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Home My WebLink AboutWQ0002431_GW GROUNDWATER FIELD/LAB FORM North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWATER SECTION Location code: 1P14HuffmanMW2 County: Caldwell Lab Number_________________________________ Quad No_____________ Serial No.________________ Date Received_____________ Time:______________ Lat._________________ Long.___________________ Rec’d By: From:Bus, Courier, Hand Del., Other:______________________________________ Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By:________________ Ck:____________ WSRO, Kinston FO, Fed. Trust, Central Off., Other:______________________ Date Reported:_______________________________ Shipped by: Bus, Courier, Hand Del., Other:____________________________ Purpose: Collector(s): Brett Laverty Date: 11/1/2010 Time: 10:24 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Huffman Finishing pH 400____________________ Spec. Cond.94_____________at 25ºC Location or Site: 4919 Hickory Blvd. Granite Falls, NC Temp.10_________________ºC Odor____________________________ Description of sampling point: Well Head Appearance______________DO, mg/L ________ ORP, mV _________ Sampling Method: Bailer Sample Interval_________________ Field Analysis By:____________________________________________ Remarks______________________________________________________________________________ LABORATORY ANALYSES BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 ug/L Organochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L Al-Aluminum 46557 ug/L Organophosphorus Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As-Arsenic 46551 ug/L Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cond. 95 µMhos/cm Cd-Cadmium 46559 ug/L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 ug/L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 ug/L Boron DOC Fe-Iron 46563 ug/L X Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 ug/L TPH-Diesel Range pH 403 units K-Potassium 46555 mg/L Alkalinity to pH 4.5 410 mg/L Mg-Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L PO4 as P Mn-Manganese 46565 ug/L X Volatile Organics (VOA bottle) Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel ug/L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 ug/L Chloride 940 mg/L P: Total as P 665 mg/L Se-Selenium ug/L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 ug/L Color: True 80 CU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (ºC): Cyanide 720 mg/L NH4 - ammonium Silica Lab Comments_____________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ GW-54 REV. 7/03 For Dissolved Analysis-submit filtered sample and write “DIS” in block. SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) Other Routine Soil Emergency Chain of Custody (circle one) (Pumping time, air temp., etc.) X X X X X X X X X X X X X X X X X X X X X X X X GROUNDWATER FIELD/LAB FORM North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWATER SECTION Location code: 1P14HuffmanMW3 County: Caldwell Lab Number_________________________________ Quad No_____________ Serial No.________________ Date Received_____________ Time:______________ Lat._________________ Long.___________________ Rec’d By: From:Bus, Courier, Hand Del., Other:______________________________________ Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By:________________ Ck:____________ WSRO, Kinston FO, Fed. Trust, Central Off., Other:______________________ Date Reported:_______________________________ Shipped by: Bus, Courier, Hand Del., Other:____________________________ Purpose: Collector(s): Brett Laverty Date: 11/1/2010 Time: 10:50 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Huffman Finishing pH 400____________________ Spec. Cond.94_____________at 25ºC Location or Site: 4919 Hickory Blvd. Granite Falls, NC Temp.10_________________ºC Odor____________________________ Description of sampling point: Well Head Appearance______________DO, mg/L ________ ORP, mV _________ Sampling Method: Bailer Sample Interval_________________ Field Analysis By:____________________________________________ Remarks______________________________________________________________________________ LABORATORY ANALYSES BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 ug/L Organochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L Al-Aluminum 46557 ug/L Organophosphorus Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As-Arsenic 46551 ug/L Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cond. 95 µMhos/cm Cd-Cadmium 46559 ug/L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 ug/L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 ug/L Boron DOC Fe-Iron 46563 ug/L X Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 ug/L TPH-Diesel Range pH 403 units K-Potassium 46555 mg/L Alkalinity to pH 4.5 410 mg/L Mg-Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L PO4 as P Mn-Manganese 46565 ug/L X Volatile Organics (VOA bottle) Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel ug/L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 ug/L Chloride 940 mg/L P: Total as P 665 mg/L Se-Selenium ug/L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 ug/L Color: True 80 CU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (ºC): Cyanide 720 mg/L NH4 - ammonium Silica Lab Comments_____________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ GW-54 REV. 7/03 For Dissolved Analysis-submit filtered sample and write “DIS” in block. SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) Other Routine Soil Emergency Chain of Custody (circle one) (Pumping time, air temp., etc.) X X X X X X X X X X X X X X X X X X X X X X X X GROUNDWATER FIELD/LAB FORM North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWATER SECTION Location code: 1P14HuffmanMW2 County: Caldwell Lab Number_________________________________ Quad No_____________ Serial No.________________ Date Received_____________ Time:______________ Lat._________________ Long.___________________ Rec’d By: From:Bus, Courier, Hand Del., Other:______________________________________ Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By:________________ Ck:____________ WSRO, Kinston FO, Fed. Trust, Central Off., Other:______________________ Date Reported:_______________________________ Shipped by: Bus, Courier, Hand Del., Other:____________________________ Purpose: Collector(s): Brett Laverty Date: 11/1/2010 Time: 10:24 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Huffman Finishing pH 400____________________ Spec. Cond.94_____________at 25ºC Location or Site: 4919 Hickory Blvd. Granite Falls, NC Temp.10_________________ºC Odor____________________________ Description of sampling point: Well Head Appearance______________DO, mg/L ________ ORP, mV _________ Sampling Method: Bailer Sample Interval_________________ Field Analysis By:____________________________________________ Remarks______________________________________________________________________________ LABORATORY ANALYSES BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 ug/L Organochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L Al-Aluminum 46557 ug/L Organophosphorus Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As-Arsenic 46551 ug/L Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cond. 95 µMhos/cm Cd-Cadmium 46559 ug/L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 ug/L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 ug/L Boron DOC Fe-Iron 46563 ug/L Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 ug/L TPH-Diesel Range pH 403 units K-Potassium 46555 mg/L Alkalinity to pH 4.5 410 mg/L Mg-Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L PO4 as P Mn-Manganese 46565 ug/L Volatile Organics (VOA bottle) Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel ug/L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 ug/L Chloride 940 mg/L P: Total as P 665 mg/L Se-Selenium ug/L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 ug/L Color: True 80 CU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (ºC): Cyanide 720 mg/L NH4 - ammonium Silica Lab Comments_____________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ GW-54 REV. 7/03 For Dissolved Analysis-submit filtered sample and write “DIS” in block. SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) Other Routine Soil Emergency Chain of Custody (circle one) (Pumping time, air temp., etc.) X X X X GROUNDWATER FIELD/LAB FORM North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWATER SECTION Location code: 1P14HuffmanMW3 County: Caldwell Lab Number_________________________________ Quad No_____________ Serial No.________________ Date Received_____________ Time:______________ Lat._________________ Long.___________________ Rec’d By: From:Bus, Courier, Hand Del., Other:______________________________________ Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By:________________ Ck:____________ WSRO, Kinston FO, Fed. Trust, Central Off., Other:______________________ Date Reported:_______________________________ Shipped by: Bus, Courier, Hand Del., Other:____________________________ Purpose: Collector(s): Brett Laverty Date: 11/1/2010 Time: 10:50 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Huffman Finishing pH 400____________________ Spec. Cond.94_____________at 25ºC Location or Site: 4919 Hickory Blvd. Granite Falls, NC Temp.10_________________ºC Odor____________________________ Description of sampling point: Well Head Appearance______________DO, mg/L ________ ORP, mV _________ Sampling Method: Bailer Sample Interval_________________ Field Analysis By:____________________________________________ Remarks______________________________________________________________________________ LABORATORY ANALYSES BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 ug/L Organochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L Al-Aluminum 46557 ug/L Organophosphorus Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As-Arsenic 46551 ug/L Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cond. 95 µMhos/cm Cd-Cadmium 46559 ug/L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 ug/L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 ug/L Boron DOC Fe-Iron 46563 ug/L Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 ug/L TPH-Diesel Range pH 403 units K-Potassium 46555 mg/L Alkalinity to pH 4.5 410 mg/L Mg-Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L PO4 as P Mn-Manganese 46565 ug/L Volatile Organics (VOA bottle) Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel ug/L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 ug/L Chloride 940 mg/L P: Total as P 665 mg/L Se-Selenium ug/L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 ug/L Color: True 80 CU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (ºC): Cyanide 720 mg/L NH4 - ammonium Silica Lab Comments_____________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ GW-54 REV. 7/03 For Dissolved Analysis-submit filtered sample and write “DIS” in block. SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) Other Routine Soil Emergency Chain of Custody (circle one) (Pumping time, air temp., etc.) X X X X PO Number #10G0801 Loc. Descr.:VOA TRIP BLANK Loc. Type:TRIP BLANK Collector:B LAVERTY Collect Date:11/01/2010 Collect Time:08:07 Date Received:11/03/2010 Time Received:08:10 Location ID:AROAPNLC County: Region:ARO Labworks LoginID SMATHIS Sample Matrix:GROUNDWATER Date Reported: NC DWQ Laboratory Section Results VisitID Sample Depth AROAPReport To River Basin 12/28/2011 Emergency Yes/No COC Yes/No Sample ID:AB65229 11/16/10Report Generated: CAS #Result/ QualifierPQLAnalyte Name Validated byAnalysis Date Method ReferenceUnits LAB SMATHIS°C2.1Sample temperature at receipt by lab 11/3/10 VOL EPA5030/624/8260 ACHANDLERug/L_TITLE_Volatile Organics in liquid 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Dichlorodifluoromethane75-71-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Chloromethane74-87-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Vinyl Chloride75-01-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Bromomethane74-83-9 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Chloroethane75-00-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Trichlorofluoromethane75-69-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloroethene75-35-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected10Methylene Chloride75-09-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25trans-1,2-Dichloroethene156-60-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Methyl Tert-Butyl Ether1634-04-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloroethane75-34-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25cis-1,2-Dichloroethene156-59-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromochloromethane74-97-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Chloroform67-66-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.252,2-Dichloropropane594-20-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2-Dichloroethane107-06-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,1-Trichloroethane71-55-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloropropene563-58-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Carbon Tetrachloride56-23-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Benzene71-43-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Dibromomethane74-95-3 11/3/10 EPA5030/624/8260 ACHANDLERug/L0.280.251,2-Dichloropropane78-87-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Trichloroethene79-01-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromodichloromethane75-27-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25cis-1,3-Dichloropropene10061-01-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25trans-1,3-Dichloropropene10061-02-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,2-Trichloroethane79-00-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Toluene108-88-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,3-Dichloropropane142-28-9 11/3/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 1 of 2 08:07Collect Time::11/01/2010Collect Date:AB65229Sample ID:AROAPNLCLocation ID: NC DWQ Laboratory Section Results VOL Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA5030/624/8260 ACHANDLERug/LNot detected0.25Dibromochloromethane124-48-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25(EDB)1,2-Dibromoethane106-93-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Tetrachloroethene127-18-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Chlorobenzene108-90-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Ethylbenzene100-41-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Bromoform75-25-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50m,p-Xylene108-38-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Styrene100-42-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,2,2-Tetrachloroethane79-34-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,1,2-Tetrachloroethane630-20-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25o-Xylene95-47-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2,3-Trichloropropane96-18-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Isopropylbenzene98-82-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromobenzene108-86-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25n-Propylbenzene103-65-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.252-Chlorotoluene95-49-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.254-Chlorotoluene106-43-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,3,5-Trimethylbenzene108-67-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25tert-Butylbenzene98-06-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2,4-Trimethylbenzene95-63-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25sec-Butylbenzene135-98-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25m-Dichlorobenzene (1,3)541-73-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25p-Dichlorobenzene (1,4)106-46-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25o-Dichlorobenzene (1,2)95-50-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25p-Isopropyltoluene99-87-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25n-Butylbenzene104-51-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected2.01,2-Dibromo-3-Chloropropane96-12-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.501,2,4-Trichlorobenzene120-82-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Naphthalene91-20-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Hexachlorobutadiene87-68-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.01,2,3-Trichlorobenzene87-61-6 11/3/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 2 of 2 PO Number #10G0802 Loc. Descr.:HUFFMAN FINISHING Loc. Type:MONITORING WELL Collector:B LAVERTY Collect Date:11/01/2010 Collect Time:10:24 Date Received:11/03/2010 Time Received:08:10 Location ID:1P14HUFFMANMW2 County:CALDWELL Region:ARO Labworks LoginID SMATHIS Sample Matrix:GROUNDWATER Date Reported: NC DWQ Laboratory Section Results VisitID Sample Depth AROAPReport To River Basin 12/28/2011 Emergency Yes/No COC Yes/No Sample ID:AB65230 1/5/11Report Generated: CAS #Result/ QualifierPQLAnalyte Name Validated byAnalysis Date Method ReferenceUnits LAB SMATHIS°C2.1Sample temperature at receipt by lab 11/3/10 WET Hach 8000 CGREENmg/LU2020Chemical Oxygen Demand in liquid 11/22/10 EPA 300.0 CGREENmg/L_TITLE_Ion Chromatography 11/9/10 EPA 300.0 CGREENmg/L1.51.0Chloride 11/9/10 EPA 300.0 CGREENmg/LU0.40.4Fluoride 11/9/10 EPA 300.0 CGREENmg/LU2.02.0Sulfate 11/9/10 NUT Lac10-107-06-1-J CGREENmg/L as NU0.020.02NH3 as N in liquid 11/3/10 Lac10-107-04-1-c CGREENmg/L as N1.00.02NO2+NO3 as N in liquid 11/3/10 Lac10-115-01-1EF CGREENmg/L as P0.120.02Phosphorus_total as P in liquid 11/4/10 Lachat107-04-1-c CGREENmg/L as N0.990.02Nitrate as N in liquid 11/5/10 Lachat107-04-1-c CGREENmg/L as N0.010.01Nitrite as N in liquid 11/3/10 MET EPA 200.7 ESTAFFORD1ug/L360050Al by ICP7429-90-5 11/10/10 EPA 200.8 ESTAFFORD1ug/LU2.02.0As by ICPMS7440-38-2 11/9/10 EPA 200.7 ESTAFFORD1ug/L4710Ba by ICP7440-38-3 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1.01.0Cd by ICPMS7440-43-9 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1010Cr by ICPMS7440-47-3 11/9/10 EPA 200.8 ESTAFFORD1ug/L3.52.0Cu by ICPMS7440-50-8 11/9/10 EPA 200.7 ESTAFFORD1ug/L300050Fe by ICP7439-89-6 11/10/10 EPA 245.1 ESTAFFORD1ug/LU0.200.2Hg 245.17439-97-6 11/9/10 EPA 200.7 ESTAFFORD1mg/L1.50.10Mg by ICP7439-95-4 11/9/10 EPA 200.7 ESTAFFORD1ug/L14010Mn by ICP7439-96-5 11/10/10 EPA 200.7 ESTAFFORD1mg/L1.60.10Na by ICP7440-23-5 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1010Ni by ICPMS7440-02-0 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1010Pb by ICPMS7439-92-1 11/9/10 EPA 200.8 ESTAFFORD1ug/LU5.05.0Se by ICPMS7782-49-2 11/9/10 EPA 200.8 ESTAFFORD1ug/L1710Zn by ICPMS7440-66-6 11/9/10 VOL EPA5030/624/8260 ACHANDLERug/L_TITLE_Volatile Organics in liquid 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Dichlorodifluoromethane75-71-8 11/3/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 1 of 5 10:24Collect Time::11/01/2010Collect Date:AB65230Sample ID:1P14HUFFMANMW2Location ID: NC DWQ Laboratory Section Results VOL Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA5030/624/8260 ACHANDLERug/LNot detected0.50Chloromethane74-87-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Vinyl Chloride75-01-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Bromomethane74-83-9 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Chloroethane75-00-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Trichlorofluoromethane75-69-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloroethene75-35-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected10Methylene Chloride75-09-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25trans-1,2-Dichloroethene156-60-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Methyl Tert-Butyl Ether1634-04-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloroethane75-34-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25cis-1,2-Dichloroethene156-59-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromochloromethane74-97-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Chloroform67-66-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.252,2-Dichloropropane594-20-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2-Dichloroethane107-06-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,1-Trichloroethane71-55-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloropropene563-58-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Carbon Tetrachloride56-23-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Benzene71-43-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Dibromomethane74-95-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2-Dichloropropane78-87-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Trichloroethene79-01-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromodichloromethane75-27-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25cis-1,3-Dichloropropene10061-01-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25trans-1,3-Dichloropropene10061-02-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,2-Trichloroethane79-00-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Toluene108-88-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,3-Dichloropropane142-28-9 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Dibromochloromethane124-48-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25(EDB)1,2-Dibromoethane106-93-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Tetrachloroethene127-18-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Chlorobenzene108-90-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Ethylbenzene100-41-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Bromoform75-25-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50m,p-Xylene108-38-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Styrene100-42-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,2,2-Tetrachloroethane79-34-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,1,2-Tetrachloroethane630-20-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25o-Xylene95-47-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2,3-Trichloropropane96-18-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Isopropylbenzene98-82-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromobenzene108-86-1 11/3/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 2 of 5 10:24Collect Time::11/01/2010Collect Date:AB65230Sample ID:1P14HUFFMANMW2Location ID: NC DWQ Laboratory Section Results VOL Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA5030/624/8260 ACHANDLERug/LNot detected0.25n-Propylbenzene103-65-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.252-Chlorotoluene95-49-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.254-Chlorotoluene106-43-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,3,5-Trimethylbenzene108-67-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25tert-Butylbenzene98-06-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2,4-Trimethylbenzene95-63-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25sec-Butylbenzene135-98-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25m-Dichlorobenzene (1,3)541-73-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25p-Dichlorobenzene (1,4)106-46-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25o-Dichlorobenzene (1,2)95-50-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25p-Isopropyltoluene99-87-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25n-Butylbenzene104-51-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected2.01,2-Dibromo-3-Chloropropane96-12-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.501,2,4-Trichlorobenzene120-82-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Naphthalene91-20-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Hexachlorobutadiene87-68-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.01,2,3-Trichlorobenzene87-61-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detectedVOC'S BY GC/MS 11/3/10 SEM EPA625/8270/3510 NGOODug/L_TITLE_Semivolatile Organics (BNAs) in liquid7440-50-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Aniline62-53-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Phenol108-95-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-chloroethyl)ether111-44-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chlorophenol, 2-95-57-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorobenzene, 1,3541-73-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorobenzene, 1,4-106-46-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected20Benzyl alcohol100-51-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorobenzene, 1,2-95-50-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Methylphenol, 2-95-48-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-chloroisopropyl)ether39638-32-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Methylphenol, 4-106-44-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10N-nitrosodi-n-propylamine621-64-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Hexachloroethane67-72-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Nitrobenzene98-95-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Isophorone78-59-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Nitrophenol, 2-88-75-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Dimethylphenol, 2,4-105-67-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Benzoic acid65-85-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-chloroethoxy)methane111-91-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorophenol, 2,4-120-83-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Trichlorobenzene, 1,2,4-120-82-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Naphthalene(SV)91-20-3 11/9/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 3 of 5 10:24Collect Time::11/01/2010Collect Date:AB65230Sample ID:1P14HUFFMANMW2Location ID: NC DWQ Laboratory Section Results SEM Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA625/8270/3510 NGOODug/LNot detected20Chloroaniline, 4-106-47-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Hexachlorobutadiene(SV)87-68-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected20Chloro-3-methyl phenol, 4-59-50-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Methylnaphthalene, 2-91-57-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Hexachlorocyclopentadiene77-47-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Trichlorophenol, 2,4,6-88-06-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Trichlorophenol, 2,4,5-95-95-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chloronaphthalene, 2-91-58-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitroaniline, 2-88-74-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dimethyl phthalate131-11-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Acenaphthylene208-96-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dinitrotoluene, 2,6-606-20-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitroaniline, 3-99-09-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Acenaphthene83-32-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Dinitrophenol, 2,4-51-28-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitrophenol, 4-100-02-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dibenzofuran132-64-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dinitrotoluene, 2,4-121-14-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Diethyl phthalate84-66-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chlorophenyl phenyl ether, 4-7005-72-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Fluorene86-73-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitroaniline, 4-100-01-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Dinitro-2-methyl phenol, 4,6-534-52-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10N-nitrosodiphenylamine86-30-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bromophenyl phenyl ether, 4-101-55-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Hexachlorobenzene118-74-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Pentachlorophenol87-86-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Phenanthrene85-01-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Anthracene120-12-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Di-n-butyl phthalate84-74-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Fluoranthene206-44-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Pyrene129-00-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Butylbenzyl phthalate85-68-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected15Dichlorobenzidine, 3,3'-91-94-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(a)anthracene56-55-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chrysene218-01-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-ethylhexyl)phthalate117-81-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Di-n-octyl phthalate117-84-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(b)fluoranthene205-99-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(k)fluoranthene207-08-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(a)pyrene50-32-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Indeno(1,2,3-cd)pyrene193-39-5 11/9/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 4 of 5 10:24Collect Time::11/01/2010Collect Date:AB65230Sample ID:1P14HUFFMANMW2Location ID: NC DWQ Laboratory Section Results SEM Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA625/8270/3510 NGOODug/LNot detected12Dibenzo(a,h)anthracene53-70-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Benzo(g,h,i)perylene191-24-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detectedNo BN/As detected by GC/MS.11/9/10 Bis(2-ethylhexyl) phthalate detected at (7.0 UG/L) below semivolatiles PQL. PC Sample Comments Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 5 of 5 PO Number #10G0803 Loc. Descr.:HUFFMAN FINISHING Loc. Type:MONITORING WELL Collector:B LAVERTY Collect Date:11/01/2010 Collect Time:10:50 Date Received:11/03/2010 Time Received:08:10 Location ID:1P14HUFFMANMW3 County:CALDWELL Region:ARO Labworks LoginID SMATHIS Sample Matrix:GROUNDWATER Date Reported: NC DWQ Laboratory Section Results VisitID Sample Depth AROAPReport To River Basin 12/28/2011 Emergency Yes/No COC Yes/No Sample ID:AB65231 1/5/11Report Generated: CAS #Result/ QualifierPQLAnalyte Name Validated byAnalysis Date Method ReferenceUnits LAB SMATHIS°C2.1Sample temperature at receipt by lab 11/3/10 WET Hach 8000 CGREENmg/LU2020Chemical Oxygen Demand in liquid 11/22/10 EPA 300.0 CGREENmg/L_TITLE_Ion Chromatography 11/9/10 EPA 300.0 CGREENmg/L2.81.0Chloride 11/9/10 EPA 300.0 CGREENmg/LU0.40.4Fluoride 11/9/10 EPA 300.0 CGREENmg/L9.12.0Sulfate 11/9/10 NUT Lac10-107-06-1-J CGREENmg/L as NU0.020.02NH3 as N in liquid 11/3/10 Lac10-107-04-1-c CGREENmg/L as N1.80.02NO2+NO3 as N in liquid 11/3/10 Lac10-115-01-1EF CGREENmg/L as P0.160.02Phosphorus_total as P in liquid 11/4/10 Lachat107-04-1-c CGREENmg/L as N1.80.02Nitrate as N in liquid 11/5/10 Lachat107-04-1-c CGREENmg/L as NU0.010.01Nitrite as N in liquid 11/3/10 MET EPA 200.7 ESTAFFORD1ug/L270050Al by ICP7429-90-5 11/10/10 EPA 200.8 ESTAFFORD1ug/LU2.02.0As by ICPMS7440-38-2 11/9/10 EPA 200.7 ESTAFFORD1ug/L3510Ba by ICP7440-38-3 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1.01.0Cd by ICPMS7440-43-9 11/9/10 EPA 200.8 ESTAFFORD1ug/L1010Cr by ICPMS7440-47-3 11/9/10 EPA 200.8 ESTAFFORD1ug/L3.22.0Cu by ICPMS7440-50-8 11/9/10 EPA 200.7 ESTAFFORD1ug/L240050Fe by ICP7439-89-6 11/10/10 EPA 245.1 ESTAFFORD1ug/LU0.200.2Hg 245.17439-97-6 11/9/10 EPA 200.7 ESTAFFORD1mg/L1.70.10Mg by ICP7439-95-4 11/9/10 EPA 200.7 ESTAFFORD1ug/L1710Mn by ICP7439-96-5 11/10/10 EPA 200.7 ESTAFFORD1mg/L120.10Na by ICP7440-23-5 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1010Ni by ICPMS7440-02-0 11/9/10 EPA 200.8 ESTAFFORD1ug/LU1010Pb by ICPMS7439-92-1 11/9/10 EPA 200.8 ESTAFFORD1ug/LU5.05.0Se by ICPMS7782-49-2 11/9/10 EPA 200.8 ESTAFFORD1ug/L1210Zn by ICPMS7440-66-6 11/9/10 VOL EPA5030/624/8260 ACHANDLERug/L_TITLE_Volatile Organics in liquid120-82-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Dichlorodifluoromethane75-71-8 11/3/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 1 of 5 10:50Collect Time::11/01/2010Collect Date:AB65231Sample ID:1P14HUFFMANMW3Location ID: NC DWQ Laboratory Section Results VOL Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA5030/624/8260 ACHANDLERug/LNot detected0.50Chloromethane74-87-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Vinyl Chloride75-01-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Bromomethane74-83-9 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Chloroethane75-00-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Trichlorofluoromethane75-69-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloroethene75-35-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected10Methylene Chloride75-09-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25trans-1,2-Dichloroethene156-60-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Methyl Tert-Butyl Ether1634-04-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloroethane75-34-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25cis-1,2-Dichloroethene156-59-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromochloromethane74-97-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Chloroform67-66-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.252,2-Dichloropropane594-20-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2-Dichloroethane107-06-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,1-Trichloroethane71-55-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1-Dichloropropene563-58-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Carbon Tetrachloride56-23-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Benzene71-43-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Dibromomethane74-95-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2-Dichloropropane78-87-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Trichloroethene79-01-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromodichloromethane75-27-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25cis-1,3-Dichloropropene10061-01-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25trans-1,3-Dichloropropene10061-02-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,2-Trichloroethane79-00-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Toluene108-88-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,3-Dichloropropane142-28-9 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Dibromochloromethane124-48-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25(EDB)1,2-Dibromoethane106-93-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Tetrachloroethene127-18-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Chlorobenzene108-90-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Ethylbenzene100-41-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.0Bromoform75-25-2 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50m,p-Xylene108-38-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Styrene100-42-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,2,2-Tetrachloroethane79-34-5 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,1,1,2-Tetrachloroethane630-20-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25o-Xylene95-47-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2,3-Trichloropropane96-18-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Isopropylbenzene98-82-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25Bromobenzene108-86-1 11/3/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 2 of 5 10:50Collect Time::11/01/2010Collect Date:AB65231Sample ID:1P14HUFFMANMW3Location ID: NC DWQ Laboratory Section Results VOL Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA5030/624/8260 ACHANDLERug/LNot detected0.25n-Propylbenzene103-65-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.252-Chlorotoluene95-49-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.254-Chlorotoluene106-43-4 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,3,5-Trimethylbenzene108-67-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25tert-Butylbenzene98-06-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.251,2,4-Trimethylbenzene95-63-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25sec-Butylbenzene135-98-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25m-Dichlorobenzene (1,3)541-73-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25p-Dichlorobenzene (1,4)106-46-7 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25o-Dichlorobenzene (1,2)95-50-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25p-Isopropyltoluene99-87-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.25n-Butylbenzene104-51-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected2.01,2-Dibromo-3-Chloropropane96-12-8 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.501,2,4-Trichlorobenzene120-82-1 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Naphthalene91-20-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected0.50Hexachlorobutadiene87-68-3 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detected1.01,2,3-Trichlorobenzene87-61-6 11/3/10 EPA5030/624/8260 ACHANDLERug/LNot detectedVOC'S BY GC/MS 11/3/10 SEM EPA625/8270/3510 NGOODug/L_TITLE_Semivolatile Organics (BNAs) in liquid7440-50-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Aniline62-53-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Phenol108-95-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-chloroethyl)ether111-44-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chlorophenol, 2-95-57-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorobenzene, 1,3541-73-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorobenzene, 1,4-106-46-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected20Benzyl alcohol100-51-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorobenzene, 1,2-95-50-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Methylphenol, 2-95-48-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-chloroisopropyl)ether39638-32-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Methylphenol, 4-106-44-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10N-nitrosodi-n-propylamine621-64-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Hexachloroethane67-72-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Nitrobenzene98-95-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Isophorone78-59-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Nitrophenol, 2-88-75-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Dimethylphenol, 2,4-105-67-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Benzoic acid65-85-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bis(2-chloroethoxy)methane111-91-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dichlorophenol, 2,4-120-83-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Trichlorobenzene, 1,2,4-120-82-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Naphthalene(SV)91-20-3 11/9/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 3 of 5 10:50Collect Time::11/01/2010Collect Date:AB65231Sample ID:1P14HUFFMANMW3Location ID: NC DWQ Laboratory Section Results SEM Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA625/8270/3510 NGOODug/LNot detected20Chloroaniline, 4-106-47-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Hexachlorobutadiene(SV)87-68-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected20Chloro-3-methyl phenol, 4-59-50-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Methylnaphthalene, 2-91-57-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Hexachlorocyclopentadiene77-47-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Trichlorophenol, 2,4,6-88-06-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Trichlorophenol, 2,4,5-95-95-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chloronaphthalene, 2-91-58-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitroaniline, 2-88-74-4 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dimethyl phthalate131-11-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Acenaphthylene208-96-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dinitrotoluene, 2,6-606-20-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitroaniline, 3-99-09-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Acenaphthene83-32-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Dinitrophenol, 2,4-51-28-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitrophenol, 4-100-02-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dibenzofuran132-64-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Dinitrotoluene, 2,4-121-14-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Diethyl phthalate84-66-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chlorophenyl phenyl ether, 4-7005-72-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Fluorene86-73-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Nitroaniline, 4-100-01-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Dinitro-2-methyl phenol, 4,6-534-52-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10N-nitrosodiphenylamine86-30-6 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Bromophenyl phenyl ether, 4-101-55-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Hexachlorobenzene118-74-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected50Pentachlorophenol87-86-5 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Phenanthrene85-01-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Anthracene120-12-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Di-n-butyl phthalate84-74-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Fluoranthene206-44-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Pyrene129-00-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Butylbenzyl phthalate85-68-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected15Dichlorobenzidine, 3,3'-91-94-1 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(a)anthracene56-55-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Chrysene218-01-9 11/9/10 EPA625/8270/3510 NGOODug/L12010Bis(2-ethylhexyl)phthalate117-81-7 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Di-n-octyl phthalate117-84-0 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(b)fluoranthene205-99-2 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(k)fluoranthene207-08-9 11/9/10 EPA625/8270/3510 NGOODug/LNot detected10Benzo(a)pyrene50-32-8 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Indeno(1,2,3-cd)pyrene193-39-5 11/9/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 4 of 5 10:50Collect Time::11/01/2010Collect Date:AB65231Sample ID:1P14HUFFMANMW3Location ID: NC DWQ Laboratory Section Results SEM Validated byCAS #Analyte Name PQL Result/ Qualifier Units Method Reference Analysis Date EPA625/8270/3510 NGOODug/LNot detected12Dibenzo(a,h)anthracene53-70-3 11/9/10 EPA625/8270/3510 NGOODug/LNot detected12Benzo(g,h,i)perylene191-24-2 11/9/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 5 of 5 PO Number #ARO Loc. Descr.:HUFFMAN FINISHING Loc. Type:MONITORING WELL Collector:B LAVERTY Collect Date:11/01/2010 Collect Time:10:24 Date Received:11/02/2010 Time Received:09:00 Location ID:1P14HUFFMANMW2 County:CALDWELL Region:ARO Labworks LoginID KJIMISON Sample Matrix:GROUNDWATER Date Reported: NC DWQ Laboratory Section Results VisitID Sample Depth AROAPReport To River Basin 12/28/2011 Emergency Yes/No COC Yes/No Sample ID:AB65256 11/29/10Report Generated: CAS #Result/ QualifierPQLAnalyte Name Validated byAnalysis Date Method ReferenceUnits Others SMATHIS°C4.6Sample temperature at receipt by lab 11/2/10 APHA2130B-20th CGREENNTU451Turbidity11/3/10 APHA2540D-20th CGREENmg/L666.2Residue_Suspended in liquid 11/8/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 1 of 1 PO Number #ARO Loc. Descr.:HUFFMAN FINISHING Loc. Type:MONITORING WELL Collector:B LAVERTY Collect Date:11/01/2010 Collect Time:10:50 Date Received:11/02/2010 Time Received:09:00 Location ID:1P14HUFFMANMW3 County:CALDWELL Region:ARO Labworks LoginID KJIMISON Sample Matrix:GROUNDWATER Date Reported: NC DWQ Laboratory Section Results VisitID Sample Depth AROAPReport To River Basin 12/28/2011 Emergency Yes/No COC Yes/No Sample ID:AB65257 11/29/10Report Generated: CAS #Result/ QualifierPQLAnalyte Name Validated byAnalysis Date Method ReferenceUnits Others SMATHIS°C4.6Sample temperature at receipt by lab 11/2/10 APHA2130B-20th CGREENNTU381Turbidity11/3/10 APHA2540D-20th CGREENmg/L336.2Residue_Suspended in liquid 11/8/10 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of the qualifier codes refer to htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist#Data_Qualifer_Codes <htp://portal.ncdenr.org/web/wq/lab/stafnfo/techassist> Page 1 of 1 GROUNDWATER FIELD/LAB FORM North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWATER SECTION Location code: Trip Blank County: Lab Number_________________________________ Quad No_____________ Serial No.________________ Date Received_____________ Time:______________ Lat._________________ Long.___________________ Rec’d By: From:Bus, Courier, Hand Del., Other:______________________________________ Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By:________________ Ck:____________ WSRO, Kinston FO, Fed. Trust, Central Off., Other:______________________ Date Reported:_______________________________ Shipped by: Bus, Courier, Hand Del., Other:____________________________ Purpose: Collector(s): Brett Laverty Date: 11/1/2010 Time: 8:07 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: VOA Trip Blank pH 400____________________ Spec. Cond.94_____________at 25ºC Location or Site: ARO Laboratory Temp.10_________________ºC Odor____________________________ Description of sampling point: Appearance______________DO, mg/L ________ ORP, mV _________ Sampling Method: Sample Interval_________________ Field Analysis By:____________________________________________ Remarks______________________________________________________________________________ LABORATORY ANALYSES BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 ug/L Organochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L Al-Aluminum 46557 ug/L Organophosphorus Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As-Arsenic 46551 ug/L Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cond. 95 µMhos/cm Cd-Cadmium 46559 ug/L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 ug/L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 ug/L Boron DOC Fe-Iron 46563 ug/L Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 ug/L TPH-Diesel Range pH 403 units K-Potassium 46555 mg/L Alkalinity to pH 4.5 410 mg/L Mg-Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L PO4 as P Mn-Manganese 46565 ug/L X Volatile Organics (VOA bottle) Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel ug/L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 ug/L Chloride 940 mg/L P: Total as P 665 mg/L Se-Selenium ug/L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 ug/L Color: True 80 CU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (ºC): Cyanide 720 mg/L NH4 - ammonium Silica Lab Comments_____________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ GW-54 REV. 7/03 For Dissolved Analysis-submit filtered sample and write “DIS” in block. SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) Other Routine Soil Emergency Chain of Custody (circle one) (Pumping time, air temp., etc.) X X GROUNDWATER FIELD/LAB FORM North Carolina Department of Environment and Natural Resources DIVISION OF WATER QUALITY-GROUNDWATER SECTION Location code: 1P14HuffmanMW3 County: Caldwell Lab Number_________________________________ Quad No_____________ Serial No.________________ Date Received_____________ Time:______________ Lat._________________ Long.___________________ Rec’d By: From:Bus, Courier, Hand Del., Other:______________________________________ Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By:________________ Ck:____________ WSRO, Kinston FO, Fed. Trust, Central Off., Other:______________________ Date Reported:_______________________________ Shipped by: Bus, Courier, Hand Del., Other:____________________________ Purpose: Collector(s): Brett Laverty Date: 11/1/2010 Time: 10:50 AM Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other: FIELD ANALYSES Owner: Huffman Finishing pH 400____________________ Spec. Cond.94_____________at 25ºC Location or Site: 4919 Hickory Blvd. Granite Falls, NC Temp.10_________________ºC Odor____________________________ Description of sampling point: Well Head Appearance______________DO, mg/L ________ ORP, mV _________ Sampling Method: Bailer Sample Interval_________________ Field Analysis By:____________________________________________ Remarks______________________________________________________________________________ LABORATORY ANALYSES BOD 310 mg/L Diss. Solids 70300 mg/L Ag-Silver 46566 ug/L Organochlorine Pesticides COD High 340 mg/L Fluoride 951 mg/L Al-Aluminum 46557 ug/L Organophosphorus Pesticides COD Low 335 mg/L Hardness: Total 900 mg/L As-Arsenic 46551 ug/L Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness (non-carb) 902 mg/L Ba-Barium 46558 ug/L Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/L PCBs TOC 680 mg/L Specific Cond. 95 µMhos/cm Cd-Cadmium 46559 ug/L Turbidity 76 NTU Sulfate 945 mg/L Cr-Chromium 46559 ug/L MBAS Residue, Total Suspended 530 mg/L Sulfide 745 mg/L Cu-Copper 46562 ug/L Boron DOC Fe-Iron 46563 ug/L X Semivolatile Organics Oil and Grease mg/L Hg-Mercury 71900 ug/L TPH-Diesel Range pH 403 units K-Potassium 46555 mg/L Alkalinity to pH 4.5 410 mg/L Mg-Magnesium 46554 mg/L Alkalinity to pH 8.3 415 mg/L PO4 as P Mn-Manganese 46565 ug/L X Volatile Organics (VOA bottle) Carbonate 445 mg/L NH3 as N 610 mg/L Na-Sodium 46556 mg/L TPH-Gasoline Range Bicarbonate 440 mg/L TKN as N 625 mg/L Ni-Nickel ug/L TPH-BTEX Gasoline Range Carbon dioxide 405 mg/L NO2 + NO3 as N 630 mg/L Pb-Lead 46564 ug/L Chloride 940 mg/L P: Total as P 665 mg/L Se-Selenium ug/L Chromium: Hex 1032 ug/L Nitrate (NO3 as N) 620 mg/L Zn-Zinc 46567 ug/L Color: True 80 CU Nitrite (NO2 as N) 615 mg/L LAB USE ONLY Temperature on arrival (ºC): Cyanide 720 mg/L NH4 - ammonium Silica Lab Comments_____________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ _________________________________________________________________________________________________________________________________________________ GW-54 REV. 7/03 For Dissolved Analysis-submit filtered sample and write “DIS” in block. SAMPLE TYPE SAMPLE PRIORITY Water (Ground Water) Other Routine Soil Emergency Chain of Custody (circle one) (Pumping time, air temp., etc.) X X X X X X X X X X X X X X X X X X X X X X X X NORTH CAROLINA GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY - GROUNDWATER SECTION County Caldwell Sample Type Sample Priority Lab Number Quad No.K72q2 Serial No.135034 Water X Routine X Date Received Time Lat.35 46 13 Long.81 23 35 Soil Emergency Rec'd by: From: Bus, Courier, Hand Del. Other Other Report To: ARO (ARO, CO, Other)Chain of Custody Data Entry by:Ck: Shipped by:Courier (Bus, Courier, Hand Del., Other) Collector(s):TMinnick Date:03 08 19 Date Reported: Time:1050 Purpose:(Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other): FIELD ANALYSES (circle one)Owner Huffman Finishing Company pH400 5.0 Spec. Cond.94 20 at 250C Location or site Upgradient of treatment facility Temp10 20 0C Odor None Description of sampling point Well Head Appearance Water dingy Sampling Method Bailer Sample Interval: 20 ft. - 30 ft. (pump,bailer,etc.) Field Analysis by:Remarks Static Water Level =5.65 ft. LABORATORY ANALYSIS (pumping time, air temp, etc.) BOD5 310 mg/l Diss. Solids 70300 mg/l Ag-Silver 46566 ug/l Organochlorine Pesticides COD High 340 mg/l Fluoride 951 mg/l Al-Aluminum 46557 ug/l Organophosphorus Pesticides X COD Low 335 H2SO4 ICE mg/l Hardness: Total 900 mg/l **X As-Arsenic 46551 ug/l Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness: (non-carb) 902 mg/l Ba-Barium 46558 ug/l Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/l PCB's X TOC 680 H3PO4 ICE mg/l Specific Cond. 95 uMhos/cm2 Cd-Cadmium 46559 ug/l Turbidity 76 NTU X Sulfate 945 ICE mg/l Cr-Chromium 46560 ug/l Residue., Suspended 530 mg/l Sulfide 745 mg/l **X Cu- Copper 46562 ug/l Fe- Iron 46563 ug/l Semivolatile Organics Oil and Grease mg/l Hg- Mercury 71900 ug/l TPH-Diesel Range pH 403 units K-Potassium 46555 mg/l Alkalinity to pH 4.5 410 mg/l Mg- Magnesium 46554 mg/l Alkalinity to pH 8.3 415 mg/l Mn-Manganese 46565 ug/l Carbonate 445 mg/l *X NH3 as N 610 mg/l **X Na- Sodium 46556 mg/l Volatile Organics (VOA bottle) Bicarbonate 440 mg/l TKN as N 625 mg/l Ni-Nickel ug/l TPH-Gasoline Range Carbon dioxide 405 mg/l *X NO2 +NO3 as N 630 mg/l Pb-Lead 46564 ug/l TPH-BTEX Gasoline Range X Chloride 940 mg/l *X P: Total as P 665 mg/l Se-Selenium ug/l Chromium: Hex 1032 ug/l **X Zn-Zinc 46567 ug/l Color: True 80 CU Cyanide 720 mg/l LAB COMMENTS :*P & N PRESERVED w/25% H2SO4 **METALS PRESERVED w/ HNO3 ICE GW-54 For Dissolved Analysis - submit filtered sample and write "DIS" in block. 22 Huffman Finishing Co. MW-2 NORTH CAROLINA GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY - GROUNDWATER SECTION County Caldwell Sample Type Sample Priority Lab Number Quad No.K72q2 Serial No.135034 Water X Routine X Date Received Time Lat.35 46 13 Long.81 23 35 Soil Emergency Rec'd by: From: Bus, Courier, Hand Del. Other Other Report To: ARO (ARO, CO, Other)Chain of Custody Data Entry by:Ck: Shipped by:Hand Delivered (Bus, Courier, Hand Del., Other) Collector(s):TMinnick Date:03 08 19 Date Reported: Time:1050 Purpose:(Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other): FIELD ANALYSES (circle one)Owner Huffman Finishing Company pH400 5.0 Spec. Cond.94 20 at 250C Location or site Upgradient of treatment facility Temp10 20 0C Odor None Description of sampling point Well Head Appearance Water dingy Sampling Method Bailer Sample Interval: 20 ft. - 30 ft. (pump,bailer,etc.) Field Analysis by:Remarks Static Water Level =5.65 ft. LABORATORY ANALYSIS (pumping time, air temp, etc.) BOD5 310 mg/l X Diss. Solids 70300 ICE mg/l Ag-Silver 46566 ug/l Organochlorine Pesticides COD High 340 mg/l Fluoride 951 mg/l Al-Aluminum 46557 ug/l Organophosphorus Pesticides COD Low 335 mg/l Hardness: Total 900 mg/l As-Arsenic 46551 ug/l Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness: (non-carb) 902 mg/l Ba-Barium 46558 ug/l Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/l PCB's TOC 680 mg/l Specific Cond. 95 uMhos/cm2 Cd-Cadmium 46559 ug/l Turbidity 76 NTU Sulfate 945 mg/l Cr-Chromium 46560 ug/l Residue., Suspended 530 mg/l Sulfide 745 mg/l Cu- Copper 46562 ug/l Fe- Iron 46563 ug/l Semivolatile Organics Oil and Grease mg/l Hg- Mercury 71900 ug/l TPH-Diesel Range pH 403 units K-Potassium 46555 mg/l Alkalinity to pH 4.5 410 mg/l Mg- Magnesium 46554 mg/l Alkalinity to pH 8.3 415 mg/l Mn-Manganese 46565 ug/l Carbonate 445 mg/l NH3 as N 610 mg/l Na- Sodium 46556 mg/l Volatile Organics (VOA bottle) Bicarbonate 440 mg/l TKN as N 625 mg/l Ni-Nickel ug/l TPH-Gasoline Range Carbon dioxide 405 mg/l NO2 +NO3 as N 630 mg/l Pb-Lead 46564 ug/l TPH-BTEX Gasoline Range Chloride 940 mg/l P: Total as P 665 mg/l Se-Selenium ug/l Chromium: Hex 1032 ug/l Zn-Zinc 46567 ug/l Color: True 80 CU Cyanide 720 mg/l LAB COMMENTS : GW-54 For Dissolved Analysis - submit filtered sample and write "DIS" in block. 2 Huffman Finishing Co. MW-2 NORTH CAROLINA GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY - GROUNDWATER SECTION County Caldwell Sample Type Sample Priority Lab Number Quad No.K72q3 Serial No.135033 Water X Routine X Date Received Time Lat.35 46 12 Long.81 23 37 Soil Emergency Rec'd by: From: Bus, Courier, Hand Del. Other Other Report To: ARO (ARO, CO, Other)Chain of Custody Data Entry by:Ck: Shipped by:Courier (Bus, Courier, Hand Del., Other) Collector(s):TMinnick Date:03 08 19 Date Reported: Time:1110 Purpose:(Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other): FIELD ANALYSES (circle one)Owner Huffman Finishing Company pH400 6.0 Spec. Cond.94 80 at 250C Location or site Downgradient of treatment facility Temp10 18 0C Odor None Description of sampling point Well Head Appearance Water clear Sampling Method Bailer Sample Interval: 5 ft. - 15 ft. (pump,bailer,etc.) Field Analysis by:Remarks Static Water Level =7.1 ft. LABORATORY ANALYSIS (pumping time, air temp, etc.) BOD5 310 mg/l Diss. Solids 70300 mg/l Ag-Silver 46566 ug/l Organochlorine Pesticides COD High 340 mg/l Fluoride 951 mg/l Al-Aluminum 46557 ug/l Organophosphorus Pesticides X COD Low 335 H2SO4 ICE mg/l Hardness: Total 900 mg/l **X As-Arsenic 46551 ug/l Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness: (non-carb) 902 mg/l Ba-Barium 46558 ug/l Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/l PCB's X TOC 680 H3PO4 ICE mg/l Specific Cond. 95 uMhos/cm2 Cd-Cadmium 46559 ug/l Turbidity 76 NTU X Sulfate 945 ICE mg/l Cr-Chromium 46560 ug/l Residue., Suspended 530 mg/l Sulfide 745 mg/l **X Cu- Copper 46562 ug/l Fe- Iron 46563 ug/l Semivolatile Organics Oil and Grease mg/l Hg- Mercury 71900 ug/l TPH-Diesel Range pH 403 units K-Potassium 46555 mg/l Alkalinity to pH 4.5 410 mg/l Mg- Magnesium 46554 mg/l Alkalinity to pH 8.3 415 mg/l Mn-Manganese 46565 ug/l Carbonate 445 mg/l *X NH3 as N 610 mg/l **X Na- Sodium 46556 mg/l Volatile Organics (VOA bottle) Bicarbonate 440 mg/l TKN as N 625 mg/l Ni-Nickel ug/l TPH-Gasoline Range Carbon dioxide 405 mg/l *X NO2 +NO3 as N 630 mg/l Pb-Lead 46564 ug/l TPH-BTEX Gasoline Range X Chloride 940 mg/l *X P: Total as P 665 mg/l Se-Selenium ug/l Chromium: Hex 1032 ug/l **X Zn-Zinc 46567 ug/l Color: True 80 CU Cyanide 720 mg/l LAB COMMENTS :*P & N PRESERVED w/25% H2SO4 **METALS PRESERVED w/HNO3 ICE GW-54 For Dissolved Analysis - submit filtered sample and write "DIS" in block. 3 Huffman Finishing Co. MW-3 NORTH CAROLINA GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY - GROUNDWATER SECTION County Caldwell Sample Type Sample Priority Lab Number Quad No.K72q3 Serial No.135033 Water X Routine X Date Received Time Lat.35 46 12 Long.81 23 37 Soil Emergency Rec'd by: From: Bus, Courier, Hand Del. Other Other Report To: ARO (ARO, CO, Other)Chain of Custody Data Entry by:Ck: Shipped by:Hand Delivered (Bus, Courier, Hand Del., Other) Collector(s):TMinnick Date:03 08 19 Date Reported: Time:1110 Purpose:(Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other): FIELD ANALYSES (circle one)Owner Huffman Finishing Company pH400 6.0 Spec. Cond.94 80 at 250C Location or site Downgradient of treatment facility Temp10 18 0C Odor None Description of sampling point Well Head Appearance Water clear Sampling Method Bailer Sample Interval: 5 ft. - 15 ft. (pump,bailer,etc.) Field Analysis by:Remarks Static Water Level =7.1 ft. LABORATORY ANALYSIS (pumping time, air temp, etc.) BOD5 310 mg/l X Diss. Solids 70300 ICE mg/l Ag-Silver 46566 ug/l Organochlorine Pesticides COD High 340 mg/l Fluoride 951 mg/l Al-Aluminum 46557 ug/l Organophosphorus Pesticides COD Low 335 mg/l Hardness: Total 900 mg/l As-Arsenic 46551 ug/l Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness: (non-carb) 902 mg/l Ba-Barium 46558 ug/l Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/l PCB's TOC 680 mg/l Specific Cond. 95 uMhos/cm2 Cd-Cadmium 46559 ug/l Turbidity 76 NTU Sulfate 945 mg/l Cr-Chromium 46560 ug/l Residue., Suspended 530 mg/l Sulfide 745 mg/l Cu- Copper 46562 ug/l Fe- Iron 46563 ug/l Semivolatile Organics Oil and Grease mg/l Hg- Mercury 71900 ug/l TPH-Diesel Range pH 403 units K-Potassium 46555 mg/l Alkalinity to pH 4.5 410 mg/l Mg- Magnesium 46554 mg/l Alkalinity to pH 8.3 415 mg/l Mn-Manganese 46565 ug/l Carbonate 445 mg/l NH3 as N 610 mg/l Na- Sodium 46556 mg/l Volatile Organics (VOA bottle) Bicarbonate 440 mg/l TKN as N 625 mg/l Ni-Nickel ug/l TPH-Gasoline Range Carbon dioxide 405 mg/l NO2 +NO3 as N 630 mg/l Pb-Lead 46564 ug/l TPH-BTEX Gasoline Range Chloride 940 mg/l P: Total as P 665 mg/l Se-Selenium ug/l Chromium: Hex 1032 ug/l Zn-Zinc 46567 ug/l Color: True 80 CU Cyanide 720 mg/l LAB COMMENTS : GW-54 For Dissolved Analysis - submit filtered sample and write "DIS" in block. 3 Huffman Finishing Co. MW-3 NORTH CAROLINA GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources DIVISION OF WATER QUALITY - GROUNDWATER SECTION County Sample Type Sample Priority Lab Number Quad No.Serial No.Water Routine Date Received Time Lat.Long.Soil Emergency Rec'd by: From: Bus, Courier, Hand Del. Other Other Report To: (ARO, CO, Other)Chain of Custody Data Entry by:Ck: Shipped by:(Bus, Courier, Hand Del., Other) Collector(s):Date:Date Reported: Time: Purpose:(Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other): FIELD ANALYSES (circle one)Owner pH400 Spec. Cond.94 at 250C Location or site Temp10 0C Odor Description of sampling point Appearance Sampling Method Sample Interval: (pump,bailer,etc.) Field Analysis by:Remarks LABORATORY ANALYSIS (pumping time, air temp, etc.) BOD5 310 mg/l Diss. Solids 70300 mg/l Ag-Silver 46566 ug/l Organochlorine Pesticides COD High 340 mg/l Fluoride 951 mg/l Al-Aluminum 46557 ug/l Organophosphorus Pesticides COD Low 335 mg/l Hardness: Total 900 mg/l As-Arsenic 46551 ug/l Nitrogen Pesticides Coliform: MF Fecal 31616 /100ml Hardness: (non-carb) 902 mg/l Ba-Barium 46558 ug/l Acid Herbicides Coliform: MF Total 31504 /100ml Phenols 32730 ug/l Ca-Calcium 46552 mg/l PCB's TOC 680 mg/l Specific Cond. 95 uMhos/cm2 Cd-Cadmium 46559 ug/l Turbidity 76 NTU Sulfate 945 mg/l Cr-Chromium 46560 ug/l Residue., Suspended 530 mg/l Sulfide 745 mg/l Cu- Copper 46562 ug/l Fe- Iron 46563 ug/l Semivolatile Organics Oil and Grease mg/l Hg- Mercury 71900 ug/l TPH-Diesel Range pH 403 units K-Potassium 46555 mg/l Alkalinity to pH 4.5 410 mg/l Mg- Magnesium 46554 mg/l Alkalinity to pH 8.3 415 mg/l Mn-Manganese 46565 ug/l Carbonate 445 mg/l NH3 as N 610 mg/l Na- Sodium 46556 mg/l Volatile Organics (VOA bottle) Bicarbonate 440 mg/l TKN as N 625 mg/l Ni-Nickel ug/l TPH-Gasoline Range Carbon dioxide 405 mg/l NO2 +NO3 as N 630 mg/l Pb-Lead 46564 ug/l TPH-BTEX Gasoline Range Chloride 940 mg/l P: Total as P 665 mg/l Se-Selenium ug/l Chromium: Hex 1032 ug/l Zn-Zinc 46567 ug/l Color: True 80 CU Cyanide 720 mg/l LAB COMMENTS : GW-54 For Dissolved Analysis - submit filtered sample and write "DIS" in block. Huffman Finishing Co.-Master WELL ABANDONMENT RECORD North Carolina Department omnvironmant.and Natural -Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 4080—C 1. WELL CONTRACTOR: - Isaac H-. Blackburn Well Contractor (IndividuaD Name Hickory Well Drilliiig Co. Well Contractor Company Name P. 0. Box 4216 Street Address Hickory NC""" 28603 City or Town State Zip Code 8� 28 1 324-0035 Area code Phone number S. WELL DETAILS: " a.Total Depth 114* " it. Diameter: 2 in. b. Water Level (Below Measuring Point): _ ft. Measuring point is 3 ft. above land surface. 6. CASING: ,Length Diameter a. Casing Depth (if known): 14 ft. 2 in. b. Casing Removed: �— ft -T— in. 7 2. WELL INFORMATION: SITE WELL ID#[if appficabte) NWT/03 S• STATE WELL PERMIT# (gapplicable) N/A COUNTY WELL PERMIT # (ifapplicable) N/A DWQorOTHERPERMlt#(ifapplicable) N/A WELL USE (Check applicable use)MMonitoring ❑ Residential ❑ M unfelpaUPublic • _0 Industria#Commercial ❑ Agricultural ❑ Recovery ❑ Injection ❑ irrigation L) Other (fist use) ' 3. WELL LOCATION: COUNTYCaldwell QUADRANGIENAME. NEARESTTOWN: Granite Falls, Y. C., 28630 9. 4919 Hickory Blvd. (Hwy. 321 South) (StmetfRoap Name, Number, Community, Subdivision: Lot No:, Parcel, Zip Code) TOPOGRAPHC/LAND SETTING: 0 Slope 0 Valley 3EFRat. ❑RidgeO Other h DISINFECTION:.. 4. Oz s .. (Amountof 65°A75%calcium hypochlortle used) SEALING MATERIAL: N at-errrant Cement .lb. Water gal. Bentonite Bentonite 25 lb. Type:❑ Slurry 9 Pellets Water S gal. Other Type mad m n Rand t ,Cement t. lb.., Water E nat.+ r: f 1 ial ." Portland Cement 45 Lbs. tom-„-1 w EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL: Filled from Top with Bentonite Pellets and Caped unth Cement. (Ceek appropriate selling) 10. WELL DIAGRAM: Draw a detailed sketch of theell on the back of this form showing total depth, depth and diameter of screens (if any) remaining LATITUDE „3.S_ _•___°DMS OR._,.]]1939. in the well, greys] interval, intervals of casing perforations, and depthsand LONGITUDE 81 _ —' °DMS OR. .390451 types of Till materlaLvsed Latitudenongffude source: =PS Oropographic map 10/31/2012 (location of well must be shown on a USGS topo map andaftached to 11. DATE WELL ABANDONED this form if not using GPS) 100 HEREBY CERTIFY THATTHIS WELL WAS ABANDONEDIN ACCORDANCE WITH 15AM C2C, ICONSTRUCTION STANDARDS, AND THATA COPY OF 4a.FACILITY- The name of the business where the well is located. Complete 4a: THIS RE EN Pa B D TO THE WELL OWNER. (Ira residardial well, skip 4a; complete 4b, "I ownerinfombzgon oNyj FACILITY In# (d applcable) NPDES Permit#NCO025135 NAMEOFFACILrry Huffman Finishing Co. W. W.T. P.sIGNA7URE O 'CERTIFIED WELL CONTRACTOR pp STREETADDRESS 4919 Hickory Blvd-. - .. Granite Fa '-a' C. 28630 SIGNATUREOF PRNAIb VVI:LLOWNERABANDONINGTHEWELLDATE City or Town State Zip CodeObepdvatewepmvnerrnusibeanindMdual nall 'bandons Ns/herresdenialwell inaccordance with 15A NCAC 2C.0113.) 46. CONTACT PERSONNVELL OWNER: , Lee Huffman Isaac Henry Blackburn 11/6/2012 NAME PRINTED NAME OF PERSON ABANDONING THE WE ILL TADDRESS Same as above A11.1Y 'Info[mation Processing, Form GW 3D Rev. 5110 WELL ABANDONMENT RECORD North Carolina Department of Environment and Natural Resources. Division of Water Quality WELL CONTRACTOR CERTIFICATION # 3692—C 1. WELL CONTRACTOR: William Joe Mull Well Contractor (IndmduaD Name Hickory Well Drilling Co. Well Contractor Company Name P. 0. Box 4216 Street Address Hickory NC 28603 CdyorTown State Zljf de t 8281 324-0035 Area code Phone number 2. WELL INFORMATION: - SITE WELL ID (if applicable) - MW1102 STATE WELL PERMIT# (ifappricable) N/A COUNTY WELL PERMIT # (ifapplicable) N/A DWO or OTHER PERMIT #(tfapplicable) N/A WELL USE (Check applicable usekMonitoring ❑ Residential ❑ MunicipaUPublic ❑ IndustriallCommercial ❑ Agricultural ❑ Recovery ❑ Injection ❑ Irrigation ❑ Other (list use) 3. WELL LOCATION: COUNTY Caldwe110UADRANGIE NAME NEARESTTOWN: Granite Falls 4919 Hickory Blvd. ( Hwy..321 South) (StreeVRoad Name, Number, Com,,rdly, Subdivision, Lot No., Panel, Zip Code) TOPOGRAPHC / LAND SETTING: ❑ Slope ❑ Valley ZAI'lat ❑ Ridge❑ Other (Check appmpriate setfing) LATITUDE 35 ._ DMs OR .771939 LONGITUDE Hl___ 'DMS OR;.390451 Latitudenongitudesource:x®GPS ❑ropogrephicmap (location of well must be shown on a USGS t0p0 map andattached to this form if not using GPS) 5. WELL DETAILS: a.Total Depth 32 ft. Diameter. 2 tn. b. Water Level (Below Measuring Point): , 20 fL Measudng point is 3.5 0. above land surface. 6. CASING: Length Diameter a. Casing Depth (f known): 32 it 2 In. b. Casing Removed: —1L —T— in. 7. DISINFECTION: 6 OZS. (Amount of 65°/a75% calcium hypochiorite used) B. SEALING MATERIAL: Neitummit Cement lb. Water. gal. Sand Camenl Cement lb. Water ai. Bentonite i Bentonite 45 lb - Type: ❑ Slurtg� Pellets r " Water S gal. Other Type material Portland Cement Amount 45 Lb. Bag w 4 9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL: Filled from Top with Bentonite Pellets and Caped with Cement. 10. WELL DIAGRAM : Draw a detailed sketch of thoen on the back of this form showing total depth, depth and diameter of screens (f any) remaining in the well, gravel interval, intervals of casing perforations, and depths and types of fill materiatvsed 11. DATE WELL ABANDONED 10/31/2012 1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE 4a. FACILITY - The name of the business where the wen is located. Complete 4ar TTHHIH 1EA NgDCj{g2gt CON ION STANDARDS, AND THATA COPY OF (If a residential wen, skip 4a; complete 4b, well owner irdomatiodonly.) THE WELLOWNER FACILITY ID#(ifappliicable) NPDE6 Permit# NC0025135 11 NAMEOFFACILrry . Huffman Y3-U!Shing CO. W.W.T. LGNATURE OF CE ED EL THE TOR / DATE STREETADDRESS 4919 Hickory Blvd. Granite Falls NC 28630 SIGRE NATUOFPRIVATE WELLOWNERABANDONING THEWELL DATE CI(yorTown State Zip Code (The private well ownermusl be an individualw rsonai bantlons hisfher residential well 4b. CONTACT PERSONMELL OWNER: in axordance with 15A NCAC 2C .0113.) Lee Huffman William Joe Mull 11/6/2012 NAME PRINTED NAME OF PERSON ABANDONING THE WE LL STREET ADDRESS Same as A OVe. Processing, Form GW-30 Rev. 5/10 n \4 County: CALDWELL Sample ID: AB65230 River Basin OFWATEq PO Number# 10GO802 Report To AROAP O� QG Dale Received: 1110312010 h r Time Received: 08:10 Collector: B LAVERTY -1 O Y Labworks LoginlD SMATHIS Region: ARO - Report Generated: 1/5/11 SampleMabix: GROUNDWATER Date Reported: 12/2812011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD COC Yes/No Loc. Descr.: HUFFMAN FINISHING Location ID: 1P14HUFFMANMW2 Collect Dale: 11/01/2010 Collect Time: 10:24 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab POL Result/ Qualifier 2.1 Units °C Method Reference Analysis Date 11/3110 Validated by SMATHIS WET Chemical Oxygen Demand in liquid 20 20 U mga Hach 8000 11/22/10 CGREEN Ion Chromatography _TITLE_ mg1L EPA 300.0 11/9/10 CGREEN Chloride 1.0 1.5 mg/L EPA 300.0 11/9/10 CGREEN Fluoride 0.4 0.4U mg/L EPA300.0 11/9/10 CGREEN Sulfate 2.0 2.0 U mg/L EPA 300.0 1119110 CGREEN NUT NH3 as N in liquid 0.02 0.02 U mg/L as N Lacl G-107-06-1-J 1113/10 CGREEN NO2+NO3 as N in liquid 0.02 1.0 mg/Las N LaclC-107-04-1-c 11/3110 CGREEN Phosphorus -total as P in liquid 0.02 0.12 mg/L as P Lac10-115-01-1 EF 11/4/10 CGREEN Nitrate as N in liquid 0.02 0.99 mg/L as N Lachat107-04-1-c 1115110 CGREEN Nitrite as N in liquid 0.01 0.01 mg/L as N Lachat107-04-1-c 11/3/10 CGREEN MET 7429-90-5 Al by ICP 50 3600 ug/L EPA 200.7 11/10/10 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA 200.8 11/9/10 ESTAFFORD1 7440-36-3 Be by ICP 10 47 ug/L EPA200.7 11/9/10 ESTAFFORDI 744043-9 Cd by ICPMS 1.0 1.0 U ug/L EPA 200.8 1119110 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 IOU ug/L EPA200.8 1119/10 ESTAFFORD1 7440-50-8 Cu by ICPMS 2.0 3.5 ug/L EPA 200.8 11/9/10 ESTAFFORDI 7439-89-6 Fe by ICP 50 3000 ug/L EPA 200.7 11/10/10 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA245.1 11/9110 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 1.5 mg/L EPA 200.7 1119/10 ESTAFFORDI 7439-96-5 Mn by ICP 10 140 ug/L EPA200.7 11/10/10 ESTAFFORDI 7440-23-5 Na by ICP 0.10 1.6 mg/L EPA 200.7 11/9/10 ESTAFFORDI 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 1119110 ESTAFFORDI 7439-92-1 Pb by ICPMS 10 IOU ug/L EPA200.8 11/9110 ESTAFFORDI 7782A9-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 1119/10 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 17 ug/L EPA200.8 11/9/10 ESTAFFORD1 Volatile Organics in liquid _TITLE ug/L EPA5030/624/8260 1113/10 ACHANDLER 75-71-8 DichlorodiFluoromethane 1.0 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919)733-3908 For a Wailed description of the Qualifier cooles refer tome1rcem.. nnu ealw.v.v nOua,_° o ro Page 1 of 5 NCOffQ La6oratorySection 9fsurts Location ID: 1P14HUFFMANMW2 Sample ID: Ae65230 Collect Date: 11/01/2010 Collect Time:: 10:24 VOL CAS # 74-87-3 Analvte Name Chloromethane PQL 0.50 ResulU Qualifier Not detected Units ug/L Method Reference EPA5030/624/8260 Analysis Date 11/3/10 Validated by ACHANDLER 75-01-4 Vinyl Chloride 0.60 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 74-83-9 Bromomethane 0.50 Not detected ug/L EPA5030/62418260 11/3110 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-69-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 75-35-4 1,1-Dlchloroethene 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 156-60.5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER 1634-044 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 75-34-3 1,1-Dichloroeth2ne 0.25 Not detected ug/L EPA5030/6241826D 1113/10 ACHANDLER 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8250 11/3/10 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 7143-2 Benzene 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 74-95.3 Dibromomethane 1.0 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 79-01-6 Trichloroethane 0.25 Not detected ug/L EPA5030162418260 1113/10 ACHANDLER 75-274 Bromodichloromethane 0.25 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 10061-01-5 cis-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 124-48-1 Dibromochloromethane 0.25 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.25 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 100-41-0 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-25-2 Bromofornl 1.0 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 108-38-3 m,p-Xylene 0.50 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 79-34-5 1, 1, 2,2-Tetrachl o roethane 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 630-20-6 1. 1, 1,2-Tetrachl oroethane 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 96-18-4 1,2,3-Trcchloropropane 0.25 Not detected ug/L EPA5030/62418260 1113110 ACHANDLER 98412-8 Isopropylbenzene 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER Laboratory Section>> 1623 Mail Service Center, Raleigh, INC 27699-1623 (919) 733-3908 Fore derailed dezenpnon come 4uareereddeawrertn Page 2 of 5 WC fDWQQ La6oratorySectron Y?Smfts TL:..tl.:I7D11`14HUFFMANMW2 Sample ID: AB65230 Collect Date: 11/01/2010 Collect Time:: 10:24 VOL Result/ Method Analysis CAS # Analvte Name POL Units validated by — Qualifier Reference Date 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA5030/62418260 1113110 ACHANDLER 95.49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 106-43-4 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/B260 1113/10 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 95-50-1 o-Dichlorobenzene(1,2) 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030162418260 11/3110 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 120412-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 81-20-3 Naphthalene 0.50 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030162418260 1113110 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER VOUS BY GUMS Not detected ug/L EPA5030162418260 11/3110 ACHANDLER SEM 7440-50-8 Semivolatile Organics (BNAs) in liquid _TITLE ug/L EPA625/8270/3510 1119110 NGOOD 62-53-3 Aniline 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 108.95-2 Phenol 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 11144-4 Bis(2-chloroethyl)ether 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 95-57-8 Chlorophenol, 2- 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 541-73-1 Dichlorobenzene, 1,3 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 106-46-7 Dichlorobenzene, 1,4- 10 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 100.51-6 Benzyl alcohol 20 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 95-50-1 Dichlorobenzene, 1,2- 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 95-48-7 Methylphenol, 2- 10 Not detected ug/L EPA6251827013510 11/9110 NGOOD 39638-32-9 Bis(2-chloroisopropyl)ether 10 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 106-44-5 Methylphenol, 4- 12 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 621-64-7 N-nitrosodi-n-propylamine 10 Not detected ug/L EPA625/827013510 1119110 NGOOD 67-72-1 Hexachloroethane 10 Not detected ug/L EPAS25/8270/3510 1119110 NGOOD 98.95.3 Nitrobenzene 10 Not detected ug/L EPA625/827013510 11/9H0 NGOOD 78-59-1 Isophorone 10 Not detected ug/L EPA625/827013510 11/9/10 NGOOD 88-75-5 Nitrophen01, 2- 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 105-67-9 Dimethylphenol, 2,4- 12 Not detected ug/L EPA6251827013510 11/9110 NGOOD 65-85-0 Benzoic acid 50 Not detected ug/L EPA6251827013510 11/9110 NGOOD 111-91-1 Bis(2-chloroethoxy)methane 10 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 120-83-2 Dichlorophenol, 2,4- 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 120-82-1 Trichlorobenzene, 1,2,4- 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 91-20-3 Naphthalene(SV) 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 73M908 Foredt.lted des.gptlon d 1h. qualifier codes refer lam, . nn nF m. an a,in, cm. 11i,,.. yaLn,^1r^3d naesiro Page 3 of 5 XC /D`VQ La6oratory Section 9?fm1ts Location ID: 1P14HUFFMANMW2 Sample ID: AS65230 Collect Dale: 11/OV2010 Collect Time:: 10:24 CAS # 106-47-8 Analvte Name Chloroanillne, 4- PQL 20 ResulU Qualifier Not detected Units ug/L Method Reference EPA6251827013510 Analysis Date 11/9/10 Validated by NGOOD 87-68-3 Hexachlorobutadlene(SV) 10 Not detected ug/L EPA625/827013510 1119110 NGOOD 59-50-7 Chloro-3-methyl phenol, 4- 20 Not detected ug/L EPA6251827013510 11/9110 NGOOD 91-57-6 Methylnaphthalene, 2- 10 Not detected ug/L EPA625/8270/3510 1119/10 WOOD 7747-4 Hexachlorocyclopentadiene 12 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 88-06-2 Trichlorophenol, 2,4,6- 10 Not detected ug/L EPA625/827013510 11/9110 NGOOD 95-95-4 Trichlorophenol, 2,4,5- 12 Not detected ug1L EPA625/8270/3510 1119110 NGOOD 91-58-7 Chloronaphthalene, 2- 10 Not detected ug/L EPA625/827013510 11/9/10 NGOOD 88-74-4 Nitroaniline, 2- 50 Not detected ug/L EPA62518270/3510 lV9/10 WOOD 131-11-3 Dimethyl phthalate 10 Not detected ug/L EPA62518270/3510 1119110 NGOOD 208-96-8 Acenaphthylene 10 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 606-20-2 Dinitrotoluene, 2,6- 10 Not detected ug/L EPA6251827013510 1119/10 NGOOD 99-09-2 Nitroaniline, 3- 50 Not detected ug/L EPA6251827013510 11/9/10 NGOOD 83-32-9 Acenaphthene 10 Not detected ug/L EPA625/827013510 11/9110 NGOOD 51-28-5 Dinitrophenol, 2,4- 50 Not detected ug/L EPA6251827013510 1119/10 NGOOD 100-02-7 Nitrophenol, 4- 50 Not detected ug/L EPA625/827013510 11/9/10 NGOOD 132-64-9 Dibenzofuran 10 Not detected ug/L EPA62518270/3510 11/9110 NGOOD 121-14-2 Dinitrotoluene, 2,4- 10 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 84-66-2 Diethyl phthalate 10 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 7005-72-3 Chlorophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 86-73-7 Fluorene 10 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 100-01-6 Nitroaniline, 4- 50 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 534-52-1 Dinitro-2-methyl phenol, 4,6- 50 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 86-30-6 N-nitrosodiphenylamine 10 Not detected ug/L EPA62518270/3510 1119/10 NGOOD 101-55-3 Bromophenyl phenyl ether, 4- 10 Not detected ug/L EPA62518270/3510 11/9110 NGOOD 118-74-1 Hexachlorobenzene 10 Not detected ug/L EPA6251827013510 11/9/10 NGOOD 87-86-5 Pentachlorophenol 50 Not detected ug/L EPA625/827013510 1119110 NGOOD 85-01-8 Phenanthrene 10 Not detected ug/L EPA625/8270/3510 11/9110 WOOD 120-12-7 Anthracene 10 Not detected ug/L EPA625/5270/3510 11/9110 NGOOD 84-74-2 Di-n-butyl phthalate 10 Not detected ug/L EPA625/827013510 11/9/10 NGOOD 206-44-0 Fluoranthene 10 Not detected ug/L EPA625/827013510 1119/10 WOOD 129-00-0 Pyrene 10 Not detected ug/L EPA62518270/3510 1119110 NGOOD 85-68-7 Butylbenzyl phthalate 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 91-94-1 Dichlorobenzidine, 3,3'- 15 Not detected ug/L EPA625/827013510 11/9110 NGOOD 56-55-3 Benzo(a)anthracene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 218-01-9 Chrysene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 117-81-7 Bis(2-ethylhexyl)phthalate 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 117-84-0 Di-n-octyl phthalate 10 Not detected ug/L EPA625/827013510 1119/10 NGOOD 205-99-2 Benzo(b)fluoranthene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 207-08-9 Benzo(k)fluoranthene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 50-32-8 Benzo(a)pyrene 10 Not detected ug/L EPA625/8270/351D 1119/10 WOOD 193-39-5 Indeno(1,2,3-cd)pyrene 12 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fatad.Wkd deeedpil.n oItha qu tf.... dee reWt. It,,, 11t-,,11 tten .ror.en.errtemierro , Page 4 of 5 NC rD'WQ La6oratory Section 9Z s=Its Location ID: 1P14HLJFFMANMW2 Sample ID: A666230 Collect Date: 11101/2010 Colleclrme:: 10:24 Result/Units Method Analysis CAS # Analvte Name PQL validated by Qualifier Reference Date 53-70-3 Dibenzo(a,h)anthracene 12 Not detected ug/L EPA625/6270/3510 11/9/10 NGOOD 191-24-2 Benzo(g,h,i)perylene 12 Not detected ug/L EPA62518270/3510 11/9110 NGOOD No BN/As detected by GC/MS. Not detected ug/L EPA625/8270/3510 11/9110 NGOOD Sample Comments phthalate detected at (7.0 UG/L) below semivolatiles PQL. PC Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3906 Foradetaded dez ption olthe 9ualifermdea relerla nn z.nM n. oa:r�a uan..:v .cousin. c:_<m11 --' nnr. Page 5 of 5 County: CALDWELL Sample to: AB65256 River Basin WATFg4 PO Number# ARO Report To �OF Gy Date Received: AROAP �O r= r Time Received: 11102/2010 09:00 , Collector. B LAVERTY O Y LebWorks LoginlD KJIMISON Region: ARO Report Generated: 11129/10 Sample Mahlx: GROUNDWATER D ate Reported: 12/28/2011 Loc. Type: MONITORING WELL Emergency Yes/No VisillD COC Yes/No Loc. Descr.: HUFFMAN FINISHING Location ID: 1P14HUFFMANMW2 Collect Date: 11/01/2010 Collect Time: 10:24 Sample Depth CAS At Analvte Name PQL ResulU Units Method Analysis Validated by ualifier Reference Date Others Sample temperature at receipt by lab 4.6 C 11/2110 SMATHIS Turbidity 1 45 NTU APHA21308-20th 1113110 CGREEN Residue —Suspended In liquid 6.2 66 mg/L APHA254OD-20th 11/8/10 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NO 27699-1623 (919) 7334908 For a detailed desorption of the qualifier codes refer to ht, 11 mml a,a.ae ner. hr.m Page 1 of 1 County: CALDWELL Sample ID: AB65231 River Basin �OF PO Number# 10GO803 Report To AROAP �O T 65 r > -y Date Received: Time Received: 11/03/2010 08:10 Collector. B LAVERTY O Y Labworks LoghID SMATHIS Region: ARO Report Generated: 1/5111 Sample Matrix: GROUNDWATER Date Reported: 12/2812011 Loc. Type: MONITORING WELL Emergency Yes/No VisitlD CDC Yes/NO Loc. Descr.: HUFFMAN FINISHING Location ID: 1P14HUFFMANMW3 Collect Date: 11/0112010 Collect Time: 10:50 Sample Depth CAS # LAB Analvte Name Sample temperature at receipt by lab POL Result/Units Qualifier 2.1 °C Method Reference Analysis Date 1113110 Validated by SMATHIS WET Chemical Oxygen Demand in liquid 20 20 U mg/L Hach 8000 11/22/10 CGREEN Ion Chromatography _TITLE_ mg/L EPA 300.0 1119110 CGREEN Chloride 1.0 2.8 mg/L EPA300.0 11/9/10 CGREEN Fluoride 0.4 0.4 U mg/L EPA300.0 1119110 CGREEN Sulfate 2.0 9.1 mg/L EPA 300.0 11/9/10 CGREEN NUT NH3 as N in liquid 0.02 0.02 U ni as N Lacl O-107-06-1J 1113110 CGREEN NO2+NO3 as N in liquid 0.02 1.8 mg/Las N Lac10-107-04-1-c 1113/10 CGREEN Phosphorus -total as P in liquid 0.02 0.16 mg/L as P L8c10-115-01-1 EF 1114/10 CGREEN Nitrate as N in liquid 0.02 1.8 mg/L as N Lachal107-04-1-c 1115110 CGREEN Nitrite as N in liquid 0.01 0.01 U mg/Las N Lachat107-04-1-c 11/3/10 CGREEN MET 7429-90-5 Al by ICP 50 2700 ug/L EPA 200.7 11/10/10 ESTAFFORDI 7440-38-2 As by ICPMS 2.0 2.0 U ug/L EPA200.8 11/9110 ESTAFFORDI 7440-38-3 Be by ICP 10 35 ug/L EPA200.7 1119110 ESTAFFORDI 7440-43-9 Cd by ICPMS 1.0 1.0 U ug/L EPA200.8 11/9/10 ESTAFFORD1 7440-47-3 Cr by ICPMS 10 10 ug/L EPA200.8 1119/10 ESTAFFORDI 7440-50-8 Cu by ICPMS 2.0 3.2 ug/L EPA 200.8 11/9110 ESTAFFORD1 7439-89-6 Fe by ICP 50 2400 ug/L EPA 200.7 11/10/10 ESTAFFORDI 7439-97-6 Hg 245.1 0.2 0.20 U ug/L EPA 245.1 1119/10 ESTAFFORDI 7439-95-4 Mg by ICP 0.10 1.7 mg/L EPA 200.7 11/9/10 ESTAFFORDI 7439-96-5 Mn by ICP 10 17 ug/L EPA 200.7 11/10/10 ESTAFFORDI 7440-23-5 Na by ICP 0.10 12 mg/L EPA 200.7 1119110 ESTAFFORDI 7440-02-0 Ni by ICPMS 10 IOU ug/L EPA200.8 1119/10 ESTAFFORDI 7439-92-1 Pb by ICPMS 10 IOU ug/L ERA200.8 11/9/10 ESTAFFORDI 778249-2 Se by ICPMS 5.0 5.0 U ug/L EPA 200.8 1119110 ESTAFFORDI 7440-66-6 Zn by ICPMS 10 12 ug/L EPA200.8 1119110 ESTAFFORDI VOL 120-82-1 Volatile Organics in liquid _TITLE ug/L EPA5030162418260 1113110 ACHANDLER 75-71-8 DichlorodlOuoromethane 1.0 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For a detailed description of thequalher coda retell. Me lLCNtasP.e_oorslnnary/e e3 �n(L^SL...... m o nlil"cmovm orcn eeen...r°b olat mew Page 1 of 5 NCQ)Uq LaboratorySection /R? urts Location ID: 1P14HUFFMANMW3 Sample ID: AB65231 Collect Date: 11/01/2010 Collect Time:: 10:60 VOL CAS At 74-87-3 Analvte Name Chloromethane PQL 0.50 Result/Units Qualifier Not detected ug/L Method Reference EPA5030/624/B260 Analysis Date 11/3/10 Validated by ACHANDLER 75-014 Vinyl Chloride 0.50 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 74-83-9 Bromomethane 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 75-59-4 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 itf3/10 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/62418260 11/3110 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 155-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 107-08-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 71-55-6 1, 1,1-Trichloroethane 0.25 Not detected ug/L EPA5030162418260 11/3110 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 7143-2 Benzene 0.25 Not detected ug/L EPA5030/624IB260 11/3/10 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/624/B260 11/3110 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 79-01-6 Trichooroethene 0.25 Not detected ug/L EPA5D30/624/8260 1'1/3/10 ACHANDLER 75-27-4 Bromodichloromethane 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 10051-01-5 Cis-1,3-Dichloropropene 0.25 Not detected uglL EPA5030162418260 11/3110 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 108-88-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA5030/62418260 1113110 ACHANDLER 124-48-1 Dibromochloromelhane 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.25 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER 127-18-4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 10D-414 Ethylbenzene 0.25 Not detected ug/L EPA5030162418260 1113110 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 108-38-3 m,p-Xylene 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624IB260 11/3/10 ACHANDLER 79-34-5 1, 1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 630-20-6 1, 1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624IB260 1113110 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected uglL EPA50301624/8260 11/3/10 ACHANDLER 96-184 1,2,3-Tdchloropropane 0.25 Not detected ug/L EPA5030/524/8260 11/3/10 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed description of the qualifier codes relerto p}L[/roan nca•vntpJ> t AanY.c+P,no/•msn.+v.-ou.0-ccm-rv,e/-,I-d.n. e�p[y�n[;+ne...ga/+rsFa•s.:.. Page 2 of 5 NC /D'WQ La6oratory Section Wrsurts Location to: 1P14HUFFMANMW3 Sample ID: AB66231 Collect Date: 11/01/2010 Collect Time:: 10:50 VUL CAS # 103-65-1 Analvte Name n-Propylbenzene POL 0.25 Result/Method Qualifier Not detected Units ug/L Reference EPA5030/62418260 Analysis Date 11/3/10 validated by ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 106-434 4-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030162418260 11/3/10 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 95-50-1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030162416260 11/3/10 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030162418260 11/3/10 ACHANDLER VOC'S BY GC/MS Not detected ug/L EPA5030/624/8260 it/3/10 ACHANDLER BEM 7440-50-8 Semivolatile Organics (BNAs) in liquid _TITLE ug/L EPA62518270/3510 11/9/10 NGOOD 62-53-3 Aniline 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 108-95-2 Phenol 10 Not detected ug/L EPA6251827013510 11/9/10 NGOOD 11144-4 Bis(2-chloroethyl)ether 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 95-57-8 Chlorophenol, 2- 10 Not detected ug/L EPA62518270/3510 11/9110 NGOOD 541-73-1 Dichlorobenzene, 1,3 10 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 106-46-7 Dichlorobenzene, 1,4- 10 Not detected ug/L EPA625/8270/3510 11/9/10 WOOD 100-51-6 Benzyl alcohol 20 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 95-50-1 Dichlorobenzene, 1,2- 10 Not detected ug/L EPA625/8270/3510 11/9/10 WOOD 95-48-7 Methylphenol, 2- 10 Not detected ug/L EPA625/827013510 11/9110 NGOOD 39638-32-9 Bis(2-chloroisopropyl)ether 10 Not detected ug/L EPA62518270/3510 1119/10 NGOOD 1064A-5 Methylphenol, 4- 12 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 621-64-7 N-nitrosodl-n-propylamine 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 67-72-1 Hexachloroethane 10 Not detected ug/L EPA625/827013510 11/9/10 NGOOD 98-96-3 Nitrobenzene 10 Not detected ug/L EPA625/827013510 1119/10 NGOOD 78-59-1 Isophorone 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 88-75-5 Nitrophenol, 2- 10 Not detected ug/L EPA625/827013510 11/9110 NGOOD 105-67-9 Dimethylphenol, 2,4- 12 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 65-85-0 Benzoic acid 50 Not detected ug/L EPA62518270/3510 1119110 WOOD 111-91-1 Bis(2-chloroethoxy)methane 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 120-83-2 Dlchlorophenol, 2,4- 10 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 120-82-1 Trichlorobenzene, 1,2,4- 10 Not detected ug/L EPA6251827013510 1119110 NGOOD 91-20-3 Naphthalene(SV) 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 For adetailed description oftho,.afrermdo. relerto a wnanrnaa„ n. w.cx. 1e., .e naC Page 3 of 5 NC(DWQ La6oratory SectionRPsufts Location ID: 1P14HUFFMANMW3 Sample ID: AB66231 Collect Dale: 11/0112010 Collect Time:: 10:60 SEM CAS # — 106-47-8 Analyte Name Chloroaniline, 4- PQL 20 Result/ Qualifier Not detected Units ug/L Method Reference EPA625/8270/3510 Analysis Date 11/9/10 Validated by NGOOD 87-68-3 Hexachlorobutadiene(S7) 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 59-50-7 Chloro-3-methyl phenol, 4- 20 Not detected ug/L EPA62518270/3510 1119/10 NGOOD 91-57-6 Methylnaphthalene, 2- 10 Not detected ug/L EPA62518270/3510 1119/10 NGOOD 77-47-4 Hexachlorocyclopentadiene 12 Not detected ug/L EPA62518270/3510 1119110 NGOOD 88-06-2 Trichlorophenol, 2,4,6- 10 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 95-95-4 Trichlorophenol, 2,4,5- 12 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 91-58-7 Chloronaphthalene, 2- 10 Not detected ug/L EPA625/827013510 1119/10 NGOOD 88-74-4 Nitroaniline, 2- 50 Not detected ug/L EPA625/827013510 ii/9/10 NGOOD 131-11-3 Dimethyl phthalate 10 Not detected ug/L EPA625/8270/3510 1119110 NGOOD 208-96-8 Acenaphthylene 10 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 606-20-2 Dinitrotoluene, 2,6- 10 Not detected ug/L EPA625/827013510 1119110 NGOOD 99-09-2 Nitroaniline, 3- 50 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 83-32-9 Acenaphthene 10 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 51-28-5 Dinitrophenol, 2,4- 50 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 100-02-7 Nitrophenol, 4- 50 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 132-64-9 Dibenzofuran 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 121-14-2 Dinitrotoluene, 2,4- 10 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 84-66-2 Diethyl phthalate 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 7005-72-3 Chlorophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 86-73-7 Fluorene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 100-01-6 Nitroaniline, 4- 50 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 534-52-1 Dinitro-2-methyl phenol, 4,6- 50 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 86-30-6 N-nitrosodiphenylamine 10 Not detected ug/L EPA625/8270/3510 1119110 WOOD 101-55-3 Bromophenyl phenyl ether, 4- 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 118-74-1 Hexachlorobenzene 10 Not detected ug/L EPA62518270/3510 1119/10 NGOOD 87-86-5 Pentachlorophenol 50 Not detected ug/L EPA62518270/3510 1119110 NGOOD 85-01-8 Phenanthrene 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 120-72-7 Anthracene 10 Not detected ug/L EPA625/827013510 11/9/10 WOOD 84-74-2 Di-n-butyl phthalate 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 206-44-0 Fluoranthene 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 129-00-0 Pyrene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 85-68-7 Butylbenzyl phthalate 10 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD 91-94-1 Dichlorobenzidine, 3,3'- 15 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 56-55-3 Benzo(a)anthracene 10 Not detected ug/L EPA625/8270/3510 1119/10 NGOOD 218-01-9 Chrysene 10 Not detected ug/L EPA625/827013510 1119/10 NGOOD 117-81-7 Bis(2-ethylhexyl)phthalate 10 120 ug/L EPA625/8270/3510 1119110 NGOOD 117-84-0 Di-n-octyl phthalate 10 Not detected ug/L EPA62518270/3510 1119/10 NGOOD 205-99-2 Benzo(b)Fluoranthene 10 Not detected ug/L EPA62518270/3510 11/9/10 NGOOD 207-08-9 Benzo(k)Ruoranlhene 10 Not detected ug/L EPA625/827013510 11/9/10 NGOOD 50-32-8 Benzo(a)pyrene 10 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 193-39-5 Indeno(1,2,3-cd)pyrene 12 Not detected ug/L EPA625/8270/3510 11/9110 NGOOD Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora deWa d desuiption olthe qualifercodesre(erto n,.-rczi.zev,. +.... nar,+ttaeen rcrns:zv-.a an 1.11- m ... �-.. .+. qr+r.5.. rcn+.•. Page 4 of 5 NC,i Laboratory Section 4fgsu&s Location ID: 1P14HUFFMANMW3 Sample ID: AS65231 Collect Dale: 11101/2010 Collect Time:: 10:60 SEM CAS # Analvte Name Result/Units PQL Method Analysis validated by Qualifier Reference Date 53-70-3 Dibenzo(a,h)anthracene 12 Not detected ug/L EPA625/8270/3510 11/9/10 NGOOD 191-24-2 Benzo(g,h,i)perylene 12 Not detected ug/L EPA6251827013510 11/9/10 NGOOD Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed descdVUon ofale qualifier Cedes relerto .imp, Page 6 of 5 County: CALDWELL Sample ID: AB65257 River Basin pF WATF/1+ PO Number# ARO ReportTo AROAP O� QGy Date Received: 11/02/2010 r >_ Time Received: Collector. B LAVERTY y � < Labworks LoginlD KJIMI KJIMISON Region: ARO Report Generated: 11/2 10 Sample Matrix: GROUNDWATER Date Reported: 12l28//2011 Loc. Type: MONITORING WELL Emergency Yes/No VlsltlD COC Yes/No Loc. Descr.: HUFFMAN FINISHING Location ID: 1P14HUFFMANMW3 Collect Date: 11/0112010 Collect Time: 10:50 Sample Depth Result/ Method Analysis CAS # Analyte Name PQL Units validated by — Qualifier Reference Date Others Sample temperature at receipt by lab 4.6 °C 1112110 SMATHIS Turbidity 1 38 NTU APHA2130B-20th 11/3/10 CGREEN Residue —Suspended in liquid 6.2 33 mg/L APHA2540D-20th 11/6110 CGREEN Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3906 Fora deailed desodption afthe quati0eraodes mrerto �m'n.c Page 1 of 1 County: Sample ID: AB65229 River Basin OF `l`lAT6q PO Number# 10GO801 ReportTo O� �G AROAP r Dale Received: Time Received : 11103/2010 08:10 Collector: B LAVERTY O Y Labworks LoginlD SMATHIS Region: ARO Report Generated: 11/16/10 Sample Matrix: GROUNDWATER Date Reported: 12/28/2011 Loc. Type: TRIP BLANK Emergency Yes/No VsitlD CDC Yes/No Loc. Descr.: VOATRIP BLANK Location ID: AROAPNLC Collect Date: 1110V2010 Collect Time: 08:07 Sample Depth Result/Units Method Analysis CAS # Analvte Name POL Validated by Qualifier Reference Date LAB Sample temperature at receipt by lab 2.1 °C 1113/10 SMATHIS VOL Volatile Organics in liquid _TITLE ug/L EPA5030/62418260 1113110 ACHANDLER 75-71-8 Dichlorodifluoromethane 1.0 Not detected ug/L EPA5030/62418260 1113/10 ACHANDLER 74-87-3 Chloromethane 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-01-4 Vinyl Chloride 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 74-83-9 Bromomethane 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-00-3 Chloroethane 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-694 Trichlorofluoromethane 0.50 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 75-35-4 1,1-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-09-2 Methylene Chloride 10 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 156-60-5 trans-1,2-Dichloroethene 0.25 Not detected- ug/L EPA5030/624/8260 11/3110 ACHANDLER 1634-04-4 Methyl Tert-Butyl Ether 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-34-3 1,1-Dichloroethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 156-59-2 cis-1,2-Dichloroethene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 74-97-5 Bromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 67-66-3 Chloroform 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 594-20-7 2,2-Dichloropropane 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 107-06-2 1,2-Dichloroethane 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 71-55-6 1,1,1-Trichloroethane 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 563-58-6 1,1-Dichloropropene 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 56-23-5 Carbon Tetrachloride 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 71-43-2 Benzene 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 74-95-3 Dibromomethane 1.0 Not detected ug/L EPA5030/62418260 1113110 ACHANDLER 78-87-5 1,2-Dichloropropane 0.25 0.28 ug/L EPA5030/624/8260 11/3/10 ACHANDLER 79-01-6 Trichloroethene 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 75-27-4 Bromodlchloromethane 0.25 Not detected ug/L EPA5030/62418260 11/3110 ACHANDLER 10061-01-5 CIS-1,3-Dlchloropropene 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 10061-02-6 trans-1,3-Dichloropropene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 79-00-5 1,1,2-Trichloroethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 108-68-3 Toluene 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 142-28-9 1,3-Dichloropropane 0.25 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed deacdptien anhe quali0ereodea reart. tie, e..-.. Pagel of 2 5VC (D`WQ La6oratory Section Pssults Location ID: AROAPNLC Sample ID: AB65229 Collect Date: 1110112010 Collect Time:: 08:07 VOL Result/Units Method Analysis CAS # Analyte Name PQL Validated by Qualifier Reference Date 124-48-1 Dibromochloromethane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 106-93-4 (EDB)1,2-Dibromoethane 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 127-18.4 Tetrachloroethene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 108-90-7 Chlorobenzene 0.25 Not detected ug/L EPA50301624/8260 11/3/10 ACHANDLER 100-41-4 Ethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 75-25-2 Bromoform 1.0 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 108-38-3 m,p-Xylene 0.50 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 100-42-5 Styrene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 79-34-5 1, 1,2,2-Tetrachloroethane 0.25 Not detected ug/L EPA50301624/8260 1113110 ACHANDLER 630-20-6 1,1,1,2-Tetrachloroethane 0.25 Not detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 95-47-6 o-Xylene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER s6-1s-4 1,2,3-Trichloropropane 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 98-82-8 Isopropylbenzene 0.25 Net detected ug/L EPA5030/624/8260 1113/10 ACHANDLER 108-86-1 Bromobenzene 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 103-65-1 n-Propylbenzene 0.25 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 95-49-8 2-Chlorotoluene 0.25 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 106-434 4-Chlorotoluene 0.25 Not detected ug/L EPA50301624/8260 1113/10 ACHANDLER 108-67-8 1,3,5-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 98-06-6 tert-Butylbenzene 0.25 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 95-63-6 1,2,4-Trimethylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 135-98-8 sec-Butylbenzene 0.25 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 541-73-1 m-Dichlorobenzene (1,3) 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 106-46-7 p-Dichlorobenzene (1,4) 0.25 Not detected ug/L EPA5030/62418260 11/3110 ACHANDLER 95-50.1 o-Dichlorobenzene (1,2) 0.25 Not detected ug/L EPA5030/624/8260 1113110 ACHANDLER 99-87-6 p-Isopropyltoluene 0.25 Not detected ug/L EPA5030/62418260 11/3110 ACHANDLER 104-51-8 n-Butylbenzene 0.25 Not detected ug/L EPA5030/624/8260 11/3/10 ACHANDLER 96-12-8 1,2-Dibromo-3-Chloropropane 2.0 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 120-82-1 1,2,4-Trichlorobenzene 0.50 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER 91-20-3 Naphthalene 0.50 Not detected ug/L EPA50301624/8260 11/3110 ACHANDLER 87-68-3 Hexachlorobutadiene 0.50 Not detected ug/L EPA5030/624/8260 11/3110 ACHANDLER 87-61-6 1,2,3-Trichlorobenzene 1.0 Not detected ug/L EPA5030/62418260 11/3/10 ACHANDLER Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Fora detailed description ofthe Quadfercodn referto Page 2 of 2 WASTEWATER TREATMENT PLANT MONITORING WELL INSTALLATION REPORT PERFORMED BY ENGINEERING AND ENVIRONMENTAL SERVICES 419 SECOND STREET, NW - HICKORY, NC 28601 P O BOX 3009 - HICKORY, NC 28603 (704) 328-2991 (704) 322-2268 FAX APR 2 0199Z J II I� FOR HUFFMAN FINISHING GRANITE FALLS, NORTH CAROLINA WASTEWATER TREATMENT PLANT MONITORING WELL INSTALLATION REPORT APRIL 3, 1992 INTRODUCTION This document, prepared by Engineering and Environmental Services (EES), contains information relating to the installation of two monitoring wells at the wastewater treatment facility of Huffman Finishing Plant, Granite Falls, North Carolina. These wells were installed to monitor the quality of the groundwater upgradient and downgradient of the wastewater treatment plant. MW-2 was installed upgradient of the plant and MW-3 was installed downgradient of the plant. One additional monitoring well unrelated to the wastewater treatment plant, MW-1 was installed on the same day. The water elevations in the three wells were used to calculate the flow direction indicated on Drawing Number 91- 075-0005. 11. 2,5 / . Av, t - of -lAe u.5 t MONITORING WELL INSTALLATIONS Monitoring well MW-2 was installed to a depth of 29 feet. A 10 foot section of .010 inch slotted 2 inch diameter PVC tubing was placed in the bottom of the well with 2 inch diameter solid PVC casing completing the installation to the top of the well. Graded filtration sand was placed around the slotted section to an elevation 2 feet above the top of the slotted section. Two feet of bentonite was poured on top of the sand and hydrated. The balance of the boring was filled with cement and grouted around the lockable casing. A 2 foot by 2 foot cement base was set around the casing of the well and a well identification tag was attached. A column of water of 14 feet - 2 inches was measured after development and recovery of the well. The top of the screen was therefore 4 feet - 10 inches below the surface of the water table. The water level in MW-2 was measured to be 7.181 feet above the measured water level in monitoring well MW-3 which was found to exhibit the lowest final water level of the wells installed. The soil throughout the boring was noted to be a weathered saprolite. Monitoring well MW-3 was installed to a depth of 15 feet - 2 inches. A 10 foot section of .010 inch slotted 2 inch diameter PVC tubing was placed in the bottom of the well with 2 inch diameter solid PVC casing completing the installation to the top of the well. Graded filtration sand was placed around the slotted section to an elevation 2 feet above the top of the slotted section. Two feet of bentonite was poured on top of the sand and hydrated. The balance of the boring was filled with cement and grouted around the lockable casing. A 2 foot by 2 foot cement base was set around the casing of the well and a well identification tag was attached. A column of water of 2 feet - 9 inches was measured after development and recovery of the well. The top of the screen was therefore 7 feet - 3 inches above the surface of the water table. The water level in MW-3 was set at 0 feet since it was found to exhibit the lowest final water level of the wells installed. -1- The soil to the depth of 14 feet was noted to be a weathered saprolite. Rock was encountered at an approximate depth of 14 feet and continued to the final depth. Well locations are indicated on Drawing No. 91-075-0005 and analytical results are summarized in a following section and included in the Appendix along with completed Chains of Custody. ANALYTICAL RESULTS Monitoring wells MW-2 and MW-3 were developed, allowed to recover, and sampled. The samples were analyzed according to the requirements of the North Carolina Department of Environment Health and Natural Resources (NCDEHNR), Asheville, North Carolina. These results are summarized in the table below. Parameter MW-2 MW-3 MOL* COD 80 320 mg/l 1 mg/l TOC 6.79 26.1 mg/1 10 mg/l NH3N BOL** BOL 5 mg/l Orthophosphate 08 10 mg/1 05 m9/1 NO3 111 62 mg/1 1 mg pH 5.26 5.58 su 01 su TDS BOL 485 mg/1 1 mg/l Cl BOL 270 mg/1 1 mg/1 SO4 37 103 m 1 m� As 001 003 mg/1 001 mg/l Cu 001 087 mg/1 001 mg/l Zn 02 04 mg/1 01 m14/1 Na 3.0 191.6 mg/1 1 mg/l TOX 014 094 mg/1 01 mg/l * Minimum Quantitation Limit ** Below Quantitation Limit -2- APPENDIX A -3- 7-tr6--jL1n(� WASTEWATER TREATMENT PLANT � BUILDING 0 50--•-�' BUILDING BUILDING BUILDING p s a N J ENGINEERING AND ENVIRONMENTAL SERVICES N PO BOX 3009 HICKORY, NC 28603 (704)3282991 HUFFMAN FINISHING, GRANITE FALLS, NORTH CAROLINA DATE SCALE APPROVAL 3/31/92 1"=120' RTB PLAN AND LOCATION DRAWING REV 0 DRAWING NO. 91-075-0004 'BUILDING EQUIPOTENTIAL I LINE - 23.27 FEET FOR ANALYTICAL RESULTS ON MW-2 SAMPLES SEE SAMPLE NUMBER MW2 91075-2-21-92-002 RESULTS ON ATTACHED ANALYTICAL G GROUNDWATER DIRECTION CALCULATED FROM WATER TABLE LEVELS IN MW-1, MW-2, AND MW-3. TREATMENT PLANT EQUIPOTENTIAL LINE - 7.181 FEET DIRECTION OF GROUNDWATER FLOW EQUIPOTENTIAL LINE - 0 FEETT FOR ANALYTICAL RESULTS ON MW-3 MW3 SAMPLES SEE SAMPLE NUMBER 91075-2-21-92.003 RESULTS ON ATTACHED ANALYTICAL ENGINEERING AND ENVIRONMENTAL SERVICES PO BOX 3009 HICKORY, NC 28603 (704)3282991 HUFFMAN FINISHING COMPANY GRANITE FALLS, NORTH CAROLINA I3//31/ 2 DATE I1'C250'I ARTBOVAL I MWWASTEWATER L CATIONSMONITORING WELLS I REV 0 DRAWINGNO. 91-075.0005 7 1 MILE 4000 5000 6000 7000 FEET 1 KILOMETER 20 FEET LEVEL ,P ACCURACY STANDARDS Y, WASHINGTON, D. C. 20242 YMBOLS IS AVAILABLE ON REOUEST N.C. 7 QUADRANGLE LOCATION ROAD CLASSIFICATION 9958"mN. 35*45' 22'30" o Primary highway, Light -duty road, hard or s''. F:o hard surface ...... improved surface tip% Secondary highway, hard surface ....... ....... _. Unimproved road...._===.e= (,Interstate Route OU. S. Route State Route GRANITE FALLS, N .0 N3545—W8122.5/7.5 1970 AMS 4755 IV SW -SERIES V842 PENT CAP - STEEL OUTER CASING - -* 21-0"X2'-0"X4" CONC SLAB o ANCHORING LUGS NEAT -CEMENT GROUT CENTERING(( GUIDE , GG SCHEDC40MINAA3TM 1785 ALL JOINTTT7TT9 SHALL BE FLUSH THREADED PELLETIZED BENTONITE CLEAN HASHED SAND OR GRAVEL CENTERING GUIDE HELL SCREEN 0.010 SLOTS PLUG - -- e 0 0 ° voo 00 Oo oe v 00 0000 ee oe o eo °, o 0o a 00 NOTE: i. BOREHOLE TO BE SIX INCHES LARGER THAN OUTSIDE DIAMETER OF CASING, 2. CASING AND SCREEN TO BE CENTERED IN BOREHOLE. 3. TOP OF WELL SCREEN MEANLHIGH SEASONAL. WATER LEVEL. 4• WELL HEAD TO BE LABELED WARNINGGSAYING: WELL ANDFNOTMCONS DERED SAFE FOR DRINKING." -7- 0 State of North_Carolina Department of Environment, Health, and Natural Resources Asheville Regional Office James G. Martin, Governor Ann B. Orr William W. Cobey, Jr., Secretary DIVISION OF ENVIRONMENTAL MANAGEMENT Regional Manager November 26, 1991 Mr. A. W. Huffman, Jr. Huffman Finishing Company - Post Office Box 170 Granite Falls, North Carolina 28630 Dear Mr. Huffman: Subject: Well Construction Permit No. 13-0110-WM-0060 Huffman Finishing Company Permit No. NCO025135 Sludge Holding Lagoon Caldwell County, North Carolina In accordance with your application received November 19, 1991, we are forwarding herewith Well Construction Permit No. 13-0110-WM-0060 dated November 26, 1991, issued to Huffman Finishing Company for the construction of two (2) monitor wells, or more as needed, at Huffman Finishing Company on Highway 321, Granite Falls in Caldwell County. If any parts, requirements, or limitations contained in this Permit are unacceptable to you, you have the right to an adjudicatory hearing before a hearing officer upon written demand to the Director within 30 days following receipt of this Permit, identifying the specific issues to be contended. Unless such demand is made, this Permit shall be final and binding. This Permit will be effective for the construction of monitor wells from the date of its issuance until the site assessment has been completed, and shall be subject to the conditions and limitations as specified therein. Attached are Well Construction Records to be completed and signed by the drilling contractor. These forms should be submitted to the Department upon completion of the wells. Sincerely, Roy Davis RMD/LKD/gc Regional Supervisor Attachments cc: Perry Nelson Carroll E. Baker In:crchangc Building, 59 Woodfin Place /+]hF:illa, N.C. 28801 • Tcicphone 704-251�6208 An Equal Opportunity Affirmarive 'Acrion Emplo'tr NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT, HEALTH, AND NATURAL RESOURCES ASHEVILLE, NORTH CAROLINA PERMIT FOR THE CONSTRUCTION OF A WELL OR WELL SYSTEM In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws, Rules and Regulations, PERMISSION IS HEREBY GRANTED TO HUFFMAN FINISHING COMPANY FOR THE CONSTRUCTION OF two (2) monitor wells, or more as needed, for Permit No. NC0025135 in the Residuum System of the Blue Ridge -Inner Piedmont Hydrogeologic Unit, located at Huffman Finishing Company on Highway U.S. 321, Granite Falls in Caldwell County, in accordance with the application dated October 4, 1991, and in conformity with specifications and supporting data, all of which are filed with the Department of Environment, Health, and Natural Resources and are considered a part of this Permit. This Permit is for well construction only, and does not waive any provisions or requirements of any other applicable laws or regulations. Construction of a well under this Permit shall be in compliance with the North Carolina Well Construction Regulations and Standards, and any other State and local laws and regulations pertaining to well construction. This Permit will be effective for the construction of monitor wells from the date of its issuance until the site assessment has been completed, and shall be subject to other specified conditions, limitations, or exceptions as follows: 1. The well driller shall notify the Asheville Regional Office prior to actual construction of the wells. Page 2 2. The wells shall be constructed with well casing and well screens that conform to requirements of the "Criteria and Standards Applicable to Water Supply and Certain Other Type Wells" (15A NCAC 2C .0100). 3. All wells shall be afforded reasonable protection against damage during construction and use. 4. The well screens shall be set of sufficient depth so there is water adequate for sampling during the seasonally low water table. 5. Provisions shall be made on the well covers to prevent surface water with possible contaminants from entering the well pits and contaminating the monitor wells. 6. Each well shall have permanently affixed an identification plate constructed of durable material and shall contain the following information: drilling contractor's name and registration number; date well completed; total depth of well; a warning that the well is not for water supply and that the groundwater may contain hazardous materials; and depth to screens. 7. Well completion, well abandonment, and water quality reports are to be submitted to the Division of Environmental Management's Groundwater Section Central Office in Raleigh. 8. When the wells have served their purpose and are of no further use, they shall be permanently abandoned according to the requirements of Section .0113 of the "Criteria and Standards Applicable To Water Supply and Certain Other Type Wells" (15A NCAC 2C). 9. If additional monitor wells, not shown on the location diagram, need to be constructed, a map showing the proposed location shall be submitted to the Asheville Regional Office. Permit issued this the 26th day of November. NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION Roy M. Davis, Regional Supervisor Division of Environmental Management By Authority of the Environmental Management Commission PERMIT NO. 13-0110-WM-0060 North Carolina - Department of Environment, Health, and Natural Resources Division of Environmental Management - Groundwater Section P.O. Box 29535 - Raleigh, N.C. 27626-0535 Phone (919) 733.3221 WELL CONSTRUCTION RECORD DRILLING CONTRACTOR: FOR OFFICE USE ONLY QUAD. NO. ,'7z SERIAL NO.. Lat. Long. . Minor Basin Basin code Header Ent GR Pc Ent STATE WELL CONSTRUCTION DRILLER REGISTRATION NUMBER: PERMIT NUMBER: 1. WELL LOCATION: (Show sketch of the location below) Nearest Town: County: (r7%/Glell (Road, Community, or Subdivision and Lot No.) DEPTH DRILLING LOG 2. OWNER �1(>C� �r ALlf&Ai ire. ('06H4&44 From To Formation Description ADDRESS T (Street or Route No.) Ce4ol Cr 7;VIj 1c::geh%-1 _ City or Town State Zip Code .SS.V7—A2/LGf".Z 3. DATE DRILLED USE OF WELL 4. TOTAL DEPTH 5. CUTTINGS COLLECTED YES ❑ NO❑ 6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO[:] 7. STATIC WATER LEVEL Below Top of Casing: FT. (Use'+' if Above Top of Casing) 8. TOP OF CASING IS FT. Above Land Surface` • Casing Terminated aVor below land surface Is Illegal unless a varlance Is Issued In accordance with 15A NCAC 2C .0118 9. YIELD (gpm): METHOD OF TEST 10. WATER ZONES (depth): 11. CHLORINATION: Type Amount If additional space is needed use back of form 12. CASING: Wall Thickness LOCATION SKETCH Depth Diameter or Weight/Ft. Material (Show direction and distance from at least two Slate From —To —Ft.— Roads, or other map reference points) From To Ft. From To Ft. 13. GROUT: Depth Material Method From —To—Ft.— From To Ft. 14. SCREEN: Depth Diameter Slot Size Material From To Ft in. in. From To Ft. in. in. From To Ft._ in. in. 15. SAND/GRAVEL PACK: Depth Size Material From To Ft. From To Ft. 16. REMARKS: Ai %nn,Ak*olP e,: tt 4, 'fi " ,7A 7_4 LZ,4— I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER SIGNATURE OF CONTRACTOR OR AGENT DATE GW-1 REV. 5r91 Submit original to Division of Environmental Management and copy to well owner. CLIENT: Engineering and Enair0mirnental Services E.L. Bo:; 3009 Attention: Mr. R. Fannister- DATE RECEIVED: February 21.. 1992 DATE REPORTED: March 12, 1992 DATE REISSUED: April 2, 1992** DATE REISSUED: April 13, 1992*** SAMPLE NUMBER SAMPLE DESCRIPTION 202-0301A Water' 91075-2-21-92-002 for COD. 202-0301 B Water; 91075-2-21-92-002 for TLC. 202-0301C Water; 91075-2-21-92-002 forNH3N. 202-0301D Water, 9 1075-2-2 1-92-002 for Orthophosphate. 202-0301E Water; 91075-2-21-92-002 for NO_. 202-0301 F Water; 91075-2-21-92-002 for pH & TDS. 202-03016 Water; 91075-2-21-92-002 for C1. 202-0301 H Water; 91075-2-21-92-002 for SO a. 202-03011 Water; 91075-2-21-92-002 for As, Cu, Zn, Na.. 202-0301J 'Hater, 91075-2-21-92-002 forTO1. PARAMETER RESULTS MQL DATE STARTED 202-0301A - COD 80 1 mg/l 2/21/92 202-0301 B - TOC 6.79 0.10 mg/1 3/6/92 202-0301 C - NH-N * 0.50 rng/I 2/26/92 * Concentrations are below Minimum Quantification Limit exceptwhere noted. HC Laboratory Certificate No_ 275_ PARAMETER RESULTS MQL DATE STARTED 202-03011) - Orthophosphate 0.08 0.05 mgil 2/21192 202-0301 E - NO3 i . i 1 0.10 rng/l 2'21 /92 202-0301 F - pH 5.26 0.01 su 2!21 t'92 - TDS " 1 mg/l 2/20I92 202-0301G - C1 0.1 mgil 2/27/92 202-0301 H - SO4 37 i rng/l 2/27/92 202-03011 - As 0.001 0.001 rngfl 2f2119.2 - Cu 0.001 0.001 rngll 2121 /92 - L,n 0.02 0.01 mg/l 2/21 J92 - Na 3.0 0.1 MQ/1 2/21 /92 202-030IJ - TOX 0.014 0.010 mg/]** 310/92 '* NOTE: Reissued due to typographical error for TOX NQL value. *x NOTE: Reissued due to typographical error for Date Started on NO3 x pH. REPORTED BY: D_ R. WessiAer — General Manager `Concentrations are below Minimum Quantification Limit except where noted. MC Laboratory Certificate No_ Z75_ CLIENT: Engineering and Environmental Services P.O. Box 3009 Hickory, N.C. 28603 !otAl-3 Attention: Mr, R. Bannister DATE RECEIVED: February 21, 1992 DATE REPORTED: March 12, 1992 DATE REISSUED: April 2, 1992 ** SAMPLE NUMBER SAMPLE DESCRIPTION 202-0302A Water,- 91075-2-2 1-92-003 for COD. 202-0302B Water; 91075-2-21-92-003 for TOC. 202-0302C Water; 91075-2-21-92-003 for NH..N. 202-05022D Water; 91075-2-21-92-003 for Orthophosphate. 202-0302E Water; 91075-2-21-92-003 for NO., 202-0302F Water; 91075-2-21-92-003 for pH & TDS. 202-0302G Water, 91075-2-21-92-003 for Cl. 202-0302H Water, 91075-2-21-92-003 for SO4. 202-03021 Water; 91075-2-2f-92-003 for As, Cu, Zn, No.. 202-0302J Water; 91075-2-21-92-003 for T OX. PARAMETER RESULTS MQL DATE STARTED 202-0302A - COD 320 1 mg!1 3!2!92 202-0302B - TOC 26.1 0.10 mg/l 3/6/92 202-0302C - NH_Pl 0.50 mgh 2i'25192 Concentrations are below Mini mum Quantification Limit except where note]. NC Laboratorg Certificate No_ Z75. -14- PARAMETER RESULTS MQL DATE STARTED 202-0302D - Orthophosphate 0.10 0.05 , mg,r, 2i2 ; �, 92 , 202-0302E - NO3 0.1 2 0.10 Mg/I 2/26/92 202-0302F - pH 5.58 0.01 su 2/21 /92 - TDS 4,55 I mg/1 2/23/92 202-03026 - Ci 270 0.1 mg/1 2/27/92 202-0302H - SO4 103 1 rng/1 2/27/92 202-03021 - As 0.003 0.001 mq/1 2/2 i i'y2 - Cu 0.O87 0.001 mg/l 2/21 /92 - Zn U.04 0.01 mg/l 2/21 /92 - No 191.6 0.1 mG/i 2/21 /92 202-03021 - TOX 0.094 0.010 mg/1** 3/6/92 }* NOTE: Reissued due to topographical error for TOO, MQL value. REPORTED BY: /C D. R. Wessi r - General Manager Concert rations are below Minimum Quantification Limit except where noted. HC Laboratory Certificate Ho- 275_ -15- Page / of ENGINEERING AND ENVIRONMENTAL SERVICES P O BOX 3009 HICKORY, NC 28603 (704) 328-2991 FAX (704) 322-2268 - CHAIN OF CUSTODY PO# �-�--/oa $ DATE LAB RECEIVING SAMPLE #_ SAMPLE # DESCRIPTION _� buw,4vA-k-r DESCRIPTION LOCATION 1,Vwl — c957— DATE d a/-9a 'I'I M E PROCESS- Z-lez, Goo PRESERVATIVE SAMPLED BY •i�Ll SAMPLE #9/o7s,2-Z/ FL -ooZ DESCRIPTION �R6v.vdeu4-1'-C LOCATION Tz,rL— ijoe, co;F,✓� DATE .221--9L TIME PROCESS/ve 3 z>s rdc ,45 cu so¢ U4 PRESERVATIVE SAMPLED BY 51'lc! L #)N nJ c?-PHs. Fly-lE SAMPLE # 9/a75 �Zi_yL_oo 3 DESCRIPTION LOCATION 4-w3 -bcx-u j2ta,, ;c,�,L DATE Z-2/_4z. TIME PROCESS.Ab� ns,roc_ Asc�r,o�,v- PRESERVATIVE F/k//,Erc mob l SAMPLED BYS-S,,,rtu TOK, zJ o•-Fuo��u� r.+� LOCATION DATE PROCESS PRESERVATIVE SAMPLED BY SAMPLE # DESCRIPTION LOCATION DATE PROCESS PRESERVATIVE SAMPLED BY SAMPLE #_ DESCRIPTION LOCATION DATE PROCESS PRESERVATIVE SAMPLED BY 'I'IME TIME TIME -16- State of North Catplina Department of Fnvironment, Health, and Natural Resources Mooresville Regional Office I:uncs C;. t 1:u'tin, {,ovcrnor Albert F. Hilton, Regional Manager lY., am W. (:nbi:v, It., .`ir•crctary DIVISION OF ENVIRONMENTAL MANAGEMENT July 25, 1990 Mr. A.W. Iiuffman, Jr. Huffman Finishing Company Lost Office Pox 170 Granite Falls, North Carolina 28630 Subject: Well Construction Permit No. 13-0110-WM-0037 Caldwell County, N.C- Dear Mr. Huffman: 7n accordance with your application received July 16, 1990, we are forwarding herewith Well Construction Permit No. 13-0110--WM-0037 dated July 25, 1990 issued to Huffman Finishing Company for the construction of two (2) monitor wells. This Permit will be effective from the date of issuance and shall be subject to the conditions and limitations as specified therein. Sincerely, 1I Brenda J. Smith, P.G. Regional Supervisor Enclosure cc: Groundwater Section Mr. Jack R. Moore, The Wooten Company JWW/pl 'i"' i•MgW iNISK Su -1 hhxnr.o-ak Fir 2ws •'Ii•Icphn, y" OB IMP" 1AX 7(}b/i/mmit0 Aar. {4pn! ! Ii.w �i lUu iv Afiir m:aiac h tj,wi finiplor�r CALDWELL COUNTY HUFFMAN FINISHING UNNAMED TRIBUTARY TO CATAWBA RIVER HICKORY & LONGVI EW U. S. 64 70,32 CATAWBA COUNTY LOCATION MAP AriM