NC0031038_Regional Office Historical File Pre 2018 (5)

FILE
_, sr�rr rr
ROY COOPER �
MICHAEL S. PECAN
Directoa-. Enwtranmtentat Quality
Certified Mail #7018 0360-2
Retu C i t ste
April 21, 2020
Jeff Titus, Manager Operation
Colonial Pipeline Company
PO Box 8
Pave Creek, NC 28130
SUBJECT: NOTICE OF VIOLATIONINTENT TO ASSESS CIVIL PENALTY
Tracking Number: NOV-2020-LV-0303
Permit No, NCO031.038
Charlotte Delivery Facility
Mecklenburg County
Bear Mr.Titus:
A review of the February 2020 Discharge Monitoring Report (DMR) for the subject facility revealed the
violation(s) indicated below:
Limit Exceedance Violation sL.
Sample Limit Reported
Location Parameter Date Valve Value Type of Violation
007 Effluent Turbidity (00070) 2/19/2020 50 65 Gaily Maximum Exceeded
007 Effluent Solids, Total Suspended - 2/29/2020 30 43 Monthly Average Exceeded
Concentration (CO530)
009 Effluent Solids, Total Suspended - 2/19/2020 45 110 Daily Maximum Exceeded
Concentration (CO530)
009 Effluent Turbidity (000 0) � /19/2020 _ 50 170 Daily Maximum Exceeded
009 Effluent Solids, Total Suspended 4 2/29/2020 30 55 Monthly Average Exceeded
Concentration (CO530)

A Notice of Violation/Intent to Issue Civil Penalty is being issued for the noted violation of North Carolina General
Statute (G.S.) 143-215.1 and the facility's NPDES WW Permit. Pursuant to G.S. 143-215. A, a civil penalty of
not more than twenty-five thousand dollars ( 25,000. 0) may be assessed against any person who violates or
fails to act in accordance with the terms, conditions, or requirements of any 'permit issued + pursuant to G.S.
143-215A.
If you wish to provide additional information regarding the noted violation, request technical assistance, or
discuss overall compliance please respond in writing within sixty f6C}1 business days after receipt of this Notice. A
review of your response will be considered alone with any information provided on the submitted Monitoring
Reports). You will then be notified of any civil penalties that may be assessed regarding the violations. If no
.. r , « r r r . « • r « « r r r • - • r « ,, « r
i r« *- r r r • « r «rr r
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isolations of
roblems,
l Order by
Regional
Office as soon as possible, not to exceed 24 hours, from 'first knowledge of any non-compliance at
the facility including limit violations, bypasses of, or failure of a treatment unit. A written report may
be required within 5 days if directed by Division staff. Prior notice should be given for anticipated or
potential problems due to planned maintenance activities, taking units off-line, etc.
If you have any questions concerning this matter or to apply for an SO , please contact Wes Bell of the
Mooresville Regional Office at 764-663-19.
Sincerely,
®o u icgn d by:
i
A14 d81AF27"42 ..,
W. Corey Basinger, Regional Supervisor
Water Quality Regional Operations Section
Mooresville' Regional Office
Division of Water Resources, NCDEQ
Cc: WQS Mooresville Regional Office - Enforcement File (Laserfiche)
NPDES Compliance/Enforcement Unit - Enforcement File (Laserfiche

If you have any questions concerning this muter or to apply for an SOC, please contact Wes Bell of the
Mooresville Regional Office at 663-1699.
Sincerely,
DocuSigned by:
A14C6$IAF 7'4 ...
W. Gorey Basinger-, Regional Supervisor
Water Quality Regional operations Section
Mooresville Regional Office
.Division of Water Resources, NCDEQ
Gcw: W S Mooresville Regional Office - Enforcement File (L,aserfiche)
NPDES ompli nce Enforce +ent Unit - Enforcement File (L,as r the

FILE
r � n
ROB" COOPS NORTH CAROLINA
UCIM1 S. REGAIN
"romp
''a CUIPEPPER
IntertwDirsoor
Certified Mail #'i 1i6 1370 0000 2S96 1204
Return i
August 7, 2018
Brian Smith
Colonial Pipeline Company
Past Office Box 87
Paw Creek, North Carolina 28130
SUBJECT: NOTICE OF DEFICIENCY
Tracking Number: NOD-2018-L -00 6
Permit No. NCO03103
Charlotte Delivery Facility
Mecklenburg County
Dear Mr, Smith,
review of the March 2018 Discharge Monitoring Report (DMR) for the subject facility revealed the ficiency(s
indicated below.
Limit gc i3 i l i �r a
Sample Limit Reported
Location Parameter betevalue Value Type of Deficiency
005 Effluent Turbidity (00070) /12 20 8 5o 55 Gaily Maximum Exceeded
Please be aware that non-compliance with your permit could result in enforcement action by the Division of
Water Resources for these and any additional violations of State law. The Mooresville Regional Office
encourages you to take all necessary actions to bring your facility into compliance.
:
North Carolina Department of Environmental Duality I Division of Water Resources
610 East Center Avenue, Suite 301, Mooresville, NC 28115
704-663-1699

Yt
f you should` 4ylissistbrice or would like to discuss this non-compliance situation, please
Bell of the Mooresville Regional Office at 704-663-1699.`
Sincerely,
DoiauSigned by:
F161FB69A2D8 A ...
for W. Grey Basinger, Regional Supervisor
Water Quality Regional Operations Section
Mooresville Regional Office
Division of Water Resources, NCDEQ
Cc: W S Mooresville Regional Office - Enforcement File (1_ sencce)
NPdES Compliance/Enforcement flint - Enforcement File (t.as rh lie
�Q
North Carolina Department of Environmental Quality { Division of Water Resources
610 East Center Avenue, Suite 301,`Mooresville, NC 28115
704-663-1699

J�OOPER
Governor
MICHA L S. RE+ AN
IMM Secretary
Water Resources S. IAA' ZIMMERMAN
Environmental Quality Director
September 26, 2017
Mr. Brian Smith, Operations Manager
Colonial Pipeline Company
Post Office Box 87
Paw Creek, North Carolina 28130
Subject: Compliance Evaluation Inspection
Charlotte Delivery Facility
NPDES Permit No. NCO 31038
Mecklenburg County
Dear Mr. Smith;
On September 7, 2017, Mr. Chad Broadway of the Mecklenburg County Water Quality Program
(MCWQP) conducted an inspection at the subject facility. This inspection was conducted as part of a
cooperative working agreement between Mecklenburg County and the division of Water Resources
(D )
The inspection' report should be self-explanatory; however, should you have any questions concerning
the report, please do not hesitate to contact Mr. Wes Bell of this Office at (704) 35-2192 and/or Mr.
Broadway at (70 ) 2 C -1497, or at wes.bell mcderrr. ov and chad.broadwa t mecklenbur coup n . ov.
Sincerely,
W. Corey Basinger, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NC SEC,)
Enclosure:
Inspection Report
cc: Rusty Rozzelle; MCWQP
MSC-1617 Central -Basement
State of North Carolina I Environmental Qualityl Water Resources ( Water Quality Regional Operations

FFF
United States Environmental Protection Agency Form Approved.
EPA Washington, D.C.20460 OMB No 2040-00 7
Water Compliance InspectionReport Approval expires 8-31-98
Section A: National Data system Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fac type
1IN 1 2 Ej 3 1 NC0031038 111 121 17/09/07 117 1 L�j 19 1SI 20LJ
1
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA ---Reserved------------
67 2.0 70 Lj 71 L�j 72 L 73 74 761 _Li f
Section B: Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include Entry Time/Date Permit Effective Date
POTW name and NPDES permit Number) 10:OOAM 17/09/07 16103/01
Charlotte Delivery Facility
Exit Time/Date Permit Expiration Date
754 Ienstead Cir
Paw Creek NC 28130 11:35AM 17/O9107 20106/30
Name(s) of Onsite Representatives)1Titie (s)/Phone and Fax Number(s) Other Facility Data
///
Joan W. Culbreath/tORC/704-399-52591
Name, Address of Responsible ciaifiitie/Phone and Fax Dumber
Contacted
Brian Smith,PO Box 87 Paw Creek NC 130/Operations Mtanager/703-517-3051/
No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & Maintenance Records/Reports
Self -Monitoring Program Sludge Handling Disposal Facility Site Review Efflue it/Receiving Waters
Laboratory
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Ins tors) Agency/OfftceiPhone and Fax Numbers Date
Water Quality Program Meckenburq County MRO /704-3 6M54491
Signature of Management Q A Reviewer Agency/Office/Phone and Fax Numbers Crate
W. Corey Basinger MRO W 2//704-23 -21
EPA Form 660-3 (Rev 9-94) Previous editions are obsoleI .
a
Page# 1

NPDES yrlmolday Inspection Type
31 NCO031038 1 121 17108l07 117 18 M

Permit: NCO031038 owner -Facility: Charlotte Delivery Facility
Inspection Gate: 09/07t fl17 inspection Type: Compliance Evaluation
Permit X22 N
(if the present permit expires in S months or less). Has the penmttee submitted a new DONE]
application?
Is the facility as described in the pemnit? a ® El ❑
Are there any special conditions for the permit? Q © M E]
Is access to the plant site restricted to the general public? ■ p 0 p
Is the inspector granted access to all areas for inspection? a © Q 11
Comment: The facili 's current Dermit became effective on 311/2016 and exDires on 013012020. The
Lail ins action of this facilily Aagconducted by Jbg LOecklenbura County'Water Qualify
Pro rani on 811' 112015.
The facility is as described in the ermit with bermed secondary containment dikes for the
bulk liquid storage area and appurtenant giging. an oil -water se orator that treats flow from
the manifold yard, and a retention Pgnd.
ecardl Keeping Yes Na NA NE
Are records kept and maintained as required by the permit? ■ 0 Q 11
Is all required information readily available, complete and current? a; 0 ❑ p
Are all records maintained for 3 years (lab. reg. required 5 y rs)'? ■ ; Q 0 Q
Are analytical results consistent with data reported on DMRs?' ■ ® Q 0
Is the chain -of -custody complete? ■ p p p
Dates, times and location of sampling
Name of individual performing the sampling
Results of analysis and calibration
Gates of analysis
Name of person performing analyses
Transported CiCs
Are DMRs complete: do they include all permit parameters? 0 © p p
Has the facility submitted its annual compliance report to users and DWQ? 11 D ■ p
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator ®` 0 ■ 11
on each shift?
Is the ORC visitation log available and current?
Is the QRC certified at grade equal to or higher than the facility classification? ■' p 1:1 p
Is the backup operator certified at one grade less or greater than the facility classification? ■ © C
Is a copy of the current NPD S permit available on site? ■ p Q Q
Facility has copy of previous year's Annual Report on file for review? [Q © ■ 11
Page# 3

certifications.
Rim Les
FFM
•RR •
ggrmit.
Operations & Maintenance Yes No NA
Is the plant generally clean with acceptable housekeeping? a 0 C
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable 13 0 1
Solids, pH, DO, Sludge Judge, and other that are applicable?
Page;

Permit: NCO031038 owner.Facility: Charlotte Delivery Facility
Inspection Date: 09107/2017 Inspection Type: Compliance Evaluation
AUt I
con
Flow Measurer
110
,action.
kn:.
ant - Effluent
@a t_wo, months by L§gggy
In as -needed basis t y Ed Wallace
trued to be well -kept and in gggq_
Yes No RA NE
it 6 tiow mme, u*vu for reporting, r
U U
M
U
Is flow meter calibrated annually'?
Is the flow meter operational?
El 0
■
0
(If units are separated) Does the chart recorder match the flow meter?
OOMO
Comment: The facility calculates flow bv usina the rational method and an on -site rain oauge, Quffall
#010, the manifold varts outfall, is allowed to discharge on a continuous basis and flow is
calculated at a oredetermineddgjjly Late,
Effigent Pipe
Yes No NA NE
Is right of way to the outfall properly maintained?
MOOO
Are the receiving water free of foam other than trace amounts and other debris?
MOOO
If effluent (diffuser pipes are required) are they operating property?
OONO
Comment: The facile y has nine outfalls. During the in§121ction, eight of the outfalls were not discharging
(OqtfaIls#OQ2-009). Outfall #010 (manifold and continuously
discharges and was
discharging during the inspection. The receiving waters below the oulfalls were free of foam
or other pollution indicators.
Page#
5

PAT MCCRORY
DONALD R. VAN DER VAART
Water Resources S. JAY ZIMMERMAN
ENVIRONMENTAL OUAUTY
bireclo,
March 31, 2016
Tom Guzikowski
Colonial Pipeline Company
PO Box 1624
Alpharetta, GA 30009-9934
t"A
Subject: NPDES Electronic Reporting Requirements and
Sixty Day Notice of Minor Modification of the NPDES Permit
Charlotte Delivery Facility
NPDES Permit Number: NCO031038
Dear NPDES Permittee:
The U.S. Environmental Protection Agency (EPA) recently published the National Pollutant Discharge
Elimination System (NPDES) Electronic Reporting Rule. The rule requires NPDES regulated facilities to
report information electronically, instead of filing written paper reports. The rule does not change what
information is required from facilities. It only changes the method by which information is provided (ie,,
electronic rather than paper -based).
EPA is phasing in the requirements of the rule over a 5-year period. The two phases of the rule, and their
key milestones, are:
• Phase 1— tarrtin on December 21, 2016, regulated entities that are required to submit Discharge
Monitoring Reports (DMRs) will begin submitting these reports electronically, instead of ion
paper. If you are currently reporting your DMR data electronically using eDMR, then you simply
need to continue reporting in the same way as you are now. The key change is that, starting on
December 21, 2016, electronic reporting of DMRs will be required, instead of voluntary.
• Phase 2 —Starting on December 21, 2020, regulated entities that are required to submit certain
other NPDES reports will begin submitting these reports electronically, instead of on paper.
Reports covered in the second phase include Notices of Intent to discharge in compliance with an
NPDES, general permit, Sewer overflow Bypass Event Reports, and a number of other NPDES
program reports.
For more information on EPA's NPDES Electronic Reporting Rule, visit
tt : ' www.e a. ov come Hance final -national- ollutant-dischar e-elimination-s stem_n des-
htt de .nc. ov about divisions water -resources r n des -electronic -re ortin or contact Vanessa
Manuel at 919-807-6392 or via email at Vanessa.Manuitl ncdenr.�ov.
State ofNotth Carolina I Environmental Quality I Water Resources
1611 Mail service Center I Raleigh, North Carolina 27699-1611
- - - - - - - - - -

Sixty' Notice of Minor Modification of the Subject NPDES Permit
• i
- • • •- • • • • -r • .• it • •
Sincerely,
J 0. , a4'
forS Jay Zimmerman, P.C.
i
Enclosure: NPIDES Permit Standard Conditions Part III - Addendum
I
Cc: NPDES Pile
Central Files
i#ie Regi nal�Office / Water Quality Program' l
I

Certified Mail # 7015 i1520 000283761817
agyra RggSipt, gnu—eAW
March 16, 2016
Tom 3 Guzikowsld
Colonial Pipeline Company
PO Box 162
Alpharetta, GA 30009-9934
SUBJECT: NOTICE OF VIOLATION & INTENT TO ASSESS CIVIL PENALTY
Tracking Number: NOV-2016-L.V-0138
Permit, No. NCO031038
Charlotte Delivery' Facility
Mecklenburg County
Dear Permittee.
A review of the November 2015 Discharge Monitoring Report (DMR) for the subject facility revealed the
violation(s) indicated below:
L.Irnit pLcMdaLigg Viola "on si
Sample Limit Reported
Location Parameter hate Value Value Type of Violation
"v.3vf 111,1/4va.a I.s� �4-1 c.+aafay -rc
10) 11/3/2015 11 720 Daily M<
in a coma ce wim me berms;' conamons, or r quire'in i mb ui di ty Pt-1 i r sac lz>z . CU PUI ,)UGI tL av %J-1.
State of North Carolina I Enviromnental QualitY j Grater Resources
610 East Center Avenue, Suite 301, Mooresville, NC 28115
704-663-109

If you wish to provide additional information regarding the noted Violation, request technical assis
assessment may be prepared.
potential problems due to planned maintenance activities, taking units off-line, etc.
Additionally and if you have not already done so, you may wish to consider registering to use the Division's new
e-DMR system for the completion and electronic submittal of monthly Discharge Monitoring Reports (DMRs).
For more information, please visit the eDMR Website at the following address:
http:I/Dortal.ncdenr.ora/web LwglqdMinLbgglipu/­edmr.
If you have any questions concerning this matter or to apply for an SOC, please contact Roberto Scheller of
the Mooresville Regional Office at 704-663-1699.
Sincerely,
W. Corey Basinger, Regional Supervisor
Water Quality Regional Operations Section
Mooresville Regional Office
Division of Water Resources, NCDEQ
Cc: WQS Mooresville Regional Office - Enforcement File
NPDES Compliance/Enforcement Unit - Enforcement File
State of North Carolina I Enviromnernal Quality I Water Resources
610 East Center Avenue, Suite 30 1, Mooresville, NC 28115
704-663-1699

Fs
®r- PAT MCCRORY
DONALD R. VAN DER VAART
Secretary
Ware rResources
ENVIRONMENTAL QUALITY .JAY ZIMMERMAN
Director
November 30, 2015
CERTIFIED MAIL #7015 1520 0002 8376 1152
RETURN RECEIPT REQUESTED
Mr. Michael N. Cutting, Operations Manager
Colonial Pipeline Company
Post Office Box 87
Charlotte, NC 28130
Subject: Notice of Deficiency (NOD)
Tracking Number NOD- 2015-LV-0154
Colonial Pipeline Company - Charlotte Delivery Facility
NPDES Permit NCO031038
Mecklenburg County
Dear Mr, Cutting:
A review of the August 2015 self -monitoring report for the subject facility revealed violations of the
following parameter at Outfall 007:
Date Parameter Reported Value Permit Limit
8/19/2015 Solids Total Suspended 51 mgA 45 mgA (Daily Maximum)
Sbc, please do . not hesitate to c*ontat Roberto* Schaller or myself at [phone],
Sincerely,
jL, Michael L. Parker, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ
cc: Wastewater Branch
MSC 1617 - Central Files Basement
RLS
State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Officel 610 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115
7046631699

.. PAT MCCRORY
t rzvrrr
DONALD RR VAN DER V ART
at. i
QU011ty
November 5, 2015
. Michael Cutting, Operations Manager
Colonial pipeline
P.O. Box 87
Par Creek, NC 28130
Subject: ' Compliance Evaluation Inspection
Colonial Pipeline
NPDES Permit No. NC ' 10207
Mecklenburg County
Dear Mr. Cutting.
Enclosed is a copy of the Compliance Evaluation Inspection for the inspection conducted at
the subject facility on November 3, 2015 by Mr. Ori Tuvia. Your representative John Cul reach
cooperation during the site visit was much; appreciated. Please advise the staff involved with this
DES Permit by forwarding a copy of the enclosed report.
The report should be self-explanatory; however, should you have any questions concerning
this report, please do not hesitate to contact Ori 'Tuvia at (7 4) 23 -2190, or at ori.tuvia cuncdenr. ov.
Sincerely,
Michael L. Parker, Regional Supervisor
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, DE
Enclosure:
Inspection Report
cc; MSC 1 17-Central Files/Basement
Mecklenburg County Health Department
Mooresville Regional Office
Location: 610 East ConterAve., Suite 301 Mooresville, NC 28115
Phone: (704) 663 `1699 \ Fax: [phone] \ Customer`Senrice: 1- 77.623- 748
Internet, www.ncwaterquaiityrorg

United Mates Environmental Protection Agency Form Approved.EPA Washington, D.C. 2C460 OMB No: 2040-0057
Water Compliance Inspection Report Approval expires 6-31-96
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/molday Inspection Type Inspector Fac Type
t
�N i5 1 3 NC 510207 Ill 12 15/11/03 �17 18 I r� l 19 �
21 t r 0
Inspection Work Days Facility elf -Monitoring Evaluation Rating B1 ��QA
67 1.0 7t0 1 71 � 72 ! N 73 74 7Ill � 80
Section B: Facility data
Name and Location of Facility Inspected (For Industrial Users discharging to POTW, also include Entry Time/Date Permit Effective Date
POTW name and NPDES oermit Number)
09:10A 15f11103 11110f12
Charlotte Delivery Facility
7524 Kenstead Cir Exit Time/Date Permit Expiration Date
Paw Creek NC 26130
10ASAM 15/11/03 16109/30
Name(s) of Onsite Representative(s)1Tities(s)1Phone and Fax Numbe ($) Other Facility Data
H/
John W. Cubreath1004-399-9525 i7043999029
Name, Address of Responsible OficiaUlitleiPhone and Fax Number
Contacted
Faron Dale Geigh,411 Gallimore Dairy Rd Greensboro NC
740997 61Environmental13 6-669-790 13 639 6462 No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
in Permit 0 Flow Measurement Operations & MaintenancE Records/Reports
10 Self -Monitoring Program 11 Sludge Handling Disposal Facility Site review Eftluent(Receiving Waters
In Laboratory
Section D}, Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of inspector(s) Agency/Office/Phone and Fax Numbers Date
On A Tuvia MRO WO11704-663.1699t
Signature of Man ement Q A Reviewer Agency/Office/Phone and Fax Numbers crate
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page# 1

NPDES yrtmotday Inspection Type
31 NG 510207 11 121 15/11/03 17 18 L +
Page##

Permit: NCG510207 Owner -Facility: Charlotte Delivery Facility
Inspection Date: 11/0312015 Inspection Type: Compliance Evaluation
C} erations & Maintenance Yes No NA N
Is the plant generally clean with acceptable housekeeping? 10 ❑ 0 ❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable
Solids, pH, DO, Sludge .fudge, and other that are applicable?
Comment: The facilitv and site aDoeared well operated and maintained. The facilitv and oufifalis are
visually insl2ected bv Colonial Pirleline riersonnel to ensure Drooer operation and safetv
Permit Yes hto i NA hLE
(If the present permit expires in 6 months or less). Has the per ittee submitted a new 0 13 11 ❑
application
Is the facility as described in the permit? 0 ❑ 0 0
Are there any special conditions for the permit? E3 0 El (El
Is access to the plant site restricted to the general public? IM 0
Is the inspector granted access to all areas for inspection E3 [3 C3
Comment;
Record Keeping Yes No NA N
Are records kept and maintained as rewired by the permit? 0 ❑ 11❑
Is all required information readily available, complete and current? M (l El 1:3
Are all records maintained for 3 years (lab. reg, required a years)? 0 d Q E3
Are analytical results consistent with data reported on DMRs? a l 1 Q
Is the chain -of -custody complete? 9 Q E C3
Dates, times and location of sampling 11
Name of individual performing the sampling 11
Results of analysis and calibration IN
Dates of analysis In
Name of person performing analyses
Transported COCs
Are DMRs complete: do they include all permit parameters? IN ® 1:1 13
Has the facility submitted its annual compliance report to users and DWQ? 1:1 13 11 El
(if the facility is = or > b MGD permitted flow) Do they operate'24/7 with a certified operator [ [�
on each shift?
Is the QRC visitation log available and current? D C 01 Q
Is the ORC certified at grade equal to or higher than the facility classification? 0 p
Is the backup operator certified at one grade less or greater than the facility classification? Q 0
Is a copy of the current NPD S permit available on site? 11 13 1 13
Page#

Permit: NCG510207 Owner - Facility: Charlotte Delivery Facility 14
Inspection Gate: 11/03/2015 inspection Type: Compliance Evaluation
Record Keeging Yes No NA NE
Facility has copy of previous year's Annual Report on file for review? 11 El N [_]
Comment: The on -site data was ,revie ed for the period of June 2612 through June 2015. Records'
re arts and Ira s were clear and well maim `ined. The f cili ene" ded the ermil limit for
lead once during the reviewed time frame dudng Aril 2013 gam lln .
Effluent Pike Yes No NA NE
Is right of way to the outfall properly maintained? 0 El 11 Q
Are the receiving water free of foam other than trace amounts and other debris? w Q
If effluent (diffuser pipes are required) are they operating properly? Q 13 11 ❑
Comment: Discharaes into tributary of Gum branch
Flow Measurement - Effluent Yes No NA NE
# Is flaw meter used for reporting? a 0 D 0
Is flow meter calibrated annually? 11 0
Is the flow meter operational? 0 El
(if units are separated) noes the chart recorder match the flow meter? [3 E]
Comment: Average flow of 50O00 Gallons J month
Laboratory Yes No NA NE
Are field parameters performed by certified personnel or laboratory? no Q Q
Are all other parameters(excluding field parameters) performed by a certified tab?
# Is the facility using a contract lab? In 0 ❑
# Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees © E
Celsius)?
Incubator (Fecal Coliform) set to 44.5 degrees Celsius+/- 0.2 degrees? ❑ El M 0
Incubator (BO D) set to 20.0 degrees Celsius +/-1,0 degrees? F1 0
Comment: Prism lab i contracted
Effluent Sampling Yes No NA NE
Is composite sampling flow proportional? © o
Is sample collected below all treatment units? Cl C1 is El
Is proper volume collected? ©❑ 0 1
Is the tubing clean? ®" o110
# Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees 11
Celsius)?
Page# 4

Permit: NCG510207 Owner « Facility: Charlotte Delivery Facility
Inspection state: 11/03/ 015 Inspection Type. Compliance Evaluation
fflgent SgM21inaYes No i~ta N
Is the facility sampling performed as required by the permit (frequency, sampling type N C3 ❑ 1:1
representative)?
Comment: Facili am lea far III re Hired erimeters -exeetl limit f r lead gagegjgring reviewed time
frame
Page#

Colonial Pipeline Company
John W Culbreath Offifice 04-3 -525
Environmental Specialist Fax — 704-399-9029
Southeast District E-mail — [e-mail]
August '18, 2014 Ai, 6 9 2014
Mr. Michael L. Parker, Regional Supervisor
Water Quality Regional OperationsSection
Division of Water resources
NFhtr—Mooresville regional Office
610 Fast Center Avenue Suite 301
Mooresville, NC 2811`5
Ike. Notice of Violation (NOV) — Effluent Limitation
Tracking : NOS'- 014-La1- 33
`NPDES Permit No. NCO 31038 - Colonial Pipeline Company
Charlotte delivery Facility
Mecklenburg County
Dear lair. Parker:
Can July 23, 2014 Colonial Pipeline Company received the above referenced Notice of Violation. Colonial does not
dispute the fact that the limit was exceeded and that it was erroneously reported as being in compliance. Events
related to hour that occurred are discussed below. The purpose of this letter is to request that the above
referenced NOV be reduced to e Notice of Deficiency (N'?) based on the information included in this
correspondence,
Records were reviewed to determine why" this eceedence occurred and why it was not telephonically reported
when the analytical report was received from Prism Laboratories back in February 2014. Normally when
e ceedences have occurred in the past the lab's information management system (LI ) has flagged any
parameter that exceeded the pre -populated permit limit. The Project Manager would notify me of the exceedence
and I would make a telephonic notification to Marcia Allocco, in the NC DENT Mooresville Regional Office. In this
case the permit limit of 300 ug/I for Total Phenolic Compounds at Outfall 009 had a reported value of 350 ug1l and
the system failed to flag it. On further investigation as to why; the system failed it was discovered that Prism's
LIMS vendor had sent an upload to the lab that would enable the system to generate an auto mail to the lab's
Project Manager (P anytime a permit limit was exceeded. Prism has been upgrading their entire network and
wanted to get their upgrade in place before uploading the new notification system. This process resulted in a
lapse between the old notification system and the new upgrade. The lab has since found a temporary work
around that will flag any exceedences until the new upload is operational.
One of the services that Prism provides is to enter the lab results electronically on the Discharge Monitoring
Report (l r) and send the completed D r to me for review before submittal, In this case the Prism PM failed to
realize the exceedence when the data was entered even though the limit was pre-printed on the bottom "Monthly
Limit" roue on the DMR, My review of the DMR was not as thorough as it normally would have been due to being
preoccupied with an emergency response situation out of state at the time. All nine outfalls at the site are sampled
monthly and each one includes Total Phenolic Compounds. It is not out of the ordinary to get hits of phenolics at
multiple outfalls be it gasoline storage tank area outfalls or distillate storage tank outfallsn Because Outfall 009 is ,,
the only outfall with a limit and does not have previous exceedences for phenolics it was simply overlooked. An 40
updated DMR for February 2014 Outfall 009 showing the non-compliance box checked is aff shed
Additional investigation was conducted to determine the contributing factors into why the phenolic result occurred.
review of operational factors did not reveal any changes that would have contributed to the exceedence. The
7524 Kenstead Circle Paw Creek, NC 28130
P.O. Box 87 Paw Creek, NC 2813

page -Notice of Violation (NOV)Effluent Limitation
phenolics result from 009 the previous month (sampled eight days prier on January 30, 2014) was 51 ugll, gust
above the report limit of 50 ugrl.,
Colonial arranged to; have Retaw Engineering, a water and wastewater engineering firm in Midlothian, VA to
validate the February 7, 2014 lab report and review historical data for the site to determine if the report and
procedures were accurate. The ReTaw review discovered several factors in the lab report that lead then to
conclude that the phenolics results were not valid. Their report with attachments is included with this letter.
s stand earlier it is not unusual to see multiple phenolic hits in multiple outfalls,any given month. Within the
I eTaw reports a table of historical phenolics results dating back to January 2013.'Outfalls 002 through 006 are
gasoline storage tank containment areas. Cutfalls 007 through 009 are distillate tank storage areas, and Outfall
010/MYO is the oil/water separator outfall for the manifold piping yard drain system. It is my understanding that
phenolics compounds are included in this NPDES permit because we store and transport distillate products such
as kerosene and fuel oil. This conclusion is based on the fact that the Groundwater Remediation Permit
NCG510000 General NPDES hermit to Discharge Petroleum Contaminated Groundwater and Similar
Wastewaters establishes a 300 ugfl limit for total phenolic compounds if the contaminant is a distillate. The
general permit does not require phenolics sampling if the contaminant is gasoline.
The detection of phenolics in any of these outfalls would be an Indicator that stormwater has come into
contact with petroleum distillate at some paint prior to discharge based on the conclusion above. There have been
no releases in any of the distillate tank dike areas, ,and no distillate whatsoever stored or transported in the
gasoline tank diked areas, "There has been no evidence of storrnwater cording into contact with any petroleum
products prior to any of these detections for phenolics. There are only two explanations for why these detections
are occurring in both the distillate and gasoline storage areas" (1) The detections are from naturally occurring
phenolics possibly present in decaying algal blooms that form' in the diked areas (see attached; photos), or (2)
laboratory error. Since our investigation has determined, that these phenolics detections could be either naturally
occurring or possibly due to lab error, there is a high likelihood that the limit was not exceeded at all, Since the lab
data is in question and potentially not valid, Colonial believes that a reduction from an NOV to a NOD is warranted
in this case,
Going forward the following practices will be implemented to address this issue:
1. A DMR checklist will be completed each month before ;the DMR is submitted to verify that all results are
entered correctly and all parameters are in compliance
. Total Phenolic Compound samples for C utfall 009 will be split and sent to two separate labs along with
field blanks to determine if lab error is involved. Additional or tfall samples will also be split periodically.
This practice will take place over the next few months to determine if there are any discrepancies
between the two results.
3. FiltrexxV EnvirosoxxO with PetroloxxO, designed to increase hydrocarbon absorption will be installed
around some of the dike drains and evaluated as to whether or not they have any effect on eliminating the
phenolics detections.
Thank you for considering this request to reduce this NOV to a' Notice of Deficiency, please respond back to me
at your earliest convenience. If you have any questions or need any additional information; l can be reached 704-
399-6269 or at the letterhead address;
Si erel,
John W.
Culbreath
Environmental Specialist
Charlotte / SC area
Enclosures
Cc: > t r
Mike Cutting - Operations Manager
Colonial Pipeline Company

A
err
2903 S g cre k Circle
Midlothian, Virginia 23112
Engineering Phone: [phone] CeW (04) -2979 Fax: [phone]
GLOSAL WATER PRACTICE Website: http:/twww.retaweng.com I Email: file? retaw ng. om
August 1, 2014
Mr, John W, C ulbreath Sent Wit 1-)nail
Colonial Pipe Company
P. 0. Box 87
Paw Creek, NC: 28130
Re: Notice of Violation of Total Phenolic Compounds
NPDES No. NCO0310238 Effluent Limitation Tracking # NOV-2014-LV-03.36
Colonial Pipe Company - Charlotte rlotte elivery Facility Class 1
Dear John:
Can behalf of Apex Companies L . , IC taw Engineering has performed a review ofthe above noted
Notice of Violation (NOV) issued by the North Carolina Department of Environment and Natural
Resources on July 22, 2014. The NOV alleges an exceedance of the NPD S permit limitation of 300
pg/L for phenolics at Ourfall 009 on February 7, 2014. The NPDES permit limit for phenolics applies
only to C utfall 009 (NpDES permit — part I (1) Effluent Limitations and Monitoring Requirements,
footnote 4). The lab test results for Clutfall 009 for February 7, 2014 was 350 p &
In order to determine the merits of this NOV, we performed the following;
1. Reviewed the NPDES Permit requirements
2. Reviewed laboratory test method, test result, chain of custody and A/QC for the sample in
question
Reviewed a total of 17 monthly laboratory test results for C utfall 009 collected between
01/0 /2013 and 06/09/2014 and performed statistical analysis of these data...
4. Reviewed the storm water discharge Sampling and Analysis flan for the CPC Delivery Facility
Phenolic compounds are synthesized industrially and they also are produced by plants and
microorganisms.
Findings
1. The sample in question was collected on 02/07/14 at 1 :50 and submitted to the lab on the same day
at 17:00 hours. laboratory description of sample is summarized in Table l .
Table 1— Labo ator Identification of Sam le
Client Sarre le ID I,ab a 1e ID Matrix Lute Sam led Date Received
Sid-Ot.TF L-0 9_O /07/14_Lab 4020139-0 hater 0 /07/1A All
2; The sample temperature was 4.5 °C . Sample temperature was above the maximum allowed
temperature: of 4 °C
3. The sample was analyzed for phenolics by Prism Laboratories Inc. of 449 Springbrook Road,
Charlotte, NC 21224 using EPA method 420. l y EPA 420.1 complies with 40 CF`R fart 136 approved
method and has a minimum detection limit of 0.027 rng/L and areporting limit oft) 05 mg/1-
4. The sample was tested 11 days, 22 hours and 40 minutes later on /19/14 at 13:30:
a. According to 40 CFR fart 136, the hold time for the sample is 28 days
b." According to the method literature — Part, 4.0 "Sample Handling and Preservation, Biological
degradation is inhibited by the addition of 1 g,/L of copper sulfate to the sample and
Markets: Municipal State * Federal Industrial * commercial Developer
Services, Planning Pemtltting # Bench scale Testing Pilot -scale studiesDistribution System _ Hydraulic & Water Quality Modeling
Engineering Design Construction Administration Reuse * Plant Operations --Process Troubleshooting & Optirnitation ."Training - O&M Manuals
Applying Innovative, Sound Engineering & Scientffic Principles & Practices to Solve Your problems

Re; Notice of Violation of Total Phenolic Compounds Page 2 of 3
NPDES No. NCO03 10238 Effluent Limitation Tracking # NOV-2014-1,V-0336
Colonial Pipe Company - Charlotte Delivery Facility —Cbm I
acidification to a PH of less than 4 with phosphoric acid. The sample should be kept at 4'C
and analyzed within 24 hours after collection".
c. Standard Methods for Examination of Water and Wastewater method requires sample to be
analyzed within 4 hours unless kept at 4 OC or lower,
d. Standard Methods for Examination of Water and Wastewater method requires "Analyze
preserved and stored samples within 28 d after collection". Sample was tested about 12 days
after collection. It is not known if proper preservation were followed.
5. The test result was 0.35 mg/l, versus the NDPES discharge limit of 0.30 mg/L
6. The lab quality assurance and quality control results are summarized in Table 2 below.
Table 2 — Laborator ualit Con I Data Stumnar,
QA/QC Result Reporting Units Spike Source % %REC RPD RPD Notes
limit Result REC Limits Limits
LCS —70-55 0�05 mg/L O�5 110 80-120
Matrix Spike 0.294 0�05 mg/L 0.5 BRL 59 80-120 M
Matrix Spike Dup 005
L;70
Note M: Matrix spike outside of the control limits.
a. The accuracy of the test is indicated by the percent recovery for the Matrix spike and must be within
the 801% to 120% range or 20 above or below the actual value. Spikes deviated by more than 40%.
Therefore the results cannot be considered accurate.
b. The precision or measure of closeness of duplicate test results to each other is indicated by the
Relative Percent Difference (RPDL Precision must be below the Critical Limit of 20. The test RPD
of 5 met the precision requirements, however, this only reinforces the accuracy of the test
procedure used.
7. There are two types of errors associated with sampling, sample handling, chain of custody, laboratory
analysis and test result calculations — a. determinate errors and b. indeterrionate errors. Determinate
errors are known, controllable and traceable errors. Indeterminate errors are impossible to predict and
trace once the error has occurred. Table 3 contains historical phenolics test results for the Colonial
Pipe Company - Charlotte Delivery Facility Ourfall 009 and other existing (unpertnitted) Outfalls.
a. The phenolics test result of 0.35 ing/L appears to be an error (outlier) as it is the only one
value out of 17 samples that exceeded the NPDES limit, with 12 out of 17 results failing
below the, Reporting limit at Ourfall 009. An outlier is statistically an unlikely result should
not be considered as it could be caused by any number of potential errors.
b. The Z-score method is the most commonly used statistical methods to identify outliers in
cluster of data points. The Z-score is calculated as follows:
Z
Where, X is the value of the measured parameter, p is the parameter mean and 6 is the
standard deviation for the data parameter. If the absolute value of Z is greater than 2.2, then
the data point is justified as an outlier (Hoaglio, D,C, and lglewicz, B. (1987), Journal of
American Statistical Association, Z-score of 2.2 implies that 98.6% of all measured data
points are normal.
c. From Table 3, the calculated Z-score of 2.86 for the test result of 0.35 mg/L means that this
value lies outside 99.6% of all possible data for Outfall 009. Similarly, the test results of 0.35
mg/L lies outside 99.5% of all possible phenolics test results measured at the Colonial Pipe
Company - Charlotte Delivery Facility.

k 1
Re: Notice of Violation of Total Phenolic Compounds rage 3 of 3
f PDES No NCO0310238 Effluent Limitation Tracking # NOV-2014-LV-0336
Colonial Pipe Company. - Charlotte t livery Facility ._Class l
Table 3 — Data front J l rac t �ha Jane 9 Q
Parameter Out all 009 All Outfalls
Total number of Number of samples 17 153
Number of samples below Reporting Limit 12 121
Number of samples bel aw i ES Limit ]fa 147
Measured value„ X 035 035
Average discharge concentration for phenolics, p 0,052 OD42
Standard Deviation, or 0.1D.1109
-Score (or -value) 2.86 2.7
Recommendations:
Colonial Pipe Company should request the NC DENR to withdraw the Notice of Violation Tracking #;
NOV-20 4-L V-0336 on the following, grounds:
1. The 2/0 /2013 sample exceeded the maximum holding temperature of 4.0 "C at the time it was
received by the lab. Sample temperature was 4.5 IC as reported by the laboratory.
2. The sample was analyzed after 12 days storage. EPA methods requires that the sample should be
analyzed within 24 hours, although 40 CFR Part 136 allows a hold time of 28 clays for preserved
samplesthat are kept at or below 4 OC.
The sample test result may not be, accurate since Prism Laboratories' QA/QC test data for spikes
yield recoveries on 5 r and 56%, well below the method acceptable range of 80% to 0%.
4. The test result of 0.35 rng/L. phenolics at Outtall 009 is an outlier (or erroneous) as supported by
irrefutable statistical analysis rasing the Z-score method for outlier identification.
5. An upset occurred at the Pollution prevention plant at the time the 2/7/2014 was collected,
Colonial pipe Company may use Upset, as a deference in accordance with Fart II Standard
Conditions for i PDES Permits, Section C" subpart 5 if indeed an upset did occur and was
reported in accordance with reporting and notification requirements of the NPDES permit.
fa. CPC" should collect a sample of gasoline and test for total phenols. If phenols are absent or
present in levels lower than detected in the discharge, this could constitute a reasonable defense.
Additionally, Colonial Pipe Company should consider further investigation including site assessment by a
qualified Engineer to determine if potential exists for activities or conditions that may lead to erratic
dischargeofhigher phenolics concentrations and to develop a pollution discharge prevention plan,
f you have any question or concem, s regarding the contents of is letter, please contract the at (804) 245-
29'79 or via email at: i tigmi .mutoti(0re(a eft .ct�n�r
'"ours Truly,
1411
Ignatius March, Phil, PE
R taw Engineering
Attachments:
a; Notice of Violation letter
b. NP ES Perntit part A (I) -- Effluent Limitations ns and Monitoring Requirements
c. Laboratory test data
it, Historical data. and statistical Outlier determination
EPA Method 420.1'
f. Sampling and Analysis ]plan for Storanvater discharge

North
rat lw(;rofy jonn t:, Z>Kvana, tit
Governor Secretary
July 22, 2014
0
L7
Mr, Mike Cuffing
Operations Manager - Charlotte/SC
Colonial Pipeline Company (CPC)
P,0, Box 87
Paw Creek, North Carolina 28130
Subject: Notice of Violation — Effluent Limitation
Tracking *1 NOV-2014-LV-0336
Charlotte Delivery Facility
NPDES Permit No, NCO031038
Mecklenburg County
Dear Mr, Cutting,
A review of the February 2014 self -monitoring report for the subject facility revealed a violation of the
following parameter at Outfall 0091-
Date Parameter RegaoRrateedg. V a If ue Permit Limit
2/7114 Total phenolic compounds 350 lig/L 300 pg/L (Daily maximum)
Remedial actions. if not already imolemented, should be taken to correct the noted any nrablerns
The Division of to Resources may pursue enforcement actions for this and any additional
violations. If the violations are of a continuing nature, not related to operation and/or maintenance
problems, and you anticipate remedial construction activities, then you may wish to consider applying
for a Special Order by Consent (SOC).
If you have questions concerning this matter or to apply for a SOC, please do not hesitate to contact
Ms. Marcia Allocco or myself at [phone].
Si
ncerely„
Michael L, Parker, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
cc: Wastewater Branch
Central Files (MSC 1617-basement)
Mo,,)resv44e Regicna! Office
Loc,ation 610 East Center Ave Sufte 301 Mooresvrle. NC 28115
Phon,e �7041 6-a 1699 � Fax 004� 663-6040 \ Customer ��erwe 1-877-623,6748
intemO hftp Rpolal ncdem orq*ebq
Am ,,, QVtro„'P 1, h - I(A, e h". W': , ,

Permit NC O031d3S
A. I• EFFLUENT I I A TI "' G REQUMEMENTS
Beginning can the effective date and lasting until expiration, the Permittee is authorized to discharge from
Outfalls 002, 003, 004, 005, 00p 007, 008, 009 and 010. Such discharges shall be limited and
monitored b the Pennittee as ecified below:
FFFLUIKNT
If'C t
CRAIRACTEIUSTICS Monthly easureut S plc arraple
etei C cable] Aveiga t.t}at#a
1,500501 Flow 13pisodic Clf ations fLluent
F005301 Total Sus nded Solids 45.0 r g1L Monthly Grab Effluent
110055611 Oil and Grease Monthly thly grab Effluent`
{It1t} urbidz 50 NTU Monthly Grab Effluent
223t? Total ph ols'e C>o o ds CiCi aMonthly Grab Affluent
34 3C} e e Monthl Crab Effluent
34CI1Ct Tolu ` e Monthl Grab Effluent
l34{1 en°zene I A 9 a Monthly Grab Effluent
[340101 Toluene 11 u L Monthly Grab Effluent
34.371 I Benzene lionthl grab Effluent
81551 lene Monthl Crab Effluent
22417 MTBE 14 onthl Grab Effluent
TAE6C Acute Toxici Annually Grab Affluent
EPA Method 625 e `-a uall b � uent
footnotes
1. Flowshall be monitored with each discharge event. During periods of no flow, the Perarittee
shall submit a signed, monthly Discharge Monitoring Report R) indicating "No discharge."
Flow may be monitored using any one of four methods:
measure flow continuously;
) calculate flow [see section A. 3.) Rational.Equation] lased on total rainfall per
unit area draining to the outfall; exclude built -upon areas(best method for facilities
with large runoff -collection ponds);
e) estimate titer at 20-minute intervals during the entire discharge event, or
d) report flow based. on discharge pump lags.
. TSS/Gail and Grease'- Where passible, the grab sample for oil and grease should be skimmed from the surface
of a quiescent calm water) zone.
Turbidity .. w Effluent shall not cause receiving stream turbidity to exceed 50 NTU. If receiving stream
background turbidity exceeds Sit NTU, effluent shall notcause this background value to increase.
4 Permit limit applies to Outfall 009 only.
5. Permit limit applies to Ou fill 10 only.
5. Acute 'Toxicity (Fathead lei ow, 2 -hour" static test), annual samples to be collected concurrently with
Benzene, Toluene, Ethyl Benzene, and Xylene TE) samples [see Special Condition A,.. ,
Qcar�ditztn
a. The Permittee shall discharge no floating solids or team visible in tither than trace amounts,
b. The Permittee shall discharge no tank solids, tank bottom water, or the rag layer.
ca Gallo 'ng hydrostatic testing (tank or pipe), the Pernfiftee shall discharge no test -water without
documenting that benzene concentration do not exceed I ,19 ugh and toluene concentrations do
not exceed 11 It

NC Certification No. 402 Case Narrative
c Certification No. 99012
Futi-Service Analytical NC Drinking Water Cori No, 3773
02121f2014
Environmental Solutions VA certification No. 460211
� r 'irs rnrr
C3ota ELAR L-A-8 Accredited Certificate No, L2307
160,4Ec 17 2!r L-A-S Accredited certificate No. L2 07
Colonial Pipeline Company Project: Charlotte NPDES Stormwater
John Culbre th Project No.- NCO031038
P.C. Sox 37 Lab Submittal Crate: 02/ 7/2014
Paw Creek, NC 28130 Prism Work Girder: 4020139
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. finless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods:
Data qualifiers are flagged individually; on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical" report.
Respectfully,
PRISMTO IES, INC.
tobbi A. Jones Reviewed By Rabbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers KeyReference:
Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All outer results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, vvithout the written consent of Prism Laboratories, Inc.
6 Springbrook Road - P.O. Box 2 0 R Charlatto, No 20224
Phone: [phone] - Toll Free Nurnber1 01 -a - Fox. 626.040

Sample Receipt Summary
t FGRi Service Anafytieal
�z to AT .fl 4[dG
Prism Work Order. 4020139
Client Sample ID
Legs Sample ID
matrix
Date Sampled
gate Ra et e+d
SW-OUTFALL- LO2/07/14-Lab
02 -0
Water
/07/1
02/07/14
W-OUT LL 9_02/07d Q Lab
4020139-02
Water
02/07/14
02107/1
SW U'TFALL-007_02/07/1 Lab
4020139-03
Water
02/07/14
02/07/14
S - UTFALL-00—02/07/1 L.ab
40 01 9-04
Water
02/07/14
/14
Slit/- COU'TFALL-003_t02/07/1 Lab
4020139-0
ter
02/07/14
02/07/14
t/it-tOU TFALL-004i , 2/07/1 Lab
40201 9-0Water
02/07/14
02/07/14
Sty- U°TFALL-005_02/07/14-Lab
40201 9-0
Water
02/07/14
0 /14
S OUTFALL-000,_0 /07/1 Lab
40201 9-0
dater
02/07/14
02t07/14
S OU"TFALL-010-YC3 02/07/14-Lab402013 -09
later
02/07/14
02107114
Samples were received in good condition at 4,5 degrees unless otherwise noted.
This report should not be reproduced, except in its entirety, wilthout the written consent of Prism Laboratories, Inc.
9 Springbmok Road - P.O 2 - Charkifte, KC 2922 2
Phone. 7 629 2 » Toll Free Number, t 99d629 2 m Fax: 62
Of �

Summary of Detections
16,
srunn.a
i
/1{1
z��sm
EnvironentaSOutions
asararrat¢s aa+.CPrism
139
Work Order. 4020139
Prism ID
client ID
Parameter
Method
Result
Units
40 -01
-OUTFAL-008,_0 /07/l —Lab
Phenolics
*4 0.1
0,34
402013 1
SVV-OUTFALL 02I 11 _La
Turbidity
*1so.1
.5
T
4020139-02
IN-OUiFALL-00 10 1 7114--
Phenolics
^420.1
a.35
MOIL
4020139-0
W-OUTF LL-00 02/07I1 —L b
Turbidity
*130.1
U
NTU
402013 -03
S-OUTFALL-00°7-02/0 11+4_Lab
Turbidity,
'130.1
2.7
NTU
4020139-04
SW UTFALL«0Q_02107114_Lpb
Phenolics
° 201
0,2
402 1 -04
SW-O TFALL-00 02f0711 _Lab
Turbidity
ffi130,1
4,O
NTU
40 0139-0
W OUTFALL-003 0 10711 _L b
Phenolics
a 20.1
0,36
mgtL
4020 9-0
SW OUTFALL-003-0210 114._Leb
Turbidity
'130.1
3,0
NTU
4020139-0
S t3UTFALL-004i? 107114_1- b
Phenolics
* 20.1
022
MOIL
402013 6
S OUTFALL-004_02/07114 L b
Turbidity
°160.1
Z8
NTU
40201 9-07
SW-O TFALL-00 0210 114 L b
Total Suspended Solids
*SM 2540 D
sc
m L
4020139-07
SW« UTFALL 5_02107114 Lab
Turbidity
°180A
5.1
NTU
4020139-06
SW- IUTFALL-006_02107114-1-ab
Turbidity
°180.1
4,6
NTU
4020139-0
SWt OUTFALL-01 t- 2107114—L Turbidity
*160:1
s.6
NTU
This report should not be reproduced, except in ft entrety, vvithout the written consent of Prism Laboratories, Inc.
9 SpringRoad -PA Box 240643 a Charlotte, NC 28724-0"3
Phone, 7 6 9-6 - Toll Free hlumben 1 016 - Fax: [phone]

t
Laboratory
§ Furt-Service
Analytical
02/21/2014
a Environmental
solutions
ib t..ak�cxass¢x'aresx sNc.
Colonial pipeline Company
Project'. Charlotte NPDES Star n ater
Client Sample ID: S 1t OUTF LL-008,,_02/07/
Attn: Jahn Culbreath
prism Sample ID: 4020139-01
P.O* Sax 87
project lea.. 1CO031038
Prism Work Order 402013
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected. 02/07/1414:40
Time Submitted,- 02/07/14 1 :00
Parameter
Result Emits Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Datemme
ID
General Chemistry Pafameters
flit Grease (HEM)
BRL
L 5.0 0.A7
1 *1664A 2f19f14 9:15
JAB P480311
Phenolics
0.34
mli& 0.060 0.027
1 * 20A 2t19I14 1 :30
MES P4803211
Total Suspended Solids
BRL
rng/L 5.0 0.90
1 *SM 2640 G 2111/14 11:A5
JAB P480166
Turbidity
GA
NTU 0.40 0.016-
1 *190.1 2011417:10
JAB P400122
Volatile Organic 602 a pez lncls b C S
Be ene
BRL
ugfL 0.50 0,054
1 *SM6200 B 2111114 15.37
VHL P4130176
Ethymenzene
SRL
ug1L 1.0 0,064
1 *SM6200 B 2111114 15:37
VHL P480176
tryp-Xillenes
BRL
a /L 2.0 0.11
1 *SM6200 B 2111/14 15:37
VHL P480176
Methyt-tert-Butyl Ether
BRL
ug1L 5.0 0.066
1 *SM6200 B 2/11114 5:37
VHL P460176
o­XYlene
SRL
u91L I'd 0.064
1 *SM6200 B 2111114 15:37
VHL P480176
Toluene
SRL
ug7L 1.0 0.057
1 *SM6200 B 2/11/14 1'5: 7
VHL P480176
Surrogate
Recovery
control Limbs
4-Bro robe r
109`
70-1 0
Dibromolluoromethane
112
70- 30
Toluen 0
104 %
70- 30
This report should not be reproduced, except an its entirety, without the written consent of Prism Laboratories, Inc,
9 Spring R P4. Box 240 - Charlotte, NC 29224-060
Phones 70442#4364 -"toll Free Number.1 001629 3&4 - Pas. 7 62 3
+ �

Laboratory Report
�a
FuH- Service Analytical $
n nosimantal sol""Ons
++ '
r
'° r„atpmsaartwwrrs: aat:
Colonial Pipeline Company
Prqject: Charlotte NPD S Stormwater
Client Semple IDSlit0U'6" , LL-0Dp 02/07/
ttm John Cultireath
Prim Semple lit: 402013 -02
P.O. Box 87
Project No,: NCO031038
Prism Work Order: 402013
Paw Creek, NC 23130
Sample Matrix: Water
Time Collected: 02/07/14 14: 0
Time Submitted: 02/07/1417:00
Parameter
Result Units Report MDL
DdWM Method Analysis Analyst Batch
Limit
Factor Datel"rinle IA
General Chemistry Parameters
tJs# Grease (HEM)
BRL
L 6.0 0,47
1 *1664A 2/19114 9:16 JAB P480311
Phenolics
0.36
MO& 0.060 0.021
1 *4220.1 21111413.30 MEll P400321
Total suspended solids
BRL
mgtL 5.0 0.90
1 ' *SCE 2540 D 2111/14 11:45 JAB P480168
Turbidity
16'
UTU 0.40 0.016
1 * 8 .1 W114 17:10 JAB P480122
Volatile Organic 602 Compounds by GCIMS
BRL
u911- 0.50 0.054
1 *SM6200 B /11114 16:03 VHL P480176
Ethyfleenzene,
BRL
ugtL 1.0 0.054
1 *SM6200 B 2111114 16:03 VHL P48017
rn'p-xyleries
BRL
ug1L 2:0 0.11
1 *SM6200 8 2111114 16:03 VHL P4B i176
Methyhte"utyl Ether
BRL
ug/L 5.0 0456
1 *SM6200 B 2t11114 16:03 VHL P480176
O-XYWM
BRL
u91L 1,0 0.064
1 *SM6200 B 2111114 16:03 VHL P480176
Toluene
BRL
ug1L 1.0 0.057
1 *SM6200 8 2111114 1 .03 VHL P4B0l76
Surrogate
Recovery ControlLimits
4-Sromrrfiuorobenzenis
1€39 0-130
Dibromorlubr thane
11 6 70- 3
Tokae 8
106 70-130
This re;iort should not be reproduced, except in Its entirety, without the written consent of Prism Laboratories, Inc.
9 Spfingbrook Road - P.O.s 240643 - Charlofte, NC 2924a0
Phone, 629 3 4 - Toll Free slu r:1.80016294364 # Fax: 7 626 0 1
1

Laboratory Report
SM t! Environmental Sclut ons
C a"ATdMMWI%MWl
02l 1/ 014
Colonial Pipeline Company
Project. Charlotte NPDES Stormwater
Client Sample ID: OUTFALL-OO 02/07/
Attn: John C lbrea h
Prism Sample ID: 4020139-03
P.O. Box 87
Project No.. CO0 1038
Pram 1tUer Order, 4020139
Paw Creek, NC 281:30
Sample Matrix Water
Time Collected. 02/07/1414:2
Time Submitted. 02/07/1417,00
Parameter
Result
Units Report MOL
Dilution Method Analysis Analyst Batch
Limit
Factor Dateftime to
General Chemistry Parameters
i9 & G (HEM)
BRL
MOIL 5.0 0.47
1 *1 A 2119/14 10:06 JAB P480311
Phenolics
BRL
L 0.050 0.027
1 *420.1 2/19/14 13:30 MES P480321
Total Suspended Solids
BRL
IL 5.0 0,90
1 *SM 2540 D 2111/14 11:45 JAR P480168
Turbidity
2.7
N!TU 0.40 0.06
1 48.1 217114 1710 jAS P480122
Volatile Organic 602 Compounds by GCIMS
8 ene
BRL
ug/L 0.50 0,054
1 °S 162008 2111/14 16:29 VHL P480176
Ethylberizene
SRL,
ug/L 1,0 0.054
1 °SM6200 8 2111/14 16:29 VHL P480176
m,p- ylenes
BRL
UQIL 2.0 0.11
i "SM6200 8 2111114 16:29 VHL P4B0176
Methyhtert Butyl Ether
BRL
ug/L 5.0 0.066
1 "SM6200 8 , 2I11/14 16:29 VHL P480176
o-Xylene
BRL
ug/L 1.0 0.064
1 'S 6200 8 2I11/14 16:29 VHL NS0176
Toluene
8RL
ug/L 110 0.067
1 "S i6200 8 241/14 16:29 VHL P4B0176
Surrogate
Recovery Control Unitts
4-Bromoftuoroberizene
110 % 70-130
D bromofiuoromethane
113 % 70• 130
T` e 8
106 70-1 0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spriatibrook Road - P.O. Box 240643 - Chartaft, Me 2822 64
Phoney 70416294364 - Toil Free Number i 1629 64 - Fax; 7041626,04091; 1 0

Laboratory Report
; [
Fuit-Service Analytical
Fnvironmentai Solutions
02/21/2014
6 Ln: AT„'S6tYt5.%N6
Colonial Pipeline Company
Project Charlotte NPDES Storrnwater
Client Sample ID: St t.7U Tl=ALL-00 02/071
Attn: John Culbreath
Prism Semple ID: 402013 4
P.O. Box 37
Project No.: NCO031038
Priem Work Order: 4020139
Peel Creek, NO 28130
Semple Matrix Water
Time Collected: 0 / 7/14 1415
Time Submitted: 02/07/1417,00
Parameter
Result
units Report MDL.
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time 10
General Chemistry Parameters
; S Grease (HEM)
SRL.
mg/L 5.0 0.47 '
1 *1 64A 2/19/14 10:06 JAB P480311
Phenolics
Oat
1L 0.00 0.27:
1 *420.1 211911413.0 MES P480321
Total Suspended Solids
BRL
1L &0 0.90
1 *S +i 2640 D 2/11/14 11:45 JAB P4 0168
Turtildtty
4.0
Fi tt 0.40 0.016
1 *1 .1 217114 17:10 JAB P400122
Volatile Organic 602 Compounds by
Benzene
BRL
ug1L 0. 0 O.054
1 *SM6200 B /11/14 1 :55 VHL P480176
Ettrybertzene
BRL
ug1L 1.0 0.054;
1 *SM6200 B 2111/1 16:65 VHL P480176
in'li-xYlenes
SRL
ug/L ZO 0.11
1 *SM6200 B 2/11114 16.55 VHL P480176
Met yl-ted-Butyl Ether
BRL
ug1L 5.0 0.056
1 *SM6200 B /11114 W66 VHL P480176
o-Xytene
BRL
u0/L 1.0 0,064
1 *SM6200 B 2JI1114 W66 VHL P480176
Toluene
SRL
ug1L 1.0 0.057
1 *SM6200 8 2/11/14 16:56 VHL P4 0176
Surroitate
Recovery Control Limits
4-Bromcifluorotienzene
109 , 70-130
Dibromofluoromethane
112 % 70-130
7oluen S
105% 70-10
This report should not be reproduced, except in its entirety„ without t the written consent of Prism Laboratories, Inc.
449 3prin tt Road - P.O. Box 240 - Charlotte, NC 28224-0643
Phone*. 29 364 -'toll Free Number. 100162943 * Fax. ? 26 1 �

Laboratory
Environmental Solutions
02121/2014
urw. a �e
c,c *ems
Colonial Pipeline Company '
Project: Charlotte FJPDES Stormwater
Client Sample ICE. SW OUTFALL-tie, 02/07/
Attn: John Culbreath
Prism Semple ICE: 4 2 139-0
.0, Box 37
Project No,: NCO031038
Prism Work Order: 4020139
Paw Creek, NC 28130
Sample Matrix. Water
Time Collected: 2/07/1414:05
Time Submitted: 2/07/1417:00
Parameter
Result Units Report - MDL.
Dilution Method Analysis Analyst Bach
Limit
Factor oatDateMme to
General Chemistry Parameters
t77 6 Gras a (HEM)
SRL
1. 6,0 0,47
1 : *1664A 2119114 W05 JAB P480311
Ptie Otte
046
0.060 0.027
1 *420.1 2119114 13. S P490321
Total Suspended Solids
BRL
mg1L 5.0 0.90
1 *SM 2540 D 2/11114 11 AS JAB P4 0166
Turbidity
3.0
NTU 0.40 0.016;
1 *1 0.1 V71141 :10 ,CAB P480422
Volatile Organit 602 Compounds by GCIMS
7;71—rl
BRL
ug1L 0.60 0.054
1 *SM6200 B 2111114 17:21 VHL P4801 6r
Ethylberizene
BRL
ug1Lo- to 0.064
1 *SM62008 2111/14 17:21 VHL P480176
rn,p­Xylenes
BRL
ug1L 2.0 0.11
1 *SM6200 B 2111/14 17,21 VHL P4 0176
Methyl - ell -Butyl Ether
BRL
u /L 5.0 0.066
1 *SM6200 B 2111114 17:21 VHL P4S017
O-Xyterre
SRL
ug1L 1.0 0.064
1 *SM5200 B 2111114 17:21 VHL P480176
Toluene
BRL
ug1L 1.0 0,057
�
1 °SM6200 S 2/11114 17: 1 VHL. P48017
r...
w � _Surropte
Recovery Control LimitsM
4-Sromolluorobenzone,
109 % 70-130
Dibrornofluoromethane
109 70-130
Toluene-0
104 70- 30
This report should not be reproduced, except in he entirety, without the written consent of Prisms Laboratories, Inc.
449 Springbroo Road > P.O. Box 240643 - Chorlothr. No 282244643
Phone [phone] • "Tolf Free Number 1 1629 3 - Fes: 7041526 CJ I
. raw

��,
Colonial Pipeline Company Project Charlotte NPDES Stormw
Attn: John Cultrreeth
.0, Box 87 project o.: IC 031038
&A-4..- AM-+-
Laboratory Report
02/21/2014
Client Semple ICE: OUT ALL-00d_ 2/071
4020139-06
02013
V 7i14114
,2/07d141 :00
Analysis Analyst Batch
Dateffirne to
Total Suspended Solids
BRL
L
5.0 0.90 1
*SM 2540 D 2111114 11AS
JAB
P480168
Turbidity
2.8
NTU
0 0.016 1
*1 0.1 217114 17.10
JAB
P480122
Volatile Organic 602 Compounds by GCIMS
Bence `
BRL"
ug11L
OM0.054" 1
*SM6200 8 2111/14 17:46
VHL
P480176
Ethybenzene
BRL
ug1L
1,0 0.0541
*SM6200 B 2111/14 17:46
VHL
P480176
rn,p. y
BRL
a dL
2.0 0.11 1
*SM6200 B 2/11/14 17:46
VHL
P480176
Methyl-t -Butyl Ether
SRL
a /L
5.0 0,056 1
*SM6200 8 111/14 17:46
VHL
P480176
o> ylene
SRL
ug1L
1.0 0.064- 1
*SM6200 B 2111#14 17.46
VHL
P480176
Toluene
BRL
UO/L
1.0 0,057' 1
*SM6200 B 2111114 17:46
VHL
P480176
surrogate
Recovery
Control Unrits
4-Brm ttutirobenz e
109
70-130
Dibrornolluoromethane
110
70-130
Toluene -rill
10
70-130
Thus report should net be reproduced, except in its entirety. without the written consent of Prism Laboratories, Inc.
449 Springbrook Read - P.O.a 240643 -+Chado te, No 28224-0643
Phone- 7041 29.6364 - Toll Free Number* 14001629.6364 * Pas: 704162 e fib �

Laboratory Report
Service Analytical
L4%f',',"JRu&,Rnvttxsmmnt�al Wutian
Q2J2fCi1
A"Mw.
Colonial Pipeline Company
Project: Charlotte NPC PS Stoat water
Client Sample ID. Situ OUTFAL -00 02/07/
Attu: John Culbreath
Prism Sample ID: 020139 7
P.O. Sox 57
Project tics.: NCO031038
Prism Work Order: 402013
Pew Creek, NC 2 130
Semple Matrix, Water '
Time Collected: 02/07/1413:55
Time Submitted:02/07/1 17-00
Parameter
Result
units Report MOL
Dilution Method Analysis ;analyst Batch
Limit
Factor Date/Tirrwl ID
General Chemistry Parameters
Ciao urea (HEM)
SRL
/L 5.0 0.47
1 ' *1664A 2/19114 10.45 JAB P4L 0311
Phenolics
SRL
/L_ 0.050 0.027
1 *420.1 2119/14 13:30 M S P4 0321
Total Suspended Solids
6.0
a g/L &0 0.90 '
1 *$2/11/14 1 .45 JAB P4110168
Tutlsld ty
6.1
NTU Onto 0.016
1 " *190.1 h14 1710 J, S P4B0122
Volatile Organic $02 Compounds by, GC/MSi
B ene
SRL
ug/L. 0.50 0,064
1 *SM6200 B 2/11/14 18:12 VHL. P480176
Ethylbonzene
BRL
ug/L 1.0 0,064
1 *SM6200 B 2/11/14 18:12 VHL P480176
m'p-Xylenes
BRL
/L. 2.0 011
1 *SM6200 B 2111/14 1812 V Le P480176
Mothyi-tert Butyl Ether
SRL
up/L 5.0 0,056
1 *SM6200 B 2111/14 18:12 VHL_ P B01 6
ci-Xitlene
SRL
ug/L to 0.064
1 *SM6200 B 2/11114 18:12 VI L P480176
Toluene
BRL
ug/L 1,0 0.057
1 *SM6200 B 2/11/14 18:12 VL L P480176
Surrogate '
Recovery control Limits
4-Bros Suss ene
10 70-130
Dibro lluoro thane
11 % 70-130
T 8
103 6 70-130
This report should not be reproduced, except in its entirety, vilithout the written consent or Prism Laboratories, Inc.
9 Sprintibirook Road m P, . Box 2 - Chadosto, NC 28224-0643
P sot as 70415294394- Toll Free Number 11-01629 3 - Pax. 70 26 PLC I

Laboratory Report
V Full-sece Analytical 0212112014
le"i", limp "
nViro"MontM solutions
Ai,smft KIColonial Pipeline Company Project- Charlofte IPDES Stormistater Client Sample ID- SW- OUTFALL-006-02/07/
Mtn- John Culbreath Prism Sample ID: 4020139-08
P.O , Box 87 Project No-' NCO031038 Prism Work Order: 4020139
Paw Creek, NC 28130 Sample Matrix: Water Time Collected: 02/07/14 13:30
Time Submitted: 02/07/14 17,00
sr Result units Report MDL = Dilution Method Analysis Analyst Batch
Limit Factor Dalefrime to
ral Chemistry Parameters
04 & Grease (HEM)
BRL
Ing/L
6.0 0A7
I
*1664A 2119/14 10:45
JAB
P480311
Ph of
BRL
mg/L
0,050 0.027
1
*420.1 2119/14 13'30
mEs
P4B0321
Total Suspended Solids
BRL
mg/L
5,0 0,90
1
*SM 2640 D 2/11114 1145
JAB
P480168
Turbidifilt
4.6
NTU
OAO 0.0116
1
*180.1 V7114 17:10
JAB
P400122
Volatile Organic 602 Compounds by GC/MS
;;nzen.
BRL
ug/L
0"50 0.054
1
*SM6200 8 2111/14 18:37
VHL
P480176
Ethythenzene
BRL
U911-
1,0 0,054
I
*SM620D B 2/11114 18:37
VHL
P4B0176
Mp-Xylenes
BRL
ug/L
2.0 0,11
1
*SM6200 B 2111/14 18:37
VHL
P4B0176
Methyl-tert-Butyl Ether
BRL-
Ug/L
610 0.066
1
*SM6200 8 2/11/14 18:37
VHL
P4S0176
o-Xylene
BRL
ug/L
1A 0.064
1
*SM6200 8 2/11114 18:37
VHL
PlIS0176
Toluene
BRL
ug/L
1'o 0,057
1
*SM6200 8 2/11/14 18:37
VHL
P480176
Surrogate
Recovery
Control Umits
4-Bromofluombenzene
109%
70-130
Dibromolluoromethane
110%
70-130
Toluene-d8l
104%
70-130
This report should not be reproduced, exoept in its entirety, without the written consent of Prism Laboratones, Inc.
449 Springbrook Road - P.O. Box 24060 - Charlotte, NC 29224-0643
Phone., 704/629-6364 - Tell Free Number. 11-4100162$43" - FlUc 7041626-M9

Laboratory Report
Fuff-Service Analytical K
Environmental Solutions
02t2l/2014
Colonial Pipeline Company
Project. Charlotte NPDES Stormwater
Client Sample lit, S UTFALL-01C-h+'1"Y"CLO
Attn: Jahn Culbreath
Prism Sample IC. 02 139-09
P.O, Sax 87
Project No.. NC 031038
Priam Work Girder. 4020139
Pay/ Creek, NC 28130
SampleMatrix: Water
Time Collected, 02/07/14 1&00
Time Submitted: 02/07/1417:00
Parameter
Result
units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateiTime ID
General Chemistry Parameters
Ct4S Grease (HEM)
BRL
L 5.0 OV
1 °t 64A 2119114 11: 0 JAB P480311
Phenol`
BRL
tL 0.050 0.027
1 "420A 2/19114 13:30 CABS P480321
Total Suspended Solids
BRL
M91L 5.0 oso
1 'SM12540 D-2/11/14 11:45 JAB P480168
Turbidity
9y5;
NTU 0.40 0.016
1 *190>1 W114 0.10 JAB P480112
Volatile Organic 602 Compounds by GCIMS
Benzene
BRL
ug/L 0.60 0,054
1 °SMI6200 6 2111/14 19:03 VHL POW$
Ethybenzene
BRL
ug/L 1.0 0,054
1 *SMI6 00 B 2111/14 19,03 VHL P48017
m,pwxylenes
SRL
u /L 2.0 0,11
1 °SM62006 2111/1 1 9:03 VHL P4B0176
Methyr tert-B Ether
BRL
ug L 5.0 0.056
1 *SM6200 S i11114 19:03 VHL P480176
o- ylene
SRL
u 1L 1.0 0.064
1 "SMi6200 B 2111114 W03 VHL P480176
Toluene
BRL
u 1L 1.0 0.057
1 "SM16200 B 2111114 19:03 VHL P4 0176
Sonlopte
Recovery Control LS '
4-Bromolluorobenzene
106 70-130
Dibromotluoromethane
106 , 70-130
Toluene -de
101 70-130
This report should not be reproduced, except in its entirety, without te written consent of Prism Laboratories, Inc.
9 Springbrook Road w P.O. Box 240 . Charlotte, NC 28224-0643
Phone: 2 -63 « Toll Free Number 1529 3 - Fax: 7 525 9

Level
FUR -Service AnMyVeW
Enrviro"Me ntol Sohdionsx
2121/14
L!4 ATffdAtF44bAt�
Colonial pipeline Company
Project, Charlotte NPDES Stormwater
Prism Work Order. 402013
Attn. John Cu breath
Time Submitted. 217/2014
5.00:OOPI
P,O. Box 87
Project No: NCO 31038
Paw Creek, NC 2813
volatile Organic 602 Compounds by GCIMS - Quality Control
Reporting
-Spike
Sou
%REC
RPC
Analyte
Result
Limit
units
Level
Result %REC
Limits RPD
Limit Notes
Batch P4 0176 - S 6200
Blank (P� Qi7b ... ._
prepared & rinalyzed.;f12l11114
Benzene
BRL
0,60
u91L
Ethybenzene
BRL
10
ug/L
m,p-Xylenes
SRL
2.0
ug/L
d etta l-t -Butyt Ether
SRL
5,0
ug/L
O-X*ne
BRL
1,0
a 1L
Toluene
BRL
1:0
ug/L
Surrogate: 4-Bromotluo nzene
54.
q&
50.00
110
70-130
Swroplis: Doromoificorometharre
55.2
ergs.
50.00
110
70-130
S ate. Toluene-0
52.1
uglL
50.00
104
70-130
LC (a 0176-0 t)....
�,,,
_._.......,.w.... ... �..............._...................... .....
-
.., ._.,..._____..,..
w...e:.»........
Prepared & Analyzed'.02111/1
. ... .. .._. Mom._.... .._,...._..,.,...........
......._ _....._.,..... .m.
.......___...,.M.._._., ..,. ..... _._....... ...
Benzene
20.7
0.50
ugfL
20.00
104
70-130
Ethylbenzene
20.4
1,0
ug/L
20.00
102
70-13
nrp-Xytenes
42,3
2.0
a /L
40,00
106
70-130
Methyl»tert Butyl Ether
21.3
5.0
a tL
20.00
107
70-130
o4ylene
21.2
1.0
uq/L
20.00
106
70-130
Toluene
20.0
1.0
ug/L
20,00
105
70-130
Surrogate: 4 robenzene
$66
ugt
50.00
t l l
70-130
Surrogate, Dibromolluorometherre
53S
u91L
50.00
107
M1 0
SwWate: -d8
52.5
digs,
50.00
105
70-130
LC0 Oup(P "70 Dt)_._ _.
PTrepared Analyzed.02/11/14
Benzene
20.2
0.50
uglL
20,00
101
70-130 2
20
Ethybenzene
19.
1:0
ug/L
20.00
99
0-130. 3
20
m,p- ylenes
40.0
2;0
ug/L
40 00
102
70-130 3
2
M 1»tedwButyl Ether
21.4
5.0
a 1L
20.00
107
70-130 0A
20
omylene
20,7
1.0
ug/L
20:00
103
70-130 2
20
Toluene
20.5
1,0
ug/L
20,00
102
70-130 2
20
Sumogate: 4-Bromolluorobenzene
54.7
u91L
50.00
109
70-130
Surrogate: Dibromolluoromethene
519
u9r1.
150.00
108
70-130
Su ate. oluenew0
52.2
ug/L
50M
104
70-130
This report should not to reproduced, ex0ept in its entirety, without:the writtensent of Prism Laboratories, Inc,
449 Springbrook R a P.O. Box 24 3- Chadotto, MC 20224-0643
Phone; 7 4 •'foil Free Number. 11629-63 -. Fax* 2

,3
eA r�& rW,
Colonial Pipeline Company Project: Charlotte NPDES Stcaotherater Prism Work
Mira: John Culbreath Time Suomi
P.O. Box 87 Project No, NCO03103
Paw Greek, NC 23130
General Chemistry Parameters - Quality Control
Level I
2/21/14
)rder. 4020139
,ad: 2171201 :00.00PM
Blank (P40012243L. 41)
PreparedAnalyzed: 02107/14__.__
Turbidity
O L 0,40 NTU
LCS (4 0122 S1 ..._
� _ _ ...
PreparedAnalyzed: 02107/14 _.
Turbidity
,4.02 0A0_ NTU
4 000 100 90-110;
Rypllcate ff400122-13L1P1} _
_ _. .._ _ Source: 40 01 9-09 w
Prepared & Analyzed:02107/14
Turbidity
10.2 0.40 NTU
9.76 4 20
Batch P4 0108 a NO PREP
Blank (P'400168«OL KI)
Prepared & Analyzed. 02/11/14
Total Suspended Solids
SRL 5,0 nVIL
LCS (P400168 S1)
Prepared & Analyzed:02/11/14
Total Suspended olids
450 5.0 C.
426.0 106 90-110
Batch P4 0311 - NO PREP
Blank (P4 31 .SLKI)
Prepared & Analyzed: 02/1 /1
Oil & Grease (HEM)
BRL 5:0 , 1L
LCS (p400311 , S1) <._... _
_ _ :u .. _:.
Prepared & Analyzed: 2/19/1
Oil & Grease (HEM)
37.3 5:0 dL
40.00 93 76-11
Batch P480321 -420.1
Blank (P4003214SLIC1j
Prepared: 02118114
Phenolics
SRL 0.060 m9n.
This report should not be reproduced, e its entirely, without the written consent of Prism Laboratories, Inc.
9 Springbrook Read - P.O. Bea 240643 - Charlotte, No 28224-0643
Phone: 7 6 3 -"fell F Number 1 01 29-9364 » Ella. 7 26-0

Level If OC Report
..;
ual-Servicre
Analytical 8
22121/14
ism
Environmental Solutions
Colonial Pipeline Company
Project:
Charlotte P Stormwater Prism Work Order: 4020139
Attn: Joan Culbreath
Time Submitted: 1201 6;00:00 PI
P.O. Box 87
Project No: NCO031038
Paw Creek, NC 28130
General Chemistry Parameters R Quality Control
Reporting
Spike Sour °RBC
RPL1
Analyte
Result
Limit Unite
Level Result %RFC Limits RPL1
Limit Notes
Batch P4B0321 - 420.1
LCS tP4 821-OS1
Prepared: 02118/14 alined: 0211911 _..
Ph of
0.552
0.050 dL
0:000 110 80-120
Matrix Spike P 0 21- S1p _._
Sou 4020139
Prepared: 02118/14rrAnalyzed: 02119/4
Phenolics
0.294
0.050 L
0.5000 BRL 59 80-120
Matrix Spike Dtrp IP400 21t 01 _
Source: 2 18 S
_
Prepared. 02118/14Analyzed.0211 /1
Phenolics
0,280_.
0,060 g L
0.5000 BRL 66 80.120 5
20
Sample Extraction Data
PropMethod: 420.t
LAb Number
Batch
Initial
Final
Ostarrime
402013 1
P480321
50 mL
50 mL
07J18114 10:35
402013 2
P480321
50 nit.
50 ml.
02l18114 10.35
40201 9-03
P480321
50 mL
50 mL
02118/14 10:35
402013
P480321
50 mL
50 mL
02/18114 10:35
402013 -05
P480321
50 mL
50 mL
02I8114 10: 5
402013
P480321
50 ML
50 int.
02118/14 10:35
4020139-07
P4S0321
so ML
50 mL
02/18114 10:35
40201 9-08
P480321
so ML
50 mL
0 118114 14:46
4020139-09
P4B03 1
so MI.
50 mL
02118/14 1 :4
Prep Method: SM6200 B
Lob Number
Satoh
Initial
Final
Didetrime
402013"1
P480176
10 mL
10 , mL
02/11114 9;00
4020139-02
P480176
10 mL
10 mL
02/11114 9:00
4020139413
P4B0176
10 mL
10 mL
02/11/14 9.00
40201 "4
P480176
10 mL
10 mL
02/11/14 9:00
02013 5
P4B01 6
10 mL
10 ml.
02/11/14 9.00
402013 -06
P4B0176
10 mL
10 mL
02111/14 9:00
402013 7
P480176
10 mL
10 ml.
02/11/14 9:00
402013 -08
P480176
10 mL
10 mL
02/11/14 9.00
402013 9
P480176
10 mL
10 mL
02111/14 9:00
This report should not be reproduced, except in its entirety„ without the written consent of Priam Laboratories, Inc.
9 Bpringb ok Road « P4. Box 240 . Charlotte, NC 28224-0643
Phone. 620 364 - Toll Free Number. 11 94364 . Fax., 7 28
0 {

Chain Of Custody #a' CRTJW-240aboraCory Account#:
Consultant Contact:
colonii Pipelifle COMMY
Site Location: Charlotte NPDES
Consulting Finn, -
Project Name: February 2014
Address:
FacilitylSite ID#-, 0840
City, State, zip-,
Colonial Pipeline PW John Culbreath
Phone,
Cost Center/AAFEk PaY Key #1533
Fax:
Requested Analysis Method
Lab Billing Control #:
,
MOO Collection
Date and Time
.0
0
0
X
Field Sample ID: Comment:
Sam*
SW-OUTFALL.0�02107114_1.
Type:
Date: Time:
Matrix
SW-OUTFA4� L LL- 009 02/0711
7 Lab
7
0
0 217/2014
Surface Wet
jl
SW-OUTFAALL 7114 L
Lib
0
2/7/2014-
Surface Wat
—
-OUTFALL-002 02JO7/14 L
7 Lab
0
0 2 014
u 00
7 Lab
0
0 W12014
Surface wet
7 Lab
0
0 2/7/201
7 Lab
7
0
0 Z71201d t 1
SurfaceWat
Lab
0
0 21712094
Surface wat
7 Lab
0
0
Surface wet
Lab
0
0 Sufface Wat
rr do
0 ON,
.............
Standard TAT
sy
Rush TAT (Fax due Close of Business CST
Due Date:
4 . ......... . .
Custody
MIT
'4 A 'Z, 7
Record
Ivp 79700 yi

ET #. 420,1 Approved for NPi ES ` (Editorial Revision 1 7 )
TITLE: Phenolics (Spectrophotometric, Manual 4-AAP
With Distillation)
ANALY°TE; Phenolics
INSTRUMENTATION: Spectrophotometer
STi RE'T No.: 32730
1.0 Scope and. Application
1.1 This method is applicable to the analysis of drinking, surface and saline
waters, domestic and industrial wastes.
1.2 The method is capable of<measuring phenolic materials at the 5 gg/L level
when the colored end product is extracted and concentrated in a solvent phase
using phenol as a standard.
13 The method is capable of`measuring phenolic materials that contain more than
0 g/L in the aqueous phase (without solvent extraction) using phenol as a
standard.
1.4 It is not possible to use this method to differentiate between different kinds of
phenols.
2 t1 Summary of Method
.1 Phenolic materials react with 4-aminoantipyr ne in the presence of potassium
ferricyanide at a pH of 10 to forth a stable reddish -brown colored antipyrine
dye. The amount of color produced is a function of the concentration of
phenolic material,
10 Comments
.1 For most samples a preliminary distillation is required to remove interfering
materials.
.2 Color response of phenolic materials with 4-amino antipyrine is not the same
for all compounds. Because phenolic type wastes usually contain a variety o
phenols, it is not possible to duplicate a mixture of phenols to be used as a
standard. For this reason phenol has been selected as a standard and any color
produced by the reaction of other phenolic compounds is reported as phenol.
This value will represent the minimum concentration of phenolic compounds
present in the sample.
4.0 Sample Handling and Preservation
4.1 Biological degradation is inhibited by the addition of 1 g/L of copper sulfate to
the sample and acidification to a pH of less than 4 with phosphoric acid. The
sample should be kept at VC and analyzed within 24 hours after collection.

5,0 Interference
5.1 Interferences from sulfur compounds are eliminated by acidifying the sample
to a pH of less than 4 with H,3PO4 and aerating briefly by stirring and adding_
Cu C) .
5.2 Oxidizing agents such as chlorine, detected by the liberation of iodine upon
acidification in the presence of potassium iodide, are removed immediately
after sampling by the addition of an excess of ferrous ammonium sulfate
(T l ). If chlorine is not removed, the phenolic compounds may be partially
oxidized and the results may be low.
0 Apparatus
6.1 Distillation apparatus, all glass consisting of a 1 liter pyre distilling apparatus
with Graham condenser.'
6.2 pH meter.
6.3 8pectr, rphoto eter for use at 460 or 510 nun.
.4 Funnels.
.5 Filter paper.
6.6 Membrane filters.
6.7 Separatory funnels;500 or 1,000'rnL.
6.8 Nessler tubes, short or long form.
.
70 reagents
T I Phosphoric acid solution, 1 + 9: Dilute 10 mL of 85% H3PO4 to 100 mL'with
distilled water.
7:2 Copper sulfate solution: Dissolve 100 g CUS04'5H2O in distilled water and
dilute to 1 liter.
7.3 Buffer solution: Dissolve 16.9 g NH4C1 in 143 mL conc. NIJ OH and dilute t
250 mL with distilled water. Two mL should adjust 100 mL of distillate to pH
10,
7.4 Aminoantipyrine solution; Dissolve 2 g of 4A P in distilled water and dilute'
to 100 mL.
7.5 Potassium ferricyanide solution: Dissolve 8 g of K3Fe(CN) in distilled water
and dilute to 100 mL.
7.6 hock phenol solution: Dissolve 1.0 g phenol in freshly boiled and cooled
distilled water and dilute to I liter. 1 mL = I mg phenol.
7.7 Working solution A`: Dilute 10 rnL stock phenol solution to 1 liter with distilled
water. mL = 10,ug phenol.
T8 Working solution 13: Dilute 100 mL of working solution A to 1000 rnL with
distilled water. 1 mL = 1 gg phenol.
79 Chloroform
710 Ferrous ammonium sulfate: Dissolve 1.1 g ferrous ammonium sulfate in 500
mL distilled water containing I mL cork. H2SO4 and dilute to 1 liter with
freshly boiled and cooled distilled water.
&0 Procedure
8.1 Distillation

8.1. i Measure 500 mL sample into a beaker. Lower er the pH to approximately
4 with 1 + 9 H31`04 (7.1) add 5 mL CuSQ solution (7.2) and transfer to
the distillation apparatus. Omit adding HYt 4 and CuSO4 if sample was
preserved as described in 4.1.
8.1.2 Distill 450 mL of sample, step the distillation, and when boiling ceases
add 50 mL of warm distilled water to the flask and resume distillation
until 500 mL have been collected.
8.1.3 if the distillate is turbid, filter through a pre ached membrane filter.
8.2 Direct photometric method
8.2.1 Using working solution A (7.7), prepare the following standards in 100
L volurnetric flasks.
L of working solution A Conc. g/L
0.5 50.0
Lit IWO
2.0 20.0
.0 500.0
8.0 800.0
1010 1000.0
8.2.2 To 100 mL of distillate or an aliquot diluted to 100 mL and/or
standards, add 2 mL of buffer solution (7.3) and mix, The pH of the
sample and standards should be 10 ± 0.2,
8.2.3 Add 2.0 mL a inoantipyrine solution (7.4) and mix.
8.2.4 Add 2.0 mL potassium ferricyanide solution (7.5) and mix.
8.2.5 After 15 minutes read absorbance at 510 n `,
.3 Chloroform extraction method
8.3.1 Using; working solution B (7.8), prepare the following standards.
Standards may be prepared by pipettfng the required volumes into the
separatory funnels and diluting to 500 mL with distilled water.
L of working solution B Conc. f,
.0 6.0
5.0 10.0
10,0 20O
20,0 4 d.0
25.0 50,0 ,
8.3.2 ' Place 500 mL of distillate or an aliquot diluted to 500 mL in a
separatory funnel. The sample should not contain more than 25, g
phenol,
8.3.3 To sample and standards add 11 mL of buffer solution (73) and mix.
The pH should be 10 t 0.2,
8.3.4 Adel 3,0 mL a inoantipyrine solution (7.4) and mix,
8.3.5 Add 3.0 rut, potassium ferricyanide solution (7.5) and mix.
8.3.8 After three minutes, extract with 25 mL of chloroform (7.9). Shake the
reparatory funnel at least 10 times, let CHCIe$ settle, shake again 10

t
times and let chloroform settle; again: Vent chloroform fumes into hood.
8.33 Filter chloroform extracts through filter paper. Donot acid more
chloroform. Carry.: out filtration in a hood. Dispose of chloroform in
environmentally acceptable manner.
&18 Read' the absorbance of the samples and standards against the blank at
460 rim.
9.0 Calculation
9.1 Prepare a standard curve y plotting the absorbance value of standards versus
the corresponding phenol concentrations.
91 Obtain concentration value of sample directly from standard curve,
10.0 Precision and Accuracy
10,1 Using the extractions procedure for concentration of color, six laboratories
analyzed samples at concentrations of 9.6, 48.3, and 93,5 ; g/L. Standard
deviations were C .99, ,1 and ±4, g/L, respectively,
0.2 Using the direct photometric procedure, six laboratories analyzed samples at
concentrations of 4 7, 48.2 and 97.0 /L. Standard deviations were ± .18,
0.48 and ± 1.58 L, respectively.
Bibliography
1, Annual Book of AS'TM Standards, fart 31, "Water", Standard D 1783-70 p553 (1976),
2 Standard Methods for the Examination of Water and Wastewater, 14th Edition,
p 4-5 1, Method 510 through 510C> (1975).

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k1locco, Marcia
Allocco, Marcia
Satterwhite, Dana
Abject: FW: Lab Certification Review Request
arcia
ooked through Standard Methods and did some Google searching and did not find anything specific about algal
ooms contributing phenol to the analysis — either as a positive interference or directly adding phenolic compounds.
)t saying there isn't —just can't find anything supporting that easily,
you want any more help — that is more specific language etc. to any of their points let me know — basically all of the
ethod references they site regarding temperature and hold time are superseded by the 40 CFR part 136 requirements
that is, the temperature requirement is now:s 6" C and the allowable hold time is 28 days (with F12SO4 to pH Q. As we
scussed footnote 4 from Table It addresses hold time.
id as we discussed the spike data points to low recovery not a positive bias. Also regarding their comments in 6.a.
garding the spike recovery — this is NOT a reflection on the accurac of the test itself as the state — wha i
'
exceeded the permit limit? Seems they should be proactive eliminating that issue if they think it is the source of the high
concentration of phenols.
If you want to discuss further or would like more specific help with language let me know
Gary
Have you signed up to receive automatic email notices of changes to policies, regulations and
resources pertaining to Wastewater/Groundwater Laboratory Certification that could have an impact
on your day to day operations? If not, send a blank email to the following address to get on the
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to
third parties unless the content is exempt by statute or other regulation,
Gary Francies
Technical Assistance/Compliance Specialist

pppppp-
Allocco, Marcia
From: Frances, Gary
Sent: Tuesday, December 16, 2014 5:17 PIA
To- Ignatius Mutoti
Cc: 'Culbreath, John W'; 'Kathy Roush'; Allocco, Marcia
Subject: RE: Colonia Pipe NOV
Ignatius
As a follow up to our phone call and your below email see my reply in RED in your email below
Gary
Have you signed up to receive automatic email notices of changes to policies, regulations and
resources pertaining to Wastewater/Groundwater Laboratory Certification that could have an impact
on your day to day operations? If not, send a blank email to the following address to get on the
list.
DENR.go.Lab_Cert-'[e-mail]
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to
third parties unless the content is exempt by statute or other regulation.
Gary Francies,
Technical Assistance/Compliance Specialist
NC WW/GW Laboratory Certification
0:[phone]
F: [phone]
INC DENR/Division of Water Resources — Water Quality Programs
Water Sciences Section — Asheville Regional Office
2090 U.S. Highway 70
Swarmanoa, NC 28778
hJ12..//p_o_r_tal-_ncdenr._or 1 jweblw abLcert &L__ qL
From: Ignatius Mutot! [mailto:[e-mail]]
Sent: Tuesday, December 16, 2014 4:15 PM
To: Francies, Gary
Cc: 'Culbreath, John W; 'Kathy Roush'
Subject: Colonia Pipe NOV
Dear Gary —
Thank you for taking the time to discuss the above matter with me. Per our telephone conversation, I am copying you
the final ruling letter from Marcia at NC DENR for your review. As this discussed, Marcia's decision relied largely on your
recommendations,
We accept your point that temperature may not play an important role even though the method still calls for 4 'C
the law, 40 CFR Part 136 now calls for 6'C maximum temperature. The law overrides — thank you
I

pppww-
go at result of 1.62 mg/L vs. the
:h the acceptable lower and
result and actual phenolics
plied to Colonial pipe sample
result.
Basically what we discussed and what this information shows is that there is a degree of uncertainty associated with
every tab analysis. One must distinguish lab analysis uncertainty with evidence that something went wrong with the
analysis, to such a degree that the result should be considered invalid. There is a difference between uncertainty and
error. In my opinion there is no evidence of any problem with the analysis that would invalidate the result. When one
discusses the uncertainty you can not only discuss the possibility that the result could be lower and thus result in a
compliant value. It must also be recognized that that same degree of uncertainty could mean the "true" answer was
actually greater than the reported concentration of 0.35 mg/L. The answer could just as easily be 0.55 mg as it could
be below compliant concentration. Uncertainty is not a one way street.
The low recovery of the matrix spike cast further doubt of the result of 0.35 mg
Yes, it does cast doubt, but once again the low recovery on the spike indicates that if there is actual matrix interference
involved it is resulting in a low recovery, so if anything the 0.35 mg/L result is a low value not a high value.
We understand that your review did not include a review of statistical data present with the request to reduce
the NOV to NOD, since there is no history of exceedances based on our statistically analysis of data, it appears
that indeed, the value 0.35 mg/L is an outlier (could be an actual value)
I may have left the wrong impression — I did not mean to imply I did not took at the statistical data at all — what I was
trying to say was that it really meant nothing in mu assessment process. The point is, past data has no direct correlation
to a future sample — especially a grab sample — that was the value at that moment- a day earlier or a day later may very
well have resulted in a much different result. My point was that it is my understanding that in making enforcement
decisions the Division does not consider that enough to invalidate a single sample event.
And my role was only to assess the data and determine in my opinion whether there was any evidence to invalidate the
result. As I said I do not think there is - that does not deny that the result may have been a statistical outlier in relation
to past samples.
We therefore request that you discuss further with Marcia and assist in our Client's request for a reduction of the NOV
to NOD based on consideration of all points presented. It is our opinion that there is sufficient evidence to cast
result. Perhaps a NOD coupled with additional more aggressive sampling and testing for phenolics would suffice. This
additional sampling and testing will confirm indeed, if compliance with phenolic is a problem.
In my opinion, while there is certainly uncertainty in the result, as there is with any sample result, there is nothing
presented that would make the sample result invalid.
As promised, I did discuss this with Marcia. She indicated that if you want to discuss further you need to contact Michael
Parker in the Mooresville Regional Office since he signed the letter. Staffs time will probably be very limit between now
and the end of the year due to the holidays so you may not receive an immediate response.
Gary
2

WA
LTMAS�
.- As -4
FILE,
HCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory John E. Skvarla, III
Governor Secretary
December 10, 2014
Mr, Jahn Culbreath
Environmental Specialist
Colonial Pipeline Company
P.O Box 8
Pave Creek, North Carolina 28130
Subject. Review of Colonial Pipeline response to Notice of Violation NOV-2014-LV-0336
Carlotte Delivery Facility
NPDES Permit No, NCO031038
Mecklenburg County
Dear Mr. Culbreath:
On August 19, 2014, this office received a response to the above reference Notice of Violation (NOV). The
NOV was issued for exceeding the permit limit for total phenolic compounds at O tfall 009 On February 7,
2014, Colonial Pipeline's NOV response requested that the; Division consider reducing the NOV to a Notice of
Deficiency (NOD). ; The response included an assertion that the elevated total phenols result might be attributed
to laboratory error or naturally occurring phenolic compounds from an algal bloom that had farmed in the diked
area that drains through Outfall 009,
Upon receipt of your correspondence staff from the Division's Laboratory Certification Branch was contacted to
review the supporting documentation included with your response. The Laboratory Certification program serves
as a vital component in the effort to ensure the quality of analytical data used for regulatory decisions by
multiple divisions within the Deportment of Environment and Natural Resources (DENR) including the Division
of Water Resource's NPDES discharge program. The Laboratory Certification program operates pursuant to
authority contained in G.S. 14-215.3( )(1) and 143-215.3(a)(10) and enacts requirements for certified
laboratories through the rules found in North Carolina Administrative Code, 15A NCAC 2H .0800. The 'program
certifies approximately 700 environmental laboratories in Forth Carolina and throughout the United States.
The review completed by the Laboratory Certification program'program's staff did not find grounds to invalidate the
February 7, 2014, sample result based on the performed analytical procedures or the passible interference from
naturally occurring algae. Therefore, the Division cannot reduce the issued Notice of Violation to a Notice of
Deficiency.
If you have questions concerning this matter please do not hesitate to contact M. Marcia Allocco or myself at
[phone]:
Sii erely,
m 4
t Michael L. Parker, Regional Supervisor
Water Quality Regional operations Section
Division of Water'Resources, NCDENR
Branch Central Files (MSC 1617-basement)
Mooresville Regional Office
Location: 616 East Center Ave., Suite 301 Mooresville, NC 28115
Phone: [phone] t Fax: (704) 6 - 6401 Customer Service: 1.87-623-6748
Internet, ttp:lipodal.ncdenrolgl eb/wq

FILE,
NCDENR Olt
North Carolina Department of Environment and Natural Resources
Pat McCrory John E, Skvaria, III
Govemor Secretary
July 22, 2014
Mr. Mike Cutting
Operations Manager - Charlotte/SC
Colonial Pipeline Company (CPC)
P.O. Box 87
Paw Creek North Carolina 28130
Subject: Notice of Violation — Effluent Limitation
Tracking #: NOV-2014-LV-0336
Charlotte Delivery Facility
NPDES Permit No, NCO031038
Mecklenburg County
Dear Mr. Cutting -
A review of the February 2014 self -monitoring report for the subject facility revealed a violation of the
following parameter at Outfall 0091-
Gate Parameter R9R2AtqValue Permit Limit
2/7/14 Total phenolic compounds 350 gg/L 300 fAg/L (Daily maximum)
Remedial actions, if not already implemented, should be taken to correct the noted any problems.
The Division of Water Resources may pursue enforcement actions for this and any additional
violations. If the violations are of a continuing nature, not related to operation and/or maintenance
problems, and you anticipate remedial construction activities, then you may wish to consider applying
for a Special Order by Consent (SOC).
If you have questions concerning this matter or to apply for a SOC, please do not hesitate to contact
Ms. Marcia Allocco or myself at [phone]:
Sincerely,
Michael ichael L. Parker, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
ccWastewater Branch
Central Files (MSC 1617-basement)
Mooresville Regional Office
Location: 610 East Center Ave., Suite 301 Mooresville, NC 28115
Phone: [phone] t Fax: [phone] \ Customer Service: 1-877-623-6748
Internet, hftpJ/portal,ncdenr.org/web/wq
An Fanal Onportuoh t Affirrnafivp Add EnnDlover - 30% RecWed,"10% P0 Consumer oarrer

AL
A410
North Carolina Department of Environn
Division of Water C
Beverly Eaves Perdue Charles Wakild, F
Governor Director
May 3, 2012
John W. Culbreath
Colonial Pipeline Company
Post Office Box 87
Paw Creek, North Carolina 28130
Subject: NOTICE OF DEFICIENCY
NOD-2012-LV-0012
Colonial Pipeline Co. Charlotte Deliver
NPDES Permit No. NCO031038
Mecklenburg County
Dear Mr. Culbreath:
A review of the January 2012 Discharge Monitoring R(
following parameter(s) at Outfall 007:
Par
a` R
FiLE/1
t
ent and Natural Resources
iality
E Dee Freeman
Secretary
)ort (DMR) revealed a violation of the
parted V41ye -=ke-rM-it -Limit -=
1 1 -Y" 19/ 1
Remedial actions should be taken to correct the cause(s) of this violation. The violations
described above should be abated immediately and properly resolved.
Thank you for your attention to this matter. This office requires that the violations as described
above be properly resolved. Unresolved violations may lead to the issuance of a Notice of
Violation and/or assessments of civil penalties.
N. C. Division of Water Quality
Mooresville Regional Office
610 East Center Avenue, Mooresville, NC 28115
Phone: [phone] k FAX: [phone]\ One
CustornerServim 1-877-623-6748 NofthCarohna
internet www,ncwaterquality.org
An Equal Opportunity t Affirmafive Action Employcr NJUMMAY

&&Aw FILE
.R.
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Bever1v Eaves, Perdue Charles Wald d, R E Dee Freeman
Governor Director Secretary
May 2, 2012
Mr, John W. Culbreath
Colonial Pipeline Company
PO Box 87
Paw Creek, North Carolina 28130
SUBJECT: Rescission of Notice of Violation
NOV-2012-LV-0213
Colonial Pipeline Company
NPDES Permit No. NCO03103 8
Mecklenburg County
Dear Mr. Culbreath:
On April 24, 2012 this office issued allotice of Violation for the violation of the total suspended solids
daily maximum permit limit reported for January 12, 2012. Upon further review and in consideration of the
measures taken by Colonial Pipeline Company to resolve the violation, I hereby rescind the subject Notice of
Violation (NOV-2012-LV-0213). A Notice of Deficiency will be issued for the total suspended solids daily
maximum limit violation. The Division's enforcement tracking databases have been modified to reflect this
change.
Should you have any questions concerning this correspondence, please contact me at [phone].
Sincerely,
Robert B. Krebs
Surface Water Quality Regional Supervisor
cc:
Point Source Compliance/Enforcement Unit
Mocnvsville Regional Office One
Location: 610 East Center Ave., Suite 301 Mooresville. NCI 29115 N () 'thCarolma
Plione: (704) 663- 1699 \ Fax: [phone]
Internet: tg,# �ortal.nod�eqr.o%tweblw

FIL
C D E IRR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Chades Wakild, P.E. Dee Freeman
Governor Director Secretary
April 24, 2012
Mr. John W. Culbreath
Colonial Pipline Company
PO Box 87
Paw Creek, North Carolina 28130
Subject: Notice of Violation — Effluent Limitations
Tracking #: NOV-2012-LV-02.13
Colonial Pipeling Outfiall 007
NPDES Permit No. NCO031038
Mecklenburg County
Dear Mr. Culbreath:
A review of the January 2012 self -monitoring report for the subject facility revealed a violation of the
following Parameter at Outfall 007:
Date Parameter Reported Value Permit Limit
01/12/2012 TSS 110 mg/I 45 mg/I daily maximum
Remedial actions, if not already implemented, should be taken to correct any problems. The Division
of Water Quality may, pursue enforcement actions for this and any additional violations. If the violations are of
a continuing nature, not related to operation and/or maintenance problems, and you anticipate remedial
construction activities, then you may wish to consider applying for a Special Order by Consent. You may
contact John Lesley of this Office for additional inform, ation.
If you have questions concerning this matter, please do not hesitate to contact Mr. Lesley or me at (704)
663-1699.
Sincerely,
Robert B. Krebs
Surface Water Protection
Regional Supervisor
cc: Point Source Branch
JL
Mooresville Regional Office
Locatlow 610 East Center Ave., Suite 301 Mooresville, NC 28115
Ishow [phone] 't Fax: [phone] k Custorner Service: 1 -877-623-6748 One
' YM
Internet www.ncwaterquality.org No Karol=
An Equal Opportunity 1 Affirmative Action Employer - 30% Rerycled/I 00% Post Consumer paper
WIMAY

s-
Aarc a
From: Krebs, Rob
Sent: Thursday, May 31, 2012 10:1 B AM
To: Allocco, Marcia; Bell, Wes; Bou'-ghazale, Samar; Browder, Dee„ Hood, Donna; Lesley, John;
Parker, Michael; Sifford, Barbara; Snider, Lon
Subject: FW. Change in Authorized Responsible Official
Attachments: EPA Administered Permit Programs and NSHAP - Updated DAR Delegation Memo
033012,FI NAL. version 2 pdf
FYI
From: Leigh, Faron D [mailto;FLeigh colpipe.com]
Seat: Thursday, May 31, 2012 10:00 AM
To: Belnick, Tom
Cc: Basinger, Corey; Krebs, Rob; Smith, Cranny
Subject. Change in Authorized 'Responsible Official
Mr. Belnick,
Please find attached a memo making changes to Colonial Pipeline Company's "Duly Authorized Responsible {official" for
our air and water programs. 1 am copying the affected Regional Supervisors within your Division on this e-mail but
please feel free to forward it to others that you think may need this information. Please note that I will be sending a
separate e-mail to the appropriate individuals within the Division of Air Quality. Thank you very much for your
assistance with this matter and please let me know if you need additional information or if I need to do something
more.
Sincerely,
F aron 1 , 1,eigli
Envii-caaanrental Specialist
Southeast 1 ietrict
FLei' h col i e.com
(3,36) 297 3 ;
This roes ss age contains PRWIT.F aFD € ND CONFIDENTIAL INFORMATION intended scr3ely for the use of the addrt.ssee(s)>naamed above.
Any disci 3! ure, distriitiedtion copying or use at the information by others is stfic.tlyy rut bfteed, If you have received this message in
error, please advise the sander by immediate retriy and eTs0ter the original message, age, Thank you,
4
a
T .
t

Colonial Pipeline Companv
(0)
Memo
Date: March Gi f. *
TO: file
AdanaWolfe*, Operations rations tanager - Texas
Kevin Cry, alskey, Operations s Manager — Louisiana
David Peeler, Operations Manager Mississippi
Troy Gibbons, Operations Manager ­ Tenn. /Alabama
Robert West, Operations Manager —Georgia
Mike Cutting*, Operations Manager —Charlotte/SC
Todd Daniel*, Associate Operations Manager Greensboro*
"rent Allen, Operation Manager —Virginia
Angie Kolar, Operations Manager _ Maryland
John Gent ler, Operations Manager —Woodbury
Steve Barnes, Associate Director of Operations, Northeast District
Randy Smith, District Environmental Manager -- Gulf, Coast District
Jeff Richards, District Environmental Manager Southeast District
Stara Carpenter, District Environmental Manager — Northeast District
►ct
Tom Cery rrra, Tom Kelly, Jeff f°rnrh r, Robert Hughes, Greg Glaze, Darren Pruitt, Gerald Reek
Frorm DougBelden, Vice President and General Manager, Operations
s
Duty Authorized Representative Delegation of:
Ir "Responsible Official" fear Purposes ofi he EPA Administered Air Permit Program
Il. "Respomible Corporate Officer' er' for Purposes of the PICA Administered f PDES Permit Program
ili. "Responsible Official" for Purposes of 40 CFR Part 63, National Emission Standards for Hazardous
Air Pollutants for Source Categories
This memo serves to document dray delegation of authority to the individuals set out below to act as Colonial's
"responsible offi ial"*., for purposes of the EPA Administered Air Permit Program (i.e. 40 Cl"R 70. ):
AdamWolfe*, Operations Manager - Texas
s Kevin Crybiskdy, Operations Manager Louisiana
David Peeler, Operations Manager — Mississippi
`rosy Gibbons, Operations Manager — Tenn./Alabama "
-4 Robert West, Operations Manager — Georgia
Mike Cutting*, Operations Manager — Charlotte/SC
- Todd Daniel*Associate Operations Manager -- Greensboro*
" er4on

pppppp,
(j) The foeffities employ more then 250 persons or have gross onnuol sales or expenditures exceeding $25
millinn (in second quarter 1980 dollars); or
hi) The delegation of authority to sucly representotives is approved in advance by the permitting authority;
As Vice President and General Manager, Operations, I am concidered a responsible official under §70,2, 1 serve as a
vital member on various Colonial policy/decision making teams, including Colonial's Leadership Team. My
responsibilities' include day-to-day oversight over Colonial's operations systern-wide. Reporting to me are Colonial's
three Directors of Operations, the Control Center Leader, and the Scheduling & Shipper Support Leader.
B. Delegation of Authority to Authorized Representatives
As provided above in 40 CFR §702(1), a duly authorized representative can act as a 'responsible, officiar if that
person is respomuble for the overall operation of one or more operating facilities applying for or subject to a permit
and the delegation of authority to such representative is approved in advance by the permitting authority,
Set out below are the individuals to whom I am delegating iny authority to act as "responsible official" and their area
of responsibility:
Adaria Wotfe*, Operations Manager - Texas. As Operations Manager -rexas, Adam Wolfe is responsible
for the overall operation of Colonial's Timas facilities and Coloniars Lake Charles Facility, Welsh Station
Facility, Church Point Facility, and Opelousas Delivery Facility in Louisiana.
Kevin Crybiskey, Operations Manager - Louisiana, As Operations Manager - Louisiana, Kevin Crybiskey is
responsible for the overall operations of Colonial's Krots Springs Facility, Baron Rouge, Tank Farm and
Facilities, and Felixville Facility in Louisiana.
David Peeter, Operations Manager - Mississippi, As Operations Manager -, Mississippi, David Peeler is
responsible for the overall operations of Coloniars Mississippi facilities and Colonial's Epes Station in
Alabama,
_4 Troy Gibbons, Operations Manager - Tenn. /Alabarna, As Operations Manager - Tenn. /Alabama, Troy
Gibbons is responsible for the overall operations of Coloniars facilities in Tennessee, overall operation of
Coloniars facilities in Alabarna (excluding Colonial's Epes Station), and Colonial's Chattanooga Junction and
Lookout Mountain Delivery Facility in Georgia,
Robert West, Operations Manager - Georgia. As Operations Manager - Georgia, Robert West is
responsible for the overall operations of Colonial's Georgia facilities from Alabarria to the Big Bear Creek BLV
(which is upstream of Athens), As Operations Manager - Georgia, Robert West is also responsible for, the
overall operations of Colonial's facilities from Atlanta Junction to the Etowah River BLV (which is
downstream of Rome).
Mike Cutting*, Operations Manager - Charlotte/W. As Operations Manager - Charlotte/SC, Mike Cutting
is responsible for the overall operations of Colonial's facilities downstream of the Big Bear Creek BLV (which
is upstream of Athens and includes Colonial's Athens and Danielsville facilities) in Georgia(. Charlotte,
Kannapolis and Gastonia facilities in North Carolina and of all CofonW's facilities in South Carolina.
Todd Daniel*, Associate Operations Manager - Greensboro*, As Associate Operations Manager
Greensboro, Todd Daniel Is responsible for the overall operation of all of cotoniars facilities in North
Carolina (with the exception of Colonial's Charlotte, Kannapolis and Gastonia facilities) and of Coloniars
Hickory Grove and Witt facilities in Virginia,
Trent Allen, Operations Manager - Virginia. As Operations Manager - Virginia, Trent Allen is responsible
for the overall operation of all of Colonial's facilities in Virginia *fth the exception of Colorvars Witt, Hickory
Grove, Remington, Bull Run, Chantilly; Fairfax, and Duties facilities).
Angie Kolar, Operations Manager - Maryland. As Operations Manager - Maryland, Angie Kolar is
responsible for the overall operations of Coloniars facilities in Maryland and Coloniars Remington, Bull Run,
Chantilly, Fairfax, and Dulles facilities located in Virginia.
John Gentzler, Operations Manager - gvoodburya As Operations Manager -- Woodbury, John Gentzler is
responsible for the overall operations of Colonial's Nev Jersey facilities (with the exception of Colonial's
Unden facility) and of Colonial's facilities in Pennsylvania.
3

Operations Manager — Georgia is responsible for the overall operations of Colonial's Georgia fadlifies from
Alabama to the Big Bear Creek 8LV (which is upstream of Athens). The Operations Manager — Georgia is
also responsible for the overall operations of Colonial's facilities from Atlanta Junction to the Etowah River
BLV (which Is downstfearn of Rome).
Operations Manager — Charlotte/W is responsible for the overall operations of Colonial's facilities
downstream of the Big Bear Creek 8LV (which is upstream of Athens and includes Colonial's Athens and
Darrielsville facilities) in Georgia, Charlotte, Kannapolis and Gastonia facilities in North Carolina and of all
Colonial's facilities in South Carolina.
-4 Associate Operations Manager — Greensboro* is responsible for the overall operation of all of Coloniars
facilities in North Carolina (with the exception of Colonial's Charlotte, Kannapolls and Gastonia facilities) and
of Colonial's Hickory Grove and Witt facilities in Virginia.
Operations Martager —Virginia is responsible for the overall operation of all of Coloniars facilities in Virginia
(with the exception of Colonial's Witt, Hickory Grove, Remington, Bull Run, Chantilly, Fairfax, and Duties
facilities).
-4 Operations Manager — Maryland is responsible for the overall operations of Colonial's facilities in Maryland
and Colonial's Remington, Bull Ron, Chantilly, Fairfax, and Dulles facilities located in Virginia,
_4 Operations Manager — Woodbury is responsible for the overall operations of Colonial's New Jersey facilities
(with the exception of Colonials Linden facility) and of Colonial's facilities in Pennsylvania.
-4 Associate Director of Operations, Northeast District is responsible for the overall operations of Colonial's
facilities in Linden, New Jersey.
Each Operations Manager, Associate Operations Manager, and Associate Director of Operations listed above is
responsible for operations in their respective areas, and are authorized to make management decisions which govern
the operation of the regulated facilities under their responsibility including (a) having the explicit or implicit duty of
making major capital investment recommendations* (b) initiating and directing other comprehensive measures to
assure long term environmental compliance with environmental laws and regulations; (c) ensuring that the necessary
systems are established or actions taken to gather complete and accurate information for permit application
requirements; and (d) having been delegated authority to sign documents in accordance with corporate procedures.
C. Delegation of Authority to Authorized Representatives
Under some state NPDES Programs, the positions identified in Section B, above may not be considered a "responsible
corporate offirer", as that term is defined tinder the respective state program. To the extent a delegation of authority
is required for the positions identified in Section B. above to be considered a duly authorized representative to act as
a 'responsible corporate officer" for purposes of the applicable state NPDES programs for other state water
programs), this memo is intended to document such delegation,
fit. National Emission Standards for Hazardous it Pollutants for Source Categories (i.e. 40 CFR
Part 63)
X My Status of "Responsible Official"
I am malting this delegation as a Colonial "responsible official" as that term is defined in 40 CFR §63,2,
40 CFR §63.2 provides, in part, the following definifions°
Responsible offirial means one of the following:
(1) For a corporation -A president, secretary, treosurer, or vice president of the corporation in charge of a
principal business function, or ony other person who performs ornflor policy or decision -making functions for
the corporation, or o duly authorized representative ofsoch person if the representative is responsible for
the overog operation of one or more manufacturing, production, or operating focffitles and either:
5

John Gentzler, Operations Manager — Woodbury, As Operations Manager — Woodbury,,John Gentzler is
responsible for the overall operations of Coloniai's New Jersey facilities (With the exception of Colonial's
Linden facility) and of Coloniat's facilities in Pennsylvania,
Steve Barnes, Assodate Director of Operations, Northeast Vistrict. As Associate Director of Operations,
Northeast District, Steve Barnes is responsible for the overall operations of Coloniars facilifies in Linden,
New Jersey.
As required by 40 CFR §63.2(1)(fi), Colonial intends to obtain the approval of this delegation from the Administrator.
Signed this 30'h day of March 2012.
Doug Belden
Vice Presiderst and General Manager, Operations
*tjfecdvedates.
(1) Adam Wolfe assuores therale of Operations Manager - Texas gffective Apfit 13, 2012, Adam succeeds Greg Glaze,
(2) Mike Cutting asstevres respcohilifities for the overoil ass, rabrois of Clabriari fadfilles davonstream of the ft Bear Creek SIV twhich is upstreom
4A thens and includes of is Athens and IhinielsuXe facifiticn) in Georgia Chatilurs tarn apofis and Gastonia *ifides in North Corisina and
ref fa Col oiawls facafties in South Carofirldeffective April 2, 2012 Mike Cutanqs title changesfrom "Operations Mmurger- Greensbuirolseirila"
to "OPMUM Manager- (harditle,6C"effective May 6,2012 Mike CuffingsucceedsAndyMortin,
For the periodof Aped 1, 2012 tolony 6,2012, A*ke Cuffingh; responsiblefor thefollaving,
for the overaft veraftons qf colonmrs jortmoss domstreom Qf the ft Bear Creek R"(which i5 upstrearn r4 Athens and includej
Colafflat's Athens and Cianielclilleflialifie-aim Gearlra, and renal tat(` ion tir foulifies lh.vuvi Cortsina, and
-4 for the overaNisuerations of all of Colonlarsfacilitan in NWh Carolina and of Cdoniars Hickory Grove and Wrafactlities in Virginia
0.) Tel Daniel, Associate Operotions Manager - Greensbool, assumes resprkisibility fir the rive rail oplrrotion of silt of Cotorval's jocifities In North
Comfina (wah the exception of CotonmPs Charlotte Xonnop* and Gastwid facifibes) and of Colonois s tick orr Grmw and mitt foaftes in
Virgmia effec&e May it 201 Z Prior to Moy 6, 201C overall operot ons of said facilities "n, under the responsibifiry of Mike Cutting
Ope-horn Manaqer - Green-sb-ol-Velme,
This redo area revises previous mrliw's datedJanuary 3, 2011 and Jorwary 4, 2012 ond reflects the 16116wing chroges in ajeos of resilwsibifides or other
(1) Ademi Wolfe, Operadom ManaW. - Texas is now responsible for the overall operation of ColoWars Texas jecifities ond Chlonlars Lake Chades
Facility, Welllw Station Faciffty, Church PiAnt Facility, ands p e .sas Delivery Facility in Louisiana, Addin assumes the inp, 01 Operatkirls Mallow
- Texas effectAw April 1,S 20,12,
(2) Mike Cuffir;y is now the Operations Manager- Charkpte/SC Mike ass the responsibilities of Operations Manager- GharloteAC effective
Apr# 1, 2012 and dw corresponding title an May 6, 2012,
04 Todd DOftiel, AS8060te QPM6--s M000ger - Greens tar is now responsible for the owyall ration of all of C616niars fordides it) North
Carolina ("dth the excepnewl of colaniati Chartatte, on pails and Gastcsira jacifideo and of Cent ors Hickory Grove and Win fiardiMo in
14ronia. Todd's new reuvmNitin become effective May 6,201Z
(4.) This memo continnes the previous memo dated Januaryf, 2011 toddreshrqj the My authorized representative de0gotion for purposes of tfae
EPA AdOgnictered A w Pe it Program ond the EPA Adnunritered NPDES Permit Program) and the Windus rnerno dated star vory 4, 2011
jaddresong the duty authcar rtied rep resenhitive delegation for purissses of Nationol Emission.Slandards for Hazoodous Air Pollutonts for source,
toteperfes),
7

NMEWR FiL
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
April 10, 2012
Mr. Michael A. Martin, Operations Manager
Colonial Pipeline Company
Post Office Box 87
Paw Creek, NC 28130
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline Company
NPIDES Permit No. NCO031038
Mecklenburg County, NO
Dear Mr. Martin:
On August 25, 2011, Olivia Edwards of the Mecklenburg County Water Quality Program (MCWQP)
conducted an inspection at the subject facility. This inspection was conducted as part of'a cooperative
working agreement between Mecklenburg County and the Division of Water Quality. The enclosed
report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not hesitate to call Ms.
Allocco, or me at this office.
Sincerely,
for Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty Rozzelle, MCWQP
John Culbreath, Colonial Pipeline Company, 7624 Kenstead Circle, Charlotte, NC 28130
RBK/OJE
Vooresville Regional Office One
-ocation: 610 East Center Ave,, Suite 301, Mooresville, NC 28115 NZ60arofina
:,hone: [phone] k Fax: [phone] \ Customer Service: 1-877-623-6748
Wurally
nta.mat• hffn,11mrfq1 nrAw nm1wPh1wn

z --
permitted'o4faft.'
M U017 Ing Z n
Le
•
Copies of effluent analytical results are readily available at the facility. Records, reports, and logs are
clear and well maintained.
FACILITY SITE REVIEW:
All of the major components of the facility were in service and appeared to be operating properly at the
time of the inspection, The facility has a General Wastewater Discharge Permit (NCG510207) to
discharge treated groundwater to an unnamed tributary of Gum Branch, a class WS-IV water in the
Catawba River Basin. The groundwater remediation system was not evaluated as part of the
inspection. The facility has a Wastewater Surface Irrigation Permit (WQ0004751), The spray irrigation
system was not evaluated as part of the inspection.
FLOW MEASUREMENT:
Flow is estimated at each outfall by calculation of the rainfall and drainage area.
LABORATORY:
Chemical analyses of effluent samples is performed by Prism Laboratories, Inc. (NC Laboratory
Certification #40). Prism Laboratories, Inc. was not evaluated during this inspection, Acute Toxicity
testing is performed by Environmental Testing Solutions, Inc. (NC Laboratory Certification Biological
#37). Environmental Testing Solutions, Inc, was not evaluated as part of this inspection.
EFFLUENTIRECEIVING WATERS:
The receiving waters were clear at the time of the inspection. No petroleum sheens were noted. The
facility discharges to an unnamed tributary to Gum Branch, which is a Class WS-IV water in the
Catawba River Basin.

NC Certification No. 402 Case Narrative
Full -Service Analytical NC Certification ter art N 0ri
IS MN�+ Drinking Water evert �!,?. 3773�u "� v//201 0
�r I Environmental Solutions
RECEIVED
DIVISION OF WATER QUALITY
"
Colonial Pipeline Company Project. Charlotte NPDES Stormwater
John Culbreath Project No.: NC 031038 A i' R — 1
P.O. Box 87 Lab Submittal Date: 09/27/ 010
Paw Creek, NC 28130 Prism Work Order: 0090620 S�1'F' SEC710N
OORES ILL : REGIONAL OFFICE
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody, Unlessotherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample, A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager Reviewed B
Data Qualifiers Key Preference.
D RPD value outside of the control limits.
LH High LCS recovery. Analyte not detected in the sample(s): No further action taken.-
M Matrix spike outside of the control limits.
SR Surrogate recovery outside the OC limits;
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All tither results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 5pringbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number. 1-8001629.6364 - Fax: 704782"409 Pi t, =

Sample Receipt Summary
Fuli-Service Analytical &
ISM I Enuironmentat Solutions
10/06/2010
U""taaetnraacswc...
Prism Work Order. 0090620
Client Sample; ID
Lab Sample ID
Matrix
©ate Sampled
Gate Received
W-COutfall-002 09/27/10 Lab
009020-01
Water
09/27/10
09/27/10
SW-Outfall-003 09/27110 Lab
0090620-0
Water
09/27110
09/27/10
SW lutfall-004 09/27110 Lab
0090620-03
Water
09/27/10
09/27/10
SW utfall-005i 09/27/10 Lab
0090620-04
Water
09/27/10
09127110
SW COutfall-006 09/27/10 Lab
0090620-09
Water
09/27/10
09127/10
S Outfall-008 09/27/10 Lab
0090620-06
Water
09/7/10
09/27/10
W-Outfall-007 09/27/10 Lab
0090620-07
Water
09/27/10
09/27/10
SW utfall-009 09/2 110 Lab
0090 0-0
Water
09/27/10
09/27/10
SW-COutfall-M C- 09/27/10 Lab
0090620-0
Water
09/27/10
09127/10
Samples received in good condition at 1.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc.
..
449 Sprintgbrook Road - P.O. Box 240643 - Charlotte; No 28224-0643
Phone: [phone] -Toll Free Number; 1-8001529.6384 -Fax, 7041825-0
l""`t' i wrwr
iorrrwuai�o�nuruuUiwuM
449

Laboratory Report
ISM
&k1V'LAR0RAT0A1P%
Full -service Analytical Is
5rtvtrnnmentat Solutions
1010612010
INC
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater
Client
Sample ID:
SW-Clutfall-002_09/27/10
Attn: John Culbreath
Prism
Sample ICI:
0090620-01
P.O. Box 87
Project No.: NCO031038
Prism
Work Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected. 09/27/10
10:30
Time Submitted: 09/27/10 15:40
Parameter
Batch
Result Units
Report
MDL
Dilution
Method
Analysis Analyst
Limit
Factor
Daterr me
ID
General Chemistry Parameters
Oil & Grease (HEM)
BRL
m91L
5.O
1.2
1 :
*1664A
9130/10 15:30
CDB
P010638
Phenolics
BRL
mg/L
0.050
0.018
1
*420.1
9/30/10 15:00
MRS
P010610
Total Suspended Solids
BRL
mg/L
5.0
1.5
1
*M 2540 D
10/1/10 13:50
JAB
POJ004
Turbidity
3.4:
NTU
0.40
0,025
1
*180.1
$128/10 9:16
JAB
P010572
5emivolatile Organic Compounds by GC/MS
1, ,4-Trichlorobenzene
BRL
ug/L
10
11
1
*625
9/29/10 15:26
KC
P010569
1,2-Dichlorobenzene
BRL
ug/L
10
2.0
1
*625
9/29/10 15:26
KC
P010569
1,3-Dichlorobenzene
BRL
ug1L
10
2A
1
"625
9/29/10 1526
KC
POIO569
1,4-Dichlorobenzene
BRL
ug1L
10
1.8
1
*625
9/29/10 15:26
KC
P010569
2.4,6-Trichlorophenot
BRL
ug1L
10
3.1
1
*625
9/29/10 '15:26
KC
P0I0569
,4-Dichlorophenot
BRL
ug/L
10
1.5
1
*625
9/29/10 1526
KC
P010569
2,4-Dimethylphenol
BRL
ugfL
10
2.4
1
*625
9129/10 15:26
KC
P0I0569
2,4-Dinittophenol
BRL'
ug/L
10
1.2
1
*625
9129/10 15:26
KC
P010569
,4-Dlnitrotoluene
BRL
ug/L
10
4,O
1 -
*625
9129110 15:26
KC
P010569
2,6-Dlnitrotoluene
BRL
ug1L
10
2.8
1
*625
9/29/10 15:26
KC
P0I0569
2-Chloronaphthalene
BRL
ug/L
10
3.0
1
*625
9/29/10 15:26
KC
P010569
2-Chlorophenol
BRL'
ug/L
10
1.7
1
*625
9/29110 15:26
KC
P010569
2-Nitrophenot
BRL <
ug/L
10
2A
1
*625
9/29/10 15:6
KC
POIO569
3,3"-Dichlorobenzidine
BRL,
ug/L
10
2.5
1
*625
9/29/10 15:26
KC
POIO569
4,6-Dinitro-2-methylphenol
BRL
ug/L
10
1.8
1
*625
9/29/10 15:26
KC
P010569
4-Bromophenyl phenyl ether
BRL
ug/L
10
2.O
1 '
*625
9/29/10 15:26
KC
P010569
4-Chloro-3-methylphenol
BRL
ug/L
10
2.2 "
1
"625
9/29/10 15:26
KC
P0I0569
4-Chlorophenyl phenyl ether
BRL
ugfL
10
2.9
1
`625
9/29/10 15:26
KC
P010569
4-Nitrophenol
BRL
ug/L
50
0,76
1
*625
9129/10 15:26
KC
POIO569
Acenaphthene
BRL
ugfL
10
4.1
1
*625
129/10 15:26
KC
P010569
Acenaphthylene
BRL
ug/L
10
2.8
1
*625
9/29110 15:26
KC
P010569
Anthracene
BILL
u/L
10
1.8
1
*625
9/29/10 15:26
KC
P0101569
Benzidine
BRL
ug/L
100
9A -
1
*625
9129/10 15:26
KC
P010569
Benzo(a)anthraoene
BRL-
ugtL
10
2.2
1 "
*625
9/29/10 1516
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
1.7
1
*625
9/29/10 15:26
KC
POIO569
Benzo(b)fluoranthene
BRL
ug/L
10
1.2
1
*625
9/29/10 15:26
KC
P010569
Benzo(g„h,i)perylene
BRL
ug/L
10
2A
1
*625
9129110 15,26
KC
P010569
Benzo(k)fluoranthene
BRL
ug/L
10
21
1
*625
9/29110 15:26
KC
P010569
bis(2-Chtoroetho; y)methane
BRL
ug/L
10
2;3
1
*625
9/29/10 15:26
KC
P010569
Bis(2-Chloroethyl)ether
BRL
ug/L
10
1.9
1
*625
9/29/10 15:26
KC
P010569
Bis(2-chloroisopropyl)ether
BRL
ug/L"
10
2.3
1
*625
9129/10 15:26
KC
P010569
Bis(2-Bthylhexyl)phthalate
BRL
ug/L
10
27
1
*625
9/29/10 15:26
KC
P010569
Butyl benzyl phthalate
BRL
ug/L
10
1:9
1
*625
9/29/10 1526
KC
P0I0569
Chrysene
BRL
ug/L
10
3:1
1
*625
9/29/10 15:26
KC
P010569
Dibenzo(a,h)anthracene
BRL
u /L
10
2:3 -
1
*625
9/29/10 15:26
KC
P0I0569
Diethyl phthalate
BRL
ugfL
10
2.2
1
`625
9/29110 "15:26
KC
P010569
Dimethyl phthalate
BRL
ugL
10
2.0
1
*625
9129/10 15:26
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone; 7041529.5354 -Toll Free Number: 1-8001529-5364 -Fax: 7
,,,.,,.
mega 7 Of 3
041525-0409

y �
Laboratory Report
MR T �,Environmental
&AOKASMA"Ift rt�..
F'Hi Service Analyboal
solutions
10/0612010
Colonial Pipeline Company Project: Charlotte NPDES Stormwater
Client Sample ID: S Outfall-002 0 /27/10
Attn: ,John Culbreath
Prism Sample ID. 0090620-01
P.O. Box 87
Project
No.: NCO031038
Prism fork Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/10 10:30
Time Submitted: 09/27/1016:40
Parameter
Result
Units
Report
MDL
Dilation -
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
tD
Di-n-butyl phthalate
BRL
ug/L
10
1.5
1
*625 9/29110 15:26
KC
POIO569
Di-n-octyl phthalate
BRL
ug/L
10
2.5
1
*625 9/29/10 15:26
KC
P010569
Fluoranthene
BRL
ug/L
10
1.5
1
r625 9/29110 15:26
KC
P010569
Fluorene
BRL
ug/L
10
4.4
1 "
*625 9/29/10 15:26
KC
P010569
Hexachlorobenzene
BRL
ug/L
10
2.1
1
*625 9129110 15:26
KC
P010569
Hexachlorobutadiene
BRL'
ugL
10
1.8
1
*625 9/29/10 15:26
KC
P010569
Hexachlorocyclopentadiene
BRL
ug/L
10
2.0
1
*625 9/29/10 15:26
KC
P010569
Hexachloroethane
BRL
ug/L
10
2.2
1
*625 9129/10 15:26
KC
P010569
Indeno(1,2,3-ed)pyrene
BRL
ug1L
10
3.6
1
*625 9/29/10 15:26
KC
P010569
lsophorone
BRL:
ug/L
10
Z6
1
*625 9129/10 15.26
KC
P010569
Naphthalene
BRL
ug/L
10
1.6
1
*625 9/29/10 15:26
KC
P010569
Nitrobenzene
BRL
ug/L
10
2.1
1
*625 9/29110 15:26
KC
P010569
N-Nitrosodimethylamine
BRL
ug1L
10
5,6
1
*625 9/291101526
KC
P010569
N-Nitroso-di-n-propylamine
BRL'
ug/L
10
2.2
1
*625 9/29/10 15:26
KC
P010569
N-Nitrosodiphenylomine
BRL'
ug1L
10
3.7
1
`625 9/29/10 15:26
KC
P010569
Pentachlorophenol
BRL
ug/L
10
2.1
1
*625 9/29/10 15:26
KC
P010569
Phenanthrene
BRL
ug1L
10
1.2
1
*625 9129/10 15:26
KC
P010569
Phenol
BRL:
ug/L
10
0.58
1
"625 9/29/10 15:26
KC
P010569
Pyrene
BRL"
ug/L
10
1.8
1
*625 9/29/10 15:26
KC
P010569
Surrogate
Recovery
LLControl Limitsµ
24,6-Tribromophenol
92 %
26-139
2-Fluorobiphenyt
83 %
41-112
2-Fluorophenol
40
10-48
Nitrobenzene-d5
79 %
34-10
Pheno1-d5
24
10-34
Terphenyl-d14
87 %
31-165
Volatile Organic Compounds by GC/PIDI LCD
Benzene
BRL
ug/L
0.50
0,066
1
*601/602 10/1/10 19:16
HPE
POJ0020
Ethylbenzene
BRL
ug/L
1.0
0.035
1
*601/602 10/1/10 19:16
HPE
POJ0020
m,p- ylenes
BRL
ug/L
2,0
0.11
1
*601/602 10/1/10 19:16
HPE
POJ0020
Methyl-tert-Butyl Ether
BRL
ug/L
5.0
0.17>
1
*601/602 10/1/10 19:16
HPE
POJ0020
o-xylene
BRL
ug/L
1,0
0,31
1
*601/602 10/l/10 19:16
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0,059
1
*601/60 10/l/10 19:16
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
�..,�,
Phone. 704t629.8354 - Toll Free Number: 1-800/6 9- 364 "- Fax. [phone]
of

Laboratory Report
n n
pn
XAOGtkATORkE$ YN4,.
Full -Service Analytical &
Environmental Sorutions
10/06/2010
Colonial Pipeline Company
Project. Charlotte NPDES
Stormwater
Client
Sample ID. SW-Outfall-003_09I27/10
Attn: Jahn Culbreath
Prism
Sample ID.
0090620-02
P.U. Box 87
Project No.: N O031038
Prism
Work Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/10 10 40
Time Submitted- 09/27/10 15,40
Parameter
Batch
Result Units
Report
MDL
Dilution
Method
Analysis Analyst
Limit
Factor
Date/Time
to
General Chemistry Parameters
Oil & Grease (HEM)
BRL
mg/L
5.0
1.2
1
*1664A
10/1/10 14:35
CDE
POJ0043
Phenolics
BRL
mg1L
0.050
0.018
1
*420.1
9/30/10 15:00
MRS
P010610
Total Suspended Solids
BRL
mg/L
5.0
1.5
1
*SM 2540 D
10/1110 13:50
JAB
POJ0024
Turbidity
2.1
NTU
0.40
0.026
1
*1 0A
9128MO 9:16
JAB
PO 0672
Semivolatile Organic Compounds by`GCIMS
1,2,4-Trichlorobenzene
BRL
ug/L
10
1.7
1
*625
9/29/10 17:10
KC
P010569
1,2-Dict lorobenzene
BRL
ug/L
10
2.0
1.
*625
9129/10 17:10
KC
P010569
1,-Dichlorobenzene
BRL
ug/L
10
2A
1
*625
9/29/10 17:10
KC
P010569
1,4-Dichlorobenzene
BRL
ug/L
10
1.8
1
*625
9/29/10 1710
KC
P010569
2,4,6-Trichlorophenol
BRL
ug/L
10
3A :
1 -
*625
9/29/10 17:10
KC
POIO569
2,4-Dici lorophenol
BRL
ug/L
10
1.5
1
*625
9/29/10 17:10
KC
P010569
2,4-Dimethylphenol
BRL-
ug7L
10
2A
1
*625
9/29/10 17:10
KC
P010569
2,4-Dinitrophenol
BRL
ug/L
10
1.2
1
*625
9/29/10 17:10
KC
P010569
2,4-Dinitrotoluene
BRL
ug/L
10
4.0
1
*625
9129/10 17:10
KC
P010569
2,6-Dinitrotoluene
BRL
= ug7L
10
2.8
1
*625
9/29/10 17:10
KC
P010569
2-Chloronaphthalene
BRL
ug/L
10
3.0
1
*625
9/29110 17:10
KC
P010569
-Chlorophenol
BRL
ug/L
10
1.7
1
*625
9129110 17:10
KC
POIO569
-Nitrophenol
BRL
ug/L
10
2A
1
*625
9/29/10 17:10
KC
P010569
3,3'-Dichlorobenzidine
BRL
ug/L
10
2.5
1 -
*625
9/29110 17:10
KC
P010569
4„6-Dinitro-2- ethylphenol
BRL
ug/L
10
1.8
1
*625
9129/10 17:10
KC
P010569
4-Bromophenyl phenyl ether
BRL
ug7L
10
2.0
1
*625
9129/10 17:10
KC
P010569
4-Chloro-3-methylphenol
BRL
ug7L
10
2.2
1
*625
9129110 17:10
KC
P010569
4-Chiorophenyl phenyl ether
BRL
ug/L
10
2.9 '
1 '
*625
9/29/10 17:10
KC
P010569
4-Nitrophenol
BRL
ug/L
50
0,76
1
*625
9129110 17:10
KC
P010569
Acenaphthene
BRL
ug/L
10
4A
1
*625
9129/10 1710
KC
P010569
Acenaphthylene
BRL
ug/L
10
2.8
1
*625
9/29/10 17:10
KC
P010569
Anthracene
BRL'
ug/L
10
1.s
1
*625
9/29110 17:10
KC
P010569
Benzidine
BRL
ug7L
100
9A
1
*625
9/29/10 1710
KG
P010569
Benzo(o)anthracene
BRL.
ug/L
10
2,2
1
"625
9/29/101710
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
1.7
1
*625
9/29110 1710
KC
POIO569
Benzo(b)fluoranthene
BRL
ug/L
10
1.2
1
*625
9/29/10 "17:10
KC
P010569
Benzo(g,h,i)perylene
BRL
ug/L
10
2.1
1"
*625
91291101710
KC
POIO569
Benzo(k)fluorantiene
BRL
ug/L
10
2.7
1
*625
9129/10 17:10
KC
P010569
bis(2-Chloroethoxy)methane
BRL
ug/L
10
2.3"
1
*625
9/29110 17:10
KC
P010569
Bis(2-Chloroethyl)ether
BRL
ug/L
10
1.9
1
*625
9/29110 17:10
KC
P010569
Bis(2-chloroisopropyl)ether
BRL
ug/L
10
2.3
1=
*625
9129/10 17:10
KC
P010569
Bis(2-Ethylhexyriphthalate
BRL
ug/L ,
10
27
1
`625
9129/10 17:10
KC
POIO569
Butyl ben yl phthalate
BRL
ug/L
10
1.9
1
*625
9/29110 1710
KC
P010569
Chrysene
BRL
ug/L
10
3A
1
`625
9/29110 17:10
KC
P010569
Dibenzb(a,h)anthracene
BRL
ug/L
10
2.3
1
*625
9/29/10 17:10
KC
P010569
Diethyl phthalate
BRIE
ug/L
10
2.2:
1
*625
9129/10 17:10
Kc
P010569
Dimeth l phthalate
BRL
ug/L
10
Zo
1
*625
9/29/10 17A0
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -
Charlotte;
NC 8224-064
Phone: [phone] - Toll Free Number. 1-800/629-6364 - Fix: 704162"40
e l

z
Laboratory Report
.'
t
F= 1€-Service Analytical &
Environments€ Sotuticns
10/0 /2010
Colonial Pipeline Company Project: Charlotte NPD S Stormwater
Client Sample ID: St-Outfall-003_09/27/10
Attn: Jahn Culbreath
Prism Sample
ID: 0090620-02
P.C. Sox 87
Project
No.. NCO031038
Prism Work Order: 0090620
Paw Greek, NC 28130
Sample Matrix: Water
Time Collected: 09127/10 10 40
Time Submitted: 09/27/10 1 :40
Parameter
Result
Units
Report MDL
Dilution
Method Analysis Analyst
etch
Limit
Factor
Date/Time
ID
Di-n-butyl phthalate
BRL
ug/L
10
1.5
1
*625 9/29/10 17:10
KC
P010569
Di-n-octyl ptthalate
BRL
ug/L
10
2.5
1
*625 9/29/10 17:10
KC
P010569
Fluoranthene
BRL
ugiL
10
1.5
1
*625 9/29/10 17:10
KC
P010569
Fluorene
BRL
ug/L
10
4A
1
*625 9129/10 17:10
KC
P010569
Hexachlorobenzene
BRL
ug/L
10
2.1
1
*625 /29/10 17:10
KC
POIO569
Hexachlorobutadlene
BRL
ug/L
10
1.8
1
*625 9/29110 17:10
KC
POIO569
Hexachlorocyciopentadiene
BRL
ug/L
10
2.0
1
*625 9/29110 17:10
KC
P010569
Hexachloroethane
BRL
ug/L
10
2.2
1
*625 9/29110 17:10
KC
P010569
Indeno(1„2,3-cd)pyrene
BRL
ugiL
10
3.6
1
*625 9129/1017:10
KC
P010569
lsophorone
BRL
ug/L
10
2.6
1
*625 9/29/10 17:10
KC
P0I0569
Naphthalene
BRL
ug/L
10
1.6
1
*625 9129110 17:10
KC
POIO569
Nitrobenzene
BRL
ug/L
10
211
1
*625 9/29/10 17:10
KC
P010569
N-Nitrosodimethylamine
BRL-
ug/L
10
5.6
1
*625 9/29110 17:10
KC
POIO569
N-Nitroso-&n-propylamine =
BRL:
ug/L
10
2.2
1
*625 9/29/10 17:10
KC
P010569
N-Nltrosod€phenylamine
BRL
ug/L
10
3.7
1
*625 9129/1017:10
KC
P010569
Pentachloropherrol
BRL
ug/L
10
2.1
1
*625 9/29110 17:10
KG
P010569
Phenanthrene
BRL
ug/L
10
1.2
1
*625 9129110 17:10
KC
P010569
Phenol
BRL
ug/L
10
0.58
1
*625 9/29/10 17:10
KC
P010569
Pyrene
BRL
ug1L
10
1,8
1
*625 9/29110 17:10
KC
POIO569
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
83 %
26-139
2-Fluorobiphenyl
80 %
41-112
2-Fluoroph not
39 %
10-48
Nitrobenzene-d5
78 %
34-102
Phenol-d5
23 %
10-34
Terphenyl-d14
75 %
31-165
Volatile Organic Compounds by GC1PIDIELCD
Benzene
BRL
ug/L
0,50
0.066
1
601/642 1011110 20:03
HPE
POJ0020
Ethylbenzene
BRL
ug/L
1.0
0.035
1
*601/602 10/1/10 20:03
HPE
POJ0020
m,p-Xylenes
BRL
ug/L
2.0
0,11
1
*601/602 10/1110 20:03
HPE
POJ0020
Methyl-tert-Butyl Ether
BRL
ug/L
5.0
0.17
1
*601/602 10/1f10 20:03
HPE
POJ0020
o-Xylere
BRL
ug/L
1.0
0.31 -
1
*601/602 1011/10 20:03
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0.059
1'
*601/602 10/1/10 20:03
HPE
POJ0020
This report should not be reproduced„ except in Its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 24054 - Charlotte, NC 29224-0643
Phone: [phone] - Toll Free Number. 1.8001629.6364 - Fax. [phone]
z9
t71 «

t x
r,
Laboratory Report
ISM I
ffl
Full-Service Analytical &
Environmental solutions
10106/2010
MM aABORArOWS, f.M
Colonial Pipeline Company
project: Charlotte NPDES Stormwater
Client
Sample ID:
SW-Outf ll-004_09/27/10-
Attn: John Culbreath
Prism
Sample ID:
0090620-03
P.O. Box 87
Project No.: NCO031038
Prism
Work Order: 0090620'
Paw Greek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/10 1320
Time Submitted: 09/27/10 1 a:40
Parameter
Result Units
Report
MDL
Dilution"
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Oil & Grease (HEM)
BRL
mg1L
5.0
1.2
1
*1664A
10/1/10 14:35
CDR
POJ0043
Phenolics
BRL
mg1L
0.050
0.018 "
1
*4 0.1
9/30110 15:00
MRS
P010610
Total Suspended Solids
BRL
mg7L
5.0
1.5
1
*SM 2540 D
10/1/10 13:50
JAB
POJ0024
Turbidity
2.2
NTU
0.40
0.026
1
*1 0.1
WWI 9:16
JAB
P010672
Sernivolatile Organic anic Compounds by'GC/MS
1,2„4-Trichloroben ene
BRL
ug/L
10
1.7
1
*625
9/29/10 17:44
KC
P010569
1,2-Dichlorobenzene
BRL:
ug/L
10
10
1
`625
9/29/10 17:44
KC
P010569
1,3-Dichlorobenene
BRL
ug7L
10
2.1
1"
*625
9/29/10 17:44
KC
P010569
1,4-Dichlorobenzene
BRL
ug/L
10
1.8
1
*625
9/29/10 1744
KC
P010569
2,4,6-Trichlorophenol
BRL
ug/L
10
3.1
1
*625
9/29/10 17:44
KC
P010569
2,4-Dichlorophenol
BRL
ug/L
10
1.5
1
*625
9129/10 17:44
KC
P010569
,4-Dimethylphen0l
BRL
ug/L
10
2A
1
*625
9129/10 1744
KC
P010569
2,4-Dinitrophenol
BRL
ug/L
10
1.2
1
*625
9129110 17A4
KC
P010569
2,4-Din€trotoluene
BRL
ug/L
10
4.0
1
*625
9/29/10 IT44
KC
P010569
2,6-Dinitrotoluene
BRL
ug/L
10
2.8
1
*625
9/29/10 17:44
KC
P010569
- hlorbnaphthalene
BRL
ug/L
10
3.0
1
*625
9/29110 17:44
KC
P010569
2-Chloropheno€
BRL"
ug/L
10
1.7
1
*625
9/29/10 IT44
KC
P010569
2-N€tropheno€
BRL
ug/L
10
2A
1
*625
9/29/10 17:44
KC
P010569
,3'-Dichlorobenzidine
BRL
ug/L
10
2,5
1 .
*625
9129/10 17:44
KC
P010569
4,6-Dinifro-2-methylphenol
BRL <
uglL
10
1.8
1
*625
9129/10 17:44
KC
P010569
4-Bromc phenyl phenyl ether
BRL
ugtL
10
2.0
1
*625
9/29/10 17:44
KC
POIO569
4-Chloro-3-methytphenol
BRL
ug/L
10
2.2
1
*625
9129/10 17:44
KC
POIO569
4-Chlorophenyl phenyl ether
BRL
ug/L
10
2.9
1
*625
9/29/10 17:44
KC
P010569
4-Nitrophenot
BRL
ug/L
50
0,76:
1
*625
9/29/10 17:44
KC
P010569
Acenapt thene
BR[_
ug/L
10
4.1
1
`625
9/29/10 17:44
KC
P010569
Acenaphthylene
BRL
ug/L
10
2.8
1
*625
9/29/10 17:44
KC
P010569
Anthracene
BRL
uglL
10
1.8
1
*625
9/29110 17:44
KC
P010569
Benzidir a
BRL
ug/L
100
9A
1
*625
9129/10 '17A4
KC
PDIO569
Ben o(a)anthracene
BRL
ug/L
10
2.2
1
*625
9/29110 17:44
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
13
1
*625
9129110 '17:44
KC
P010569
Benzo(b)fiuoranthene
BRL
ug/L
10
12
1
*625
9/29/10 17:44
KC
P010569
Benzo(g,h,i)peryl ne
BRL
ug/L
10
2A
1
*625
9/29110 17A4
KC
POi0569
Benzo(k)fluoranthene
BRL
ug/L
10
2:7
1
*625
9/29110 17:44
KC
PO OS69
bis(-Chloroethoxy)methane
BRL
ug/L
10
2.3
1
*625
9129110 17:44
KC
P0I0569
Sis(2-Chloroethyl)ethef
BRL
ug/L
10
1.9
1
*625
9/29110 17:44
KC
P010569
Bis(2-chloroisopropyl)ether
BR)
ug/L
10
2.3
1
*625
9/29110 17:44
KC
P010569
Bis(2-Bthylhexyl)phtha€ate
BRL
ug/L
10
2,7
1
*625
9/29/10 17:44
KC
POIO569
Butyl benzyl phthalate
BRL.
ug/L
10
1.9
1
*625
9/29110 17:44
KC
P010569
Chrysene
BRL'
ug/L
10
3A
1
`625
9/29110 17:44
KC
P010569
Dibenzo(a„h)anthracene -
BRL
ug/L
10
Z3
1
*.625
9729110 17:44
KC
P010569
Diethyl phthalate
BRL
ug/L
10
2.2
1
*625
9/29/10 17:44
KC
P010569
Dimethyl phtha€ate
BRL
ug/L
10
2.0
1
*625
9/29110 17:44
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc,
449 xpringbrook Road • P.O. Box 240643 - Charlotte,
NC 28224-0643
,..
Phone: [phone] - Toll Free Number: 1-800/6r29-6364 - Fax: [phone]
P
of

A -1 �k
Laboratory Report
Ak
Full-Service Analytical &.
..
10/06/2010
,,
Environmental Solutions
Colonial Pipeline Company Project: Charlotte NPDES Stormwater
Client Sample
IDSW tOutfall-004 09/27/10
Attn: John Culbreath
Prism Sample
ID: 0090620-03
P.O. Box 87
Project No.:
NCO031038
Prism Work Order: 0090620
Paw Greek, NC 28130
Sample Matrix: Water
Time Collected:
09/27/10 13`20
Time Submitted: 09/27/10 15:40
Parameter
Result
Units
Report MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
DatefTlme
10
Di-n-butyl phthalate
BRL
ug/L
10
1.5
1
`625 9/29110'17A4
KC
P010569
Di-n-octyl phthalate
BRL
ug/L
10
2.5
1
*625 9/29/10 17:44
KC
POIO569
Fluoranthene
BRL-
ug/L
10
1.5
1
*625 9/29110 17:44
KC
P010569
Fluorene
BRL
ug/L
10
4A
1
*625 9/29110 17:44
KC
P010569
Hexachlorobenzeae
BRL
ug/L
10
2.1
1
*625 9/29110 17:44
KC
P010569
Hexachlorobutadiene
BRL
ug7L
10
1.8
1
*625 9/29/10 17:44
KC
P010569
Hexachibrocyclop ntadiene%
BRL
ug/L
10
2.0
1
*625 9/29/10 17:44
KC
P010569
Hexachloroethane
BRL.
ug7L
10
2.2
1
*625 9/29/10 17:44
KC
P010569
Indeno(1,2,3-cd)pyrene
BRL-
uglL
10
3.6
1
*625 9129/10 17:44
KC
P010569
isophorone
BRL
ug/L
10
2.6
1
*625 9129/10 17:44
KC
P010569
Naphthalene
BRL
ug/L
10
1.6
1
*625 9/29/10 17:44
KC
P010569
Nitrobenzene
BRL
ug/L
10
2.1
1
`625 9/29/10 17:44
KC
P010569
N-Nitrosodfinethylamfne
BRL
ug/L
10
5.6
1
*625 9/29/10 17:44
KC
P010569
N-Nitroso-di-n-propylamine
BRL
ug/L
10
2.2 ,
1 '
*625 9/29/10 17:44
KC
P010569
N-Nitrosodiphenylamine
BRL
ug/L
10
3.7
1
*625 9/29/1017A4
KC
P010569
Pentachlorophenof
BRL
ug7L
10
2.1 '
1
*625 9/29/10 17:44
KC
P010569
Phenanthrene
BRL
u/L
10
1.2
1
625 9/29/10 17:44
KC
P010569
Phenol
BRL,
ug/L
10
0,58
1
*625 9129/10 17:44
KC
P010569
Pyrene
BRL
ug/L
10
1.8
1
*625 9/29110 17:44
KC
P010569
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
2 -139
2-Fluorobiphenyl
68 %
41-11
-Fluorophenol
33 %
70-48
Nitrobenzene-d5
67 %
34-102
Phenol-d5
19
10-34
Terphenyf-d14
68 %
31-165
Volatile Organic Compounds by G /PID/ELCD
Benzene
BRL
ug/L
0,50
0,066
1.
*601/602 10/1110 20:50
HPE
POJ0020
Ethylbehzene
BRL
ug/L
1.0
0.035
1
*601/602 1011110 20:50
HPE
POJ0020
tn,p-Xyl nes
BRL
ug/L
2.0
0.11
1
*601/602 10/1110 20:60
FIFE
POJ0020
ethyt-tert-Butyl Ether
BRL
ug/L
5;0
0.17
1
*601/602 1011110 20:50
HPE
POJ0020
o-Xylene
BRL
ug/L
1;0
0.31,
1
*6011602 10/1/10 20:50
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0.059
1
*601/602 10/1/10 20:50
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte; NO 28224.0643
.,...�.�..
Phone. 7041 2"364 - Toll Free Number: 1-8001529.6364 - Faux. 704152E-0409
Page
8 7 35

;.
Laboratory Report
z` t Full -Service Analytical 8
ISM Environmental Solutions
10/06/2010
Colonial Pipeline Company
Project: Charlotte NPD S Stor lwater
Client
Sample ID.
S Outfall-005_09/27/10
Attn: John Culbreath
Prism
Sample ID:
0090620-04
P,O. Box 87
Project No,,. N O0 1038
Prism
Work Order, 0090620
Paw Creek, NC 28130
Sample Matrix, Water
Time Collected. 09/
7/10 13:30
Time Submitted: 09/27/10 1:40
Parameter
Result Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Oil & Grease (HEM)
BRL
mg/L
5.0
1.2 "
1
*1664A
1011110 15:00
CDE
POJ0043
Phenolics
BRL
mg/L
0.050
0,018
1
*420A
9130/10 15 00
MRS
P010610
Total Suspended Solids
BRL
mg/L
&0
1.5
1
*SM 2540 D
10/1110 13:50
JAB
POJ0024
Turbidity
2.4:
NTU
OAO
0.026
1
*180A
9128/10 9:16
JAB
P010672
rnivolatCle Organic Compounds by"GC/MS
1,2,4-Trlchlorobenzene
BRL
ugfL
10
1.7
1
*625
9/29/10 18:18
KC
P010569
1,2-Dici iorobenz ne
BRL
ug/L
10
2.0
1 ;
*625
9/29/10 18:18
KC
POIO569
1,-Dichlorobenzene
BRL.
ug/L
10
2.1
1
*625
9/29/10 18:18
KC
POIO569
1,4-Dichlorobenzene
BRL
ug7L
10
1.8
1
*625
9/29110 "18:18
KC
P010569
2,4,6-Trchlorophenot
BRL
ug/L
10
3.1 -
1
*625
9/29/10 18:18
KC
POIO569
2,4-Dichlorophenol
BRL
ug/L
10
1.5
1
*625
9129/10 18:18
KC
POIO569
2,4-Dimethyiphenot
BRL
ugfL
10
2A
1
`625
9/29110 18:18
KC
P010569
2,4-Dinitrophenol -
BRL
ug7L
10
1,2
1
*625
9/29/10 18:18
KC
P010569
,4-Dinitrotoluene
BRL
ug/L
10
4.0
1
*625
9/29/10 18:18
KC
P010569
2,6-Dlnitrotoluene-
BRL
ug/L
10
2.8
1
*625
9/29/10 18:18
KC
P010569
2-Chlorc naphthalene
BRL
ugJL
10
10
1
*625
9/29/10 1818
KC
P010569
2-Chlorophenol
BRL
ug/L
10
1.7
1
*625
9129/10 18:18
KC
P010569
2-Nitrophenot
BRL
ug7L
10
2A '
1-
*625
9/29/10 18:18
KC
P010569
3,T-Dichlorobenzidine
BRL
ug7L
10
2.5
1
*625
9/29110 18:18
KC
P010569
4,6-Dinitro-2-methylphenol
BRL
ug7L
10
1,8 "
1
*625
9129/10 18:18
KC
P0I0569
4-Bromophenyt phenyl ether
BRL
ugfL
10
2.0
1
*625
9/29/10 "18:18
KC
POIO 69
4-Chlore-3-methylphenot
BRL
ug7L
10
2.2
1
*625
9/29/10 18:18
KC
P010569
4-Chlorophenyt phenyl ether
BRL
ug/L
10
2.9
1
*625
9/29/10 18:18
KC
P010569
4-Nitrophenol
BRL:
ug7L
5o
0,76
1
*625
9/29/10 18:18
KC
P010569
Acenaphthene ;
BRL
ug/L
10
41
1
*625
9129/10 18,18
KC
P010569
Acenaphthylene
BRL
ug7L
10
Z8
1;
*625
9129110 18:18
KC
P010569
Anthracene
BRL
ug/L
10
1,6
1
*625
9/29/10 18:18
KC
POIO569
Benzidine
BRL
ug/L
100
9A
1
*625
9/29/10 '18:18
KC
P010569
Benzo(4)anthracene
BRL
ug7L
10
2.2
1.
*625
9/29/10 18:18
KC
P010569
B nzo( )pyrene
BRL
ugfL.
10
11
1
*625
9/29/10 18:18
KC
POIO569
Benzo(b)fluoranthene
BRL.
ug/L
10
1,2
1
*625
9/29110 18:18
KC
P010569
Benzo(g,hJ)perylene
BRL
ugiL
10
2A
1
*625
9/29110 18:18
KC
P010569
Benzo(k)fluoranthene
BRL
ugfL
10
27
1
*625
9/29/10 18:18
KC
P010569
bis(2-Chloroethoxy)methane
BRL
ug/L
10
2:3
1"
*625
9/29/10 18:18
KC
P010569
Bis(2-Chloroethyl)ether
BRL.
ugfL
10
1.9"
1
*625
9/29/10 18:18
KC
P010569
Bis(2-ci loroisoprepyl)ether
BRL
ugiL
10
2.6
1
*625
9/29/10 18:18
KC
P0I0569
Bis(2-Ethythexyl)phthalate
BRL
ug/L
10
2.7
1
*625
9/29/10 1818
KC
P010569
Butyl benzyl phthalate
BRL.
ug/L
10
1.9
1
*625
9/29110 18:18
KC
P010569
Chrysene
BRL
ugiL
10
3.1
1
*625
9/29/10 18:18
KC
POIO569
Dibenzo(a,h)anthracene
BRL
ug/L
10
2.3
1
*625
9129/10 18:18
KC
P010569
Diethyl phthalate
BRL.
ug/L
10
12
1
*625
9/29/10 18:18
KC
P010569
Dimethyl phthalate
BRL
ugiL
10
2.0
1
*625
9/29/10 18:18
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 • Charlotte, NC 28224-0643.
�,
'
Phone. 704/62"364 - Toll Free Number: 1-8001629-6364 -
Fax: [phone]
f

*
Laboratory Report
5 ;
FDA
��'t+�xxnrxxaate, tad.
FuibService Analytical 8
Environnientai Solutions
10/06/2010
Colonial Pipeline Company Project: Charlotte NPDES Stormwater
Client Sample
ID: SW Outfall-00 _0 /27/10—
Attn: John Culbreath
Prism Sample
ID: 0090620-04
P.O. Box 87
Project
No.: NCO031038
Prism Work Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected:
09127/10 13: 0
Time Submitted. 09/27/10 1 a:40
Parameter
Result
units
Report MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor;
Date/Time
ID
Di-n-butyl phthalate
BRL `
ugfL
10
1.5
1
*625 9/29110 18:18
KC
P01O569
Di-n-octyl phthalate
BRL
ug1L
10
2.5
1
*625 9/29110 18:18
KC
P010569
Fluoranthene
BRL"
ug/L
10
1.5
1 ,"
*625 9/29110 18:18
KC
P010569
Fluorene
BRL
ug/L
10
4A
1 "
*625 9/29/10 1&18
KC
P010569
Hexachlorobenzane
BRL
ugfL
10
21
1
*625 9/29110 18:18
KC
P010569
Hexachlorobutadiene
BRL
ug1L
10
1.8
1
*625 9/29110 18:18
KC
P010569
Hexachlorocyclopentadiene
BRL
ug/L
10
2.0 :
1
*625 9/29/10 18:18
KC
P010569
Hexachlproethane
BRL
ug/L
10
2.2
1
*625 9/29/10 18:18
KC
P010569
€ndeno(1,2,3-cd)pyrene
BRL
ug1L
10
3.6
1
*625 9129/1018:18
KC
P010569
lsophorone
BRL.
ug1L
10
2.6
1
*625 9/29110 18:18
KC
P010569
Naphthalene
BRL
ug/L
10
1.6
1
*625 9/29/10 18:18
KC
P010569
Nitrobenzene
BRL
ugfL
10
2A
1
*625 9/29/10 18:18
KC
P010569
N-Nitrosodimethylamine
BRL
ugfL
10
5.6
1
*625 9/29/10 18:18
KC
POIO569
N-Nitroso-di-n-propylamine
BRL
ug1L
10
2.2
1
*625 9/29/10 18:18
KC
P010569
N-Nitrosodiphenylamine
BRL
ugtL
10
3.7
1
*625 9/29/10 18:18
KC
P=569
Pentachlorophenol
BRL
ugfL
10
Z1
1
`625 9/29/10 18:18
KC
P010569
Phenanthrene
BRL
ug1L
10
1.2
1
*625 9/29/10 18:18
KC
P010569
Phenol
BRL
ugfL
10
0,58
1
*625 9/29/10 18:18
KC
P010569
Pyrene
BRL
ug1L
10
1.8
1 -
*625 9/29110 18:18
KC
P010569
Surrogate
Recovery
Control Limits
24,6-Tribromophenol
85%
26-139
2=Fluorobiphenyl
85 %
41-112
2-Fluorophenol
41%
10-48
Nitrobenzene-d5
8 %
34-102
Phenol-d5
24 %u
1034
Terphenyl-dl4
82 %
31-165
Volatile Organic Compounds by GC/PIDIELCD
Benzene
BRL
ugtL
0.50
0,066
1
*601/602 10t1/10 21:37
HPE
POJ0020
Ethylbenzene
BRL
ug/L
1.0
0,035
1
*601/602 10/1110 21:37
HPE
POJ0020
m,p-Xyl nes
BRL.
ug/L
2.O
0,11
1
*601/602 10/1/10 21:37
HPE
POJ0020
Methyl -tort -Butyl Ether
BRL
ug/L
5.0
0,17
1
*6011602 10/1110 21.37
HPE
POJ0020
o-Xylene
BRL
ug/L
1.0
0.31
1
*6011602 1011/10 21:37
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0.059
1
*6011602 1011/10 21:37
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 >pringbrook Road - P.O. Box'240643 • Charlotte, NC 28224-0643
Phone: [phone]$64 •Toll Free Number: i-80015+3•364 -Fax: 704f82ii-0409
.. ,� .�,.
Page 1 f '
5

Laboratory Report
LODFu9M3 ruica Analytical &
*1 Environmental Solutions
��'�,aei+iwaroa�e� rrac,:�:
10/06/2010
Colonial Pipeline Company
Project: Charlotte NPD S Stormwater
Client
Sample ID:
SW Outfall-006_09/27110
Attn: John Culbreath
Prism
Sample ID:
0090620-05
P.0, Box 87
Project No,: NCO031038
Prism
Work Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/10 13:4
Time Submitted: 09/27110 15:40
Parameter
Result Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor =
Dateliirne
ID
General Chemistry Parameters
Oil & Crease (HENS)
BRL
mg/L
&0
1,2
1
*16 +4A
1011/10 15:00
CDE
POJ0043
Phenolics
BRL
mg1L
0.050
0.018
1
*4201
9130/10 15:00
MRS
P010610
Total Suspended Solids
BRL
mg/L
5.0
1.5
1
*SM 2540 D
10/1/10 13:50
JAB
POJ0024
Turbidity
4.1 "
NTIJ
0,40
0.026 '
1
*180A
9129/10 :16
JAB
P010672
Semivolatile Organic Compounds by GiC1M
1,2,4-Trichlorobenxene
BRL
ug/L
10
1.7
1
*625
9129/10 18:52
KC
P010569
1,2-Dichlorobenzene
BRL
ug/L
10
2.0
1
*625
9/29/10 18:52
KC
P010569
1,3-Dichlorobenzene
BRL
ug/L
10
2A
1
*625
9/29/10 18:52
KC
P010569
1,4-Dichlorobenzene
BRL
ug/L
10
1.8
1
*625
9/29/10 18:52
KC
P010569
2,4,6-Trichlorophenot
BRL
ug/L
10
3A
1
*625
9/29/10 18:52
KC
P010569
2,4-Dichlorophenol
BRL
ug1L
10
1.5
1
*625
9/29110 18:52
KC
POIO569
2,4-Dimethylphenot
BRL
ug/L
10
2A
1
*625
9129/10 18:52
KC
POIO569
2,4-Dinitrophenof
BRL
ug/L
10
1.2
1
*625
9/29110 18:52
KC
P010569
2„4-Dinitrotoluene"
BRL
ug/L
10
4.0
1
*625
9/29/10 18:52
KC
POIO569
,6-Dinitrotoluene
BRL
ug/L
10
2.8 '
1
*625
9129110 18:52
KC
P010569
-Chloronphthatene
BRL
ug/L
10
3.0
1
*625
9f29/10 18:52
KC
P010569
2-Chlorophenot
BRL
ug/L
10
1.7
1
*625
9/29110 18:52
KC
P010569
2-Nitrophenol
BRL
ug/L
10
2A
1
*625
9/29/10 18:52
KC
P010569
3,3"-Dichlorobenzidine
BRL
ug/L
10
2.5
1
*625
9/9/10 18:52
KC
P010569
4,6-Dinitro-2-met ylphenot
BRL"
ug/L
10
1,8
1
*625
9129/10 18:52
KC
POIO569
4-Bromophenyl phenyl ether
BRL
ug/L
10
2.0
1
*625
9129/10 18:52
KC
POIO569
4-Chloro-3-methylphenot
BRL
ug/L
10
2.2
1
*6225
9/29/10 18:52
KC
P010569
4-Chlorophenyl phenyl ether
BRL
ug/L
10
2.9
1
*625
9/29/10 18:52
KC
P010569
4-Nitrophenot
BRL
ug/L
50
0.76
1 ;
*625
9/29110 18:52
KC
P010569
Acenaphthene
BRL
ug/L
10
4.1
1
*625
9/29/10 18.52
KC
P010569
Acenaphthylene
BRL
ug/L
10
2.8
1
*625
9/29/10 18:52
KC
POIO669
Anthracene
BRL
ug/L
10
1.8
1
*625
9/29110 18:52
KC
P010569
Benzidine
BRL'
ug/L
100
9.4
1
*625
9129/10 18:52
KC
P010569
Benzo(u)anthracene
BRL
ug/L
10
2.2
1
*625
9f29/10 16:52
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
17
1
*625
9/29110 18:52
KC
P010569
Benzo(b)ftuoranthene
BRL
ug/L
10
1.2
1
'*.625
9/29110 18:52
KC
P01069
Benzo(g,i1,i)perylerre
BRL
ug/L
10
2.1
1
`625
9/29/10 18:52
KC
P010569
Benzo(k)fluoranthene
BRL
ugfL
10
2.7
1
`625
9129/10 18:52
KC
P010569
bis(2-Chloroethoxy)methane
BRL
ug/L
10
23
1
*625
9129110 18:52
KC
POIO569
Bis(2-Chloroethyl)ether
BRL
ug/L
10
1,9
1
*625
9/29/10 18:52
KC
P010569
Bis(2-chloroisopropyl)ether
BRL
ug/L
10
2.3
1
*625
9/29/10 18:52
KC
POIO569
Bis(2-Ethylhexyl)phthatate
BRL
ug/L
10
2.7
1
*625
9/29/10 18:52
KC
P010669
Butyl benzyl phthalate
BRL
ug/L
10
1.9
1
*625
9/29110 18:52
KC
P010569
hrysene
BRL
ug/L
10
3.1
1
`625
9/29110 18:52
KC
P010569
Dibenzo(a,h)anthracene
BRL
ugrL
10
2.3
1
*625
9129/10 18:52
KC
P010569
Diethyl phthalate
BRL
ug/L
10
21
1
*625
9/29110 18. 2
KC
P010569
Dimethyl phthalate
BRL
ug/L
10
2.0
1
*625
9/29/10 18. 2
KC
P0I0569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte,
NC 29224-0643
Phone. [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone]
page
1197 35

r
Laboratory Report
R I S I
ERRF
40-Service Analytical &
Solutions
10/0612010
RING:
Enviroornentsl
Colonial Pipeline Company Project: Charlotte NPDES Stormwater
Client Sample ID. SW-Outfall-006 09/27110-
Attn: John Culbreath
Prism Sample ID: 0090620-05
P,O. Box 87
Project No.:
NCO031038
Prism WorkOrder-, 0090620
Paw Creek, NC 28130
Sample Matrix: Water
;
Time Collected: 09/27/10 13`:45
Time Submitted: 09127/10 1 :40
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Datef rime
ID
Di-n-butyl phthalate
BRL
ug/L
10
1.5
1 *625 9129/10 18:52
KC
P0I0569
DI-n-octyC phthalate
BRL
ug/L
10
2.5
1 *625 9/29110 18:52
KC
POIO569
Fluoranthene
BRL
ug/L
10
1.5
1 *625 9/29110 1&52
KC
P010669
Fluorene
BRL
ug7L
10
4A
1 *625 9/29/10 18:52
KC
POIO669
Hexachl srobenzene
BRL
ug/L
10
2A
1 *625 9/29/10 18:52
KC
P010569
Hexachlorobutadiene
BRL
ugfL
10
1.8
1 *625 9/29/10 18:52
KC
P010569
Hexachlorocyclopentadiene
BRL'
ug/L
10
2.0
1 *625 9/29110 18.52
KC
P010569
Hexachloroethane
BRL
ugfL
10
2.2
1 *625 9/29/10 18:52
KC
P010569
lndeno(1,2,3-cd)pyrene
BRL-
ug/L
10
3.6
1 *625 9/29/10 18:52
KC
POI4569
Isophorc ne
BRL-
ug/L
10
2.6
1 *625 9/29/10 18:52
KC
P010569
Naphthalene
BRL
ugfL
10
1.6
1 *625 9/29/10 18:52
KC
P010569
Nitrobenzene
BRL
ugfL
10
2A
1 *625 9/29/10 18:52
KC
P010569
N-Nitrosodimethylamine
BRL"
ug/L
10
5.6
1 *625 9/29110 18:52
KC
P010569
N-Nitroso-di-n-propylamine
BRL
ugfL
10
2,2 %
1 *625 9/29/10 18:52
KC
P010569
N-Nitrosodiphenyla ine
BRL
ug1L
10
3.7
1 *625 9/29/10 18:52
KC
POIO 69
Pentachlorophenot
BRL
ugtL
10
2.1
1 *625 9/29/10 1&52
KC
P010569
Phenanthrene
BRL:
ugfL
10
1.2
1 *625 9129/10 18:52
KC
P010569
Phenol
BRL
ugfL
10
0.58 "
1 *625 9129/10 18:52
KC
P010569
Pyrene ,
BRL
ugfL
10
1.8
1 *25 9/29/10 18:52
KC
P010569
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
85 %
26-139
2-Fluorobiphenyl
78
41-112
2-Fluorophenol
9 %
10-48
Nitrobenzer e-d5
75 o
34-102
Phenol-d
24 %
10-34
T rphenyl-d14
79 %
31-165
Volatile Organic Compoundsby GCIPIDIELCD
Benzene
BRL
ug/L
0.50
0,066
1 *601/602 10f1/10 22.24
HPE
POJ0020
thylbenzene
BRL
ugfL
1.0
0,035
1 *601/602 10/1/10 22:24
HPE
POJ0020
m,p-Xylenes
BRL
ug7L
2.0
0,11
1 *601/602 10/1110 22:24
HPE
POJ0020
Methyl-tert-Butyl Ether
BRL
ug/L
5.0
0.17
1 *601/602 10/1110 22:24
HPE
POJ0020
o-Xylene
BRL
ugfL
1:0
0,31
1 *6011602 10/1/10 22:24
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0,059
1 *6011602 10/1110 22:24
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240 - Charlotte, NC 28224.0643
Phone: [phone]i364 - Toll Free Number: 1.8001629- 364 .
Fax: 7041 2"409
c�972
7777,
wirwrrrwwww

Laboratory Report
Alamad
Fuir- ervica Analytical &
Eaviroornantal solutions
10/06/2010
�c.n '. sv�rs teat...
..
Colonial Pipeline Company
Project: Charlotte NPDES
Stormwater
Client
Sample ID:
SW Qutfall-008_09/27110
Attn: John Culbreath
Prism
Sample ID.
0090620-06
P.Q. Box 87
Project No.: NCO031038
Prism
Work Order:
0090620
Paw Creek, NC 28130
Sample Matrix: 'Water
Time
Collected: 09/ 7/10 11 00
Time
Submitted. 09/27/10 15:40
Parameter
Result Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
IC
General Chemistry Parameters
Oil & Grease (HEM)
BRL
mg/L
5.0
1.2
1
*1664A
10/1/10 15:00
CDE
POJ0043
Phenolics
BRL'
mg/L
0,050
0,018
1
*420A
9130110 15:00
MRS
P010610
Total Suspended Solids
BRL
mg/L
5.0
1.5
1
*SM 2540 D
10/4/10 16:48
JAB
POJ0054
Turbidity
Ca
NTU
0.40
0.026
1
*1 0A
9128110 915
JAB
P010 72
Semiv latile Organic Compounds by GCIMS
1,24-Trichlorobenzene
BRL
ug/L
10
1.7
1
*625
9/29/10 19:27
KC
P010569
1,2-Dichlorobenzene
BRL
ug/L
10
2.0
1
*625
9/29/10 19:27
KC
P010569
1,3-Dichlorobenzene
BRL
ug/L
10
2A
1
*625
9/29/1019,27
KC
P010569
1,4-Dichlorobenzene
BRL;
ug/L
10
1:8
1
*625
9129/10 19:27
KC
P010569
2,4,6-Trichlorophenot
BRL
ug/L
10
3.1
1
*625
9/29/10 1:27
KC
P010569
2,4-Dichlorophenol
BRL
ug/L
10
1�5
1
*625
9/29/10 19:27
KC
P010569
2,4-Dimethylphenol
BRL
ug/L
10
2.A
1.
*625
9129/10 % 7
KG
P010569
2,4-Dinitrophenol
BRL
ug/L
10
1:2
1
*625
9/29110 19:27
KC
P010569
2,4-Dlnitrototuene'
BRL:
ug/L
10
4:O
1
*625
9129/10 19:27
KC
P010569
2,6-Dinitrotoluene
BRL
ug/L
10:
2.8 '
1
*625
9/29/10 19:27
KC
P010569
2-Chloronaphthalene
BRL
" ug/L
10
3.0
1
*625
9/29110 19:27
KC
P010569
2-Chlorophenol
BRL
ug/L
10
1.7
1
*625
9129/10 9:27
KC
P010569
-Nitrophenol
BRL'
ug/L
10
2.A
1
*625
9129/10 19:27
KC
P010569
3,3'-Dichlorobenzidine
BRL
ug/L
10
2,5
1
*625
9/29/10 19:27
KC
P010569
4,6-Dinitro-2-methylphenot
BRL
ug/L
10
1.8
1
*625
-9/29/10 19:27
KC
P010569
4-Bromc phenyl phenyl ether
BRL
ug/L
10
2.0 '
1
*625
9/29/10 19:27
KC
P010569
4-Chtoro-3-methylphenol
BRL
ug/L
10
2,2 '
1
*625
9/29/10 19:27
KC
P010569
4-Chlorophenyl phenyl ether
BRL
ug/L
10
2.9
1
`625
9129110 19:27
KC
P010569
4-Nitrophenot
BRL
ug/L
50
0.76"
1
*625
9129/10 19:27
KC
P010569
Acenaphthene
BRL`
ug/L
10
4A
1
*625
9/29/10 19:27
KC
P010569
Acenaphthylene
BRL
ug/L
10
2.8
1
*625
9129110 19:27
KC
P010569
Anthracene
BRL
ug/L
10
1.8
1
*625
9129/10 19:27
KC
P010569
Benzidine
BRL
ug/L
100
9.4
1
*625
9/29110 19:27
KC
P010569
Benzo(a)anthracene
BRL
ug/L
10
Z2
1
*625
9/29110 19:27
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
1.7
1
*625
9129110 19:27
KC
P010569
Benzo(b)fluoranthene
BRL
ug/L
10
1,2
1
*625
9/29/10 19:27
KC
P010569
Benzo(g,ti,l)perylene
BRL
ug/L
10
2A
1
*625
9129/10 19:27
KC
P010569
Benzo(k)ftuoranthene
BRL_
ug/L
10
21
1.
*625
9/29110 19:27
KC
P01069
bis(2-Chloroethoxy)methane
BRL
ug/L
10
2,3
1
*625
9/29110 19:27
KC
P010569
Bis(2-Chlorcethyl)ether
BRL
ug/L
10
1.9
1
*625
9/29110 19:27
KC
POIO569
Bis(2-chloroisopropyl)ether'
BRL
ug/L
10
2.3
1
*625
9129/10 19:27
KC
POIO569
Bis(2-Ethythexyl)phthalate
BRL
ug/L
10
2.7
1
*625
9129/10 19:27
KC
P010569
Butyl benzyl phthalate
BRL
ug/L
10
1.9
1
*625
4129110 19:27
KC
P010569
Chrysene
BRL
ug/L
10
31
1
*625
9129/10 19:27
KC
P010569
Dibenzo(a,h)anthracene
BRL
ug/L
10
2.3 -
1
*625
9129/10 19:27
KC
P010569
Diethyl phthalate
BRL
ug/L
10
2.2
1
*625
9/29110 19:27
KC
P010569
Dimethyl phthalate
BRL
ug/L
10
2:0
1
*625
9/29110 19:27
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte,
No 28 24.0643
Phones 7041629-6364 -Toll Free Number: 1-800/629-6364 - Fax. [phone]
age
=

M
Laboratory Report
is M I
F'11-Service Analytical
Solutions
10/0612010
v�
(Environmental
Colonial Pipeline Company Project. Charlotte
NPD S Stormwater
Client Sample ID: SW-Outfall-008-09/27/10
-
Attn: Jahn Culbreath
Prism Sample ID: 0 90620-06
P,O. Box 87
Project o.:
NCO031038
Prism Work Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/10 11:00
Time Submitted: 09/ 7/10 15:40
Parameter
Result
Units
Report MDL
Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Di-n-butyl phthalate
BRL
ug/L
10
1.5
1
*625 9/29110 19:27
KC
P010569
Di-n-octyl phthalate
BRL
ug/L
10
2.5
1
"625 9/29/10 19:27
KC
P010569
Fluoranthene
BRL
ug/L
10
1.5
1
*625 9/29/10 19:27
KC
P010569
Fluorene
BRL
ug1L
10
4.4
1
*625 9/29/10 19:27
KC
P0I0569
Hexachlorobenzene
BRL
ug/L
10
2.1
1
*625 /29/10 19:27
KC
P010569
Hexachlorobutadiene
BRL
ug/L
10
1,8
1
*625 9/29/10 19:27
KC
P010569
Hexachlorocyclopentadiene
BRL
ug/L
10
2.O
1
*625 9/29/10 19:27
KC
POIO569
Hexachloroethane
BRL
ug/L
10
2.2
1
*625 9/29/10 19:27
KC
P010569
Indeno(1,2,3-cd)pyrene
BRL
ug/L
10
3,6
1
*625 9/29/10 19:27
KO
P010569
lsophorone
BRL
ug1L
10
2.6
1 "
*625 9/29/10 19:27
KC
P010569
Naphthalene
BRL
ug/L
10
1.6
1
*625 9/29/10 19:27
KC
P010569
Nitrobenzene
BRL-
ug/L
10
2.1
1
*625 9/29/10 19:27
KC
P010569
N-Nitrosodimethylamine
BRL
ug1L
10
5,6
1
*625 9/29/10 19:27
KC
POIO569
N-Nitroso-di-n-propylamine "
BRL
ug/L
10
2.2
1
*625 9/29/10 19:27
KC
P010569
N-Nitrosodiphenylamine
BRL
ug/L
10
3.7
1 ,
*625 9/29/10 19:27
KC
P010569
Pentachlorophenol
BRL
ug/L
10
21
1:
*625 9/29/10 19:27
KC
P0I0569
Phenanthrene
BRL
ug/L
10
1.2
1
*625 9/29/10 19:27
KC
P0I0569
Phenol
BRL
ug1L
10
0,58
1
'625 9/29/10 19:27
KC
P010569
Pyrene
BRL
uglL
10
1.8
1
*625 9/29/10 19:27
KC
P010569
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
92 `i*
26-139
2-Fluorobiphenyl
79 %
41-112
2-Fluorophenol
38 %
10-46
Nitrobenzene-d5
77 %
34-102
Phenol-d
3 %
10-34
Terphenyl-04
77 %
31-165
Volatile Organic Compounds by GC/PiD/EL.CD
Benzene
BRL
ug/L
0.50
0,066
1
*601/602 10/l/10 23:10
HPE
POJ0020
Ethylbenzene
BRL
ug/L
1.0
0.03
1
`601/602 1011/10 223:10
HPE
POJ0020
m,p-Xylenes
BRL
ug/L
2,0
0.11
1
*601/602 10/1110 23:10
HPE
POJ0020
Methyl -tent --Butyl Ether
BRL
ugtL
5.0
0,17
1
*601/602 1011/10 23:10
HPE
POJ0020
o-Xylene
BRL
ug/L
1.0
0.31
1
*601/602 10/1/10 23:10
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0.059
1
*601/602 10/1110 23:10
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643
Phone: [phone] - Toil Free Number. 1-800r529-6364 .
Fax: [phone]
�I
'14,.

Laboratory Report
Loom'"
FuU-Service Analytical&
solutions
10106/2010
�'�`r a80PATOmes, me,.
Environmental
Colonial Pipeline Company
Project: Charlotte NPD S Stormwater
Client
Sample ID:
SWGutf ll-007_0 /27/10-
Attm John Culbreath
Prism
Sample ID:
0090620- 7
P.G. Box 87
Project No.: NCO031038
Prism
Work Order:
0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/1014:00
Time
Submitted: 0917/10 15:40
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Bach
Limit
Factor.
DatelTirne
ID
General Chemistry parameters
Oil & Grease (HEM)
BRL
mg/L
5.0
1,2
1
1664A
10/1110 15:30
CDE
POJ0043
Phenolics
BRL"
mg/L
0,050
0,018
1
*420.1
9130/10 15:00
MRS
PO 0610
Total Suspended Solids
BRL
mg/L
5.0
1.5
1
*SM 2540 D
1014/10 16:48
JAB
POJ0054
Turbidity
7.1
NTU
0.40
0.026
1
*180.1
9/28110 916
JAB
P010672
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
ug/L
10
13
1
*625
9129/10 20:02
KC
P010669
1,2-Dichlorobenzene
BRL
ug/L
10
2,0
1
*625
9/29110 2002
KC
P010569
1,3-Dichlorobenzene
BRL
ug/L
10
2A
1
*625
9129/10 20:02
KC
P010569
1,4-Dichlorobenzene
BRL
ug/L
10
1.8
1
*625
9/29110 20:02
KC
P010569
2,4,6-Trichlorophenol
BRL
ug/L
10
3A
1
*625
9129/10 0:02
KC
P010569
2,4-Dictlorophenol
BRL
u91L
10
1,5 :
1
*625
9129/10 20:02
KC
P010569
,4-Dimethylphenol
BRL
ug/L
10
2,4
1
*625
9/29/10 20:02
KC
POIO569
2,4-Dinitrophenol
BRL
ug/L
10
1.2
1
*625
9129110 0:02
KC
P010569
2,4-Dinitrotoluene
BRL'
ugtL
10
4.0
1
*625
9/29110 20:02
KC
P010569
2,6-Dinitrotoluene
BRL
ugfL
10
2.8
1
*625
9/29/10 20:02
KC
P0I0569
2-Chlor inaphthatene
BRL'
ug/L
10
3.0 :
1
*625
9/29/10 20:02
KC
P010569
-Chlorophenol
BRL
ug/L
10
1,7
1
*625
9/29110 20:02
KC
POIO569
2-Nitrophenol
BRL
ug/L
10
2.4 ;
1
*625
9/29110 20:02
KC
P010569
3,3'-Dichlorobenzidine
BRL
ug/L
10
2.5
1
*625
9129/10 0:02
KC
P010569
4 6-Dinitro-2-methylphenol
BRL
ug/L
10
1.8 -
1
*625
9129/10 20:02
KC
P010569
4-Bromophenyl phenyl ether
BRL
ug/L
10
2.0 :
1
*625
9/29/10 20:02
KC
P010569
4-Chlor-3-methylphenot
BRL
ug/L
10
2,2
1
*625
9/29/10 20:02
KC
P010569
4-Chlorophenyt phenyl ether
BRL
ug/L
10
2.9
1
*625
9/29110 20:02
KC
P010569
4-Nitrophenol
BRL
ug/L
50
0,76
1
*625
9129/10 20:02
KC
POIO569
Acenaphthene
BRL
ug/L
10
4A
1
`625
9/29/10 20:02
KC
P010569
Acenaphthylene -
BRL
ug1L
10
2.8
1
*625
9129/10 20:02
KC
P010569
Anthracene
BRL
uglt.
10
1.8 '
1
*625
9/29/10 0:02
KC
POIO569
Benzidine
BRL
ug/L
100
9.4
1
*625
9/29/10 20:02
KC
P010569
Benzo(a)anthracene
BRL
ug/L
10
22
1
*625
9/29110 20:02
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
11
1
*625
9/29/10 20:02
KC
POIO569
Benzo(b)fluoranthene
BRL
ug/L
10
1.2
1
*625
9/29/10 20:02
KC
P010569
Benzo(g,h,i)peryl ne
BRL
ug/L
10
2.1
1
*625
9/29110 20:02
KC
P010569
Benzo(k)fluoranthene
BRL
ug/L
10
2.7
1
*625
9/29110 20:02
KC
P010569
bis(2-Chloroethoxy)methane
BRL
ug/L
10
23
1
*625
9129/10 20:02
KC
P010569
Bis(2-Chloroethyl)ether
BRL
ug/L
10
1.9
1
*625
9/29110 20:02
KC
P010569
Bis(2-chloroisopropyl)ether
BRL
ug1L
10
2,3
1
*625
9/29110 20:02
KC
P010569
Bls(2-Ethylhexyl)phthalate
BRL
ug/L
10
17
1
*625
9129/10 20:02
KC
P010569
Butyl benzyl phthalate
BRL
ug/L
10
1.9
1
*625
9129/10 20:02
KC
P010569
Chrysene
BRL
ug/L
10
3,1
1
*625
9129/10 20:02
KC
P010569
Dibenzc(a,h)anthracene
BRL
ug/L
10
2.3
1
*625
9/29110 20:02
KC
P010569
Diethyl phthalate
BRL
ug/L
10
2.2
1
*625
9129/10 20:02
KC
P010569
Dimethyl phthalate
BRL
ug/L
10
2.0
1
*625
9/29/10 20:02
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc
449 rpringbrook Road - P.O. Box 240643 - Chadoi%
NC 8224-OW
Phone: [phone] - Toil Free Number: 1-8001629.6364 - Fax: [phone]

N
rAw,% �W-
) Company
kftn' John Culbreath
3.0, Box 87
Charlotte NPDES Stormwa,
qo.: NCO031038
law Creek, NC 28130 Sample Matrix: Water
-neter Result Units
Laboratory Report
10/06/2010
Client Sample ID: SW-Outfall-007-09/27/10—
Prism Sample ID: 0090620-07
Prism Work Order-, 0090620
Time Collected: 09/27/10 14:00
Time Submitted- 09/27/10 15:40
Dilution Method Analysis Analyst Batch
Factor Date/Time ID
jy phthalate
BRL
ug/L
10
i's
1
*625
9/29/10 20:02
KC
P010569
,tyl phthalate
BRL
ug/L
10
Z5
1
*625
9129110 20:02
KC
P010569
nthene
BRL
ug/L
10
1.5
1
9/29/10 20:02
KC
P010569
no
BRL
ug/L
10
4A
1
*625
9129110 20:02
KG
P010569
hforobenzene
BRL
ug/L
10
2.1
1
*625
9/29110 20:02
KC
P010569
hiorobutadiene
BRL
ug/L
10
1,8
1
*625
9/29/10 20:02
KC
POf0569
hlorocyclopentadiene
BRL
ug/L
10
2,0
1
*625
9129110 20:02
KC
P010569
hloroethane
BRL
ug/L
10
2.2
1
'625
9/29/10 20:02
KC
P010569
)(1,2,3-cd)pyrene
BRL
ug/L
10
3,6
1
*625
9/29/10 20:02
KC
P010569
)rone
BRL
ugIL
10
2,6
1
*625
9129/10 20:02
KC
P010569
ialene
BRL
ug/L
10
i's
1
*625
9/29/10 20:02
KC
P010569
anzene
BRL
ug/L
10
21
1
*625
9/29110 20:02
KC
P010569
N-Nitrosodimethylamine
BRL
ug/L
10 5.6
1
*625 9/29/10 20:02
KC
P010569
N-Nitroso-di-n-propylamine
BRL
ug/L
10 12
1
*625 9/29/10 20:02
KC
P010569
N-Nitrosodiphenylamine
BRL
ug/L
10 3.7
1
*625 9129/10 20:02
KC
P010569
Pentachlorophenol
BRL
ug/L
10 2.1
1
*625 9/29/10 20:02
KC
P010569
Phenanthrene
BRL
ug/L
10 11
1
*625 9129/10 20:02
KC
P010569
Phenol
BRL
ug/L
10 0.58
1
*625 9129110 20:02
KC
POIO569
Pyrene
BRL
ug/L
10 1.8
1
*625 9/29/10 20:02
KC
P010569
Surrogate
Recovery
Control Limits
2,4,6-Tribrornophenol
78%
26-139
2-Fluorobiphenyl
70%
41-112
2-Fluorophenol
38%
10-48
Nitrobenzene-dS
67%
34-102
Phenol-d5
23%
10-34
Terphenyl-dl 4
68%
31-165
Volatile Organic Compounds by GC/PID/ELCD
Benzene
BRL
ug/L
050 0,066
1
'6011602 1011/10 23.57
HPE
POJ0020
Ethylbenzene
BRL
ug/L
1.0 OMS
1
*601/602 10/1/10 23:57
HPE
POJ0020
m,p-Xylenes
BRL
ug/L
2,0 0,11
1
*601/602 10/1110 23'57
HPE
POJ0020
Methyl-tert-Butyl Ether
BRL
ug/L
5,0 0,17
1
*601/602 10/1/10 23:57
HPE
POJ0020
o-Xylene
BRL
ug/L
1'0 0.31
1
*601/602 10/1/10 23:57
HPE
POJ0020
Toluene
BRL
ug1L
1'0 0.059
1
*601/602 10/1/10 23:57
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, No 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax. [phone]
e'16
of,35

Laboratoty Report
a
Ism
ABORATORMS, WC
Full -Service Anatyticat &
Environmental Solutions
10106/2010
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater
Client
Sample ID:
S Clutfall-009_09/27/10
Attn: John Culbreath
Prism
Sample ID:
0090620-08
P.O. Box 87
Project No.: NCO031038
Prism
Work Order: 0090620
Paw Greek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/10 14 10
Time: Submitted: 09/27/10 15:40
Parameter
Result Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DatelTinle
ID
General Chemistry Parameters
Oil & Grease (HEM)
BRL
mglL
5,0
1.2
1
*1 64A
10/1/10 15:30
CDE
POJ0043
Phenolics
BRL
/L
0.050
0,018
1
*420.1
9130/10 15:00
MRS
P010610
Total Suspended Solids
llA
mg/L
6.0
1.6
1
* M 2640 D
10/4110 16.48
JAB
POJ0064
Turbidity
9s
NTU
0.40
0.026 "
1
*180A
9128/10 915
JAB
P010672
Semivolatile Organic Compounds byGC/MS
1, ,4-Trichlorobenzene
BRL
ugfL
10
1.7 ;
1
*625
9129/10 20:36
KC
P010569
1,2-Dichlorobenzene
BRL"
ugfL
10
2.0
1
*625
9129/10 20:36
KC
P010569
1,3-Dichlorobenzene
BRL
ug7L
10
21
1
*625
9/29/10 0:36
KC
P010569
1,4-Dichlorobenzene
BRL
ug/L
10
1.8
1
*625
9/29/10 20:36
KC
P010569
2,4,6-Trichlorophenol
BRL
ug/L
10
3.1
1
`625
9/29/10 20:36
KC
P010569
,4-Dichlorophenol
BRL
ug/L
10
1.5
1
*625
9/29/10 20:36
KC
P010569
2,4-Dimethylphenof
BRL
ug/L
10
2A
1
*625
9/29/10 20:36
KC
P010569
2,4-Dinitrophenol
BRL
ug/L
10
1.2
1
*625
9129110 20:36
KC
P0I0569
2 4-Dinitrotoluene
BRL
ug/L
10
4.0
1
*625
9/29/10 20:36
KC
P010569
2,6-Dinitrotoluene
BRL
ug/L
10
2.8
1
*625
9/29110 20:36
KC
P010569
-Chloronaphthatene
BRL
ug/L
10
3.0
1
*625
9/29/10 20:36
KC
POIO569
2-Chlorophenot
BRL
ug/L
10
1.7
1
*625
9/29/10 20:36
KC
POIO569
-Nitrophenot
BRL
ug/L
10
2A
1
*625
9/29/10 0:36
KC
P0I0569
3,3'-Dichlorobenzidine
BRL
ug/L
10
2.5
1
*625
9/29/10 20:36
KC
P010569
4,6-Dinitro-2-methylphenol
BRL
ug/L
10
1.8
1
*625
9129/10 20:36
KC
P010569
4-Bromophenyt phenyl ether
BRL
ug/L
10
2.0
1
*625
9/29/10 20:36
KC
P010569
4-Chloro-3-methylphenot
BRL
ug/L
10
2.2
1
*625
9129/10 20,36
KC
P010569
4-Chlorophenyl phenyl ether
BRL
ug/L
10
2.9
1
*625
9129/10 20.36
KC
P010569
4-Nitrophenol
BRL
ug/L
50
0,76:
1
`625
9/29/10 20:36
KC
P010569
Acenaphthene
BRL
ug/L
10
4A
1
*625
9/29/10 20,36
KC
P010569
Acenaphthylene
BRL
ugfL
10
2.8
1
*625
9129/10 20:36
KC
POI0569
Anthracene
BRL
ug/L
10
1.8
1
*625
9/29/10 20:36
KC
P010569
Benzidine
BRL
ug/L
100
9.A
1
*625
9/29/10 0:36
KC
P010569
Benzo(a)anthracene
BRL
ug/L
10
2:2"
1
*625
9/29/10 20:36
KC
P010569
Benzo(e)pyrene
BRL
ug/L
10
1.7
1
*625
9/29/10 20:36
KC
P010569
Benzo(b)fluoranthene
BRL
ug/L
10
1.2
1
*625
9129/10 20.36
KC
P010569
Benzo(g,h,i)per lene
BRL
ug/L
10
2A
1
*625
9129110 20:36
KC
P010569
Benzo(k)fluoranthene
BRL
ug/L
10
2:7
1
*625
9/29/10 20:36
KC
P010569
bis(2-Chloroethoxy)methane
BRL
ug/L
10
2.3
1
*625
9129/10 0:36
KC
P010569
Bis(2-Chloroethyl)ether
BRL
ug/L
10
1.9
1
*625
9129/10 20:36
KC
P010569
Bis(2-chlorolsopropyl)ether
BRL
ug/L
10
2.3
1
*625
9129110 20:36
KC
P010569
Bls(-Fthylhexyl)phthalate
BRL
ug/L
10
2.7
1
*625
9129/10 20:36
KC
P010569
Butyl benzyl phthalate
BRL
ug/L
10
1.9
1
*625
9129/10 20:36
KC
P010569
Chrysene
BRL
ug/L
10
3.1
1
*625
9/29/10 20:36
KC
P010569
Dibenzo(a,h)anthracene
BRL
ug/L
10
2.3
1
`625
9/29/10 20:36
KC
P010569
Diethyl phthalate
BRL
ug/L
10
2.2
1
*625
9/29/10 20:36
KC
P010569
Dimethyl phthalate
BRL
ug/L
10
2,O
1
*625
9/29/10 20:36
KC
P010569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc,
449 Springbrook Road - P.O. Box 240643 -
Charlotte, NC 28224-0643
77
Phone: [phone] - Tall Free Number: 1-800/629-6364 - Fax: [phone]

I Fufi,Sorvice Analytical
Environmental Solutions
:lipefine Company Project: Charlotte NPDES Stort
i Culbreath
87 Project No.: NCO031038
,k, NC 28130 Sample Matrix Water
Result Units Report
Limit
Di-n-butyl phthalate
BRL
ugIL
10
Di-n-octyl phthalate
BRL
ug/L
10
Fluoranthene
BRL
ugtL
10
Fluorene
BRL
ug/L
10
Hexachlorobenzene
BRL
ugh.
10
Hexachlorobutadiene
BRL
ugIL
10
Hexachlorocyclopentadiene
BRL
ug/L
10
Hexachloroethane
BRL
ug/L
10
tndeno(1,2,3-od)pyrene
BRL
ug/L
10
Isophorone
BRL
ug/L
10
Naphthalene
BRL
ug/L
10
Nitrobenzene
BRL
ug/L
10
N-Nitrosodimethylamine
BRL
ug/L
10
N-Nitroso-di-n-propylamine
BRL
ug/L
10
N-Nitrosodiphenylamine
BRL
ug/L
10
Pentachlorophenol
BRL
uglL
10
Phenanthrene
BRL
ug/L
10
Phenol
BRL
ug1L
10
Pyrene
BRL
ug/L
10
Surrogate
24,13-Tribrom
2-Fluorobipht
2-Fluorophen
Nitrobenzene
Phenol-dS
Terphenyl-dl,
Volatile Organic Compounds by GC/PIDIELCD
Laboratory Report
10/06/2010
Client Sample ID: SW-Outfall-009-09/27/10—
Prism Sample ID, 0090620-08
Prism Work Order: 0090620
Time Collected: 09/27/10 1410
Time Submitted:09/27/10 15:40
Dilution
Method
Analysis Analyst
Batch
Factor
Date/Time
ID
1
*625
9/29/10 20,36
KC
P010569
1
*625
0/29/10 20:36
KC
P010569
1
*625
9129/10 20:36
KC
P010569
1
*625
9/29110 20:36
KC
P=569
1
*625
9/29110 20:36
KC
POIO569
1
*625
9/29110 20:36
KC
P010569
1
*625
9/29110 20:36
KC
P010569
1
*625
9129/10 20:36
KC
P010569
1
*625
9129/10 20:36
KC
P010569
1
*625
9/29/10 20:36
KC
P010569
1
*625
9/29110 20:36
KC
P010569
1
*625
9/29110 20:36
KC
P010569
1
*625
9/29/10 20:36
KC
P010569
1
*625
9/29/10 20:36
KC
P010569
1
*625
9/29/10 20:36
KC
POIO569
1
*625
9/29110 20-,36
KC
P010569
1
*625
9/29/10 20:36
KC
P010569
1
*625
9/29/10 20:36
KC
P010569
1
*625
9/29/10 20:36
KC
POIO569
Recovery
Control Limits
al 88%
26-139
78%
41-112
40%
10-48
79%
34-102
24%
10-34
82%
31-165
Benzene
BRL ug/L 0.50 0.066 1 *6011802
10/2110 0:44
HPE
POJ0020
Ethylbenzene
BRL ug/L 1.0 0.035 1 *601/602
1012110 0:44
HPE
POJ0020
m,p-Xylenes
BRL ug/L 2.0 0.11 1 *6011602
1012t10 0:44
HPE
POJ0020
Methyl-tert-Butyl Ether
BRL ug/L 5.0 017 1 *601/602
10/2110 0:44
HPE
POJ0020
o-Xylene
BRL ug/L 1.0 0.31 1 *601/602
10/2/10 0:44
HPE
POJ0020
Toluene
BRL ug/L 1.0 0.069 1 '601/602
1012110 0:44
HPE
POJ0020
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
440 Springbrook Road - P.O. Box 240643 - Charlotte, NO 28224-0643
Phone. [phone] - Toll Free Number- 1-8001629-6364 - Fax: 7OV626-0409
C
18 of,

Laboratory Report
M I
Fait-Servioe Analytioat $
Environmental SoWbons
10/06/2010
.. yAWRAT00ift WC.'
Colonial Pipeline Company
Project: Charlotte NPDES Stor water
Client
Sample ID:
S - lutfall-MYO-09/27/10
Attn: John Culbreath
Prism
Sample ID:
0090620-09
P'O. Box 87
Project No.: NCO031038
Prism
Work Order: 0090620
Paw Creek, NC 28130
Sample Matrix: Water
Time Collected: 09/27/1014:30
Time Submitted: 09/27/10 1 :40
Parameter
Result Units
Report
MDL
Dilutions
Method
Analysis Analyst
Batch
Limit
Factor `
Date/Time
to
General Chemistry Parameters
Oil & Crease (HEM)
BRL
mg1L
5.0
1.2
1
*1664A
10/1/10 15:30
CDE
POJ0043
Phenolics
BRL
mg/L
0.050
0,018
1
*420A
9130/10 15:00
MRS
P010610
Total Suspended Solids
6.6
MOIL
6.0
1.6
1
*SIN 2640 D
1014110 16:48
JAB
POJ0064
Turbidity
11
NTU
0.40
0.026
1
*1 0.1
9/28110 16
JAB
P010672
Semivolatile Organic Compounds by GC1MS
1,2„4-Trfchlorobenzene
BRL
ug/L
10
1.7
1
*625
9/29/10 21:10
KC
P010569
1,2-Dichlorobenzene
BRL
ug/L
10
2.0
1
*625
9/ 9110 21:10
KC
P010569
1,-Dichlorobenzene
BRL
ug/L
10
2A
1
*625
9/29/10 21:10
KC
POIO569
1,4-Dichlorobenzene
BRL
ug/L
10
1,8
1
`625
9/29110 21:10
KC
P010569
2,4,6-Trichlorophenol
BRL
ug/L
10
3A
1
*625
9/29/10 21:10
KC
P010569
2,4-Dichlorophenol
BRL
ugfL
10
1.5
1
*625
9/29110 21:10
KC
P010569
2,4-Dimethylphenot
BRL-
ugfL
10
2A
1
*625
9/29/10 21:10
FCC
P010569
2,4-Dfnitrophenot :
BRL
ug/L
10
1.2
1
*625
3/29/10 21:10
KC
P010569
2,4-Dinitrotoluene
BRL
ug/L
10
4.0
1
*625
9/29/10 2110
KC
P010569
2,6-Dinitrotoluene
BRL
ugfL
10
2,8
1
*625
9/29/10 21:10
KC
P010569
2-Chloronaphthatene
BRL
ug/L
10
3.0
1
*625
9129/10 2110
KC
P010569
2-Chlorophenot
BRL
ug/L
10
1.7
1
*625
9/29/10 1:10
KC
P010569
2-Nitrophenof
BRL
ug1L
10
2.4
1 -
*625
9/29/10 21:10
KC
POIO569
3,3'-Dichlorobenzidine
BRL'
ugtL
10
2.5
1
*625
9/29110 21:10
KC
PGIO569
4,6-Dinftro-2-methylphenot
BRL
ug/L
10
1.8
1
*625
9/29/10 21:10
KC
P010569
4-Bro ophenyt phenyl ether
BRL
ugfL
10
2.0
1
*625
9/29/10 21:10
KC
POIO569
4-Chloro-3-rnethylphenot
BRL
ug1L
10
2.2
1
`625
9129/10 21:10
KC
POi0569
4-Chlorcphenyl phenyl ether
BRL
u/L
10
2,9
1
*625
9/29/10 1:10
KC
P010569
4-Nitrophenot
BRL
ug/L
50
0.76
1
*625
9/29/10 1:10
KC
P010569
Acenaphthene
BRL
ug/L
10
4.1
1
`625
9/29110 21:10
KC
P010569
Acenaphthylene
BRL
ug1L
10
2,8
1
*625
9/29110 21.10
KC
P010569
Anthrecene
BRL
ug1L
10
1.8
1
*625
9129110 21:10
KC
P010569
Benzidine
BRL
ug/L
100
9.4
1
*625
9129/10 21:10
KC
P010569
Benzo(a)anthracene
BRL
ug/L
10
2.2
1
*625
9/29/10 21:10
KC
P010569
Benzo(a)pyrene
BRL
ug/L
10
1.7
1
*625
9/29/10 21:10
KC
P010569
Benzo(b)fluoranthene
BRL
ug/L
10
1.2
1
*625
9129/10 21:10
KC
P010569
Benzo{g,h,i)perytene
BRL
ug/L
10
2A
1
*625
9/29/10 21:10
KC
P010569
Benzo(k)ffuoranthene
BRL
ug/L
10
21
1
*625
9129/10 21:10
KC
P010569
bfs(2-Chforoethoxy)methane
BRL
ug/L
10
2.3
1
*625
9/29110 21:10
KC
POIO569
Bis(2-Ctlloroethyl)ether
BRL
ug1L
10
1.9 -
1
*625
9/29110 21:10
KC
P010569
Bis(2-chloroisopropyl)ether
BRL
ug1L
10
2:3
1
*625
9/29/10 21:10
KC
P010569
8is(2-Ethyfhexyl)phthalate
BRL
ug/L
10
21
1
`625
9/29/10 21:10
KC
POIO569
Butyl benzyl phthalate
BRL
ugfL
10
1.9
1
*625
9/29/10 21:10
KC
P010569
Chrysene
BRL
ug/L
10
3.1
1
*625
9/29/10 21:10
KC
P010569
Dibenzo(a,h)anthracene
BRL
ug/L
10
2.3
1
*625
9/29/10 21:10
KC
P010569
Diethyl phthalate
BRL
ug1L
10
2.2
1
*625
9/29110 1:10
KC
P010569
Dimethyl phthalate
BRL
ug/L
10
2.0
1
*625
9/29/10 21:10
KC
POIO569
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "
449 Springbrook Road - P.O. Box 240643 -
Charlotte,
NC 282244643
,
Phone. [phone] . Toll Free Number: 1-8001629-6364 - Fax: [phone]
P7
17775

s
Laboratory Report
�*
Full -Service Analytical &
Solutions
10106/2010
l� tA9ClRAYX]UtE�, tNC,
Environmental
Colonial Pipeline Company Protect. Charlotte PIPDES Stormwater
Client Sample ID. SW-Outfall-MYCli09/27/10
Attn. John Culbreath
Prism Sample ID. 0090620-09
P.t . Box 87
Project No.:
NCO031038
Prism Work Girder, 0090620
Paw Greek, NC 28130
Sample Matrix: Water
Time Collected. 09/27/10 14:30
Time Submitted: 09/27/10 15.40
Parameter
Result
Units
Report
MDL
Dilution Method Analysts Analyst
Batch
Limit
FactorDater me
ID
Di-nµbutyl phthalate
BRL
ugfL
10
1.5
1 *625 9/29/10 21:10
KC
P010569
Di-n-octyl phthalate
BRL
ug7L
10
2.5
1 *625 9/29110 21:10
KC
P010569
Fiuoranthene
BRL
ugiL
10
1.5
1 *625 9/29/10 21:10
KC
POIO569
Fluorene
BRL
ugfL
10
4A
1 *625 9/29/10 21:10
KC
P010569
Hexachlorobenzeie
BRL
ug/L
10
2.1
1 *625 9129110 21:10
KC
POIO569
Hexachlorobutadiene
BRL
ug/L
10
1.8
1 *625 9/29/10 21:10
KC
P010569
Hexachlorocyclopentadiene
BRL
ug7L
10
2.0
1 *625 9129/10 2110
KC
P010569
Hexaehlomethane
BRL
ugfL
10
2.2
1 *625 9/29/10 21:10
KC
P010569
tndeno(1,2,3-cd)pyrene
BRL
ugiL
10
3.6
1 *625 9/29/10 21:10
KC
P010569
Isophorone
BRL
ug/L
10
2.6
1 *625 9/29/10 21:10
KC
P010569
Naphthalene
BRL
ugfL
10
1.6
1 *625 9/29/10 21:10
KC
P010569
Nitrobenzene
BRL
ugiL
10
2.1
1 *625 9129/10 21:10
KC
P010569
N-Nltrosodimethylamtne
BRL
ugiL
10
5.6
1 `625 9/29/10 21:10
KC
POI0569
N-Nitroso-di-n-propylamine
BRL
ugfL
10
2.2
1 ' *625 9129/10 21:10
KC
P010569
N-Nitrosodiphenyte ine
BRL
ugiL
10
3.7
1 *625 9129/10 21:10
KC
P010569
Pentachlorophenol
BRL'
ugiL
10
2.1
1 *625 9/29/10 21:10
KC
P010569
Phenanthrene
BRL
ug/L
10
1.2
1: *625 9/29/10 21:10
KC
P010569
Phenol
BRL`
ug/L
10
0,58
1 *625 9/29110 21:10
KC
P010569
Pyrene'
BRL-
ugfL
10
1.8
1 *625 9/29/10 21:10
KC
P010569
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
92 %
26-139
2-Fluorobiphenyl
89 %
41_112
2-Fluorophenol
44 %
10-48
Nitrobenzene-d5
90 %
4- 0
Phenol-d5
27 %
10-34
Terphenyl-d14
84 %
31-165
Volatile Organic Compounds by CC/PIDIELCD
Benzene
1.1
trg1L
0.60
0.066
1 *6011602 1012/10 1:31
HPE
POJ0020
Ethylbenzene
1.4
ag/L
1.0
0.036
1. *6011602 10/2110 1.31
HPE
POJ0020
m,p-xylenes
BRL"
ugiL
2.0
0,11
1 *601/602 10/2/10 1:31
HPE
POJ0020
Methyl-tert-Butyl Ether
BRL
ug/L
5.0
0.17
1 *601/602 1012/10 ;1:31
HPE
POJ0020
o- ylene
BRL
ug/L
1.0
0.31
1 *601/602 10/22/10 1:31
HPE
POJ0020
Toluene
BRL
ug/L
1.0
0.059
1 *601/602 1012/10 1:31
HPE
POJ0020
This report should not be reproduced„ except in its entirety, without the written consent of Prism Laboratories„ Inc,
449 Springbrook Road - P.O. Box 240643 - Charlotte,
NC 28224-0643 � �.„,..
�,�.,
Phone. [phone] - Toll Free Number. 1.800IS29-6364 - Fax: [phone]
�
Of 5

4 R
. ,.
Level 11 OC e{� ortt
';�Y,i .( ruil- #�(VSt70 Analytical
`ii environmental Solutions
ISM
0/6/10
�tAOfeitRY'pGdf.R kNC..:
Colonial Pipeline Company
Project, Charlotte NPDES Stormwater
Prism Work Order. 0090620
Attn: John Culbreath
Time Submitted: 9/27/10 .40:00PM
P.0, Box 87
Project No: NCO031038
Paw Creek, NC 28130
Volatile Organic Compounds by GCIPIDIELCO - Quality Control
Reporting
Spike
Source
°DREG RPD
Analyte
Result
Limit
Units
Level
Result °DREG
Limits RPD Limit Notes
Batch POJ0020 - NO PREP
dank(POJ0020.BLK1)
Prepared & Analyzed:1€}1011100
_..
Benzene
BRL
0,5ti
ug1L
Ethylbenzene
BRL
1.0
ug/L
m,p-xylenes
BRL
2.0
ug/L
Methyt-tert-Butyl Ether
BRL
5.0
ugiL
o-ylene
BRL
1,0
ug/L
Toluene
BRL
10
ug/L
Blank (POJ0020-BLK2)
Prepared: 10101/10 Analyzed: 10/02/10
Benzene
BRL
0,50
ug/L
Ethylbenzene
BRL
1,0
ug1L
m,p-Xylenes
BRL
2.0
ugtL
Methyl-tert-Butyl Ether
BRL
5:0
ugiL
o-ylene
BRL
1:0
ug/L
Toluene
BRL
1:0
ug/L
LC (POJ0020-BSI)
Prepared& a Analyzed: 10/01 /10
Benzene
19.9
0,50
ugiL
2b„0
100
39-150
Ethylbenzene
20.1
1,0
ugiL
20.0
100
32-160
lsopropyl Ether
19.1
5.0
ug1L
0.0
95
72-120
m,p-Xyl nes
41.0
2,0
ugiL
40.0
103
77-129
Mothyt- ert-Butyl Ether
17.6
5,0
ugiL
20,0
88
75-123
Naphthalene
17.2
6.0
ug/L
20.0
86
65-128
o-ylene
19.6
10
ug/L
20.0
98
75-131
Toluene
19.8
1.0
ugiL
20.0
99
46-143
Xylenes, total
BRL
3,0
ugiL
MCI,
67-131
Surrogate. 1.4- iflu rrobenzene (PID)
23.6
ugiL
260
94
52-15
LCS (POJ0020-BS2)
Prepared 8 Analyzed: 10/01/10
Benzene
19.2
0,50
ug1L
M0
96
39-150
Ethylbenzene
19.5
1,0
ugiL
20.0
97
32-160
Isopropyl Ether
18.7
5:0
ugiL
20.0
94
72-120
m,p-Xylenes
39.3
2:0
ug1L
40.0
98
77-129
Methylfert-Butyl Ether
17.8
5.0
u 1L
MO
89
75-123
Naphthalene
19.8
5;0
ugiL
O
99
65-128
o-Xylene
19.4
1.0
ug/L
20.0
97
75-131
Toluene
19.1
1.0
ug1L
20.0
95
46-148
Xytenes, total
BRL
10
ug1L
60.0
67-131
Surrogate: 1,4-Difluorobenzene (PID)
24.4
ugfL
25.0
97
52-151
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte; NC 28224-0643
51
Phone: [phone] - Toll Free Number. 1- 001629.6364 _ Fax: [phone]
f 1 77 1
r

Level 1100 Report
sya Full -Service Analytical
I
10/6/10
Environicarntar Solutions
xti A%?OWk1S MM I
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater
Prism Work Girder:
0090620
Attn: John Cul reath
Time Submitted: I27/10
3:40:OOPM
P.O. Box 87
Project No: NCO0 1038 `
Paw Creek, NC 28130
Volatile Organic Compounds by GCIPIDIELCD - Quality Control
Reporting
Spike
Source
%REC
RPD
Analyte
Result Limit Units
Level
Result
%REC
Limits
RPD
Limit
Notes
Batch POJ0020 - NO PREP
Matrix Spike (POJ0020.MS1)
Source: 0090 20-01
A
Prepared & Analyzed:' 10/01/10
_
Benzene
148ry
5.0 ug/L
200
BRL
74
39-150
15
Ethylberzene
173 10 ug/L
200
BRL
87
32-160
14
Isopropyl Ether
136 50 ug1L
200
BRL
68
72-120'
14
M
m,p-Xylenes
364 20 ug/L
400
BRL
91
77-129
13
Methyl-tert-Butyl Ether
132 50 ugfL
200
BRL
66
75-123
11
M
Naphthalene
190 s0 ug/L
200
BRL
95
65-128
1
o-Xylene
159 10 ug/L
200
BRL
79
75-11
22
Toluene'
154 10 ug1L
200
BRL
77
46-148
13 "
Xylenes, total
BRL 30 ugfL
600
BRL
68-132
22
Surrogate: 1,4-Diftuorobenzene (PID)
18,2 ugfL
260
73
52-151
Matrix Spike Du (POJO020-MSD1)
Source: 0090 20-01
Prepared & Analyzed: 10/01/10
Benzene
179 &0 ugfL
200
BRL
90
39-150
19
Is
D
Ethylbenzene
178 10 ug7L
200
BRL
89
3 -160
3
14
Isopropyl Ether
175 50 ugfL
200
BRL
87
72-120
25
14 -
D
,p-ylenes
379 20 ug/L
400
BRL
95
77-129
4
13
Methyl -tart -Butyl Ether
171 50 ug7L
200
BRL
86
75-123
26
11
D
Naphthalene
192 50 ugfL
200
BRL
96
65-1 8
0.6
1
o-Xylene
183 10 ug/L
200
BRL
91
75-131
14
22 "
Toluene
180 10 ug/L
200
BRL
90
46-148
16
13
D
Xylenes total
BRL 30 ugfL
600
BRL
68-132
22
Surrogate: 1,4-Diftuarobenzene(PID)
23,6 ugfL
25.0
94
52-151
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc:
449 Springbrook Road - P.O. Box 240W - Charlotte„ NC 8224-0643
.,�.
Phone: [phone] - Toll Froe Number: 1-8001629-6364 - Fax:
7041628 0409
Pag;
22C1

Level 11 CSC Report
Analytical &
AEnvironitiontal
IS
10/6/100
aFuii-Service
;� ( Solutions
v
Mv�'" gTCPflW CW�
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater Prism Work Order:: 0090620
Attn: Mahn Culbreath
Time Submitted. /27110 3:40:OOPM
RID, Box 87
Project Nib: NCO0
1038
Paw Creek, NC 28130
5ernivolatile organic Compounds by GC/M$ - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units Level Result %REC Limits RPD Limit Notes
Batch P010669 - 62
Blank (P010669-SLK1)
Prepared & Analyzed: 09128110
1,2,4-Triohlorobenzene
BRL
10
ug/L
1,2-Dichiorobenzene
BRL
10
ug/L
1,3-Dlchlorobenzene
BRL
10
ug/L
1,4-Dichlorobenzene
BRL
10
ug/L
2,4,6-Trihtorophenol
BRL
10
ug/L
2,4-Dichloropherrol
BRL
10
ugfL
2,4-Dimethylphenot
BRL
10
ug/L
2.4-Dinitrophenot
BRL
10
ug/L
,4-Dinit'otoluene
BRL
10
ug/L
2,6-Dinitrotoluene
BRL
10
ug/L
2-Chlorc naphthalene
BRL
10
ug/L
2-Chlorophenol
BRL
10
ug/L
2-Nitrophenol
BRL
10
ug/L
3,3"-Dichlorobenzidine
BRL
10
ug/L
4,6-Dinitro-2-methylphenol
BRL
10
ug/L
4-Brorn phenyl phenyl ether
EIRL
10
ug/L
4-Chloro-3-methylp enot
BRL
10
ug/L
4-Chlorophenyl phenyl ether
BRL
10
ug/L
4-Nitrophenol
BRL
50
ugL
Acenaphthene
BRL
10
ug/L
Acenaphthylene
BRL
10
ug/L
Anthracene
BRL
10
ug/L
Benzldine
BRL
100
ug/L
Benzo(a)anthracene
BRL
10
ug/L
Benzo(a)pyrene
BRL
10
ug/L
Benzo(b)fluoranthene
BRL
10
ug/L
Benzo(g,h,i)perylene
BRL
10
ug/L
Benzo(k)fluoranthene
BRL
10
ug/L
bis(2-hloroethoxymethane
BRL
10
ug/L
Bis(2-Cloroethyl)ether
BRL
10
ug/L
Sis(2-chloroisopropyl)other
BRL
10
uglL.
Bis(2-Ethylhexyt)phthalate
BRL
10
ug/L
Butyl benzyl phthalate
BRL
10
ug/L
Chrysene
BRL
10
ug/L
Dibenzo(a,fuanthracene
BRL
10
ug/L
Methyl phthalate
BRL
10
ug/L
Dimethyl phthalate
BRL
10
ug/L
Di-n-butyl phthalate
BRL
10
ug/L
Di-n-octyl phthalate
BRL
10
ug/L
Fluoranthene
BRL
10
ug/L
Fluorene
BRL
10
ug/L
Hexach orobenzene
BRL
10
ug/L
Hexachlorobutadiene
BRL
10
ug/L
Hexachloroeyctopentadiene
BRL
10
ugfL
Hexachloroethane
BRL
10
ug L
lndeno(1,2,3-cd)pyrene
.BRL
10
ug/L
This report should not be reproduced, except In
449 Springbrook Road . F
Phone. [phone] - Toll Fri
written consent of Prism Laboratories, Inc.
lotte, NC 28224-064
5364 - Fax; 7041626.0409 Page 23 Of 3

Level 11 QC Report
.
P uII-Servf e Analytical s
nvironmentet Solutions
10/6110
"'l APC MC% WC.
Colonial Pipeline Company Project. Charlotte NPDES Stormwater
Prism Work Order, 0090620
Attn: John Culbreath
Time Submitted. /27/10 3.40MPM
P.O. Box 87
Project No. NCO031038
Paw Creek, NC 28130
Sernivolattle Organic Compounds by GAMS - Quality Control
Reporting
Spike
Source
%REC RPD
Analyte
Result
Limit
Units
Level
Result %REC
Limits RPD Limit Notes
Batch P010669 _ 626
Blank (Frdl0569-BLK1)
Prepared & Analyzed. 09/28/10
Isophorone
BRL
10
ug/L
Naphthalene
BRL
10
ug/L,
Nitrobenzene
BRL
10
ug/L
N-Nitrosodimethylamine
BRL
10
ugfL.
N-Nitroso-di-n-propylamine
BRL
10
ug/L
N-Nitrosodiphenylamine
BRL
10
ug/L
Pentachlorophenot
BRL
10
ug/L
Phenanthrene
BRL
10
ugfL
Phenol '
BRL
10
ug/L
Pyrene ,
BRL
10
ug/L
Surrogate 2,4,6-Tribromophenol 78.5
ugfL
100
78
26-139"
Surrogate:2-Fluorabiphenyl
39.2
ugfL
50.0
78
41-112
Surrogate:2-Fluorbpherlol:
41.0
ugfL
100
41
10-48
Surrogate: Nitrobertzene_d5
39.2
ug/L
50.0
78
34-102
Surrogate: Pheno%cis
25.3
ug/L
100
25
10-14
Surrogate: Terphenyl-04
46.9
ug/L
WO
82
1-165
t,CS(PO(0569-BSI)
Prepared Analyzed:09/28/10
1,2,4-Trichlorobenaene
75A
10
ug/L
100
75
44-142:
1,2-Dichlorobenzene
67.2
10
ug/L
100
67
32-129
1,3-Dlchlorobenzene
68.5
10
ug/L
100
68
20-124
1,4-Dlchlorobenzene
69.2
10
ug/L
100
69
20-124
2,4,6-Trlchlorophenol
83.1
10
ug/L
100
83
37-144
2,4-Dichlorophenol
75.6
10
ug/L
100
76
39-135
2,4-Dimethylphenol
77.5
10
ug/L
100
78
32-1 t9
2,4-Dinitrophenol
67.6
10
ug/L
100
68
10-191:
2,4-Dinitrotoluene
99.8
10
ug/L
100
100
39-139
2,6-Dinitrotoluene
94.2
10
ug/L
100
94
50-158'
2-Chloronaphthatene
70A
10
ug/L
100
70
60-118
2-Chlorophenot
72A
10
ug/L
100
72
23-134
2-Nitrophenol
76A
10
ug/L
100
76
29-182
„3"-Dichlorobenz dine
92A
10
ug/L
100
92
10-262
4,6-Dinitro-2-methylphenot
96.8
10
ug/L
100
97
10-181
4-Bromephenyl phenyl ether
84.e
10
ugfL
100
85
53-127
4-Chloro-3-methylphenot
79.7
10
ug/L
100
80
22-147
4-Chlorc phenyt phenyl ether
88,2
10
ug/L
100
88
25-158 ,
4-Nitrophenot
32,0
00
ug/L
100
32
10-132
Acenaphthene
85.8
10
ug/L
100
86
47-145
Acenaphthylene
87.1
10
ug/L
100
87
33-14
Anthracene
87.1
10
ug/L
100
87
27-133
Senzidine
204
100
ug/L
100
204
15-150 LH
Benzo(a)anthracene
96A
10
ug/L
100
96
33-143
Benzo(8)pyrene
99.8
10
ug/L
100
100
17-163
Benzo(b)fluoranthene
95A
10
ug/L
100
95
24-159
Benzo(g,h,i)perylene
96.3
10
ug/L
100
96
10-219
Benzo(k)fluoranthene
107
10
ug/L
100
107
11-162
bis(2-Ct loroethoxy)methane
86,0
10
ug/L
100
86
33-184
This report should not be reproduced, except In its entirety,
without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, No 28224-0643
Phone. [phone] -
Tall Free Number: 1-8001629-6364 - Pax: 704152"409
35

"M
LC_
S
BiS(
Bis(
BIS(
Buty
Chry
Dibe
Diet,
Dim
Di-n
Di-n
Flu
Fluo
Hex
Hex
Hex
Hex
Inde
Iso
Nap
NO
N-N
N-N
N-N
Pen
Phe
Phe
Pyre
Su
Su
So
So
Su
Sit
RA Full -Service nalytical &
I R ISM I Environmental Solutions
or
onial Pipeline Company Project, Charlotte NPDES Storm
I- John Culbreath
il Box 87 Project No: NCO031038
v Creek, NC 28130
ilvolatile Organic Compounds by GCIMS - Quality Control
Reporting
ilyte Result Limit Units
h P010669 - 626
(P010669-SSI) Pri
2-Chloroethyl)ether 80A 10 ug1L
2-chloroisopropyt)ether 87.2 10 ug/L
2-Ethylhexyl)phthatate 106 10 ug/L
I benzyl phthalate 105 10 ug/L
sene 90,0 10 ug/L
nzo(a,h)anthracene 97,3 10 ug/L
yt phthalate 85'5 10 ug/L
ethyl phthalate 76.9 10 ug/L
-butyl phthalate 91.6 10 ug/L
-octyl phthalate W6 10 ug/L
anthene 937 10 ug/L
rene 91"1 10 ug/L
achlorobenzene 85"1 10 ug/L
achlorobutadiene 72,5 10 ug/L
achlorocyclopentadiene 8(:L5 10 ug/L
chloroethane 69.0 10 ug/L
no(1,2,3-od)pyrene 99,11 10 ug/L
,horone 901 10 ug/L
fithatene 7&8 10 ug1L
benzene 84.7 10 ug/L
itrosodimethylamine 51.7 10 ug/L
itroso-di-n-propylamine 90A 10 ug/L
itrosodiphenylamine 101 10 ug/L
tachlorophenol 872 10 ug/L
nanthrene 88,9 10 ug/L
nol 292 10 ug1L
ne 103 10 ug/L
,ogate: 2,4,6-Tribrontophenal 91,0 uglL
,ogate: 2-Fluarobitittenyl 476 U91L
,ogate: 2-Fluorophenol 45,7 uglL
ogate. Nitrobenzene-cis44.3 ug1L
,ogate: Phenol-l:15 28,5 ug1L
,ogate: Terphenyl-d14 51,8 U91L
Level If QC Report
10/6/10
water Prism Work Order: 0090620
Time Submitted: 9/27/10 3:40:001"M
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
pared & Analyzed: 09/28110
100 80 12-158
100 87 36-166
100 106 10-158
100 105 10-152
100 90 17-168
100 97 10-227
100 85 10-114
100 77 10-112
100 92 10-118
100 100 10-146
100 94 26-137
100 91 59-121
100 85 10-152
100 72 24-116
100 80 27-120
100 69 40-113
100 99 10-171
too 90 21-196
100 79 21-133
100 85 35-180
100 52 10-119
100 90 10-230
100 101 69-142
100 87 14-176
100 89 54-120
100 29 10-112
100 103 52-115
too 91 26-139
50,0 95 41-112
100 46 10-48
50.0 89 34-102
100 28 10-34
50,0 104 31-165
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springlarook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-80016294364 - Fax- 7041626-0409 1 P7�qe
Level If QC Report
10/6/10
water Prism Work Order: 0090620
Time Submitted: 9/27/10 3:40:001"M
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
pared & Analyzed: 09/28110
100 80 12-158
100 87 36-166
100 106 10-158
100 105 10-152
100 90 17-168
100 97 10-227
100 85 10-114
100 77 10-112
100 92 10-118
100 100 10-146
100 94 26-137
100 91 59-121
100 85 10-152
100 72 24-116
100 80 27-120
100 69 40-113
100 99 10-171
too 90 21-196
100 79 21-133
100 85 35-180
100 52 10-119
100 90 10-230
100 101 69-142
100 87 14-176
100 89 54-120
100 29 10-112
100 103 52-115
too 91 26-139
50,0 95 41-112
100 46 10-48
50.0 89 34-102
100 28 10-34
50,0 104 31-165
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springlarook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-80016294364 - Fax- 7041626-0409 1 P7�qe
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springlarook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-80016294364 - Fax- 7041626-0409 1 P7�qe

Level 11 QC Report
OD
Yl';ISM
Fuli-Servics Analytical 8
Environmental Solutions
10/6/10
&"��aopwopvs 'Ma
Colonial Pipeline Company Project: Charlotte NPDES Stormwater
Prism Work Order:
0090620
Attn: John Culbreath
Time Submitted: 9/27/10
3:40:00PM
P.O. Box 87
Project No: NCO0 1038
Paw Creek, NC 28130
Sernlvr latile Organic Compounds by GC1MS - Quality Control
Reporting
Spike
Source
%REC
RPD
Analyte
Result
Limit
Units
Level
Result %REC
Limits
RPD
Limit- Notes
Batch P010669 » 626
LCS Chip (P010669-13SM)
Prepared & Analyzed: 09/28/10
v
®.
1,2,4-Trichlorobenzene
82.3
10
ug/L
100
82
44-142
9
20
1.2-Dichlorobenzene
75,0
10
ug/L
too
75
3 -129
11
20 ;
1,3-Dichlorobenzene
75.6
10
ugCL
100
76
20-124
10
20
1,4-Dichlorobenzene
76,0
10
ug/L
100
76
20-124
9
20
2,4,6-Trichlorophenol
88,0
10
ug/L
100
88
37-144
6
20
2,4-Dichlorophencl
77A
10
ug/L
100
77
39-135
2
20:
2,4-Dimethylphenot
80.0
10
ug/L
100
80
3-119
3
20
2.4-Dinitrophenol
743
10
ug/L
100
74
10-191
9
20 ,
2,4-Dinitrotoluene:
115
10
ug/L
100
115
39-139
14
20
2,6-Dinitrotoluene
106
10
ug/L
100
106
50-158"
11
20
2-Chlorc naphthalene
78.1
10
ug/L
100
78
60-118
10
20
2-Chlorophenol
73.9
10
ugfL
100
74
23-134
2
20
2-Nitrophenol
78.3
10
ug/L
100
78
29-182
3
20
3,3'-Diichlorobenzidine
111
10
ug/L
100
111
10-262
18
20
4,6-Dinitro-2-methylphenol
97.5
10
ug/L
100
97
10-181
0.7
20
4-Bromophenyt phenyl ether
103
10
ug/L
100
103
53-127
20
20
4-Chloro-3-methylphenol
85.8
10
ugfL
100
86
22-147
7
20
4-Chlomphenyl phenyl ether
971
10
ug1L
100
97
25-158
10
20
4-Nitrophenol
38.6
50
ug1L
100
39
10-132
19
20
Acenaphthene
91.7
10
ugfL
100
92
47-145
7
20
Acenaphthylene
94,0
10
ug/L
100
94
33-145
8
20
Anthracene
102
10
ug1L.
100
102
27-133
16
20
Benzidine
249
100
ug1L
100
249
15-150
20
20 LH
Benzo(a)anthracene
113
10
ugfL
100
113
33-143 -
16
- 20
Benzo(e)pyrene
116
10
ug/L
100
116
17-163
15
20-
Benzo(b)fluoranthene
115
10
ug/L
100
115
24-159
19
20
Benzo(g,h,i)perylene
109
10
ugfL
100
109
10-219
13
20
Benzo(k)iluoranthene
116
10
ug1L
100
116
11-162
9
20
bis(2-Chloroethoxy)methane
90,5
10
ug1L
100
91
33-184
5
20
Bis(2-Chloroethyl)ether
84.3
10
ug/L
100
84
12-158
5
20:
Sis(2-ct loroisopropyl)ether
92.6
10
ugCL
100
93
36-166
6
20
Bis(2-Ethylhexyl)phthalate -
121
10
ug/L
100
121
10-158
13
20
Butyl benzyl phthalate
120
10
ug/L
100
120
10-152
13
20
Chrysene
102
10
ug/L
100
102
17-168
12
20
Dibenzo(a,h)anthracene
114
10
ug/L
100
114
10-227 "
15
20
Diethyl phthalate
94.2
10
ugfL
100
94
10-114
10
20
Dimethl phthalate
85.2
10
ugfL
100
85
10-112
10
20
Di-n-butyl phthalate
100
10
ug/L
100
100
10-118
9
20
Di-n-octyl phthalate
112
10
ug1L
100
112
10-146
12
20
Fluoranthene
102
10
ugtL
100
102
26-137 '
9
20'
Fluorene
98.4 :
10
ug/L
100
98
59-121
8
20
Hexachlorobenzene
99.3
10
ug/L
100
99
10-152
15
20
Hexachlorobutadiene
76.8
10
ug/L
100
77
24-116
6
20
Hexachlorocyclopentadiene
86.7
10
ug/L
100
87
27-120
7
20;
Hexachloroethane
77.5
10
ug/L
100
77
40-113
12
20`
Indeno(1,2,3-cd)pyrene
118
10
ug/L
100
lie
10-171
17
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.D. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] -
Toll Free Number: 1-8001629.63 4 • Fax. [phone]
1 t7=

w
Level 11 QC Report
Full-ServiceAnalytical 9
MR"!.,
ism nvironmental Solutions
10/6/10
Colonial Pipeline Company
Project: Charlotte'NPDES Stormwater
Prism Work Order 0090620
Attn: Jahn Culbreath
Time Submitted: 9/27/10 3;AU00PM
P.O. Box 87
Project o: NCO031038
Paw Creak, NC 28130
Semiv latile Organic Compounds by GCIMS - Quality Control
Reporting
Spike
Source
%REG
RPD
Analyte
Result
Limit
Units
Level
Result
°DREG
Limits
RPD' - Limit Notes
Batch'P01066 - 625
LCSDup{P010669-BSD1)
Prepared& Analyzed: 09128110
_.
lsophorone
96,2
10
ug/L
100
96
21-196
7 20 .
Naphthalene
85.7
10
ug/L
100
86
21-133
8 20
Nitrobenzene
91.5
10
ug/L
100
92
35-180
8 20 '
N-Nitrosodimethylamine
59A
10
ug/L
100
59
10-119
14 20:
N-Nitroso-di-n-propylamine
06.1
10
uglL
100
96
10-2 0
6 20
N-Nitrosodlphenylamine
118
10
ug/L
100
118
69-142
15 20
Pentachlorophenol
96.6
10
ug/L
100
97
14-176
10 20
Phenanthrene
107
10
ug/L
100
107
54-120
19 20
Phenol
28.0
10
ug/L
100
28
10-112
4 20
Pyrene '
125
10
ug/L
100
125
52-115
19 20 LH
Surrogate:2,4,6-Trlbromophenol
92.8
ug/L
100
93
26-139
Surrogate,, .-FluorobJehenyl
47 7
uglL
W 0
95
41-112
Surrogate:2-Fluorophenol
43.5
uglL
100
44
10-48
Surrogate. Nitrobenzene-d5
45.1
uglL
56r0
90
34-102
Surrogate. PhenoW5
26,3
uglL
100
26
10-34
Surrogate: Terphenyl-d14
58.1
u91L
5ti.0
116
31-165
Matrix Spike (P010569-MS1)
Source: 0090 20-01
Prepared. 09/28/10 Analyzed: 09/29/10
� � �
1,2,4-Trlchloroben ene
153
20
ug/L
200
BRL
77
44-142
1,2-Dichlorobenzene
137
20
ug/L
200
BRL
68
32-129
1,3-Dichiorobenzene
141
20
ug[L
200
BRL
71
20-124 "
1,4-Dichlorobenzene
144
20
ugtL
200
BRL
72
20-124
2,4„6-Trichlorophenol
171
20
ug/L
200
BRL
86
37-144
2,4-Dichlorophenol
159
20
ug/L
200
BRL
80
39-135
2,4-Dimethylpheriol
160
20
ug/L
200
BRL
80
-119
2,4-Dinitrophenol "
160
20
ug/L
200
BRL
80
10-191
2,4-Dinitrotoluene
192
20
ug/L
200
BRL
96
39-139
2,6-Dinitrotoluene
182
20
ug/L
200
BRL
91
50-158
2- hloronaphthalene
146
20
ug/L
200
BRL
73
60-118
2-Chlorophenol
148
20
ug/L
200
BRL
74
3-134
2-Nitrophenol
159
20
ug/L
200
BRL
79
29-182
3,3'-Dichlorobenzidine
180
20
ug/L
200
BRL
90
10-262
4,6-Dinitro-2-methylphenol
184
20
ug/L
200
BRL
92
10-181 ;
4-Bromophenyl phenyl ether
176
20
ug/L
200
BRL
88
53-127
4-Chioro-3-methylphenol
170
20
ug/L
200
BRL
85
22-147
4-Chlorophenyi phenyl ether
173
20
ug/L
200
BRL
87
25-158
4-Nitrophenol
98.9
100
ug/L
200
BRL
49
10-13
Acenaphthene
174
20
ug/L
200
BRL
87
47-145
Acenaphthylene
174
20
ug/L
200
BRL
87
33-145
Anthracene
175
20
ug/L
200
BRL
87
27-133"
Benzidine
221
200
ug/L
200
BRL
110
15-150
Benzo(a)anthracene
191
20
ug/L
200
BRL
95
33-143
Benzo()pyrene
195
20
ug/L
200
BRL
97
17-163
Benzo(b)fluoranthene
205
20
ug/L
200
BRL
103
24-159
Benzo(g,h,i)perylene
210
20
ugd.
200
BRL
105
10-219
Benzo(k)fluoranthene
163
20
ug/L
200
BRL
82
11.162
bis(2-Chloroethozy)methane
168
20
ug/L
200
BRL
84
33-184
This report should not be reproduced, except in its entirety,
without the written
consent of Prism Laboratories, Inc.
449 $pringbrook Road - P.A. Box 240643 - Charlotte, NC 28224.0643
..,.
' 35
Phone: [phone] -
Toll Free Number. 1-8001629-6364 - Fax:
704/ 25-0409
18 f

Level 11 QC Report
Full -Service
ISM
AWN"'L
Analytical &
10/6110
.- Environmental
Solutions
A 6 0T00t0$..IW-
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater
Priam Work Girder: 0090620
Attn: Jahn Cul reath
Time Submitted: 9/27/10 3:40:OOPM
P.f3, Box 87
Project No: NCO031038
Paw Creek, NC 28130
Sernivolatiie Organic Compounds by GC/MS - Quality Control
Reporting
Spike
Source
%REC RPO
Analyte
Result
Limit
Units
Level
Result
%REC
Limits RPD Limit Notes
Batch P010669 - 626
Matrix Spike (POi0669-MS1)
Source: 0090620-01
Prepared: 09/28/10 Analyzed: '09/29/10
Bis(2-Chloroethyhether
151
20
ug/L
200
BRL
76
12-158
Bis(2-chloroisopropyl)ether
170
20
ug1L
200
BRL
85
36-166
Bis(2-Ethylhexyl}phthala1e
196
20
ug/L
200
BRL
98
10-158
Butyl benzyl phthalate
194
20
ug/L
200
BRL
97
10-152
hrysene
181
20
ug1L
200
BRL
91
17-168
Dibenzo(a,hmanthracene
221
20
ugtL
200
SRL
110
10-227
Diethyl phthalate
158
20
ug1L
200
BRL
79
10-114
pimethyl phthalate
133
20
ug/L
200
BRL
67
10-112
Di-n-butyt phthalate
171
20
ug/L
200
BRL
86
10-118
Di-n-octyl phthalate
149
20
ug/L
200
BRL
75
10-146
Fluoranthene
174
20
ug/L
200
BRL
87
6-137
Fluorene
179
20
ug/L
200
BRL
89
59-121
Hexachlorobenzene
170
20
ug/L
200
BRL
85
10-152
Hexactdorobutadiene
148
20
ug1L
200
BRL
74
24-116
Hexachlorocyclopentadiene
167
20
ug/L
200
BRL
83
26-122
Hexachloroethane
144
20
ug/L
200
BRL
72
40-113
tndeno(, ,3-cd)pyrene
223
20
ug/L
200
EARL
112
10-171
Isophorone
177
20
ug/L
200
BRL
89
1-196
Naphthalene
164
20
ug/L
200
BRL
82
1-133
Nitrobenzene
169
20
ug/L
200
BRL
84
3 -180
N-Nltrosodimethylamine
140
20
ug/L
200
BRL
70
10-119
N-Nitroso-di-n-propylamine
175
20
ug/L
200
BRL
88
10-230
N-Nitrosodiphenylamine
199
20
ug/L
200
BRL
99
57-156
Pentac lorophenol
176
20
uglL
200
BRL
88
14-176
Phenanthrene
179
20
ug1L
200
BRL
89
54-120
Phenol
86.6
20
ug/L
200
BRL
43
10-112
Pyrene
226
20
ug/L
200
BRL
113
52-115 -
Surrogate: 2,1,8-THbrornophenol
170
u91L
200
85
26-139
Surrogate 2-Fluorobiphenyf
88.8
ug/L
100
89
41-112
Surrogate, 2-Fluoropherrol
110
091L
200
55
10-48 SR
Surrogate: Nitrobenzene-cl5
82,5
uglL
100
83
34-102
Surrogate: Phenol-d
80 3
uglL
200
40
10-34 SR
Surrogate: Terphenyt-04
102
ug/L
100
102
31-165
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc,
449 Sprincgbrook Road - P.O. Box 240643 - Charlotte, NC 29224-0643
Phone: [phone] -
Tali Free Number: 1- 001629.6364 - Fax:
7041525.0409
3

4 , .
Level 11 QC Report
ortt
u a : Fair Service Analytical
10/6110
Envirt nmentat Solutions
• l h6 PAYY5PIE MM
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater
Prism Work Order. 0090620
Attu: Jahn Cul reath
Time Submitted: 9/27/10
3:40:OOPM
P.U. Box 87
Project No: NCO031038
Paw Creek, NC 28130
Sern#volable, Organic Compounds by GCIMS - Quality Control
Reporting
Spike
Source
%REC
RPD
Analyte;
Result
Limit
Units
Level
Result
%REC
Limits
RPD
LimitNotes
Batch P010669 - 626
Matrix Spike Dup (P010569-MSD1)
Source: 0090620-01
Prepared: 09/28/10 Analyzed: 09/29/10
1,2,4-Trihlorobenene
168
20
ug/L
200
BRL
84
44-142
9
30
1,2-Dichlorobenzene
154
20
ug/L
200
BRL
77
2-129
12
34
1,3-Dichlorobenzene
158
20
ug/L
200
BRL
79
20-124
11
36
14-Dichlorobenzene
159
20
ug/L
200
BRL
80
20-124
10
35'
2,4,6-Trichlorophenol
197
20
ug/L
200
BRL
98
37-144
14
30 "
2,4-Dichlorophenol
173
20
ug1L.
200
BRL
87
39-135
8
33
2,4-Dimethylphenot
177
20
ug/L
200
BRL
88
32-119
10
36
2.4-Dinitrophenol
195
20
ug/L
200
BRL
97
10-191 -
19
41
„4-Dinitrotoluene'
225
20
ug/L
200
BRL
112
39-139
16
24
2,6-Dinitrotoluene'
222
20
ug/L
200
BRL
111
50-158
20
28
2-Chloronaphthalene
162
20
ug/L
200
BRL
81
60-118
11
30
2-Chlorophenol
169
20
ug/L
200
BRL
85
23-134
14
37:
2-Nitrophenot
178
20
ug/L
200
BRL
89
29-182
11
33
3,3'-Dichlorobenzidine
208
20
ug/L
200
BRL
104
10-262
14
34
4,6-Dinitro-2-meth 1phenol
226
20
ug/L
200
BRL
113
10-181
21
35
4-Bromdphenyl phenyl ether
203
20
ug/L
200
BRL
101
53-127
14
21
4-Chlorc-3-methylphenol
195
20
uglL
200
BRL
98
22-147
14
25
4-Chlorephenyl phenyl ether
201
20
ug/L
200
BRL
101
25-158
15
29
4-Nitrophenol
130
100
ug/L
200
BRL
65
10-132
28
40-
Acenaphthene
187
20
ug/L
200
BRL
93
47-145
7
33
Acenaphthylene
196
20
ug/L
200
BRL
98
33-145
12
30
Anthracene
201
20
ug/L
200
BRL
100
27-133
14
27
Benzidire
245
200
ug/L
200
BRL
122
15-150 '
10
50
Senzo( )anthracene
226
20
ug/L,
200
BRL
113
33-143
17
18
Benzo(a)pyrene
228
20
ug/L
200
BRL
114
17-163
16
21
Senzo(b)fluoranthene
-227
20
ug/L
200
BRL
114
24-159
10
34
Benzo(g,h,hperylene
260
20
ug/L
200
BRL
130
10-219
21
27
Senzo(k)ftuoranthene
205
20
ug1t,
200
BRL
102
11-162
23
39-
bis(2-Chloroethoxy)methane
184
20
ug/L
200
BRL
92
33-184
9
30
Bis(2-Chloroethyfiether
170
20
ug/L
200
BRL
85
12-158
12
33
Bis(2-chloroisoprcpyl)ether
192
20
ug/L
200
BRL
96
36-166
13
34
6ls(2-EthylhexyI)phthalate
237
20
ugtL
200
BRL
118
10-158
19
21
Butyl benzyl phthalate
228
20
ug/L
200
BRL
114
10-152'
16
: 23
Chrysene
205
20
ug/L
200
BRL
102
17-168
12
22
Dibenzo(a,h)anthracene
273
20
ug1L
200
BRL
137
10-227
21
28
Diethyl phthalate
180
20
ug/L
200
BRL
90
10-114
13
2
Dimethyl phthalate
147
20
ug/L
200
BRL
74
10-112
10
25
Di-n-butyl phthalate
194
20
ug/L
200
BRL
97
10-118
13
24
Di-n-octyl phthalate
186
20
uglL
200
BRL
93
10-146
22
21 D
Fluoranthene
187
20
ug/L
200
BRL
93
26-137 '
7
26
Fluorene
200
20
ug/L
200
BRL
100
59-121
11
30
Hexachlorobenzene
194
20
ug/L
200
BRL
97
10-152
13
29
Hexachlbrobutadiene
163
20
ug/L
200
BRL
82
24-116
10
35
Hexachlprocyclopentadiene
179
20
ug/L
200
BRL
90
26-122
7
36
Hexachtcroethane
163
20
ug/L
200
BRL
82
40-113
13
37
Indeno(9,2,3-ed)pyrene
276
20
ug/L
200
BRL
138
10-171
21
34
This report should not be: reproduced, except in Its entirety, without the written consent of Prisr
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone; 7041 29-8 64 - Toll Free Number: 1-800/629.6364 - Fax; 704/626-04
Laboratories, Inc.
Pc

F'11-Service Analytical &
fit= M I EnVlronTnantW Solutions
`„ ILA Tram tWp
niel Pipeline Company Project: Charlotte NPDBS Stormwati
John Culbreath
Box 87 Project No: NCO031038
Creek, NC 28130
volatile Organic Compounds by GClMS - Duality Control
Reporting Spike
tte Result Limit Units Level
M*Jffr#1*K*W*W
Level It QC Report
10/6/10
Prism Work Order. 0090620
Time Submitted: 9/27/ 10 3.40:OOPM
aurce %REC RPD
esult %REC Limits RPD Limit Notes
09129/10
Isophorone
198
20
ug/L
200
BRL
99
21-196
11
27
Naphthalene
177
20
ug/L
200
BRL
89
21-133
s
35
Nitrobenzene
182
20
ug/L
200
BRL
91
35-180
7
34
N-Nitrosodimethylamine
146
20
ugtL
200
BRL
73
10-119
4
45
N-Nitroso-di-n-propylamine
194
20
ug/L
200
BRL
97
10- 30
10
33
N-Nitrosodiphenyla ine
220
20
ug/L
200
BRL
110
57-156
10
26.
Pentachlorophenol
214
20
ug/L
200
BRL
107
14-176
19
36
Phenanthrene
212
20
ug/L
200
BRL
106
54-10
17
23
Phenol
104
20
ug/L
200
BRL
52
10-112
18
43
Pyrene
271
20
ug/L
200
BRL
136
52-115
18
31
Surrogate: 2,4,6-Tribmirophenol
198
ug/L
200
99
26-139
Surrogate:2-Fluoroblphenyl
100
ucglL
100
100
41-112
,Surrogate:2-Fluorophenal
136
ug/L
200
68
10-48
SR
Surrogate: Nitrobenzene_d5
2.4
ug&
100
92
34-102
Surrogate: Phenol-d5
102
u91L
200
51
10-34
SR
Surrogate: Terphenyl-d14
127
ug/L
100
127
1-165
This report should not be reproduced, except In its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/62 - 364 - Fax: 70415 5w0409
.Y..rr.r.wwu.

Level 11 QC Report
Felt -Service Analytical
&ACP .,� ism Frevironmernal Solutions
1016/10
iASORArCifi f"'r INC.
Colonial Pipeline Company
Project: Charlotte NPDES Stormwater Prism Work Order: 0090620
Attn: Jahn Culbreath
Time Submitted: /27110 3:40:OOP►vl
P.O, Box 87
Project No, NCO031038
Paw Creek, NC 28130'
General Chemistry Parameters . Quality Central
Reporting
Spike Source %REC RPD
Analyte
Result Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P010672 - NO PREP
Blank (P010 72-BLKI)
Prepared & Analyzed: 09/28/10
Turbidity
BRL 0,40 NTU
LCS (P010672•13SI)
Prepared & Analyzed. 09/28/10 _
Turbidity
4.40 0.A0 NTU
4.00 110 90-110
Duplicate (PO10672-17 P1)
Source: 0090620-09
Prepared & Analyzed. 9/28/10
Turbidity
18.5 0 A0 NTU
17.7 4 20
Batch P010610 - 420.1
Blank (PO10610•BLKI) _
_
Prepared: 09/29/10 Analyzed: 09/30/10
Phenolics
BRL 0.050 mg/L
LC S (PO10610-BSI)
_
Prepared: 09/29/10 Analyzed: 09/30110
Phenolics
0.567 0,050 mg1L.
0600 94 80-120
Batch P01063 - NO PREP
Blank (Po10638-BLKI)
Prepared & Analyzed:09/30/10
Oil & Grease (HEM)
BRL 5:0 mgtL
LCS (P IO638-BSI)
Prepared & Analyzed: 09/30/10
Oil & Grease (HEM)
33.6 5.0 mgtL
4 i.0 84 78-114
Batch POJ02 - NO PREP
Blank (POJ0024-BLKI) uµ
Prepared & Analyzed: 10/01110 rr mm
Total Suspended Solids
BRL 5.0 mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 �,
Phone: [phone] - Tall Free Number; 1.8001629-6364 - Fax: [phone] i 17

ll M
Lave[ 11 QC Report
Fail -services Analytical &
Environmental solutions
APRF"LASCRATORIES,
10/6/10
. lac:
Colonial Pipeline Company
Project: Charlotte NPIJES Stormwater Prism Work Order: 0090620
Attn: Jahn Cu#breath
Time Submitted: 9/27/10
3:40.00PM
P,O. Box 87
Project o: NCO031038
Paw Creek, NC 28130
General Chemistry Parameters --Quality Control
Reporting
Spike Source %REC '
RPC
Analyte
Result Limit Units
Level Result %REC Limits RPD
Limit Notes
Batch POJ00 - NO PREP
LCS (PJ0024-SS1)
Prepared & Analyzed: 10/01/10
Total Suspended solids
400 5.0 mgtL
406 98 90-110
Batch POJ004 - NO PREP
Blank (POJ0043-BLK°I) '
Prepared & Analyzed. 10/01/10
Oil & Grease (HEM)
BRL 5.0 mg/L
LCS (POJ0043-BSI)
Prepared & Analyzed: 10/01/10
Oil & Grease (HEM)
36.7 5:0 mg/L
40O 92 78-114
Matrix Spike (PQJ0043-MS7)
Source, 0090 20-03
Prepared & Analyzed: 10/01/10
Oil & Grease (HEM)
35.3 5.0 mgfL
44A BRL 79 78-114
Batch POJ0054 - NO PREP
Blank (POJ0054-BLK1)
Prepared & Analyzed: 10/04/10
Total Suspended Solids
BRL 50 mg/L
LCS (POJ0054-BS1)
Prepared & Analyzed:: 10/04/10
Total Suspended Solids
' 420 50 mg/L
406 104 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643
Phone: [phone] - loll Free Number: 1-8001629-6364 - Pax. 7041626-0409
,,,,, �,.,,,
Paige - 0 3
��IIXMOXYI�INYWI@FYe115MIF�N

Sample Extraction Data
Prep Method. 420.1
Lab Number
Batch
Initial
Final
gate
0090620-01
P010610
50
mL
50 mL
09/29/10
0090620-02
P010610
50
mL
50 mL
09/29/10
0090620-03
P010610
50
mL
50 mL
09/29110
0090620-04
P010610
50
mL
50 mL
09129/10
0090620-05
P010610
50
mL
50 mL
09/29/10
0090620-06
P010610
50
mL
50 mL
09/29i10
0090620-07
P010610
50
mL
50 mL
09129110
0090620-08
P010610
50
mL
50 mL
09/29/10
009060-09
P010610
50
mL
50mL
09/29/10
NO PREP
Lab Number
Batch
Initial
Final
pate
009062 -01
P010572
100
mL
100 mL
09/28/10
0090620-01
POJ0024
500
mL
500 mL
10101/10
0090620-01
P010635
900
mL
900 mL
09/30/10
0090620-02
P010572
100
mL
100 mL
09128110
0090620-02
POJ0024
500
mL
500 mL
10/01/10
0090620-02
POJ0043
900
mL
900 mL
10/01/10
0090620-03
P010572
100
mL
100 mL
09/28/10
0090620-03
POJ0024
500
mL
500 mL
10/01/10
0090620-03
POJ0043
900
mL
900 mL
10/01/10
0090620-04
PGJ0043
900
mL
900 mL
10/01/10
0090620-04
P010572
100
mL
100 mL
09128110
0090620-04
POJ0024
500
mL
500;mt-
10101/10
0090620-05
P010572
100
mL
100 mL
09/28/10
0090620-05
POJ0043
900
mL
900 mL
10/01/10
0090620-05
POJ0024
500
mt-
500 mL
10101110
00906 0-06
POJ0054
500
mL
500 mL
10/04/10
0090620-06
POJ0043
900
mL
900 mL
10/01/10
0090620-06
P010572
100
mL
100 mL
09/28110
0090620-07
P010572
100
mL
100 mL
09/28/10
0090620-07
POJ0043
900
mL
900 mL
10101/10
0090620-07
POJ0054
500
mL
500 mL
10/04/10
0090620-08
P010572
100
mL
100 mL
09/28/10
0090620-08
POJ0043
900
mL
900 mL
10/01/10
0090620-08
POJ0054
500
mt.
500- mL
10/04/10
0090620-09
POJ0054
500
mL
500 mL
10/04/10
0090620-09
P010572
100
mL
100 mL
09 28/10
0090620-09
POJ0043
900
mL
900 mL
/01/10
10/01/10
Prep Method. 626
Lab Number
Batch
Initial
Final
mate
0090620-01
P010569
1000
mL
1 mL
09129/10
0090620-02
P010569
1000
mL
9 mL
09/29/10
0090620-03
P010569
1000
mL
1 mL
09/29/10
0090620-04
P010569
1000
mL
1 mL
09/29110
0090620-05
P010569
1000
mL
'I mL
09/29/10
0090620-06
P010569
1000
mL
1 mL
09/29/10
0090620-07
P010569
1000
mL
1 mL
09/29/10
00906 0-08
P010569
1000
mL
1 mL
09/29/10
0090620-09
P010569
1000
mL
1 mL
09/29/10
NO PREP
Lab Number
Batch
Initial
Final
Date
This report should not be reproduced, except to Its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643
Phone: [phone] - loll Free Number, 1-8001629.6364 - Fax: [phone]

Sample Extraction Data
NO PREP
Lab Number
Batch
Initial
Final
hate
0090620-01
POJ0020
10
mL
10 mL
10101/10
0090620-02
POJ0020
10
mL
10 mL
10/01110
0090620-03
POJ0020
10
mL
10 mL
10101110
0090620-04
POJ0020
10
mL
10 mL
10/01/10
0090620-05
POJ0020
10
mL
10 mL
10/01/10
0090620-06
POJ0020
10
mL
10 mL
10/01110
0090620-07
POJ0020
10
mL
10 mL
10/01/10
0090620-08
POJ0020
10
mL
10 mL
10/01/10
0090620-09
POJ0020
10
mL
10. mL
10101/10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax. [phone] + t

ti
4 MP
I )404jia�lp:
550
mmm
IMITTT MIT I MIT 7WOMMENNIMMUNNEW I
ME
L9
wfflpy
sted Analysis Method
Oz

RECEIVED
DIVISION OF WATER QUALITY
1"r
FEB1 Colonial`Pipeline Company
awn SECTIUN
John W. Culbreath Office _ 704-399-5259
Environmental Specialist Fax [phone]
Southeast District E-mail [e-mail]
February 16, 2011
Mr. Rob Krebs
Regional Supervisor, DWQ -Surface Water Protection
NC ENR
Mooresville Regional Office
610 East Center Avenue
Mooresville, NC 2811
Re: Benzene Exceedence
NPDES Permit No. NCO031 I38 - Colonial Pipeline Company
Charlotte Delivery Facility
Mecklenburg County
Dear Mr. Krebs.
The analytical report for the January 19, 2011 sampling event at the above referenced facility revealed'
a permit exceednce for benzene from Outfall 010/MYO. The result from that outfall was 1.7 ug/l,
which exceeded the permit limit for benzene of 1.19 ug/l. A notification was made both telephonically
and via e-mail to John Lesley in the Mooresville Regional Office upon learning of the excedence on
February 10, 2010.
Colonial requests that your department not issue a Notice of Violation for the following, reasons:
Outfall 010/MYO is the discharge point from the facility's manifold yard oil / water separator.
Under normal operations Colonial has been able to maintain compliance at this outfall. It has been
non -detect for volatile organic compounds for the past two years, with the exception of a few minor
detections of xylenes (<10 ug/I) and toluene (<5 ug/1), and one detection of benzene (1.1 ug/1).
Colonial had performed some maintenance activities in the manifold area during late December 2010
and early January 2011. One of the maintenance activities that had been performed was in an area
associated with an old petroleum releaser This activity involved an excavation approximately 10' x 10'
x ' which' disturbed soils that contained residual petroleum contamination as a result of that releaser
Colonial believes that exposure of the excavation to the snow and stormwater events that occurred
during that period allowed some of the residual soil contamination to leach out and enter; the
subsurface stormwater drainage system, resulting in the exc eden e at the outfall.
Colonial views any type of non-compliance of a permit or regulation as a serious issue and i
committed' to investigating and addressing the root cause of such an event to prevent any repeat
occurrences. A recommendation that came out of our internal review of this issue was to develop a list
of best management practices (RMP's) specific to maintenance activities that take place in the
manifold area that could potentially lead to an exceede ce at this outfall. These BMP's will b
developed in the next few weeks and communicated to the Charlotte facility's operation and
7524 Kenstead Circle Pave Creek, NC 28130
P.Q. Box 87 ;Paw Creek, NC 28130

pr
VpPage2�
;
A9r. t ob Krebs - Benzene exceedence
February 16,2011
maintenance personnel in our annual Environmental Compliance training that is held each year in
March.
I hope you will consider this request. If you have any questions or need any additional information, I
can be ruched 704-399-5 59 or at the letterhead address.
Sincerely,
John W. Culbreath
Environmental Specialist
Enclosure
Colonial Pipeline company

Leal v. Jahn
Culbreath, Jahn W [JCulbre
Thursday, February 10, 201
Lesley, Jahn
Richards, Jeff W
E: Benzene limit exceedence-
)e.com]
M
Pipeline Co. - NPDES Permit No. NCO031038
) document notification to NCDENR of a benzene
renzene sample collected on January 19, 2011 was
vpq ac tha rlicarharnc. nnint from nrir mnnifnld grpq
oil/water separator (OWS). The OWS has been cleaned since this exceedence occurred.
As we discussed, 1 will be submitting a letter to Rob Krebs, Regional Supervisor explaining the upset condition that we
believe may have contributed to this exceedence.
Thank you.
John Culbreath
John W. Culbreath
Environmental Specialist
Colonial Pipeline Company - Southeast ist ict
Office- 7-399-5259

�'A
12N= MOMOMM FILE,,
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governer Director Secretary
December 22, 2010
Mr. Andy Martin, Operations Manager
Colonial Pipeline Company
Pest Office Box 87
Paw Creek; NC 2138
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline. Company
NPD S Permit No, NCO0310 8
Mecklenburg County, NC
Dear Mr, Martin:
Can August 23, 2010, Jeff Mitchell of the Mecklenburg County Water Quality Program (MCWQP)
conducted an inspection at the subject facility. This inspection was conducted as part of a cooperative
working agreement between Mecklenburg County and the Division of Water Quality, The enclosed
report should be self-explanatory.
If you have any questions concerning this report or any rather matters, please do not hesitate to call Ms.
Allocco or me at this office,
Sincerely,
n 4
, ` 1
for Robert B, Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc; Rusty Roelle, MCQP
RBK/JGM
Mooresville Regional Office
Location: 610 East Center Ave., Suite 301, Mooresville, NC 28115 On
Phone: [phone] t Fax: [phone] Customer Service:1-877-623-6748 NofffiCarohtia
Internet: http://portals cdenr,org/web/wq
An Equal Opportunity 1 Affirmative Action Employer- 300% Recycled/1 o°/a Post Con Sumer paper XMI11rallil

GENERAL:
The facility was last inspected on October 22, 2009, by Jeff Mitchell of the Mecklenburg County Water
Quality Program (MCWQP).
PERMIT.
The current permit became effective; on March 1,2006, and expired on June 30, 2010. A permit
renewal application was submitted December 29, 2009. The new permit is currently under review by
the Division of Water Quality. Until the new permit is issued the facility should continue to operate
under the requirements of the expired permit.
The permit authorizes the discharge of stormwater and treated effluent from the water pollution central
system. The portion of the facility associated with the NPDES treatment works consists of spill control
basins surrounding the aboveground; petroleum storage tanks, the manifold yard, and an oil/water
separator, with the flow routed to a retention pond. The permit properly describes the facility and
appears adequate for the wastewater being discharged, The permit provides that after March 1, 2008,
the facility is authorized to discharge from outfalls 002, 003, 004, 005, 006, 007, 008, 009, and MYQ-
Maniold Yard Qutfall. The facility is now required to sample as outlined in the permit at all permitted
outfalls.
The certification classification for NCO031038 requires that the facility have an operator in responsible
charge (QRC) with a grade 1 Physical Chemical Water Pollution Control System (PC-1) certification.
The facility is staffed ( RC and back-up) with personnel that possess the appropriate operator
certification.
RECORDS/REPORTS:
Copies of effluent analytical results are readily available at the facility. Records, reports, and logs are
clear and well maintained.
FACILITY SITEREVIEW:
All of the major components of the facility were in service and appeared to be operating properly at the
time of the inspection. The facility has a General' Wastewater Discharge Permit (NCG510207) to
discharge treated groundwater to an unnamed tributary of Gun Branch, a class WS-IV water in the
Catawba River Basin. The groundwater remediation system was not evaluated as part of the
inspection. The facility has a Wastewater Surface Irrigation Permit (WQ0004751). The sprayirrigation
system was not evaluated as part of the inspection.
FLOW MEASUREMENT:
Flow is estimated at each outfll by calculation of the rainfall and drainage area.
LABORATORY.
Chemical analyses of effluent samples is performed by Prism Laboratories, Inc. (NC Laboratory
Certification #40).' Prism Laboratories, Inc.; was not evaluated during this inspection. Acute Toxicity
testing is performed by Environmental Testing Solutions, Inc. (NC Laboratory Certification Biological
#37). Environmental Testing Solutions, Inc. was not evaluated as part of this inspection.
Mooresville Regional Office
Evocation: 610 East Center Ave., Suite 301, Mooresville, NC 28115 rte Phone: [phone] Fax: [phone] Customer Service: 1-877-623-6748 N6fthCarohna
Internet: http://por al.ncdenr.org/web/wq
An Equal Opportunity 1Affara€ive Action Employer 30% Recycled/10 a Post Consumer paper €

EFFLUENT/RECEIVING WATERS:
The receiving waters were clew at the time of the inspection. No petroleum sheens were
facility discharges to an unnamed tributary to Gum Branch, which is a Class -IV water i
Catawba Rarer Basin. .
SELF -MONITORING PROGRAM:
;eptions;
ance_of a Notice

a
tl
FILE
NCDENR
IF Noah Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen N. Sullins [lee Freeman
Governor Director Secretary
May 1 , 201 0
Ken Barimo, Operations Manager
Colonial Pipeline Company
Post Office Box 87
Paw Creek, NC 2 130
SUBJECTS Compliance Evaluation `Inspection
Colonial Pipeline Company
NPIES Permit No. NC03 13 8
Mecklenburg County, NC
Lear Mr. Barimo::
On October 22, 2009, Jeff Mitchell of the Mecklenburg County Water (duality Program (MCW P)
conducted an inspection at the subject facility. This inspection was conducted as part of a cooperative
working agreement between Mecklenburg County and the Division of Water (duality. The enclosed
report should be self-explanatory,
If you have any questions concerning this report or any ether matters, please do not hesitate to call Ms.
Allocco or me at this office.
Sincerely,
for Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty Rozzelle, MCWC, P
RBKJadm
Mooresville Regional Office
Location: 610 East Center Ave., Saute 301, Mooresville, NC 23115 One
Phone: [phone] t Fax; (704) 66MO40 ! Customer Service: 1-877-623-6748 o1 hCarC}h a
Internet: hgp:Hportal,ncdenr.org/web/wg
An Equal Opportunity % Affirmative Action Employer- 30% Recyde,1!10% Past Consumer oaper

P ITNE RA L:
The facility was last inspected on July 30, 2008 by Mr.
Water Quality Program ( CW{ P). A Compliance Evaluation
, 2008.
'ERIMIT.
°ibes the facility
4arch i, 2008, ;
MYO-Manifol(
tied outfalls.
C0031038 requ;
nical Water Pol
trpher Elmore of the Mecklenburg County
action (CEI) Report Was issued. on August
pines on .Tune 30, 2010. The permit
vvater pollution control system. The
tr sists of spill control basins surrounding
Dil/water separator, with the flow routed to
rs adequate for the wastewater being
y is authorized to discharge from outfalls
itfall. The facility is now required to
RTk
ffluent analytical results are readily available at the facility. Records, reports, and logs
itai.ned.
,VI W:
time of the inspection.
FLOW MEASUREMENT:
Flow is estimated at each outfall by calculation of the rainfall and drainage area.
LA ORATOR"Yc
The peg ittee contracts with Prism Laboratories, Inc. (NC Laboratory Certification #40) to perfor
chemical analyses and acute Toxicity testing specified in the permit. Prism Laboratories Inc. was ,not
evaluated during this inspection:
EFLUE T CIEIVI WATERS;
The receiving waters were clear at the time of the inspection. No petroleum sheens were noted'. I
facility discharges to an unnamed tributary to Crum Branch., which is a Class W -IV water in the Cata b€
Basin.
Mooresville Regional Office Location: 610 East Center Ave,, Suite 301 Mooresville, NC 28115 One
Phone: [phone] t Fax: [phone] l Customer Service.1-677-623-6748North(
lntemet: hftp;Jfportal.ncdenr.orglwebovq
An F-CUal 00 ortunity i Affirmative Action, Emolot er - 30 Recvcled710% Post Consumer oaoer; Awl
e
the

R,O G RAM:
ng Reports ( Rs) were reviewed for the period June 2008 throi
.,mitt e met most permit effluent limits and monitoring frequen i
aeeption:

+'
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Celeen H. Sullins Dee Freeman
Governor Director Secretary
March 23, 2010
Mr. Jahn Culbreath, Environmental Specialist
Colonial Pipeline Company
Post Office Box 87
Paw Creek, North Carolina. 28130
Subject. Notice of Violation — Ef, Pent Limitations
Tracking #`: NCV-201U t19
Colonial Pipeline Company
NPDES Perrnit No. NCO031038
Mecklenburg County
Dear Mr. Culbreat:
A review of the December 2009 self -monitoring report for the subject facility revealed a violation of the
following parameter at Outfall 010/MY :
Date Parameter Reported Value Permit Limit
12/9/09Benzene 11 ug;/I I.19 ug/I (daily maximum)
Remedial actions, if not already implemented, should be taken to correct any problems. The Division
of dater (,duality may pursue enforcement actions for this and any additional violations. If the violations are o
a continuing nature, not related to operation and/or maintenance problems, and you anticipate remedial
construction activities, then you may wish to consider applying for a Special Order by Consent. You may
contact John Lesley of this Office for additional information.
If you have questions concerning this matter, please do not hesitate to contact Mr. Lesley or me at (70 )
663-1699.
Sincerely,
Robert B. Krebs
Surface Water Protection
Regional Supervisor
cc. Point Source Branch
Mecklenburg County Water Quality Protection
JL
Mooresville Regional Office
Location 610 East Center Ave., Suite 301 Mooresville, NC 281,15 One
Phone. [phone]Fax: [phone] ti Customer Service: 1-877-623-6748 NorthCarolina
Internet. wvrm.ncwaterquafity,ora
Natura.1111
An Equal Opportunity i Affirmative Action Employer— 30% Recycied110% Post Consumer paper

f-
AWA'r-
HCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
February 26 2010
John W. Culbreath
Colonial Pipeline
Post Office Box 87
Paw Creek, North. Carolina 28130
Subject; Notice of Violation - Effluent Limitations
Trading ##: NOV-2410-LV-007
Colonial Pipeline company
NPDES Permit No. NCO03103 8
Mecklenburg County
Dear Mr. Culbreath.
A review of the November ` 009 self -monitoring report for the subject facility revealed a violation of the
following parameter:
Pipe Parameter Reported Value Permit Limit
014 YO Benzene 4.7 a /l 1.19 ug/l
An explanation of the violation was attached to the Discharge Monitoring Report; therefore, no response to this
Notice is necessaryy.
Remedial actions, if not already implemented, should be taken to correct any problems. The Division of Water
Quality may pursue enforcement actions for this and any additional violations. If the violations are of a continuing nature,
not related to operation and/or maintenance problems, and you anticipate remedial construction activities, then you may
wish to consider applying for a Special Girder by Consent. You may contact Mr. Jahn Lesley of this Office for additional
information.
If you have questions concerning this matter, please do not hesitate to contact Mr. Lesley or me at 744/663-1699.
Sincerely,
Robert B. Krebs
Surface Water Protection
Regional Supervisor
cc: Point Source Branch
Mecklenburg County eater Quality Protection
Mooresville Regional Office
Location: 610 East Center Ave., Suite 301 (Mooresville, NC 28115 Onc
Phone: [phone] l Fax [phone] \ CUStOrrlet Service. 1-877-623-6748 N6rthCarolina
lnternethtry trir i v s,
An Equal Opportunity \ Affirmative Action Employer - 50% Recycled/10% Post Consumer pear

Allocco, Marcia
From: Culbreath, Jahn W [[e-mail]]
Seat: Monday, November 30, 2009 2:55 PM
T: Allocco, Marcia
Cc: Richards, Jeff W
Subject: NPDES Permit No. NCO031038 -Colonial Pipeline Co. -Benzene exceedence
Ms. Alloco:
I spoke with Mike Parker this afternoon and he informed me that the voice mail that I had left on his machine last
Wednesday, November 25`h was forwarded to you. As I stated in the voice mail, one of our outfall (0101MYO) sample
results for benzene was 4.7 ug/I,'exceeding the 1.19 ug/I limit in the permit. The exceedence was reported to me by the
lab on the morning the 25th This outfall is the discharge of the manifold yard oil/water separator. This is the first
exceedence from this outfall since we began monthly sampling in March 2008. The separator was checked for the
presence of free petroleum product and none was evident.
We are awaiting results from a re -sample to determine if the previous result was valid. If we get; back similar results, we
will arrange for a crew to clean the separator, hopefully later this week.
If you have any questionsor need additional information please let me know.
Thank you.
John Culbreath
John W. Culbreath
Environmental Specialist
Colonial Pipeline''Cor a - Southeast District
Office- 704-399-5 59

A74LA.
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coieen H. Sullins Dee Freeman
Governor Director r Secretary
October 21, 2009
Mr. Michael Andy Martin
tl
Colonial Pipeline Company � ..'
7524 Kenstead'Cir
Paw Creek, NC 28130
Subject: Renewalltice
NPDES'P -tiit NCO031038
Paw Creep Terminal
Mecklenburg County
Dear Permittee;
Your NPDES permit; expires on June 30, 2010. 'Federal (40 CFR 122.41) and North Carolina (15A
NCAC 2H.0105 (e)} regulations state that permit renewal applications must be filed at least 180 days prior
to expiration of the current permit. If you have already mailed your renewalapplication, you may
disregard this notice.
Your renewal package must be seat to the Division postmarked no later than January 1, 2010.
Failure to request renewal by this date may result in a civil penalty assessment. Larger penalties may be
assessed depending upon the delinquency; of the request.
If any wastewater discharge will occur after June 30, 2010, the current permit must be renewed.
Discharge of wastewater without a valid permit would violate North Carolina General Statute 143-215.1;
unpermitted discharges of wastewater may be assessed civil penalties of up to $25,000 per day.
If all wastewater discharge has ceased at your facility and you wish to rescind this permit, contact
e at the telephone number or address listed below.
Use the enclosed checklist to complete your renewal package. The checklist identifies the items you
must submit with the permit renewal application. If you have any questions, please contact me at the
telephone number or e-mail address listed below.
Sincerely,
Charles H. Weaver, Jr.
NPDES Unit
cc Central Files
a,
"DES Fi e
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 One
512 North Salisbury Street, Raleigh, North Carolina 27604 N6fthCarohna
Phone: [phone] FAX [phone] charies,weaver@ncdenr,gov Naturally
An Equal Opportunity/Affirmative Action Employer - 50% Recycledl10% Post Consumer Paper

NPDES PERMIrl
for all renewal packages:
e permit and documenting any changes at the f
igned original and two copies.
1 a consul
ion must
II.B. 1 Lb
.ems must be submitted by any Municipal or Industrial facilities dischargLng
)ter:
classified as Primary Industries (see Appendices A-D to 'Fide 40 of the Code of Federal
.22) and ALL Municipal facilities with a permitted flow > 1.0 MGD must submit a
knalysis (PPA) M' accordance with 40 CFR Part 122.21.
ruirement does NOT apply to privately owned laciUdes treating 100%
`ewater, or JaciUdes which discharge non -process wastewater (cooKng
ckwash, etc.)
Send the completed renewal package to:
Mrs. Dina Sprinkle
NC DENR / DWQ / Point Source Branch
1617 Mail Service Center
Raleigh, NC 27699-1617

\N A 7-,- Michael R Easley, Governor
William G- Ross Jr., Secretary
� North Carolina Department of Environment and Natural ResOUTUS
Coleen H. Sullins, Director
Division of Water Quality
November 7, 2008
CERTIFIED MAIL 7007 1490 0004 4510 0646
RETURN RECEIPT REQUESTED
Mr. Ken Barimo
Colonial Pipeline Company
Post Office 87
Paw Creek, North Carolina 28130
Subject: Notice of Violation - Effluent Limitations
Tracking #: NOV-2008-LV-0529
Colonial Pipeline Company Outfall 003 W\IVTP
NPDES Permit No. NCO031038
Mecklenburg County
Dear Mr. Barimo:
A review of the July 2008 self -monitoring report for the subject facility revealed a
violation of the following parameter:
Pipe Parameter Reported Value Permit Limit
003 Total Suspended Solids 67 mg/1 (daily maximum) 45 mg/l (daily maximum)
Remedial actions, if not already implemented, should be taken to correct any problems.
The Division of Water Quality may pursue enforcement actions for this and any additional
violations. If the violations are of a continuing nature, not related to operation and/or
maintenance problems, and you anticipate remedial construction activities, then you may wish
to consider applying for a Special Order by Consent. You may contact Mr. John Lesley of this
Office for additional information.
If you have questions concerning this matter, please do not hesitate to contact Mr.
Lesley or me at 704/663-1699,
Sincerely,
d�
Robert B. Krebs
Surface Water Protection
Regional Supervisor
cc: Point Source Branch
Mecklenburg County Water Quality Protection
Mailing Address Phone [phone] Location NOne
��C,aro&a
610 East Center Avenue, Suite 301 Fax [phone] East Center Avenue, Suite 301 atitra
Mooresville, NC 28115 mooresviuc, North Carolina V71/
Internet: nmmL.ncrxFaeergna#Ety c ra Customer Service 1-877-623-6748
An Equal OpportunitylAffirmative Acfion Employer - 50% Recycled/10% Post Consumer Paper

keMichael F. Easley, Govern tir
William G, Ross Jr„ Secretary 14 1*4
North Carolina Department of Environment and Natural Resources
Coleen H. Sullins, Director
Division of Water Quality
August 14, 2008
Mt. Ken Barimo
Operations Manager
Colonial Pipeline Company
Past Office Box 87
Paw Greek, NC 28130
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline Company
Charlotte Delivery Facility
NPDES Permit No. NNG0034
Mecklenburg County, NC
Dear Mr. Barimo:
Enclosed is a copy oft e Compliance Evaluation Inspection report for the inspection
conducted at the subject facility on July 30, 2008, by Mr. Christopher Elmore of the
Mecklenburg County Water Quality Program (M Wt P). This inspection was conducted as part
of a cooperative working agreement between Mecklenburg County and the Division of Water
Quality. Please provide the facility"s Operator in Responsible Charge with the findings of the
inspection by forwarding a copy of the enclosed report.
The enclosed report should be self-explanatory; however should you have any questions
concerning this report or any other matters, please do not hesitate to call Ms. Marcia Allocco or
me at this Office, (70) 63-1699.
Sincerely,
.for Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty R.ozzelle, M WQP
NaarthCarolina
: VC?77I6 ltl
Mooresville Regional Office Division of Water Quality Phone 704-663-I6 9 Customer Service
Internet. w ww ncti -ter pLd t c r„ 61 Q Fast Center Ave, Suite 301 Mooresville, NC 28115 Fax [phone]
An Equal Opportunity/Affirmative Action Employer - 50% Recy led/10% Post Consumer Paper

Transaction Code NPDES Permit No. YR/MO/DAY Inspection Type Inspector Facility Type
N 5 NCO031038 08/07/30 C C 2
Remarks:
Inspector: Mecklenqb!Egg �Count X Water Quality Program
Inspection Work Days Facility Self -Monitoring Evaluation Rating BI QA ,.,.,.,,,.Reserved......
0,75 3 N N
L—
EPA For.
Entry Time: Permit Effective Date:
,ovation of Facility Inspected: 09:30 am March 1, 2006
eline Company Exit Time:
livery Facility I I - 10 pm Permit Expiration Date:
ad Circle Date: June 30, 2010
County, No Carolina July 30, 2008
Dn-Site Representatives ------Title(s) -------- Phone No(s):
lbreath / Environmental Specialist / Phone: [phone]
.iards / District Environmental Project Manager / Phone: [phone]
Wdress of Responsible Official: Title: Operations Manager
�imo
eline Company Phone No. Contacted?
Sox 87 [phone] No
NC 28130
L:g Flow Measurement Operations & Maintenance LJ Sewer Overflow
its JE Self -Monitoring Program El Sludge Handling/Disposal El Pollution Prevention
eview El Compliance Schedules E3 Pretreatment Program El Multimedia
vino Waters Laboratory Stormwater Other:
--F"v- kaj. A
tore MCWQP/[phone] August 5, 200
.viewer, Agency/Office: D t
R — Division of Water Quality
60-3 (Revised 3-85) Previous Editions are Obsolete

FGEL:
The Mecklenburg County Water Quality Program (MCWQP) last inspected the facility on
July 9, 2007. A Compliance Evaluation Inspection (CEl) Report was issued on July 23, 2007.
PERMIT:
The current permit became effective on March 1, 2006, and expires on June 30, 2010.
The permit authorizes the discharge of stormwater and treated effluent from the water pollution
control system. The portion of the facility associated with the NPDES treatment works consists
of spill control basins surrounding the aboveground petroleum storage tanks, the manifold yard,
and an oil/water separator, with the flow routed to a retention pond. The permit properly
describes the facility and appears adequate for the wastewater being discharged. The permit
provides that after March 1, 2008, the facility is authorized to discharge from outfalis 002, 03,
004, 005, 006, 007, 008, 009, and MYO-Manifold Yard Outfall. The facility is now required to
sample as outlined in the permit at all permitted outfalis.
The certification classification for NC003103 8 requires that the facility have an operator
in responsible charge (ORC) with a Grade 1 Physical Chemical Water Pollution Control System.
(PC-1) certification. The facility is staffed (ORC and back-up) with personnel that possess the
appropriate operator certification.
RECORDS/REPORTS:
Copies of effluent analytical results were readily available at the facility. Records;
reports, and logs were clear and well maintained.
FACILITY SITE VIEW:
All of the major components of the facility were in service and appeared to be operating
properly at the time of the inspection.
FLOW MEASUREMENT:
Flow is estimated at each outfall by calculation of the rainfall and drainage area.
LABORATORY:
The permittee contracts with Prism Laboratories, Inc. (NC Laboratory Certification #40)
to perform all chemical analyses and toxicity testing specified in the permit. Prism Laboratories,
Inc. was not evaluated during this inspection.
EFFLUENT/RECEIVING WATERS:
The receivingwaters were clear at the time of the inspection. No petroleum sheens were
noted. The facility discharges to an unnamed tributary to Gum Branch, which is a Class W -1V

N
14
in the Catawba River Basin.
F-MONITORING PROGRAM:
[he review period. Sample collection, preservation,
Lr adequate.
iANCE:
ipeline personnel t(
remain locked in the closed position unless inspections are performed by facility personnel.

,4 Michael F. Easley, Governor 01
William G. Ross Jr:, Secretary
North Carolina Department of Environment and Natural Resources
0 "C Coleen H. Sullins, Director
Division of Water Quality
August 14, 2008
Mr, Ken Banmo
Operations Manager
ColonialPipeline Company
Post Office Box 87
Paw Creek, NC 2813
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline Company
Charlotte Delivery Facility
NPDES Pe it No. NCO031038
Mecklenburg County, NC
Dear Mr.. Bario,
Enclosed is a copy of the Compliance Evaluation Inspection report for the inspection
conducted at the subject facility on July 30, 2008, by Mr. Christopher Elmore of the
Mecklenburg County Water Quality Program (CP). This inspection was conducted as part
of a cooperative working agreement between Mecklenburg County and the Division of Water
Quality, Please provide the facility's Operator in Responsible Charge with the findings of the
inspection by forwarding a copy of the enclosed report.
The enclosed report should be self-explanatory; however should you have any questions
concerning this report or any other matters, please do not hesitate to call Ms. Marcia Allocco or
me at this Office, [phone]
Sincerely,
vfvr Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty Rozzelle, MCWQP
N One Carolina
✓�ft��lll't7��lf
077161
Mooresville Regional Office Division of Water Quality Phone [phone] Customer Service
Internet: vyvvrv.ncvyaterqut it�,�.org 610 East Center Ave, Suite 301 Mooresville, NC 28115 Fax [phone]- i23-6748
An Equal Opportun tylAffirmative Action Employer— 50% Recycled/10% Post Consumer Paper

0•o81* United States Environmental Protection Agency:
NPDES Compliance Inspection Re
< e Division of
lty, Mooresville Region
1 1 is 1 1
4
! « ITT
®e •
• • ' • r •
Phone
�IIIYII
•
III III
!
�Rr�• ! �® a ••. e •
* e
�'
'
aM�� '� �141
� r � • �
• •
� '•. •. '-
a r:
EPA Form 560-3 (Revised 3- 5) Previous Editions are Obsolete

PFGE7NERAL:
The Mecklenburg County Water Quality Program (MCWQP) last inspected the facility on
July 9, 2007. A Compliance Evaluation Inspection (CEI) Report was issued on July 23, 2007.
PERMIT:
The current permit. became effective on March 1, 2006, and expires on June 3, 2010.
The permit authorizes the discharge of stdrmwater and treated effluent from the water pollution
control system. The portion of the facility associated with the NPDES treatment works consists
of spill control basins surrounding the aboveground petroleum storage tanks, the manifold yard,
d an oil/water separator, with the flow routed to a retention pond. The permit properly
describes the facility and appears adequate for the wastewater being discharged. The permit
provides that after :March 1,2008, the facility is authorized to discharge from outfalls 002, 003,
00, 00, 006, 007, 08, 009, and MYO-Manifold Yard Outfall. The facility is now required: to
sample as outlined in the permit at all permitted outfalls.
The certification classification for NCO031038 requires that the facility have an operator
in responsible charge (ORC) with a Grade 1 Physical Chemical Water Pollution Control System
(PC-1) certification. The facility is staffed (ORC and back-up) with personnel that possess the
appropriate operator certification.
RECORDS/REPORTS:
Copies of effluent analytical results were readily available at the facility. Records,
reports, and logs were clear and well maintained.
FACILITY SITE REVIEW.
All of the major components of the facility were in service and appeared to be operating
properly at the time of the inspection.
FLOW MEASUREMENT:
Flow is estimated of each outfall by calculation of the rainfall and drainage area.
LABORATORY:
The permittee contracts with Prism Laboratories, Inc. (NC Laboratory Certification 40)
to perform all chemical analyses and toxicity testing specified in the permit. Prism Laboratories,
Inc. was not evaluated during this inspection.
EFFLUENT/RECEIVING WATERS:
The receiving waters were clear at the time of the inspection. No petroleum sheens were
noted. The facility discharges to an unnamed tributary to Gum Branch, which is a Class WS-IV

water in the Catawba River Basin.
SELF -MONITORING PROGRAM:
Discharge Monitoring Reports (DMRs) were reviewed
he review period. Sample collection, preservation, an
r adequate.
ACE:

Colonial Pipeline Company
John W Culbreath AIEP Office — 704-399-5259
Environmental Specialist Fax — 704-399-9029
Southeast District AUG I j 2008 E-mail —[e-mail]
July 28, 2008 OA
North Carolina Division of Water Quality AUG 1 4 2008
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Turbidity Exceedence / Outfall 009 June 2008
NPDES Permit No. NCO031038 - Colonial Pipeline Company
Charlotte Delivery Facility
Mecklenburg County
Dear sir / madam:
Enclosed you will find the Discharge Monitoring Reports (DMRs) for the June 2008 monitoring
period for the above referenced facility. A turbidity result of 55 NTU was reported for Outfall
009, exceeding the 50 NTU permit limit. A sample from the receiving stream was not
collect turbidity samples from both the discharge and the receiving stream on the next
quarterly sampling event. If the exceedence continues appropriate measures will be taken to
improve the discharge turbidity.
If you have any questions or need any additional information, I can be reached 704-399-5259
or at the letterhead address.
Sincerely,
John W.4Culbreath
Environmental Specialist RECEIVED
Enclosures
AUG 18
NC DENR MRO
M-Surface Water Protection
7524 Kenstead Circle Paw Creek, NC 28130
P.O. Box 87 Paw Creek, NC 28130

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) [K]
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements El
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the pennittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part ILE.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel property gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations,"
Ken S. Barimo
P ee (Please print or type)
-1-a -0 C9
Signature of Permittee*** Date
(Required unless submitted electronically)
PO Box 87 Paw Lreek, NC 28130 704-399-8513 _julbreaQcoiqe com 6/30/2010
PermilleeAddress Phone Number e-mail addren Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at hZ%—en—r—,state.ncu w finkin ' in rination ages.
gL--qs and g to the unit s information p
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period,
ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

EFFLUENT
■

I PPV
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) El
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements D
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens,
public health or the environment Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances, A written subinission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is mmcompfian4 please I!gc_h a list of corrective actions being taken and a time -table for
Improvements to be made as required by Part ILL6 of the NPDES permit
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Ken S. Barinio
Permittee (Please type)
Siinitu of Pennittee*** Date
(Required unless submitted electronically)
PO Box 87 Paw Creek, NC 28130 704-399-8513 [e-mail] 6/30/2010
Permittee Address Phone Number e-mail addmss Permit Expiration Date
ADDITIONAL CERTMED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h22.e�nnstate.n�c.us/w s and linking to the unit's information pages.
Use only units oftneasurement designated in the reporting facility's NPDES permit for reporting data,
No Flow/Discharge From Site: Check this box ifno discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DR for the entire monitoring period.
0RCOnSIte?: ?RC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
***Signature ofPermittee: if signed by other than the permittee, then the delegation ofthe signatory authority must be on
file with the state per 15A NCAC 2B M06(b)(2)(D):
Page 2

EFFLUENT
mum►
I -)I I I ►v I I I I I I I I I I I I I I I I

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet pentrit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements ED
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
It the facility is noneompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part ILE.6 of the NPDES, permit
"I certifyunder penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations,"
Ken S. Barimo
Permittee (Pie se print or type)
Signature of Pennittee** Date
(Required unless submitted electronically)
PO Box 87 Paw Creek, NC 28130 704-399-8513 [e-mail] 6/30/2�01O
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) CertificationNo.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at b2g,ML,state .nc.qs1w As and linking to the unit's information pages.
Use only units oftneasurement designated in the reporting facility's NPDES permit for reporting data,
No Flow/Diseharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
0RCOnSlte?: ORC must visit facility and document visitation of facility as required per 15A NCAC 80.0204.
*"Signature ofPermittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

ppprp,
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements El
Noncompliant
The pennittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomesi aware of the circumstances,
H the facility Is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part H.E. of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete, I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations,"
Ken S. Burling
Permittee (Please riat or type)
ZY
Signature of Permitted*** Date
(Required unless subnritted electronically)
PO Box 87 Paw Creek, NC 28130 704-399-8513 _Jcujbrea@oolp1pooDm 6/30/2010
Pennittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.uslwqs and linking to the unit's information pages.
Use only units of measurement`designated in the reporting facility's NPDES permit for reporting data,
No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
Signature of Permittee- If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D),
Page 2

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements r ---- I
I V I
(including weekly averages, if applicable) L-2�
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements El
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment Any information shall be provided orally within 24 hours from the time the ttee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility Is noncompliant, please jililgit a fist of corrective actions being taken and a time -table for
improvements to be made as required by Part HX6 of the NPDES permit
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and'imprisonment for knowing violations,"
Ken S. Barimo
Penniftee (Please print or type)
Signature of Pemiiftee*** Date
(Required unless submitted electronically)
PO Box 87 Paw Creek, NC 28130 704-399-8513 _Jculbres@colpi �.com 6/30/2010
Permince, Address Phone Number e-mail address Permit Fxpiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.ne.us/was and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data,
No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G 0204.
***Signature ofPermittee: If signed by other than the pennittee, then the delegation ofthe signatory authority must be on
file with the state per 15A NCAC 2B.0506(b)(2)(D),
Page 2

EFFLUENT
ffm
om
I.

Facility Status. (Please cheek one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements El
Noncompliant
The permittee shall report to the director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by fart H.E.6 of the NPDES permit
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly ;gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowingviolations."
Ken S. Barimo
Thee (Please print or type)
-
Signature ofPe ttee*** Date
(Required unless submitted electronically)
PO Box 87 Paw Creek, NC' 28130 704- 99-8513 )culbreat colp1:pe.co ot30/201
Pennittee Address Phone Number e-mail address Permit F,xpiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enrstate.nc.usfwus and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204.
*** Signature of Permittee. If signed by other than the perniittee, then the delegation of the signatory authority must be on
file with the state per I5A NCAC B .0506(b)(2)(D):
Page 2

•
not= mm own= m
�I�mm
mmmms
pjvtmpjm
.emit; JM&R 45 ug I I
Fonn MR-1 (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F-1
Noncompliant
The penniffee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to he made as required by Part KE.6 of the NPDES permit+•..
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the personor persons who managed the system, or those'persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. 1 am aware that there are significant penalties for submitting false information, including the possibility of
fires and imprisonment for knowing violations,"
Ken S. Barium
Permittee (Please print or type)
!Nig-nature Date
(Required unless submitted electronically)
PO Box 87 Paw Creek, NC 28130 704-399-8513 [e-mail] 6/30/2010
Pernmittee Address Phone Number e-mail addrm Permit Expiration Late
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3) Certification No,
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Sections web site at h2o.eru.state.nc.0 fwgs and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site; Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site7< ORC must visit facility and document visitation of facility as required per I SA CAC 8 .0204.
*** Signature of Per ittee: If signed by other than the per ittee, therm the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D):
Page

PV
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and samplingfrequencies do NOT meet permit requirements
Noncompliant
The pennittee shall report to the Director or the appropriate Regional Orrice any Noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the prmittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances.
If the facility is noneompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be madeas required by Part II.E,6 of the NPDES permit.
" 1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted, Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Ken S. Barimit
Permittee (Please print or type)
tgnature of P itiee*** Date
(Required unless submitted electronically)
PC? Box 87 Paw Cak NC 28130 704-399-8513 [e-mail] 6/30/2010
Permittee Address Phone Number a -mail address Pe nit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory () Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPD ES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us1w s and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge from Sher Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
* ORC On SHO: ORC must visit facility and document visitation of facility as required per l5A NCAC 8 .0204.
***Signature oC Permittee: If signed by other than the p rmittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

Facility Status•. (Please check one of the following)
All monitoring data and sampling frequencies meet perndt requirements
(including weekly averages, if applicable)
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens
public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee
became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee
becomes aware of the circumstances
If the facility is noncompliant, please attach a list of corrective actions being taken and atime-table for
improvements to be made as required by Part ILE.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Ken S. Barimo
Perrin (Please print or type)
Signature of Permittee*** Bate
(Required unless submitted electronically)
PO Box 87 Paw Creek, NC 28130 704-399-8513 iculbrea6colpipo.com 6/30/2010
Permutes Address Phone Number e-mail address Permit Expiration irate
ADDITIONAL CERTIFIED LA130RATORIES
Certified Laboratory () Certification No.
Certified Laboratory (3) Certification No.
Certified Laboratory (4) Certification No.
Certified Laboratory (5) Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state nc uslwcts and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPD S permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DhIR for the entire monitoring period.
** ORC On Site?: CIRC must visit facility and document visitation of facility as required per 15A NCAC 8G .0214.
***Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

NNA Michael F. Easley. Governor *�
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Colleen Sullins, Director
Division of Water Quality
August 31, 2007
Mr, John Culbreath
Colonial Pipeline Company
PC) Box 87
Paw Creek, NC 261
Subject: Toxicity Test Results
Colonial Pipeline Charlotte Delivery Facility
NPDES Permit No. NCO031038
Mecklenburg County, NC
Dear Mr. ulbreth.
Enclosed is a copy of the tonicity test results relative to the inspection conducted at the
subject facility on August 14, 2007 by Ms. Donna Hood of this office. The effluent sample was
collected on August 14, ; 007 by Donna Hood of this Office for use in an acute toxicity test. The
test utilizing this sample resulted in a pass.
The report should be self-explanatory; however should you have any questions
concerning this report, please do not hesitate to contact Ms. Hood or me at (7 4) 63-1699.
Sitcerely,
1-416
Robert B. Krebs
Surface Water Protection Regional Supervisor
Enclosure
cc. Central Files
Susan Meadows, Aquatic Toxicology Unit
Mecklenburg County LUESA
Mecklenburg County Health Department
DH
' .:�
Regional Office, 610 East Center Avenue, Suite 301, Mooresville, NC 281 l5 [phone] Customer Sear
1.877-623-674l

peline Company
elivery Facility
-mit No. NCO031038
itic toxicity test using a grab sample of effluent discharged from Colonial Pipeline -
to Gum Branch (7Q 10 of 0.00 CFS). A whole effluent sample was collected August 14,2007 by
MR O staff for use in an acute Pimephalespromelas definitive toxicity test. The LC50 for the
sample was greater than 100%. Toxicity test information follows:
Test Type 24-hour Pimephales promelas definitive
Test Concentrations 20, 40, 70, 90, and 100% sample
Test Result LC > 100%
Control Survival 100%
Test Treatment Survival 100% at 100% effluent
Sample pH 7.16 SU
Sample conductivity 105 micromhos/cm
Sample Total Residual Chlorine <0.0052 mg/L
Test results for this sample indicate that the effluent would not be predicted to have acute
water quality impacts on receiving water.
Basin: CTB34
N Vb9m
NC. Division of Water Quality, Mooresville Regional Office, 610 East Center Avenue, Suite 301, Mooresville, NC 29115 [phone] Customer Service
1-877-623-6748

IYQ
August 1, 2006
John W. Culbreath
Colonial Pipeline -Charlotte
PO .Pox 87
Paw Creek, NC 28130
€+.._1__._._s_ XT—..—..
;e:
of this letter is to call your attention to problems'
DMRs affect our staffs ability to prov
=1
Attention: Michele P
Division of "Water Qi
Central Files
1617 Mail Service
Raleigh, North Carolina 2
Michael Ex Easley, Governor
William C. Ross Jr., Secretary
'orth Carolina Department of Environment and Natural Resources
Alan W. Klimek, P. E. Director
on m w
AUK L4Prr
1
he following address.
k
1617
AUG 0 2 2006
,
you for your assistance in this hatter.
Sincerely,
Michele Phillips
cc:
Central Files
None I
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699.1617 Phone: [phone] Customer Service
Internet http:tth o.enrstate.nc.us 512 N. Salisbury St. Raleigh, NC 27604 Fax: [phone]
An Equal OpportunitylAffirrnative Action Employer

Nonce of Iiicompiete riscb.arge Monitoring Report
. it Number
Facility:
County*
DMR Month and Yun
The Division of Water Qualitydeems the aforementioned DMR as incomplete, clue to the
fold pan(s): (Mae seethe higghlighted areas on the attached DMRfor details.)
The written values art illegible.
The. Avetage, Maxiinum, and/or the Minimum data points have been omitted.
The Units of Measure have been omitted or incorrect
e DMR Parameter Codes have been omitted.
w -Ak acha
-34 0
t .?1 ' dtr h i& A'111E r 4in,17f—fi 1,6 4, ice. "aif . I fii P; r

xxrr mn Aloo 310 3 9 DIS(
INAL . ONE,COPY.
*IAL FILES
Seat MONTH M 'OfYE -d 6
CLASS! CO TY ' CC c A1AVk&-
(
G SAMPLE -Tl* N t + c A
— -
'RATOR IN RESPONSI13LE CHARGE) DATE
CERTIFY THAT TINS REPORT IS
LETE TO THE BEST OF My KNO E
si5I7tt,)-
1
�1
IL t
- g ..,
Mapc". *r. ':'
30
AVERAGE
a ,{«d
( *#0 /, <5.e 7ftt
DP.uYY1 S'om ,k R-1. t
(Rev` I )

Notice of Incomplete Dis
im r: t4&vu31o3Y
The written values are illegible
Monitoring Report
DMR as incomplete due to the
attached MR for details!
Ants have been emitted
,orrect
snolics, total recoverable, which you reported, our database shows the c(
14030'(Benzene), 34010 (Toluene) and 34694 (Phenol, single compound:
rTn this office if the analytical method used was indeed what ;you reporte
update your form template with the correct code and resubmit per the enclosed letter.

E(E )NT
NPDES PERMIT NO. NCO031038
DISCHARGE NCB.-001 — MONTH — June — YEAR-2006—
FACILITY NAME Colonial —Pipeline Company
CLASS P/C COUNTY Mecklenburg_
CERTIFIED LABORATORY (1)_Prism Laboratories, Inc.
—CERTIFICATION NO.402
—
(list additional laboratories on the backsidelpage 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC)
— John C
reathGRADE PC-1 CERTIFICATION NO.-28846 —
PERSOS) COLLECTING SAMPLES John Culbreath—
N(
3 ORC PHONE _ 704-399-5259
CHECK BOX IF ORC HAS CHANGED
NO FLO'W1 DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to:
4
ATTN: CENTRAL FILES
(E
DIVISION OF WATER QUALITY
URE OF OP P- -TOR IN U—SPONISIBLE CHARGE) DATE
-A
1617 MAIL SERVICE CENTER
BV, SSIGNATVRE�ICERTIFI'THAT'VIIISRLI'ORTIS
a SSIGNATVPE�ICEJ
RALEIGH, NC 27699-1617
UR�ATE AND COMPLETE TO THE REST OF MY KNOWLEDGE.
1) COMPLETE IPLEJ
50050 00530 00556
34481
54371 4235
81551 22417 32730
FLOW
ENTER PARAMETER CODE ABOVE
NAME AND UNITS BELOW
er uNt Lj
,t <
rnm F-H-Rs -7WBN.N I MGD -MZIL mv/L
ugll, I ma NTU
LLLLLL.,
2 730 8 y
777
===77T7777777-
N
777
777777::w
61 710 8 Y
N
10
: LIZE
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7777777=77777=777
14
16 930 6 y
77
18
777777,7,',:
20t 830 8 Y 0.0-145 11 <5.0
<1,0-
<1,0 <1.0
<3.O <5,0 -0,050 1 12
22 700 2 Y
--77=
24 N
26 N
27,
28
29, LLLLLL
N
77777===7777777777
At ERAGE 0.0791 11 <5JI
<1.0
<1.0 <1.0
<3.0 <5.0 <0.050 12
7=7;=

Michael F. Easley, Goverr
William G. Ross Jr, Secretx
NAlan W. Klimek, RE, Director
Division of Water Quality
June 23, 2006
Mr. Kirby Smith, General Manager -Operations
Colonial Pipeline Company
Post Office ]fox 1624
Alpharetta, Georgia 30009
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline Company
Charlotte Delivery Facility
ICES Permit No. NCO031 3
Mecklenburg County, NC
Dear Mr. Smith:
On; May 12, 2006, Mr. Christopher Elmore of the Mecklenburg County Water Quality
Program conducted an inspection at the subject facility. This inspection was conducted as part o
a cooperative working agreement between Mecklenburg County and the Division of Water
Quality. The enclosed report should be self-explanatory.
If you have any,questions concerning this report or any other matters, please do not
hesitate to call Mr. John Lesley or me at this Office.
Sincerely,
1-Ir
D. Rex Gleason, P. E.
Surface Water Protection Regional Supervisor
Enclosure
cc: Rusty Roelle,MCLQP
cfe
File: Wry 003103&0506
Ncoi�,e Cres n
DE ;OYMAY
Mooresville Regional Office Division of Water Quality Phone [phone] Customer Service
Internet: u v er till v. r * 610 East Center Ave„ Suite 301 Mooresville, NC 28115 Fax [phone] 3-6748
An Equal Opportunity/Affirmative Action Employer - 50 R ded/10% Post Consumer Paper

Signature c
John esle
EPA Form 36
c
Permit No. YR(MO/DAY In
31038 06/05/12
Remarks.°
Inspector: Mecklenbur o Water t
y Self -Monitoring Evaluation Rating
3
Section 13: Facility Dab
Entr
s ecte : 10.II
Exit`
1:1
Date
na May
isible Official:
Sludge
x Pretreat
� I"
;vised 3- 5) Previous Editions are Obsolete
:uuo
1.5500 May 1, 2006
Date:

Vvili
and
'he facility was last inspected by MCWQP on June 3, 2005 by Mr. Christopher Elmore
,,cklenburg County Water Quality Program (MCWQP
harge of stormwater and treated effluent from the water pollution
f the facility associated with the NPDES treatment works consists
ling the above ground petroleum storage tanks, the manifold.yard,
h the flow routed to a retention pond.
-,scribes the facilitv and avnears adecivate for the wastewater beine
Copies of effluent analytical results are readily available at the facility. Records, reports,
�gs are clear and well maintained.
LITY SITE REVIEW:
the retention pond in accordance with NPDES permit requirements.
Prism Laboratories, Inc. (N.C. Certification # 402) performs chemical analysis and
effluent toxicity analysis of effluent samples. Prism Laboratories was not evaluated under this
EFFLUENT/RECEIVING WATERS:
The effluent was clear at the time of the inspection. No petroleum sheens were noted.
The facility discharges to an unnamed tributary to Gum Branch, which is a Class WS-IV water in
the Catawba River Basin.

WRING PROGRAM:

Division of
Ierrtr
Jum
e Company
:1624
rgza 30009
SUBJECT: Compli
Colonii
Charlol
DE'.
Iveclrl
s:
R
liment and NaturalResources
r Quality
William G. Fuss, Jr., Secretary
Alan W. Klimek, P ., Director
, 2QU5
nce Evaluation Inspection
I Pipeline Company
to Delivery Facility
kPermit No. NCO031038
ftburg County, NC
County and the Division of Water
or any other natters, please do not
ice.
V-.
D. Rex Gleason, P. R.
* Surface WaterProtection Regional Supervisor
-
Enclosure
c: Rusty Rozzelle,MCWQ'
�RCrlcf
File; WQ 003103 .0605
Mooresville Ronal Office -One
610 East Center Avenue, Sub 301, Mooresville, North Carolina 2611
Phone: 7 -16 r 1 Fax. 763.6 t Internet: h2o.ent.state.nc.us Nawra(lff
An Equal tad unity/ ffir atly Action Employer - 50% Recyc 1ti t Consumer r

ENE
ay 24, 2004. A Compliance e Evaluation
n report was issuedon June 3, 2004.
C;
he current pennit became effective on Septem
icharged-
Z,C O S PORTS:
properly at the time of the inspection.
FLOW MEASUREMFNT.-
Flow is estimated by weekly instantaneousflaw measurements at the discharge pipe from
the retention pond, in accordance with NPDES perinit requirements.
LABORATORY.-
­U­
e t
tuzcrty,Mmulyw4lo e nt s aLVI pe o by .
Certification # 402). Prism Laboratories was not evaluated under this
`
Ion.

,Iq4N
EFFLUENT/RECEIVING WA
The effluent clear at the time of the inspection. No petroleum sheens were noted.
The twility discharges to an unnamedtributary to Gum Branch, which is a Class WS-TV water in
the Catawba River Basin.
SELF -MONITORING PROGRAM:
T%:- _._L..,.�..-- A 6,�.....s.m,..' .... 'Yf ,.........,.a.,. i'T`Y% %Y]._..0. m__,_r,_ .,.___ ....____ J P_ . 1_ _. Y A s{ r ^^ • a1 9
Records indicate
requirements.S lc
OPERATIONS & MA
Tbe facility and �
d daily I
Discharge valvei
locked and 1n the closed
J
,olation
and €u
n and sa&ty. _
g con ents remain
by facility
personnel.

ital Technician
e u , Suite
115
.kienburg County
n.
r a ,* a. a •+* a s r a ..: a a r.. r a ;W
Office —704-399-5259
Fax — 04-399 9029
harlotte DeliveryFacility
ce
t the cutf ll.
Sincerely,
John W. Culbreath
v
c. John McCulloch - MCLUESA
Jerry Ashcroft— CPC OperationsManager
Jeff Richards — SED Environmental Project Manager
JAN 0.7
VVAI
P.O.87 PawCreek, NC 28130

NCDENR
North
WSW
September 9
owski
line Company
Lis date may result in a civil asses
ie request,
G checklist to complete your renewal pack
-- 7 _— L.,.., i
Michael F. Easle
Govern(
William G. Ross, Jr., Secretat
Alan W. Klimek, P.E., Director
Division of Water Quality
Renewal Notice
D SPermitNCX)03138
Paw Creek Terminal
cklenburg County
>r to expiration of the current
:e.
belcaw.
Sincerely,
41
Charles R Weaver, Jr.
DES Unit
cc: Gentral Files
ill 5 File
1617 Mail Service Center, Raleigh, North Carolina 27699-1 17 919 7 -5083 extension 511 (fax) 919-733-0719
VISIT us ONTHE INTERNET @ hftp://h2o.enrstate.ne.us/NPDES e-mail: chadesmeaver ncmali.net

�I Te inal
A414VASltv,1.20.11 ii
rg mil,.,V
original and two copies.
2 is no renewal fe
e.
it
Lt the facility since
or an Authorized
ansultant) prepares
ty delegated to any
ie Code of Federal
nest submit
es ftvjd,7g 100%
tewater cac Olin
�quired with ;our

, \NWNt4 A Miefutel E Easin
'bz� William G. Ross it, Sw:
North Carolina Deparmient of Environment WW Natural Reso
Alan W. Klirnek, P. E Dit
Division ofWaterot
Coleen H. Sullins, Deputy oil
Division of Water Qt
June 3, 2004
Mr. W. D. Scott, §"r-Vice President
Colonial Pipeline C61UP-My
Post Office Box 18 855
Atlanta, Georgia
SUBJECT: NOTICE OF DEFICUENCY
Compliance Evaluation Inspection
Colonial Pipeline Company
Charlotte Delivery Facility
NPDES Permit No. NCO031038
Mecklenburg County, N.C.
Dear Mr. Scott:
On May 24, 2004, Ms. Crystal Taylor of the Mecklenburg County Water Quality Program
hesitate to call Mr. Richard Bridgeman or me at this Office.
Sincerely,
14� i
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
Enclosure
cc: Rusty Rozzelle, MCWQP
DRG/cat
File: WQ 0031038.504
,one
No hCarolina
4&raffy Division of Waw Quality, Momm"He ReVowd Office, 919 North Main Strve� Moormville NC 28115 [phone] Custewer So
I-M423.6

United States Environtnental Protection Agency, Wa
ICES Compliance ce Inspection Report
North Carolina Department of Environment and Ni
Division of Water Quality, Mooresville Regi
F
,non, DC 20460 Form Approved
OMB No. 2040-0003
1 Resources A*"WA Approval Expires
Office NCD 7i31/85
Transaction Code NPDES Permit No. Y /DAY Inspection' Type Inspector Facility Type
N 5 NC O031038 04/05/24 C
C 2
Remarks:
Inspector: Mecklenburg County Water all Program
Inspection Work mays Facility Self -Monitoring Evaluation Rating BI QA
....Reserved..... ..
0.6 3 N N
..i8 ,•4d 4Y�", `la`,"... ... F,`x,C k, 1 4"''y
'k;\?'r "tsF•bl`�.�;rF,: 4vr*,`;Y;iA ,: ,44MY A4e,�FFMiv ,F th # US icy 'F,§ s' ^:
,ttS
Entry Tune:
Pernnt Effective late:
Name and Location of Facility Inspected 2.05 pin
September 1, 2001
Colonial Pipeline Company Exit Time.
Charlotte Delivery Facility c3 Put
Permit Expiration late.
724 Ike tend Circle late.
June e 30, 2005
Mecklenburg County, North Carolina May 24, 2004
Na e(s) of tan -Site Representatives Title(s) -Phone No(s):
Mr. John Culbreath / Envirownental Technician / Phone: [phone]
Mr. Jeff Titus / District Environmental Project Manager 1 Phone:- 704-399-8266
Dame and Address of Responsible Official: Title: Senior Vice -President
Mr. W.D. Scott
Colonial Pipeline Company Phone No.
Contacted?
P.C. Box. 18855 (40) 261-1470
No
Atlanta, Georgia 30326
is 9 `hp @ �4�p"
ny a ,3 s y
YS Nvi"-.ern .F°i .a�'i*
. . r..i dvwary r,.rrc1
( Permit Flow Measurement Operations & Maintenance
j
ED Sewer Overflow
Records/Reports Z Self -Monitoring Program Sludge Handling/Disposal
(l Pollution Preventic
Facility Site Review El Compliance Schedules Pretreatment Program
El Multimedia
Effluent/Receivisig, Waters Z Laboratory, [� Stormwater
Other.
tor(s):
!et(s) for Summary
Date:
May 25, 2004
Date:
3 (Revised 3-85) Previous Editions are Obsolete , -

PEl
t
con.
tiort report i ed n 19, 2003.
4IT
ar
MAW
ty 29 2003..A Compliance Evaluation
t t t • � t• t
t •t t r � t 11
r
were noted, except as follows.
DMR for 5/2003 did not include the test result for the Acute Toxicity
Ducted on / 0/2003.
ITE REVIEW:
,tendon pond discharges through Out001. Stormwater from the manifoli
r
t t � " t . t •" t t" t

F
LABORATORY:
Chernical analysis ofeffluent samples is performed by Prism Laboratories, Inc. (N.C.
Certification # 402). effluent toxicity analysis is conducted by L'I T En ' on tal, Inc, (N.C.
Certification # 022). Prism Laboratories and ETT Environmental were not evaluated under this
inspection.
EFFLUENT/RECEIVING S.
The effluent water was clear at the time ofthe inspection. No petroleum sheens or odors
were noted. The facility discharges to an unnamed tributary to Gum Branch, which is a Class
WS-IV water in the Catawba River Basin.
SELF -MONITORING PROGRAM. -
Discharge Monitoring Reports (I were reviewed for the period. April 2003 through
March 2004. The reports indicate that the facility was in compliance with perinit effluent limits
during this period, except as follows:
IONS & MAINTENANCE:
e facility and site appeared ell operated and maintained. The facility and outfall are
,pected daily by facility to ensure proper operation and safety.
charge valves from the secondary above ground storage tank containments remain
in the closed position until an inspection is performed by facility personnel.

r L4-)-
F,O� \NA Michael Govenw
William G. Ross Jr, Swetuy
North Carolina Deparorwa of Environment and Natural Resources
7
Alan W. Klin**. P. E. Director
Division of Water Quality
Coleen ff. Sullins, Deputy Direcw
Division of Water Quality
June 2, 2004
Mr. W.D. Scott, Senior Vice President
Colonial Pipeline Company
'Post Office Box 18855
Atlanta, GA 30326
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline Company
Charlotte Delivery Facility
NPDES Permit No. NCG510207
Mecklenburg County, N.C.
Dear Mr. Scott:
Th� enclosed report &uld be self-explanatory.
If you have any questions concerning this report or any other matters, please do not
hesitate to call Mr. Richard Bridgeman or me at tWs Office.,
Sincerely,
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
Enclosure
cc: Rusty Rozzelle, MCWQP
DRG/cat
WQ File 510207�504
IYV7h2tMr,a(lyDivmonofWatw9w,hty, MoorosvilleltegjonalOffice� 919 North Mon Street� MwresvilleNC29115 [phone] customor

United Statai
.'North Car4
IVIA VA YY "L6 l �"L ttRli Olt, 1Y V4
Transaction Code NPDES Permit No. MO/DAY
N 5 NCGO0510207 04/05/24
Remark,,
Inspector: Mecklerrur Coup
Inspection' Work Days Facility Self -Monitoring Evaluation Ratu
0.5
tion of Facility Inspected:
Company
ry Facility
;ircle
uty, North Carolina
gton , DC 20460
Form Approved
OMB No: 2040-0003
A*IA'r
ural Resources Approval Expires
NCdE R
aalOffice
7/31185
System Colon
Inspection Type
Inspector Facility Type
C
C 2
later uali Pros
BI QA
....Reserved ..........:..
NN
Entry Time:
Permit Effective Date:%
2:05 pin
October 1, 2001
Exit Time:
3:43 pra
Permit Expiration (late:
Date.
September 30, 2006
May 2, 2004
Jeff Titus 1 District Environmental Project Manager / Phone: [phone]
Nance and Address of Responsible Official: Title: Senior Vice -President
Mr. W.D. Scott
Colonial Pipeline Company Phone No, Contacted?
P.O. Box 18855 404-261-1470 No
Atlanta,, Georgia 30326
g q,,7 .. �
LK Pemit
[ Flow Measurement
L!J Operations & Maintenance
[ ] Sewer Overflow
i Records/Reports
ietf-Monitoring Program ;
0 Sludge Handling/Disposal
[ Pollution' Prevention
Facility Site Review
Q Compliance Schedules
❑ Pretreatment Program
Multimedia
Effluent/Receiving Waters
® Laboratory
El Stormwater
tither:
An areas are rated sausiactory untess oche se mmcatea. bee Attacneu Nneet(s) for Nummary
Signature(s) of Inspector(s): Agency/Office/Telephone: Hate:
Crystal Taylor CWQPI(704) 336-5500 May 25, 2004
Signature of Reviewer; Agency/Office Date:
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

GENERAL:
e facility last inspected on May 29, 2003 by Nis. Crystal 'Taylor of the Mecklenburg
County Water Quality Pro ( C QP). A Compliance evaluation Inspection (CEI) Report
was issued on June 19, 2003.
Ply
The current permit became effective on October 1, 2001 and expires on September 30,
2006. The permit authorizes the discharge of treated groundwater to an unnamed tributary of
Gum Branch, a class WS-IV water in the Catawba River Basin.
The portion of the facility associated with the NPDES treatment works consists of five
five groundwater recovery wells, an oil/water separator, equalization tank, low profile tray -type
stripper,air iron filtration unit, holding tank, particulate filter, and two 1,800 pound granular
activated carbon vessels connected in series.
The current permit properly describes the facility d appears adequate for the waste
stream being treated.
RECORDS/REPORTS:
The is not required to complete and submit Discharge Monitoring Reports
(D ), however, the permit o require the facility to maintain on -site records of all " ge
monitoringdata. The on -site monitoring data was reviewed for the period June 2003 through
March h 2004. The records were clear, organized, and well maintained; no discrepancies were
noted..
FACIELITY
e facility discharges to an unnamed tributary to Gum. Branch, which then discharges to
the on -site retention pond. The retentionpond discharges to an unnamed tributary to Gum
Branch, d Class WS-IV water in the Catawba River Basin. The effluent of the retention pond is
monitored under the NPDESPermit NCO031038.
All of the major components of the facility in service and appeared o be operating
properly at the time of the inspection.
O S T
Flow is measured on the effluent line using line totalizing flow meter capable of
producing instantaneoustotal flow measurements. This is an acceptable instantaneous method
for NPDES reporting.
Discharges from the groundwater remediation system are intermittent.

Q TORY:
e effluent was not c
odors were noted in the recei
r-tvtctc dim,
apses is prriummu py rnsm iauorwones, inc. �iNt— iaoordEory
►oratories was not evaluated during this inspection.
scharging at the time of the inspection. No petroleum sheens or
ing stream. No visual impacts were noted in the receiving stre
was reviewed for the period June 2003 through `March 2004. The
meters during this period.
ATIONS & MAINTENANCE:
routine preventative maintenance on all components of the groundwater treatment system

ATTORNEYS AT LAW
on 2020 Charlotte Plaza • 201 South College Street
Charlotte-, North Carolina 28244-2020
ns
704.344� 1117
Telephone.
Facsimile. 704.344.1483
Dn, PLLC Richard C. Gaskins, Jr.
Email: rgaskins(&,hgfmlaw.com
March 22, 2004
Mr. D. Rex Gleason
Water Quality Regional Supervisor
M UP
Division of Water Quality
North Carolina Department of Environment
and Natural Resources
Mooresville Regional Office
919 North Main Street
Mooresville, North Carolina 28115
Re: Colonial Pipeline - Charlotte Delivery Facility
APDES Permit No. NCO031038
NO V-2004-L V-0005
Mecklenburg County
Dear Rex:
•

Hamilton Gaskins Fay & Moon,1PLLC
Mr. D. Rex Gleason
March 22, 2004
Page
w
e •
,ration pond. Because of the quick
1114 X4 V V40 WR "AJ
VW11buValli JdlllplQ, n i✓Vit:4Q111GLd.' j yv uiYji Vi vvii4v nQ. FJuuzV v,4uvaa tau
limits.
ti •
;e from the CITGO facility.
gathered additional data pursuant to an approved sampling and analysis plan. The additional
sampling demonstrates that there is no significant difference between the runoff from any of the
diked areas at Colonial's facility.
Discussion
The NOV will create problems for Colonial because it is a non -appealable decision that
will be used by others as evidence that Colonial has violated the law. A company's record of
compliance is significant when government agencies are making decisions about allowing new
projects, issuing permits, or assessing penalties. Furthermore, it is our understanding that there is
the potential that DENIM will issue a_penalty based upon this NOV. The NOV issued. against
Colonial should be rescinded'and no penalty should be issued because it is well established under

Hamilton Gaskins Fay & Moon, PLLC
Mr. D. Rex Gleason
March 22, 2004
Page 3
caused by a third party.
p or control of a reg
%1W UV 11"i
mitee should not be cited for a violation
�t ifa dischargefrom another./acility
(onial's perndt.
� ­1_ - A - - 0 - - A,'% T T 0 ty
N.C. Gen. Star. § 143-
;e, pumping, pouring, emptying,
Ite
n to flow through a facility is not a
[aw. Colonial did not cause an increase
t would have resulted in a violation of the
)rtable quantity of either oil or benzene
Mater Act and North Carolina law do not
.e exceedance caused by CITGO's release.
on of either federal or State law, DENR issued a Notice of
GO's release. In essence, DENR is saying that thelaw and the
authority to require Colonial to cleanup effluent from a third party, the NPDES permit is
unenforceable to the extent that DE NR contends that the permit requires Colonial to cleanup the
CITGO discharge so that it complied with the effluent limitations contained in the permit. Thus,
it cannot be a violation of the permit to have an exceedance caused solely by the acts of a third
party.
The Third Party Defense is built into the Clean Water Act and North Carolina law
Just in case there is any question about liability for third -party releases, the Clean Water
Act and North Carolina law also contain an explicit third -party defense to liability. The Clean
Water Act provides that "notwithstanding any other provision of law" an owner or operator of a
facility is not liable "where such discharge was caused solely by (A) an act of God, (B) an act of
war, (C) negligence on the part of the United States Government, or (D) an act or omission of

Hamilton Gaskins Fay & Moon, IP LC
r. D. Rex Gleason
March 22, 2004
Page
The CITGO release was are upset condi
Emission was or was not negligent,; or an
1321(f), (g). North Carolina law contains a
-215.3(b)(2)(d) of the North Carolina
wful if the discharge was caused solely by
i act or omission was or was not negligent."
r
rates that the permit is not intenneet to
p rsons fr to liability f r actions talon
•
of the NOV was clone at the explicit direction ofMCDEP personnel.
It is against public policy to issue the NOV to Colonialfor a'release by a third party.
The State has an interest in encouraging companies to act in an environmentally
responsible manner, This is the point of most environmental laws. It would create a disincentive
for companies to cooperate with other facilities and regulators if DENR penalized a company for
a release from a third party. Colonial was not required to tape a sample on April 23, but it
assisted with the cleanup, and took a sample of the impacted tributary to assist MCDEP's
investigation. From an environmental perspective, it is not beneficial to create an incentive for
Colonial to route the effluent from ether facilities around the Colonial retention pond or to create
an incentive for Colonial to fail to sample the effluent from the retention pond when there is a
suspected release from another facility. However, unless the proposed NOV is rescinded,
Colonial would have been better off if it had routed C1TGO's effluent around the retention pond

Hamilton Gaskins Fay & Moon, PLLC
\4r, D. Rex Gleason
eh 22, 2004
Page
In essence, Colonial is being penalized for.
ENR should use its discretion to refrain
that receives discharges from ether petroleum facilities.
VV r' ly y urs
Richard C. t Uains, Jr
RCG/dsw
cc: DENR Point Source Compliance 1 Enforcement Unit

March 29 2004
MEMORANDUM
TO Dave Goodrich
NPDES Unit
FROM. D. Rex Gleason
PREPARED BY: Richard Bride n
SUBJECT: Colonial Pipeline — Charlotte Delivery Facility
DES Permit No. NCO03 03
Mecklenburg County, NC
Attached please find a request from the attorneys for Colonial Pip
Notice of Violation (NC V-2 -L -0005) issued on January 8, 2004. T
to a Benzene limit violation occurring during April 2003.
e Notice was issued in response
As you will note in the letter from Mr. Gash , of Hamilton Gaskins Fay & Moon, it is the
ciity also has a permitted discharge (NPDES
ty discharges is l of 3 UT's to Gum Branch
off' from the CITGQ facility ultimately enter Colonial's retention pond.
out Alan Ill° ek;(signed by Dave Goodrich) dated September 23, 2002.
to rescind the Notice unless it is likely that the Division will modify the designated effluent sampling
location.
Gaskins will be notified of our intention with respect to the Notice, and of our
correspondence to you. Please contact us with any questionsor comments.
Attachment

milton 2020 Charlotte Plaza - 201 Soui
Charlotte, North Carol
skins Telephor
v
& Facsimil
March 22, 2004
Mr. D. Rex Gleason
Water Quality Regional Supervisor
Division of Water Quality
North Carolina Department of Environment
and Natural Resources
Mooresville Regional Office
919 North Main Street
Mooresville, North Carolina 28115
Re: Colonial Pipeline - Charlotte Delivery Facility
NPDES Permit No. NCO031038
NOV-2004-LV-0005
Mecklenburg County
Dear Rex:
In January, Colonial Pipeline Company ("Colonial") recei,
MAR
ORNEYS AT LAW
College Street
m 2S244-2020
;r,
also renews its request to be allowed to sample a location that is representative of Colonial's --------
opera lonsra �er ocatron tat receives disi!I3iIIIIIf,::, front other petroleum facilities.
Facts
On April 21, 2003, Colonial personnel discovered what appeared to be a release of a
petroleum product flowing onto the Colonial property from the CITGO facility through a small
tributary that flows into Colonial's stormwater retention pond. Subsequent investigation
suggested that an oil/water separator tank on CITGO's property had overflowed into the
tributary. The appropriate governmental authorities and CITGO were immediately notified of
the release. Colonial and CITGO mobilized their response teams and absorbent material was

Hamilton'Gas kins Fay & Moon, PLLC
Mir. D. Rex Gleason
March 22, 2004
Page 2
deployed to prevent free product from reaching the rel
response, the impact of the release was minimal.
Although the response by Colonial and CITGC
from reaching the retention pond, odors were detected
April 22, 2003. Although not required, Mecklenburg
Protection ("MCDEP") requested that Colonial collect
at a location near the CITGO property line that -Was ur
contamination on the Colonial property. An analysis (
elevated levels of BTEX, MTBE and naphthalene at b,
constituents except benzene -were below the effluent sl
the retention pond outfall. The level of benzene at the
slightly in excess of the permit limit of 1.19 ug/I. Thc
ME=
W.,
Colonial's request to be allowed to sample representative outfalls from Colonial's facility at that
time because DENR contended that there was insufficient data. Since that time, Colonial has
gathered additional data pursuant to an approved sampling and analysis plan. The additional
sampling demonstrates that there is no significant difference between the runoff from any of the
diked areas at Colonial's facility.
Discussion
The NOV will create problems for Colonial because it is a non -appealable decision that
will be used by others as evidence that Colonial has violated the law. A company's record of
compliance is significant when government agencies are making decisions about allowing new
projects, issuing permits, or assessing penalties. Furthermore, it is our understanding that there is
the potential that DE NR will issue a penalty based upon this NOV. The NOV issued 'ac-,ainst
Colonial should be rescinded and no penalty should be issued because it is well established under

a ilton`Gask ns Fay a& Moon, PLL
Mr. D. Rex Gleason
March 22 2004
Page 3
North Carolina law and the NPDES program that a permitee should not be cited for a violation
caused ba third party.
It is not a violation of Colonial's NPDES'perm t if a dischar:; e f -om another facility
causes an exceedance of an effluent limit in Colonial's permit.
Nothing in the Clean Water Act or North Carolina law allows DENR to require Colonial
to treat, cleanup, or otherwise be responsible for discharges caused by third,pgdes, In general,
the +Clean Water Act, and related North Carolina law impose liability on the person or persons
who had ownership or control of a regulated substance immediately prior` to its release into the
environment. The Clean Water Act and North Carolina law make it illegal to discharge a
pollutant without a permit. See 42 U.S.C. §§ 1311 and 1342. Under the Clean Water Act., a
"discharge" is defined as "the addition of a pollutant" to a waterbody. See 42 U.S.C.
13 2(12). Forth Carolina law requires permits for activities that ``increase the quantity of
waste discharge through any outlet .. to any extent which would result in any violation of the
effluent standards or limitations established for any point source .. ° " N.C. Gen. Stat. § 143-
215.1(4). A "discharge" is defined as "emission spillage, leakage, pumping, pouring, emptying
,
or d ping of oil or other hazardous substances into waters of the State...." Id. § 143-
215.77(4) Moreover, "discharge" does not include a release of less than reportable quantity of
oil or a hazardous substance. Id.
Merely allowing contaminated water in a stream to flow through a;facility is not a
"discharge of a pollutant" and is not a violation of the law. Colonial did not cause an increase
the quantity of benzene in the tributary to an extent that would have resulted in a'violation of the
during the relevant time period. Therefore, the Clean Water Act and North Carolina law do not
authorize any action to be taken against Colonial for the exceedance caused. by CITGO's release.
Although not a violation of either federal or State law, DENR issued a ;Notice o
Violation to Colonial for CITGO's release. In essence, DENR is saying that the law and the
DES permit required Colonial to cleanup CITGO's release. Because DENR lacks statutory
authority to require Colonial to cleanup effluent from a: third party, the NPDES permit is
enforceable to the extent that DENR contends that the permit requires Colonial to cleanup the
CITGO discharge so that it complied with the effluent limitations contained in the permit. Thus,
it cannot be a violation of the pen -nit to have an exceedance caused solely by the acts of a third
party.
The Third Party ,Defense is built into the Clean Water Act and North Carolina lawn
Just in case there is any question about liability forthird-party releases, the Clean Water
Act and North Carolina law also contain an explicitthird-party defense to liability. The Clean
Water Act provides that "notwithstanding any other provision of law" an owner or operator of a
facility is not liable "where such discharge was caused solely by (A) an act: of God, (B) an act of
war, (C) negligence on the part of the United States Government, or (D) an act or omission o

* Hamilton +Gaslans Fay & Moon, PLLC
D. Rex Gleason
March 22, 2004
Page 4
other party without regard to whether such act or emission was or was not negligent, or any
combination of the foregoing clauses." 42 U.S.C. §§ 1321(f), (g). North Carolina law contains a
similar third -party defense. Specifically, section 143-21'5.83(b)(2)(d) of the North Carolina
General Statutes provides that a discharge is not unlawful if the discharge was caused solely by
44an act or omission of a third party, whether any such act or omission was or was not negligent."
Yhe CITGO release was an upset condition under the terms co, f Colonial's NPDESpermit
The concept of a third-partydefense is built into every NPDES permit through the
—standard upset condition provision. Colonial's NPDES permit, like every father NPDES permit,
contains a provision that creates a defense for upset conditions. Section 15..5 of the NPDES '
permit defines an "upset" as "an exceptional incident in which there is unintentional and

Hamilton Gaskns Fay & Moon, PLLC
Mr. D. Rex Gleason
March 22 2004
Page
d ignored MCDEP's request to conduct sampling
acting in an environmentally responsible manner. I
from issuing a Notice of Violation in this situation.
Conclusion
Colonial respectfully requests that the Notic
.and that the record reflect that the exceedance was
third party. To avoid a similar problem in the futur
In essence, Colonial is being penalized: for
)ENR should use its discretion to refrain
owed to sample a location that is representative of Colonial's operations rather than a location
that receives discharges from other petroleum facilities.
ZVer ly y�
Ricdard C. Gaskins, Jr.
RCG1ds
c: DENR Point Source Compliance / Enforcement Unit

)e2of
onial Pipeline
y 27,2003
needed. If you have any questions 1 can be reached at 74-399-5259.
Sincerely,
Jahn W. C;ulbreath
Sr. Environmental Technician
Enclosures
Cc Rex Gleason- NCDENR Mooresville'
Crystal Taylor- MCDEP
Colonial Pipeline Company

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C)A �pq
Michael E. Eas
William G, Ross
> North Carolina Department of Environment and Natu
Alan W. Klimek,
Division of
May 27, 2003
CM # 70012510 0004 8286 9021
rCERT EU L
SET CE QtESTE
John Culbreath, Terminal Manager
Colonial Pipeline Company
7524 Kentstead Circle,
Charlotte, NC 2813
SUBJECT: NOTICE OF VIOLATIO
G.S. 143-215.7 _ (ail iPollution and Hazardous
Substances Control Act of 1978
Discharge of Oil
Colonial Pipeline Company
7524 Kenstead Circle, Charlotte
Mecklenburg County, N.C.
Dear Mr. Culbreath:
Chapter 143, Article 21 of the North Carolina general Statutes (g.S.) authorizes and
directs the Environmental management Commission of this Department to protect and preserve
li w
April
Live working agreement b
3 a result of this investigat
following condition was found on the property in violation of C.S. 14-215.83(a):
discharge of #2 Fuel oil to the ground at 7524 Kenstead Circle.
To comply with state law, it will be necessary to immediately discontinue all illegal
discharge activity, to collect, remove and properly dispose of the discharge, and to restore all
affected areas as nearly as may be to the conditions existing prior to the discharge. It is
recommended that you implement corrective actions to eliminate the potential for recurrent illegal
discharges.
NCDENz;
Mooresville Regional Office, 919 North Main Street, Mooresville, NC 2811
PHONE [phone] Customer Service
EFL [phone] 1 800 623-7748

Jahn Culbreath
Colonial Pipeline Company
Page Two
May 27, 2003
Be advised that, pursuant to G.S. 143-215.88A any person who intentionally or
negligently discharges coil or tither hazardous substances, or knowingly causes or permits the
discharge of oil in violation of G.S. 143-21 .83( ), or who fails to report a discharge as required
by NCGS 143-215.85,or who fails to comply with the clean up requirements of G.S. 1 -
15.4(a) shall incur, in addition to any other penalty provided by law, a penalty in an amount
not to exceed five thousand dollars ($5,00 .00) for each such violation. Penalties of not more
than twenty-five thousand doll ($25,000.00), or twenty-five thousand dollars 25, 00.00) per
day ;ifthe violation is of a continuing nature, may also be assessed for any damage to the surface
waters of the State that may result from the unpermitted discharge. You will be advised of any
enforcement recommendation concerning this matter.
It is requested that you respond, in writing, to this Notice, indicating the measures taken
to collect and remove the discharge, to prevent future discharges, and to restore all affected areas.
The response should also indicate the disposal location for any removed discharge material and
y removed contaminated soils or waters. Please address your response to me by no later than
June 1, 2003. Also, please send a! copy of this response to Mr. Rusty Rozzelle of M+CWQP` at
700 North Tryon. Street, Suite 205, Charlotte, N.C. 28202.
If you have any questions concerning this matter, please do not hesitate to contact
Richard Bridgeman or me at 7€14/663-169 .
Sincerely,
D. Ilex Gleason, P.E.
Water Quality Regional Supervisor
cc: Rusty Rozzeile, MCWQP
IJRG/cat
FILE:' II: ICWQ\NOV\0 00S48a.no-,f

NO: I
SERVICE REQUESTIM
2003-00548
WQC
LIST: Crystal A. Taylor
VEST: Citizen's Request
1111: IC-F(1)-CI
RDER
@ 17:35
REQUESTING PARTY INFO
:T: JOHN CULBREATH
4YMORKPLACE:
S:
;S PHONE NO: [phone] HOME PHONE NO:(
ATION PROMPT:
FACILITY INFO
-------
4y: COLONIAL PIPELINE CO. -PAW CREEK TERMINAL 03102206
Sa 7524 KENSTEAD CR
PAW CREEK NC 28130— -
:T.-
:T.s Dan C. Miller
40: [phone]
- - ACTIVITIES
REQUESTED..:
)reath with Colonial pipeline reported that they had a discharge of approximately #2 Fuel Oil
rAKEN. ...... :
Ouct in the main line wells.
boratory Results (4/22103), Waste Disposal Mainfest (4115/03).
DATE: 05/05/2003
TAKEN BY: Crystal A. Taylor
it
iated soil as possible. They had some,
3o used a vac truck to collect the free I

PAGE NO:
SERVICE REQUESTIWORK ORDER
----- SAMPLES
DISPOSITION, ETC..
NOTIFIED REQ PARTY:
Y
TIME ON SITE:
:00
VERBAL OR WRITTEN:
V
TRAVEL TIME:
1:00
GATE. NOTIFIED:
04115/ 003
ADMIN TIME:
:00
NOTICE OF VIOLATION:
Y
MILEAGE:
0
LEGAL ACTION:
N
SITE VISITS:
0
WELL SAMPLE:
N
RECALL DATE:
/ f
OUTFALL SAMPLE.:
N
STATUS:
OPEN
LAKE/STREAMSAMPLE:
N
DATE CLOSED:
I 1
EMERGENCY RESPONSE:
N
REVIEWED BY: 1 1

tf� MichaelF. ey ov r
� v
William G. Ross Jr., Secretary
? North Carolina Department nt ofEnvironment ancl Natural Resources
Alan W. Klimek,P.'E. Director
Division of Water Quality
Coleco H. SullinsDeputy Director
Division of Water Quality
January 8, 2004
CERTIMD MAIL
RETURN'RECEIPT RE!2UESTED' 7003 22600001 3491 1104
John W. Culbreath
Senior Environmental Technician
Colonial Pipeline Company
7524 Kenstead Circle
P.O. Box. 87
Paw Creek, NC 2130
Subject: Notice of Violation - Effluent Limitations
Colonian Pipeline - Charlotte Delivery Facility
I)ES Permit No NCO31038
NOV-2004-LV-000
Mecklenburg County
Dear Mr. Culbr thw
ter"
Parameter eyorted Value Limit
Benzene 3.1 µg/L 1. 19 gg/L FIN
.,..7 �, .t. ,.+.. a — ux.u.. e✓ —w a.w. cawxd Lxwxx"A uucrauacsaRvax.:
If you have questions concerning this matter, pleasedonot hesitate to contact Mr. Bridgeman or
me at 704/663-1699.
Sincerely,
D. Ilex Gleason, P.E.
Water Quality Regional Supervisor
cc: Paint Source Compliance/Enforcement Unit
RMB
�I
t�ow�ihCarolitta
✓ rt C t ltf Division of Water ity, t4i lle Ftegionai c . 919 North �i le NC 28115 [phone] Customi
1-877-6

POOColonial Pipeline Company
John W Culbreath Office - 704-39"259
Senior Environmental Technician Fax- 704-399-9029
Mid -Atlantic District E-mail - jculbr"@colpipe.com
June 6, 2003
Mr. Rex Gleason
NCDENR
Division of Water Quality
919 North Main Street
P.O. Box l0 9 2003
Mooresville, NC 28115
Re- Notice of Violation /Discharge of it _Y SECTION
Charlotte Delivery Facility /April 15, 2003 WATERWALff
Colonial Pipeline Company
Mecklenburg County
Dear Mr. Gleason:
I received the above referenced Notice of Violation dated May 27, 2003 for the discharge of
#2 fuel oil to the ground. A report detailing the incident was submitted to Andrew Pitner,
NCDENR Mooresville office on Mav 17, 2003. Below is a summary of the measures taken to
of soil, water, and product associated with the release is also ino

ison-NCDENR
003
WTT
.me to 208 gallons.
t to the Haz-Mat Transportat
e that time
service. A new filter vessel and O-ring assembly is on order. Steps are in taken to
require replacement of the 0-ring at each filter change and to conduct more frequent
inspections once the unit is returned to service.
If you have any questions or need any additional information, I can be reached 704-
399-5259 or at the letterhead address.
Sincerely,
4ohn W. C�ul`breath
Senior Environmental Technician
Enclosures
Cc: Rusty Rozzelle— MCWQP
Kim Spears — CPC Operations Manager
Jeff Titus— CPC District Env. Project Manager
com"I'll Pipwine Company

7
June
4r. W.D. Scott, Senior Vice President
"Olonial Pipeline Company
lost Office Box 18855
Wanta, Georgia 30326
SUBJECT: Coml
Colo]
Clwl
NPD',
Mecl
)ear Mr. Scott:
r'l— X If- in 1)AA12 'Xf
Michael 14,"Xasley, Go
William G. Ross, Jr.,Sec
North Carolina Department of Environment and Natural Rew
Alan W. Klimek, P.E., 0
Divisiond Water
,2002
ince Evaluation Inspection
I Pipeline Company
Le Delivery Facility
Permit No, NCO03103 8
iburg County, N.C.
hesitate to call Mr. Richard Bridgeman or me at this Office.
Sincerely,
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
Enclosure
cc: Rusty Rozzell e, MCWQP
CAT
File: WQ 003103&603
Mooresville Regional Offirce, 919 North Main Street, Mooresville, NC 28115
DNE (704) 663w1699 Customer Service
(70,4) 663-604,0 1 800 623-7748

NPIDES Permit No. YR/MO/DAY Inspection
NCO031038 03/05/29 C
Remarks:
Facility Self -Monitoring Evaluation Rating
3
low
)003
,sae Inspector Facility Type
C 2
Pram
QA ......... ..Reserved.. ....
N
Entry Time:
Permit Effective Date:
Name and Location of Facility Inspected: 10:00 am
September 1, 2001
C
Colonial Pipeline Company Exit Time:
Charlotte Delivery Facility 12:00 pro
Perntit Expiration Date:
7524 Kenstead Circle s Date:
June 30, 2005
Mecklenburg County, North Carolina May 2, Z003
Narne(s) of On -Site Representatives Title(s) Phone No(s):
Mr. John Culbreath / Enviromneirtal Technician / Phone: [phone]
Mr. Jeff Titus / District Environmental Project Manager 1 Phone: [phone]
Name and Address of Responsible Official. Title: Senior
S dice-President
-President
=Vice
Mr. W.D. Scott
Colonial Pipeline Company
[(404)
Phone No.
P.O. Box 18855
Contacted?
261-1470ic
) I
Atlanta, Georgia 30326
No
Al
Q
Permit Flow Measurement L9 Operations & Maintenance
Sewer Overflow
Records/Reports Self -Monitoring Program Sludge Handling/Disposal
El Pollution Prevention
Facility Site Review Compliance Schedules ❑ Pretreatment Program
El Multimedia
Effluent/Receiving Waters Labarat2a for water
Other:
Section D: Summar y of Findinis/Cimuneats '
All areas are rated satisfactory unless otherwise
indicated. See Attached Sheet(s) for Summary
Signature(s) of Inspector(s):
Agency/Office/Telephone:
Date:
Crystal Taylor � � JAI—
MCWQP/[phone]
June 12, 2003
Signature of Reviewer:
Agency/Office
Date:
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

ENERAL:
ation Inspection report was issued on Feb.
dIT:
/REPORTS:
January 30,2002. ACompliance
12,2002.
-if ective on September 1, 2001 and expires onJune 30, 2005.
of storm water and treated effluent from the water pollution
a water runoff, surface tank and piping compounds with
routed to a retention pond.
crepancies were noted.
REVIEW:
the retention pond and eventually discharged through Outfall 001 e
The facility discharges to an unnamed tributary to Gum Branch, which is a Class WS-lV
water in the Catawba River Basin.
All of the major components of the facility were in service and appeared to be operating,
properly at the time of the inspection.
FLOW MEASUREMENT:
Flow is estimated by weekly instantaneous flow measurements at the discharge pipe from
the sedimentation basin, in accordance with NPDES permit.

LABORATORY:
Chemical analysis of effluent samples is perfonned by Prism Laboratories, Inc. (N.C.
Certification # 402). Effluent toxicity analysis is conducted by ETT Environmental, Inc. (N.C.
Certification # 022). Prism Laboratories and ETT Envirom-nental were not evaluated under this
inspection.
EFFLUENT/RECEIVING WATERS:
The effluent water was slightly turbid at the time of the inspection due to the recent
rainfall. No petroleum sheens or odors were noted. The discharge did not appear to have a
detrimental impact on the receiving stream. The facility discharges to an unnamed tnbutary to
Gum Branch, which is a Class WS-IV water in the Catawba River Basin.
SELF -MONITORING PROGRAM:
Discharge Monitoring Reports (DMRs) were reviewed for the period October 2001
through March 2003. The reports indicate that the facility was meeting permit effluent limits and
monitoring frequencies during this period. The records were clear, organized, and well
maintained; no discrepancies were noted.
OPERATIONS & MAINTENANCE:
The facility and site appeared well operated and maintained. The facility and outfall, are
visually inspected daily by facility staff to ensure proper operation and safety.
Discharge valves from the secondary above ground storage tank containments remain
locked and in the closed position until an inspection is performed by facility personnel.

VN4A7 r'
F
Michael R Easley, Qovemor
William G. Ross Jr., Secretary
North Carolina {department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality.
June 10, 2002
r. John W. Culbreat�,..
Colonial Pipeline
P.O. Pox 87
Paw Creep, N.C. 2 130
�iN 1 1 2002
Subject. Notice of Deficiency
Acute Toxicity Testing
Colonial Pipeline/Charlotte Facility
NPDES No. NC 03103
Mecklenburg County
Culbreath.
My staff has received and reviewed Colonial Pipeline's 5/1/02 acute effluent toxicity report.
During review of the AT-2 form, it was noted that the test was performed as a pass/fail toxicity
test.
ISENEMMillim
I :t` _ -> �is iilatte , you are encouraged to call me or Lance
Ferrell at 91) 733-13.
Sincerely,
a r /r*
% / a er t
Matt Matthews, Supervisor
Aquatic Toxicology Unit
o , a
c
r. Robert Kelley- TT Environmental, Inc.
Central Files
Customer Service Environmental Sciences Branch 1621 Mail Service Center Raleigh, NO 27699-1621 (91 ) 733-9960
1800 2 -7748

mppppp�
\,N Alrcr�,
Michael I
William G. Ross, Jr, E
C
> Department of Environment and Natural Ri
Gregory J, Thorpe, Ph.D,, Acting
Division of Watt
February 12, 2002
Mr. W. D. Scott, Senior Vice President
Colonial Pipeline Company
Post Office Box 18855
Atlanta, Georgia 30326
SUBJECT: Compliance Evaluation Inspection
Colonial Pipeline Company
Charlotte Delivery Facility
NPDES Permit No. NCO031038
Mecklenburg County, N.C.
Dear Mr. Scott:
On January 30, 2002, Ms. Crystal Taylor of the Mecklenburg County Department of
Env irom-nental Protection conducted an inspection at the subject facility. This inspection was
.. 11 1 l^4 a 1A
of Water Quality. The enclosed report should be self-explanatory.
f you have any questions concerning this report or any other matters, please do not
to call Mr. Richard Bridgeman or me at this Office.
Sincerely,
D. Rex Gleason, P. E.
Water Quality Regional Supervisor
,usty Rozzelle, MCDEP
0031038.202
Division of Water Quality 919 North Main Street Mooresville, NC 28115 Phone [phone]
Fax [phone]

fzT(r$r1W.W FROM
N 5 NC0031038 02/01/30 C C 2
Remarks:
lnspector: Mecklenb2M Copt .y Environmental Protection
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 QA
..........Reserved............
0.6 3 N N
Section 11: Facility Data
Entry Time:
Permit Effective Date:
Name and Location of Facility Inspected: 9:35 am
September 1, 2001
Colonial Pipeline Company Exit Time:
Charlotte Delivery Facility 11:30 am
Permit Expiration Date:
7524 Ike teal Circle Date:
June 30,2005
Mecklenburg County, North Carolina January 30, 2002
Name(s) of On -Site Representatives --Title(s)----Pbone No(s):
Mr. John Culbreath / Enviromnental Technician / Phone: [phone]
Mr. Jeff Titus / District Environmental Project Manager / Phone: [phone]
Name and Address of Responsible Official: Title: Senior Vice -President
Mr. W.D. Scott
Colonial Pipeline Company Phone No.
Contacted?
P.O. Box 18855 [phone]
NO
Atlanta, Georgia 30326
Section Q
Areas Evaluated During Insnection
Permit Flow Measurement Z Operations& Maintenance
sewer overflow
Records/Reports Self -Monitoring Program Sludge Handling/Disposal
El Pollution Prevention
Facility Site Review Compliance Schedules Pretreatment Program
El Multimedia
Effluent/Receiving Waters Laboratory Stormwater
El Other:
Section D.- Summary of Findings/Comments
All areas are rated satisfactory unless otherwise indicated. See Attached Sheet(s) for Summary
Signature(s) of Inspector(s): Agency/Office/Telephone:
Date:
Crystal Taylor MCDEP/[phone]
February 4, 2002
Signature of Reviewer: Agency/Office
Date:
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

PPPPPP"
GENERAL:
The facility was last inspected by 1v CDE
Inspection report was issued. on July 18, 211.
PERMIT:
V
i June 2, 2001. A Compliance Evaluation
low is estimated by weekly instantaneous flow measurements at the discharge pipe from
ne tation basin, in accordance with NPDES permit modification letter dated December

LABORATORY:
r- •
u!a !
Discharge M{
through September
d monitoring f egt
I One (
maxit
was n
(CEI)
loci
untai were not evwuaEea unuer tuts
tot appear to have a detrimental impact on the receiving stream
M.
eu well operated and maintained. The facility and outfall are
ity staff to ensure proper operation and safety.
ie secondary above ground storage tank containments remain
until an inspection is performed by facility personnel.