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HomeMy WebLinkAbout20070812 Ver 1_07a - LAB RESULTS (2)_20080502TestAmerica THE LEADER IN ENVIRONMENTAL TESTING, ANALYTICAL REPORT Job Number: 640-14341-1 Job Description: Badin Lake For: Environmental Services, Inc. 1980-A Parker Ct Stone Mountain, GA 30087 Attention: Jason Lancaster t. ' l? Tim Preston Project Manager II timothyr.preston@testamericainc.com 12/21/2007 These test results meet all the requirements of NELAC. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. TestAmerica Tallahassee Florida Department of Health Certification No. E81005 TestAmerica Savannah Florida Department of Health Certification No. E87052 TestAmerica Laboratories, Inc. TestAmerica Tallahassee 2846 Industrial Plaza Drive, Tallahassee, FL 32301 Tel (850) 878-3994 Fax (850) 878-9504 www.teslanle_ricamc.cpm Page 1 of 167 12/21/2007 Job Narrative 640-J14341-1 Comments No additional comments. Receipt Alt samples were received in good condition within temperature requirements. GC/MS Semi VOA The following samples were diluted due to the nature of the sample matrix: R-1, R-1b, R-1c, R-1Dub, R-1 Dub b and R-1Dub c. Elevated reporting limits (RLs) are provided. No other analytical or quality issues were noted, GC Semi VOA No analytical or quality issues were noted. Metals No analytical or quality issues were noted. General Chemistry No analytical or quality issues were noted. Organic Prep No analytical or quality issues were noted. Page 2 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 540-94341-1 R-1 Arsenic 6.3 0.88 mg/Kg 6010B Barium 51 0.88 mg/Kg 6010B Chromium 16 0.88 mg/Kg 6010B Iron 26000 8.8 mg/Kg 6010B Lead 7.6 0.44 mg/Kg 60108 Mercury 0.028 0.017 mg/Kg 7471A Percent Moisture 57 0.010 % PercentMoisture 640-14341-2 R-1 B Arsenic 3.7 0.96 mg/Kg 6010B Barium 41 0.96 mg/Kg 6014B Chromium 14 0.96 mg/Kg 60106 Iron 17000 9.6 mg/Kg 6010B Lead 5.6 0.48 mg/Kg 6010B Percent Moisture 73 0.010 % PercentMoisture 640-14341-3 R-1 C Arsenic 3.5 0.88 mglKg 6010B Barium 39 0.88 mglKg 601OB Chromium 14 0.88 mglKg 6010B Iron 16000 8.8 mg/Kg 6010B Lead 5.8 0.44 mg/Kg 6010B Mercury 0.020 0.017 mg/Kg 7471A Percent Moisture 74 0.010 % PercentMoisture 640-14341-4 RADUB Arsenic 4.7 0.95 mg/Kg 60108 Barium 43 0.95 mg/Kg 60106 Chromium 14 0.95 mg/Kg 6010B Iron 20000 9.5 mg/Kg 6010B Lead 6.0 0.48 mglKg 6010B Mercury 0.021 0.017 mgXg 7471A Percent Moisture 66 0.010 % PercentMoisture TestAmerica Tallahassee Page 3 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-5 Arsenic Barium Chromium Iron Lead Mercury Percent Moisture 640-14341-6 Arsenic Barium Chromium Iron Lead Mercury Percent Moisture R-1 DUB B R-1 DUB C 640-14341-7 BR-1A Anthracene Benzo[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo [g, h, i] perylene Benzo[k]fluoranthene Chrysene Dibenz(a, h)anthrace ne Fluoranthene Indeno[1,2,3-cd]pyrene Phenanthrene Pyrene PCB-1242 PCB-1260 Arsenic Barium Chromium Iron Lead Mercury Cyanide, Total Percent Moisture TestAmerica Tallahassee 4.2 0.93 mg/Kg 6010B 40 0.93 mg/Kg 6010B 14 0.93 mg/Kg 6010B 18000 9.3 mg/Kg 6010B 5.7 0.46 mg/Kg 6010B 0.021 0.019 mg/Kg 7471A 71 0.010 % PercentMoisture 4.1 0.94 mglKg 6010B 38 0.94 mglKg 6010B 13 0.94 mglKg 6010B 17000 9.4 mg/Kg 6010B 5.2 0.47 mg/Kg 6010B 0.019 0.019 mg/Kg 7471A 70 0.010 % PercentMoisture 3200 930 ug/Kg 82700 20000 930 ug/Kg 8270C 20000 930 ug/Kg 8270C 27000 930 ug/Kg 8270C 14000 930 ug/Kg 8270C 15000 930 ug/Kg 8270C 20000 930 uglKg 8270C 5000 930 ug1Kg 8270C 29000 930 ug/Kg 8270C 14000 930 ug/Kg 8270C 9500 930 ug/Kg 8270C 22000 930 ug/Kg 8270C 2400 180 ug/Kg 8081A_8082 520 180 ug/Kg 8081A_8082 2.2 0.87 mg/Kg 6010B 39 0.87 mg/Kg 6010B 10 0.87 mg/Kg 6010B 9000 8.7 mg/Kg 6010B 23 0.43 mg/Kg 6010B 0.047 0.020 mg/Kg 7471A 21 1.4 mg/Kg 9012A 64 0.010 % PercentMoisture Page 4 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-8 BR-1 B Anthracene 3300 950 ug/Kg 82700 Benzo[a]anthrace ne 20000 950 ug/Kg 8270C Benzo[a]pyrene 21000 950 ug/Kg 82700 Benzo[b]fluoranthene 29000 950 ug/Kg 8270C Benzo[g,h,i]perylene 15000 950 ug/Kg 8270C Benzo[k]fluoranthene 14000 950 ug/Kg 8270C Chrysene 22000 950 ug/Kg 8270C Dibenz(a,h)anthracene 5200 950 ug/Kg 8270C Fluoranthene 30000 950 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 16000 950 ug/Kg 8270C Phenanthrene 9800 950 ug/Kg 8270C Pyrene 23000 950 ug/Kg 8270C PCB-1242 2200 190 ug/Kg 8081A_8082 PCB-1260 300 P 190 ug/Kg 8081A_8082 Arsenic 1.6 0.93 mg/Kg 6010B Barium 35 0.93 mg/Kg 6010B Chromium 9.0 0.93 mg/Kg 6010B Iron 8200 9.3 mg/Kg 6010B Lead 17 0.46 mg/Kg 6010B Mercury 0.042 0.019 mg/Kg 7471A Percent Moisture 65 0.010 % PercentMoisture 640-14341-9 BR-1 C Anthracene 3900 990 ug/Kg 8270C Benzo[a]anthrace ne 26000 990 ug/Kg 8270C Benzo[a]pyrene 26000 990 ug/Kg 8270C Benzo[b]fiuoranthene 41000 990 ug/Kg 8270C Benzo[g,h,i]perylene 17000 990 ug/Kg 8270C Benzo[k]fluoranthene 19000 990 ug/Kg 8270C Chrysene 28000 990 ug/Kg 8270C Dibenz(a,h)anthracene 6000 990 ug/Kg 8270C Fluoranthene 38000 990 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 17000 990 ug/Kg 8270C Phenanthrene 12000 990 ug/Kg 8270C Pyrene 29000 990 ug/Kg 8270C PCB-1242 1500 P 190 ug/Kg 8081A_8082 PCB-1260 480 190 ug/Kg 8081A_8082 Arsenic 1.9 0.89 mg/Kg 6010B Barium 36 0.89 mg/Kg 6010B Chromium 9.1 0.89 mg/Kg 6010B Iron 8700 8.9 mg/Kg 6010B Lead 17 0.45 mg/Kg 6010B Mercury 0.035 0.019 mg/Kg 7471A Percent Moisture 66 0.010 % PercentMoisture TestAmerica Tallahassee Page 5 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-10 BR-2A Anthracene 830 210 uglKg 8270C Benzo[a]anthracene 6200 210 ug/Kg 8270C Benzo[a]pyrene 6300 210 ug/Kg 8270C Benzo[b]fluoranthene 8700 210 ug/Kg 8270C Benzo[g,h,i]perylene 4500 210 ug/Kg 8270C Benzo[k]fluoranthene 4100 210 ug/Kg 8270C Chrysene 6300 210 ug/Kg 8270C Dibenz(a,h)anthrace ne 1700 210 ug/Kg 8270C Fluoranthene 8400 210 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 5200 210 ug/Kg 8270C Phenanthrene 2500 210 ug/Kg 8270C Pyrene 6200 210 ug/Kg 8270C Arsenic 2.0 0.85 mg/Kg 6010B Barium 39 0.85 mg/Kg 6010B Chromium 12 0.85 mg/Kg 6010B Iron 12000 8.5 mg/Kg 6010B Lead 13 0.43 mg/Kg 60148 Mercury 0.037 0.017 mg/Kg 7471A Percent Moisture 68 0.010 % PercentMoisture 640-14341-11 BR-2B Anthracene 610 220 ug/Kg 82700 Benzo[a]anthracene 5400 220 uglKg 8270C Benzo[a]pyrene 5400 220 ug/Kg 8270C Benzo[b]fluoranthene 8500 220 ug/Kg 8270C Benzo[g,h,i]perylene 3800 220 ug/Kg 8270C Benzo[k]Fluoranthene 4700 220 ug/Kg 8270C Chrysene 5400 220 ug/Kg 82700 Dibenz(a,h)anthracene 1400 220 ug/Kg 8270C Fluoranthene 6900 220 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 4000 220 ug1Kg 8270C Phenanthrene 2000 220 ug/Kg 8270C Pyrene 5500 220 ug1Kg 8270C Arsenic 23 0.91 mg/Kg 6010B Barium 39 0.91 mg/Kg 6010B Chromium 13 0.91 mg/Kg 6010B Iron 12000 9.1 mg/Kg 6010B Lead 13 0.45 mg/Kg 6010B Mercury 0.033 0.018 mg/Kg 7471A Percent Moisture 69 0.010 % PercentMoisture TestAmerica Tallahassee Page 6 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-12 BR-2C Acenaphthene 230 210 ug/Kg 8270C Anthracene 890 210 ug/Kg 8270C Benzo[a]anthracene 7500 210 ug/Kg 8270C Benzo[a]pyrene 7700 210 ug/Kg 8270C Benzo[b]fluoranthene 11000 210 ug/Kg 8270C Benzo[g,h,i]perylene 5600 210 uglKg 8270C Benzo[ic]fluoranthene 6500 210 uglKg 8270C Chrysene 7300 210 ug/Kg 8270C Di benz(a,h)anthracene 2100 210 ug/Kg 8270C Fluoranthene 10000 210 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 6500 210 ug/Kg 8270C Phenanthrene 2900 210 uglKg 8270C Pyrene 7200 210 ug/Kg 8270C PCB-1254 150 110 ug/Kg 8081A 8082 Arsenic 2.2 0.93 mg/Kg _ 6010B Barium 43 0.93 mg/Kg 6010B Chromium 14 0.93 mg/Kg 6010B Iron 13000 9.3 mg/Kg 6010B Lead 15 0.47 mg/Kg 6010B Mercury 0.034 0.019 mg/Kg 7471A Percent Moisture 69 0.010 % PercentMoisture 640-14341-13 BR-2 DUBA Anthracene 540 210 uglKg 8210C Benzo[a]anthracene 4000 210 uglKg 8270C Benzo[a]pyrene 4500 210 uglKg 8270C Benzo[b]fluoranthene 7000 210 ug/Kg 8270C Benzo[g,h,i]perylene 3200 210 ug/Kg 8270C Benzo[k]ftuoranthene 3800 210 ug/Kg 8270C Chrysene 4300 210 ug/Kg 8270C Dibenz(a,h)anthracene 1200 210 ug/Kg 8270C Fluoranthene 5600 210 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 3300 210 ug/Kg 8270C Phenanthfene 1600 210 ug/Kg 8270C Pyrene 4300 210 ug/Kg 82700 PCB-1254 200 110 ug/Kg 8081A 8082 PCB-1260 120 110 ug/Kg _ 8081A 8082 Arsenic 2.4 0.88 mg/Kg 6010E Barium 42 0.88 mg/Kg 6010B Chromium 14 0.88 mg/Kg 6010B Iron 13000 8.8 mg/Kg 6010B Lead 14 0.44 mg/Kg 60106 Mercury 0.031 0.019 mg/Kg 7471A Percent Moisture 69 0.010 % PercentMoisture TestAmerica Tallahassee Page 7 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-14 BR-2 DUB B Anthracene 630 220 ugXg 8270C Benzo[a]anthracene 4800 220 ug/Kg 8270C Benzo[a]pyrene 4900 220 uglKg 8270C Benzo[b]fluoranthene 7400 220 ug/Kg 8270C Benzo[g,h,i]perylene 3500 220 ug/Kg 8270C Benzo[k]fluoranthene 4800 220 ug/Kg 8270C Chrysene 5100 220 ug/Kg 8270C Dibenz(a,h)anthracene 1300 220 ug/Kg 8270C Fluoranthene 6300 220 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 3700 220 ug/Kg 8270C Phenanthrene 1900 220 ug/Kg 8270C Pyrene 5100 220 uglKg 8270C PCB-1254 170 110 uglKg 8081A 8082 Arsenic 2,1 0.96 mglKg _ 6010B Barium 40 0.96 mglKg 6010B Chromium 13 0.96 mg/Kg 6010B Iron 12000 9.6 mg/Kg 6010B Lead 13 0.48 mg/Kg 6010B Mercury 0.034 0.017 mg/Kg 7471A Percent Moisture 70 0.010 % PercentMoisture 640-14341-15 BR-2 DUB C Anthracene 250 210 ug/Kg 8270C Benzo[a]anthracene 1800 210 uglKg 8270C Benzo[a]pyrene 1900 210 uglKg 8270C Benzo[b]fluoranthene 3000 210 uglKg 8270C Benzo[g,h,i]perylene 1300 210 ug/Kg 8270C Benzo[k]fiuofanthene 1400 210 ug/Kg 8270C Chrysene 1900 210 ug/Kg 8270C Dibenz(a,h)anthracene 480 210 ug/Kg 8270C Fluoranthene 2500 210 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 1300 210 ug/Kg 8270C Phenanthrene 710 210 ug/Kg 82700 Pyrene 1900 210 ug/Kg 8270C PCB-1254 210 100 ug/Kg 8081A 8082 Arsenic 2.1 0.95 mg/Kg 6010B Barium 38 0.95 mg/Kg 6010E Chromium 13 0.95 mg/Kg 6010B Iron 12000 9.5 mg1Kg 6010B Lead 12 0.48 mglKg 6010B Mercury 0.034 0.019 mgXg 7471A Percent Moisture 68 0.010 % PercentMoisture TestAmerica Tallahassee Page 8 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number; 640-14341-1 Lab Sample ID Client Sample ID Analyte Result 1 Qualifier Reporting Limit Units Method 640-14341-16 SA-1 A Anthracene 180 170 ug/Kg 8270C Benzo[a]anthracene 1000 170 ug/Kg 8270C Benzo[a]pyrene 1100 170 uglKg 8270C Benzo[b]fluoranthene 2000 170 uglKg 8270C Benzo[g,h,i]perylene 850 170 ug/Kg 8270C Benzo[k]fluoranthene 760 170 ug/Kg 8270C Chrysene 1100 170 ug/Kg 8270C Dibenz(a,h)anthracene 350 170 ug/Kg 8270C Fluoranthene 1500 170 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 870 170 ug/Kg 8270C Phenanthrene 570 170 ug/Kg 82700 Pyrene 1100 170 ug/Kg 8270C Arsenic 3.6 0.90 mg/Kg 60108 Barium 43 0.90 mg/Kg 6010B Chromium 14 0.90 mg/Kg 60106 Iron 18000 9.0 mg/Kg 6010E Lead 14 0.45 mg/Kg 60106 Mercury 0.030 0.020 mg/Kg 7471A Cyanide, Total 1.9 1.3 mg/Kg 9012A Percent Moisture 61 0.010 % PercentMoisture 640-14341-17 SA-1 B Benzo[a]anthracene 750 180 ug1Kg 8270C Benzo[a]pyrene 830 180 ug/Kg 8270C Benzo[b]fluoranthene 1400 180 ug/Kg 8270C Benzo(g,h,i]perylene 640 180 ug/Kg 8270C Benzo[k]fluoranthene 510 180 ug/Kg 8270C Chrysene 820 180 ug/Kg 8270C Fluoranthene 1100 180 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 630 180 ug/Kg 8270C Phenanthrene 500 180 ug/Kg 8270C Pyrene 890 180 ug/Kg 8270C PCB-1260 89 87 ug/Kg 8081A 8082 Arsenic 3.5 0.92 mg/Kg 60106 Barium 41 0.92 mg/Kg 60106 Chromium 13 0.92 mg/Kg 6010B Iron 17000 9.2 mg/Kg 60108 Lead 13 0.46 mg/Kg 6010B Mercury 0.030 0.018 mg/Kg 7471A Cyanide, Total 1.8 1.3 mg/Kg 9012A Percent Moisture 62 0.010 % PercentMoisture TestAmerica Tallahassee Page 9 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-18 SA-1 C Benzo[a]anthracene 660 170 ug/Kg 8270C Benzo[a]pyrene 780 170 uglKg 8270C Benzo[b]fluoranthene 1200 170 ug/Kg 8270C Benzo[g,h,i]perylene 470 170 ug/Kg 8270C Benzo[k]fluoranthene 670 170 ug/Kg 8270C Chrysene 790 170 ug/Kg 8270C Dibenz(a,h)anthracene 190 170 ug/Kg 8270C Fluoranthene 950 170 ug1Kg 8270C Indeno[1,2,3-cd]pyrene 420 170 ug/Kg 8270C Phenanthrene 370 170 uglKg 8270C Pyrene 690 170 ug/Kg 8270C Arsenic 3.5 0.95 mg/Kg 6010B Barium 39 0.95 mg/Kg 60108 Chromium 12 0.95 mg/Kg 6010B Iron 16000 9.5 mg/Kg 6010B Lead 12 0.48 mg/Kg 60108 Mercury 0.027 0.019 mg/Kg 7471A Cyanide, Total 2.0 1.3 mg/Kg 9012A Percent Moisture 61 0.010 % PercentMoisture 640-14341-19 SA-2 A Benzo[a]anthracene 490 190 uglKg 8270C Benzo[a]pyrene 560 190 uglKg 8270C Benzo[b]fluoranthene 920 190 uglKg 8270C Benzo[g,h,i]perylene 430 190 ug/Kg 8270C Benzo[k]fluoranthene 390 190 ug1Kg 8270C Chrysene 580 190 ug/Kg 8270C Fluoranthene 710 190 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 420 190 ug/Kg 8270C Phonanthrene 280 190 ug/Kg 8270C Pyrene 590 190 ug/Kg 8270C Arsenic 3.1 0.92 mg/Kg 60106 Barium 42 0.92 mglKg 6010B Chromium 13 0.92 mg/Kg 6010E Iron 15000 9.2 mg/Kg 60106 Lead 11 0.46 mg/Kg 6010B Mercury 0.028 0.019 mg/Kg 7471A Percent Moisture 65 0.010 % PercentMoisture TestAmerica Tallahassee Page 10 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job dumber: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result! Qualifier Limit Units Method 640-14341-20 SA-2 B Benzo[a]anthracene 660 180 ug/Kg 8270C Benzo[a]pyrene 720 180 ug/Kg 8270C Benzo[b]fluoranthene 1200 180 ug/Kg 8270C Benzofg,h,i]perylene 590 180 ug/Kg 8270C Benzo[k]fiuoranthene 470 180 ug/Kg 8270C Chrysene 720 180 ug/Kg 8270C Fluoranthene 920 180 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 590 180 ug/Kg 8270C Phenanthrene 340 180 ug/Kg 8270C Pyrene 720 180 ug/Kg 8270C Arsenic 2.5 0.87 mg/Kg 6010B Barium 36 0.87 mg/Kg 6010B Chromium 11 0.87 mg/Kg 60106 Iron 13000 8.7 mg/Kg 6010B Lead 9.1 0.43 mg/Kg 6010B Mercury 0.024 0.019 mg/Kg 7471A Percent Moisture 64 0.010 % PercentMoisture 640-14349-21 SA-2 C Benzo[a]anthrace no 480 190 uglKg 8270C Benzo[a]pyrene 530 190 uglKg 8270C Benzo[b]fluoranthene 820 190 ug/Kg 8270C Benzo[g,h,i]perylene 360 190 ug/Kg 8270C Benzo[k]fluoranthene 340 190 ug/Kg 8270C Chrysene 490 190 ug/Kg 8270C Fluoranthene 600 190 ug/Kg 8270C Indeno[1,2,3-cd]pyrene 350 190 ug/Kg 8270C Phenanthrene 210 190 ug/Kg 8270C Pyrene 540 190 ug/Kg 8270C Arsenic 2.9 0.94 mg/Kg 6010B Barium 41 0.94 mg/Kg 60108 Chromium 13 0.94 mg/Kg 60108 Iron 15000 9.4 mg/Kg 6010E Lead 11 0.47 mg/Kg 6010B Mercury 0.028 0.019 mg/Kg 7471A Percent Moisture 66 0.010 % PercentMoisture TestAmerica Tallahassee Page 11 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-22 SA-3 A Benzo[a]anthracene Benzo]a]pyrene Benzo[b]fluoranthene Chrysene Fluoranthene Pyrene Arsenic Barium Chromium Iron Lead Mercury Percent Moisture 640-14341-23 SA-3 B Benzo[a]anthrace no Benzo[a]pyrene Benzo[b]fluoranthene Benzo]g,h J]peryleno Benzo[k]ftuoranthene Chrysene Fluoranthene Indeno[1,2,3-cd]pyrene Pyrene Arsenic Barium Chromium Iron Lead Mercury Percent Moisture TestAmerica Tallahassee 230 180 uglKg 8270C 260 180 ug/Kg 82700 360 180 ug/Kg 8270C 220 180 ug/Kg 8270C 280 180 ug/Kg 8270C 260 180 ug/Kg 8270C 3.2 0.92 mg/Kg 6010B 44 0.92 mg/Kg 6010B 14 0.92 mg/Kg 6010B 15000 9.2 mg/Kg 6010B 9.0 0.46 mg/Kg 6010B 0.026 0.020 mglKg 7471A 63 0.010 % PercentMoisture 270 170 ug/Kg 8270C 310 170 ug/Kg 8270C 480 170 ug/Kg 8270C 200 170 ug/Kg 8270C 180 170 ug/Kg 8270C 280 170 ug/Kg 8270C 300 170 ug/Kg 8270C 190 170 ug/Kg 8270C 280 170 ug/Kg 8270C 3.4 0.93 mglKg 6010B 47 0.93 mg/Kg 6010B 16 0.93 mg/Kg 6010B 16000 9.3 mg/Kg 6010B 22 0.46 mg/Kg 60108 0.027 0.019 mg/Kg 7471A 60 0.010 % PercentMoisture Page 12 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result / Qualifier Limit Units Method 640-14341-24 SA-3 C Senzo[a]antheacene 270 180 ug/Kg 8270C lenzo[a]pyrene 300 180 ug/Kg 8270C Benzo[b]fluoranthene 450 180 ug/Kg 8270C Benzo[k]fluoranthene 210 180 ug/Kg 8270C Chrysene 260 980 ug/Kg 8270C Fluoranthene 320 180 ug/Kg 8270C Pyrene 300 180 ug/Kg 8270C Arsenic 2.8 0.89 mg/Kg 6010B Barium 43 0.89 mg/Kg 601OB Chromium 14 0.89 mg/Kg 601OB Iron 15000 8.9 mg/Kg 6010B Lead 8.6 0.45 mg/Kg 6010B Mercury 0.027 0.018 mg/Kg 7471A Percent Moisture 64 0.010 % PercentMoisture 640-14341-25 SA-4 A Acenaphthene 1100 910 ug/Kg 8270C Anthracene 3100 910 ug/Kg 8270C Benzo[a]anthracene 21000 910 ug/Kg 8270C Benzo[a]pyrene 23000 910 ug1Kg 8270C Benzo[b]fluoranthene 30000 910 uglKg 8270C Benzo[g,h,i]perylene 16000 910 ug1Kg 8270C Benzo[k]fluoranthene 12000 910 ug1Kg 8270C Chrysene 21000 910 ug/Kg 8270C Fluoranthene 30000 910 ug1Kg 8270C Indeno[1,2,3-cd]pyrene 17000 910 ug1Kg 8270C Phenanthrene 10000 910 ug/Kg 8270C Pyrene 23000 910 ug/Kg 8270C PCB-1254 720 180 uglKg 8081A_8082 Arsenic 2.2 0.88 mg/Kg 6010B Barium 45 0.88 mg/Kg 6010B Chromium 13 0.88 mg/Kg 60108 Iron 13000 8.8 mg/Kg 6010B Lead 13 0.44 mg/Kg 6014E Mercury 0.027 0.019 mg1Kg 7471A Cyanide, Total 2.6 1.4 mg/Kg 9012A Percent Moisture 63 0.010 % PercentMoisture TestAmerica Tallahassee Page 13 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Dumber: 640-14341-1 Lab Sample ID Client Sample ID Reporting Analyte Result 1 Qualifier Limit Units Method 640-14341-26 SA4 B Acenaphthene 1900 920 uglKg 8270C Anthracene 5500 920 ug/Kg 8270C Benzo[a]anthracene 39000 920 ug/Kg 8270C Benzo[a]pyrene 42000 920 ug/Kg 8270C Benzo[b]fluoranthene 58000 920 ug/Kg 8270C Benzo[g,h,i]perylene 29000 920 uglKg 8270C Benzo[k]fluoranthene 21000 920 ug/Kg 8270C Chrysene 37000 920 uglKg 8270C Fluorene 1600 920 ug/Kg 8270C Fluoranthene 53000 920 uglKg 8270C Indeno[1,2,3-cd]pyrene 33000 920 uglKg 8270C Phenanthrene 19000 920 uglKg 8270C Pyrene 39000 920 uglKg 8270C PCB-1254 840 180 uglKg 8081A_8082 Arsenic 2.0 0.93 mglKg 6010B Barium 47 0.93 mg/Kg 6010B Chromium 13 0.93 mg/Kg 6010E Iron 12000 9.3 mg/Kg 6010B Lead 12 0.46 mg/Kg 6010B Mercury 0.027 0.020 mg/Kg 7471A Cyanide, Total 3.0 1.4 mg/Kg 9012A Percent Moisture 64 0.010 % PercentMoisture TestAmerica Tallahassee Page 14 of 167 12/21/2007 EXECUTIVE SUMMARY - Detections Client: Environmental Services, Inc. Job Number; 640-14349-1 Lab Sample ID Client Sample ID Reporting Analyte Result! Qualifier Limit Units Method 640-14341-27 SA-4 C Acenaphthene Anthracene Benzo[a]anthrace ne Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g, h,i]perylene Benzo[k]fiuoranthene Chrysene Fluorene Fluoranthene Indeno[1,2,3-cd]pyrene Phenanthrene Pyrene PCB-1254 Arsenic Barium Chromium Iron Lead Mercury Cyanide, Total Percent Moisture TestAmerica Tallahassee 1700 940 ug/Kg 8270C 4900 940 ug/Kg 8270C 34000 940 ug/Kg 8270C 38000 940 ug/Kg 8270C 56000 940 ug/Kg 82700 25000 940 ug/Kg 8270C 16000 940 ug/Kg 8270C 34000 940 ug/Kg 82700 1400 940 ug/Kg 82700 48000 940 ug/Kg 8270C 27000 940 ug/Kg 8270C 16000 940 ug/Kg 82700 36000 940 uglKg 8270C 880 190 ug/Kg 8081AW8082 2.1 0.96 mg/Kg 6010B 47 0.96 mg/Kg 6010B 13 0.96 mg/Kg 6010B 13000 9.6 mg/Kg 6010B 13 0.48 mg/Kg 6010B 0.029 0.019 mg/Kg 7471A 2.2 1.4 mg/Kg 9012A 65 0.010 % PercentMoisture Page 15 of 167 12/21/2007 METHOD SUMMARY Client: Environmental Services, Inc. Job Number: 640-14341-1 Descri tion Lab Location Method Preparation Method Matrix: Solid Semivolatile Organic Compounds by GCMS - Low Levels TAL SAV SW846 8270C Ultrasonic Extraction TAL SAV SW846 3550B Organochlorine Pesticides & Polychlorinated Biphenyls by Gas TAL SAV SW846 8081A8082 Chromatography Ultrasonic Extraction TAIL SAV SW846 3550B Inductively Coupled Plasma - Atomic Emission Spectrometry TAL SAV SW846 6010B Acid Digestion of Sediments, Sludges, and Soils TAL SAV SW846 3050B Mercury in Solid or Semisolid Waste (Manual Cold Vapor TAL SAV SW846 7471A Technique) Mercury in Solid or Semi-Solid Waste (Manual Cold TAL SAV SW846 7471A Fluoride (Potenliometric, Ion Selective Electrode) TAL SAV MCAWW 340.2 Deionized Water Leaching Procedure (Routine) TAL SAV ASTM DI Leach Total and Amenable Cyanide (Automated Colorimetric, with TAL SAV SW846 9012A Off-Line Distillation) Cyanide Extraction Procedure for Solids and Oils TAL SAV SW846 9013 Total and Amenable Cyanide (Auto. Colorimetric TAL SAV SW846 9012A Cyanide, Weak Acid Dissociable TAL SAV SM18 SM 4500 CN I Cyanide Distillation for Weak Acid Dissociable Cyanide TAL SAV SM20 SM 4500 CN I Matrix: Water Semivolatile Organic Compounds by GCMS - Low Levels TAL SAV SW846 8270C Continuous Liquid-Liquid Extraction TAL SAV SW846 3520C Organochlorine Pesticides & Polychlorinated Biphenyls by Gas TAL SAV SW846 8081A8082 Chromatography l Continuous Liquid-Liquid Extraction TAL SAV SW846 3520C Inductively Coupled Plasma - Atomic Emission Spectrometry TAIL SAV SW846 6010B Acid Digestion of Waters for Total Recoverable or TAL SAV SW846 3005A Mercury in Liquid Waste (Manual Cold Vapor Technique) TAL SAV SW846 7470A Mercury in Liquid Waste (Manual Cold Vapor TAL SAV SW846 7470A Fluoride (Potentiometric, Ion Selective Electrode) TAL SAV MCAWW 340.2 Total and Amenable Cyanide (Automated Colorimetric, with TAIL SAV SW846 9012A Off-Line Distillation) Total and Amenable Cyanide (Auto. Colorimetric TAL SAV SW846 9012A Cyanide, Weak Acid Dissociable TAL SAV SM18 SM 4500 CN I Cyanide Distillation for Weak Acid Dissociable Cyanide TAL SAV SM20 SM 4500 CN I Lab References: TAL SAV = TestAmerica Savannah TestAmerica Tallahassee Page 16 of 167 12/21/2007 METHOD SUMMARY Client: Environmental Services, Inc. Job Number: 640-14341-1 Description Lab Location Method Preparation Method Method References: ASTM = ASTM International MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions, SM18 = "Standard Methods For The Examination Of Water And Wastewater", 18th Edition, 1992. SM20 = "Standard Methods For The Examination Of Water And Wastewater", 20th Edition." SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Tallahassee Page 17 of 167 12/21/2007 SAMPLE SUMMARY Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Sam le ID Client Sample ID Client Matrix Date/Time Sampled Date/Time Received 640-14341-1 R-1 Solid 12/04/2007 0820 12/06/2007 0850 640-14341-2 R-1b Solid 12/04/2007 0820 12106/2007 0850 640-14341-3 R-1c Solid 12/0412007 0820 1210612007 0850 640-14341-4 R-1Dub Solid 12104/2007 0830 12/06/2007 0850 640-14341-5 R-1 Dub b Solid 12/0412007 0830 12/06/2007 0850 640-14341-6 R-1Dubc Solid 12104/2007 0830 12/0612007 0850 640-14341-7 BR-1a Solid 12104/2007 1040 12106/2007 0850 640-14341-8 BR-1b Solid 12104/2007 1040 12/0612007 0850 640-14341-9 BR-1c Solid 12104/2007 1040 1210612007 0850 640-14341-10 BR-2a Solid 12/04/2007 1100 12106/2007 0850 640-14341-11 BR-2b Solid 1210412007 1100 12106/2007 0850 640-14341-12 BR-2c Solid 12/0412007 1100 12106/2007 0850 640-14341-13 BR-2 Dub a Solid 1210412007 1115 12/06/2007 0850 640-14341-14 BR-2 Dub b Solid 12/0412007 1115 12/0612007 0850 640-14341-15 BR-2 Dub c Solid 12104/2007 1115 1210612007 0850 640-14341-16 SA-1 a Solid 1210412007 1200 12/06/2007 0850 640-14341-17 SA-1 b Solid 12/04/2007 1200 12/0612007 0850 640-14341-18 SA-1 c Solid 12/04/2007 1200 12/06/2007 0850 640-14341-19 SA-2 a Solid 12/0412007 1215 12106/2007 0850 640-14341-20 SA-2 b Solid 12104/2007 1215 12106/2007 0850 640-14341-21 SA-2 c Solid 12/04/2007 1215 12106/2007 0850 640-14341-22 SA-3 a Solid 12/0412007 1230 12/06/2007 0850 640-14341-23 SA-3 b Solid 12/0412007 1230 12/06/2007 0850 640-14341-24 SA-3 c Solid 1210412007 1230 12/06/2007 0850 640-14341-25 SA-4 a Solid 1210412007 1245 12/0612007 0850 640-14341-26 SA-4 b Solid 1210412007 1245 12/0612007 0850 640-14341-27 SA 4 c Solid 12/04/2007 1245 12/0612007 0850 640-14341-28 EB-1 Water 12/0412007 0815 1210612007 0850 640-14341-29 EB-2 Water 12/04/2007 1400 12106/2007 0850 TestAmerica Tallahassee Page 18 of 167 12/21/2007 SAMPLE RESULTS TeskAmerica Tallahassee Page 19 of 167 12/21/20Q7 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: R-1 Lab Sample ID: 640-14341-1 Date Sampled: 1210412007 0820 Client Matrix: Solid % Moisture: 57,5 Date Received: 12106/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GCIMS Semivolatiles - D Preparation: 3550E Prep Batch: 680-93303 Lab File ID: d7948.d Dilution: 10 Initial WeightlVolume: 30.14 g Date Analyzed: 12/1912007 1905 Final WeightiVolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <160 160 Acenaphthylene <160 160 Anthracene <160 160 Benzo[a]anthracene <160 160 Benzo[a]pyrene <160 160 Benzo[b]fluoranthene <160 160 Benzo[g,h,i]perylene <160 160 Benzo[k]fluoranthene <160 160 Chrysene <160 160 Dibenz(a,h)anthracene <160 160 Fluorene <160 160 Fluoranthene <160 160 Indeno[1,2,3-cd]pyrene <160 160 Naphthalene <160 160 Phenanthrene <160 160 Pyrene <160 160 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 20 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: R-1b Lab Sample ID: 640-14341-2 Date Sampled: 12/0412007 0820 Client Matrix: Solid % Moisture: 73.1 Date Received: 1210612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 35508 Prep Batch: 680-93303 Lab File ID: 0949A Dilution: 10 Initial Weight/Volume: 30,48 g Date Analyzed: 12/19/2007 1928 Final WeightfVolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <250 250 Acenaphthylene <250 250 Anthracene <250 250 Benzo[a]anthrace ne <250 250 Benzo[a]pyrene <250 250 Benzo[b]tluoranthene <250 250 Benzo[g,h,i]perylene <250 250 Benzo[k]fluoranthene <250 250 Chrysene <250 250 Di benz(a,h)anthrace ne <250 250 Fluorene <250 250 Fluoranthene <250 250 Indeno[1,2,3-cd]pyre ne <250 250 Naphthalene <250 250 Phenanthrene <250 250 Pyrene <250 250 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 21 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: R-1c Job Number: 640-14341-1 Lab Sample ID; 640-14341-3 Date Sampled: 12/04/2007 0820 Client Matrix: Solid % Moisture: 73.5 Date Received: 1210612007 0850 8270C Semivolatiie Organic Compounds by GCMS - Low Levels Method: 82700 Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7950.d Dilution: 10 Initial Weight/Volume: 30.17 g Date Analyzed: 12/1912007 1951 Final WeightlVolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <250 250 Acenaphthylene <250 250 Anthracene <250 250 Benzo[a]anthrace no <250 250 Benzo[a]pyrene <250 250 Benzo[b]fluoranthene <250 250 Benzo[g,h,i]perylene <250 250 Benzo[k]fluoranthene <250 250 Chrysene <250 250 Dibenz(a,h)anthracene <250 250 Fluorene <250 250 Fluoranthene <250 250 Indeno[1,2,3-cdjpyrene <250 250 Naphthalene <250 250 Phenanthrene <250 250 Pyrene <250 250 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 22 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: R-1 Dub Job Number: 640-14341-1 Lab Sample ID: 640-14341-4 Date Sampled: 12/0412007 0830 Client Matrix: Solid % Moisture: 66.3 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GUMS Semivolatiles - D Preparation: 355013 Prep Batch: 680-93303 Lab File ID: d7951.d Dilution: 10 Initial WeightfVolume: 30.31 g Date Analyzed: 12/1912007 2014 Final WeightfVolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Anaiyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <200 200 Acenaphthylene <200 200 Anthracene <200 200 8enzo[a]anthracene <200 200 Benzo[a]pyrene <200 200 Benzo[b]fiuoranthene <200 200 Benzo[g,h,i]perylerne <200 200 Benzo[k]Fluoranthene <200 200 Chrysene <200 200 Dibenz(a,h)anthracene 400 200 Fluorene <200 200 Fluoranthene <200 200 Indeno[1,2,3-cd]pyrene <200 200 Naphthalene <200 200 Phenanthrene <200 200 Pyrene <200 200 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29- 122 7estAmericaTallahassee Page 23 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: R-1Dub b Lab Sample ID: 640-14341-5 Date Sampled: 12/0412007 0830 Client Matrix: Solid % Moisture: 70.7 Date Received: 1210612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7952.d Dilution: 10 Initial Weight/Volume: 30.00 g Date Analyzed: 12/1912007 2036 Final WeightlVolume: 1 mL Date Prepared: 12/13/2007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (uglKg) Qualifier RL Acenaphthene <230 230 Acenaphthylene <230 230 Anthracene <230 230 Benzo[a]anthracene <230 230 Benzo[a]pyrene <230 230 Benzo[b]fluoranthene <230 230 Benzo[g,h,i]perylene <230 230 Benzo[k]fluoranthene <230 230 Chrysene <230 230 Dibenz(a,h)anthracene <230 230 Fluorene <230 230 Fluoranthene <230 230 Indeno(1,2,3-cd]pyrene <230 230 Naphthalene <230 230 Phenanthrene <230 230 Pyrene <230 230 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 24 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc, Job Number: 640-14341-1 Client Sample ID: R-1 Dub c Lab Sample ID: 640-14341-6 Date Sampled: 1210412007 0830 Client Matrix: Solid % Moisture: 70.5 Date Received: 12/0612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7953.d Dilution: 10 Initial Weight/Volume: 30.24 g Date Analyzed: 12/1912007 2100 Final WeightlVolume: 1 mL Date Prepared: 12/13/2007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (uglKg) Qualifier RL Acenaphthene <230 230 Acenaphthylene <230 230 Anthracene <230 230 Benzo[a]anthrace ne <230 230 Benzo[a]pyrene <230 230 Benzo[b]fluoranthene <230 230 Benzo[g,h,i]perylene <230 230 Benzo[k]fluoranthene <230 230 Chrysene <230 230 Dibenz(a,h)anthracene <230 230 Fluofene <230 230 Fluoranthene <230 230 1ndeno[1,2,3-cd]pyre ne <230 230 Naphthalene <230 230 Phenanthrene <230 230 Pyrene <230 230 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 25 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-1a Job Number: 640-14341-1 Lab Sample ID: 640-14341-7 Date Sampled: 12/04/2007 1040 Client Matrix: Solid % Moisture: 64.1 Date Received: 12/06/2007 0850 8270C Semivolatilo Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94258 Instrument ID: GCMS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7972.d Dilution: 50 Initial Weight/Volume: 30.23 g Date Analyzed: 12120/2007 1212 Final WeightfVolume: 1 mL Date Prepared: 12113/2007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ugtKg) Qualifier RL Acenaphthene <930 930 Acenaphthylene <930 930 Anthracene 3200 930 Benzo[a]anthracene 20000 930 Benzo[a]pyrene 20000 930 Benzo[b]fiuoranthene 27000 930 Benzo[g,h,i]perylene 14000 930 Benzo[k]fluoranthene 15000 930 Chrysene 20000 930 Di benz(a, h)a nth race ne 5000 930 Fluorene <930 930 Fluoranthene 29000 930 Indeno[1,2,3-cd]pyrene 14000 930 Naphthalene <930 930 Phenanthrene 9500 930 Pyrene 22000 930 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29- 122 TestAmerica Tallahassee Page 26 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: BRAb Lab Sample ID: 640-14341-8 Date Sampled: 1210412007 1040 Client Matrix: Solid % Moisture: 65.3 Date Received: 1210612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 82700 Analysis Batch: 680-94258 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7973.d Dilution: 50 Initial Weight/Volume: 30.42 g Date Analyzed: 12/2012007 1235 Final WeighWolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <950 950 Acenaphthylene <950 950 Anthracene 3300 950 Benzo[a]anthrace ne 20000 950 Benzo[a]pyrene 21000 950 Benzo[b]fluoranthene 29000 950 Benzo[g,h,i]perylene 15000 950 Benzo[k]fluoranthene 14000 950 Chrysene 22000 950 Dibenz(a,h)anthracene 5200 950 Fluorene <950 950 Fluoranthene 30000 950 Indeno[1,2,3-cd]pyrene 16000 950 Naphthalene <950 950 Phenanthrene 9800 950 Pyrene 23000 950 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 27 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-1c Job Number: 640-14341-1 Lab Sample ID: 640-14341-9 Date Sampled: 12/04/2007 1040 Client Matrix: Solid % Moisture: 66.3 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94258 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7974.d Dilution: 50 Initial Weight/Volume: 30.08 g Date Analyzed: 12120/2007 1258 Final Weight/Volume; 1 mL Date Prepared: 1211312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <990 990 Acenaphthylene <990 990 Anthracene 3900 990 Benzo[a]anthracene 26000 990 Benzo[a]pyrene 26000 990 Benzo[b]fluoranthene 41000 990 Benzo[g,h,i]perylene 17000 990 Benzo]k]fluoranthene 19000 990 Chrysene 28000 990 Dibenz(a,h)anthracene 6000 990 Fluorene <990 990 Fluoranthene 38000 990 Indeno[1,2,3-cd]pyrene 17000 990 Naphthalene <990 990 Phenanthrene 12000 990 Pyrene 29000 990 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 28 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: BR-2a Lab Sample ID: 640-14341-10 Date Sampled: 12/04/2007 1100 Client Matrix: Solid % Moisture: 68.2 Date Received: 12/0612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7957.d Dilution: 10 Initial Weight/Volume: 30.11 g Date Analyzed: 12119/2007 2231 Final WeightlVolume: 1 ml Date Prepared: 12!1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <210 210 Acenaphthylene <210 210 Anthraceno 830 210 Benzo]a]anthrace ne 6200 210 Benzo[a]pyrene 6300 210 Benzo[b]fluoranthene 8700 210 Benzo(g,h,i]perylene 4500 210 Benzo[k]fluoranthene 4100 210 Chrysene 6300 210 Dibenz(a,h)anthracene 1700 210 Fluorene <210 210 Fluoranthene 8400 210 Indeno[1,2,3-cd]pyrene 5200 210 Naphthalene <210 210 Phenanthrene 2500 210 Pyrene 6200 210 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 29 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: 13R-2b Lab Sample ID: 640-14341-11 Date Sampled: 12104/2007 1100 Client Matrix: Solid % Moisture: 69.1 Date Received: 12106/2007 0850 82700 Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7958.d Dilution: 10 Initial Weight/Volume: 30.09 g Date Analyzed: 12/19/2007 2254 Final WeighVVolume: 1 mL Date Prepared: 12113/2007 1259 Injection Volume: 1 uL Analyte QryWt Corrected: Y Result (ug1Kg) Qualifier RL Acenaphthene <220 220 Acenaphthylene <220 220 Anthracene 610 220 Benzo[a]anthracene 5400 220 Benzo[a]pyrene 5400 220 Benzo[bjfluoranthene 8500 220 Benzo[g,h,i]perylene 3800 220 Benzo[k]fiuoranthene 4700 220 Chrysene 5400 220 Dibenz(a,h)anthracene 1400 220 Fluorene <220 220 Fluoranthene 6900 220 Indeno[1,2,3-cd]pyrene 4000 220 Naphthalene <220 220 Phenanthrene 2000 220 Pyrene 5500 220 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 30 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: BR-2c Lab Sample 1D: 640-14341-12 Date Sampled: 12/0412007 1100 Client Matrix: Solid % Moisture: 68.8 Date Received: 1210612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GUMS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7959.d Dilution: 10 Initial Weight/Volume: 30.06 g Date Analyzed: 12/19/2007 2317 Final Weight/Volume: 1 mL Date Prepared: 12113/2007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene 230 210 Acenaphthylene <210 210 Anthracene 890 210 Benzo[a]anthracene 7500 210 Benzo[a]pyrene 7700 210 Benzo[b]fluoranthene 11000 210 Benzo[g,h,ilperylene 5600 210 Benzo[k]fluoranthene 6500 210 Chrysene 7300 210 Di benz(a,h)anth race ne 2100 210 Fluorene <210 210 Fluoranthene 10000 210 Indeno[1,2,3-cd]pyrene 6500 210 Naphthalene <210 210 Phenanthrene 2900 210 Pyrene 7200 210 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 31 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc, Job Number: 640-14341-1 Client Sample ID: BR-2 Dub a Lab Sample ID: 640-14341-13 Date Sampled; 1210412007 1115 Client Matrix: Solid % Moisture: 68.9 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GUMS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7960.d Dilution: 10 Initial Weight/Volume: 30.19 g Date Analyzed: 12119/2007 2340 Final Weight/Volume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <210 210 Acenaphthylene X210 210 Anthracene 540 210 Benzo[a]anthrace ne 4000 210 Benzo[a]pyrene 4500 210 Benzo[b]fiuoranthene 7000 210 Benzo[g,h,i]perylene 3200 210 Benzo[k]fluoranthene 3800 210 Chrysene 4300 210 Dibenz(a,h)anthracene 1200 210 Fluorene <210 210 Fluoranthene 5600 210 Indeno[1,2,3-cd]pyre ne 3300 210 Naphthalene <210 210 Phenanthrene 1600 210 Pyrene 4300 210 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmericaTallahassee Page 32 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2 Dub b Job Number: 640-14341-1 Lab Sample ID: 640-14341-14 Date Sampled: 12104/2007 1115 Client Matrix: Solid % Moisture: 69.9 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GUMS Semivolatiles - D Preparation: 35506 Prep Batch: 680-93303 Lab File ID: d7961.d Dilution: 10 Initial Weight/Volume: 30.18 g Date Analyzed: 1212012007 0002 Final Weight/Volume: 1 mL Date Prepared: 12/13/2007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <220 220 Acenaphthylene <220 220 Anthracene 630 220 Benzo[a]anthracene 4800 220 Benzo[a]pyrene 4900 220 Benzo[b]fluoranthene 7400 220 Benzo[g,h,i]perylene 3500 220 Benzo[k]fluoranthene 4800 220 Chrysene 5100 220 Dibenz(a,h)anthracene 1300 220 Fluorene <220 220 Fluoranthene 6300 220 Indeno[1,2,3-cdjpyrene 3700 220 Naphthalene <220 220 Phenanthrene 1900 220 Pyrene 5100 220 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmericaTallahassee Page 33 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2 Dub c Job Number; 640-14341-1 Lab Sample ID: 640-14341-15 Date Sampled: 12104/2007 1115 Client Matrix: Solid % Moisture: 68.4 Date Received: 1210612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method; 8270C Analysis Batch: 680-94176 Instrument ID: GUMS Semivolatiles - D Preparation: 35506 Prep Batch: 680-93303 Lab File ID: d7962.d Dilution: 10 Initial WeighWolume: 30.16 g Date Analyzed: 12/2012007 0025 Final WeighUVolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <210 210 Acenaphthylene <210 210 Anthracene 250 210 Benzo[a]anthrace ne 1800 210 Benzola]pyrene 1900 210 Benzolb]fluoranthene 3000 210 Benzo[g,h,i]perylene 1300 210 Benzo[k]fluoranthene 1400 210 Chrysene 1900 210 Dibenz(a,h)anthracene 480 210 Fluorene <210 210 Fluoranthene 2500 210 1ndeno[1,2,3-cd]pyrene 1300 210 Naphthalene <210 210 Phenanthrene 710 210 Pyrene 1900 210 Surrogate %Rec Acceptance limits 0-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 34 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-1 a Lab Sample ID: 640-14341-16 Date Sampled: 1210412007 1200 Client Matrix: Solid % Moisture: 61.1 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 82700 Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7963.d Dilution: 10 Initial Weight/Volume: 30.18 g Date Analyzed: 12/2012007 0048 Final Weight/Volume: 1 mL Date Pfepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWil Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <170 170 Acenaphthylene X170 170 Anthracene 180 170 Benzo[a]anthrace ne 1000 170 Benzo[a]pyrene 1100 170 Benzo[b]fluoranthene 2000 170 Benzo[g,h,i]perylene 850 170 Benzo[k]fluoranthene 760 170 Chrysene 1100 170 Dibenz(a,h)anthracene 350 170 Fluorene <170 170 Fluoranthene 1500 170 Indeno[1,2,3-cd]pyrene 870 170 Naphthalene <170 170 Phenanthrene 570 170 Pyrene 1100 170 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29- 122 TestAmerica Tallahassee Page 35 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job !Number: 640-14341-1 Client Sample ID: SA-1 b Lab Sample ID: 640-14341-17 Date Sampled: 12104!2007 1200 Client Matrix: Solid % Moisture: 62.5 Date Received: 12/0612007 0850 82700 Semivolatile Organic Compounds by GCMS - low levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7964.d Dilution: 10 Initial Weight/Volume: 30.22 g Date Analyzed: 12/20/2007 0111 Final WeightlVolume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifler RL Acenaphthene <180 180 Acenaphthylene <180 180 Anlhracene <180 180 Be nzo[a]a nth race no 750 18G Benzo[a]pyrene 830 180 Benzo[bifluoranthene 1400 180 Senzo[g,h,i]perylene 640 180 Benzo[k]fluoranthene 510 180 Chrysene 820 180 Dibenz(a,h)anthracene <180 180 Fluorene <180 180 Fluoranthene 1100 180 1ndeno[1,2,3-cd]pyre ne 630 180 Naphthalene <180 180 Phenanthrene 500 180 Pyreno 890 180 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 36 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-1 c Lab Sample ID: 640-14341-18 Date Sampled: 12/04/2007 1200 Client Matrix: Solid % Moisture: 61.4 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-93843 Instrument ID: GC/MS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7936.d Dilution: 10 Initial WeightlVolume: 30.30 g Date Analyzed; 12/1712007 2312 Final Weight/Volume: 1 mL Date Prepared: 12/1312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <170 170 Acenaphthylene <170 170 Anthracene <170 170 Benzo[a]anthracene 660 170 Benzo[a]pyrene 780 170 Benzoib]fluoranthene 1200 170 Benzo[g,h,i]perylene 470 170 Benzo[k]fluoranthene 670 170 Chrysene 790 170 Dibenz(a,h)anthracene 190 170 Fluorene X170 170 Fluoranthene 950 170 Indeno[1,2,3-cd]pyrene 420 170 Naphthalene <170 170 Phenanthrene 370 170 Pyrene 690 170 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 37 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample In: SA-2 a Lab Sample ID: 640-14341-19 Date Sampled: 12104/2007 1215 Client Matrix; Solid % Moisture: 64.6 Date Received: 12106/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GCIMS Semivolatiles - D Preparation: 3550B Prep Batch: 680-93303 Lab File ID: d7965.d Dilution: 10 Initial Weight/Volume: 30.06 g Date Analyzed: 12/20/2007 0134 Final WeightlVolume: 1 mL Date Prepared: 1211312007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug1Kg) Qualifier RL Acenaphthene <190 190 Acenaphthylene <190 190 Anthracene <190 190 Benzo[a]anthrace ne 490 190 Benzo[a]pyrene 560 190 Senzo[b]fluoranthene 920 190 Benzo[g,h,i]perylene 430 190 Benzo[k]fluoranthene 390 180 Chrysene 580 190 Dibenz(a,h)anthracene <190 190 Fluorene <190 190 Fluoranthene 710 190 Indeno[1,2,3-cd]pyreno 420 190 Naphthalene <190 190 Phenanthrene 280 190 Pyrene 590 190 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 38 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-2 b Lab Sample ID: 640-14341-20 Date Sampled: 12/04/2007 1215 Client Matrix: Solid % Moisture: 63.7 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94176 Instrument ID: GUMS Semivolatiles - D Preparation: 35506 Prep Batch: 680-93303 Lab File ID: d7966.d Dilution: 10 Initial WeightNolume: 30.19 g Date Analyzed: 1212012007 0157 Final WeighttVolume: 1 mL Date Prepared: 12113/2007 1259 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (uglKg) Qualifier RL Acenaphihene <180 180 Acenaphthylene <180 180 Anthracene <180 180 Benzo[a]anthracene 660 180 Benzo]a]pyrene 720 180 Benzo[b]Fluoranthene 1200 180 Benzo[g,h,i]perylene 590 180 Benzo[k]fluoranthene 470 180 Chrysene 720 180 Dibenz(a,h)anthracene <180 180 Fluorene <180 180 Fluoranthene 920 180 Indeno[1,2,3-cd]pyrene 590 180 Naphthalene <180 180 Phenanthrene 340 180 Pyrene 720 180 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 39 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample 10: SA-2 c Job Number: 640-14341-1 Lab Sample ID: 640-14341-21 Date Sampled: 12/0412007 1215 Client Matrix: Solid % Moisture: 65.5 Date Received: 1210612007 0850 8270C Semivoiatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94116 Instrument ID: GC/MS SemiVolatiles - K Preparation: 35506 Prep Batch: 680-93073 Lab File ID: k4819.d Dilution: 10 Initial WeighYVolume: 30.03 g Date Analyzed: 12115/2007 1319 Final Weight/Volume: 1.0 mL Date Prepared: 12/11/2007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <190 190 Acenaphthylene <190 190 An[hracene <190 190 Benzo[a]anthracene 480 190 Benzo[a]pyrene 530 190 Benzo[b]fluoranthene 820 190 Benzo[g,h,i]perylene 360 190 Benzo[k]Fluoranthene 340 190 Chrysene 490 190 Dibenz(a,h)anthracene <190 190 Fluorene <190 190 Fluoranthene 600 190 Indeno[1,2,3-cd]pyrene 350 190 Naphthalene <190 190 Phenanthrene 210 190 Pyrene 540 190 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 40 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-3 a Job lNumber: 640-14341-1 Lab Sample ID: 640-14341-22 Date Sampled: 12/04/2007 1230 Client Matrix: Solid % Moisture: 62.7 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94116 Instrument ID: GCIMS SemiVolatiles - K Preparation: 3550B Prep Batch: 680-93073 Lab File ID: k4820.d Dilution: 10 Initial Weight/Volume: 30.05 g Date Analyzed: 12115/2007 1342 Final Weight/Volume: 1.0 mL Date Prepared: 1211112007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (uglKg) Qualifier RL Acenaphthene <180 180 Acenaphthylene <180 180 An1hracene <180 180 Benzo[a]anihfacene 230 180 Benzo[a]pyrene 260 180 Benzo[b]Fluoranthene 360 180 Benzo[g,h,i]perylene <180 180 Benzo[k]fluoranthene <180 180 Chrysene 220 180 Dibenz(a,h)anthracene <180 180 Fluorene <180 180 Fluoranthene 280 180 Indeno[1,2,3-cd]pyrene <180 180 Naphthalene <180 180 Phenanthrene <180 180 Pyrene 260 180 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 41 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-3 b Lab Sample ID: 640-14341-23 Date Sampled: 12104/2007 1230 Client Matrix: Solid % Moisture: 60.5 Date Received: 12/0612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94 1 1 6 Instrument ID: GUMS SemiVolatiles - K Preparation: 3550B Prep Batch: 680-93073 Lab File ID: k4821.d Dilution: 10 Initial WeightlVolume: 30.05 g Date Analyzed: 12/1512007 1405 Final Weight/Volume: 1.0 mL Date Prepared: 12/11/2007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <170 170 Acenaphthylene <170 170 Anthracene <170 170 Be nzo [a]anth race ne 270 170 Benzo(alpyrene 310 170 Benzo[blfluoranthene 480 170 Benzo[g,h,i]perylene 200 170 Benzo[k]fluoranthene 180 170 Chrysene 280 170 Dibenz(a,h)anthracene <170 170 Fluorene <170 170 Fluoranthene 300 170 Indeno(1,2,3-cd]pyrene 190 170 Naphthalene <170 170 Phenanthrene <170 170 Pyrene 280 170 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 42 of 167 12/21/2007 Analytical Data Client; Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-3 c Lab Sample ID: 640-14341-24 Date Sampled: 12104/2007 1230 Client Matrix: Solid % Moisture: 63.8 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 82700 Analysis Batch: 680-94116 Instrument ID: GC/MS SemiVolatiles - K Preparation: 35508 Prep Batch: 680-93073 Lab File ID: k4822.d Dilution: 10 initial Weight/Volume: 30.13 g Date Analyzed: 12/1512007 1428 Final Weight/Volume: 1.0 mL Date Prepared; 12/11/2007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene <180 180 Acenaphthylene <180 180 Anthracene <180 180 Benzo[a]anthrace ne 270 180 Benzo[a]pyrene 300 180 Benzo[b]fluoranthene 450 180 Benzo[g,h,i]perylene <180 180 Benzoik]fluoranthene 210 180 Chrysene 260 180 Dibenz(a,h)anthracene <180 180 Fluorene <18D 1$0 Fluoranthene 320 180 Indeno[1,2,3-cd]pyrone <180 180 Naphthalene <180 180 Phenanthrene <180 180 Pyrene 300 180 Surrogate %Rec Acceptance Limits o-Terphenyl D 0 29 - 122 TestAmerica Tallahassee Page 43 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client: Sample ID: SA-4 a Job Number: 640-14341-1 Lab Sample ID: 640-14341-25 Date Sampled: 12/04/2007 1245 Client Matrix: Solid % Moisture: 63.1 Date Received: 12/0612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94258 Instrument ID: GC/MS Semivolatiles - D Preparation; 3550B Prep Batch: 680-93073 Lab File ID: d7975.d Dilution: 50 Initial Weight/Volume: 30.01 g Date Analyzed: 1212012007 1321 Final Weight/Volume: 1.0 mL Date Prepared: 12111/2007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene 1100 910 Acenaphthylene <910 910 Anthracene 3100 910 Benzo[a]anthracene 21000 910 Benzo[a]pyrene 23000 910 Benzo[b]fluoranthene 30000 910 Benzo[g,h,i]perylene 16000 910 Benzo[k]fluoranthene 12000 910 Chryseae 21000 910 Di benz(a, h)anthracene <910 910 Fluorene <910 910 Fluoranthene 30000 910 Indeno[1,2,3-cd]pyrene 17000 910 Naphthalene <910 910 Phenanthrene 10000 910 Pyrene 23000 910 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 44 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA4 b Job Number: 640-14341-1 Lab Sample ID: 640-14341-26 Date Sampled: 12/04/2007 1245 Client Matrix: Solid % Moisture: 63.7 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-94258 Instrument ID: GC1MS Semivolatiles - D Preparation; 35508 Prop Batch: 680-93073 Lab File ID: d7976.d Dilution: 50 Initial Weight/Volume: 30.02 g Date Analyzed: 12/2012007 1344 Final WeighVVolume: 1.0 mL Date Prepared: 12/1112007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene 1900 920 Acenaphthylene <920 920 Anthracene 5500 920 Benzo[a]anthracene 39000 920 Benzo[a]pyrene 42000 920 Benzo[b]fiuoranthene 58000 920 Benzo[g,h,i]perylene 29000 920 Benzo[k]Fluoranthene 21000 920 Chrysene 37000 920 Dibenz(a,h)anthracene <920 920 Fluorene 1600 920 Fluoranthene 53000 920 Indeno[1,2,3-cd]pyrone 33000 920 Naphthalene <920 920 Phenanthrene 19000 920 Pyrene 39000 920 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 45 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-4 c Lab Sample ID: 640-14341-27 Date Sampled: 1210412007 1245 Client Matrix: Solid % Moisture: 64.7 Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCIVIS - Low Levels Method: 8270C Analysis Batch: 680-94258 Instrument ID: GC/MS Semivolatiles - D Preparation: 35506 Prep Batch: 680-93073 Lab File ID: d7977.d Dilution; 50 Initial WeightlVolumo: 30.10 g Date Analyzed; 12120/2007 1407 Final Weight/Volume: 1.0 mL Date Prepared: 12111/2007 1312 Injection Volume: 1 uL Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL Acenaphthene 1700 940 Acenaphthylene <940 940 Anthracene 4900 940 Benzo[a]anthracene 34000 940 Benzo[a]pyrene 38000 940 Benzo[b]fluoranthene 56000 940 Benzo[g,h,i]perylene 25000 940 Benzo[k]fluoranthene 16000 940 Chrysene 34000 940 Dibenz(a,h)anthracene <940 940 Fluorene 1400 940 Fluoranthene 48000 940 Indeno[1,2,3-cd]pyrene 27000 940 Naphthalene <940 940 Phenanthrene 16000 940 Pyrene 36000 940 Surrogate %Rec Acceptance Limits o-Terphenyl 0 D 29 - 122 TestAmerica Tallahassee Page 46 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: E13-1 Job Number: 640-14341-1 Lab Sample ID: 640-14341-28 Date Sampled: 12/04/2007 0815 Client Matrix: Water Date Received: 12/0612007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-93964 Instrument ID: GCIMS Semivolatiles - D Preparation; 3520C Prep Batch: 680-93236 Lab File ID: d7843.d Dilution: 1.0 Initial WeightlVolume: 1060 ml Date Analyzed: 12/1312007 1327 Final Weight/Volume: 1 mt Date Prepared: 12/11/2007 1430 Injection Volume: 1 uL Analyte Result (uglL) Qualifier RL Acenaphthene <0.19 0.19 Acenaphthylene <0,19 0.19 Anthracene <0.19 0.19 Benzo[a]anthracene <0.19 0.19 Benzo[a]pyrene <0.19 0.19 Benzo[b]fuoranthene <0A9 0.19 Benzo[g,h,i]perylene <0.19 0.19 Benzo[k]fluoranthene <0.19 0.19 Chrysene <0.19 0.19 Dibenz(a,h)anthracene <0.19 0.19 Fluorene <0.19 0,19 Fluoranthene <0,19 0.19 Indeno[1,2,3-cd]pyrene <0.19 0.19 Naphthalene <0.19 0.19 Phenanthrene <0.19 0.19 Pyrene <0.19 0.19 Surrogate %Rec Acceptance Limits o-Terphenyl 62 44 - 123 TestAmericaTallahassee Page 47 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: E13-2 Job Number: 640-14341-1 Lab Sample ID: 64D-14341-29 Date Sampled: 12/0412007 1400 Client Matrix: Water Date Received: 12/06/2007 0850 8270C Semivolatile Organic Compounds by GCMS - Low Levels Method: 8270C Analysis Batch: 680-93964 Instrument ID: GUMS Semivolatiles - D Preparation: 3520C Prep Batch: 680-93236 Lab File ID: d7844.d Dilution: 1.0 Initial Weight/Volume: 1030 mL Date Analyzed: 12/13/2007 1350 Final Weight/Volume: 1 mL Date Prepared: 1211112007 1430 Injection Volume: 1 uL Analyte Result (ug/L) Qualifier RL Acenaphthene <0.19 0.19 Acenaphthylene <0.19 0.19 Anthracene <0.19 0.19 Benzo[a]anthracene <0.19 0.19 Benzo[a]pyrene <0.19 0.19 Benzo[b]fluoranthene <0.19 0.19 Benzo[g,h,i]perylene <0.19 0.19 Renzo[k]fluoranthene <0.19 0.19 Chrysene <0.19 0.19 Dibenz(a,h)anthracene <0.19 0.19 Fluorene <0.19 0.19 Fluoranthene <0.19 0.19 Indeno[1,2,3-cd]pyre ne <0.19 0.19 Naphthalene <0.19 0.19 Phenanthrene <0.19 0.19 Pyrene <0.19 0.19 Surrogate %Rec Acceptance Limits o-Terphenyl 45 44 - 123 TestAmerica Tallahassee Page 48 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: R-1 Lab Sample ID: 640-14341-1 Client Matrix: Solid % Moisture: 57.5 Analytical Data Job Number: 640-14341-1 Date Sampled: 12/0412007 0820 Date Received: 12/0612007 0850 8081A?8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: ml14043,d Dilution: 1.0 Initial Weight/Volume: 30.38 g Date Analyzed: 12114/2007 2123 Final Weight[Volume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <77 77 PCB-1248 <77 77 PCB-1254 <77 77 PCB-1260 <77 77 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 41 26 - 140 DCB Decachlorobiphenyl 49 X 50 - 129 TestAmerica Tallahassee Page 49 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID; R-1 b Job Number: 640-14341-1 Lab Sample ID: 640-14341-2 Date Sampled: 12/04/2007 0820 Client Matrix: Solid % Moisture: 73.1 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114044.d Dilution: 1.0 Initial Weight/Volume: 30.46 g Date Analyzed: 12/14/2007 2142 Final WeightlVolume: 1D mL Date Prepared: 1211312007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ugft) Qualifier RL PCB-1242 <120 120 PCB-1248 <120 120 PCB-1254 <120 120 PCB-1260 <120 120 Surrogate %Rec Acceptance Limits Tetra chIoro-m-xylene 47 26 - 140 DCB Decachlorobiphenyl 57 50 - 129 TestAmerica Tallahassee Page 50 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID; R-1c Job Number; 640-14341-1 Lab Sample ID: 640-14341-3 Date Sampled: 12/0412007 0820 Client Matrix: Solid % Moisture: 73.5 Date Received: 12106/2007 0850 8081A?8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114045.d Dilution: 1.0 Initial Weight/Volume: 30.20 g Date Analyzed: 12114/2007 2202 Final Weight/Volume: 10 mL Date Prepared: 12/13/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <120 120 PCB-1248 <120 120 PCB-1254 <120 120 PCB-1260 <120 120 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 49 26 - 140 DCB Decachlorobiphenyl 62 50 - 129 TestAmerica Tallahassee Page 51 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: R-10ub Lab Sample ID: 640-14341-4 Date Sampled: 12104/2007 0830 Client Matrix: Solid % Moisture: 66.3 Date Received: 12106/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: ml14046.d Dilution: 1.0 Initial Weight/Volume: 30.16 g Date Analyzed: 12114/2007 2221 Final WeightNolume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) QuaVier RL PCB-1242 X98 98 PCB-1248 X98 98 PCB-1254 <98 98 PCB-1260 X98 98 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 49 26 - 140 DCB Decachlorobiphenyl 60 50 - 129 TestAmerica Tallahassee Page 52 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: R-1 Dub b Job Number: 640-14341-1 Lab Sample ID: 640-14341-5 Date Sampled: 12/04/2007 0830 Client Matrix: Solid % Moisture: 70.7 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated 131phenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3560B Prep Batch: 680-93304 Lab File ID: m114047.d Dilution: 1.0 Initial Weight/Volume: 30.06 g Date Analyzed: 1211412007 2240 Final WeighUVolume: 10 mL Date Prepared: 1211312007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <110 110 PCB-1248 <110 110 PCB-1254 <110 110 PCB-1260 <110 110 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 50 26 - 140 DCB Decachlorobiphenyl 60 50 - 129 TestAmerica Tallahassee Page 53 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: R-1 Dub c Job Number: 640-14341-1 Lab Sample ID: 640-14341-6 Date Sampled: 12/0412007 0830 Client Matrix: Solid % Moisture: 70.5 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 35508 Prep Batch: 680-93304 Lab File ID: m114048.d Dilution: 1.0 Initial WeighUVolume: 30.20 g Date Analyzed: 1211412007 2300 Final Weight/Volume: 10 mL Date Prepared: 12/1312007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <110 110 PCB-1248 <110 110 PCB-1254 <110 110 PCB-1260 <110 110 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 72 26 - 140 DCB Decachlorobiphenyl 78 50 - 929 TestAmerica Tallahassee Page 54 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: BR-1a Lab Sample ID: Client Matrix: 640-14341-7 Solid % Moisture: 64.1 Date Sampled: 12/0412007 1040 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114049.d Dilution: 2.0 Initial Weight/Volume: 30.13 g Date Analyzed: 12114/2007 2319 Final WeightNotume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID; PRIMARY Analyte DryWt Corrected: Y Result (uq/Kg) Qualifier RL PCB-1242 2400 180 PCB-1248 <180 180 PCB-1254 <180 180 PCB-1260 520 180 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 82 26 - 140 DCB Decachlorobiphenyl 70 50 - 129 TestAmerica Tallahassee Page 55 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: BR-1b Lab Sample li]: 640-14341-8 Client Matrix: Solid % Moisture: 65.3 Analytical Data Jab Number: 640-14341-1 Date Sampled: 12/0412007 1040 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC Semivolatiles - M Preparation: 35508 Prep Batch: 680-93304 Lab Pile ID: m114050.d Dilution: 2.0 Initial WeightlVolume: 30.50 g Date Analyzed: 1211412007 2339 Final Weight/Volume: 10 mL Date Prepared: 12/13/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (uglKg) Qualifier RL PCB-1242 2200 190 PCB-1248 <190 190 PCB-1254 <190 190 PCB-1260 300 P 190 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 90 26 - 140 DCB Decachlorobiphenyl 94 50 - 129 TestAmerica Tallahassee Page 56 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: 811-1c Job Number: 640-14341-1 Lab Sample ID: 640-14341-9 Date Sampled: 12/0412007 1040 Client Matrix: Solid % Moisture: 66.3 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC Semivolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114051.d Dilution: 2.0 Initial Weight/Volume: 30.35 g Date Analyzed: 12/1412007 2358 Final WeightNolume: 10 mL Date Prepared: 1211312007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 1500 P 190 PCB-1248 <190 190 PCB-1254 <190 190 PCB-1260 480 190 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 72 26 - 140 DCB Decachlorobiphenyl 88 50 - 129 TestAmerica Tallahassee Page 57 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID; BR-2a Lab Sample ID: Client Matrix: 640-14341-10 Solid % Moisture: 68.2 Date Sampled: 12/04/2007 1100 Date Received: 1210612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analys"s Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114052.d Dilution: 1.0 Initial Weight/Volume: 30.14 g Date Analyzed: 12115/2007 0018 Final Weight/Volume: 10 mL Date Prepared: 12/13/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWI Corrected: Y Result (uglKg) Qualifier RL PCB-1242 <100 100 PCB-1248 <100 100 PCB-1254 <100 100 PCB-1260 <100 100 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 41 26 - 140 DCS Decachlorobiphenyl 48 X 50 - 129 TestArnerica Tallahassee Page 58 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SR-2b Job (Number: 640-14341-1 Lab Sample ID: 640-14341-11 Date Sampled: 12/04/2007 1100 Client Matrix: Solid % Moisture: 69.1 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Riphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: mll4053.d Dilution: 1.0 Initial Weight/Volume: 30.18 g Date Analyzed: 12115/2007 0037 Final WeightNolume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <110 110 PCB-1248 <110 110 PCB-1254 <110 110 PCB-1260 <110 110 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 32 26 - 140 DCB Decachlorobiphenyl 39 X 50 - 129 TestAmerica Tallahassee Page 59 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: BR-2c Lab Sample ID: 640-14341-12 Client Matrix: Solid % Moisture: 68.8 Analytical Data Job Number: 640-14341-1 Date Sampled: 12/04/2007 1100 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A 8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 35506 Prep Batch: 680-93304 Lab File ID: m114054.d Dilution: 1.0 Initial Weight/Volume: 30.19 g Date Analyzed: 12/1512007 0057 Final Weight/Volume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <110 110 PCB-1248 <110 110 PCB-1254 150 110 PCB-1260 <110 110 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 37 26 - 140 DCB Decachlorobiphenyl 43 X 50 - 129 TestAmericaTallahassee page 60 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: 1311-2 Dub a Job Number: 640-14341-1 Late Sample ID: 640-14341-13 Date Sampled: 12104/2007 1115 Client Matrix: Solid % Moisture: 68.9 Date Received; 12/06/2007 0850 8081A_8082 brganochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114055.d Dilution: 1.0 Initial Weight[Volume: 30.11 g Date Analyzed: 12/1512007 0116 Final WeightlVofume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <110 110 PCB-1248 X110 110 PCB-1254 200 110 PCB-1260 120 110 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 72 26 - 140 DCB Decachlorobiphenyl 84 50 - 129 TestAmericaTallahassee Page 61 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2 Dub b Job Number: 640-14341-1 Lab Sample ID: 640-14341-14 Date Sampled: 12/04/2007 1115 Client Matrix: Solid % Moisture: 69.9 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument 10: GC SemiVolatiles - M Preparation: 35508 Prep Batch: 680-93304 Lab File ID: m114056.d Dilution: 1.0 Initial WeightiVolume: 30.27 g Date Analyzed: 12/15/2007 0136 Final Weight/Volume: 10 mL Date Propared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <110 110 PCB-1248 <110 110 PCB-1254 170 110 PCB-1260 <110 110 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 61 26 - 140 DCB Decachlorobiphenyl 67 50 - 129 TestAmerica Tallahassee Page 62 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: 1311-2 Dub c Job Number: 640-14341-1 Lab Sample ID: 640-14341-15 Date Sampled: 12/0412007 1115 Client Matrix: Solid % Moisture: 68.4 Date Received: 12/06!2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 35508 Prep Batch: 680-93304 Lab File ID: m114057.d Dilution: 1.0 Initial Weight/Volume: 30.07 g Date Analyzed: 12115/2007 0155 Final Weight/Volume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <100 100 PCB-1248 <100 100 PCB-1254 210 100 PCB-1260 <100 100 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 64 26 - 140 DCB Decachlorobiphenyl 72 50 - 129 TestAmerica Tallahassee Page 63 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Jab Number: 640-14341-1 Client Sample ID: SA-1 a Lab Sample ID: 640-14341-16 Date Sampled: 12/04/2007 1200 Client Matrix: Solid % Moisture: 61.1 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Balch: 680-93304 Lab File ID: m114058.d Dilution: 1.0 Initial Weight/Volume: 30.14 g Date Analyzed: 1211512007 0215 Final Weight/Volume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID; PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <84 84 PCB-1248 <84 84 PCB-1254 <84 84 PCB-1260 <84 84 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 55 26 - 140 DCB Decachlorobiphenyl 72 50 - 129 TestAmericaTallahassee Page 64 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-1 b Lab Sample ID: 640-14341-17 Client Matrix: Solid % Moisture: 62.5 Analytical Data Job Number: 640-14341-1 Date Sampled: 12/04/2007 1200 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyis by Gas Chromatography Method: 8081A_8082 Analysis Batch; 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114059.d Dilution; 1.0 Initial Weight/Volume: 30.24 g Date Analyzed: 12/15/2007 0234 Final Weight/Volume: 10 mL Date Prepared: 12/1312007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <87 87 PCB-1248 <87 87 PCB-1254 <87 87 PCB-1260 89 87 Surrogate °1%Rec Acceptance Limits Tetrachloro-m-xylene 72 26 - 140 DCB Decachlorobiphenyl 69 50 - 129 TestAmerica Tallahassee Page 65 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Jab Number: 640-14341-1 Client Sample ID: SA-1 c Lab Sample ID: 640-14341-18 Date Sampled: 12/0412007 1200 Client Matrix: Solid % Moisture: 61.4 Date Received: 12/0612007 0850 80BIA_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: n111406O.d Dilution: 1.0 Initial Weight/Volume: 30.50 g Date Analyzed: 12/15/2007 0254 Final WeighUVolume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <84 84 PCB-1248 <84 84 PCB-1254 <84 84 PCB-1260 <84 84 Surrogate %Rec Acceptance Limits Tetrachioro-m-xylene 44 26 - 140 DCB Decachlorobiphenyl 51 50 - 129 TestAmerica Tallahassee Page 66 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-2 a Jab Number: 640-14341-1 Lab Sample ID: 640-14341-19 Date Sampled: 12/0412007 1215 Client Matrix: Solid % Moisture: 64.6 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114061.d Dilution: 1.0 Initial WeighUVolume: 30.11 g Date Analyzed: 12/1512007 0313 Final Weight/Volume: 10 mL Date Prepared: 12/13/2007 1830 Injection Votume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <93 93 PCB-1248 <93 93 PCB-1254 <93 93 PCB-1260 <93 93 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 36 26 - 140 DCB Decachiorobiphenyl 42 X 50 - 129 TestAmerica Tallahassee Page 67 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-2 b Lab Sample ID: Client Matrix: 640-14341-20 Solid % Moisture: 63.7 Date Sampled: 12/04/2007 1215 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A8082 Analysis Batch: 680-93715 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93304 Lab File ID: m114062.d Dilution: 1.0 Initial Weight/Volume: 30.31 g Date Analyzed: 12/15/2007 0333 Final WeightNolume: 10 mL Date Prepared: 12113/2007 1830 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB--1242 <90 90 PCB-1248 <90 90 PCB-1254 <90 90 PCB-1260 <90 90 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 36 26 - 140 DCB Decachlorobiphenyl 48 X 50 - 129 TestAmerica Tallahassee page 68 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-2 c Job Number: 640-14341-1 Lab Sample ID: 640-14341-21 Date Sampled: 12/04/2007 1215 Client Matrix: Solid % Moisture: 65.5 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A8082 Analysis Batch: 680-93447 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93195 Lab File ID: m112013.d Dilution: 1.0 Initial WeightlVolume: 30.16 g Date Analyzed: 12/1212007 1549 Final WeightNolume: 10 mL Date Prepared: 12/1112007 1800 Inject€on Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <95 95 PCB-1248 <95 95 PCB-1254 <95 95 PCB-1260 <95 95 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 58 26 - 140 DCB Decachlorobiphenyl 71 50 - 129 TestAmerica Tallahassee Page 69 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: SA-3 a Lab Sample ID: 640-14341-22 Date Sampled: 12/0412007 1230 Client Matrix: Solid % Moisture: 62.7 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A8082 Analysis Batch: 680-93447 Instrument ID: GC SemiVolatiles - M Preparation: 35506 Prep Batch: 680-93195 Lab File ID: m112014.d Dilution: 1.0 Initial Weight/Volume: 30.18 g Date Analyzed: 12112/2007 1608 Final WeightlVolume: 10 mL Date Prepared: 12111/2007 1800 Injection Volumo: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <88 88 PCB-1248 <88 88 PCB-1254 <88 88 PCB-1260 <88 88 Surrogate %Rec Acceptance Limits Totrachloro-m-xylene 58 26 - 140 DCB Decachlorobiphenyl 75 50 - 129 TestAmerica Tallahassee Page 70 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-3 b Job Number: 640-14341-1 Lab Sample ID: 640-14341-23 Date Sampled: 12/0412007 1230 Client Matrix: Solid % Moisture: 60.5 Date Received: 12/06/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A 8082 ? Analysis Batch: 680-93447 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93195 Lab File ID: m112015.d Dilution: 1.0 Initial Weight/Volume: 30.00 g Date Analyzed: 1211212007 1628 Final Weight/Volume: 10 mL Date Prepared: 1211112007 1800 Injection Volume: 2 Lit Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <83 83 PCB-1248 <83 83 PCB-1254 <83 $3 PCB-1260 <83 83 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 63 26 - 140 DCB Decachlorobiphenyl 78 50- 129 TestAmerica Tallahassee Page 71 of 167 12/21/2007 Analytical Data Client: Environmental Services, inc. Client Sample ID: SA-3 c Job Number: 640-14341-1 Lab Sample ID: 640-14341-24 Date Sampled: 12104/2007 1230 Client Matrix: Solid % Moisture: 618 Date Received: 1210612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Siphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93447 Instrument ID: GC SemiVolatiles - M Preparation: 35508 Prep Batch: 680-93195 Lab File ID: m112016.d Dilution: 1.0 Initial WeighWolume: 30.08 g Date Analyzed: 12112/2007 1647 Final Weight/Volume: 10 mL Date Prepared: 12111/2007 1800 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <91 91 PCB-1248 <91 91 PCB-1254 <91 91 PCB-1260 <91 91 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 48 26 - 140 DCB Decachlorobiphenyl 60 50 - 129 TestAmerica Tallahassee Page 72 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-4 a Lab Sample ID: 640-14341-25 Client Matrix: Solid % Moisture: 63.1 Analytical Data Job Number: 640-14341-1 Date Sampled: 1210412007 1245 Date Received: 12106/2007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93447 Instrument ID: GC SemiVoiatiles - M Preparation: 3550B Prep Batch: 680-93195 Lab File ID: m112017.d Dilution: 2.0 Initial WeightlVolume: 30.11 g Date Analyzed: 12112/2007 1707 Final Weight/Volume: 10 mL Date Prepared: 1211112007 1800 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug1Kg) Qualifier RL PCB-1242 <180 1180 PCB-1248 <180 180 PCB-1254 720 180 PCB-1260 <180 180 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 68 26 - 140 DCB Decachlorobiphenyl 75 50 - 129 TestAmerica Tallahassee Page 73 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-4 b Job Number: 640-14341-1 Lab Sample ID: 640-14341-26 Date Sampled: 12/0412007 1245 Client Matrix: Solid % Moisture: 63.7 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93447 Instrument ID: GC SemiVolatiles - M Preparation: 35508 Prep Batch: 680-93195 Lab File ID: m112018.d Dilution; 2.0 Initial WeighUVolume: 30.16 g Date Analyzed: 1211212007 1726 Final Weight/Volume: 10 mL Date Prepared: 12111/2007 1800 Injection Volume: 2 uL Column ID: PRIMARY Analyte DryWt Corrected: Y Result (ug1Kg) Qualifier RL PCB-1242 <180 180 PCB-1248 <180 180 PCB-1254 840 180 PCB-1260 <180 180 Surrogate %Rec Acceptance limits Tetrachloro-m-xylene 72 26 - 140 DCB Decachlorobiphenyl 55 50 - 129 TestAmerica Tallahassee Page 74 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA4 c Lab Sample ID: 640-14341-27 Client Matrix: Solid % Moisture: 64.7 Analytical Data Job Number: 640-14341-1 Date Sampled: 12104/2007 1245 Date Received: 1210612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93447 Instrument ID: GC SemiVolatiles - M Preparation: 3550B Prep Batch: 680-93195 Lab File ID: m112019.d Dilution: 2.0 Initial Weight/Volume: 30.02 g Date Analyzed: 1211212007 1746 Final Weighl/Volume: 10 mL Date Prepared: 12/1112007 1800 Injection Volume: 2 uL Column ID: PRIMARY Anaiyte DryWt Corrected: Y Result (ug/Kg) Qualifier RL PCB-1242 <190 190 PCB-1248 <190 190 PCB-1254 880 190 PCB-1260 <190 190 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 137 26 - 140 DCB Decachlorobiphenyl 133 X 50 - 129 TestAmerica Tallahassee Page 75 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: EB-1 Job Number: 640-14341-1 Lab Sample ID: 640-14341-28 Date Sampled: 12/0412007 0815 Client Matrix: Water Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Biphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93295 Instrument ID: GC SemiVolatiles - J Preparation: 35200 Prep Batch: 680-93087 Lab File ID: jI10015.d Dilution: 1.0 Initial WeightiVolume: 1030 mL Date Analyzed: 12/11/2007 1742 Final Weight/Volume: 10 mL Date Prepared: 12110/2007 1445 Injection Volume: 2 uL Column ID: PRIMARY Analyte Result (ug1L) Qualifier RL PCB-1242 <0.97 0.97 PCB-1248 <0.97 0.97 PCB-1254 <0.97 0.97 PCB-1260 <0.97 0.97 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 71 35 - 120 DCB Decachlorobiphenyl 60 14-115 TestAmerica Tallahassee Page 76 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: ES-2 Lab Sample ID: 640-14341-29 Client Matrix: Water Analytical Data Job Number: 640-14341-1 Date Sampled: 12/0412007 1400 Date Received: 12/0612007 0850 8081A_8082 Organochlorine Pesticides & Polychlorinated Siphenyls by Gas Chromatography Method: 8081A_8082 Analysis Batch: 680-93295 Instrument ID: GC SemiVolatiles - J Preparation: 3520C Prep Batch: 680-93087 Lab File It): j110016.d Dilution: 1.0 Initial WeighUVolume: 1030 mL Date Analyzed: 1211112007 1805 Final Weight/Volume: 10 mL Date Prepared: 1211012007 1445 Injection Volume: 2 uL Column ID: PRIMARY Analyte Result (uglL) Qualifier RL PCB-1242 <0.97 0.97 PCB-1248 <0.97 0.97 PCB-1254 <0.97 0.97 PCB-1260 <0.97 0.97 Surrogate %Rec Acceptance Limits Tetrachloro-m-xylene 56 35 - 120 DC6 Decachlorobiphenyl 16 14-115 TestAmerica Tallahassee Page 77 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: R-1 Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-1 Solid Date Sampled: Date Received: 12104/2007 0820 12/06/2007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93371 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93138 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.14 g Date Analyzed: 12112/2007 0244 Final Weight[Volume: 100 ML Date Prepared: 12110/2007 1406 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 6,3 0,88 Barium 51 0.88 Cadmium <0.44 0.44 Chromium 16 0.88 Iron 26000 8.8 Lead 7.6 0.44 Selenium <2.2 2.2 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial WeightfVolume: 1,17 g Date Analyzed: 12/13/2007 1612 Final Weight/Volume: 50 mL Date Prepared: 12/11/2007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0,028 Qualifier RL 0.017 TestAmerica Tallahassee Page 78 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: R-1b Lab Sample ID: Client Matrix: 640-14341-2 Solid Date Sampled: Date Received: 12104/2007 0820 1210612007 0850 60108 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93371 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93138 Lab File ID: N/A Dilution: 1.0 Initial WeightNolume: 1.04 g Date Analyzed: 12/12/2007 0249 Final WeightNolume: 100 mL Date Prepared: 12/1012007 1406 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 3.7 0.96 Barium 41 0.96 Cadmium <0.48 0.48 Chromium 14 0.96 Iron 17000 9.6 Lead 5.6 0.48 Selenium X2.4 2.4 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMAN1 Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial WeightNolume: 1.05 g Date Analyzed: 12113/2007 1615 Final WeightNolume: 50 mL Date Prepared: 12/1112007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury <0.019 0.019 TestAmericaTallahassee page 79 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: R-1c Lab Sample ID: 640-14341-3 Client Matrix: Solid 60108 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93371 Instrument ID: ICP/AES Preparation: 3050E Prep Batch: 680-93138 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.13 g Date Analyzed: 12112!2007 0254 Final Weight/Volume: 100 mL Date Prepared: 12110/2007 1406 Analyte DryWt Corrected: N Result (mglKg) Qualifier RL Arsenic 3.5 0.88 Barium 39 0.88 Cadmium <0.44 0.44 Chromium 14 0.88 Iron 16000 8.8 Lead 5.8 0.44 Selenium <2.2 2.2 Analytical Data Job Number: 640-14341-1 Date Sampled: 12/04/2007 0820 Date Received: 12/0612007 0850 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: Preparation: 7471A Prep Batch: 680-93249 Lab File ID: Dilution: 1.0 Initial WeighWolume Date Analyzed: 1211312007 1617 Final Weightolume: Date Prepared: 1211112007 1159 Analyte Mercury DryWt Corrected: N Result (mglKg) 0.020 Qualifier LFEMANI NIA 1.17 g 50 mt_ RL 0.017 TestAmerica Tallahassee Page 80 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: R-113ub Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-4 Date Sampled: 12/0412007 0830 Client Matrix: Solid Date Received: 12/06/2007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 60108 Analysis Batch: 680-93371 Instrument ID: ICP/AES Preparation: 3050B Prep Batch: 680-93138 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.05 g Date Analyzed: 1211212007 0259 Final WeightNolume: 100 mL Date Prepared: 12/1012007 1406 Analyte DryWt Corrected: N Result (mglKg) Qualifier RL Arsenic 4.7 0.95 Barium 43 0.95 Cadmium <0.48 0.48 Chromium 14 0.95 Iron 20000 9.5 Lead 6.0 0,48 Selenium <2.4 2.4 Method: Preparation: Dilution: Date Analyzed Date Prepared Analyte Mercury 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) 7471A Analysis Batch: 680-93642 Instrument ID: 7471A Prep Batch: 680-93249 Lab File ID: 1.0 Initial WeightNolume: 12/1312007 1620 Final Weight/Volume: 1211112007 1159 DryWt Corrected: N Result (mg/Kg) 0.021 Qualifier LEEMANI NIA 1.20 g 50 mL RL 0.017 TestAmerica Tallahassee Page 81 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: R-1 Dub b Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-5 Solid Date Sampled: Date Received: 1210412007 0830 1210612007 0850 60106 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93371 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93138 Lab File ID: N/A Dilution: 1.0 Initial WeightfVolume: 1.08 g Date Analyzed: 12/12/2007 0303 Final WeightlVolume: 100 mL Date Prepared: 12110/2007 1406 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 4.2 0.93 Barium 40 0.93 Cadmium <0.46 0.46 Chromium 14 0.93 Iron 18000 9.3 Lead 5.7 0.46 Selenium <2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LFFMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: N/A Dilution: 1.0 Initial Weight[Volume: 1.04 g Date Analyzed: 12113/2007 1623 Final Weight/Volume: 50 mL Date Prepared: 12111/2007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.021 0.019 TestAmerica Tallahassee page 82 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: R-1 Dub c Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-6 Date Sampled: 12/0412007 0830 Client Matrix: Solid Date Received: 1210612007 0850 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93371 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93138 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.06 g Date Analyzed: 12/12/2007 0308 Final Weight/Volume: 100 mL Date Prepared: 12/1012007 1406 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 4.1 0.94 Barium 38 0.94 Cadmium <0.47 0.47 Chromium 13 0.94 Iran 17000 9.4 Lead 5.2 0.47 Selenium <2.4 2.4 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: Preparation: 7471A Prep Batch: 680-93249 Lab File ID: Dilution: 1.0 Initial WeightNolume: Date Analyzed: 1211312007 1631 Final WeightNolume: Date Prepared: 12/11/2007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.019 Qualifier LEEMAN1 NIA 1.07 g 50 mL RL 0.019 TestAmerica Tallahassee Page 83 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-1a Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-7 Solid Date Sampled: Date Received: 12104/2007 1040 12/0612007 0850 60108 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93371 Instrument ID: ICPYAES Preparation: 3050B Prep Batch: 680-93138 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.15 g Date Analyzed: 12112/2007 0313 Final Weight/Volume: 100 mL Date Prepared: 12/10/2007 1406 Analyte DryWt Corrected: N Result (mgtKg) Qualifier RL Arsenic 2.2 0.87 Barium 39 0.87 Cadmium <0.43 0.43 Chromium 10 0.87 Iron 9000 8.7 Lead 23 0.43 Selenium <2.2 2.2 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial WeightNolume: 1.01 g Date Analyzed: 12/13/2007 1634 Final Weight/Volume: 50 mL Date Prepared: 12111/2007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.047 Qualifier RL 0.020 TestAmericaTallahassee Page 84 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: IBRA b Jab Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-8 Solid Date Sampled: Date Received: 12/04/2007 1040 12/0612007 0850 601013 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 30508 Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.08 g Date Analyzed: 12/1612007 2129 Final Weight/Volume: 100 mL Date Prepared: 12/11/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 1.6 0.93 Barium 35 0.93 Cadmium <0.46 0.46 Chromium 9.0 0.93 Iron 8200 9.3 Lead 17 0.46 Selenium <2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial WeighWolume: 1.06 g Date Analyzed: 12/1312007 1636 Final Weight/Volume: 50 mL Date Prepared: 1211112007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.042 0.019 TestAmerica Tallahassee Page 85 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-1c Job Number: 640-14341-1 Lab Sample ID: 640-14341-9 Date Sampled: 12/04/2007 1040 Client Matrix: Solid Date Received: 12106/2007 0850 8a1UB Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: N/A Dilution: 1.0 Initial WeightNolume: 1.12 g Date Analyzed: 12/16/2007 2153 Final WeightNolume: 100 mL Date Prepared: 12/11/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 1.9 0.89 Barium 36 0.89 Cadmium <0.45 0.45 Chromium 9.1 0.89 Iron 8700 8.9 Lead 17 0.45 Selenium <2.2 2.2 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LFFMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.04 g Date Analyzed: 12/13/2007 1639 Final Weight/Volume: 50 ml Date Prepared: 12111/2007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.035 Qualifier RL 0.019 TestAmerica Tallahassee Page 86 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2a Job Number; 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-10 Solid Date Sampled: Date Received: 12/0412007 1100 12/06/2007 0850 60108 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 60108 Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 30506 Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeighWolume: 1.17 g Date Analyzed: 12/1612007 2157 Final Weightolume: 100 mL Date Prepared: 1211112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.0 0.85 Barium 39 0.85 Cadmium <0.43 0.43 Chromium 12 0.85 Iron 12000 8.5 Lead 13 0.43 Selenium <2.1 2.1 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method; 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.20 g Date Analyzed: 1211312007 1642 Final WeightNolume: 50 mL Date Prepared: 12/1112007 1159 Analyte Mercury DryWt Corrected: N Result (mglKg) 0.037 Qualifier RL 0.017 TestAmerica Tallahassee Page 87 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: 13R-2b Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-11 Solid Date Sampled: Date Received: 1210412007 1100 1210612007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAFS Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.10 g Date Analyzed: 12116/2007 2202 Final Weight/Volume: 100 ml Date Prepared: 12/11/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.3 0.91 Barium 39 0.31 Cadmium <0.45 0.45 Chromium 13 0.91 Iron 12000 9.1 Lead 13 0.45 Selenium X2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LFEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.10 g Date Analyzed: 12113/2007 1645 Final Weight/Volume: 50 ml Date Prepared: 12/11/2007 1159 Analyte Mercury DryWt Corrected: N Result (mglKg) 0.033 Qualifier RL 0.018 TestAmericaTallahassee Page 88 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2c Job Number: 640-14341-1 Lab Sample ID: 640-14341-12 Date Sampled: 12/0412007 1100 Client Matrix: Solid Date Received: 1210612007 0850 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 60106 Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightfVolume: 1.07 g Date Analyzed: 1211612007 2216 Final Weight/Volume: 100 mL Date Prepared: 12111/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.2 0.93 Barium 43 0.93 Cadmium X0.47 0.47 Chromium 14 0.93 Iron 13000 9.3 Lead 15 0.47 Selenium X2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMAN1 Preparation: 7471A Prep Batch: 680-93249 Lab File ID: N/A Dilution: 1.0 Initial Weight/Volume: 1.05 g Date Analyzed: 12/13/2007 1647 Final Weight/Volume: 50 mL Date Prepared: 12/11/2007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.034 Qualifier RL 0.019 TestAmerica Tallahassee Page 89 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2 Dub a Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-13 Solid Date Sampled: Date Received: 12104/2007 1115 12!0612007 0850 60108 Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.13 g Date Analyzed: 12/1612007 2221 Final Weight/Volume: 100 mL Date Prepared: 12111/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.4 0.88 Barium 42 0.88 Cadmium <0.44 0.44 Chromium 14 0.88 Iron 13000 8.8 Lead 14 0.44 Selenium <2.2 2.2 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.04 g Date Analyzed: 12/13/2007 1650 Final Weight/Volume: 50 mL Date Prepared: 1211112007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.031 0,019 TestAmerica Tallahassee Page 90 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: BR-2 Dub b Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-14 Date Sampled: 12/04/2007 1115 Client Matrix: Solid Date Received: 12/06/2007 0850 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 4.04 g Date Analyzed: 12/1612007 2226 Final Weight/Volume: 100 mL Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg1Kg) Qualifier RL Arsenic 2.1 0.96 Barium 40 0.96 Cadmium X0.48 0.48 Chromium 13 0.96 Iron 12000 9.6 Lead 13 0.48 Selenium <2.4 2.4 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: Preparation: 7471A Prep Batch: 680-93249 Lab File ID: Dilution: 1.0 Initial Weight/Volume: Date Analyzed: 1211312007 1653 Final WeighWolume: Date Prepared: 12/1112007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.034 Qualifier LEEMANI NIA 1.16 g 50 mL RL 0.017 TestAmerica Tallahassee Page 91 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: BR-2 Dub c Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-15 Solid Date Sampled: Date Received: 1210412007 1115 12/06/2007 0850 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICP/AES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.05 g Date Analyzed: 12/1612007 2230 Final WeighWolume: 100 mL Date Prepared: 1211112007 0829 Analyte DryWt Corrected: N Result (mglKg) Qualifier RL Arsenic 2.1 0.95 Barium 38 0.95 Cadmium <0.48 0.48 Chromium 13 0.95 Iron 12000 9.5 Lead 12 0.48 Selenium <2.4 2.4 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial WeightNolume: 1.08 g Date Analyzed: 12/1312007 1655 Final Weight/Volume: 50 mL Date Prepared: 12/11/2007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.034 0.019 TestAmerica Tallahassee Page 92 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-1 a Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-16 Solid Date Sampled: Date Received: 12/0412007 1200 12/0612007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 30506 Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.11 g Date Analyzed: 12/1612007 2235 Final WeightNolume: 100 ml Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 16 0.90 Barium 43 0.90 Cadmium <0.45 0.45 Chromium 14 0.90 Iron 18000 9.0 Lead 14 0.45 Selenium <2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LFEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.00 g Date Analyzed: 12/1312007 1704 Final WeightNolume: 50 mL Date Prepared: 12/11/2007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.030 0.020 TestAmerica Tallahassee Page 93 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-1 b Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-17 Solid Date Sampled: Date Received: 12/0412007 1200 12/0612007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightNolume: 1.09 g Date Analyzed: 12/1612007 2240 Final Weight/Volume: 100 ML Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 3.5 0.92 Barium 41 0.92 Cadmium <0.46 0.46 Chromium 13 0.92 Iron 17000 9.2 Lead 13 0.46 Selenium <2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LFFMAN1 Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.12 g Date Analyzed: 1211312007 1707 Final WeightNolume: 50 mL Date Prepared: 1211112007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.030 0.018 TestAmerica Tallahassee Page 94 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-1 c Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-18 Date Sampled: 1210412007 1200 Client Matrix: Solid Date Received: 1210612007 0850 6010B Inductively Coupled Plasma-Atomic Emission Spectrometry Method: 60108 Analysis Batch: 680-93808 Instrument ID: ICP/AES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeighWolume: 1.05 g Date Analyzed: 12/1612007 2244 Final Weight/Volume: 100 mL Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 3.5 0.95 Barium 39 0.95 Cadmium <0.48 O A8 Chromium 12 0.95 Iron 16000 9.5 Lead 12 0.48 Selenium <2.4 2.4 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: Preparation: 7471A Prep Batch: 680-93249 Lab File ID: Dilution: 1.0 Initial WeightlVolume: Date Analyzed: 12/13/2007 1709 Final WeightfVolume: Date Prepared: 12/11/2007 1159 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.027 Qualifier LEEMANI N/A 1.08 g 50 mL RL 0.019 TestAmerica Tallahassee Page 95 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-2 a Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-19 Solid Date Sampled: Date Received: 12/0412007 1215 12106!2007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICP/AES Preparation: 30506 Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightlVolume: 1.09 g Date Analyzed: 1211612007 2249 Final Weight/Volume: 100 mL Date Prepared: 1211112007 0829 Analyte DryWt Corrected: N Result (mg1K9) Qualifier RL Arsenic 3.1 0.92 Barium 42 0.92 Cadmium <0.46 0.46 Chromium 13 0.92 Iron 15000 9.2 Lead 11 0.46 Selenium <2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93642 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93249 Lab File ID: NIA Dilution: 1.0 Initial WeighWolume: 1.03 g Date Analyzed: 12/13/2007 1712 Final Weight/Volume: 50 mL Date Prepared: 12/11/2007 1159 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.028 0.019 TestAmerica Tallahassee Page 96 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-2 b Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-20 Date Sampled: 1210412007 1215 Client Matrix: Solid Date Received: 1210612007 0850 60108 Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 60106 Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightlVolume: 1.15 g Date Analyzed: 1211612007 2254 Final Weight/Volume: 100 mL Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.5 0.87 Barium 36 0.87 Cadmium <0.43 0.43 Chromium 11 0.87 Iron 13000 8.7 Lead 9.1 0.43 Selenium <2.2 2.2 Method: Preparation: Dilution: Date Analyzed Date Prepared Analyte Mercury 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) 7471A Analysis Batch: 680-93642 Instrument ID: 7471A Prep Batch: 680-93249 Lab File ID: 1.0 Initial Weight/Volume: 12/13/2007 1715 Final Weight/Volume: 12/1112007 1159 DryWt Corrected: N Result (mg/Kg) 0.024 Qualifier LEEMAN1 NIA 1.04 g 50 mL RL 0.019 TestAmerica Tallahassee Page 97 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-2 c Lab Sample ID: 640-14341-21 Client Matrix: Solid Analytical Data Job Number: 640-14341-1 Date Sampled: 12/04/2007 1215 Date Received: 12/06/2007 0850 601013 Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICP/AES Preparation; 30506 Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightNolume: 1.06 g Date Analyzed: 12/16/2007 2259 Final WeightlVolume: 100 mL Date Prepared: 12/11/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.9 0.94 Barium 41 0.94 Cadmium <0.47 0.47 Chromium 13 0.94 Iron 15000 9.4 Lead 11 0.47 Selenium <2.4 2.4 7471A Mercury in Solid or Semisolid Waste (Ma nual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93475 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93247 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.04 g Date Analyzed: 1211212007 1041 Final Weight/Volume: 50 mL Date Prepared: 12/1112007 1149 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.028 0.019 TestAmerica Tallahassee Page 98 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-3 a Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-22 Solid Date Sampled: Date Received: 12104/2007 1230 12106/2007 0850 6010E Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 30506 Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.09 g Date Analyzed: 1211712007 1114 Final Weight/Volume: 100 mL Date Prepared: 12111/2007 0829 Analyte DryWt Corrected: N Result (mglKg) Qualifier RL Arsenic 3.2 0.92 Barium 44 0.92 Cadmium X0.46 0.46 Chromium 14 0.92 Iron 15000 9.2 Lead 9.0 0.46 Selenium X2.3 2.3 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93475 Instrument ID: LEEMANI Preparation: 7411A Prep Batch: 680-93247 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.00 g Date Analyzed: 12/1212007 1050 Final Weight/Volume: 50 mt Date Prepared: 12/11/2007 1149 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Mercury 0.026 0.020 TestAmerica Tallahassee Page 99 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-3 b Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-23 Date Sampled: 12/04/2007 1230 Client Matrix: Solid Date Received: 12106/2007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightNolume: 1.08 g Date Analyzed: 12117/2007 1119 Final Weight/Volume: 100 ml Date Prepared: 12/11/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 3.4 0.93 Barium 47 0.93 Cadmium <0.46 0.46 Chromium 15 0.93 Iron 16000 9.3 Lead 22 0.46 Selenium <2.3 2.3 Method: Preparation: Dilution: Date Analyzed Date Prepared Analyte Mercury 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) 7471A Analysis Batch: 680-93475 Instrument ID: 7471A Prep Batch: 680-93247 Lab File ID: 1.0 Initial Weight/Volume: 12/1212007 1053 Final Weight/Volume: 12111/2007 1149 DryWt Corrected: N Result (mg/Kg) 0.027 Qualifier LEEMANI NIA 1.06 g 50 mL RL 0.019 TestAmerica Tallahassee Page 100 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-3 c Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-24 Solid Date Sampled: Date Received: 12/04/2007 1230 12106/2007 0850 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 60108 Analysis Batch: 680-93808 Instrument !D: ICPIAES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight[Volume: 1.12 g Date Analyzed: 1211712007 1123 Final Weight/Volume: 100 mL Date Prepared: 1211112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.8 0.89 Barium 43 0.89 Cadmium <0.45 0.45 Chromium 14 0.89 Iron 15000 8.9 Lead 8.6 0.45 Selenium <2.2 2.2 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93475 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93247 Lab File ID: NIA Dilution: 1.0 Initial WeightlVolume: 1.11 g Date Analyzed: 1211212007 1056 Final Weight/Volume: 50 mL Date Prepared: 12/1112007 1149 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.027 Qualifier RL 0.018 7estAmericaTallahassee Page 101 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: SA-4 a Job Number: 640-14341-1 Lab Sample ID: Client Matrix: 640-14341-25 Solid Date Sampled: Date Received: 12104/2007 1245 12/06/2007 0850 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICP/AFS Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 1.13 g Date Analyzed: 12/1712007 1137 Final Weight(Volume: 100 mL Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.2 0.88 Barium 45 0.88 Cadmium <0.44 0.44 Chromium 13 0.88 Iron 13000 8.8 Lead 13 0.44 Selenium <2.2 2.2 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93475 Instrument ID: LEEMANI Preparation: 7471A Prep Batch: 680-93247 Lab File ID: NIA Dilution; 1.0 Initial WeightiVolume: 1.03 g Date Analyzed: 1211212007 1058 Final Weight/Volume: 50 mL Date Prepared: 12/1112007 1149 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.027 Qualifier RL 0.019 TestAmerica Tallahassee Page 102 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-4 b Analytical Data Job Number: 640-14341-1 Lab Sample ID: 640-14341-26 Date Sampled: 12/0412007 1245 Client Matrix: Solid Date Received: 12/06/2007 0850 6010B Inductively Coupled Plasma - Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: ICP/AES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightlVolume: 1.08 g Date Analyzed: 12117/2007 1143 Final WeightNalume: 100 mL Date Prepared: 12111/2007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.0 0.93 Barium 47 0.93 Cadmium <046 0.46 Chromium 13 0.93 Iron 12000 9.3 Lead 12 0.46 Selenium <2.3 2.3 Method: Preparation: Dilution: Date Analyzed Date Prepared Analyte Mercury 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) 7471A Analysis Batch: 680-93475 Instrument ID: 7471A Prep Batch: 680-93247 Lab File ID: 1.0 Initial WeightNolume 12/1212007 1101 Final Weight/Volume: 12/11/2007 1149 DryWt Corrected: N Result (mg/K9) 0.027 Qualifier LEEMAN1 NIA 1.00 g 50 mL RL 0.020 TestAmericaTallahassee Page 103 of 167 12/21/2007 Client: Environmental Services, Inc. Client Sample ID: SA-4 c Lab Sample ID: 640-14341-27 Client Matrix: Solid 6010B Inductively Coupled Plasma -Atomic Emission Spectrometry Method: 6010B Analysis Batch: 680-93808 Instrument ID: iCP1AES Preparation: 3050B Prep Batch: 680-93199 Lab File ID: NIA Dilution: 1.0 Initial WeightiVolume: 1.04 g Date Analyzed: 12/17/2007 1150 Final Weight/Volume: 100 mL Date Prepared: 12/1112007 0829 Analyte DryWt Corrected: N Result (mg/Kg) Qualifier RL Arsenic 2.1 0.96 Barium 47 0.96 Cadmium <0.48 0.48 Chromium 13 0.96 Iron 13000 9.6 Lead 13 0.48 Selenium <2.4 2.4 Analytical Data Job Number: 640-14341-1 Date Sampled: 12/0412007 1245 Date Received: 12/06/2007 0850 7471A Mercury in Solid or Semisolid Waste (Manual Cold Vapor Technique) Method: 7471A Analysis Batch: 680-93475 Instrument ID: Preparation: 7471A Prep Batch: 680-93247 Lab File ID: Dilution: 1.0 Initial WeighWolume: Date Analyzed: 12112/2007 1104 Final WeighWolume: Date Prepared: 12/11/2007 1149 Analyte Mercury DryWt Corrected: N Result (mg/Kg) 0.029 Qualifier LEEMAN1 NIA 1.06 g 50 mL RL 0.019 TestAmericaTallahassee Page 104 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: EB-1 Job Number: 640-14341-1 Lab Sample ID: 640-14341-28 Date Sampled: 12104!2007 0815 Client Matrix: Water Date Received: 12/0612007 0850 60106 Inductively Coupled Plasma -Atomic Emission Spectrometry-Total Recoverable Method: 6010B Analysis Batch: 680-93370 Instrument ID: ICPIAES Preparation: 3005A Prep Batch: 680-93140 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 1211212007 0016 Final Weight/Volume: 50 mL Date Prepared: 12110/2007 1412 Analyte Result (ug/L) Qualifier RL Arsenic <10 10 Barium <10 10 Beryllium <4.0 4.0 Cadmium <5.0 5.0 Chromium <10 10 Iron <50 50 Lead <5.0 5.0 Selenium <10 10 Method: Preparation: Dilution: Date Analyzed Date Prepared Analyte Mercury 7470A Mercury in Liquid Waste (Manual Cold Vapor Technique) 7470A Analysis Batch: 680-93296 Instrument ID: LEEMANI 7470A Prep Batch: 680-93141 Lab File ID: NIA 1.0 Initial WeighWolume: 50 mL 12/11/2007 1251 Final Weight/Volume: 50 mL 12/1012007 1424 Result (ug1L) <0.20 Qualifier RL 0.20 TestAmerica Tallahassee Page 105 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Client Sample ID: EB-2 Job Number: 640-14341-1 Lab Sample ID: 640-14341-29 Date Sampled: 12/0412007 1400 Client Matrix: Water Date Received: 12/0612007 0850 60106 Inductively Coupled Plasma -Atomic Emission Spectrometry-Total Recoverable Method: 6010B Analysis Batch: 680-93370 Instrument ID: ICPIAES Preparation: 3005A Prep Batch: 680-93140 Lab File ID: NIA Dilution: 1.0 Initial Weight/Volume: 50 mL Date Analyzed: 12/12/2007 0021 Final Weight/Volume: 50 mL Date Prepared: 12110/2007 1412 Analyte Result (ug1L) Qualifier RL Arsenic <10 10 Barium <10 10 Beryllium <4.0 4.0 Cadmium <5.0 5.0 Chromium <10 10 Iron <50 50 Lead <5.0 5.0 Selenium <10 10 Method: Preparation: Dilution: Date Analyzed: Date Prepared: Analyte Mercury 7470A Mercury in Liquid Waste (Manual Cold Vapor Technique) 7470A Analysis Batch: 680-93296 Instrument ID: LEEMANI 7470A Prep Batch: 680-93141 Lab File ID: NIA 1.0 Initial Weight/Volume: 50 mL 1211112007 1254 Final WeighUVolume: 50 mL 12/1012007 1424 Resuit (ug/L) <0.20 Qualifier RL 0.20 TestAmerica Tallahassee Page 106 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: R-1 Lab Sample ID: 640-14341-1 Date Sampled: 12104/2007 0820 Client Matrix: Solid % Moisture: 57.5 Date Received: 12/06/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <9.4 mg1Kg 9.4 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/14/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.2 mg/Kg 1.2 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/14/2007 0514 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12/12/2007 1300 Cyanide, Total <1.2 mg1Kg 1.2 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/1412007 0514 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12/12/2007 1300 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.1 mg/Kg 1.1 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12111/2007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12111/2007 0629 Percent Moisture 57 % 0,010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 1211012007 1220 Client Sample ID: R-1b Lab Sample ID: 640-14341-2 Date Sampled: 1210412007 0820 Client Matrix: Solid % Moisture: 73.1 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <15 mg/Kg 15 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12114/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.8 mg/Kg 1.8 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12114/2007 0516 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12112/2007 1300 Cyanide, Total <1,8 mg/Kg 1.8 1.0 9012A Anly Batch: 680-93525 Date Analyzed 1211412007 0516 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12112/2007 1300 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Di ssociable <1.9 mg/Kg 1.9 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/11/2007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12/1112007 0629 Percent Moisture 73 % 0.010 1.0 PercentMoisture Anly Batch: 680-93 1 1 6 Date Analyzed 1211012007 1220 TestAmerica Tallahassee Page 107 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID; R-1c Lab Sample ID: 640-14341-3 Date Sampled: 12104/2007 0820 Client Matrix: Solid % Moisture: 73.5 Date Received: 12106/2007 0850 Analyte Result Dual Units RL Dil Method Fluoride-S <15 mg/Kg 15 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12114/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.9 mg/Kg 1.9 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/14/2007 0517 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12/12/2007 1300 Cyanide, Total <1.9 mg/Kg 1.9 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/1412007 0517 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 1211212007 1300 Analyte Result Dual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.8 mg/Kg 1.8 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/11/2007 1226 DryWt Corrected: Y Prep Batch; 680-93191 Date Prepared: 12/11/2007 0629 Percent Moisture 74 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 Client Sample ID: R-113ub Lab Sample ID: 640-14341-4 Date Sampled: 12/0412007 0830 Client Matrix: Solid % Moist ure: 66.3 Date Received: 12/06/2007 0850 Analyte Result Dual Units RL Dil Method Fluoride-S <12 mg/Kg 12 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/14/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.5 mg1Kg 1.5 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/14/2007 0518 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12/1212007 1300 Cyanide, Total <1.5 mg/Kg 1.5 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12!1412007 0518 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12112/2007 1300 Analyte Result Dual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.4 mg/Kg Anly Batch: 680-93253 Date Analyzed 12/11/2007 1226 Prep Batch: 680-93191 Date Prepared: 1211112007 0629 Percent Moisture 66 % Anly Batch: 680-93116 Date Analyzed 12/10/2007 1220 1.4 1.0 SM 4500 CN I DryWt Corrected; Y 0.010 1.0 PercentMoisture TestAmerica Tallahassee Page 108 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample 1D: R-1Dub b Lab Sample ID: 640-14341-5 Date Sampled: 12104/2007 0830 Client Matrix: Solid % Moisture: 70.7 Date Received: 12/06/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <14 mg/Kg 14 1,0 340.2 Anly Batch: 680-93684 Date Analyzed 12/1412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.7 mglKg 1.7 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/1412007 0520 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12/1212007 1300 Cyanide, Total <1.7 mg/Kg 1.7 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/1412007 0520 DryVyt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12/1212007 1300 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.6 mg1Kg 1.6 1.0 SM 4500 CN Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared ; 1211112007 0629 Percent Moisture 71 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 1211012007 1220 Client Sample ID: R-1Dub c Lab Sample ID: 640-14341-6 Date Sampled: 12104/2007 0830 Client Matrix: Solid % Moist ure: 70.5 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <13 mglKg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/1412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.7 mg1Kg 1.7 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12114/2007 0521 DryWt Corrected: Y Prep Batch; 680-93323 Date Prepared : 12112/2007 1300 Cyanide, Total <1.7 mg1Kg 1.7 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/14/2007 0521 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12112/2007 1300 Analyte Result Qua] Units RL Dil Method Cyanide, Weak Acid Dissociable <1.7 mg/Kg Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 Prep Batch: 680-93191 Date Prepared; 12111/2007 0629 Percent Moisture 70 % Anly Batch: 680-93116 Date Analyzed 1211012007 1220 1.7 1.0 SM 4500 CN DryWt Corrected: Y 0.010 1.0 PercentMoisture TestAmerica Tallahassee Page 109 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID; BR-1a Lab Sample ID: 640-14341-7 Date Sampled: 12/0412007 1040 Client Matrix: Solid % Moisture: 64.1 Date Received: 12/0612007 0850 Analyte Result Qua[ Units RL Dil Method Fluoride-S <11 mg/Kg 11 1A 340.2 Anly Batch: 680-93684 Date Analyzed 1211412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93525 Date Analyzed 1211412007 0521 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 1211212007 1300 Cyanide, Total 21 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/14/2007 0521 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12/1212007 1300 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.3 mg/Kg 1.3 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12/1112007 0629 Percent Moisture 64 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/10/2007 1220 Client Sample ID: BR-1b Lab Sample ID: 640-14341-8 Date Sampled: 1210412007 1040 Client Matrix: Solid % Moisture: 65.3 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12114/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12114/2007 0522 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12112/2007 1300 Cyanide, Total <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12114/2007 0522 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12112/2007 1300 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.4 mg/Kg Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 Prep Batch: 680-93191 Date Prepared: 12/1112007 0629 Percent Moisture 65 % Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 1.4 1.0 SM 4500 CN I DryWt Corrected: Y 0.010 1.0 PercentMoisture TestAmerica Tallahassee Page 110 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: 13R-1c Lab Sample ID: 640-14341-9 Date Sampled: 12104/2007 1040 Client Matrix: Solid % Moisture: 66.3 Date Received: 12106/2007 0850 Analyte Result Qual Units RL oil Method Fluoride-S <12 mg/Kg 12 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12!1412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.5 mglKg 1.5 1.0 9012A ANy Batch: 680-93525 Date Analyzed 1211412007 0523 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12/12/2007 1300 Cyanide, Total <1.5 mg/Kg 1.5 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12/14/2007 0523 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared : 12/1212007 1300 Analyto Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.5 mg/Kg 1.5 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12111/2007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared : 1211112007 0629 Percent Moisture 66 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 Client Sample ID: BR-2a Lab Sample ID: 640-14341-10 Date Sampled: 1210412007 1100 Client Matrix: Solid % Moisture: 68.2 Date Received: 1210612007 0850 Analyto Result Qual Units RL Dil Method Fluoride-S <13 mg/Kg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 1211412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.6 mg/Kg 1.6 1.0 9012A Anly Batch: 680-93525 Date Analyzed 1211412007 0524 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12112/2007 1300 Cyanide, Total <1.6 mglKg 1.6 1.0 9012A Anly Batch: 680-93525 Date Analyzed 12114/2007 0,524 DryWt Corrected: Y Prep Batch: 680-93323 Date Prepared: 12/1212007 1300 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Di ssociable <1.5 mg/Kg 1.5 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12111!2007 0629 Percent Moisture 68 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 TestAmerica Tallahassee Page 111 of 167 12/21/2007 Client: Environmental Services, Inc. Analytical Data Job Number: 640-14341-1 General Chemistry Client Sample ID: BR-2b Lab Sample ID: 640-14341-11 Date Sampled: 12104/2007 1100 Client Matrix: Solid % Moisture: 69.1 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <13 mg/Kg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12114/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.6 mg/Kg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12117/2007 0842 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 1211312007 1201 Cyanide, Total 0.6 mg/Kg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 1211712007 0842 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/1312007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.6 mg/Kg 1.6 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared : 12/1112007 0629 Percent Moisture 69 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 Client Sample ID: BR-2c Lab Sample 10: 640-14341-12 Date Sampled: 12/04/2007 1100 Client Matrix: Solid % Moist ure: 68.8 Date Received: 1210612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <13 mg/Kg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12114/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.6 mg/Kg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12117/2007 0844 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 12113/2007 1201 Cyanide, Total <1.6 mg/Kg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/17/2007 0844 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 1211312007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.6 mg/Kg Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 Prep Batch: 680-93191 Date Prepared: 1211112007 0629 Percent Moisture 69 % Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 TestAmerica Tallahassee page 112 of 167 1.6 1.0 SM 4500 CN I DryWt Corrected: Y 0.010 1.0 PercentMoisture 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: BR-2 Dub a Lab Sample ID: 640-14341-13 Date Sampled: 12/0412007 1115 Client Matrix: Solid % Moist ure: 68.9 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <13 mg/Kg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 1211412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.6 mglKg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/17/2007 0845 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 12/13/2007 1201 Cyanide, Total <1.6 mg1Kg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12117/2007 0845 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 1211312007 1201 Analyte Result Qual Units RL DO Method Cyanide, Weak Acid Dissociable <1.6 mglKg 1.6 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/11/2007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared : 12/11/2007 0629 Percent Moisture 69 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/10/2007 1220 Client Sample 1D: BR-2 Dub b Lab Sample ID: 640-14341-14 Date Sampled: 12104/2007 1115 Client Matrix: Solid % Moist ure: 69.9 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <13 mg/Kg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/14/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.7 mglKg 1.7 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/17/2007 0847 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 12/1312007 1201 Cyanide, Total <1.7 mglKg 1.7 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/17/2007 0847 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 12/13/2007 1201 Anatyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.6 mg/Kg Anly Batch: 680-93253 Date Analyzed 12/11/2007 1226 Prep Batch: 680-93191 Date Prepared: 12/11/2007 0629 Percent Moisture 70 % Anly Batch: 680-93116 Date Analyzed 12/10/2007 1220 TestAmerica Tallahassee Page 113 of 167 1.6 1.0 SM 4500 CN I DryWt Corrected: Y 0.010 1.0 PercentMoisture 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: SR-2 Dub c Lab Sample ID: 640-14341-15 Date Sampled: 12104/2007 1115 Client Matrix: Solid % Moisture: 68.4 Date Received: 1210612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <13 mg/Kg 13 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/1412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.6 mg/Kg 1.6 1.0 9012A Anly Batch: 680-93723 Date Analyzed 1211712007 0848 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/13/2007 1201 Cyanide, Total <1.6 mglKg 1.6 1,0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0848 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/1312007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.5 mg/Kg 1.5 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12/1112007 0629 Percent Moisture 68 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 Client Sample tD: SA-1 a Lab Sample ID: 640-14341-16 Date Sampled: 1210412007 1200 Client Matrix: Solid % Moisture: 61.1 Date Received: 12/0612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <10 mg/Kg 10 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 1211412007 1324 DryWt Corrected: Y Cyanide, Amenable <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0849 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12113/2007 1201 Cyanide, Total 1.9 mg/Kg 1.3 1A 9012A Anly Batch: 680-93723 Date Analyzed 12!1712007 0849 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12113/2007 1201 Analyte Result Qual Units Rt- Dil Method Cyanide, Weak Acid Dissociable <1.2 mg/Kg 1.2 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12111/2007 0629 Percent Moisture 61 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/10/2007 1220 TestAmerica Tallahassee Page 114 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 Client Sample ID: Lab Sample ID: Client Matrix: Analyte SA-1 b 640-14341-17 Solid Result General Chemistry % Moisture: 62.5 Qual Units Date Sampled: Date Received: RL 12/04/2007 1200 12106/2007 0850 Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/14/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0902 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/1312007 1201 Cyanide, Total 1.8 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0902 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/13/2007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.2 mg/Kg 1.2 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared: 12/11/2007 0629 Percent Moisture 62 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 Client Sample ID: SA-1 c Lab Sample 1D: 640-14341-18 Date Sampled: 1210412007 1200 Client Matrix: Solid % Moisture: 61.4 Date Received: 1210612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <10 mg/Kg 10 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12114/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12117/2007 0850 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12113/2007 1201 Cyanide, Total 2.0 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12117/2007 0850 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12113/2007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.2 mg/Kg Anly Batch: 680-93253 Date Analyzed 12111/2007 1226 Prep Batch: 680-93191 Date Prepared: 12111/2007 0629 Percent Moisture 61 % Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 1.2 1.0 SM 4500 CN I DryWt Corrected: Y 0.010 1.0 PercentMoisture TestAmerica Tallahassee Page 115 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Jab Number: 640-14341-1 General Chemistry Client Sample ID: SA-2 a Lab Sample ID: 640-14341-19 Date Sampled: 12104/2007 1215 Client Matrix: Solid % Moisture: 64,6 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/14/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/17/2007 0851 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 12/1312007 1201 Cyanide, Total <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0851 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared : 12/1312007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Di ssociable <1.4 mg/Kg 1.4 1.0 SM 4500 CN I Anly Batch: 680-93253 Date Analyzed 12/1112007 1226 DryWt Corrected: Y Prep Batch: 680-93191 Date Prepared : 12/11/2007 0629 Percent Moisture 65 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 Client Sample ID: SA-2 b Lab Sample ID: 640-14341-20 Date Sampled: 12104/2007 1215 Client Matrix: Solid % Moisture: 63.7 Date Received: 12106/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93684 Date Analyzed 12/14/2007 1324 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0852 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/1312007 1201 Cyanide, Total <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93723 Date Analyzed 12/1712007 0852 DryWt Corrected: Y Prep Batch: 680-93479 Date Prepared: 12/1312007 1201 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.3 mg/Kg Anly Balch: 680-93253 Date Analyzed 12/1112007 1226 Prep Batch: 680-93191 Date Prepared: 12/11/2007 0629 Percent Moisture 64 % Anly Batch: 680-93116 Date Analyzed 12/10/2007 1220 1.3 1.0 SM 4500 CN I DryWt Corrected: Y 0.010 1.0 PercentMoisture TestAmerica Tallahassee Page 116 of 167 12/21/2007 Client: Environmental Services, Inc. Analytical Data Job Number: 640-14341-1 General Chemistry Client Sample ID: SA-2 c Lab Sample ID: 640-14341-21 Date Sampled: 12/04/2007 1215 Client Matrix: Solid % Moist ure: 65.5 Date Received: 12/0612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <12 mg/Kg 12 1.0 340.2 Anly Batch: 680-93682 Date Analyzed 12114/2007 1133 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12118/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared : 1211712007 1132 Cyanide, Total <1A mq/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 1211812007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared : 12117/2007 1132 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.5 mg/Kg 1.5 1.0 SM 4500 CN I Anly Batch: 680-93256 Date Analyzed 12111/2007 1234 DryWt Corrected: Y Prep Batch: 680-93200 Date Prepared : 1211112007 0834 Percent Moisture 66 % 0.010 1.0 PercenlMoisture Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 Client Sample ID: SA-3 a Lab Sample ID: 640-14341-22 Date Sampled: 12104/2007 1230 Client Matrix: Solid % Moisture: 62.7 Date Received: 12/0612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93682 Date Analyzed 12/14/2007 1133 DryWt Corrected: Y Cyanide, Amenable <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12118/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared : 1211712007 1132 Cyanide, Total <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12118/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared : 1211712007 1132 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.2 mg/Kg 1.2 1.0 SM 4500 CN I Anly Batch: 680-93256 Date Analyzed 12111/2007 1234 DryWt Corrected: Y Prep Batch: 680-93200 Date Prepared : 12111/2007 0834 Percent Moisture 63 % 0.010 1.0 PercentMoisture Anly Batch: 680-9 31 1 6 Date Analyzed 12/10/2007 1220 TestAmerica Tallahassee Page 117 of 167 12/21/2007 Client: Environmental Services, Inc. Analytical Data Job Number: 640-14341-1 General Chemistry Client Sample ID: SA-3 b Lab Sample ID: 640-14341-23 Date Sampled: 12/04/2007 1230 Client Matrix: Solid % Moisture: 60.5 Date Received: 12/06/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <10 mg/Kg 10 1.0 340.2 Aoly Batch: 680-93682 Date Analyzed 12114/2007 1133 DryWt Corrected: Y Cyanide, Amenable <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12118/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared: 12117/2007 1132 Cyanide, Total <1.3 mg/Kg 1.3 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12118/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared: 12117/2007 1132 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.2 mg/Kg 1.2 1.0 SM 4500 CN I Anly Batch: 680-93256 Date Analyzed 1211112007 1234 DryWt Corrected: Y Prep Batch: 680-93200 Date Prepared: 12111/2007 0834 Percent Moisture 60 % 0.010 1.0 PercentiNoisture Anly Batch: 680-93116 Date Analyzed 12/1012007 1220 Client Sample ID; SA-3 c Lab Sample ID: 640-14341-24 Date Sampled: 1210412007 1230 Client Matrix: Solid % Moisture; 63.8 Date Received: 12/0612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93682 Date Analyzed 12114/2007 1133 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12/18/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared: 12117/2007 1132 Cyanide, Total <1A mg/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12118/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared: 12/17/2007 1132 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.3 mg/Kg 1.3 1.0 SM 4500 CN I Anly Batch: 680-93256 Date Analyzed 1211112007 1234 DryWt Corrected: Y Prep Batch; 680-93200 Date Prepared : 12/1112007 0834 Percent Moisture 64 % 0.010 1.0 PercentMoisture Anly Batch; 680-93116 Date Analyzed 12/1012007 1220 TestAmerica Tallahassee Page 118 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: SA-4 a Lab Sample ID: 640-14341-25 Client Matrix: Solid % Moisture: 63.1 Date Sampled: 12104/2007 1245 Date Received: 12/06/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93682 Date Analyzed 12/14/2007 1133 DryWt Corrected: Y Cyanide, Amenable <1.4 Anly Batch: 680-93982 Prep Batch: 680-93765 Cyanide, Total 2.6 Anly Batch: 680-93982 Prep Batch: 680-93765 mg/Kg 1.4 1.0 9012A Date Analyzed 12/1812007 1311 DryW1 Corrected: Y Date Prepared: 12117/2007 1132 mg/Kg 1.4 1.0 9012A Date Analyzed 12/18/2007 1311 DryWt Corrected: Y Date Prepared: 12/17/2007 1132 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1.3 mg/Kg 1.3 1.0 SM 4500 CN I Anly Batch: 680-93256 Date Analyzed 12111/2007 1234 DryWt Corrected: Y Prep Batch: 680-93200 Date Prepared: 12/11/2007 0834 Percent Moisture 63 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 Client Sample ID: SAA b Lab Sample 1D: 640-14341-26 Date Sampled: 12104/2007 1245 Client Matrix: Solid % Moisture: 63.7 Date Received: 1210612007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93682 Date Analyzed 12/14/2007 1133 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 1211812007 1311 DryWt Corrected: Y Prep Batch; 680-93765 Date Prepared: 1211712007 1132 Cyanide, Total 3.0 mg/Kg 1.4 1.0 9012A Anly Batch; 680-93982 Date Analyzed 12/18/2007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared: 12117/2007 1132 Analyte Result Qua! Units RL Dil Method Cyanide, Weak Acid Dissociable <1A mg/Kg 1.4 1.0 SM 4500 CN J Anly Batch: 680-93256 Date Analyzed 12/11/2007 1234 DryWt Corrected: Y Prep Batch: 680-93200 Date Prepared: 12111/2007 0834 Percent Moisture 64 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 TestAmericaTallahassee Page 119 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: SA-4 c Lab Sample ID: 640-14341-27 Date Sampled: 12/04/2007 1245 Client Matrix: Solid % Moist ure: 64.7 Date Received: 12/06/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride-S <11 mg/Kg 11 1.0 340.2 Anly Batch: 680-93682 Date Analyzed 12/1412007 1133 DryWt Corrected: Y Cyanide, Amenable <1.4 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 1211812007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared : 1211712007 1132 Cyanide, Total 2.2 mg/Kg 1.4 1.0 9012A Anly Batch: 680-93982 Date Analyzed 12/1812007 1311 DryWt Corrected: Y Prep Batch: 680-93765 Date Prepared : 1211712007 1132 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <1A mg/Kg 1.4 1.0 SM 4500 CN I Anly Batch: 680-93256 Date Analyzed 12/1112007 1234 DryWt Corrected: Y Prep Batch: 680-93200 Date Prepared : 1211112007 0834 Percent Moisture 65 % 0.010 1.0 PercentMoisture Anly Batch: 680-93116 Date Analyzed 12110/2007 1220 Client Sample ID: EB-1 Lab Sample ID: 640-14341-28 Date Sampled: 1210412007 0815 Client Matrix; Water Date Received: 12/0612007 0850 Analyte Result Qual Units RL Dil Method Fluoride <0.20 mg/L 0.20 1.0 340.2 Anly Batch: 680-93651 Date Analyzed 12/1412007 1049 Cyanide, Amenable <0.010 mg1L 0.010 1.0 9012A Anly Batch: 680-93983 Date Analyzed 1211812007 1311 Prep Batch: 680-93847 Date Prepared : 12118/2007 0646 Cyanide, Total <0.010 mg/L 0.010 1.0 9012A Anly Batch: 680-93983 Date Analyzed 12118/2007 1311 Prep Batch: 680-93847 Date Prepared : 12/18/2007 0646 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Dissociable <0.010 mg1L 0.010 1.0 SM 4500 CN I Anly Batch: 680-93257 Date Analyzed 12/11/2007 1236 Prep Batch: 680-93202 Date Prepared : 12/11/2007 0836 TestAmerica Tallahassee page 120 of 167 12/21/2007 Analytical Data Client: Environmental Services, Inc. Job Number: 640-14341-1 General Chemistry Client Sample ID: EB-2 Lab Sample ID: 640-14341-29 Date Sampled: 12104!2007 1400 Client Matrix: Water Date Received: 12/06/2007 0850 Analyte Result Qual Units RL Dil Method Fluoride <0.20 mg/L 0.20 1.0 340.2 Anly Batch: 680-93651 Date Analyzed 12114/2007 1049 Cyanide, Amenable <0.010 mg/L 0.010 1.0 9012A Anly Batch: 680-93983 Date Analyzed 12/18/2007 1311 Prep Batch: 680-93847 Date Prepared: 12/18/2007 0646 Cyanide, Total <0.010 mg1L 0.010 1.0 9012A Anly Batch: 680-93983 Date Analyzed 12/18/2007 1311 Prep Batch: 680-93847 Date Prepared; 12/18/2007 0646 Analyte Result Qual Units RL Dil Method Cyanide, Weak Acid Di ssociable <0.010 mg/L 0.010 1.0 SM 4500 CN Anly Batch: 680-93257 Date Analyzed 12/11/2007 1236 Prep Batch: 680-93202 Date Prepared: 12111/2007 0836 TestAmerica Tallahassee Page 121 of 167 12/21/2007 DATA REPORTING QUALIFIERS Client: Environmental Services, Inc. Job Number: 640-14341-1 Lab Section Qualifier Description GC/MS Semi VOA F MS or MSD exceeds the control limits 4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D. GC Semi VOA X Surrogate exceeds the control limits P The lower of the two values is reported when the % difference between the results of two GC columns is greater than 40% Metals 4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. General Chemistry F MS or MSD exceeds the control limits TestAmerica Tallahassee Page 122 of 167 12/21/2007