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NC0089842_Regional Office Historical File Pre 2018
RECEIVE Cdt Laserfelche QRO MOORESVILLE EGONA . OFFICE L October 23, 201 FOUNDATION FOR THE CAROLINAS Mr. Edward Watson NC DEt - Division of Water Resources 0 t4o d€ ,z t o 610 East Cuter Avenue Mooresville, NC 28115 Re: Request to Rescind Permit y NPDES Permit NCO08 842 Carolina Theatre -- Groundwater R.emediation Project Grade I Physical -Chemical WPCS 230 North Tryon Street Charlotte, Mecklenburg County, NC: 28202 Dear Mr. Watson, Construction activities have progressed through the phase during which there was a potential for groundwater to be encountered and which would have required dewatering and treatment of such groundwater. No discharges to surface waters have occurred or will occur under the referenced permit. Consequently, 230 North Tryon, LLC respectfully requests that the referenced permit be rescinded, 230 North Tryon, LLC is managed by Foundation For The Carolinas. If you have questions or comments, please contact u. Best Regards; Laura . S I. Senior Vice President 230 North Tryon, LLC cc, Joe Nestor, ECS Joseph Patrick Nester <JNestor@ecslimited.com> Wednesday, December 5, 2018 6:04 PM Watson, Edward M Richard Grubbs; Matthew F. McDuffie, P.G. [External] Carolina Theatre Ed I understand that you have tentatively scheduled 12- 0-18 mid to bete morning for a pre -system installation site visit. I have checked my schedule and may have a conflict. I may need to pickup my daughter from airport at 8 a, so later (after 10:30) in morning may be better for me. Also from our conversation, we understand that you believe NCDEQ may allow our client to install and operate a treatment system to handle water produced from dewatering and which may be impacted by chlorinated compounds while awaiting issuance of an NPDES permit. JOSEPH PA CT{ NESTOR j Environmental Senior Project Manager T 704.525.5152 1 C 704.280,742 1812'Center Park Drive, Suite D i Charlotte I NC 128217 ECS SOUTHEAST, E P w rw ec limited.com CELEBRATING 30 YEARS - ENP 2018 Top 500 Firms #7 .inkedin I E cebook I Twitter L:.on i ential,,l"proP"ietary.' mess agelo taL"£'iit`ents, Delete 3??€''asag£'lattantim; nts if not intended recipient, This message has been analyzed by Deep Discovery Email: Inspector: 1 Watson, Edward Regards, Ed Edward Watson Hydrogeologist Water Quality Regional Operations Section Division of Water Resources North Carolina Department of Environmental Quality 704 235 2198 Office 704 235 6040 Fax ed ard. atson n dery ggv 610 E. Center Ave. Suite 301 Mooresville; NC 28115 3 Hey Wes, See below.... Would this discharge be allowed without a NPDES permit? Jolixt AIA)affiwli. Envii,rwantental Staperviswor 4`hawrI4)tte-'VIvrkIenhur0, Slorni Water Servires NVA'Ster Quality 111row"grans 2 145 Sattle Avesine Charlotle, Aq, Office: 980/31 1-:1219 Nloh , i1e: 9110/721-3760 hop-1/ Storm Waters WHY statement: We are passionate about making our environment safe and healthy by reducing flood losses and improving water quality for all. STORM -,WATER r services From: Miller, Craig <cmmiller@cicharlotte.nc.us> Sent: Friday, November 09, 2018 2:23 PM To: O'Reilly, Kristen <koreilly@ci.charlotte,nc.us>; McCulloch, John <John.McCulloch@mecklenburgcountync.gov>; Broadway, Chad <Chad. Broadway@ meckle n bu rgco u ntync.gov> Subject: [External]FW: [EXT] Carolina Theatre LCAUTION- This email originated from outside of the organization. Do not click links or open attachments unless you recognize the sender and know the content is safe. Please see below & attached info. How do you all feel about this? From: Joseph Patrick Nestor [,mailto:JNestor,'@ecslii-nited,com] Sent: Friday, November 9, 2018 12:15 PM To: Miller, Craig< Cc: Richard Grubbs <Li!;Iiard�'cDc�acol igat heatrecit,o .rg>; Matthew H. McDuffie, P.G. <MMQuffie @ecsIimiced. com> su ect: [EAT] Carolina Theatre WELL ABANDONMENT RECORD For Internal Use ONLY: 1. Well Contractor information: WELL ABANDONMENT DETAIL Jeffrey Grant 7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same Well Contractor Name (or well owner personally abandoning well on hiAer property) well construction/depth, only I GW-30 is needed. Indicate TOTAL NUMBER of 4328-B wells abandoned: NC Well Contractor Certification Number 7b. Approximate volume of water remaining in well(s): (gal.) JG Drilling, LLC FOR WATER SUPPLY WELLS ONLY: Company Name 2. Well Construction Permit #: 7000252 7c. Type of disinfectant Used: List all applicable well construction permits 0.e. (TIC, County, State, Variance, etc.) if known 7d. Amount of disinfectant used:.: 3. Well use (check well use). Water Supply Well: fie. Sealing materials used (check all that apply): OAgricultural OMunicipallPublic 9 Neat Cement Grout Cl Bentonite Chips or Pellets O eothermal;(Heating/Cooling Supply) C2Residential Water Supply (single) Cl Sand Cement Grout 0 Dry Clay ❑industrial/Commercial OResidential Water Supply (shared) 0 Concrete Grout 0 Drill Cuttings Cilrri tion D Specialty Grout Cl Gravel Non -Water Supply Well: 0 Bentonite Slurry ❑ Other (explain under 7g) @ onitoringORecovery injection Well: 7f. For each material selected above, provide amount of materials used: OAquifer Recharge OGroundwater Remediation Portland Cement 65 ii3s. OAquifer Storage and Recovery 0Salinity Barrier OAquifer Test OStormwater Drainage Bentonite 1.7 lbs. OExperimental Technology OSubsidence Control C)Geathcrmal (Closed Lapp) C7Tracer 7g. Provide a brief description of the abandonment procedure. CiGeathermal (Heatm Coalin ReturnCiOther (ex lain under ? Trenmie grout neat cement grout from 40° b s. to grounurface'. 4. Date well(s) abandoned: 7-18-18 So. Well location: Carolina Theatre Facility/Owner Name Facility 1D# (if applicable) S. Certification: MOORESViLLE REGIONAL OFFICE 101 E. 6th Street, Charlotte, NC 28217 7-18-18 Physical Address, City, and Zip Signature of Certified Well Contractor or Well 0;;ner- Date Mecklenburg County Parcel Identification No. (PIN) By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with !SA NCAC" 02C .0100 or 2C 0200 Well Construction Standards 5b. Latitude and longitude in degreeslminuteslsecands or decimal degrees. and that a copy of this record has been provided to the well owner, (if well field, one latilong is sufficient) 9. Site diagram or additional well details: 35.228302 iN 80.840427 You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. NSTRUC_TION DETAILS OF WELLLS} ,BEING ABANDONED Attach well construction record(s) ifewulable. Far:multiple injection or non -water .supply webs SUBMITTAL iN TRUCTi NS ONLY with the Same construction/abandonment, you can submit oner jrrtrl Unknown t i s i G, �>a. AII His. For Wells: Submit this form within 30 days of completion of well 6a. Well ID#s � � of abandonment to the following: `It JUL40 depth: Division of Water Resources, Information Processing Unit, 6b. Total well (£i) 1617 mail Service Center, Raleigh, NC 27699-1617 '� lob. For Infection Wells: in addition to sending the form to the address in 10a also bc. Borehole diameter; (in.) above, submit one copy of this form within 30 days of completion of well Py y p abandonment to the following: 6d. Water level below ground surface: 25.21 (£t) Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 6e. Outer casing length (if known): None lft,) loc. For Water Supply At Injection Wells: In addition to sending the form to the address(es) above;, also submit one copy of this form within 30 days; of completion 6C Inner length known): of well abandonment to the county health department of the county where abandoned. casing/tubing (if --30 fft) 6g. Screen length (if known): 1 Form GW-30 Nortb Carolina Department of Environmental Quality- Division of Water Resources : Revised 2-22-2016 c ,©.�.�:,:,w��.»- .»■ - i DW Form \ Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements (including weekly averages, if applicable) Compliant All monitoring data and sampling frequencies do NOT meet permit requirements E] Noncompliant The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by Part II.E.6 of the NPDES permit. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." LAURA SMITH Permittee (Please print or type) SENIOR VICE PRESIDENT 230 NORTH TRYON, LLC Signature of Permittee*** Date (Required unless submitted electronically) 220 NORTH TRYON STREET, CHARLOTTE NC 28202 / 704 973 4562 / LSMITH@FFFC.01 30-Jul-24 Permittee Address Phone Number e-mail address Permit E,xpiration Date ADDITIONAL CERTIFIED LABORATORIES Certified Laboratory (2) —Certification No. Certified Laboratory (3) —Certification No. Certified Laboratory (4) Certification No. Certified Laboratory (5) —Certification No. PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit at (919) 807-6300 or by visiting http://portal.nedenr.org/web/wq/swp/1)s/tipdes/appforms. Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there acre no data to be, entered for all of the parameters on the DMR for the entire monitoring period. ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NC AC 8G M04, Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on file with the state per 15A NCAC 2B 0506(b)(2)(D). Page 2 ^~~^ ~- THEATRE ~-_- . - �_ ~` '. ` 24 25 26 27 28 [2 29 MAXIMUM MINIMUM Monthly Lil"it Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements (including weekly averages, if applicable) Compliant All monitoring data and sampling frequencies do NOT meet permit requirements El Noncompliant The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the titne the permittee becomes aware of the circumstances. If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by Part ILE.6 of the NPDES permit. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." LAURA SMITH Perinittee (Please print or type) SENIOR VICE PRESIDENT 230 NORTH TRYON, LLC Tig—nature of Pertnittce*** Date (Required unless submitted electronically) 220 NORTH TRYON STREET, CHARLOTTE NC 28202 704 973 4562 / LSMITH@Fl7r, C.01 30-Jul-24 Permittee Address Phone Number e-niail address permit Expiration Date ADDITIONAL CERTIFIED LABORATORIES Certified Laboratory (2) —Certification No. Certified Laboratory (3) Certification No. Certified Laboratory (4) —Certification No. Certified Laboratory (5) —Certification No. PARAMETER CODES parameter Code assistance may be obtained by calling the NPDES Unit at (919) 807-6300 or by visiting http://portal.ncdenr,org/web/wq/swp/ps/npdes/appforms. Use only units of measurement designated in the reporting facility's NPDES permit for rel,-K)rting data. No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to te- entered for all of the parameters on the I)MR for the entire monitoring period. ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G M04� Signature of Permittee: I f signed by other than the permittee, then the delegation ofthe signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). Page 2 PF EFFLUENT ry: IN I E-0 0 2019 (4 NPDE,S PERMIT NO. NCO089842 DISCHARGE NO. 001 MONTH JULY YEA01PA' 10 ;cassItAGWI Ct FACILITY NAME CAROLINA THEATRE - GROUNDWATER REMEDIATION PROJECT CLASS I jt,,1F<A, CKLENBURG CERTIFIED LABORATORY (1) N/A CERTIFICATION NO. N/A ( list udditional laboratories on the backside/page 2 of this tors ) OPERATOR IN RESPONSIBLE CHARGE (ORC) N/A GRADE WA CERTIFICATION NO. N/A PERSON(S) COLLECTING SAMPLES— N/A ORCPHONE N/A CHFCK BOX IF ORC HAS CHANGFI) IZ3 No F1,0W I DISCHARGE FROM STEE Mail ORIGINAL and ONE COPY to: ATTN* CENTRAL FILE-S x AN ORC HAS NOT BEEN DI IGNAT Q— DIVISION OF WATER RESOURCES (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE 1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS .LALEIGI, NC 276"-1617ACCURATE AND COMPLETETO THE BEST OF MY KNOWLEDGE. MM-- 4 P VQ 011'1'1� G�ONAI- OFFICX DWR Form MR- I - 1 (08/05) Facility Status: PF All monitoring data and s (including All monitoring data and camp The permittee shall report to the Director or the a threatens public health or the environment. Any permittee became aware of the circumstances, A 'Please check one of the following) tripling fretItrencies meet permit requirements weekly averages, if applicable) Compliant ng frequencies do NOT meet permit requirements E:1 Noncompliant propriate Regional Office any noncompliance that potentially ifort-nation shall be provided orally within 24 hours from the time the written submission shall also be provided within 5 days of the time me permitice necomes aware of the circumstances. If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by Part ILEA of the NPDES permit. "I certify, under penalty of law, that this docurnent and all attachments were. prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." LAURA SMITH Permittee (Please print or type) SENIOR VICE PRESIDENT 230 NORTH TRYON, LLC Signature of Permittce*** Date (Required unless submitted electronically) 220 NORTH TRYON STREET, CHARLOTTE NC 28202 704 973 45621 LSMI'FH@FfqC.01 30-Jul-24 Permittee Address Phone Number e-mail address Permit Expiration Date, ADDITIONAL CERTIFIED LABORATORIES Certified Laboratory (2) Certification No. Certified Laboratory (3) —Certification No. Certified Laboratory (4) —Certification No, Certified Laboratory (5) Certification No. PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit at (919) 807-6300 or by visiting http://portai,ncdenr,org/web/wq/swp/ps/npdes/appforms. Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. No Flow/Discharge From Site: Check this box if no discharge occur,,; and, as a result, there are no data to be entered for all of the parameters on the DMR for the entire, monitoring period. ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204. Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on file with the state per 15A NCAC 2B 0506(b)(2)(D). 11'age 2 From. McCulloch, John <John.M Culloch@mee lenbur+ count nc. ov Sent: Friday, November 9, 2018 2.32 PM To Bell, Wes Subject: [External] FW: [External] [EXT] Carolina Theatre Attachments: 2018-11-0- TK-6 and T -7 Analytical Results Total VOCs,pdf CAUTION: Hey Wes, See below.... Would this discharge be allowed without a NPDES permit? t°Irtrrlotile-iireekl+evahverg Shorts Witter 'dery rew Witter Quollity Program 2 145 tsittit Avesnrre t`.ixnrlotto. lit` 28202-52 3 offire: 980/':31,1-3219 !�llan3ri3eb. 9+3343, `'t-37f3t1 htt rhxrrtertterre. ` r�'�ir��w afar Storm Waiter's WHY statement: We are passionate about making our environment safe and healthy by reducing flood losses ,and improving water quality for all. te110fft %rt RMOSTU"RM WATER tO wl''i" cas From: Miller, Craig <cmmiller cl.charlotte.nc.us> Sent: Friday, November 09, 2018 2.23 PM To O'Reilly, Kristen koreilly cl.charlotte.nc.us>; McCulloch; John John. cCulloch@ ecklenburgcountync.gov>; Broadway, Chad <Chad.Broadway(e mecklenburgcountync.gov Subject: [External]FW: [EXT] Carolina Theatre CAUTION. This email originated from outside of the organization. Do not click links or open attachments unlessyou recognize the sender and know the content is safe. Please see below & attached info. How do you all feel about this From. Joseph Patrick Nestor [mailto:JNestor `ec lirmted.com) Sent. Friday, November 9, 201 12.15 PM To: Miller, Craig <crnMill r@ci,charlotte.nc.us Cc Richard Grubbs <Rchard carolinatheatreclt.or > Matthew H. McDuffle, P.G. MMcDuffie ecslimited.com Subject. [EXT] Carolina Theatre t p ' IL: 7ItIs emPP'llg'snated fromthe Internet. Oo not dick any Images, links or ripen any attachments unlessyou recognize and trust the sender and P no the content is safe. Please forward all suspicious email to bad mail charlottenc.gov. Craig: God morning. As i indicated in voice mall messages, the Carolina Theatre site has water from drilling operations which they wish to remove from the site. We may have discussed how they have been handling drilling spoils in the past but I will say it again to be certain you are clear. Drilling spoils consisting of solids (soil and rock cuttings) and water are deposited into a frac tank, After solids settle, water is decanted to another fr c tank with two compartments. Water is removed when additional capacity is rewired. Solids are removed as additional capacity Is required and are solidified and disposed in a Subtitle tlandfill. In the past, water which was removed was treated and discharged at a permitted off -site industrial wastewater treatment facility, The water was handled in this manner, because analyses indicated the presence of PCE in concentrations which exceed NC surface water standards. ES recommended that before a batch of water is removed from the site that it be analyzed for VOCs. This recommendation has been followed. A copy of the most recent analyses are attached. Samples (TK-f and TK-7) were taken from each of the compartments into which decanted water is stored. Our client has requested ECS to look into the possibility that this particular batch of water may discharged to the City of Charlotte Stor water System, As indicated in the results, chloromethane was detected at concentrations of 2.7 and 2.6 ug/I and toluene was detected at concentrations of 1.3 and 1.5 ug/i in samples TKm6 and TK- , respectively: There is no IBC surface water standard for chloromethane. The NC surface water standard for Class C water (Sugar Creek and Irwin Creek are Class C streams) for toluene is 11 ug/l. It is estimated that approximately 6,000 gallons of water are stored. If discharge of this particular batch of water is permitted by the City of Charlotte, ECS recommends that water be pumped through a bag filter or similar device to remove possible suspended sediments: Please ,give this request consideration and let us know If the discharge of this particular batch of water can be allowed. JOSEPH PATRICK NESTOR I Environmental Senior Project Manager 7 704.5253152 I C 704,280342 1812 Center Park Drive, Suite a I Charlotte I NC 128217 S SOUTHEAST, LLf' www.ecslimited.com CELEBRATING 30 YEARS - EMIR 2018 Top 500 Firms 47 Linkedin I Faceb qk I Twitter {„:i1'jit,�(=P"i afpr °, `?J �s�+,{��"��`l7 �"{:7`#�"5'�.iC�c',r'e;�`r4e..7(^5"Y#: Cit.�..�'e'd_#,? s5 :`*�7L���;���.If:`. C. �7?Y�iv�: . s tj r't Vc .t. e vdet rec4 pia "It This message 1 gas been analyzed by Deep Discovery Email 2 Inspector. RN L EMAIL. This email originated from the Internet. Do not click any images, links or open any attachments unless you recognize and trust the sender and know the content is safe. Please forward all suspicious email to kad,. p's6 r€c tip r s. Craig. Good morning. As I indicated in voice mail messages, the Carolina Theatre site has water from drilling operations which they wish to remove from the site. We may have discussed how they have been handling drilling spoils in the past but I will say i again to be certain you are clear. Drilling spoils consisting of solids (soil and rock cuttings) and water are deposited into a frac tank. After solids settle, water is decanted to another frac tank with two compartments. Water is removed when additional capacity is required. Solids are removed as additional capacity is required and are solidified and disposed in a Subtitle D landfill. in the past, water which was removed was treated and discharged at a permitted off -site industrial wastewater treatment facility. The water was handled in this manner, because analyses indicated the presence of PE in concentrations which exceed NC surface water standards. ECS recommended that before a batch of water is removed from the site that it be analyzed for VOCs. This recommendation has been followed. A copy of the most recent analyses are attached. Samples (TK-6 and T -7) were taken from each of the compartments into which decanted water is stored. Our client has requested ECS to look into the possibility that this particular batch of water may be discharged to the City of Charlotte Stormwater :System. As indicates! in the results, chloromethane was detected at concentrations of 2.7 and 2.6 ugl and toluene was detected at concentrations of 1.3 and 1.5 ug/I in samples TK-6 and TK-7, respectively. There is no NC surface water standard for chloromethane. The NC surface water standard for Class C water (Sugar Creek and Irwin Creek are Class C streams) for toluene is 11 ug 1. It is estimated that approximately 6,000 gallons of water are stored. If discharge of this particular batch of water is permitted by the City of Charlotte, ECS recommends that water be pumped through a bag filter or similar device to remove possible suspended sediments. Please give this request consideration and let us knew if the discharge of this particular batch of water can be allowed. I SEPH PAT, PICK NESTOR I Envfironmenfa eniorr Project Manager 812 Center Park Drive, S9,flte D I Charlotte € NC 1 28217 yEC�S S ^ SOUTHEAST, LLP CELEBRATING 30 YEARS , ENR 2018 p 500 Firms # 7. LinkedIn i i 3 3d" C 'wittel.. ..,... This message has been analyzed by Deep Discovery Email Inspector. 2 Pace Analytical Services, LLC ry/�++ p 9 00 Kincey Ave. Suite 100 a lyddl Huntersville, NC 28078 (704)875-909 QUALITY CONTROL DATA CROSS REFERENCE FABLE Project: CAROLINATHEATER Pace Project No.: 92405744 Analytical Lab ID Sample 1D QC Batch Method QC Batch Analytical Method Batch 9240 744001 TK-6 EPA8260B 439851 92406744002 % TK-7 EPA 8260B 439851 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Carte: 11/06/2018 01:47 PM without the written consent of mace Analytical Services, LLC. a Page 15 of 16 HAII5 -OF- USTODY Analytical Request Document P A l i af' Chain- of -Custody is a LEGAL DOCUMENT Complete all relevent fields Company Billing Informatfow w Addresst Report To. Email To: k w, Copy To,, Site Collection Info/Address Customer Project Name/Number State: County/City: Time Zone Collected .,..__- '.` i 1PT )nrC 3cTI JET Phone: r SiteAFacility IN d: Compliance Monstorin 7 Erna&... Yes J )No Collected By (print.): Purchase Order lf. DW PWS ID Jk tic+uje ts: DtV Location Circle! Cratie,led Ely Lugoature): Tor round Date Required: im r e sate y l>Rc e an ice, .,. ( )Yes (:)No Sample Wspcasat „ RushField Filtered (if applicable): I 1 Dispose as appropriate t 1 Return 1 1 Sarre pay I ") Next Day ( ] Yes f Ilse I l Archive .. C 12 csay ( 13 Dav ( 1 d nay ( 15 Day E ) tioldi (Expedite Charges APPjv) Analysis:_ * tvituns Codes (Insert in Matrix box belcywj. Drinking Water (DW), Ground Water (GW), Wastewater (WW), Product (P), Soil/Solid (Sid, Oil (OL), Wipe (WP), Air (AR). Tissue (75), Sioassay (Bl, Vapor (V), Other (OT) Camp # Collected (or Res tr of Customer Sample ID Matrix Grab Composite Start) Composite End Cl Ctnt fate Time Date Tim i= Customer Remarks / Special Conditions J )Possible Hazards,_.._ Type of Ice Used:µ Wet Blue Dry None Packm MateriafUsed. Radche m sample(s) screened (<500 corn). Y N NA Relinquished by/Company; (Signature) I Datej` ime: Received by/Company; (Signature) u� f Relinquished by/Company: (Signature) j Dans/Timer Received by/Company; (Signatures) Relinquished bYlCes pony. (Signature)Date/Time: Received kyj tampany: (Signature) l LAB USE ONLY- Afflx workorder f E ALL SHADED AF 924OS744 Container Preservative Ta.. Lab Project Manager: `« Preservative Tidies: (T nitric acid, (2) suifuric acid, l5) hydrochloric and, $a} r,,cctirrrrr hydroxide, (5) I'mc acetate, (6) methanol, (7) sodium bisulfate, (a) %odium thrasulf te, is) hexane, (A) ascorbic acid, (0) ammonium sulfate. (C) arninc ,lum hydroxide, (D) YSP, (u) 0"preserved. bil Other Anal st s Lab Profile (Line, LaA le Receipt Checrlatf Custody Seals Present/Intact Y Ncltx_ Custody Signatures present Y n 4A, Collector Signature Present YrN NA Battles Intact 'Nt NA Correct Bottle.� N NA sufficient volume 'Y" N NA Samples Received on ice �Y'N NA VOA _ Headspa ce Acceptable %, N NA USDA Regulated Suits Y N :Ai7F: Samples in Holding Time Y ly, t#osidual chlorine, Present Y N Yx"R Cl Strips. Sample pH Acceptable...�.,.,�u. ..., ..Y N NA pH Strips,. .Sulfide Present Lead Acetate :;trips: LAB USE ONLY Lab Sample f Cov mnt s: SHORT HOLDS PRESENT (<72 hours). Y N11 N/A Lab Sample Temperature lnf u Lab "Tracking ki. Temp Blank Received. Y N NA """k " a a ) Therm lit#: _� ate. _ ° � µ Y Corder 1 Ternp Upon Receipt, pC Samples rt+cedved via. Cooler i Thereat Corr. Fatter: �oC FEDEX UPS 'eiieeat Courier face Courier Cooler 1 CorrectedTepp:n oC DatelTlme; MTJL LAB USE ONLY Cmnmentsr Table tl. Acctnum.; Date/Time: Template: Trip Blank Receive& Y ; N NA Prelogim HCL McOH TSP Other Date/Time. p ; =YCS/ s): Page. PB. il. t y Pace Analytical Services, t LC actQ y 9000 Kincey Ave. Suite 100 Huntersville, NC 28078 wwwpecelIme0ont(704)875-9092 QUALITY CONTROL DATA Project: CAROLI ATHEA'ER Pace Project No.: 92405744 MATRIX SPIKE SAMPLE: 2416954 92405098006 Spike MS MS % Re Parameter units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ugIL NO 20 21A 107 70-130 1,1,1-Trichloroethane ugJL ND 20 22.0 110 70-130 1,1,2„2-Tetracloroethe ugiL NO 20 23.3 117 70-130 1,1,2-Trichloroethane ug1L ND 20 22,7 113 70-130 1,1-Dichloroethane ug1L ND 20 218 119- 70-130 1,1-Dichloroethene ugJL NO 20 25.5 128 70-166 1,1-Dichloropropene< ugiL ND 20 19.8 99 70-130 1,2,-Trichlorcbenzene ugJL NO 20 19:1 96 70-130 1, ,-Trichloropropane- ug1L ND 20 23.7 119 70-130 1,2,4-Trichlorobenzene ugJL NO 20 21.1 105 70-130 1,2-Dbromo-3-chloropropane ug1L NO 20 18A 92 70-130 1,2-Dibromoethane(EDB) ugJL ND 20 19.1 96 70-130 1,2-t ichlorobenzene ug1L ND 20 22.6 113 70-130 1,2-Cichloroethane ugJL NO 22.7 113 70-130 1,2-Dchloropropane ugJL NO 20 23,2 116 70-130 1,3-Dichlorobenzene ug1L ND 20 22A 112 70-130 1,3-Dichloropropane : ugJL ND 20 19.2 96 70-130 1,4-Dichlorobenzene ugJL NO 20 2.9 114 70-130 2,-Dichloropropane ugJL NO 20 21.6 108 70-130 2-Butanone (MEK) ug1L ND 40 37.0 92 70-130 2-Chlorotoluene ug1L ND 20 22,0 110 70-130 2-Hexanone ugJL ND 40 46,6 117 70-130 4-Chlorotoluene ugJL NO 20 22.3 112 70-130 4-Methyl-2-pentanone (MIRK) ugJL ND 40 43.9 110 70-130 Acetone ug1L NO 40 , 45:2 113 70-10 Benzene ugtL ND 20 23.7 119 70-148 Bromobenzene ugJL NO 20 21.7 109 70-130 Bromochloromethane ug/L NO 20 24.5 122 70-130 Bromodichloromethane ug1L NO 20 22Z 112 70-130 Brotnoform ugJL ND 20 17.2 86 70-130 Bromoethane ugJL NO 20 16.1 80 70-130 Carbon tetrachloride ug1L NO 20 24.3 122 70-130 Chlorobenzene ug1L ND 20 23,0 115 70-146 Chloroethane ugJL NO 20 26A 132 70-130 M1 Chloroform ugJL NO 20 23A 115 70-130 Chlotomethane ugiL ND 20 18.7 94 70-130 cis-1,2-Dichloroethene ugJL ND 20 23.6 118 70-130 cis- 13-Dichloropropene ug1L NO 20 19.7 98 70-130 Dibromochloromethane ugiL NO 20 16.8 84 70-130 Dibromomethane ugiL NO 20 22.6 113 70-130 Dichlorodifluoromethane ugJL NO 20 14.0 70 70-130 Diisopropyl ether ug1L NO 20 17.3 87 70-130 Ethylbenzene ugiL ND 20 236 118 70-130 He achloro-1 3-butadiene ugJL NO 20 22.2 ill 70-130 mp-ylene ugJL NO 40 48.8 122 70-130 Methyl-tert-butyl ether ug1L ND 20 17.2 86 70-130 Methylene Chloride ugiL NO 20 262 131 70-130 M9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11106/2018 01:47 PM without the written consent of Pace Analytical Services, LLC, Page 11 of 16 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 � � # Huntersville, NC 28078 WwwPacarsirs, Cam (704)875-9092 QUALITY CONTROL DATA Project: CAROLINATHEATER Pace Project No.: 92405744 MATRIX SPIKE SAMPLE.: 2416954 92405098006 Spike ' MS Ms % Rec Parameter Units Result Conc. Result % Rep Limits Qualifiers Naphthalene ug/L ND 20 18.9 94 70-130 o-Xylene ug/L ND 20 24,7 124 70-130 p-Isopropyltoluene ug/L ND 20 2:6 113 70-130 Styrene ug/L ND 20 244 122 70-10 Tetrpchloroethene ug/L ND 20 21.7 109 70-130 Toluene ug/L ND 20 23.2 116 70-155 trans-1,2-Dichloroethene ug/L ND 20 24,0 120 70-130 trans-1,3-Dichloropropene ug/L ND 20 201 101 70-10 Triehloroethene ug/L ND 20 21.1 105 69-151 Trichlorofluortmethane ug/L ND 20 23.0 115 70-130 Vinyl acetate ug/L ND 40 31.0 78 70-130 Vinyl;; chloride ugfL ND 20 22.A 112 70-10 Xylene (Total) ug/L ND 60 73,5 122 70-130 1,2-Dichloroethane-d4 (S) °lQ 105 70-130 4-Bro ofluorobenzene (S) % 106 70-130 Toluene-d8 (S) °le 102 70-130 SAMPLE DUPLICATE: 2416953 92405098005 Dup Parameter Units Result Result RPD Qualifiers 1, 1, 1,2-Tetrachloroethane ug/L ND ND 1, 1, 1 -Trichloroethane ug/L ND ND 1, 1, 2,2-Tetrachloroethane ug/L ND ND 1,1;2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethen ug/L ND ND 1,1-Dichloropropene ug/L ND ND 1,2,3-Trichlorobenzene ug/L ND ND 1,,-Trichlorpropane ug/L ND ND 1,2,-Trichlorobenzene ug/L ND ND 12-Dibromo--chloropropane ug/L ND ND 1,2-Dibromoethane (EDB) ug/L ND ND 1,-Dichlorobenzene ug/L ND ND 1,2-ihloroehane ug/L ND ND 1.-Dichloropropane ugfL ND ND 1,3-Dichlorobenzene ug/L ND ND 1,3-Dichloropropane ug/L ND ND 1,4-Dichlorob nzene ug/L ND ND 2,2-Dichloropropane ug/L ND ND 2-Butanone (MEK) ug/L ND ND 2-Chlorotoluene ug/L ND ND 2-Hexanone ug/L ND ND 4-Chlorotoluene ug/L ND ND 4-Methyl-2-pentanone (MIRK) ug/L ND ND Acetone ug/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Dater 11/06/018 01:47 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 12 of 16 rpm ace yfil Wiewnadombscom Pace * Ana —cat Service-t s r. 9800 Kincey Ave. Su Huntersville, NC QUALITY CONTROL DATA Project: CAROLINA THEATER Pace Project No.: 92 05744 SAMPLE DUPLICATE. 2416953 92405098005 Dup, Parameter Units Result Result RPD Qualifiers Benzene ug/L ND 28J Bromobenzene ugfL ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ugfL ND ND Bromofor ug/L _ ND ND Bromomethane ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chlommethane g/L ND ND cis-1 „2-Dichloraethene ugfL ND ND cis-1,-Dichloropropen ug/L ND NO Dibroochloroethane ugfL ND ND Dibronnomethane ug/L ND NO Dichlt rodifluoromethane ug1L. ND ND Dtisopropyi ether u/L NO ND ; Ethylbenzene ug/L ND ND Hexai hloro-1,-butadiene ug1L ND ND', m&p-Xylene ugfL ND ND Methyl-tert-butyl ether ug1L ND ND Methylene Chloride ug1L ND NO Naphthalene ug/L ND NO o-ylene ugfL ND ND p-lsopropyttolue ug1L ND ND Styrene ugfL ND ND Tetra hloroethene ug/L ND NO Toluene ug/L ND NO trans-1,2-Dichloroethene ug1L ND NC? trans- 1, 3-Dichloropropene ugfL ND ND Trichioroethene ug/L ND ND Trichlorofluoromethane ug1L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene (Total) ugfL ND ND 1,2-Dichloroethane-d4 (S) % 86 85 2 4-Bromofluorobenzene (S) % 166 112 6 Toluene-d8 (S) °1' 119 117 Results presented on this page are In the units Indicated by the "Unks" column except wherry an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/0612018 01:47 PM without the written consent of Pace Analytical Services, LLG. Page 13 of 16 +��+�} p % Pace Analytical Services, LLC ttirCi # ! 9800 KinceyAve. Suite 100 Huntersville, NC 28078 WWWPacewscm (704)875-9092 QUALIFIERS Project: CAROLINATHEATER Pace Project o.: 92405744 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Cluantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) . Matrix Spike (Duplicate) DUP - Sample Duplicate RPD -Relative Percent Difference NC - Not Calculable. S - Silica Gel - Glean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Rcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PAI-C Pace Analytical Services - Charlotte ANAL TE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced„ except in full, Dater 11/06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 16 Pace Analytical Services, CLC P* / r j e ce /�t t 980o incey Ave. Suite 100 Nuntersvitle, NC 28078 (704)87*.r9092 QUALITY CONTROL DATA Project: CARt7LINATHEATER Pace Project No.: 92406744 LABORATORY CONTROL SAMPLE. 24169E Spike LCS L % Rao Parameter Units Corte. Result ale Rec Limits Qualifiers 2,2-Dichloropropane ugfL 50 52A 104 40-160 -utanone (MEK) uIL 100 109 109 61-144 2-Chlorotoluene ug/L 50 52:8 106 74-13 -Hexanone ug1L 100 103 103 68-143 4-Chlorotoluene ugrL 50 52.5 105 7-13 4-Methyl-2-pentanone (MIBK) ugrL 100 103 103 72-135 Acetone ugrL 100 117 117 4-146 Benzene ug/L 50 56.3 113 80-125 Bromobenzene ugiL 50 52.6 105 7 -125 Broochloroethane ugrL 50 59.4 119 71-125 Bromodichloromethane ugrL 50 54A 109 7 -124 Bromoform ugrL 50 49,6 99 71-128 Bromomethane ug1L 50 41.3 83 40-160 Carbon tetrachloride ugrL 50 55:5 111 69-131 Chlorobenzene ugrL 50 52:0 104 81-122 hlcroethane ugiL 50 449 90 3-148 Chloroform ugrL 50 56.5 113 73-127 Chloromethane ugrL 50 45,8 92 44-1 6 cis-12-Dichloroethene ugiL 50 57:6 115 74-12 cis-1 „3-Dichloropropene ug1L 50 52:8 106 72-132 Dibromochloromethane uglL 50 49A 99 78-125 Dibromomethane uglL 50 51.7 103 82-10 Dichlorodifluoromethane ugrL 50 42.0 84 4-157 Diisopropl ether ug1L 50 49.9 100 69-15 Ethytbenzene ug/L 50 51.2 102 79-121 Hexachloro-1,3-butadiene ugrL 50 53.3 107 72-131 m p-Xylene ug/L 100 105 105 81-124 Methyl-tert-butyl ether ug1L 50 51.3 103 74-131 Methylene Chlorine ug£L 50 60.4- 121 64-133 Naphthalene ugrL 50 53.6 ' 107 73-133 o-Xylne ugrL 50 53.3 107 79-131 p-isopropyltoluene ug1L 50 51A 103 80-1 1 Styrene ugiL 50 53.7 107 84-126 Tetrachlomethene ug/L 50 50A 100 78-122 Toluene ug1L 50 47.3 95 0-121 trans-I.2-Dichloroethene ugrL 50 60.0 120 71-127 trans-1,3-Dichloroprrpene uglL 50 53A 106 69-141 Trichloroethene ugrL 50 52.5 105 78-122 Trichlorofiuoromethane ugrL 50 52.2 104 53-137 Vinyl acetate ugrL 100 104 104 40-160 Vinyl chloride ugrL 50 49.5 99 58-137 Xylene (Total) ugrL 150 159 106 81-126 1,2-t ichlor thane-d4 (S) % 109 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) °la 95 70-10 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC, Page 10 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 t alce 8114icaj Huntersville, NC 28078 wwwpacetarSsMe (704)875-9092 QUALITY CONTROL DATA Project: C ROLI ATHEATER Pace Project No.: 92405744 METHOD BLANK: 2416951 Matrix: Water Associated Lab Samples: 92405744001, 9240574400 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/L NO 1.0 11102/18 08:06 Ethylbenzene ; ug1L ND 1.0 11/02/18 08:05 Hexachloro-1,3-butadiene ug7L NO 1.0 11102/1808:05 m&p- ylene ug1L ND 2.0 11/02/18 08:05 Methyl-tert-butyl ether ug1L ND 1.0 11/02118 08:05 Methylene Chloride ug/L NO 2.0 11/02118 08:05 Naphthalene `' ug1L NO 1.0 11/02/18 08:05 o-Xyl ne ug/L NO 1.0 11/02118 08:05 p-isopropyltoluene ug1L NO 1.0 11/02/18 08:05 Styrene ug1L ND 1.0 11/02/18 08:05 Tetrachloroethene ug1L ND 1.0 11/02/18 08:05 Toluene ug1L ND 1.0 11102/18 08,05 trans-1,2-Dichloroethene ug1L ND 1.0 11102I18 08:0 trans-1,3-Diohloropropene ug1L NO 1.0 11/02/18 08:05 Trichloroethene ug1L NO 1.0 11/02/18 08:05' Trichlorofluoromethane' ug1L NO 1.0 11102/18 08:05 Vinyl acetate ug1L ND 2.0 11/02/18 08:05 Vinyl chloride ug1L NO 1.0 11/02/18 08:05 Xylene (Total) ug1L NO 1.0 11/02/18 08:05 1,2-Dichloroethane-d4 (S) % 81 70-130 11102118 08:05 4-Bromofluorobenzene'(S) % 111 70-130 11/02/18 08:05 Toluene-d8 (S) % 119 70-130 11/02/18 08:05 LABORATORY CONTROL SAMPLE: 2416952 Spike LCS LCS % Rec Parameter Units Cone. Result % Rae Limits Qualifiers 1,1,1,2-Tetrachloroethane ug1L 50 56.5 113 80-125 11,1-Tnchloroethane ug/L 50 54.5 109 71-129 1,1 „2„2-Tetrachloroethane ug1L 50 51.9 104 79-124 1,1,2-Trichlorcethane ug1L 50 56.6 113 85-125 1,1-Dichloroethane ug/L 50 56.9 114 73-126 1,1-Dichlor thene ug1L 50 56A 113 56-135 1,1-Dichloroprbpene ug1L 50 54.0 108" 74-135 1,2,3-Trichlorobenzene ug1L 50 53.8 108 73-135 1,2,3-Trichloropropane ug1L 50 54.3 109 7 -130 1,24-Trichlorobenzene ug/L 50 53:6 107 75-134 1,2-Dibromo-3-chloropropane ug1L 50 48.3 97 71-13 1,2-Dibromoethane ( DB) ug/L 50 52.6 105 83-124 1,2-Dichlorobenzene ug1L 50 50.0 100 80-133 1,-Dichloroethane ug1L 50 57.7 115 67-128 1, -Dichloropropane ug/L 50 58.6 117 -132 1,3-Dichlorobenzen ug1L 50 51.3 103 77-130 1;3-Dichloropropane ug/L 50 53A 107 76-131 1,4-Dichlorobenzen ug1L 50 49.9 100 7-130 :Results presented on this page are in the units indicated by the "Units" column excerpt where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dater 11/06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 Y Pace natytica: sivic CLC e to r tri7 �i t/ a 9800 Kinney Ave Suite 100 Huntersville, NC 28078 wwwpocehftcom (704)875.9092 QUALITY CONTROL DATA Project: CAROLINATHEATER " Pace Project No.: 92405744 QC Batch: 439851 Analysis Method: EPA 8260B QC Batch Method: EPA 8260B Analysis Description: 8260 MSV Low Level Associated Lab Samples: 924057 Opt, 9240574400 METHOD BLANK: 2416951 Matrix: Water Associated Lab Samples: 92405744001, 9240744002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachlor thane ug/L ND 1.0 11/02/18 08:05 1, 1, 1 -Trichloroethane ug/L ND 1.0 11/02/18 08:05 1,1,2.2-Tetrachlor thane ug/L ND 1.0 11102/18081.05 1,1,2-Trichlorcethane ug/L ND 1.0 11/02/18 08:05 1,1- ilchloroethane ug/L ND 1.0 11/02/18 08:05 1,1-Dichloroethene ug/L ND 1.0 11/02/18 08:05 1,1-Dichloropr pene ug1L ND 1.0 11/02/18 08:05 1,2,3-Trichlorobenzene ug/L ND 1.0 11102tt808:05 1,2,-Trlchloropropane ug/L ND 1.0 11/02118 08:05 1,2,4-Trichlorobenzene ug/L ND 1.0 11/02/18 08:05 1,2-Dibromo-3-chloropropane ug/L ND 2.0 11102/18 08:05 1,2-Dibromoethane (EDB) ug/L ND 1.0 11/02/18 0805 1,2-Dichioro nzene ug/L ND 1 0 11/02/18 08:05 1,2-Dichlor thane ug/L ND 1.0 11/02/18 08:05 1,2-Dlchloropropane ug/L ND 1.0 11/02/18 08:05 1,3-Dichlorobenzene ug/L ND 1.0 11/02118 08.05 1,3-Dichloropropane ugiL ND 1.0 11/02/18 08:05 1.4-Dichlorobenzene ug/L ND 1.0 11102118 08:05 2,2-Dichloropropane ug/L ND 1.0 11/02/18 08:05 2-Butanone (MEK) ug/L ND 5.0 11/02/18 08:05 2-Chlorotoluene ug/L ND 1.0 11/02118 08:05 2-Hexanone ug/L ND &0 11102118 08:0 4-Chlorotoluene ug/L ND 1.0 11/02118 08:05 4-Methyl-2-pentanone (MIRK) ug/L ND 5.0 11/02/18 08:06 Acetone ug/L ND 25.0 11/02118 08:05 Benzene ug/L ND 1,0 11/02/18 08:05 Bromobenzene ug/L ND 1.0 11/02/18 08:05 Broinochloromethane ug/L NO 1.0 11/02/18 08:0 Bromodichloromethane ug/L ND 1.0 '11/02/18 08:0 Bromoform ug/L ND 1.0 11/02/18 08,05 Bromomethane ug/L ND 2.0 11/02/18 08:05 Carbon tetrachloride ugJL NO 1,0 11102/18 08:05 Chlorobenzene ug/L ND 1.0 11/02/18 08:05 Chloroethane ug/L ND 1.0 11/02/1808:05 Chloroform ug/L ND 1.0 11102/18 08:0 Chloromethane ug/L ND 1.0 11/02/18 08:05 cis-1 2-Dichloroethene ug/L ND 1.0 11/02/18 08:05 cis- 1„-Dichloropropene ug/L ND 1.0 11/02118 08:05 Dibromochloromethane ug/L ND 1.0 11/02/18 08:05 Dibroomethne ug/L ND 1.0 /1/02118 08:05 Dichlcrodifluoromethane ug/L ND 1.0 11/02/18 08:05 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the "result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: "11 /06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16 Pace Analytical Services, LLC ��++ ca m, lyica 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 ? wwwvp tebs cam (704)875-9092 ANALYTICAL RESULTS - Project: CAROLINATHEATER Pace Project No.: 9205744 Sample: T -7' Lab ICI: 92406744002 Collected: 11/02J18 09:53Received: 11/02/18 10: 5 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No Quat 8260 MSV Low Level Analytical Method. EPA 82608 Toluene 1.6 ug/L 1.0 1 11/0211813:01 108-88- 1,2,3-Trichlorobenzene ND ug/L 10 1 11/0211813:01 87-61-6 1, ,4-Trichlorobenzene ND ug/L 1.0 1 11102/1813.01 120-82-1 1,1,1-Trlchloroethane ND ug/L 1.0 1 11/02/1813:01 71-55-6 1,1,2-Trichloroethan ND ug/L 1:0 1 11/0211813:01 79-00-5 Trichloroethene ND ug/L 1,0 1 11/02/1813:01 79-01- Trichl lrofluoro ethane ND ug/L, 1.0 1 11/02/18 1301 75-69-4 1,2,3-Trichlorcpropane ND ug/L 1:0 1 11/02/1813:01 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/02118 13:01 108-05-4 Vinyl chloride ND ug/L 10 1 11/02118 13:01 75-01-4 Xylene (Total) ND ug/L 1,0 1 11102118 13:01 1330-20-7 m&p-Xylene ND ug/L 2,0 1 11/02/1813:01 179601-23-1 o-Xytene ND ug/L 1;0 1 11102/18 1:01 05-47-6 Surrogates 4-Brormofluorobenzene (S) 110 % 70-1 0 1 11/02/1813:01 460-00-4 1,2-Dlchloroethane-d4 (S) 92 % 70-1 0 1 11/0211813:01 17060-07-0 Toluene-d (S) 113 % 70-130 1 11102/1813:01 2037-26- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/018 0147 PM without the written consent of Pace Analytical Services, LLG, Page 7 of 16 Pace Analytical Services, LLC c rat j tyt1 t 1 j 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 wwwpawiabs'com (704)875-9092 ANALYTICAL RESULTS Project: CAROLINATHEATER Pace Project No.: 92405744 Sample: TK-7 Lab ilk: 924066744002 Collected: 11102/18 09:5 Received: 11/02118 10 35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qal 820 MSV Low Level Analytical Method: EPA 82608 Acetone Nth ug/L 26,0 1 11/0211813:01 67-64-1 Benzene ND ug/L 1.0 1 11/02/18 13:01 71-43-2 Bromobenzen ND ug/L 1.0 1 111021181301 108-86-1 Bromochloromethane ND ug/L 1:0 1 11/02/18 13:01 74-97.5 Bromodichloromethane ND ug/L 1.0 1 11/0211813:01 75-27-4 Bron oform ND ug/L 1.0 1 11/02/18 13:01 5-25- Bron omethane ND ugfL 2,0 1 11/02/18 13:01 4-83-9 2-Butanone (E) ND ug/L 5.0 1 11/02/18 13:01 8-93-3 Carbon tetrachloride ND ug/L 1:0 1 ; 11/02/18'13:01 56-23-5 Chlorobenzen ND ug/L 1.0 1 11/0211813:01 108-90-7 Chioroethane ND ug/L 1:0 1 11/02/1813:01 75-00- Chloroform ND ug/L 1;0 1 11/0211813:01 7-66-3 Chloromethate .6 ugfL 1.0 1 11/0211313:01 4-87-3 2-Chlorotoluere ND ug/L 1.0 1 11/0211813:01 95-49-8 4-Chlorotoluene ND ug1L 1:0 1 11102/1813:01 106-43-4 1,2- ibromo-3-chloropropane ND ug1L 2:0 1 11/02/18 13:01 96-12-8 Dibromochloromethane ND ug/L 1;0 1 1110211813:01 124-48-1 1,2-C ibrom thane (EDB) ND ug/L 1'0 1 11102/18 13:01 106-93-4 Dibromomethane ND ug/L 1:0 1 11102/1813:01 74- 5-3 1.2-Dichlorobenzen ND ug/L 1;0 1 11/02/18 13:01 5-50-1 1,3-ichlorobenzene ND ug/L 1.0 111102/1813:01 41-73.1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/02/18 13:01 106-4 -7 Dichlorodifluoromethane ND ug/L 1.0 1 11/02/1813:01 75-71-8 1,1-Dichloroethene ND ug/L 1.0 1 11/02/18 13:01 75-34- 1,2-Dichlor thane ND ug/L 1.0 1 11/02/18 13:01 107-06-2' 1, 1 -Dichloroethene ND ugiL 1.0 1 11/02/18 13:01 75-35-4 cis-1, -Dichloroethene ND ug/L 1.0 1 11/02/18 13:01 156-69-2 trans-1,2-Dichloroethene ND - ug/L 1;0 1 11/02/18 13:01 156-60-5 1,2-Dichloropropane ND ugfL 1.0 1 1110/1813:01 78-87-5 1,3-Dichloropropane" ND ug/L 1'0 1 1110211813:01 142-28-9, 2,2-Dchloropropane ND ug/L 1.t 1 11/02/18 13:01 94-20-7 1,1-Dichloropropene ND ug/L 1'0 1 11/0211813:01 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/02/18 13:01 10061-01-5 trans-1,3-Dichioropropene ND ug/L 1:0 1 11/02/1813,01 10061-02-6 Dtaopropyl ether ND ug/L 1:0 1 11/021181101 108-20-3 Ethylbenzene' ND ug/L 1.0 1 11/02/1813:01 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 11/0211813:01 87-68-3 2-Hexanone ND ug/L 5.0 1 11/02/1813:01 91-78-6; p-isopropyltoluene ND ug1L 1:0 1 11/02/18 13:01 99-87- Methylene Chloride ND ug/L 2.0 1 11/02118 13:01 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5,0 1 11/02/18 13:01 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/02/18 13:01 1634-04-4 Naphthalene ND tag/L 1'0 1 11/0211813:01 91-20-3 Styrene ND ug/L 1,0 1 11/02/18 13:01 100-42-5 1,1„12-Tetrachloroethane ND ug/L 1:0 1 11102/1813,01 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/02/1813:01 79-34-5 Tetrachloroethane ND ug/L 1.0 1 11102/1813:01 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11106/2018 01:47 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 Pace Analytical SorAces, LLC aceAmIj4kal 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 wwwpaoefabs'vvr; (704)875-9092 ANALYTICAL RESULTS Project: CAROLINATHEATER Pace Project No.: 92405744 Sample: TK-6 LablD: 92406744001 Collected: 11/02/18 09:45 Received: 11/02/18 10:35 Matrix, Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual 8260 MSV Low Level Analytical Method: EPA 8260B Toluene 11;3 ug/L 1'0 1 11102/18 12,28 108-88-3 1,2,3-Trichlorobenzene NO ug/L 1.0 1 11102/18 12:28 87-61-6 1,2,4-Trichlorobenzene NO ug/L 1.0 1 11/02/18 12:28 120-82-1 1,1,1-Trichloroethane NO ug/L 1.0 1 11102118 12:28 71-55-6 1,1,2-Trichloroethane NO ug/L 1'0 1 11/02/18 12:28 79-00-5 Trichloroethene ND ug/L 1.0 1 11/02/18 12,28 79-01-6 Trichlorofluoromethane NO ug/L 1'0 1 11102118 12:28 75-69-4 1,2,3-Trichloropropane NO ug/L 1,0 1 11/02/18 12:28 96-18-4 Vinyl acetate NO ug/L 2,0 1 11102118 12:28 108-05-4 Vinyl chloride NO ug/L 1.0 1 11/02/18 12:28 75-01-4 Xylene (Total) NO ug/L 1'0 1 11/02/18 12:28 1330-20-7 m&p-Xylene NO ug/L 2,0 1 11/02/18 12:28 179601-23-1 o-Xylene NO ug/L 1'0 1 11/02/18 12.28 95-47-6 Surrogates 4-Bromofluorobenzene (S) ill % 70-130 1 11102118 12:28 460-00-4 1 .2-Dichloroethane-d4 (S) 87 % 70-130 1 11102/18 12:28 17060-07-0 Toluene-d8 (S) 113 % 70-130 1 11/02/18 12:28 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 Pace Analytical Services„ LLC p+al' 9800 Kinney Ave. Suite 100 c yt tr Hunter uitle, NC 28078 wwwp"krts cm (704)875-9092 ANALYTICAL. RESULTS Project: CARCOLINATHEATER Pace Project No.: 92405744 Sample: TK-6 Lacs ID. 92405744001 Collected: 11/02/18 09:45 Received: 11/02/18 10:35 Matrix: Water Parameters Results units Report Limit DF Prepared Analyzed CAS No. Qual $260 MSV Low Level Analytical Method: EPA 82608 Acetone NO ug/L 25.0 1 11/02/18 12:28 67-64-1 Benzene NO ug/L 1.0 1 1110211812:28 71-43-2 Brom benzene NO uglL 1.0 1 11/02/18 12:28 108-86-1 Bromochloromethane- NO ug/L 1.0 1 11/02/18 12:28 74-97- Bromodichloromethane NO ug/L 1.0 1 1110211812:28 7-27-4 Bromoform NO ug/L 1:0 1 11102118 12:28 7 -25-2 Bromomethane NO ug/L 2.0 1 11/02/18 12:28 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 11102/18 12:28 7-93-3 Carbon tetrachloride NO ug/L 1.0 1 11102/18 12:28 5 -23-5 Chlorobenzene NO ug/L 1.0 1 11102/18 12:28 108-90-7 Chloroethane NO ug/L 1.0 1 11/02118 1:28 7 -00-3 Chloroform NO ug/L 1:0 1 11/02/18 12:28 6-66-3 Chloromethane 21 ug/L 1.0 1 11102/18 12:28 74-87- 2-Chlorotoluene Ni ug/L 1.0 1 1110211812:28 95-49-8 4-Chl rotoluene NO ug/L 1.0 1 11/02/18 12:28 106-4 -4 1,2-Dibromo-3-chloropropane NO ug/L 2.0 1 1110211812:28 96-12-8 Dibromochlorornethane ND ug/L 1.0 1 11102/18 12:28 124-48-1 1,2-D bromoethane (EDB) NO ug/L 1.0 1 11102/18 12.2 1 6-93-4 Dibromomethane NO ug/L 1.0 1 11/021181228 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 11/02/18 12:28 9 -50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 11/02118 12:28 541-73-1 1,4-DCchlorobenzene NO ug/L 1'0 1 11/02/18 12:28 106-46-7 Dichlorodifiuoromethahe NO ug/L 1:0 1 11/02/18 12:28 75-71-8 1,1-Dichloroethane NO ug/L 1 0 1 11/02/18 12:28 7 -34-3 1,2-Dichloroethane NO ug/L 1'0 1 11/02/18 12:28 107-06-2 1,1-Dichloroet ene NO ug/L 1.0 1 11/02/18 12:28 7 - 5-4 cis-1,2-Dichloroethene NO ug/L 10" 1 11/02/18 12:28 156-59- trans- 1,2-Dichloroethene NO ugJL 1.0 1 11/02/18 12:28 156-60-5 1,2-Dichloropropane NO ug/L 1:0 1 11102/1812:28 78-87-5 1,3-Dichloropropane NO ugJL 10 1 11102/18 12:28 142-28-9 2,2-Dlchloropropane ND ug/L 1:0 1 11102/18 12:28 594-20-7 1,1-Di hloropropene NO ug/L 1.0 1 11/02118 12:28 563-58-6 cis-1,3-Dichtoropropene NO ug/L 1.0 1 11/02118 12:28 10061-01- trans-1,3-Dichloropropene NO ug/L 1.0 1 11/02/18 12:28 10061-02-6 Dlisopropyl ether ND ug/L 1.0 1 11/02/18 12:28 108- 0- Ethylbenzene NO ug/L 1.0 1 11/02/18 12:28 100-41.4 Hexachloro-1.3-butadiene ND ug/L 1:0 1 11/02118 12:28 87-68-3 2-Hexanone NO ug/L 5.0 1 11/02/18 12:28 591-78-6 p-lsopropyltoluene NO ug/L 1.0 1 11/02/18 12:28 99-87-6 Methylene Chloride NO ug/L 2.0 1 11/02118 12:28 75-09- 4-Methyl-2-pentanone (MIRK) NO ug/L 5.0 1 11/02118 12:28 108-10-1 Methyl-tert-butyl ether NO ug/L 10 1 11/02118 12:28 634-04- Naphthalene NO ug/L 1.0 1 11/0211812:28 91-20-3 Styrene NO ug/L 10 1 11102118 i12:28 100-42-5 1,1,1;2-Tetrachloroethane NO ug/L 1.0 1 11/02/18 12:28 630-20-6 1,1,2,2-Tetrac loroethane NO ug/L 1.0 1 11/02118 12:28 79-34-5 Tetrachloroethene NO ug/L 1:0 1 11/02118 12:28 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /06/2018 01:47 "PM without the written consent of mace Analytical Services, PLC, Page 4 of 16 Pace Analytical Services, LLC /gy 9800 Kincey Ave. Suite 100 C1p �� ij Huntersville, NC 28078 wwwpacslacsoom (704)87-a-9092 SAMPLE ANAL TE COUNT Project` GAROLINATHEATER Pace Project No.. 92405744 Analytes Lab ID Sample Ili Method Analysts Reported Laboratory 9240 744001 TIC-6 EPA 8260B GAW 63 PAST-G 92406744002 TK-7 EPA8260B GAW 63 PA I-G REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 16 Pace Anaiyticat ervicos, LLC 9800 Kincey Ave. Suite 100 ace"IyAcal Huntersville, NC 28078 wwwpoosiatimm (704)875-9092 CERTIFICATIONS Project: CAROLINA THEATER Pace Project No,: 92405744 Charlotte Certification lDs 9800 Kincey Ave, Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA1 70028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Cerfification #,, 37706 Kentucky UST Certification * 84 North Carolina Field Services Certification #' 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification * 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LAC. Page 2 of 16 // Pace Analytical Services; LLC incey Ave. Suite 100 aC ?r 1�1 980{iH ntersville, NC 28078 wwwpscews cam (704)875-9092 November 06, 2018 Joe Nestor ECS Southeast 1812 Center Park Drive Suite D Charlotte, NC 28217 RE. Project: CAROLINA THEATER Pace Project No.. 92405744 Dear Joe Nestor: Enclosed are the analytical results for sample(s) received by the laboratory on November 02, 201& The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell tsylor.ezell@pacelabs.com (704)8 5-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 16 DEQ / D / NPDES Quick Facts — EAA Review NPDES Permit NCO089842 Emil DelDuco, Compliance & Expedited Permitting Unit / 91-707-9125 08NOV2018 Carolina Thea:... *e• ,230 North Tryon® 1 I III III / iindustrial,..,. , 4 f� . privatelyowned, .. P. o'.. classified r > i a in Creek IIII Rj u k8- PUjj iI ...�� 4.. Impaired u for III j Charlotte a N Facifill Description: This permit was requested in the event that excavation activities during the restoration of Carolina Theatre lead to contact with contaminated groundwater. Groundwater samples in 206 and 2007 showed VOC contamination above NC groundwater standards. Samples in June 2018' indicated. VOC concentrations have fallen below standards. If contaminated groundwater is encountered, it will be treated and discharged to stormwater system, which discharges to UT Irwin Creek. Treatment Components a temporary dewatering and groundwater remediation system for during construction consisting of, 0 9000 gallon steel mini frac settling tank 0 5 horsepower transfer pump * Bag filter skid with 2 bag filters (25 micron) * 2 ProAct/Carbonair MPC 131PC liquid phase carbon adsorber in series (1300 lbs GAC each) * A hose kit and flow totalizer Feasible Alternatives: 1. Connect to W WTP — City of Charlotte prohibits discharge of groundwater to POTW 2. Land application — parcel of land is only 95 feet wide (0.434 acres). Neighboring properties are valued at $5 Million +, not considering demolition costs. 3. Wastewater reuse — Not practical given duration of project (<1 month) 4. No viable combinations of aforementioned alternatives 5. Surface water discharge — optnon of ECS that this is the only viable option given the short duration of the project, costs of alternatives, and ,prohibitions to other discharge options. EC knows of similar dewatering projects in area that have been approved (NCO088371, NCO089443, NCO089656). Did not do 20 year PVCA for other alternatives. Carolina Theatre ECS Project No. 6819 Treatment Components Bag Filter Bag Filter KrystilKlear KrystilKlear Carbonair Carbonair' Model .88or Model 88or ModelMPC13/PC13 ModelMPC13/PC13 Equal. Equal GAC Vessel or GACVessel or (25 micron (25 micron Equal Equal Holding/Settling Tank element) element) (1,300I.BSGAC) - (1,300 LBS GAC) 5,000-Gallon FracTank or Equal F --* - - :From :Excavation Transfer Pump To Stormwater 5-HP Single Phase System Rated at Min flow 50 gpm @ 98' TDH Rated at Mac flow140 gpm @ 80' TDH or Equal State of North Carolina Division of Water Resources Water Quality Regional Operations Section Environmenuil Staff Report Quality To: E NPDES Unit ❑ Nun -Discharge Unit Application No.: (NCO089842) Attn: (Emir DelDuco inRaleigh) Facility name: Charlotte Theatre From: Edward Watson Mooresville Regional Office Nate: This form has been ada ted from the non -discharge facility staff report to document the review of both non - discharge and NPDES permit a = lications and/or renewals. Please com fete all sections as they are applicable. I. GENERAL AND SITE VISIT INFORMATION I . Was a site visit conducted? E Yes or (D No a. Date of site visit: 12/20/201 b. Site visit conducted by: Edward Watson and Maria Schutte c. Inspection report attached? ❑ Yes or E No d. Person contacted: Richard Grubbs and their contact information: (704) 973 - 4503 ext. e. Driving directions: Travel south on 1-7 for a rox. 20 miles and take exit I I NC-16/1-277/ Brookshire ?~ . Turn left toward downtown Charlotte and mere onto NC- 16S exit I I -A. Continue on NC-16 S for '1.1 miles and take exit 313 toward Church t/Tryon St. Merge onto w I I th St and take the first right onto N. Tryon St. 230 N. T on is on the left just Dast E 6th St 2. Discharge Point Latitude:35.233595 Longitude:-80.846685 Latitude: Longitude: 3. Receiving stream or affected surface waters: Irwin Creek Classification: C River Basin and Subbasin No. 11.137.1 Describe receiving stream features and pertinent downstream uses. Impaired with metals, Lead, Copper and Zinc. II. PROPOSED FACILITIES: NEW APPLICATIONS I. Facility Classification: PC I is anticipated as this is groundwater treatment Proposed flow: 28,800 god maximum flow. Current permitted flaw: N/A. This is anew permit. 2. Are the new treatment facilities adequate for the type of waste and disposal system? E Yes or El No If no, explain: The proposed treatment spears to be adequate for the type of contaminants erected. 3. Are site conditions (soils, depth to water table, etc.) consistent with the submitted reports? ® Yes ❑ No 0 N/A If no, please explain: 4. Des the plans and site map represent the actual site (property lines, wells, etc.)? ® Yes Q No C] N/A If no, please explain: FORM: WQROSSR 04-1.4 Page I of 3 ENV Is the proposed residuals management plan adequate? ❑ Yes ❑ No ® N/A If no, please explain: This is not a Non -Discharge hermit application. 6. Are the proposed application rates (e g., hydraulic, nutrient) acceptable? Q Yes ❑ No Z N/A If no, please explain. This is not a Non -Discharge permit application. 7. Are there any setback conflicts for proposed treatment, storage and disposal sites? ❑ Yes or E No If yes, attach a map showing conflict areas. NIA. 8. Is the proposed or existing groundwater monitoring program adequate? El Yes ❑ No Z N/A If no, explain and recommend any changes to the groundwater monitoring program. 9. For residuals, will seasonal or ether restrictions be required? ❑ Yes ® No Z N/A If yes, attach list of sites with restrictions (Certification I3) Describe the residuals handling and utilization scheme: 10. Possible toxic impacts to surface waters: Only in the event of a treatment system failure. IL . Pretreatment Program (POTWs only); N/A III. REGIONAL OFFICE RECOMMENDATIONS 1. Do you foresee any problems with issuance/renewal of this permit? ❑ Yes or Z No If yes, please explain: 2. List any items that you would like the NPDES Unit or Non -Discharge Unit Central Office to obtain through an additional information request: Item Reason 3. List specific permit conditions recommended to be removed from the permit when issued Condition Reason 4. List specific special conditions or compliance schedules recommended to be included in the permit when issued: Condition Reason I Chronic Toxicity Monitoring to be performed during periods of batch discharge. FORM: WQRQSSR 04-14 Page 2 of PP5. Recommendation: Ej Hold, pending receipt and review of additional information by regional office E] Hold, pending review of draft permit by regional office ❑ Issue upon receipt of needed additional info anon Issue [] Deny (Please state reasons. 6. Signature of report preparer: Edward Watson I /I >/i2019 Docuftned by: Signature of regional supervisor: A11 p` Date: 1/ 16/ 19 K sss FaesaaD84A3... ADDITIONAL REGIONAL STAFF REVIEW ITEMS There is an existing 2-inch diameter PVC pipe that enters the storm drain from a dis-used irrigation vault that should be capped to prevent unnecessary discharge from entering into the storm drain. On December 20, 2018 MRO staff performed a technical assistance site visit for permit application NCO089842, Carolina. Theatre. O staff met with ECS Limited Staff, Joe Nestor and Chris t rrell, and Mr. Richard Grubbs of Carolina "Theatre. The primary purpose of this permit is to cover a temporary dewatering system to be used during construction where the groundwater is impacted by chlorinated solvents. The City of Charlotte/Charlotte Water dries not allow the discharge of groundwater remediation system effluent into their collection system and WWTPs. The proposed system is designed to be operated sporadically with discharge to an established storm drain outfall. Treatment of the water appears to meet requirements to reduce the pollutants, though the most recent data does not note exceedances of those constituents. The storm drain outfall leads to an impaired stream (Irwin Creek). Due to the irregularly occurring flow, it is recommended that chronic toxicity sampling be tied to periods when discharge actually occurs and that the permittee provide additional information about the quantity and frequency of the flow when the operation is put in place. FORM: WQROSSR 04-14 Page 3 of WELL ABANDONMENTRECORD For Internal Use ONLY: 1. Well Contractor Information: WELL ABANDONMENT DETAILS Jeffrey Grant 7a. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same Well Contractor Name (or well owner personally abandoning well on his/her property) well construction/depth, only I GW-30 is heeded. Indicate TOTAL NUMBER of 4328-g wells abandoned: NC Well Contractor Certification Number 7b. Approximate volume of water remaining in well(s): (gal.) JG Drilling, LL,C FOR WATER SUPPLY WELLS ONLY. Company Name 2. Well Construction Permit #: 7000523 7c. Type of disinfectant used: List all applicable well construction permits (i.e. UlC, County, State, Variance, etc.) itknown ?d. Amount of disinfectant used: 3. Well use (check well use); Water Supply Well: 7e. Sealing materials used (check all that apply) ❑Agricultural ❑Municipal/Public IN Neat Cement Grout 0 Bentonite Chips or Pellets ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply(single) ❑ Sand Cement Grout ❑ Dry Clay ❑Industrial/Commercial ❑Residential Water Supply (shared) ❑ Concrete Grout ❑ Drill Cuttings ❑Irri ation ❑ Specialty Grout ❑ Gravel Non -Water Supply Well: ❑ Bentonite Slurry ❑ Other (explain under 7g) IlMonitoring ❑Recovery Injection Well: 7£ For each material selected above, provide amount of materials used: ❑Aquifer Recharge ❑Groundwater Remediation Portland Cement 65 lbs. ❑Aquifer Storage and Recovery ❑Salinity Barrier ❑Aquifer Test ❑Stormwater Drainage Bentclnite li? . ❑Experimental Technology ❑Subsidence Control 7g. Provide a brief description of the abandonment procedure: ❑Geothermal (Closed Loop) ❑Tracer ❑Geothermal (Heatin Coolie Return) ❑Other (explain under 7) Trenmle grout neat Cement grout from, bgs. to groundaurface. 4. Date well(s) abandoned: 7-1$-18 5a. Well location: Carolina Theatre Facility/Owner Name Facility ID# (if applicable) 8. Certification: 101 E. 6th Street, Charlotte, NC 28217 7-1 8-18 Physical Address, City, and Zip signature of Certified Well Contractor or Well Owner Date Mecklenburg By signing this form, 1 hereby certify that the well(s) was (were) abandoned in County Parcel Identification No. (PIN) accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction ,Standards and that copy of this record has been provided to the well owner. 56. Latitude and longitude in degrees/minutes/seconds or decimal degrees: of'well field, one tat/long is sufficient) 9. Site diagram or additional well details: 35.2283a2 $(�. $G) (}tl" % You may use the back of this page to provide additional well site details or well N W abandonment details. You may also attach additional pages if necessary. CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED SUBMITTAL INSTRUCTIONS Attachw^ellconstructionrecords)ifin,ailable. For multiple uye.chon or non -water supply wells ONLY with the :same construction abandonment, your can submit one, form. 10a. For All Wells: Submit This Form within 30 days of completion of well 6a. Well ID#: Unknown abandonment to the following: Division of Water Resources, Information Processing Unit, 6b. Total well depth: 40 (ft.) 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Injection Wells: In addition to sending the form to the address in 10a 6c. Borehole diameter: (in) above, also submit one copy of this form within 30 days of completion of well abandonment to the following: 6d. Water level below ground surface: 2.21 ft.)" ( Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 None 6e,'Outer casing length (if known): (fit.) 10c. For Water Supply &'Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where 6f. Inner casing/tubing length (if known): 0 (ft.) abandoned. 6g: Screen length (if known): 10 (ft.) Forin GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2.22-2016 f Carolina Theatre s ♦. MGD )8NOV2018 I ype 411 W kc privately owned, 1.0 M D Facility glass PC-1 (not classified) County Mecklenburg Permit Status New li egi RO Office Stream Characteristics Deceiving Stream Ur to Irwin Creek Stre Classification C Stream Segment 11-137-1 Drainagebasin Catawba Summer,7Q1O (cfs) 0 Sub in [ 03 C) 8-32 [05 030501030101 ] Winter 7QIO (cfs) 0 Use Support Impaired for 30Q2 (cfs) 0 303(d) Listed Cu, Ph & Zn Average Flow (cfs) 0 State grid G 15N IWC (0/0) % USGS `l±`opo Quad Charlotte F, Facility Description: This permit was requested in the event that excavation activities during the restoration of Carolina Theatre lead to contact with contaminated groundwater. Groundwater samples in 2006 and 2007 showed VOC contamination above NC groundwater standards. Samples in June 2018 indicated VOC concentrations have fallen below standards. If contaminated groundwater is encountered, it will be treated and discharged to stormwater system, which discharges to UT Irwin Creek. Treatment Components a temporary dewatering and groundwater remedia ion system for during construction consisting of; * 9000 gallon steel midi frac settling tank * 5 horsepower transfer pump Bag filter skid with 2 bag filters (25 micron) * 2 ProActlCarbonair MPC 13IPC liquid phase carbon also ber in series (1300 lbs GAC each) a A hose kit and flow totalizer Feasible Alternatives. 1 Connect to WWTP -- City of Charlotte prohibits discharge of groundwater to P r ' 6" DF a€>s � x Pace Analytical Services, LLC / j e 9870 Klncey Ave Suite 100 Huntersv[Ile, NC 28078 > (704)875-9092 F November 06, 2018 Joe Nestor CS Southeast 1`812 Center Park Drive Suite l Charlotte, NC 28217 Rig: Project: CAROLINATHEATER Pace Project No.. 92405744 Gear Jae Nestor: Enclosed are the analytical results for sample(s) received by the laboratory on November 02, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor Ezell to lor.ezellC,.r' cel bs,co IORATORY ANALYSIS ae reproduced, except in full, ! of Pace Analytical Services, LAG. Page 1 of 16 Pace Analytical:Services, LL 9800 Kincey Ave. Suite 100 Huntersville, NO 28078 www,paMabs,wm (704)875-9092 CERTIFICATIONS Project: CAROLINA THEATER Pace Project No,: 92405744 Charlotte Certification IDs 9800 Kincey Ave, Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NEkAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Chinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification : 5342 Virgini FLAP Certification * 460221 North Carolina Wastewater Certification #: 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 1 a 1�zAnalytical* Project: CAROLINATHEATER Pace Project No,: 92405744 Lab ID Sample ID 92406744001 TK-6 924067 02 TK-7 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Analytes Method Analysts Reported Laboratory EPA8260B GAW 63 PASI- EPA 8260B t3AW 63 PAST-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full„ without the written consent of Pace Analytical Services, LLC. Page 3 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite'100 00 Huntersville, NC 28078 Wmempecewscom (704)875-9092 ANALYTICAL RESULTS , Project: CARt7LINATHEATER Pace Project No.., 92405744 Sample: TK-6 Lab lD: 92406744001 Collected: 11/02118 09:45 Received: 11/02/18 10:35 Matrix: Water Parameters. Results Units Report Limit OF Prepared Analyzed CAS No Cual $260 M SV Low Level Analytical Method: EPA 8 608 Acetone ND ug/L 25.0 1 11/02118 12:28 67-64-1 Benzene NO ug/L 1.0 1 11/02118 12:28 71-43-2 Bromobenzene NO ug/L 1.0 1 11/02/1812:28 108-86-1 Bromochloromethane NO ugIL 1,0 1 11/02/181 :28 74-97-5 Bromodichloromethane NO ug/L 1.0 1 11/02/1812:28 7-27-4 Bromoform ND ug/L 1.0 1 11/02/1812:28 75-25-2 Bromomethane NO ug/L 2:0 1 11/0/1812:28 74-8-9 2-But none (MEK) NO ug/L 5.0 1 11/02118 12:28 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/0211812:28 56-23-5 Chlorobenzen NO ug/L 1.0 1 11/02/1812:28 108-90-7 Chloroethane NO ug1L 1.0 1 11/0211 12:28 75-00-3 Chloroform NO ug/L 1.0 1 11/02/1812:28 67-66- hloromethane 2.7 ug/L 1.0 1 11/02/1812:28 4-87- 2-Chlorotoluene ND ug/L 1.0 1 11/02118 12:28 95-49-8 4-Chlorotoluene NO ug/L 1:0 1 11/02/1812:28 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2;0 1 11/02118 12:28 96-12-8 Dbromochlorr methane NO ug/L 1:0 1 11/02/1812:28 124-48-1 1,2-Dibromoethane ( DB) NO ug/L 1:0 1 11/02118 12:28 106-93- Dibromomethane NO ug/L 1.0 1 11/02/1812:28 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 1110211812:28 9 -50-1 1,3-Dichlorobenzene ND ug/L 1.0= 1 11/02/1812:28 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 11/02/1812:28 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 11/02118 12:28 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11102/1812:28 7 -34-3 1,2-Dichloroethan ND ug/L 1.0 1 11/02/1812:28 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 11102/1812:28 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 11102/1812:28 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/02/1812:28 1 6-60-5 1,2-Dchloropropane NO ug/L 1.0 1 11/02/1812:28 78-87-5 1,3-Dchloropropane ND ug/L 1.0 1 11102/1812:28 12-8-9 2,2-Dichloropropane ND ug/L 1.0 1 11/02118 12:28 5 4-20-7 1, 1 -Dichloropropene NO ug/L 1.01 11/02118 12:28 5 3-58-6 cis-1,-Dichloropropene NO ug/L 1.0 1 11/02/1812:28 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/02118 12:28 10061-02-6 Diisopropyl ether NO ug/L 1.0 1 11/02118 12:28 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/02118 12:28 100-41-4 Hexachloro-1,3-butadiene NO ug/L 1.0 1 11/02/1812:28 87-68-3 -Hexanone NO ug/L 5.0 1 11/0211812:28 591-78-6 p-isopropyltoluene NO ug/L 1.0 1 11/0211812:28 99-87-6 Methylene Chloride NO ug1L 2.0 1 11/02118 12:28 75-09-2 4-Methyl-2-pentanone (MIRK) NO ug1L 5.0 1 11/02/1 12:28 108-10-1 Methyl -tent -butyl ether ND ug/L 1,0 1 11/02/1 12:28 1634-04-4 Naphthalene ND ug/L 1.0 1 11/02118 12:28 91-20-3 Styrene NO ug1L 1'0 1 11/02/1812:28 100-42-5 1,1,12-Tetrachloroethane NO ug/L 1.0 1 11/02/11:28 630-20-6 1,1,22-Tetrachloroethane ND ug/L 1.0 1 11/02118 12:28 79-34-5 Tetrachloroethene ND ug/L 1.0 1 1110 /1812:28 1 7-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full; Date: 11106/2018 01:47 PM without the written consent of Pace Analytical Services, LLG. Page 4 of 1 Pace Analytical Services, LLC + e 1!�?CeAnalytical 9800 Kincey Ave, Suite:100 Huntersville, NC 8078 WWW'Pacalobstom (704)875-9092 ANALYTICAL RESULTS Project: CAROLINA THEATER Pace Project No,: 92405744 Sample: TK 6 Lab lD: 92405744001 Collected: 11/02118 09A5 Received. 11102/18 10:35 Matrix: Water Parameters Results Units Report Limit ' Dl= Prepared Analyzed CAS No, Qual 260 MISV Low Level Analytical Method EPA 82608 Toluene 1.3 ug]L 1.0 1 11102/1812:28 108-88-3 1,2,3-Trichlorobenzene ND ug1L 1.0 1 11/0211812:28 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/02/1812:8 10-8-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11/0211812:28 71-55-6 1,1,2-Tdchloroethane NO ug/L 1.0 1 11102/18 1:28 79-00-5 Trichloroethene NO ug1L 1.0 1 11/02/1812:28 7-01-6 Trichlorotiuoro thane ' ND ug/L 1.0 1 11/02/1812:28 75-69-4 1,2,3-Trichloropropane NO ug/L 1.0 1 11/02/1812:28 96-18-4 Vinyl acetate NO ug1L 2.0 1 11/0211812:28 108-05-4 Vinyl chloride - ND ug/L 1.0 1 11/02/1812:28 75-01-4 ylene (Total) ' NO ug/L 1.0 1 11/02/18 12:28 1330-20-7 m&p-Xylene NO ug/L 2D 1 11102/1 12:28 179601-2 -1 o-Xyle e NO ug/L 1.0 1 11/0211 12:28 95-47-6 Surrogates 4-Srornofluoro enzene (S) 111 % 70-130 1 11/0211812:28 460-00-4 1,2-Dichloroethane-d4 (S) 87 % 70-130 1 11/02/18 1 :28 17060-07-0 Toluene-d8 (S) 113 % 70-130 1 11/02118 12:28 037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date:/1106/2018 01 A7 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 d = j An l ticaf) w, Pate Analytical Services, LLC 9800 Kincey Ave, Suite:100 Huntersville, NC 28078 (704)875-092 Project: CAROLINA THEATER Pace Project No.: 92405744 Sample: TK.7 Lab ID: 92405744002 Collected: 11102118 09:5 Received: 11/02/18 10: 6 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260B Acetone ND ug/L 25,0 1 11/0211813:01 67-64-1 Benzene NO ug/L 1.0 1 11/02/1813:01 71-43-2 Bromobenzene NO ug/L 1.0 1 11/02/1813:01 108-86-1 Bromochloromrthane NO ug/L 1:0 1 11/02/1813:01 74-97-5 Bromodichloromethane ND ug/L 10 1 11/02/1813:01 75-27-4 Bromoform ND ug/L 10 1 11/0211813:01 5-25-2 Brornomethane NO ug/L 2.0 1 11102/1813:01 7 -8 -9 -Butanone (MEK) ND ug1L 5.0 1 11/0211813,01 78-93- Carbon tetrachloride- NO uglL 1.0 1 11/02/1813:01 5-23-5 Chlorobenzene NO ug/L 1.0 1 11/02/1813:01 108-90-7 Chloroethane NO ug/L 1.0 1 11/02/18"13:01 75-00-3 Chloroform NO ug1L 1.0 1 11/02/1813:01 67-66-3 Chloromethane 2.6 ug/L 1.0 1 11/02/1813:01 74-87-3 -Chlorotoluene ND ug/L 1:0 1 11/0211813:01 95-49-8 - 4-Chlorotoluene NO ug/L 1:0 1 11/02/1813:01 106-43- 1,2-Dbromo-3-chloropropane NO ug/L 2,0 1 11/02/1813:01 96-12- Dibromochloromethane NO ug1L 1.0 1 11/02/1813:01 124-48-1 1,2-Dbromoethane (EDB) ND ug/L 1.0 1 11/02/1813:01 106-93-4 Dibrormomethane NO ug/L 1:0 1 11/02/1813:01 74- 5-3 1,2-Dchlorobenzene NO ug/L 1.0 1 11/02/1813:01 95-50-1 1,3-Dchiorobenzene NO ug/L 1.0 1 11/02/1813:01 541-73-1 1,4-Dlchlorobenzeno ND ug/L 1.0 1 11/0211813:01 106-46-7 Dlchlorodifluoromethane NO ug/L 1:0 1 11/02/181:01 75-71-8 1,1-Dlchloroethane NO ug/L 1.0 1 11/02/18;13:01 75-34-3 1,2-Dlchloroethane ND ug/L 1,0 1 11/02/1813:01 107-06-2 1,1-Dlchlor thene ND ug/L 1.0 1 11/0211813:01 75-35-4 cis-1, -Dichloroethene NO ug/L 1.0 1 11102/1813:01 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 1110211813:01 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 11/0211813:01 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 11/02/18 13,01 1 2-28-9 2,-Dichloropropane NO ug/L 1:0 1 11/02/1813:01 594-20-7 1,1-Dichloropropene NO ug1L 1.0 1 11/02/1813:01 563-58-6 cis-1,-Dichlorc propene' ND ug/L 1.0 1 11/02118 13:01 10061-01- trans- 1,3-Dichloroprop ne NO ug/L 1,0 1 11/02/1813:01 10061-02-6 Diisopropyl ether NO ug/L 1 0 1 11/02118 13.01 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/02/1813:01 100-41-4 Hexa hloro-1,3-butadiene NO ug/L ID 1 11102/18 1 :01 87-68-3 2-Hexanone ND ug/L 5,0 1 11/02/1813:01 691-78-6 p-Isopropyltoluene NO ug/L 1.0 1 11102/1813:01 95-87-6 Methylene Chloride NO ug/L 2.0 1 11/02/18 13:01 75-09-2 ; 4-Methyl-2-pentanone (MIB) ND ug/L 5D 1 11/02/18'13:01 108-10-1 Methyl -tent -butyl ether NO ug/L 1:0 1 11/0211813:01 1634-04-4 Naphthalene NO ug/L 1.0 1 11/02/1813:01 91-20-3 Styrene ND ug/L 1.0 1 11/02/1813:01 ' 100-42-5 1,1,1,2-Tetrachloroethane NO ug/L 1.0 1 11/02/1813:01 630-20-6 1,1,2,2-Tetrac loroethane NO ug/L 1 0 1 11/02/1813:01 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/02/1813:01 17-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/0612018 01,47 PM without the written consent of lace Analytical Services, LLC, Page 6 of 16 Pace Analytical services, LLC p� Cp"MicalHuntersville, 9800 Kincey Ave. Suite 100 NC 28078 Wwwwcowaom (704)875-9092 ANALYTICAL RESULTS Project: CARQLINATHEATER Pace Project No.: 9405744 Sample: TK-T Lab l0: 92406744002 Collected: 11102/18 09:53 Received: 11/02/18 10 35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 82608 Toluene 1.6 ug/L 1.0 1 11/02/1813:01 108-88-3 1,2,-Trichlorobenzene ND ug/L 1:0 1 11/02/18 13:01 8 -61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/02/1813:01 1 0-8 -1 1,1,1-Trichlorothane ND ug/L 1.0 1 11/02/1813:01 71-55-6 1„1„2-Trichloroethane ND ug/L 1.0 1 11/02/1813:01 7-00- Trichloroethene ND ug/L 1.0 1 11/02/1813:01 79-01-6 Thchlorofluoromethane ND ug/L 1.0 1 11/02/1813:01 75-69-4 1,2,3-Trichloropropane ND ug/t 1.0 1 11/02/1813:01 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/02/18 13:01 108-05-4 Vinyl chloride ND ug/L 1.0 1 11102/1813:01 75-01-4 Xylen (Total) ; ND ug/L 1.0 1 11102/18 13:01 1330-20-7 m&p- ylene ND ug/L 2.0 1 11102/1813:01 179601-23-1 o-Xyl ne ND ug/L 1.0 1 11/02/1813:01 95-47-6 Surrogates 4-Eromofluorobenzene (S) 110 % 70-1 0 1 11/02/1813:01 460-00-4 1,2-Dichloroethane-d4 (S) 92 % 70-130 1 11/02/1813:01 17060-07-0 Toluene-d8 (S) 113 % 70-1 0 1 11/02/18 13:01 20 7-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11106/ 018 01:47 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 Pace Analytical Services, L LC • jaf y // e 4f I�i( 5800 Kincey Ave. Suite trio Huntersville, NC 28078 .... www'pacalabs'act"(704)875-9092 QUALITY CONTROL DATA Protect: CARQLINATHEATER Pace Protect No,: 92405744 QC Batch; 439851 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92405744001, 92405744002 METHOD BLANK: 2416951 Matrix: Water Associated Lab Samples: 92405744001, 92405744002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1„2-Tetrachioroethane ug/L ND 1.0 11102/18 08:05 1, 1, 1 -Trichloroethane ug1L ND 1.0 11/02/18 08:05 1,1,2;2-Tetrachloroethane ug/L ND 1.0 11102118 08:05 1,1,2-Trichloro thane ug/L NO 1.0 11/02118 08:05 1,1-Dichloroethane ug/L NO 1,0 11/02/18 08:05 1,1-Dichloroethene ug/L NO 1.0 11/02118 08::05 1,1-Dichloropropene ug/L NO 1.0 11102/18 08:05 1,2,3-Trichlorobenzene ug/L NO 1,0 11/02118 08:05 1,2,3-Trichloropropane ug1L ND 1.0 11/02/18 08:05 1,2,4-Trichlorobenzene ug/L NO 1.0 11/02/18 08:05 1,-Dibromo-3-chloropropane ug/L ND 2.0 11102/18 08:05 1,2-Dbromoethane (EDB) ug/L NO 1.0 11/02118 08:05 1,2-Dichlorobenzene uglL ND 1,0 11/02118 08:05 1,2-Dichloroethane ug/L ND 1.0 11/02/18 08:05 1,2-D chloropropane ug/L NO 1,0 11/02/18 08:05 1,3-Dichlorobenzene ug/L NO 1.0 11/02118 08:05 1,3-Dichloropropane ug/L NO '1.0 11/02/1808:05 1,4-Dichlorobenzene ug/L NO 1,0 11/02/18 08:05 2,2-Dichloropropane ug/L NO 1,0 11/02/18 08:05 2-Butanone (MEK) ug/L ND 5.0 11/02/18 08:05 2-Chlorotoluene ug/L NO 1.0 11/02118 08:05 2-Hexanone ug/L NO 5,0 11102/18 08:05 4-Chlorotoluene ugly ND 1.0 11/02118 08:05 4-Methyl-2-pentanone (MIRK) ug/L NO 5.0 11/02/18 08:05 Acetone ug/L NO 25.0 11/02/18 08:05 Benzene ug/L ND 1.0 11102118 08:05 Bromobenzene uglL ND 1,0 11102/18 08:05 Brotmochloromethane ug/L NO 1.0 11/02/18 08:05 Bromodichioromethane ug/L NO 1.0 11/02/18 08:0 Brorroform ug/L NO 1.0 11102118 08:05 Bromomethane ug/L ND 2.0 11/02118 08:05 Carbon tetrachloride ug/L NO 1,0 11/02/18 08:05 Chloroben ene ug/L NO 1.0 11102118 08,05 Chloroethane ug/L NO 1.0 11102/18 08:05 Chloroform ug/L NO 1.0 11/02/18 08:05 Chloromethane ug/L NO 1.0 11102/18 08:05 cis-12-Dichloroethene ug/L NO 1.0 11102/18 08:05 cis-1 3-Dichloropropene ug/L NO 1.0 11102/18 08:05 Dibromochloromethane ug/L NO 1.0 11/02118 08:05 Dibromomethane ug?L ND 1.0 11/02/18 08:05 Dichlorodifluoromethane ug/L ND 1.0 11/02/18 08.05 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11106/2018 01:47'PM without the written consent of Pace Analytical Services, U_C. Page of 16 Pace Analytical Services, LLC wwwpaceltdrs card QUALITY CONTROL. DATA Project: CAROLINA THEATER Pace Project No.: 92405744 METHOD BLANK: 2416951 Matrix:Water Associated Lab Samples: 92405744001,92405744002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dilsopropyl ether ugiL ND 1.0 11/02/18 08,05 L ND 1 n 11/02118 npAnr m ulnek SV111C, m, Gouf o (704)875-9052 mu y(benzene ugl Hexa hloro-1,3-butadiene ug/L ND 1.0 11/02118 08:05 m p-Xylene ug/L ND 2.0 11/02/18 08,05 Meth l-tert-butyl ether ug/L NO 1.0 11/02118 08:0 Methylene Chloride ugtL NO 2.0 11102/18 08:05 Naphthalene ug/L ND 1.0 11/02/18 08:05 o-Xylene ug1L ND 1,0 11102/18 0&0 p-Isopropyltoluene ugiL ND 1.0 11/02/18 08:05 Styrene ug/L ND 1.0 11/02/18 08:05 Tetrachloroethene ug/L NO 1.0 11/02/18 08:05 Toluene ug/L ND 1.0 11102118 08.05 trans-1,2-Dichloroethene ug/L ND 1.0 11102/18 08:05 trans-1,3•Dichloropropene ug/L NO 1.0 1110211808:05 Trichlcoroethene ug/L ND 1.0 11/02118 08 05 Trichlorofluoromethane ug/L ND 1.0 11/02/18 08:05 Vinyl acetate ug/L ND 2.0 11/02/18 08:05 Vinyl chloride ug/L ND 1,0 11/02/18 08:05 ' Xylene (Total) ug/L ND 1 °0 11/02/18 08:05 1,2-Dichloroefhane-d4 (S) % 81 70-130 11/02/18 08,05 4-Bromofluorobenzene (S) °1 111 70-130 11/02/18 08:05 Toluene-d8 IS) % 119 70-130 11/02/18 08:05 LABORATORY CONTROL SAMPLE: 241 952 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 56.5 113 80-12 1, 1, 1 -Trichloroethane ug/L 50 54,5 109 71-129 1,1,2,2-Tetrachloroethane ug/L 50 51.9 104 79-124 1,1, -Tn hloroethane ugiL 50 %6 113 85-125 1, 1 -Dichloroethane u/L 50 56.9 114 73-126 1,1-Dichloroethene ug/L 50 56A 113 66-135 1, 1 -Dichloropropene ug1L 50 54.0 108 74-135 1,2,3-Trichlorobenzene ug1L 50 53,8 108 73-136 1,2,3-Trichloropropane ug/L 50 543 109 75-130 1 „2,4-Trichlorobenzene ug1L 50 53.6 107 75-134 1,2-Dibromo-3-chloropropane ug/L 50 483 97 71-133 1,2-Dibromoethane (EDB) ug1L 50 52.6 105 83-124 1,2-Dichlorobenzene ugiL 50 50.0 100 80-133 1,2-Dichloroethane ug/L 50 57.7 115 67-128 1,2-Dichloropropane ` ugiL 50 58.6 117 75-132 1,3-Dichlorobenzene ugiL 50 51.3 103 77-130 1,3-Dichloropropane ug/L 50 53A 107 76-1 1 1,4-Dichlorobenzene ug/L 50 49.9 100 78-130 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11106/2018 01:47 PM without the written consent of Pace Analytical Services, LLC: Page 9 of 16 Dace Analytical Services, LLC 9800 Kinney Ave. Suite 100 ru lafy "U Nuntersvilie, Ni; 25975 (704)875-9092 QUALITY CONTROLDATA Project: CAROLINATHEATER Pace Project No.: 92405744 LABORATORY CONTROL SAMPLE: 2416952 Spike LCS LC % Rec Parameter Units Conc. Result % Ree Limits Qualifiers 2,2-Dichloropropane ug/L 50 52.1 104 40-160 2-Butanone (MEK) ug/L 100 109 109 61-144 -Chlorotoluene ug/L 50 52.8 106 74-132 2-Hexanone ug/L 100 103 103 68-143 4-Chlorotoluene ug/L 50 52.5 105 76-133 4-Methyl-2-pentanone (MIBK) ug/L 100 103; 103 7 -135 Acetone ug/L 100 117 117 48-146 Benzene ug/L 50 5&3 113 80-125 Bromobenzene ug/L 50 52.6 105 75-12 Bromochloromethane ug/L 50 59A 119 71-125 Bromodichloromethan ug/L 50 54A 109 78-1 4 Bromoform ug/L 50 49.6 99 71-128 Bromomethane ug1L 50 413 83 40-160 Carbon tetrachloride ug/L 50 55,5 11l 69-131 Chlorobenzene ug/L 50 52,0 104 81-122 Chloroethane ug/L 50 44.9 90 9-148 Chloroform ug/L 50 56.5 113 73-127 Chloromethane ug/L 50 45.8 92 44-146 cis-1,2-Dichloroethene ug/L 50 57.6 115 74-124 cis-13-Dichloropropene uglL 50 52.8 106 72-132 Dibromochloromethane ug/L 50 49A 99 78-125 Dibromomethane ug/L 50 511 103 82-120 Dichlorodifluoromethane ug1L 50 42.0 84 34-157 Diisopropyl ether ug/L 50 49.0 100 69-135 Ethylbenzene ' ug/L 50 51.2 ' 102 79-121 Hexachloro-1,3-butadiene ug/L 50 533 107 7 -1 1 m&p-Xylene ug/L 100 105 105 81-124 Methyl-tert-butyl ether ; ug/L 50 51.3 103 74-1 1 Methylene Chloride ug/L 50 60A 121 64-133 Naphthalene ug/L 50 53:6 107 73-13 o-Xylene ug/L 50 53.3 107 79-131 p-isopropyltoluene ug/L 50 51A 103 80-1 1 Styrene ug/L 50 517 107 126 Tetrachloroethene ug/L 50 50A 100 78-122 Toluene ug/L 5o 473 95 80-121 trans-1,2-Dichloroethene ug/L 50 60,0 120 71-127 trans-1,3-Dichoropropne ug/L 50 531 106 9-141 Trichloroethene ug1L 50 52.5 105 78-12 Trichlorofluoromethane uglL- 50 52.2 104 53-137 Vinyl acetate uglL 100 104 ' ' 104 40-160 Vinyl chloride ug/L 50 49,5 99 58-137 Xylere (Total) ug/L 150 159 106 81-126 1,2-Dichloroethane-d4 (S) % 109 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 95 70-130 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date.' 11/06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC, Page 10 of 16 Pace Analytical Services, LLC } f 9800 Kincey Ave. Suite 100 alce lxi t e Huntersviiie, NC 28078 (704)e75- 092 QUALITY CONTROL DATA Project: CAROLINA THEATER Pace Project Na.: 92405744 MATRIX SPIKE SAMPLE: 2416954 92405098006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1.1,1,2-Tetrachloroethane ug/L ND 20 21.4 107 70-10 1, 1, 1 -Trichloroethane ug/L ND 20 22.0 110 70-130 1,1,2,2-Tetrachloroethane ug/L ND 20 23.3 117 70-130 1,1,2-Trichloroethane ug/L ND 20 22.7 113 70-130 1,1-Dichloroethane ug/L ND 20 23,8 119 70=-130 1,1-Dichloroethene ugiL ND 20 25.5 128 70-166 1,1-Dichioropropene ug/L ND 20 %8 99 70-130 1,2,3-Trichlorobenzene ug/L ND 20 19.1 96 70-10 1,2,3-Trichloropropane ugfL ND 20 23.7 119 70-130 1,2,4-Trichlorobenzene, ug/L ND 20 21A 105 70-130 1,2-Dibromo--chloropropane ug/L ND 20 18.4 92 70-130 1,2-Dibromoethane (EDB) ug/L ND 20 19.1 96 70-130 1,2-Dichlorobenzene ug/L NO 20 22.6 113 70-130 1,2-Dichloroethane ug/L NO 20 22.7 113 70-130 1,2-Dichloropropane ug/L ND 20 23.2 116 70-130 1,3-Dichlorobenzene ug/L ND 20 22A 112 70-130 1,-Dichloropropane ug/L ND 20 19.2 96 70-130 1,4-Dichlorobenzene ug/L ND 20 22.9 114 70-130 2,2-Dichloropropane ug/L NO 20 21.6 108 70-130 2-Butanone (MEK) ug/L ND 40 37.0 92 70-130 2-Chlorotoluene ug/L ND 20 22.0 110 70-130 2-Heanone ug/L NO 40 46.6 117 70-130 4-Chlorotoluene ug/L ND 20 22.3 112 70-130 4-Methyl-2-pntanone (MIRK) ug/L NO 40 43.9 110 70-130 Acetone ug/L ND 40 45,2 113 70-130 Benzene a /L NO 20 23.7 119 70-148 Bromobenzene ug/L ND 20 213 109 70-130 Bromochloromethane ug/L ND 20 24,5 122 70-130 Bromodichloro ethane ug/L ND 20 22.5 112 70-130 Bromoform ug/L ND 20 17.2 86 70-130 Bromomethane ug/L ND 20 1&1 80 70-130 Carbon tetrachloride ug/L NO 20 24.3 122 70-10 Chlorpbenzene ug/L NO 20 23.0 115 7-146 Chloroethane' ug/L ND 20 26A 132 70-130 M1 Chloroform ug/L ND 20 211 115 70-130 Chioromethane ug/L ND 20 18.7 94 70-10 cis-1,-Dichloroethene ug/L ND 20 23.6 118 70-10 cis-1,-Dichloropropene ug/L ND, 20 19.7 98 70-10 Dibromochloromethane ug/L NO 20 16.8 84 70-130 Dibromomethane ug/L ND 20 22.6 113 70-130 Dichlorodifluoromethane ugfL ND 20 ` 14.0 70 70-130 Diiisopropyl ether ug/L NO 20 17.3 87 70-130 Ethylbenzene ug/L ND- 20 23.6 118 70-130 Hexachloro-1,3-butadiene ug1L ND 20 22.2 1i1 70-130. m&p- ylene ug/L ND 40 48.8 122 70-130 Methyl-tert-butyl ether ugfL NB 20 17.2 86 70-130 Methylene Chloride ug/L ND 20 262 131 70-130 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01 A7 PM without the written consent of Pace Analytical Services, LLG: Page 11 of 16 Face Analytical Services, LLC f s a�nn i4icat 9800 1(incey Ave. Suite 100 Huntersvilie, NC 28078 Wwwpooews'ann (744)875-9092 QUALITY CONTROL DATA Project: CAROLINA THEATER Pace Project No.: 92405744 MATRIX SPIKE SAMPLE: 2416954 92405098006 Spike MS MS ado Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Naphthalene uglL ND 20 18.9 94 70-130 o-Xylene ug/L NO 20 24.7 124 70-130 p-isoropyltolune ug/L NO 20 2.6 113 70-130 Styrene ug/L NO 20 24.4 122 70-130 Tetrachloroethene ugJL ND 20 21.7 109 70-130 Toluene ug/L NO 20 23.2 116 70-15 trans-1,2-Dichloroethene ug/L NO 20 24.0 120 70-130 trans-1,3-Dichloropropene ug/L ND 20 20.1 101 70-130 Trichtoroethene ug/L NO 20 21A 105 69-151 Trichlorofluorornethane ug/L NO 20 2:0 115 70-130 Vinyl acetate ug/L NO 40 31.0 78 70-130 Vinyl chloride ugJL ND 20 22A 112 70-1 0 Xylene (Total) ug/L ND 60 73.5 122 70-1 0 1,2-Dichloroett ane-d4 (S) ° 106 70-130 4-Brornofluorobenzene (S) °la 106 70-130 Toluene-8 (S) ° 102 0-10 SAMPLE DUPLICATE: 2416953 92405098005 Dup Parameter Units Result Result RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 1,1;1-Thchloroethane ug/L ND NO 1,1,22-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ugIL NO ND 1,1-Dichloroethane ug/L NO NO 1,1-Dichloroethene ug/L NO NO 1,1-Dichloropropene ug/L ND NO 1,2,3-Trichlorobenzene ug/L NO NO 1,2,-Trichloropropane > ug/L ND ND 1,2,4-Thchlorobenzene ug]L ND NO 1,2-Dibromo-3-chloropropane ug/L ND ND 1,2-Dibromoethane (EDB) ug/L ND NO 1,2-Dichlorobnzene ug/L ND NO 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND NO 1,3-Dichlorobenzene ug/L ND ND 1,3-Dichioropropane ug/L NO NO 1,4-Dichlorobenzene ug/L NO NO 2,2-Dichloropropane ug/L ND ND 2-Butanone (MEK) ug/L ND NO 2-Chlorotoluene ugJL ND NO 2-He anone ug/L ND ND 4-Chlorotoluene ug/L NO NO 4-Methyl-2-pentanone (MIRK) ug/L NO ND Acetone ug/L NO NO Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the -result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in: full, Date: 11/06/2018 01:47 PM without the written consent of Pace Analytical Services, LLC, Page 12 of 16 Pace Ana al Services,Lc. f( e Affif di✓ ly 984o Kincey Ave, Suite lido Huntersville, NC 28078 talx. (704)875-9092 QUALITY CONTROL DATA Project: CAROL.INA THEATER Pace Project No.: 9405744 SAMPLE DUPLICATE: 2416953 92405098005 Dup Parameter Units Result Result RPO Qualifiers Benzene ug/L NO .28J , Bromoberlrzene ug/L ND ND Bromochloromethane ug/L NO NO, Bromodichioromethane ug/L ND NO Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon tetrachloride ug/L NO NO Chlorobenzen ug/L NO ND Chloroethane ug/L NO NO Chloroform ug/L ND NO Chloromethane ug/L ND NCB cis- 1,-Dichloroethene = ug/L NO ND cis- 1, 3-Dichloropropeneug/L ND ND Dibromochloromethane ug/L. NO NO Dibromomethane ug/L NO NO Dichlorodifluoromethane ug/L NO NO Diisopropyl ether uglL ND NO Ethylbenzene ug/L ND NO Hexachloro-1,3-butadiene ug/L NO NO m&p-Xylene ug/L ND NO Methyl -tent -butyl ether ug/L ND ND Methylene Chloride ug/L ND ND Naphthalene ug/L NO ND o-Xylene ug/L NO NO p-Isopropyltoluene ug/L NO NO Styrene ug/L NO ND- Tetrachloroethene uglL ND ND Toluene ug/L ND NO trans-1,2-Dichloroethene ug/L ND NO trans-1,3-Dichloropropene ug/L NO ND Trichloroethene ug/L NO NO Trichlorofluoromethane ug/L NO NO Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND NO Xylene (Total) ug1L ND ND 1,2-Dichloroethane-d4 (S) % 86 85 2 4-Bromofluorobenzene(S) % 106 112 6 Toluene-d8 () % 119 117 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:47 PM without the written consent of Pace Analytical Services, LLG, Page 13 of 16 Pace Analyftal Services, LLo 9800 Kincey Ave. Suite 100 l'iv;aCemal0cal HuntersWile, NC 28078 W wPau t ,ec (704)875-9092 QUALIFIERS Project: CAROLINATHEATER Pace Project N.: 92405744 DEFINITION DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration: Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference' NC - Not Calculable. S - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a'combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAG Institute. LABORATORIES PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (_CS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/0612018 01,47 PM wiihout the written consent of Pace Analytioal Services, LLC. Page 14 of 16 Pace Analytical Services, LLC a AwlyticalHuntersvlle, 9800 Kincey Ave. Suite 100 NC 28078 (704)878-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: CAROLINATHEATER Pace Project No.; 92405744 Analytical Lab 1D Sample ID QC Hatch Method QC Batch Analytical Method Batch 92405744001 TK-6 EPA8260B 439851 92406744002 TK»7 EPA'8260B 439851 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date; 11/06/2018 01:47 Pal without the written consent of Pace Analytical Services, LLLC. Page 15 of 1 &J0# 92 CHAIN -OF -CUSTODY Analytituest cal ReqDocument tAB USE ONLY -Affix Worluardisr/D : PkeAnalyftcal- Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevant €elrlsMT" Cornpanv. Billing lnforrxatlon. ALL SHADED At 92409744 Address! container Preservative Type, ';'-6b Project m2 I I I I I -- ----- Report TO: Email To: Preservative Types.(1) nitric acid, (Z) sulfuric acid, (3) hydrocleadc acid, (4S codkir -'FA e 'V (61 methanol, (7) sodium bisuffitte, Rh sodium thiosuffate, (9) hexane, {Al ascorbic at Copy To: Site Collection snfo[Address< (C) ammonium hydroxide, (D) TSPI, (U) Unpreverved, (01 Other Analyses ItAb Proftle/Unt Customer Project Name/Number State. County) ity: Time Zone Collected: Lab SaMP14 f JPT[ IMTt ICT I JET Custody S4 Phone; 17 1# 1 w. Site Facility ID fr, Compliance Monitoring? Custody SJ 'Ll", ( I Yes ]No collector EmaiL Settles IT Putt a s e Order OW PYUS 10 Correct at sufficion t a. C acetate, ulfate, Quo e #: Day Location Co Samples Received on Too Collected By (signature): Turnaround Date Required: frrr rely Parked on ice: v0A - Readspacris Acceptable R Be )ye 5 NO USDA Regulated Soilit Y N ,iia Samples in Holding Time y N Sample Disposal: 7eld T, ftema (if —a police bie): Residual Chlorine Present y N Dirpose as appropriate f I Return Same Day Next Day I Jye5 ( )No C1 Strips: I lArchi_ ve�12 Day [ 13 Day 14 Day ( )5 Day Sample pit Acceptable y N srl strips; (Expedite Charges Apply) Analysis: - ---- --------- - ------- --- ---- - - - ------ ------ PR sulfide Present Y Ui'�A Matrix Codes (insert in Matrix box belpvv). Drinking Water (DW), Ground Water (GW), Wastewater (WW), 'WW)' Lead Acetate strips: (OT Product (P), Soil/Solid (51.), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Smassay (8), Vapor (V), Other (OT) file USE ONLY. Comp Collected (or Res 4 of i Lab sample # Comatents: d Customer Sample ID Matrix Grab Composite Start) Composite End Cl Carts Date Time Date Time - -------- -- . ... . .... . Customer Remarks l Special Conditions Possible Hazards: Type Of Ice Usect Wet Blue Dry None SHORT HOLDS PRESENT (02 hours); Y NN/A Lab Sample Temperature l0w Packing Material Used. Lab Tracking #ts 08_ Temp Blank Received Y tv NA Therm 01h Ther 11426 Cooler I Temp Upon Recelpt-, LL_LOC Samples received via: Cooler I Therm Corr, Factor Radchem sampleb;) screened (<500 cpm)., Y N NA FEDEX UPS I �", 14,nt, 66 �t Courier, Pace Courier Cooler I Corrected Temp. . aC Relan ° ad by/Company; (Signature) Dabt/Turre. Received by/Compony: (Signature) Datettrfirne: MTi. LAB USE ONLY Comments: Table A YX- Arcanum: Tel#wby/Company; (Signature) Dixte/Tirinr Received by/Compaoy; (Signature) Date/Time: Trip Blank Template- Received;Y N NA prelogim, HCL MeOH TSP Other Relinquished by/Ccunpany: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM: Non Cenformance(s)- Page. YES / NO of: