HomeMy WebLinkAboutNCG080583_2020 DMR_20210119 (2)aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
September 08, 2020
Mr. Michael DeBraske
Schneider National, Inc.
PO Box 2545
Green Bay, WI 543062545
RE: Project: SNI-Charlotte, NC
Pace Project No.: 92492195
Dear Mr. DeBraske:
Enclosed are the analytical results for sample(s) received by the laboratory on August 24, 2020. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
nicole.gasiorowski@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Mr. Michael DeBraske, GEI Consultants, Inc.
Derek Townsend, Schneider National
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 11
aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 11
aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92492195001
SP-1
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
92492195002
SP-3
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
92492195003
SP-4
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
92492195004
SP-5
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
92492195005
SP-6
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
92492195006
SP-7
EPA 1664B
HH
1
PASI-C
SM 2540D-2011
RED
1
PASI-A
EPA 9040C
SMK
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 11
aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
Sample: SP-1
Lab ID: 92492195001 Collected:
08/21/20 12:35
Received:
08/24/20 13:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
09/08/20 08:54
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Asheville
Total Suspended Solids
15.9 mg/L
2.5
1
08/27/20 19:44
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
4.4 Std. Units
0.10
1
08/30/20 12:38 H3
Sample: SP-3
Lab ID: 92492195002 Collected:
08/21/20 12:45
Received:
08/24/20 13:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
5.4 mg/L
5.0
1
09/08/20 08:55
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
101 mg/L
11.1
1
08/27/20 19:44
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.1 Std. Units
0.10
1
08/30/20 12:49 H3
Sample: SP-4
Lab ID: 92492195003 Collected:
08/21/20 13:00
Received:
08/24/20 13:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
09/08/20 08:55
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
774 mg/L
50.0
1
08/27/20 19:46
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.3 Std. Units
0.10
1
08/30/20 12:55 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 11
aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
Sample: SP-5
Lab ID: 92492195004 Collected:
08/21/20 13:15
Received:
08/24/20 13:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
09/08/20 08:55
2540D Total Suspended Solids
Analytical Method: SM 2540D-2011
Pace Analytical Services - Asheville
Total Suspended Solids
128 mg/L
12.5
1
08/27/20 19:46
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
5.0 Std. Units
0.10
1
08/30/20 13:01 H3
Sample: SP-6
Lab ID: 92492195005 Collected:
08/21/20 13:30
Received:
08/24/20 13:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
09/08/20 08:56
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
230 mg/L
25.0
1
08/27/20 19:48
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.2 Std. Units
0.10
1
08/30/20 13:07 H3
Sample: SP-7
Lab ID: 92492195006 Collected:
08/21/20 13:45
Received:
08/24/20 13:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
Oil and Grease
ND mg/L
5.0
1
09/08/20 08:56
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Pace Analytical Services - Asheville
Total Suspended Solids
57.2 mg/L
10.0
1
08/27/20 19:49
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
5.9 Std. Units
0.10
1
08/30/20 13:12 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 11
aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
QC Batch: 564879 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006
METHOD BLANK: 2994150 Matrix: Water
Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 09/08/20 08:48
LABORATORY CONTROL SAMPLE:
2994151
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 39.3
98
78-114
MATRIX SPIKE SAMPLE:
2994152
35573607001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
<1.3 40
16.3
40
78-114 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 11
aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
QC Batch: 562905 Analysis Method: SM 2540D-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006
METHOD BLANK: 2985122
Matrix:
Water
Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5
08/27/20 19:32
LABORATORY CONTROL SAMPLE:
2985123
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
236
94 90-110
SAMPLE DUPLICATE: 2985124
92492230001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 220 224 2
SAMPLE DUPLICATE: 2985125
92491919001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 1950 1980 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 11
aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
QC Batch: 563307 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006
SAMPLE DUPLICATE: 2986843
92493044001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.3 6.3 1 H3
SAMPLE DUPLICATE: 2986844
92492422001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.7 6.7 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 11
aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALIFIERS
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 11
aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SNI-Charlotte, NC
Pace Project No.: 92492195
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92492195001
SP-1
EPA 1664B
564879
92492195002
SP-3
EPA1664B
564879
92492195003
SP-4
EPA1664B
564879
92492195004
SP-5
EPA1664B
564879
92492195005
SP-6
EPA1664B
564879
92492195006
SP-7
EPA1664B
564879
92492195001
SP-1
S M 2540D-2011
562905
92492195002
SP-3
S M 2540D-2011
562905
92492195003
SP-4
S M 2540D-2011
562905
92492195004
SP-5
S M 2540D-2011
562905
92492195005
SP-6
S M 2540D-2011
562905
92492195006
SP-7
SM 2540D-2011
562905
92492195001
SP-1
EPA 9040C
563307
92492195002
SP-3
EPA 9040C
563307
92492195003
SP-4
EPA 9040C
563307
92492195004
SP-5
EPA 9040C
563307
92492195005
SP-6
EPA 9040C
563307
92492195006
SP-7
EPA 9040C
563307
Date: 09/08/2020 03:59 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 10 of 11
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Page 11 of 1