 ug/L 1
Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L 1
Anthracene 120-12-7 625.1 ND 1.6 ug/L 1
Benzidine 92-87-5 625.1 ND 8.0 ug/L 1
Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L 1
Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L 1
Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L 1
Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L 1
Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 1
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L 1
Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L 1
bis(2-Chloro-1-methylethyl)ether 108-60-1 625.1 ND 1.6 ug/L 1
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L 1
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L 1
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 1
2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 1
2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 1
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L 1
Chrysene 218-01-9 625.1 ND 1.6 ug/L 1
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 1
2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L 1
Diethylphthalate 84-66-2 625.1 ND 1.6 ug/L 1
Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1
2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L 1
Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug/L 1
2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1
2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1
2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1
Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1
1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 ug/L 1
Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1
Fluorene 86-73-7 625.1 ND 1.6 ug/L 1
Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L 1
Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1
Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1
Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L 1
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1
Isophorone 78-59-1 625.1 ND 1.6 ug/L 1
Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1
Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1
2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 19 of 51

VV I II,I1 V■N LI■ . VI UNI IIV V V I I It./V N I INV N' V V I I•IV
Client:S&ME, Inc. Laboratory ID:VF16069-003
Description:HPE-3 Matrix:Aqueous
Date Sampled:06/15/2020 1730
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/24/2020 2213 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 1
N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 1
N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1
N-Nitrosodiphenylamine(Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1
Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1
Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1
Phenol 108-95-2 625.1 ND 1.6 ug/L 1
Pyrene 129-00-0 625.1 ND 1.6 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1
2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1
Run 1 Acceptance
Surrogate Q Y.Recovery Limits
2-Fluorobiphenyl 93 37-129
2-Fluorophenol 50 24-127
Nitrobenzene-d5 81 38-127
Phenol-d5 60 28-128
Terphenyl-d14 110 10-148
2,4,6-Tribromophenol 89 41-144
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 20 of 51

VI WLI..VV■IIVl■UIV U VVLU sr U 4 % {.11 lM I VYJ
Client:SBME,Inc. Laboratory ID:VF16069-003
Description:HPE-3 Matrix:Aqueous
Date Sampled:06/15/2020 1730
Date Received:06/16/2020
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 1 06/19/2020 2310 DAL1 06/17/2020 1358 57236
2 608.3 3665A 608.3 1 06/19/2020 2114 DAL1 06/17/2020 1358 57236
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aldrin 309-00-2 608.3 ND 0.040 ug/L 1
Aroclor 1016 12674-11-2 608.3 ND 0.40 ug/L 2
Aroclor 1221 11104-28-2 608.3 ND 0.40 ug/L 2
Aroclor 1232 11141-16-5 608.3 ND 0.40 ug/L 2
Aroclor 1242 53469-21-9 608.3 ND 0.40 ug/L 2
Aroclor 1248 12672-29-6 608.3 ND 0.40 ug/L 2
Aroclor 1254 11097-69-1 608.3 ND 0.40 ug/L 2
Aroclor 1260 11096-82-5 608.3 ND 0.40 ug/L 2
gamma-BHC(Lindane) 58-89-9 608.3 ND 0.040 ug/L 1
alpha-BHC 319-84-6 608.3 ND 0.040 ug/L 1
beta-BHC 319-85-7 608.3 ND 0.040 ug/L 1
delta-BHC 319-86-8 608.3 ND 0.040 ug/L 1
Chlordane 57-74-9 608.3 ND 0.40 ug/L 1
4,4'-DDD 72-54-8 608.3 ND 0.040 ug/L 1
4,4'-DDE 72-55-9 608.3 ND 0.040 ug/L 1
4,4'-DDT 50-29-3 608.3 ND 0.040 ug/L 1
Dieldrin 60-57-1 608.3 ND 0.040 ug/L 1
Endosulfan I 959-98-8 608.3 ND 0.040 ug/L 1
Endosulfan II 33213-65-9 608.3 ND 0.040 ug/L 1
Endosulfan sulfate 1031-07-8 608.3 ND 0.040 ug/L 1
Endrin 72-20-8 608.3 ND 0.040 ug/L 1
Endrin aldehyde 7421-93-4 608.3 ND 0.040 ug/L 1
Heptachlor 76-44-8 608.3 ND 0.040 ug/L 1
Heptachlor epoxide 1024-57-3 608.3 ND 0.040 ug/L 1
Toxaphene 8001-35-2 608.3 ND 0.40 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q %Recovery Limits Q %Recovery Limits
Decachlorobiphenyl 58 20-131 55 20-131
Tetrachloro-m-xylene 66 30-132 96 30-132
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
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Page 21 of 51

Client:S&ME,Inc. Laboratory ID:VF16069-003
Description:HPE-3 Matrix:Aqueous
Date Sampled:06/15/2020 1730
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 06/28/2020 2319 BPK 06/17/2020 1643 57262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Copper 7440-50-8 200.8 ND 5.0 ug/L 1
Lead 7439-92-1 200.8 ND 1.0 ug/L 1
Zinc 7440-66-6 200.8 25 10 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 22 of 51

Client:S&ME, Inc. Laboratory ID:VF16069-004
Description:HPE-4 Matrix:Aqueous
Date Sampled:06/15/2020 1600
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (pH)SM 4500-H B-2011 1 06/17/2020 1759 SRB 57300
1 (TSS)SM 2540D-2011 1 06/18/2020 1837 MOM 57413
1 (SGT-HEM(n) 1664B 1 06/28/2020 0000 GLT 58335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
pH @ 18°C SM 4500-H B-20 6.9 su 1
TSS SM 2540D-2011 19 2.6 mg/L 1
SGT-HEM(non-polar material) 1664B ND 5.0 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 23 of 51

•VIi4HUV V I WU IIIV VV 1uhIJ V tCIUMV w' VV I II•IV
Client:S&ME,Inc. Laboratory ID:VF16069-004
Description:HPE-4 Matrix:Aqueous
Date Sampled:06/15/2020 1600
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 06/17/2020 0332 JTH 57177
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acrolein 107-02-8 624.1 ND 5.0 ug/L 1
Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1
Benzene 71-43-2 624.1 ND 1.0 ug/L 1
Bromodichloromethane 75-27-4 624.1 ND 1.0 ug/L 1
Bromoform 75-25-2 624.1 ND 1.0 ug/L 1
Bromomethane(Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1
Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L 1
Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L 1
Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1
2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1
Chloroform 67-66-3 624.1 ND 1.0 ug/L 1
Chloromethane(Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1
Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1
1,2-Dichlorobenzene 95-50-1 624.1 ND 1.0 ug/L 1
1,3-Dichlorobenzene 541-73-1 624.1 ND 1.0 ug/L 1
1,4-Dichlorobenzene 106-46-7 624.1 ND 1.0 ug/L 1
Dichlorodifluoromethane 75-71-8 624.1 ND 2.0 ug/L 1
1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1
1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1
1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1
cis-1,2-Dichloroethene 156-59-2 624.1 ND 1.0 ug/L 1
trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1
1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1
cis-1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1
trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1
Ethylbenzene 100-41-4 624.1 ND 1.0 ug/L 1
Methylene chloride 75-09-2 624.1 ND • 1.0 ug/L 1
1,1,2,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1
Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1
Toluene 108-88-3 624.1 ND 1.0 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 624.1 ND 1.0 ug/L 1
1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1
1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1
Trichloroethene 79-01-6 624.1 2.2 1.0 ug/L 1
Trichlorofluoromethane 75-69-4 624.1 ND 1.0 ug/L 1
Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 92 70-130
Toluene-d8 103 70-130
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 24 of 51

Client:S&ME, Inc. Laboratory ID:VF16069-004
Description:HPE-4 Matrix:Aqueous
Date Sampled:06/15/2020 1600
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/25/2020 1424 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 625.1 ND 1.6 ug/L 1
Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L 1
Anthracene 120-12-7 625.1 ND 1.6 ug/L 1
Benzidine 92-87-5 625.1 ND 8.0 ug/L 1
Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L 1
Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L 1
Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L 1
Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L 1
Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 1
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L 1
Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L 1
bis(2-Chloro-1-methylethyl)ether 108-60-1 625.1 ND 1.6 ug/L 1
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L 1
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L 1
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 1
2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 1
2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 1
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L 1
Chrysene 218-01-9 625.1 ND 1.6 ug/L 1
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 1
2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L 1
Diethylphthalate 84-66-2 625.1 ND 1.6 ug/L 1
Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1
2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L 1
Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug/L 1
2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1
2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1
2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1
Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1
1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 ug/L 1
Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1
Fluorene 86-73-7 625.1 ND 1.6 ug/L 1
Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L 1
Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1
Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1
Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L 1
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1
Isophorone 78-59-1 625.1 ND 1.6 ug/L 1
Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1
Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1
2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 25 of 51

VVI III V IC4LII4.• VU ttIUI vv.11.1dvw.•% w' VV/1MI ,
Client:S&ME,Inc. Laboratory ID:VF16069-004
Description:HPE-4 Matrix:Aqueous
Date Sampled:06/15/2020 1600
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 06/25/2020 1424 JCG 06/18/2020 1800 57423
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 1
N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 1
N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1
N-Nitrosodiphenylamine(Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1
Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1
Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1
Phenol 108-95-2 625.1 ND 1.6 ug/L 1
Pyrene 129-00-0 625.1 ND 1.6 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1
2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 74 37-129
2-Fluorophenol 40 24-127
Nitrobenzene-d5 66 38-127
Phenol-d5 66 28-128
Terphenyl-d14 90 10-148
2,4,6-Tribromophenol 69 41-144
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 26 of 51

SO USA..VV...V.MI II.V I VV...V.MVJ {A.•M I VYV
Client:S&ME,Inc. Laboratory ID:VF16069-004
Description:HPE-4 Matrix:Aqueous
Date Sampled:06/15/2020 1600
Date Received:06/16/2020
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 1 06/19/2020 2325 DAL1 06/17/2020 1358 57236
2 608.3 3665A 608.3 1 06/19/2020 2128 DAL1 06/17/2020 1358 57236
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aldrin 309-00-2 608.3 ND 0.040 ug/L 1
Aroclor 1016 12674-11-2 608.3 ND 0.40 ug/L 2
Aroclor 1221 11104-28-2 608.3 ND 0.40 ug/L 2
Aroclor 1232 11141-16-5 608.3 ND 0.40 ug/L 2
Aroclor 1242 53469-21-9 608.3 ND 0.40 ug/L 2
Aroclor 1248 12672-29-6 608.3 ND 0.40 ug/L 2
Aroclor 1254 11097-69-1 608.3 ND 0.40 ug/L 2
Aroclor 1260 11096-82-5 608.3 ND 0.40 ug/L 2
gamma-BHC(Lindane) 58-89-9 608.3 ND 0.040 ug/L 1
alpha-BHC 319-84-6 608.3 ND 0.040 ug/L 1
beta-BHC 319-85-7 608.3 ND 0.040 ug/L 1
delta-BHC 319-86-8 608.3 ND 0.040 ug/L 1
Chlordane 57-74-9 608.3 ND 0.40 ug/L 1
4,4'-DDD 72-54-8 608.3 ND 0.040 ug/L 1
4,4'-DDE 72-55-9 608.3 ND 0.040 ug/L 1
4,4'-DDT 50-29-3 608.3 ND 0.040 ug/L 1
Dieldrin 60-57-1 608.3 ND 0.040 ug/L 1
Endosulfan I 959-98-8 608.3 ND 0.040 ug/L 1
Endosulfan II 33213-65-9 608.3 ND 0.040 ug/L 1
Endosulfan sulfate 1031-07-8 608.3 ND 0.040 ug/L 1
Endrin 72-20-8 608.3 ND 0.040 ug/L 1
Endrin aldehyde 7421-93-4 608.3 ND 0.040 ug/L 1
Heptachlor 76-44-8 608.3 ND 0.040 ug/L 1
Heptachlor epoxide 1024-57-3 608.3 ND 0.040 ug/L 1
Toxaphene 8001-35-2 608.3 ND 0.40 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q %Recovery Limits Q % Recovery Limits
Decachlorobiphenyl 73 20-131 71 20-131
Tetrachloro-m-xylene 65 30-132 95 30-132
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
FI=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 27 of 51

IVY -.111V
Client:S&ME, Inc. Laboratory ID:VF16069-004
Description:HPE-4 Matrix:Aqueous
Date Sampled:06/15/2020 1600
Date Received:06/16/2020
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 06/28/2020 2326 BPK 06/17/2020 1643 57262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Copper 7440-50-8 200.8 ND 5.0 ug/L 1
Lead 7439-92-1 200.8 ND 1.0 ug/L 1
Zinc 7440-66-6 200.8 ND 10 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 28 of 51

QC Summary
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 29 of 51

Inorganic non-metals - MB
Sample ID:VQ57413-001 Matrix: Aqueous
Batch:57413
Analytical Method:SM 2540D-2011
Parameter Result Q Dil LOQ Units Analysis Date
TSS ND 1 1.0 mg/L 06/18/2020 1837
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 30 of 51

Inorganic non-metals - LCS
Sample ID: VQ57413-002 Matrix: Aqueous
Batch:57413
Analytical Method:SM 2540D-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
TSS 250 250 1 100 90-110 06/18/20201837
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
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Page 31 of 51

Inorganic non-metals - MB
Sample ID:VQ57631-001 Matrix: Aqueous
Batch:57631
Analytical Method:SM 2540D-2011
Parameter Result Q DII LOQ Units Analysis Date
TSS ND 1 1.0 mg/L 06/21/2020 1639
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 32 of 51

Inorganic non-metals - LCS
Sample ID:VQ57631-002 Matrix: Aqueous
Batch:57631
Analytical Method:SM 2540D-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
TSS 250 250 1 99 90-110 06/21/20201639
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
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Page 33 of 51

Inorganic non-metals - MB
Sample ID:VQ58335-001 Matrix: Aqueous
Batch:58335
Analytical Method: 1664B
Parameter Result Q Dil LOQ Units Analysis Date
SGT-HEM(non-polar material) ND 1 5.0 mg/L 06/28/2020 1304
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
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Page 34 of 51

Inorganic non-metals - LCS
Sample ID:VQ58335-002 Matrix: Aqueous
Batch:58335
Analytical Method: 1664B
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
SGT-HEM(non-polar material) 20 19 1 95 64-132 06/28/2020 1304
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
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Page 35 of 51

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Semivolatile Organic Compounds by GC/MS - LCS
Sample ID:VQ57423-002 Matrix: Aqueous
Batch:57423 Prep Method: 625.1
Analytical Method:625.1 Prep Date: 06/18/2020 1800
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil %Rec Limit Analysis Date
Acenaphthene 20 21 1 107 47-145 06/22/2020 1238
Acenaphthylene 20 21 1 105 33-145 06/22/2020 1238
Anthracene 20 20 1 100 27-133 06/22/2020 1238
Benzidine 100 51 1 51 1-150 06/22/2020 1238
Benzo(a)anthracene 20 21 1 107 33-143 06/22/2020 1238
Benzo(a)pyrene 20 21 1 105 17-163 06/22/2020 1238
Benzo(b)fluoranthene 20 23 1 113 24-159 06/22/2020 1238
Benzo(g,h,i)perylene 20 23 1 117 1-219 06/22/2020 1238
Benzo(k)fluoranthene 20 23 1 116 11-162 06/22/2020 1238
4-Bromophenyl phenyl ether 20 21 1 103 53-127 06/22/2020 1238
Butyl benzyl phthalate 20 23 1 114 1-152 06/22/2020 1238
bis(2-Chloro-1-methylethyl)ether 20 19 1 95 36-166 06/22/2020 1238
4-Chloro-3-methyl phenol 20 21 1 107 22-147 06/22/2020 1238
bis(2-Chloroethoxy)methane 20 20 1 101 33-184 06/22/2020 1238
bis(2-Chloroethyl)ether 20 20 1 101 12-158 06/22/2020 1238
2-Chloronaphthalene 20 20 1 102 60-120 06/22/2020 1238
2-Chlorophenol 20 15 1 77 23-134 06/22/2020 1238
4-Chlorophenyl phenyl ether 20 21 1 104 25-158 06/22/2020 1238
Chrysene 20 22 1 111 17-168 06/22/2020 1238
Dibenzo(a,h)anthracene 20 23 1 116 1-227 06/22/2020 1238
3,3'-Dichlorobenzidine 20 14 1 69 1-262 06/22/2020 1238
2,4-Dichlorophenol 20 19 1 95 39-135 06/22/2020 1238
Diethylphthalate 20 22 1 111 1-120 06/22/2020 1238
Dimethyl phthalate 20 23 1 113 1-120 06/22/2020 1238
2,4-Dimethylphenol 20 21 1 103 32-120 06/22/2020 1238
Di-n-butyl phthalate 20 21 1 104 1-120 06/22/2020 1238
4,6-Dinitro-2-methylphenol 20 19 1 96 1-181 06/22/2020 1238
2,4-Dinitrophenol 40 32 1 80 1-191 06/22/2020 1238
2,4-Dinitrotoluene 20 24 1 120 39-139 06/22/2020 1238
2,6-Dinitrotoluene 20 23 1 113 50-158 06/22/2020 1238
Di-n-octylphthalate 20 20 1 98 4-146 06/22/2020 1238
1,2-Diphenylhydrazine(as azobenzene) 20 20 1 100 1-150 06/22/2020 1238
bis(2-Ethylhexyl)phthalate 20 25 1 125 8-158 06/22/2020 1238
Fluoranthene 20 21 1 106 26-137 06/22/2020 1238
Fluorene 20 21 1 107 59-121 06/22/2020 1238
Hexachlorobenzene 20 22 1 112 1-152 06/22/2020 1238
Hexachlorobutadiene 20 18 1 92 24-120 06/22/2020 1238
Hexachlorocyclopentadiene 100 68 1 68 1-150 06/22/2020 1238
Hexachloroethane 20 18 1 88 40-120 06/22/2020 1238
Indeno(1,2,3-c,d)pyrene 20 22 1 111 1-171 06/22/2020 1238
Isophorone 20 24 1 118 21-196 06/22/2020 1238
Naphthalene 20 21 1 103 21-133 06/22/2020 1238
Nitrobenzene 20 20 1 102 35-180 06/22/2020 1238
2-Nitrophenol 20 20 1 101 29-182 06/22/2020 1238
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 41 of 51

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: VQ57423-002 Matrix: Aqueous
Batch:57423 Prep Method: 625.1
Analytical Method:625.1 Prep Date: 06/18/2020 1800
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil %Rec Limit Analysis Date
4-Nitrophenol 40 39 1 98 1-132 06/22/2020 1238
N-Nitrosodimethylamine 20 22 1 110 1-150 06/22/2020 1238
N-Nitrosodi-n-propylamine 20 22 1 112 1-230 06/22/2020 1238
N-Nitrosodiphenylamine(Diphenylamine) 20 20 1 99 1-150 06/22/2020 1238
Pentachlorophenol 40 39 1 98 14-176 06/22/2020 1238
Phenanthrene 20 20 1 99 54-120 06/22/2020 1238
Phenol 20 14 1 72 5-120 06/22/2020 1238
Pyrene 20 23 1 113 52-120 06/22/2020 1238
1,2,4-Trichlorobenzene 20 19 1 93 44-142 06/22/2020 1238
2,4,6-Trichlorophenol 20 21 1 106 37-144 06/22/2020 1238
Surrogate Q % Limit Rec Acceptance Rec
2-Fluorobiphenyl 102 37-129
2-Fluorophenol 56 24-127
Nitrobenzene-d5 102 38-127
Phenol-d5 74 28-128
Terphenyl-d14 109 10-148
2,4,6-Tribromophenol 114 41-144
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 42 of 51

Organochlorine Pesticides and PCBs - MB
Sample ID: VQ57236-001 Matrix: Aqueous
Batch:57236 Prep Method: 608.3 Cleanup: 3665A
Analytical Method:608.3 Prep Date: 06/17/2020 1358
Parameter Result Q Dil LOQ Units Analysis Date
Aldrin ND 1 0.040 ug/L 06/19/2020 2137
Aroclor 1016 ND 1 0.40 ug/L 06/19/2020 0000
Aroclor 1221 ND 1 0.40 ug/L 06/19/2020 0000
Aroclor 1232 ND 1 0.40 ug/L 06/19/2020 0000
Aroclor 1242 ND 1 0.40 ug/L 06/19/2020 0000
Aroclor 1248 ND 1 0.40 ug/L 06/19/2020 0000
Aroclor 1254 ND 1 0.40 ug/L 06/19/2020 0000
Aroclor 1260 ND 1 0.40 ug/L 06/19/2020 0000
gamma-BHC(Lindane) ND 1 0.040 ug/L 06/19/2020 2137
alpha-BHC ND 1 0.040 ug/L 06/19/2020 2137
beta-BHC ND 1 0.040 ug/L 06/19/2020 2137
delta-BHC ND 1 0.040 ug/L 06/19/2020 2137
Chlordane ND 1 0.40 ug/L 06/19/2020 2137
4,4'-DDD ND 1 0.040 ug/L 06/19/2020 2137
4,4'-DDE ND 1 0.040 ug/L 06/19/2020 2137
4,4'-DDT ND 1 0.040 ug/L 06/19/2020 2137
Dieldrin ND 1 0.040 ug/L 06/19/2020 2137
Endosulfan I ND 1 0.040 ug/L 06/19/2020 2137
Endosulfan II ND 1 0.040 ug/L 06/19/2020 2137
Endosulfan sulfate ND 1 0.040 ug/L 06/19/2020 2137
Endrin ND 1 0.040 ug/L 06/19/2020 2137
Endrin aldehyde ND 1 0.040 ug/L 06/19/2020 2137
Heptachlor ND 1 0.040 ug/L 06/19/2020 2137
Heptachlor epoxide ND 1 0.040 ug/L 06/19/2020 2137
Toxaphene ND 1 0.40 ug/L 06/19/2020 2137
Surrogate Q %Rec Acceptance
Limmitit
Decachlorobiphenyl 79 20-131
Tetrachloro-m-xylene 69 30-132
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 43 of 51

Organochlorine Pesticides and PCBs - LCS
Sample ID:VQ57236-002 Matrix: Aqueous
Batch:57236 Prep Method: 608.3 Cleanup: 3665A
Analytical Method:608.3 Prep Date: 06/17/2020 1358
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Di! % Rec Limit Analysis Date
Aldrin 0.80 0.67 1 84 42-140 06/19/2020 2152
gamma-BHC(Lindane) 0.80 0.64 1 80 32-140 06/19/2020 2152
alpha-BHC 0.80 0.66 1 83 37-140 06/19/2020 2152
beta-BHC 0.80 0.64 1 81 17-147 06/19/2020 2152
delta-BHC 0.80 0.72 1 90 19-140 06/19/2020 2152
4,4'-DDD 0.80 0.76 1 95 31-141 06/19/2020 2152
4,4'-DDE 0.80 0.71 1 89 30-145 06/19/2020 2152
4,4'-DDT 0.80 0.71 1 88 25-160 06/19/2020 2152
Dieldrin 0.80 0.77 1 96 36-146 06/19/2020 2152
Endosulfan I 0.80 0.71 1 89 45-153 06/19/2020 2152
Endosulfan II 0.80 0.71 1 89 1-202 06/19/2020 2152
Endosulfan sulfate 0.80 0.77 1 97 26-144 06/19/2020 2152
Endrin 0.80 0.71 1 88 30-147 06/19/2020 2152
Endrin aldehyde 0.80 0.73 1 91 60-140 06/19/2020 2152
Heptachlor 0.80 0.67 1 83 34-140 06/19/2020 2152
Heptachlor epoxide 0.80 0.69 1 87 37-142 06/19/2020 2152
Surrogate Q % Rec Acceptance
Limmitit
Decachlorobiphenyl 74 20-131
Tetrachloro-m-xylene 67 30-132
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 44 of 51

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 49 of 51

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PACE ANALYTICAL SERVICES, 'LLC
s ee'p faviaomawnar Semlozs,Inc-
tlOtw�rcotNma1bOC►t600t1C- Efre
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Sample Receipt Checklist(SRC) ` dt>aee: r"
Clint; SAME Cooler in _, by/dote:DM0 106/16/2026
_ Lou: VF1 b 069
�+1..�Were custodyseals present on the cooler?
minim
2.Ifcustod scats were esere were intact and unbroken?
.H Strip ID: 20-110 Chlorine Strip ID: NA Toted Mt,H2
Original temperature
upon receipt f Derived(Corrected)temperature upon receipt %Sol id Snap-Cup 1D; NA
1.8 /1.1 °C O. /0.9 oc NA /NA °c NA /NA 'C —'
Method:ITetn.. .tore Blank❑Against Bottles IR fun ID: 5 lit Gun Correction Factor: 0 °C
Mcleod of coolant: 0 Wet lee ❑ Ice Packs ❑ m Ice ❑ None
3:
❑ yes. No-� If temperature o:any cooler exceeded 6.0°C,was Project Manager Notified?PM was Notified by:phone/email face-to-face(circle one).
(J Yes 0 No '.INA 4. Is the commercial courier's packing slip attached to this form?
®Yes Q x . 5. Were proper custody procedures(relinquished/received)followed?
Z Yes LING: 6. Were sample Into listed on the COC?
Ycs 0 No 7. Were sample[Ds listed on all sample containers?
Q Yes L`]No III 8. Was collection data do dine listed on the COC?
'I Yes ■No 9. Was collection date it time listed an all sem�ontainers7
Q Yes ❑No T0.Did all container libel information • date,time) a et with the COC?
Yes ❑No 11. Were tests to he performerd listed on the COC?
Yes ❑No I Did all samples arrive in the proper containers for each test and/or in good condition
(unbroken,lids en,etc.)?
!I yes In No 13.Was adequate sample volume available?
■ No 14.Were all temples received within Sri the holding time or 48 hoses,whichever comes fast?
L� 'I •��15.Were : start.les conlaincts missl .• excess(circle one)samples Not listed Os1 COC?
D Ycs PI No ❑ 16.For VOA and RSIC-175 samples,were bubbles present>'pce-sine"(/"ar 6mm in diameter)
in , oldie VOA vials?
WI Yes 0 No Mg 17.Were all DROhrntals/nuuient . , ,lea received at a , or<2?
❑Yes ! , "A E3 1S,Were all cyanide Samples received at a , >12 and sulfide sampk s received at a , 1>9?
❑Yee ! 0, 19. eae .I ;., LC: IT hi 4 eyrie', . . (t t.5 ' tamp ey frve otrest e
❑Yn t! No .I 20.Were client remarks/requests(i.c.regcested dilutions,MS/MSD designations,etc..)
correctly tr macn'bed from the COC into the comment section in LIMS?
Yes 'I No 21.Was rite quote number listed on the container label?Tf
Quote it
asep[e Preservations (Must he completed for any sample(s)incorrectly preserved or with headspuc c.)
pies) NA were received incorrectly preserved rednd were adjusted accordingly
sample receiving 'h NA mLofcirele one:H2SO4,HNO3,ITCI,NaOH using SR 0 )\A
Inc •
ofpreservation A . if more than one preservative is needed,please note in the comments below.
wen received with hubbies>6 rem in diameter.
Sautples(s)NA well received with r TRC>0.5 1ng/L(1f419 is no)and were
accordinglyadjusted sample receiving with sodium tlriosuWats(Na5S2O,)with Shealy ID: NA
'SR bercode labels appi ed by: I3MG/MI.142 Date 06r16/2020
Comments:
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 51 of 51