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HomeMy WebLinkAboutNCG080583_2020 DMR_20210119 (2)aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 September 08, 2020 Mr. Michael DeBraske Schneider National, Inc. PO Box 2545 Green Bay, WI 543062545 RE: Project: SNI-Charlotte, NC Pace Project No.: 92492195 Dear Mr. DeBraske: Enclosed are the analytical results for sample(s) received by the laboratory on August 24, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Michael DeBraske, GEI Consultants, Inc. Derek Townsend, Schneider National REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 11 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SNI-Charlotte, NC Pace Project No.: 92492195 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 11 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: SNI-Charlotte, NC Pace Project No.: 92492195 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92492195001 SP-1 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A 92492195002 SP-3 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A 92492195003 SP-4 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A 92492195004 SP-5 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A 92492195005 SP-6 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A 92492195006 SP-7 EPA 1664B HH 1 PASI-C SM 2540D-2011 RED 1 PASI-A EPA 9040C SMK 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 11 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SNI-Charlotte, NC Pace Project No.: 92492195 Sample: SP-1 Lab ID: 92492195001 Collected: 08/21/20 12:35 Received: 08/24/20 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 09/08/20 08:54 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 15.9 mg/L 2.5 1 08/27/20 19:44 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 4.4 Std. Units 0.10 1 08/30/20 12:38 H3 Sample: SP-3 Lab ID: 92492195002 Collected: 08/21/20 12:45 Received: 08/24/20 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease 5.4 mg/L 5.0 1 09/08/20 08:55 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 101 mg/L 11.1 1 08/27/20 19:44 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.1 Std. Units 0.10 1 08/30/20 12:49 H3 Sample: SP-4 Lab ID: 92492195003 Collected: 08/21/20 13:00 Received: 08/24/20 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 09/08/20 08:55 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 774 mg/L 50.0 1 08/27/20 19:46 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.3 Std. Units 0.10 1 08/30/20 12:55 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 11 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SNI-Charlotte, NC Pace Project No.: 92492195 Sample: SP-5 Lab ID: 92492195004 Collected: 08/21/20 13:15 Received: 08/24/20 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 09/08/20 08:55 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 128 mg/L 12.5 1 08/27/20 19:46 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 5.0 Std. Units 0.10 1 08/30/20 13:01 H3 Sample: SP-6 Lab ID: 92492195005 Collected: 08/21/20 13:30 Received: 08/24/20 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 09/08/20 08:56 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 230 mg/L 25.0 1 08/27/20 19:48 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.2 Std. Units 0.10 1 08/30/20 13:07 H3 Sample: SP-7 Lab ID: 92492195006 Collected: 08/21/20 13:45 Received: 08/24/20 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 09/08/20 08:56 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 57.2 mg/L 10.0 1 08/27/20 19:49 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 5.9 Std. Units 0.10 1 08/30/20 13:12 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 11 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SNI-Charlotte, NC Pace Project No.: 92492195 QC Batch: 564879 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006 METHOD BLANK: 2994150 Matrix: Water Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 09/08/20 08:48 LABORATORY CONTROL SAMPLE: 2994151 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 39.3 98 78-114 MATRIX SPIKE SAMPLE: 2994152 35573607001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L <1.3 40 16.3 40 78-114 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 11 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SNI-Charlotte, NC Pace Project No.: 92492195 QC Batch: 562905 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006 METHOD BLANK: 2985122 Matrix: Water Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/27/20 19:32 LABORATORY CONTROL SAMPLE: 2985123 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 236 94 90-110 SAMPLE DUPLICATE: 2985124 92492230001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 220 224 2 SAMPLE DUPLICATE: 2985125 92491919001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1950 1980 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 11 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SNI-Charlotte, NC Pace Project No.: 92492195 QC Batch: 563307 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92492195001, 92492195002, 92492195003, 92492195004, 92492195005, 92492195006 SAMPLE DUPLICATE: 2986843 92493044001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.3 6.3 1 H3 SAMPLE DUPLICATE: 2986844 92492422001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.7 6.7 0 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 11 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: SNI-Charlotte, NC Pace Project No.: 92492195 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/08/2020 03:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 11 aceAnalytical www.paeelabs.enm Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SNI-Charlotte, NC Pace Project No.: 92492195 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92492195001 SP-1 EPA 1664B 564879 92492195002 SP-3 EPA1664B 564879 92492195003 SP-4 EPA1664B 564879 92492195004 SP-5 EPA1664B 564879 92492195005 SP-6 EPA1664B 564879 92492195006 SP-7 EPA1664B 564879 92492195001 SP-1 S M 2540D-2011 562905 92492195002 SP-3 S M 2540D-2011 562905 92492195003 SP-4 S M 2540D-2011 562905 92492195004 SP-5 S M 2540D-2011 562905 92492195005 SP-6 S M 2540D-2011 562905 92492195006 SP-7 SM 2540D-2011 562905 92492195001 SP-1 EPA 9040C 563307 92492195002 SP-3 EPA 9040C 563307 92492195003 SP-4 EPA 9040C 563307 92492195004 SP-5 EPA 9040C 563307 92492195005 SP-6 EPA 9040C 563307 92492195006 SP-7 EPA 9040C 563307 Date: 09/08/2020 03:59 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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