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NCG140382_2020 DMR_20210105
ANNUAL SUMMARY DISCHARGE MONITORING REPORT (DMR) — STORMWATER SUBMIT TO CENTRAL OFFICE* General Permit No. NCG140000 Calendar Year 2020 *Report ALL STORMWATER monitoring data on this form (include "No FloWT'No Discharge" and Benchmark Exceedances) from the previous calendar year to the DEQ by MARCH 1 of each year. Certificate of Coverage No. NCG14 0� 1K] 20 Facility Name: Carolina Ready Mix and Builders Supply, LLC County: Buncombe Phone Number: (828 686-3040 Certified Laboratory Pace Analytical Lab # 40 Lab # Total no. of SDOs monitored 1 Stormwater Discharge Outfall (SDO) No. 001 VMA OutfalI? Yes ❑ No ❑✓ Is this outfall currently in Tier 2 for any parameter? Yes ❑ No ✓❑ Was this outfall ever in Tier 2 during the past year? Yes ❑ No Q✓ If this outfall was in Tier 2 last year, was monthly monitoring discontinued? Yes, enough consecutive samples below benchmarks to decrease frequency ❑ Yes, received approval from DEMLR to reduce monitoring frequency ❑ Other ❑ Outfall No. Total Rainfall, inches Total Suspended Solids (TSS), m /1 pH, SU Non -polar O&G (EPA Method 1664 ( SGT-HEM)) , mg/I (VMA) If applicable New Motor Oil Usage (gal/mo.) Ifapplicable Stormwater Benchmarks Date Sample Collected, mo/dd/yr Indicate NO FLOW if applicable 2.00 Circle Benchmark 100/50 31.7 6.0-9.0 7.8 15 N/A >55 gallmo. average requires TSS and Non polar 0&G monitoring N/A 05/18/20 11/11/20 1.50 31.7 8.6 ND ND Permit Date 8/1/2017 — 6/30/2022 Last Revised 8-22-2015 Certificate of Coverage No. NCG14 l 30®2❑ CERTIFICATION "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." [Required by 40 CFR §122.22] Signature Date 01 /05/2021 Mail Annual Summary Stormwater DMR to the NCDEQ Central Office: Note the address is correct - Central Files is housed in DWR (not DEMLR) N.C. Department of Environmental Quality (DEQ) Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files Telephone (919) 807-6300 Questions? Contact DEMLR Stormwater Permitting Staff in the Central Office at: (919) 707-9220 Permit Date 8/1/2017 — 6/30/2022 Last Revised 8-22-2015 NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG140000 Ready -Mixed Concrete Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG14 0 3 8 2 Person Collecting Samples: Gary Kilker Facility Name: Carolina Ready Mix and Builders Supply LLC Laboratory Name: Pace Analytical Facility County: Buncombe Laboratory Cert. No.: 40 Discharge during this period: 0■ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? 0 Yes ❑ No If so, which Tier (I, II, or III)? parr n• analvriral Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter %'Parameter Outfall Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class Class C N/A Date Sample Collected MM/DD/YYYY 05/18/20 46529 24-Hour Rainfall in inches 2.00 C0530 TSS in mg/L (100 or 50*) 31.7 00400 pH in standard units (6.0 — 9.0) 7.8 Non -Polar Oil & Grease in 00552 mg/L (15) for drainage areas that use > 55 gal/mo of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 01 /05/21 Signature of V rmittee or Delegated Authorized Individual Date L-ii 0 LL z_ w 0 F— z 0 G C Q .E V / i 0 in Ln J 0 W Q V tO v ) Z FC_ C W a J Q W Z W Q +,. Ll J cr w❑ LU ❑g O EE Q �I o J a.'� Jo LU " C7 I— z O O O w z z J O Q J J f— w a a z z 2�i D O _ o U Q Q O= LA of U a o N Q 0 V �I J J M( V O 4 O (z V) zLLJ J { 6 C is _ LC ` QLijt(-� 3 Q } % Vi 0 O0 e O z Q u F- oc LL o lyj U O O LL zE �aoa Uz u 0 Q v �•, LL O LL O G 1= J_Ln U = d' f w u Q w w w C. U a o 0 a) � N Q c m O E N 0 O ` `J Yt t• to s' F CE T O ` c m_ O C ' c � O a0) O ^ C V wC J N \p0 O �E �m a = ,_ Q CL� O) 3 V LL oU0o Z \ 1 0 z m \ r, a (V to w- > O � v N N b1J v J Cl- H Y E > a O a .0 ro � LJ a) o tD a` () a a)CL C E !6 � O a) Q ai Y iJ Y � N E a/ 0 E a O O DO v 1�0 (U ru T� Y N a1 y E v v E c L O a C w Nc aj O a c w L L� M d to o E 0 v c O O a T U ^ L O O Ip = U N n C H O v�v W Q) 2 O c 3 7 = of Y v O E 0 O L a a0 y O U C z c v 'on 'a ` .Q Q U O 4/ E u Iv(u °Y O -0 O o 3L Y c ` O 0 U N a Y M X > v a) - ELn w E c \ ,-1 w t cw O O � a E n N K a Q C p O \O p O O U L a) Q O V1 Y Q _ N Q @ Vt fa ri O L v v r z 2 E o V tw j 'p \ O a) E E OJ .� u m >' C u 0 O n Y o z cco(Aa) E Ln C) a N N C C O H O � � bD F- C `= T O V CO L O t L yJ O v C S� t O 3 � y o0 Z c VI M � � i L 1 W 'C 1 M � 1 c o Vn cn O O I- b Ol = J H E 3 L � M f0 �+ rn v1 ar al u (£p i d ai V V O 1 i co 0 o z 5 o L � \ ro Y '>= O O a1 aJ N o Y E 6 LC E V i o i v� p v N O E v U N O N C c _ = m Vi Ia ra J a u ❑ (� L V U i f6 (U E o L O ai W v .� 3 3 o c In C ro a1 O N- O O O_ LI C O m E w Z u c (U c o O a Z , a v n LU O E z Ln L s c aJ + Y p O_ _U "O O LU J Q M i O 'D O C Q U C c p' v- _ O •c N O d w > 3 u ? -0T 2 E Y z is -0 0 E al v O J L n Q Z s "a CO vbD dal J p c < `) la LL F-- "C 7 m E an p S O N v- C u O . Q Q w Z O O C p 0 ? 0 ar Y } Z 00 4, 3 m o g E c E a Y p c p v o Q 3 p (U W E .E to w OC L al C o vOi z w a, tw 0 wO m x z Elw co -p aJ .fl tL Ln n3 L Q U N al w z O ° °A o m w T OD m r• N t a 2 Y 01 0 O w 0 O W Y r1 O_ O (O O w Y to Ur u ON w Z O Oi m e cp c m o f- a v} N O ` S� z C ra C C Y Q T Y 0 3 c LL a, ' o w 'O _O d v O U Z W f0 CU 0 c 'L L l7 v N a Q O �` w v 0 E c= z U a In 0- c t p O v :_ O 0 3= Z F- + �``f m a O O Q L Q J Y y O r Z p N p o � v a m Fl mil > O M u:^ c .� w 3 m a a w 2 S .Y.+ko m .0 5 a r-i = O V L > = A ,� ra N n� - 1r'm�lt'antttent'ctl Quality Stormwater Discharge Qutfall (SDQ) Qualitative Monitoring Report ro,-guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land-resources/ n pdes-stormwatcr-gps Permit No.: N/C or Certificate of Coverage No.: N/C/G/ / / y /©%T / % / X Facility Name: 04 a oU h a. ---C:P a C_ %>e _ County: —Eto +-rt arv.�SPhone No. Inspector: �� A- (4-1 Pam, q L..- mac? - Date of Inspection: cs 0 tl (� a Time of Inspection: Total Event Precipitation (inches): 0 - 0 .._..... _.._._.._................. _...... _......... ._...... _.__ .......... ___............... ............. All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfali. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: of Pennittee or Designee) 1. Outfall Description: Outfall No. on Receiving Stream: Structure (pipe, ditch, etc.): d' Ve- f - Describe the industrial activities that occur within the outfall drainage area: .__ C v try e- ::>(�-- Page 1 of 2 S WU-242, Last modi I ied 06/01 /2019 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: I 4_ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Yt © V)t-- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: l 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ( I� 2 3 4 5 7. Is there any foam in the sttoorm'water discharge? O Yes 0 No. 8. Is there an oil sheen in the stormwater discharge? OYes A No. 9. Is there evidence of erosion or deposition at the outfall? O Yes SONo. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 011111 (�Iace Anapical www.pabelabs,com June 01, 2020 Gary Kilker Carolina Ready Mix 606 Old US Highway 70 Ridgecrest, NC 28770 RE: Project: STORMWATER 051820 Pace Project No.: 92478058 Pace Analytical Services, LLC 2226 Riverside Dr. Asheville, NC 26804 (828)254-7176 Dear Gary Kilker: Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2020. The results relate only to the samples included In this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: Pace Analytical Services -Asheville If you have any questions concerning this report, please feel free to contact me, Sincerely, //�--<u.. N —... Chris Derouen chdstophenderouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, j« without the written consent of Pace Analytical Services, I.I.C. tOg�gtA,, Page 1 of 13 (�;ZeAnalj4ical � www.paoslad9,csro Project: STORMWATER 051820 Pace Project No.: 92478058 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Flodda/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 CERTIFICATIONS North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virglnia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, oxcept In full, without the written consent of Pace Analytical Services, LLC, Page 2 of 13 0-47 aceAnalydcal www,pacalabs,csm Project: STORMWATER 051820 Pace Project No.: 92478058 Lab ID Sample ID 92478058001 MARS14ALL 92478058002 FLETCHER 92478058003 SWANNANOA PASI-A = Pace Analytical Servloes -Asheville Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 20804 (828)254.7176 SAMPLE ANALYTE COUNT Analytes Method Analysts Reported Laboratory SM 254OD-2011 MJP 1 PASI•A EPA 9040C SMK 1 PASI-A SM 254OD-2011 MJP 1 PASI-A EPA904DC SMK 1 PASI-A SM 2.540D-2011 MJP 1 PASI-A EPA9040C SMK 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Page 3 0f 13 without the wrltton conaant of Pace Analytical Services, LLC. Pace Analytical Services, LLC ® 2226 Riverside Dr. aceAnalytica! Asheville, NC 28804 www.pacela6s,com (828)254-7176 ANALYTICAL RESULTS Project: STORMWATER 051820 pace Project No.: 92478058 Sample: MARSHALL Lab ID: 92478058001 Collected: 05/18/20 11:20 Received: 05/19/20 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 43.2 mg/L 25.0 1 05121/2011:42 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.4 Std. Units 0.10 1 06/01/20 15:23 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/0112020 04:25 PM without the written consent of Pace Analytical Services, 41-C, Page 4 0( 13 (�IaceAnalytical www.pacol3bs.com ANALYTICAL RESULTS Project: STORMWATER 051820 Pace Project No.: 92478058 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 20804 (628)254-7176 Sample: FLETCHER Lab ID: 92478058002 Collected: 05/18/20 07:10 Received: U511912U UtWu Mt Parameters Results Units Report Limit DF Prepared Analyzed 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 61.3 mglL 12.5 1 05/21/20 11:43 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.2 Std. Units 0.10 1 06/0112015:14 Date: 06101/2020 04:25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. CAS No. Qual H3 Page 5 of 13 aceAnalAcal 00 www.pacclabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: STORMWATER 051820 Pace Project No.: 92478058 Sample: SWANNANOA Lab ID: 9247805B003 Collected: 05/18/20 08:35 Received: 05/19/20 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual 2640D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 31.7 mg/L 6.2 1 05/21/2011:43 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 7.8 Sid, Units 0.10 1 00/01/20 15:16 H3 Date: 06/01/2020 04:25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, LLC. Page 6of13 aceAnalytical www.pacolobs com QUALITY CONTROL DATA Project: STORMWATER 051820 Pace Project No.: 92478058 QC Batch: 542864 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92478058001, 92478058002, 92478058003 METHOD BLANK: 2891867 Matrix: Water Associated Lab Samples: 92478058001, 92478058002, 92478058003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 05/21/2011:42 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2891868 Spike LCS LCS % Rt:o Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 266 106 90-110 SAMPLE DUPLICATE: 2891869 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2891870 Parameter Units Total Suspended Solids mg/L 92478197001 Dup Result Result RPD Qualifiers 266 272 1 92478214001 Dup Result Result RPD Qualifiers 607 618 2 Results presented on this page arc in the units Indicated by the "Units" column oxceptwhere an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date; 00/01/2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical WWW.pacelabT.l;om QUALITY CONTROL DATA Project: STORMWATER 051820 Pace Project No.: 02478058 QC Batch: 544392 Analysis Method: EPA 9040C QC Batch Method: EPA 904DC Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 924780580D1, 92478058002, 92.478058003 SAMPLE DUPLICATE: 2898998 92477877001 Dup Parameter Units Result Result RPD Qualifiers pi -I at 25 Degrees C Std, Units 7.1 7.0 1 H3 SAMPLE DUPLICATE: 2898997 92478588001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Sid. Units 7.8 7.8 0 H3 Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Results presented on thls page are fn the units Indicated by the "Units" column except -here an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08101l2020 04:25 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 (�IaceAnalytical www.pacolabs.com QUALIFIERS Project: STORMWATER 051820 Pace Project No.: 92478058 DEFINITIONS DF - Dilution Factor, it reported, represents the factor applied to the reported data due to dilution of the sample aliquot, ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitdle by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte Is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Date; 06/01/2020 04�25 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical 5ervices, LLC. Page 9 of 13 �JceAnaVical" www.pacelabs.com f QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER 051820 Pace Project No.: 92478058 Lab ID Sample ID QC Batch Method 92478058001 MARSHALL SM 254DD-2011 92478058002 FLETCHER SM 254OD-2011 92478058003 SWANNANOA SM 254OD-2011 9247BO58001 MARSHALL EPA9040C 92478058002 FLETCHER EPA 9040C 92478058003 SWANNANOA EPA9040C Date: 061011202D 04:25 PM Paco Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QC Batch Analytical Method 542864 542864 542864 544392 544392 544392 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, LLC. Analytical Batch Page 10 of 13 r r�° Document Name: Document Revised: February 7, 2018 !� Sample Condition Upon Receipt(SCUR) Pap 1 of 2 eCBAnBI}It1Cc�! Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving sa ples; Asheville Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ i Client Name: Project#: WO# : 92478058 .C,(TlrOhri"1)�cd-c+ Mt� Courier: IIIfI�!l��I IIIIII■II []Fed Ex ❑UPS USPS Client ❑ Commercial ❑Pace ❑Other:_ 92478058 Custody Seat Present' Yes 1ZNo Seals Intact? QYes/ No J / Date/IetNa6 Person Euomininp Contents Xfttft'amodek ]oil' F�'fii•'a'. s - - - • _ - - - - - _ - _. � Dra saw�tes anpwGe`-aw a beCr+ soertr {YI.r^rtcral,, Comments/Disaepancy: ti.io ? C;stDdv Present? QfJo j]M/A 1. Sa c-es Arrived vntf'.in Hold Time? es No N A 2. Shm-, Mold Time Analysis (<72 hr.)? aes MN. N/A 3. Rish Turn Around Time Requested? Yes No ❑N/A 4. Sufficient Volume? Yes No ❑N/A S. fCorrect Containers Used? -Pace Containers Used? Ycs Yes []No ❑N/A I]No ❑N/n 6. Containers Intact? as [3No N/A 7. Dissolved analysis: Samples Field Filtered? ❑Ycs .ZJNo ❑N/A S. Sample Labels Match COC? -tnciudes Date/Time/ID/Analysis Mntrlx:_ l leadspace In VOA vials (>5-Ginm)? pfYes W-1 ©ves ❑No ❑N/A NoLNIA 9. 10. _ Trip Blank Present? Trip Blank Custody Seals Present? ❑ves [lyus ❑No11. No COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review; Project Manager SRF Review! Date/Time: Date: Few Data -, 4 1 3 LJI-Il ••: Page 11 of 13 P /,-PkeAna&IiMl Document Name: Sample Condition Upon Recelpt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No., F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, COhform, l'OC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box Is to list number of bottle Project H WO# • 92478058 PM: CD1 Due Date: 06/03/20 CLIENT: 93-Car011naR a N z ? N :Z ¢ a ✓_ v t Z otit O -0 N N .z ' N u 7 -2_ .N u O N « J v C .ao O a, E E o T Z 7 v 2 " .i t7 ,� V u c V 19 v E E c .E E E E 0 C 4 .�-, 4 J�. 0 > p > E 0 a r- o > E a ro E E s o ff iQ ¢ E p Q E P E v a m a a m a m a m Jf a m Z a m N "a to ti a m u. C7 Q r l~? 4 ¢ 4 U ¢ ¢ U) O R 00 7 > A > > a wt ut a m th 4 } l7 o 2 5 � 1 — >3 9 10 it 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation ad)usted Amount of Preservative added Lot A AM— 11 n Mote: Whenever there Is a discrepancy affecttn8 North Carolina compeance samples, a copy ui uus ,c, ,,,� , Out of hold, incorrect preservative, out of temp, incorrect containers. Page 12 of 13 £ 610 £ b abed NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG140000 Ready -Mixed Concrete Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG141 0 3 8 2 Person Collecting Samples: Gary Kilker Facility Name: Carolina Ready Mix and Builders Supply, LLC Laboratory Name: Pace Analytical Facility County: Buncombe Laboratory Cert. No.: 40 Discharge during this period: X Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑ Yes ■❑ No If so, which Tier (I, II, or III)? Part A: Analytical Monitoring Requirements for Outfalls with Industrial Activities— Benchmarks in (Red) Parameter =' Parameter Outfall Outfall Outfall Outfall Outfall Code N/A Receiving Stream Class Class C N/A Date Sample Collected MM/DD/YYYY 11/11/20 46529 24-Hour Rainfall in inches 1.50 C0530 TSS in mg/L (100 or 50*) 31.7 00400 pH in standard units (6.0 — 9.0) 8.6 Non -Polar Oil & Grease in 00552 mg/L (15) for drainage areas that use > 55 gal/mo of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): Tested for oils per company policy 1 once per year. Non -detected. Usage on oils below cutoff limits, <55 on engine and hydraulic oil "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." or Delegated Authorized Individual 1 /05/21 Date i w 0 ,LL V Z 0 Z 00 G m a • E W Ln a) N E N o T W Z E O O V J W p o_ CO U � Z a a Z aao (� m oM i I a > U Z O 0 O V u O2 F _U Z F- LL J_ 0~C U w Q U LL V) W J a Q H C7 Z H W J O u Z O Ln W w a QC cf LLI C S Z ❑ O W ❑ N N M1 W O co N z O J Z cr Z O 2 O O U a a o a s a e E CO H C fV O M1• on N > C s •� r O• C Cg�— Z m o H A � r C in a+ O G1 w j C LA 0 C r J N 0\A G E o e- M m� � 00 v � a O Y N y v OJ 4r LL O \O O o E Z O Z i-� 3 O M n aJ N N j O v " U v Q) J d . v > a O v � v f0 c � v o O v a Y aJ C flC- N E (� N 0 a n i N EA � � aJ E aJ O - a Ln o � T � � Y a) E C t p v E O a; E L � m E `o -o c p O ry T E 5 v as a c `o C7 on Y = Y v O E L � � L fa b0 y z C N 'm Q N Q U pE ' aJ O a-'co U L N N =- vv O � '- v o L O o v 3 Y Z c a Y 0 o u 4 Y n x > v v w ,n 1 W L 7 E' O O U c a E n N cc v c o v o\ Q s o 0 _ 'p ti -0 M v w v ° o\ � CD o — O a v z ' E U > � \ N E E O , L v° Y LL 3 u V Q O L a1 z C ' Y > o (A � E N N I X = L = CO v O G � C o •� L6 N OA _ T Z O O O s L }+ O v C O � O ��� N N 3 � Lv z a O _ o�C M •A v � r = o_ U " O > S M uj C r E M v m _ v =' a a h Ln N E CD r 'Am M 0 F- a O -C W v 2 J C L Ln •vt Q � Z O � a 1D F- m � N N = W �+ O am a \ N Lp u O !' N v M v r O O V E � r O �z !" O � O O z LL, r J Q O Lu O r z Q Q U z 0 LL O w z U L Li X ❑ Y or Ln Q w � r S U z LLJ Co M1 LU z cO O G LL, O LL S o F- Q 0 S uj F- H Q J z U O u. U of Z) :DO O r r w Q Q 2 S L Li Q z u a z O U uj 11 O a z O C Oo O N v C = E N y Up (d o U > 3 3 Y o U C Y C - L O v O O- -O C U C N N o f° E c = W _ = O - O O U1 v L CL Q s c E O_ w > C 7 O E (0 i o 0 OJ •3 c C O' N O C 41 O v E m L — c + O O a OJ N O -0 CO N _ � Y -0 a E c a E 0--a C U 7 O .0 a v = ra c O O 'y Y 3 c E N H •O % E 7 ca ro O •Y o > .c E C C aS.+ an v E v aco O co s --, ra t 6m, v ++ UJ a aO a O O C Y O ru � U 3 Q C a = O = C Qpp w O O i � - Y m' a>m C -0 v v N O d M N @ C S = O � s C Y Q u o O E M ci Ln ri O N O M 0 O N 41 E v a *40 - f rwir onmen:tai Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdcq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N_/C/ / / / / / / / or Certificate of Coverage No.: N_/C/G/(I /'q /4 /3 /8 /�/ (- Facility Name: f, 1, e >"0, Rea di.. Irl ; X �f' % ! S ) ��`� LL er County: _R k n tow- _ .--Phone No. gc lk ` ��30 y d Inspector: Date of Inspection: % / j Time of Inspection,: Total Event Precipitation (inches): ) . 6 ----...._.—...__... _..... ...... ___._._.._.___.__........._....__................... _......._.._.._......._.___._All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pcnnittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of &mittee or Designee) 1. Outfall Description: Outfall No. 00 / Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: O y� cr .e tl2 &N Q rN u 7rA-1._7_ I t i h !� Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge _using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: E it 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): h a V�-L 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stonnwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspen ftd Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 0 2 3 4 5 7. Is there any foam in the stonnwater discharge? O Yes §�> No. 8. Is there an oil sheen in the stormwater discharge? Oyes -do No. 9. Is there evidence of erosion or deposition at the outfall? o Yes - No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 December 01, 2020 Gary Kilker Carolina Ready Mix 606 Old US Highway 70 Ridgecrest, NC 28770 RE. Project: Stormwater 11/11 Pace Project No.: 92505579 Dear Gary Kilker: Enclosed are the analytical results for sample(s) received by the laboratory on November 12, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 11*'PaceAnal�f�'ical ti' J` www.pace]abs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 11/11 Pace Project No.: 92505579 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification M 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification M 460222 Aw REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Project: Pace Project No.: Stormwater 11/11 92505579 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92505579001 MARSHALL SM 254OD-2011 ALP 1 PASI-A EPA 9040C NAL 1 PASI-A 92505579002 FLETCHER SM 2540D-2011 ALP 1 PASI-A EPA 9040C NAL 1 PASI-A 92505579003 SWANNANOA PLANT EPA 1664B CJM 1 PASI-C EPA 1664E CJM 1 PASI-C SM 2540D-2011 ALP 1 PASI-A EPA 9040C NAL 1 PASI-A PAS I -A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 f r. 5ceAnalytical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Stormwater 11/11 Pace Project No.: 92505579 Sample: MARSHALL Lab ID: 92505579001 Collected: 11/11/20 16.05 Received: 11/12/20 08:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 13.2 mg/L 2.5 1 11/14/20 12:02 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.4 Std. Units 0.10 1 11/30/20 17:27 H3 Date: 12/01 /2020 09:23 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Stormwater 11/11 Pace Project No.: 92505579 Sample: FLETCHER Lab ID: 92505579002 Collected: 11/11/20 12:40 Received: 11/12/20 08:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 43.1 mg/L 2.5 1 11/14/20 12:02 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 8.7 Std. Units 0.10 1 11/30/20 17:26 H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 aceAnal{/�'ical J` www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: Stormwater 11/11 Pace Project No.: 92505579 Sample: SWANNANOA PLANT Lab ID: 92505579003 Collected: 11/11/20 10:05 Received: 11/12/20 08:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 11/25/20 12:06 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 11/25/20 12:06 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 31.7 mg/L 2.5 1 11/14/20 12:02 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 8.6 Std. Units 0.10 1 11/30/20 17:25 H3 Date: 12/01 /2020 09:23 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 15 -.",raceAnalyticalo www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 582959 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92505579003 METHOD BLANK: 3082581 Associated Lab Samples: 92505579003 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 3082582 Parameter Units Oil and Grease mg/L MATRIX SPIKE SAMPLE: 3082583 Parameter Units ,and Grease mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11/25/2012:06 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 34.5 86 78-114 35589884015 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers 2.6J 40 33.6 78 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 12/01 /2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 laceAnalyfical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 582960 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92505579003 METHOD BLANK: 3082591 Associated Lab Samples: 92505579003 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 3082592 Parameter Units Total Petroleum Hydrocarbons mg/L MATRIX SPIKE SAMPLE: 3082593 Parameter Units :al Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 11 /25/20 12:06 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 19.6 98 64-132 35589884015 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers S.OU 20 10.2 38 64-132 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 15 �aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 580382 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92505579001, 92505579002, 92505579003 METHOD BLANK: 3070275 Matrix: Water Associated Lab Samples: 92505579001, 92505579002, 92505579003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/14/20 12:00 LABORATORY CONTROL SAMPLE: 3070276 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 228 91 90-110 SAMPLE DUPLICATE: 3070324 92505572001 Dup Parameter Units Result Result RPD Qualifiers tal Suspended Solids mg/L 51.4 52.2 2 SAMPLE DUPLICATE: 3070325 92505597001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 202 275 31 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 15 Ar / .�PaceAnalytleal www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: Stormwater 11/11 Pace Project No.: 92505579 QC Batch: 583262 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92505579001, 92505579002, 92505579003 SAMPLE DUPLICATE: 3084062 92505579003 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 8.6 8.6 0 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 ace AnalXical www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Project: Stormwater 11/11 Pace Project No.: 92505579 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01/2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 15 j aceAnalytical' www.pacelabs.com Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Stormwater 11/11 92505579 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92505579003 SWANNANOA PLANT EPA 1664B 582959 92505579003 SWANNANOA PLANT EPA 1664B 582960 92505579001 MARSHALL SM 2540D-2011 580382 92505579002 FLETCHER SM 2540D-2011 580382 92505579003 SWANNANOA PLANT SM 254OD-2011 580382 92505579001 MARSHALL EPA 9040C 583262 92505579002 FLETCHER EPA 9040C 583262 92505579003 SWANNANOA PLANT EPA 9040C 583262 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/01 /2020 09:23 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 15 Document Name: Document Revised: October 28, 2020 2acle Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: F-CAR-CS-033-Rev.07 Issuing Authority: Pace Carolinas Quality Office Analytical' Laboratory receiving samples: Asheville Ff Eden[—] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑ WO : 9`0'5055 / 9 MEE, Client Name: 1., �1i f �`o, � r, // 1 f Project #:�I I �) Courier: [Fed Ex [-]UPS ❑USPS QQ Client ❑ Commercial ❑Pace ❑Other: 92505579 Custody Seal Present? ❑Yes ❑No Seals Intact? Oyes ❑No I Date/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer.« _ Wet ❑Blue "" ❑Yes ❑Pio []N/A ❑None❑IRGuniD: > Type of Ice; Correction Factor: Cooler Temp:Add/Subtract (°C) Temp should be above freezing to VC ' ❑samples out of temp criteria. Samples on ice, cooling process Cooler Temp Corrected (°C): / has begun USDA Regulated Soil ( 'N/A, water sample) Did samples originate irra quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, —A D.—I., 01-17 Fly nNn Comments/Discrepancy: Chain of Custody Present? Yes ❑No N/A 1. Samples Arrived within Hold Time? Yes ONO ❑N/A 2. Short Hold Time Analysis (02 hr.)? ❑Yes : jao ❑N/A 3. Rush Turn Around Time Requested? []Yes QNa ❑N/A 4. Sufficient Volume? oYes ONO N/A 5. Correct Containers Used? -Pace Containers Used? )Yes Yes ONO ONO ❑N/A ❑N/A 6. Containers Intact? OYes ONO ❑N/A 7. Dissolved analysis: Samples Field Filtered? Dyes ONO N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Pves ONO ❑N/A 9. Headspace in VOA Vials t>S•6mm)? (]yes ONo !PN/A:l /A10. Trip Blank Present? Des ONO 11. Trip Blank Custody Seals Present? ❑Yes ❑No /A COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑No CLIENT NOTIFICATION/RESOLUTION Person contacted: • Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date/Time: Dates Date: Page 13 of 15 '1 �,;a eAna0cat' Document Name: Sample Condition Upon Receil Document No.: F-CAR-CS-033-Rev.07 *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples, Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottles Document Revised: October 28, 2020 Page 2 of 2 Issuing Authority: Oarp rnrniina�. r)uality Offire W:92505579 PM: CD1 Due Date: 11/30/20 CLIENT: 93-Cairo 1 i naR z z 2 ? M > v V V V V > > A _ N V z R ` ? o m M'lei n Q n D v O 0 a = —° c' m c O v 0 T A 4 Z O vi ` �. Z a trt o c^ T > Y "� a s z c D e c c ``! = Z v v N u m is Y u ro+v u a y u vo E n` .n E Q E N x p( Z T fl s N Y i_ N j a a Q E E E a E E E E .yyo v o w E m E E E E a N{ '> i{I J 0 0 0 _ov Ln CJ O O 0 D Lo v n N o ul ^ 0 E M N v M p v (� H x H M M v. M ¢ M iR a: 01 A d Cn sa Y i t9 r In r N a o t7 In « q d m a m M m ems+ LL m O. m a m 6. m n6 m 3 t.9 a t7 a l7 a l9 a U' Q l7 a t7 a to > t7 > t9 o> 0 r.. i y CL � u. �, pM m a > o 1 � I 1 2 i 3 ' j � % I a I i s i 6 7 8 I 9 i 10 i 12 i i 12 i f pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time presetvation Amount of Preservative Lot # adjusted i added Note: Whenever there is a discrepancy affecting North Carolina compliance sampies, a copy of tms Corm win ca sent to cre nuru+�mu Out of hold, incorrect preservative, out of temp, Incorrect containers, Page 14 of 15 SL 10 SL abed I rR cr CL E 0 0 E 4" 0 cr Ci < 0 LL 10 44 Z :EC) a) (NIA) saldweS pe OL, O pols"O (NIA) 001 UO POAInW-4 (N/A) OuPc)NO lenpise'd 0 U, dV01 . . ........... w (77' T W w Xq aseeig PUB po Hd x x x x rSSl x x x N/A ISO.L SGSAIL'UV cl w loueqlevi 4 N i COZSZeN HOeN 13H co W 0- CONH E jj m z hi "6 0 POSZH idun oC; CL a. c a E ui < cL a. a. SN3NfY1NO3 JO z wl w N011031*100 IV diA31dv4vs a fn -j a. -i a. a z (n tn 0 Q uj w W 0 I L RdAi 21MVS (Yel ol S.Poz F;IwA Q.$) 3CODYwIvvi p 0 E r z V) 'm u 3 0- Ou 0 < 0 Q 0 71 3: .0 3: E 0 u 0 u c w CL E J t 8 E u C, 0 <n # W311 r—=# W=311- m 6 . c N1 0 t) If fi w 0- --q