NC0021962_Regional Office Historical File Pre 2018 (2)

PAT MCCRQRY
�.Goveinor
DONALD R. VAN DER VAART
.w
Water Resources S. JAY ZIMMERMAN
ENWRONMENIAL OUALIrr
June 24, 2016
E ,w.
�W
Scott Eaton
CITGO Petroleum Corporation
3877 Flowers Rd
Atlanta, GA 3036
Subject: NPDES Electronic Reporting Requirements
Charlotte Terminal
NPDES Permit Number: NCO021962
Dear NPDES Permittee:
The U.S. Environmental Protection Agency (EPA) recently published the National Pollutant Discharge
Elimination System (NPDES) Electronic Reporting Rule. The rule requires NPDES regulated facilities to
report information electronically, instead of filing written paper reports. The rule does not change what
information is required from facilities. it only changes the method by which information is provided (i,e.,
electronic rather than paper -based):
EPA is phasing in the requirements of the rule over a 5-year period. The two phases of the rule, and their
key milestones, are:
• Phase 1—Starting on December 21, 2016, regulated entities that are required to submit Discharge
Monitoring Reports (DMRs) will begin submitting these reports electronically. If you are currently
reporting your DMR data electronically using eDMR, then you simply need to continue reporting
in the same way as you are now. The key change is that, starting on December 21, 2016,
electronic reporting of DMRs will be required, instead of voluntary,
• Phase 2 —Starting on December 21, 2020, regulated entities that are required to submit certain
other NPDES reports will begirt submitting these reports electronically, Reports covered in the
second phase include Notices of Intent to discharge in compliance with an NPDES general permit,
Sewer Overflow/'Bypass Event Reports, and a number of other NPDES program reports.
Incorporating Electron e Reporting Requirements into NPDES permits
The NPDES Electronic Reporting Rule requires authorized NPDES programs to incorporate electronic
reporting requirements into NPDES permits beginning December 21, 2015. Under the new rule, the
electronic reporting process supersedes the paper reporting process, According to our files, your NPDES
permit became effective after November 2013, and should contain the requirement to electronically
report your Discharge Monitoring Reports using NC DWR's eDMR system,
In addition to requiring permittees to report information electronically, the rule also requires permittees
to identify the initial recipient for the NPDES electronic reporting data [see 40 CFR 122.41(l)( )], initiol
State of North Carolina ( Environmental Quality I Water Resources
1617 Mail Seraiee Center 1 Raleigh, North Carolina 27699-1617
919 807 6300

recipient of electronic NPDES information from WDES-regulatedfacilities (initial recipient) means the
entity (EPA or the state authorized by EPA to implement the NPDES program) that is the designated entity
for receiving electronic NPDES Data [see 40 CFR 127,2(b)]. Permittees are required to electronically
submit the required NPDES information to the appropriate initial recipient, as determined by EPA. By July
18, 2016, EPA must identify and publish on its web site and in the Federal Register a listing of initial
recipients by state and by NPDES data group. Once available, you can use EPA's web site to find out or
determine the initial recipient of your electronic submission.
NC DR has submitted a request to EPA to be the initial recipient for the following NPDES data groups:
1. Discharge Monitoring Reports;
2. General Permit Reports [Notices of Intent to discharge (NOls); Notices of Termination (NOTs)];
3. Pretreatment Program Reports; and
4. Sewer Overflow/Bypass Event Reports
EPA's web site will also link to the appropriate electronic reporting tool for each type of electronic
submission for each state. Instructions on how to access and use the appropriate electronic reporting
tool will be available as well.
For more information on EPA's NPDES Electronic Reporting Rule, visit
electronic-[tp2qtgjA. For more information on electronic reporting to NC DWR, visit
or contact Vanessa
Manuel at 919-807-6392 or via email at Vanessa.Mgpu! ncdenr:gov.
Sincerely,
Je&e,tj 0. POJAr�
for S. Jay Zimmerman, P.G.
Cc: NPDES File
Central Files

Pat Mc
Govemd
Xwl
e
NCDENR
North Carolina Department of Environment and Natural Resources
Donald van der Vaatt
sreta
September 2, 2018
�ies Utke
Petroleum Corporation
Tice Sox 58
°ee, NC 2818 ;
SUBJECT: Compliance Evaluation inspection
CITG? Petroleum/Charlotte Terminal
NPD S Permit NCO0219 2
Mecklenburg County, N
Ir. Utke:
at wes.bell ncdenr. ov and illiam.ansen mecklenbur coon `n. ov.
Sincerely;
r d
Pw.,'
Michael L. Parlor, Regional Supervisor
Mooresville Regional Office
Waiter Quality Regional; Operations Section
Division of Water Resources, DENR
Enclosure:
Inspection Report
MSC 161 — Central files basement
Rusty: Rozzelle, MCWQP
Wt
Mooresville Regional Office
Location: 610 East Center Ave., Suite 311 Mooresviil , NC 26115
Phone: [phone] t Fax: [phone] Customer 6erviow 1.877- 23-6743
Internet: http:11portaLnc6enr,argtweb1wq
An Equal Opportunity l Aftlrrnative Action Employer — 5U°Io RKyd dllUWk Post Consumer paper

United States Environmental Protection Agency Form Approved,
EPA Washington, D.C. 20460 OMS No, 2040-0057
Water Compliance Inspection Report Approval expires 8-31-96
Section A: National Data System Coding (i.e., PCS)
Transaction Code NPDES yr/mo/day Inspection Type Inspector Fee Type
2 U 3 NCO021962 111 121 15/07/29 117 18 LI—JI 19 � 20LJ
211 11 1 1 1 1 1 1 111
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 OA
67 1.0 7014 1 71 IN 1 72 1 N 731 1 174751 111 1 1_1180
Section B. Facility Data
Name and Location of Facility Inspected (For Industrial Users discharging to POTVV, also include Entry Time/Date Permit Effective Date
POTVV name and NPDES permit Number) 10:OOAM 15107/29 11/01/01
Charlotte Terminal
7600 Mount Holly Rd Exit Time/Date Permit Expiration Date
Charlotte NO 28214 11:30AM 15107/29 15/06/30
Name(s) of Onsite Representative(s)fTitles(s)/Phone and Fax Number(s) Other Facility Data
11f
Robert Edward Durham/ORC1704-392-32361
Name, Address of Responsible Officialf'ritle/Phone and Fax Number
Contacted
Jim Utke,PO Box 58 Paw Creek NO 28130/Terminal Manager/704-392-3236/ No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit Flow Measurement Operations & maintenance RecordS/RepOrts
Self -Monitoring Program Facility Site Review EffluentlReceiving Waters Laboratory
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) Agency/Office/Phone and Fax Numbers Date
Water Quality Program Meckenburg County MRO WQI/704-336-54491
Signature of Management 0 A,Raviewer Agency/OfficatPhone, and Fax Numbers Date
Wes Bell MRO W(X/7(9-663-1699 Ext. 2 I
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete.
Page#

yr/mo/day Inspection Type 1
11 121 15/07,29 _.. 117 18
Page# 2

Permit: NC0021962 Owner - Facility, Charlotte Terminal
inspection pate. 07/29/2015 inspection Type: Compliance Evaluation
Permit Yes No NA NE
(if the present permit expires in 6 months or less). Has the permittee submitted a new N El 013
application?
Is the facility as described in the permit? so 110
# Are there any special conditions for the permit? El 0 ME]
Is access to the plant site restricted to the general public? In n 00
Is the inspector granted access to all areas for inspection? so 1:1 11
Comment: The Division received the Oermit renewal agglication on 12116/14, The reissued pqrmLt,,
became effective on 2/1L 2QI§.
The properly is fenced and gated.
The previous inspection was conducted on 8/30/11 by MgWQP.
Record Kee in )Los, No NA_N_E
Are records kept and maintained as required by the permit? 0 C1 0 13
Is all required information readily available, complete and current? 0 El 11 1:1
Are all records maintained for 3 years (tab, reg. required 5 years)? 11 0 oil
Are analytical results consistent with data reported on DMRs? M 0 0 C1
Is the chain -of -custody complete? M 0 0 El
Dates, times and location of sampling M
Name of individual performing the sampling
Results of analysis and calibration
Dates of analysis
Name of person performing analyses
Transported CM
Are DMRs complete: do they include all permit parameters? Is 0011
Has the facility submitted its annual compliance report to users and DWQ? 0 0 M 0
(If the facility is = or > 5 MGD permitted flow) Do they operate 2417 with a certified operator 11 El In 0
on each shift?
Is the CRC visitation log available and current? M 0 0 11
Is the `ORC Certified at grade equal to or higher than the facility classification? M 0 0 El
Is the backup operator certified at one grade less or greater than the facility classification? 0 0 El 0
Is a copy of the current NPDES permit available on site? 11 0 11 0
Facility has copy of previous years Annual Report on file for review? 11 0 M 13
Comrnent: Discha[ge Monitoring Re ores (DMRs) were reviewed for the eLod Mgy 2g14 through Mgy,
2015. No limit violations were reported. All QMRs were found to be full y ggrnRlute during the
review proce§s.
Page# 3

permit- NCO021962 Owner - Facility: Charlotte Terminal
Inspection Date: 07/2912015 inspection Type: Compliance Evaluation
Laboratory Y s No NA NE
Are field parameters performed by certified personnel or laboratory? a El 110
Are all other parameters(excluding field parameters) performed by a certified lab? 0 Q 11 ❑
Is the facility using a contract lab? M Q 11
Is proper temperature set for sample storage (kept at less than or equal to 6,0 degrees
Celsius)?
Incubator (Fecal Coliform) set to 44.5 degrees Celsius+/- 0.2 degrees? © 0 0 p
Incubator (BOD) set to 20.0 degrees Celsius +/-1.0 degrees? © ❑ 0 ❑
Comment: ESC Lab Sciences Certification #41 has been contracted to gerforml effluent analyses.
Effluent Sampllna Yes No NA NE
Is composite sampling flow proportional? 11 0 In El
Is sample collected below all treatment units? IN Q © Q
Is proper volume collected? [ Q
Is the tubing clean? Q (N Q
# Is proper temperature set for sample storage (kept at less than or equal to 6.0 degrees
Celsius)?
Is the facility sampling performed as required by the permit (frequency, sampling type ❑ ® Q
representative)?
Comment: The subject ermit re uires effluent grab samples.
Operations & Maintenance Yes No N& NE
Is the plant generally clean with acceptable housekeeping? W Q 0
Does the facility analyze process control parameters, for ex: MLSS> MCRT, Settleable ` Q 11 11 11
Solids, phi, DO, Sludge Judge, and other that are applicable?
Comment: All ntact wat r is hauled off -site _by Crystal Clean. The hauli_ng i§ locum n ed with dates
guantft, and fre uenc . The facili only dichar es stormwater from their seconda
containment areas. The ORC kM a log book detailin a dail -ins a tign checklist as a
Q&QC measure.
Flow Measurement - Effluent Yes No NA <NE
# Is flow meter used for reporting? Cl El 0 0
Is flow meter calibrated annually? © 0 M Q
Is the flow meter operational? © ❑ M D
(If units are separated) Does the chart recorder match the flow meter? 0
Comment: Flow calculations/measurements are erforrned in accordance with the subject permit.
Page# 4

Permit- NCO021962 owner. Facility, Charlotte Terminal
Inspection Date. 07129/2015 Inspection Typo- Compliance Evaluation
Eff—Imeol E'Re )(e_$ No NA Ng
Is right of way to the outfall properly maintained? Is 0 0 0
Are the receiving water free of foam other than trace amounts and other debris? 11 El 1:1 1:1
If effluent (diffuser pipes are required) are they operating property? 13 El M El
Comment: At the JiLngt cif the in§pecti2n, there was no gilschg[g2 corning from, the guLtfall. No signs of
pollujign were noted at the di§ghargg or receiving stream,
Page#

P"A
Amp -A
NCD�HR
North Carolina Department of Environmer
Division of Water Qua
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
April 10,
Mr. James Utke, Terminal Manager
CITGO Petroleum Corporation
Post Office Box 58
Paw Creek, NC 28130
SUBJECT: Compliance I
CITGO Petro",
NPICES Penn
Mecklenburg
Dear Mr. Utke:
I be self-explanatory.
,2
[nation Inspection
). NUO021902
rity, NC
Allocco or me at this office.
Sincerely,
for Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty Rozzelle, MCWQP
RBK/JGM
Mooresville Regional Office One
400resville, NC 28115 Nofffi
D t Customer Service: 1-877-623-6748 Nah

United States Environmental Protection Agency Form Approved.
EPA Washington, DC 20460 OMB No, 2040-0057
Water Compliance Inspection Report Approval Expires 8/31/98
g
zw�
Transaction Code PDES Yr/Mo/Day Inspection Type Inspector Facility Type
N 5 NCO021962 11/08/30 C C 2
Remarks:
Inspector- Mecklenburg County Water Quality Program
Inspection Work Days Facility Self -Monitoring Rating BI QA Reserved
O.8 3 N N
Name and L tacation of Facility Inspected: Entry TrnelC)ate. Permit Effective:
7600 Mount Holly Road Exit Time/late: Permit Expires:
Mecklenburg County, NC 11:15 a.m. June 30, 2015
_44—ame(s)'of —On-Site R'e—pre—s-en—tatives—/Titie'l-Ph—on—August 30, 2011
e —Number:
Mr. James Utke / Terminal Manager / [phone]
Mr, Robert Durham / ORC / [phone]
Name and Address of Responsible Official: Title: Terminal Manager
Mr. James Utke Phone Number: [phone]
Citgo Petroleum Corporation
P.O. Box 58 Contacted: Yes
Charlotte, North Carolina 28130
T Rems
�g "MR,
�'g ie­g­ '7777 """T'72
"o,
11M
"go"
Permit 0 Flow Measurement Z Operations & Maintenance E3 Sewer Overflow
Records/Reports N Self -Monitoring Program N Sludge Handling Disposal Ej Pollution Prevention
• Facility Site Review E] Compliance Schedules 0 Pretreatment Program El Multimedia
• Effluent/Receiving Waters N Laboratory EJ Storm titer' Other:
10111,111,111,11 31`111'1'�'
MAO
See Attached Summary
Signature(s) of Inspectors}: Agency/Office/Telephone: Date:
Jeff Mitchell MCWQP/ [phone] August 31, 2011
S�i�qr Tature of Re. vieZ�,' k,� A enQy/Office: Cleat
yre of Revie'_ Division of Water Quality
Marcia Allocco Surface Water Protection — Mooresville Regional Office April 5, 2012
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete

r
GENERAL.
The facility was last inspected on August 25, 2010, by Jef
Quality Program (MCWQP).
PERMIT:
Mitchell of the Mecklenburg County Water
td expires on June 30, 2015. The permit
1.
iit properly describes the facility and
>ray irrigation system (Permit No.
,i,erformed after the inspection. The review indicated the permit is still active until it was
-cember 1, 2011.
"PORTS:
The permittee needs to include this information on all future DMRs.
FACILITY SITE REVIEW:
The runoff from the covered fueling rack and manifold area flow to a holding tank, The facility contracts
FCC Environmental to haul the fueling rack wastewater from the holding tank off -site for disposal. The
stormwater collected in the aboveground storage tank containment basins is visually inspected and can be
manually released through Outfall 001, or the stormwater can be discharged through a spray irrigation system.
All of the major components of the facility treatment works were in service and appeared to be operating
properly at the time of the inspection.
FLOW MEASUREMENT:
Flow measurement is accomplished by multiplying the known flow rate from the discharge pipe by the
discharge duration, Based on the current permit, this is an acceptable flow measurement method.
LABORATORY:
Chemical analysis of effluent samples and acute toxicity testing is performed by Environmental Science
Corp., (NC Laboratory Certification #375 & #041). Environmental Science Corp. was not evaluated asp of
this inspection,

EFFLUENT/RECEIVING WATERS:
Outfall 001 consists of a riprap-lined ditch, which flows to an unnamed tributary to Gum Branch, which
is a Class WS-IV water in the Catawba River Basin. The facility was not discharging at the time of the
inspection.
SELF -MONITORING PROGRAM:
Monthly monitoring reports were reviewed for the period June 2014 through May 2011. The reports
indicate that the facility was in compliance with permit effluent limits during this period. However, the
permittee was flagged by the Division's Compliance database for not monitoring the effluent fro?utfall 001
for EPA 625 analyses in the last half of 2011. A review of the noted DMRs found that an EPA parameter code
is not notated on the top of the DMR coal when the EPA 625 analyses were reported. The Division's data
entry staff does not enter any data unless it has a corresponding EPA parameter code; this generated the
monitoring violation. Please use EPA parameter code 76028 on future DMRs that report EPA 625
analyses.
OPERATIONS & MAINTENANCE:
The facility and site appeared well operated and maintained.

V A.*',A* FILE
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen N. Sullins Bee Freeman
Governor Director Secretary
October 12, 251
Mr, James Utke, Terminal Manager`
CITGO Petroleum Corporation
Post Office Box 58
Paw Creek, NC 28130
SUBJECT, Compliance Evaluation Inspection
CITGO Petroleum Corporation -Charlotte Terminal
NPDES Permit No, NCO021962
Mecklenburg County, NC
Dear Mr, Utke:
On August 25, 2010, Jeff Mitchell of the !Mecklenburg County Water Quality Program (MCWQP)
conducted an inspection at the subject facility. This inspection was conducted as part of a cooperative
working agreement between Mecklenburg County and the Division of Water Quality. The enclosed
report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not hesitate to call Ids.
Allocco or me at this office.
Sincerely, y5�,
for Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc� Rusty I ozzelle, MCW P
RBK/JGM
Mooresville regional office
Location: 616East Center Ave,, Suite301, Mooresville, No 28115 (One
Phone: (7t14) 663-1699 1 Fax: [phone] k Customer Service: 1-8i 7-623-6748 Nth Carollina'
4n#,:>mc,f•,ht#n•11«rr,rt�t nrriesrrrnmhur htexrri: ��.ra �,a >*aA.+YI �iIi

United States Environmental Protection Agency Form Approved.
Washington, DO 20460 OMB No, 2040-0057
EPA
r8
Water Compliance Inspection Repot Approval Expires /31/98
Section A: National Data System Coding
Transaction Code NPDES Yr,'Mo/Day Inspection Type Inspector Facility Type
N 5 NCO021962 10/08/25 C C 2
Remarks:
lnspector. Mecklenburg County Water Quality Program
Inspection Work Days Facility Self -Monitoring Rating B1 QA Reserved
0,7 4 N N
Name and i.ocation of Facility Inspected: Entry Tiellate Permit effective:
Citgc Petroleum Corporation I
7600 Mount Road Exit Time/Date: Permit Expires:
Mecklenburg County, NC 11:45 a,m. /Aug. 25, 2010 June 30, 2010
Narne(s) of On -Site Re presentatives/TitielP hone Number:
Mr. James Utke / Terminal Manager / [phone]
Name and Address of Responsible Official: Title: Terminal Manager
Mr. James Utke
Citgo Petroleum Corporation Phone Number: [phone]
P,O. Box 58
Charlotte, North Carolina 28130 Contacted: Yes
Section C. Areas Evaluated During Inspection
Permit Flow Measurement Z operations & Maintenance Sewer Overflow
Records/Reports Z Self -Monitoring Program Z Sludge Handling Cisposal= Pollution Prevention
Z Facility Site Review El Compliance Schedules El Pretreatment Program El Multimedia
M Effluent/Receiving Waters Laboratory El Stormwater El Other,
Sedlon D:'Summary'of Findings/Comments,,
See Attached Summary
Signature(s) of Inspector(s): Agency/Office/Telephone: Date:
Jeff Mitchell MCWQPI [phone] September 1, 2010
Signature of Reviewer: AgencyTdffice: Date:
_1y 11 i [ C>
CDENR — Division of Water Quality
Marcia Allocco Surface Water Protection — Mooresville Regional Office October 12, 2010
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete

Mr. James Me, CITGO Petroleum Corporation
NCO021962 C i, Page
October 12, 2010
GENERAL:
The facility was last inspected on August 27, 2009, by Jeff Mitchell of the Mecklenburg
County Water Quality Program (MC QP):
PERMIT:
The current permit became effective on June 1, 2006, and expired on June 20, 2010. A permit
renewal application had been submitted. A permit renewal application was submitted February
2010. The new permit is currently under review by the Division n of Water Quality. Until the new
permit is issued the facility should continue to operate under the requirements of the expired
permit.
The permit authorizes the discharge of stormwater/wastewater from Outfall 001 The
current permit lists the NPDES treatment works as consisting of a waste holding tank and a
bermed area with flow siphon and hand -operated discharge valve. The permit properly
describes the facility and appears adequate for the wastewater being discharged.
The certification classification for NCO021962 requires that the facility have an operator
in responsible charge (OiRC) with a Grade 1 Physical Chemical Water Pollution Control System
(PC-1) certification. The facility is staffed (ORC and back-up) with personnel that possess the
appropriate operator certification.
RE CaRCi IREPCiRT
Discharge Monitoring Reports (DMf s) and
for the period June 2009 through May 2010. The r
with the following exception of the August 2009 DN
on the DMR for the monitoring conducted on Augu
monitorin requirements in the permit (NCO021962
iboratory analytical reports were reviewed
ports appeared to be properly completed
volatile organic analysis was not noted
k 27, 2009, as required by the semi-annual
. The inspection found that the analysis had
been performed, but was omitted from the August 2009 DMR. An amended DMR should be
submitted to the Mooresville Regional Office of the Division of Water Quality,
FACILITY SITE REVIEW:
The runoff from the cowered fueling rack and manifold area flaws to a holding tank. The
facility contracts Allied Energy Corporation to haul the fueling rack wastewater from the holding
tank off site for disposal;
The stormwater collected in the aboveground storage tank containment basins is visually
inspected and can be manually released through Outfall 001, or the stormwater can be
discharged through a spray irrigation system (Permit No. WQ0019911). The spray irrigation
system has been in operation since February 2002. The spray irrigation system was not
evaluated `as part of this inspection.
All of the major components of the facility treatment works were in service and appeared
to be operating properly at the time of the inspection.

Mr ,James'utke, CITGO Petroleum Corporation 14
NCO021962 CI I, Pane
October 12, 2010
FLOW MEASUREMENT:
Flow measurement is accomplished by multiplying the known flow rate from the
discharge pipe by the discharge duration, Based on the current permit, this is an acceptable
flow measurement method.
LABORATORY:
Chemical analyses of effluent samples are performed by Environmental Science
Corporation, {NC Laboratory Certification }. Environmental Science Corporation was not
evaluated during this inspection. Acute Toxicity testing is performed by Meritech, Inc. (NC
Laboratory Certification #13). Meritech, Inc. was not evaluated as part of this inspection.
EFFLUENT/RECEIVING WATERS:
Outfall 001 consists of a riprap-lined stitch, which flows to an unnamed tributary to Gum
Branch, which is a Class WS-IV water in the Catawba River Basin. The facility was not
discharging at the time of the inspection.
SELF - MONITORING PROGRAM:
Monthly monitoring reports were reviewed for the period June 2009 through May 2010.
The reports indicate that the facility was in compliance with permit effluent limits and monitoring
frequencies during this period.
OPERATIONS & MAINTENANCE:
NCE:
The facility and site appeared well operated and maintained.

NINA
r
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
Januaryi26, 2010
CERTIFIED MAIL ITEM 7007 0710 0000 5376 9147 - RETURN RECEIPT REQUESTED
Mr. Sett Eaton
CI TGO ]Petroleum Corporation
377 Flowers Rd
Atlanta, GA 30360
Subject; Notice of Violation
Failure to Submit Renewal Application
NPDE S Permit NC00219 2
Charlotte Terminal
Mecklenburg County
Dear Per itto :
The subject permit's expiration date is dune 30, 2010 Federal [40 CFR 1.221 and state (15A NCAC
► t, a .t �. s t
.t
t t

William G. Ross Jr ,"Secret:
North Carolina Department of Environment and natural Resourc
4�4
Coleen K. Sullins, Director
Division of Water Quality
August 14, 200
Mr. James Utke, Tenninal Manage:
CITGO Petroleum Corporation
Past Office Box 58
Paw Creek, NC 2800
SUBJECT: Compliance Evaluation Inspection
CITGO Petroleum Corporation -Charlotte Terminal
NPDES Permit No. NCO0219 2
Mecklenburg County, NC
Dear Mr. Utke s
On July 22, 2008, Mr. Christopher Elmore of the Mecklenburg County Water (duality
Program conducted an inspection at the subject facility, This inspection was conducted as part of
a cooperative working agreement between Mecklenburg County and the Division of Water
Quality. The enclosed report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not
hesitate to call Ms. Marcia A locco or me at (70 ) fi =1699.
Sincerely;
for Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty Roselle, MCWQ
cfe
File: W076161
,"c hCttrrIzna
HCQENR z Nrzzllzy
Mooresville Regional Office Division of Water Quality Shone 704-663-1699 Customer Service
Internet: cor�kv.nco�ateri u2ili =orb 610 East Center Ave, Suite 301 Mooresville, NC 78115 Fax [phone]
An Equal Opportunity/Affirmative Action Employer— 50% Recycled110% Post Consumer Paper

�on, IDC 2046011,
)ffice
Section A: National Data System Coding
Transaction Code NPDES
Permit No, YRjMO/DAY Inspection Type Inspector Facility Type
N 5 NC0021962
08/07/22 C C
2
Remarks:
Insnector: Me-1-1-1-- Count Water unlit r Pro ram
Inspection Work Days Facility
Self -Monitoring Evaluation Rating BI QA
....,,.....Reserved....
0.75
4 N N
Section B: Facility Data
Entry Time:
Permit Effective Date:
Name and Location of Facility
Inspected: 09:30 am
June 1, 2006
Citgo Petroleum Corporation
Exit Time:
7600 Mount Holly Road
10:20 am
Permit Expiration Date:
Charlotte, North Carolina
Date:
June 30, 2010
1 07122/2008
Name(s) of On -Site Representatives ------- Title(s) -------- Phone No(s):
Mr. Jarnes Utke / Terminal Manager / [phone]
Name and Address of Responsible Official: Title:
Mr. James Utke
Terminal Manager
Citgo Petroleum Corporation
Phone No.
Contacted?
P.O. Box 58
Charlotte, North Carolina 28130
[phone]
Yes
1
Section C.
Areas Evaluated During Inspection
ED Permit
Flow Measurement El Operations& Maintenance
El Server Overflow
[DRecords/Reports
Self -Monitoring program Ej Sludge Handling/Disposal
0 Pollution Prevention
Facility Site Review
Compliance Schedules El Pretreatment Program
El Multimedia
Effluent/Receiving Waters
0 Laboratory El Stormwater
El Other:
Section D. Summary of Findings/Comments
All areas are rated satisfactory unless otherwise indicated. See Attached Sheet(s) for Summary
Signature(s) of Inspector(s):
Agency/Office/Telephone:
Date:
Christopher Elmore
MCWQP/[phone]
August 5, 2008
Si a e of Reviewe
ein cy/Office:
DIte',
�Occo
N ENR — Division of Water Quality
Marcia Al
Surface Water Protection — Mooresville Regional Office
August 13 2008
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

GENERAL:
The facility was last inspected on July 16, 2007 Mr. Christopher Elmore of the
Mecklenburg County Water Quality Program (MCW( P). A Compliance Evaluation Inspection
Report was issued can July 23, 2007.
PERMIT:
The current permit became effective on June 1, 2006, and expires on June 30, 2010. The
permit authorizes the discharge of stor water/wastewater from Outfall 001.
The current permit lists the NPDES treatment works as consisting of a waste holding tank
d a berined area with flow siphon and hand -operated discharge valve. The permit properly'
describes the facility and appears adequate for the wastewater being discharged.
The certification classification for NCO021962 rewires that the facility have an operator
in re pon
(PC-1) ct
approprr
RECOR
for the pt
e operator certification.
!S PORTS.
;charge Monitoring Reports (DMRs) and laboratory analytical reports were reviewed
were clear, organized, and well maintained; no discrepancies were noted.
FACILITY SITE REVIEW:
The runoff from the covered fueling rack and manifold areas flows to a holding tank-. The
facility contracts Allied. Energy Corporation to Haul the fueling rack wastewater from the holding
tank off site for disposal.
The sto ` water collected in theaboveground storage tank containment basins is visually
inspected and can be manually released through Outfall 001, or the sto water can be discharged
through a spray irrigation system (Pe it No. WQ0019911). The spray irrigation system has
been in operation since February 2002. The spray irrigation system was not evaluated as pat of
this inspection.
All of the major components of the facility treatment works were in service and appeared
to be operating properly at the time of the inspection.:

FLOW MEASUREMENT:
Flow measurement is accomplished by multiplying the known flow rate froi
hod.
#395) to perform all chemical analyses specified in the pennit and with Meritech, Inc. (NC
Laboratory Certification #165) to perform the toxicity testing specified in the permit). Neither
Severn Trent Laboratories nor Meritech, Inc. was evaluated as part of this inspection.
EFFLUENT/RECEIVING WATERS:
Outfall 001 consists of a riprap-lined ditch, which flows to an unnamed tributary to Gum
Branch, which is a Class S-IV water in the Catawba River Basin. The facility was not
discharging at the time of the inspection,
SELF -MONITORING PROGRAM:
Monthly monitoring reports were reviewed for the period June 2007 through May 2008.
The reports indicate that the facility was in compliance with permit effluent limits during this
period and that all parameters, sample collection, preservation, and transportation techniques
appeared adequate.
OPERATIONS & MAINTENANCE:
The facility and site appeared well operated and maintained.

\N A Tk- Michael F. Easley, Governor
William G. Ross Jr., Secretary
7 North Carolina Department of Environment and Natural Resources
Coleen H, Sullins, Director
Division of Water Quality
November 10, 2008
Mr. James Utke, Terminal Manager
CITGO —Paw Creek Bulk Terminal
Post Office Box 58
Paw Creek, NC 28130
Subject: Toxicity Test Results
CITGO — Paw Creek Bulk Terminal
NPDES Permit No. NCO021962
Mecklenburg County, NC
Dear Mr. Utke:
Enclosed is a copy of the toxicity test results relative to the inspection conducted
at the subject facility on September 23, 2008 by John Lesley of this Office. Whole
effluent samples were collected for use in an acute 24-hour Pimephales promelas
definitive toxicity test. The test utilizing these samples resulted in a LC50 >100%.
Tina rannrf chni dri hA -_a1f_PYn1Anntnrw hnwavP.r Phnt ild voti hAvP qnv ClUestions
concerning this report, please do not hesitate to contact Mr. Lesley or me at (704) 663-
1699.
Sincerely,
Robert B. Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Central Files
Susan Meadows, Aquatic Toxicology Unit
Mecklenburg County Water Quality Protection
Mailing Address Phone [phone] Location No
One
hCarolirta
610 East Center Avenue, Suite 301 Fax [phone] East Center Avenue, Suite 301
Mooresville, NC 28115 Mooresville, North Carolina
Internet: www.ncwater(malitv,orP Customer Service 1-877-62J-6748
An Equal Opportunity/Affirmative Action Employer - 50% Recycled/1 0% Post Consumer Paper

CITGO -Paw Creek Bulk Terminal
NPDES Permit No. NCO021' 62
Page 2
Whole effluent samples were collected. can September 23, 200
a LC50 (the concentration of effluent that is lethal to % of the to
Toxicity test information follows:
Test Type 24-hour Pin
Test Concentrations 0, 125, 2
Test Result
Control Survival
Test Treatment Survival 100%'
Sample pH
Sample Conductivity i
Sample Total Residual Chlorine
The LC50 for this sample indicates that the effluent would
water quality impacts on the receiving stream.
ite

Division of Wai
November -1
MEMMANDUM
To:
Rob Krebs
Regional Supervisor, Surface 14
Through:
Cindy A. Moore`*
Supervisor, Aquatic Toxicology
From:
Carol Hollenkainp(Y
Quality Assurance Officer, Aqu
Subject:
Whole effluent toxicity test rest
Citgo-Paw Creek Bulk Termina,
NPDES Pen -nit # NCO021962/0
Mecklenburg County
The aquatic toxicity test using a grab sample of effluen
M
luality
18
"rotection, MRO
I oxicology Unit
greater than 100%. Toxicity test information follows.
Test Type 24-hour Phnephales promelas definitive
Test Concentrations 0, 115, 25, 50, 75, and 100% sample
Test Result LC50>100%
Control Survival 100%
Test "treatment Survival 100% in the 90% treatment
Sample PH 7.41 SU
Sample Conductivity 78.1 micromhos/ern
Sample Total Residual Chlorine <0. 10 mg/l
The LC50 and measured water quality parameters for this sample indicate that the effluent would not be
predicted to have acute water quality impacts on receiving water. Please contact us if further effluent
toxicity monitoring is desired. We may be reached at [phone]
Basin: CTB 34
cc: Central Files
John Lesley, MRO
Aquatic Toxieology Unit Environmental SciencesSection

\N A Michael F. Easley, Governor `
William G. Ross Jr., Secretary
North Carolina Ikpartment of Environment and Natural Resources
pr
3 "C Coleen H. Sullins, Director
Division of Water duality
August 7, 2007
r. James Luke, Terminal Manager
CITGO Petroleum Corporation
Fast Office Box 58
Paw Creek, NC 28130
SUBJECT: Compliance Evaluation Inspection
CITGO Petroleum Corporation -Charlotte Terminal
NPI ES Permit No. NCO0219 2
Mecklenburg County, NC
Dear Mr. Lake;
Enclosed is a copy of the Compliance Evaluation Inspection' report for the inspection
conducted at the subject facility on July 16, 2007, by Mr. Christopher Elmore and Ms. Amber
Linden of the :Mecklenburg County Water; Quality Program (MCWQP). This inspection was
conducted as part of a cooperative working agreement between Mecklenburg County and the
Division of Water Quality. Please provide the facility's Operator in Responsible 'Charge with the
findings of the inspection by forwarding a copy of the enclosed report.
The enclosed report should be self-explanatory; however should you have any questions
concerning this report or any other matters please do not hesitate to call M. Marcia Allocco or
e at this Office,
Sincerely,
for Robert B. „ Krebs
Regional Supervisor
Surface Water Protection
Enclosure
cc: Rusty Roelle, MCWQP
Peggy Finley, MR — Aquifer Protection
cfe
Filer WQ 00 19610707
N UiCarolina
C ENR �Ir�tltl"lil�
Mooresville Regional Office Division of Water Quality Phone [phone] Customer Service
Internet: 610 East Center Ave, Suite 301 Mooresville, NC 28115 Fax [phone] I-877-6 3-6748
An Equal Oppodunity/Affirmative Action Employer — 50% Recycledt10% host Consumer Paper

United States Environmental Protection Agency, Washington, DC 20460
Approv
NPDES Compliance Inspection Report ;%Form
ARM
OMB No. 2040
b6i
V North Carolina Department of Environment and Natural Resources
NCD--
Approval Expi.
Division of Water Quality, Mooresville Regional Office
7/31/85
Section A: National Data System Coding
Transaction Code NPDES Permit No. YR/MO/DAY Inspection Type Inspector
Facility Type
N 5 NC0021962 07/07/16 C C
2
Remarks:
Insnector: M-1-1--l­­ Count
Inspection Work Days Facility Self -Monitoring Evaluation Rating BI QA
Reserved,. .
0.75i 4 N N
Section B: Facility Data
Entry Time: Permit Effective Date:
Name and Location of Facility Inspected: 09:50 am June 1, 2006
Citgo Petroleum Corporation Exit Time-
7600 Mount Holly Road 10:30 am Permit Expiration Date:
Charlotte, North Carolina Date: June 30, 2010
07/16/2007
Name(s) of On -Site Representatives ------Title(s) -- — ---- Phone No(s):
Mr. James Utke / Terminal Manager / [phone]
Name and Address of Responsible Official: Title:
Mr. James Utke
Terminal Manager
Citgo Petroleum Corporation
- Phone No.
Contacted?
P.O. Box 58
Charlotte, North Carolina 28130
[phone]
Yes
Section C*
Areas Evaluated During Inspection
Z Permit Flow Measurement Z Operations& Maintenance
Sewer Overflow
Z Records/Reports Z Self -Monitoring Program Sludge Handling/Disposal
0 Pollution Prevention
Facility Site Review [3 Compliance Schedules Pretreatment Program
C] Multimedia
Effluent/Receiving Waters ED Laboratory El Stormwater
Other:
Section D: Summary of Findings/Comments
All areas are rated satisfactory unless otherwise indicated. See Attached Sheet(s) for Summary
Signature(s) of Inspector(s): Agency/Office/Telephone:
Date:
Christopher Elmore MCWQP/[phone]
July 24, 2006
Signature of Reviewer: Agency/Office:
Date:
NCDENR — Division of Water Quality
Marcia Allocco Surface Water Protection — Mooresville Regional Office
August 7, 2007
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

GENERAL:
The facility was last inspected on April 2, 2006, by Mr. Christopher Elmore of the
Mecklenburg County Water Quality Program (MCWCP). A Compliance Evaluation Inspection
Report was issued on May 22, 2006.
PERMIT:
The current permit became effective on June 1, 2006, and expires on June 30, 2010. The
permit authorizes the discharge of sto water w stewater from Outfall 001.
The current permitted treatment system consists of a waste holding tank and a bermed
area with flow siphon and hand -operated discharge valve. The permit properly describes the
facility and appears adequate for the wastewater being discharged.
The certification classification for NCO0 1962 requires that the facility have an operator
in responsible charge ( RC) with a Grade I Physical Chemical Water Pollution Control System
(PC-1) certification. The facility is staffed. (CRC and back. -up) with personnel that possess the
appropriate operator certification:
RECORDS/REPORTS:
Discharge Monitoring Reports (DMRs) and laboratory analytical reports were reviewed
for the period May 2006 through May 2002. The reports appeared to be properly completed. All
data:.:, reports, operational logs, and manifests were readily available at the facility. The records
were clear, organized, and well maintained; no discrepancies were noted.
FACILITY SITEREVIEW:
The runoff from the covered fueling rack and manifold areas flows to a holding tank. The
facility contracts Allied Energy Corporation to haul the fueling rack wastewater from the holding
tank off site for disposal.
The storrowater collected in the aboveground storage tank containment basins is visually
inspected and can be manually released. through Cutfall 001, or the stormwater can be discharged
through a spray irrigation system (Permit No. WQ0019911)., The spray irrigation system has
been in operation since February 2002. The spray irrigation system was not evaluated as part of
this inspection.
All of the major components of the facility treatment works were in service and appeared
to be operating property at the time of the inspection.
FLOW MEASUREMENT:
Flow measurement is accomplished by multiplying the known flow rate from the
discharge pipe by the discharge duration. Based on the current permit this is an acceptable flow
measurement method.

C
LABORATORY:
The permittee contracts with Severn Trent Laboratories, Inc. - Mobile (NC Laboratory
Certification #395) to perform all chemical analyses specified in the permit and with Meritech,
Inc. (NC Laboratory Certification # 165) to perform the Acute toxicity testing specified in the
permit. Neither Severn Trent Laboratories, Inc. - Mobile nor Meritech, Inc. was evaluated
during this inspection,
EFFLUENT/RECEIVING WATERS:
Outfall 001 consists of a riprap-lined ditch, which flows to an unnamed tributary to Gum
Branch; a Class S-IV water in the Catawba River Basin. The facility was not discharging at
the time of the inspection.
SELF -MONITORING PROGRAM:
Monthly monitoring reports were reviewed for the period May 2006 through May 2007.
period.
Records indicate that all parameters, sample collection, preservation, and transportation
techniques appear adequate.
OPERATIONS & MAINTENANCE:
The facility and site appeared well operated and maintained,

�. V lr
0 Michael F. Easley, Govemor
William fl. Ross 7r., Secretary
North Carolina Department of Environment and Natural Resources
1, Alan W. Klimek, P. E. Director
Division of Water Quality
�.IVY-UTUNMtO6.
August 17, 2006 AND NATURAL pE 1150E ,
91,
James Citke,
Citgo Petroleum Corporation
7600 Mount Holly Ind.AUG 18
Charlotte, 28214 �dt
Subject: Notice of Incomplete Discharge Monitoring Deport NCO021962
Bear Pe ittee:
QUALITYWATER 4
The purpose of this letter is to call your attention to problems with the recent submittal of the Discharge
Monitoring Report D )'from your facility, As you may know, the data recorded on your DMR is keyed
into the Division's database. Our data entry staff has informed me of problems with your recent DMR
submittal. until these problems have been corrected, your DMR will be considered incomplete. Please
see the attached form along with a copy of the problem DMR for details regarding the DMR's deficiency.'
Incomplete or illegible DMRs affect our staff s ability to provide a timely and effective evaluation of DMR
submittals. Please be aware that until the Division receives a corrected DMI2, you may be considered
noncompliant with your NPDES permit and 1 A NCAC 02B .0506, and you may be subject to further
enforcement action. Please take the necessary steps to correct the problems and submit two copies of the
ended DMR within fifteen (15) days of the date of this letter to the following address:
Attention: Michele Phillips
Division of Water Quality
Central Files
117 Mail Service Center
Raleigh, North Carolina 27699-1617
Future DMR submittals with the same or similar problems will be unacceptable. If you have any questions
about the proper completion of DMRs, please contact Michele Phillips at 919-7 -. 083 Ext. 534. Thank
you for your assistance in this matter.
Sincerely,
Michele Phillips
cc:
Central Files
Now Carolina
Wavily
N. C.Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Phone: [phone] Customer Service
Internet httpJ1h2o.enr.state.nc.us 512 N. Salisbury St, Raleigh, NC 27604 Fax: [phone]
An Equal Opportunity/Affirmative Action Employer

Notice of Incomp
:, 1,6
1jivi \ IVIU 11 dilu 1 cm.
The Division of Water Quality deems the
following r ason(s): (Please see highligh
LJ The Average, Max
filar Minimum data
ve been omitted or are
gard to parameters 3423 (Benzene, dissely
'Phenolics, totalrecoverable), which you ret
be 34030 (Benzene), 34010 (Toluene) and 3
toring Report
as incomplete due to the
-hed DMR for details)
ave been emitted
the lab actually analyzed for the codes our database shows. If the latter is correct please
update your form template with the correct code and resubmit per the enclosed letter.

WA
} , Michael F. Easley, Govern
William G. Ross Jr., SecretaryCO t
North Carolina Department of Environment and Natural Resources
{ Alan W. Klimek, P.E. Director
Division of Water Quality
May 22, 2006
Mr. James Utke, Terminal Manager
CITGO Petroleum Corporation
Past OfficeBox 58
Paw Creek, NC 28130
SUBJECT. Compliance Evaluation Inspection
CITGO Petroleum Corporation -Charlotte Terminal
NPDES Permit No. NCO021962
Mecklenburg County, NC
Dear Mr. Utke:
On April 25, 2006, Mr. Christopher Elmore of the Mecklenburg County Water Quality
Program conducted an inspection at the subject facility. ; This inspection was conducted as part o
a cooperative working agreement between Mecklenburg County and the Division of Water
Quality. The enclosed report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not
hesitate to call Mr. John Lesley or me at 704166 -1699.
Sincerely,
(_,77 L . Rex Gleason, P.E.
" Surface Water Protection Regional Supervisor
Enclosure
cc. Rusty Rozzelie, MC QP
cfe
File: WQ 0021962,0406
Caro in
one
Car �%(
Mooresville Regional Office Division of Water Quality Phone 704-663-I699 Customer Service
Internet: xuw.ncwaterquality or * 610 East Center Ave, Suite 30I Mooresville, TIC 28115 Fax [phone]-63-6748
An Equal Opportunity/Affirmative Action Employer — 50% Recycled/10% Past Consumer Paper

FM
hm
,nal Office
Transaction Code NPDES Permit No. YR/MO/DAY Inspection Type Inspector Facility Type
N 5 NCO021962 06/04/25 C C 2
Remarks:
Inspectov M--p—qCount Water unlit Pro tarn
-
Inspection Work Days Facility Self -Monitoring Evaluation Rating BI CAA Reserved .....
0.75 1 4 N N
ON
Christopher Elmore MCWQP/[phone] May 22, 2006
Signature of Revie r. Agency/Office: Date:
John Lesley DWQ-SWP/Mooresville Regional Office/(704-663-1699 May 22, 2006
EPA Form 3560-3 (Revised 3-85) Prev 0as Editions are Obsolete

GENERAL:
The facility was last inspected on June 9, 2005 by Mr. Christopher Elmore of the
Mecklenburg County Water Quality Program (MCWQP). A Compliance Evaluation Inspection
Report was issued on June 20, 2005.
PERMIT:
The current permit became effective on September 1, 2001, and expired on June 30,
2005. The facility continues to discharge under the constraints of the expired permit. The permit
authorizes the discharge of stormwater/wastewater from Outfall 001.
The current permit lists the NPDES treatment works as consisting of an oil/water
facility contracts US Filter, Inc. and Allied Energy Corporation to haul the fueling rack
wastewater from the holding tank off -site for disposal.
The stormwater collected in the aboveground storage tank containment basins is visually
inspected and can be manually released through Outfall, 001, or the stormwater can be discharged
through a spray irrigation system (Permit No. WQOO 199 11). The spray irrigation system has
been in operation since February 2002.
All of the major components of the facility treatment works were in service and appeared
to be operating properly at the time of the inspection.
FLOW MEASUREMENT:
Flow measurement is accomplished by multiplying the known flow rate from the
discharge pipe by the discharge duration. Based on the current permit, this is an acceptable flow
measurement method.

) TORY.
•. ..v«•�. xr,w.vax wvvax, .aaav♦ v. ww ax.v:.r v+bbA bi.a.4bVN NU xl64Ak A, bAAAk.J"aAAti�.iV£V #.AVAA.
EFFLUENT/RECEIVING WATERS.
Cutfall 001 consists of a riprap-lined ditch, which flaws to an
Branch, which is a Class-'W -IV water in the Catawba River Basin.'
discharging at the time of the inspection.
SELF -MONITORING PROGRAM:
Monthly monitoring reports were reviewed for the period Ma
2006. The reports indicate that the facility was in compliance with p(
this period:.
Records indicate that all parameters, sample collection, prescr
techniques appear adequate.
OPERATIONS r& MAINTENANCE:
The facility and site appeared well operated and maintained.
valzon, anu iransporcacin

#
#
• #
#
Ins,pection Sum' narjL: (additional comments ma v be included on attached �qes
The spray irrigation system consists of a bermed bulk storage tank area, a 1.5 HP pump, two inch
PVC line and ten spray irrigation nozzles. The spray irrigation system is used to discharge the
stormwater from the aboveground storage tank containment basin. The starter is discharged
on -site onto a 1.5-acre spray field of fescue grass. There is no discharge of wastes to surface
waters.
Is afollow-up inspection necessary yes X no
Inspector(s) Name(s)/Title(s) Christopher Elmore/Environinental Specialist
Telephone No. 704-336-5500 Fax No. 704-336-4391
Date of Inspection April 25. 2006

Spray Irrigation Inspection Page 2
Citgo Petroleum Corp. Permit #WQOO 19911
Type
Activated Sludge Spray, low rate
Activated Sludge Spray, high rate
Activated Sludge Drip, low rate
Lagoon Spray, low rate
Reuse (Golf Courses)
Recycle /Reuse
Single Family Spray, low rate
Single Family Drip
Infiltration System
X Other See comment below.
Treatment
Y Are treatment facilities consistent with those outlined in the current permit.
Y Do all treatment units appear to be operational. If no, note below.
I List any action items necessary for each unit.
Comment:
Lagoons N/A
Primary (check any/all that apply)
Influent structure (free of obstructions)
Banks/berms (are there signs of seepage, overtopping, down cutting or erosion)
Vegetation (is there excessive vegetation on the lagoon bank
Liner (if visible, is it intact)
Baffles/curtains (in need of repair)
Freeboard (>2 feet from overtopping)
Staff gauge ( clearly marked)
Evidence of overflow (vegetation discolored or laying down/broken)
Unusual color (very black, textile colors)
Foam (are antifoam agents used)
Floating mats (sludge, plants, inorganics)
Excessive solids buildup (from bottom)
aerators/mixers operational (if present)
Effluent structure (free of obstructions, easily accessible)
Comment -The irrigation water for the spM irrigation system is pumped out of the benned store e
tank containment basin at the facility. No la dons are present on the site.
Lagoon Secondary N/A

St)rav Irrieation Inspection Page 3
Citgo Petroleum Corp. Permit #WQ0019911
Influent nump station
--X—All pumps present, operational —Bypass structure present
— Bar screen, maintained Free of excessive debris
Bars evenly spaced —Bars excessively corroded
—Back-up power
Comment:
Aeration Basin N/A
aeration pattern even across surface of unit
—easily accessed
Comment:
Clarifiers N/A
weirs level —scum rack operational easily accessible
Comment:
Return PMMps N/A
in place operational
Filters N/A
—media present —air scour operational —clear well free of solids
Residuals N/A
storage/treatment if storage is greater than 24 months, Surface Disposal permit?)
Comment:
Disinfection N/A
If gas, is storage safe?
Is it dual feed system?
How do you know it is working?
If tablets - are tablets present?
Effluent Storage
LAGOON(s) SEPTIC TANK(s)—A_ABOVE GROUND TANK OTHER
Rumber of months storage_ Spill control plan on site

Spray Irrigation Inspection Page 4
Citgo Petroleum Corp. Permit #" Q001 911
Lagoon Is lagoon lined.
Above ground tank Aerated Mixed
In ground t Aerated Mixed
Drying beds Concrete storage pad
Comment:
Disposal final end use)
Is application equipment in need repair? No Are buffers adequate? Yes
Are cover crops the type specified in permit? Yes In need of improvement? No
Signs of runoff'?No Signs ofponding? No
Comment: All corm orients of the s stem appeared to be opeLrating properlyat the time of the inspection,
Yes Is the acreage specified in the permit being utilized?
Yes Is the application equipment present and operational?`
No Are there any limiting slopes in disposal fields?
No Are restrictions for use of these areas specified?
Yes Is permit being followed?
No Is there evidence of runoff or drift?
Yes Are monitoring wells called for in permit present?
Yes Is site access restricted in accordance with permit?
Comment.:
Yes Is permit available upon request?
Yes Are monitoring reports present. NDMR :X NDAR X
Yes Are operational logs present?
Yes Are lab sheets available for review?
Yes Do lab sheets support data represented on NDMR or NDAR?
Yes Are annual soil reports available?
Yes Are operation and maintenance records present? Y Complete Y
No Has permittee received any public complaints in the last 12 months?
Comment':.

ALT,747-KWA
A*A
ORR
CE
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Michael F. Easley, Governor William G. Ross, Jr., Secretary
Alan W. Klimek, F.E., Director
June 20,2005
. James Utke, Terminal Manager
CITGO Petroleum Corporation
Post Office 58
Paw Creek, NC 28130
SUBJECT: Compliance Evaluation Inspection
CITGO Petroleum ion-t: lat a Terminal
TJES'Permit No. 1 CO0: 1962
Mecklenburg County, NC
Dear Mr. TJtke
On June 9, 2005, Mr. Christopher Elmore of the Mecklenburg County Water Quality
Program conducted an inspection at the subject facility. This inspection nd of
Quahiy. The enclosed report should be self-explanatory.
r vnee hn-era anv niu-ttinm nn incr this ri-,nnrt nr nnv nther tt It _ An
xe at 704/663- 699.
Sincerely,
D. Rex Gleason, P.E.
Enclosure
cc: Rusty Rozzelle, MCWQP
i7RG/cfe
rite. WQ0021967-0605
e
Ptaone: 1ti1i / Pax: i � / Internet: ho.etrr. e.nc,us Xatmm(ly
An Equal Opportunliy/Afirmatly Action Employer- 50% Recycled/10% Post Consumer Paper

United States Environmental Protection Agency, Washington, DC 20460 ffl�-Nwj Form Approved
NPDES Compliance Inspection Report OMB No, 2(40-0003
Nordi Carolina Denartme of Environment and Natural Resources AU'A AnDroval E\Dires
Division of Water Quality, Mooresville Regional Office NCDENR
Section A: National Data System Coding
Transaction Code NPDES Permit No. YRIMO/DAY Inspection Type Inspector Facility Type
Inspector: Mecklenburg County Water Quality Program
Inspection Work Days Facility Self -Monitoring Evaluation Rating BI QA ........ ...Reserved. ...........
Entry Time: Permit Effective Date:
iame and Location of Facility Inspected: 10:00 am September 1, 2001
'itgo Petroleum Corporation Exit Time:
'600 Mount Holly Road 10:50 am Perntit Expiration Date:
'harlotte, North Carolina June 30,2005
06/09/2005
4ame and Address of Responsible Official: Title:
,itgo Petroleum Corporation Phone No. Contacted?
LQ Flow Measurement Operations & Maintenance L
ED Self -Monitoring Program Sludge Handling/Disposal E
iew El Compliance Schedules Pretreatment Program E
I
'
' ^
�(s) for Summary
June 15,
A.gency/Office Date:
itions are Obsolete

GENERAL:
The facility was last inspected on :May 18, 2004 by Ms. Crystal Taylor of the
Mecklenburg County Water 'Quality Program (MC'Wt P). A Compliance Evaluation Inspection
Report was issued. on June 29, 2004.
PERMIT:
The current permit became effective on September 1, 2001, and expires can June 30, 2005.
The permit authorizes the discharge of stonn water/wastewater from. Outfall 00 .
The current permit lists the NPDES treatment works as consisting of an oil/water
separator, an equalization tank, a second oil/water separator, a diffused aeration system, an, d a
detention pond with an underflow siphon. The actual treatment works currently in operation
consist of the detention pond and underflow siphon.
e current permit does not accurately describe the facility treatment works. Changes to
the facility treatment works should be indicated on the new permit to be issued in July of2005.
CO PORTS
Discharge e Monitoring Reports ) and laboratory analytical reports were reviewed
for the period April 2004 through April 2005. The reports appeared to be properly completed.
All data, reports, operational logs, and manifests were readily available at the facility. The
records were clear, organized, and wellmaintained; no discrepancies were noted.
FACILITY SITEREVIEW:
F - o • r• o i r �,
-co; plashed by multiplying the known flow rate from the
duration. Based on the current permit, this is an acceptable flow

LABORATORY:
Chemical ical alysis of effluent samples was performed by Severn "Trent Laboratories, (NC
Laboratory Certification 3 5). Severn `rent Laboratory was not evaluated under this
inspection.
EFFLUENT/RECEIVING WATERS.
Outfall 001 consists of a riprap-lined ditch, which flaws to an unnamed ibut to Gum
Branch, which is a Class W -1V water in the Catawba River Basin. The facility was not
discharging at the time of the inspection.
SELF -MONITORING PROGRAM:
DMRs were reviewed for the period April 2004 through April 2005. e reports indicate
that the facility was in compliance with permit effluent limits during this period.
techniques appear adequate.
OPERATIONS & MAINTENANCE:
e facility and site appeared well operated and maintained,

A Michael F. Easley
Governor
NOD William G. Ross, Jr., Secretary
z1S
7 —NR
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
September 9, 2004
Scott Eaton
CITGO Petroleum Corporation
3877 Flowers Road
Atlanta, GA 30360
Subject: Renewal Notice
NPICES Permit N00021962
Paw Greek Terminal
Mecklenburg County
Dear Permittee:
Your NPICES permit expires on June 30,2005. Federal (40 CFR 122.41) and North Carolina (15A NCAC 2HO105(e))
regulations require that permit renewal applications must be filed at least 180 days prior to expiration of the current permit. If
you have already mailed your renewal application, you may disregard this notice.
To satisfy this requirement, your renewal package must be sent to the Division postmarked no later than January 1,
depending upon the delinquency of the request.
ror4d essliste -7y6ri rn� cobrac�the 66346"
Use the enclosed checklist to complete your renewal package. The checklist identifies the items you must submit with
the permit renewal application, If you have any questions, please contact me at the telephone number or e-mad address listed
below.
Sincerely,
Charles H Weaver, Jr.
NPDES Unit
cc: Central Files
NPDES File
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Visrr us ON THE INTERNET @ hftp-//h2o.enr.state.ne.us/NPDES
919 733-5083, extension 511 (fax) 919 733-0719
e-mail: [e-mail]

NPDESPe
Paw Crt
Meckler
The followinpr item.,, are RFOI TTRFD fear
sucn
U An,.
SOHc
plan
origi
The fo'
proces
Industri,,
Regulari
Priorit)r .
The as
domo
IECLI aLIVA LVV'V
it NCO021962
Terminal
xg County
enewal Dacknes:
.. 1
)y attached),
warea AAerbackwash, etc.)
PLEASE NOTE:
Due to a change in fees effective January 1, 1999, there is no renewal fee' required with your
application package.
Send the completed renewal package to:
Mr. Charles H. Weaver, Jr.
NC DE / Water Quality/ NPDE S Unit
1617 Mail Service Center
Raleigh, NC, 27699-1617

SOC PRIORITY PROJECT: Yes— No_X
To: Permits and iEngineering Unit
Water Quality Section
Attention: Cam" Bryant
Date: March 4, 2005
NPIDES STAFF REPORT AND RECOMMENDATION
Co3r. Mecklenburg
MRO No. 05-
Pe rmit No. NCO021962
PART I - GENERAL INFORMATION
1. Facility and Address: Citgo Petroleum Corporation
7600 Mt. Holly Road
Paw Creek, N.C. 28214
2. Date of Investigation. 02-28-05
3. Report Prepared By. Samar Bou-Ghazale, Env. Engineer 1
4. Per Contacted and Telephone Number: Mr. Jim, Utke, Ternunal Manager, to
[phone].
Kenstead Circle in the Paw Creek Community.
6. Discharge Point(s). List for all discharge points:
Latitude: 35* 16 52" Longitude: 80* 56'02ft
Attach all.S.G.S. map extract and indicate treatment facility site and dischargepoint onmap.
USGS Quad No.: F 15 SW USGS Quad Name: Mountain Island Lake
7. Site size and expansion arc consistent with application?
Yes X No— If No, explain:
8. Topography (relationship to flood plain included): Sloping at the to of I to 2%. The site is
not located in a flood plain.
9. Location of nearest dwelling: The nearest dwelling is approximately 500 feet from the site.

1 a. Receiving sftm or affected surfitce waters: Unnamed Tributary to Gum Branch.
a.Classification: WS IV
b. River Basin Sub in No.. Catawba; 03-08-34
C. Describe receiving s and pertinent downstream s. The receiving
is a wet weather ditch tributary to Gum Branch.
PART H - DESCRIEPTION OF DISCHARGE AND TREATMENT WORKS
1. a. Volume of wastewater to be permitted: The discharge from
treatment system has been ceased. The storniwater flow is not limited.
b. What is the current permitted capacity of the wastewater treatment ` ? N/A.
c. Actual treatment capacity ofthe current facility (current design capacity)?N/A.
CL Date(s) d construction activities allowed by previous Authorizations to Construct
issued in the previous two years: /A
e. Please provide a description of existing or substantially constructed wastewater
treatment y product spills from loading rack are stored a
holding for offsite disposal. Stormwater from the site is discharged into a
dike constructed around the tank firin through. outfall 001 (Please note that there
is no detention pond at the facility)
f. Please provide a description of proposed wastewater treatment facilities: N/A
g. Possible toxic to surfacewaters: Due to nature of the wastewater
could be some toxicity concem
IL Pretreatinent Pro (POTWs only):N/A.
2Residuals`' utilization/disposal scheme: The waste collected 'in the holdmg
tank and bottom in the tank farm are pumped and hauled by US Filter
Commy, teI -800 535-9694.
3. Treatment plant c ifii `on: Class I
4. SIC Cod(s). 5171
Primary: 39 Secondary: 73
Main Treatment Unit ' Code: 53000
Page

PART M - OTHER PERTINENT O ,ATIQN
1. Is this facility being constructed withConstruction Grant Funds or are any public monies
involved (municipals only)? NIA-
1 Special - cn ` or limitations (including to i it requests: N/A
3, important SQC, JOC or Compliance Schedule es: (please indicate) NIA.
4. Alternative Analysis ' Evahatiow. Has the facility evaluated all of the non -discharge
options available. Please provide regional perspective for each option ed.
esrcm',rA *%^ Ts*m1mPr ,."f at flits tuns-, to P- higtP sdtt-rnntivE'+a i nr-- the fAcilitv is nnt t2
RATIONS
from 1 0 12/2004, revealed no vialatio
It is recommended that the NPDES permit be renewed.
S" ofRepv P
Water ioSupervisor
1Jatd
'age 3

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Jan
Scutt Eaton
CA Petroleum
3877 Flowers d.
Doraville, Georgia 30360
Dear Mr Ea)
Michael
Williani G. Rw.
of Envittonwat and NA
Alan Wa Klima
Division of
..
'j
11, 2005
NPDES Pennit k 000219 6
Citgo Petroleum 'Ier al-Chadotte
Mecklenburg ty
If have any additionalconcerning renewal of the subjectt, please t me at
extension 520.
Sincerely,
C,arolyyn Bryant
Paint Source Bmach
ee. CEN1
Nodh CarolinaDivision ofWater Quality 1617 MAd Sarvice Catter Ralci* NC 276 -1617 (919) 7- 15 Oxitorner Seivice
Int 1; t o state c. 512 N. i. r Raleigh, NC 27604 FAX [phone]-6` 4

December 16, 2004
Mr. Charles Weaver
North Carolina DENR
NPDES Unit
1617 Mail Service Center
Raleigh, NC. 27699-1617
Ar. Weaver,
3tions.
I ndFIK YVU IVI YVUI 01-tClItIVII It' U11-7 IIIL4uu�-&
ons, please call me at 770-458-8322.
tly,
Eaton
tanager, CITGO Petroleum
2004

NPDFS PERAUT APPLICATION - SHORT FORM - 'tract "ng
For manufacturing or commercial facilities with a discharge <1 MGD
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 2 7'6'9►9-161 '
http://h2o.enr.state.nc.us/NPDES/
NPDES Permit Number
Please print or type
1. Contact Information:
Facility Name +
Owner Name
Street Address
L,
city
State / Zip Cade
Telephone Number (" )
Fax Number ( C )
e-mail Address t t ¢ x
Operator Name fith o-rKa- i - c
Street .Address [. � {
4. P YP`
k.
city
State /;Zip Carle "i 7 t to 9
County ,
Telephone Number (e tl
2. Location of facility producing discharge:
Check here if same as above ED
Facility Name (If different from above)
Street Address or State Road
city
State / Zip Cade
County
3. Ownership Status:
Federal State Private M Public E
4. Standard Industrial Classification (SIC) cod (). l -7
S. Number of a ployee. _13-
6. Principal product(s) produced. 0C ("
Principal raw 'material(s) consumed:-- 4) �
`?. Principal pros ss(es); i t f C 1 7-lox) r�
Page i of 3 Version -0810

9. C
Jrruai
July
i
A
it
.l4AU9.;L K'A4RUU%;C;U VS. 1%,aW 1VAd44'K14A A"A4Ji u
Consumed
(AVERAGE)
February March April May;
August September October Nover
,er week discharge occurs: C
i� ■
June
December
Ittpte industrial proce,,
11. List all permits, construction approvals and/or applications (check all
numbers or check none if not applicable).
e Permit Number
e F
El None
Non -Attainment
UIC
Ocean Dumping
NPI)ES-tr
Dred of Fill Pe .ts--
P aU
RCRA
NESHAPS
Other
AV
Page 2 of
cG s:
r
RATING MCA 1i)
tat apply and provide permit
-it Number
i !� 52 i
Version -0810

NPDES PERAUT APPLICATION - SHORT FORM C-Manufacturing
For manufacturing or commercial facilities with a discharge. <1 MGD
12. Number of separate discharge points:
13. Name of receiving stream(s) (Provide a map showing the exact location of each ou(fall, including
latitude and longitude)-.
7-6
14. Do you add any chemicals that may be discharged? (Please list and explain source and
potential amounts.)
15. Is this facility located on Native American lands? (check one)
r--"-n
)rF,s L—J NO EE
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
77- EATNO M"467,6:pe,
rated name of Person signin g- Title
2-116 /,0 V
Signature f App ica t Ddte'
North Carol' )AGeneral Stat 143-21 &6 (b)(2) provides that: Any person who knowingly makes any false statement representation, or certification in any
provides a punishment by a fine of not more than $10,000 or imprisonment not more than 5 years, or both, for a similar offense.)
Page 3 of 3 Version -08103

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ui REFERENCE: CITGO PETROLEUM CORPORATION
r DRAWING NUMBER 147-100-E
tu DATED 9t4t 7.
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REVISION DATED 3/22191,
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Notice of Incomplete Discharge Monitoring Report
PermitNumber: t 'Cl
acuity:
'.aunty:
►MR Month and Year:
following reasons) (Please see the highlighted areas on the attached DMRfor
details.)
The written values are illegible.
The Average, Maximum, and/or the Minimum data paints have been emitted.
Ll The Units of Measure have been omitted or are incorrect.
LJ The DMR Parameter {odes have been omitted.
Other:
o
a
a

Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P. E. Director
Division of Water Quality
.Dater December 15, 2005
OFRCE
James Utke
7600 Mount Holy Rd
Charlotte, NC 28214 600'
Subject: Notice of Incomplete Discharge Monitoring Report NCO021962
Dear Permittee:
The purpose of this letter is to call your attention to problems with the recent submittal of the Discharge
Monitoring, Report (DMR) from' your facility. As you may know, the data recorded on your DMR is keyed
into the Division's database. Our data entry staff has informed me of problems with your recent DMRi
submittal. Until these problems have been corrected, your DMR will be considered incomplete. Please
see the attached form along with a copy of the problem DMR for details regarding the DMR's deficiency.
Incomplete or illegible DMRs affect our staff's ability to provide a timely and effective evaluation of DMR
submittals. Please be aware that until the Division receives a corrected DMR, you may be considered
noncompliant with your NPDES permit and I5A NCAC 02B .050E, and you may be subject to further
enforcement action. Please take the necessary steps to correct the problems and submit two copies of the
amended DMR within fifteen (15) days of the date of this letter to the following address:
Attention: Michele Phillips
Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Future DMR submittals with the same or similar problems will be unacceptable. If you have any questions
about the proper completion of DMRs, please contact Michele Phillips at 919-733-5083 Ext. 534. Thank
you for your assistance in this matter.
Sincerely;
Michele Phillips',
cc:
Central Files
Noa� h�arolina
FtlWlfl'ldy
M C, Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Phone: [phone] Customer Service
Internet: ftp://h2o.enr.state.no.us 512 N, Salisbury St. Raleigh, NC 27604 Fax: [phone]
An Equal Opportunity/Affirmative Action Employer

,t.,tk-
W A Michael
William G. Ross Jr. secretary
P North Carolina Departn=t of Euviroan ewn and Natural Resources
Alan W. KlfiP. E. Dinatir
Division ofWater Quality
Coleen H. Sullins, Deputy Director
Division of Water Quality
June 2, 2003
. James Utke, Terminal Manager
CITGO Petroleum Corporation
Post Office Box 58
Paw Creek, NC 28130
SUBJECT: Compliance Evaluation Inspection
CITGO Petroleum Corporation -Charlotte Terminal
.DES Permit No. NCO021962
Mecklenburg County, NC
Dear Mr. Utke.'
Can May 18, 2004, Ms. Crystal Taylor of the Mecklenburg County Water Quality
Program conducted an inspection at the subject facility. This inspection was conducted as part of
a cooperative working agreement between Mecklenburg County and the Division of Water
Quality. The enclosed report should be self-explanatory.
If you have any questions concerning this report or any other matters, please do not
hesitate to call Mr. Richard Bridgeman or me at 704/663-1 99.
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Enclosure
Rusty Rqzzelle, MC WQP
IRCxlcat
Fite_WQ 0021961504
Ore
�rtttc tins
Q t`tt l FF7ivisian of ty, lie Re i 919 N it vi1Te NC 28115 [phone] Customer Service.
l-s° .623-6748

K vary s United States Environmental Protection Agency, Washington ,IBC 20460 Form Approved
Aft
ICES Compliance Inspection Report O No. 2040-0003
No Carolina Department of Environment and Natural ResourcesA Approval Expires
AP
Division of Water Quality, Mooresville Regional Office NCDENK 7/31/85
Section A:.Wationl Data System Coding
Transaction Code NPDES Permit No. Y O/DAY Inspection Type Inspector Facility Type
N 5 NC0196 04/05/18 C C 2
Remarks:
Inspector: Mecklenburg Ccaun Water Qua1i Pro anz
Inspection Work Days Facility Self -Monitoring Evaluation Rating BI QA .........Reserved ........:..
03 3 N N
a. , ' ; a„", n.... x x
Entry Time:
Permit Effective Date: s
Name and Location of Facility Inspected:
1:1Opm
September 1, 2001
Cit o Petroleum Corporation,
Exit Time.
7600 Mount Holly Road
2: 0pin
Permit Expiration Date:
Charlotte, North Carolina
Date:
June 30, 2005
05/18/04
Name(s) of inn -Site Representatives Tales) Phone
No(s).:
Mr. James Ute / Terminal Manager / (704) 32-323
Name and Address of Responsible Official:
Tale:
James Utke
Terminal Manager
Citgo Petroleum Corporation
hone No.
Contacted°?
P.O. Box 58
Charlotte,No Carolina 28130
:(704)9-326
Yes
Section C
s<EM�alaated ICtttrm '"spew on
-PennitZ
2
Flow Measurement
Z Operations & Mainten ce
Sewer Overflow
Records/Reports Z Self -Monitoring Program
jl Sludge Handling/Disposal
[ Pollution Prevention
Z Facility Site Review ® Compliance Schedules
Pretreatment Program
El Multimedia
ZEffluent/Receiving Waters Laboratory
Sto water
F-1 other -
All areas are rated satisfactory unless otherwise indicated, See Attached Sheet(s) for Summary
Signature(s) of Inspector(s): Agency/Office/Telephone: hate.
Crystal Taylor MCWQP/[phone] May 21, 2004
Signature of Reviewer: Agency/Office Date:
EPA;Form 3560-3 (Revised3-85) Previous Editions are Obsolete

GENERAL:
The facility was last inspected on May 20, 2003 by lbs. Crystal Taylor ofthe
Mecklenburg County Water Quality Program (MCWQP). A Compliance Evaluation Inspection
Report was issued on June 10, 2003.
PERMIT:
e current permit became effective on September 1 2001, and expires on June 30, 2005.
The it authorizes the discharge of storm ter/ e ter from Out all 001.
e portion of the facility associated with the :l E treatment works consists of an
oil/water separator, an equalization tank, a second oil/water separator, a diffused aeration system,
and a detention pond with an underflow siphon'.
The current permit properly describes the facility d appears adequate for the waste
stream being treated.
RECORDS/REPORTS:
Discharge Monitoring Reports (D d laboratory analytical reports were reviewed
for the period November 2002 through March 2004. The reports appeared to be properly
completed. All data, reports, operational logs, and manifests were readily available at the
facility. The records were clear, organized, and well maintained; no discrepancies were noted.
FACILITY SITE REVIEW:
The runoff from the covered fueling rack and manifold areas flows through two oil/water
separators, an equalization tank, an air stripper, two carbon filters, then flaws to a holding tank.
The facility contracts US Filter, Inc. to haul the fueling rack wastewater from the holding tank
off -site for treatment and disposal. All of the NPDES treatment works for this waste stream
remain intact at the facility.
The storm water collected in the aboveground storage containment basins is visually
inspected d can be manually released through Outfall 001.If deemed necessary, this storm
water can be routed through an oil/water for prior to discharge at Outfall 001. The facility
has ailed a spray irrigation system (Permit No. WQ0019911) to discharge the storm ter
from the aboveground storage tank containment basin. The spray .irrigation system has been in
operation since February2002.
Any product collected by the oil/water separators is transferred to a holding tank and
eventually hauled tiff -site by US Filter, Inc..
All of the major components of the facility treatment works were in service and appeared
o be operating properly at the time of the inspection.
FLOW MEASURENWNT:
Flow measurement is accomplished by multiplying the known flow rate from the
discharge pipe by the discharge duration. Based on the current permit, this is an acceptable fltr
measurement method.

LABORATORY:
Chemical analysis of effluent samples was performed by Severn Trent Laboratories, (NC
Laboratory Certification #395). Severn, Trent Laboratory was not evaluated under this
inspection.
EFTLUEITT /RECEIVING WATERS.-
Outfidl 001 consists of a riprap-lined ditch, which flows to an unnamed tributary to Gum
Branch, which is a Class WS-lV water in the Catawba River Basin. The facility was not
discharging at the time of the inspection.
'SELF-MONTTORING PROGRAM.-
ng this period, except as follows:
transportation techniques appear adequate.
OPERATIONS & MAINTENANCE:
The facility and site appeared well operated and maintained.

WN4 A
411 �Itr�xs Nord
Alan W. Klimek,
December 10, 20
CERTHIED MAIL CM # 70012510 0004 8287
RETURN RECEITT REQUESTED
Mr. Scott Eaton
Southeast Environmental and Safety Manager
Citgo Petroleum Corp.
P.O. Box 47427
Doravik Georgia 30362
Subject: Notice of Violatil
Paw Creek Termi
NPDES Permit N
NOV-2003-LV-0
Mecklenburg Cot
Dear Mr. Eaton:
6
3684
,2
Division of
Cotten H. Sullins, D
Division of
me at 704i663-1699.'
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
cc: Point Source Compliance/Enforcement Unit
RMB
Mooresville Regional Office, 919 North Main Street,'Mooresville, North Carolina 28115
Phone [phone] Customer Service
Fax [phone]

FAk
3877 Flowers Rd.
Doraville, Ga. 3036
June 1, 2003
r. Richard Bridgeman tjCWT.
NATURALAND RFSOURCES
Water Quality t Fn z,T , RN14 ,�., C,
Mooresville Regional Office�
919 North Main St.
Mooresville, N.C. 2811.5 JUN 1
. Rusty Rozzelle
MCWQP
700 North Tryon St.y1i
Suite 20 __ WATER IJ
U SECTION
Charlotte, N.C. 28202
Mel Rechtman
4 WIC-E 11 `' Floor
U.S. EPA Region 4
61 Forsyth. St. SW
Atlanta, Ga.3003-8960
:Dear Sirs,
Please find the enclosed response to the notice of violation issued recently in
connection with the release of petroleum at the CITGO Petroleum Corp. in Charlotte,
N.C. on April 21, 2003. We at CITGO Petroleum deeply regret the release of petroleum
to the environment, but once the release occurred, we spared no effort to mitigate the
possible environmental damage. I have instructed S&ME Inc. to document CIT 's
response to the release and I have enclosed their report,
Sincerely,
.,.
Scott Eaton
E,&H Manager; Southeast Region

A
ARL,
MOORES �
F",
t.
June 11 `h, 2003
CITGO Petroleum Corporation
Past Office Box 47427
Doraville, Georgia 3036
ATTENTION: Mr. Scott Eaten
Reference: POST SPILL RECOVERY OBSERVATIONS
CITGO Petroleum Corporation
Charlotte, North Carolina
S&ME Project 14-90-295
Dear Mr. Eaton:
On June OS'`, 2003 Mr. David Klemni of S&N1E met with Mr. Jim Utke of CITGO Petroleum
Corporation to observe the post cleanup efforts from the ,April 21', 2003 PCW tank overfill. Mr.
Utke escorted Mr. Klemm to the areas where the cleanup effort had been conducted. These included
observing the location of the original release, walking the drainage feature through a wooded area
and onto the Colonial Pipeline property, and observing the areas where underfloor dams had been
constructed and absorbent booms had been deployed. Photographs were taken to document the
cleanup effort. The photographs were taken as close as possible to the previous photographs taken
during the cleanup effort. A copy of the photographs are attached.
The general observation of the cleanup was very good. There was no remaining visible flowing sheen
on the water surface, the unerflow dams had been removed and the areas re -seeded with grass, and
the absorbent booms and pads had been removed and disposed. A key observation in the stream on
the Colonial Pipeline property was the existence of aquatic life including multiple schools of small
minnows, tadpoles and frogs, and small bluegill sunfish.
S E, Inc. [phone]
155 Tradd Street [phone] fax
Spartanburg, South Carolina 29301 [phone] Greenville www.sfneinc.com

Post Spill Recovery Observations S& - Project 1264-90-29
CITGO Petroleum Corporation June 2003
The details of the release and disposition of the recovered materials are as follows:
I . Approximately 83 5 gallons of mixed gasoline/diesel fuel was released from a Process Contact
Water P ) tank on April 21, 2003. The fuel mixture entered a drainage feature which
flowed to an unnamed tributary of Gum Branch. Gum Branch was not affected by the
release. The 835 ,gallon estimate should represent a fair approximation of the release as it was
contained within the unnamed tributary, Virtually all the product was recovered utilizing
absorbent pads and vacuum trucks with the aid of flushing the drainage ditch and creek with
uncontaminated stormwater stored in the onsite containment area.
Disposal of the recovered crater and fuel was manifested by HAZ-MAT Transportation and
Disposal of Charlotte, North Carolina. The manifests indicate disposal of a total of 885
gallons of water and product of which 835 gallons were reported as product. A total of
drums of absorbent pads and booms were manifested for disposal by A&D'Environmental of
High Point, North Carolina.
. The spilled occurred on April 21", 2003 and was discovered at approximately 4:00 PM.
Recovery efforts were initiated immediately and were completed by the afternoon of April
3 The cause of the spill was an overfilled PW tank.
. The spill entered a drainage ditch and flowed to an unnamed tributary of Gum Branch on the
adjacent Colonial Pipeline Company property. The release was contained within the unnamed
tributary and did not affect Gum Branch. Gum Branch eventually flows to the Catawba
River.
. A Site Location :Map is attached as Figure 1 which indicates the location of the CITGO and
Colonial properties and the affected unnamed tributary.
A Site Plan is attached. as Figure 2.
7. The extent of the spill is indicated on the attached Figure 2.
8. Photographs taken during both during the cleanup effort, as well as following cleanup are
included.
2

Post Spill Recovery Observations S&NM Project 1 64-90- 95
CITGO Petroleum Corporation June 2003
We appreciate the opportunity to be of service to CIT O Petroleum Corporation . If you have any
questions regarding this information, please do not hesitate to call.
Sincerely;
SME, INC.
k °wMa
David E. Memm, P.G. Robert Hall, P.E.
Project Manager Senior Environmental Engineer
D. Rex Gleason; Water Quality Supervisor, NCDENR
Rusty Ro elle, MCW+Q
Mel Rechtman, USEPA Region
Env03/649095/Sp ll Response/Post Observations
3

Post Spill Recovery Observations S&NE Project 1264- 0-295
CIT O Petroleum Corporation June 2003
PHOTOGRAPHS TAKEN r DURING
CLEANUPEFFORTS
4

9

m
m

c�
m: � ,gym ��•a� �, a, 4a..�. ,. �.r .,x,. :c�� ��,u, ,. �. ""W.���r�%,,�.�a r.3 .�.'� :�.;��,,�?�:�a,. �., �_'��,�.� �., a,., � .i�. sk`,�a '�.„
N

Post Spill recovery Observations
CITGO Petroleum Corporation
1

9

Post Spill Recovery Observations
CTTGO Petroleum Corporation
I
S&ME Project 1264-90-2 5
June 2003

Post Spill Recovery Observations
iTGO Petroleum Corporation
Im

12

L Post Spill Recovery Observations S& Project 1264-90-295
CITGO Petroleum Corporation June 2003
PHOTOGRAPHS
TAKEN FOLLOWING CLEANUP
EFFORTS
1

Post Spill Recovery Observations
CITGO Petroleum Corporation
lei
S&Nffi Project 12 4-90-295
June 2003

IN

"N

UNDERFLOW
ESTIMATED EXTENT DAM #
OF SPILL
UNCERFLOW
DAM #1
low
MA
0 0
�' PClINT t)F RELEASES �.- -
*•,
c
NOTE
REFERENCE, CITCO PETROLEUM CORPORATION c a
DRAWING NUMBER 147-140--E
DATED 9/4 57, REVISION DATED Rc /91
q7
NVtFkENQlNfiANiENNO
VJ a
COLONIAL PIPELINE COMPANY
DRAWING NUMBER 7-CHA-P2, DATED 5-87 SITE PLAN
CITGCI PETRMEUM CORPORATION
CHARLOTTE, NORTH CAROLINA
JOB NO' 164-90 295 DATE: 06•-10 -03 nQURE No:

Manifest Document No.
filal Se rV1"ces.. Ina Page i j
MJ}NIFEST i
{ EMERGENCY HONE NO. OFFICE BOX 484 TEL [phone]
' } ti ,} 34- 7i50 N GH POINT,, NC 27262 FAX (336) 43 -7? 2
GENERATOR INFORMATION
USEPA iC
Street Address Mailing Address Tone NVC016
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®, N,C 28237
PO. No.
i
:1�4L WASTE Job . 's
GENERATOR LOCATION - WORK CONTRACTED BY
NAME117
Bill To (If different from information at left)
ORIGINATINGApDREss' E I c IC MAILING ADDRESS ADDRESS 1 (
STATE " ZIP CITY 4______ST
ATE ZBP
PHONE NO, PHONE NO.
CONTACT NAME CONTACT NAME
DES. OF WASTE. '
No. ype tlracts
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Physical *a # N 4
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b. Maiing Address. P.O. Box 37392
t�harlotte N C 57
ORIGINAL , FINAL T4.0. * YEL1
'pvrcv aaa..rcuaca tur Pavvw uaafrvam. maataacat atauucau"wm us wayvmr a
RATOR

HAZ-MAT 16097
TRANSPORTATION AND DISPOSAL Manifest No.
P O. BOX 37392 - CHARLOTTE, N.C. 28237
1-704 332-5600
FAX (7M) 375-7183
NON -HAZARDOUS SPECIAL WASTE Job N.
77
.......... .......... ..........
GENERATOR LOCATION WORK CONTRACTED BY
NAME6Bill To (if different from information at left)
F7 t
ORIGINATING ADDRESS NAME
zc:I
ol-001
MAILING ADDRESS ADDRESS —talDc
CIT)4�ST ATE ZIP CITY'"T ATE ZIP
PHONE NO. PHONE NO.
CONTACT NAME CONTACT NAME
DES, OF WASTE: 7—'
>No. Mype nits uanttly
NO-
7�LLONF_,
QUANTITY
I WATER, OIL & COOLANT PUMPED FROM TANKS OR DRUMS LINE TOTAL
Z. OFF SPEC LIGHT OIL, WATER & GAS PUMPED FROM TANKS OR DRUMS
1 55 GALLON DRUMS REMOVED - SOLID
455 GALLON DRUMS REMOVED - UQUO
S. .472 'a 7
9. ARRiVALTIME.
�o. DEPARTURE TIME: 100 AWL
GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been properly
described, classified and packaged, and is in proper condition for transportation according to applicable regulations, AND, if the waste is a treatment residue of a previously restricte(
hazardous waste subject to the Land Dis oral Restrictions, I certify a we t4riat the waste has been treated in accordance with the requirements of 40 CFR Part 268 and is no longs
a hazardous waste as defined by 40 art .
. .. ... ...... J A
GeneratorI Atpofef! �Lnf Na e Signature -Shipment CIaFe
TRANSPORTER
T
El� PORTIERAW,
H A AZ - TRANSPORTER 11 MAT
TRANSPORTATION AND DISPOSAL e. Name
R O� BOX 37392 - CHARLOTTE, N.G. 28237
f. Address --
a. Driver 'Name Title t4,4
g. Driver Name / Title
5we
b. Phone N c. Truck No. A44, F-1 1 h, Phone Na. L Truck No,
Hazardous Waste Transporter Permits 1, Transporter 11 Permit Nos.
::SPAN 1111111
E 6
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104,814
d F
Shnnent D Driver Signature Date
MLT'log-,
ME MISP
Site Name: hU:_MAL'fir An%;lp �i �J �11 n a. Phone No. 704-332-5600
Physical Address: ZIP_aWJQa Avenue b, Maiing Address: Ro. Box 31M
Qh&r1QA%_N_Q, _Z8237
e. Discrepancy Indicallion Space
This is to ceddy that all non-huardous material removed from above location has been rectived and will be disposed of in accordance with applicable local, state and federal regulations in the following manner: (1) Petroleum products
are blended Into a beneficial reusable fuel for use in large industrial burners. (2) Waste waters are to be treated with polymers, PH adjusters, and a floccutant, then flows through a dissolved air flotation system for pretreatment separation,
then into the CMUD sanitation sewer system under Permit ILIP15012. (3) Sludges from treatment systems are hauled to EPA approved facilities for proper disposal. Manifest and certificate of disposal are On file,
(4) Out treatment system operates on a flortm, filcoput a is and product should be processed within seven days,
SIGNATURE Ott FACILITY FF!2ffiQ� DATE
ORIGINAL - FINAL Y.S,6. - YELLOW - OrSfll . PINK - ISTTSA - GOLO - GENERATOR

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,Z-MAT TION AND DISPOSAL Manifest No.
I CHARLOTrE, N.C. 28237
432-5
600PO. No.
375-7183 Job No,o,3
OUS SPECIAL WASTE
SM. TANKS OWDRUMS
-D-S-OD
frictions, I certify and warrant that the waste has been treated in accordance with the requirerner
lame Signature
and 004 Should be Promssed 44thin seven days.
NMI
MORE=
a. Phone No.
b, Maiing Address: aQ_Bkx 3719
2
Charlotte. N.Q._a&E
lilies for proper disposal, Manifest and certificate of disposal are on fill

AID DISPOSAL
IAT Manifest No. 16080
ZLOTT , N.C, 28237 5600 P.O. No.
-7 i 3
Job No. '
PECIAL WASTE
3R L AT! WORK. CONTRACTED BY
z:
Bill To (if different from information a
,IC ADDRESS � � NAME
)DRESS ADDRESS
STATE —ZIP CITY
PHONE NO,
aAME c= NAME
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N PORTER t!
TRANSPORTATION AND DISPOSAL e. Name `
P. C. BOX 37392 CHARLOTTE, N.C, 28237 f. Address' �
r Name 1 Tide - `` g. Driver Name / Title
N0 ``L ` `' ` c. Truck No, h. Phone No. I. Truck No.
rus Waste Transporter Permits I. Transporter II Permit Nos.
D048461310
et Sianatura Shiment Date Driver Signature irnent Date
a

CITGO Petroleum
Richard Bridgeman
Division of Water Quality
919 North Main Street
Mooresville, NC 2811
CITGO
1P.0, Box 5
Paw Creek, NC 28 130
June 25, 2003
Ih
This letter is in response to the Notice. of Violation that CITGO received regarding the NPDES
inspection by Crystal 'Taylor on May 20, 2003. According to the Self -Monitoring section of the NOV,
there were three exceptions listed as deficient.
As a background reference, CITGO received a spray irrigation permit number WQ0019911 dated
January 7, 2002 to discharge tank farm storm water through a spray irrigation process. The intention of this
system and permit was to completely eliminate any discharges through the existing NPDES outfall; permit
number NC0021962. The issuance of the spray irrigation permit was expected during the latter part of
2001 but was not received until January of 2002. We did not anticipate any NPDES discharges in 2002,
Because of the delay in issuance, it was necessary to discharge through the NPDES systern for two days in
January. At the time, all normal monthly discharge parameters were sampled as per permit requirements.
Unfortunately, the annual requirement for acute toxicity was not taken.
• The Division of Water Quality has already issued a Notice of Violation regarding the Toxicity
requirement. We discussed this situation with Mr. Kevin Bowden, and Mr. Jimmy Overton issued
the NOV dated May 30, 2003. 1 have enclosed a copy for your review.
• The MTBE was properly sampled during January, but was not included on the January report. The
level was non -detect and I have included a copy of the lab report for your review and
consideration.
• There was an ETA method 624/625 sample taken for the spray irrigation permit in June of 2002.
This sampling is from the exact same strearn as the NPDES permit and was reported as required
for the spray irrigation permit. I have included a copy for your review and consideration,
As you can see by the documentation we have provided, the only item required by the NPDES
permit that we failed to provide the agency was the toxicity test for 2002. In past years the toxicity test has
always been within state standards, and we have no reason to believe it would not have been within
standards during our one time discharge in 2002. Our failure to take this one sample does not represent any
willful intent on our part to circumvent the sampling and reporting requirements of our permit_
Thanks again,
� P
im Utke
cc: Rusty Rozzelle, MCWQ
Scott Eaton, CITGO Petroleum

Michael F. Easley
(} t; Governor
William G. Ross, Jr., Secretary
Department of Environment and Natural Resources
t "C Alan W. Klimek, P.E, Director
Division of Water Quality
May 30, 2003
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. Jim Utke
Terininal Manager
P.O. Box 58
Paw Creek, North Carolina 28130
SUBJECT: NOTICE OF VIOLATION
Effluent Toxicity Testing
NPDES Permit No, NC0021962
Citgo — Paw Creek Terminal
Mecklenburg County
Dear Mr, Utke:
This is to inform you that the Environmental Sciences Branch has not received your toxicity self
monitoring report form for the year 2002. This is in violation of Title 15A of the North Carolina Administrative'
Cade, Chapter 2, Subchapter 2B, Section .0506 (a)(1)(A) which states that"monthly monitoring reports shall be
filed no later than 30 days after the end of the reporting period for which the report was made."
Your Discharge Monitoring Report for January 2002 indicates flow, but does not indicate that an acute
toxicity test was conducted during January.
Kevin Bowden from the Aquatic Toxicity Unit contacted; you on 5l1103 to discuss this incident.
Apparently, the facility did not conduct a toxicity test in January 2002 because the facility was anticipating
issuance of a non -discharge permit from the Division of Water Quality. Please be reminded that requirements of
the NPDES Permit are in force until such time that the NPDES Permit is rescinded.
While,our office recognizes that failing to conduct toxicity testing in January 2002 was simply a
misunderstanding, we, must remain consistent in our response to toxicity non -reporting events. You will be
considered noncomphant;with the reporting requirements contained in your NPDES Permit for 2002 until you
make acceptable demonstration to the Environmental Sciences Branch that the report form was submitted to this
office within the required reporting. period, In addition if within the next twelve (12) months, future reports are
not received within the re aired time frame 'you may be assessed a civil malt' ,
The reverse side of thi3'Notice contains a summary of important toxicity monitoring and reporting
requircrnents. Please read this one page summary and it you have any questions concerning this Notice, please
contact Mr. Kevi
owden with the Aquatic Toxicology Unit at [phone].
Sincerely,
�Tnmuerton
Assistant Water Quality Section Chief
For Environmental Sciences
cc: Rex Gleason- Mooresville Regional Office
John Lesley- Mooresville Regional Office
Kim Colson/Non-Discharge Permitting Unit
Aquatic Toxicology Unit Files
Central Files
Customer Service Environmental Sciences Branch
800 623-7748
1621 Mail Service Center Raleigh, NC 27699-1621
[phone]

6y !
900 Lakeside Drive • Mobile, AL 36693 • Tel: 253 Err, 6�13 < Fax: [phone] • wwwr,stl-inc.com
STL Mobile
LOG NO- M2-;0820
Received: 01 FEB 0
Reported: 11 FEB 0
Mr. Scott Eaton
CITOO Petroleum Corporation
Client PO. No.; 45001.87170
P.O. Box 47427
Doraville, GA 30362
CC:- Mr. Rob Durham
Project. Charlotte - Monthly,NPDES
Sampled By: Client
Cade: 163020212
! } REPORT OF RESULTS
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID ,SAMPLES
TIME SAMPLED
Discharge--- __-_____-
0820-1___ Stormwater-----------Discharge---------------------------------------
__aY;z
".
PARAMETER
20820-1
Volatiles in TCLP Extract
----
Benzene, ug/1
<1.
Ethylbenzene; ug/1
<1.0
Toluene, ug/1
2.0
ylenes, ug/1
c2.0
WoY
a ysas Date
02.05.02
y�
Analysis Time
23:19
Analyst
PV
Suspended Solids (1.60.2), mg/1
2
Analysis Date
02.03.0
Analysis Time
% 13.34
Analyst
Ui
Total Recoverable Phenolics (420.1.)
Phenolics, Total Recoverable, mg/l
c0.010
Analysis Date
02.04.02
Analysis Time
09:00
Analyst
AH
Oil and Crease - HEM (1664A)
n-hexane extractable material (HEM), mg/l
<5.0
Analysis Date
02.04.0
Analysis Time
08:10
Analyst`
SS
STL Mobile is a part of Severn Trent Laboratories, Inc.

900 Lakeside Drive • Mobile, AL 36693 • Tel: [phone] • Fax: [phone] • www stl-inc.com
STL Mobile
iaOG NO: M2.20820
Received: 01 FEB 02
Reported; 11 FEB 02
Mr. Scott Eaton
°
CITGO'Petroleum Corporation
Client PO. No.: 4500187170
P.O. Box 47427
Doraville, GA 30362
CC:- Mr. Rob Durham
Projects Charlotte - Monthly NPDES
Sampled By: Client
Code. 163020212
1 REPORT OF RESULTS
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
TIME SAMPLED
208 0-1 Stormwater Discharge
01-25-0 /09:00
PARAMETER
20820-1
pH '(EPA 1.50.1)
----------
pH , UNITS _s
7.2
Analysis Date
02.04-.02
Analysis Time
09:10
Analyst
RS
Turbidity (180.1), NTU
29
Analysis Date
02.01-.02
Analysis Time
16:43
Analyst
dp
REFERENCE: EPA 40 CFR Part 16
STL Mobile's North Carolina Certification No.
3�5.
STL Mobile is a part of Severn Trent Laboratories; Inc:

a a
do tktva + , A!. « Ted 39 65d 63 Fsx 34 6 • wwwstl inc.easn M
obos
Loa Ni M2-24815
Asceivadt 29 J= 0
Mr. Scott Eaton
CI ketrole= corporation client M No.:48t301E371Tt7
P.O. SCx 47427
Doraville, GA 30362
CC: Mr. DOLV d XIeMM�rc��€�c't� xlot - tp star/1�64 sampled By: Client'
Code; 09402071.1
pop-T OF RBSTJLTS page ?
.._
----------
---------- -----------__- ----_- ----_-
4tIS-1
volatile Organic compounds
Acrolein (Pro ) , "uq/1 <20
ry'jitx=le, /I < t
Benz/11, CI
t'Z1�3,
Bromoforn, /1 1.0
Bros e (methyl b e) r t9/1 <1.0
Carbon tetracb1orid , /1 1.0
ChIcrobeazene, ugli '41. 0
Chloroeethaxm' us/1 41..0
2-chloroethylvinyl ether, ugli 'e25
o fr rcn, u7/1 1.0
C1210roweth=e (Metbyl chloride), u5/1 1.0
Dibrvmachl. s, /l <1..0
i, 4-1ichlc# use , v/1 <1. 0
Dicb1orobromomethaAft, ug/3
1., ..Dichloroet tat gr/1 �..0
1 1-Ili o thane, / a 1.
aig-1,-Dichloroetbene, tag/l <1..0
trans- 1, 2-7.lchlorce a u9/1 'el.i
cis-1, 3 DiC13lo r0V e, ugr/1 < . 0
1
a s n----------
cnunNiawsirtartnfnNnqNvlxvds 31 MR WVWH TOOT ff inr

'
� ,r
goo a Drh* • Mobile, AL 3 3 • U 334 W 6633 • Fes: 3.34 666 6696 • wxw-St r=.cam
&ecei~ved: 29 JUN 02`
Reported; 11 JUL 0
. Scott Eater
CSC Petroleum CO Oratiexx
Chet i. bra.. 5CIt�197� ��
P.O. Box 47427
M aVille, GA 30.362
CC. Mr. David Kl proe rlatte - S t,o=w ter f 64- 90- .95
S led BY: Client
Cade. 09492071
gT OF RSA T
Page 2
LOGS NO SAMP.L33 VES :r, vro= SAMPLES
'I P
o
w
-a tester
_ ------------ -
-
24815-1
PARAMSTER
trays-1, 3-iCh l#? 'opXOPOne, /
l
. �}
<1.
leatlaylzr , as.,JJ J°
Methyleno cs'Y IO:Cide. (Di arometh te) , U911
<5. 0
py
J,1, 2, 2.-Tet `0Chl *r t , Ug l
<1. 0
p)
Toluene, u 1l g j
0
q ##ggpp ��rv. q
rp�y
p�
"41.
1,�Cyl esy,. Total, /lp�{
yy 0/�
110
g b
93
Surrogate - Vibromo4lu0-- *
2Oi t
Surrogate - Tol a-d8
0aa
ysiff ate
15.28
Time
d q86 'ON W AIS 0.1 LI 'K of

, AL 93 i s 334 66 33 * Fa 666goo L*r 66 • yvwue c cam e4lobi
LOO go -24815
Received: 29 JM 0
"Ported: 11 JUL 02
. Scott Eaton c1a. aat FCC. No.: 45001071.70
CITGO Petroleum .t
P.O. BOX 47427
r�craVjjle, CA 30362
CC: ter. David Klemm proj t:Cbarlotte - tezmwater/1254-90I 293
Sampled Bar: Clieut
Code: 094820711
REPOPT OF RESMTS Pa5e
LOG No CRIPTJ: , LIOU= SMMMS T
IME qAMPLM
-------------
----------
4g15-»;1 sto '. ter ,».__.-----_---------_---
- .. .. _ -.. - 24 aIS-1
---------- ----------
iVolatile 0rq&Ujc compounds <10
Acenaphtheme, Ug/l <10
Acenaphthyleae-, uV/1 <10
Antbxaceue, usr/1 <80
senzidiva, USA <10
9e o W hra eUa, g-/1 <10
3,4- rca lu0rarLt *, a `/l -CIO
Beo fad +ass , 9/1 10
* (, h, i) Pis 1 e U /1 <10
- aphsz� rlpb s xl ether, UV/3 10
But 'jnzy1ph at, /1 gl
big( - craetbyl)ether, u /l <lt
elo
�E- C+rc7-2- 1.p <1.0
:2-chloronapttthaleftg, U9r/'1 <10
1
4- Or"0 heUY1P reUY1 "bar, 4
/1
ChxysenB, 'tom /1 410
<100
vib z (a h)acs , UgIl <10
Di-n- l , /l <103 , :31-ZA orb idinft, / 1- <10
, 4-X>ichlorop 1, S/1 <10
Die rlph{thal ta, f l

Wo La e, AL 36SS3 * T G 44 6M Fiot334 646 6Ww sN irk camSTL M4we
KOt - 4 15
Reporte6t 11 02
, soott, seton, li t PC. Igo.. 41400157170"
cxTao Pet, 'oievm corporation
P.0 . Box 47427
Doravi:I:Lo, 3036
r. David Xle= project, Charlott~e
swV14d By. Cla t
RnpogT OF RZSMTSRage, 4
- M r n+ r w.F W — tee. +} S 1
' 'hY3.ph lat-e, ugly <50
4, 6-Dini. ' -3- Ylph (4, -�1xxi tr�a-c � a 3 r l 50
, 4-V tr b l r /:L <10
,4-D t tc�lta" e, jl <110
2, 6- trQtC ft, "t1VI <0
Di,-n-o atryipb la , us' l <10
,city
bis ( -S yl yI) Ph1.at 0 , u /1 Io
h ca cl , 1
ugt' <10
H car tada , /1 <
rl A car cyclop t ene usr/3 lO
rj wt e, n911 1
(1, ,3- " ?pY e, / <10
i
0
Naphthalene, ug fl 1
- i ro cal. (0-N1trop l) r 1 <50
4-Si.tx capa
1 (p- t l) , ug/`l 50
y- itrO t1 y3 ixse, a 1.0
j3. Alt}
yxw,

P M
g • goW4l , AL 36693 TeL [phone] Fars AU 666 6696 t ++}}
NO; `24015
Reported; 11 7UL 0
P.O. Box 474,27
u villa, a& 30362
Ct^c low. Davld raem project. �rl�the - �t xf 64� 0- 95
Sampled By; Client
Code: 094 20711
PORE` OF ASSMTSPage
LOG No Lu DESCRIPTION PTI is I9 ., _ _ Tn4S
_ _ SAMPLM
-------------
4SIS-1 Stormwater
- , 2* bis (I~ ohlorogr a) ba t2¢ h1 t x i c rrc Y < t
l)e h 1, ug/ <50
he ' e, /l
phenol, ug/l , •�3 0
Pyranef/l <1
2,4,-TriC.hlargph9nol, sx-'/ 7
Sus ` at. - 2- ixio obighexayl 65
it
Surrogate - phenolw4s 6
surrogate - T6 l-;da4 76
Analya:Ls Date 7 Rx5"i
Analys:La Time
Analyst
Total Suspended Solids (260-2) 3.0
Total suspeudad Sa'i .ds, fl 07.0 . 2
Analysis TiTne S

a, A
Mr. Scutt Eat
czwo Patro-10
3 * 7e4 665 603 • ';W 666 $60 S irt' Sil. ' e
LCO NO! 'M2-24815
Receiv6d a 0
Izaported. JUL 0
Corporation Gist po. No z 4500187170
CCx M .David KIOMM ProJect: Charlotte
Be led BY: Client
Code:
REPORT CAP REMTS
,
DATE/LOG
ITO SAMPIX DRSCRIPTIOX LXOVID SAVMLB$T
IME SA142LED
815-1 Storrs tax
--------- w-------------
-------
Toter e�
coverabl rt �olico (420*1)
0.01
PhanoliCS, Total Recoverable' l
07.02.02
l Si.s Data
10;30
Analysis Time
Analyst
Oil and Greade - E03X ��
see extractable material ( } g
'45 * U
xa-
07. 0 .0
Analysis Time
1w
Analyst
PH (EPA 150.1)
617
06.29.02
Azalywie Date
y
A=alysis Y ime
RVX
rw»- ---I-.-+---------------
�SVMMCSsKpA 40 C VR 'part 136
STL Mobile's North C!Sroliza Certification No.
3 5.

Michael F.
William C, R
June
James Utke, Terminal Manager
CITGO Petroleum Corporation
Post Office Box 58
Paw Creek, NC 28130
SUBJECT: NO'
Con
CIT
NP
Mec
Dear Mr. Utke:
20.
a
VIOLATION
valuation Inspection
o. N0021962
inty, NC
xrz County Water Quality
3pection was conducted as part of
and the Division of Water
hesitate to call Mr. Richard Bridgernan or me at 704/663-1699.
Sincerely,
D. Rex Gleason, P.E.
Water Quality Regional Supervisor
Enclosure;
cc: Rusty Rozzelle, MCWQP
cat
File: WQ 0021961503
Z7nr%,*-
Mooresville Regional Office, 919 North Main Street, Mooresville, NC 28115
'HONE(744) 1M Castor

"'60
inn
nental Protection Agency, Washington, D
,ompliance Inspection Report
rtment of Environment and Natural Resou
liter Quality, Mooresville Regional Office
*
Farm Apprord
OMB No. 2040-0003
Approval Expires
"7/31 /85
*. *
py
* ,
! •. ....... 8 *. • ra
1
• W i %
►..:. ♦ M •i 1.
I
i
!
i *
W W, W W
w
I„ I III I I
�W
EPA Form 3560-3 (Revised 3-85) Previous Editions are Obsolete

for the
COMPI(
facilit3
he facility was last inspected on February 11, 2002 by Ms. Crystal Taylor of the
t"
�RDS/REFORTS:
V SITE REVIEW:
- �nd frothe m abovegro storage tank containment basin. The spray irrigation system has been in
operation since February 2002.
Any product collected by the oil/water separators is transferred to a holding tank mid
eventually hauled off -site by US Filter, Inc.
All of the major components of the facility treatment works were in service and appeared
to be operating properly at the time of the inspection.
YLOW MEASUREMENT:
Flow measurement is accomplished by multiplying the known flow rate from the
discharge pipe by the discharge duration. Based on the current permit, this is an acceptable flow
measurement method.

NZ'
lyh
are be
transp
RATIE
MCEIVING WATERS:
e tion.
LULUb 011 ki) Manure to mannor errment LYA . 4/02.-).
ply monitoring of effluent MTBE during January 2002. This
to monitor effluent MTBE.
eter , with the exception of the parameters listed above,
rtnit requirements. Sample collection, preservation; and
.quate.
CE:
well operated and intained.

May 30.
CERTIFIED MAIL
RE
N CEIPT IIE STEZ3
Jim Utke`-
Terminal Manager
P.J. Box 58
Pavv Creek, North Carolina? 130
SUBJECT: NOTICE OF VIOLATION
Effluent' Toxicity Testing
ICES Permit No. NCO02196'
Citgo -- Paw Creek Terminal
Mecklenburg County
Bear Mr. Utke:
This is to inform you that the Environmental Spier
monitoring report form for the year 2002. This is in violate
Michael F. Easley
Governor
WithamG. Ross Jr., Secretary
Department of Environment and Natural Resources
Alan W. Klimek, F .B., Director
Division of Water {duality s
2003
ces Branch has not received your toxicity self-
n of Title 15A of the North Carolina Administrative
rich states that "monthly monitoring reports shall be
)d for which the report was made."
Your Discharge Monitoring Report for January'-ZU02 tnettcates tdow, out Saes not, acud'.at" malt all `d
toxicity test was conducted during January.
Kevin Bowden from the Aquatic 'Toxicity Unit contacted you on 5/l/03 to discuss this incident.
Ann rrnntly. the facility did not conduct a toxicity test in January 2002 because the facility was anticipating
d GS.�i3 A6L+♦axe. cap n aw.....s.. ...,... _,. _... _ _ s .
contact Mr, Kevin Bowden the Aquatic Toxicology Unit at (9 I ) 733- 136i
Sincerely,
U4:j;��.,
tmnile Overton
Assistant Water Quality Section Chief
For Environmental Sciences
cc:
John Lesley- lvlooresville Regional Office
Kim Colson/Ni'on-Discharge Perrnitting unit
Aquatic Toxicology Unit Files
Central Files
'
NCDENR
Customer Service Environmental Sciences Branch 1621 Mail Service Gunter Raleigh, NC 2 6 9 16 1 (913f 33 2 i
800 623-774

WHOLE EFFLUENT TOXICITY MONITORING AND RI
> The following items are provided in an effort to assist you with identil
testing and reporting information. Please take time to review this informat
all the
about your toxicity testing requirement, please contact Mr. Kevin Bowdet
2136 or another Unit representative at the same number.
> The VgnMittee is responsible for ensuring that toxicity testing is conduct
toxicity report forms are appropriately filed.
> The reporting of whole effluent toxicity testing data is a dual jgqqiLe�,
I —
appropriate parameter code) on your monthly Discharge Monitoring Repot
RMATION
ie permit requirement and that
North Carolina Division of Water Quality
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
IN ADDITION
Toxicity test data (original "AT" form) must be submitted to the following address:
North Carolina Division of Water Quality
Environmental Sciences Branch
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
> Toxicity test results shall be riled with the Environmental Sciences Branch no later than 30 days after the end of the
reporting period leg, January test result is due by the end of February).
> Toxicity test condition language contained in your NPDES permit may require use of multiple concentration toxicity testing
upon failure of any single quarterly toxicity test. If the initial pass/fail test fails or if the chronic value is lower than the
permit limit, then at least two multiple concentration toxicity tests (one per month) will be conducted over the following two
months. As many analyses as can be completed will be accepted. If your NPDES permit does not require use of multiple
concentration toxicity testing upon failure of any single quarterly test, you may choose to conduct either single
concentration toxicity testing or multiple concentration toxicity testing per the Division's WET enforcement initiatives
effective July 1, 1999„ Follow-up multiple concentration toxicity testing will influence the Division's enforcement response,
> Toxicity testing months are specified by the NPDES Permit, except for NPDES Permits which contain episodic toxicity
monitoring0 requirements (eg, if the testing months specified in your NPDES permit are March, June, September, anc
December, then toxicity testing must be conducted during these months).
Should the permittee fail to monitor during a month in which toxicity monitoring is required, then monthly monitoring will
be in iramechately until such time that a single r",t is pass,-d, Upon Passing this monthly test requirement. the permittee will
revert to the quarterly months specified in the permit. Please note that your permit may or may not contain this language.
> If your NPDES Permit specifies episodic monitoring and your facility does not have a discharge from January I -June 30,
then you must provide written notification to the Environmental Sciences Branch by June 30 that a discharge did riot occur
during the first six months of the calendar year,
Z�
If you receive notification from your contract laboratory that a test was invalidated, you should immediately notify the
Environmental Sciences Branch at [phone] and provide written documentation indicating why the test was
invalidated and the date when follow-up testing, will occur.
1JUI-L I L;Pvik, I VU dakkjutu a N, I u�, t,v I IV " V'I
form, The AT form must also be signed by the performing lab supervisor.
To determine if your AT test forms were received on time by the Division of Water Quality, you may consider submitting
your _toxicity test results cortified mail return receipt requested to the Environmental Sciences Branch.