WQ0004910_Monitoring - 10-2020_20201123 (2)

GW-59A COMPLIANCE REPORT FORM Permit # GlI D D
(Submit one each monitoring period with GW-59 forms.)
1l
1
Enter date monitoring results were due. 12L 'u Will this monitoring report (GW-59 and GW-594)
YES
NO
be submitted after the established due date. r
c,)„j Ne II Jock- dowru 6v: c� �
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
%w PJl�kl� i��<< 1 �� 10W A.7
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Officeforguidance.
4
Are any monitored constituents equal to or above the established standards?
YES
N
If the answer to question 4 is "NO'; skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO'; skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is havifto at the review and compliance
boundaries surrounding this facility. Failure to do so may subject e permittee to a Notice of Violation,
fines, and/or penalties.
77
3 00)
8
The person completing this portion (GW-59A) of the monitorin port iNbuld Sign below and submit this
form with GW-59 forms for required wells to the address provided at the topw�the current GW-59 form.
w.�
1 hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
V 2-
tigrAture of Permittee (or Aufhorized Agent) Date'
GW-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 11/16/20
Facility Name: Town of Woodland
Non -Discharge WQ0004910 UIC
Permit Name (if different):
NPDES Other
Facility Address: 414 Jameson Ave Woodland NC 27897
TYPE OF PERMITTED OPERATION BEING MONITORED
414 Jameson Ave Woodland NC 27897
County Northampton
❑■ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Raymond S. Eaton
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: WWTP irrigation fields
No. of wells to be sampled: 5
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW1
Date sample collected: 10/06/20
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2 in.
pH 00400: 7 units Temp. 000lo: 19.5 °C
DRY at
Depth to Water Level 82546:6.5 ft. below measuring
p g point Screened Interval: 13 ft. to
18
ft. Spec. Cond. 000sa: µ Mhos
time of
sampling,
Measuring Point is 2 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling:
4
gallons
Appearance clear
here:
❑
Samples for metals were collected unfiltered: ❑■ YES
El NO and field acidified: El YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:10/06/20-10/14/20
Laboratory Name: Envirnment 1, Inc
Certification No.
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.28
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.06
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 97
mg/L
Al - Aluminum oilo5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 <1.00
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 19
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS *Ld�SSING UjVi ,
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑■ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <0.04
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen: NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 11/16/20
Facility Name: Town of Woodland
Non -Discharge WQ0004910 UIC
Permit Name (if different):
NPDES Other
Facility Address: 414 Jameson Ave Woodland NC 27897
TYPE OF PERMITTED OPERATION BEING MONITORED
414 Jameson Ave Woodland NC 27897
County Northampton
0 Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Raymond S. Eaton
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: WWTP irrigation fields
No. of wells to be sampled: 5
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW3
Date sample collected: 10/06/20
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2 in.
pH 00400: 6.8 units Temp. 000lo: 19.9 °C
DRY at
Depth to Water Level 82546:6.9 ft. below measuring point Screened Interval: 13 ft. to
18
ft. Spec. Cond. 00094: µMhos
time of
—
sampling,
Measuring Point is 2 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling:
4
gallons
Appearance clear
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:10/06/20-10/14/20
Laboratory Name: Envirnment 1, Inc
Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.10
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P006650.07
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 114
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.04
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 39
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ■❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo610 0.04
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH,as N: Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.05-02-2017

r
SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• • .
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 11/16/20
Facility Name: Town of Woodland
Non -Discharge WQ0004910 UIC
NPDES Other
Permit Name (if different):
Facility Address: 414 Jameson Ave Woodland NC 27897
TYPE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
414 Jameson Ave Woodland NC 27897 County Northampton
❑■ Spray Field ❑ Remediation:
Contact Person: Raymond S. Eaton
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: WWTP irrigation fields
No. of wells to be sampled: 5
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW6
Date sample collected: 10/06/20
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter. 2 in.
pH 00400: 6.8 units Temp. 000lo: 19.1 °C
DRY at
Depth to Water Level 82546:6.7 ft. below measuring point Screened Interval: 13 ft. to
18
ft. Spec. Cond. 00094: µMhos
time of
—
sampling,
Measuring Point is 2 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling:
4
gallons
Appearance clear
here:❑
Samples for metals were collected unfiltered: K YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:10/06/20-10/14/20
Laboratory Name: Envirnment 1, Inc
Certification No.
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.18
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.14
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 703oo 202
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 <1.00
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 79
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <0.04
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines an,: imprisonment for knowing violations.
Perrinittew1or Authorized Aqent) Name and Title - Please print or type Siq.4turgrbf Permittee (or Authorized Aqent) (Date)
GW-59 Rev. 05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 11/16/20
Facility Name: Town of Woodland
Non -Discharge WQ0004910 UIC
NPDES Other
Permit Name (if different):
Facility Address: 414 Jameson Ave Woodland NC 27897
TYPE OF PERMITTED OPERATION BEING MONITORED
414 Jameson Ave Woodland NC 27897
County Northampton
❑■ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Raymond S. Eaton
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: WWTP irrigation fields
No. of wells to be sampled: 5
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW8
Date sample collected: 10/06/20
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2 in.
pH 00400: 6.7 units Temp. 000io: 19.2 °C
DRY at
Depth to Water Level 82546:7.1 ft. below measuring point Screened Interval: 13 ft. to
18
ft. Spec. Cond. 00094: µMhos
time ofsampling,
Measuring Point is 2 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling:
4
gallons
Appearance clear
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:10/06/20-10/14/20
Laboratory Name: Envirnment 1, Inc
Certification No.
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.04
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.25
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 109
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 <1.00
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 14
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 0.05
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn -Manganese 01055
ug/L
,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.05-02-2017

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 11/16/20
Facility Name: Town of Woodland
Non -Discharge WQ0004910 UIC
NPDES Other
Permit Name (if different): &e 414— _2TY V %
Facility Address:
TYPE OF PERMITTED OPERATION BEING MONITORED
County Northampton
❑■ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field El Remediation:
Contact Person: Raymond S. Eaton
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: WWTP irrigation fields
No. of wells to be sampled: 5
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW9
Date sample collected: 10/06/20
FIELD ANALYSES:
WAS
Well Depth: 18 ft.
Well Diameter: 2 in.
pH 00400: 6.3 units Temp. 000lo: 20.0 °C
DRY at
Depth to Water Level 82546:7 ft. below measuring
point Screened Interval: 13 ft. to
18
ft. Spec. Cond. 00094: µMhos
time of sampling,
Measuring Point is 2 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling:
4
gallons
Appearance clear
here:❑
Samples for metals were collected unfiltered: ❑■ YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:10/06/20-10/14/20
Laboratory Name: Envirnment 1, Inc
Certification No.
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 rl
/100mL
Nitrate (NO3) as N 00620 0.09
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.08
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 703oo 216
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.08
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 83
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 0.06
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.05-02-2017

��doQo��c��� Flo ��c�oQpoQa�c�d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
TOWN OF WOODLAND
P.O. BOX 297
WOODLAND ,NC 27897
PARAMETERS
BOD, mg/l
Fecal Coliform (MF), /100 Mls
Total Suspended Residue, mg/l
Ammonia Nitrogen as N, mg/l
Total Kjeldahl Nitrogen as N,mg/1
Nitrate -Nitrite as N, mg/l (calc)
Nitrate Nitrogen as N, mg/l
Nitrite Nitrogen as N, mg/l
Total Phosphorus as P, mg/l
Total Phosphorus as P, mg/l
Total Organic Carbon, mg/l
Chloride, mg/l
Total Dissolved Residue, mg/l
Total Nitrogen, mg/l (calc)
Effluent
34
210
82
1.16
10.84
0.43
0.06
0.37
3.69
870
1370
11.27
Drinking Water ID: 37715
Wastewater ID: 10
PHONE (262) %bb-o2UO
FAX [phone]
ID#: 254
DATE COLLECTED: 10/06/20
DATE REPORTED : 11/10/20
REVIEWED BY:
Well #1
Well #3
Well #6
Well #8
Analysis
Method
Date Analyst
Code
10/06/20
KDS
521OB-11
< 1
< 1
< 1
< 1
10/06/20
HJO
9222D-06
10/07/20
HJO
2540D-11
<0.04
0.04
<0.04
0.05
10/07/20
KES
350.1 112-93
10/08/20
KES
351.2 112-93
353.2 112-93
0.28
0.10
0.18
< 0.04
10/07/20
DTL
353.2 112-93
10/06/20
KES
353.2 112-93
10/08/20
TLH
365.4-74
0.06
0.07
0.14
0.25
10/13/20
DTL
365.4-74
< 1.00
1.04
< 1.00
< 1.00
10/14/20
SEJ
531 OC-11
19
39
79
14
10/12/20
JMS
4500CLB-11
97
114
202
109
10/08/20
HJO
2540C-11

EADmIMEOPM % hmpudid
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: TOWN OF WOODLAND
P.O. BOX 297
WOODLAND, NC 27897
REVIEWED BY:
VOLATILE ORGANICS
STD. METHODS 620OC-11
PHONE [phone]
FAX [phone]
CLIENT ID: 254
ANALYST: DTL
DATE COLLECTED: 10/06/20 Page: 1
DATE ANALYZED: 10/09/20
DATE REPORTED: 11/10/20
PARAMETERS, ug/l
Well #6
Well #8
Well #9
1. Benzene
<0.50
<0.50
<0.50
2. Bromobenzene
<0.50
<0.50
<0.50
3. Bromochloromethane
<0.50
<0.50
<0.50
4. Bromodichloromethane
<0.50
<0.50
<0.50
5. Bromoform
<0.50
<0.50
<0.50
6. Bromomethane
<0.50
<0.50
<0.50
7. N-Butylbenzene
<0.50
<0.50
<0.50
8. Sec-Butylbenzene
<0.50
<0.50
<0.50
9. Tert-Butylbenzene
<0.50
<0.50
<0.50
10. Carbon Tetrachloride
<0.50
<0.50
<0.50
11. Chlorobenzene
<0.50
<0.50
<0.50
12. Chloroethane
<0.50
<0.50
<0.50
13. Chloroform
<0.50
<0.50
<0.50
14. Chloromethane
<0.50
<0.50
<0.50
15. 2-Chlorotoluene
<0.50
<0.50
<0.50
16. 4-Chlorotoluene
<0.50
<0.50
<0.50
17. Dibromochloromethane
<0.50
<0.50
<0.50
18. 1,2-Dibromo-3-Chloropropane
<0.50
<0.50
<0.50
19. 1,2-Dibromoethane
<0.50
<0.50
<0.50
20. Dibromomethane
<0.50
<0.50
<0.50
21. 1,2-Dichlorobenzene
<0.50
<0.50
<0.50
22. 1,3-Dichlorobenzene
<0.50
<0.50
<0.50
23. 1,4-Dichlorobenzene
<0.50
<0.50
<0.50
24. Dichlorodifluoromethane
<0.50
<0.50
<0.50
25. 1,1-Dichloroethane
<0.50
<0.50
<0.50
26, 1,2-Dichloroethane
<0.50
<0.50
<0.50
27. 1,1-Dichloroethene
<0.50
<0.50
<0.50
28. Cis-1,2-Dichloroethene
<0.50
<0.50
<0.50
29. trans-1,2-Dichloroethene
<0.50
<0.50
<0.50
30. 1,2-Dichloropropane
<0.50
<0.50
<0.50
31. 1,3-Dichloropropane
<0.50
<0.50
<0.50
32. 2,2-Dichloropropane
< 0.50
< 0.50
< 0.50
33. 1,1-Dichloropropene
<0.50
<0.50
<0.50
34. Cis-1,3-Dichloropropene
<0.50
<0.50
<0.50
35. trans- 1,3-Dichloropropen e
<0.50
<0.50
<0.50
36. Ethylbenzene
<0.50
<0.50
<0.50
37. Hexachlorobutadiene
<0.50
<0.50
<0.50
38. Isopropylbenzene
<0.50
<0.50
<0.50
39. 4-Isopropyltoluene
<0.50
<0.50
<0.50
40. Methylene Chloride
<0.50
<0.50
<0.50
41. Naphthalene
<0.50
<0.50
<0.50
42. Propylbenzene
<0.50
<0.50
<0.50
43. Styrene
<0.50
<0.50
<0.50
44. 1,1,1,2-Tetrachloroethane
<0.50
<0.50
<0.50
45. 1,1,2,2-Tetrachloroethane
<0.50
<0.50
<0.50
46. Tetrachloroethene
< 0.50
< 0.50
<0.50
47. Toluene
< 0.50
< 0.50
< 0.50
48. 1,2,3-Trichlorobenzene
<0.50
<0.50
<0.50

ElMonamM Flo hcupumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: TOWN OF WOODLAND
P.O. BOX 297
WOODLAND, NC 27897
REVIEWED BY:
VOLATILE ORGANICS
STD. METHODS 620OC-11
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT ID: 254
ANALYST: DTL
DATE COLLECTED: 10/06/20 Page: 2
DATE ANALYZED: 10/09/20
DATE REPORTED: 11/10/20
PARAMETERS, ug/l
Well #6
Well #8
Well #9
49. 1,2,4-Trichlorobenzene
<0.50
<0.50
<0.50
50. 1,1,1-Trichloroethane
<0.50
<0.50
<0.50
51. 1,1,2-Trichloroethane
<0.50
<0.50
<0.50
52. Trichloroethene
<0.50
<0.50
<0.50
53. Trichlorofluoromethane
<0.50
<0.50
<0.50
54. 1,2,3-Trichloropropane
<0.50
<0.50
<0.50
55. 1,2,4-Trimethylbenzene
<0.50
<0.50
<0.50
56. 1,3,5-Trimethylbenzene
<0.50
<0.50
<0.50
57. Vinvl Chloride
<0.50
<0.50
<0.50
58. Total Xylenes
< 1.00
< 1.00
< 1.00
59. Methyl Tert Butyl Ether
< 1.00
< 1.00
< 1.00

Enw,umn(PRI Flo hmpumbd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: TOWN OF WOODLAND
P.O. BOX 297
WOODLAND, NC 27897
REVIEWED BY:
VOLATILE ORGANICS
RTD. METHODS 620OC-11
PHONE [phone]
FAX [phone]
CLIENT ID: 254
ANALYST: DTL
DATE COLLECTED: 10/26/20 Page: 1
DATE ANALYZED: 10/29/20
DATE REPORTED: 11/03/20
PARAMETERS, ug/l
Well #1
Well #3
1. Benzene
<0.50
<0.50
2. Bromobenzene
<0.50
<0.50
3. Bromochloromethane
<0.50
<0.50
4. Bromodichloromethane
<0.50
<0.50
5. Bromoform
<0.50
<0.50
6. Bromomethane
<0.50
<0.50
7. N-Butvlbenzene
<0.50
<0.50
8. Sec-Butylbenzene
< 0.50
< 0.50
9. Tert-Butvlbenzene
<0.50
<0.50
10. Carbon Tetrachloride
<0.50
<0.50
11. Chlorobenzene
< 0.50
< 0.50
12. Chloroethane
<0.50
<0.50
13. Chloroform
< 0.50
< 0.50
14. Chloromethane
<0.50
<0.50
15. 2-Chlorotoluene
<0.50
<0.50
16. 4-Chlorotoluene
<0.50
<0.50
17. Dibromochloromethane
<0.50
<0.50
18. 1,2-Dibromo-3-Chloropropane
<0.50
<0.50
19. 1,2-Dibromoethane
< 0.50
< 0.50
20. Dibromomethane
<0.50
<0.50
21. 1,2-Dichlorobenzene
<0.50
<0.50
22. 1,3-Dichlorobenzene
<0.50
<0.50
23. 1,4-Dichlorobenzene
<0.50
<0.50
24. Dichlorodifluoromethane
<0.50
<0.50
25. 1,1-Dichloroethane
<0.50
<0.50
26. 1,2-Dichloroethane
<0.50
<0.50
27. 1,1-Dichloroethene
<0.50
<0.50
28. Cis-1,2-Dichloroethene
<0.50
<0.50
29. trans- 1,2-Dichloroethene
<0.50
<0.50
30. 1,2-Dichloropropane
<0.50
<0.50
31. 1,3-Dichloropropane
<0.50
<0.50
32. 2,2-Dichloropropane
<0.50
<0.50
33. 1,1-Dichloropropene
< 0.50
< 0.50
34. Cis-1,3-Dichloropropene
<0.50
<0.50
35. trans -1,3-Dichloropro pene
<0.50
<0.50
36. Ethylbenzene
<0.50
<0.50
37. Hexachlorobutadiene
< 0.50
< 0.50
38. Isopropylbenzene
<0.50
<0.50
39. 4-Isopropyltoluene
<0.50
<0.50
40. Methylene Chloride
<0.50
<0.50
41. Naphthalene
<0.50
<0.50
42. Propylbenzene
<0.50
<0.50
43. Styrene
<0.50
<0.50
44. 1,1,1,2-Tetrachloroethane
<0.50
<0.50
45. 1,1,2,2-Tetrachloroethane
<0.50
<0.50
46. Tetrachloroethene
<0.50
<0.50
47. Toluene
<0.50
<0.50
48. 1,2,3-Trichlorobenzene
<0.50
<0.50

Bmwohnum Flo hmpumUd
114 OAKIviurV I uFiiVc
GREENVILLE, N.C. 27858
CLIENT: TOWN OF WOODLAND
P.O. BOX 297
WOODLAND, NC 27897
REVIEWED BY:
VOLATILE ORGANICS
STD. METHODS 620OC-11
Drinking Water ID: 37715
Wastewater ID: 10
iiUNL (2bL) io6-0206
FAX [phone]
CLIENT ID: 254
ANALYST: DTL
DATE COLLECTED: 10/26/20 Page: 2
DATE ANALYZED: 10/29/20
DATE REPORTED: 11/03/20
PARAMETERS, ug/l
Well #1
Well #3
49. 1,2,4-Trichlorobenzene
<0.50
<0.50
50. 1,1,1-Trichloroethane
<0.50
<0.50
51. 1,1,2-Trichloroethane
<0.50
<0.50
52. Trichloroethene
< 0.50
< 0.50
53. Trichlorofluoromethane
< 0.50
< 0.50
54. 1,2,3-Trichloropropane
<0.50
<0.50
55. 1,2,4-Trimethyylbenzene
< 0.50
< 0.50
56. 1,3,5-Trimethylbenzene
<0.50
<0.50
57. Vinyl Chloride
<0.50
<0.50
58. Total Xvlenes
< 1.00
< 1.00
59. Methyl Tert Butyl Ether
< 1.00
< 1.00

ENW'r@flH(M Flo hmpudid
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
TOWN OF WOODLAND
P.O. BOX 297
WOODLAND ,NC 27897
Well #9
Analysis
Method
PARAMETERS
Date
Analyst
Code
Fecal Coliform (MF), /100 Mls
< 1
10/06/20
HJO
9222D-06
Ammonia Nitrogen as N, mg/l
0.06
10/07/20
KES
350.1 R2-93
Nitrate Nitrogen as N, mg/l
0.09
10/07/20
DTL
353.2 R2-93
Total Phosphorus as P, mg/l
0.08
10/13/20
DTL
365.4-74
Total Organic Carbon, mg/l
1.08
10/14/20
SEJ
531OC-11
Chloride, mg/l
83
10/12/20
JMS
4500CLB-11
Total Dissolved Residue, mg/l
216
10/08/20
HJO
2540C-11
Drinking Water ID: 37715
Wastewater ID: 10
PHUNE [phone]
FAX [phone]
ID#: 254
DATE COLLECTED: 10/06/20
DATE REPORTED : 11/10/20
REVIEWED BY: ;y

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Environment 1, Inc.
P.O. Box 7085, 114 Oakmont Dr.
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CHAI OF CUSTODY RECORD
Page I of 2
environment l inc .com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] •Fax [phone]
CHLORINE
CLIENT: 254 Week: 46
❑ UV
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CHEMICAL PRESERVATION
OODLAND NC 27897
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CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
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SAMPLES COLLECTED BY:
(Please Print)
SAMPLES RECEIVED IN LAB AT —1j, °C
R"QUISH BY (S .) AM LER)
DATE/TIME
RECE D B (SIG.)
l� DATElT1ME
COMMENTS:
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RELIN UISHED BY (SIG.)
DATErnME
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DATEIrIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FORM #5 Grab sample in the blocks above for each parameter requested. NQ
w 385516

SAMPLING INSTRUCTIONS AND FORM COMPLETION
FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE
TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE
SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING
REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE.
1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation
and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any
samples analyzed outside of the required guidelines will be "qualified" This means that a note will be included on the sample result and
"Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations.
2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not
permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the
temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is
a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much
ice as will fit in the cooler.
3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The
laboratory will either provide the preservative in the sample bottle, or in the case of 40 ml. Volatiles Vials, provide a bottle of Acid with
detailed instructions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the
bottle is required for proper chemical preservation. Unless specific instructions are provided for a test or bottle (example: cyanide or
volatile organics), fill sample bottles to the bottom of the bottle threads. This will leave a small air space for shaking the sample to mix with
any preservative and again prior to analysis. The lab must verify proper chemical preservation upon arrival in the lab and will note this
information in the spaces provided on the front of this form.
4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will
provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen
and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the
dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles.
Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for
Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total
Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the
"Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have
Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that
you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any
neutralization is performed.
S) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as
well as Composite start dates and times can be recorded in the "comments" section.
6) Other information required to be completed by the client are:
Collection Date and Collection Time for each sample location Temperature at Time of Collection
Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished
Other added sample locations and analyses required Type Of Disinfection
Deletion on the form for any samples which are not needed (example: dry upstream location)
Any other information felt to be pertinent should be included in the "Comments" section
CONSIDERATIONS:
Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be
collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis.
BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the
right to establish required sample collection and delivery dates in order to meet the required holding times.
CAUTION
Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals
for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping
container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek
medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection.

Ti
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Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr. Page 2 of 2
C7 PPn,,d1P NJC 77RSR
environment 1 inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] •Fax [phone]
CHLORINE
pH CHECK (LAB)
CLIENT: 254 Week: 46
Ij UV
G
G
CONTAINER TYPE, P/G
DWN OF WOODLAND
NONE
Ij
O. BOX 297
CHEMICALPRESERVAT10N
OODLAND NC 27897
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CHAIN OF CUSTODY (SEAL) MAINTAINED
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SAMPLES COLLECTED BY:
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SAMPLES RECEIVED IN LAB AT q 1C
R INQUIS D Y(SI (S PLER)
DATETIME
RECEI ED (SIG.) 1
DATEMME
COMMENTS:
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RELIN UISHED BY (SIG.)
DATEMME
RECEIVED BY (SI :)
DATE/TIME
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED BY (SIG.)
DATEMME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for
FORM #5 Grab sample in the blocks above for each parameter requested. N A 385515

SAMPLING INSTRUCTIONS AND FORM COMPLETION
FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE
TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE
SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING
REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE.
1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation
and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any
samples analyzed outside of the required guidelines will be "qualified" This means that a note will be included on the sample result and
"Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations.
2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not
permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the
temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is
a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much
ice as will fit in the cooler.
3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The
laboratory will either provide the preservative in the sample bottle, or in the case of 40 ml. Volatiles Vials, provide a bottle of Acid with
detailed instructions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the
bottle is required for proper chemical preservation. Unless specific instructions are provided for a test or bottle (example: cyanide or
volatile organics), fill sample bottles to the bottom of the bottle threads. This will leave a small air space for shaking the sample to mix with
any preservative and again prior to analysis. The lab must verify proper chemical preservation upon arrival in the lab and will note this
information in the spaces provided on the front of this form.
4) Chlorine Neutralization. Some samples require that any Total Chlorine Residual be removed at the time of collection. The lab will
provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen
and Ammonia Nitrogen) where this is not possible due to interferences between the required chemical preservation (Acid) and the
dechlorinating agent. Therefore, these samples must be de -chlorinated at the time of collection before being placed in our sample bottles.
Sodium Thiosulfate is the chemical of choice to neutralize chlorine. It must be added to your sample and then the sample checked for
Total Chlorine before the sample is poured in our bottle. Facilities using chlorine for disinfection should have a means of measuring Total
Chlorine. Non -chlorinated sample sources will not need to be checked. The person neutralizing the chlorine must put his initials in the
"Chlorine Neutralized at Collection" row on the front of this form above the proper parameter. Samples such as Coliforms (which have
Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that
you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any
neutralization is performed.
5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as
well as Composite start dates and times can be recorded in the "comments" section.
6) Other information required to be completed by the client are:
Collection Date and Collection Time for each sample location Temperature at Time of Collection
Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished
Other added sample locations and analyses required Type Of Disinfection
Deletion on the form for any samples which are not needed (example: dry upstream location)
Any other information felt to be pertinent should be included in the "Comments" section
CONSIDERATIONS:
Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be
collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis.
BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the
right to establish required sample collection and delivery dates in order to meet the required holding times.
CAUTION
Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals
for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping
container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek
medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection.

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr. Page 1 of 1
Greenville, NC 27858
environment 1 inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone [phone] • Fax [phone]
CHLORINE
CLIENT: 254 Week: 46
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NOODLAND NC 27897
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CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
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SAMPLES COLLECTED BY:
(Please Pri
SAMPLES RECEIVED IN LAB AT °C
REIN QUISHEJ� B (SIG.) SAMPLER)
DATEITIME /
REC�Y (SIG.
DATEMME
COMMENTS:
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PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for
FORM #5 Grab sample in the blocks above for each parameter requested. N _ 384119

SAMPLING INSTRUCTIONS AND FORM COMPLETION
FAILURE TO PROPERLY CHILL, CHEMICALLY PRESERVE, COLLECT IN PROPER BOTTLE
TYPES, MEET REQUIRED HOLDING TIMES, NEUTRALIZE CHLORINE IN CHLORINE
SENSITIVE SAMPLES, AND SEAL COOLERS WITH TAPE WILL RESULT IN SAMPLES BEING
REJECTED BY THIS LABORATORY AS PER NORTH CAROLINA REGULATORY CODE.
1) Samples not falling within the required guidelines will need to be re -collected. The client will be contacted and informed of any deviation
and asked to collect another set of samples. The client may request the laboratory to proceed with the analyses of the current samples. Any
samples analyzed outside of the required guidelines will be "qualified" This means that a note will be included on the sample result and
"Chain of Custody" specifying the deviation. The laboratory is also required to send a letter to the State noting the deviations.
2) Sample Temperature. Samples for compliance monitoring must be chilled with wet ice to a temperature of 6C or less. Freezing is not
permitted. Samples delivered to the lab shortly after collection may not have had enough time to be chilled below 6C. In this case the
temperature at time of collection must be noted in the space provided. The samples will meet the requirements of the regulation if there is
a temperature drop from the time of collection until received in the lab. Regardless, all samples should be packed in wet ice using as much
ice as will fit in the cooler.
3) Sample Chemical Preservation. Many samples require a chemical preservation such as Sulfuric Acid or Sodium Hydroxide. The
laboratory will either provide the preservative in the sample bottle, or in the case of 40 ml. Volatiles Vials, provide a bottle of Acid with
detailed instructions on how to collect the sample. Never rinse sample bottles before collecting samples. Any residue or liquid in the
bottle is required for proper chemical preservation. Unless specific instructions are provided for a test or bottle (example: cyanide or
volatile organics), fill sample bottlestbFpf.the. bottle threads. This will leave a small air space for shaking the sample to mix with
any preservative and again prior to analysis. 'the lab must verify proper chemical preservation upon arrival in the lab and will note this
information in the spaces providc4,on the fronto€this (Qrm„
4) Chlorine Neutralization. Some samp*s+r tdre that and Total Chlorine Residual be removed at the time of collection. The lab will
provide the proper neutralizing agent in the sample bottle when technically possible. There are some samples (Total Kjeldahl Nitrogen
and Ammonia Nitrogen) where FM is ndt possible due 1b interferences between the required chemical preservation (Acid) and the
dechlorinating agent. Therefore, these sampl mpst be de-c lorinated at the time of collection before being placed in our sample bottles.
Sodium Thiosulfate is the chemical of choictto n(utralize'Klorine. It must be added to your sample and then the sample checked for
Total Chlorine before the sample is pound in our bottle. Fa 'lities using chlorine for disinfection should have a means of measuring Total
Chlorine. Non -chlorinated sample sources will not need toe checked. The person neutralizing the chlorine must put his initials in the
"Chlorine Neutralized at Collection" row orphe front oftlls form above the proper parameter. Samples such as Coliforms (which have
Thiosulfate in the bottles shipped from the lab) will be checked for proper neutralization upon arrival in the lab. It is also required that
you note the "Total Chlorine at Collection" on the front of this form for any sample locations applicable. This value would be before any
neutralization is performed.
5) A "C" for Composite Sample or a "G" for Grab Sample should be placed in the box for all requested parameters. Grab temperatures as
well as Composite start dates and times can be recorded in the "comments" section.
6) Other information required to be completed by the client are:
Collection Date and Collection Time for each sample location Temperature at Time of Collection
Printed name of person or persons collecting samples Signature, Date, and Time samples are relinquished
Other added sample locations and analyses required Type Of Disinfection
Deletion on the form for any samples which are not needed (example: dry upstream location)
Any other information felt to be pertinent should be included in the "Comments" section
CONSIDERATIONS:
Coliform and Enterococci samples have a holding time of 6 hours from time of collection to time of analysis. Therefore, samples should be
collected as late in the day as possible to allow enough time for transportation, checking in at the lab and analysis.
BOD, Nitrate, Ortho Phosphorus, Settleable Matter, Turbidity, Color, and MBAS samples have a 48 hour holding time. The lab reserves the
right to establish required sample collection and delivery dates in order to meet the required holding times.
CAUTION
Sample bottles may contain acids or other corrosive and potentially harmful chemicals. Laboratories are required to add these chemicals
for certain analyses in order to comply with EPA preservation requirements. Use extreme care when opening and handling the shipping
container and bottles. If any chemical should get into your eyes, on your skin or on your clothes, flush liberally with water and seek
medical attention. Material Safety Data Sheets (MSDS) are available upon request which specify proper handling and personal protection.