NC0006009_Regional Office Physical File Scan Up To 1/20/2021 (2)

DIVISION OF WATER QUALITY
October 20, 1998
MEMORANDUM
To: Tom Belnick
Through: Matt Matthews 0"ft-
From: Melissa Rosebrock
Subject: Galey &,Lor dustries ,Inc. = Caroleen Plant_ --
Biocide/Ch cerm aI Treatment Use
NPDES No. NC0006009
Rutherford County
Galey & Lord Industries, Inc. has submitted Nalco products 734.6 and 2593 for approval. Data
submitted by the facility concerning the dosage rate of the biocides, degradation, system volume,
average daily discharge, toxicity of the active ingredient(s) and/or breakdown products, and minimum
stream flow have also been reviewed and evaluated.
Please note, we have used the more, geographically appropriate Ceriodaphnia dubia LC50 value of
15.0 mg/L in calculating the regulated limitation for Nalco 2593. This value is from page 6 of the
attached MSDS and is based on a 1.5% solution of the active ingredients. This revision did not change
the final analysis portion of the worksheet (part IV; page 3).
Calculations summarized on the accompanying worksheet predict that the use of these products at
the stated dosage rates and discharge conditions will not result in toxic impact to aquatic life in the
receiving stream. Therefore, the use of Nalco 7346 and 2593 as biocides at Galey & Lord Industries,
Inc. - Caroleen Plant is deemed acceptable.
If there are questions concerning this review please contact me at [phone].
Attachments
cc: Forrest Westall-ARO
Central files

Galey & Lord Industries - Caroleen Plant Biocide Worksheet
►.
PERMIT#: NC0006009, Outfall 002
RECEIVING STREAM: Second Broad River
7Q10 (cfs): 51.20
I.W.C.%: 0.005
4
PRODUCT: NALCO 7346
ACTIVE INGREDIENT: 60% 1 BROMO-3-CHLORO-5,5DIMETHYLHYDANTION
27.4% 1 DICHLORO-5,5 DIMETHYLHYDANTION
15% 1 DICHLORO-5-ETHYL-5-METHYLHYDANTION
HALF LIFE (DAYS):
0.146
LC50 OF SELECTED TOX DATA (MG/Q): 0.15
DECAY RATE:
4.7260
DOSAGE RATE (GRAMS/DAY):
545
AVG DAILY DISCHARGE (MGD):
0.001719
VOLUME OF SYSTEM (MIL. GAL'S):
0.0123
7Q10 (cfs): 51.20
I.W.C.%: 0.005
STEADY STATE DISC CONC: 2.4059
DEGRADATION FACTOR: 4.866
APPLICATION FACTOR: 0.050
INSTREAM BIOCIDE CONC: 0.00013
REGULATED LIMITATION: 0.0075
PASS/FAIL: PASS
PRODUCT: NALCO 2593
ACTIVE INGREDIENT:
1.15%
5-Chloro-2-methyl-4-isothiazolin-3-one
0.35%
2-Methyl-4isothiazolin-3-one
HALF LIFE (DAYS):
22.00
STEADY STATE DISC CONC:
104.9386
LC50 OF SELECTED TOX DATA (MQ/L):
15.0
DEGRADATION FACTOR:
0.171
DECAY RATE:
0.0314
APPLICATION FACTOR:
0.010
DOSAGE RATE (GRAMS/DAY):
836.0
AVG DAILY DISCHARGE (MGD):
0.001719 INSTREAM BIOCIDE CONC:
0.0055
VOLUME OF SYSTEM (MIL. GAL'S):
0.0123
REGULATED LIMITATION:
0.15
PASS/FAIL:
PASS

Subject: NC0006009 Galey&Lord Industries- Caroleen Plant
Date: Mon, 19 Oct 1998 14:29:17 -0400
From: "Tom Belnick" <[e-mail]. nc.us> Internal
To: Melissa Rosebrock<[e-mail]>
I just talked with Ed Horton, Director of Engineering (336-665-3091),
and he said that microbiocides NALCO 2593 and NALCO 7346 are only used
in the cooling towers and are discharged only out of.0utfall 002. No
biocides are discharged out of Outfall 001. Therefore, the supplemental
biocide info that G&L submitted only covers Outfall 002 discharges.
[e-mail]
N.0 DENR-DWQ/NPDES Unit
P.O.Box 29535, Raleigh NC 27626-0535
Work: [phone] ext. 543
Fax: [phone]
of 1 10/20/98 7:56 AM

Subject: Re: #2 Re: NC0006009 Galey&Lord Industries- Caroleen Plant
',)ate: Mon, 19 Oct 1998 15:41:53 -0400
From: "Tom Belnick" <[e-mail]> Internal
To: Melissa Rosebrock <melissa [e-mail]>
Based on my conversation today with Ed Horton, it sounds like all
biocides discharge out of Outfall 002 only. I'll add a biocide condition
to the bottom of effluent sheets for both 001 and 002 (i.e., all
biocides must be approved before use by DENR....) incase biocides are
added to Outfall 001 in the future.
Melissa Rosebrock wrote:
> so where does there boiler blowdown discharge.... 001 or 002? _their
> letter states that copper and residual chorine are used in cooling
> towers AND/OR boilers ..........................then it states that no
> biocide is added to the boiler blowdown....... i see,what you
> mean...... very confusing.....
> their letter states that the biocides are added to airwashers which
> discharge through 001 along with sanitary and boiler
> blowdown...... another discrepancy.......
> i will work on 002 unless i hear othewise....
[e-mail]
N.0 DENR-DWQ/NPDES Unit
P.O.Box 29535, Raleigh NC 27626-0535
Work: [phone] ext. 543
Fax: [phone]
of 1 10/20/98 7:55 AM

r Division of Water Quality/NPDES Unit
October 13,1998
MEMORANDUM
TO: Melissa Rosebrock, Aquatic Toxicology Unit ES-6
FROM: Tom Belnick v4+ . 513
THROUGH: NA
SUBJECT: Biocide Data for Galey and Lord- Caroleen Plant, Rutherford County
NPDES Permit No. NC0006009
Melissa- The permittee submitted the attached supplemental biocide data last week. They are requesting
approval for microbiocides NALCO 2593 and 7346 to cooling towers which discharge blowdown to
Outfall 002. I have a call. in to the permittee to verify whether any biocides will be discharged via
Outfall 001, since I'm confused by their cover letter regarding this matter. In the last permit round,
DWQ had approved biocide-2593 for Outfall 004 (whic subsequently was renamed Outfall 002), but I
found nothing previously approved for Outfall 001.
The final permits are due to be issued October 26th, and we are shooting for Oct 16th to get them to
Dave Goodrich for final review and signature. I know- not much time- but just do the best you can.
Thanks.
cc: NPDES file

October 5, 1598
Mr. David Goodrich
NCDENR - DWQ/NPDES Unit
P.O.-Box 29535
Raleigh, NC 27626-0535
P. o. Box 35528
Greensboro, North Carolina 27425-0528
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Z 024 571 871
RE: Supplemental Information for the
NPDES Permit Renewal for the Galey & Lord Industries, Inc. Caroleen Plant
Caroleen; North Carolina'
Permit #NC0006009
Dear Mr. Goodrich:
Enclosed are three copies of the completed biocides worksheets and supporting .data for the addition of
Nalco Microbiocides 2593 and 7346 to the cooling towers "which discharge blowdown into Outfall_ 002.
These worksheets are provided in support of the renewal application for the Galey & Lord Caroleen Plant
(Permit #NC0006009) NPDES permit submitted May .22, 1998. :Outfall 002 receives cooling tower
condensate from a total of six cooling towers.
Please note that copper and residual chlorine are comnonents of water treatment the
cooling towers and/or oilers. oth chemicals exist in the products in very low, quantities. As shown on
page 4 of the biocide workshed for Nalco 2593, copper is discharged in a concentration well below the
water quality action level. Additionally, in re onse to yo a tember 9, ,1998 draft permit cover letter,
NO biocide is added t the boiler blowdo e same two biocides dded *to -the cooling tower systems
are dd it washers, which "discharge blowdown into utfall 001 with the sanitary wastewater and
boiler blowdown. The dosage and flow provided in the 1993 permit application have not changed, thus
the loci a wor heels provided in the 1993 application are still accurate. The copper'concentration in the,
discharge, however, is half of that listed on the biocide worksheet, since the latest MSDS indicates its
concentration is.0.025% instead of 0.05%.
Should you have any questions, please contact me at (336)' 665-3091. We look forward to receiving a
renewed permit in the near future. "
Sincerely,
GALEY & LORD INDUSTRIES, INC.
F� w
Mr. Edwin W'. Horton.
Director of Engineering
Attadhments
cc Jake irilson, Caroleen Plant
Bensinger & Garrison Environmental, Inc
G

irYts„ .,
Bensinger ,& Garrison
� h
ENVIRONMENTAL, INC
Bluefield',Engineeririg P.C` P.O. BOX 14609 RTP, NC 27709 = :.
J PHONE [phone]t_
" FAX [phone]
tr
J
r c _
- SUPPLEMENTAL INFORMATION FOR THE
t Y
x .NPDES RENEWAL`
7 t 1 t 4 c 3 d t
T.
GALEY &LOB INDUSTRIES,JNC.
i,
CAROI�EEleT PLANT['
CAROLEEN;, NORTH CA.ROLINA
PERMIT NO. NC0006009
SEPTEMBER 30,1998

I P
CERTIFICATION
Bensinger & Garrison Environmental, Inc: certifies that it has used standard and accepted practices in
completion of this project. The undersigned (and their appointees) shall have no liability or obligation .
to any party other than Galey & Lord Industries, Inc. (and their successors or assigns) and the
undersigned's obligations (and their appointees') are limited to fraudulent statements herein made or
to negligence.
4riAeAM aAffL Nc)/9cq,
Angela M. Ceroli Date
Environmental Engineer
V-P
k H. Garrison, Jr. Date
VP/Senior EnvironmeL Engineer
Bensinger & Garrison Environmental, Inc.
I

BIOCIDE WORKSHEETS
r Bensinger & Garrison Environmental, Inc.

Facility Name: Galey & Lord - Caroleen Plant NPDES #: NC 0006009
BIOCIDE/CHEMICAL TREATMENT
WORKSHEET-FORM 101
The following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
North Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
returned with all appropriate data entered into the designated areas with calculations performed as indicated.
I. Facility Name Galey & Lord Industries, Inc. - Caroleen Plant
NPDES # NC 00060Q2------ Outfall # 002
County Rutherford
Receiving Stream 2nd Broad River _ 7Q10 51.2 (cfs)
(All above information supplied by the Division of Environmental Management)
What is the Average Daily Discharge (A.D.D.) volume of the water handling systems to the receiving water body?
A.D.D. = 0.001719 (in M.G.D.)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
(A.D.D.) X 100 (0.0017) X 100 - 0.0052
1WC = (7Q10)(0.646) + (A.D.D) — ( 51.2) (0.6 4 6) + (0.0017)
This value (IWC) represents the waste concentration to the receiving stream during low flow conditions.
H. What is the -name of the whole product chemical treatment proposed for use in the discharge identified in Part I?
Nalco 7346 Microbiocide
Please list the active ingredients and percent composition:
1-Bromo-3-chloro-5,5-dimethylhydantoin 60.0 %
1,3-Dichloro-5,5-dimethylhydantoin 27.4
1,3-Dichloro-5-ethyl-5-methylhydantoin
10.6
What feed or dosage rate (D.R.) is used in this application? The units must be converted to maximum .grams
of whole product used in a 24hr period.
D.R.= 545 grams/24hr period
Please note, fluid'ounces (a volume) must be converted to grams (a mass). The formula for this conversion is:
Grams of product = fluid oz, of product X r1 gal. water X 8.34 lbs. X specific gravity of product -X 453.59 4
128 fl. oz. 1 gal. water 1 lb.
D.E.M. Form 101 (2/95) 1

Facility Name: Galey & Lord - Caroleen Plant NPDES #: NC 0006009
Outfall 002 - Nalco 7346
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for this estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.)
Volume= 0.0123 million gallons
What is the pH of the handling system prior to biocide addition? If unknown, enter N/A. 7.5 - 8.0 s.u.
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk. The
degradation must be stated at pH level within 1/2 pH standard unit within handling system. Enter the half life (Half
Life is the time required for the initial produWtodegrde to half of its original concentration). Please If
copies of the sources of this data.
H.L. = 0.146 Days (3.5 hrs)
The decay rate is equal to 1 H.L. X 0.69 = 4.73 =Decay Rate (D.K.)
Calculate degradation factor (D.F.). This is the first order loss coefficient.
' D.F. = A.D.D. + (D.K.) = (0.0017) + ( 4.73 ) = 4.87
(Volume) ( 0.0123 )
Calculate Steady State Discharge Concentration:
Dischg Conc. _ (D.R.) ( 545 } _ 2.404 mg/I
(D.F.)(Volume)(3785) ( 4.87 ) ( 0.0123 ) (3 7 8 5 )
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischq. Conc.) x (IWC%) ( 2.404 ) x ( 0.0052 ) _ 0.00013 mg/I
100 100
Receiving Saeam Concentration
III. Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be in
mg/1). Please provide copies of the sources of this data.
Organism
Bluegill Sunfish
Fathead Minnow
Rainbow Trout
Daphnia
Ceriodaphnia dubia
Sheepshead Minnow
Mysid Shrum
Eastern Oyster
Test Duration
96 hrs
LC50 (mgl)
1.2
96 hrs
0.71
96 hrs
.0.5
48 hrs
0.4
48 hrs
0.15
96 hrs
1.4
96 hrs
0.93
96 hrs
0.84
D.E.M. Form 101 (2/95) 2

14. j Galey & Lord - Caroleen Plant 0006009
racility Name: NPDES. #: NC
Outfall 002 - Nalco 7346
Choose the lowest LC50 listed above:
Enter the LC50: 0. 15
If the half life (H.L.) is less than 4 days, perform the following calculation.
Regulated Limitation = 0.05 x LC50 = 0.0075 mg/I
If the half life (H.L.) is greater than or equal to 4 days or unknown, perform the following calculation.
Regulated Limitation = 0.01 x LC50' = mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
0.0075
mg/liter
From Part II enter the receiving stream concentration:
0.00013 mg/liter
IV. Analysis.
If the receiving stream concentration is greater than the calculated regulated. limitation, then this biocideper�
unacceptable or use.
. IN -
lW" '
Signature Date
Person in Responsible Charge
Person Completing This Worksheet
(1i Different From. Above)
Angela M.'Ceroli
Bensinger & Garrison Environmental, Inc.
�c r
n F M Fnrm 101 f7/Qi1 , 'I

Facility Name: Galey & Lord - Caroleen Plant NPDES #: NC 0006009
,,
BIOCIDE/CHEMICAL TREATMENT
WORKSHEET-FORM 101
The following calculations are to be performed on any biocidal products ultimately discharged to the sl)rface waters of
North Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
returned with all appropriate data entered into the designated areas with calculations performed as indicated.
I. Facility Name Galey & Lord Industries, Inc. - Caroleen Plant
NPDES # NC 0006009 Outfall # 002
County Rutherford
Receiving Stream - 2nd Broad River 7Q10 51.2 (cfs)
(All above information supplied by the Division of Environmental Management)
What is the Average Daily Discharge (A.D.D.) volume of the water handling systems to the receiving water body?
A.D.D. = 0.001719 (in M.G.D.)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
`IWC - (A.D.D.) X 100 _ (0.0017Y X 1 00 _ 0.0052 %
(7Q10)(0.646) + (A.D.D) . - ( 51.2 ).(0.6 4 6) + (0_0017 )
This value (IWC) represents the waste concentration to the receiving stream during low flow conditions.
H. What is the name of the whole product chemical treatment proposed for use in the discharge identified in Part I?
Nalco 2593 Microbiocide
Please list the active ingredients and percent composition:
_ 5-Chloro-2-nethyl-4-isothiazolin-3-one __ _ 1.15 %
2-Iethyl-4-isothiazolin-3-one 0.35 %
What feed or dosage rate (D.R.) is used in this application? The units must be converted to maximum grams
of whole product used in a 24hr period.
D.R.= 836 grams/24hr period
Please note, fluid ounces (a volume) must be converted to grams (a mass). The formula for this'conversion is:
Grams of product = fluid oz. of product X 1 gal. water X 8.34 lbs. X specific gravity of product -X 453.59 Q.
128 fl. oz. 1 gal. water 1 lb.
D.E.M. Form 101 (2/95) 1

Fecility Name: Galey & Lord - Caroleen Plant NPDES #: NC 0006009,
Outfall 002 - Nalco 2593
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for this estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.)
Volume= 0.0123 million gallons
.What is the pH of the handling system prior to biocide addition? . If unknown, enter N/A. 7.5 - 8.0 s.u.
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk. The
degradation must be stated at pH level within 1/2 pH standard unit within handling system. Enter the half life (Half
Life is the time required for the initial product to degrade to half of its original concentration). Please provide
copies of the sources of this data.
H.L. = 22 Days /11
® 1
The decay rate is equal to 1 X 0.69 = 0.0314 =Decay Rate (D.K.)
H.L.
Calculate degradation factor (D.F:). This is the first order loss, coefficient.
A.D.D (0.0017 ) _ 0.171
' D.F. = (Volume) + (D.K:} _ ( 0.0123 ) + (0.0314 ) -
Calculate Steady State Discharge Concentration:
836
Dischg Conc. _ (D.F.)(Vollume)(3785) ( 0.171 ( ) ( 0.0123 ) ) (3 7 8 5) - 104'92 mg/I
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischg. Conc.) x (IWC%) ( 104.92 ) x ( 0.0052 ) 0.0055
100 - 100 = mg/I
Receiving Stream Concentration
Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be in
mg/I). Please provide copies of the sources of this data.
Organism
Mysid Shrimp
Shee shead Minnow
'l
Test Duration
96 hrs
96 hrs
LC50 (mgl)
18
32
D.E.M. Form 101 (2/95) 2

acility Name` Galey & Lord - Caroleen Plant NPDES #: NC 0006009
Outfall 002 - Nalco 2593
Choose the lowest LC50 listed above:
Enter the LC50: 18
If the half life (H.L.) is less than 4 days, perform the following calculation.
Regulated Limitation = 0.05 x LC50 = mg/I.
If the half life (H.L.) is greater than or equal to 4 days or unknown, perform the following calculation.
Regulated Limitation = 0.01 x LC50 = 0.18 mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
M
g/liter
From Part II enter the receiving stream concentration:
0.0055
IV. Analysis.
mg/liter
If the receivina stream concentration is greater than the calculated regulated limitation,- then this biocide is .
unacceptable for use.
Lid
�bl
Signature
Person in Responsible Charge
Ar,4& k 611,cyL
Person Completing This Worksheet
(r Different From Above)
Angela M..Ceroli
Bensinger & Garrison Environmental, Inc.
1197417-
=910
D.E.M. Form 101 (2/95) 3 .

Galey & Lord — Caroleen Plant NPDES #: NC 0006009
FaZility Name:
Outfall 002 - Nalco 2593
Supplemental Metals Analysis
if copper, zinc, or chromium are present in the proposed biocidal compound, complete this worksheet. A separate form
must be used for each metal and/or metal compound present in the biocide. List the metal, its chemical formula, molecular
weight (MW), formula weight (FW), and the concentration of the metal compound in the biocide (MCC). Complete a
separate form for every metal present in the biocide.
Metal _ Chemical Formila Molecular Weight of Metal Formula Weight Concentration in Biocide
EXAMPLE
Copper CUS04.5H2O 63.546 g/mole 249.680 g/mole 0.2
Copper Cupric Nitrate 0.0257 as Cu in biocide
Dosage rate of Biocide (DR) (from page 1):
DR = 836 grams/day
Average Daily Discharge (ADD) (from page 1):
ADD = 0.0017,19 million gallons/day
Discharge Concentration (DC) of Biocide:
DR ( 836 grams /day) = 486,329 grams/million gallons
ADD - (0.001719 million gallons/day)
Convert DC' to micrograms/liter (ppb):
1 x .106 ltg/g 128,489 u /l
DC (Ilg/9=486,329 DC (gr�ms/million gal) x 6 = g
3.785 x 10 liters/million gal.
Calculate the fraction of metal in, the metal -containing compound (MF):
WV ( grams/mole) _
MF = FW = ( grams/mole)
Calculate the fraction of metal in the biocidal compound (BF):
BF = MI MCC% _ x 100
x = 0.00025
(100)
Calculate the concentration of metal in the discharge (M):
128 489 0.00025
M = DC x BF = � ug/I x
= 32.12 ug/I
Calculate the instream metal concentration (IMC) at low -flow conditions:
IWC % 0.0052 % = 0.0017 ug/I
IMC = M x--= 32.12 ug/I x 1
100 00
Reguiated limitation of metal (from below): 7 µg/I
NC General Statutes 15A NCAC 213.0211 cefine:
Copper- 7 ug/l vrater quality action level' Zinc- 50 µg/1 water quality action level'
Chromium- 50 µg/I water quality stan�ard
('Values -.vhich exceed action levels must be addressed directly by aquatic toxicity testing.)
D.E.M. Form 101 (2/95) 14

SUPPLEMENTAL CALCULATIONS AND DATA
Bensinger & Garrison Environmental, Inc.
I

SUPPORTING CALCULATIONS FOR BIOCIDE WORKSHEETS
SECTION II:
Justification for System Volume for Outfall 002:
Source
Cooling Tower #1
Cooling Tower #2
Cooling Tower #3
Cooling Tower 94
Cooling Tower #5
Cooling Tower #6
Cooling Tower Blowdown
Total System Volume
(Outfall 002)
Vendor Information Sheets:
Volume
4,320
4,320
489
489
489
489
1,719 (gpd)
12,315 gallons
See attached MSDS' and vendor- information sheets for both biocides Nalco 2593 and 7346,
which provide the half-life information used in the biocide worksheet calculations.
SUPPLEMENTAL METALS ANALYSIS:
Per the MSDS for Nalco 2593, copper is contained at 0.025% as cupric nitrate, a constituent of
the biocide (see page 9 of 11 of the MSDS dated 10/15/97). Theref6re, 0.00025 is the fraction
(BF) of copper in the biocidal compound, -and no further calculation is required.
Bensinger & Garrison Environmental, Inc.

IVIh I G"1P%L_ v-JP% - G I I LJM I f1 %-af7 G G I
PRODUCT
NALCO 7346 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hours) (800) I-M-ALERT
SECTION 01 CHEMICAL PRODUCT AND COMPANY IDENTIFICATION
TRADE NAME: NALCO 7346 MICROBIOCIDE
DESCRIPTION: A blend of halogenated substituted hydantoins
NFPA 704M/HMIS RATING: 3/3 HEALTH 1/1 FLAMMABILITY 1/1 REACTIVITY OXY OTHER
O=Insignificant 1=Slight 2=Moderate 3=High 4=Extreme
SECTION 02 COMPOSITION AND INFORMATION ON INGREDIENTS
Our hazard evaluation has identified-the.following chemical ingredient(s) as
hazardous under OSHA's Hazard Communication 'Rule, 29 CFR 1910.1200. Consult
Section 15 for the nature of, the hazard(s).
INGREDIENTS) CAS # APPROX.%
1-Bromo-3-chloro-5,5-dimethyl4ydantoin 16079-88-2 60.0
1,3-Dichloro-5,5-dimethylhydantoin 118-52-5 27.4
1,3-Dichloro-5-ethyl-5-methylhydantoin 89415-87-2 10.6
SECTION 03.HAZARD IDENTIFICATION
EMERGENCY OVERVIEW:
DANGER: Harmful if swallowed. -Highly .corrosive. Causes eye and skin damage.
Irritating to nose and throat. Avoid breathing dust. Use with adequate
ventilation... Do not get into eyes, on skin or clothing. Wear rubber gloves,
chemical goggles and face shield when handling. Wash thoroughly after
handling. Immediately -remove contaminated clothing and wash before reuse.
Empty containers may contain residual product. Do not reuse container
unless properly reconditioned.
PRIMARY ROUTE(S)
OF EXPOSURE: Eye, Skin, Inhalation
EYE CONTACT:
Can cause severe. irritation. Corrosive to the eyes
with possible permanent damage depending on the
length of exposure and on the first aid action given.
SKIN CONTACT:
Can cause severe irritation. Corrosive to the skin with
ossible permanent damage depending on the length of
exposure and on the first aid action given. Can cause
allergic contact dermatitis in susceptible individuals.
INHALATION:
Can r.:ause severe respiratory irritation. Can be
corrosive to the mucous membranes and the lungs.
Can cause an allergic reaction in --susceptible individuals.
SYMPTOMS,OF EXPOSURE: A review of available data does not identify any.
PAGE 1 OF 10
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NARERMLLE, ILLINOIS 60563-1198
AREA 630-305-1000

MATERIAL SAFE-1 Y WATA 5HF=ET
PRODUCT
NALCO
NALCO 7346 MICROBIOCIDE-
• ..Emergency Telephone Number
Medical [phone] (24 hoursp (800) I-M-ALERT
SECTION 06 ACCIDENTAL RELEASE MEASURES
IN CASE OF TRANSPORTATION ACCIDENTS, CALL THE FOLLOWING 24-HOUR
TELEPHONE NUMBER (800) I-M-ALERT or [phone]. ,
SPILL CONTROL AND RECOVERY:
Solid spills: Sweep or vacuum up and reclaim into recovery or salvage drums
for disposal. Wear the protective equipment specified in Section 8 . Refer to
CERCLA in Section 15.
This product is toxic to fish. It should not be directly discharged
into lakes, ponds, streams, waterways or public water supplies.
SECTION 07 HANDLING AND STORAGE
Storage : Keep container closed when not in use.
SECTION.08 EXPOSURE''CONTROLS'.AND PERSONAL PROTECTION
RESPIRATORY PROTECTION::: Respiratory protection.not normally needed. -If
significant dusting'occurs-,. wear.either a _disposable dust mask or a cartridge
respirator with prefilter or high efficiency,cartridge.
For large spills, entry into large tanks, vessels or enclosed small spaces
with inadequate ventilation, --a positive pressure, self -contained _breathing_.
apparatus is recommended.
VENTILATION: If significant dusting occurs, local exhaust ventilation is
recommended.
PROTECTIVE EQUIPMENT: Wear impermeable gloves,.boots, aprons or a slicker suit
to avoid skin contact. Chemical goggles and face shield are also.recommended.
The availability of an eye wash fountain and safety shower is recommended.
If clothing is contaminated, remove. clothing and thoroughly wash the affected
area. Launder contaminated -clothing before reuse.
HUMAN EXPOSURE CHARACTERIZATION: Based on Nalco's,recommended.product
application and our recommended -personal protective equipment,.
the potential human exposure is: MODERATE.
PAGE 3.OF 10
NALCO CHEMICAL COMPANY ONE NALCO CENTER • NAPERVILLE, ILLINOIS 60563-1 1 S6
AREA 630-305-1000

MAIh.KIALSAt-t1Y WAIAbHhhI
11 - )N-'
NALCO
PRODUCT
NALCO 7346 MICROBIOCIDE-
Emergency Telephone Number
Medical [phone] (24 hours? (800) I-M-ALERT
SECTION 11 TOXICOLOGICAL INFORMATION i CONTINUED )
SECTION 12 ECOLOGICAL INFORMATION
This product is toxic to fish. Do not discharge into lakes, streams, -ponds or
public water unless in accordance with NPDES permit.,For guidance contact your
Regional Office of the EPA. Do not contaminate water by cleaning of container
and equipment or disposal of wastes. Apply this product only as specified on
this label. .
AQUATIC DATA: Results below are based on the product.
96 hour static acute LCs, to Bluegill Sunfish= 1.2 ppm
96 hour static acute LC,, to Fathead'Minnow = 0.71 ppm
96 hour static acute LC,, to Rainbow Trout = 0.5 ppm,
48 hour static acute LCs, to Daphnia 0.4 ppm
48 hour static acute LC,., to Ceriodaphnia.dubia. .15 pp
96 hour static acute LC,, to.Sheepshead Minnow = 1.
96 hour static acute ;LC,_,.to Mysid Shrimp = 0.93.ppm
96 hour. static acute LC,,,. to. Eastern.Oyster = 0.84 ppm .
AQUATIC DATA: Results below are based on dehalogenatd product
(5,5-dimethylhydantoin)
96 hour static acute LC,, to Rainbow Trout— 6,100 mg/L
48 hour static acute LC,, to Daphnia = 1,300 mg/L
96 hour static acute LC,,, to Fathead Minnow = 8,100 mg/L
96 hour -static acute LC,, to Sheepshead Minnow = 13,300 mg/L
96 hour static acute LC,, to Grass Shrimp = 12,000 mg/L
96 hour static acute LC,, to American Oyster = 14,200 mg/L
OTHER STUDIES:
Avian Toxicity: Results below are based.on similar active ingredients:
Dietary LCs, (Bobwhite Quail) = Greater than 5,620 ppm
Dietary LC,, (Mallard Duck) = Greater than 5,620 ppm
Acute oral LDs, (Bobwhite Quail) = 1,359 mg/kg
Acute oral LDs, (Bobwhite Quail) = Greater than 2,510 mg/kg
If released into the environment, see CERCLA.in Section 15.'
ENVIRONMENTAL HAZARD AND EXPOSURE CHARACTERIZATION.:' Based on_our Hazard
PAGE 5 OF 10
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NAPERVILLE, ILLINOIS 60563-119B
AREA 630-305-1000

MATERIALSAFEIY UA1A5.HhhI
PRODUCT
NALCO,7346 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hour# (800) I-M-ALERT
SECTION 17 RISK CHARACTERIZATION
Due to our commitment to Product Stewardship, we have evaluated the human
and environmental hazards and exposures of this product. Based on our
recommended use of this product, we have characterized the product's general,
risk. This information should provide assistance for your own risk
management practices. We have evaluated our product's risk as follows:
* The human risk is: MODERATE.
* The environmental risk is: MODERATE:
Any use inconsistent with Nalco's recommendations may affect our risk
characterization. Our sales representative will assist you to determine. if
your product application is consistent with our recommendations. Together
we can implement an appropriate risk management process.
This product material. safety data sheet provides health and safety
information. The product is to be used in applications consistent with
our product literature. Individuals handling this product should be
informed of the recommended:. safety precautions and should have access
to this information. For any other, uses, exposures should. be- evaluated
so that appropriate handling practices and training programs can be
established to insure safe workplace operations. Please consult your
local sales representative for any further information.
SECTION 18 REFERENCES - -- - - - - --
Threshold Limit Values for Chemical Substances and Physical Agents and
Biological Exposure- Indices, American Conference of Governmental
Industrial Hygienists, OH.
Hazardous Substances Data Bank, National Library of Medicine, Bethesda,
Maryland (CD-ROM version), Micromedex, Inc., Englewood; CO.
IARC Monographs on the Evaluation of the Carcinogenic Risk of Chemicals
to Man, Geneva: World Health Organization, International Agency for
Research on Cancer.
Integrated Risk Information System, U..S. Environmental Protection Agency,
Washington, D.C. (CD-ROM version), Micromedex, Inc., Englewood, CO.
Annual Report on Carcinogens, National Toxicology Program, U.S. Department
of Health and Human Services, Public Health Service..
Title 29 Code of Federal Regulations, Part 1910, Subpart Z, Toxic and
PAGE 9 OF 10
NALCO CHEMICAL COMPANY ONE NALCO CENTER •. NAPERVILLE. ILLINOIS 60563-1 1 SS
AREA 630-305-1000

BCDIMi�"��,b ,
�l�cdc,tc�-
BCDMH is d- hydantoin stabilized, bromine and chlorine based
oxidizing biocide. The products utilizing _this chemistry are
registered with the EPA for use in recirculating cooling
systems. The BCDMH products are in a dry form Vili.ch dissolve in
water to form hypobromou, and hypochlorous acids which .function
as active bioeidal constituents.
The overall rate of hydrolysis'and consumption of active halogen
is influenced by the halogen demand. imposed by the actual
operating system. The mono halogen compound hydrolyzes very
slowly in the absence of halogen demand. This generally results
in an operating 'system which contains very low or non -detectable
levels of free available halogen, but holds halogen in reserve
to meet the bi.odemand requirement..
Field, experience has shown that,. unlike chlorine, good
biological control is obtainable in many cases even in the
absence of detectable free available halogen. Total and free
available halogen levels can be monitored using various test
kits includirig a Hach DPD test kit or an amperometric titration
test method.
The dry product is generally fed using a brominator designed to
give consistent; disclution and feed rates.' -It can either be
slug fed or continuously with a free residual generally around
or below 0.2 ppm. The maximum free halogen residual as.ClZ
should not exceed 0.5 ppm. For continuous feed applications it
is desirable to check halogen residual levels at least daily.
In the case of slug treatment, residuals should be checked
during the time of biocide feed and shortly thereafter to
determine the peak level of system halogen.
BCDMH chemistry has been successfully used at many facilities to
replace chlorine gas. Generally it has been found that 1 pound
of tablets, fed on a slug basis will replace 5 to 7 pounds of
chlorine gas.
POst=ft(�' brand fax
treansmftta! memo 7671 #mpagm i �

2.0
N
w
1.6
cc
1.2
c
c
tM 0.8
0
0.4
a
IL
C
Typical Halogen F.rofile for Slug Fed BCDMH
,c J - 4 0 6 7 $
Time, Hours

Comparison of.'Hydrolysis Mechanisms
NALGO 7343 TAB (BCDMH)
CH CH, /0
HjQ �
/N-CI
_ V
O ,
All Chlorine 8peclea
CH R . /0 .
CI''N NCI
v
If
0
+ Hour
C11
H-- _0—� + HOC!
CIlN NCH
V
II
' � o
CH, CH, /0
1!
O
CH, R
- rN
iN_H
lb. N3-C1 H
0 ,o
+ HOC1
+ HOCI
R x.CHS (DCQgIJ)
Hyd[olysis'of 2nd halogen (dilorine) is slower, parlicularly la the N- t CL, and is reversible: this
or represents the "stablizalion" of halogen by the hydantoln sing,
CH?CH, ji0Cb1EH) Consumption of halogen at the "reservoir' of halogen.
og pushes Ibis equilibrium to the right, in essence supplying halogen "on
clemand'
I9egeneralon of active Br by attire Cl is well known chemistry:
Reducing Br- HOCI
HOBr Ag-- gent -� - HOBr t CI-

MATERIAL SAFETY DATA SHEET
LP4
NALCO
SECTION 1 PRODUCT IDENTIFICATION
PRODUCT
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) .. (800) I-M-ALERT
TRADE NAME: NALCO 2593 MICROBIOCIDE
DESCRIPTION: An aqueous solution of substituted isothiazolinone
NFPA•704M/HMIS RATING: 3/3 HEALTH 0/0 FLAMMABILITY 0/0 REACTIVITY 0 OTHER
O=Insignificant 1=Slight 2-Moderate 3=High 4-Extreme
SECTION 2 COMPOSITION/INGREDIENT INFORMATION
Our hazard evaluation has identified the following chemical ingredient(s) as
hazardous under OSHA's Hazard Communication Rule, 29 CER 1910.1200. Consult
Section 15 fo:- the nature of the hazard(s),
INGREDIENT(S) CAS # APPROX.%
5-chloro-2-methyl-4 isothiazolin-3-one 26172-55-4 1.15
2-methyl-4-isothiazolin-3-one 2682-20-4 0.35
SECTION 3 HAZARD IDENTIFICATION
EMERGENCY OVERVIEW:
DANGER: Corrosive. Causes eye damage and skin burns. May cause allergic skin
reaction.. May be harmful if inhaled. May be fatal•if swallowed or absorbed
through the skin. Do not get in eyes, on skin, or on clothing. Wear goggles
and face shield and rubber gloves when handling. Avoid breathing vapor or mist.
Avoid contamination of food. Do not take internally.- Wash --thoroughly after
handling.
PRIMARY ROUTE(S) OF EXPOSURE: Eye, Skin, Inhalation
EYE CONTACT: Corrosive to the:eyes with possible permanent damage
depending on the length of exposure and on the first
aid action given.
SKIN CONTACT: Corrosive to the skin, possibly resulting, in third degree
burns depending on the length of exposure and on the first
aid action given. Can -be harmful if absorbed. Can cause
allergic contact dermatitis in susceptible individuals.
INGESTION:. Can be fatal.
INHALATION: Can be corrosive to the mucous membranes and the lungs.
Can cause an allergic reaction in susceptible individuals.
SYMPTOMS OF EXPOSURE: A review of available data does not identify any
symptoms from 'exposure not previously mentioned.
AGGRAVATION OF EXISTING CONDITIONS: A review -of available data does not
PAGE 1 OF 11 ,
NALCO CHEMICAL COMPANY ONE NALCO CENTER • NAPERVILLE. ILLINOIS 60562-1 lea
AREA 630-3M-1000

MATERIAL SAFETY DATA SHEET
P4'
NALCO
PRODUCT
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medleal'[phone] (24 hours) (1300) I M-ALERT
SECTION 3 HAZARD IDENTIFICATION ( CONTINUED )
identify any worsening of existing conditions.
SECTION 4 FIRST AID INFORMATION
EYES: Immediately flush for at least 15 minutes while holding
eyelids open: Call a physician at once.
SKIN: wash thorougly with soap and rinse with water. Remove and
wash contamiriatbd clothing before reuse_
INGESTION:. Do not induce vomiting.. Drink promptly a large quantity of
milk, egg whites, gelatin solution, or,'if these are not
available, drink large quantities of water. Avoid alcohol.
Call a physician immediately.
INHALATION: Remove immediately to fresh air. If not breathing, apply
artificial respiration. If breathing is difficult, give
oxygen. Calla physician.
NOTE TO PHYSICIAN:'" Based on the individual reactions of the patient, the
physician's ju4.gment should be used to control symptoms and clinical condition.
CAUTION: If unconscious, having trouble breathing or in convulsions, do not
induce vomiting or give water.
NOTE TO PHYSICIAN: Probable mucosal-damage may contraindicate the use, of
gastric lavage. Measures against -circulatory shock, respiratory depression
and convulsions -may be -needed.
SECTION 5 FIRE FIGHTING
FLASH POINT: None
EXTINGUISHING MEDIA: Not applicable
UNUSUAL FIRE AND EXPLOSION HAZARD:"May evolve NOx, SOx or HC1 under fire
Conditions. Containers exposed in a fire should be cooled with water to
prevent vapor pressure buildup.leading to a rupture. Do not let material
evaporate to dryness.
SECTION 6 ACCIDENTAL RELEASE MEASURES
IN CASE OF TRANSPORTATION ACCIDENTS, CALL THE FOLLOWING 24-HOUR
TELEPHONE NUMBER (800) I-M-ALERT or [phone].
SPILL CONTROL AND RECOVERY:
PAGE 2 OF 11
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NAPERVILLE, ILUNOIS 60563-1 1 Se j
AREA e30"305-9C=

MATERIAL SAFETY DATA SHEET
NALCO
PRODUCT
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) (800) I-M-ALERT
SECTION 6 ACCIDENTAL RELEASE MEASURES ( CONTINUED )
Small liquid spills: Contain with absorbent material, such as clay, soil or -
any commercially available absorbent. Shovel reclaimed liquid and absorbent
into recovery or salvage drums for disposal. Refer to CERCLA in Section 15.
Large liquid spills: Dike to prevent further movement and reclaim into
recovery or salvage drums or tank truck for disposal. Refer to CERCLA
in Section 15.
For large indoor spills, evacuate employees and ventilate area. Those
responsible for control.and recovery should wear the protective equipment.
specified in Section 8 .
This product is toxic to fish. It should not be directly discharged into
lakes, ponds, streams, waterways or public water supplies.
SECTION 7 HANDLING AND STORAGE
Storage Keep container closed when not in use_
SECTION 8 EXPOSURE CONTROLS/PERSONAL PROTECTION
RESPIRATORY PROTECTION:. If it is possible to.generate significant levels of
vapors or mists, a NIOSH approved or equivalent respirator is recommended.
For large spills, entry into large tanks, vessels or enclosed small spaces
with inadequate ventilation, a positive pressure, self-contained breathing
apparatus is recommended.
VENTILATION: General ventilation is recommended. Additionally, local exhaust
ventilation is recommended where vapors, mists -or aerosols may be released.
PROTECTIVE EQUIPMENT: Wear gloves, boots, apron and a face shield with
chemical splash goggles. (Based on test data obtained from materials of
construction, the following recommendations are listed for gloves along with
their break -through times: Butyl rubber (greater than 8 hours); polyvinyl
chloride (greater than 7.5 hours) and neoprene coated (greater than 6 hours).
A full slicker suit is recommended if gross exposure is possible.
The availability of'an eye wash fountain and safety shower is recommended.
If clothing is contaminated, remove clothing and thoroughly wash the. affected,
Area. Launder contaminated clothing before reuse.
i -
PAGE 3 OF 11
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NAPEFMLLE. ILLINOls ro56_3-9 i se
AREA 630.305-1 C= -

MATERIAL SAFETY DATA SHEET
(PRODUCT
NALCO
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) (800) I-M-ALERT
SECTION B EXPOSURE CONTROLS/PERSONAL PROTECTION ( CONTINUED }
HUMAN EXPOSURE CHARACTERIZATION: Based on Nalco's recommended product
application and our recommended personal protective equipment,
the potential human exposure is: LOW.
SECTION 9 PHYSICAL AND CHEMICAL PROPERTIES
COLOR: Pale yellow to green FORM: Liquid- ODOR: Mild
DENSITY: 6.•6 lbs7gal.
SOLUBILITY IN WATER: Completely
pH (NEAT) = 3.- 5 ASTM E-70
FREEZE POINT: 25 Degrees F ASTM D-1177
FLASH POINT: None
VOLATILE ORGANIC
COMPOUND (VOC): 0.07 lbs/gal. EPA METHOD 24
NOTE: These physical properties are typical values for -this product.
SECTION 10 STAFILITY.AND REACTIVITY
INCOMPATIBILITY;. None known
THERMAL DECOMPOSITION PRODUCTS: In the event of Combustion CO, CO2, NOx,
SOX, HC1 may be formed. Do not breathe smoke or fumes. wear suitable
protective equipment.
SECTION 11 TOXICOLOGICAL INFORMATION
TOXICITY STUDIES: Toxicity studies h'ave been -conducted on this product.
The results are shown below.
ACUTE ORAL TOXICITY (ALBINO RATS): LD50 = 3,810 mg/kg
95% Confidence Limit - 3,530 - 4,.220 mg/kg
ACUTE DERMAL TOXICITY (ALBINO RABBITS):
LD50 = Greater than 5,000 mg/kg
ACUTE INHALATION TOXICITY (ALBINO RATS):
For solution of 1% active ingredients' LC50 = 13.7 mg/L
COMMENTS: Four-hour nominal concentration For a solution containing 1%
active ingredients.
SKIN IRRITATION INDEX DRAIZE RATING: Severe irritant
PAGE 4 OF 11
NsaLOO CHEMICALL COMPANY ONE NALCO CENTER - NAPERVILLE. ILLINOIS 60563-1 1 S6
ARFA 830.305-1000

MATERIAL SAFETY DATA SHEET
*4
NALCO
PRODUCT
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) (800) I-M-ALERT
SECTION 11 TOXICOLOGICAL INFORMATION ( CONTINUED )
EYE IRRITATION INDEX DRAIZE RATING: 'Corrosive (corneal damage)
SKIN SENSITIZATION: This product is a human sensitizer in its undiluted form.
A Guinea pig (Buehler Technique) sensitization study with an induction dosage
of 90 ppm of active ingredients followed by a insult of 429 ppm of active
ingredients was positive. '
A human repeated insult patch study of 28 ppm active ingredients followed by
a insult of 56 ppm of active ingredients resulted in no effect to the subjects
tested.
SUBCHRONIC TOXICITY_ RESULTS: A 90-day dietary study in dogs of 840 ppm of the
product's active ingredients -resulted in no mortalities or pathological
findings. A 90^day dermal study in rabbits of 0.4 mg/kg/day of the product's
active ingredients resulted in irritation but no pathological effects.
CHRONIC TOXICITY RESULTS: A teratology study with rabbits and rats was
negative with dosages of active ingredient ranging from 1.5 mg/kg to 15 mg/kg.
Mutagenicity results were equivocal. A 30-month skin painting mouse study,
with applications of 400 ppm of active ingredients three times per week
showed no increase tumor frequency over control animals.
HUMAN HAZARD -CHARACTERIZATION: Based on our hazard -characterization,
the potential human hazard is: HIGH,
SECTION 12 ECOLOGICAL INFORMATION
CHEMICAL OXYGEN DEMAND (COD): 20,000 ppm
TOTAL ORGANIC CARBON (TOC): 7,850 ppm
AQUATIC DATA: Active ingredient.
6 day static acute LC50 to Bluegi,ll Sunfish = 0.54 ppm
Standard Deviation of 6 day LC50 = 0.47 - 0.62 ppm
6 day dynamic acute LC50 to Fathead Minnow = 0.12 ppm
Standard Deviation of 6 day LC50 = 0.06 - 0.15 ppm
48 hour acute LC50 to Daphnia Magna - 0.13 - 0.19 ppm
PAGE 5 OF 11
NALCO ChMMICAL COMPANY ONE NALCO CENTER - NAPERVILLE. ILUNOIS aosas-1 'I sa
AREA B3G3W-1000

MATERIAL SAFETY DATA SHEET
(PRODUCT
NALCO
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical (800) 462-53713(24 hours) (800) I-M-ALERT
SECTION 12 ECOLOGICAL INFORMATION ( CONTINUED )
6 day dynamic acute LC50 to Rainbow Trout = 0,.14 ppm
Standard Deviation of 6 day LC50 = 0.12 - 0.17 ppm
96 hour static acute LC50 to Sheepshead minnow = 0.3 ppm
Standard Deviation of 96 hour LC50 = 0.18 -.0.50 ppm
Results below are based on a 1.5% solution of the active ingredients
48 hour acute LC50 to Ceriodaphnia Dubia = 15 mg/L
48 hour no observed effect concentration is 10 mg/L based on no mortality or
abnormal effects.
OTHER STUDIES: Avian species:
Acute oral LDS to Bobwhite Quail = 97 mg/kg
Standard Deviation of LD50 a 64 - 114 mg/kg
8 day dietary LD50 to Pekin Duck = 560.ppm.of active ingredients
ik AQUATIC DATA: Product.
96 hour static acute LC50 to Mysid = 18 mg/L
96 hour no observed effect concentration is.less than 10 mg/L based on no
mortality or abnormal effects.
TOXICITY RATING: Moderately toxic
96 hour static acute LC50 to Sheepshead Minnow = 32 mg/L
96 hour no observed effect concentration is 18 mg/L based on no mortality or
abnormal effects.
TOXICITY RATING: Moderately toxic
If released into the environment, see CERCLA in Section 15.
ENVIRONMENTAL HAZARD AND EXPOSURE CHARACTERIZATION.' Based on our Hazard
Characterization, the potential environmental hazard is: HIGH.
Based on Nalco's recommended product application and the product's -
characteristics, the potential environmental.exp.osure is: LOW_
PAGE 6 OF 11
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NAPERVILLE, 1LUNOI8 60S83-1 '198
AREA E,'aC3'xK-1000

MATERIAL SAFETY DATA SHEET
k. )w
NALCO
SECTION 13 DISPOSAL CONSIDERATIONS
PRODUCT
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) (800) I-M-ALERT
DISPOSAL: If this product becomes a waste, it does not meet the criteria of
a hazardous waste as defined under the Resource Conservation and Recovery Act
(RCRA) 40 CFR 261, since it does not have the characteristics of Subpart C,
nor is it listed under Subpart D.
PESTICIDE DISPOSAL: Pesticide wastes are hazardous. Improper disposal of
excess pesticide, spray mixture, or rinsate is a violation of Federal Law.
If these wastes cannot be disposed of'by use according to label 'instruction,
contact your State Pesticide or Environmental Control Agency, or the Hazardous
Waste representative at the nearest,EPA Regional Office for guidance.
METAL CONTAINERS: Triple rinse (or equivalent). Then offer for recycling or
reconditioning, or puncture and dispose of in a sanitary landfill, or by other
procedures approved by state and local authorities.
PLASTIC CONTAINERS: Do not reule empty container. Triple rinse (or equivalent).
Then puncture and dispose of in a sanitary landfill, or, if allowed by state
and local authorities, by burning_ If burned, stay out of smoke.
SECTION 14 TRANSPORTATION INFORMATION
PROPER SHIPPING NAME/HAZARD CLASS MAY VARY BY PACKAGING, PROPERTIES,
AND MODE OF TRANSPORTATION. TYPICAL PROPER SHIPPING NAMES FOR THIS
PRODUCT ARE:'
ALL TRANSPORTATION MODES
UN/ID NO
HAZARD CLASS - PRIMARY
PACKING GROUP
IMDG PAGE NO
IATA PACKING INSTRUCTION
IATA CARGO AIRCRAFT LIMIT
FLASH POINT
TECHNICAL NAME(S)
RQ LBS (PER PACKAGE)
RQ COMPONENT(S)
CORROSIVE LIQUID, ACIDIC,
ORGANIC, N.O.S.
UN 3265
8 - CORROSIVE
II
8147-1
CARGO: 812
30 L (MAX NET QUANTITY PER PACKAGE)
NONE
ISOTHIAZOLINONE MICROBIOCIDE
NONE
NONE
SECTION 15 REGULATORY INFORMATION
The following regulations apply to this product.
FEDERAL REGPLATIONS:
PAGE 7 OF 11
NALCO cmr=MICAL COMPANY ONE NALCO CENTER • NAPERVILLE, IL,LINOIS S05e3-119B
AAeA e30-305-1000 1

MATERIAL SAFETY DATA SHEET
NALCO
PRODUCT
7NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) (boo) I-M-ALERT
SECTION 15 REGULATORY INFORMATION ( CONTINIIED )
OSHA'S HAZARD COMMUNICATION RULE, 29 CFR 1910.1-200:
Based, on our hazard evaluation, the following ingredients in this product are
hazardous and the reasons are shown below.
5-chloro-2-methyl-4 isothiazolin-3-one - Corrosive, sensitizer
2-methyl-4-isothiazolin-3-one - Corrosive, sensitizer
5-chloro-2-methyl-4 isothiazolin-3-one
TWA 0.1 mg/m3, STEL 0.3 mq/m3 TLv
Manufacturer's recommendation
CERCLA, 40 CFRr-117, 302:
Notification of spills of this product is not required.
SARA/SUPERFUND.JLMENDMENTS AND REAUTHORIZATION ACT'OF 1986
(TITLE III) —SECTIONS 302, 311, 3.12 AND 313:
SECTION 302 - EXTREMELY HAZARDOUS SUBSTANCES (40 CFR 355):
This product does.not contain ingredients listed in Appendix A and B-as an
Extremely Hazardous Substance.
SECTIONS 311'and 312 - MATERIAL SAFETY DATA SHEET REQUIREMENTS (40 CFR 370):
Our hazard evaluation has found this product to be hazardous. The product
should be reported under -the following. EPA hazard categories; -
XX Immediate (acute) health hazard
-- Delayed (chronic) health hazard
-- Fire hazard-
-- Sudden release of pressure hazard
-- Reactive hazard
Under SARA 311 and 312, the EPA has established threshold quantities for the
reporting of hazardous chemicals. -The current thresholds are: 500 pounds or
the threshold planning quantity (TPQ); whichever is lower, for extremely
hazardous substances and 10,000 pounds for all other hazardous chemicals.
SECTION 313 - LT;T OF TOXIC CHEMICALS (40 CFR 372):
This product contains the following ingredient(s), (with CAS # and % range)
which appear(s) on the List of Toxic Chemicals.
Magnesium nitrate '.(nitrate compounds). 10377-60-3 1-5
TOXIC SUBSTANCES CONTROL ACT (TSCA):
PAGE 8 OF 11
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NAPERML.LE, ILLINOIS B06E3-1198
AREA e=-3 -9 000 !

MATERIAL SAFETY DATA SHEET
PRODUCT
NALCO
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical (600) 462=5378 (24 hours (800) I-M-ALERT
SECTION 15 REGULATORY INFORMATION ( CONTINUED )
The active ingredients are exempted under-TSCAand regulated under FIFRA as
follows. All the inert ingredients are found on the TSCA Master Inventory
List.
FEDERAL INSECTICIDE, FUNGICIDE AND RODENTICIDE ACT (FIFRA):
EPA Reg. No. 1706-153. This product is registered for use as a microorganism
control chemical used in industrial recirculating cooling water tower
systems, used in brewery pasteurizers, and used in air washer systems.
In all cases follow -.instructions on the product label.
RESOURCE CONSERVATION AND RECOVERY ACT (RCRA), 40 CFR 261'SUBPART C 6 D:
Consult Section 13 for RCRA classification.
FEDERAL WATER POLLUTION CONTROL ACT; CLEAN WATER ACT, 40 CFR 401.15
(formerly Sec. 307), 40 CFR 116 (formerly Sec. 311):
This product contains the following ingredients covered by the Clean Water Act:
Cupric nitrate - Section 307, 311
CLEAN AIR ACT, Sec. Ill (40 :CFR 60), Sec. 112,(40.CFR 61, 1990'Amendments),
Sec. 611 (40 CFR 82, CLASS I and II Ozone depleting substances):
This product does not contain ingredients covered by.the Clean Air Act.
STATE REGULATIONS:
CALIFORNIA PROPOSITION 65:
This product does not contain any chemicals which require warning under
California Proposition 65.
MICHIGAN CRITICAL MATERIALS:
This product contains the.following substance(s) identified on the Michigan
Critical Materials Register:
Copper, as Cu = 0.025%
STATE RIGHT TO KNOW LAWS:
The following state(s) identify the ingredient(s) shown below as hazardous:
California - Copper
Massachusetts, New Jersey; Pennsylvania - magnesium nitrate
INTERNATIONAL REGULATIONS:
This is not,a WHMIS controlled product under The House of Commons of Canada
PAGE 9 OF 11
NALCO CHEMICAL COMPANY ONE NALCO CENTER • NAPERVILLE. ILLINOIS 60563-1199
AREA OCKNO05-1 C=

MATERIAL SAFETY DATA SHEET
(PRODUCT
NALCO
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours) (800) I-M-ALERT
SECTION 15 REGULATORY INFORMATION A CONTINUED )
Bill C-70.
SECTION 16 OTHER INFORMATION
Note: Other toxicological results are available upon request.
It is strongly recommended that this product be educted for safety reasons.
If pumping is the only viable alternative, use special care when doing
maintenance on either the pump or feed lines. Do not dump buckets of
this product.
SECTION 17 RISK CHARACTERIZATION
Due to our commitment to Product Stewardship, we have evaluated the human
and environmental hazards and exposures of this product. Based on our
recommended use of this product, we have characterized the product's general
risk. This information should provide assistance for your own risk
management.prGtitices. We have evaluated our product's risk as follows:
The human risk is: LOW.
The environmental risk is: LOW.
Any use inconsistent with Nalco's recommendations may affect our risk
characterization. Our sales -`representative will assist you to determine if
your product application is consistent with our recommendations. Together
we can implement an appropriate risk management process.
This product material safety data sheet provides health and safety
information. The,product is to be'used in applications consistent with
our product literature. Individuals handling.this product should be
informed of the recommended safety precautions'and should have access
to this information. For any other uses, exposures should be evaluated
so that appropriate handling practices and training.programs can be
established to insure safe workplace operations. Please consult your
local sales representative for any further information.
SECTION IS REFERENCES
Threshold Limit Values for Chemical "Substances and Physical Agents and
Biological Exposure Indices, American Conference of Governmental
Industrial Hygienists, OH.
Hazardous Substances Data Bank, National Library of Medicine, Bethesda,
PAGE 10 OF• 11
NALCO CHEMICAL COMPANY ONE NALCO CENTER - NAPERVILLE, ILUNOIS eC 1196
AREA S30.-J06-1000

__ ----- ___ ---- ..... a..., ..a.a.. va as - yy VVY
0 • CBC12 . 0. CA% lV"
R-C> A --an' l'
Q
} - CaCIa
0 0 0 0:
N_ _ c1 " a—Ce x—eH g—CH3
3 C 3 r
• 5 �- S 5 —"" S
C1 CI
0 0
S
as
0♦ 0 ' O
n
C—CSC C—xA—C83 HC—C—FHICs3
110
0� O
\ C—CrLZ— C—YH2
HO
�G—CIt2—C GH2
HO OR
off OS
CHy— C 01,
OH
i 0 -
0i
H—C
SOS
=03 — Cp2
Major degradative pathway of (he calcium chloride salts of Methylchlaroisothiazolinone (1)
and Methylisothiazolinona (11) (bracketed structures are postulated)

UUIZO/aa 10:11 "Diu JU5 LU60 t;NV1HN HLER 5FEY 100W
Metabolic Pathway of N - Methyl lsothiazolone
�
x=HorCl
c metndou n,
h►+� PY�$
CH.,
PAAEMT
H,GNH-Ct0)-CH�O�H
"r
IH,�-H-C(0}-cH�CF�6,8•I
���
nr-me�j+►•merraptap�rvp►anamlde ra�tca�
�
H,c-fiH-C(GrCH
N-me�yl acetam�
�
4 �
I
r *
H,0-NH-C(%-COJ4
mi�ara
N-meuryr exams ac d
cry
1i�0-l�f-CC=H
l�me�ftyl carbamlc acid

VV/ 40f VO 14.1L LNUOU JVJ ZVOO
Ll Y U0 IlLili bYfX
Wood
1. Degradation and Metabolism
Study
Half-life
5-chloro-2-methyl-4- 2 methyl-4-isothiazolin-s-one Jd`"
isothiazolin-3-one
Hydrolysis pH 5 = stable pH 5 -stable
PH 7 = PH 7 = stable
Photolysis PH 9 day pH 9 = stable
Y$i 6.6 d 11.1 days
Aerobic Aquatic Metabolism 0.72 d 0.38 days
Anaerobic Aquatic 0.20 days
Metabolism
Aerobic Soil Metabolism 0.23 days
II. Bioaccumuiation-
A. Qctanol: Water Partition Coefficient
5-chloro-2-methyl-4-isoihiazolin-3-one tog P = 0.4
2 methyl-4-isothiazolin-3-one log P = -0.5 .
B. Bioconcentration
The bioconcentration factor (BCF) was determined in bluegili sunfish.
Whole Fish - - , _50X-
The time for 50% of the'{C-residues to depurate was less than 2 days.
Detoxification of Isothiazolinones by pretreatment with NaHS03(cieaves isothiazoline .
ring) significantly decreased the toxicity to Bluegill sunfish.

State of North Caroiina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
A4
�ID: E101R
Facsimile Cover Sheet
To.- --jeLin 70X
Fax: _ _ _
From: ►�'� e, LrV) C Xj MODE VrIi i
Phone: [phone]$3 extension S�
Fax: [phone]
pages. including this cover sheet.
Comments:
JL&ANh-e-et lol hK b,oci,
O�4-{��ta I 100) —� AM
i Liu
�C 000bopq-6=Alehd
M
0
73Vb
TP19v 3 ki e) Ya,'PPdI Pio ri I
P.O. Box 29535; Raleigh, North Carolina 27626-0536 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% =ycledl 10% post-aonsumerpaper
6T/10'd K: TT , 86, Z ipr 6TZ0-22Z-6T6:XE3 3 ' d-W3G

1et00PM CRROLEEM GALE:Y &LORD
P.1
RAt,�Y � I�QrRi) �rmgs't� IbIC.
�O,�7Cd19
•CA]bDIEBN. N C, ZSOla
To; W. TomBdddt FRI 9194334719 :
troy. JAI Wllscm pate: 07/099
Fte: Workshm palm 101 ft Nalco 7346 P"es 14 b*ftg cwer shod
O IAA" A For MW Q Piewle omrmt U Pbm ft* o pWW R39 ela
�y���eanrmanra��
rN
00t
6oi1-14 3j(%dd.oQA
Icy 73A A0440tc
6WO 'd 6£:TT 86, Z .Inr 6TZ0-22L-6T6:Xpd 3 ' d-W3Q

4.
7l •` . 0 ' ga 1a; 00PM CAROLEM GALEY &LORD
F.2
9I0CIDIJCl.1EMICAL TROATMENT
WORKSHEET-FORM 101
The loltowlnQ calculations are to be performed on any biotidal produCIC Ultimately discharged to Iris 9"uriace waler9 el
This Wprltsheet MUD; be completed separalolY for each hiocldal-prodrlCl in use. This workshaat is iv Ce
North Caroline.
returned Wflh oB appropriate data entered Into The dsolpnated arags with oalcUlall= pedormad
as indicated,
l; t=acuity Name
Burlington Tnduet:ries CarAillF ou�t'sil aAl
ivayD&S # NC NCOoo6009 � •
Ruthax`i°ard
county Mi D 51 2
ilecElving Strt3am end Bro-d PAVC* ,
(AI( above InlOMM110n aupp>jed by the DIviSTon oI Environmenla{ Management) '
Whot is the Average Dolly O(scharge (A.p.t7.) volume of the wallet {tiandtinq �yalems la the r4cetvtng water body?
A.D.D.: 01005 (in M.t3.D.)
ploa6e calculate the IrldtroOn VVaste Conceritratlon (IWO to percent)) or this diaGharge Using Tha dale +gntarad
above.
AID)MIN x 100
IWQ-5 ���� X 0.6 ♦ (A.D�- .
.005 . 100
51.2 .�(0. 4b) • 4 (.nr)5- )
This valU6 IWC) represents the wraste cancentrallon to the receiving dream during low flow condiliotls.
{ ,
e the name of t11e whole product chernir+al Ireatmmt proposed for ul4e in the dISChardo identified in Fars 17
il. Tunica 7346 Mierobioci.de
Please (I$t the active ingredlenls and porcent C0rnPc sllian: 40 to 70 •Io
i-Stoma-3-cnlora-5 y� d=ntoin 20 to 40 er.
1 8-Dialtloro-5 3-dirae•tb Ih domain tp� 0 N.
1,3-biehloro-t:-ath 7.�5-mel+hy�h danto�n .��
Note: It Ingrvdionts contain the metals tioppar, phromiuty7, artlnc, alga eomplels papl d. ed to earno of whole.
W."t lead or dosage ram (O.A.) la used in this application? The unity must be canveri 9
• -product Used par daY.
D.R.e 545 grarnslday.
D.�.M.Paxm ldl (719x) 1
6T/0'4 OV:TT 86, Z Inr 6TZ0-22Z-6T6:Xp3 3 ' d-W3Q

JUL 02 '98 1?:00pM CAR9LEEN GAL.EY 8LORD
j Surlirngton Induatriae Cdro2o= Plant NPAES Q405009
Facility Name:
Out:fxu 001 — "8100 -1346
Estimate total udlume of the water handling system between entry at blocidal product and NPDE$II disChtirge
lde justification for this estimate (system plume; averxgi cyciag ppr
pginl. On an mttached ohdrt please prov
blowdown. holding lagoon alxe. etc.)
Volurnaa 0.050 million flaltvns
. 7.5 to" 8.0- S.U.
What is the pH of ttte handling system prior to biocide addition? If unknown, enter NIA.
What is the decay We (D.1<.) of the product? It ur►known, Assume no deoey (D.K.=o) and prncoed to asterisk.
The degradation must be slated at pH levee within 1!2 pH standard unit within handling system. Entsr the half
Ile ¢-fall Lug;1a the tlrt9j required far the Inlllsl product to degrade to hall of Its oftinal carTcBmralionj. PIlsSf+
provide copies of the sources of this data. '
H.L. = 1 Days
The decay rate is equal to HK-. X 0,66 a. b9 .decay Rale:p�.K.j
K.L.
Calculate degradatiOn factor (p.F.). this 19 tne*iitstorder lo5s Ocelficient.
o.doa j 0.79
D.F. w A.D.Q. * (D.K.) _ -- 0.69 -.-
(Voiume) ( 0.05 .
calculate Straady RON Discharge Conoentration: 345
Dischg Cane. s (D.F.j(Valu1T1e)(3785j * ( 0,39 ) ( 0,05 a
CaICvIE;te coacentratlon of biocide instream during low flow conditions. ,
inecolving Strnam Concentration) ,
o, 00055 melt
f 3d9 } x f O.OlS
Mlacho, Conc.) x (lWG4/1 100
100
a 3.65 mgll
Ftaaaivlrg -aerials Conaentraticn
Calculate regulated limitation
all Lc.50 data available for the whole product according to the tollowIng gotumrig' (Note that units should be
In rng. Pleise provide copies of the sources of this data. Z50 [MA
Durailon
96 hra
Blnsgitl sunfish
1.
Vatrh a ad Minnow
ra '
Rainbow Trout 9 bwa — .
~' 45 Ers
0.4
Dnphnis
Ceriodaptiniat dubia !�8 hYa
xe3.
shetyshead Minnow
Mysid 9hsitnp 96 hz$ 0.9a
Eastern bystar
DSM. Foml 101-M92) 2
6Z/b0'd OV:TT - 86,- z ipf 6TZO-22Z-6T6.Xi?3
3 ' d-W3Q

JUL 02 '98 12:01PM CRROLEEN G�EY'&LORD P. 4
' Busliagtoo Iadastsies CAsoleen Plant �POF-S #: NC t)Ot)6004
Facility Name; _1.440
Choose the lowest LC50 listed above: ;
Enter the LCSD: 0 - r-
if the halt life (H.L-) is less' than 4 days, perio o to0751owing calcrunlat`on.
Regulated Llrrtitat[on = 0.05 x LCSO =
1f ihs hall life (H.L.) is greater roan 4 days or unknown, partorm the tollowlmg calculation. ;
t�apulated LitYt�tation • 0.01 x LC50
s ro date regulated limitallon Irom the Caiculatlons immedlately above and place In thle blank:
Choose tbe pp P
0.0075 mgltiter
From Part It enter the receiving dream concelmtfation:
0100055 ntQ�llter
lv- Analysis.
tt the rgcaiuing atroarn eanceritrallon Is greater than the calculated regulated limtlatlon. than this bloclde is'
unacceptable for use.
E �
Name (Pcfml�
Data
Parson in Raspensible Charge
Form 101 (7192) 3
6T/SO'd Ob:TT 86, Z Inf 6TZO-22Z-6T6:X123
3 ' d-W3Q

JUL 02 '98 12:OiPM CRROLEEN GRI_EY &LORD P,5
i
OUTFALI 001
N¢timata of the total volume of the water handling system between
enter of the biocidal product and NFD%6 dischairge point is based on
th4 volumeof water in the system 44 fcllowu:
®optic Tank 20,000 gallons
Inside sump 7,000 gallons
outside Sump 7,000 gallons
r Wasis,000 aailen„i
00tal Volume 50, 00o gallons
6T/90 'd OV: TT 86, Z Inf 6TZ0-22Z-6%: XP-� 3 8 d-W3Q

yjUL 02 Age 12'0iPM CAROLEEN GALEY &LORD I I I ! P.6
` MATERIAL SAFF-TY pAT4 S EET
PRODUCT
`.. NP•LM 7346 IUCMDBIccnSE
Bmercency ralalshens. Number
Medical (70e) 920.1510 (24 h0urm)
SECTION t PRODUCT IDENTIFICATION
pp igoN: A blffA of Wcgemted eubetituW hydari 0iM
NM 704M/ISMS BAfiMm: 3/3 FLAIM 1/3. FLM2Mn 1'Y 1/1 REwrrjM 0 CMMM
0.71mig + i fjcait I=Sllght IWA6]Mtg 3-Righ 4-Mch=e
BmCT;QN- Z HASARDOYTi3 ZNaRZ;o=ZNTff
= hazed rvaluation-has identified the following ahmilcal ingradi,ant:(s) as .
hazardads urAar• mars HazaM. C=UjjCMtjc0 Mae, 29 CM 193.0.1200, bonsult
section 14 Cor the nature of the bazatd(s) .
3-3 IDI= (S) mmx.%
J.-arcmc�-3—cla=04 16079-98-2 40-70
1, 3 DiCYaL3, 5-dl;;thy]hydat Win 118-32-5 30-40
1, 3-Dida=c� -3-ethyl.-,5-methylhydantoi n 89415-87 2 10-20
VECTI.ON 3 PRLMAUTIOINARY LABIOL INrORNATION
LIANG ; xa=fUl. if MIload. High .1Y Corrosive. causes eya and Skip damage,
xrAtmt%g to nose and tht-04t, Avoid breathing dust. Vim with adequate
vertill�tiart. Do not get into ayss, an skin or clot hire: Wear .xubb0- gloves,
d=lcal goggl" grid fWa WjJQ3A when handling. Wash th rmftdly tft eEr!
kmrdjir4UtWdiately ra ►eve contaminated 'alvthi V arid, wash before reuse.
�caont:aLmrs nay Contain MW%ldl producb, Do riot muse =nt&Lle.
agg prpppxly reconditioned.
$ECTICN 4 BZRST AID IEFOZMTIGPI
LACES: Flush opm immadiataly with plenty of water for at
least 15 minutes- tall a phyeiai4n at: or=.
SI{3N: MmodiatmLy Wipe away use mstarla1. With a dry Clot to while
teMVJg Contaminated Clothing W4 ohm. Undr� a satgy 5bg4W,
wash atfact4d areas th cry with a amounts of watu WA 1
9mpp if available, for at es
Team 15 min + Get im0ediate 1tMAUCA
radical attention. Discard .or dG=nta &at-8 clot-hirg and shags.
aN: �nediately ejive aavp- a glasses of tea =.. Do Mr irdMa votttitir�g.
If vrmLitixir� occurs give f'luu' a again.- Have physician 4atarmim
It Patin s i= aLUowes , induction of widt;.ir�q ore atrian
of stomach, Do not give any ddM by mouth to an =carmiglcm or
PACE 1 Or 8
JY GNE r,1 LCo ciskmR + NA.OIVFiVILLK. iL61 O1 150 80-1 IWO
MA6r_12 rpmIMICAL C=;��r
6T/Z0'd 0V:TT 86,.Z Inf 6TZ0-9-2Z-6T6;XP� 3 ' d-W3Q

• r, JUL 02 '98 12:02RM CAROL -FEN GALEY "JV T9FIALr SAFETY RA`CA PAZET
PaoNcT
NALOO hTA� 7�40
6'margancy relvpha�»® Alurnbee
Medical (70911920.1510124 houh)
SMOTION A Ti LAST AID INFORMATION { CQN'i'INVED
canvu..lsjM perMn • C,,�U imacdiate w4 dieal attenzt �.
M&M=OH: Ra=a fr= area to frasoh air. if not breathiM, oleo;. airday
and start awth-to-mouth Utirictal ira"on ar use a
�_� reayirator. Gd
et ate meal attention, Xf
vJ.r!ti n Ic havim trouble hreathing. tran0p=t to medical Ca
arid, if available, give supplemental oxyW, '
NGTS TG VW=CTM.- 8ascd on the :LrAividual reactions of tho pat*V� , the
ysicianrs judgment should be used to vontxol sjgptoms and clini 1 condition.
'bable mtaosal dAMOO may contnairl UCatO the uss Or gastric IAVMVG.
613CTrCN S HEALTH EFFECTS INFORMATION
pAIINARY W]i'L'i(s) OF EXF0SM.' Eye, Mon, 1rhalation
En m! can causa aavwra irritation. Corr'osivla to tha ayaz
with possibla pet anent damaga depazding on the
1�tgM of expasura tsW an the first • aid action giyw,
SIMT T: Can cause .severe! irritation. cozr=ive to the kin with
,possible pemwmnt damage deperAinq : Qn the lareth of
exposure on the first did actionqiiVM, Q-91. ;cause
&UP,rga a contact derznatitig 3 tl a individuals.
Can cause sevens respiratory ion Can be '
caa�iva to t ho ==us and the luzVd.
Can cause an allMic Mction in eusceptible_individuals.
SDW=z or EMSUPZ: A review of available data does not ide ti,fy any
f= exposure riot previously nentiat)ed.
i� any worsanirlg of eXisti�Tlg:coAt�di ons.iw of avai.lablQ delta does not
JdV*BECTIOZJ 6 TQ:KICCLOGY INFOPMTXOK
ACC]TE 'i,1 CITY E'I'I7DIE5 t Antos t�oxirity etudiss have been ccrAucted
on this product. Ths results a>:e anaHm below.
ACT.t'L ORAL mxicLTSt (AiBIM RATS) ; W50 = 468 11g/k9
PRIMARY s= rauT*r cN T= (ArbnM RADHrrs) : Carroaiva
FRIMM EYE TF71!MATMN TEST (AI.a= PABsns) . Carroaiva
PAGE Z OF 8
NALGO ONIAM1CAU C93MFIANY ONE NALGO CENTLR w
nnPA "IMn-Inn-1 nnrz
6T/80'd Tb:TT 86, Z inf 6TZ0-22Z-6T6:XP3 3,' d-W39
11gig

JL L 02 ' 98 12 a o?-pm CAROLER4 GALEY &LORD
P.g
MATERIAL SAFETY DAT $al �T
PRODUCT
#44.
N A t-C O M= 7346 MOROB:10 E
Emefooncy Telophaile Nurnb,ar ;
Madloat tMa) 920-151 O (24 hQUP)
sZCTroN 7 PHYSY= ANb cxEM;CAL PROPERTIES
coUM: White ' • ]?i7Rt+i: iquatta� ASS Fr70 t
Pi f lei molutian) T thm 1.0 a 77 Degreos F AMN D•-1390
SPa C c hvm: AMM U-21-117
SING pond: 248 - 296 DogrMs C A= r -93
FLASH Foint 329 Dogrees F' (PA9CC)
EVAPa=QN R1 'E Less than AMM D1901!
(Ethar
EY Vim: 7OMA thzn 0.5
NO► 1 nesa physical ties are typical values fOr this pr'cxhtct.i
nEQ�ZtiN 6 FSA$ ANf� MXPLOSIO i INFORMATION
rUm p©in: 329 Degree F (F ) X=4 D-93
Mo=st= MIA! Based on tha NM guide. e dty chemi mll fcadt, carbon
diaodde or,other ��$� agent suiuse
for Cl.sss A firm, Use water to
coal mntalnwg to fire. - For large Liar,. U" water spray of fog,
thoroughly dreru-hirq the b=rjM naiarial.. Wnar self-car*ained respizatotY
SECTION 9 REACTIVITY INFORMATION
INOUGAT32I tTY: Avoid oxidizable mixt=Q, hydrates aril 'water. Chenidtl Mzard
at -Ong oo
ridizing agent. Avoid contact of heat product with oarganmc materials.
Mix only with water in an appzo� feeding ��• dsa clean dry 0 i1s-
po not a this prodlAct to ar�y dispensir device CA rests; of any
Zej(rc5,s,fo'n".�Cc-ntaMin4tiOn
Such =a may cause a vio exit r ion loa to tir9 with mcist� organic matter, of 0 er cheaaicalc may
start a chemical rear ion with genarat .on of heat, liberation of haf zdous
9- and possible generation of fire re and exploMn. In c=o of c0nt=1i=tivn
or d aeo well � t xd Cpnpltl0000d with 1 v11�s off vra te � in
o�
�ce;�Y•
S=p=: Avoid high twrpwat=mt dirwt Sunlight and moiSture.
f �De�i�ng �u�ida�ified gtmvpe=a twsz above 32.9 17egVe" k!
SECTION 19 PERSONAL PROTECTION SQUIPHPNT
RF. �IRAn1RY PRa.U=ON: 1 pfratoa:y prob�oti.on nnti na liX newed., If;
ME3OF8
ues.r_n c1.1WMjr-AL. eoerlPAN"r QN9 NALCD GONTUn •
ILLIN910 SUPOW-1 Ka®
6T/60•d TV:TT 86, Z Tpf 6TL0-22Z-6T6:XP3 -3 ' d-W39

r ILL e2 ►98 12'-02PM CARa-EEN GALEY & IiDA�'EF�ll�l. AFETY DA'jrA oNaET
JoA4
bit ALC O
PRODUCT
NA= 7346 1
E�arpenayTe1e hand Number
Medical (7001020-1510 (14POUR
OFCTION 1.0 pERSQUIL pROTECTTON EQU17HE 1T
I ;co1�TTN�p )
we= eithSr a dlt7Qai�la dtsa� mask cr a ct�l�:ridg�
$ignifi mnt dusting i =5Cr I high e�icienc`Y cartridge.
respirator with yr
ills, large? ta4Or vessels or epclosmlL �
For large to vla'ft lati017� jnto a yrezmxe;-d sj rr3se �-rontajnad
With �droao¢�at�'•
"VPmtus
VZrj=ATzoN t If gigaficant dust -irk
pOcu'rs' loca3 ea�latfgt vonUUtjon in
r��• •
pWiECrM 'q': Wear inpureable g1mes, boat 8i pprcm w a 51j k, suit
Cne=c
�G 11V01� S}tiT� C011tdGt• a l goggles " face w are also teC�•
Tte av,�Lilability of an eye Wa& fOUntZin and Saf6t-y shU48
Lf s =ntamiNted, �a cl•oti;•in4 and tl�orquo y wash the ef=hp
If olotAW-er can#�mamWore rouse.
awrclta a1othirig se
SECTION 11 SPILL An DISTOSAL jjjFOpQATION
IN CA9 OF �=SPO fig• CAGE M FOLLCJWING 24-H�m
,MpR�bm ZtLMM (708-920-1510)
Sam 03NI'ROL mu R
Solid spills.. sweep or vao= up W.4 reclaim into re�cavery or salvage drut�t�6
jCr -di Wear e prota=ive e��t qD&_ in
�5re�ion 10. Refer to
A��th
tion l4,
Tis � is tcxifish,�, ayes � �z3� �1.3uUy �'�
irlto ���
gzSp0=—. Xf this product bo=m a warts► it meets theigrl a of axy Act
ba=jcus Waste as dafined order the Res == Can -'mot
(gyp,) 40 CFR 261. H*Zazdau» wastes D00"
As _a hazazdeu3 solid wa$te� it must lea disposed of in a lid Hazardous
Waste$ Treatment, Stargge and Disposal facility in a� with local►
stlAt,'O and t®dexal requlatiOns.
SECTION 12 zNVTA0NMENVAL INFOIiM,ATION
An or
This praduct im toxic to fir�h. Do rot c3iscl�arga �t:o� s*conrt� :b Y�
public water unless in aecasdancA with NMIM P�
PAGE 4 Or 0
NA1.012 llRMICAL C13MPANY pNL FINAL hP .�ns.1p� • r�APE•RVIL.LE. IL.
t.
6T/QT'd ZV:TT 86, Z Inf 6TZO-22Z-6T6:Xp3
198
3 ' d-W3Q

Jul W "�19 1p-03PM CARC)LEEN GALEY &LORD
P.10
MATERIAL SAFE- Y DAT4 SHEET
P4'.,
NALCO
PROOUGT
madlca1
NAACO 7346
n• Number
G(�4hours)
sEc%ZQN 12 mmXAQmmTA&
t CONTINUED-)
DO not cmtamimte water try cleaning of tm*Ainas
Rscji01�a1 Office of the, FAA. rode ant as spac died an
aanndd zpmeriC or di,�osal. oD vrast�.+. �ZY ` � X
Aq=TC DM'- gesults below arc based on =8 Product.
9B how �Ir_atia ac� T rl�o to Bluagill smf ish = 1.2 PAm
96 ha= static acute L60 to Fathiad M1rr�ow = 0.71
PPM
96 hour stAtic amto WSO to Rainbow Trout m ot• S ppm
48 hour' 6tatia acut�m i�d to paphnia = 06 d m a 0.15 pplit
48 boos static acute.S.CSo to Cariccb h 1.6 ppm
96 hour static acute I,CSa to Shaep� 1.
98 h= static acute 1�o to NYBid mw
96 hoar static acuta =0 to Sastarn OX = 0.98
mm
AQW7C I=&'- Ruts be].aw era bm#s cn dahalogor►atd XCkC .
(5, S-climekl�Ylhyr]an�°ixlj ..
t 6,100 MIL
- 96 hour' vatic ac0,� I�So to .� T� 48 has; static �t LC'50 to Dapinzia - J.,300 mg/L ,
96 bosh static acute 100 to pithead Mi.Tl M = 8,100 7cg/L
96 ham' static adta =0 to S ve*ead XiMOV - 13,300 ng/L
96 h= static- 4ete-1=0 tO Grass Slw'RV ' 12100o n41L -
96 hour static aauto W50 to American Oyster = 14;200 mg/L
If t1lease
into the arivirorrrmnt, see CEp=A in Section 3A .
8DCT10H i� �►a,�isPoitTy►TSQ22 =1aFORMATTQkt .
RaT MPkR SHiFPM i 'g+I� CODE - Oox= 1470
, N.O.S.
r���nan�l, s, � Drams, 5-nt
sZeTTON 14 REGULATORY 121POMTXON
r atiOrm sPPLY to .this prcduCt-
T� tollvWilx� �. .
Based on o= hazard mraluation, the follcwfrg ingr di,en,is in.this P *duct aso
PA(Z5OF8
• NAPEP
.._. ,.,.. e.u�ufr►A1 rM rrlCaluV MNP NALCO CENT�Fi
6Z/TI'd ZV:TT 86, Z inf 6TN-22Z-6T6:Xp3
3 ' d-W39
Ion

ii
JUL 02 '98 12� e3P�1 CFIROLEFJ`! GALE1 &l40_ � �R1AL SAFETY QA rl r-ET
PP4
IOIALC O
PRODUCT
NM= 7346
Smorgency Tele hone NiirnbeY
Modl4al (708) 9�G-1s1 O (�4 hau�e�
NUED
SDCTIOM i4 ANG=TORY INPO1tMATxON ( ONT-----
hazardcug ard the reasons are stlarm below.
i
ty�zrtoir - Corrosive, oxidizer
1, 3-Did-Toro-•5, p'Dimethylhydantoin = 'TM 0.2 mgjm9, 5r M 0.4 elm
��t/Trav
1, 3-DichlorCrS r 5-DiMthy3hydantoin ■ TM 0.2 'ttt /M2 # SM 0.4 mg/m9
K mufaCtlr: Qr, s reca=andat10n
;S•�thlri� �QT1 hy�l9rit'AiYI a 0.2 It1�J�
V=Ufactu� a
CM%=A/=fMWQM, 40 CM 117► 302:
Nabificati.on of spills at this product is not required.
AM RJMWVWXZA Off ACT or. 1980
(Tm= Yiz) — SI=ONS 302, 311, m AND 313:
SEIC (RI 302 — EaPIZ EGY H7MOUS SUWrANCE'S (40 CM 355) ; ` ,
is podgy does not oontm4n ingre,dierlts 3,tgted in �x A and B as an
Exh=in*ly H4zardrus sobatance. '
5=ONS 311. and 312 MAT�iIATa SA�'Y L1�A (40 � 370) ;
our 1==td evaluatL= has four,d tnifs proms to be nazaraous. 1#,e prOdur-t
ffihaxld be reported under the following EPA hazard cat .g=ies:
XC Mmediate {a=te) realth hazard
— Aelayed (ohro=nia) health hazard ;
xX Firs bAu r'd
— & ddeA raja= of press= MZa� �
-- pactive hazard
S=ON 31n - i,IST Or MXIC GIMCCAT S (40 CFR 372) :
This pr*h=t dMS not contain ingredients on the List of. '!.brio Chenuaalt.
TO)ac mwfANCM M--M AL AM (TSM)
ntia prodwt i.s exmptod under T= and ragulatod timder FZM- =0
rota are on the Lwig ntary List.
iF,L II151' .CCSDD, 3GICIDT m PA m=CIDE Am (INFRA) = i
i
PAGE 5 OF S
• i i
i
i
NALCO CNI3MiCAL COMPANY CN8 NALGO CENT' IR # NAP�RVILL9, 1LL1 Q1� OMEiC-i idE3
ARC!'A 70M-MCM-I C CQ
6WT *d ZV: TT 86, Z Inr 6TZ0-22&6T6: XP3 3 ' d-W3Q

jUj_ 82 '98 12-.g4PM CFAOLM GALEY &LORD ; F. 2
MATERIAL SAFFEiY DATA S ERY
4 PRODUCT
NALGO r o �3 .
7rszc�oaz >�
Emergenoy�"6140119"a Number
Medlad (WSJ 920-i 5i 0 w Mrs)
SNCTIQii 14 1tEC1=XT0RY Y111?0VMAT;10Xt ( adNTx210NA )
EPIA Rom. I$0. 38905-12-1706' `, US prpd=t is registwed for vm as a
]�s�etr00>:ga1716►tt cmtxal chemical used in Idust rial r*Qix=1atirxg arm
gyt3t8Zltg aix washer
Ina�. c �1OW J � � thewhen used � IW-'Q
;0t3faCE =SERVAMON AND yZmVERY ACT (1:tI:i2A), 40 CAR 261 S[)B>:'M C &' Di
Car�ult gveation 1-t far RMA, elaaaificKti.on.
FMMQL R FC?I,=CH CDNTML ACTT CxLEM YID► M ACT, 40 CM 401,151 ;
tom c if I:�ea# g07ediarts aria a40 CFR pwificic l,Y ate•
I7one oP i.Y1s ,
CLUM AIR A= W, 111 (40 CFR 00) , sac. 112 (40 cm 61, 1990 r-*z) t
Thas Product dues not mntain h r*djents Mvgred 13Y tha Clan Air Act,.
� PF�iPGS�MON 66:
This product does not contain any chcd ais which rWtiY'e warning under
0a1,.ifcrsia proposition 65.
NICMQW CRMM' MATERIUS' CriticalThis pdu&es donot. M*Ain ing'r en s listed en the Michigan
Mat�3:s Regis. ;
s %= MMU TO 140W IMM ! tram : $�3ta Right to Knowduct iS a registered biocide and is exec
MVEM=c , z�xcx�s s
Mlis P=duct is a x-egi slrersd bi oaids WA is a=gpt tram wlas under me HMISR
of OMM= of Camda E.M C-70.
SECTION 1S AMITIONAL INFORMATION
Mato int*ma1 number LQN042291 '
8�q'�ION 18 USER'S RE5FQV9XBYLITY
This preduot met=Ul safety data OhMh crv' des health. and Mfet
inf'o�tion. �Ihe duct is to be U "d in applications; oo s3isteat w-1#h
our prQduat literature. individuals � + Pit sr� �:
itiforased of the reccm�wred safety precazttions and hr�uld ha
PAGE 7 or A
i
A. #.,on&rnwwuv nr.io ruai rr1 r.FN78A9 s NARMFIVILLM ILL1N019 80 60-1166
6T/�T 'd ZV: TT 86, L Inf- 6TL0-�2L-6T61 x1e3 3 ' d-W3Q

P.13
• jUL g2 ?98 12124PM CAROLEEN eRLer -{UAT RtAL SAFETYDATA
PRODUCT.
[�1 A 1..0 C7 r�,r�aa 734� r
finergenoY Tolophant N&mber
M1ajC;Ai (o8) 2204 510 (24,11aurs)
SECTION 16 USER'S RM57oNsIBILITY (, coN'xsHCfFD )
to this We nratien. For any othm usmal expc=OS shoWA ba eval ted
se txiat app=priata han lirjg practices and t,rairdN can jfi
"tafished to ensure safe Y+vtC}claar�tians. lsa�e ocnvlult yo:sr
local sales representative for any ir�ormmatiors.
SECTION 17 BIBLIOGRAPHY
Al�n�iiA4L RM2= ON fCCbam, u.s_ r*par of Health mid
Servicre�,
Public Health SeXvim, pB 33-135859, 1983:
UM Sa9IC gcxjmc� off'. PO2ECASt Doul1., S.,
D �as17d Adlmir� Mom. O, . ads-
N. Y,, Znd G ticm, 1980.
CfffI+ = IMZARDS OF fnM Womat=r proctor, N. H., and Fi ghesr LT - ?• r WS. r
1. p. I.ipincx>h Crn =M--. N.Y. , 1981-
iq=ms Or 7timsom mum=B, Sari N, Itvim: ed•, Van
Na�sarid old Y, N.it:, sth edition,. -1984. .
MW ICNd M.M C.9 MM EV==CN Or M CAirCa OGMC: R15K OF C3=, CAW
M MAN, GPl m; world Health prjanizatian t n*A= atiorm1 Agency f cA-
march Oil Cancer, 1972-1977.
pAxyl.'Y'& 7i`iW=RLU MGIENE AND MXIOQLAGY, ClaytOnt G. D. , Claytony P.. E. r
oz., John Wiley and Sans, N. Y., 3rd editien, Vol. 2 A-Cr 1981. ;
pMISM Or rjo= M7=S ON MWCAL svesWCffi, v's. Ltl t t
Health and Human Services, Public Health Service, Cer%:r for Di
seake
control, National lnstituta for Ccaupation&l Safety and Health, I-St3
aupplw,mt of 198i^1982 edition, Vol. 1-31.- CHI 2924.
Title 29 Code CL' TWOXal Ptagaati=-A part igloo SulTart Z, Toxic am
zardaus Substances, r ational Safety and Malthrttin
:Ad
H�aistratio2i
THRE LD MMIT 'VALUES IM CHEMCAL SU55TANCES AND PfiYSYCAL ACC IN q
wdRK = mwnwm=W= Dn=m , Americanen
i Conferan of�
ci,cQ_ ,�.+� Trdustrial KygieniatA, ON.
rpmBY: Ricky A. Stack %=8 VrM-,, TmdC01 i5b
DAB aIA=j 11/06/92 nATE PR : 05/27/93
PAGE 8OF8
NALGO frHl3MMAL COMPANY ONE NALGO PON""919 f1ApERvtLLL. 11 Llrv0t6 ��e 119E3
6T/VT'd ZV:TT 86, Z int 6TZO-22Z-6Z6.:XP� 3 ' d-W3Q

A 62 '98 12:05pM CAROLEEN GALEY &LOM P.1a
L
peca Fa -tor N lQo 7346
The decay factor for Nalco 7346 was providAd by R. A. StackhQase,
Toxicologist, Nalco Chemical Company. Mr. StacXhousa can be
reached at [phone]. ;
I
6T/ST 'd ZV: TT 86, z Inf 6TZ0-9-L-6%: xPA 3 ' d-W3Q

t . i
NI'DES PERMIT APPLICATION - SHORT FORM C
To be filed only by persons engaged in manufacturing and mtning
N."C. Department of Environment and Natural Resources
Division of 'Water Quality / NPDES Unit
P. 0.13ox 29535, Raleigh, NC 2767-6-0535
Please print or type
1. Applicant and facility producing discharge
A. Name. fey & I,ord .Xndustries, Inc. - Caroleen Plant
B. Mailing address of applicant--
1. Street addressIr , P.O. BOX 158
2. City Caroleen 3, County 1tutherford
4. State M 5. Zip Code 2W19
C. Location of facility:
1. Street U-S- y 221-A
2. City-Caroleen 3. County lh�therford
4. State W, 5. Zip Code, 28019
D. Telephone Number (704 ) 657-63761244
E. Fax Number (704 ) 657-6376 XMG _
2. Standard Industrial Classification (SIC) code(s): 2281
3. Number of employees: 175
4. Principal product(s) produced: Yarn
Principal raw material(s) consumed Cottoa 6 93ntheti.c fiber
S. Principal process(es): Yara T8324acturiM
6. Amount of principal product produced or raw material consumed
(r :cf .n f!�nnrs rnnxwmed andfor units of nradawliaal_
rod, Produced
Raw a ansumed
(AV EPAGE)
Product Produced r
Raw Matenal Consumed
(PEAK)
er Day
63,318 lbs.
73,590 lbs. roduced
per Month
J,848,869 lbs.
2,526,943 lbs. yarn produced
per Year
1 600,000 lbs.
22,187,0W 1b. yam pioduced
7.. (a) Check here if discharge occurs all year ® , or
(b) Circle the month(s) in which discharge occurs: January February March April
May Jurie July August Septethber October November Dec6mber
(c) Days per week dis0i%rgc occurs: Hmday - Friday
NOTE: If the facility has separate discharge points,(outfalls) or multiple industrial processes, incli de a
schematic diagram of wastewater flow at the facility.
Short Form C Version 9-97
6T/9T'd 89:TT 86, Z Inr 6TZ0-22Z-6T6:X12.3 3 '8 d-W3Q

NP17ES PERMIT APPLICATION, SHORT FORM C
To he filed only by persons engaged in manufacturing and min g
B. Types of wastewater discharged to surface waters only (check as applicable).
DisLa
Vo ume tr
charge per operating dFlow ay (GALLONS PER OPERATING DAY)
Sanitary = daily average 100
+ boiler blo xWm 9608
Coo ing water, etc. - dai y average 1719 0
(6 coolang towers) .
process water - daily average 0 0
Maximum per operating day for 13,170
total discharge (all types)
A
9. If any of the types of wastewater identified in item S (either treated or untreated) are discharged to
places other than surface waters, record the amount(s) discharged below: K/A
A. Municipal sewer system,l
13. Underground well —mod
C. Septic tank d
p. Evaporation lagoon or pond_ end
E. Other, specify
10. Number of separate discharge points'-
2
. 11. Name of receiving waters}-
Second.Broad River
12. roes your discharge contain or is it passible for your discharge to 7 contain one or more ofthe following
substances added as a result of your operations, activities, or processes. Circle all that apply;
aluminum ammonia beryllium cadmiurn chromium lorine (residual
copper cyanide lead mercury nickel oil and grease
phenols selenium zinc
None of the above
I certify that l am familiar witli the information contained in the application and that to the best of my
knowledge and belief such information is true, complete, and accurate -
Edwin W. Horton Director of Engineering
Printed name of Person Signing Title
Signature of Applicant
uate
_� S`/ I
North Carolina General Statute 143-215,6 (b)(2) provides that: Any person who knowingly makes any false statement
representation, or certification in any application, "record, report; plan, or other document files or required to be maintained
under Article 21 or regulations of the Environmental Management Conurtission implementing that Article, or who falsifies,
tampers with, or knowly renders inaccurate any recording or monitoring device or method required to be operated or
maintained under Article 21 or regulations of the Environmental Managernnent Commission implementing that Article, shall be
ilty of .n;sdemeanor pur+ishable bya fine not to exceed $10,000, or by imprisonment not to exceed Six months, o by both.
I S.C. Section 1001 provides a punishment by a fine of not more than sl0,000 or imprisonment not'more than 5 ears, or
both, for a similar offense.)
Version 9-97
Short Form C
6T/ZT'd 8b:TT 86, Z ipf 6TZ0-�2Z-6T6:XPJ 3 2 d-W3Q

rn
0
M
M
N
61
pl
X
rd
w
06
a.
w
A
�-- US 221 A
Stomywater Drains . • - -- • • • G...........
A
13- :. o
o..:.......... ...... EI.; ....:....:.-.p-
4�
y Uq2
NPDES ��-----
Soiler
Sheet Runoff
Runoff
Seoond Broad River —
�U
DATE: fvtaY 1989
P,I-ro: NO.: '10Ut79a
.B ensiriger & GarrqInc..
Environmental, gCALE: Not to Saalo
DRAWN BY: palnY Lord
FILE: Cynowon Plant NPD@9
Bluefield. Engineering, P.C.
001
Oil
NPDES
Galey & Lord - Caroleen Plant
Caroleen, NC

� - r
COOLING TOWERS
(6 TOWERS TOTAL)
l 1271.9 gpd (ave.)
NPDES OUTFALL 002
FDOUTSTIC WASTEWATER
& BOILER DLOWDO"
SANITARYMM
1.
Septic tank
2-
Holding tank
3.
Dosiiag tank .
3.
Sand Filters
4.
Chlorinator
5.
Dechlorinator
9,608 gpd (ave.)
NPDLS OUTF,ALL 001
Bcasinger & Garrison FIGURE 2 - NPDES Discharge Process Flow
Environmental, Inc. Diagram
Bluefield Engineering, P.C. Galey & Lord
SCALE: Not to Scale
pR0J60TNO.; 100698 Caroleen Plant
DATE: Ni2y'1ees
DRAWN ev: RES Caroleen, North Carolina -
FILE: Gaffey a LON - camlcl*n raaoHs
Fig =
6I/61-'d 6b:Iti 86, z Inr 6Tz0-i2&6T6;Xp3 3 8 d-W3Q

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary'
A. Preston Howard, Jr., P.E., Director
0 UNA
.9
IT41
00
IDEHNFzI
Division of Water Quality
Environmental Sciences Branch
4401 Reedy Creek Road
Raleigh, N.C. 27607
FAX:(919) 733=9959
Date S�
FAX TO: FAX NUMBER: 70 1v,5-7. 43 ,6
exf, aVo
FROM: Meci -55a %lose b ro C
PHONE: I q- 7 33, 13 G
NO. OF PAGES INCLUDING THIS SHEET:
Gzae�a� coda-c.�t msa5 �d �e�_-e�,
49
Environmental -Sciences Branch 4401 Reedy Creek Road Raleigh, North Carolina 27607
Telephone [phone] -FAX # [phone]
An Equal Opportunity Affirmative Action Employer 501% recycled/10% post consumer paper

Facility Name:
NPDES #: NC
BIOCIDE/CHEM[CAL TREATMENT
WORKSHEET-FORM 101
The following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
North Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
returned with all appropriate data entered into the designated areas with calculations performed as indicated.
I. Facility Name
NPDES # NC Outfall #
County
Receiving Stream 7Q10 (cfs)
(All above information supplied by the Division of Water Quality)
What is the Average Daily Discharge (A.D.D.) volume of the water handling systems to the receiving water body?
A.D.D. = (in M.G.D.)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
(A.D.D.) X 100 _ ( ) X 100 _
IWC = (7Q 10) (0.646) + (A.D.D) — ( )(0.646) + %
This value (IWC) represents the waste concentration to the receiving stream during low flow conditions.
What is the name of the whole product chemical treatment proposed for use in the discharge identified in Part I?
Please list the active ingredients and percent composition:
°
What feed or dosage rate (D.R.) is used in this application? The units must be converted to maximum grams
of whole product used in a 24hr period.
D.R.= grams/24hr period
Please note, fluid ounces (a volume) must be converted to grams (a mass). The formula for this conversion is:
Grams of product = fluid oz. of product X 1 gal. water X 8.34 Ibs. X specific gravity of product X 453.59 a.
128 fl. oz. 1 gal. water 1 lb.
D.W.Q. Form 101 (2/95) 1

Facility Name: NPDES #: NC
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for this estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.)
Volume= million gallons
What is the pH of the handling system prior to biocide addition? If unknown, enter N/A.
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk. The
degradation must be stated at pH level within 1/2 pH standard unit within handling system. Enter the half life (Half
Life is the time required for the initial product to degrade to half of its original concentration). Please provide
copies of the sources of this data.
H.L. = Days
The decay rate is equal to H1L X 0.69 = =Decay Rate (D.K.)
Calculate degradation factor (D.F.). This is the first order loss coefficient.
D.F. _ (�o) + (D.K.)
Calculate Steady State Discharge Concentration:
Dischg Conc. _ ( (D.F.)(Vollume)(3785) _ ( ) ( ) ) (3 7 8 5) = mg/I
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischg. Conc.) x (IWC%) __ ( ) x ( ) _ mg/I
100 100
Receiving Stream Concentration
III. Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be in
mg/1). Please provide copies of the sources of this data.
Organism Test Duration LC50 (mg4)
D.M.Q. Form 101 (2/95) 2

Facility Name: NPDES #: N
Choose the lowest LC50 listed above:
Enter the LC50:
If the half life (H.L.) is less than 4 days, perform the following calculation.
Regulated Limitation = 0.05 x LC50 = mg/I
If the half life (H.L.) is greater than or equal to 4 days or unknown, perform the following calculation.
Regulated Limitation = 0.01 x LC50 = mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
mg/liter
From Part II enter the receiving stream concentration:
mg/liter
IV. Analysis.
If the receiving stream concentration is greater than the calculated regulated limitation, then this biocide is
unacceptable for use.
Name (Print)
Signature Date
Person in Responsible Charge
Person Completing This Worksheet Date
(If Different From Above)
D.W.Q. Form 101 (2/95) 3

Facility Name:
NPDES #: N
Supplemental Metals Analysis
If copper, zinc, or chromium are present in the proposed biocidal compound, complete this worksheet. A separate form
must be used for each metal and/or metal compound present in the biocide. List the metal, its chemical formula, molecular
weight (MW), formula weight (FW), and the concentration of the metal compound in the biocide (MCC). Complete a
separate form for every metal present in the biocide.
Metal
EXAMPLE
Copper
Chemical Formula Molecular Weight of Metal Formula Weight Concentration in Biocide
CuSO4 5H20 63.546 g/mole 249.680 g/mole 0.2 %
Dosage rate of Biocide (DR) (from page 1):
DR = prams/day
Average Daily Discharge (ADD) (from page 1):
ADD = million gallons/day
Discharge Concentration (DC) of Biocide:
DC = DR _ ( grams /day) _ grams/million gallons
ADD — ( million gallons/day)
Convert DC to micrograms/liter (ppb):
DC (µg/1) = DC (grams/million gal) x 3.785 x110
/ 1061ters//miglion gal. ug/I
Calculate the fraction of metal in the metal -containing compound (MF):
MF = MN — ( grams/mole) _
FW — ( grams/mole)
Calculate the fraction of metal in the biocidal compound (BF):
BF = MF x MCC % —
100
x
(100)
Calculate the concentration of metal in the discharge (M):
M = DC BF = ug/I x
Calculate the instream metal concentration (IMC) at low -flow conditions:
IMC = M x IW00% = ug/I x 100 % = ug/I
Regulated limitation of metal (from below): ug/I
C General Statutes 15A NCAC 213.0211 define:
Copper- 7 µg/I water quality action level* Zinc- 50 µg/I water quality action level*
Chromium- 50 µg/I water quality standard
(*Values which exceed action levels must be addressed directly by aquatic toxicity testing.)
D.W.Q. Form 101 (2/95) 4

FEB 2 31993
LJ
February 19, 1993
PHILIP H. KLEIN
BURLINGTON IND., CAROLEEN
PO BOX 158
CAROLEEN, NC 28019
Subject: NPDES PERMIT NO. NC0006009
RUTHERFORD COUNTY
Dear Permittee:
The subject permit issued on 6/28/90 expires on 11/30/93. North
Carolina General Statute (NCGS) 143-215.1(c) requires that an
application for permit renewal be filed at least 180 days prior to the
expiration date. As of the date of this letter, the Division of
Environmental Management had not received an application for renewal.
If operation of a discharge or waste treatment facility is to occur
after the permit's expiration,date, or if continuation of the permit is
desired, it must not be allowed to expire. A renewal request must be
submitted no later than 180 days prior to the permit's expiration date.
Operation of the waste treatment works or continuation'of a discharge
after the expiration date would constitute a violation of NCGS 143-215.1
and could result in assessment of civil penalties of up to $10,000 per
day. If continuation of the permit is desired, failure to request
renewal at least 180 days priok to expiration will result in a civil
assessment of at least $250.00; larger penalties may be assessed
depending upon the delinquency of the request.
A renewal application shall consist of the following information:
1. A letter requesting the renewal.
2. The completed application form (copy attached), signed and
submitted in triplicate, referenced in Title 15 of North Carolina
Administrative Code (15A NCAC) Subchapter 2I1 .0105(a).
3. A processing fee (see attached schedule)- in accordance with 15A
NCAC 2H .0105(b). The application processing fee is based on the
design or permitted flow, whichever is appropriate, listed in the
first categories of facilities.
4. Primary industries listed in Appendix A of Title 40 of the
Code of Federal Regulations, Part 122 shall also submit a
priority pollutant analysis in accordance with Part 122.21.

5. Facilities which have not been constructed within the last
permit cycle and are therefore, considered "new" facilities,
shall also submit an Engineering Alternatives Analysis,
referenced in 15A NCAC Subchapter 2H .0103 and Subchapter
2B .0201(c).
6. If the facility covered by this permit contains some type .of
treatment works, a narrative description of the sludge management
plan must be submitted with -the application for the renewal.
In addition to penalities referenced above, a permit renewal
request received after the expiration date will be considered as
a new application and will require the higher application fee..
15A NCAC 2H .0105(b)(2) requires payment of an annual
Administrative and Compliance Monitoring fee for most permitted
facilities. You will be billed separately for that fee (if
applicable), after your permit is approved.
The letter requesting renewal, the completed Permit application,
and appropriate fee should be sent to:
Permits and Engineering Unit
Division of Environmental Management
Post Office Box 29535
Raleigh, North Carolina 27626-0535
The check should be made payable to the North,Carolina Department'of
Environment, Health, and Natural Resources which may be abbreviated as
DEHNR.
If there are questions or a need for additional information
regarding the permit renewal procedure, please contact me or any
individual in the NPDES Group at telephone number [phone].
Sincerely,
Original -Signed By. l
Coleen H. S60W
Coleen Sullins, P.E.
Supervisor, NPDES Permits Group
cc:shretilte�Reg►ona�l4 icy
Permits and Engineering Unit
Central Files

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office .
0
A 'F4
00% 00W% Nook
I DEHNF1
WATER QUALITY SECTION
December 16, 1993
Mr. Phillip H. Klein
Director of Engineering
Burlington Industries , Inc.
Post Office Box 21207
Greensboro, North Carolina 27420
Subject: Compliance Evaluation Inspection
Status : In -Compliance
Burlington Industries
Caroleen Plant
Wastewater Treatment Facility
NPDES Permit Number NC0006009
rtord County
Dear Mr. Klein:
.An inspection of the wastewater treatment system serving
Burlington Industries Caroleen Plant was conducted on November 17,
1993. Based .upon observations made �and results of samples
collected, the system was judged to be in compliance with its NPDES
Permit Number NC0006009. A copy of the inspection report and,
laboratory analysis is enclosed for your records.
Review of monthly monitoring data submitted by the facility from
November 1992 thru October 1993, indicate the facility to be in
compliance with their monthly average limits.
Mr. Sam McKinney and Mr. Jake Wilson's time and assistance in
conducting the inspection is appreciated. It was a pleasure to
visit your facility and find it so well maintained and operated. If
there are any questions concerning this report or if I can be of
assistance, please contact me at 704/251-6208 .
Sincerely,
Donald R. Price
Wastewater Consultant
Enclosure
xc: Jake Wilson
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

1 J0
Unked States,Environmental Protection Agency
Washington, D. C. 20460
EPA NPDES Compliance Inspection Report
Form Approved
OMB No. 2040-0003
Approval Expires ,_3;_$5
Section A: National Data System Coding
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1U l JfJJC1010101 &1016117 11- 1lg'1311 Id,11A 17
Remarks
I -
Reserved facility Evaluation Rating
6A I -1 J 69 ; 7� , ;
81 GA ------ -------- Reserved --- i __ _ 66
71u ; : 7k�] .. .: 7k-, LJ 74 <.- ]ol .I I I: 1 I : 180 s.. , -•:_
Section B: Facility Data .
Name and :Location of Facility Inspected 1
Bur /;v`y � Oti. Zt��r4 5 f �/`�S' � C-{ � 0 leek T /tE H
Entry Ime
AM ❑ PM
/� t
Permit Effective Date
� u , / 1%,90
Exit Time/Date
Permit' lration Date, .
Dp O
/, , ,BO x ls�
Cav'o/ee.vt N�C, 2 �O/9
'.
%•Z;;�tJ y3 // /
/I/od, �o /9y3 `
Name(s) of On -Site Representatives)
Title(s)
'Phone No(s)
Name, Address of Responsible Official
,Nrk%rwJ iju✓1,+�t0�... ��
TitI
�/ EG�OV/ . 0T IAIec,r ►'�
Phone No. =`
Contacted
6V-ee�s bo oZ .2
l / 37 �-.2
P Yas 12 No
Section C: Areas Evaluated During Inspection
(S = Satisfactory, M = Marginal, U = Unsatisfactory, N='Not Evaluated)
Permit
Records/Reports
Facility Site Review
S
Flow Measurement
.Laboratory
Effluent/Receiving Waters
Pretreatment
Compliance°Schedules
Self -Monitoring Program
Operations & Maintenance
S(udge''Disposal
Other: .
S
s .
j
Section D: Summary- of Findings/Comments (Attach additional sheets ff necessary) '
Perl�,�- w,t -
S�►� I� pesk % f
11,9J
800. 3� J�/L
.2 3 /L Ore-ra k �►-rek-
TS 5 34 /L
�
� f w•y /�: a� w� l/ rn�,k fG , ih ��
fec6./. ;Zoo/oD
��►
ry OY
/Ocifi?� ,Sp
Nam (s) and Sig*hature(s) of Inspector(s)
Agency/Office/Telephone
Date
' 492Og
42 16--/3..-
ure f Review r
Agency/Office ,
Date
Regulatory,Office Use Only
Action Taken
Date
Com lance tatus
❑
Non m.Iiance
Compliance
'PA Form 3560-3 (Rev. 3-85) Previous editions'are obsolete

INSTRUCTIONS
Section A: National Data System Coding (i.e., P.CS)
Column 1: Transaction Code: Use N, C, or'D for New, Change, or Delete. All inspections will be new
unless there is an error in the data entered. -
Columns 3-11: NPDES Permit'No. Enter the facility's NPDES permit number. (Use the Remarks
columns to record the State permit number, if necessary.)
Columns 12-17: Inspection :Date. Insert the date -entry was made into the facility. Use the
year/month/day format (e,g., 82/06/30 = June 30, 1982).
Column 18: Inspection:Type. Use one of the codes listed below to describe the type of inspection::;
._A _ —..Performance. Audit E_—Corps_of.Erigrs-Inspection S_— Compliance Sampling
B L Enforcement Case Support X — Toxic Sampling
C —,Compliance.-Evaluation P — Pretreatment
I. D Diagnostic R — Reconnaissance Inspection i
Columrt`19:"Itispectot Code. Use -one of the codes listed below to describe the lead agency -in the
inspection.
C — Contractor or Other Inspectors (Specify in N — NbC Inspectors
Remarks columns) R —EPA Regional Inspector
E — Corps of Engineers S — State Inspector
:.jJ Jpjr�t:;E'A/State-Inspectors—EPA lead - T-Joint State/EPA Inspectors —State lead
d'-j
Column 20..Faci.lity_Type.-Use- one of the codes below .to.describe the facility.
1 —Municipal. Publicly Owned Treatmen(Works (POT
Ws) with 1972 Standard Industrial Code
2 —Ind ,.gri_al. Otherthan mu.nicipal,.agricultural, and Federal .facilities.
3 —Agricultual.-Facilitiesciassifiedwith :7,972-SIC-0111 to 0971.
_4 . Federal.: Facilities identified as Federal _by the EPA Regional _Office.
,Columns 21-66: Remarks. These columns are reserved for remarks at the discretion of the Region.
Column 70: Facility Evaluation Rating. Use information gathered during tie inspection (regardless
of inspection type) to evaluate the quality of the facility self -monitoring program. Grade the program
using a scale of 1 to 5 with a score of 5 being used for very reliable self -mon Loring programs, 3 being
satisfactory, and 1 being used for very unreliable programs.
.Column 71: Biomonitoring Information. Enter D for static testing. Enter F for flow through testing.
'Enter N for no biomonitoring.
Column 72: Quality Assurance Data Inspection. Enter Q if the inspection was conducted as
followup on quality assurance sample results. Enter N otherwise.
`Columns 73-80: These columns are reserved for regionally defined information.
Section' B: Facility Data
This section is self-explanatory.
Section C: Areas Evaluated During Inspection
Indicate findings,(S, M, U, or N) in the appropriate box. Use Section D and additional sheets as
necessary. Support the findings, as necessary, in a brief.narrative report. Use the headings given on
the report form (e.g., Permit, Records/Reports) when discussing the areas evaluated during the
inspection. The heading marked "Other" may include activities such as SPCC, BMP's, and multime-
dia concerns.
Section D: Summary of Findings/Comments
Briefly summarize the inspection findings. This summary should abstract the pertinent inspection
findings, not replace the narrative report. Reference a list of attachments, such as completed
checklists taken from- the NPDES Compliance Inspection Manuals and pretreatment guidance
documents, including effluent data when sampling has been done. Use extra sheets as necessary.
EPA Form 3560-3 (Rev. 3-851 Reverse

DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIELD -LAB FORM (DM1)
For Lab UseUNLY/2�3
-- -'-
Lab Number:
COUNTY
O f'
PRIORITY - SAMPLE TYPE
-
I �7
Date Received: /�`�1 ^�f J Time:
RIVER BASIN 169Y Q
❑AMBIENT ❑ QA
❑ STREAM
EFFLUENT
Rec'd by _From:
Bus_Couriie H=arnd Del
REPORT TO: RO RO MRO RRO WaRO WIRO WSRO TS
AT BM
❑
❑
❑
COMPLIANCE CHAIN
LAKE
INFLUENT
DATA ENTRY_ BY:
Other
OF CUSTODY
❑EMERGENCY
❑ ESTUARY
_
REPORTED:
Shipped by; Bus Courier, Sta(t then
-DAT=L'
COLLECTOR(•S); J' P
LOCATION:G(r
Estimated BOD Range: 0• 5-2 25-65/40-130 or 100 plus
STATION
Seed:. Yes No ❑ Chlprinated: Yes M_ No ❑
REMARKS: eC q I J ��✓�C{ G 1
< ( 0o
Station7.
Date Begin (yy/mm/dd)
Time Begin
Date End
Time End
Depth DM DB DBM
Value Type—
A H L
Composite
T S
11
Sample 'tyke
{: G) GNXX
t 1
f) 2
3
- 4
5
BODS 310 Q3 1118/1
Chloride 940
COD High 340 mg/1
Chi a:'Tri 32217 ug/I
COD Low 335 mg/1
Chi a: Corr 32209 ug/I
Coliform: MF Fecal 31616 / /100m1
Pheophytin a 32213 — ug/l
Coliform: MF Total 31504 /100ml
Color: True 80 Pt -Co
`6
_ 7
8
9
10
1_2
13
14
15
16
1 17
18
191
20
Coliform: Tube Fecal 31615 /100ml
Color:(pH' �) 83 ADMI
Coliform: Fecal Strep 31673 /100ml
Color: pH 7.6 82 ADMI
Residue: Total 500 mg/I
—
Cyanide 720 mg/I _
Volatile 505 mg/I
Fluoride951 mg/I
Fixed 510 mg/I
Formaldehyde 71880 mg/1/1
Residue: Suspended 530 mg/I
Grease and Oils 556 mg/I
Volatile 535 m9/1
Hardness Total900 mg/l
Fixed 540 mg/I
Specific Cond. 95 uMhos/cm2
pH 403 P units
lD
MBA'S 38260 mg/I
Acidity to pH 4.5 436 mg/I
Phenols 32730 ug/1
Acidity to pH 8.3 435 mg/1
Sulfate 945 m 9/1
Alkalinity to pH 8.3 415 -2o mg/l
Sulfide 745 mg/I
Alkalinity to pH 4.5 410 mg/I
TOC 680 mg/1
Turbidity 76 NTU
NH3 as N 610
IT as N 625
NO2 plus NO3 as N 630 mg/I
-mg/I
--
P: Total as P 665
1104 as P 70507 --^ --_-mg/l
P: Dissolved as P 666-- - _ -- _.._` mg/I
Cd{Cadmium 1027_— —u(JA
Cr-Chromittmfrotal1034 — ug/1
Cu-Copper 1042
NFNlckel 1067 --- ug/l
Pb I,eacl 1051 - «g/l/l
Zn-'Zinc 1092 ug/1
Ag•Stiver 1077- --ug/l
AI -Aluminum 1105 ug/I
Be -Beryllium 1012
-ug/l
Ca•COciurn 916 mg/l
Co -Cobalt 1037 ug/l
Fc•Iron 1045 ug/1
LI-lithium 1132 _ uu/!
_
-'-
Mg-Magnesium.927 mg/I
Mn'-Manganese 1055 ug:l
Na-Sodium 929 mu.'I
Arsenic:Total 1002
Se -Selenium 1147 - -__..c 7'1
Hg-Mercury 71900
Organochlorine Pesticides
Organophosphorus Pesticides
-
Acid Herbicides ---`---
Base/ Neutral I:xrractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg"i.,
-
Phytoplankton ----
Sampling Point %
Conductance at 25 C
Water Temperature (C)
D.O. mg/I
pH
^Alkalinity
Acidity
Air Temperature (C)
pH 8.3 pfi 4.5
pli 4.5 pH 8.3
2
94
10
300 1.
400 1•
82244 1 431
82243182242
20
Salinity %
Precipition On/day)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
can Stream Depth ft.
Stream Width ft.
480
45
32
36
1351
1350
135
64
14

r
3" 5Aa
WOW
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Z007

DIVISION OF ENVIRONMENTAL MANAGEMENT
September 23, 1993
MEMORANDUM:
To: Charles Alvarez
Through: Matt Matthews mAti
From: Melissa Rosebrock
Subject: Burlington Industries/Caroleen Plant-Outfall 004
Use of Nalco 2593 Biocide
NPDES No. NC0006009
Rutherford County
Burlington Industries/Caroleen Plant (outfall 004) has submitted Nalco 2593 biocide for review.
Data submitted by the subject facility concerning the dosage rate of the compound, system volume,
average daily discharge, toxicity of the active ingredients and/or breakdown products, and minimum
stream flow have also been reviewed and evaluated. Note that we did not receive biocide worksheets for
the use of Nalco 7346 and 2593. which appear to be discharged through outfall 001 (see attached 7/28/93
memo from Philip Klein).
In reviewing the submitted materials, a discrepancy was noted in calculating the regulated
limitation (part III, pages two and three). The toxicity data supplied by the facility utilizes an LC50 of
18.Omg/l for the mysid shrimp. Given the geographical location of the facility in the foothills, the more
appropriate toxicity data would be for the fathead minnow (LC50=0.12ppm, see page 6 of the attached
MSDS). This toxicity data was for the active ingredient and since the facility will be using a 1.5% active
formulation we have made the appropriate conversion (LC50=8.Omg/1). These revisions did not alter the
final analysis portion of the worksheet (part IV, page three).
Calculations summarized- on the accompanying worksheet predict that the use of Nalco 2593 at
the stated rate and discharge conditions will not result in a toxic impact to aquatic life in the receiving
stream. Therefore, the use of this product as a biocide at Burlington Industries/Caroleen Plant-Outfall
004 is deemed acceptable.
If there are questions regarding this review please contact me at [phone].
Attachments
cc: Forrest Westall-ARO
Central files

s -J
Burlington Industries-Caroleen (004) BIOCIDEWORKSHEET
PERMIT#: NC0006009
RECEIVING STREAM: Second Broad River
7Q10 (cfs): 51.20
I.W.C%: 0.03
PRODUCT: Nalco 2593
ACTIVE INGREDIENT: 5-chloro-2-methyl-4-isothiazolin-3-one 1.15%
2-methyl-4-isothiazolin-3-one 0.35%
HALF LIFE (DAYS):
10.00
STEADY STATE DISC CONC:
48.707008
LC50 OF SELECTED TOX DATA (MG/L):
8
DEGRADATION FACTOR:-
1.400 '-- -`
DECAY RATE:
0.0690
APPLICATION FACTOR:
0.010
DOSAGE RATE (GRAMS/DAY):
2230
AVG DAILY DISCHARGE (MGD):
0.0115 -
INSTREAM BIOCIDE CONC:
0.0169
VOLUME OF SYSTEM (MIL. GAUS):
0.00864
REGULATED LIMITATION:
0.08
PASS/FAIL:
PASS

DIVISION OF ENVIRONMENTAL MANAGEMENT
Water Quality
Permits and Engineering Unit
August 9, 1993
To: Melissa Rosebrock,, Aquatic Toxiweaselcology
From: Charles Alvarez, Environmental Engineer, 14PDES Permits
Subject; Burlington Industries, Caroleen Plant, NC000,6009
Attached is a copy of information sent related to the biocide use for
Outfall 004 that has been reinstated at the request of Burlington
.Industries for this facility.The water from this outfall will not go
through any.treatment and Will need to be reviewed for
nonpoisonfishyology. Please comment as to whether the request is
appropriate.
If you need any more information please call me at 733-5083 ext
553.
CEI\JE®RE
VG 1
ENVIRONMENTAL SCIENCES
8M%CB
I

f
Burlington Industries, Inc.
,CERTIFIED MAIL
RETURN RECEIPT REQUESTED
July 28, 1993
North Carolina Department of'Environment,
Health and Natural Resources
Permits and Engineering Unit
Division of Environmental Management
Post Office Box 29535
Subject: Burlington Industries Caroleen Plant
NPDES Permit No. NC0006009
Renewal Application
Attention: Mr. Charles Alvarez
Dear Mr. Alvarez:
Executive Offices
P. 0. Box 21207
Greensboro, North Carolina 21420
In a letter dated May 18, 1993, Burlington Industries requested
renewal of the subject NPDES permit which expires on 11/30/93.
This renewal application requested deletion of outfalls 002, 003,
and 004 through which cooling tower blowdown was.discharged. All
facility wastewater including cooling tower blowdown was to be
conveyed through the septic tank and sand filter system and out
outfall 001.
We have since determined, that discharge of all' cooling tower
blowdown through outfall 001 will exceed the+capacity of the sand
filter. We request that outfall 004 continue to be permitted. We
estimate the discharge through that outfall will be on the order of
11,500 gallons per day. We have enclosed a revised Short Form D,
which has been -modified to reflect this cooling, water discharge
(Attachment 1).
The cooling tower blowdown .which will be discharged through outfall
UO049' will be treated with the biocide �.N_aalc_o 2;59'u3z A biocide
worksheet for this discharge is contained in Attachment 2,.\
. k
Bleed -off from the' air washers will continue to be discharged h�o
through the -septic tank and sand filter system and out outfallOOtl �.
This water• will typically be treated with`+ a:Ico�;' 734u6 A biocide
worksheet, for .this discharge.is contained in Attachment 2. As.
_necessary, the air washer water may -be. treated- with Nalco 2 r9,3
instead ''of Nalco�7.346. Use of Nalco 2593 has previously been,
approved by the Division of nvviRn ental Management. A revised
l
%C,P*

July 28, 1993
Page 2
biocide worksheet for the discharge of Nalco 2593 through outfall
001 is also contained in Attachment 3.t" Na OcAtadva .�
Material safety data sheets and decay rate data for the biocides
are contained in Attachment 4.- The biocide worksheets have been
prepared based on average daily discharge volumes and normal
operation.
Please contact Miriam White, Division Environmental Engineer, at
[phone] or Jake Wilson, Plant' Engineer, at [phone]
with any questions or comments regarding this permit application.
ely,
ili H. Klein
Director of Corporate
Engineering
cc: M. White
J. Wilson
S. Meador

ATTACHMENT 1
NPDES PERMIT APPLICATION

NORTH CAROLINA DEPT. OF W_._RAL RESOURCES AND COMKJNITY k-,- - OPMEHT
ENVIRONMENTAL MANAGEMENT C"ISSION
NATIONAL POLLUTANT DISCHARGE ELIMINATION "SYSTEM AIPLica1110M ►psiUER
APPLICATION FOR PERMIT. TO DISCHARGE - SHORT FORM D. FOR
AGE KCY
USE DATE RECEIYEn-
To be filed only by services, .m olesale and retail trade,
and other .commercial establishments including vessels
YEAR M0. Der
Do not atteopt to complete this fors without reading the accompanying instructions
iloase print or type
1. Na+ne, address, and teleohone'riumber of facility producing discharge
A. Na.+e Burlington Industries Caroleen Plant
d. Street address "Highway 22 A, ox 5
C. ,City Caroleen 0. Stat@ NC
E. County Rutherford F. ZIP 28019 -
G. Telephone No. - (704 657-6376.
Area
Co de
2. SIC
(Leave blank)
4. Number of tmployees 403
4. Nature of business. Yarn Manufacturin:e
5. (a) Check here if discharge occurs all rear, or
(b) Check the month(s) discharge occurs-
1. 0 January 2.0 February 3:0 Ksrch 4.0 April S.0Kay _
6.13 June 7. C July 1.0 August 9.0 54ptr*tr 10.0 October
11. 0 No v embe r . 12. a Dec an+be r
(c) How many days per weak;
2.0 2-3- 3.0 4-6. 4 -t�66-7
6. Types of waste water discharged to surface waters only•(check is topTicabit)
Discharge per
operating day
A. Sanitary, daily
average
Flow, gallons per operating.day
Volume treated before .
discharging (percent)
0.1-949 Y000-4994 5000-4499 10,000- 50.000 lior+t 0.1- 30- 65- 95-
49.9" or Pore 29.9 64.9 94.9 100
(1) (2) (3), (4) (5). (6) (7) (8) (4) (10)
1. Coo.ling water, etc., X
daily average
C. Other discharge(s). �.'.
daily ay.trage; X
Specify*
D. 'M&xiMuni per operat-
ing day for combined r X
discharge (01- types)
*Limited amounts of water, generated from facility cleaning.
- f

• ►_ 0 any of the types of waste if -,if ied in item 6. either treated or w�-�}} '
treated, art discharged to plies_/othor then surface waters. N+tck Mlar�._1
es appl table. N/A
Waste .water is discharge,d,to:
0.1-"9
(1)
1000-1999
(Z)
5000-99l9
(3)
10..00049."1
(4)
50,0W or more
(5)
A. Mun i t i tw l' t&w, r system
H. Ikuf.•rgnrnkl wl)
•
C. Septic -tank
D. Evaporation lagoon or pond
'
E. Other, specify:
8. Number of separate discharge points:
A.101 8 XZ-3 C.O 6-5 - D.O 6 or more
9. Na.0 of rece(ving water or waters 2nd Broad River
.10. Does your discharge contain or is it possible for your discharge to contain
one or Port of the following substances f4did as a result of your operations,
activities, or processes: apnDnia, cyanide, aluminum, beryllium, eldmius.
chromium, topper, lead, r»rcu , nickel, selenium, Zinc, pf*nols, all MW
grtsse. and chlorine (residual.
A .Xyt t 1. r, no
1 certify that 1 am familiar with the inforowtton. contained in the application and
that to the best of my knowlardr and belief such information is trve, complete, and
accurate.
Printed Kama of Person Signing
Title
Data Application sign , .1.
rth Carolina General Statute 143-215.6(b)(2) provideB that: Any person who knowingly miiw.s
f false etatenent,representat on, or certification in airy &pplicat�one'-record; report,.plan,
other document files. -or required to be maintained"undar Article .21 or regulations of the
,ira=eatal Management Coumisslop implarn4nir�.ng.that Article, or who falsifieat taarpers Uith,
.knowly render& inaccurate any recording or toonitorlU 4jrvics or cethod required to be
hated or tlain%ained. under Ay�;tale: 2.1•: o!c rep ,latiocs-•of the Environznent&I X ageraant Comissi
�lenentfng that, Article, xha11"•be''yu4jtT: •qf i. iaisdemeanor punishable., by a -fine not to- exceed
1,000, or by imprisonmpnt• nbt' to exceed &ix months, or by both. (18 U.S.C. Section 1001 pro7:
)unishment by a fine'of'iiot' more than. $10,000' or irprison3*nt not r►ore than 5 years, or both,
r asimilar offense.)

n
ATTACHMENT 2
OUTFALL 004 BIOCIDE WORRSHEET
11

BIOCIDE/CHEMICAL TREATMENT
WORKSHEET-FORM 101
The following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
North Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
returned with all appropriate data entered into the designated areas with calculations performed as indicated.
I. Facility Name Burlington Industries — Caroleen Plant — 0utfall 004
NPDES # NC 0006009
County Rutherford
Receiving Stream 2nd Broad River
7Q10 51.2 (cis)
(All above information supplied by the Division of Environi-nental Management)
What is the Average Daily Discharge (A.D.D.) volume of the water handling systems to the receiving water body?
A.D.D. = 0.0115 (in M.G.D.)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
(A.D.D.) x 100 (.0115) X 100 IWC = 7_Q10 x 0.646) + (A.D.D.) — ( 51.2 )(0.646) + (.0115)
0.035 Qfo
i
This value (IWC) represents the waste concentration to the receiving stream during low flow conditions.
II. What is the name of the whole product chemical treatment proposed for use- in the discharge identified in Part I?
Nalco 2593 Microbiocide
Please list the active ingredients and percent composition:
5-chloro-2-methyl-4-isothiazolin-3-one 1.15 %
2-methyl-4-isothiazo-lin-3-one 0.35 %
Note: If ingredients contain the metals copper, chromium, or zinc, also complete page 4, ,Supplemental Metals Analysis
What feed or dosage rate (D.R.) is used in this application? The units must be converted to grams of whole
product used per day.
D.R.= 2230 grams/day
D.E.M. Form 101 (7/92) 1

C
1�1 ' '
Fnrility Name:
Burlington Industries Caroleen Plant NPDES it: NC NC0006009
outfall 004
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for this estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.) Cooling Tower i : 4,320 gallons
Volume= 0.00864 million gallons Cooling Tower 2: 4;320 gallons
What is the pH of the handling system prior to biocide addition? It unknown, enter NIA. 7.5 to 8.0 S.U.
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk.
The degradation must be stated at pH level within 1/2 pH standard unit within handling system. Enter the half
life (Half Life is the time required for the initial product to degrade to half of its original concentration). Please
provide copies of the sources of this data.
H.L. = 10 Days
The decay -rate is equal to I 1 L X 0.69 = 0.069 =Decay Rate (D.K.)
Calculate degradation factor (D.F.). This is the first order loss coefficient.
(Volume)
D.) (0.00860115 j + (0.069 ) = 1.40
D.F. _ ��_ + (D.K.) _ -
Calculate Steady Slate Discharge Concentration: ( 2230 �) 48.7
D(D.R.) - — 3 7 8 5) = mg/I
ischg Conc. _
(D.F.)(Volume)(3785) - ( 1.40 ) (0.00864 )
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischq Conc.) x (IWC%) _ ( 48.7 ) x ( 0.035 - ) _ 0.017 mg/I
100 100
Recaiving Stream Concentration
111. Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be
in mg/1). Please provide. copies of [lie sources of this data.
Organism Test Duration LC50 (nV)
*tysids 96 hrs
Sheepshead Minows 96 hrs
18
D.L.M. Form ,101 (7/92) 2

Facility Name:
Burlington Industries Caroleen Plant NPDES it: NC 0006009
Outfall 004
Choose the lowest LC50 listed above:
Enter the LC50: 18 .
If the half life (H.L.) is less than 4 days, perform the following calculation.
Regulated Limitation = 0.05 x LC50 = mg/I
If the halt life (H.L.) Is greater than 4 days or unknown, perform the following calculation.
Regulated Limitation = 0.01 - x LC50 = 0.18 mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
0.18 mg/liter
From Part II enter the receiving stream concentration:
0.017 mg/liter
IV. Analysis.
It the receiving stream concentration is greater than the calculated regulated limitation, then this biocide is
unacceptable for use.
Name (Print)
Signature
Person in'Responsible Charge
Date
A2030 31 123Qs
wt
00
C\j
CO
`2��818t Lbg4���

w
Facility Name:
Burlington Industries Caroleen Plant NPDES ll: NC 0006009
Outfall 004
Supplemental Metals Anatvsls
it copper, zinc, or chromium are present in. the proposed biocidal compound, complete this worksheet. A
separate form must be used for each metal and/or metal compound present in the biocide. List the metal,
Its chemical formula, molecular weight (MW), formula weight (FW), and the concentration of the metal
compound in the biocide (MCC). Complete a separate form for every metal present in the biocide.
Metal
EXAMPLE
Copper
Chemical Formula
Metal
CUS04.5H20 63.546 g/mole 249.680 g/mole 0.2 %
Copper Cupric Nitrate -
Dosage rate of Bioclde (DR) (from page' 1):
DR 2230 grams/day
Average Daily Discharge (ADD) (from page 1):
ADD = 0.0115 million gallons/day
Discharge Concentratlon (DC) of Blocide:
0 05% aG Clu m biocide*
DR ( 2230 grams/day) 193,913
a grams/million gallons
DC = ADD = ( million gallons/day)
Convert DC to,micrograms/llter (ppb):
DC (µg/i) =193, ql 1 DC (grams/million gal) x 1 x6106 tiq/g _ 51,232 ug/I
t 3.785 x 10 liters/million gal.
Calculate the traction of metal In the metal -containing compound (MF):
* MF = NON = ( grams/mole) _
FW ( grams/mole)
.Calculate the fraction of metal In the blocldal compound (BF):
MCC % a x % _ 0.0005
t BF = MF x 100 (100)
Calculate the concentration of metal in the discharge (M):
M = DC x BF = 51,232 ug/I x 0.0065 = . 25.6 ug/I
Calculate the instream metal concentration (IMC) at low -flow condltlons:
IWC % ' 25.6 . 0.035 % 0.0090 ug/l
iMC = M x 100 ug/I x - 100
Regulated limitation of, metal. (from below): 7 ugll
NC Genelal Stalules 15A NCAC 213.0211 doline:
Copper- 7 µg/I water quality action level' Zlnc- 50 µg/I water quality action level'
Chromium- 50 µg/I water quality standard
(•Values'which exceed action levels must be addressed directly by aq,Ualic toxicity testing.)
D.E.M- Fnrm 101 (7192) 4

..MATERIAL SAFETY DATA SHEET.
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION '1 PRODUCT IDENTIFICATION
TRADE NAME: NALCO 2593 MICROBIOCIDE
DESCRIPTION: An aqueous 'solution of substituted isothiazolinone
NFPA 704M/HMIS RATING: 3/3 HEALTH 0/0 FLAMMAB-ILITY 0/0,REACTIVITY 0 OTHER
O=Insignificant 1=Slight 2=Moderate '3=High' 4=Extreme
SECTION 2 HAZARDOUS INGREDIENTS
Our hazard evaluation has identified the following chemical ingredient(s) as
hazardous under OSHA's Hazard Communication Rule, 29 CFR 1910.1200. Consult
Section 14 for.the nature of the hazard(s).
INGREDIENT(S) CAS # APPROX.%
5-chloro-2-methyl-4.isothiazolin-3-one 26172-55-4 1.15
2-methyl-4-isothiazolin-3-one 2682-20-4 0.35
SECTION 3 PRECAUTIONARY LABEL INFORMATION
DANGER: Corrosive. Causes eye'damage and skin burns. May cause allergic
skin reaction. Maybe harmful if inhaled. May be fatal if swallowed or
absorbed through the skin. Do not get in -eyes, on skin, or on -clothing. Wear
goggles or face shield and rubber gloves_ when handling. Avoid breathing vapor
or mist. Avoid contamination of food. Do not take internally. Wash,
thoroughly after handling.
SECTION- 4 FIRST AIDINFORMATION
EYES: Immediately flush for at least 15 minutes.while'holding''
eyelids open. Call a physician at. once.
SKIN: Wash thorougly.with soap and rinse with water._ Remove and
wash contaminated clothing before reuse.
INGESTION: Do not induce vomiting. Drink promptly_ a.large quantity of
milk; egg. whites, gelatin -solution, or, if these are not
available, drink large quantities of water. Avoid alcohol.
Call a physician immediately -
INHALATION: Remove immediately to fresh air. If not breathing, apply
artificial respiration. If breathing is difficult, give
oxygen., Call a physician.
NOTE TO PHYSICIAN: Based,on the individual reactions of the patient, the
physician's judgment.should,be used to control symptoms.. -and clinical condition.'
CAUTION: If unconscious, having trouble breathing,or in convulsions, do not
PAGE. 1 OF. 10

il
MATERIAL SAFEr�Y DATA SHEET.
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 4 FIRST AID INFORMATION CONTINUED )
induce vomiting or give,water.
NOTE TO PHYSICIAN: Probable mucosal•damage may contraindicate the use
of gastric lavage. Measures against circulatory shock, respiratory
depression and convulsions may be needed.
SECTION "S HEALTH EFFECTS INFORMATION ��--
PRIMARY ROUTE(S) OF EXPOSURE,: Eye, Skin, Inhalation
EYE CONTACT: Corrosive to the eyes with possible permanent damage
depending on the length of exposure and on the first
aid action given.
SKIN CONTACT: Corrosive to the skin, possibly resulting in third
degree burns depending on,.the length of exposure and
on the first aid action given. Can be harmful if
absorbed. Can cause allergic contact dermatitis in
susceptible individuals.
INGESTION: Can be fatal.
INHALATION: Can be.corrosive to the mucous membranes and -the
lungs. Can cause an all reaction in susceptible
individuals.
SYMPTOMS OF EXPOSURE: A review of, available data does not identify any
symptoms from exposure not previously mentioned.
AGGRAVATION OF EXISTING CONDITIONS: A review of available data does
not identify any worsening of existing conditions.
SECTION 6 TOXICOLOGY INFORMATION
ACUTE TOXICITY STUDIES: Acute toxicity studies have been conducted on
this product. The results are shown below.
ACUTE ORAL -TOXICITY (ALBINO RATS):. LD „ = 3,810 mg/kg
.95% Confidence Limit = 3,530 - 4,220 mg kg
ACUTE DERMAL TOXICITY (ALBINO RABBITS):
LDso = Greater than 5,000 mg/kg
ACUTE INHALATION TOXICITY (ALBINO RATS):
For'solution of 1% active ingredients LC,. = 13.7 mg/L
t
PAGE 2. OF -10

r
MATERIAL SAFE':' DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number.'
M6dlcal [phone] (24 hours)
SECTION 6 TOXICOLOGY -INFORMATION ('CONTINUED )
COMMENTS: Four-hour nominal concentration for a solution containing 1%
active ingredients.
SKIN IRRITATION INDEX DRAIZE RATING: Severe irritant
EYE IRRITATION INDEX DRAIZE RATING: Corrosive (corneal damage)
SKIN SENSITIZATION: This product'is a human sensitizer in its'undiluted form.
A Guinea pig (Buehler Technique) sensitization study with an induction
dosage of 90 ppm of active ingredients followed by a insult of 429 ppm
of active ingredients was positive.
A human repeated insult patch study of 28 ppm active ingredients
followed by a insult of 56 ppm of active ingredients resulted in no
effect to the subjects tested.
SUBCHRONIC TOXICITY RESULTS: A 90-day dietary study in dogs of 840 ppm of the
Product's active ingredients resulted in no mortalities .or pathological
findings. A 90-day dermal study in rabbits of 0.4 mg/kg/day of.the product..'s
active ingredients resulted in no irritation or pathological eff-ects.
CHRONIC TOXICITY 'RESULTS: A teratology study with rabbits and rats was
negative with dosages of active ingredient. ranging from 1.5 mg/kg to 15 mg/kg.
Mutageni'city results were equivocal.- A.30-month-skin painting mouse study
with applications of 400 ppm of active ingredients three times per week
showed no increase tumor frequency over control animals. -
SECTION 7 PHYSICAL AND CHEMICAL PROPERTIES
COLOR: Pale yellow to green .FORM: Liquid ODOR: Mild
DENSITY: 8.6 lbs/gal.
SOLUBILITY IN WATER: Completely,
pH'(NEAT) = 3 -' 5 ASTM E-70
FREEZE POINT: 25 Degrees F ASTM D-1177.
FLASH POINT: None
NOTE: These physical properties are typical values -for this product.
SECTION 8 FIRE AND EXPLOSION, INFORMATION
FLASH POINT: None
EXTINGUISHING MEDIA: Not applicable
PAGE 3 OF.' 10

MATERIAL SAFE' DATA SHEEN'
PRODUCT
NALCO 2593.MICROBIOCIDE
emergency Telephone Number
Medical [phone] (24 hours)
SECTION 8 FIRE AND EXPLOSION INFORMATION
CONTINUED ).
UNUSUAL FIRE AND EXPLOSION HAZARD: May evolve NOx, SOx or HC1 under fire
conditions. Containers exposed in a fire should be cooled with water to
prevent vapor pressure buildup leading to a rupture. Do not let material
evapo Late to ,dryness.
SECTIION 9 REACTIVITY INFORMATION
INCOMPATIBILITY: None known
THERMAL DECOMPOSITION PRODUCTS: In the event of combustion CO, CO,,, HOx,
Sox, HC1 may be formed. Do not breathe' smoke or fumes. Wear suitable
protective equipment.
SECTION 10 PERSONAL PROTECTION EQUIPMENT
' 1•
RESPIRATORY PROTECTION: If it is possible to generate significant levels of.
vaporslor mists, a NIOSH approved or equivalent respirator is recommended.
For large spills, entry into large tanks, vessels or enclosed -,small
spaces1with inadequate ventilation, a pressure -demand, self-contained
.breathing apparatus is recommended.
VENTILATION: General ventilation is recommended. Additionally, local exhaust
ventilation is recommended where vapors, mists or aerosols maybe.released.
PROTECTIVE;EQUIPMENT: Wear gloves, boots, apron and a face shield with
chemical splash goggles. (Based on .test data obtained from materials of
construction, the following recommendations are listed for gloves along with
their break -through .times: Butyl rubber (greater than 8 hours); polyvinyl
chloride (greater -than 7.5 hours) and neoprene coated (greater than 6 hours-).
A full Islicker suit As recommended if gross exposure is -possible.
The availability of an eye,wash fountain and safety shower is recommended.
If clothing is contaminated, remove clothing and thoroughly wash the
affected area. Launder contaminated clothing before reuse.
SECTION 11 SPILL AND DISPOSAL INFORMATION'
IN CASE OF TRANSPORTATION ACCIDENTS, CALL THE FOLLOWING 24-HOUR
TELEPHONE NUMBER (708-920-1510)
SPILL CONTROL AND RECOVERY:
PAGE 4 OF -10

MATERIAL SAFE'i f DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALGO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 11 SPILL AND DISPOSAL INFORMATION ( CONTINUED )
Small liquid- spills: Contain with absorbent material, such as clay, soil or
any commercially available absorbent. Shovel reclaimed liquid and absorbent
into recovery or salvage drums for disposal. Refer to CERCLA in Section 14.
Large liquid spills: Dike to prevent further movement and reclaim into
recovery or salvage drums or tank -truck for disposal. Refer to CERCLA
in Section 14.
For large indoor spills, evacuate employees -and ventilate. area. Those
responsible for control and recovery should wear the protective equipment
specified.in Section 10.
This product is - toxic to fish. It should ,not be directly discharged
into lakes, ponds, streams, waterways or public water supplies.
DISPOSAL: If this product becomes a"waste, it meets the criteria of a
hazardous waste as defined under the Resources Conservation andl Recovery
Act (RCRA) 40 CFR 261. Hazardous Waste D002.
As a hazardous liquid waste, it must be solidified with stabilizing agents
(such as sand., fly ash, or.cement) so that no free liquid remains before
disposal to a licensed industrial waste landfill (Hazardous Waste Treatment;
Storage and Disposal facility).. A hazardous liquid waste can also be
incinerated in accordance with local, state, and federal regulations.
Pesticide wastes are toxic. Improper disposal of excess pesticide,. spray
mixture., or rinsate is a violation of Federal Law. If these wastes cannot be
disposed of by use according to label instruction, contact your State
Pesticide or Environmental Control Agency, or.the Hazardous Waste
representative at the nearest EPA Regional Office for guidance.
METAL CONTAINERS: Triple rinse (or equivalent). Then offer for recycling or
reconditioning, or puncture and dispose of in a sanitary landfill, or.by'other
procedures approved by state and local authorities.
PLASTIC CONTAINERS: Do not reuse empty container. Triple rinse (or
equivalent). Then puncture and dispose -of in a sanitary landfill, or, if
allowed by"state and local authorities, by burning. If burned, -stay out of
smoke.
SECTION 12 ENVIRONMENTAL INFORMATION
CHEMICAL OXYGEN DEMAND (COD): -20,OA6 mg/L
PAGE 5 .OF 10
e

�1 MATERIAL SAFEDATA SHEET
-PRODUCT
NALCO 2593 MICROBIOCIDE
NALGO
Emergency Telephone Number _
Medical [phone] (24 hours)
SECTION 12 ENVIRONMENTAL INFORMATION ( CONTINUED )
TOTAL ORGANIC CARBON (TOC'): .7,850 mg/L
AQUATIC DATA: Active -ingredient.
6 day static acute LC,, to.Bluegill Sunfish = 0.54 ppm
Standard Deviation of 6 day LC,, = 0.47 - 0'.62 ppm
6 day dynamic acute LC „ to Fathead Minnow_ = 0.12 ppm
Standard Deviation of 6 day LC,, = 0.06 -,0.15 ppm
48 hour acute LC,, to Daphnia Magna 0.13 - 0.18 ppm
6 day dynamic acute LC,, to Rainbow Trout=..0.14 ppm
Standard Deviation of 6 day LC,, = 0.12 - 0.17 ppm
96 hour static acute LC, to Rainbow Trout = OA ppm
Standard Deviation of 96 hour LC,, = 0.18 0.50 ppm
OTHER STUDIES: Avian species:
Acute oral LD „ to Bobwhite Quail = 97 mg/kg
Standard Deviation of LD „ = 64 - 114 mg/kg
8 day dietary LD „ to Pekin Duck = 560 ppm of active ingredients
AQUATIC -DATA: Product.
104
00 0
96 hour static acute LC „ to MysidS = 18 mg/L
96 hour no observed effect concentration is less than 10 mg/L based on no
mortality 'or abnormal `effects.
TOXICITY RATING: Moderately toxic
96 hour static acute LC, to Sheepshead Minnow = 32 mg/L"
96 hour no observed effect concentration is 18 mg/L based on no mortality or
abnormal effects.
TOXICITY RATING: Moderately toxic
If released into the environment, See CERCLA in Section 14.
_ PAGE;: 6, OF 10
"At f`r7 r'91V=&A1C�A1 f-r1Mt3AlV1Z Mmr= nine rnr) r`GIVTFfa •-NAPPRVII_I F_ II I INfIIP RC75F;19-1'1FIR '

.e
NALCO
IVIA r r-nIAL. 5Ht-t_( tJH I H bHEE't
PRODUCT
: NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 13.-TRANSPORTATION INFORMATION
DOT PROPER SHIPPING NAME/HAZARD CODE - CORROSIVE LIQUID, N.O.S.
• CORROSIVE MATERIAL UN 1760
.CONTAINS - 5-CHLORO-2-METHYL-4-ISOTHIAZO
LIN-3-ONE, CUPRIC NITRATE
SECTION 14 REGULATORY INFORMATION
The following regulations apply to this product.
FEDERAL REGULATIONS:
OSHA'S HAZARD COMMUNICATION RULE, 29.CFR 1910.1200:
Based on our -hazard evaluation, the following ingredients in -this product are
hazardous and the reasons are shown below.
5-chloro-2-methyl-4 isothiazolin-3-one —Corrosive, sensitizer
2-methyl-4-isothiazolin-3-one - Corrosive, sensitizer
5-chloro-2-methyl-4 isothiazolin-3-one (mist or aerosol) = 0.5 mg/m3 TLV
Manu'facturer's recommendation
CERCLA, 40 CFR 117, 302:
This product contains cupric nitrate, a Reportable Quantity (RQ) substance
and if 52,000 pounds of.product are released, it requires notification to the
NATIONAL RESPONSE CENTER, WASHINGTON, D. C.- (-1-800-424-8802).
SARA/SUPERFUND AMENDMENTS AND REAUTHORIZATION ACT OF 1986
(TITLE III) - SECTIONS.302, 311, 312 AND 313:
SECTION 302-- EXTREMELY HAZARDOUS SUBSTANCES (40 CFR 355):
This product does not contain ingredients.listed in Appendix A and B as an
Ex"tremely'Hazardous Substance.
SECTIONS 311 and 312 MATERIAL SAFETY DATA SHEET REQUIREMENTS ('40 CFR.370):
Our hazard -evaluation has found this product to be hazardous. The product
should be reported under the following EPA hazard categories:
XX Immediate (acute) health hazard
-- Delayed -(chronic) health hazard
-- Fire hazard
-- Sudden release of pressure hazard.
-- Reactive hazard
SECTION 313 - LIST OF -TOXIC CHEMICALS (40 CFR 372):
PAGE- 7 OF 10,
NALCO CHEMICAL COMPANY, ONE .NALCO -CENTER • ,NAPERVILLE. ILLINOIS 60563-1 196

MATERIAL SAFE'` DATA SHEET
NALGO
PRODUCT
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION,14 REGULATORY INFORMATION ( CONTINUED )
This product.does not contain ingredients,,on the List of Toxic Chemicals.
TOXIC SUBSTANCES CONTROL ACT (TSCA):`
The active ingredients are exempted under TSCA and regulated under FIFRA as
follows. All the inert ingredients are found on the TSCA Master Inventory
List.
FEDERAL INSECTICIDE, FUNGICIDEAND RODENTICIDE ACT-(FIFRA):
EPA Reg. No.,1706-153. This product is registered for use as a microorganism,
control chemical used -in industrial recirculating cooling water tower
systems, used in brewery,pasteuriz.ers, and used in air washer systems. In all_
cases follow instructions on the product label.
RESOURCE CONSERVATION AND RECOVERY ACT (RCRA), 40 CFR 261 SUBPART C &"D:
Consult Section 11 forRCRA classification.
.FEDERAL WATER -POLLUTION CONTROL ACT, CLEAN WATER ACT', 40 CFR 401.15
(formerly Sec. 307), 40 CFR 116 (formerly Sec. 311):
This product contains the following ingredients covered by the Clean Water Act:
Cupric nitrate - Section, 307, 311
CLEAN'AIR ACT; 40 CFR 60,_ SECTION 111,,40 CFR 61, SECTION 112:
This product does not contain ingredients covered by the Clean Air.Act.
STATE REGULATIONS:
CALIFORNIA PROPOSITION 65:
None of the chemicals on the current Proposition 65 list are known to be
present in this product.
MICHIGAN CRITICAL MATERIALS:
This product contains the following substance(s) identified on the Michigan
Critical Materials Register:
Copper,, as Cu =, 0.05%..
STATE RIGHT TO 'KNOW LAWS:
PAGE '8 OF 10
NALCO CHEMICAL COMPANY.ONE;.'.NALCO CENTER • -N4 ERVILLE, ILLINOIS 6056371196

MATERIAL �At-E� � DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION.14 REGULATORY INFORMATION (CONTINUED )
The following.state(s) identify the ingredients) shown below as hazardous:
California — Copper
Massachusetts, New Jersey, Pennsylvania - magnesium nitrate
INTERNATIONAL REGULATIONS:
This is not'a WHMIS controlled product under The House of Commons of Canada
Bill C-70.
SECTION 15 ADDITIONAL INFORMATION
Note: Other toxicological results are available upon request.
SECTION 16 USER'S RESPONSIBILITY
This product material safety data sheet provides health and safety
information. The product is to be used in applications consistent with
our product literature. •Individuals handling this product should be
informed of the recommended safety precautions and should have access
to. this information. For any other uses, exposures should be evaluated
so.that appropriate handling practices and training programs can be
established to ensure safe workplace operations. Please consult your
local sales representative for any further information.
SECTION 17-BIBLIOGRAPHY'
ANNUAL'REPORT ON CARCINOGENS, U.S. Department of Health'and 'Human Services,
Public Health Service, PB 33-135855, 1983..
CASARETT AND-DOULL'S TOXICOLOGY, THE BASIC SCIENCE,OF' POISONS, Doull, J.,
Klaassen, C..D.., and Admur, M. 0., eds.,'Macmillian Publishing Company, Inc.,.
N..Y., 2nd edition, 1980.
CHEMICAL HAZARDS OF THE -WORKPLACE, Proctor, N. H., and Hughes, J. P., eds.,
J. P. Lipincott Company, N.Y., 1981.
DANGEROUS PROPERTIES'OF INDUSTRIAL MATERIALS, Sax, N. Irving, ed., Van
Nostrand Reinhold Company, N.Y., 6th edition, 1984.
IARC MONOGRAPHS ON THE EVALUATION OF THE CARCINOGENIC RISK -OF CHEMICALS'
TO MAN, Geneva: World Health.organization,-International Agency for
Research on Cancer, 1972-1977. ;
PAGE 9' OF 10
lip
NALCO CHEMICAL- COMPANY ONE NAL' CO CENTER • NAPERVILLE. ILLINOIS 60563-1 196

• ' MATERIAL SAFE- DATA SHEET
PRODUCT
NALCO 2593. MICROBIOCIDE
NALC
Emergency Telephone Number
Medical (roe) 920-1510 (14 hours)
SECTION 17'BIBLIOGRAPHY ( CONTINUED.
PATTY'S INDUSTRIAL HYGIENE -AND TOXICOLOGY,. Clayton, G. D., Clayton; F. E.
eds., John Wiley and SoAS,- N. Y., 3rd'edition, Vol. 2-A-C, 1981.
REGISTRY OF TOXIC EFFECTS ON,CHEMICAL SUBSTANCES,'U.S.,Department.of
Health and Human Services, Public Health Service, Center for Disease
Control, National Institute for occupational Safety and Health, 1983
supplement of 1981-1982 edition, Vol.•1-3, OH, 1984. �-
Title 29 Code of Federal Regulations -Part 1910, Subpart Z, Toxic and --
Hazardous Substances, Occupational Safety and Health Administration (OSHA).
THRESHOLD LIMIT VALUES FOR CHEMICAL SUBSTANCES AND PHYSICAL AGENTS IN THE
WORKROOM ENVIRONMENT WITH,INTENDED CHANGES_, American Conference.,of-
Governmental Industrial Hygienists, `OH.
PREPARED BY: Ricky A._Stackho.use PhD., Toxicologist
DATE.CHANGED: 08/28/91 DATE PRINTED: 09/28/91

'®NALCO CHEMICAL COMPANY
ONE NALCO CENTER a NARERVILLE. ILLINOIS E05133-119B ❑ AREA 708-305-1000
May 18, 1993
Ms. Marian White
Burlington Industries
Burlington House Annex
P.O. Box 691
Burlington, N.C. 27216
Subject: Nalco 2593 -Degradation
Dear Ms. White:
As discussed over the telephone this morning, I am sending for your reference information on the
half-life ( t�,) ,of the active ingredients in Nalco 2593.
The actives are isothiazolines and are identified in the references as RH-651 and RH-573. The
dissipation rates shown in Figure 5 are for complete degradation of the compound as described in
the document. A half-life of less than 10 days seems appropriate for the concentrations which
would be expected in a typical cooling water tower system.
Keep in mind that the degradation of the Isothiazolines are temperature and pH dependent and
are accelerated in the presence of strong nucleophiles or reducing agents.
I hope this information will satisfy your needs. If you have any questions, please feel free to
contact me directly.
Sine6r ly, -
./Claudee H. Wol , MSc.
Corporate Toxicologist
CHW/cw
enc.

-SUMMARY
Kathono WT and Kathon WT 1.5% biocides are
biodegradable at use levels. The degradation of
RH-651, the major active ingredient, begins with
ring opening and elimination of chloride ion.
Degradation leads to the formation of a variety of
small organic acids, methylamine, carbon dioxide
and elemental sulfur. The degradation products
have no measurable environmental impact.
INTRODUCTION
In 1915, Krzeminski et al. (1) described fate of the
active ingredients (Figure 1) of Kathon'WT bio=
cides in -a' variety of systems. A degradation
pathway was presented based on the metabolites
that were -identified. The folldwing is an updated
summary of the, current -understanding of the
environmental fate of Kathon WT biocides.
0 0
l-
N CI N "CH,
RH-651 RH-573
5-Chloro-2-methyl7.4- 2-Methyl-4-
isdthiazolin-3=one isothiazolin-3-one
FIGURE 1 — ACTIVE INGREDIENTS IN
KATHON WTAND KATHON WT 1.5%
BIOCIDES
INITIATION OF DEGRADATION
The degradation of RH-651and'RH-573' is accel-
erated by exposure to three key chemical and
physical factors:
• Temperatures above 500C for extended pe-
riods of time.
• High pH, generally above pH' 9.
• Strong reducing agents such as bisulfite
ion, or strong nucleophiles such -as mer--
captans and amines. .
Krzeminski et al. showed that the rate of degrada-
tion - of low .levels of RH-651 increases with
increasing pH and,to a more limited. extent, with
increasing tempi,__,�ure.-This suggested that
basic hydrolysis plays a major role in initiating the
degradation process of RH-651. However, low
levels .of nucleophiles, in-particular,mercaptans,
significantly accelerate the degradation of un
stabilized RH7651 in water (Figure 2). The reac-
tiyity of these nucleophiles increases as pH in-
creases. Therefore, it is likely that the pH
dependent degradation of RH-651 is initiated by
trace: levels of sulfides, -mercaptans or :other
nucleophilic species. This is consistent with the
fact that the addition of low levels of cupric ion, a
sulfide scavenger- (Ksp for CuS is -2 x 10-47 at
180C), to Kathon WT biocides significantly im-
proves stability.
The initial attack of nucleophiles on RH=65.1 can
be at sulfur or at carbon-5, although attack at
sulfur predominates. The reasons for the differ--
ent reaction sites maybe related to different ionic
characteristics of the nucleophiles. Nucleophilic
attack at sulfur results in cleavage of the nitrogen -
sulfur bond and is illustrated in Figure 3A. Attack
at carbon-5 results in addition of the nucleophile
at carbon-5 followed by rapid elimination of
chloride ion as shown in Figure 3B.
DEGRADATION PRODUCTS AND
PATHWAY
The degradation products from aqueous solutions
of use levels of RW651 were identified after
exposure to elevated temperature, elevated pH
and glutathione. Similar distributions of degra-
dation: products were seen in each of the three
systems. The products found were consistent
,with the major'metabolites identified by Krzemin-
ski et al. in the systems,they studied. The major
degradation pathway of RH-651 is shown in
Figure 4. The key steps in -the degradation path-
way .are:
1. Initiationby a nucleophile attacking
RH-651 at sulfur resulting in ring -opening.
2.. Rapid degradation of the intermediate. ad-.
duct: to N-methylmalonamic acid,-ehloride
ion, hydrogen sulfide and an oxidized form
of the nucleophile.
3...:. Propagation of, degradation through the .
reaction of released hydrogen sulfide with
another molecule of. RH-651.
4. Degradation of N-methylmalonamic acid to
small organic. acids' (malonic, acetic,
formic), methylamine; and carbon dioxide.

:0
100
%\ —& — 0 ppm SH-
80 — -0 — 1250 ppm SH-
C
---- 2500 ppm SH-
60 \
CD \
CrLO
40 \
\ 20
\, a \
0 ;
0 5 10 15
Days
20
FIGURE 2 — EFFECT OF SULFIDE ON THE DEGRADATION OF 10%
UNSTABILIZED RH-651 (w/w) INCUBATED AT 55°C
A. Nucleophilic Attack at Sulfur
O O
1 + Nu: ----, CI - / NH-CH3
N
Cl S� \CH3 Si -Nu. "
B. Nucleophilic Attack at Carbon-5
O 0
CI S CH3 Nu S� CH3
FIGURE 3 — INITIAL ATTACK OF NUCLEOPHILES ON RH-651 '
1
-2-

•r
--\
0
Initiation
J, N-CH, + FISHCI S�
I
0
I NH -CH,
Cl SSR
Release of Chloride Ion H2O
0
N-CH, + RSO,H + HCI + H,S
H
0 O or
H RS-SR
Propagation
N-methylmalonamic acid
0
ISSH
NH -CH,
CI
Formation of Elemental Sulfur H2O
0
NHCH,
+ HCI + S° + H,S
OH
0
H2O+
0
OH
.+ CH,NH2.HCI.
OH
0 methylamirie,hydrochloride
malonic acid
Release of Carbon Dioxide
CH,COOH, HCOOH, CO,
0
J1
CI S
FIGURE 4 — MAJOR DEGRADATION PATHWAY OF RH-651
—3—
2
I

1--N
-
` The major degradation products of RH-651 are
is rapidly degraded o CO2 by primarily biological
small biodegradable organic molecules, chloride
mechanisms in soil.
ion and elemental .sulfur. Chlorine and chlori-
nated organic molecules are not formed as
RH-651 degrades.. Degradation products arising
Dissipation in Activated Sludge Waste Water
from use level concentrations of Kathon WT bio-
Treatment Plants
cides should have no impact on the environment.
Laboratory studies performed in model activated
sludge waste water- treatment plants demon -
ENVIRONMENTAL FATE STUDIES
strate that:
Biodegradation in Natural River Water
• Kathon WT biocides rapidly dissipate in
activated sludge. Figure 6A shows a greater
Radioassays indicate that the active ingredients
than 90% reduction of the active ingre-
in Kathon WT biocides are readily biodegradable
dients.
in natural river water (Figure 5).
• Dissipation of Kathon WT biocides is ac-
companied by a corresponding reduction in
The, half life of each active ingredient is related to
total organic halogen levels as seen in
the initial concentration tested. The most rapid
Figure 6B.
degradation occurs at the lowest concentrations,
• Chlorinated organics do not accumulate in
which would occur following dilution of an ef-
the sludge.
fluent water stream.
• Activated sludge performance is unaffected
by Kathon , WT :biocides. Chemical oxygen
Dissipation in a.Typical Soil
demand (COD) and dissolved organic car-
bon (DOC) removal rates are not affected by
About,28% of 14C applied to non -sterile soil as
the addition of Kathon WT biocides -to the
RH-651 was released as 14CO2 from no
model feed influent.(Figures 7A and 713). In
soil after 41 days. However,14C release as 14CO2
addition, levels of viable bacteria and fungi
was less than 1 % from sterile soil over the same
in the sludge are also unaffected by the
ti-me period. This indicates that RH-651
presence of Kathon WT biocides.
100
- 0 - 0.006 ppm RH-651
--0-- 0.06 pprb RH-651
80 _6,— 0.6 ppm RH-651
t
--f-- _0.6 ppm RH-573
60
(D .
cc
40.
o � ,
r .
.20 `.
0 10 20 30
Days
FIGURE 5 '— DISSIPATION OF RH-651 AND RH-573 IN RIVER WATER

0
a0
a
1 0
1 0
0
A. Kathon WT Biocides B. Total Organic Halogens
Active Ingredient (TOX)
Influent
Effluent
E
a
a
Influent Effluent .
Activated Sludge Unit Operating Parameters:
Aeration Tank Volume: 3450 ml
Sludge Concentration: 2 - 4 g/L
Hydraulic Retention Time: 3 hours
Oxygen in Aeration Tank: 2.5 - 3.0 mg/L
Influent: Synthetic model feed (DIN 38412, part 24)
Acclimatization of Sludge: No prior exposure to Kathon WT biocides
FIGURE 6 = DISSIPATION OF KATHON WT BIOCIDES
IN A LABORATORY ACTIVATED SLUDGE PLANT
CONCLUSIONS
The work described here demonstrates that the
environmental impact of. Kathon WT biocides is
minimal because:
• Kathon WT biocides are high performance
products used at very.low levels.
• Kathon WT biocides biodegrade rapidly at
use levels.
• The degradation products are common,
small organic acids, chloride ion, methyla-
mine, elemental sulfur and carbon dioxide.
• Degradation of Kathon WT biocides does
not result in the release of chlorine or
persistent chlorinated organic species to
the environment.
• Kathon WT biocides used at typical treat-
ment levels do not affect the performance of
wastewater treatment plants.
LITERATURE CITED:
1. Krzeminski, S. F., Brackett, C. K., Fisher, J.
D., Spinnler, J. F, J.Agric. Food Chem., Vol.
23, No. 6 (1975),.1060-1075.
2. Mobiou, C. H., Cordes -Tolle, M., "Organi-
sche Ha loge nverbindungen in Abwassern
der Papiererzeugung," Wochenblatt fur
Papierfabrikation, 23/24 (1988)1021-1032.
—5—

NPDES WASTE LOAD ALLOCATION
PERMIT NO.: NC0006009
PERMITTEE NAME: Burlington Industries _
FACILTI'Y NAME: r '•n orirInclustffes Carole en
p ..
Facility Status: Existing 4 lj- f '
Permit Status: Renewal
Major Minor
Pipe No.: 001
Design Capacity: 0.018 MGD
Domestic (% of Flow): 100 %
Industrial (% of Flow):
Comments:
RECEIVING' STREAM: Second Broad River
Class: WS-III
Sub -Basin: 03-08-02
Reference USGS Quad: F11SE (please attach)
County. Rutherford
Regional Office: Asheville Regional Office
Previous Exp. Date: 11/30/93 Treatment Plant Class: I
Classification changes within three miles:
Requested by: Charles Alvarez
Prepared by:
Reviewed y
Date: 6/8/93
Date: ? f 9 3
Date: �O
gh-
Modeler
Date Rec.
#
Drainage Area (mi ) d Avg. Streamflow (cfs):.?��
7Q10 (cfs) .$"d' Winter 7Q10 (cfs) Y6 30Q2 (cfs)
Toxicity Limits: IWC % Acute/Chronic
Instream Monitoring:
Parameters
Upstream
Downstream
Location
Location
Effluent
Characteristics
Summer
Winter
BODS. (mg/1)
30
NH3-N (mg/1) ,
L /
D.O. (mg/1)
n�
TSS (mg/1)
30
F. Col. (/100 ml)
200
pH (SU)
UV
P
i R
n n r�
AU'
111993
Comments:

Facility Name:
NPDES No.:
Type of Waste:
Facility Status:
Permit Status:
Receiving Stream:
Stream Classification:
Subbasin:
County:
Regional Office:
Re.questor-
Date of Request:
Topo Quad:
JUL 2 2 1993
FACT SHEET FOR WASTELOAD ALLOCATION
Request # 74961"
Burlington Industries t,4 0 1
5L-%j Li, U.3 ,a aL V
NNCC06009
100% Domestic
Existing
Renewal
Second Broad River
WS-III
030802
Rutherford
Asheville
Alvarez
6/10/93
F11SE
Stream Characteristic:
USGS #
Date:
Drainage- Area (mi2):
206-
Summer 7Q1,0 (cfs):
58
Winter 7Q10-(cfs):
86
Average Flow (cfs):
288
30Q2 (cfs):
IWC.(%):
Wasteload Allocation Summary
(approach taken, correspondence with region, EPA, etc.)
Facility requesting renewal of NPDES permit. Tech Support recommends renewal of existing
limits since facility has 100% domestic wastewater w/ no modifications.
Special Schedule Requirements and additional comments from Reviewers:
Recommended by: Date:
Reviewed by
Instrearn Assessmenj-
Regional isor
ly Permits Regional
RETURN TO TECHNICAL SERVICES BY:
7/14/93
AUG 1 7 1993

Existing Limits:
Wasteflow (MGD):
BOD5 (mg/1):
NH3N (mg/1):
.. DO (mg/1):
TSS -(mg/1):
Fecal Col. (/100 ml):
pH (SU):
Residual Chlorine (µg/l):
Temperature (°C):
"1
Recommended Limits:
Wasteflow (MGD):
BOD5 (mg/l):
NH3N (mg/1):
DO (mg/1):
TSS (mg/1):
Fecal Col. (/100 ml):
pH (SU):
Residual Chlorine (µg/1):
Temperature (°C):
CONVENTIONAL PARAMETERS
Monthly Average
'Summer Winter
0.018
30
monitor
nr
30
200
nt
monitor
monitor
Monthly Average
Summer Winter
0.018
30
monitor
nr
30
200
nr
monitor
monitor
Limits Changes Due To:
Change in 7Q10 data
Change in stream classification
Relocation of discharge
Changein wasteflow
Other (onsite toxicity study, interaction, etc.)
Instream data
New regulations/standards/procedures
New facility information
WQ or EL
MR
Parameter(s) Affected
1
Parameter(s) are water quality limited. For some parameters, the available load capacity of
the immediate receiving water will be consumed. This may affect future water quality based
effluent limitations for additional dischargers within this portion of the watershed.
• R
_X No parameters are water quality limited, but this discharge may affect future allocations.
.t

INSTREAM MONITORING REQUIREMENTS
Upstream Location:
Downstream Location:
Parameters:
Special instream monitoring locations or monitoring frequencies:
MISCELLANEOUS INFORMATION & SPECIAL CONDITIONS
J
Adequacy of Existing Treatment
Has the facility demonstrated the ability to meet the proposed new limits with existing treatment
facilities? Yes No
If no, which parameters cannot be met?
Would a "phasing in" of the.new limits be appropriate? Yes No
If yes, please provide a schedule (and basis for that schedule) with the regional
office recommendations:
If no, why not?.
Special Instructions or Conditions
Wasteload sent to EPA? (Major) (Y or N)
(If yes, then attach schematic, toxics spreadsheet, copy of model, or, if not modeled, then old
assumptions that were made, and description ,of how it fits into basinwide plan)
Additional Information attached? (Y or N) If yes, explain with attachments.

MEMO
TO: �l l''' e
T�IVfh
�`1L✓ )n)i
y
u
jo
From:
�I'AJ �dl�- � lek
SUBJECT: %� ({d tNg7t�N C4r0%PefU �1a�
&- xo ctV, 7'0,- 5
Se ti
15 lJ L5 � V 15
AUG 1 11993
WATER QUALI'i;' SECTION
ASHEUILL REGIONAL/km-z_-
OFFICE '
C crVC S �
STATE
� Q. -t North Carolina Department of Environment,
Health and Natural Resources
Printed on Recycled Paper
s wun •neE

mown
PM PMR
Burlington Industries, Inc. Executive Offices
P. 0. Box 21207
Greensboro, North Carolina 27420
CERTIFIED MAIL -
RETURN RECEIPT REQUESTED
July 28, 1993
L^s -
North Carolina Department of Environment,
i
Health and Natural Resources
Permits and Engineering Unit
Division of Environmental Management =.
Post Office Box 29535
Subject: Burlington Industries Caroleen Plant
NPDES Permit No. NC0006009
Renewal Application
Attention: Mr: Charles Alvarez
Dear Mr. Alvarez:
In a letter dated May 18, 1993, Burlington Industries requested
renewal of the subject NPDES permit which expires on 11/30/93.
This renewal application requested deletion of outfalls 002, 003,
and 004 through which cooling tower blowdown was discharged. All
facility wastewater including cooling tower blowdown was to be
conveyed through the septic tank and sand filter system and out
outfall 001.
We have since determined that discharge of all cooling tower,
blowdown through outfall-001 will exceed the capacity of the sand
filter. We request that outfall 004 continue to be permitted. We
estimate the discharge through that outfall will be on the order of
11,500 gallons -per day. We have enclosed .a:revised_Short Form D,
which has been modified to reflect this cooling water discharge
(Attachment 1).
The cooling tower blowdown which will be discharged through outfall
004-.will-be treated with the biocide Nalco 2593. A; biocide .
worksheet for this discharge is,contained in Attachment 2.
Bleed -off from the 'air .washers will continue to be discharged
through the septic tank and sand filter system and out outfall 001.
This water will typically be treated, with Nalco 7346. A.biocide .
worksheet for this discharge is, contained in Attachment 2.- As
necessary, the air washer water may be treated with Nalco 2593
instead of Nalco 7346. Use' of Nalco 2593 has previously been
approved by the Division of EnvO ;n ental Management. A revised
� \NSA
n

ram\
July 28, -1993
Page 2
biocide worksheet for the discharge of Nalco 2593 through outfall
001 is also contained in Attachment 3.
Material safety data sheets and decay rate data for the biocides
are contained in Attachment 4. The biocide worksheets have been
prepared based on average daily discharge volumes and normal
operation.
Please contact Miriam White, Division Environmental Engineer, at
[phone] or Jake Wilson, Plant Engineer,- at'[phone]
with any questions.or.comments regarding this permit application.
J - ely,
H. Klein
Director of Corporate
Engineering
cc: M. White
J. Wilson
S. Meador
I
L.

F
IAP
DEFT. OF' 'URAL RESOURCES AHD COMMNITy(� lELOPME?(T
iET{TAL MANAGEMEN` eA' ISSION
i, POLLUTANT DISCHARGE ELIMINATION SYSTEMArvLrrAtlOn �a,n�Ea
TION FOR PERMIT TO DISCHARGE - SHORT FORM G Foa
AGENCY
d only by services, w++olesale and retail trade. USE DATE aECEIVEn
om ercial establishments includtng'vessels
YEAR MQ. DAY
Do not attempt -to Complete this form without reading the accompanying instructions
[lease print or type
1. Name, Address, and teleohone'numbar of facility producing discharge
A.. Nave Burlington Industries Caroleen Plant
d. Street address Highway 22 A, 7=x 5
C. City Caroleen D. State NC
E. County Rutlierford
G. Telephone No. (704) r 657-6376 UPF. ► 28019
Area
Co de
2. SIC
(Leave.blank)
4. Number of employees 403
4. Nature Of business Yarn kanufacturing.
5. (a) Check here if discharge occurs all ytar)(, or
(b) Check the month(S) discharge occurs:
1.13 January 2. 0 February 3. (3 Karch 4.0 Apri 1 5. 0 May
6.0 June 7. O July d. O August 9.0 Septtnber 10.0 October
11. O November 12. a Dece.+ber
(c) How many days per reek:
1.131 2.0 2-3 3.0 4-S...
6. Types of waste water discharged to surface waters only••(check as ibplicable)
Discharge per
operating day
A. Sanitary, daily
average
I. Cooling.water, e:c.,
daily average
C. Other discharge(s),
daily average;
Specify*
D. Maximum per operat-
ing day for combined
discharge (,all types)
Flow, gallons per operating day
Volume treated btfore
discharging (percent)
0.1-999 1000-4999 1 5000-4999 10,000- 50,000 None 0.1= 30- 65- 95•
- 49,999 or more .- 29.0 $4.9 94.9 100
(1) (2) (3) (4) (5) (6) (7) (8) (9) (10)
X
*Limited amounts of water.generated from facility cleaning.

of the types of waste td�eiiClfird in item 6, either treated or wv-
,ni art di s cU rged to p l a cts o the r ti►ai+ surface wato n . ch AK k below
;aop (cable. N/A
wsu water is discharged to:
0.1-"9
{1)
1000-4"9
(2}
WOO-""
(3)
10,00049.999 "
S0.DW or We
A. MunlLipol te+w•r system
H, ikn�•rgr•�ru►�i wall
r. Septir -tank
D. Evaporation lagoon or pond
E. Other, specify:
8. Number of separate discharge points:
1�.Xh 1 5.X2-3 C.O;-S D.O 6 or non
9. Man* of receiving water or waters 2nd Broad River
.10. Does your discharge contain or is it possible for your discharge to contain'
one or wort of the following substances e44td as a result of your operations,
activities, or processes: aft+ta+ia, cyanide; a umimum, beryllium, cadmium,
chromium, copper, lead, vertu , nickel, selenium, zinc, p++enols, oil and
grtase, and chlorine (residual.
A.Xyes 3. r, no
1 certify that I in familiar with the inform tion contained in the application and
that to the best of my knowledge and belief tuch information is true, compiete. and
accurate.
Printed Mane of Person Signing �^
GvJa,N���t►rJC_
Title
Date Application Sign@
7
s
h Carolina General Statute 143-215.6(b)(1) provides that: Ahy parson who knowingly mYk!!1
false statement repreaentat on, or certification in any applicat�on,*record, report, pIan,
ther-document files or required to be =intained•undar Article 21 or regulations of the
ronnental M n.agement Commissf,on implpt*nVtng that Article, or who falsifies, tampers 'With.
zowly renders inaccurate any:rtcordfng or nonitorinj 4rvice or method required to be
3ted or maintained under (Mtale 21•: of regulations -of the KnvironnentaLl Hanagament Co=mi9M
anenting that Atticle, s1a1Vbe''Tdat- •pf k -ilsdemeat or punishable by a -fine not to exceed
VM, or by imprisonma.nt•not to exceed six months, or Lby both. (18 U.S.C. Section 1001 pra7_
iishment by a fine of'iiot more than $10.000' or iarpriso=tsnt not noraz than S years, or both,
a similar offense.)

BIOCIDEJCHEMICALTREATMENT
`-- WORKSHEET-FORM 101
- med on any biocidal products ultimately discharged to the surface waters of
=rns afe to be perfor ch biocidal product in use. This worksheet
completed separately for eais, to be
. wortcsheet must be P p erformed as indicated.
ropr;ate data.entered into the designated areas with calculations
apP
'== fall 004
Fac7;ty Name
Burlington Industries — Caroleen P an —
S # NC 0006009
NPDE 51.2
County
Rutherford 7Q10 (cfs)
Stream 2nd Broad River
Receiving , ,-_. --
lied b the Division of ciiviiv""1e" la' ,vianaye�„ s `stems to the 'receiving water body?
(All above information supp Y
What is the Average Daily Discharge (A.D.D.) volume of the water handling y
A.D.D. = 0.0115 (in M.G.D.) the data entered
Please calculat
e the Instream Waste Concentration (IWC in percent) of This discharge using
above.
(A\D.D.) x 100
IWC = (7Q10 x 0.646) + (A.D.D.)
0.035 %',
(.0115 ) X 100
( 51.2 ) (0.646) + (.0115)
o the receiving stream during low flow conditions.
This value (IWC) represents
the waste concentration t
le product chemical
treatment proposed for use, in the discharge identified in Part I?
What is the name of the who
Nalco 2593 Microbiocide
percent composition: 1,15
Please list the active ingredients and p %
5—chloro-2—methyl-4-isothiazolin-3—one 0.35 %
2—methyl-4—sothiazolin-3—one`%
0/0
en
i er, chromium, or zinc, also complete page 4,
Note: If ingredients contain the metals coPP
rams of whole
What feed or dosage rate (D.R.)
is used in this application? The units must be converted to g
product used per day.
D.R.= 2230 grams/day
D:E.M. Form 101 (7/92)
1

rF`rlington Industries. Caroleen Plant NPDES 1l: NC NC0006009
J.= ^outfall 004
to local volume of [lie water handling system between entry of biocidal product and NPDES discharge
r On an attached sheet please provide justification for this estimate (system volume, average cycles per
`bjowdown, holding lagoon size, etc.) Cooling Tower 1 • 4,320 gallons
Cooling Volume= 0.00864 million gallons g Tower 2: 4 , 320 gallons
What is the pH of the handling system prior to biocide addition? If unknown, enter N/A. 7.5 to 8.0 S.U.
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk.
The degradation must be staled at pH level within 1/2 pH standard unit within handling system. Enter the half
life (Half Life is the time required for the initial product to degrade to hall of its original concentration). Please
provide copies of the- sources of this data.
H.L. = 10 Days
The decay rate is equal to L. X 0.69 = 0.069 =Decay Rate (D.K.)
Calculate degradation factor (D.F.). This is the first order loss coefficient.
D.F. = A_( D.D.) + (D.K.) — ( .0115) + (0.069 ) = 1.40
(Volume) —(0.00864 )
Calculate Steady State "Discharge Concentration: 2230
(D.R.) _ ( ) 48.7
Dischg Conc. _ (D.F.)(Volume)(3785) _ ( 1. 40 )(0.00864 ) (3 7 8 5) = mgil
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischg. Conc.) x (IWC%) ( 48.7 ) x ( 0.035 ) 0.017
100 — - 100 = mg/)
Receiving Stream Concentration
-.Calculate regulated limitation.._
List all LC50 data available for the whole product according to the following columns. (Note that units should be
in mg/i). Please provide copies of the sources of this data.
Organism Test Duration LC50 (mgl)
Mysids
Sheepshead Minows
96 hrs
96 hrs
18
32
D.E.M. Form 101 (7/92) 2

l
riznaton Industries Caroleen Plant NPDES It: NC 0006009
rtpucfall 004
:} e the lowest LC50 listed above:
er the LC50: 18
`t1 the halt life (H.L.) is less than 4 days, perform the following calculation.
Regulated Limitation = 0.05 x LC50 = Mg/I
If the half life (H.L.) is greater than 4 days or unknown, perform the following calculation.
Regulated. Limitation = 0.01 - x LC50 = 0.18 mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
0.18 mg/liter
From Part II enter the receiving stream concentration:
0.017 mg/liter
Analysis.
It the receiving stream concentration is greater than the calculated regulated limitation, then this biocide is
unacceptable for use.
Name (Print) �.
_ 7-2 L 9�
Signature Date
Person in Responsible Charge - —
,Z00 3112�Q
00

'gurlington Industries Caroleen Plant NPDES it: NC 0006009
Outfall 004
x" Slrpulementa) Metals Analysls
wfr(,
zinc, or chromium are present in the proposed biocidal compound, complete this_ worksheets A
form must be used for each metal and/or metal compound present in the biocide. List the metal,
;al formula, molecular weight (MW), formula weight (FW), and the concentration of the metal
i in the biocide (MCC). Complete a separate form for every metal present in the biocide.
Chemical Formula Molecular Weight of Metal Formula Weiaht Concentration in Biocide
EXAMPLE'
Copper CuSO44 5H2O 63.546 g/mole 249.680 g/mole 0.2 %
topper _Cupric Nitrate 0_052 as Cis in biocide*
)osage rate of Bloclde (DR)_ (from page 1):
)R - 2230 -grams/day
%verage Daily Discharge (ADD) (from page 1):
kDD = 0.01.15 'million gallons/day
)Ischarge Concentration (DC) -of Bloclde:
)C = DR = 2230. - grams/day) 193,913 -grams/million gallons
ADD ( million gallons/day) _
;onvert DC to micrograms/liter (ppb):-
IC (µg/1) =19-3 91,3 DC (grams/million.gat) x 1 x 10 6 u 919 = 51,232 ug/i
3.785 x 106 liters/million g.al.
;alculate the traction of metal In the metal -containing compound (MF):
MW ( -grams/mole) _
IF = FW = ( grams/mole) 7�.
:alculate the fraction of metal In the blocidal compound (BF):
F = MF x. MCC
= x (100) % = 6.0005
alculate the concentration of metal In the discharge (M);
I -= DC x BF = 51,232 ug/l x 0.0005 a 25.6 ug/I
alculate the Instream metal concentration (IMC) at low -flow conditlons:
IWC % 25.6 0.035 % 0.0090
7C = M x 100 = ug/l x - 100
= ug/l
egulated limitation of metal (from below): ug/i
NU uenetal Statutes toA NuAL, zty.uz I I uellne:
Copper- 7 µg/l water quality action level' Zinc- 50 µg/l water quality action level'
Chromium- 50 µg/1 water quality standard
('Values'which exceed action levels must be addressed directly by aquatic toxicity testing.)
9!
T) T7 M T-nrm 101 (7/92) 4 1

.d
Facility Name:
NPDES No.:
Type of Waste:
Facility Status:
Permit Status:
Receiving Stream:
Stream Classification
Subbasin:
County:
Regional Office:
Requestor:
Date of Request:
Topo Quad:
FACT SHEET FOR WASTELOAD ALLOCATION
Burlington Industries - Caroleen
NNCC06009
100% Domestic
Existing
Renewal
Second Broad River
WS-III
030802
Rutherford
Asheville
Alvarez
6/10/93
F11SE
Request #
7490
J11L 2 L 1993
i
Stream Characteristic:
USGS #
Date:
Drainage Area (mi2): 206
Summer 7Q10 (cfs): 58
Winter 7Q10 (cfs): 86
Average Flow (cfs): 288
30Q2 (cfs):
IWC (%):
Wasteload Allocation Summary
(approach taken, correspondence with region, EPA, etc.)
Facility requesting renewal of NPDES permit. Tech Support recommends renewal of existing
limits since facility has 100% domestic wastewater w/ no modifications.
Special Schedule Requirements and additional comments from Reviewers:/----
/a,
Recommended by: �• Date: 7/14/93 _
Reviewed by
Instream Assessment: Date: 7 9
Regional isor: Date:
Permits ngineering: Date:
AUG 17 1993
RETURN TO TECHNICAL SERVICES BY:

CONVENTIONAL PARAMETERS
Existing Limits:
Monthly Average
Summer Winter
Wasteflow (MGD):
0.018
BODS (mg/1):
30
NH3N (mg/1):
monitor
DO (mg/1):
nr
TSS (mg/1):
30
Fecal Col. (/100 ml):
200
PH (SU):
nr
Residual Chlorine (µg/l):
monitor
Temperature ("C):
monitor
Recommended Limits:
Monthly Average
Summer Winter WQ or EL
Wasteflow (MGD):
0.018
BODS (mg/1):
30 EL
NH3N (mg/1):
monitor
DO (mg/1):
nr
TSS (mg/1):
30 EL
Fecal Col. (/100 ml):
200
PH (SU):
nr
Residual Chlorine (µg/1):
monitor
Temperature (°C):
monitor
Limits Chanaes Due To:
Change in 7Q10 data
Change in stream classification
Relocation of discharge
Change in wasteflow
Other (onsite toxicity study, interaction, etc.)
Instream data
New regulations/standards/procedures
New facility information
Parameter(s) Affected
Parameter(s) are water quality limited. For some parameters, the available load capacity of
the immediate receiving water will be consumed. This may affect future water quality based
effluent limitations for additional dischargers within this portion of the watershed.
CAM
_X_ No parameters are water quality limited, but this discharge may affect future allocations.

3
INSTREAM MONITORING REQUIREMENTS
Upstream Location:
Downstream Location:
Parameters:
Special instream monitoring locations or monitoring frequencies:
MISCELLANEOUS INFORMATION & SPECIAL CONDITIONS
Adequacy of Existing Treatment
Has the facility demonstrated the ability to meet the proposed new limits with existing treatment
facilities? Yes No
If no, which parameters cannot be met?
Would a "phasing in" of the new limits be appropriate? Yes No
If yes, please provide a schedule (and basis for that schedule) with the regional
office recommendations:
If no, why not?
Special Instructions or Conditions
Wasteload sent to EPA? (Major) (Y or N)
(If yes, then attach schematic, toxics spreadsheet, copy of model, or, if not modeled, then old
assumptions that were made, and description of how it fits into basinwide plan)
Additional Information attached? (Y or N) If yes, explain with attachments.

SOC PRIORITY ,,OJECT.- Yes No X
IF YES, SOC NUMBER
TO: PERMITS AND ENGINEERING UNIT
WATER QUALITY SECTION
ATTENTION: Charles Alvarez
DATE: June 17, 1993
NPDES STAFF REPORT AND RECOMMENDATION
COUNTY Rutherford
PERMIT NUMBER NC0006009
PART I - GENERAL INFORMATION
1. Facility and Address: Burlington Caroleen Plant
Post Office Box 158
Caroleen, N. C. 28019
2. Date of Investigation: Margh 30, 1993
3. Report Prepared By: James R. Reid
f�
4. Persons Contacted and Telephone Number: Sam McKinney
704-657-6376
5. Directions to Site: Facility is located on US Hwy 221-A in
Caroleen (Rutherford Co) near the point at which the highway
crosses the Second Broad River.
6. Discharge Point(s), List for all discharge points:
Latitude: 350 16' 45" Longitude: 810 48' 00"
Attach a USGS map extract and indicate treatment facility site and
discharge point on map.
U.S.G.S. Quad No. U.S.G.S. Quad Name Forest City, N. C.
7. Site size and expansion area consistent with application?
_X_ Yes No If No, explain:
8. Topography (relationship to flood plain included): Flat area
adjacent to flood plain.
Page 1

1
` 9. Location of nearest dwewling: Apprnd-amtely 500 feet.
10. Receiving stream or affected surface waters: Secnond Broad River.
a. Classification: C
b. River Basin and Subbasin No.: BRD 030802
C. Describe receiving stream features and pertinent downstream
uses: Source of process water, wildlife support, recreation,
and agriculture.
PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS
1. a. Volume of wastewater to be permitted 0.018 MGD (Ultimate
Design Capacity)
b. What is the current permitted capacity of the Wastewater
Treatment facility? 0.018
C. Actual treatment rapacity of the current facility (current
design capacity 0.018
d. Date(s) and construction activities allowed by previous
Authorizations to Construct issued in the previous two years:
None
e. Please provide a description of existing or substantially
constructed wastewater treatment facilities: Septic tank,
surface sand filter., chlorination.
f. Please provide a description of proposed wastewater treatment
facilities:
g. Possible toxic impacts to surface waters: None anticipated.
h. Pretreatment Program (POTWs only):
in development approved
should be required not needed X
2. Residuals handling and utilization/disposal scheme: Septage hauler
with disposal at Cone Mills Cliff_si.de or the Town of Spindale.
a. If residuals are being land applied, please specify DEM
Permit Number
Residuals Contractor
Telephone Number
b. Residuals stabilization: PSRP PFRP OTHER
Page 2

c. Landfill•
d. -Other disposal/utilization scheme (Specify):
3. Treatment plant classification (attach completed rating sheet): I
4. SIC Codes(s): 2211
Wastewater Code(s) of actual was not particular facilities
i.e., non -contact cooling water discharge from a metal .plating
company would be 14, not 56.
Primary 02 Secondary 14
Main Treatment Unit Code: .46007
PART III "OTHER"PERTINENT INFORMATION
1. Is this facility being constructed with Construction Grant -Funds
or are any public monies involved. (municipals only)?
2. Special monitoring or limitations (including toxicity) requests:
r
3. Important SOC, JOC, or Compliance Schedule dates: (Please
indicate)
Date
Submission of Plans and Specifications,
Begin Construction
Complete Construction
4. Alternative Analysis Evaluation: Hasthe facility evaluated all
of the non -discharge options available. Please provide regional
perspective for each option evaluated.
Spray Irrigation:
Connection to Regional Sewer System:
Subsurface:
Other disposal options:
5. Other Special Items:
Page 3

FART IV - EVALUATION AND RECOMMENDATIONS
vid
Facility -is consistent l.y4operated. Re__new permit with only one
discharge pipe 001 (all cooling water, have been connected to the
WWTP operatin as �ipe 001).
ign ure of Report Preparer
r
W ter Quality Regional Supervisor
/? /ss3
ate
Page 4

O i
948
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427 4]' ou CL FFSIDE 1.3 Ml.,'y 430OOOm E IM ERIOP.--C EOlD6iCAl SURVEr
CHESNEE, S. C. II MI. \ iCLIFFSIDE 0-4, MI.
-- 1 MILE ROAD CLASSIFICATION
6000 7000 FEET
1 KILOMETER Heavy-duty Light -duty. .
Medium -duty Unimproved dirt
U. S. Route 0 State Route

Name of Pla`,_
Owner or Contact Person:l)vs�,r
Mailing Address: 'T
County: �R,)4h" Telephone: -?yrl_
NPDES Perm No. NC00 D U Nondisc. Per. No.
IssueDate: /0 U O Expiration Date: 3 j 3 O
f _
Existing Facility Li New Facility
Rated By: �Avt&s-s !2 -2 i r�? Date: 3
Reviewed -(Train. & Cert.) Reg. Office
Reviewed (Train. & Cert.) Central Office
OR `]t
AAlj0 `NrJ Grade
Plant Class: (circle one)
ITEM
POINTS
(1) Industrial. Pretreatment Units and/or
Industrial Pretreatment Program
(see: definition No. 33) 4
(2) PaalSi.FLOW OF PLANT IN GPD
(not applicable to non -contaminated cooling waters, sludge
handlrng facilities. for water purification plants, totally,
closgdr::cycledsystems(def.,Nor:11),-and facilities
consiSling; only -of-- Item, (4) (d)' or Items (4) (d) and -(11)
0 -- 20,000..........................
20,001 - 50,000.......................... 2
.........:
s 3
100001 -- 250,000......... ? 4
250:001 - 500,000 ............ .
SOO,OI)1: _ ......... 5
1,000,001 -- 2;000,000 .... :. - - _
and u .. • . • • • 10
2,000,001
( p) - rate 1 point additional for each
200,000,gpd capacity up to a
%-,maximum7of=-30
-
Design- Flow (gpd) ;
(3) PRELIMINARY.,UNITS (see definition no. 32)
Screens..:.... :: 1
....
Mechamcal Screens, Static Screens or
(,Comminuting:.,Devices .
c) -Grit Removal ... 1
or
(d) Mechanical or Aerated Grit Removal :.:.. , • ; _ • 2
(e) Flow Measuring Device .......................
or 1
(f) Instrumented Flow Measurement .. ........ . • �
(g) Preaeration .......... (
(h) Influent Flow •Equaliza[ion ................... 2
(i) Grease or Oil Separators - Gravity ........ 2
Mechanical .......... 3
Dissolved Air Flotation. 8
6) Prechlodnalion 5
(4) PRIMARY TREATMENT UNITS
(a) Septic Tank (see definition no. 433 .............. r2 (b) Imhoff Tank .... .............................. 5
(c) Primary Clarifiers .... .
• (d) Sell ling Ponds or Settling Tanks for Inorganic 5
Non -toxic Materials (sludge handling facilities
for water purification plants, sand, gravel,
stone, and other mining operations except
recreational activities such as gem or goid
mining) . • .. , .................................. 2
Total j5;jo nts
(5) SECONDARY TREATMENT -UNITS
(a) Carbonaceous: Stage
(i)Aeration - High Purity Oxygen System ... • .
Diffused Ail System
Mechanical Air System (fixed,
floating.or rotor)
:•.: !S.eparate:Sludge, Reaeiatior�' _ _
Trickling7,,Filter
High: Rate.._........: "
Standard Rate .......
Packed•Tower: ..-.:
(i i i) Biological=iAerated'_Filter: or Aerated•= _ .
Biological Filter ................... .
(iv) Aerated Lagoons ...........
(v) Rotaling'Bioloigic4'Contactors '; ; .`_ •'
(vi) Sand -Filtei5-'
intermittent biological
reclrculaUngiologtcal''"
(vii) Stabilzahon�Lagoons .... .
(viii)Clarifier .:
(ix) Single stage s(Istem .foY'combined
carbonaceous removal of"BOD °arid --'
nitrogenous removal by_' nil�ific�tron
(see def.<-No. 2)' (Points' for';this. item"
have to' be in 'a'dc)itiow lo` items `(5)' (a) ° {' •
(i) throu9h`(5)-`(a) (vitiryr=:`.:
(x) Nutrient•,addit%ns to enhance BOD
removal-..
(xi) Biological Culture ("Super Bugs") addition
to enhance"organ "C",6 mpound remo,val :
(b) Nitrogenous Stage •-`-:�rF
(i) Aeialion High -Purity Oxygen System
Diffused Air -System-
:,°> `liieohtan'icah'Air'Sysl"em (fixed,-"
ti Sepaiale Sludge Reaeralion .....
(ii) Trickling Filler�-
High Rate'.. , . _ • . • .. _
Standard, Rate ............
Packe`6T6wer..........
(iii) Biological Aerated Filter or Aerated
Biological Filler ............
(iv) Rotating Biological Contactors ........... .
(v) Sand Filler -
intermittent biological ....... .
recirculating biological . . . .
(vi) Clarifier ... ..... . . . ................... .
20
10
8
3
7
5
5
10
10
10
C`2
3
5
8
5
5
20
10
8
3
7
5
5
10
10
2
3
5

,,6) TERTIARY Oil ADVANCED TREATMENT U,
(a)
Activated Carbons Beds - ,
without carbon regeneration .............. ... .
5
with carbon regeneration .........
1 5
(b)
powdered or Granular Activated Carbon Feed -
without carbon regeneration .................
5
with carbon regeneration ...................
is
(c)
Air Stripping ................... . . . . . .....
5
(d)
Denitrification Process (separate process) . . . . .
1 0
(e)
Electrodialysis ..............................
5
(f)
Foam Separation .............................
5
(g)
Ion Exchange ................................
5
(h)
Land Application of Treated Effluent
(see definition no. 22b) (not applicable for
sand, gravel, stone and other similar mining
operations)
(i) on agriculturally managed sites (See del.
No. 4) ...................................
1 0
(ii) by high rate infiltration on non -agriculturally
managed sites (includes rotary distributors
and similar fixed nozzle systems) ...........
4
(iii) by subsurface disposal (includes low pressure
pipe systems and gravity, systems except at.
plants consisting of. septic lank and nitrifica-
tion lines only) .............................
4
(i)
Microscreens..................................
5
(j)
Phosphorus Remoral by Biological Processes
(See def. No. 26) ............................
20
(k)
Polishing Ponds - without aeration .......
2
with aeration ..........
5
(1)
Post Aeration - cascade ..............
0
diffused or mechanical ...
5
(m)
Reverse Osmosis ...............................
5
(n)
Sand or Mixed -Media Filters - low rate ...........
2
high rate ..........
5
(o)
Treatment processes for removal of metal or
cyanide......... i�............................
15
(p)
Treatment processes for removal of toxic
materials other than metal or cyanide .........
1 a
SLUDGE TREATMENT
(a)
Sludge Digestion Tank - Healed ...............
10
Aerobic ...............
5
Unheated .............
3
(b)
Sludge Stabilization (chemical or thermal) .......
5
(c)
Sludge Drying. Beds - Gravity .................
2
Vacuum Assisted .......
5
(d)
Sludge Elutriation .............................
5
(e)
Sludge Conditioner (chemical or thermal) ...... _ .
5
(f)
Sludge Thickener (gravity) ......................
5
(g)
Dissolved .Air, Flolalion Unit
(not applicable to,,a unit rates as (3) n .........
'8
(h)
Sludge Gas Utilization (including gas storage) ....
2
(i)
Sludge- Holding Tank - ,Aerated .................
5
Non -aerated .............
2
(j)
Sludge Incinerator - (not including,. activated
carbon regeneration)......
10
(k)
Vacuum Filler, Centrifuge or Filler Press or other
similar dewalering devices ........ :.. 4 ........
10
(8);SLUDGE DISPOSAL (including incinerated ash)
(a) Lagoons__. ...............................
2
(b)
Land Application (surface and subsurface)
(see definition 22a)
-where the facility holds the land app. permit ..
1.0
-by contracting to a land application operator who
holds the land application permit .............
-land application of sludge by a contractor who does
not ho!d the permit for the wastewater treatment
facility where the sludge is generated ........ _
10
(c)
Landfilled (burial) . _ ............................
5
(9) DISINFECTION
(a)
Chlorination .. . . . . . .. . .............. .....
(b)
Dechlorination ........................
5
(c)
Ozone ..............................
5
(d)
Radiation ..........................
5
(10) CHE-MICAL ADL )tJ SYSTEM (S) (See definition No 9)
(not applicao e 10 chemical additions rated as ilern .
(3) (I). (5) (a) (xi). (5) (a). (5) (b). (7) (b). (7) (e).
(9) (a), (9) (b), or (9) (c) 5 points each: List:
c
c
c
c
(t1) MISCELLANEOUS UNITS
(a) Holding Ponds, Holding Tanks or Settling Ponds
for Organic or Toxic Materials including wastes
from mining operations containing nitrogen and/or
phosphorous compounds in amounts significantly
greater than is common for domestic wastewater .... 4
(b) Effluent Flow Equalization (not applicable to storage
basins which are inherent in land application systems). 2
(c) Stage Discharge (not applicable to storage basins
inherent in land application systems ........................................ 5
(d) Pumps._ ...... :...................... -.............................................
(e) Stand -By Power Supply.................................................................. 3
(f) Thermal Pollution Control Device ............................................. 3
TOTAL POINTS
CLASSIFICATION
Class I........_._.._ .:............... ...... _........ ...... 5 25 Points
Class Il......... ...... ...................
...... - ........ __.. 26- 50 Points
ClassIII ............. _.......................................:.4 51- 65 Points
Class IV ................................................... 66- Up Points
Facilities. having a rating of one through foul points, inclusive,
do not require.a certified operator. •_;Classificaliori- of all -other
facilities requires a comparable grade operator in responsible
charge. .
Facilities having an activated sludge process will be assigned
a minimum classification of Class If.
Facilities having treatment processes for. -the' removal of metal
or cyanide will be assigned a minimum classification of Class 11.
Facilities having treatment processes for the biological removal
of phosphorus ' will be _assigned a. minimum classification of Class
In -plant processes and related control equipment which are an
integral part of industrial production shall not be considered waste
treatment. Likewise, discharges of wastewater from residences
having a design flow of 1.000 gpd or less, shall.not be subject to
rating. . _ .
ADDITIONAL COMMENT -

a: -
State of North Ca na
Department of Environment,
Health and Natural Resources
Division of Environmental Management
\ James B.. Hunt, Jr., Governor
J Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
J` t
June 3, 1993
Ar4
�EHNF = I
Fju-N 7 1993
VA
0
Mr. Philip H. Klein Subject: NPDES Permit Application
Burlington Industries PO BOX 158 NPDES Permit No.NC0006009
Caroleen, NC 28019 Burlington Industries
Dear Mr. Klein.: Rutherford County
This is to acknowledge receipt of the following documents on May 26, 1993:
Application Form
Engineering Proposal (for proposed control facilities),
Request for permit renewal,
Application Processing Fee of $400.00,
Engineering Economics Alternatives Analysis,
Local Government Signoff,
Source Reduction and Recycling,
Interbasin Transfer,
Other Sludge Management Plan, Biocide Sheets,
The items checked below are needed before review can begin:
Application Form
Engineering proposal (see attachment),
Application Processing Fee of
Delegation of Authority (see attached)
Biocide Sheet (see attached)
Engineering Economics Alternatives Analysis,
Local Government Signoff,
Source -Reduction and Recycling,
Interbasin Transfer,
Other
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX 91'9-733-9919
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post-consuiner paper

If the application is not made complete within thirty (30) days, it will be
returned to'you and may be -resubmitted when complete.
This application has been assigned to Charles Alvarez
(919/733-5083) of our Permits Unit for review. You will e a vise of any
comments recommendati-ons, questions or other information necessary for the
review of the application.
I am, by copy of this letter,'requesting that our Regional Office
Supervisor prepare a staff report and recommendations regarding this
discharge. If you have any questions regarding this applications,
please contact the review person listed -above.
Sincerely;
— ' CC: Asheville Regional Office Coleen H. Sullins, P.E.
a

NVRTHCAROLINA DEPT. OF NATURAL RESOURCES AND COlftNITY DEVELOPMENT
ENVIRONMENTAL MANAGEMENT COMMISSION
NATIONAL. POLLUTANT DISCHARGE ELIMINATION. SYSTEM AtvLlrAtlON 1umm
APPLICATION FOR PERMIT TO DISCHARGE - SHORT FORM G FOR 0 0 l a a
AGENCY o
to be filed otily by services. wholesale and retail trade. USE • DATE RECLIVIn
and other commercial establishments including vessels Pq 1 5-1 71 S ';2, b
TEAll Mo. DAY
Do not attempt to co.Qlete this form without reading the accoapanying instructions � 40 0.0
Please print or type �r3"
1. Name, address, and telephone number of facility producing discharge
A. Nsme Burlington Industries Caroleen Plant
8, Street address Highway 22 A,Box 5•6
C. City Caroleen D. State NC
E. County Rutherford F. jlp 28019
G. Telephone No.. [phone]
Area
Code
2. SiC
(Leave blank) L
3. Number of employees 403
4. Nature of business Yarn Manufacturing
T •�
5. (a) Check here if discha �' rn ZZ
discharge occurs all year or
(b) Check the month(s) discharge occurs:
1. c January 2.O February 3.0 Marth 4.0 April 5.0 May — -
6.13June . 7.O July 8.0 August 9.0 Septesber 10.0 October
11.0November 12.0 December
(c) How many days per week:
2. 0 2-3 3.0 4-5. 4 .)(6-7
6. Types of waste water discharged to surface raters only•(check as applicable)
Discharge per
operating day
A. Sanitary, daily
average
8. Cooling water, etc..
daily average
C. Other discharge(s).
daily average;
Speciry*
D. Maximum per operat-
ing day for combined
discharge (all•types)
I Flow, gallons per operating day
0.1-999 1000-4999 5000-4999 10.000-
49.999
(1) (2) (3) (4)
X
X
X
X
*Limited amounts of water generated from facility cleaning.
Volume treated before -
distharging (percent)
$0.000 clone 0.1- 30- 65- 95.
or more 29.9 64.9 9/,4 100
,(s) (6) (7) (8) (9) (10)
X
. I 1 .I 1X -

r�
of the types of taste Identified in item 6, either treated or Vn-
` treated. are discMrged to places other tMn Surface 'wsters, check below
as applicable. N/A
Waste water is discharged to:
0.1-999
(1)
1000-4M
(2)
S000-9lf9
(3)
10,00049."11
(4)
SO.D00 or more
(S)
A. KmIt pal %ew•r System
N. Ikni•rgt•auttl M•11
C. eptir -tank
D. Evaporation lagoon or pond
E. Other, specify:
8. Mumber of separate discharge points:
A.)k1 11.132.3 C.13 4.5 0.a 6 or Iwre
9. Name of receiving water or waters 2nd Broad River
.10. Does'your discharge contain or Is it possible for your discharge to contain
one or more of the following substances jj= as a result of your operations, ,
activities, or processes: amnunis, cyanid', aluminum, beryllium, cadmium,
chromium, copper, lead, mercu , nickel, selenium, tint, phenoli, •il and �v
grease, and chlorine (rtsldual�.
A.Xyes S.Qno a
1 certify that i in familiar with the information contained in the application and -
that to the best of my knowledge and belief such information Is true, complete, and --
accurate.
Printed K of Person Signing
/71t1t
Date Application Sig d
Sig re of Applicant
� -17
•_
r.
ram'.
jZ
crz
th Carolina General Statute 143-215 .6 (b) (2) provides that: Any person who -knowingly mako.5
falsa statement representation, or certification rz any applicat�on,*record, report, plan,
other document files or required to be maintained*undsr Article 21 or regulations of the
ira=e.atal M- anagement Commission implomant$.ng.that Article, or vho falsifies, taaroers v th.
knowly renders inaccurate any• r6co>;ding or nonitoritlg 4svice or Method required to be
rated or maintained under Ap�XQ1e 2.1•: ot- regulatiocs -of the Environzeatal Management Co=missi
lementi'ng that Article, ahaZ3''be'=j�tiro .vf it misdemeanor punishable by a -fine not to exceed
.001, or by imprisonm}nt•not to exceed six months, or by both. (18 U.S.C. Section 1001 prnv:.
unishment by a fine of"mot more than $10,g00'or imprisonaant not nore than 5 years, or both,
a similar offense.)
0

_ 1
MEMORA-- DUM:
DIVISION OF ENVIRONMENTAL MANAGEMENT
To: Charles Alvarez
Hugh: .Matt klatthews IY\.0,11
rom: Melissa Rosebrock �tU'
Subject:
sub
dail
June 22, 1993
Burlington Industries-Caroleen Plant
Use of Biocides
NPDES No. NC0006009 '
Rutherford County
Burlington Ind ustries-Caroleen Plant has submitted Nalco 259') microbiocide for review. Data
itted by the subject facility concerning the dosage rate of the compound, system volume, average
discharge, and minimum stream flow have also been reviewed and evaluated.
In reviewing the submitted materials, it was noted that both the cooling tower blowdown
(containing -Nalco 259')) and the sanitary wastewater are treated and discharged through outfall 001.
Burlington Industries-Caroleen Plant does not need approval from our office for biocide use because
there is no direct discharge. All cooling tower blowdown is first discharged to the septic tank sand filter
and then discharged through outfall 001 to the Second Broad River. However, Jim Reid (Asheville
Regional Office 6/8/9') phone conversation) felt that the septic tank sand filter would only provide an
additional retention time of 24-48 hrs. and not actually treat the biocide and requested that the use of the
biocide be reviewed.
While reviewina the submitted Biocide 101 Worksheet, we found a discrepancy in the toxicity
data supplied by the facility. The more appropriate LC50 value would be 0.12 reported for the 6 day
acute fathead minnow test (see page 6 of 10 of the attached MSDS). The toxicity data reported was for
the -active ingredient and since the facility will.be using a 1.5% active formulation we have made the
appropriate conversion. Calculations summarized on the accompanying worksheet predict that the use
of this compound at the stated rates and retention times will not result iii toxic impacts to aquatic life in
the receiving stream. Therefore, the use of Nalco 2593 as a biocide at Burlington Industries-Caroleen
Pla it is deemed acceptable.
If there are questions regarding this review please contact me at [phone].
t
Att chments
cc: or -rest Westal'1AR.O >t° .. D k -u U L
Central files
F-J-LN 2 4 IM
VVi11 ER UJAUTY SECTIM
�SHEVILLE REGIOI AL -OFFICE

Burligton Industries-Caroleen Plant BIOCIDE WORKSHEET
PERMIT#: NC0006009
RECEIVING STREAM: Second Broad River
7010 (cfs): 45.00
I.W.C.%: 0.017
PRODUCT: Nalco 2593
ACTIVE INGREDIENT: 5-CHLORO-2-METHYL-4-ISOTHIAZLOIN-3-ONE 1.15%
2-METHYL-4-ISOTHIAZOLIN-3-ONE 0.35%
Cupric nitrate 0.05%
HALF LIFE (DAYS):
10.50
LC50 OF SELECTED TOX DATA (MG/L):
8.00
DECAY RATE:
0.07
DOSAGE RATE (GRAMS/DAY):
21.00
AVG DAILY DISCHARGE (MGD):
0.005
VOLUME OF SYSTEM (MIL. GAL'S):
0.043
STEADY STATE DISC CONC: 0.7090
DEGRADATION FACTOR:
0.182
APPLICATION FACTOR:
0.010
INSTREAM BIOCIDE CONC:
0.0001
REGULATED LIMITATION:
0.08
PASS/FAIL:
PASS
C

DIVISION OF, ENVIRONMENTAL MANAGEMENT
. Water Quality -
Permits and Engineering Unit
June 3, 1993
To: Melissa Rosebrock, Aquatic Toxicology
From: Charles Alvarez, Environmental Engineer, NPDES Permits
Subject: Burlinton Industries, NC0006009, Rutherford County
Caroleen Plant, Biocide Review '�
Attached is a copy of the 101 Worksheet for Burl. Ind. - Caroleen
Plant. Please review the biocides used and comment whether they
are appropiate at the concentrations used. If you need any more
information please call me at 733-5083 ext 537.
AN 0 7 1991
BVIRO-WENTAIL SCIENCES' BRAI%,Ch

/^ 71%
1+~
Burlington House Fabrics Group A division of Burlington Industries
P.O. Box 691
Burlington, N.C. 27215
May 18, 1993
North Carolina Department of Environment, CERTIFIED MAIL i
Health and Natural Resources RETURN RECEIPT REQUESTER -.'.
Permits and Engineering Unit
Division of Environmental Management.
Post Office Box 29535 ' =
Raleigh, North Carolina 27625-0535 `y
Subject: NPDES Permit No. NC0006009
Renewal Application
Attention: Ms. Coleen Sullins, P.E.
Supervisor, NPDES Permits Group
Dear Ms. Sullins:
We hereby request renewal of NPDES Permit No. NC0006009 which
expires on 11/30/93. We have attached three completed application
forms (Attachment 1) and the permit application processing fee for
major modifications of $4.00.
Only sanitary wastewater (including extremely limited amounts of
water from facility cleaning) and cooling tower blowdown are
discharged from this facility. Previously, the sanitary.wastewater
had been -discharged through outfall 001, and the cooling tower
blowdown had been discharged through outfalls 002, 003, and 004.
We have modified our piping system, and both: --sanitar-y.;:.Wastewater
and- _cool_ ingv :tower-- blowdown -;are-:: treated: - and- discharged:..; through
=outfall''' 001: Only stormwater is -now discharged through outfalls
002, 003, and 004. The renewal permit should, therefore, not
,include the discharge of cooling tower blowdown through outfalls
002, 003, and 004.
The cooling tower blowdown does contain a biocide. Use of this
biocide has previously been approved by the Division of
Environmental Management (Attachment 3). Based on a review of the
biocide worksheet, we have determined that our usage of the biocide
results in discharge concentrations below those previously
approved. We have at a revised biocide worksheet which
includes the supplemental metals analysis (Attachment 2).
NO
r\.1 c'�

May 18, 1993
Page 3
We request our permit be modified to specify reporting of • daily
flow not instantaneous flow for discharge 001.. Our present flow
measurement system consists of a calculation based on the number of
times the dosing 'tank discharges to the sand filters. Each
discharge is registered on a counter. We. multiply the counter
number by the dose tank volume to monitor our flow.
Your' letter dated February 19, 1993 requires primary industries
complete a priority pollutant analysis, and new facilities evaluate
engineering alternatives. Based on conversations with Forest
Westall of your Asheville Regional office we understand those
requirements are not applicable to our facility as we do not
discharge process wastewater and are not considered a new facility.
f
Your February 19, 1993 letter also requests a description of sludge
management: Approximately 8,000 gallons of sludge are pumped from
the septic tank annually. 'This sludge is transported by Honeywagon
Express to the Cliffside or Spindale Wastewater Treatment Plants.
Please contact Miriam White at Burlington House Division
Engineering [phone], or Jake Wilson'at the Caroleen Plant
[phone]', with any questions or comments regarding this
permit renewal.
Sincerely,
BUA1,PGTON INDUSTRIES,, INC.
Philip H. Klein
Director of Corporate
Engineering
cc: M. White _
J. Wilson
S. Meador

w
ATTACHMENT I
NPDES PERMIT APPLICATION
Ji
I

X }
NORTH CAROLINA DEPT. OF Kt i-JRAL RESOURCES AND COMMUNITY
ENVIRONMENTAL MANAGEMENT COMMISSION-.
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
APPLICATION FOR PERMIT TO DISCHARGE - SI4ORT FORM D
To be filed otily by services, wholesale and retail trade,
and other commercial establisiv#ents including vessels
DEVELOPMENT
FOR
AGENCY
USE
APPL I W I ON i t of R
d
62ad6ao9
DATE RECEIYtU
3
a
'L �. DAY
Do not attempt to complete this fors without reading the accompanying instructions 5 SG00 0 a
Please print or type
1. N w.. address, and telephone nuwber of facility producing discharge
A. Nine Burlington Industries Caroleen Plant
B. Street address Highway . 22 A,Box Ibb
C. Ci ty Caroleen D. State NC
E. County Rutherford F. ZIP 28019
G. Telephone No. [phone]
Area
Co de
2. SIC
(leave blank)
J'
3. Nvmber of employees 403
4. Mature of business — Yarn ManufacturinE
v
5. (a) Check here if dischrpe occurs all year, Or
a J
C-
(b) Check the month(s) discharge occurs:
1.0 January 2.0 February 3.0 Karch 4.0 April 5.0Kay c '
6.0 June 7. 0 July 8. a August 9.0 54ptr+btr 10. 0 October = i
11. 0 Hovemb•er 12. 0 Decawber
(c) How many days per week:
1.01 2.0 2-3 3.0 4-S. 4)6-7
6, Types of waste water discharged to surface waters only•(check as applicable)
IFlow, gallons per_operattng day _ _ I VOiu-e treated before
l - discharging (percent)
W,.6..
operating day
0.1-999 1000-4999 SOdO4999 10,0C+0-
50100o None
0.1-
30-
65-
95-
49,999
or more
29.9
64.9
94.9
100
(1) (2) (3) (4)
CS) (6)
(7)
(8)
(9)
(10)
A. Sanitary, daily
X
average
X
8. Cooling water, etc.,
daily average
X
X
C. Other diischarge(&),
..',
daily average;
X-
Y
specify*
ing day for combined
discharge (all, typef )
X
*.Limited amounts of water generated from facility cleaning.

y r�
1. If any of the types of Waste iL_: 'i`fied in item i,' auger treated, or VR-
d treated, are diScUrped to plans other UW Surface waters, Ch*Ck beta
as. applicable. N/A
Waste water is discharged to:
0.1-"9
1000-1ll9
S000-""
10,00049.M
50,000 or more
A. MunlLlpal ww•r %ystem-
H•Il.nli•rgnwuHl w�1I
..
-
C. Septlr•tank
U. Evaporation lagoon,' or pond
E. Other, specify:
a. Number of separate discharge points: ,
A.)61 E. 132-3 . C.93 I-5 D.a 6 or more
9. Nuue of receiving water or waters 2nd Broad River
.10. 0oe1`rour discharge'contain 'or is i.t possible for 'your discharge to contain
one or sore of the following substances Jd&Jas a result of your operations,
activities; or ,processes: jivonia, tyantde, ai uRinum, beryllium, Cadmium,
chrem iuw,.Copper, lead,'wercul, nickel, selenium, tint, phenols, N1 &W
grease, and -chlorine (residual). .
AXyes s.r,no
1 certify that i in familiar with the information contained iA the application and
that to�the best of my knowledge and belirf such infvsiation is true, CoMlets, and
accurate.
i
Printed Kawejo.f Person Signing
I�'ec av— 0f C_rQ0i-Atf— iNP�r'�iv�
Title
ace Application s1 d
Sig�Atare of Applicant
th Carolina General Statute "143-215.6(0(2) provides that: Any" person who knowingly >alki-3
false statement representations or certification is any application,'records report, plan,
other document files .or' required to be maintained.undar Articl•a . 21 or. regulations of the
'ironnental 'daaastm.ent Commission. implomonttag that Articles or who falsifies, taamers with,
knovly renders "inaccurste aay: ricor-ding or nonitorilj Ovice or taethod required to be
rated or maintained under'Xj�;tale.2.1•:ot regulatioe's•of the-Enviro=eUtsl Haaageesent Coasissi
lepentfng that Article, ehaZifbe'yul4ty, v 'a misdemeanor ,punishable by at •fine not to exceed.
!snoR, or by imprisonmiint, not to exceed. six months, or by both. (18, U.S.C. Segtiori 1001 prn7_
,unishment by a fine of'noi more than '$10;000. or" istpriaourent not nose than S -years, or both,
,.a -similar offense.)
J

ATTACHMENT 2.
BIOCIbE WORKSHEETS
I

4 1
Facility Name: Burlington Industries Caroleen Plant
NPDES it: NO NC0006009
Supplemental Metals Analysts
If copper, zinc, or chromium are present in the proposed biocidal compound, complete this worksheel. A
separate form must be used for each metal and/or metal compound present in the biocide. List the metal,
its chemical formula, molecular weight (MW), formula weight (FW), and'the concentration of the metal
compound in the biocide (MCC). Complete a separate form for every metal present in the biocide.
Metal Chemical Formula Moiocular Weight of Metal Formula Welglll
EXAMPLE
Copper CuSO4�5H20 .63.546 g/mole 249.680 g/mole
Copper Cupric Nitrate 63.546
Dosage rate of Blocfde (DR) (from page 1):
DR = _ 21 grams/day
Average Daily Discharge (ADD) (from page 1):
ADD = 0.005 . million gallonslday
Concentration in Biocide
0.2 %
0.05% as,Cu in biocide *
Discharge Concentration (DC) of" Blocfde:
DR ( 21 grams/days_ _ 4,200 grams/million gallons
DC = ADD _ (� million gallonslday).
Convert DC to micrograms/liter (ppb):
1 x 106 µq/q - 1,110 ugll
DC (µg/l) 4,200 DC (grams/million gal) x 6 -
3.785 x 10 liters/million gal.
Calculate the fraction of metal In the metal -containing compound (MF):
NNV grams/mole) _
MF = FW _ ( grams/mole)
.Calculate the fraction of metal in the biocidal compound (BF):
MCC % = x % __ 0.0005
BF = MF x 100 (100) - - - - - -
Calculate the concentration of metal in the discharge (M):
1,110 0.005 _ 0.555 ug/I
M=DCxBF= ug/Ix -
Calculate the instream metal concentration (IMC) at low -flow conditions:-.
0'. 017 % 0.00009
IMC = M x IWC % .555 = 0ug/I x 1 00 = ig/I
100
Regulated limitation of metal (from below): 7 ug/l
NC General Statutes 15A NCAC 2B.0211 define:
Copper- 7 µg/I water quality action level' Zinc- 50 µg/l. water quality action level'
Chromium- 50 µg/I water quality standard
('.Values'which exceed action levels must be addressed directly by aghatic toxicity testing.)
D.F.M. Fol-M 101 (7/92)

BIOCIDE/CHEMICAL TREATMENT
r
WORKSHEET-FORM 101
-he following calculations are to be performed on any biocidal products ultimately discharged to the surface waters of
,lorth Carolina. This worksheet must be completed separately for each biocidal product in use. This worksheet is to be
eturned with all appropriate data entered into the designated areas with calculations performed as indicated.
I. Facility Name Burlington Industries Caroleen Plant
NPDES # NC `• N0O006009
County- Rutherford
2nd Broad River 7Q10 45 (CIS)
Receiving Stream
(Ali above information supplied by the Division of Eniviroiimental f-vlan,agement)
What is the Average Daily Discharge (A.D.D.) volume of the water Dandling systems to the receiving water body?
0.005 (in M.G.D.) (Estimated average daily discharge of water treated
A.D.D.with biocide)
Please calculate the Instream Waste Concentration (IWC in percent) of this discharge using the data entered
above.
(A.D.D.) x 100 (•0.005) X 100
IWC = (7Q10 x 0.646) + (A.D.D.) ( 45 )(0.646) + -('0.005)
_ 0.017
This value (IWC) represents the waste concentration to the receiving stream during low flow conditions.
What is the name of the whole product chemical treatment proposed for use in the discharge identified in Part I?
Nalco 2593 Microbiocide
Please list the active ingredients and percent composition:
5-chloro-2-methyl-4 isothiazolin-3-one
- - - -1.15 %
2-methyl-4-isothiazolin-3-one
0.35 %'
o/
0
0
o/
0
Note: It ingredients contain the metals copper, chromium, or zinc, also complete page 4, qupplemenjal Metals Analysis
What feed or dosage rate (D.R.) is used in this application? The units must be converted .to grams.oi whole
product used per day.
D.R.= 21 grams/day'
D.E.M. Form 101 (7/92) 1

P.
Facility Name:
Burlington Industries Caroleen Plant NPDES 41: NC NC0006009
Estimate total volume of the water handling system between entry of biocidal product and NPDES discharge
point. On an attached sheet please provide justification for -this estimate (system volume, average cycles per
blowdown, holding lagoon size, etc.) _
Volume= 0.043 million gallons
7.5 to 8.0 S.U.
What is the pH of the handling system prior to biocide addition? If unknown, enter N/A.
What is the decay rate (D.K.) of the product? If unknown, assume no decay (D.K.=O) and proceed to asterisk.
The degradation must be stated at pH level within 1/2 pH standard unit within handling. system. Enter the half
life (Half Life is the time required for the initial product to degrade to half of its original concentration). Please
provide copies of the sources of this data.
H.L.= 10.5 Days (Half—life information provided by Nalco Chemical Company)
The decay rate is equal to - 1 X 0.69. 0.066 =Decay Rate (D.K.)
H.L.
Calculate degradation factor (D.F.). This is the first order loss coefficient.
A.D.D. 0.005 + ( 0.066) = 0.182
D.F. _ (Volume) + (D.K.) _ (U. U4J)
Calculate Steady State Discharge Concentration: 21 0.709
Dischg Conc. _ (D.R.) — I$2 ( 0.043 3 7 8 5) - mg/I
. (D.F.)(Volume)(3785) ( )( ) (
Calculate concentration of biocide instream during low flow conditions.
(Receiving Stream Concentration)
(Dischg Conc.) x (IWC%)
100
( 0.709 ) x ( 0.017 ) 0.00011
= 100
mg/I
Receiving Stream Concentration
III. Calculate regulated limitation.
List all LC50 data available for the whole product according to the following columns. (Note that units should be
in mg/l). Please provide copies of the sources of this data.
Organism Test Duration LC50 (mgl)
Mysids
Sheepshead Minows
-v
18
96 hrs
96 hzs 32
z. TIEN Fnrn-1 101. (7/92.) 9

_ t
Burlington Industries Caroleen Plant NPDES It: NC NC0006009
Facilil Name
Y
Choose the lowest LC50 listed above:
Enter the LC50: 18
If the half life (H.L.) is less than 4 days, perform the following calculation.
Regulated Limitation = 0.05 x LC50 = mg/I
If the half life (H.L.) is greater than 4 days or unknown, perform the following calculation.
Regulated Limitation = 0.01 x LC50 = 0.18 mg/I
Choose the appropriate regulated limitation from the calculations immediately above and place in this blank:
0.18
mg/liter
From Part II enter the receiving stream concentration:
0.00011 mg/liter
IV. .Analysis. ;
It the receiving stream concentration is greater than the calculated regulated limitation, then this biocide is
unacceptable for use.
Name (Print)
Signature Date
Person in Responsible Charge
r

ti
Estimate of total volume of water handling system between entry of
biocidal product and NPDES discharge point is based.on the volume
of water in'the.system as follows:
Septic Tank 20',000 gallons
Tower #1. 4,320 gallons
Tower #2 4,320-gallons
Inside Sump 7,000 gallons
Outside Sump 7,000 gallons
TOTAL VOLUME 42,640 gallons

MATERIAL SAFE",__)'DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 1 PRODUCT IDENTIFICATION
TRADE NAME:, NALCO 2593 MICROBICCIDE
DESCRIPTION: An aqueous solution of -substituted isothiazolinone
NFPA 704M/HMIS RATING:' 3/3 HEALTH 0/0 FLAMMABILITY 0/0 REACTIVITY 0 OTHER
O=Insignificant, 1=Slight 2=Moderate 3=High 4=Extreme .
SECTI'ON 2 HAZARDOUS INGREDIENTS
Our hazard evaluation has identified. the following chemical ingredient(s) as
hazardous under OSHA's Hazard Communication Rule, 29 CFR 1910.1200. Consult
Section 14 for"the nature of the-hazard(s)..
INGREDIENTS) CAS # APPROX.%
5=chloro-2-methyl-4 isothiazolin-3-one .26172-55-4 1.15
2-methyl-4-isothiazolin-3-one 2682-20-4 0.35
SECTION 3 PRECAUTIONARY LABEL INFORMATION
DANGER: Corrosive. Causes eye damage and skin -burns. May cause allergic
skin reaction. May be harmful if.inhaled. May be fatal if swallowed or
absorbed through the skin. Do not get in eyes, on skin, or on.cldthing. Wear
goggles or face shield -and rubber gloves when handling. Avoid breathing vapor
or mist. Avoid contamination of food. Do not take internally.. Wash.
thoroughly after handling.
SECTION 4 FIRST AID'INFORMATION
EYES: Immediately flush for at least 15 minutes while holding
eyelids open.. Call a physician at -once.
SKIN:, Wash'thorougly with soap and rinse with water. Remove and
wash contaminated clothing before reuse.
.INGESTION: Do not induce vomiting. Drink promptly a large quantity of
milk, egg whites, gelatin solution, or, if these are not
available, drink, large quantities of water.. Avoid alcohol_.
Call a physician -immediately.
INHALATION: Remove immediately to fresh air. -If not breathing, apply
artificial respiration. If breathing is difficult, give
-,oxygen. Call a -physician.
NOTE TO PHYSICIAN: Based.on the individual reactions of the patient, the
physician's judgment- should be used to control symptoms and clinical condition.
,CAUTION: If unconscious, having trouble breathing or in convulsions, do'not
PAGE 1 OF 10

MATERIAL SAF
PRODUCT.
DATA SHEET
NALCO.,
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number'
Medical [phone] (24 hours)
SECTION 4 FIRST AID INFORMATION ( CONTINUED•)
•induce vomiting or give,water.
NOTE TO PHYSICIAN: Probable mucosal damage.may contraindicate the use
or -gastric lavage. Measures against circulatory shock, respiratory
depression and convulsions may be needed.
SECTION. 5 HEALTH EFFECTS INFORMATION
PRIMARY ROUTE(S) OF EXPOSURE: Eye, Skin, Inhalation
EYE CONTACT:
Corrosive to=the eyes with possible permanent damage.
depending on the length of exposure and on the first
aid action given.
SKIN CONTACT:
Corrosive to the skin, possibly resulting in third
degree burns depending on the length of exposure and
on the first aid action given. Can be harmful if
absorbed. Can cause allergic contact dermatitis in.
susceptible individuals.
INGESTION:
Can be fatal.
INHALATION:
Can be corrosive to the mucous membranes and the
lungs. Can cause an allergic reaction in susceptible.
individuals.
SYMPTOMS OF -EXPOSURE: A review of available data does not identify any
symptoms from
exposure not•previouslg mentioned.
AGGRAVATION OF EXISTING CONDITIONS:. A review of available data -does
not identify any worsening of existing conditions)
SECTION 6 TOXICOLOGY INFORMATION
ACUTE TOXICITY STUDIES: Acute toxicity studies have been conducted on
this product. The results are shown below.
ACUTE ORAL TOXICITY (ALBINO RATS): LD „=-3,810 mg/kg
95% Confidence.Limit = 3,530--4,220 mg/kg
ACUTE DERMAL.TOXICITY (ALBINO RABBITS),:
LD,o = Greater than 5,000 mg/kg ,
ACUTE, INHALATION TOXICITY. (ALBINO RATS): -
For solution of 1% active ingredients LC,, = 13.7 mg/L
PAGE 2 OF 10
NALCO CHEMICAL COMPANY; ONE, NALCO CENTER. NAPERVILLE. ILLINOIS 60563-1 1 Se

MATERIAL SAFE," DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 6 TOXICOLOGY INFORMATION ( CONTINUED
COMMENTS: Four-hour nominal concentration for a solution containing 1%
active ingredients.'
'
SKIN IRRITATION INDEX DRAIZE RATING: Severe.i�:ritant
1 .
EYE.IRRITATION INDEX DRAIZE RATING:- Corrosive (corneal damage)
SKIN SENSITIZATION: This product is a human sensitizer in its undiluted form.
A Guinea pig (Buehler Technique) sensitization'study;with an induction
.dosage of 90'ppm of active ingredients followed by a -insult of 429 ppm
of active ingredients was positive:
A human repeated insult patch study of 28 ppm active ingredients
followed by a insult of 56 ppm of active ingredients resulted in no
effect to the subjects tested.
SUBCHRONIC TOXICITY RESULTS: A 90-day dietary study in dogs of 840 ppm of the
product's active ingredients resulted in no mortalities or pathological.
findings. A 90-day dermal study in rabbits of 0.4 mg/kg/day of the product's
active ingredients resulted in no irritation or pathological effects.
CHRONIC TOXICITY RESULTS: A teratology study with rabbits and rats was
negative with dosages of active ingredient ranging -from 1.5 mg/kg to 15 mg/kg.
Mutagenicity results were equivocal., A 30-month skin painting mouse study
with applications of 400 ppm of -active ingredients three times per week
showed no -increase tumor frequency over control animals.
SECTION 7 PHYSICAL AND CHEMICAL.PROPERTIES
COLOR: Pale ,yellow to�green FORM: Liquid _ _ ODOR: Mild
DENSITY: 8.6 lbs/gal. -
SOLUBILITY IN WATER: Completely
pH (NEAT).= 3 - 5 ASTM E-70
FREEZE POINT: 25 Degrees F ASTM D-1177-
FLASH POINT: None
NOTE:. .These physical properties -are --typical values -for this product.
SECTION 8 FIRE AND EXPLOSION -INFORMATION. -
FLASH POINT: None-.
EXTINGUISHING MEDIA: Not applicable
PAGE- 3 OF 10
NALCO CHEWCAL COMPANY ONE NALCO CENTER'- NAPERVILLE,- ILLINOIS 60563-1 198

MATERIAL SAFE'" DATA SHEEN'
PRODUCT
NALCO
NALCO 2593 MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 8 FIRE AND EXPLOSION INFORMATION ( CONTINUED )
UNUSUAL FIRE AND EXPLOSION HAZARD: May evolve NOx, SOx or HCl.under fire
conditions. Containers exposed in afire should be cooled.with water to
prevent vapor. pressure buildup leading to a rupture. Do no.t.let 'material
evaporate to dryness.
SECTION 9 REACTIVITY INFORMATION
INCOMPATIBILITY: None known
THERMAL DECOMPOSITION PRODUCTS: In the event of combustion CO, CO,, NOx,
SOx, HCl may be formed. Do not breathe' smoke or fumes. Wear suitable
protective equipment.
SECTION 10 PERSONAL PROTECTION EQUIPMENT
RESPIRATORY PROTECTION: 'If it is possible to generate significant levels. of
vapors or mists, a NIOSH approved or- equivalent respirator is recommended.
For large spills, entry into large tanks,. vessels -or enclosed.small
spaces with inadequate ventilation, a pressure -demand, self-contained
breathing apparatus is recommended.
VENTILATION: General ventilation is recommended. Additionally, local exhaust
ventilation is recommended'where vapors, mists or aerosols.may be released.
PROTECTIVE EQUIPMENT: Wear gloves, boots, apron and a face shield with
chemical splash goggles. (Based on test data obtained from materials of.
construction, the following recommendations are listed for gloves along with
their break -through times: Butyl rubber (greater than 8 hours); polyvinyl
chloride (greater than 7'.5 hours) and neoprene coated (greater than 6 hours).
A full slicker'suit is recommended if gross'_exposure-is posslble.-
The availability of an eye wash fountain and safety shower is :recommended.
If clothing is contaminated, remove clothing and thoroughly wash the
affected area. Launder contaminated clothing before reuse.
SECTION 11 SPILL AND DISPOSAL INFORMATION
IN CASE OF TRANSPORTATION ACCIDENTS, CALL THE FOLLOWING 24-HOUR
TELEPHONE NUMBER (708-920-1510)
SPILL CONTROL AND RECOVERY:
PAGE - 4 OF 10
NALCO CHEMICAL COMPANY ONE; NALCO CENTER ILLINOIS 60563-1 198

MATERIAL SAF� `Y DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
Emergency Telephone Number.
Medical (708) 920-151.0 (24 hours)
SECTION 11 SPILL AND DISPOSAL INFORMATION ( CONTINUED )
Small liquid spills: Contain with absorbent material, such as clay, soil or
any commercially available absorbent.' Shovel reclaimed.liquid-and absorbent
into recovery or salvage drums for disposal. Refer to CERCLA in-Section.14.
Large liquid spills: Dike to prevent further movement and reclaim into
recovery or salvage drums.or tank truck for disposal.. Refer to CERCLA
in.Section 14..
For large indoor spills, evacuate employees and ventilate area. Those
responsible for control and recovery should wear the protective equipment
specified in Section 10.
This product is toxic to fish. 'It should not be directly discharged
into lakes, ponds', streams, waterways or public water supplies.
DISPOSAL: If this product becomes a waste, it meets the criteria of a
hazardous waste as defined under the Resources Conservation and Recovery
Act (RCRA) 40 CFR 261. Hazardous Waste D002.
As a hazardous liquid waste, it must be solidified with stabilizing agents
(such as sand, fly ash, or cement) so that no free liquid remains before'
disposal to a licensed industrial waste landfill (Hazardous Waste Treatment,
Storage and Disposal facility).. A hazardousrliquid waste can also be
incinerated in.accordance with local, state, and federal regulations.
Pesticide wastes are toxic. Improper -disposal of excess pesticide, spray
mixture, or rinsate is a'violation of Federal Law. If these wastes cannot be
disposed of by use according.to label instruction, contact your State
Pesticide or: Environmental Control Agency, or the Hazardous Waste
representative at the nearest EPA Regionk—"Office -for guidarrce:
METAL CONTAINERS: Triple rinse (or equivalent). Then offer for recycling or
reconditioning, or puncture and dispose of in a sanitary landfill, or by other
procedures approved by state and local authorities.
PLASTIC CONTAINERS: Do not reuse empty container. Triple rinse (or
equivalent). Then puncture and dispose of in a sanitary landfill, or; if.
allowed by state and local authorities,by burning. If burned,.stay out of
smoke.
SECTION 12 ENVIRONMENTAL INFORMATION
CHEMICAL OXYGEN DEMAND (COD): 20,000 mg/L.
u
PAGE 5 OF 10
NA1 ^n nL�C wRIP+A� P+rlwA nil wlV rinlC AIAI !'+r'1 r".c NITC� I�1 n.00 O\/II 1 C 11 1 IA If"'11C C!"IG C�7-A A OC

MATERIAL SAFFrY DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE'
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 12--ENVIRON14ENTAL INFORMATION CONTINUED•)
TOTAL ORGANIC -CARBON (TOC): 7,850 mg/L'
AQUATIC DATA,:- Active ingredient.
6 day static acute LC,a.to Bluegill Sunfish = 0.54 ppm
Standard Deviation of 6'day LC „ _= 0.47 - 0.62
6 day dynamic acuteChC;;':; toLFathead�t innow=..0:12�ppmY
Standard Deviation of 6 day LCs, = 0.06 -�0.15 ppm•
.I
48 hour acute LCs, to Daphnia Magna = 0.13 - 0.18 ppm
6 day dynamic:acute.LCs,-.to Rainbow Trout=,0.14.ppm
Standard Deviation of 6.day LC,., = 0.12..- 0.17 ppm
96 hour static acute LC,, to Rainbow Trout = 0.3 ppm
Standard Deviation of 96 hour LC,,, = 0.18 - 0.50 ppm
OTHER STUDIES: Avian.species:
Acute oral LDs, to Bobwhite Quail.= 97 mg/kg
Standard Deviation of LD,,,= 64 = 114 mg/kg
8 day dietary LDs, to Pekin Duck = 560 ppm of.active ingredients
AQUATIC DATA: Product..
96.hour static acute LCso to Mysids = 18 mg/L.
96 hour no observed effect concentration is less than 10-mg7L based on -no
mortality or'abnormal effects.
TOXICITY RATING: Moderately toxic
96 hour static acute-LCs, to Sheepshead Minnow = 32 mg/L
96 hour no observed effect concentration is 18 mg/L based on no,mortality or
abnormal -effects.'
TOXICITY RATING: Moderately toxic
If released into the environment,,see•:CERCLA in Section 14.
PAGE. 6 OF 10
- r -
NALCO CHEMICAL COMPANY ONE NALGO CENTER • NAPERVILLE. ILLINOIS_ 60563-1 198

MATERIAL SAFE Y DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE .
NALCO
Emergency Telephone Number
Medical [phone] (24 hours)
SECTION 13 TRANSPORTATION INFORMATION,_
.DOT PROPER SHIPPING NAME/HAZARD CODE - CORROSIVE LIQUID, N.O.S.
CORROSIVE MATERIAL UN 1760
CONTAINS - 5-CHLORO-2-METHYL-4-ISOTHIAZO
LIN-3-ONE,=:-CUPRIC NITRATE
SECTION 14 REGULATORY INFORMATION
The following regulations apply to this product.
FEDERAL REGULATIONS:
OSHA'S HAZARD COMMUNICATION RULE, 29 CFR 1910.1200:
Based on our hazard evaluation, the following ingredients. in this product are
hazardous and the reasons are shown below.
5-chloro-2-methyl-4 isothiazolin-3-one - Corrosive, sensitizer
2-methyl-4-isothiazolin-3-one - Corrosive, sensitizer
5-chloro-2-methyl-4 isothiazolin-3-one (mist or aerosol) = 0.5 mg/m' TLV
Manufacturer's recommendation
CERCLA, 40 CFR 117, 302:'
This product contains cupric nitrate, a Reportable Quantity (RQ)'substance
and if 52,000 pounds of product are released, it requires notification to 'the
NATIONAL'RESPONSE CENTER, WASHINGTON, D. C.-(1-800-424-8802).
SARA/SUPERFUND AMENDMENTS AND REAUTHORIZATION ACT OF.1986
(TITLE III) - SECTIONS 302, 311, 312 AND 313:.
SECTION-302 - EXTREMELY HAZARDOUS SUBSTANCES (40 CFR 355):
This product does. not contain ingredients listed in Appendix A and B as an
Extremely Hazardous Substance. - - - - -
SECTIONS 311 and 312 - MATERIAL SAFETY DATA SHEET REQUIREMENTS (40 CFR 370):
Our hazard evaluation has found this product to be hazardous. The product
should.be reported under the. following EPA hazard categories:
XX Immediate (acute) health hazard
-- Delayed (chronic) health hazard
-- Fire hazard
-- Sudden release of pressure hazard
-- Reactive hazard
SECTION 313 —LIST OF TOXIC CHEMICALS-(40 CFR 372):
PAGE 7.OF 10'
NALCO CHEMICAL COMPANY ONE NALGO CENTER • NAPERVILLE. ILLINOIS 60563-1196
AREA 70R-305-1 000

MATERIAL SAF1
DATA SHEET
o .
NALCO
PRODUCT
NALCO 2593-MICROBIOCIDE
Emergency Telephone Number
Medical [phone] (24 hours)'
SECTION 14 REGULATORY INFORMATION ( CONTINUED),.
This product does not contain ingredients on.the List of Toxic. Chemicals.
TOXIC SUBSTANCES CONTROL ACT (TSCA):
The active ingredients are exempted under TSCA and regulated under FIFRA as
follows. All the inert ingredients are found on the TSCA Master Inventory
List.
FEDERAL INSECTICIDE, FUNGICIDE AND RODENTICIDE ACT (FIFRA): - .-
EPA Reg.. No..1706-153. This product is registered for use asa microorganism
control chemical used in industrial'recirculating cooling water tower-
systems, used in brewery pasteurizers, and used in air washer systems. In all
cases follow instructions on the product label.
RESOURCE CONSERVATION AND RECOVERY ACT (RCRA), 40 CFR 261 SUBPART C & D:
Consult Section 11 for RCRA classification. -
F-EDERAL WATER POLLUTION CONTROL ACT, CLEAN WATER ACT, 40 CFR 401.15
(formerly Sec. 307), 40 CFR 116 (formerly Sec. 311):
This product contains the following -ingredients covered by the Clean Water Act:
`Cup=: c: nit=ate•:.== Section, 307_,,. 311�
CLEAN AIR ACT, 40 CFR 60, SECTION 11.1, 40 CFR 61, SECTION 112:
This product does not contain ingredients.covered by the Clean Air Act.
STATE REGULATIONS:
CALIFORNIA PROPOSITION 65:
None of the'chemicals on the current Proposition 65 list are known to be
present in this product.
MICHIGAN-CRITICAL MATERIALS:
This product.contains the following substance(s) identified on.the Michigan
Critical Materials Register:
Copper;: as Cu 0 05s-�
STATE RIGHT TO KNOW LAWS:
PAGE 8 OF 10_•
NALCO CHEMICAL COMPANY ONE .NALGO CENTER �- NAPERVILLE, ILLINOIS .60563-1 1 98

MATERIAL SAFE-7Y DATA SHEET
PRODUCT
NALCO 2593 MICROBIOCIDE
NALCO
4. Emergency Telephone Number
Medical (708) 920.-1510 (24 hours)
SECTION'14,REGULATORY INFORMATION ( CONTINUED )
The following state(s) identify'the ingredients) shown below as hazardous:'
California - Copper
Mas'sachusets, New'Jersey, Pennsylvania -,magnesium nitrate
INTERNATIONAL REGULATIONS:
This is not a WHMIS controlled product under The House of Commons of Canada
Bill C-70.
SECTION 15 ADDITIONAL INFORMATION 1
Note: Other toxicological results.are available upon request.
SECTION 16-USER'S RESPONSIBILITY
This product material safety data sheet provides health and safety
information., The product is to be used in applications consistent with
our product literature. . Individuals handling this. product should be.
informed of the recommended safety precautions and should have access
to .this information. For any other uses, exposures.should be evaluated
so that appropriate handling practices and training programs can be
established to ensure safe workplace operations. Please consult your
local sales representative for any further,information.
SECTION 17 BIBLIOGRAPHY'
ANNUAL REPORT ON CARCINOGENS, U.-S. Department of Health and Human Services,
Public Health Service, PB 33-135855, 1983.
CASARETT AND DOULL'S TOXICOLOGY, THE BASIC SCIENCE OF POISONS,.Doull, J..,
Xlaas'sen, C.D., and Admur, M..0., eds.; Macmillian,Publzshing-Company, Inc.,
N. Y., 2nd edition, 1980.
CHEMICAL HAZARDS OF THE WORKPLACE, Proctor, N. H., and Hughes, J. P., eds.,-
J. P. Lipincott Company, N.Y., 1981..
DANGEROUS -PROPERTIES OF INDUSTRIAL MATERIALS, Sax, N. Irving, ed.,.Van
Nostrand-Reinhold Company, N.Y., 6th edition, 1984.
'IARC MONOGRAPHS ON THE. EVALUATION OF THE CARCINOGENIC RISK OF CHEMICALS
TO MAN, Geneva: World Health Organization, International Agency for
Research 'on "cancer, 1972-1977.
PAGE 9 OF 10
NALCO CHEMICAL COMPANY ONE NALCO CENTER r� NAPERVILLE, ILLINOIS 60563-1 198.

4NAL'CO CHEMICAL COMPANY
. ONE NALCO CENTER ❑ NAPERVILLE, ILLINOIS B0563-1'I 9B 0 AREA 70B-305-1000
May 18, 1993
Ms. Marian White
Burlington Industries
Burlington House Annex
P.O. Box 691
Burlington, N.C. 27216
Subject: Nalco 2593 -Degradation
Dear Ms. White:
As discussed over the telephone this morning, I ain sending for your reference information on the
half-life ( t�J of the active ingredients in Nalco 2593.
The actives are isothiazolines and are identified in the references as RH-651 and RH-573. The
dissipation rates shown in Figure 5 are for complete degradation of the compound as described in
the document. A half-life of less than 10 days seems appropriate for the concentrations which
would be expected in atypical cooling water tower system.
Keep in mind that the degradation of the Isothiazolines are temperature and pH 'dependent and
are accelerated in the presence of strong nucleophiles or reducing agents.
I hope this -information will satisfy your needs. If you have any questions, please feel free to
contact me directly.
S ing,6�ly,
L-c�C
'Claude H. Wol ,MSc.
Corporate Toxicologist
CHW/cw
enc.

SUMMARY
Kathon® WT and Kathon WT 1.5% biocides are
biodegradable at use levels. The degradation of
RH-651, the major active ingredient, begins with
ring opening and elimination of chloride ion.
Degradation leads to the formation of a variety of
small organic acids, methylamine, carbon dioxide
and elemental sulfur. The degradation products
have no measurable environmental impact.
INTRODUCTION
In 1975, Krzeminski et al. (1) described fate of the
active ingredients (Figure 1) of Kathon WT bio-.
cides in a variety of systems. A degradation
pathwaywas presented based on the metabolites
that were identified. The following is an updated
summary of the current understanding of the
environmental fate of Kathon WT biocides.
0 0
N I N
CI S� �CH3 S� "CH,
RH-651 RH-573
5-Chloro-2-methyl-4- 2-Methyl-4-
isothiazolin-3-one isothiazolin-3-one
FIGURE 1 — ACTIVE INGREDIENTS IN
KATHON WT AND KATHON WT 1.5%
BIOCIDES
INITIATION OF DEGRADATION
The degradation of RH-651 and RH-573 is accel
erated by exposure to three key chemical and
physical factors:
• Temperatures above 500C for extended pe-
riods of time.
• High pH, generally -above pH 9.
• Strong reducing agents such as bisulfite
ion, or strong nucleophiles such as mer-
captans and amines.
Krzeminski et al. showed that the rate of degrada-
tion of low levels of RH-651 increases with
increasing pH and, to a more limited extent, with
increasing temper; ' e. This suggested that
basic hydrolysis pla),,— -najor role in initiating the
degradation process of RH-651. However, low
levels of nucleophiles, in particular mercaptans,
significantly accelerate the degradation of un-
stabilized RH-651 in water (Figure 2). The reac-
tivity of these nucleophiles increases as pH in-
creases. Therefore; it is likely that the pH
dependent degradation of RH-651 is initiated by
trace levels of sulfides, mercaptans or other
nucleophilic species, This is consistent with the
fact that the addition of low levels of cupric ion, a
sulfide scavenger (Ksp for CuS is 2 x 10-47 at
180C), to Kathon WT biocides significantly im-
proves stability.
The initial attack of nucleophiles on RH-651 can
be at sulfur or at carbon-5, although attack.at
sulfur predominates. The reasons for the differ-
ent reaction sites may be related to different ionic
characteristics of the nucleophiles. Nucleophilic
attack at sulfur results in cleavage of the nitrogen -
sulfur bond and is illustrated in Figure 3A. Attack
at carbon-5 results in addition of the nucleophile
at carbon-5 followed by rapid- elimination of
chloride ion as shown in Figure 3B.
DEGRADATION PRODUCTS AND
PATHWAY
The degradation products from aqueous solutions
of use levels of RH-651 were identified after
exposure to elevated temperature, elevated pH
and glutathione. Similar distributions of degra-
dation products were seen in each of the three
systems. The products found were consistent
with the major metabolites identified by Krzemin-
ski et al. in the systems they studied. The major
degradation pathway of RH-651 is shown in
Figure 4. The key steps in the degradation path-
way are:
Initiation by a nucleophile attacking
RH-651 at sulfur resulting in ring -opening.
2. Rapid degradation of the intermediate ad-
duct to N-methylmalonamic acid, chloride
ion, hydrogen sulfide and an oxidized form
of the nucleophile.
3. Propagation of degradation through the
reaction of released hydrogen sulfide with
another molecule of RH-651.
4. Degradation of N-methylmaIona mic acid to
small organic acids (malonic, acetic,
formic), methylamine, and carbon dioxide.

100
1
—0-- 0 ppm SH-
80.
= -0'—, 1250 ppm SH-
c
C:
�;
- -- 2500 ppm SH-
fO
60
�
\
CC
I
40
`\
M
`\
a
\
20
\,
a
\
� v
0
0 5
10 15
Days
20
{ FIGURE 2 — EFFECT OF.SULFIDE ON THE DEGRADATION OF 10%
UNSTABILIZED RH-651. (w/w) INCUBATED AT 550C
A. Nucleophilic Attack at Sulfur
0 0
+ Nu: ► Cl / NH-CH3
N
CI S� �CH3 . S-Nu '
B. Nucleophilic Attack at Carbon-5
0 0
iN\ + Nu: , I N + CI-
Cl e S CH3 Nu S� �CH3
FIGURE 3 — INITIAL ATTACK OF NUCLEOPHILES ON RH-651
—2—

a,.
0
Initiation
N-CH, + RSH
CI S"
NH -CH,
I.
CI SSR
Release of Chloride Ion H2O
0
N-CH; + RS03H + HCI + H,S
H
or
o
0 Q RS SR 0
H` Propagation
N-methyl ma Iona mic acid I N-CH,
CI
O S
NH -CH,'
' I
Cl SSH
Formation of Elemental Sulfur H2O
0
NHCH,
+ HCl-+ S° + H,S
OH
0
H30+
OH
+" CH,NH2•HCI
OH
,0 methylamine hydrochloride r.
malonic acid
Release of Carbon Dioxide
CH,COOH, HCOOH, CO,
FIGURE 4-- MAJOR DEGRADATION PATHWAY OF RH-651
-3-

The major degradation products of RH-651 are
small biodegradable organic molecules, chloride
ion and elemental sulfur.. Chlorine and chlori-
nated -organic molecules are not formed as
RH-651 degrades. Degradation products arising
from use level concentrations of Kathon WT bio-
cides should have no impact on the environment.
ENVIRONMENTAL FATE STUDIES
Biodegradation in Natural River Water
Radioassays indicate that the active ingredients
in Kathon WT biocides are readily biodegradable
in natural river water (Figure 5).
The half life of each active ingredient is related to
the initial concentration tested. The most rapid
'degradation occurs at the lowest concentrations,
which would occur following dilution of an ef-
fluent water stream.
Dissipation. in a Typical Soil
About 28% of 14C applied to non -sterile soil as
RH-651 was released.as 14CO2 from non -sterile
soil after41 days. However,14C release as 14CO2
was less than 1 %-from sterile soil over the same
time period. This indicates that RH-651.
100-%*
is rapidly degraded to CO2 by primarily. biological
— mechanisms in soil.
Dissipation in Activated Sludge Waste Water
Treatment Plants
Laboratory studies performed in model activated
sludge waste water treatment plants demon-
strate that:
• Kathon WT biocides rapidly dissipate in
activated sludge. Figure 6Ashows a greater
than 90% reduction of the active ing %,3-
dients.
• Dissipation of Kathon WT biocides is ac-
companied by a corresponding reduction in
total organic halogen levels as seen in
Figure 6B.
• Chlorinated organics do not accumulate in
the sludge.
• Activated sludge performance is unaffected .
by Kathon WT biocides. Chemical oxygen
demand (COD) and dissolved organic car-
bon (DOC) removal_ rates are not affected by
the addition of Kathon WT biocides to the
model feed influent (Figures 7A and 713). In
addition, levels. of viable bacteria and fungi
in the sludge are. also unaffected by the
presence of Kathon WT biocides.
—0— 0.006 ppm RH-651
80
--0— 0.06 ppm RH-651
�
—iN— 0.6 ppm RH-651
t
-- E-- 0.6 ppm RH-573
60
40
h
20
0
0 10 20 30
Days
FIGURE 5 = DISSIPATION OP.RH-651 AND RH-573 IN RIVER WATER
—4—

� r
ATTACHMENT 3
BIOCIDE APPROVAL

State of North Carolina
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor
William W. Cobey, Jr., Secretary
January 10, 1992
Mr. Jacob M. Wilson
Burlington Industries, Inc.
P.O. Box 158
Carofeen, NC 28019
George T. Everett, Ph. D.
Director
Subject: NPDES Permit No. NC0006009
Biocides Additives
Caroleen Plant
Rutherford County
Dear Mr. Wilson:
The Division of Environmental Management (OEM) has reviewed the information in the
letter of December 3, 1991, concerning the use of Nalco 2593 in the cooling water _systems at t
your facility near Caroleen.. Our review has revealed that Nalco 2593 should be appropriate for
use in your application. Therefore, -the DEM grants approval to Burlington Industries, Inc. for
the use of the above mentioned additive in its cooling water at the Caroleen plant.
Should you plan to change to a different additive in the future, you should contact this
office and submit the appropriate information for approval prior to the change.
If you have any questions, please contact Mr. Dale Overcash at [phone].
cc: Mr. Ken Eagleson
Mr. Dale Overcash
Y
Sl4erely,
_�t. George T.
rett
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer
0

op
State of North Carolina
Department of Environment, Health, and Natural Resources
Asheville Regional Office
James G. Martin, Governor
William W. Cobey, Jr., Secretary
DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
April 30, 1992
Mr. Philip H. Klein
Director of Engineering
Burlington Industries, Inc.
Post Office Box 21207
Greensboro, North Carolina 27420
Dear Mr. Klein,
Ann B. Orr
Regional Manager
Subject: Compliance Sampling Inspection
Status: In -Compliance
Burlington Industries
Caroleen Plant
Wastewater Treatment Facilities
NP ES Permit Number NC000600.9
uther`�ord County
An inspection of the wastewater treatment system serving Burlington
Industries' Caroleen Plant was conducted by Mr. Forrest Westall and the
writer on April 1, 1992. Based upon observations made and samples
collected, the system was judged to be operating in compliance with the
requirements of its NPDES Permit Number NC0006009. A copy of the
inspection report and lab analysis is enclosed for your records.
To help maintain a state of compliance the following suggestions
are offered:
(1) Clean out and remove the accumulated solids from the laterals
feeding wastewater to the sand filter bed. This will help to
improve distribution over the filter bed surface .
(2) Lightly rake the filter bed, and add filter sand up to the
bottom of the lateral surface, making sure the sand is level
over the filter bed. This will help to prevent channeling and
ponding that was noted on the filter surface during the
inspection.
0
Interchange Building, 59 WoodHn Place, Asheville, N.C. 28801 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Philip H. Klein
April 30, 1992
Page Two
(3) Clean out the accumulated leaf matter in the bottom of the
Chlorine contact basin. On -site measurement of the residual
chlorine indicated > 2.20 mg/l. Residual chlorine should be
controlled to meet.the demand to kill the pathogenic.bacteria
and still not cause harm to the receiving stream. Monitoring
.the residual chlorine with EPA approved methods will help in
maintaining the necessary dose in order to.achieve this.
Review of monthly monitoring reports .from February 1991 till
February'1992, indicate a Flow -violation in November 1991 and a Fecal
Coliform violation in December. These two reports were erroneously
calculated and should be amended by the ORC and resubmitted.
The facility has three other discharges listed in the permit, pipes
002, 003, and 004. On -site inspection revealed no discharge from the
pipes. It is suggested the facility contact Mr. Jim Reid about
removing these discharges from the permit.
Thank 'you
any questions
704-252-6208.
Enclosure
for the opportunity to visit your facility. If there are
concerning this report, please contact me at
Sincerely,
Donald R. Price
Wastewater Consultant
xc: Jake•Wilson, Burlington Caroleen Plant
James R. Reid
Dan Ahern, EPA

:n ronmenral Proleciion Agcncv ...-s
vv"I"9ron.0 C 20-060
FOrrn Approved
E PA NPDES Com Compliance Inspection Repnort
P
OMBNo:Eoires7-3
1�
Approval Expires 7-31 -85
Section A: National Data System Coding
Transaction Code NPDES yr/mo/day Inspection Type Inspector FFac T
fUInlIC lololol6l0l0191>> t91.9101flolll17 t� tqL5j 2
Remarks
1111111111111111111111111111111111111111IIIIII
Evaluation Rating 81 QA - ' 66
Reserved Facility ------•-•---------Reserved------- = =-------
67L U 69 7� 71u 7� 73LU 74 751 1 1 1 1 I. 180
Section 8: Facility Data
Name and Location of Facility Inspected Entry Time
BctNlih9 f 6ft Z'hduS�FN�t°S - Ca Yo/eeh %ant r, 3D ❑ AM Q PM
XT
Permit Effective Date
1990
P.D. <3 isS
K
Permit Expiration Date
Ak0, .30 / 9,3
Exit Time/Date
GaYol e�h N. C, .� SDI `l 3;00 Pi" 3111 AA
Name(s) of On -Site Representative(s) Title(s)
TQKc P/aYt�►- �ti�ihees''
Phone No,(s)
C7o�)10"5r7• (v376
so-W i?'lekihne /ah�- /s'lainteh Q�oe
Name, Address of Responsible Official
t��i l:P H. Kle; hl ,&t r/i'•�q �'o�t ��tqr',
Title
�J'{r`eC'f-OY' b
P. �, .box ��•? o% l�,l
Greens doNo /�I C, '.Z %�j���
Gh /hePY'in
P Pone No. �+
/� 37�� gb
Conta(c�tted
❑ Yes 1pl No
Section C: Areas Evaluated During Inspection
(S = Satisfactory, M = Marginal, U = Unsatisfactory, N = Not Evaluated)
s
Permit
Records/Reports
Facility Site Review
S
Flow Measurement
Laboratory
Effluent/Receiving Waters
Al
Pretreatment
Compliance Schedules
Self -Monitoring Program
/H
Operations & Maintenance
Sludge Disposal
Other:
S
^%
s
S
S
Section D: Summary of Findings/Comments (Attach additional sheets it necessary)
Petv-4 mefer Perm,`t L.;'" tgH6&1 semPle- ReSt~ 11F-
FLow 0019 M6D
.aoD 30 .may& ;k An) IL
Ts S 3 0 -%)A w.o. It vj, < I wt5 /L
1 Cdl�-�or.►,
F-eca zao/too urtl Mo. qvj, < to/!oo M/
ho7� <6.d how >jZ) 6,29 (OK -Site 6.3 CLa6�
Fae,;I Ao'll MOVIItor res;dctq CjZ el f fV0Ve e4'0
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oP SaLA-Q of �iii-eY bed CoOd hel P reve nt- Pohl;h 4- e_ �e A fft'A
Review o- P; le -5 .S ,
incQ;cates ,�a�;l,'t� S�toa(� �'e-Sad ;t !1 �9I 4- 1.2A VAM,
Name(s) and Sig iature(s) of Inspector(s)
Agggeency//�J�
Date
E/ 1LOffice/Telephone
t� V 70 6..2 es
ignatur of Revi er
Agency/Office
Date
Regulatory Office Use Only
Action Taken
Date
omplr nce Status
❑
Noncompliance
Compliance

DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIELD -LAB FORM (DM1)
COUNTY
PRIORITY
SAMPLE TYPE
0
RIVER BASIN /L$t1.G�
❑AMBIENT
❑
❑ 12EFFLUENT
REPORT TO: RO RO MRO RRO,WeRO WiRO WSRO TS
QA
STREAM
AT BM
5COMPLIANCE
❑ CHAIN
❑ LAKE El
I
r Otheer
Other
INFLUENT
❑EMERGENCY
OF CUSTODY
❑
Shipped by; Bus Courier, Staff,'Other
ESTUARY
Pn i-ah H.. nNI.V
3
Lab Number:
5 2
Date Received:
Time:
�w��
Rec'd by:
From: Bus-Courie and
DATA ENTRY BY:
r^
tPJ
CK: •
/.-
- (' 2
DATE REPORTED:
'?
Sampling Point %
Conductance at 25 C
Water Temperature (C)
D.O. mg/l
pH
Alkalinity
Acidity
Air Temperature (C)
pH 8.3 pH 4.5
pH 4.5 pH 8.3
2
94
10
800 10 "
400 •
82244 431
82243 182242
20
Salinity %
Precipltion Wday)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
can Stream Depth ft.
Stream Width ft.
480
45
32
36
1351
1350 1
35
64 14

N
State of North Carolina
'Department of Environment, Health, and Natural Resources
512 North Salisbury Street • Raleigh, North Carolina 27604
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
April 20, 1993-
Mr. Phillip H. Klein
Director of Engineering
Burlington Industries , Inc.
Post Office Box 21207
Greensboro North Carolina. 27420
Subject: Compliance Sampling Inspection
Status: In -Compliance
Burlington Industries
Caroleen Plant
Wastewater Treatment
Facilities
NPDES Permit Number NC0006009
Rutherford County
Dear Mr. Klein:
An inspection of the wastewater treatment system serving
Burlington Industries Caroleen Plant was conducted on on March 30,
1993 . Based upon observations.made and samples collected, the system
was judged to be operating it compliance with its NPDES Permit Number
NC0006009. A copy of the inspection report and laboratory analysis is
enclosed for your records.
The following suggestions are offered to help the facility
maintain a state of compliance:
(1) On -site measurement of residual chlorine indicated > 2.20
mg/l. Residual. chlorine this high in the discharge could
possibly impact the receiving stream. Chlorine residual is
difficult to.control with the tablet chlorinator used at the
facility. An immediate solution to the problem would be to
install a tablet de -chlorination unit at the effluent end of
the chlorine contact chamber.
Interchange Building, 59 Woodfin Place, Asheville, NC. 28801 • Telephone [phone]
An Equal Opportuniry Affirmative .fiction Employer

___llip H. Klein
ipril 20, 1993
Page Two
(2) A. timer control on the lift station following the.septic
tank would help control the flow to the dosing tank and help
in equalizing the.wear on the pumps. During the inspection
the -pumps were not alternating in operation.
Any addition in the treatment facility would require consent from
the Division of Environmental Management, in the form of an
Authorization to Construct.
Review of monthly monitoring data submitted by the facility from
February 1992 thru January 1993, indicate the facility to be in
compliance with their monthly average limits.
Sam McKinney's time and assistance -in conducting the inspection
is greatly appreciated. It was a pleasure to visit your facility and
find it so well maintained and operated. If there are any questions
concerning this report or if I can be of any assistance, please
contact me at 704-251-6208 .
Enclosure
Jake Wilson
James R. Reid
xc:
Sincerely,
Donald R. Price
Wastewater Consultant

United States Environmental Protection Agency
Washington, D.- C. 20460
- +" Z = ` .
Form Approved
.s' k
at NPDES Compliance inspection Report
OMB No. 2040-0003
ApprovaIExpires 7-31;85-'.;+
Section A: National Data System Coding
Transaction Intt spection Type Inrs�pel c.t.o. r_ ,Fac TLy.:p.e
11EA,U'I. Code
_
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27
Remarks
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Permit
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Records/Reports
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Action Taken
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DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIELD -LAB FORM (DM1)
COUNTY E�4
PRIORITY
SAMPLE TYPE
0
RIVER BASIN � /N`�
❑AMBIENT ❑
7
❑ STREAM
.
®
REPORT TO. R FRO MRO RRO WaRO WiRO WS,RO TS
QA
EFFLUENT
AT BM
❑ CHAIN
❑ LAKE
❑ INFLUENT
Other
COMPLIANCE
Shipped by: Bus Cgprier Other
taff,
OF CUSTODY
❑EMERGENCY
ESTUARY
1
COD High 340
4 ><I
Coliform: MF Fecal 316
5 oliformc MF Total 3151
6 Coliform: Tube Fecal $
7 Coliform: Fecal Strep 3
A I Residue: Total 500
O mgA
mg/l
mg/l
1 l0 /100ml
/100ml
/100ml
/100ml
11
Residue: Suspended 530 41 mg/l
12
Volatile 535 - mg/l
1&
Fixed 540 mg/1
14
pH 403 units
15
Acidity to pH 4.5 436 mg/1
�16
Acidity to pH 8.3 435 mg/1
17
Alkalinity to pH 8.3 415 mg/l
18
Alkalinity to pH 4.5 416 mg/l
19
TOC 680 mg/l
20
Turbidity 76 NTU
Chloride 040 mg/I
Chi a: Tri 32217 ug/1
Chi it: Corr 32209 USA
Pheophytin a 32213 _ ug/1
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color: pH 7.6 82 ADMI'
Cyanide 720 mg/l
Fluoride 951 mg/1
Formaldehyde.7'1880 mg/l
Grease and Oils556 mg/l
Hardness Total900 mg/l
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/l
Phenols 32730 ug/l
Sulfate 945 mg/l
Sulfide 745 mg/l,
For Lab Use ONLY
Lab Number: d % 0
Date Recelve�d: 3^30 93 Time:
Rec'd by: J From:: Bus-Courie -Hand Del
DATA ENTRY BY: 6 4-oL CK:c S ('
DATE REPORTED: ' S — 7 5
NH3 as N 610 mg/l
KN. as N 625 mg/l
NO2 plus NO3 as N 630 mg/l
P: Total as P 665 mg/l
PO4 as P 70507 mgA
P: Dissolved as P 666 mg/l
Cd-Cadmium 1027 ugA
Cr-Chromium:Tota1,1034 69A
Cu-Copper 1042 ug/l
Ni-Nickel 1067 ug/1
Pb-Lead 1051 USA
Zn-Zinc 1092 ugA
Ag ilver 1077 ug/l
Al -Aluminum 1105 ug/1
Be -Beryllium 1012 ug/l
Ca -Calcium 916 mgA
Co -Cobalt 1037 ug/l
Fe -Iron 1045 ugA
Li -Lithium 1132 USA'
Mg -Magnesium 927 mg/l .
Mn-Manganese 1055 ug/l
Na-Sodlum 929 mg/l
Arsenic:Total 1002 ug/l
Se -Selenium 1147 USA
Hg-Mercury 71900 ug/i
Organochlorine Pesticides
Organophoepiwrus Pesticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoplankton
Sampling Point %
Conductance at 25 C
Water Temperature (C)
D.O. mgA
pH
Alkalinity
Acidity
Air Temperamre (C)
pH 8.3 pH 4.5
pH 4.5 pH 8.3
2
94
10
300 .
400 If
82244 431
82243 182242
20
Salinity %
Precipition On/day)
Cloud Cover %
Wind Direction 07eg)
Stream_ Flow Severity
Turbidity Severity
Wind Velocity M/H
can Stream Depth ft.
Stream Width ft.
480
145
132
136
11351
1350
35
64
14

/
`
<EX88/MP
COMPLIANCE EVALUATION
ANALY%I% REPORT
PAGE
'
PERMIT--NC00060O9
PIPE--00i
REPORT
PERIOD'
r
9202-1301
LOC--LE
' `
WILITY--BURLINGTON
IND^�,
CAROLEEN
DE%IGN FLOW--
.Oi8O
CLASS--f� ,
--
]CATION CAROLEEN
.
'�
..
�
,
RE�I ^
O N/COUNTY--Oi
�
RUTHERFORD
�
50050
00310
00530
O06iO
:3i6i6
50060
000hO
'
]NTH
Q/MGD
.
BOD
RE%/T%%
NH3+NH4-
FEC COLI
CHLORINE
TEMP
[MIT F
.Oi8O F
30.00
F 30.0
F 260^0`
NOL
NOL
`
�
2/02
'.OiiO
i ,35
-
`
' .350
8.75
[MIT F
'
AM F
30.00
F 30.0
NOL
F 200.0
NOL
NOL
Z/O3
.OiO8
3.45
2.8O
`
.38O
ii.40
�
2/04
.OiO5
4.80
LE%%THAN
.60
LE%%THAN
.370
13.48
�/O5'
\ ^\)ii9'
`9~00
'
LE%ITH'AN
.O8
LISSTHAN
� .350
i7.80
/6
.0i15`
^
't.50
LE%% AAN�
' .03
6.5
.280
20.^11)
2/07
.
.012O
i.80
LE%%THAN
.35
30.i
. '
.400
24.30
.
'
`
1�40
LE%%THAN
.33
20.2
' .332 '
22.50
.
`
.OiiK
' 185
'
LE%%THAN
.i3
i4.9
.4iO
2i.00
iO
.0i27
.
2.25
.5
.07
.O
.540
i3.5O
`
.Oi31
`
3.00
LE%%THAN
`
.44
23.6
.50O
i 3.00
'/i2
`
.Oi35
4.50
LE%%THAN
.20
3.3
.530
8.60
'
.0106
i.55
-
-
LE%%THANLE%%THAN
LEWTHAN
.510
8.75
!ERAGE
,
!0ii8
2.95
.5
.5O
i4.O^
.401
15.28
\XIMUM
.0i44
V.00
. .5
2.80
3O. i
040
24.3{i
»;
04IMUM
.0Y0O
.85
LE%%THAN
LE%STHAN
LE%%THAN
.280
8.60
DT
MGD
MG/L
. MG/L
MG/L
6/100ML
MG/L
^
DE� C'
/
/
�
/

Burlington Industries, Inc.
March 1, 1993
Mr. James R. Reid
NC Dept. of Environmental Health & Natural Resources
Div. of Environmental -Management
Water Quality Section
59 Woodfin Avenue
Asheville, NC 28801
Dear Mr. Reid:.
SUBJECT: FECAL COLIFORM LIMIT FOR PERMIT #NC0006009
A division of Burlington Industries
Caroleen Plant
P.O. Box 158
Caroleen, North Carolina 28019
In reviewing the operation of our waste treatment plant for 1992, we have
found we exceeded the daily limit for fecal coliform on three occasions.
The first occurrence was on July 7; the second on August 18, and the third
on November 3. At no time have we exceeded the geometric mean for the
month.
We have not been able to determine what caused the rise in fecal coliform.
Our records show residual chlorine has not been below 0.1. The only
possible cause could be trash in the chlorine contact chamber. We have
enclosed the chamber with a screened -in building to prevent further trash
from getting in the contact chamber.
We will continue to monitor our plant and take whatever steps are necessary
to operate within parameters -specified by -our permit.
Sincerely,
Steve Meador
Plant Manager
jb
CC: Miriam White.- BH Annex
Jim Wright - Corp.'Eng./3330
Don Price - NC Dept. of Environmental Health & Natural Resources
n L5 � L5 ll � 15
ti MAR 3 PA
!!! WATER ¢UALI*
/NSECTION
,U.SP _ ASHEVILL RE

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Environmental Management
59 Woodfin Place Asheville, North Carolina, 28802
PHILIP H. KLEIN
PO BOX 158
CAROLEEN NC 28019
April 5, 1993
/ S
ck.I v () :�
ozeCT
SUBJECT: Notice of Violation - Effluent Limitations
NPDES No. NC0006009
BURLINGTON IND., CAROLEEN
RUTHERFORD County
Dear PHILIP H. KLEIN:
Review of subject self -monitoring report for the month
of February, 1993 revealed violation(s) of the following
parameter(s):
Reported Limits
Pipe Parameter Value/Unit Value/Type/Unit
001 50050 Q/MGD
.0660 MGD .0180 FIN MGD
Remedial actions, if not already implemented, should be
taken to correct the problem(s). The Division of Environmental
Management may pursue enforcement actions for this and any
additional violations of State Law. If you have questions or if
you need assistance, please call this office at 704/251-6208.
Sincerely,
Roy Davis
Regional Supervisor
CC: Central Files
GKBDEX96/BL

}
d �,a srA7F o-�
O
State of North Carolina
Department of Environment, Health, and Natural Resources
Asheville Regional Office
James G. Martin, Governor Ann B. Orr
William W. Cobey, Jr., Secretary Regional Manager
DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
February 18, 1992
Mr. Philip H. Klein
Burlington Industries, Caroleen
Post Office Box 158
Caroleen, North Carolina 28019
Subject: NOTICE OF VIOLATION
Effluent Limitations
NPDES Permit Number NCO06009
Burlington Industries, Caroleen
Rutherford County
Dear Mr. Klein:
Review of subject self -monitoring report for the month of
December, 1991, revealed violation(s) of the following parameter(s):
Pipe
001
Parameter
31616 FEC COLI
Reported
Value/Unit
4500.0 #/100 M
Limits
Value/Unit
200.0 FIN #/100 M
The prompt attention to this matter, as described in Mr. Steve
Meador's letter of January 3, 1992 is appreciated. However, please be
aware that the Division may pursue enforcement actions for this and any
additional violations of State Law or permit requirements. If you have
questions or need to discuss this, please call Mr. James Reid at
704/251-6208.
Sincerely,
Roy M. Davis, Regional Supervisor
Division of Environmental Management
xc: Rutherford County Health Department
James R. Reid
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Burlington Industries, Inc.
January 17, 1992
Mr. James R. Reid
NC Dept. of Environmental Health & Natural Resources
Div. of Environmental Management
Water Quality Section
59 Woodfin Place
Asheville, NC 28801
SUBJECT: MY LETTER OF JANUARY 3, 1992
Dear Mr. Reid:
A division of Burlington Industries
Caroleen Plant
P.O. Box 158
Caroleen, North Carolina 28019
The enclosed copy of the report of laboratory analysis from Pace, Inc.
on.our effluent sample of January 7 shows our fecal-coliform bacteria
level is well below the 200/100ml allowed by -our permit. -
Sincerely,
Steve Meador
Plant Manager
jb
Enclosure
CC: Dale Hughes - BH Annex
J: Wright- - Corp. Eng./3330
B. Latta- BH Annex
.T. LeJeune - Corp. Eng./3330
RECEIVE[)
Water Quoty Sntion
w o A JAB! 21 119.9.2
Asheville Regional otfi
/A/ U. S.P•
Asheville, North Caroli,

C461
PN
REPORT OFa LAb u�ATORY ANALYSIS
C O R P_0 fl A T E 0
-THE ASSURANCE OF QUALITY
-
Burlington Industries, .Inc:
January 14, 1992;
PO Box 158
PACE Project Number: A20107522
Caroleen, NC 28019
Attn: Mr. ' Jak'e Wi Tson
;
Client Reference: Monthly -Monitoring"
PACE Sample.Number:"
93 0000690
Date Collected:
01/.07/92
Date Received:
01/07/92
Client Sample ID::
Effluent
Parameter
Units.
:MDL
- INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
act a 'for
col/m
Q NI
Biochemical Oxygen Demand,, 05 Day.
Mg/L
1.,0'. 2.0
Nitrogen;. Ammonia
mg/L
0.05 .-G.42
Solids, Total Suspended "
mg/L.
0'.1 ND
MDL Method,Detection Limit
NO Not detected at or'above the
MDL:
These data have been -reviewed and are
approved for
release.
" .
�-
l
Barbara M. Miller
Superv-isor, Inorganic 'Chemistry
54 flavenscroft Drive Offices` Serving: Minneapolis, Minnesota
Charlotte, North -Carolina An Equal Opportunity Employer
Asheville, NC 28801
Tampa, Florida
Asheville, North Carolina
TEL: [phone]
Iowa City; Iowa-
New York, New York
FAX: [phone]
San Francisco, California
Pittsburgh, Pennsylvania
Kansas City, Missouri
. Denver, Colorado
Los Angeles, California

Burlington Industries, Inc.
January 3, 1992
NC Dept. of Environmental Health & Natural Resources
_Div.. of Environmental Management.
Water Quality Section
59 Woodfin Place
Asheville, NC 28801
A division olTwlington Industries
Caroleen Plant
P.O. Box 158
Caroleen, North Carolina 28019
Subject: Violation of Fecal Coliform Limit for Permit NC0006009
Gentlemen:
During the month of December 1991., we experienced a violation of our
fecal coliform limit. The actual level of fecal coliform measured
on December 17 was 9000/100ml and our permit allows 200/100m1.
On December.l5, our plant shut down for Christmas vacation. Over a
period of the next three days, -our air washers were dumped to -allow
for maintenance.on.the air washers. This large volume of water
caused the chlorine to be washed out of the contact chamber. Our
operator -pulled his sample during this time. A new sample is being
tested to be sure we are°back in compliance. The results of this
sample will be reported to you as soon as they are received.
Our operator will closely monitor residual chlorine during periods
of increased flow to be sure this does not happen again. -
Residual chlorine on December 31: 3
Sincerely,
Steve Meador
Plant Manager
jb
CC": Dale Hughes - BH Annex
>1
\W,
'N U. s P
EC iE 1 V i"ID
Water Quality SectiG� �i
JAN 8,- 11091
Asheville Regional Ctrs
Asheville, [forth Carolin.

R_.
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, -HEALTH AND NATURAL RESOURCES
Division of Environmental Management
59 Woodfin Place Asheville, North Carolina 28802
January 6, 1992
PHILIP H. KLEIN
PO BOX 158
CAROLEEN NC 28019
SUBJECT: Notice of Violation - Effluent Limitations
NPDES No. NC0006009
BURLINGTON IND., CAROLEEN
RUTHERFORD County
Dear PHILIP H. KLEIN:
Review of subject self -monitoring report for the month
of November, 1991 revealed violation(s) of the following
parameter(s):
Reported Limits
Pipe Parameter Value/Unit Value/Type/Unit
001 50050 Q/MGD .1060 MGD .0180 FIN MGD
Remedial actions, if not already implemented, should be
taken to correct the problem(s). The Division of Environmental
Management may pursue enforcement actions for this and any
additional violations of State Law.. If there are questions or
a need for assistance, please call this office at 704/251-6208.
Sincerely,
R_6�1 a"A"
Roy Davis
Regional Supervisor
CC: Central Files
GKBDEX96/BL

. _0
State'. of North G�, . lina
'Department of Environment
and Natural Resources'
Division -of Water Quality
James B Hunt, Jr., Governor
Wayne McDevitt, Secretary
A: Preston Howard; Jr.-_' P.E., Director
NCDENR'
November 9, 1998
Mr. Edwin W. Horton _
Galey & Lord Industries, Inc: < !,
P.O.Box 158 AFC
Caroleen, North Carolina 28109?n%':
9 Subject:
J.
Dear Mr. Horton:
NPDES Permit Issuance
Permit No. NC0006009
G&L/Caroleen Plant
Rutherford County
In accordance with the application for discharge permit received on May 28, 1998, the
Division is forwarding herewith the subject state - NPDES permit. This permit is issued pursuant
to the requirements of North Carolina General Statute 143-215.1 and the Memorandum' of
Agreement between North Carolina and the U.S. Environmental Protection Agency dated
December 6, 1983.
The following changes were incorporated into this NPDES permit renewal:
• For Outfall 001, monitoring requirements and effluent limits were added for pH. In
addition, a biocide condition was added for this outfall, requiring pre -approval of any
biocides that may be added to this discharge.
• For Outfall 002, monitoring requirements for all parameters (flow, temperature; TRC,
pH) were changed from monthly to 2/Year. This. reflects current monitoring
requirements for cooling tower blowdown under general permit conditions.
• Microbiocide additives Nalco 2593 and Nalco 7346 have been approved for use in the air
washer discharge.via Outfall 001 at the same dosage and discharge conditions as. stated in
the 1993 Biocide Worksheets: In addition, the same biocides have been approved for use
y in the cooling water discharge via Outfall 002 at the dosages and discharge conditions
stated in the September 30. 1998 Supplemental Information Report:' Should you utilize a
different additive in the future or increase the dosage, you should contact this, Division
and submit the appropriate" information for approval prior to the change.
The permit expiration date has been changed to July 31, 2003.
If any parts, measurement frequencies or sampling requirements contained in this permit
are unacceptable to you, you have the right to an adjudicatory hearing upon written request
within thirty (30) days following receipt of this letter. This request must be in the form of a
written petition, conforming to Chapter 150B of the North. Carolina General Statutes, and filed
with the office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North Carolina
27611-7447. Unless such a demand is made, this permit shall be final and binding. -
Please take notice that this permit is not transferable. Part II, EA. addresses the
requirements to be followed in case of change in ownership or control of this. discharge.
Ibis permit does not affect the legal requirements to obtain other .permits which may be
required by the Division of Water Quality or permits required'by the Division of Land Resources,
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Page 2 i \
Mr: Edwin Horton
Galey.and Lord Industries, Inc:
November 9; 1998
Coastal Area Management Act, or any other Federal or Local governmental permits may be J
required.
If you have any questions or need additional information, please contact Mr. Tom
Belnick, telephone number [phone], extension 543.
Sincerely,
Original Signed B
David A. Goodrich
A. Preston Howard, Jr., P.E.
cc: Central Files
NPDES Unit, Permit File
heyiilile Re iona e" Water %ualj ,
Point Source Compliance/Enforcement Unit
Aquatic Toxicology Unit , -
U.S.EPA, Roosevelt Childress

In compliance with the provision of North Carolina General Statute 143.215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Galey and Lord Industries, Inc.
is hereby authorized to discharge wastewater from a facility located at
Caroleen Plant
U.S. Highway 221-A
Caroleen, North Carolina
r ~` Rutherford County
to receiving waters designated as Second Broad River in the Broad River Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in
Parts I, II, III, and IV hereof. _
This permit shall become effective December 1, 1998.
This permit and authorization to discharge shall expire at midnight on July 31, 2003.
Signed this day November 9, 1998.1
original Signed By
David, A. Goodrich
A. Preston Howard, Jr., P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

1
Permit No. NC0006009
SUPPLEMENT TO PERMIT COVER SHEET
I Galey and Lord Industries, Inc.
is hereby authorized to:
1. Continue to operate a 0.018 MGD wastewater treatment facility (Outfall 001)
consisting of a septic tank, surface sand filter, chlorination, and tablet dechlorination
to treat domestic wastewater and boiler blowdown at Galey and Lord Industries, Inc.-
Caroleen Plant, U.S. Highway 221-A, Caroleen, Rutherford County (See Part IIIA of
this permit), and
2. Continue to discharge cooling tower blowdown through Outfall 002, and
3. Discharge wastewater from said treatment works at the locations specified on the
attached map into Second Broad River, which is classified WS-IV waters in the Broad
River Basin.

i
Latitude: 351645
Longitude: 814800
USGS Quad #: F11SE -N
River Basin #: 030802
Receiving Stream: Second Broad R
Stream class: wS-1y
Galey & Lord Industries,
Caroleen Plant
NC 0006009.
Rutherford County

A (1). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - FINAL
Permit No. NC0006009
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge domestic wastewater and
boiler blowdown from outfall serial number 001. Such discharges shall be limited and monitored by the Permittee as specified below:
,EFFLUENT ' _.;
,.., .:
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'" .aY , i rat, A t£ „' . t s i .✓
a ;-+,. h`.:'�.d,. '' f •�
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.. e
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:.. yx r.. Da
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. „t.. K.. `s;. `S a g 3`
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r r 'Maximums r
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Weekly
Instantaneous
I or E
BOD, 5 day, 20°C
30.0 mg/I
45.0 mg/I
2/Month
Grab
E
Total Suspended Residue
30.0 mg/I
45.0 mg/I
2/Month
Grab
E
NH3 as N
Monthly
Grab
E
Total Residual Chlorine
2/Week
Grab
E
Temperature2
Weekly
Grab
E
pH
2/Month
Grab
E
Fecal Coliform (geometric mean)
200/100 ml
400/100 ml
2/Month
Grab
E
Notes:
1 Sample locations: E - Effluent, I — Influent
2 The temperature of the effluent shall not cause an increase in the temperature of the receiving stream of more than 2.8°C above natural temperatures, and
and in no case cause the receiving water temperature to exceed 32°C.
3 The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
There shall be no chromium, zinc, or copper added to the treatment system except as pre -approved additives to biocidal compounds. The permittee shall obtain
authorization from the Division prior to utilizing any biocide in the discharge. The permittee shall notify the Director in writing not later than ninety (90) days prior
to instituting use of any additional biocide used in air washer system which may be toxic to aquatic life other than those previously reported to the Division.
Such notification shall include completion of Biocide Worksheet 101 and a map locating the discharge point and receiving stream.
There shall be no discharge of floating solids or visible foam in other than trace amounts.

A (2). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - FINAL
Permit No. NC0006009 '
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge cooling tower blowdown
from outfall serial number 002. Such discharges shall be limited and monitored by the Permittee as'specified below: .
IEFF-CUENT".CHARAC� ;E I T
rrt= T R STI.CS)
F ccY r ,R
1 �7!•`Y� t3, �e.,Sj rt
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s
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FrequencY..,TYPe 1��
erage „ .,Averages �r-..MaximumrP:<ti
. a fLo
k cation.. .
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2/Year
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E
Temperature2
2/Year
Grab
E
Total Residual Chlorine3
2/Year
Grab
E
ITHT
2Near
Grab
E
Notes:
1. Sample locations: E — Effluent
2. The temperature of the effluent shall not cause an increase in the temperature of the receiving stream of more than 2.8°C above natural temperatures, and
and in no case cause the receiving water temperature to exceed 32°C.
3. Monitoring requirements apply only if chlorine is added to the treatment system.
4. 1 The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
There shall be no chromium, zinc, or copper added to the treatment system except as pre -approved additives to biocidal compounds. The permittee shall obtain
authorization from the Division prior to utilizing any biocide in the cooling water. The permitte shall notify the Director in writing not later than ninety (90) days
prior to instituting use of any additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported to the Division.
Such notification shall include completion of Biocide Worksheet 101 and a map locating the discharge point and receiving stream.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
l+

r '
I
PART I
motion B. Schedule of Compliance
4
1. The permittee shall comply with Final Effluent Limitations specified for discharges in accordance
with the following schedule:
Permittee shall comply with Final Effluent. Limitations by the effective date of the permit unless
specified below. _
2. Permittee shall- at all times provide the operation and maintenance necessary. to operate the
existing facilities at optimum efficiency.
I No later than 14 calendar days following a date identified in the above schedule of compliance,
the permittee shall submit either a report of progress or, in the case of specific actions being
required by identified dates, a written notice of compliance or noncompliance. In the latter case,
the notice shall include the cause of noncompliance, any remedial actions taken, and the
probability of meeting the next schedule requirements.

Part II
Page 1 of 14
1.
2.
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
The Director of the Division of Water Quality.
Means the Division of Water Quality, Department of Environment, Health and Natural Resources.
3. EMC
4.
61
Used herein rneans the North Carolina Environmental Management Commission.
The Fede al Water Pollution Control Act, also known as the Clean Water Act, as amended, 33 USC
1251, et. seq.
a. The "monthly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured during a calendar month on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
month. It is therefore, an arithmetic mean found by adding the weights of the pollutant found
each day of the month and then dividing this sum by the number of days the tests were
reported. The limitation is identified as "Monthly Average" in Part I of the permit.
i
b. The weekly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured during the calendar week (Sunday - Saturday) on which daily discharges are
sampled and measured, divided by the number of daily discharges sampled and/or measured
during such week. It is, therefore, an arithmetic mean found by adding the weights of
pollutants found each day of the week and then dividing this sum by the number of days the
tests were reported. This limitation is identified as "Weekly Average" in Part I of the permit.
c. The ',maximum daily discharge" is the total mass (weight) of a pollutant discharged during a
calendar day. If only one sample is taken during any calendar day the weight of pollutant
calculated from it is the "maximum daily discharge.' This limitation is identified as "Daily
Maximum," in Part I of the permit.
I
d. The ','average annual discharge" is defined as the total mass of all daily discharges sample
and/or measured during the calendar year on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
year. It is, therefore, an arithmetic mean found by adding the weights of pollutants found each
day of the year and then dividing this sum by the number of days the tests were reported. This
limitation is defined as "Annual Average" in Part I of the permit.

Part II
Page 2 of 14
6. Concentration Measurement
a. The "average monthly concentration," other than for fecal'coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or, measured during -a calendar month on
which daily discharges are sampled and measured, divided by the number of daily discharges
sampled and/or. measured during such month .(arithmetic mean of the daily .concentration
values). The daily concentration value is equal to the concentration of a composite sample or in
the case of grab samples is the arithmetic mean (weighted by flow value) of all the samples
collected during that calendar day. The average monthly count for fecal coliform bacteria is.
the geometric mean of the counts for samples collected during a. calendar month. This
limitation is identified as "Monthly Average" under "Other Limits" in Part I of the permit.
b. The "average weekly concentration;' other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled, and/or measured during a calendar week
(Sunday/Saturday) on which daily discharges are sampled and measured divided by the
number of daily discharges sampled and/or measured during such week (arithmetic mean of the
daily concentration values). The daily concentration value is equal to the concentration of a
composite sample. or in the case of grab samples is the arithmetic mean (weighted by flow
value) -of all the samples collected during that calendar day. The average weekly count for
fecal coliforrn bacteria is the geometric mean of the counts 'for samples collected- during a
calendar week. This limitation is identified as "Weekly Average" under "Other Limits" in.
Part I of the permit.
c. The "maximum daily concentration" is the concentration of a pollutant discharge during a
-calendar day.. If only one -sample is taken during any calendar day. the concentration of
pollutant calculated from it is'the "Maximum .Daily Concentration". It is identified as "Daily
Maximum" under "Other Limits" in Part I of the permit.
d. The "average annual concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges. sampled-and/or.'measured during a calendar year on
which daily discharges are sampled and measured, divided by the number of daily. discharges
sampled and/or measured during such year (arithmetic mean of the- daily concentration
values). The..daily concentration value is equal to the concentration of a composite sample or in
the case of grab samples is the arithmetic mean (weighted by flow value) of all the samples
collected during that -calendar day . The average yearly count for fecal coliform bacteria is the
geometric mean of the counts for samples collected during a calendar year: This limitation is
identified as "Annual Average" under "Other Limits" in Part I of the permit.
e. The "daily average concentration",(for dissolved oxygen) is the minimum allowableamount of
dissolved oxygen required to be available in the effluent prior to discharge averaged over a
calendar day. If only one dissolved oxygen sample is taken over a calendar day, the sample is
considered to be the "daily average concentration" for the discharge. It is identified as "daily
average" in the text of Part I.
f. The. "quarterly average concentration" is ' the average of all samples taken over a calendar
quarter. It is identified as "Quarterly Average Limitation" in the text of Part I of the permit.
g. A calendar quarter is defined as one of the following distinct periods: January through March,
April through June, July through September, and October'through December.

Pan Il
Page 3 of 14
7. Other Measurements
a. Flow, (MGD): The flow limit expressed in this permit is the 24 hours average flow, averaged
monthly. It is determined as the arithmetic mean of the total daily flows recorded during the
calendar month.
I
b. An "instantaneous flow measurement is a measure of flow taken at the time of sampling, when
both the sample and flow will be representative of the total discharge.
c. A "continuous flow measurement is a measure of discharge flow from the facility which occurs
continually without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for
infrequent maintenance activities on the flow device.
8. TyRes of Samples
a. Composite Sample: A composite sample shall consist of:
(1) a series of grab samples collected at equal time intervals over a 24 hour period of discharge
and combined proportional to the rate of flow measured at the time of individual sample
collection, or
(2) a series of grab samples of equal volume collected over a 24 hour period with the time
intervals between samples determined by a preset number of gallons passing the sampling
point. Flow measurement between sample intervals shall be determined by use of a flow
recorder and totalizer, and the present gallon interval between sample collection fixed at
no greater than 1 /24 of the expected total daily flow at the treatment system, or
(3) a single, continuous sample collected over a 24 hour period proportional to the rate of flow.
In accordance with (1) above, the time interval between influent grab samples shall be no
greater than once per hour, and the time interval between effluent grab samples shall be no
greater than once per hour except at wastewater treatment systems having a detention time of
greater than 24 hours. In such cases, effluent grab samples may be collected at time intervals
evenly spaced over the 24 hour period which are equal in number of hours to the detention time
of the system in number of days. However, in no case may the time interval between effluent
grab samples be greater than six (6) hours nor the number of samples less than four (4) during a
24 hour sampling period.
i
b. Grabs Sample: Grab samples are individual samples collected over a period of time not
exceeding 15 minutes; the grab sample can be taken manually. Grab samples must be
representative of the discharge or the receiving waters.
I
9. Calculation of Means
I
a Arithmetic Mean: The arithmetic mean of any set of values is the summation of the individual
values divided by the number of individual values.
I
b. Geometric Mean: The geometric mean of any set of values is the Nth root of the product of the
individual values where N is equal to the number of individual values. The geometric mean is
equivalent to the antilog of the arithmetic mean _of the logarithms of the individual values.
For purposes of calculating the geometric mean, values of zero (0) shall be considered to be one
C. Weighted by Flow Value: Weighted by flow value means the summation of each concentration
times its respective flow divided by the summation of the respective flows.

Part II .
Page 4 of 14
10. Calendar Day
A calendar day is defined as the period from.midnight'of one day until midnight of the next day.
However, for purposes of this permit, any consecutive 24-hour period that reasonably represents
the calendar day maybe used for sampling.
11. Hazardous Substance
A hazardous substance means any substance designated under 40 CFR Part 116 pursuant to Section
311 of the Clean Water Act.
12. Toxic Pollutant . . .
A toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
ECTION B. GENERAL CONDITIONS
The permittee must comply with all conditions of this permit.. Any permit noncompliance
constitutes a violation of.the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit renewal application.
a. The permittee shall comply with effluent standards or prohibitions established under section
307(a) of the C1ean.Water Act for toxic pollutants and with standards for sewage sludge use or
disposal established under section.405(d) of the Clean Water Act within the time provided in
the regulations that establish,these standards or prohibitions or standards for sewage sludge
use or disposal, even if the permit has not yet been modified to incorporate the requirem¢nt.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a
civil penalty not to exceed $25,000 per day, for each violation. Any person who -negligently
violates any permit .condition is subject to criminal penalties of $2,500.. to $25,000. per day of
violation, or imprisonment for not more than 1 year,.or both. Any.person who knowingly
violates permit conditions is subject to criminal penalties of $5,000 to $50,000 per day of.
violation, or imprisonment for not more than 3 years, or both. Also,.any, person who violates a
permit condition may be assessed awadministrative penalty not to exceed' $10,000 per violation
with the maximum amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33
US.C.1319 and 40' CFR 122AI (a)]
c. Under state law, a civil penalty of not more than ten thousand dollars ($10,000) per ,violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: North Carolina General;Statutes § 143-215.6A]
d. Any person may beassessed an administrative penalty by the Administrator for violating
section 301, 302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation
implementing any of such .sections in a permit issued under section 402 .of the Act.
Administrative penalties for Class I violations are not to :exceed $10,000 pei violation, with
the maximum amount of any Class I penalty assessed not to exceed $25,000. Penalties for Class
II violations are not to exceed $10,000 per day for each day during ,which the violation
continues, with the maximum amount of any Class ll penalty not to exceed $125,000.

Part H
Page 5 of 14
2.
3.
4.
5.
a
a
8.
9.
The pemuttee shall take all reasonable steps to minimize or prevent any discharge or sludge use or
disposal in violation of this permit which has a reasonable likelihood of adversely affecting
human health or the environment.
Except asp provided in permit conditions on 'Bypassing" (Part I1, C-4) and 'Tower Failures" (Part It,
C-7), nothing in this permit shall be construed to relieve the permittee from any responsibilities,
liabilities or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of
the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for consequential damages,
such as fish kills, even though the responsibility for effective compliance may be temporarily
Nothing lin this permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permittee is or may
be subject to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321.
Furthermore, the permittee is responsible for consequential damages, such as fish kills, even
though the responsibility for effective compliance may be temporarily suspended.
The issuance of this permit does not convey any property rights in either real or personal property,
or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personalf rights, nor any infringement of Federal, State or local laws or regulations.
This permit does not authorize or approve the construction of any onshore or offshore physical
structures or facilities or the undertaking of any work in any navigable waters.
The provisions of this permit are severable, and if any provision of this permit, or the application
of any provision of this permit to any circumstances, is held invalid, the application of such
vrovision to other circumstances, and the remainder of this permit, shall not be affected thereby.
The permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any
information which the Permit Issuing Authority may request to determine whether cause exists for
modifying, revoking and reissuing, or terminating this permit or to determine compliance with this
permit. I The permittee shall also furnish to the Permit Issuing Authority upon request, copies of
records :required to be kept by this permit.
If the permittee wishes to continue an activity regulated by this permit after the expiration date of
this permit, the permittee must apply for and obtain a new permit.
�J

Part I1
Page 6 of 14
10. )Expiration of Permit
The permittee is not authorized to discharge after the expiration date. In order to receive
automatic authorization to discharge -beyond the expiration date, the permttee shall submit such
information, forms, and fees as are required by the agency authorized to issue permits no later than
180 days prior to the expiration date.. Any permittee that has not requested renewal at least 180
days prior to expiration, or any permittee that does not have a permit after the expiration and has
not requested renewal at least 180 days prior to expiration, will subject the permittee to enforcement
procedures as provided in NCGS 143-215.6 and 33 USC I251 et. seq.
11. Sii^;y Reouirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed
and certified.
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer.or vice• president
of the corporation in charge of a principal business function, or any other person who
performs similar.policy or decision makingfunctions for the corporation, or (b) the manager
of one or more manufacturing production or operating facilities employing more than 250
persons or having gross annual sales or expenditures exceeding 25. million (in second quarter
1980 dollars), if authority to sign documents has been assigned or delegated to the manager
in accordance with corporate procedures.
-� (2) For a partnership or sole proprietorship: by a general partner or the .proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official.
b. All reports required by the permit and -•other information requested by the Permit Issuing
Authority shall be signed by a person described above or -by a duly •authorized representative of
that person. A person is a -duly authorized representative only if.
(1) . The authorization is made in writing by a person described above;
(2) The authorization specified, either an individual or.a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of 'equivalent
responsibility, or an individual or position having overall responsibility for environmental
matters for the company. (A duly authorized representative may thus be either a named
individual or any in occupying a named position.); and '
(3) The written authorization is submitted to the Permit Issuing Authority.
C. Certification. Any person signing a documentunder paragraphs a. .or b. -of this section shall
make the following certification:
"I certify, under penalty of law; that this document and all attachments were prepared under
my direction or supervision in accordance with a system designedto assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering
the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."

Part II
Page 7 of 14
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request
by the permittee for a permit modification, revocation and reissuance, or termination, or a
notificatio In planned changes or anticipated noncompliance does not stay any permit condition.
13. Permit Modification Revocation and Reissuance, or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and
modifying the permit, revoking and reissuing the permit, or terminating the permit as allowed by.
the laws, iules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122 and
123; Title I 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North
Carolina General Statute 143-215:1 et. al.
14.
1.
2.
All previous National Pollutant Discharge Elimination System Permits issued to this facility,
whether for operation or discharge, are hereby revoked by issuance of this permit. Me exclusive
authority) to operate this facility arises under this permit. The authority to operate the facility
under previously issued permits bearing this number is no longer effective. ) The conditions,
requirements, terms, and provisions -of this permit authorizing discharge under the National
Pollutant I Discharge Elimination System govern discharges from this facility.
Pursuant) to Chapter 90A-44 of North Carolina General Statutes, and upon classification of the
facility by' the Certification Commission, the permittee shall employ a certified wastewater
treatment plant operator in responsible charge (ORC) of the wastewater treatment facilities. Such
operator must hold a certification of the grade equivalent to or greater than the classification
assigned to the wastewater treatment facilities by the Certification Commission. The permittee
must also employ a certified back-up operator of the appropriate type and any grade to comply
with the conditions of Title 15A, Chapter 8A .0202. The ORC of the facility.must visit each Class 1
facility a,t least weekly and each Class II, III, and IV facility at least daily, excluding weekends
and holidays, and must properly manage and document daily operation and maintenance of the
facility and must comply with all other conditions of Title 15A, Chapter 8A .0202. Once the
facility is classified, the permittee shall submit a letter to the Certification Commission which
designates the operator in responsible charge within thirty days after the wastewater treatment
facilities l are 50% complete.
The permittee shall at all times properly operate and maintain all facilities and systems of
treatment and control (and related appurtenances) which are installed or used by the permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also
includes adequate laboratory controls and appropriate quality assurance procedures. This provision
requires the operation of back-up or auxiliary facilities or similar systems which are installed by a
permittee only when the operation is necessary to achieve compliance with the conditions of the
permit.

Part II
Page 8 of 14
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity" in order to maintain compliance with the condition, of this
permit.
4. Bypassing of Treatment Facilities
a. Definitions
(1) "Bypass" means the -known diversion of waste streams from any portion of a treatment
facility including the collection system, which is not a designed or established.or operating
mode for the facility.
(2) "Severe property damage" means substantial physical damage to property, damage to the
treatment facilities which causes them to become inoperable, or substantial and permanent
loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage does not mean economic loss caused by delays in
production. .
b. By not exceeding limitations.
The permittee may allow any bypass to occur which does not cause effluent limitations to be
exceeded, but only if it also is for essential maintenance to assure efficient operation. These
bypasses are not subject to the provisions of Paragraphs c. and d. of this section.
c. Notice
(1) Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall
submit prior notice, if possible at least ten days before the date of the'bypass; including an -
evaluation of the anticipated quality and affect of the bypass.
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated bypass as
required in Part II, E. 6. of this permit: (24 hour notice).
d. Prohibition of 'Bypass
(1) Bypass is prohibited and the;Permit Issuing Authority may take enforcement action against
a permittee for bypass, unless: '
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property
damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment
facilities;- retention of untreated wastes or maintenance during normal periods of
equipment downtime. This condition is not satisfied if adequate backup equipment should
have been installed in the exercise of reasonable engineering judgment -to prevent.. a bypass
which occurred during normal periods of equipment downtime or preventive maintenance;
and
(C) The permittee submitted notices as required under Paragraph c. of this section.
(2) The Permit Issuing Authority may approve an anticipated bypass, after considering its
adverse affects, if the Permit Issuing Authority determines that it will meet the three
conditions listed above in Paragraph d. (1) of this section.

_ Part II
Page 9 of 14
S. URsets
a. D
6.
7.
Is
means an exceptional incident in which there is unintentional and temporary
pliance with technology based permit effluent limitations because of factors beyond the
ble control of the permittee. An upset does not include noncompliance to the extent
by operational error, improperly designed treatment facilities, inadequate treatment
s, lack of preventive maintenance, or careless br improper operation.
b. Effect ;of an upset.
An upset constitutes an affirmative defense to an action brought for noncompliance with such
technology based permit effluent limitations if the requirements of paragraph c. of this
condition are met. No determination made during administrative review of claims that
noncompliance was caused by upset, and before an action for noncompliance, is final
administrative
istrative action subject to judicial review.
c. Conditions necessary for a demonstration of upset.
A permittee who wishes to establish the affirmative defense of upset shall demonstrate,
through properly signed, contemporaneous operating logs, or other relevant evidence that:
(1) An upset occurred and that the permittee can identify the cause(s) of, the upset;
(2) The permittee facility was at the time being properly operated; and
(3) The permittee submitted notice of the upset as required in Part II, E. 6. (b) (B) of this permit.
(4) The permittee complied with any remedial measures required under Part I1, B. 2. of this
pI rmit.
d. Burden of proof.
In any enforcement proceeding the permittee seeking to establish the occurrence of an upset has
the burden of proof.
Solids, sluldges, filter backwash, or other pollutants removed in the course of treatment or control of
wastewaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such
as to prevent any pollutant from such materials from entering waters of the State or navigable
waters of the United States. The permittee shall comply with all existing federal regulations
governing the disposal of sewage sludge. Upon promulgation of 40 CFR Part 503, any permit issued
by the Permit Issuing Authority for the utilization/disposal of sludge may be reopened and
modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR Part 503. The
permutes shall comply with applicable 40 CFR Part 503 Standards for the Use and Disposal of
Sewage Sludge (when promulgated) within the time provided in the regulation, even if the permit
is not modified to incorporate the requirement. The permittee shall notify the Permit Issuing
Authority of any significant change in its sludge use or disposal practices.
The permittee is responsible for maintaining adequate safeguards as required by DEM Regulation,
Title 15A, North Carolina Administrative Code, Subchapter 2H, .0124 Reliability, to prevent the
discharge of untreated or inadequately treated wastes during electrical power failures either by
means of alternate power sources, standby generators or retention of inadequately treated effluent. �,

' Part II
Page 10 of 14
SECTION D -MONITORING AND RECORDS_
1.
1. Representative Sampling
Samples collected. and measurements taken, as required herein, shall be characteristic .of the
volume and nature of the, permitted discharge. Samples collected at a frequency less than daily
shall be taken on a day and time that is characteristic of the discharge over the entire period
which the sample represents. All samples shall be taken at the monitoring points specified in this
permit and, unless otherwise specified, before the effluent joins or is diluted by any other
wastestream, body of water, or substance., Monitoring points shall, not be changed -without
notification to and the approval of the Permit Issuing Authority.
2.. Repo_ rtine
Monitoring results obtained during the. previous month(s) shall besummarized for each month and
reported on a monthly Discharge Monitoring Report (DMR) Form (DEM No. MR 1, 1.1, 2, 3) or
alternative forms approved by the Director; DEM, .postmarked no later than the 30th day
following the completed reporting period.
The first DMR is due on the last day of the month following the issuance'of the permit or -in the case
of a new facility, on the last day of. the month following the commencement of discharge.
Duplicate signed copies of these, and all other reports required herein, shall be submitted to the
following address:
Division of Water Quality.
Water Quality Section
ATTENTION: Central Files
�j Post Office Box 29535
Raleigh,, North Carolina 27626-0535
3. Flow Measurements
Appropriate flow measurement devices and, methods consistent with accepted scientific practices
shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges. The devices shall be installed, calibrated and maintained to ensure that the
accuracy of the measurements are consistent with the accepted capability of that type of device.
Devices selected shall be capable of measuring flows with a maximum deviation of less than + 10%
from the true discharge rates throughout the range of expected discharge volumes. Once -through
condenser cooling water flow which is monitored by pump logs, or pump hour meters as specified in
Part I of this permit and based on the manufacturer's pump curves shall not be subject to this
requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published
pursuant to NCGS 143-215.63 et. seq, the Water and Air. Quality Reporting Acts, and to regulations
published pursuant to Section 304(g), 33 USC 1314, .of the Federal Water Pollution Control Act, as
Amended, and Regulation 40 CFR 136; or in ,the case of sludge use or disposal, approved under 40
CFR 136, unless otherwise specified in 40 CFR 503, unless other test procedures have been specified
in this permit.
To meet the intent of the monitoring required by this permit, all test procedures must produce
n minimum detection and reporting levels that are below the permit discharge requirements and all
J data -generated must. be reported down to the minimum detection'or lower reporting level of the -
procedure. If no approved methods are determined capable of achieving minimum detection and

5
6.
7.
8.
(� Part 11
iPage 11 of 14
reporting levels below permit discharge requirements, then the most sensitive (method with the
lowest possible detection and reporting level) approved method must be used.
I
Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this permit shall,
upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for
not more than two years per violation, or by both. If a conviction of a person is for a violation
committed after a first conviction of such person under this paragraph, punishment is a fine of not
more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or both.
Except for records of monitoring information required by this permit related to the permittee's
sewage sludge use and disposal activities, which shall be retained for a period of at least five
years (or longer as required by 40 CFR 503), the permitted shall retain records of all monitoring
information, including all calibration and maintenance records and all original strip chart
recordings for continuous monitoring instrumentation, copies of all reports required by this permit,
for a period of at least 3 years from the date of the sample, measurement, report or application.
This period may be extended by request of the Director at any time.
For each measurement or sample taken pursuant to the requirements of this permit, the permittee
shall record the following information:
a. The date, exact place, and time of sampling or measurements;
b. The individuals) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individuals) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
The permittee shall allow the Director, or an authorized representative (including an authorized
contractor acting as a representative of the Director), upon the presentation of credentials and other
documents as may be required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions
of this permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this permit; and
d. Samlple or monitor at reasonable times, for the purposes of assuring permit compliance or as
otherwise authorized by the Clean Water Act, any substances or parameters at any location.

Part II
Page 12 of .14
( SECTION E. REPORTING REQUIREMENTS
1. Change in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit.
The discharge of any ,pollutant identified in this permit more frequently than or at a level in excess
of that authorized shall constitute a violation of the permit.
2. Planned Changes'
The permittee shall give notice to the Director as soon as possible of any planned physical
alterations or additions to the permitted facility. Notice is required only when:
a. The alteration or addition to a pehnitted facility may meet one of the criteria for determining
whether a facility is"a new source in 40 CFR Part 122.29 (b); or-
b. The alteration or addition could significantly change the nature or increase the quantity of
pollutants discharged. This notification applies to pollutants which are subject neither to
effluent limitations in the permit, nor to notification requirements. under 40 CFR Part 122.42 (a)
c. The alteration or addition results in a significant change in the permittee's sludge use or
disposal practices,. and such alternation,, addition or change may justify the application of
permit conditions that are different from or absent in the existing permit,. including notification
of additional use or disposal sites not reported during the permit application process or not
reported pursuant to an approved land application plan'.
3. Anticipated Noncompliance
The permittee shall give advance notice to the Director of any planned changes in the permitted
facility or activity which may result in noncompliance with permit requirements.
4. ` Transfers
This permit is not transferable to any person except after notice to the Director. The "Director may
require modification or revocation and reissuance of the permittee, and incorporate such other
.requirements as may be necessary under the Clean Water Act.
S. Monitoring_ Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit.
a. Monitoring results must be reported'on a Discharge Monitoring Report (DMR) (See Part II. D.2
of this permit) or forms provided by the Director for reporting results of monitoring of.sludge use
or disposal practices-
b. If the permittee monitors any pollutant more frequently than required by the permit, using test
procedures specified in Part II, D. 4. of this permit or in the case of sludge use or disposal,
approved under 40 CFR 503, or as specified.in this permit, the results of this monitoring shall be
included in the_calculation and reporting of the data submitted in the DMR.
c. Calculations -for all limitations which require averaging -of measurements shall utilize an
arithmetic mean unless otherwise specified by the Director in the permit.

Part II
Page 13 of 14
6. Twenty-four Hour Reporting
a. The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment. Any information shall be
provided orally within 24 hours from the time the permittee became aware of the
circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances. The written submission shall contain a
description of the noncompliance, and its cause; the period of noncompliance, including exact
dates ,and times, and if the noncompliance has not been corrected, the anticipated time it is
expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence
of the noncompliance.
i
b. The following shall be included as information which must be reported within 24 hours under
this paragraph:
(1) Any unanticipated bypass which exceeds any effluent limitation in the permit.
(2) Any upset which exceeds any effluent limitation in the permit.
(3) Violation of a maximum daily discharge limitation for any of the pollutants fisted by the
Director in the permit to be*reported within 24 hours.
c. The Director may waive the written report on a case -by -case basis for reports under paragraph
b. above of this condition if the oral report has been received within 24 hours.
7. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of
this permit at the time monitoring reports are submitted. The reports shall contain the information
listed in Part II. E. 6. of this permit.
Other Information
I
Where the permittee becomes aware that it failed to submit any relevant facts in a permit
application, or submitted incorrect information in a permit application or in any report to the
Director, lit shall promptly submit such facts or information.
9. Noncompliance Notification
The permittee shall report by telephone to either the central office or the appropriate regional
office of the Division as soon as possible, but in no case more than 24 hours or on the next working
day folio' ing the occurrence or first knowledge of the occurrence"of any of the following:
a. Any !occurrence at the water pollution control facility which results in the discharge of
significant amounts of wastes which are abnormal in quantity or characteristic, such as the
dumping of the contents of a sludge digester; the known passage of a slug of hazardous substance
through the facility; or any other unusual circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of
adequate wastewater treatment such as mechanical or electrical failures of pumps, aerators,
compressors, etc.
c. Anyi failure of a pumping station, sewer line, or treatment facility resulting in a by-pass
directly to receiving waters without treatment of all or any portion of the influent to such
station or facility.

s
Part II
Page 14 of 14
Persons reporting such occurrences by telephone shall also file a written report in letter form within
5 days following first knowledge of the occurrence.
10. Availability of Reports
Except for data determined to be confidential under NCGS '143-215.3(a)(2) or Section 308 of the
Federal Act, 33 USC 1318, all reports prepared in accordance, with the terms shall. be available for
public inspection at the offices of the Division of Water Quality. As required by the Act, effluent
data shall not be considered confidential. Knowingly making any false statement on any such
report may result in the imposition of criminal penalties as provided for -in NCGS 143-215.1(b)(2) or
in Section 309 of, the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement,
representation, or certification in any record or other .document submitted or required to be
maintained_ under this permit, including monitoring reports or reports of compliance or
noncompliance shall, upon conviction, be punished by a fine of not more than $10,000 per violation,
or by imprisonment for not more than two years per violation, or by both.

a.
14
C.
10
PART III
OTHER REQUIREMENTS
No construction of wastewater treatment facilities or additions to add to the plant's treatment
capacity or to change the type of process utilized at the treatment plant shall be begun until Final
Plans and Specifications have been submitted to the Division of Water Quality and written approval
and Authorization to Construct has been issued.
The permiti tee shall, upon written notice from the Director of the Division of Water Quality, conduct
groundwater monitoring as may be required to determine the compliance of this NPDES permitted
facility with the current groundwater standards.
The perm-dgee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe:
a.That any activity has occurred or will occur which would result in the discharge, on a routine or
frequent basis, of any toxic pollutant which is not limited in the permit, if that discharge will
exceedlthe highest of the following "notification levels';
(1) One, hundred micrograms per liter (100 ug/1);
hundred micrograms per liter (200 ug/1) for acrolein and acrylonitrile; five hundred
rograms per liter (500 ug/1) for 2.4-dinitrophenol and for 2-methyl-4.6-dinitrophenol; and
milligram per liter (I mg/1) for antimony;
(3) Five (5) times the maximum concentration value reported for that pollutant in the permit
application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine
or infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will
exceed the highest of the following "notification levels';
(1) Five hundred micrograms per liter (500 ug/1);
(2) One milligram per liter (1 mg/1) for antimony;
(3) Ten (10) times the maximum concentration value reported for that pollutant in the permit
The permittee shall continually evaluate all wastewater disposal alternatives and pursue the most
environmentally sound alternative of the reasonably cost effective alternatives. If the facility is in
substantial non-compliance with the terms and conditions of the NPDES permit or governing rules,
regulations or laws, the permittee shall submit a report in such form and detail as required by the
Division evaluating these alternatives and a plan of action within sixty (60) days of notification by the
Division.

4 V ♦ 1P n ' t
PART IV
ANNUAL ADMIIVI.STER NG AND COMPLIANCE MONITORING FEE
REQUIREMENTS
A. The permittee must pay the annual administering and compliance monitoring fee
within 30 (thirty) days after being billed by the Division. Failure to pay the fee in
a timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause this
Division to initiate action to revoke the permit.
500 copies of this public document were printed at a cost of $135.50 or $.27 per copy.

State of North C�.ti-�,lina .
Department of Environment,
_ Health and Natural Resources
Division of Environmental Management
,James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. Ralph Gibson
Galey and Lord Industries
P. O. Box 35528
Greensboro, NC 27425-0528
Dear Mr. Gibson:
ALT74 :!OVA
jD F= F l
July 5, 1994.
Subject: NPDES No. NC0006009
Galey and Lord Industries
formerly
Burlington Industries
Rutherford County
In accordance with your request received May 16, 1994, we are forwarding herewith
the subject permit) The only changes in this per(nit are in name and ownership. We also updated
the permits to current DEM regulations. This permit is issued pursuant to the requirements of
North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North
Carolina and the U. S. Environmental. Protection Agency dated December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this
permit are unacceptable to you, you have the right to an adjudicatory hearing upon written
request within thirty (30) days following receipt of this letter. This request must be. in the
form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes,
and filed with the Office of Administrative Hearings, Post Office Drawer 27447, Raleigh, North
Carolina 27611-7447. Unless such demand is made, this decision shall be final and binding.
Please take notice that this permit is not transferable. Part II, EA. addresses the
requirements to be followed in case of change in ownership or control of this discharge.
This permit does not affect the legal requirement to obtain otherpermits which may be
required by the Division of Environmental Management or permits required by the Division of
Land Resources, Coastal Area Management.Act or any other Federal or Local governmental
permit that may be required. If you have any questions concerning this permit, please contact
Susan Robson at telephone number 919/733-5083.
cc: Mr. Jim Patrick, EPA
egionaf • , e
Compliance
Central Files-_
Technical Support Branch
Kim Brantley
Aquatic Toxicology Unit
Ori§lflflPf �rled By
David A. Goodrich
A. Preston Howard, Jr., P.E.
`1
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

a °
Permit No. NC0006009
STATE OF NORTH CAROLINA
DEPARTMENT'OF ENVIRONMENT, HEALTH; AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North'Carolina General Statute 143-215.1,
other lawful standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Galey & Lord Industries, Inc.
is hereby authorized to discharge wastewater from a facility located at
The Caroleen Plant
US Highway 221-A
Caroleen
Rutherford County
to receiving waters designated as Second Broad River in the Broad River Basin
in accordance with effluent limitations, monitoring requirements, and other conditions set forth in
Parts I, II, and III hereof.
This permit shall become effective July -5, 1994
This permit and the authorization to discharge shall expire at midnight on November 30, 1998
Signed this day July 5, 1994
Original Signed By
®avid A, Goodrich
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

Permit No. NC0006009
SUPPLEMENT TO PERMIT COVER SHEET
Galey & Lord Industries, Inc.
is hereby authorized to:
1. Continue to discharge 0.018 MGD from a wastewater treatment facility consisting of a septic
tank, surface sand filter and chlorination (Outfall 001) and cooling tower blowdown (Outfall
002) located at The Caroleen Plant, US Highway 221-A, Caroleen, Rutherford County (See
Part III of this Permit), and
2. Discharge from said treatment works at the location specified on the attached map into Second
Broad River which is classified Class WS-IV waters in the Broad River Basin.
F

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A. O. EFFLUENT LIMITATIONS AND MONITORING.REQUIREMENTS, FINAL
Permit No. NC0006009 ,
During the period beginning
on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial number 001.
Such discharges shall be limited and monitored by the permittee as specified below:
Effluent Characteristics
Discharge Limitations
Monitoring
Requirements
'
Measurement
Sample _
'Sample
Monthly Avg_, Weekly Avg. Daily Max
Frequency
Type
Location
Flow
0.018 MGD
Weekly
Instantaneous
I or E
BOD, 5 day, 200C
30.0 mg/I 45.0 mg/I
2/Month
Grab
E
Total Suspended Residue
30.0 mg/I, 45.0 mg/I
2/Month
Grab
E
NH3 as N
Monthly
Grab
E
Fecal Coliform (geometric mean)
200.0 /100 ml 400.0 /100 ml
-2/Month
Grab
E —�
Total Residual Chlorine
2/Week
Grab
E
Temperature
Weekly
Grab
E
*Sample locations: E - Effluent, I -Influent
There shall be no discharge of floating solids or visible foam in other than trace amounts.
' 1

J. o
A. (). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FINAL Permit No. NC0006009
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge from
outfall(s) serial number 002. Such discharges shall be limited and monitored by the permittee as specified below:
Effluent Characteristics
Discharge Limitations Monitoring
Requirements
Lbs/day Units Lspecifyj Measurement
Sample
*Sample
Mon. Avg. Daily Max Mon. Ava. Daily Max. Frequency
Txpe
Location
Flow
Monthly
Instantaneous
. E
Temperature
* * * Monthly
Grab
E, U, D
Total Residual Chlorine***
Monthly
Grab
E
IJ
THERE SHALL BE NO CHROMIUM, ZINC, OR COPPER ADDED TO THE TREATMENT SYSTEM EXCEPT AS PRE -APPROVED
ADDITIVES TO BIOCIDAL COMPOUNDS.
* Sample Locations: E - Effluent, U - Upstream, D - Downstream
** The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving stream of more than 2.8°C and in
no case cause the ambient water temperature to exceed 32°C.
*** Monitoring requirements only apply if chlorine is added to the cooling water.
The permittee shall obtain authorization from the Division of Environmental Management prior to utilizing any biocide in the cooling water (See
Part III of this Permit).
The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units and shall be monitored monthly at the effluent by grab
sample.
There shall be no discharge of floating solids or visible foam in other than trace amounts.

I PART
Section B. Schedule of Compliance
1. The permittee shall comply with Final Effluent Limitations specified, for discharges in
accordance with the following schedule:
Permittee shall comply with Final Effluent Limitations by the effective date of the permit unless
specified below.
2. Pernvttee shall at all times -provide the operation and maintenance necessary to operate the
existing facilities at optimum efficiency.
. No later than 14 calecidar days followingz date -identified in the above schedule of compliance,
the permittee shall submit either a report of progress or, in the case of specific actions being
required by identified dates, a written notice of compliance or noncompliance. In the latter
case, the notice shall include the cause of noncompliance, any remedial actions taken, and the
probability of meeting the next schedule requirements.

Part II
� Page 1 of 14
PART II
STANDARD CONDITIONS FOR NPDES PERMITS
SECTION A. DEFINITIONS
1. Permit Issuing Authority
The Diredtor of the Division of Environmental Management.
2. DEM or Divisi
Means the Division of Environmental Management, Department of Environment, Health and
Natural Resources.
3. EN1C
Used herein means the North Carolina Environmental Management Commission.
4. Act or "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended, 33
t;SC 1251, et. seq.
5. Mass/Da�- Measurements
a. The j'monthly average discharge" is defined as the total mass of all daily discharges
sampled and/or measured during a calendar month on which daily discharges are sampled
and measured, divided by the number of daily discharges sampled and/or measured during
such I month. It is therefore, an arithmetic mean found by adding the weights of the
pollutant found each day of the month and then dividing this sum by the number of days
the tests were reported. The limitation is identified as "Monthly Average" in Part I of the
t,ermt.
b. The '1'weekly average discharge" is defined as the total mass of all daily discharges sampled
and/or measured durin; the calendar week (Sunday - Saturday) on which daily discharges
are siampled and measured, divided by the number of daily discharges sampled and/or
measured during such week. It is, therefore, an arithmetic mean found by adding the
weights of pollutants found each day of the week and then dividing this sum by the
number of days the tests were reported. This limitation is identified as "Weekly Average"
in Part I of the permit.
c. The maximum daily discharge" is the total mass (weight) of a pollutant discharged during
a calendar day. If only one sample is taken during any calendar day the weight of pollutant
calculated from it is the "maximum daily discharge." This, limitation -is identified as "Daily
Maximum," in Part I of the permit.
d. The'average annual discharge" is defined as the total mass of all daily discharges sampled
and/or measured during the calendar year on which daily discharges are sampled and
measured, divided by the number of daily discharges sampled and/or measured during such
year. It is, therefore, an arithmetic mean found by adding the weights of pollutants found
each day of the year and then dividing this sum by the number of days the tests were
reported. This limitation is defined as "Annual Average" in Part I of the permit.

1 Part II
Page 2 of 14
6. Concentration Measurement
a. The "average monthly concentration," other than for fecal coliform bacteria, is the sum of
the concentrations of all daily discharges sampled and/or measured during a calendar_ month
on which daily discharges are sampled and measured, divided by the number of daily
discharges sampled and/or measured during such month (arithmetic mean of the daily
concentration values). The daily concentration value is equal to the concentration of a
composite sample or in the case of grab samples is the arithmetic mean (weighted by flow
value) of all the samples collected during that calendar day. The. average monthly count for
fecal coliform bacteria is the geometric mean of the counts for samples collected during a
calendar month. This limitation is identified as "Monthly Average" under "Other Limits" in
Part I of the permit.
b. The "average weekly concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar week
(Sunday/Saturday) on which daily discharges are sampled and measured divided by the
number of daily discharges sampled and/or measured during such week (arithmetic mean of
the daily concentration values). The daily concentration value.is equal to the concentration
of a composite sample or in the case of grab samples is the arithmetic mean (weighted by
flow value) of all the samples collected during that calendar day. The average weekly count
for fecal coliform bacteria is the geometric mean of the counts for samples collected during
A* calendar week. This limitation is identified as "Weekly Average" under "Other Limits" in
Part I of the permit.
c. The "maximum daily concentration" is the concentration of a pollutant discharge during a
calendar day. If only one sample is taken during any calendar day the concentration of
pollutant calculated from it is the "Maximum Daily Concentration". It is identified as
"Dail}" Maximum" under "Other Limits" in Part I of the permit.
d . The "average annual concentration," other than for fecal coliform bacteria, is the sum of the
concentrations of all daily discharges sampled and/or measured during a calendar year on
which. daily discharges are sampled and measured divided by the number of daily
discharges sampled and/or measured during such year (arithmetic mean of the daily
concentration values). The daily concentration value is equal to the concentration of a
composite sample or in the case of grab,samples is -the arithmetic mean (weighted by flow
value) of all the samples collected during.that calendar day'. The average yearly count for
fecal'coliform bacteria is the geometric mean of the counts for samples collected during a
calendar year. This limitation is identified as "Annual Average" under "Other Limits" in
Part I of the permit.
e. The "daily average concentration" (for dissolved oxygen) is the minimum allowable amount
of dissolved oxygen required to be available in the effluent prior to discharge averaged
over a calendar day. If only one dissolved oxygen sample is taken over a calendar day, the
sample is considered to be the "daily average concentration" for the discharge. It is
identified as "daily average" in the text of Part I-.
f. The "quarterly average concentration" is the average of all samples taken over a calendar
quarter. 'It is identified as "Quarterly Average Limitation" in the text of Part I of the permit.
g. A calendar quarter is defined as one of the following distinct periods: January through
March, April through June, July through September; and October through December.

�J
Part II
Page 3 of 14
7. Other Measurements
a. Flow,` (MGD): The flow limit expressed in this permit is the 24 hours average flow,
averaged monthly. It is determined as the arithmetic mean of the total daily flows recorded
during the calendar month.
b. An "instantaneous flow measurement" is a measure of flow taken at the time of sampling,
when iboth the sample and flow will be representative of the total discharge.
c. A "continuous flow measurement" is a measure of discharge flow from the facility which
occurs continually without interruption throughout the operating hours of the facility. Flow
shall be monitored continually except for the infrequent times when there may be no flow
or for infrequent maintenance activities on the flow device.
8. Types of ISamnles
I
a. Composite Sample: A composite sample shall consist of:
i
(1) a!series of grab samples collected at equal time intervals over a 24 hour period of
discharge and combined proportional to the rate of flow measured at the time of
individual sample collection, or
(2) a series of grab samples of equal volume collected over a 24 hour period with the time
intervals between samples determined by a preset number of gallons passing the
sampling point. Flow measurement between sample intervals shall be determined by
use of a flow recorder and totalizer, and the present gallon interval between sample
collection fixed at no greater than 1/24 of the expected total daily flow at the treatment
system, or
(3) a�sinole, continuous sample collected over a 24 hour period proportional to the rate of
flow.
In accordance with (1) above, the time interval between influent grab samples shall be no
greater than once per hour, and the time interval between effluent grab samples shall be no
greater than once per hour except at wastewater treatment systems having a detention time
of greater than 24 hours. In such cases, effluent grab samples may be collected at time
inter] -als evenly spaced over the 24 hour period which are equal in number of hours to the
detention time of the system in number of days. However, in no case may the time interval
bet".1een effluent grab samples be greater than six (6) hours nor the number of samples less
than four (4) during a 24 hour sampling period.
b. Grab Sample: Grab samples are individual samples collected over a period of time not
exceieding 15 -minutes; the grab sample can be taken manually. Grab samples must be
representative of the discharge or the receiving waters.
i
9. Calculation of Means
a Arithmetic Mean: The arithmetic mean of any set of values is the summation of the
indi�•idual values divided by the number of individual values.
b. Geometric Mean: The geometric mean of any set of values is the Nth root of the product of
the individual values where N is equal to the number of individual values. The geometric
mean is equivalent to the antilog of the arithmetic mean of the logarithms of the individual
values. For purposes of calculating the geometric mean, values of zero (0) shall be
considered to be one (1).

Part II
Page 4 of 14
Weighted by Flow Value: Weighted by flow value means the summation of each
concentration times its respective flow divided by the summation of the respective flows.
10. Calendar Dav
A calendar day is defined as the period from midnight of one day until midnight of the next
day. However, for purposes of this permit, any consecutive 24-hour period that reasonably
represents the calendar day may be used for sampling.
11. Hazardous Substance
A hazardous substance means any subs tan ce.'designated under 40 CFR, Part 116 pursuant to
Section 311 of the Clean Water Act.
12. Toxic Pollutant
A toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
SECTION B. GENERAL. CONDITIONS
1. Duty to Comply
The permittee must comply with all conditions -of this permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit renewal
application.
The permittee shall comply with effluent standards or prohibitions 'established under
section 307(a) of the Clean Water Act for toxic pollutants and with standards for sewage
sludge use or disposal established under section 405(d) of the Clean Water Act within the
time provided in the regulations that establish these standards or prohibitions or standards
for sewage sludge use or disposal, even if the permit has not. yet been modified to
incorporate the requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to
a civil penalty not to exceed S25,000 per day for each violation. Any person who
negligently violates any permit condition is subject to criminal penalties of 52,500 to
525,000 per day of violation, or imprisonment for not more than 1 year, or both. Any
person who knowingly violates permit conditions is subject to criminal penalties of $5,000
to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. Also,
any person who violates a permit condition may be assessed an administrative penalty not
to exceed $10,000 per violation with the maximum amount not to exceed $125,000. [Ref:
Section 300 of the Federal Act 33 U.S.C. 1310 and 40 CFR 122.41 (a)]
c. Under state law, a civil penalty of not more than ten thousand dollars ($10,000) per
violation may be assessed against any person who violates or fails to act in accordance with
the terms, conditions, or requirements of a permit. [.Ref: North Carolina General Statutes
§ 143-215.6A]
d. Any person may be assessed an administrative penalty by the Administrator for violating
section 301, 302, 306, 307, 308, 318, or 405 "of the Act, or any permit condition or
limitation implementing any, of such sections in a permit issued under section 402 of the
Act. Administrative penalties for Class I violations are not to exceed $10,000 per violation,
with the maximum a, mount of any Class I penalty assessed not to exceed $25,000.

Part II
Page 5 of 14
3
4.
5.
i
Penalties for Class II violatioi
which) the violation continues,
exceed $125,000.
Duo; to Mitigate
I
s are not to exceed $10,000 per day for each day during
with the maximum amount of any Class II penalty not to
The permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use
or disposal in violation of this permit which has a reasonable likelihood of adversely affecting.
human health or the environment.
ivil and 'Criminal Liabili
Except as provided in permit conditions on "Bypassing" (Part II, C-4) and "Power Failures"
(Part II, C-7), nothing in this permit shall be construed to relieve the permittee from any
responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3,143-
215.6 or !Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is
.responsible for consequential damages, such as fish kills, even though the responsibility for
effective compliance may be temporarily suspended.
Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve
the permittee from an), responsibilities, liabilities. or penalties to which the permittee is or may
be subject to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321.
Furthermore, the permittee is responsible for consequential damages, such as fish kills. even
though thie responsibility for effective compliance may be temporarily suspended.
i
The issuance of this permit does not convey any property rights in either real or personal
propem l or any exclusive privileges, nor does it authorize any injury to private property or any
invasion of personal rights, nor any infringement of Federal, State or local laws or regulations.
6. Onshore for Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical
structures or facilities or the undertaking of any work in any navigable waters.
7.
The pro` �isions of this permit are severable, and if any provision of this permit, or the
application of any provision of this permit to any circumstances, is held invalid, the application
of such provision to other circumstances, and the remainder of this permit, shall not be affected
thereby.
The permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any
information which the Permit Issuing Authority may request to determine whether cause exists
for modifying. revoking and reissuing, or terminating this permit or to determine compliance
with this permit. The permittee shall also furnish to the Permit Issuing Authority upon
request. 1copies of records required to be kept by this permit.

i
L Part II
Page 6 of 14
9. Duty to Reapp]v
If the permittee wishes to continue an activity regulated by this permit after the expiration date
of this permit, the permittee must apply for and obtain a new permit.
10. Expiration of Permit
The permittee is not authorized to discharge after the expiration date. In order to receive
automatic authorization to discharge beyond the expiration date, the pem-inee shall submit such
information, forms, and fees as are required by the agency authorized to issue permits no later
than IN days prior to the expiration date. Any permittee that has not requested renewal. at least
180 days prior to expiration, or any permittee that does not have a permit after the expiration
and has not requested renewal at least 180 days prior to expiration, will subject the permittee to
enforcement procedures as provided in NCGS 143-215.6 and 33 US 1251 et. seq.
11. Signatory Requirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be
signed and certified.
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate. officer. For the purpose of this Section,
a responsible corporate officer means: (a-) a president, secretary; treasurer or vice
president of the corporation in charge of a principal business function, or any other
person who performs similar policy or decision making functions for the corporation,
or (b) the manager of one or more manufacturing production or operating facilities
employing more than 250 persons or having gross annual sales or expenditures
exceeding 25 million (in second quarter 1980 dollars), if authority to sign documents
has been assigned or delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal
executive officer or ranking elected official.
b. All reports required by the permit and other information requested by the Permit Issuing
Authority shall be signed by a person described above or by a duly authorized
representative of that person. A person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility for
the overall operation of the regulated facility or activity, such as, the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for
environmental matters for the company. (A duly authorized representative may thus be
either a named -individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Permit Issuing Authority.

Part II
Page 7 of 14
12.
13
c. Certification. Any person signing a document under paragraphs a. or b. of this section
shall make the following certification:
"I certify, under penalty of law, that this document and all attachments were prepared under
my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a
request by the permittee fora permit modification, revocation and reissuance, or termination,
or a notification of planned changes or anticipated noncompliance does not stay any permit
condition'.
Permit :Modification. Revocation and Reissuance, or Termination
The issuance of this permit does not prohibit the permit issuing authority from reopening and
modifying the permit, revoking and reissuing
la the permit, or terminating the permit as allowed
by the �!s, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts
122 and 123, Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and
North Carolina General Statute 143-215.1 et. al.
14. Previous Permits
All previous National Pollutant Discharge Elimination System Permits issued to this facility,
whether for operation or discharge, are hereby revoked by issuance of this permit. [The
exclusive authority to operate this facility arises under'this permit. The authority to operate the
facility under previously issued permits bearing this number is no longer effective. ] The
conditions, requirements, terms, and provisions of this permit authorizing discharge under the
National IPollutant Discharge Elimination System govern discharges from this facility.
Pursuant! to Chapter 90A-44 of North Carolina General Statutes, and upon classification of the
facility by the Certification Commission, the permittee shall employ a certified wastewater
treatment plant operator in responsible charge (ORC) of the wastewater treatment facilities.
Such operator must hold a certification of the grade equivalent to or greater than the
classification assigned to the wastewater treatment facilities by the Certification Commission.
The permittee must also employ a certified back-up operator of the appropriate type and any
grade tolcomply with the conditions of Title 15A, Chapter 8A .0202. The ORC of the facility
must visit each Class I facility at least weekly and each Class II, III, and IV facility at least
daily, excluding weekends and holidays, and must properly manage and document daily
operation and maintenance of the facility and must comply with all other conditions of Title
15A, Chapter 8A .0202. Once the facility is classified, the:.permittee shall submit a letter to the
Certification Commission which designates the operator in responsible charge within thirty
days after the wastewater treatment facilities are 5057c complete.

0 Part II
Pace 8 of 14
2. Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of
treatment and control (and related appurtenances) which are installed or used by the permittee to
achieve compliance with the conditions of this permit. Proper operation and maintenance also
includes adequate laboratory controls and appropriate quality assurance procedures. This
provision requires the operation of back-up or auxiliary facilities or similar systems which are
installed by a permittee only when the operation is necessary to achieve compliance with the
conditions of the permit.
3. Need to Halt or Reduce not a Defense
It shall not be a defense for- a permittee in an enforcement action that it would have been
necessary to halt or reduce the permitted activity in order to maintain compliance with the
condition of this permit.
4. Bvpassinaof Treatment Facilities
a. Definitions
(1) 'Bypass means the known diversion of waste streams from any portion of a treatment
facility including the collection system, which is not a designed or established or '
operating mode for the facility.
(2) "Severe property damage" means substantial physical damage to property, damage to
the treatment facilities which causes them to become inoperable, or substantial and
permanent loss of natural resources -which can reasonably be expected -to occur in the
absence of a bypass. Severe property damage does not mean economic loss caused by
delays in production.
b. Bypass not exceeding limitations.
The permittee may allow any bypass to occur which does not cause effluent limitations to
be exceeded, but only if it' also is for essential maintenance to assure efficient operation.
These bypasses are not. subject to the provisions of Paragraphs c.. and d. of this section.
c. 'Notice
(1) Anticipated bypass. If the permittee knows in, advance of the need for a bypass, it
shall submit prior notice, if possible at least ten days before the date of the bypass;
including an evaluation of the"anticipated quality and affect of the bypass.
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated bypass as
required in Part II, E. 6. of this permit. (24.hour notice).
d. Prohibition of Bypass
(1) Bypass is prohibited and the Permit Issuing Authority may take enforcement action
against a perrruttee for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property
damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary
treatment faciiities, retention of untreated wastes or maintenance during normal

.� Part II
Page 9 of 14
pieriods of equipment downtime. This condition is not satisfied if adequate backup
equipment should have been installed in the exercise of reasonable engineering
judgment to prevent a bypass which occurred during normal periods of equipment
doh ntime or preventive maintenance; and
(C) The permittee submitted notices as required under Paragraph c. of this section.
(2) The Permit Issuing Authority may approve an anticipated bypass, after considering its
adverse affects, if the Permit Issuing Authority determines that it will meet the three
conditions listed above in Paragraph d. (1) of this section.
5. Upsets
a. Definition.
I
"L'pse,t " means an exceptional incident in which there is unintentional and temporary
noncompliance with technology based permit effluent limitations because of factors
beyond the reasonable control of the permittee. An upset does not include noncompliance
to the extent caused by operational error, improperly designed treatment facilities,
inadequate treatment facilities, lack of preventive maintenance, or careless or improper
operation.
b . Effect' of an upset.
An upset constitutes an affirmati>-e defense to an action brought for noncompliance with
such technology based permit effluent limitations if the requirements of paragraph c. of this
condition are met. No determination made during administrative review of claims that
noncompliance was caused by upset, and before an action for noncompliance, is final
administrative action subject to judicial review.
c. Conditions necessai-y for a demonstration of upset.
1
A permittee who wishes to establish the .affirmative defense of upset shall demonstrate,
throuzh properly signed, contemporaneous operating logs, or other relevant evidence that:
(1) An upset occurred and that the permittee can identify the cause(s) of the upset;
(2) The permittee facility was at the time being properly operated; and
(3) The permittee submitted notice of the upset as required in Part II, E. 6. (b) (B) of this
(4) The permittee complied with any remedial measures required under Part II, B. 2. of this
o.'ermit.
d. Burden of proof.
In any enforcement proceeding the permittee seeking to establish the occurrence of an upset
has tie burden of proof.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or
control of waste„vaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in
a manner such as to prevent any pollutant from such materials from entering waters of the State
or navigable waters of the united States. The permittee shall comply with all existing federal
�I
i

0 Part II
Page 10 of 14
regulations governing the disposal of sewage sludge. Upon promulgation of 40 CFR Part 503,
any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40
CFR Part 503. The permittee shall comply with applicable 40 CFR Part 503 Standards for the
Use and- Disposal of Sewage Sludge (when promulgated) within the time provided in the
regulation, even if the permit is not modified to incorporate the requirement. The permittee.
shall notify the Permit -Issuing Authority of any significant change in its sludge use or disposal
practices.
7. Power Failures
The permittee is responsible for maintaining adequate safeguards as required by DEM
Regulation, Title 15A, North Carolina Administrative Code, Subchapter 2H, .0124 Reliability;
to prevent the discharge of untreated or inadequately treated wastes during electrical power
failures either by means of alternate power sources, standby generators or retention of
inadequately treated effluent.
SECTION D. MONITORING ANTD RECORDS.
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the
volume and nature of the permitted discharge. Samples collected at a frequency less than daily
shall be taken on a day and time that is characteristic of the discharge over the entire period
which the sample represents. All samples shall be taken at the monitoring points specified in
this permit and, unless otherwise specified,, before the effluent joins or is diluted by any other
wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority.
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month
and reported on a monthly,Discharge Monitoring Report (DMR) Form (DEM No. MR 1,1.1, 2,
3) or alternative forms approved by the Director, DEM, postmarked no later than the 30th day
following the completed reporting period.
The first D1MIRis due on the last day of the month following the issuance of the permit or in the
case of a new facility, on the last day of the month following the commencement of discharge.
Duplicate signed copies of these, and all other reports required herein, shall be submitted. to the
following address:
Division of Environmental Management
Water Quality Section
ATTENTION: Central Files
Post Office Box 29535
Raleigh, North Carolina 27626-0535 "
3.` Flow Measurements
Appropriate flow measurement devices. and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy.and reliability of measurements of
the volume of monitored discharges: The devices shall be installed, calibrated and maintained
to ensure :that the accuracy of the measurements- are consistent with the accepted capability of
that type of device. Devices selected. shall be capable of measuring flows with a maximum
deviation of less than + 10% from the true disc;,prge rates throughout the range of expected

�+ ! Part II
Page 11 of 14
At
discharge volumes. Once -through condenser cooling water flow which is monitored by pump
logs, or pump hour meters as specified in Part I of this permit and based on the manufacturer's
IM pump cu ies shall not be subject to this requirement.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published
pursuant to NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to
regulations published pursuant to Section 304(g), 33 USC 1314, of the Federal Water
Pollution Control Act, as Amended, and Regulation 40 CFR 136; or in the case of sludge use or
disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless
other test procedures. have been specified in this permit.
To meet the intent of the monitoring required by this permit, all test procedures must produce
minimumldetection and reporting levels that are below the permit discharge requirements and
all data generated must be reported down to the minimum detection or lower reporting level of.
the procedure. If no approved methods are determined capable of achieving minimum
detection land reporting levels below permit discharge requirements, then the most sensitive
(method with the lowest possible detection,and reporting level) approved method must be used.
5. Penalties for Tampering
I
The Clean Water Act provides that any person who falsifies, tampers with, 'or knowingly
renders inaccurate, any monitoring device or method required to be maintained under this
permit shall, upon conviction, be punished by a fine of not more than S10,000 per violation, or
by imprisonment for not more than two years per violation, or by both. If a conviction of a
person is ifor a violation committed after a first conviction of such person under this paragraph,
punishment is a fine of not more than S20,000 per day of violation, or by imprisonment of not
more than 4 years, or both.
6. Records Retention
I
Except for records of monitoring information required by this permit related to the permittee's
sewage sludge use and disposal activities, which shall be retained for a period of at least five
years (or longer as required by 40 CFR 503), the permittee shall retain records of all
monitoringa information, including all calibration and maintenance records and all original strip
chart recordings for continuous monitoring instrumentation, copies of all reports required by
this permit, for a period of at least 3 years from the date of the sample, measurement, report
or application. This period may be extended by request of the Director at any time.
►A
For each measurement or sample taken pursuant to the requirements of this permit, the
permittee shall record the following information:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d . The individuals) who performed the analyses;
e. The analytical techniques or methods used; and
f. The i zsults of such analyses.

(�0 � Part II
Page 12 of 14
8. Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized
contractor acting as a representative of the Director), upon the presentation of credentials and
other -documents as may be required'by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, -at reasonable times, any records that must be kept under the
conditions of this permit; -1
c. Inspect at reasonable times any. facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or
as otherwise authorized, by the Clean Water Act, any substances or parameters at any
location.
SECTION E REPORTING REQUIREMENTS
1. Chanee in Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this
permit. The discharge of any pollutant identified in this permit more frequently than or at a
level in excess of that authorized shall constitute a violation of the permit.
2. Planned Changes
The .permittee shall give notice to the Director as soon as possible of any planned physical
alterations or additions to the permitted facility. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for determining
whether a facility is a new source in 40 CFR Part 122.29 (b); or
b. The alteratiori or addition could significantly change the nature or increase the quantity of
pollutants discharged. This notification applies to'pollutants which are subject neither to
effluent limitations in the permit, nor to notification requirements under 40 CFR Part 122.42
(a) (1).
c. The alteration or addition results in a significant ch-ange in the permittee's sludge use or
disposal practices, and such alternation, addition or change may justify the application of
permit conditions that are different from or absent in the existing permit, including
notification of additional use or disposal sites not reported during the permit application
process or not reported pursuant.to an approved land application plan.
- J
3. Anticipated Noncompliance
The permittee shall give advance notice to the Director of any planned changes in the permitted
facility or activity which may result in noncompliance with permit requirements.

Part II
Pace 13 of 14
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director
may require modification or revocation and reissuance of the permittee and incorporate. such
other requirements as may be necessary under the Clean Water Act.
5. Monitoring Reports
Monitoring results shall be reported, at the intervals specified elsewhere in this permit.
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part H.
D. 2 of this permit) or forms provided by the Director for reporting results of monitoring of
sludge use or disposal practices.
b. If the,permittee monitors any pollutant more frequently than required by the permit, using
test procedures specified in Part II, D. 4. of this permit or in the case of sludge use or
disposal, approved under 40 CFR 503, or as specified in this permit, the results of this
monitoring shall be included in the calculation and reporting of the data submitted in the
D110R`.
c. Calculations for all limitations which require averaging of measurements shall utilize an
arithmetic mean unless otherwise specified by the Director in the permit.
6, Twenty-four Hour Reporting
I
a. The permittee shall report to the central office or the appropriate regional office any
noncompliance which may endanger health or the environment. Any information shall be
provided orally within 24 hours from the time the permittee became aware of the
,circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances. The written submission shall contain a
description of the noncompliance, and its cause; the period of noncompliance, including
exact dates and times, and if the noncompliance has no been corrected, the anticipated time
it is expected to continue; and steps taken or planned to reduce, eliminate, and prevent
reoccurrence of the noncompliance.
b. The follmvin shall be included as information which must be reported within 24 hours
under this paragraph:
(1) Any unanticipated bypass which exceeds any effluent limitation in the permit.
(2) Any upset which exceeds any effluent limitation in the permit.
(3) Violation of a maximum daily discharge limitation for any of the pollutants listed by the
Director in the permit to be reported within 24 hours.
c. The iDirector may waive the written report on a case -by -case basis for reports under
paragraph b. above of this condition if the oral report has been received within 24 hours.
7.
The permittee shall report all instances of noncompliance not reported under Part H. E. 5 and 6.
of this permit at the time monitoring reports are submitted. The reports shall contain the
information listed in Part II. E. 6. of this permit.

0 Part II
Page 14 of 14
8. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in a permit
application, or submitted incorrect information in a permit application or in any report to the
Director, it shall promptly submit such facts or information.
9. Noncompliance Notification
The permittee shall report by telephone to either the central office or the appropriate regional
office of the Division as soon as possible, but in no case more than 24 hours or on the next
working day following the occurrence or first knowledge of the occurrence of any of the
Mowing:
a. Any occurrence at the water pollution control facility which results in the discharge of
significant amounts of wastes which are abnormal in quantity or characteristic, such as the
dumping of the contents of a sludge digester; the known passage of a slug of hazardous
substance through the facility; or any other unusual circumstances. .
b.. Any process unit failure, due to known or unknown, reasons, that render the facility
incapable of adequate wastewater treatment such as mechanical or electrical failures of
pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass
directly to receiving waters without treatment of all or any portion of the influent to such
station or facility.
Persons reporting, such occurrences by telephone shall also file a written report in letter form
«ithin 5 days following first knowledge of the occurrence.
10. Availability o�ports
Except -for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of
the Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be
available for public inspection at the offices of the Division of Environmental Management. As
required by the Act, effluent data'shall not be -considered confidential. Knowingly making any
false statement on any such report may result in the imposition of criminal penalties as provided
for in ?CGS 143-215.1(b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who. knowingly makes any false statement,
representation, or certification in any record or other document submitted or required to be
maintained under this permit; including monitoring reports or reports of compliance or
noncompliance shall, upon conviction, be punished by a fine. of not more than 510,000 per
violation, or by -imprisonment for not more than two years per violation, or by both.

PART III
OTHER REQUIREMENTS
1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs
from industries using the municipal system may be present in the permittee's discharge. At
such time as sufficient information becomes available to establish limitations for such
pollutants, this permit may be revised to specify effluent limitations for
any or all of such other pollutants in accordance with best practicable technology or water
quality standards.
2. Under no circumstances shall the permittee allow introduction of the following wastes in
the waste treatment system:
a.. Pollutants which create a fire or explosion hazard in the POTW, including, but not
limited to, wastestreams with a closed cup flashpoint of less than 140 Degrees
Fahrenheit or 60 degrees centigrade using the test methods specified in ATSM
standards D-93-79, D-93-80, or D-3278 (incorporated by reference, see 40 CFR
260.11). This prohibition does not apply to any aqueous solution containing less than
24 percent alcohol by volume which would otherwise be a hazardous waste under 40
CFR 261.21 by virtue of having a closed cup flashpoint of less than 140 degrees
Fahrenheit or 60 degrees centigrade;
b. Wastes which will cause corrosive structural damage to treatment works, and in no
discharges with pH less than 5.0 standard units unless the system is specifically
designed to accommodate such discharges;
c. Solid or viscous substances in amounts which cause obstructions to the flow in sewers
or interference with the proper operation of the treatment works;
d. Wastewaters at a flow rate and/or pollutant concentration which will cause an
inhibition or disruption of the POTW, its treatment processes, operation, or sludge
use and disposal;
e. Heat in amounts which will inhibit biological activity in the treatment works, resulting
in interference but in no case heat in such quantities that the temperature at the treatment
works influent exceeds 40°C (104°F) unless the works are designed to
accommodate such heat;
f. Petroleum oil, nonbiodegradable cutting oil, or products of mineral oil origin in
amounts that will cause interference or pass through;
g. Pollutants which result in the presence of toxic gases, vapors, or fumes within the
POTW in quantity that may cause acute worker health and safety problems;
h. Any trucked or hauled pollutants, except at discharge points designated by the POTW.
3. With regard to the effluent requirements listed in Part I of this permit, it may be necessary
for the permittee to supplement the requirements of the Federal Pretreatment Standards (40
CFR, Part 403) to ensure compliance by the permittee with all applicable effluent
limitations. Such actions by the permittee may be necessary regarding some or all of the
industries discharging to the municipal system.

Part III
4. The permittee shall require any industrial discharges into the permitted system to meet
Federal Pretreatment Standards promulgated in response to Section 307(b) of the Act.
Prior to accepting wastewater from any significant industrial user, the permittee shall either
develop and submit to the Division a Pretreatment Program for approval per 15 NCAC 2H
.0907(a) or modify an existing Pretreatment Program per 15 NCAC 2H .0907(b).
5. This permit shall be modified, or alternatively, revoked and reissued, to incorporate or
modify an approved POTW Pretreatment Program or to include a compliance schedule for
the development of a POTW Pretreatment Program as required under Section 402(b)(8) of
the. Clean Water Act and implementing regulations or by the requirements of the approved
State pretreatment program, as appropriate.
No construction of wastewater treatment facilities or additions to add to the planfs treatment
capacity or to change the type of process utilized at the treatment plant shall be begun until Final
Plans and Specifications have been submitted to the Division of Environmental Management
and written approval and Authorization to Construct has been issued.
C." Groundwater Monitoring
The permittee shall, upon written notice from the Director of the Division of Environmental
Management, conduct groundwater monitoring as may be required to determine the compliance
of this NPDES permitted facility with the current groundwater standards.
All POTWs must provide adequate notice to the Director of the following:
1. Any new introduction of pollutants into the POTW from an indirect discharger which
would be subject to section 30.1 or 306 of CWA if it were directly discharging those
pollutants; and
2. Any substantial change in the volume or character of pollutants being introduced into that
POTW by a source introducing pollutants into the POTW at the time of issuance of the
permit.
3. For purposes of this paragraph, adequate notice shall include information on (1) the quality
and quantity of effluent introduced into the POTW, and (2) any anticipated impact of the
change on the quantity or quality of effluent to be discharged from the POTW.

i Part III �� Permit I.NC0006009
E. The permittee shall not use any biocides except those approved in conjunction with the permit
application. The permittee shall notify the Director in writing not later than ninety. (90) days prior
to instituting use of any additional biocide used in cooling systems which may be toxic to aquatic
life other than those previously reported to the Division of Environmental Management. Such
notification shall include completion of Biocide Worksheet Form 101 and a map locating the
discharge point and receiving stream.
A
l

PART IV
ANNUAL ADMINISTERING AND COMPLIANCE MONITORING FEE REQUIREMENTS.
A. The permitted must pay the annual administering and compliance monitoring fee within 30
(thirty) days after being billed by the Division. Failure- to pay the fee in a timely manner in
accordance with 15A NCAC 2H .0105(b)(4) may cause this Division to initiate action to
revoke the permit.

State of North I
Department of
and Natural Re
Division of Water
Michael F. Easley, Governor
William G. Ross Jr., Secretary
Gregory J. Thorpe, Ph.D., Acting Director
j October 15, 2001
Edwin W. Horton, Director of Engineering
Galey & Lord Industries
P.O. Box'35528
Greensboro, NC 27425-0528
Subject: Rescission of NPDES Wastewater Permit
Galey & Lord Industries — Caroleen Plant
NPDES Permit No. NC0006009
Rutherford County
Dear Mr. Horton:
14
1 • FA
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
I-o_
_ OCT 2 5 2001 j
Regarding your request for rescission of the subject wastewater permit, staff of the
Asheville Regional Office has confirmed that this permit is no longer required. Therefore, in
accordance with your request, individual NPDES wastewater permit number NC0006009 is
rescinded, effective immediately.
If in the future you wish to again discharge wastewater to the State's surface waters, you
must first apply for and receive a new NPDES Permit: Operating a facility without a valid
NPDES Permit will subject the responsible party to a civil penalty of up to-$10,000 per day.
If it would be helpful to discuss this -matter further, I would suggest that you Roger
Edwards of the Asheville Regional Office at 828-251-6208 or Rob Lang of our Central Office
at 919-733-5083, extension 361.
Sincer ,
Gregory J. Thorpe, Ph.D., Actin irector
Division of Water Quality
cc: Asheville Regional Oice--
Point Source Compliance/Enforcement Unit — Rob Lang
NPDES Unit
Technical Assistance and Certification Unit
DWQ Budget Office - Fran McPherson
Central Files
EPA - Roosevelt Childress
1617 Mail Service Center, Raleigh, NC 27699-1617 Telephone [phone] Fax [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/10% post -consumer paper

-Caroleen WTP
Subject: Caroleen WTP
Date: Wed, 7 Nov 2001 15:43:53 -0500
From: Ed Horton <[e-mail]>
To: "Roger Edwards (E-mail)" <[e-mail]>
CC: Billy Faulk <[e-mail]>, Lee Landreth <[e-mail]>
Thanks for taking the time to meet at the Caroleen Plant and review the alternatives for dealing with the strorm water
infiltration into the sanitary waste system. We will proceed with the following actions as agreed to in our meeting.
1. Cut a ten foot section out of the 12 inch sewer main near where the line comes out of the ground.
2. Fill both the septic tank and the the pump well with sand leaving the lift pumps in place.
These actions will complete all .requirements related to the closure of the waste treatment plant.
If you have questions or need more information call me at 336-665-3091.
Thanks,
Ed
1 of 1 11/7/2001 4:04 PM

Re: NC0006009 - Galey & Lord (Caroleen)
Subject: Re: NC0006009 - Galey & Lord (Caroleen)
Date: Mon, 15 Oct 2001 12:29:39 -0400
From: Rob Lang <[e-mail]>
Organization: N.C. Division of Water Quality, Point Source Compliance/Enforcement Unit
To: Roger Edwards <[e-mail]>
Thanks, Roger. I'll rescind away.....
Roger Edwards wrote:
> Rob,
> I did not get by Galey & Lord-Caroleen Plant to check the septic tank. However,
> I had a phone conversation with Edwin Horton, Director of Engineering stating
> septic tank had been pumped so no discharge can occur. So proceed with the
> rescission of the NPDES Permit. I will make a visual observation as soon as I
> can.
> Thanks,
> R. Edwards
> Rob Lang wrote:
> > Roger,
> > Did you have a chance to verify the status of this discharger? I'll proceed
> > with the permit rescission if you give it the green light. Thanks...
> > Rob
> > Roger Edwards wrote:
> > > The industry is closed. I inspected the facility August 30, 2001. I Will
> > > check the septic tank this week to see if it was pump down to prevent a
> > > discharge. Will e-mail you with my findings.
> > > R. Edwards
> > > Charles Weaver wrote:
> > > > Roger - we got a letter today from this permittee sayin the plant would
> > > > be shut down and all wastewater discharge would cease by 9127101.
> > > > Have you heard about this?
> > > > If so, is.it.true? We'd be happy to rescind their permit.
> > > > Let me (or Rob Lang) know when you can.
> > > > Thanks,
> > > > CHW
> > > Roger Edwards - [e-mail]
> > > North Carolina Dept. of Environment and Natural Resources
> > > Asheville Regional Office
> > > Division of Water Quality - Water Quality Section
> > > 59 Woodfin Place
> > > Asheville, NC 28801
> > > Tel: [phone]
> > > Fax: [phone]
1 of 10/15/2001 12:43 PM

Re: NC0006009 - Galey & Lord (Caroleen)
Subject: Re: NC0006009 - Galey & Lord (Caroleen)
Date: Mon, 01 Oct 2001 15:15:31 -0400
From: Roger Edwards <[e-mail]>
Organization: NC DENR - Asheville Regional Office
To: Charles Weaver <[e-mail]>
CC: Rob Lang <[e-mail]>
The industry is closed. I inspected the facility August 30, 2001. I will
check the septic tank this week to see if it was pump down to prevent a
discharge. Will e-mail you with my findings.
'R. Edwards
Charles Weaver wrote:
> Roger - we got a letter today from this permittee sayin the plant would
> be shut down and all wastewater discharge would cease by 9127101.
> Have you heard about this?
> If so, is it true? We'd be happy to rescind their permit.
> Let me (or Rob Lang) know when you can.
> Thanks,
> CHW
Roger Edwards - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
59 Woodfin Place
Asheville, NC 26801
Tel: [phone]
Fax: [phone]
Roger Edwards <[e-mail]>
NC DENR - Asheville Regional Office
Division of Water Quality - Water Quality Section
I of 1 10/1/2001 3:19 PM

NC0006009 - Galey & Lord (Caroleen)
Subject: NC0006009 - Galey & Lord (Caroleen)
Date: Mon, 01 Oct 2001 14:46:45 -0400
From: Charles Weaver <[e-mail]>
To: Roger Edwards <[e-mail]>
CC: Rob Lang <Rob. ,[e-mail]>
Roger - we got a letter today from this permittee sayin the plant would
be shut down and all wastewater discharge would cease by 9/27/01.
Have you heard about this?
If so, is it true? We'd be happy to rescind their permit.
Let me (or Rob Lang) know when you can.
Thanks,
CHW
1 of 1 10/1/2001 3:16 PM

W A7 Michaelel
\p�pF FRQG v
Governor
William G. Ross, Jr., Secretary
North Carolina Department of Environment.and Natural Resources
> Gregory J. Thorpe, Ph.D.
O Y Acting Director
Division of Water Quality
Asheville Regional Office
WATER QUALITY SECTION
September 11, 2001
Mr. Edwin W. Horton .
Galey and Lord Industries
Post Office Box 158
Caroleen, North Carolina 28109
Subject: Compliance Evaluation Inspection
Status: In Compliance
NPDES Permit Number NC0006009
QGaley and Lord
Garoleen Plant.WWTP .
Rutherford County
Dear Mr. Horton:
The Division of Water Quality conducted the above referenced inspection on August 30,
2001. The monthly discharge monitoring reports were reviewed for July 2000 through June 2001,
indicate no monitoring violations.
The sand filter must have all vegetation removed and the sand should be raked smooth.
The distribution laterals appear to have a build up of material in the discharge holes. This
material should be removed to allow even flow to the sand filter.
It is understood the manufacturing plant will cease operation within the next few weeks.
The wastewater treatment facility should be pumped down to prevent discharge after closing.
The Company will need to request the National Pollutant Discharge Elimination System (NPDES)
Permit be rescinded or placed on an inactive status.
If you or your staff have questions regarding this report or if I may be of assistance, please
contact me at 828-251-6208.
Sincerely,
Roger C. Edwards
Wastewater Consultant
Enclosure
cc: Mr. William McKinney, ORC
-D
Water Quality Section, 59 Woodfin Place, Asheville, NC 28801-2414 Telephone: [phone] Customer Service
Fax: [phone] 623-7748

NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
NPDES Compliance Inspection Report
Section A: National Data System Coding
I
Transaction Code NPDES YR/MO/DAY Inspection Type Inspector Facility
Type
N 5 NC0006009 01/09/11 S S 2
Section B: Facility Data
Name and Location of Facility Inspected
Entry Time:
Permit Effective:
Galey Et Lord Industries -Car Ioteen Plant
Highway 221 Alt.
Exit Time/
Permit Expiration:
P.O. Box 158
Caroteen, North Carolina 28109
Name(s) of On -Site Representative(s) Title(s) Phone No(s)
William McKinney I ORC 828-657-6376
Name, Address of Responsible Official
Title
Edwin W. Horton i
Director of Corporate Engineering
Phone No.
Contacted?
P.O. Box 35528
Greensboro, North Carolinas 27425
336-379-2884
No
Section C: Areas
Evaluated During Inspection (S - Satisfactory, M - Marginal, U - Unsatisfactory.,. N - Not -Evaluated)
S Permit S
Flow Measurement N Pretreatment M Operations Et Maintenance
S Records/Reports N
Laboratory S Compliance Schedules S Sludge Disposal
M Facility Site Review S
Effluent/Receiving Waters S Self -Monitoring Program Other:
Section!
D: Summa : of; .Findin s/Comments/Com pliance Status Attach additional sheets if necessary)
No monitoring violations for the review period of July 2000 through June 2001.
The sand filter must have all vegetation removed and the sand raked smooth.
The distribution laterals should have material removed from the discharge holes.
The National Pollutant Discharge Elimination System (NPDES) Permit should be rescinded or placed on inactive statues when the manufacturing plant ceases
operation.
i
Compliance Status: X
Compliance
Name(s) and Signatur of Inspectors
Agency/Office/Telephone
Date
RogerC. Edwards I� , ,�_
NC-DWQ/ARO/828-251-6208
Signature of Revie
Agency/Office/Telephone
Date
) 0
NC-DWQ/ARO/828-251-6208
Z'
I N

State of North Carolina
Department of Environment
and Natural Resources
Asheville Regional Office
James B. Hunt, Jr., Governor
Bill Holman, Secretary
Kerr T. Sevens, Director WATER QUALITY SECTION
Division of Water Quality
October 12, 2000
Mr. Edwin W. Horton
Galey and Lord Industries
Post Office Box 158
Caroleen, North Carolina 28109
a
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Subject,: Compliance Sampling Inspection
Status: In Compliance
NPDES Permit Number NC0006009
Galey and Lord
Caroleen Plant WWTP
Rutherford County
Dear Mr. Horton:
The Division of Water Quality conducted the above referenced
inspection on September 28, 2000'. National Pollutant Discharge
Elimination System (NPDES) Permit effluent samples were collected by
the inspector during the inspection. The attached report contains
National Pollutant Discharge Elimination System (NPDES) Permit limited
parameters and sample results for those parameters. The facility is
operating within the limits established in the NPDES Permit.
The monthly Discharge Monitoring reports reviewed from September
1999 through August 2000, indicate no monitoring violations. The
discharge monitoring report data were compared to contract laboratory
reported data and no transcription errors were found'. The time and
assistance of Mr. -William McKinney, during the inspection was
appreciated.
If you or your staff have questions regarding this report or if I
may be of assistance, please contact me at 828-251-6208.
Sincerely,
ogeVC . Edwards
Wastewater Consultant
Enclosure
CC: Mr. William McKinney, ORC

United States Environmental Protection Agency
Form Approved
Washington, D.C. 20460
OMB
No. 2040-0003
EPA . NP®ES Compliance Inspection Report
Approval Expires 7-31-85
Section A: National Data System Coding
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type
1 IN 1 2 u j 3 NC0006009 11 12 00/09/28 17 18 IS
19 IS 1 u 2012
Remarks -
IIIIIIIIIII�IIIIIIIIIIIIIIIIIIIlllllll•IIIIIIIIII
' Reserved Facility Evaluation Rating BI QA
Reserved 66
67 lU 69 i 70 3 71 I I 72 I I 73 I I J 74
�J
75 80
Secti�onJB: FacilityLDatfe
Jame and Location of Facility Inspected
Entry Time
Permit Effective Date
laley and Lord Industries
11:55 AM
Dec. 1, 1998
'. O. Box 35528
Exit Time/Date
Permit Expiration Date
Greensboro, NC 27425
12:45 PM
July 31, 2003
slame(s) of On -Site Representative(s)/Title(s)
Phone No(s)
vir. William McKinney, ORC I
828-657-6376
Jame, Address of Responsible Official
Title
v1r. Edwin W. Horton
Director of Corporate Engineering
8 O '. Box 3552
1.
Phone No.___—F
Contacted
sboro, 27425, i
336-379-2884
No
section C: Areas Evaluated During Inspection CODES S - Satisfactory M - Marginal U - Unsatisfactory
N - Not evaluated/Not applicable
$
Permit I
i
Records/Reports
Facility Site Review
$
Flow Measurement
Laboratory
Effluent/Receiving Waters
N
Pretreatment
Compliance Schedules
Self -Monitoring Program
$
Operations &Maintenance
Sludge Disposal
Other: row 15
$
$
$
$
$
$
$
Section D: Summary of Findings/Comments (Attach additional sheets if necessary)
acility is operating in accordance with NPDES Permit limits. NPDES• Permit limits and sample results are listed below.
ffluent Characteristics Monthly Average Sample Results
'SOD 30.0 mg/I < 2 mg/I
'otal Suspended Solids 30.0 mg/I < 2.5 mg/I
ecal Coliform 200/100 ml <2/100 ml
ammonia Nitrogen No limit < 0.1 mg/I
lame(s) and Signature(s) of Inspecto�(s)
Agency/Office/Telephone
Date
.OGER C. EDWARDS
/�
DWQ/ARC) 828-251-6208
/ L . -- i Ct:Y
Q 2 0�3
ignatfire,o Reviewer ' ' _
Agency/Office
Da
DWQ/ARC) 828-251-6208
Regulatory Office Use Only
i
,ction Taken
Date
Compliance Status
EI �Noncompliance
P- Compliance

— - - ---• . -IV 1nvivt•I11114 I R,L MANAGEMENT WATER QUALITY FIELD -LAB FORM 1-11 For Lab Use ONLY
COUNTY1A
PRIORITY SAMPLE TYPE
RIVER BASIN 2 J{D
Rnrvxl TO- PRO MRO RRO WaRO WIRO WSRO TS El ❑ QA ❑ STREAM EFFLUENT
AT BM
Other ❑COMPLIANCE ❑ CHAIN ❑ LAKE INFLUENT
Shipped by: Bus Courie , taff thOF CUSTODYer EMERGENCY ❑ESTUARY
COLLECTOR(S): CLtJ I S
Lab Number:
Date Recalved:
- '' ( 1 Tfine-
Rec,d by:
From: Bus- Couri9t-Nand De
DATA ENTRY BY:
`•+—^ CK. �,{r
DATE REPORTED:
Estimated BOD Range. 0-5 -2)25-65/40-130 or1000 plus STATION LOCATION: VA
Seed: Yes Ly' Na [] Chlorinated: Yes R No ❑ REMARKS:
Statian Date Begin (yy/mm/dd) Ttme Begin Date End
t' Time End Depth DM b8 DBM Value Type Composite Sample Tyre
() Z l S A H L T S BI C f GJ GNXX
2
1
to,ODS
310 C, 'I mg/I
2
COD High 340 mg/I
3
COD Low 335 m9/1
4
olfform: MF Fecal 31616 /100m1
5
Conform: MF Total 31504 /100mI
6
Conform: Tube Fecal 31615 /100011
7
Collform: Fecal Strep 31673 /100m1
g
Residue: Total 500 mg/1
9
Volatile 505 mg/l
10
Fixed 510 mg/I
11
esidue: Suspended 530 C mg/l
• �._
12
Volatile 535 mg/1
13
Fixed 540 mg/I
14
PH 403 units
15
Acidity to pH 4.5.436 mg/I
16
Acidity to pH 8.3 435 mg/l
17
Alkalinity to pH 8.3 415 mg/l
18
Alkalinity to pH 4.5 430 mg/1
1.9
TOC 680 mg/1
i0
Turbldity 76 NTU
Chloride 940 mg/I
Chi a: Tri 32217 ug/I
Chi a: Corr 32209 ug/I
Pheophytin a 32213 ug/1
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color: pH 7.6 82 ADMr
Cyanide 720 mg/I
Fluoride 951 mg/l
Formaldehyde 71880 mg/l
Grease and Oils 556 mg/1
Hardness Tota1900 mg/i
Specific Cond. 95
uMh
MBAS 38260 mg/I
mg/I
Phenols '32730 ug/I
Sulfate 945 mgA
Sulflde 745 mg/I
PoInEX (Conductance at 25 C stet Temperature D.O, mg/1
94
Salinity AS
480
10 1300 (.
Precfpition (Wday) Cloud Cover E
H3 as N 610
TKN as N 625 mg/I
NO2 plus NO3 as N 630 mg/i
P: Total as P 665 mg/1
PO4 as P 70507 In
P: Dissolved as P 666 mg/1
Cd-Cadmium 1027 ug/I
Cr-Chiomium:Totai 1034 awl
CuCopper.1042 ug/1
NI -Nickel 1067 ug/I
Pb-Lead 1051 ug/I
Zn-Zinc 1092 ugA
Ag-Sllver 1077 ug/i
AI -Aluminum 1105 ug/I
Be-Beryllfum 1012 ug/I
Ca-Calefum 916 mg/I
Co -Cobalt 1037 ug/I
Fe -Iron 1045 ug/I
PH
Alkalinity
Pif 8.3 pH 4.5
36
is 132244
Direction (beg) Stream Flow Severity
rrr
Li-Lfthium 1132 ug/1
Mg-Magnesiam 927 mg)
Mn-Manganese 1055 ug/;
No -Sodium 929 mg/
Arsenfc:Total 1002 ug/l
Se -Selenium 1147 ug/1
Hg-Mercury 71900 ug/1
Organochlorine Pesticides
Omnnophospiwrus Pesticides
Actd Hmbicfdes
Base/ Neutral Extractable Organics
Acfd Extractable Organics
Purges Pie Organics (VOA bottle reg•d►
PhyEoplanktdW I' L S
Acidity
PH 4,5 pH
Severity I Wind Velocity M/H
—•r- I c, l' I- ; —,,Z, 0 F e . i-,z c k
Stream Depth ftj Stream Width ft.
DMl/Revised 10/86 '

GKEX78/MY
10/04/2000
COMPLIANCE EVALUATION
ANALYSIS
REPORT
PERMIT--NC0006009
PIPE--001
REPORT PERIOD:
9909 -0008 LOC --- E
FACILITY--GALEY
&
LORD IND-CAROLEEN
DESIGN FLOW--.
.0180 CLASS--1
LOCATION--CAROLEEN
REGION/COUNTY--01
RUTHERFORD
50050
003.10
00530
00610
31616
50060
MONTH
Q/MGD
BOD
RES/TSS NH3+NH4-
FEC COLI
CHLORINE
99/09
.0060
20.30
1.0
.00
1.0
.009
99/10
.0052
1.20
.2.0
.00
1.0
.000
99/11
.0060
.00
.5
.00
1.0
.000
99/12
.0060
.00
.0
.00
1.0
.005
00/01
.0069
.00
A.
.00
1.0
.000
00/02
.0070
.00
.0
.42
1.0
.007
00/03
.0075
.00
.0
.14
1.0
.023
00/04
.0082
1.20
.0
3.70
1.0
.011
00/05
.0066
.00
.0
.00
1.4
.025
00/06
.0082
.00
0
.00
1.0
.020
00/07
.0090
.00
.0
.24
1.0
.000
00/08
.0090.
4.00
.0
.00
1.0
.001
AVERAGE
0071
2.22
.2
.37
1.0
.008
MAXIMUM
.0090
20.30
2.0
3.70
1.4
.025
MINIMUM
.0052
.00
.0
.00
1.0
.000
UNIT
MGD
MG/L
MG/L
MG/L
##/100ML
MG/L

& Lord-Caroleen
Subject: Galey & Lord-Caroleen
Date: Mon, 22 Oct 2001 13:29:31 -0400
From: Roger Edwards <[e-mail]>
Organization: NC DENR - Asheville Regional Office
To: Ed Horton <[e-mail]>
CC: Billy Faulk <[e-mail]>
Mr. Horton,
In regard to our discussion of stormwater at the Caroleen Plant ste
there is no exposure to any product, raw, intermediate, or final nor is
there any activity at the facility, therefore no permitted stormwater.
Please, let me know when all wastewater tankage is filled with
sand/soil.
If I can be of assistance, contact me at 828-251-620.8.
R. Edwards
Roger Edwards - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
59 Woodfin Place
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Roger Edwards <[e-mail]>
NC DENR - Asheville Regional Office
Division of Water Quality - Water Quality Section
of 1 10/23/2001 7:43 AM

Re: Galey & Lord Caroleen Plant
Subject: Re: Galey & Lord Caroleen Plant
Date: Tue, 27 Nov 2001 12:25:13 -0500
From: Roger Edwards <[e-mail]>
Organization: NC DENR - Asheville Regional Office
To: Robert Farmer <[e-mail]>
Robert,
Rescind the NCG permit for the Galey & Lord Caroleen Plant.
closed.
Thanks,
R. Edwards
Robert Farmer wrote:
The plant is
> I just got their request. If you want to, you can just send me another
> E-mail, with your recommendation to rescind, and I'll do it.
> thanks
> Robert
> Roger Edwards wrote:
> > Robert,
> > I am faxing you the request for rescission of NCG170175 for the above
> > referenced facility. I have made a site inspection and the facility is
> > closed. If you have any questions let me know.
> > Thanks,
> > R. Edwards
> > Roger Edwards - [e-mail]
> > North Carolina Dept. of Environment and Natural Resources
> > Asheville Regional Office
> > Division of Water Quality - Water Quality Section
> > 59 Woodfin Place
> > Asheville, NC 28801
> > Tel: [phone]
> > Fax: [phone]
Roger Edwards - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
59 Woodfin Place
Asheville, NC 28801
Tel: [phone]
Fax: [phone]
Roger Edwards <[e-mail]>
NC DENR - Asheville Regional Office
Division of Water Quality - Water Quality Section
1 of2 11/27/2001 12:31 PM

CVd1g&1Or4 ' P.O. Box 35528 Greensboro, North Carolina 27425-0528 Tel. [phone]
November 12, 2001
Roger Edwards
NCDENR _
Water Quality Section
59 Woodfin Place
Asheville, IV. C. 28801-2414
NOr a 9 �101
RE: Galey & Lord Industries, Inc.ER
Caroleen Plant, Rutherford County #c'fiI L REGIONAL,'! ;(.'F
Storm Water Permit #NCG170175
Dear Mr. Edwards:
We discussed the need for a storm water permit at the Caroleen Plant and agreed that one was not
needed. This is a formal request to have the Permit #NCG170175 terminated. Let me know if I
need to take other action.
Thanks for your continuing assistance.
If you have questions or need more information please contact me at 336-665-3091.
Sincerely,
GALEY & LORD INDUSTRIES, INC.
Edwin W. Horton
Director of Engineering
Post -it® Fax Note 7671
Date/1 2-7 l
paogesI. r
To AP-
From -__
Co./Dept.
Co. n 2^V
Phone #
PhoneeR"' —ZSI—G't-n�
Fax #
Fax #
AMERICA'S TEXTILE
ENC
O RAGI G
EXCRELLENTCE -

State of North Carolina
Department of Environment LT?WA
and Natural Resources 4 a
Division of Water Quality �YV;
Michael F. Easley, Governor William G. Ross Jr., SecretaryNCDENR
Gregory J. Thorpe, Ph.D.,Acting Director NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
November 30, 2001
Edwin W Horton
Galey & Lord Indust/Caroleen
PO Box 35528
Greensboro NC 27425
Subject: Rescission of NPDES Permit
Permit No. NCG170175
Galey & Lord Indust/Caroleen
Rutherford County
Dear Edwin Horton:
Reference is made to your request for rescission of the subject NPDES Permit.
Staff of the Asheville Regional Office have confirmed that this Permit is no longer
required: Therefore, in "accordance with your request, NPDES Permit No. NCG170175
is rescinded, effective immediately.
If in the future you wish to again discharge stormwater to the State's surface waters,
you must first apply for and receive a new NPDES Permit. Operating a facility without
a valid NPDES Permit will subject the responsible party to a civil penalty of up to
$10,000 per day.
If it would be helpful to discuss this matter further, I would suggest that you contact
the Water Quality staff, Asheville Regional Office at [phone].
Sincer ,
Gregory J.-Thorpe, Ph.D.
cc: Rutherford County Health Department
�Ashev Ile=Water Quality Regional Sup ervisor:_w/attachments
Point Source Bfancii = Bradley -Bennett'-" -
Operator Training and Certification
Point Source Compliance - Robert Farmer - w/attachments
Mr. Roosevelt Childress, EPA
Central Files - w/attachments
Fran McPherson, DWQ Budget Office
1617 Mail Service Center, Raleigh, North -Carolina 27699-1617 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

%j,ucy m i.uru t.aroieen riant
Subject: Galey & Lord Caroleen Plant
Date: Tue, 27 .Nov 2001 09:09:15 -0500
From: Roper Edwards <[e-mail]>
Organization: NC DENR - Asheville Regional Office
To: Ropert Farmer <[e-mail]>, Ed Horton <[e-mail]>
Robert,
I am faxing you
referenced facil
closed. If you
Thanks,
R. Edwards
Roger Edwards -
North Carolina I
Asheville lje clot
Division of- XWate
59 Woodfin Plac(
Asheville, NC 2£
Tel: [phone](
Fax: [phone]
Roger Edwards
NC DENR - Ashei
Division of Water
REMOVE OPTION
'ERSONAL DATA FACIL
FACILITY NAME> GAL
ADDRESS:
STREET: P.O. BOX
CITY: GREENSBOR
TELEPHONE 336 665
STATE CONTACT> EVA
1=PROPOSED,2=EXIST
LAT: 3516490 LONG
ATE APP RCVD
ATE STAFF REP REQS
ATE STAFF REP RCVD
SATE TO P NOTICE
SATE OT AG COM REQS
SATE OT AG COM RCVD
ATE TO EPA
)ATE FROM EPA
'EE CODE ( 0 ) 1=(>
'=(GP49,73)8=(GP76)
'OMMENTS:
[ESSAGE: *** DATA
the request for rescission of NCG170175 for the above
ity. I have made a site inspection and the facility is
have any questions let me know.
[e-mail]
ept;7;�6f Environment and Natural Resources
al -office
r Quality - Water Quality Section
801
8
2
e Regional Office
ality - Water Quality Section
NPDES FACILITY AND PERMIT DATA 11/29/01 09:02:33
TRXID 3NU KEY NCG170175
TTY APPLYING FOR PERMIT REGION
�Y & LORD INDUST/CAROLEE*** COUNTY> RUTHERFORD 01
ZAILING (REQUIRED) LOCATION (REQUIRED)
�5528 STREET: U.S. HIGHWAY 221-A
) ST NC ZIP 27425 CITY: CAROLEEN ST NC ZIP 28019
3091 DATE FEE PAID: 01/21/99 AMOUNT: 80.00
1S PERSON IN CHARGE EDWIN W. HORTON
3=CLOSED 1 1=MAJOR,2=MINOR 2 1=MUN,2=NON-MUN 2
08148000 N=NEW,M=MODIFICATION,R=REISSUE> R
01/21/99 WASTELOAD REQS
WASTELOAD RCVD
SCH TO ISSUE
DATE DRAFT PREPARED
DATE DENIED
DATE.RETURNED
I / DATE ISSUED 08/01/99 ASSIGN/CHANGE PERMIT
EXPIRATION DATE 07/31/04
_OMGD),2=(>1MGD).,3=(>O.lMGD),4=(<O.1MGD),5=SF,6=(GP25,64,79),
1=(GP13,34,30,52)0=(NOFEE) DIS/C 73 _ _ _ _ CONBILL ( _ )
ELETED SUCCESSFULLY ***

P.O. Box 35520 - Greensboro, North Carolina 2742MS28 Tei. (335) 565.3()63
November 12. 2001 '
R r Edwardi
N(DI7NR
Water Quality Section q.,n
r
59 Woodfin Place
A511OVille, N. C. 28801-241.4
R F. Galey & L,ord Industries, Inc.
Carolecri Plant, Rutherford County
Storm Water Permit #NCG1 70175
Dear Mr. Edwards:
We LIISCLIssed the. need, for a storm water permit at the Caroleen Plant and agreed that one was not
flctj,ded This is a formal request to have the Permit #NCG170175 terminated. Let me know if' I
need to take other action.
Thanks for your continuing assistance.
If ti1011 hilVe t[Liestions or need more information plessi contact me at 336-665-3091,
shicerely.
"iA11 Y & l.,ORD MMUSTRI.ES, INC.
-Edivin W Horton
Dircotor of I .nl;inet ring
cc: Billy Faulk -'Flint
Jack Garrison - B&O
PW4r Fax Npte
76571
06)
Toa
From
r )Afe
WDOM
co. Alzo
PhD" 0
Phnne.
g
- z 671 - LL2.JL_

.. r
NORTH = iOLINA DEPARTM T OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
ASHEVILLE REGIONAL OFFICE
WATER QUALITY SECTION
August 25, 1999
Mr. Edwin W. Horton
Galey and Lord Industries
Post Office Box 158
Caroleen, North Carolina 28109
Subject: Compliance Sampling Inspection
Status: In Compliance
Y6NPDES Permit Number NC0006009
Galey and Lord
Caroleen Plant WWTP
Rutherford County
Dear Mr. Horton:
The Division of Water Quality conducted the above
referenced inspection on August 10, 1999. Samples were
collected by the inspector during the inspection. The
attached report contains National Pollutant Discharge
Elimination System (NPDES) Permit limited parameters and
sample results for those parameters. The facility is
operating within the limits established in the NPDES Permit.
During the inspection I observed a small amount
vegetation growing on the sand filter, this should be
removed. A schedule should be established to prevent
vegetation growth on the sand filter. The replacement of
the top four inches of sand has not been accomplished. This
was noted in the last three (3) inspections, I recommend the
sand replacement be addressed as soon as possible. The
wastewater treatment is otherwise well operated and
maintained.
The monthly Discharge Monitoring reports reviewed from
July 1998 through June 1999, indicate no monitoring
violations. The time and assistance of Mr. William
McKinney, during the inspection was appreciated. If you or
your staff have questions regarding this report, or if I may
be of assistance, please contact me at 828-251-6208.
Sincerely,
R gC. Edwards
Wastewater Consultant
Enclosure
CC: Mr. William McKinney, ORC
INTERCHANGE BUILDING, 59 WOODFIN PLACE, ASHEVILLE, NC 28801-2414
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - SO% RECYCLED/10% POST -CONSUMER PAPER

r_1
NORTH CAROLINA D - TMENT OF ENVIRONMENT, HEALTH, AM NATURAL RESOURCES
NPDES Compliance Inspection Report
L... Section A:'National!D'ata.System•.coding
Transaction Code NPDES YR/MO/DAY Inspection Type Inspector Facility Type
N 5 NC0006009 99/08/10 S S I
Section 6- Facility- Data
Name and Location of Facility Inspected
Galey and Lord Industries, Inc.
Entry Time:
Permit Effective:
1:05 PM
P.O. Box 158
Caroleen, North Carolina 28109
Exit Time/Date:
Permit Expiration:
2:15 PM 08/10/99
Name(s) of On -Site Represe
tative(s) Title(s) Phone No(s)
William McKinney
ORC 828-657-6376
Name, Address of Responsible
Official
Title
Edwin W. Horton (same
as above)
Plant Manager
Phone No.
Contacted?
828-657-6376
NO
Seetrbtt QAreas.Evaluated
'During _Inspection 5- Satis actoryi.A: Marginal :'U -' Unsatis acfoty, N Not Evalttated)
...__-_.._:....
_
:....-_
S Permit S
.
Flow Measurement N/A Pretreatment S Operations & Maintenance
S Records/Reports N
Laboratory S Compliance Schedules S Sludge Disposal
S Facility Site Review S
Effluent/Receiving Waters S Self -Monitoring Program * Other:
$eci�on
-
D Summary of Fmdmgs/Comments/Compliance Status (Attach: addmonal sheets )f necessary) _:
_.. -
Facility is operating in accordance
_
with NPDES Permit limits. NPDES Permit limits and sample results are listed below.
Effluent Characteristics
Monthly Average Sample Results
BOD
30.0 mg/I < 2 mg/I
Total Suspended Solids
30.0 mg/I < 1.0 mg/I
I
Fecal Coliform
200/100 ml <2/100 ml
Ammonia Nitrogen
No limit < 0.1 mg/I
Compliance Status:
X Compliance * Deficiency * Non -Compliance
Name(s) and Signatur f,lnsp cto
1^
Agency/Office/Telephone
Date
Roger C. Edwards 04"�
-�
NC-DWQ/ARO/704-251-6208
08/24/99
Sig_�to� of R view
Agency/Office/Telephone
NC-DWQ/ARO/704-251-6208
Date
'U a
Iv

DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY FIELD -LAB FORM (DM1)
COUNTY 2,A
PRIORITY SAMPLE TYPE
0
RIVER BASIN
❑AMBIENT
❑
❑
REPORT TO• RO FROO MRO RRO WaRO W,RO WSRO TS
QA
STREAM
EFFLUENT
AT BM
❑
COMPLIANCE ❑ CHAIN
❑ LAKE
❑
Other
Other
INFLUENT
F— r nh rT� ANr v
Lab Number: 4- (c7 �14V
Date Received: O ( 19' I Time: 3 O
Rec'd- by: 5--- From: Bus-Courie -Hand De
DATA ENTRY BY: 15 CK:
DATE REPORTED:
Shipped by: Bus Co`uriiee left Other
OF CUSTODY
❑EMERGENCY
❑ESTUARY
COLLECTOR
�^�
Estimated BOD Range: 0-5
- 5 25-65/40-130 or 100 plus
STATION LOCATION: =
Seed: Yes l No ❑
Chlorinated: Yes �—"No ❑
REMARKS:
Station #
Date Begin (yy/mm/dd)
Time Begin
Date End
Time End
Depth DM DB DBM
Value Type
Composite
Sample Ty e
TM
9q
(33Z�
A H L
T S B
C GNXX
- 1
OD5 310 G mg/I
. `2
COD High 340 mg/I
3
COD Low 335 mg/I
4
'Coliform: MF Fecal 31616 G /100ml
5
Coliform: MF Total.31504 /100ml
6
Coliform: Tube Fecal 31615 /100ml
7
Coliform: Fecal Strep 31673 /loom,
g
Residue: Total 500 mg/I
C1
Volatile 505 mg/1
10
Fixed 510 mg/I
11
Residue: Suspended 530 G mg/I
12
Volatile 535 mg/I
13
Fixed 540 mg/I
14
pH 403 units
15
Acidity to pH 4.5 436 mg/I
l "16
17
Acidity to pH 8.3 435 mg/I
Alkalinity to pH 8.3 415 mgA
18
Alkalinity to pH 4.5 410 mg/I
19
TOC 680 mgA
on
Turbidity 76 NTU
Chloride 940 mg/I
Chi a: Tri 32217 ug/I
Chi a: Corr 32209 ug/I
Pheophytin a 32213 ug/I
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color: pH 7.6 82 ADMI
Cyanide 720 mg/1
Fluoride 951 mg/I
Formaldehyde 71880 mg/1
Grease and Oils 556 mgA
Hardness Total900 mg/I
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/I
Phenols 32730 ug/I
Sulfate 945 mgA
Sulfide 745 mg/1
H3 as N 610 G ©r mg/I
TKN as N 625 mg/I
NO2 plus NO3 as N 630 mgA
P: Total as P 665 - mg/I
PO4 as P 70507 mgA
P. Dissolved as P 666 mg/1
CdCadmium 1027 ug/I
Cr-Chromium:Total1034 ug/I
Cu-Copper 1042. ugA
Ni-Nickel 1067 ugA
Pb-Lead 1051 ugA
Zn-Zinc 1092 ug/I
Ag-Silver 1077 ugA
Al -Aluminum 1105 ug/I
Be -Beryllium 1012 ug/I
Ca -Calcium 916 mgA
-Co-Cobalt 1037 ug/I
Fe -Iron 1045 ug/I
Li -Lithium 1132 ug/I
Mg -Magnesium 927 mg/I
Mn-Manganese 1055 ug/I
Na-Sodium 929 mg/I
Arsenic -Total '1002 ug/I
Se -Selenium 1147 ug/I
Hg-Mercury 71900 ug/I
Organochlorine Pesticides
Organophosptwms Pesticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoplankton A�4 N<"\ `
Sampling Point %
Conductance at 25 C
Water Temperature
D.O. mg/1
pH
Alkalinity
83
Acidity
AirTeiiperrature (Ci d ,�
`�
pH pH 4.5
pH 4.5 pH 8.3 <
2
94
10
300 .
400 .
82244 431
'�
82243 82242
,20 /► �!
Salinity %
Precipition (In/day)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H[ean
Stream Depth.R
St`reeafiMath fL \rr
U� V`
480
45
32
36
1351
1350
35
4
4
J
N,
X
,/Revised 10/86

DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIELD -LAB FORM (DM1)
COUNTY �t_L L '� PRIORITY SAMPLE TYPE
'D 0
RIVER BASIN D ❑AMBIENT ❑ QA ❑ STREAM LET EFFLUENT
REPORT TO: O FROFRO MRO RHO WaRO WIRO WSRO TS
AT BM
Other ❑COMPLIANCE ❑ CHAIN ❑ LAKE ❑ INFLUENT
Other OF CUSTODY
F— r_wh n.o r%rar v
Lab Number: '�2 (7 a D'
Date Received: �� '�' �1 Y Time:
Rec'd by: From: Bus-Courigr-Hand DA
DATA ENTRY BY: cS" CK:
Shipped by: Bus Courrller, S�taf Other ❑ EMERGENCY ❑ ESTUARY DATE REPORTED:
COLLECTOR(S): L O' /� �Jj -
Estimated BOD Range: 0-5 -25 25-65/40-130 or 100 plus STATION LOCATION: ti 2b
Seed: Yea E;�' No ❑ Chlorinated: Yes ❑ No [D REMARKS:
Station)"
jDate�tnBegin (yy/mm/dd)
Time Begin
Date End
Time End
Depth DM DB DBM
Value Type
Composite
Sample Ty e
7 U 2
13 2
A H L
T S B
C 9 GNXX
_ 1
OD5 310
2
COD High 340 mg/1
3
COD Low 335 mg/I
4
llform: MF Fecal 31616 /100ml
5
-
Coliform: MF Total 31504 /100ml
6
Coliform: Tube Fecal 31615 /loom]
7
Col►form3 Fecal Strep 31673 /100ml
8
Residue: Total 500 mg/I
9
Volatile 505 mg/I
10
Fixed 510 mg/I
11
Residue: Suspended 530 , f mg/1
12
Volatile 535 mg/I
k
13
Fixed 540'1 mg/1
14
pH 403 A units
15
Acidity to pH 4.5 436. mg/1
16
Acidity to pH 8.3 435 mg/1
17
Alkalinity to pH 8.3 415 mg/l
18
Alkalinity to pH 4.5 410 mg/I
19
TOC 680 mg/1
20
Turbidity 76 NTU
Chloride 940 mg/1
Chi a: Tri 32217 ug/I
Chi a: Corr 32209 ug/I
Pheophytin a 32213 ug/I
Color: True 80 Pt -Co
Color:(pH ) 83 ADM[
Color: pH 7.6 82 ADMI
Cyanide 720 mg/1
Fluoride 951 mg/I
Formaldehyde 71880 mg/I
Grease and Oils 556 mg/1
Hardness Total900 mg/1
Specific Cond. 95 uMhos/cm2
MBAS 38260 '_ mg/I- '
Phenols 32730 ug/I
Sulfate 945 mg/I
Sulfide 745 mg/I
H3 as N 610 0 J mgA
r
TKN as N 625 mg/1
NO2 plus NO3 as N 630 mgA
P: Total as P 665 mg/I
PO4 as P 70507 mg/I
P: Dissolved as P 666 mg/I
CdCadmium 1027 ugA
Cr-Chromlum:Total1034 ugA
Cu-Copper 1042 ug/I
Ni-Nickel 1067 ug/I
Pb-Lead 1051 ug/I
Zn-Zinc 1092 ug/I
Ag-Silver 1077 ug/I
AI -Aluminum 1105 ug/I
Be -Beryllium 1012 ug/I
.Ca -Calcium 916 mgA
Co -Cobalt 1037 ug/I
Fe -Iron 1045 ug/I
Li -Lithium 1132 '. ug/I
Mg -Magnesium 927 mg/I
Mn-Manganese 1055 ug/I
Na-Sodium 929 mg/l
Arsenic:Total 1002 ug/I
Se -Selenium 1147 ug/I
Hg-Mercury 71900 ug/I
Organochlorine Pesticides
Organophosphorus Pesticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
BAyitop(� !O%ZJ U U LS Pi I S
nrrrAn
VER9024
Sampling Point %
Conductance at 25 C
Water Temperature (C)
D.O. mg/I
pH
Alkalinity
8.3 4.5
Air T`l
AaidiI � � �J
pH pH
p H4.5 HIV 1
2
94
10
300 0
400 •
82244 431
82243 8i 242 L_.c,__ 20___ f
Salinity %
Precip►tion On/day)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
can Stream-D`epth'k Sti 66 Width ft.
480
145
132
136
11351
1350
35
64 4
10/86

z NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
ASHEVILLE REGIONAL OFFICE
WATER QUALITY SECTION
December 18, 1998
Mr. Edwin W.-Horton
Galey and Lord Industries
P. O. Box 158
Caroleen, NC 28109
Subject: Compliance Sampling Inspection
Status: In Compliance
��'Galey
NPDES Permit Number NC0006009 and Lord WWTP
Caroleen Plant
Rutherford County
Dear Mr. Horton:
The Division of Water Quality conducted the above
referenced inspection on December 1, 1998. Samples were
collected by the inspector during the inspection. The
attached report contains National Pollutant. Discharge
Elimination System (NPDES) Permit limited parameters and
sample results for those parameters. The facility is
operating within the limits established in the NPDES Permit.
The repairs/improvements to the sand filter suggested
in the two.(2) previous inspection reports have been.
completed, with the exception of addition of graded sand to
the filter sand. I understand the sand has been ordered and
the sand will be added as soon as possible. The wastewater
treatment is well operated and maintained.
The monthly Discharge Monitoring reports reviewed from
November, 1997 through October 1998, indicate no monitoring
violations. The time and assistance of Mr. William McKinney,
during the inspection was appreciated. If you or your staff
have questions regarding this report, or if I may be of
assistance, please contact me at 828-251-6208.
Sincerely,
Roger C. Edwards
Wastewater Consultant
cc: Mr. Jake Wilson, Plant Engineer
Mr. William McKinney, ORC
INTERCHANGE BUILDING, 59 WOODFIN PLACE, ASHEVILLE, NC 28801-2414
PHONE [phone] FAX 828-2S1-6452
AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - SO% RECYCLED/10% POST=CONSUMER PAPER

United State:: -onmental Protection Agency
Form Approved
Vc`_,_:,_`gton, D.C. 20460
OMB No. 2040-0003
PA � NPDES
Compliance Inspection Report
Approval Expires 7-31-85
Section A: National Data System Coding
Transaction Code
NPDES yr/mo/day Inspection Type Inspector Far Type
1 IN J 2 u
3 NC0006009 11 12 98/12/01 17 18 IS 1 19 I I 20 u
I I I I I I
Remarks
I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I
2' ) Reserved Facility Evaluation
Rating BI QA Reserved 64
67 l__IU 69
,.
70 13 I 71 I I 72 I I 73 � 74 75 80
u
I Section B: Facility Date
NameName and Location of Facility Inspected
Entry Time
Permit Effective Date
Galey and Lord Industries
I
1:15 PM
Dec. 1, 1998
P. O. Box 35528
Exit Time/Date
Permit Expiration Date
Greensboro, NC 27425
i
2:00 PM
July 31, 2003
Name(s) of On -Site Rep resentative,(s)/fitle(s)
Phone No(s)
Mr. William McKinney, ORC
828-657-6376
Name, Address of Responsible Official
Title
Mr. Edwin W. Horton
I
Director of Corporate Engineering
P. O. Box 35528
Phone No.
Contacted
Greensboro, NC 27425
i
33 6-3 79-2884
No
Section C: Areas Evaluated During
Inspection CODES S - Satisfactory M - Marginal U - Unsatisfactory N - Not evaluated/Not applicable
S
Permit
Records/Reports
Facility Site Review
I
S
Flow Measurement
Laboratory
Effluent/Receiving Waters
N
Pretreatment
Compliance Schedules
Self -Monitoring Program
S
Operations &Maintenance
Sludge Disposal
Other: row 15
S
S
S
S
S
S
S
Section D: Summary of Findings/Comments (Attach additional sheets if necessary)
Facility is operating in accordance
with NPDES Permit limits. NPDES Permit limits and sample results are listed below.
Effluent Characteristics lI
Monthly Average. Sample Results
BOD
30.0 mg/I. < 2 mg/I
f
Total Suspended Solids I
30.0 me < 1.0 mg/I
Fecal Coliform
200/100 ml <2/100 ml
Ammonia Nitrogen
No limit 0.1 mg/I
Name(s) and Signature(s) of Inspictor(s)
Agency/Office/Telephone
Date
ROGER C. EDWARDS
�-
DWQ/ARO 828-251-6208
/z / 9
Signa r eviewer
Agency/Office
Dat
DWQ/ARO 828-251-6208
/
Regulatory Office Use Only
Action Taken
Date
Compliance Status
Noncompliance
Compliance

NPDES PERMIT APPLICATION - SHORT FORM C
To be filed only by persons engaged in manufacturing and mining a
N. C. Department of Environment and Natural Resources JUN 12 i99�
Division of Water Quality / NPDES Unit
P. O. Box 29535, Raleigh, NC 27626-0535 y r
Please print or type
1. Applicant and facility producing discharge
A. Name Galey & Lord Industries, Inc. — Caroleen Plant
B . Mailing address of applicant:
1. Street address P.0. Box 158
2. City Caroleen 3.
County Rutherford
4. State NC 5..
Zip Code 28019
C- Location of facility:
1. Street U.S. Highway 221 A
2. City Caroleeri 3.
CountyRutherford
4. State NC 5.
Zip Code 28019
D. Telephone Number (704 ) 657-6376 X244
E. Fax Number (704 ) (57-F,uh
x24n
2. Standard Industrial Classification (SIC) code(s): 2281
3. Number of employees: 175
4. Principal product(s) produced: Yarn
Principal raw material(s) consumed: Cotton & gynthetic fiber
5. Principal process(es): Yarn manufacturing
6. Amount of principal product produced or raw material consumed
(T iSt cnPrific w=anntc rnncumPd anti/nr imitc of rmrinrti.+++l
(Product Produced
Raw MateriM Consumed
(AVERAGE)
Product Producedjr
Raw Matenal Consumed
(PEAK)
—per Day
63,318 lbs.
73,590 lbs. yarn produced
per Month
-.1,848,869 lbs.
2,526,943 lbs. yarn produced
per Year
18,OOb;000 lbs.
22,187,000 s yarn produced
7. (a) Check here if discharge occurs all year © , or
(b) Circle the month(s) in which discharge'occurs: January February March April
May June July August September October November . December
(c) Days per week discharge occurs: Monday Friday
NOTE: If the facility has separate discharge points (outfalls) or multiple industrial processes, include a
schematic diagram of wastewater flow at the facility.
Short Form C Version 9-97

NPDES PERMIT APPLICATION - SHORT Fr �,:,q C
To be filed only by persons engaged in manufacturing,and mining
Types of wastewater discharged to surface waters only (check as applicable).
Discharge per operating day
Flow ML
Volume treated before discharging
(GALLONS PER OPERATING DAY)
(PERCENT
Sanitary -daily average
+ boiler blowdown
9608
100
Cooling water, etc. - daily average
1719
(6 coolong towers)
0
Process water - daily average
•
0
0
Maximum per operating day for
13,170
0
total discharge (all types)
9. If any of the types of wastewater identified in item 8 (either treated or untreated) are discharged to
places other than surface waters, record the amount(s) discharged below: N/A
A. Municipal sewer system gpd
B . Underground well god
C. Septic tank gpd
D. Evaporation lagoon or pond gpd
E. Other, specify end
10. Number of separate discharge points: 2
11. Name of receiving water(s): Second Broad River
12. Does your discharge contain or is it possible for your discharge to contain one or more of the following
substances added as a result of your operations, activities, or processes? Circle all that apply:
aluminum
ammonia
beryllium_ cadmium
chromium hlorine (residual
copper
cyanide
lead mercury
nickel oil and. grease
phenols
selenium
zinc
None of the above
I certify that I am familiar with the information contained in the application and that to the best of my
knowledge and belief such information is true, complete, and accurate.
Edwin W. Horton Director of Engineering
Printed name of Person Signing Title
Signature of Applicant
§72- V 9 �
Date
North Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false statement
representation, or certification in any application, record, report, -plan, or other document files or required to be maintained
under Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies,
tampers with, or knowly renders inaccurate any recording or monitoring device or method required to be operated or
maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be
18ittyty of a misdemeanor punishable by a fine not to exceed $30,000, or by impprisonment not to exceed six months, or by both.
LI.S.C. Section 1001 provides a punishment by a fine of not more than $10,000 or imprisonment not more than 5 years, or
both, for a similar offense.)
Short Form C Version 9-97

US 221 A-
Stormwater Drains ......... p...........
........o
o....................
a .....;....; o
�.. o........ .......... a ........ D
©....... D........ a
V002 vnccL nunVn
on
NPDES
Second Broad River
BeriSlrigeY & GaYY1SOri F-AC) J May 6
998
PROJECT NO.: '10069
Environmental, Inc. SCALE: Not to SC2I0
E:)FiAWN BY: RES
FILE: C.. & Lord
Bluefield Engineering, P.C. Caroleen Plant NPOES
FIGURE 1 - NPDES Discharge Pi
Galey & Lord - Caroleen Plant I
Caroleen, NC

COOLING TOWERS
(6 TOWERS TOTAL)
DOMESTIC WASTEWATER
& BOILER BLOWDOWN
SANITARY
WWTP
1.
Septic tank
2.
Holding tank
3.
Dosing tank
1,719 gpd (ave.)
3.
Sand Filters
4.
Chlorinator
5:
Dechlorinator
9,608 gpd (ave.)
NPDES OUTFALL 001
Bensinger & Garrison FIGURE 2 - NPDES Discharge Process Flow
Environmental, Inc. Diagram
Bluefield Engineering, P.C.
SCALE: Not to Scale Galey p Lord
DATE:PROJECT NO.: May 96
19 Caroleen Plant
DATE: May 1998
DRAWN BY: RES Caroleen North Carolina
FILE: Galey 8 Lord -Caroleen NPDES ,
Fig 2

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality .
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
July 7, 1998
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Edwin W. Horton
Galey & Lord Ind - Caroleen
P.O. Box 158
Caroleen, NC 28019
SUBJECT: NOTICE OF VIOLATION -
Galey & Lord Ind - Caroleen
Rutherford County
NPDES No. NC0006009
Dear Edwin Horton:
1••
1:3 E N F10
This is to inform you that your monthly monitoring report for April 1998 has not been received by
the Division of Water Quality. This is in violation of Part 11, condition D.2 of the NPDES permit, as
well as 15A NCAC 2B .0506 (a), which requires the submittal of Discharge Monitoring Reports no later
than the 3& day following the reporting period. Failure to submit reports as required will subject the
violator to the assessment of a civil penalty of up to $10,000 per violation.
To prevent further action, please submit this report within 15 days of receipt of this notice to the
address below:
Division of Water Quality
Point Source Compliance / Enforcement Unit
P.O. Box 29535
Raleigh, NC 27626-0535
You will be considered noncompliant with the self -monitoring requirements of yourNPDES permit until
the report has been submitted.
We appreciate your assistance in this matter. If you have any questions about this letter or discharge
monitoring reports, please contact the Water Quality Section staff of our Asheville Regional Office at
[phone] or Susan Wilson at [phone], ext. 215.
Sincerely,
rk. Preston Howard, Jr., P.E.
cc: Compliance/Enforcement
Regional -Supervisor
Central Files
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Cara _(.3
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor .
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
N =FNR
Mr. Edwin W. Horton
Galey & Lord Industries, Inc.
P.O.Box 158
Caroleen, North Carolina 28109
September 9, 1998
SEp 1995-
} r i°quit CaE�AMUL ,sr
Subject: - NPDES_Draft=Permit
Permit No. NC0006009
Caroleen Plant
:Rutherford County
Dear Mr. Horton:
Please find enclosed a DRAFT NPDES permit that has been prepared for the subject facility -
by the Division of Water Quality (DWQ). I encourage you to review this -document very carefully
to ensure thorough understanding of the information, conditions and requirements contained herein.
The following changes were incorporated into this DRAFT permit:
-� For Outfall 002, monitoring requirements for all parameters (flow, temperature, -TRC, „_..
pH) were -changed from monthly to 2/Year.� This reflects current monitoring
requirements for cooling tower blowdown under general permit conditions.
• For Outfall 001, monitoring requirements and effluent limits were added for 'pH. ' In' -
addition, a biocide condition was added for this outfall, requiring pre -approval of any
additional biocides added to the treatment system.
• The permit expiration date has-been changed to July 31, 2003.
Currently, biocide additive Nalco 2593 has been approved in the cooling water in Outfall
002, and biocide additive Nalco 7346 is being reviewed for use in the boiler blowdown in Outfall.
001.
Please review this DRAFT permit carefully and submit any written comments to ' the
following address by October 9, 1998: NCDENR, DWQ/NPDES Unit, P.O.Box 29535,
Raleigh, North Carolina 27626-0535, Attn: David Goodrich.
If you have any questions or need additional information, please contact Mr. Tom Belnick,
telephone number [phone], extension 543.
Sincerely,
David Goodrich, NPDES Supervisor
cc: Asheville Regional Office, Water Quality f L '--
NPDES Unit =
Aquatic Toxicology (Attn:'Melissa Rosebrock)
DEH
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Permit No. NC0006009
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
f TO DISCHARGE WASTEWATER UNDER THE
f
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
f:
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and Iregulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Galey and Lord Industries, Inc.
i
is hereby authorized to discharge wastewater from a facility located at
Caroleen Plant
U.S. Highway 221-A
Caroleen, North Carolina
Rutherford County
to receiving waters designated as Second Broad River in the Broad River Basin
in accordance' with effluent limitations, monitoring requirements, and other conditions set forth in
Parts I,11, III,I and IV hereof.
This permit shall become effective xxxxx.
This permit and authorization to discharge shall expire at midnight on July 31, 2003.
Signed this d
DRAFT
A: Preston Howard, Jr., P.E., Director
Division of Water Quality
,By Authority of the Environmental Management Commission

ait No. NC0006009
SUPPLEMENT TO PERMIT COVER SHEET°
Galey and Lord Industries, Inc.
is hereby authorized to:
1. Continue to operate a 0.018 MGD wastewater treatment facility (Outfall 001)
consisting of aseptic tank, surface sand filter and. chlorination to treat domestic
wastewater and boiler blowdown at Galey and Lord Industries, Inc.- Caroleen Plant,
U.S. Highway, 221-A, Caroleen, Rutherford County (See Part IIIA 'of this permit), and
2. Continue to discharge cooling tower.blowdown through Outfall 002, and
3. Discharge wastewater from said treatment woks at the location specified on the '
attached map into Second Broad River, which is"classified WS-IV waters in the Broad -
River Basin. _ _

1
•
21 e . •9/6 .
It Col sepoll
-
'� peso � �� ,• ,.` ���
I37
e• • ' o
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s.
�y� .I . •�r
g '' oa• 11 nlCh • �i
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2119
�•, � as � � /� � S I%�(/�-/
I
Latitude: 351645
Longitude: 814800
USGS Quad #: F11SE
River Basin #: 03086
Receiving Stream: - Second Broad R
Stream class: WS-IV
Galey & Lord Industries
Caroleen Plant
NC 0006009
Rutherford County
Z

A (1). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - DRAFT Permit No. NC00060
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge domestic wastewater and
boiler blowdown from outfall serial number. 001. Such discharges shall be limited and monitored by the Permittee as specified below:
:EFFLU ` 1
ENT'"CHARACTERISTICS, r yy. k `",,,..„
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Flow A.
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:•: Weekly
Instantaneous
I or E
BOD, 5 day, 200C
30.0 mg/I
45.0 mg/I
2/Month
Grab
E
Total Suspended Residue
30.0 mg/I
45.0 mg/I
2/Month
Grab
E
NH3 as N
Monthly
Grab
E
Total Residual Chlorine
2/Week
..Grab
E
Temperature
Weekly
Grab
E
pH
2/Month
Grab
E
Fecal Coliform­ (geometric mean)
200/100 ml
400/100 ml
2/Month
Grab
E
Notes:
1 Sample locations:`E = Effluent, I = Influent
2. -'The temperature of the effluent shall not cause an increase in the temperature.of the receiving stream of more than 2.8°C above natural temperatures, and
. . and in no case cause the receiving water temperature to exceed 32°C. , .
3 The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
There shall be no chromium, zinc, or copper added to the treatment system except as pre -approved additives to biocidal compounds. The permittee shall obtain
authorization from the Division prior to utilizing any biocide in the discharge. The permittee shall notify the Director in writing not later than ninety (90) days prior
to instituting use of any'additional biocide used in boiler blowdown systems which may be toxic to aquatic life other than those previously reported to the
Division. Such notification shall include completion of Biocide Worksheet 101 and a map locating the discharge point and receiving stream.
There shall be'no discharge of floating solids or visible foam in other than trace amounts.

A (2). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS - DRAFT Permit No. NC0006009
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge cooling tower blowdown
from outfall serial number 002.- Such discharges shall be limited and monitored by the Permittee as specified below:
+EFFLU NT,.;CHARa►CTEaISTICS
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:.., r1!
✓. r . r �,t'Y �.,{r{.
Fre uenc ��,�
}{ q Y�;��•,., ;Nt�trar.°rYP
-Flow
21Year.-
—Instantaneous—
E
Temperature2, '
2/Year-
Grab
E
Total Residual Chlorine
2/Year..:
Grab
E
PH
Wear
Grab
E
Notes:
1. Sample locations: E - Effluent
2. The temperature of the effluent shall not cause an increase in the temperature of the receiving stream of more than 2.8°C above natural temperatures, and
and in no case cause the receiving water temperature to exceed 32°C.
3. Monitoring requirements apply only if chlorine is added to the treatment system.
4. The pH shall hot be less than 6.0 standard units nor greater than 9.0 standard units.
There shall be no'chromium, zinc', or copper added to the treatment system except as pre -approved additives to biocidal compounds. The permittee shall obtain
authorization from the Division prior to utilizing any biocide in the cooling water. The permitte shall notify the Director in writing not later than ninety (90) days
prior to instituting use bf any additional biocide used in cooling systems which may be toxic to aquatic life other than those previously reported to the Division.
Such notification shall include completion of Biocide Worksheet 101 and a map locating the discharge point and receiving stream..
There shall be no discharge of floating solids or visible foam in other than trace amounts.

DENR/DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0006009
r •aci , :, ormatton� x
:._ ,.-x _ m _...za......e...�.
mPlant
Facility Name
Galey & Lord Industries, Inc.- Caroleen
Permitted ow:
0.018
Facility ass:
Facility/PermitStatus:-
(i.e.-New, Modification,
Existing or Renewal)
Renewal
ounty:
Rut e or
tream ., eteristics z
6..`..., _ .v* 1.Lt>+s ri'r_\�; dw&'r a......".�:: . _R.3.,,_we-s. uk $`� t�d :sS"x`.a....d.ra:.X ..n3 ,, u...:..�c*.tY�...me�:ei
Receiving Stream:
Second
BroadRiver
Stream Classification:_WS-IV
u asm:
roa ver asm
Drainage Area (mi ):
206
Summer c s
Winter c s :
86
cs:
NA
Average Flow c s :
288
IWC 10.05%
Regional Office: I
Asheville
opo ua :
Changes Incorporated into Permit Renewal
N�ropose tinges M `
, s parameters " , ecte ,
axis or c ange sU�
Change monitoring trequency
T16w,­p1T,'Femperature,—=
Make monitoring frequencies
from monthly to 2/Year for
similar to general permit
Outfall 002 effluent (cooling
conditions for cooling tower
tower blowdown).
blowdown. The current
general permit conditions for
boiler blowdown only
requires semi-annual
monitoring for these
parameters.
Remove instream monitoring
Temperature
Not required in general permit
for Outfall 002
conditions.
Add biocide condition to
l3iocides
It appears that biocides are
Outfall 001
_
being used at both Outfalls x,:
001 and 002, and the biocide
Special Condition only ;
_
appeared at the bottom -of the';
002 effluent page.'
Add mots and monitoring tor
Ph
Minimum monitoring tbr p
Outfall 001:
required per 2B:0500 .
monitoring regulations for
SIG 4952.

-Change permit expiration at
from 11/30/98 to 7/31/2003.
Permit expiration
Renew permit according to.
Broad -River Basin Planning
Schedule.
NC0006009
Summary
Minor facility manufactures yarn. Outfall 001 contains sanitary wastewater plus boiler,
blowdown (combined total of 9608 gpd, treated), while Outfall 002 contains cooling
water from 6 cooling towers (1719 gpd, untreated). There is no process wastewater
discharged. Both outfalls discharge to the Second Broad River in the Broad River-.- - - _
Basin. The Second Broad River is classified WS-IV waters, and is not listed as a 303(d) . = -
impaired �vaterbody. I left stream classification as WS-IV, although file info varied
(WS-III, WS-IV, C); WS-IV seems to fit the latest classification description (Classified
8/3/92; Index No. 9-41-(14.5)).
Permit Changes
Permit application indicated that TRC and copper are components of water treatment
chemicaN used as biocides in the cooling water (002). I contacted their consultant (Jack
Garrison, [919-484-8536) who said the current additives were all approved during last
permit cycle. Based on file info and discussion with AgTox (Melissa Rosebrock), only
NALCO biocide 2593 was previously approved for Outfall 004. This outfall was
subsequently renamed Outfall 002 after the facility closed the original outfall 002 and
003. I asked facility to resubmit biocide 101 worksheets for NALCO biocide 7346,
which is currently being used in Outfall 001. Add biocide condition for each outfall
based on current usage.
Monitoring at Outfall 002 (cooling tower blowdown) was changed to reflect current
monitoring frequencies in general permit conditions.
DMR Data. No compliance problems over past few years. Good BOD, TSS, NH3, and
FC control. No pH data reported for Outfall 002, despite limit and monthly monitoring
required *'in current permit. No upstream/downstream temperature data reported for
Outfall 062 despite requirement in current permit [Note: NPDES is recommending that
upstream/,downstream monitoring be removed in permit renewal, since it is not required
in generalp permit].
Staff Report. The file contains an ARO staff report (dated 6/17/93) which rated the
facility as� Class I. The new permit application lists dechlorination at Outfall 001,
although no ATC is in file for this addition. If this is true, will need to add 5 points to
facility rating, which would still remain a Class I rating. ARO- is dechlor installed at
001?
WLA/Receiving Water. The last WLA was conducted in 6/93 using the current design
flow (0.018 MGD). Secondary limits were recommended. There was no toxicity for
TRC or ammonia based on mass balance calculation.

O
L�
f
DENRIDWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
NPDES No. NC0006009 (Continued)
Proposed Schedule for Permit Issuance
Draft Permit to Public Notice: 09/09/98
Permit Scheduled to Issue: 10/26/98
State Contact -
If you have any questions on any of the above information or on the attached
permit, please contact Tom Belnick at [phone], extension 543.
Copies of the following are attached to provide further information on the permit :-
development:
• Draft Permit
NPDES Recommendation by: Date: 7-
Regional Office Comments
This space is used by the Regional office personnel to identify specific concerns in
reference to issuance of the subject permit.
Regional Recommendation by: Date: '
Reviewed By:
Regional Supervisor: Date:
NPDES Unit: Date:

r- .
State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
-May 29, 1998
Mr. Edwin W..Horton
Galey & Lord Industries, Inc.
P.O. Box 158
Caroleen, North Carolina 28019
DEN R
Subject: NPDES Permit Renewal Application = --
Permit NC0006009
Gale_y-&=Lord=Industries
Rutherford County
Dear Mr. Horton:
The Division received your permit renewal application and renewal fee of $200.00 (paid by
check # 104233) on May 28, 1998. Thank you for submitting this package in a timely fashion.
The permit renewal for this facility has been assigned to Tom Belnick of the NPDES Unit. Mr.
Belnick will contact you if further information is needed to complete the permit renewal. If you have
any additional questions concerning renewal of the subject permit, please contact Mr. Belnick at (919)
733-5083, extension 543.
Sincerely,
141
Charles H. Weaver, Jr.
NPDES Unit
cc: Central Files
Asheville -Regional Office, Water_Q.uality Section
NPDES File
P.O. Box 29535, Raleigh, North Carolina 27626-0535 919 733-5083, extension 511 (fax) 919 733-0719
An Equal Opportunity Affirmative Action Employer Charles—[e-mail]

��' Galey�I.ord
March 16, 1998
North Carolina Department of
Environment and Natural Resources
Asheville Regional Office
Division of Water Quality
NPDES Unit
------
Asheville, NC 28801
Attention: Mr. Roger C. Edwards
Wastewater Consultant
Subject: NPDES-Permit Number NC0006009
Galey & 'Lord WWTP
Caroleen Plant
Rutherford County
Dear Mr. Edwards:
The purpose of this letter is to inform you that Ralph M. Gibson has retired from Galey
& Lord Industries, Inc in 1995 and Edwin W. Horton is his replacement.
Please change your records accordingly.
Your attention to this matter is appreciated.
Sincerely,
GALEY & LORD INDUSTRIES, INC.
Edwin W. Horton
Director of Corporate Engineering
/du
P. O. Box 35528
Greensboro, North Carolina 27425-0528
cc: Permit File
NCDEHNRIet G

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor .
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
March 5, 1998
Ralph Gibson
Galey & Lord Industries
P.O. Box 35528
Greensboro, NC- 27425
NC DEN R
Subject: Renewal of NPDES Permit No. NC0006009
Caroleen Plant
Rutherford County
Dear Permittee:
The subject permit expires on November 30, 1998. North Carolina General Stature 143.215.1(c) requires that an
application for permit renewal be filed at least 180 days prior to the expiration date.
To satisfy this requirement, your renewal package must be sent to the Division postmarked no later than June 3,
1998. Failure to request renewal by June 3, 1998 will result in a civil assessment of at least $250.00. Larger
penalties may be assessed depending upon the delinquency of the request.
If any wastewater discharge will -occur after November 30, 1998 (or if continuation of the permit is desired), the
permit must not be allowed to expire. Operation of waste treatment works or continuation of a discharge after
November 30, 1998 would violate NCGS 143-215.1 and could result in assessment of civil penalties of up to
$10,000 per day.
If all wastewater discharge has ceased at the subject facility and you wish to rescind this permit, contact Robert
Farmer of the Division's Compliance Enforcement Unit at [phone], extension 531. You may also. contact
the Asheville Regional Office at [phone] to begin the rescission process.
Use the enclosed checklist to complete your renewal package. The checklist identifies the items which you must
submit when applying for renewal of the subject permit.
If you have any questions, please contact me. My telephone number, fax number and e-mail address are listed
below.
Sincerely, 4
arles H. Weaver, Jr.
NPDES Unit
cc: Central Files
Asheville -Regional Office, Water Quality Section
P.O. Box 29535, Raleigh, North Carolina 27626-0535 919 733-5083, extension 511 (fax) 919 733-0719
An Eaual Opportunity Affirmative Action Eniblover Charles [e-mail]

NC DENR / DWQ / NPDE�c
Permit Renewal Applications
Renewal Package Checklist
NPDES Permit No. NC0006009
Galey & Lord Industries
Rutherford Countv
The following it Itter ms are REQUIRED for all renewal packages:
F-1 A cover requesting the renewal and documenting any changes at the facility
since issuance of the last permit. Submit one signed original and two copies.
❑ The completed application form (copy attached), signed by the permittee or an
Authorized Representative. Submit one signed original and two copies.
❑ If an Authorized Representative is preparing the renewal package, documentation
must be provided from the permittee defining the person or company preparing the
renewal package as an Authorized Representative (see Part II.B.1Lb. of the NPDES
permit). I
F-1
A renewal fee of $200 in accordance with 15A NCAC 2H .0105(b). The fee is based
on wastewater flow from the Caroleen Plant discharge. Make checks payable to NC
DENR. See the note below concerning fee amounts.
F-1
A narrative description of the sludge management plan at the subject facility. If
your facility has no sludge management plan, explain the reason for this in your
cover letter. Submit one original and two copies.
The following requirement does NOT apply to municipal or nonindustrial facilities.
The following item applies to Industrial facilities only:
F-1. Industrial facilities classified as Primary Industries (listed in Appendix A of Title 40 of
the Code of�Federal Regulations, Part 122) must submit a Priority Pollutant Analysis
in accordance with 40 CFR Part 122.21.
For renewal p
For renewal
the completed renewal package and appropriate fee to:
Mr. Charles H. Weaver, Jr.
NC DENR / DWQ / NPDES
P.O. Box 29535
Raleigh, North Carolina 27626-0535
postmarked on or prior to June 3, 1998, submit a fee of $200.
postmarked AFTER June 3, 1998, submit a fee of $400.

',2ate of North Carolina �-
" Department of Environment
and Natural Resources _ ,r
Asheville Re ional Office - ^�`'w'
--- Division of Water Quality
_ NCDEN
=James B. Hunt, Jr., Governor-, ORTH CAROLINAFPARTMEN
Wayne McDevitt, Secretary - - E"viRo"Meru ""° N aruw� REsi
WATER ; QUALITY SECTION_
'- December •G-2', - 1997
Subject: Compliance Sampling Inspection
Status: In Compliance =
NPDES Permit 'Number NC0006009
Galey and Lord WWTP .
Caroleen Plant
Rutherford County
The Division of Water Quality conducted the above referenced
inspection on December 9, 1997. Samples were collected by the
inspector during the inspection. The attached report contains
National Pollutant Discharge Elimination System (NPDES). Permit
limited parameters and sample results for those parameters. The
.-Tacility'is operating within the limits.established in the NPDES
' Permit
In discussions with the operator, Mr. William McKinney, it
is understood that repairs "recommended .in the October 23, 1996
report will be -completed during the December 22, 1997 shut down.
Recommendations were made to the operator on spacing/placement of
wholes in the new laterals and,installation of .valves at the head
of the. new laterals. The spacing/placement of wholes in the
laterals and valves at the .head of the laterals will allo%
control of the flow over the sand filter.
59 Woodfin Place, Asheville, North Carolina 28801
'Telephone [phone] Fax [phone]
An Equal Opportunity Affirmative Action Employer

Mr. Gibson
December 221 1997
Page two
Th! monthlyDischarge Monitoring
f g g reports reviewed from
November.1996 through October 1997, indicate the facility had one
. (1),..daily _ maximum violation of fecal coliform.' The time and
assistance of Mr: William McKinney, during. -the inspection was
appreciated. If you or your staff have questions regarding this
report,jor if I may be of assistance, please contact me at 704-
251-620g8g.
Sincerely,
fo
er C. Edwards
Wastewater Consultant
CC: Mr. Jake Wilson, Plant Engineer
Mr�. William McKinney, ORC

United States Envirol!al Protection Agency Form Approved
Washington, D.C. 20460 OMB No. 2040-0003
Approval Expires 7-31-85
P . ..NPDES Compliance -Inspection Report
Section A: National Data System Coding
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac Type _
1 IN 2 U _ - 3 .N00006009 11 12 97/12/09 17 18 U
19 IJ I 20
' Remarks , _ -...'
I I I - I I I I 'I 'I I I I I I I ,I I -I I `I I I I I I I I' ,I I I I I I I �I Iv.I'
II I- I I I' I •1 I ,h
" Reserved - Facility Evaluation Rating -. - --�• -- - BI QA -
Reserved--
67 69 u
70 3 71 I ' I 72 I uI .. - 73 I I ' ' I 174
L_J�
- 75 80
Section B: Facility Date
Name and Location of Facility Inspected
Entry Time
Permit Effective Date
Galey and Lord Industries
1:00 pm
.
July 5, 1994
P. O. Box 35528
Exit Time/Date
Permit Expiration Date
t
Greensboro27425
'=NC
2:00 pm
Nov. `30 ' 1998
Name(s) of On -Site Representative(s)fTitle(s) r," •
Phone No(s) ,
Mr. William McKinney, ORC.
704-657-6376
Name, Address of Responsible Official
Title
Mr. Ralph Gibson
Director of Engineering
P. O. Box 35528
Phone No.
Contacted
Greensboro, . NC 27425
919-379-2884
No
Section C: Areas Evaluated During Inspection CODES S - Satisfactory M - Marginal _ U - Unsatisfactory
- N - Not evaluated(Not applicable
S ::
Permit
Records/Reports
Facility Site Review
S
Flow Measurement
Laboratory
Effluent/Receiving Waters
N
Pretreatment
Compliance Schedules
Self -Monitoring Program
S
Operations &Maintenance
Sludge Disposal
Other. row 15
S _
N
N
S
S
S
S
Section D: Summary of Findings/Comments (Attach additional
sheets if necessary)
Facility is operating in accordance with NPDES Permit limits. NPDES Permit limits and sample results are listed below.
Effluent Characteristics Monthly Average Sample Results
BOD 30.0 mg/I < 2 mg/I
Total Suspended Solids 30.0 mgA < 1.0 mg/I
Fecal Coliform 200/100 ml <2/100 ml
Ammonia Nitrogen No limit 0.1 mg/1
Replacement of laterals and three inches of sand on the sand filter is to be completed the week of December 22; 1997.
Name(s) and Signature(s) of Inspector(s)
Agency/Office/Telephone
Date
ROGER C. EDWARDS
�% ✓
DWQ/ARO 704-251-6208
gnat re Reviewer
Agency/Office
Date
_
DWQ/ARO 704-251-6208
J obihx
Regulatory Office Use Only
Action Taken -
Date
Compliance Status
13 N9ncompliance
®/Compliance

DIVISION OF ENVIRONMENTAL MANAGEMENT W For Lab Use ONLY
AT
ER QUALITY FIELD -LAB FORM %DM1)
COUNTY_PSA
PRIORITY
SAMPLE TYPE
RIVER BASIN
>'
❑AMBIENT [I
❑
REPORT TO:
O FROROMRO RRO WaRO WIRO WSRO TS
QA
STREAM
EFFLUENT
AT BM
❑ COMPLIANCE ❑ CHAIN
El LAKE
❑ INFLUENT
Other
Other
Shipped by: Bus Courier, Staff Other
OF CUSTODY
❑ EMERGENCY
❑ ESTUARY
Lab Number: :2
y
Date Received: /oZ— 2 7? Time:
Rec'd by:
From: Bus-Couri -Hand D 1
DATA ENTRY BY:
CK: SI'
DATE REPORTED:
IQ — / p - 7 7
COLLECTOR(b): (dJ S
Estimated BOD Range: -5/-25/25-65/40-130 or 100 plus STATION LOCATION: C Z/�
Seed: Yes B"'No ❑ Chlorinated: Yes LAY No ❑ REMARKS:
Station ,� Date Begin (yy/mm/ddd)) Time Begin Date End Time End Depth DM DB DBM Value Type Composite Sample T
r ` 7 1 `L Q/ 13 z � A H L T S B C 1G GNXX
1
lE
17
18
19
20
OD5 310 C mg/I
COD High 340 mg/1
COD Low 335 mg/I
oliform: MF Fecal 31616 C /100m1
Coliform: MF Total 31504 /100ml
Coliform: Tube Fecal 31615 /loom]
Coliform: Fecal Strep 31673 /100m1
Residue: Total 500 mg/I
Volatile 505 mg/I
Fixed 510 mg/1
...,,Residue:
Suspended 530 mg/I
Volatile 535 mg/I
Fixed 540 mg/I
pH 403 units
Acidity to pH 4.5 436 mg/I
Acidity to pH 8.3 435 mg/1
Alkalinity to pH 8.3 415 mg/l
Alkalinity to pH 4.5 410 mg/I
TOC 680 m9A
Turbidity 76 NTU
Chloride 940 mg/I
Chi a: Tri 32217 ug/1
Chi a: Corr 32209 ug/1
Pheophytin a 32213 ug/1
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color: pH 7.6 82 ADMI
Cyanide 720 mg/I
Fluoride 951 mg/I
Formaldehyde 71880 mg/I
Grease and Oils 556 mg/I
Hardness Total900 mg/I
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/I
Phenols 32730 ug/I
Sulfate 945 mg/I
Sulfide 745 mg/1
3 as N 610 D , mg/I
Y
TKN as N 625 mg/1
NO2 plus NO3 as N 630 mg/I
P: Total as P 665 mg/l
PO4 as P 70507 mgA
P: Dissolved as P 666 mg/l
Cd-Cadmium 1027 ugA
CrChromium:Tota11034 ugA
Cu-Copper 1042 ug/I
NI -Nickel 1067 ugA
Pb-Lead 1051 ug/1
Zn-Zinc 1092 ugA
Ag Silver 1077 ugA
Al -Aluminum 1105 ug/I
Be -Beryllium 1012 ug/I
Ca -Calcium 916 mgA
Co -Cobalt 1037 ug/1
Fe -Iron 1045 ugA
Sampling Point %
Conductance at 25 C
Water Temperatum (C)
D.O. mgA
pH
Alkalinity
Acidity `!Q 1� °�>�
Air Temperatuie.(C)
pH 8.3 pH 4.5
pH 4.5 pH 8.3::. , .1
/0'
2
94
10
300 •
400 •
82244 1431
82243 182242 at•.,.
<20
Salinity %
Precipitlon Wday)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
Stream Depth=ft�
Stream Width fL
[ean
480
45
32
36
1351
1350
138
a
4
ti

't-'4DIVISION OF ENVIRONMENTAL MANAGEMENT- WATER QUALITY FIELD -LAB FORM (DM1)
0
'., COUNTY
��`�"
1� PRIORITY
SAMPLE TYPE
RIVER BASIN
❑AMBIENT
[I
❑
E
�` REPORT TO:
O RO MRO RRO WaRO WIRO WSRO TS
QA
STREAM
EFFLUENT
AT BM
❑COMPLIANCE
❑CHAIN
❑LAKE
❑ INFLUENT
Other
❑
OF CUSTODY
❑
t:— r .h n�. nh3l V
Lab Number: /I g) p
Date Received: iv -a3 " 16 Time: a ' Q
Rec'd by: li From: Bus-Courtq!-Hand el
DATA ENTRY BY: CK, L9 W t
Shipped by: Bus Courier, Stalk 0 her EMERGENCY ESTUARY DATE REPORTED:_
:,.,COLLECTOR (.S): ��IC
Estimated BOD Range: 0-5/5-25/25-65/40-130 or 100 plus STATION LOCA�TI/ON:
-Seed: Yes G3-"No ❑ Chlorinated: Yes 2 No ❑ /V REMARKS: C of-)() fp Q rr
Station # Date Begin (yy/mm/dd) Time Begin Date End Time End Depth DM DB DBM Value Type Composite Sample Ty e
•. 9Cy 23 A H L T S B C GNXX
i `.' .•. 1
BOD5 310 .. 7 C mg/1
at
COD High 340 mg/I
2
3
COD Low 335 mg/1
oliform: MF Fecal 31616 /loom]
4
i 5
,
Coliform: MF Total 31504 /loom]
6
Coliform: Tube Fecal 31615 /100ml
Coliform: Fecal Strep 31673 /100ml
8
Residue: Total 500 mg/I
9
Volatile 505 mg/1
! 10
Fixed 510 mg/1
11
Residue: Suspended 530 mg/I
' 12
Volatile 535 mg/I
13
Fixed 540 mg/1
14
pH 403 units
15
Acidity to pH 4.5 436 mg/1
16
Acidity to pH 8.3 435 mg/1
4.7
Alkalinity to pH 8.3 415 mg/1
18
Alkalinity to pH 4.5 410 mg/1
19
TOC 680 mg/I
on
Turbidity 76 NTU
Chloride 940 mg/l
Chi a: Tri 32217 ug/1
Chi a: Corr 32209 ug/1
Pheophytin a 32213 ug/I
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color: pH 7.6 82 ADMI
Cyanide 720 mg/1
Fluoride 951 mg/I
Formaldehyde 71880 mg/1
Grease and Oils 556 mg/I
Hardness Total900 mg/I
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/1
Phenols 32730 ug/I
Sulfate 945 mg/1
Sulfide 745 mg/1
H3 as N 610 D mg/i
TKN as N 625 mg/1
NO2 plus NO3 as N 630 mg/l
P: Total as P 665 mg/1
PO4 as P 70507 mgA
P: Dissolved as P 666 mg/I
Cd-Cadmium 1027 ug/1
CrChrondum:Total1034 ugA
Cu-Copper1042 ug/I
NI -Nickel 1067 ug/I
Pb-Lead 1051, ug/l
Zn-Zinc 1092 ug/I
Ag-silver 1077 ug/I
AI -Aluminum 1105 ug/1
Be -Beryllium 1012 ug/1
Ca -Calcium 916 mg/I
Co -Cobalt 1037 ug/I
Fe -Iron 1045. ug/I
LI-Lithium 1132 ug/1
big -Magnesium 927 mg/1
Mn-Manganese 1055 ug/1
Na-Sodium 929 mg/l
Arsenic -Total 1002 ug/I
Se-Selenlum 1147 ug/1
Hg-Mercury 71900 ug/l
Organochlorine Pesticides
Organophosphorus Pesticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Ph lop l vkt'
wW
R ;
Sampling Point %
Conductance at 25 C
Water Temperature (C)
D.O. mgA
pH
Alkalinity
pH 8.3 pH 4.5
c I
pH 4.5 8.�1?Y
Air 7i'er petal )
/
2
94
10
300 .
400 If
82244 431
82243 1 - 4.2_
2
Salinity %
Precipltlon Qn/day)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity l/H
Nn StSeam,Depthz
Stream 1A71 t.
480
45
32
36
1351
1350
35
v,
DMl/Revised 10/86

e of North Carolii r `
epartment of Environment,
Health and Natural Resources ` •
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary E, H N R A. Preston Howard, Jr., P.E., Director
Asheville Regional Office
WATER QUALITY SECTION
November 5, 1996
Mr. Ralph Gibson
Galey and Lord -Industries
P. O. Box 35528
Greensboro, NC 27425-0528
Subject: Compliance Sampling Inspection
Status: In Compliance
NPDES Permit Number NC0006009
Galey and Lord WWTP
Caroleen Plant
N Rutherford County
Dear Mr. Gibson:
The,Division of Environmental Management conducted the above
referenced inspection on October 23, 1996. Samples were collected
by the inspector during the inspection. The attached report
contains National Pollutant Discharge Elimination System (NPDES)
Permit limited parameters and sample results. for those
parameters. 'The facility is operating within the limits
established in the NPDES Permit.
During the inspection observations were made that several of
the distribution laterals have deteriorated resulting in their
breakage. I suggest these laterals be -repaired or replaced as
soon as possible. This will prevent a lateral failure, that
would allow a area of the sand filter to be flooded. In
addition, areas of the sand filter appear to receive more of the
wastewater flow, than other areas. In the area that receive
greater flow the sand has accumulated solids. I suggest, removing
two (2) inches of sand and solids in these areas and replacing it
with new sand.
The monthly Discharge Monitoring reports reviewed from
September 1995 through August 1996, indicate the facility is
operating consistently in compliance. The time and assistance of
Mr. William McKinney, during the inspection was appreciated. If
you or your staff have questions regarding this report, or if I
may be of assistance, please contact me at 704-251-6208.
Interchange Building, 59 Woodfin Place g4ft�FAX [phone]
Asheville. North Carolina 28801 N� An Equal Opportunity/Affirmative Action Employer
Voice 704 251-6208 _ 50% recycles/ 1 (No post -consumer paper

I�
li.
Mr. Gibson
November i5, 1996
Page two,
CC: Mr.,iJake Wilson, Plan
Mr.;William McKinney,
Sincerely, G�
f".,
C. Edwards
Wastewater Consultant
t Engineer
ORC

f, United States E, imental Protection Agency ! Form Approved
WaN
.;rm, D.C. 20460 OMB No. 2040003
Approval Expires 7-31-85
AV tNPDES Compliance Inspection Report
Section A: National Data System Coding
Transaction Code
NPDES yr/mo/day Inspection Type Inspector Fac Type
1 L 1 2 IJ 3 NC0006009 11 12 96/10/23 17 18 L_.J
19 U 20 U
IIIIIIIIIIIIIIIIII(Illlllllllllllllllllllllllll
Remarks
" Reserved Facility Evaluation Rating
BI QA
Reserved 46
67 11 _L� I 169 70 3
L_L L�
71 IonI 72 I I 73 l I 1174
IB:
75 80
3 Section Facility Date
Name and -Location of Facility Inspected
Entry Time -
Permit- Effective Date
Galey and Lord Industries
10:55 am
July 5, 1994
P. O. Box 35528
Exit Time/Date
.
Permit Expiration Date
Greensboro, NC 27425
11:20 am.
Nov. 30, 1998'
Name(s) of On -Site Representative(s)fritle(s)
Phone No(s)
Mr. William McKinney, ORC
704-657-6376'
Name, Address of Responsible Official
Title
Mr. Ralph Gibson
Director of Engineering
P. O. Box 35528
Phone No.
Contacted
Greensboro, NC 27425
919-3 79-2884
No
Section C: Areas Evaluated During Inspection
CODES Q S - Satisfactory M - Marginal U - Unsatisfactory
N - Not evaluated(Not applicable
S
Permit
S
Flow Measurement
N
Pretreatment
S
Operations & Maintenance
Records/Reports
Laboratory
Compliance Schedules
Sludge Disposal
S
N
N
S
Facility Site Review
Effluent(Receiving Waters
Self -Monitoring Program
Other. row 15
S
S
S
Section D: Summary of Findings/Comments (Attach additional sheets if necessary)
Facility is operating in accordance with NPDES Permit limits. NPDES Permit limits and sample results are listed below.
Effluent Characteristics
Monthly Average Sample Results
BOD
30.0 mg/l 2.5 mg/I
Total Suspended Solids
30.0 mg/I < 1.0 mg/l
Fecal Coliform
200/100 ml <2/100 ml
Ammonia Nitrogen.
No limit 0.2 mg/I
Name(s) and Signature(s) of Inspector(s)
Agency/Office/Telephone
Date
ROG R C. EDWARDS
DWQ/ARO 704-251-6208
Si Reviewer
Agency/Office
D e
DWQ/ARO 704-251-6208
��49 z
Regulatory Office Use Only
Action Taken
Date
Compliance Status
Noncompliance
��Compliance

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office
WATER QUALITY SECTION
October 11, 1995
Mr. Ralph Gibson
Galey and Lord Industries
P. O. Box 35528
Greensboro, NC 27425-0528
Dear Mr. Gibson:
Subject: Compliance Sampling Inspection
Status: In Compliance
NPDES Permit Number NC0006009
Galey and Lord WWTP
Caroleen,'Plant
Ruth ord County
The Division of Environmental Management conducted the above
referenced inspection on September 26, 1995. Samples were
collected by the inspector during the inspection. The attached
report contains National Pollutant Discharge 'Elimination System
(NPDES) Permit limited parameters and sample results for those
parameters. The facility is operating within the limits
established in the NPDES Permit.
The monthly Discharge Monitoring reports reviewed from July
1994 through July 1995, indicate the facility is operating
consistently in compliance. The time and assistance of Mr. Sam
McKinney, during the inspection was appreciated. If you or your
staff' have questions regarding this report, or if I may be of
assistance, please contact me at 704-251-6208.
Sincerely,
fTC. Edwards
Wastewater Consultant
cc: Mr. Jake Wilson, Plant Engineer
Mr. Sam McKinney, ORC
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
. An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

United States Env,' iental Protection Agency
Form Approved
I Washi,•. ._*, D.C. 20460
OMB No. 2040-0003
•
EPA NPDES Compliance Inspection Report
Approval Expires 7-31-85
�i Section A: National Data System Coding
Transaction Code
NPDES yr/mo/day Inspection Type Inspector Fac Type
1 IN2 15 I
u u
3 N00006009 l l 12 95/10/1 1 17 18 $
IS
19 I$ I 20 � 2
u u.
I I I I I I I I I
I
Remarks
I I I I I I I I I I I I I I I I I I I I I I I( I I
I I I I I I I I I I
21 Reserved Facility Evaluation
Rating BI QA
Reserved 66
67 L _1 U 69 it
70 13u I 71 I I 72 I LI 73 � 74
75 80
Secti�onJB: Facility Date
Name and Location of Facility Inspected
Entry Time
Permit Effective Date
Galey and Lord Industries ;
9:45 am
July 5, 1994
P. O. Box 35528
Greensboro, NC 27425
Exit Time/Date
Permit Expiration Date
i
10:15 am
Nov. 30, 1998
Name(s) of On -Site Representative(s)nitle(s)
Phone No(s)
Mr. William McKinney, ORC �I
i
704-657-6376
Name, Address of Responsible Official
Title
Mr. Ralph Gibson
Director of Engineering
P. O. Box 35528
Greensboro, NC 27425
Phone No.
Contacted
919-379-2884
No
Section C: Areas Evaluated During Inspection
S
Permit
i
Records/Reports
Facility Site Review
S
Flow Measurement
Laboratory
Effluent/Receiving Waters
N .
Pretreatment
Compliance Schedules
Self -Monitoring Program
S'
Operations & Maintenance
Sludge Disposal
Other: row 15
S
N
N
S
S
S
S
4 Section D: Summary of Findings/Comments (Attach additional sheets if necessary)
Facility is operating in accordance with NPDES Permit limits. NPDES Permit limits and sample results are listed below.
Effluent Characteristices Monthly Average Sample Results
BOD 30.0 mg/I 3.3 mg/I
Total Suspended Solids II 30.0 mg/I 1.0 mg/I
Fecal Coliform 200/100 ml <10/100 ml
I
i
I'
I
Name(s) and Signature(s) of Inspeccor(s)
Agency/Office/Telephone
Date
ROGER C. EDWARDS 11
e• i (A
DEM/ARO 704-251-6208
�-6-
Si u f Reviewer 1'
Agency/Office
DEM/ARO 704-251-6208ze
I Daifi
Al51.
l
b�
Regulatory Office Use Only
Action Taken
Date
Compliance Status
1
Nogcompliance ,
��Compliance
.:

For Lab Use ONLY
DIVISIONN OF ENVIRONMENTAL MANAGEMENT WATER QUALIT FI D-LAB FORM (DM1)
COUNTY PRIORITY SAMPLE TYPE
RIVER BASIN ❑AMBIENT ❑ QA ❑ STREAM LJ EFFLUENT
REPORT TO: RO FRO MRO RRO WaRO WIRO WSRO TS
AT BM ❑ COMPLIANCE ❑ CHAIN ❑ LAKE ❑ INFLUENT
Other
OF CUSTODY
Shipped by: Bus Courier Staff, they ❑ EMERGENCY ❑ ESTUARY
Lab Number: 12(
[ 7
Date Received: /'oZ(�—�,� Time: T d 0
Rec'd by: S-✓
I From: Bus•Courri)e an e
DATA ENTRY BY:
V-- CK:
DATE REPORTED:$—
COLLECTOR(.5): � r 1 �$ �
STATION LOCATION:
Estimated BOD Range: 0-5/5-25/25-65/40-130 or -100 plus �� F
Seed: Yes 2L No ❑ Chlorinated: Yes g- No ❑ REMARKS: -
Station Ae Date Begin (yy/mm/ddd) Time Begin Date End Time End Depth DM DB DBM Value Type Composite Sample Type
/ 7 O b oo -0L I A H L T, S B C O GNXX
1
BOD5 310 3. 3 mg/I
2
COD High 340 mg/1
3
COD Low 335 mg/1
4
oliform: MF Fecal 31616 �D /100ml
5
Coliform: MF Total 31504 /loom]
6
Coliform: Tube Fecal 31615 /loom]
Coliform: Fecal Strep 31673 /loom]
8
Residue: Total 500 mg/I
9
Volatile 505 mg/I
10
Fixed 510 mg/1
11
Residue: Suspended 530 mg/I
12
Volatile 535 mg/I
13
Fixed 540 mg/I
14
pH 403 units
1.5
Acidity to pH 4.5 436 mg/I
16
P
Acidity to pH 8.3 435 mg/1
-� 17
Alkalinity to pH 8.3 415 mgA
18
Alkalinity to pH 4.5 410 mg/I
19
TOC 680 mg/1
20
Turbidity 76 NTU
Chloride 940 mg/1
Chi a: Tri 32217 ug/I
Chi a: Corr 32209 ug/I
Pheophytin a 32213 ug/I
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color: pH 7.6 82 ADM]
Cyanide 720 mg/I
Fluoride 951 mg/I
Formaldehyde 71880 mg/I
Grease and Oils 556 mg/1
Hardness Total900 mg/I
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/1
Phenols 32730 ug/I
Sulfate 945 mgA
Sulfide 745 mg/l
NH3 as N 610 D ` mg/1
TKN as N 625 mg/l
NO2 plus NO3 as N 630 m9A
P: Total as P 665 mg/I
PO4 as P 70507 mgA
P: Dissolved as P 666 mgA
Cd-Cadmium 1027 ug/I
CrChromiunuTotal1034 ug/I
Cu-Copper 1042 ug/I
Ni-Nickel 1067 ug/I
Pb-Lead 1051 ugA
Zn-Zinc 1092 ugA
Ag-Silver 1077 ugA
Al -Aluminum 1105 ug/I
Be -Beryllium 1012 USA
Ca -Calcium 916 mgA
Co -Cobalt 1037 ug/I
Fe -Iron 1045 ugA
Li -Lithium 1132 ug/I
Mg -Magnesium 927 mg/1
Mn-Manganese 1055 ug/I
Na-Sodium 929 mg/1
Arsenic -Total 1002 ug/I
Se -Selenium 1147 ug/I
Hg-Mercury 71900 ug/l
Organochlorine Pesticides
Organophosphorus Pesticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoplankton
Sampling Point %
Conductance at 25 C
Water Temperature (C)
D.O. mg/1
pH
Alkalinity
Acidity
Air Temperature (C)
pH 8.3 pH 4.5
pH 4.5 pH 8.3
2
94
10
300 If
400 1•
82244 431
82243 182242
20
Salinity %
Precipition 0n/day)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
Mean Stream Depth ft.
Stream Width fL
480
45
32
36
1351
1350
35
64
4
i
DM1/Revised 10/86

FmfNorth Carolinaent of Environment,
th and Natural Resources
.ion of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B.. Howes, Secretary
A./P/reston Howard, Jr., P.E., Director
May 12, 1995
Ralph Gibson
Galey & Lord Industries
P.O. Box 35528
Greensboro, NC 27425
4
Subject: General Permit No. NCG170000
Galey & Lord Industries
COC NCG 170175
Rutherford County
Dear Ralph Gibson:
In accordance with your application for discharge permit received on March 8, 1995, we are forwarding
herewith the subject certificate of coverage to discharge under the subject state - NPDES general permit. This
permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the
Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated
December 6, 1983.
If any parts, measurement frequencies or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual permit
application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the Division
of Environmental Management. The Division of Environmental Management may require modification or
revocation and reissuance of the certificate of coverage.
This permit does not affect the legal requirements to obtain other permits which may be required by the
Division of Environmental Management or permits required by the Division of Land Resources, Coastal
Area Management Act or any other Federal or Local governmental permit that may be required.
If you have any question concerning this permit, please contact MR. BILL MILLS at telephone number
919/733-5083.
,cc_:.Asheville =Regional=Off ce---�
P.O. Box 29535, Raleigh, North Carolina 27626-0535
An Equal Opportunity Affirmative Action Employer
Sincerely, Signod dY
(,:tri�Eitck �.
�oioen H. Sullins
A. Preston Howard, Jr. P.E.
Telephone [phone] FAX [phone]
50% recycled/ 10% post -consumer paper

"— STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT, HEALTH., AND NATURAL RESOURCES
DIVISION OF ENVIRONMENTAL MANAGEMENT
GENERAL PERMIT NO. NCG170000
CERTIFICATE OF COVERAGE No. NCG170175
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Galey & Lord Industries
is hereby authorized to discharge stormwater from a facility located at
Galey & Lord Industries
Hwy. 221A
Caroleen, NC
Rutherford County
to receiving waters designated as Second Broad River in the Broad River Basin
in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III
and IV of General Permit No. NCG170000 as attached.
This certificate of coverage shall become effective May 12, 1995.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day May 12, 1995.
3y
;i
A. Preston Howard, Jr., P.E., Director
Division of Environmental Management
By Authority of the Environmental Management Commission

-900
100
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�.��--r1�'' ,,, J///� �r � �{-�—�r��`.

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office
'ALIT
C)EHNR
WATER QUALITY SECTION
February 10, 1995
Mr. Ralph Gibson
Galey and Lord Industries
P. O. Box 35528
Greensboro, NC 27425-0528
Subject: Compliance Sampling Inspection
Status: In Compliance
NPDES Permit Number N00006009
Galey and Lord WWTP
Caroleen Plant
Rutherford County
Dear Mr. Gibson:
The above referenced inspection conducted on January 12,
1995., by the Division of Environmental Management. The facility
was in good operational condition with all equipment functioning
as designed. Samples collected at the time of the inspection
indicate the facility is operating within the NPDES Permit
limits.
The assistance of Mr. William
appreciated during the inspection.
questions regarding this inspection
please, do not hesitate to contact
McKinney, was helpful and
If you or your staff have
or if I may be of assistance
me at 704-251-6208.
Sincerely,
Roger C. Edwards
Wastewater Consultant
CC: Mr. Jake Wilson, Plant Engineer
Mr. William McKinney, ORC
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Ak
United States Envir mental Protection Agency
Form Approved
Washington, D.C. 20460
OMB No. 2040-0003
Approval Expires 7-31-85
NPDES Compliance Inspection Report
Section A: National Data System Coding
`
Transaction Code
NPDES yr/mo/day Inspection Type Inspector Fac Type
1 2I5 I
I� 1�J
3 NC0006009 11 12 94/01/12 17 18 L
19 I I 20I` i
I I I I I I I I I I I
Remarks
I I I I I I I I I I I I I I I I I I I I I I I I
I I I I I I I I I• I I
" Reserved Facility Evaluation Rating BI QA
Reserved 55
67 L._J U 69 70 u 13 I 71 I onI 72 IuI 73 � 74
77-180
Section B: Facility Date
Name and Location of Facility Inspected
Entry Time
Permit Effective Date
Galey and Lord Industries
11:00 am
July 5, 1994
P. O. Box 35528
Greensboro, NC 27425
Exit Time/Date
Permit Expiration Date
11:35 am
Nov. 30, 1998
Name(s) of On -Site Representative(s)/ritle(s)
Phone No(s)
Mr. William McKinney, ORC
704-657-6376
Name, Address of Responsible Official
Title
Mr. Ralph Gibson
Director of Engineering
P. O. Box 35528
Phone
Contacted
Greensboro, NC 27425
919-379-2884
No
Section C: Areas Evaluated During Inspection
S
Permit
Records/Reports
Facility Site Review
S
Flow Measurement.
Laboratory
Effluent/Receiving Waters
N
Pretreatment
Compliance Schedules
Self -Monitoring Program
S
Operations & Maintenance
Sludge Disposal
Other: row 15
S
N, , -
N
S
S
S
S
Section D: Summary of Findings/Comments (Attach additional sheets if necessary)
Facility is being operated in accordance with NPDES Permit. Results of samples collected the day of inspection are as follows:
Effluent Characteristics
Monthly average Sample Results
BOD
30.0 mg/I 4.5 mg/I
Total suspended Solids
30.0 mg/I 2.0 mg/I
Fecal Coliform
200/100 ml <10/100 ml
Name(s) and Signature(s) of Inspector(s)
Agency/Office/Telephone
Date
ROGER C. EDWARDS
DEM/ARO 704-251-6208
S' of Vviewar
Agency/Office
Date
DEM/ARO 704-251-6208
115�5—
a
Regulatory Office Use Only
Action Taken
Date
Compliance Status
❑ Noncompliance
compliance

i -
February.l5, 1994
Mr. Roger C_ Edwards
Wastewater Consultant
Dept. of Environment,
59 Woodfin Place
Asheville, NC 28801
Dear Mr. Edwards:
Health & Natural Resources
P.O. Box 159
Caroleen, North Carolina 28019
On January 14,- 1995, the 2nd. Broad River rose 10 to 12 feet above its
banks and flooded the chaste treatment -plant at the Galey & Lord
Caroleen Plant. The septic tank, sand filter bed, and. chlorine
contact chamber 'were all flooded, and when the waters receded enough
that we could get to the plant, all tanks had large amounts of silt in
them. It took four days to get the plant back in operation.
The sand filter had varying levels of silt so -the silt and 4" of sand
were removed. New sand was put back and leveled. The septic tank
water chamber, where the pumps are located, was pumped clean of --all
silt and pumps were put.back in operation. The -chlorine contac•c
chamber was pumped clean of silt and put back in operation.
Enclosed is a copy of the first lab report after the flood_ As you
can see,'all parameters are well within limits_
If you would like to visit to check the plant, please give us a call
at 704 657-6376 or drop in if you are.in the area_
Sincerely,' -
Steve Meador
Plant Manager
W.
Enclosure
ake Wilson
Plant Engineer

I N C O R P O R A T E D
d�jace.,
THE ASSURANCE OF QUALITY
Galey & Lord (Formerly Burlington Ind)
PO Box 158
Caroleen, NC 28019
Attn: Mr. Jake Wilson
Client Reference: Monthly Monitoring
PACE Sample Number:
Date Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
REPORT OF LABORATORY ANALYSIS
Units MDL
February 01, 1995
PACE Project Number: A50124509
93 0056547
O1/24/95
01/24[95
Effluent
Bacteria, Fecal Coliform col/100ml 10 <10
Biochemical. Oxygen Demand, 05 Day mg/L 2.0 13
Solids, Total Suspended mg/L 1 4.0
These data have been reviewed and are approved for release.
&AWm- mt&
Barbara M. Miller
Supervisor, Inorganic Chemistry
0
Sherry L. Ratzlaff
Supervisor, Bioassay Department
54 Ravenscroft Drive An Equal Opportunity Employer
Asheville, NC 28801
TEL:[phone]
FAX:[phone]

State of North Carolir a'
Department of Environment,
Health and Natural Resources
ivision of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
James
Preston Howard, Jr., P.E., Director
January 17, 1994
Attn: Ralph Gibson
Galey And Lord Industries
P.O. Box 35528
Greensboro, NC 27425
-.r
Subject: Units Of Measurement on DMRs
Galey And Lord Industries
NPDES No.: NC0006009
[Rutherford -County
Dear Mr. Gibson:
Recent submittals of Discharge Monitoring Reports (DMRs) from the subject facility have shown
values for total residual chlorine reported in micrograms per liter (ug1l). These reported values are well
below -the current detection limit for this parameter and inconsistent with values previously reported by the
facility in milligrams per liter (mg/1). The Division's recent modification of DMRs included a change in the
printed units of measurement for total residual chlorine from mg/l to ug/l. It is believed the facility is
continuing to report mg/1 results for this parameter, but listing those results as ug/l values.
Total residual chlorine is not a limited parameter in this NPDES permit and results of its monitoring
may be reported using units of measurement of either mg/l or ug/l. If you wish to continue to report total
residual chlorine values in mg/l, clearly mark through the ug/l units on the Division's pre-printed MR-1
form and write "mg/l" above that space. If you wish to report in ug/l, testing results in mg/l may be
converted from mg/1 to ug/l by multiplying the value in mg/l by 1000. Once a decision has been made as
to which units of measurement will be used, it is requested the facility remain consistent in its reporting
practice. Submitting reports which include correct units of measurement helps ensure efficient computer
data entry and compliance evaluation.
Please make this change in reporting as soon as possible. Facilities which submit DMRs
exhibiting incorrect units of measurement are subject to the issuance of a Notice of Violation.
If you have any questions about this
contact Mr. Shannon Langley at (919) 733-
cc: Compliance/Enforcement
CRegional_Office _-_ � �5�,�
Central Files '
or any other questions concerning DMRs, please
'tension 581.
1V Sincerely,
0,15
���Robert L. Sledge, Supery or
K Compliance Group
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIEL -LAB FORM (DM1)
COUNTY WUql PRIORITY / SAMPLE TYPE
RIVER BASIN kPoWD 0
❑AMBIENT QA ❑ STREAM E EFFLUENT ✓ '
REPORT TO: RO FRO MRO RHO WaRO W[RO WSRO TS ❑
AT BM ❑ COMPLIANCE ❑ CHAIN ❑ LAKE ❑ INFLUENT
Other OF CUSTODY
Shipped by: Bus Courier Staff Other EMERGENCY ❑ESTUARY
COLLECTOR(S): 4S?2 ` �
Estimated BOD Range 0=5 5-25/25-65/40-130 or 100 plus STATION LOCATION:
Seed: Yes No El Chlorinated: Yes No ❑ REMARKS:
Station Date Begin (yy/mm/dd) Time Begin Date End Time End Depth DM DB DBM Val
9.5' , ©I 95,01 , 17-
1
OD5 310 t/ S mg/1
1
w 2
COD High 340 mg/1
^3
COD Low 335 mg/I
4
Coliform: MF Fecal 31616 /100ml
5
Coliform: MF Total 31504 /100ml
6
Coliform: Tube Fecal 31615 /100ml
7
Coliform: Fecal Strep 31673 /100ml
8
Residue: Total 500 mg/I
9
Volatile 505 mg/I
10
Fixed 510 mg/I
11
esidue: Suspended 530 mg/I
12
Volatile 535 mg/I
13
Fixed 540 mg/I
14
pH 403 units
15
Acidity to pH 4.5 436 mg/I
— -16
i
Acidity to pH 8.3 435 mg/I
_
Alkalinity to pH 8.3 415 mg/I
18
Alkalinity to pH 4.5 410 mg/1
19
TOC 680 mg/I
20
Turbidity 76 NTU
Chloride 940 mg/I
Chi a: Tri 32217 ug/1
Chi a: Corr 32209 ug/I
Pheophytin a 32213 ug/1
Color: True 80 Pt -Co
Color:(pH ) 83 ADM[
Color: pH 7.6 82 ADMI
Cyanide 720 mg/1
Fluoride 951 mg/l
Formaldehyde 71880 mg/1
Grease and Oils 556 mg/I
Hardness Total900 mg/I
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/l
Phenols 32730 ug/I
Sulfate 945 mgA
Sulfide 745 mg/I
Fnr Lah riaa r)Nr V
Lab Number: SS
Date Received: Time: 3 ' 3 O
Rec'd by: From: Bus-Couri -Hand Del
DATA ENTRY BY: CK: 1',%A;—
DATE REPORTED:
A H L
NH3 as N 610 mgA
TKN as N 625 mg/1
NO2 plus NO3 as N 630 mgA
P: Total as P 665 mg/1
PO4 as P 70507 mgA
P: Dissolved as P 666 mgA
CdCadmium 1027 ugA
Cr-Chromium.Total1034 ugA
Cu-Copper 1042 ug/1
Ni-Nickel 1067 ug/1
Pb-Land 1051 ug/I
Zn-Zinc 1092 ug/1
Ag- ilver 1077 ug/1
Al -Aluminum 1105 ug/I
Be -Beryllium 1012 ug/I
Ca -Calcium 916 mgA
Co -Cobalt 1037 ug/1
Fe -Iron 1045 ugA
Composite Sample T
T S B C r GNXX
Li -Lithium 1132 ug/l
Mg -Magnesium 927 mg/I
Mn-Manganese 1055 ug/I
Na-Sodium 929 mg/1
Arsenic:Total 1002 ug/l
Se-Selenlum 1147 ug/l
Hg-Mercury 71900 ug/l
Organochlorine Pesticides
Organophosphorus Pesticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoplankton
Sampling Point.%
Conductance at 25 C
Water Temperature (C)
D.O. mg/1
pH
Alkalinity
Acidity
Air Temperature (C)
pH 8.3 pH 4.5
pH 4.5 pH 8.3
2
94
10
300 1.
400 1•
82244 1431
82243 182242
20
Salinity %
Precipition On/day)
Cloud Cover %
Wind Direction (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
[eanStream Depth ft.
Stream Width ft.
480
45
32
36
1351
1350
35
4
4
DMI/Revised 10/86

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
Nann B. Guthrie, Regional Manager
Asheville Regional Office
MEMORANDUM
ATRA
40
EDEHNF=?k
WATER QUALITY SECTION
October 28, 1994
TO: Jay Lucas, Permits and Engineering Unit
THROUGH: Forrest R. We to O Regional Water Quality
Supervisor
p��J
FROM: ` Roger Edwards, Wastewater Consultant
SUBJECT: Galey & Lord flow increase to'treatment facility
�A
I do see any problem with the addition of 500 gallons per
day to the treatment facility, providing that it contains no
algicide or biocide.
Interchange Building, 59 Woodfin Place, Asheville, N.C. 28801 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
August 4, 1994
Attn: Ralph Gibson
Galey And Lord Industries
P.O. Box 35528
Greensboro, NC 27425
�.l 0
[D E F1
Subject: Units Of Measurement on DMRs
Galey And Lord Industries
NPDES No.: NC0006009
.Rsurhetfofc_Coun� ,yam
Dear Mr. Gibson:
J
Recent submittals of Discharge Monitoring Reports (DMRs) from the subject facility have shown
values for total residual chlorine reported in micrograms per liter (ug/1). These reported values are well
below the current detection limit for this parameter and inconsistent with values previously reported by the.
facility in milligrams per liter (mg/1). The Division's recent modification of DMRs included a change in the
printed units of measurement for total residual chlorine from mg/l to ug/l. It is believed the facility is
continuing to report mg/1 results for this parameter, but listing those results as ug/l values.
Total residual chlorine is not a limited parameter in this NPDES permit. and results of its monitoring
may be reported using units of measurement of either mg/1 or ug/l. If you wish -to continue to report total
residual chlorine values in mg/l, clearly mark through the ug/l units on the Division's pre-printed MR-1
form and write "mg/l" above that space. If you wish to report in ug/l, testing results in mg/1 may be
converted from mg/l to ug/l by multiplying the value in mg/l by 1000. Once a decision -has been made as
to which units of measurement will be used, it is requested the facility remain consistent in its reporting
practice. Submitting reports which include correct units of measurement helps ensure efficient computer
data entry and compliance evaluation.
Please make this change in reporting as soon as possible. Facilities which submit DMRs
exhibiting incorrect units,of measurement are subject to. the issuance of a Notice of Violation.
If you have any questions about this matter or any other questions concerning DMRs, please
contact Mr. Shannon Langley at [phone], extension 581.
cc:
SReg-oRa_O_f: cei
Central Files
ON
Sincerely,
SIVII �1�
Dianne Williams Wilburn, Supervisor
Compliance Group
P.O. Box 29535, Raleigh, North Carolina 27626=0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

16:20 FROM DEM WATER QUALITY SECTION TO
ARO P.02/02
October 4, 1994
North Carolina Department of
Environment, Health and Natural Resources
Division of Environmental Management
P. 0. Box 29536
Raleigh, NC 27626-0535
Attention: Mr. David Goodrich
Subject: Plant Modernization
Galey & Lord Industries, Inc.
Caroleen Plant
Caroleen, NC
NPOES Permit #NC0006O09
Dear Nr. Goodrich:
P. 0. Box 35526
Greensboro, North Carolina 2742"528
VAIOt/
f v
w
Attempted several times earlier today to contract you by telephone and
was not successful. Galey & Lord is planning to modernize the Caroleen
Plant during the next two (2) years. This project will impact the
wastewater discharge only minimally due to cooling water over -flow from
air compressor cooling towers (not to exceed 500 gal/day).
If required, we will request permit revision.
Please acknowledge receipt of this letter by Fax (Fax #[phone]).
Should you have questions, please call me at telephone [phone].
Your early response to this request and continuing assistance is
appreciated.
Sincerely yours,
GALEY & LORD INDUSTRIES, INC.
Ralph M. Gibson
Director of Engineering
CC: M. Harmon - G&L/Greensboro
1869�
TOTAL P.A?

urlin on Industries, 1 c.
U May 3, 1994
Mr. David Goodrich
North Carolina Department of'Etvironment,
Health and Natural Resources
Division of Environmental Management
P. 0. Box 29535
Raleigh, NC 27626-0535
Re: NPDES Permit No. NC0006009
Caroleen Plant
Burlington Industries° Inc.
Caroleen, NC
Rutherford County
Dear Mr. Goodrich:
Executive Offices
P. 0. Box 21207
Greensboro, North Carolina 27420
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
This is to advise you that effective April 29, 1994, Burlington
Industries,Inc. has sold the Caroleen Plant to:
Galey & Lord Industries, Inc.
P. 0. Box 35528
Greensboro, NC 27425-0528
By copy of this letter, Burlington Industries, Inc. is notifying Galey &
Lord Industries, Inc. that the existing permit to operate this waste
treatment facility is non -transferable and must be reissued by your
office to the new owner. Burlington Industries, Inc. will assist the new
owner in requesting the new permit, and you can expect to hear from them
i-n the near future.
If you have any questions in regard to this change, please contact me at
910-379-2943.
Very truly yours,
BURLINGTON INDUSTRIES, C
Theodore H. LeJeune
Engineering Manage
Environmental Systems
THL/ j w
FT
WATER FUALITY SECTION
AStIEVILL REGIONAL OFFICE

cc: i�Mr.__J-ames—R—Reid =°
NC DEHNR
Water Quality Section
59 Woodfin Avenue
Asheville, NC 28801
Mr. Charles A. Blalock
Executive V.P. Manufacturing
Galey & Lord Industries, Inc.
P. 0. Box 35528
Greensboro, -NC 27425-0528
Telephone: [phone]
R. Gibson - Galey-& Lord
J. Wilson - Caroleen
B. Hatcher - 3330/T-5
File

1994 11e36 FROM C-nD^[_EEN—GALEV&LORD
,Y 1
,
k akjdo
e
May 6,1994
North Carolina De artme�nt of
Environment, Health and
Natural Resources
Division of Environmental Management
P. 0. Box 29535
Raleigh, NC 27626-053.5
Attention: Mr. David Goodrich
Subject: Change of Ownership
Re -Issuance of Permit
NPDES Permit No. NCO006009
Galey & Lord Industries, Inc.
Caroleen Plant
Rutherford County
Dear Mr. Goodrich:
TO 807 s 51645250607278
P. O. Box 35528
Greensboro, North Carolina 27425`OM
Gale & Lord Industries, Inc. became the new owner of the subject former
Burlington Industries Plant on April 30,1994 and as such intenSs to operate the
'aroleen Plant in the saute manner and subject to the same permit lmutations as
required by the existing permit.
Therefore, I am requesting that subject permit be issued to-
Galey & Lord Industries, Inc.
Caroleen Pbmt
P. Q. Box 158
U.S. Hwy 221A
Caroleen, NC 28019
I have enclosed a permit processing fee of One -Humored Dollars ($100.00).
If you have questions or require additional information; please contact Ralph
Gibson at telephone [phone].
G

/1994 11:36 FROM C^'^'-EEN-GRLEY&LORD
Pa a Two
5/9/94
Letter: D. Goodrich
1
Please send. all pe= dts to:
Ralph M. Gibson
Director of E eeri%
Galey & Lord dustr�ies, Inc.
P.O. Box 35528
Greensboro, NC 27425-0528
Sincerely,
GALEX & LORD INDUSTRIES, INC.
Charles A. Blalock
Executive Vice -President,
Manufacturing
cc: R. Gibson - G&L/Greensboro
M. Harmon - G&L/Greensboro
S. Meador - G&L/Caroleen
J. Wilson - G&L/Caroleen
J. Stuart G&L/Greensboro
Permit File
Enclosure:
TO 807�7-""h51645250607278 P.05
r