HARGETT FARM FILE (GORDON PROPERTY)_Regional Office Historical File Pre 2018

e 8, 2015
A file review was made of the Gordon Property located at 5516 Old Paigeland/ Marshville Road.
On November 25, 1997 the WSW on the Gordon property was sampled of Nitrates, Total Coliform, Fecal
Coliform, VOC's, SVOC's, Mg, and Fe. The laboratory results reported no returns for VOC's and SVOC's.
Iron (Fe) was reported below 2L Drinking water standards.
On December 2, 1997 a memo was issued to Mr. Gordon from the Union County Health Department of
the presence of coliform bacteria being present in his WSW. Ultraviolet Fluorescence indicated the
sample was positive for E. coli bacteria. In this memo, Mr. Gordon was advised to disinfect or boil water
from the WSW prior to using the well water for drinking or cooking.
Manganese report @0.27mg/L, for a soil sample collected on 3/25/1998. This value was required to be
calculated based on Soil inorganic — water partitioning Coefficient (Koc) which is required to perform the
calculation from soil to GW standards and therefore determine an equivalence value that could be
compared to the 2L GW drinking water standards. The calculation for Mn using the soil sample data
provided, converts to approx. 65 mg/kg. As the resulting soil sample calculated to 0.27mg/L, the soils
sample is below the potential GW impact standards. This page is attached as part of the file review.
Nitrates reported @ 32mg/L. The 2L standard for drinking water is 10mg/L. This is in exceedance of the
2L standards for drinking water. Notification was sent to Mr. Gordon on January 14, 1998 addressing
the exceedance of Nitrates and Mr. Gordon was advised the WSW on the property not be used for the
purpose of drinking and cooking.
In 1997, the Hargette property which is adjacent to the Gordon property had Chicken coups. These
chicken coups could have been a source for the Nitrates and the E.coli. The Hargette property never
became completely permitted for Poultry and Swine an eventually went out of business. In 1997, the
chicken coups were reported to have been destroyed by Hurricane Hugo. However Hugo came through
North Carolina in 1989. A historic search indicates the tropical system during the 90's was the likely
cause of the chicken coup destruction would have been Hurricane Fran or Berta which affected North
Carolina during the 1996 Hurricane Season. The chicken coups were not reconstructed and only
remnants of the chicken coups were present during GW sample collection event in 1997.
With the removal of the Chicken Coups, and therefore the source for the Nitrates and Coliform bacteria
have been mitigated. The old Hog Lagoon appears to be partially infilling, although water is still present
in 90% of the lagoon.
In 1998 Mr. Gordon disconnected the original WSW and drilled a new well. In February of 1998 the new
Gordon well was sampled for Nitrates and the sample results were reported as 4.4mg/L. This is within
the 2L standard for drinking water.
The Hargette property is now being used as a residence and a Google Earth search indicates an Equine
presence on the property. This site was sampled for Nitrates on February 16, 1998. A report was issued

March 16, 1998 indicating Nitrate levels at this site were reported to be below 2L standards for
WSWs.
Based on analytical data and the conversion table attached, the constituents of concern reporting at
below Groundwater impact limits, this file can be considered to be closed.
Sincerely,
Edward Watson
Hydrogeologist
NCDENR, WQROS, MRO

INACTIVE HAZARDOUS SITES BRANCH
PRELIMINARY SOIL REMEDIATION GOALS (PSRG) TABLE
(Updated First & Third Quarter of Calendar Year)
MARCH 2O15
Both health -based and protection of groundwater remediation goals must be met. The protection of groundwater remediation
goals listed on this table are only one alternative for achieving protection of groundwater criteria. Please refer to REC or State -
lead Guidance documents for additional information on protection of groundwater remediation goals, procedures for adjusting
preliminary remedial goals and other criteria that may affect remediation goals (e.g. ecological receptors, cross -media
contamination). In addition, if sensitive environments are present, the branch may require the adjustment of remediation goals
and/or the proposed remedial alternative. Values revised since last edition are in bold.
Csat JContaminant
CAS No.
Preliminary
Residential
Health Based
Soil
Remediation
Goal (PSRG)'
(mg/kg)
Basis
Preliminary
Industrial
Health Based
Soil
Remediation
Goal (PSRG)'
(mg/kg)
Basis
Foot
note
Protection of
Ground
water PSRG2
(mg/kg)
Foot
note
Hydrogen Chloride
7647-01-0
1.0E+05
Max
1.0E+05
Max
Hydrogen Fluoride
7664-39-3
6.2E+02
N
9.4E+03
N
Hydrogen Sulfide
7783-06-4
1.0E+05
Max
2.4E+06
N
Hydroquinone
123-31-9
8.9E+00
C
3.8E+01
C
Imazalil
35554-44-0
1.6E+02
N
2.2E+03
N
Imazaquin
81335-37-7
3.0E+03
N
4.2E+04
N
Iodine
7553-56-2
1.6E+02
N
2.4E+03
N
Iprodione
36734-19-7
5.0E+02
N
6.6E+03
N
Iron
7439-89-6
1.1E+04
N
1.0E+05
Max
1.5E+02
3
Isobutyl Alcohol
78-83-1
3.6E+03
N
5.0E+04
N
Isophorone
78-59-1
5.6E+02
C
2.4E+03
C
2.1E-01
3
Isopropalin
33820-53-0
1.8E+02
N
2.4E+03
N
Isopropanol
67-63-0
2.4E+04
N
1.0E+05
Max
Isopropyl Methyl Phosphonic
Acid
1832-54-8
1.2E+03
N
1.6E+04
N
4-Isopropyl toluene
99-87-6
NA
NA
6.8E-01
4
Isoxaben
82558-50-7
6.2E+02
N
8.2E+03
N
JP-7
NA
8.6E+07
N
1.0E+05
Max
Kerb
23950-58-5
9.2E+02
N
1.2E+04
N
Lactofen
77501-63-4
2.4E+01
N
3.2E+02
N
Lead Compounds
7
-Lead acetate
301-04-2
1.9E+00
C
8.2E+00
C
Lead and Compounds
7439-92-1
4.0E+02
N
8.0E+02
N
2.7E+02
3
Lead subacetate
1335-32-6
1.4E+01
C
2.7E+02
C
Tetraethyl Lead
78-00-2
1.2E-03
N
1.6E-02
N
Linuron
330-55-2
2.4E+01
N
3.2E+02
N
Lithium
7439-93-2
3.2E+01
N
j 4.6E+02
N
Londax
83055-99-6
2.4E+03
N
3.2E+04
N
MCPA
94-74-6
6.2E+00
N
8.2E+01
N
MCPB
94-81-5
1.2E+02
N
1.6E+03
N
MCPP
93-65-2
1.2E+01
N
1.6E+02
N
Malathion
121-75-5
2.4E+02
N
3.2E+03
N
Maleic Anhydride
108-31-6
1.2E+03
N
1.6E+04
N
Maleic Hydrazide
123-33-1
6.2E+03
N
8.2E+04
N
Malononitrile
109-77-3
1.2E+00
N
1.6E+01
N
Mancozeb
8018-01-7
3.6E+02
N
5.0E+03
N
Maneb
12427-38-2
6.2E+01
N
8.2E+02
N
Manganese (Non -diet)
7439-96-5
3.6E+02
N
5.2E+03
N
6.5E+01
3
Mephosfolan
950-10-7
1.1E+00
N
1.5E+01
N
Page 11 of 23

ppppppp-
COUNTY
1'NION
QUAD NO
REPORT 10
MRO
COLLECTORIS►
C ripm,
DATE
3.14.92
TIME
PURPOSE
LABORATORY ANALYSIS
It I ( gfuc
BOD )10 mg Kg
COD Ifigh 340 mg Kg
COD I.ov. )15 nut Kg
Cobform MF Fecal 11616
ucwrrm MF lo,,d )1504
TOC mg Kg
T trbn,ty N I 1 l
Residue . Suspended t10 nog Kg
Total Sunvirded solids mg Kg
pit units
Alkalmnr to rll 4 5 me Kg
Alkalmlti In plI A 1 mg Kg
Cntxrute nog Kg
RKMMnatc me I.g
Cathrt dmstde mg Kg
Chlocde mg 1, It
Chromium 11et I012 uc Kg
Coke True An c u
Csan,de 7`1) mg Kit
COMMENTS:
DIVISION Ell 011A1 'I V
Chemistry Laboratory Report / Ground Willer Quality
SAMPLE PRIORITY
J ROUTINE EMERGENCY
El CI MIN OF CUSTODY
S❑ SAMPLE TYPE
(hsne, IIARGF.TTF. FARM
I -.V,,•n ,,, Site
Descnrtion of sampling point
Sampling hledud
It"naks
Diss Solids 70300
mg/Kg
Ilumide 951
mg/Kg
I lardncss tutal 4W
n,giKg
I lardness Innn-carb) 402
m(v'Kg
Phenols 12710
ugKg
Specific fond 95
umh,,&cm2
Sulfate
m(vKS
Sulfide 741
mg,Kg
SIBAS
mg'Kg
Od and Cmase
mg'Kg
Silica
mg/Kg
It on
Iormaldchvde
mg'L
X
N111 as N h10
95
mwK8
X
I KN as N A25
310
mg/Kg
X
NO2 ' NO 1 as n 630
270
mglKg
X
1' 1 otal as P M5
<O 02
n,g Kg
Pt )4
mg'Kg
Ag-Silver 46566 mg/Kg
AI -Aluminum 46557 mgiKg
As -Arsenic 46551 mg/Kg
Ba-Barium 46559 -wKg
Ca -Calcium 46552 mg/Kg
Cd-Cadium 46559 mg/Kg
Cr-Chromium 46560 mg/Kg
Cu- Copper 1042 mg/Kg
Fe- Iron 1045 mg/Kg
I Ig- Mcicury 71900 mtyFg
K-Potassium 46555 mg/Kg
Mg- Magnesium 927 mwKg
Kin -Manganese 1055 mg/Kg
Na- Sodium 929 mg/Kg
Ni-Nickel mg/Kg
Pb-Lead 46564 mg/Kg
Se -Selenium mg/Kg
Zn -Zinc 46567 mg'Kg
Lab Nunda, R(M753
Date Received
3/26/98
Time Received
A 30 AM
Received By
if;
P' l,''ed H, 1)S
I ).iir icp��ncd 4/16P79
Otganochicume 1'esticidcs
Organophosphorus Pesticides
Nitrogen 1'eslicides
Acid Herbicides
Semivolatiles
TPII-Diesel Range
Volatile Organics (VOA bo01c )
I I'll -Gasoline Range
TPII-111 EX Gasoline Range
N.C. DfI pr. O ,
X.N'YZRON,ML Nr, tiAi: cr
N NATUP,,AL T*V,�()Ujt(_ ;b
APR 2 1 1998
ICV Of €MEMENTEI VAMMEq
°"li CMML
E007'J PAIR

PPP_ 5i>'��Cr
OUNDWATER FIELD/LAB FORM
County Uti ro/L/
/V
0 u a d No "I h7 , Serial No.
Lat. Y1 '12 -26 ,2 Long. 'n (-' -7 /Z,'i
Report To: ARO, FRO, RO RO, WaRO, WiRO, L
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bu ourier and Del., Other•
Collector(s): L' , Date 3 2
FIELD ANALYSES
pH400
Temp.io
Appearance
Field Analysis By:
Spec. Cond.94 at 250 C
_ oC Odor
North Carolina
Department of Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
A14431
rj r it r A QRITY
er outine
at -oil ❑ Emergency
❑ Other
hain of Custody —0
Lab Number
Date Received, Time
Rec'd by:_,2�_ From: Bys,-Courier, HAnd Del.,
Other:
Data Entry By:_
Date Reported:
Ck:
Purpose:
Time Baseline, Com laint, Corn liance LUST, Pesticide Stud Federal Trust, Other:
Owner C%r?'41r� /1i11Z6/7r p 7°`�°'"► y'
Location or site
Description of sampling point
Sampling Method Sample Interval
Remarks iP��' ���' etc)
iounxxna Ime. au term etc. i
LABORATORY ANALYSES
BOD 310 mg/1 Diss. Solids 70300 mg/I A - Silver 46566 u I Organochlorine Pesticides
COD High 340 nig/l Flouride 951 m /I At - Aluminum 46557 u /I Organophosphorus Pesticides
COD Low 335 m /1
Hardness: Total 9m 1
As - Arsenic 46551 u /l
Nitrogen Pesticides
Colilorrn: MF Fecal 31616
Hprdness non-carb 902 m I
Ba - Barium 46558 u /I
Acid Herbicides
_/1001111
Colilonn: MF Total 31SO4 /10011i1
PhenqlS 32730u /l
_
Ca - Calcium 46552 ma/ I
PCB's
TOC 680 m /1
Specific Cond. 95 uMhos/cnr'
Cd - Cadmium 46559 u /I
Turbidity 76 NTU
Sullale 945 m /l
Cr - Chromium 46560 u /I
Residue., Suspended 530 nig/I
Sulfide 745 rn /I
Cu - Copper 46562 ug/I
Fe - Iron 46563 u /I
Semivolatile Organics
Oil and Grease m /l
Hg - Mercury 71900 ug/I
TPH - Diesel Range
pH 403 unit
K - Potassium 46555 mg/I
Alkalinity to pH 4.5 410 mg/l
M - Magnesium 46554 m /I
_
Alkalinity to pH 8.3 415 nig/t
Mn - Manganese 46565 ug/I
Carbonate 445 nig/I
✓
as N 610 rn /I
Na - Sodium 46556 m /l
Volatile Organics (VOA bottle)
Bicarbonate 440 m 1
TPH - Gasoline Range
Carbon dioxide 405 mg/I
+ NO as N 630 m /I
Pb - Lead 46564 u I
TPH - BTEX Gasollre Range
Chloride 940 mg/t
P: Total as P 665 mg/I
Se - Selenium u /I
Chromium: Hex 1032 u /l
Zn - Zinc 46567 u /I
Color: True 80 CU
Cyanide 720 mg/I
Lab Comments:
GW-54 REV UW, For Dissolved Analysis - submit filtered sample and write "DIS" in blc

PPPPPPF'
COLNTY
UNION
QUAD NO
REPORT TO
SIRO
COLLECTOMS)
C PIPPIN
DATE
1121�t1
TIME
PURPO%F
LABORA7ORV ANAIASIS
Rccnmal ( )free
BOD 310 inµ Kg
COD Ihgh 140 inµ Kµ
COD Low 115 inµ I: It
Coliform INF Fecal 11616
Cohform hit total 11504
TOC inµ Kµ
Turbiftty N 1l+
Residue. Suspended 510 ins his
Total Suspended solids inµ Kµ
rll units
Alkal+nrty to PI s 5 inµ Kg
.AI►alm'ty to rll 6 1 inµ Kg
Crbonre inµ Kµ
Bicarbonate mg Kµ
Carbon d'mrdc ma Kµ
Chlmide n+r. Ka
Chromium Iles 1012 ul• Au
Corm True gn
cyanide 7:0
COMMENTS:
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Ground Water Quality
SAMPLE PRIORITY
❑ROUTINE 117MERGF.NCY
.�❑ CHAIN OF CUSTODY
El SAMPLE TYPE
Owner IIANGF.TTF. FARM
I.ncation or Site
Ilewioptlon of sampling point
Sampling Method
Remark
Dm Solids 70100
mryKg
1 luor ide 951
mg/Kg
I Imilmss total 9M
mgrKg
I lvdness (non-crb)902
mtvKR
Nitwit 12730
ugiKg
Specific Cond 95
umhosa12
Sulfate
mg•Kg
Sulfide 745
mg/Kg
MIIAS
mg/Kg
Oil and Grease
mryKg
Silica
mg/Kg
Ifoton
Formaldehyde
mg"L
X
NIIIa,N610
260
mg;Kg
X
1 KN as N 625
350
mgtKg
X
NO2 •NO1 u it 610
430
mg'Kg
X
P l otal asp 665
<0.02
mg Kg
pill
ma Kg
lahNumhcr 8(;0754
Date Received '
3/26/98
Time Received
g 10 ANI
Received By
J(;
Released Ile Uti
Date reported 4/16l9a
Oiganocidminc Pesticides
Organophosphonrx Pesticides
Nioogen I'cslicides
Acid Ilcthicidcs
Semivolatilcs
TPII-Diescl Range
Volatile Organics IVOA Kittle)
1 PII-Gasoline Range
'I PI I-111 EX Gasoline Range
N.C.
APR 21 1998
WYtSl9#i �F F�1�fWENT

ppp�SAj4Pg
fJ
North Carolina
GROUNDWATER FIELD/LAB FORM
; s { ► _Akf
�'
Department of Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
County. UAJ ro1y
Quad No n' hl ► Serial No.
Lat. 34 V I 2 Long. k(,) -' 7 /l , Zf
Report To: A110, FRO, CRO)HRO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:_
Shipped by: Bu ourier and Del., Other-
Collector(s): L1, i/ Date 3 l S r IV
FIELD ANALYSES
SAMPLE TYPE SAMPLX.PRIORITY
❑ 14W er outine
Soil ❑ Emergency
❑ Other
Mt-hain of Custody 10
Time
pH400 Spec. Cond.94 at 250 C
Ternp.10 oC Odor
ADDearance
Field Analysis By:
I ARCIRATCIRY ANAI Y.qF.q
BOD, 310 niyil
COD High 340 niy/I
COD Low 335 mc/l
_
Colilottiv MF Fecal 31616 /1011111
_
Colilotim MF Total 31504 /tOUnd
_
TOC 680 11lo/I
_
Turbidity 76 NtU
Residue., Susponded 530 mg/I
pt1 403 unil,
Alkalinily to pH 4.5 410 rng/I
Alkalinity to pH 8.3 415 lily/1
Caibonalo 445 mg/I
-Bicarbonate 44o 111c1/1
_
Carbon dioxide 405 mg/I
_
Chloride 940 nig/l
Chromium: Hex 1032 uy/I
_
Color: True e0 CU
_
Cyanide 720 mg/I
Lab Comments:
Lab Number —
Dale Received Time 0 : • 50
Rec'd by: Horn: Bus, -Courier, I nd Del.,
Other.
Data Entry By: -
Date Reported:
Ck:
Purpose:
Baseline, Complaint, Compliance11 LbUST, Pesticide Study, Federal Trust, Other:
Owner C- R "'1C �� /-!i) iz 64-77 F
Location or site llxz-1 '�' / /¢IDrJ&
Description of sampling�oin1 _ 501E r
Sampling Method Sample Interval
Remarks (Hump, bales, ek l
(pun,4.,y lone. ao remp ulc 1
O►ganochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCB's
Semivolatile Organics
TPH - Diesel Range
Volatile Organics (VOA bottle
TPH - Gasoline Range
TPH - EITEX Gasoline Range
GW-54 REV 7196 For Dissolved Analysis - submil fillered sample and write "DIS" in bl,

PPV
COUNTY
('"ION
QUAD NO
REPORT TO
MRO
COLLF('TORIS)
C PIPPIN
DATE
31V99
TIME
PURPOSE
LABORA-1 URY ANALYSIS
Rrgraoal Office
ROD )10 mg Kg
('OI) IbRh 140 mg Kg
COD Low 115 mg l g
Cohfmn Mr recal 11616
Cohfc n klF Taal )1504
TOC mµ Kg
TwMtrty NIII
Reudue . Sugrrded t 10 mµ Kg
Taal Sugwded anlyds mg Kg
pit units
Alkabrury to pl1 4 5 mg Kg
Alkalinity to pit 9 3 inµ Kg
Carbonate mg Kot
Bicat+onae mg Kit
Cahn dwslde inµ Kit
Chlaide mµ Kµ
Chrrnnmm Ilea 1012 uµ Kµ
( DIM T f.e ltV "I
(-v anrdt 7N me Kµ
COMMENTS
l Mner
I .canon of Sne
I)eanpte— of sampling point
Samphng %Iclhod
Remarks
DIVISION OF WATER OIIAIJ71-
Chemistry Laboralory Reporl / (:round Wriler Quality
SAMPLE PRIORITY
El ROUTINE 11NIERGENCY
El CIIAIN OF CUSTODY
S❑ SAMPLE TYPE
IIARGETTE FARM
Dos Sabds 70300
mg'Kg
I lunrlde 951
-"g
I ladness lolal 900
mg'T:g
Ilardness (non-carb)902
mg/Kg
Phenols 32730
ugKg
Specific Cond 95
umhoelcm2
Sulfale
mtv K g
Sulfide 745
mgiKg
M11:1S
mgrKg
(hl and (ilease
mgACg
Shcca
mgK8
B—n
I rentaldehvde
mgt
X
`:I l t as N 610
120
mg, -Kg
X
I KN as N 625
330
mg Kg
X
NO2 • NO3 as n 630
220
mg'Kg
X
P I Deal as P fa+5
<0.02
MgKg
P()4
mg Kg
Ag-Silver 46566 mg/Kg
AI -Aluminum 46557 mg/Kg
As -Arsenic 46551 mg/Kg
Ba-Barium 46558 mg/Kg
Ca -Calcium 46552 mg/Kg
Cd-Cadium 46559 mg(Kg
Cr-Chromium 46560 mg/Kg
Cu-Copper 1042 mg!Kg
Fe- Iron 1045 mg/Kg
I Ig- Metcury 71900 mgfKg
K-Potassium 46555 mgfKg
Mg- Magnesium 927 mg%KS
Afn-Manganese 1055 mg/Kg
No- Sodium 929 mg/Kg
Ni-Nickel mgiKg
Pb-Lead 46564 mg/Kg
Se -Selenium mwKg
J-n Zinc 46567 mg'Kg
Lab Numhcr 8(:11755
Date Received
3/26/98
Time Received
9 30 AM
Received IIv
101
Released By DS
[)are reported 4/16/9/
Organochlorine Pesticides
Organophosphorus 1'eslicides
Nitrogen Pesticides
Acid Ilerbicides
Semivolatiles
'1 PI I -Diesel Range
Volatile Organics (VOA Wide)
TPII-Gasoline Range
'IPII-B"I EX Gasoline Range
N.C. 1]>; ". �lfi
�.I1T1y
G NATURAL J:,j;)UR(_T,8
APR 21 1998
WV4104 OF INVI)Mf5Th 4.'l MEiVT
04=lf Iftu AL laic[
8Ga755 MAR

OUNDWATER FIELD/LAB FORM
County U�U ro/L/
Quad No "' h" ' Serial No.
Lat. _y - "2 z 6 -2. Long, k U -' 7 12 , '�
Report To: ARO, FRO, R0:)ARO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bu ourier and Del., Other—
Collector(s): �� ✓ ,1, V Date 3 1
FIELD ANALYSES
pH400 Spec. Cond.94 at 250 C
Ternp.ro oC Odor
Appearance
—
Field Analysis By:
LABORATORY
ANALYS-ES
SAMPLETYPE I
❑ W er Mdlut nY
Soil r-
❑ Emergency
❑ Other
hain of Custody
North Carolina
Department of Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
Lab Number
Date Received , CI I\Time
Rec'd b,�` From: B s Courier, Hay cl Del.,
Other:
Data Entry By: Ck:
Date Reported:
Purpose:
Time Baseline, Complaint, Compliance LUST Pesticide Study, Federal Trust, Other:
Owner 77(t„de0(m)
Location or site
Description of sampling oint _'v.1L
Sampling Method ��_ �! %" Sample Interval
Remarks rP"""• Ual0. ac )
(r>•MrYrry Ivne• au lanp etc.)
BOU 310 rr) /1
Drss. Solids
COD High340 rrly/I
70300 n1/I
Flouride 951 nlg/I
A - Silver 46566 u /I
Organochlorine Pesticides
At -Aluminum 46551 u /I
Orgartopttospttorus Pesticides
COD Low 335 my/I
Hardness: Total 9Uo
Colilorrn: MF Fecal 31616 /100111I
rna/1
Hardness (non-carb) 902 rng/I
As - Arsenic 46551 u /I
Nitrogen Pesticides
Ba - Barium 46558 u /I
Acid Herbicides
rl: MF Total 3I5U4 /t00m1
Phenols 32730 uy/I
Ca - Calcium 46552 /l
PCB's
TOC 68
TOC m !I
_5cihc Cond. 95 uMhosicni,
DeSulfate
rn
Cd - CadmiUln 46559 u /I
Turbidityy 76 NTU
945 In /I
Cr - Chromium 46560 u /I
Residue., Suspended 530 rng/I
Sullide 745 m /I
Cu - Copper 46562 u /I
Fe - Iron 46563 uy/I
Sentivolatile Organics
PH 403 unit
Oil and Grease nt /I
Hg - Mercury 71900 ug/I
TPH - Diesel Range
_
K - Potassium 46555 my/I
Alkalinity to pll 4.5 410 mg/I
—
Mg - Magnesium 46554 rng/1
Alkalinity to pit 8.3 415 n)g/l
Carbonate 445
V
Mn - Manganese 46565 u /1
Illy/l
1 as N 610 ml /1
Na - Sodium 46556 In /I
Volatile Organics (VOA bottle)
Bicarbonate 440 nur/I
Ni - Nickel
—
Carbun dioxide 405 my/I
d
NO as N 630 me /1
tiff/I
Pb - Lead 46564 ug/I
_
TPH - Gasoline Ran e
TPH - BTEX Gasollne Range
Chlondo 94U nut/I
sr
P: Total P
_
Chlonuun): I lox Iu32 L19/_I
as 665 nu1/1
So - Selonium ul1/I
'
Zn - Zinc 46561 u ,/I
_
Color: true ao CU
Cyanide 720
Lab VVIIIments.
GW-54 REV 7191; For Ui•csulved Analysi,; - submit filtered sample and write "UIS" in fib

COUNTY
UNION
QUAD NO
REPORT TO
%IRO
COLLECTOR(S)
(' PIrrIN
DATE
)-IlVll
TIME
PURPOSE:
LABORM ORY ANALI SIS
COM%IFNIS
Rrit—al Office
DIVISION OF WATER 011ALI I Y
Chemistry Lahoralory Report / Ground N der Quality
SAMPLE PRIORITY
❑' ROUTINEEMERGENCY
.�� COAIN OF CUSTODY ❑
In SAMPLE TYPE
(hvnet IIARGE'TTF- FARM
I ,K aw•n or Site
Ite ctq,6nn of sampling point
Sampling Method
Rrrnatks
Ag-Siher 46566 mg'Kg
AI -Aluminum 46557 mg/Kg
As -Arsenic 46551 mg/Kg
lin-Datium 46558 mg/Kg
Ca -Calcium 46552 mg/Kg
Cd-Cadium 46559 mg/Kg
Cr-Chromium 46560 mgiKg
Cu- Copper 1042 mg/Kg
Fe- Iron IG45 nrg/Kg
Ilg- Mercury 71900 mg/Kg
K-Potassium 46555 mg/Kg
Mg- Magnesium 927 mWKg
Mn-Manganese 1055 mg'Kg
Na- Sodium 929 mg%Kg
Ni-Nickel mg'Kg
Pb-Lead 46564 mWKg
Se -Selenium mg'Kg
7_n 7-inc 40567 mg'Kg
Lab Number 8(i0757
Date Received
3/26199
11
Time Received
9 30 AM
Received By
JG
Released IJy DS
Date reported 4/16/98
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Iles bicidcs
Scmivolatiles
TPII-Dicsel Range
Volatile Organics (VOA bottle)
U'll-(iaudine Range
I1111-IIIEX Gasoline Range
N.C. D-a-IrL Or
& NATURAL
APR 21 1998
21W191 @F ENVIM 111L Ittlbt TENT
kg�?—..341LLE MOIL rK1
6Go757 MAR

GROUNDWATER FIELD/LAB FORM 5'4 pJAT]
�l of / A l i�!
County U�j ro/v SAMPLETYPE OVA 1 IOAiTY
Quad No Kj Nl r Serial No. El Wester outine
Lat. Yl V Zt ,l Long. `f0 ' 7 12,Z/ Soll ❑ Emergency
❑ Other
Report To: ARO, FRO, RO RO, WaRO, WiRO, hain of Custody
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bu ourier and Del., Other-
Collector(s): L� , l - �� ✓ Date 3 2 S' 1V Time
North Carolina
Department of Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
0
Lab Number XC-2 O 7S
Date Received J) Ln ('7 dime U - 0
Rec'd by:� From: 1341 Courier, Hind Del.,
Other:
Data Entry By: -
Date Reported:
Ck:
Purpose:
Baseline, Complaint, Compliance LUST Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner C-- ""I I //'I4f I/ ' IE«bo.l
pH400 Spec. Cond.94 at 250 C Location or site #111Z
Temp.10 oC Odor Description of sampling point s`�' L
Appearance Sampling Method //� �! '�' Sample Interval
Field Analysis By: Remarks (Puny,, baler, etc
(Wrr"rq I.ne, an reap. etc.l
LABQRA I URY ANALYSES
BOD- 310 nut/I Disc. Solids 70300 nw/I A - Silver 46566 u /I
Flouride 951 rng/I At - Aluminum 46557 u /I
Hardness: Total 9oo mg/1 As - Arsenic 46551 ug/I
_Hardness (non-carb) 902 mg/I Ba - Barium 46558 u /I
_ PhenolS 32730 ua/I Ca - Calcium 46552 rng/I
_ S12ecihc Coed, 95 uMhos/cnrCd - Cadmium 46559 uu/1
_ Sulfate 945 Ing/I Cr - Chromium 46560 u /I
Sulfide 745 rng/I Cu - Copper 46562 u /I
_ Fe - Iron 46563 ug/I
Oil and Grease m /l Hg - Mercury 71900 ug/I
_ K - Potassium 46555 mg/1
Mg - Magnesium 46554 rng/I
_ Mn - Manganese 46565 ug/I
✓ 5,N1.as N 610 Ing/l Na - Sodium 46556 mg/mull Ni -Nickel u�+ NO as N 630 nu /1 Pb - Lead 46564 ug/I
_ P: Total as P 665 n1g/I Se - Selenium ug/I
Zn - Zinc 46567 ug/I
COD High 340
n1g/I
COD Low 335
Ing/1
Colilorm: h1F Fecal31616
/IOOnd
Colilorm: MF lolal31504
/1001111
TUC 680
1119/1
Turbidity 76
N I U
Residue., Suspended 53o
mg/I
pH 403
unit:
Alkahrnly to pH 4.5 410
(Tig/I
Alkalinity to pH 81 415
n1g/I
Carbonate 445
1119/1
Blcart)OM110 440
11111/1
Ca1bon d1oX1d0 405
111(j/1
Chloride 940
Ing/I
Chronuurn: Hex 1032
Color: True 80
CU
Cyanide 720
Ing/I
Lab Comments:
1e Pesticides
horus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCB's
Sernivolatile Organics
TPH - Diesel Range
Volatile Organics (VOA bottlo)
TPH - Gasoline Range
TPH - BTEX Gasollrle Range
GW-54 REV 7i96 For Dlssulvod Anal) sis - submil liltered sample and w6le "DIS" in bl,

PPPPPP"`
COL'NT\
UNION
QUAD tit)
REPORT In
MRO
COLLECTORS)
(- Pirm,
DATE.
3,24Lv11
TIME
PURPOSE
LABORA-I ORY ANALYSIS
Reg..•nal 011ice
HOD 110 ma Kg
COD Iligh )40 mg Kg
COD t. 335 mg Kg
Colrform %IF I Mal 11616
Cohform MF loW 31504
1(X- mg Kg
/ ur6rurs Nil?
R mdue - 5usperrlal ! 10 rng Kit
ToW Suspended solrJs mg Kit
PI1 urns
AlWrmty to pit 4 5 mg Kg
AlkshnIty to pll 6 ) mg Kg
Carbonate mg Kg
Htcarhnoate mg Kit
Catt,on dwo Oc mg Kg
Chl—le mg Kg
( hrrrrrwm Ilya 101: ug Kg
(dro Lue go c u
( v.,J, 7:0 mg Kg
CO\IME\1S
l by na
1 rat or Site
Description of sampling point
Saunplmg Method
Remvks
DIVISION OF WA-1 Elt QUALITY
(-hemislry Laboralon Report 1 Ground %%wer Qualily
SAMPLE PRIORI I Y
lROUT INE El EMERGENCY
.X❑ CHAIN OF ('l!STUDY ❑
Ej SAMPLE TYPE
IIARG ETTE FARM
1)iss Solids 70300
mg, -Kg
I lumide 951
mg/Kg
Ilvdness total 9W
mg/Kg
Ilvdness (non-earb)902
mg/Kg
Phenols 12730
uwxg
SlmciGc Cond 95
umhos cm2
Sulfate
mgKg
Sulfide 745
mglKg
MBAS
mg Kg
Od and (irease
mg'Xg
Snc�a
mg,Kg
Iforun
1 nr maldehvde
mg9,
N
Nil IasN610
0.18
m&Kg
X
1 KN as N 623
200
mg/Kg
X
N0>2 'NO) as It 630
0.37
mg"Kit
X
P t otal as P 665
3.2
mg xg
1'UJ
mg'K9
Ag-Silver 46W mg/Kg
AI -Aluminum 46557 mglKg
As -Arsenic 46551 mg/Kg
Ba-Darium 46558 mg(Kg
Ca -Calcium 46552 mg/Kg
Cd-Cadium 46559 mg/Kg
Cr-Chromium 46560 mg/Kg
Cu- Copper 1042 mgfKg
Fe- Iron 1045 mg/Kg
IIg- Mercury 719W mg/Kg
K-Potassium 46555 mg/Kit
Kilt- Magnesium 927 mg/Kg
hin-Manganese 1055 mg/Kg
Na- Sodium 929 mg/Kg
Ni-Nickel mg/Kg
I'b-Lead 46564 mg/Kg
Se -Selenium mg/Kg
Zn Zinc 46567 IrwKg
Lah Numbet 8G0156
Dane Keceis ed J/26/98
I in c Recci%ed 8 30 Ah1
Received By 11
Released By DS
Dale reported 4/16199
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Iletbicides
Semivolatiles
TPII-Diesel Range
Volatile Organics (VOA Wide)
I I'll-(iasolinc Range
'1 PIUBI EX Gasoline Range
N.C. Pv'?f r- O
CN VIItnItiP.4fsiv'f. I-EAI:Vh
& NATURAL 1ZSS_0UIiCfS
APR 21 1998
6IW%!4N OF ENVIRGN>' IVAL rt"SGUNT
1,�,;,;s�LE fit OFFFCf
aGO756 MAR

5 %4 V North Carolina
ROUNDWATER FIELD/LAB FORM V Department of Environment, Health, and Natural Resources
�/ t P i DIVISION OF WATER QUALITY - GROUNDWATER SECTION
County UAU ro k/
Quad No l /»' Serial No.
Lat. -)q 1�2 11"'2 Long. '?5-0 ! 7 /2,'Iy
Report To: ARO, FRO, RO�iRO, WaRO, WiRO, L
WSRO, Kinston FO, Fed. 1 rust, Central Oil., Other:
Shipped by: Bu ourier land Del., Other-
Collector(s): L) .J, V r b1 Date 3 1 � . 1V
FIELD ANALYSES
pH400 Spec. Cond.94
Tentp.1e oC Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
BOU 310 111(),
COD High 340 mg/l
COD Low 335 1119M
_
Cohlorm: MF Fecal 31616 /1pUrn1
_
Cohlorm: MF Total 31504 /tUOrnl
_
TOC 680 111-9/1
Turbidity 76 N I U
Residue., Suspended 530 nlg/l
pH 403 and
Alkahndy to pH 4.5 410 nlg/I
_
Alkalinity to pH 8.3 415 mg/I
_
Carlxmate 445 rny;l
_
Bicarbonate 440 rnu/I
_
carbon dioxide 405 mg/I
_
Chlonde 940 rng/I
_
Chromwrn: Hex 1032 u9/1
_
Color: true au CU
Cyanide 72o mg/I
Lab Comments:
at 250 C
SAMPLE TYPE' EtH10RITY.
❑ W er oulir�t�
Soil ❑ Emergency
❑ Other
hain of Custody
Lab Number D ?
Date Received ,---5 a,7 Gi ime
Rec'd 14y: Front: 13+is. Brier, tdatld Del.,
Other:
Data Entry By: -
Date Reported:
Ck:
Purpose:
Time Baseline, Complaint, Cornpliartce LUST, Pesticide Sludy, Federal Trust, Other:
Owner 6 /f 1? �41 r� /-/i)iz 6/77� (Eucb oe.)
Location or site /I br_`ITz-
Description of samplingi it '0. L
Sampling Method Sample Interval
Remarks Gump, baler, etc.)
4"T"rq 1me. au Temp otc )
Diss. Solids 70300 nlq/I
Ag - Silver 46566 uq/I
—
Flouride 951 rnq/I
Al - Aluminum 46551 uq/1
Hardness: Total goo mull
As - Arsenic 46551 29/1
Hardness (non-carb) 902 mg/1
Ba - Barium 46558 uu/l
_
Phenols 32730 uy/1
Ca - Calcium 46552 mg/I
_
-5pecilic Cond. 95 UMltos/Cnl'
Cd - Cadrniulll 46559 ug/I
Sulfate 945 111(1/1
Cr - Chronuurn 46560 ug/l
Sulfide 745 Ing/l
Cu - Copper 46562 uq/I
Fe - Iron 46563 u9/1
Oil and Grease mq/I
Ftg - Mercury 71900 u9/1
K - Polassiun) 46555 Ing/I
Mg - Magnesium 46554 rnq/l
Mn - Manganese 46565 uq/I
it -as N 610 111(1/1
_
Na - Sodium 465W nu /1
r
Ni - Nickel uu/I
, NO as N 630 In /I
Pb - Lead 46564 ug/I
P: Total as P 665 nlcl/l
Se - Selenium uq/l
Zn - Zinc 46567 uq/l
Organochlorine Pesticides
Organophosphorus Pesticides
Nilrogen Pesticides
Acid Herbicides
PCB's
Semivolalile Organics
TPH - Diesel Range
Volahle Organics (VOA bottle)
TPH - Gasoline Range
TPH - BTEX Gasollre Range
GW•54 FIEV n96 For Dissolved Analysis - submit filleted sample and write "DIS" in bl•

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UNDWATER FIELD/LAB FORM
County U�j <0it/ SAMPLE TYP . 'If '�
Quad No �'1 /17 1 Serial No. O W�ler f l �ou�l �e
y Soil El Emergency
Lat. 3y 5Z z(� -� Long. `f0 � 7 12 ❑ Other
North Carolina
Department of Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
Lab Number —
Dale Received,
Rec'd b{r:__It�
CRO)FIRO,
Other:
Report To: ARO, FRO, WaRO, WiRO, hain of Custody Data Entry By: Ck:
WSRO, Kinston FO, Fed. Trust, Central Olf., Other: Date Reported:
Shipped by: Bu ourier and Del., Other
Purpose:
Collector(s): 61- , Dale 3 - III Time Baseline, Complaint, Compliancer,� LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner 611frz"411-) /1�17261f--77/=
pH400 Spec. Cond.9., at 250 C Location or site /7///I1 br_`17-4, Aw l,-\ ,_'/ /�'�l7
Ternp.10 oC Odor Description of sampling��inI
Appearance Sampling Method 'w'�! %�' Sample Interval
PP Irlu,14,. WON. Mc 1
Field Analysis By: Remarks
(yunKwly Inq, an lemy. Mt 1
I AanDATnDV AKIAI VCFc
BOD 310 Ingil
Diss. Solids 70300 1110
Aft - Silver 46566 ug/I
COD High 34o mg/1
Flouride 951 mg/1
AI - Aluminum 46557 ug/I
COD Low 335 n1g/1
Hardness: Total 900 n10
As - Arsenic 46551 u /1
F
Cohlonn: MF Fecal 31616 /1UUIn1
Hardness (non-carb) 902 mg/I
Ba - Barium 46558 u /I
Cohlo►m: MF Total 31504/1001111
Phewls 32730 _ wall
Ca - Calciurn 46552 nu1/
:::'
TOC 680 mg/1
Specific Cond. 95 uMhos/cnr'
Cd - Cadmium 46559 ug/1
Turbidity 76 N l U
Sulfate 945 n1g/1
Cr - Chromium 46560 u /l
Residue., Suspended 530 mg/l
Sulfide 745 n1 /I
Cu - Copper 46562 u /I
Fe - Iron 46563 ugll
Oil and Grease mgll
Hg - Mercury 71900 ug/I
pl l 403 unit!
_
K - Potassium 46555 mg/I
Alkalinty to pH 4.5 410 mg/I
M - Ma(nesium 46554 In/I
Alkalinity to pH 8.3 415 Ing/I
Mn - Manganese 46565 u /I
Carbonate 445 nrg/l
'�
t as N 610 In /l
Na - Sodium 46556 me /1
Bicarbonate 440 nrg/I
Nr - Nickel u0/I
_
Carbon dioxide 405 nrg/l
+ NO as N 630 rn /l
Pb Lead 46564 ug/I
Chloride 940 mg/1
P: Total as P 665 mg/l
Se - Selenium ug/I
Chromium: Hex 1032 u /I
Zn - Zinc 46567 ug/I
Color. True 80 CU
Cyanide 720 mg/I
_
Lab Comments:
GW-54 FIFV 7,96 For Dissolved Analysis - submit filtered sample and write "DIS" in bl,
—/ r- -) (") —2
Time X
From: ,Bus, Courier, Oland Del.,
lochllorine Pesticides
loohosohorus Pesticides
Nilrogen Pesticides
Acid Herbicides
PC13's
Semivolatile Organics
TPH - Diesel Range
Volatile Organics (VOA bot
TPH - Gasoline Range
TPH - BTEX Gasolim Ran

COUNTY I'NW11
QUAD NO
REPORT 10 1IRO
COLLECTORIS) ( I•II`PIN
DATE )2S9t
TIME
PURPOSE
LABORA-1.ORV ANAINSIS
Regional Office
BOD 310 mp, ► it
COD 168h W) mg Kit
COD Lew 115 mg Kg
Colrform \IF Feed 11616
Cotrform KIF Iad 71504
IOC mg Kp
T urba6ty Nit'?
Resudut . 5u4wridrd 510 mg kit
IoW Suspended solids mg Ka
p11 anon
Alkdmm to pll 4 5 mK F:p
Alkdinity to pll 13 mg Kg
Carbonate mg Kg
Brcarlx•nale mIt Kg
Carbon dtovde mp Kp
Chloride nrh Kp
Chrmtium Ills 101] ua Kg
Colin I rur 5n r or
llanrdt T7n n.r Ka
COMMF.N I S
0"'C'
I —m-n or Site
Descnpnon of sampling point
Sarnpbnp Method
Remark
DIVISION OF WATER QUALI IN
Chemistry Laboralom Report / Ground Water Quality
SAMPLE PRIORITY
IROU11INE El EMERGENCY
.�� ('lIA1N OF CUSTODY ❑
SAMPLE TYPE
HARGE l l F. FARM
Drss Solids 70300
mg/Kg
I I—, ode 951
mg,Kg
Ilardness total900
mg/K8
Ilardness (non-carb)902
mg/Kg
Phenols 32730
ugrKg
Specific Cond 95
umhos.cm2
Sulfate
mglKg
Sulfide 745
mglKg
\1HAS
mg/Kg
Oil and (irease
mg/Kg
Silica
lg,Kg
Huron
1 onnaldehvde
mg'L
\
NII1 as N610
048
mg Kg
\
I 1 N as N 625
100
mg -Kg
\
NI12 r NO3 as n 630
028
ma -Kg
P I utal as P ad
6 5
mg'KIt
Pl )1
mg -Kg
Ag-Silver 46566 mg/Kg
AI -Aluminum 46557 mglKg
As -Arsenic 46551 mg/Kg
Ba-Barium 46558 mg/Kg
Ca -Calcium 46552 mg/Kg
Cd-Cadium 46559 mg/Kg
Cr-Chromium 46560 mg/Kg
Cu- Copper 1042 mg/Kg
Fe- Iron 1045 mg/Kg
Jig- Mercury 71900 -FAg
K-Polassium 46555 n1tr)Kg
h1g- Magnesium 927 mg•Kg
Mn-Manganese 1055 mg/Kg
Na- Sodium 929 mWKg
Ni-Nickel mg;Kg
Pb-Lead 46564 mg/Kg
Se -Selenium mg"KIt
7-n Zinc 46567 mg;Kg
Lah Number 8C0759
Date Received
3/26/98
Time Received
8 30 AM
Received By
)G
Rcicnccd liv I)S
Date rcporled 4/16/98
Organmliforine Pesticides
Organophosphorus Pesticides
Vitro¢en Pesticides
I Acid Herbicides I
Volatile
It'll -Gasoline Range
IPH-BTEX Gasoline Range
APR 21 1998
�'1 �F ENt7RDNMFsYi� N RENT
`S��lE Rlq{ g
8G0759 MAR

' z�=-� North Carolina
OUNDWATER FIELD/LAB FORM Department of Environment, Health, and Natural Resources
lJ J I DIVISION OF WATER QUALITY - GROUNDWATER SECTION
CountyyAJo,ul
Quad No '��Sena) No.
Lat. �q V 2L ' Long. "ls" (,) .' 7 12, z/
Report To: ARO, FRO, �1R0,1R0, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central OII., Other:_
Shipped by: Bu ouni land Del., Other:
Collector(s): L� - ✓,' ✓ Date 3
FIELD ANALYSES
H
P 400 Spec. Cond.91 at 250 C
Ternp.10 _or_ Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
BOD, 310
COD High 3,10
my/I
COD Low 335
C01.10.m: MF Fecal 31616
mull
/IOQnd
Cohlolml Mr lotal 31504
IOC Goo
_/InUlnl
n1t�/1
Turbidily 76
N I U
_
Residue., Suspended 530
111g/I
P11,103
unit-,
Alkalmity to pH 4.5 410
111g/I
Alkalinity to pil 8.3 415
Iny/I
Carbonate 445
rng/I
_Bicaibonale 440
n1g/1
Calbon dioxide 405
1111j/I
Chlonde 940
1110/1
C111gnnun: Hex 1032 ug//I_
Color: True 80 Cu-
Cyanide 720 111n/1
Lab Comments:
SAMPLE TYPE SAMPLE PRIOHITY
� 9}F(
WWer [ououttin`e'
Soil El Emergency
❑ Other
hain of Custody
Lab Number
Date Received _, (p Time
ec'd by: From: B r�
Os, Courier, lialid Del.,
Other:
Data Entry By: -
Date Reported:
Purpose:
Time Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
Owner � �� r71110 / li17Z G%77% k,rcie Oft)
or site /l /a/w'?
Description of sampling point wTL
Sampling Method elt"4;-! %�' Sample Interval
Remarks IPurry,, baler, etc 1
Ck:
au tamp
Diss. Solids 70300 n1 1/I
Flouride 951 niq/1
Ag - Silver 46566 ug/I
At - Aluminum 46557 ug/I
—
Hardness: Total goo n1g/I
As - Arsenic 46551 u /I
—
Hardness (non-carb) 902 11u1/1
Ba - Barium 46558 u 1/I
Phgnols 32730 ua/I
Ca - Calcium 46552 ni 1/1
—
Sls_Cond. 95 MhoS/rani'
Cd - Cadmiu11146559 u r/I
Sulfate 945 rn 1/I
Cr- Chromium 46560 u /l
_
Sulfide 745 rng/I
Cu - Copper 46562 u /I
—
Fe - Iron 46563 ug/I
—
Oil and Grease mg/I
Hg - Mercury 71900 ug/I
—
K - Potassium 46555 111g/1
Mg - Magnesium 46554 mq/I
- Manganese 46565 ug/I
Pit as N 610 nu /I
_Mn
Na - Sodium 46556 niq/I
A N 625 nUJ[L
+ NO as N 63o In /I
_Ni - Nickel u g/I
hb - Lead 46564 ug/I
P: Total as P 665 rn 1/I
Se - Selenium u 1/I
—
Zn - Zinc 46567 u NI
Gw•54 IIEV 7196 For Dissolved Analysis - subnol lillerod sample and write "DIS" in bI(,—
Organochlorine Pesticides
Oiganophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCB's
Seinivolatile Organics
TPH - Dlesel Range
—1 Volatile Organics (VOA bottle)
_ TPH -Gasoline Range
TPH - BTEX Gasollre Ranae

Division of Environmental Management
GROUNDWATER SECTION
fit 2^i:AilJi �.L ii1 �11
MAR 31 1998
CHAIN OF CUSTODY RECORD WlDti et t �^ s T�,i ; :N .,, �T
For Investigation of � Incident No.
Samples collected and GW-54 forms completed by:
No. of
Lab ��Y I Gyaod I Location Data _ Timo Containers
)�-,r-�ii.�l MI ���r1��� �rn,.,�, l/a7G.y+ /��l �, .�,��,.� I ?-1C-w1 /v5 I r - I
(
7s
r
I
(
I
I
,p,D�Clce/Time
Rel�ie(Si
Cp,
tur
Re. C Oy( i �ture)-
ec)Xy
I /
Rel.
I Rec. by
I /
Rel.
Method of Shipment:
Rec.. by
/
14J
�?CL'ritV
iy:? 3rC r✓✓=TI:`ii101':
�a1 "7 _ ----
Lpr'X y
arc
Qr�za
t 3,4
3 i3
Lab Nc.
From Thr u h I
'`"'
Cor,taine, s
qn i sis
y
Falinqu'sh d by I
F,acaived by I
Date / 7ine
White copy - GVV meaoquariers , t anary Lwpy — L.C" 1 11 I.UV7 ""ko" "

AN,s1i�
NCDENR
Jerry Gordon
JAMES B. HUNTJR. 5516 Paigeland Road
GOVERNOR Monroe, North Carolina 28112
WAYNE MCDEVITT
SECRETARY
Subject:
Dear Mr. Gordon,
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
January 14, 1998
Well Water Sample Results
On November 25, 1997, I sampled the well located on the property owned by
George Hargutt and serving your house located at 5516 Paigeland Road, Monroe, North
Carolina 28112. The well was sampled or total and fecal coliform bacteria, nitrates, iron,
manganese, volatile organic compounds and semi -volatile organic compounds. The
results are presented below and represent conditions in the well at the time of sampling.
Constituent
Total coliform
Fecal Coliform
Nitrates (NO2+NO3)
Iron
Manganese
Volatile Organic Compounds
Semi -Volatile Organic
Result
Drinking Water Standai
lab error
I colony per 100 ml H2O
lab error
I colony per 100 ml H2O
32 mg/1
10 mg/1
<50 ug/L
300 ug/L
270 ug/L
50 ug/L
None Detected
None Detected
The level of nitrates and manganese exceed the drinking water standards. Manganese is
not considered harmful, but does affect the water's taste and may stain laundry and
household fixtures. The nitrates are considered harmful. I am forwarding a copy of these
results to Ken Rudo, the State Toxicologist. He will make a determination on whether or
not the water is safe to use based on the level of contamination. Should you have any
questions please call me at 704-663-1699 ext. 268.
Sincerel
Chuck ipp
enclosure: Sample Results
cc. Gerald Hargutt
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 281 15
PHONE [phone] FAX [phone]
AN Eq UAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

COUNTY:
UNION
QUAD NO:
REPORT TO
MRO
COLLECTOR(S)
: PIPPIN
DATE:
1125/97
TIME:
PURPOSE:
LABORATORY ANALYSIS
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Ground Water Quality
SAMPLE PRIORITY
X❑ ROUTINE EMERGENCY
Regional Office X❑ CHAIN OF CUSTODY ❑
W❑ SAMPLE TYPE
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal 31616 /loom[
Coliforn: MFTotal 31504 /loom]
TOC mg/l
Turbitity NTU
Residue., Suspended 530 mg/L
Total Suspended solids mg/L
PH units
Alkalinity to pH 4.5 mg/L
Alkalinity, to pH 8.3 mg/L
Carbonate mg/L
Bicarbonate mg/L
Carbon dioxide mg/L
Chloride mg/L
Chromium: Hex 1032 ug/L
Color True 80 C.U.
Cyanide 720 mg/L
COMMENTS:
Owner:
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
JERRY CORDON
Diss. Solids 70300 mg/L
Fluoride 951 mg/L
Hardness: total 900 mg/L
Hardness: (non-carb) 902 mg/L
Phenols 32730 ug/L
Specific Cond. 95 umhos/cm2
Sulfate mg/L
Sulfide 745 mg/L
MBAS mg/L
Oil and Grease mg/L
Silica mg/L
Boron
Formaldehyde mg/L
X
NH3 as N 610 0.07 mg/L
X
TKN as N 625 0.3 mg/L
*
NO2 +NO3 as n 630 32 11WIL
P: Total as P 665 mg/L
PO4 mg/L
Ag-Silver 46566 ug/L
AI -Aluminum 46557 ug/L
As -Arsenic 46551 ug/L
Ba-Barium 46558 ug/L.
Ca -Calcium 46552 mg/L
Cd-Cadium 46559 ug/L
Cr-Chromium 46560 ug/L
Cu- Copper 1042 ug/L
X
Fe- Iron 1045 <50 ug/L
Hg- Mercury 71900 ug/L
K-Potassium 46555 mg/L
Mg- Magnesium 927 mg/L
X
Mn-Manganese 1055 270 ug/L
Na- Sodium 929 mg/L.
Ni-Nickel ug/L
Pb-Lead 46564 ug/L
Se -Selenium ug/L
Zn Zinc 46567 ug/L
Lab Number 7132548
Date Received
1126/97
Time Received
8;50
Received By
DS
Released By DS
Date reported : 1/5/98
Organochlorine Pesticides
Organ phosphorus Pesticides
Nitrogen Pesticides
I I Acid Herbicides I
IX I Volatile Organics (VOA bottle)
TPH-Gasoline Range
TPH-BTEX Gasoline Ramt
7G2548.NOV

EHNR/DWQ LABORATORY
VOLATILE ANALYTICAL REPORT
LAB NO.7G2548
REPORTED BY VA
CHECKED BY CG
REVIEWED BY CG
SAMPLE TYPE: WATER
ANALYSIS RESULTS
SUPERVISOR REK
DATE 12/2/97
ENTERED BY
DATE
75-35-4
1, 1 -Dichloroethene
.-W-=w
U
96-18-4
1,2,3-Trichloropropane
0.25 U
75-09-2
Methylene Chloride
10
U
108-86-1
Bromobenzene
1 U
156-60-5
trans-1,2-Dichloroethene
0.75
U
95-49-8
2-Chlorotoluene
0.25 U
75-34-3
1,1-Dichloroethane
0.25
U
106-43-4
4-Chlorotoluene
0.25 U
590-20-7
2,2-Dichloropropane
o.25
U
541-73-1
1,3-Dichlorobenzene
0.25 U
156-59-4
cis-1,2-Dichloroethene
0.25
U
106-46-7
1,4-Dichlorobenzene
0.25 U
67-66-3
Chloroform
0.25
U
95-50-1
1,2-Dichlorobenzene
0.25 U
74-97-5
Bromochloromethane
0.75
U
96-12-8
1,2-Dibromo-3-Chloropropane
1 U
71-55-6
TdiehtoToethane
U
120-82-1
1,2,4-Trichlorobenzene
0.25 U
563-58-6
1,1-Dichloropropene
0.25
U
87-68-3
Hexachlorobutadiene
0.25 U
56-23-5
Carbon Tetrachloride
0.75
U
87-61-6
1,2,3-Trichlorobenzene
0.75 U
107-06-2
1,2-Dichloroethane
0.25
U
1634-04-4
Methyl-tert-butyl ether
5 U
79-01-6
Trichloroethene
0.25
U
71-43-2
Benzene
1 U
78-87-5
1,2-Dichloropropane
0.25
U
108-88-3
Toluene
1 U
75-27-4
Bromodichloromethane
0.25
U
100-41-4
Ethyl benzene
1 U
74-95-3
Dibromomethane
1
U
108-38-3
m,p-Xylenes
2 U
10061-01-5
cis- 1,3-Dichloropropene
0.25
U
95-47-6
o-Xylene
1 U
10061-02-6
trans- 1,3-Dichloropropene
0.25
U
100-42-5
Styrene
1 U
79-00-5
1,1,2-Trichloroethane
0.25
U
98-82-8
Isopropylbenzene
1 U
127-18-4
Tetrachloroethene
0.25
U
103-65-1
n-Propylbenzene
1 U
142-28-9
1,3-Dichloropropane
0.25
U
108-67-8
1,3,5-Trimethylbenzene
1 U
124-48-1
Dibromochloromethane
0.75
U
98-06-6
tert-Butylbenzene
1 U
106-93-4
1,2-Dibromoethane
1
U
95-63-6
1,2,4-Trimethylbenzene
1 U
108-90-7
Chlorobenzene
0.25
U
135-98-8
sec- Butyl benzene
1 U
630-20-6
1,1,1,2-Tetrachloroethane
0.25
U
99-87-6
p-isopropyltoluene
1 U
75-25-2
Bromoform
0.5
U
104-51-8
n-Butylbenzene
1 U
79-34-5
1,1,2,2-Tetrachloroethane
0.75
U
91-20-3
Naphthalene
1 U
TQL- Target Quantitation Limit- Subject to
change due to instrument sensitivity
T- Tentatively Identified, not confirmed
E- Estimated Value
U- Samples analyzed for this compound but not detected
N- Sample not analyzed for this compound
D- Detected below quantitation limit
M- GC/MS Analysis performed
COMMENTS:
mg/L mg/L
Gasoline Range Estimated Total Petroleum Hydrocarbon 0.25 N
Other ouroeables detected Detected
(up to 10 highest peaks)
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.
ug/L

REPORTED BY PH
CHECKED BY NTG
REVIEWED BY PTD
SAMPLE TYPE: WATER
b&-0J-3
108-95-2
111-44-4
95-57-8
541-73-1
106-46-7
100-51-6
95-50-1
95-48-7
108-60-1
106-44-5
621-64-7
67-72-1
98-95-3
78-59-1
88-75-5
105-67-9
65-85-0
111-91-1
120-83-2
120-82-1
91-20-3
106-47-8
87-68-3
59-50-7
91-57-6
77-47-4
88-06-2
95-95-4
91-58-7
88-74-4
131-11-3
L208-96-8
EHNR/DWQ LABORATORY
SEMI -VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
LAB NO. 7G2548
SUPERVISOR REK
DATE 12/10/97
ENTERED BY
DATE
ANILINL
10
U
606-20-2
2,6-DINITROTOLUENE
10 U
PHENOL
10
U
99-09-2
3-NITROANILINE
50 U
BIS(2-CHLOROETHYL) ETHER
10
U
83-32-9
ACENAPHTHENE
10 U
2-CHLOROPHENOL
10
U
51-28-5
2,4-DINITRO PHENOL
50 U
1,3-DICHLOROBENZENE
10
U
100-02-7
4-NITRO PHENOL
50 U
1,4-DICHLOROBENZENE
10
U
132-64-9
DIBENZOFURAN
10 U
BENZYL ALCOHOL
20
U
121-14-2
2,4-DINITROTOLUENE
10 U
1,2-DICHLOROBENZENE
10
U
84-66-2
DIETHYL PHTHALATE
10 U
2-METHYL PHENOL
10
U
7005-72-3
4-CHLOROPHENYL PHENYL ETH
10 U
BIS(2-CHLOROISOPROPYL) ETHER
10
U
86-73-7
FLUORENE
10 U
4-METHYL PHENOL
10
U
100-01-6
4-NITROANILINE
50 U
N-NITROSO-DI-N-PROPYLAMINE
10
U
534-52-1
4,6-DINITRO-2-METHYL PHENOL
50 U
HEXACHLOROETHANE
10
U
86-30-6
N-NITROSODIPHENYLAMINE
10 U
NITROBENZENE
10
U
101-55-3
4-BROMOPHENYL PHENYL ETHE
10 U
ISOPHORONE
10
U
118-74-1
HEXACHLOROBENZENE
10 U
2-NITRO PHENOL
10
U
87-86-5
PENTACHLORO PHENOL
50 U
2,4-DIMETHYL PHENOL
10
U
85-01-8
PHENANTHRENE
10 U
BENZOIC ACID
50
U
120-12-7
ANTHRACENE
10 U
BIS(2-CHLOROETHOXY) METHANE
10
U
84-74-2
DI-N-BUTYL PHTHALATE
10 U
2,4-DICHLORO PHENOL
10
U
206-44-0
FLUORANTHENE
10 U
1,2,4-TRICHLOROBENZENE
10
U
129-00-0
PYRENE
10 U
NAPHTHALENE
10
U
85-68-7
BUTYLBENZYL PHTHALATE
10 U
4-CHLOROANILINE
20
U
91-94-1
3,3'-DICHLOROBENZIDINE
20 U
HEXACHLOROBUTADIENE
10
U
56-55-3
BENZO(A)ANTHRACENE
10 U
4-CHLORO-3-METHYL PHENOL
20
U
218-01-9
CHRYSENE
10 U
2-METHYL NAPHTHALENE
10
U
117-81-7
BIS(2-ETHYLHEXYL) PHTHALATE
10 U
HEXACHLOROCYCLOPENTADIENE
10
U
117-84-0
DI-N-OCTYL PHTHALATE
10 U
2,4,6-TRICHLORO PHENOL
10
U
205-99-2
BENZO(B)FLUORANTHENE
10 U
2,4,5-TRICHLORO PHENOL
10
U
207-08-9
BENZO(K)FLUORANTHENE
10 U
2-CHLORO NAPHTHALENE
10
U
50-32-8
BENZO(A)PYRENE
10 U
2-NITROANILINE
50
U
193-39-5
INDENO(1,2,3-CD)PYRENE
10 U
DIMETHYL PHTHALATE
10
U
53-70-3
DIBENZO(A,H)ANTHRACENE
10 U
ACENAPHTHYLENE
10
U
191-24-2
BENZO(G,H,I)PERYLENE
10 U
NO BASEINEU
DETECTED BY
COMMENTS:

SEMIVOLATILE ORGANICS REPORT - DWQ LAB PAGE 2
RAL OR ACID EXTRACTABLE ORGANICS
GC/MS.
FOUR OF SIX SURROGATE STANDARDS
ABOVE QC LIMITS. SIX OF ELEVEN
MATRIX SPIKE STANDARDS ABOVE QC
LIMITS.
LAB NO. 7G2548
TQL- Target Quantitation Limit- Subject to
change due to instrument sensitivity
T- Tentatively Identified, estimated concentration
E- Estimated Value
U- Samples analyzed for this compound but not detected
N- Sample not analyzed for this compound
D- Detected below quantitation limit
H- Holding time exceeded

fiat*s� of CG=! a' 7- ar `.
Tel eonor -
Directions to Site:
Nature of Comolaint:
C,Aj
grid, (LA"—
- Tv� � ��.� - ��►. cam_ 'Irlf
Received
Ia lns��
Date;%�—
'C
Time: ._.._
Investigated BL:
Corresoondence Pre yared BY:
Date(s)'of Investigations -----------
Date (s) of Report:

JAMES B. HUNT JR.
GOVERNOR Jerry Gordon
t 5516 Paigeland Road
Monroe, North Carolina 28112
. ',,WAYNE McDEvrrr
'SECRETARY `f
Subject:
Dear Mr. Gordon,
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
March 16, 1998
Well Water Sample Results
On February 16, 1998, I sampled your new well at 5516 Paigeland Road, Monroe,
North Carolina. The well water sample was tested for nitrates. The sample results
represent conditions in the well at the time of sampling. The level of nitrates
(NO3+NO2) in the well water sample was 4.4 parts per million. The drinking water
standard for nitrates is 10 parts per million. I am continuing my investigation of the
- groundwater in the area. I will keep you informed of any new information. Should you
have any questions please call me at 704-663-1699 ext. 268.
enclosure: Sample Results
cc. Gerald Hargutt
7
Sincerel
Chuck Pippin, P.G.
Hydrogeologic Technician
�� �`
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 281 15
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/1 Oq POST -CONSUMER PAPER

COUNTY
UNION
QUAD NO
REPORT TO :
MRO
COLLECTOR(S)
PIPPIN
DATE
2/16/98
TIME
PURPOSE:
LABORATORY ANALYSIS
COMMENTS
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Ground Water Quality
SAMPLE PRIORITY
El ROUTINE EMERGENCY
Regional Office X❑ CHAIN OF CUSTODY
W❑ SAMPLE TYPE ❑
Owner JERRY GORDAN
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
Diss. Solids 70300 m./L
Fluoride 951 mg/L,
_
I lardness: total 900 mg/L
I lardness: (non-carb) 902 mg/L
Phenols 32730 ug/L
Specific Cond. 95 umhos/cm2
Sulfate mg/L
Sulfide 745 mg/L
AIBAS mg/L
Oil and Grease mg/L
Silica mg/L
Boron
Formaldehyde mg/L
X
N113 as N 610 <0.01 mg/L
X
IKN as N 625 0.1 mg/L
X
NO2 +NO3 as n 630 4.4 mg/L
P Total as P 665 mg/L
1'04 mg/L
Ag-Silver 46566 ug/L
AI -Aluminum 46557 ug L
As -Arsenic 46551 ug/L
Ba-Barium 46558 ug/1
Ca -Calcium 46552 mg/L
Cd-Cadium 46559 ug/L
Cr-Chromium 46560 ug/L
Cu- Copper 1042 ug/L
Fe- Iron 1045 ugfL
Hg- Mercury 71900 ug/L
R-Pumssium 46555 mg/1
Mg- Magnesium 927 mg/L
Mn-Manganese 1055 ug/I,
Na- Sodium 929 mg/L
Ni-Nickel ug/L
Pb-Lead 46564 ug/L
Se -Selenium ugh
Zn_Zinc 46567 ug/L
oy
IvA'j'Ui URAY,7W
`SOURCES
MAR12991
Lab Number :
8G0406
Date Rccci"j
-2)17l98
Time Received
900 AM
Received By
DS
Released By : DS
Date reported : 3/10/98
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
Semivolaliles
TPH-Diesel Range
Volatile Organics (VOA bottle)
TPH-Gasoline Range
71'1I-10 EX Gasoline Range
:A.91rMIR vI';".SEMI
ri L of fICE
6G0406.FEB

UNDWATER FIELD/LAB FORM pll'WiuP(l
North Carolina
Department of Environment, Health, and Natural Resources
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
F
niy 1) /UJ-O/t/ SAMPLE TYPE AM 'RIORITY
Lab Number _
Quad No_V ��" �- Serial No. ❑Water outine
Lat. `f �Z 2C��7/ Long. 10 ? 1 El soil ❑ Emergency Dale Received
❑ Other Rec'd by:Aa
Other:
Report To: ARO, FRO�RRO, WaRO, WiRO, El chain of Custody Data Entry By: Ck:
WSRO, Kinston FO, F Trust, Central Off., Other: Date Reported:
Shipped by: Bus, Hand Del., Other
Purpose:
Collector(s): Dated ' /6 Time Z�70C� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
F I E L I A A E�(c rile one)
Abyt�, � Owner r r� 0 ,�
pH400 Spec. Cond.94 at 250 C Location or site I (o
Temp.10 oC Odor Description of sampling poiinnt� g P
Appearance Sampling Method Z�� and ism, -;l- Sample Interval_
Field Y� Remarks
Analysis B (Pump, baler, etc)
Y
LABORATORY ANALYSES (pumpug lime, air lemp etc)
Diss. Solids 70300 m /I
Flouride 951 m /I
A - Silver 46566 u /I
At - Aluminum 46557 u /I
Hardness: Total goo m /I
As - Arsenic 46551 u /I
Hardness non-carb 902 m /I
Ba - Barium 46558 u /I
Phenols 32730 u /I
Ca - Calcium 46552 m /I
fi Mh ni'
Cd - Cadmium 46559 u 1/I
Sulfate 945 rn /I
Cr - Chromium 46560 u /I
Sulfide 745 m /I
Cu - Copper 46562 u /I
Fe - Iron 46563 u /I
Oil and Grease m ll
Hg - Mercury 71900 ug/I
K - Potassium 46555 rng/I
M - Magnesium 46554 m /I
Mn - Manganese 46565 u /I
NH as N 610 rn /I
Na - Sodium 46556 rn /I
NO + NO as N 630 nl /I
Pb - Lead 46564 u /I
P: Total as P 665 m /I
Se - Seleniurn u /I
Zn - Zinc 46567 u /I
Lab Comments:
GW-54 REV. 7/96 For Dissolved Analysis - submit filtered sample and write "DIS" in ble
VTI_�)Time
_ From: Bus ouri , Hand Del.,
Organochlorine Pesticides
Organophospho.rus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCB's
Sernivolatile Organics
TPH - Diesel Range
Volatile Organics (VOA bottle)
TPH - Gasoline Range
TPH - BTEX Gasoline Ranee

7-2
Sf elegy
MW --,, 057,E lo�t/T,f1,rs_�ti�rt�v
/- /,.(, 0
GG,;�IZ : ) 1! -2s -�) : kt)� = 3.-�[12-16-W ; k6t = 0?6
/ i�i2laCi . 41b
(D 2�/ t�ISro���iT��> �Ul� �fr�l€� �f �= ki !�✓�
I I�o,2tki ) fi

-i _

4
NCDENR
JAMES B. HUNT JR. Jerry Gordon
GOVERNOR 5516 Paigeland Road
Monroe, North Carolina 28112
WAYNE MCDEVITT
SECRETARY
Subject:
Dear Mr. Gordon,
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
February 4, 1998
Well Water Sample Results
On February 4, 1998, I received Dr. Rudo's health risk evaluation for the well
water sample collected on November 25, 1997. Dr. Rudo recommends that the water not
be used for drinking or cooking purposes. I will be returning to sample your well and
others in the area. I will keep you informed of any significant findings. Should you have
any questions please call me at 704-663-1699 ext. 268.
Sincere ,
Chuck Pippin, P.G.
Hydrogeologic Technician
enclosure: health risk evaluation
cc. Gerald Hargutt
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 28115
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY/AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER
Cif

d .r+ SrATF o
1 3
North Carolina
Department of Health and Human Services arGsv�L�
Division of Epidemiology
P.O. Box 29601 • Raleigh, NC 27626-0601
James B. Hunt Jr., Governor
DATE Z y
MEMORANDUM
H. David Bruton, M.D., Secretary
TO: bye V h
���� �i�� ,v �S � 1
FROM: Kenneth Rudo, Ph.D., Toxicologist
Medical Evaluation and Risk Assessment Branch
Occupational and Environmental Epidemiology Section
SUBJECT:
)s►Ll��j��s�e�
Attached is the Occupational and Environmental Epidemiology Section's drinking water health -
risk evaluation for the well water sample from the above site. Recommendations for continued
water use are also provided.
If you have any questions, please call me at [phone].
KR/rm
North Carolina: Host of the 1999 Special Olympics World Summer Games

COUNTY:
UNION
QUAD NO:
REPORT TO :
MRO
COLLECTOR(S)
: PIPPIN
DATE:
11/25/97
TIME:
PURPOSE:
LABORATORY ANALYSIS
Regional Office
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L
Coliform: MF Fecal 31616 /loom]
Coliform: MF Total 31504 /loom]
I urbnny NTU
Residue., Suspended 530
mg/L
Total Suspended solids
mg/L
PH
units
Alkalinity to pH 4.5
mg/L
Alkalinity to PH 8.3
Bicarbonate mg/L
Carbon dioxide mg/L
Chloride mg/L
Chromium: Hex 1032 ug/L
Color: True 80 C.U.
Cyanide 720 mg/L
"OMMENTS :
Owner
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Ground Water Quality
SAMPLE PRIORITY
X�ROUTINE EMERGENCY
X❑ CHAIN OFCUSTODY ❑
l SAMPLE TYPE
JF.RRY GORDON
Diss. Solids 70300 mg/L
Fluoride 951 m9/L
Hardness: total 900 mg/L
Hardness: (non-carb) 902 mg/L
Phenols 32730 ug/L
Specific Cond. 95 umhos/cm2
Sulfate mg/L
Sulfide 745 mg/L
MBAS mg/L
Oil and Grease mg/L
Silica mg/L
Boron
Formaldehyde mg/L
X
NH3 as N 610 0.07 mg/L
wglbfffda- .' 32 *mg/L'
P: Total as P 665 mg/[,
tiall
PO4 mg/L
Ag-Silver 46566 ug/L
AI -Aluminum 46557 ug/L
As -Arsenic 46551 ug/L
Ba-Barium 46558 ug/L
Ca -Calcium 46552 mg/L
Cd-Cadium 46559 ug/L
Cr-Chromium 46560 ug/L
Cu- Copp" 1042 ug/L
X
Fe -Iron 1045 <50 ug/L
fig- Mercury 71900 ug/L
K-Potassium 46555 mg/L
Mg- Magnesium 927 mg/L
X
Mn-Manganese 1055 270 ug/L
Na- Sodium 929 mg/L
Ni-Nickel ug/L
Pb-Lead 46564 ug/L
Se -Selenium ug/L
Zn Zinc 46567 ug/L
Lab Number 7G2548
Date Received
11126/97
J�
Time Received
8;50
Received By
DS
Released By : DS
Date reported : 1/5/98
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
I I Acid Herbicides I
IX I Volatile Organics (VOA bottle)
TPH-Gasoline Range
TPH-BTEX Gasoline Range
7G2548.NOV

North Carolina Department of Environment, Health, and Natural Resources
Division of Epidemiology
Occupational and Environmental Epidemiology Section
Medical Evaluation and Risk Assessment Branch
Drinking Water Health Risk Evaluation
General
NI C,., County
DATE LABORATORY NUMBER
() Based on these analytical results, this water should be considered safe for normal usage.
() Chemical analysis did not show any contamination. Water should be resampled if odor or taste
persists.
(X) The water should not be used for drinking or cooking purposes.
() Based on these analytical results, this water is highly contaminated and should not be used for
drinking, cooking, or bathing/showering.
() The laboratory results are not conclusive, please resample.
PLEASE INDICATE ON LAB SHEET THAT IT /S A RESAMPLE AND PROVIDE PREVIOUS
SAMPLES NUMBER(S)
(X) COMMENTS:
The nitrate drinking water standard is 10 pgm The nitrate level in your well water is either above or close
to the drinking water standard Continued consumption especially for pregnant women or infants six
months of age and younger, may pose an increased health risk based on these nitrate levels
For further information, contact Dr. Ken Rudo, Occupational and Environmental Epidemiology Section,
[phone].
DEHNR 3891 (1/96)
Occupational and Environmental Epidemiology Section (Review 1/97)

MEMORANDUM TO:
FROM:
DIVISION OF WATER QUALITY
January 16, 1998
Dr. Ken Rudo
Chuck Pippin
SUBJECT: Request for Health Risk Evaluation
for Well Sampling Results
Staff of the Mooresville Regional Office requests that a health risk evaluation for
sampling results from water supply wells be completed and sent to our Office. Your
evaluation will be sent to the well owner by the MRO.
If you have questions or need additional information, please contact me at (704)
663-1699.
Attachment (s): Sampling Results

COUNTY.
UNION
QUAD NO
REPORTTO :
MRO Regiona1011ice
COLLECTOR(S)
PIPPIN
DATE:
11/25/97
TIME
_
PURPOSE Ow
LABORATORY ANALYSIS
BOD 310 mgl1,
COD Iligh 340 mWL
COD Low 335 mg/L
Coliform: hIF Fecal 31616 /IOOmI
Coliform: NIF Total 31504 /100ml
TOC mg/l
Turbitity NTU
Residue., Suspended 530 mg/L
Total Suspended solids mg/L
PH units
Alkalinity to pH 4.5 mg/L
Alkalinity to pl1 8 3 mg/L
Carbonate mg%L
Bicarbonate mg,L
Carbon dioxide mgiL
Chloride mu,L
Chromium Ilea 1032 uat
Color True 80 cu
Cyanide 720 mg1L
COMMENTS:
net
Location or Site
Description of sampling point
Sampling Method
Remarks:
DIVISION OF \VATER QUALITY
Chemisf- Laboratory Report / Cround Water Qualify
SAMPLE PRIORITY
ROUTINE EMERGENCY
] CHAIN OF CUSTODY
FISANIPLE TYPE ❑
JERRY GORDON
Uiss. Solids 70300 mg/L
Fluoride 951 mg/L
Hardness: total 900 mg/L
Hardness:(non-carb)902 mg/L
Phenols 32730 ugfL
Specific Cond. 95 umhos/em2
Sulfate mg/L
Sulfide 745 mg/L
MBAS mg/L
Oil and Grease mg/L
Silica mg/L
Boron
Formaldehyde mg/L
X
NM as N 610 0.07 mg/L
X
TKN as N 625 0.3 mg/L
X
NO2 +NO3 as n 630 32 tng/L
P Total as P 665 mail
PO4 mu/L
Ag-Silver 46566 ug/L
AI -Aluminum 46557 ug/L
As -Arsenic 46551 ug/L
Ba-Barium 46558 ug/L
Ca -Calcium 46552 mg/L
Cd-Cadium 46559 ug/L
Cr-Chromium 46560 ug/L
Cu- Copper1042 ug/L
X
Fe -Iron 1045 <50 ug/L
Hg- Mercury 71900 ug/L
I< -Potassium 46555 me/L
Nlg- Magnesium 927 mg/L
X
Nln-Nlanganese 1055 270 ug/L
Na- Sodium 929 mg/L
Ni-Nickel ug/L
Pb-Lead 46564 ug/L
Se -Selenium ug/L
Zn Zinc 46567 ug/L
Lab Number
7(;i2548
Date Received
11/26/97
Time Received
8,50
Received By :
DSnpt,
Released By DS
Datc tcpurtcd 1/5/98
Organochlorine Pesticides
Organophosphorus Pesticides
Nitrogen Pesticides
Acid Herbicides
X Semivolatiles
TPH-Diesel Range
X Volatile Organics (VOA bottle)
TPII-Gasoline Range
TPH-BTBX Gasoline Ranee
7G2548 NOV

GROUNDWATER FIELD/LAB FORM
County 0 /JIU
Ouao 61 � �
¢jNSerial No.
Lat. q 5)- ,2(-. N Long. 62 2-7 1-2. ,.34i
North Carolina
R t Department of Environment, Health, and Natural Resources f DIVISION OF WATER QUALITY - GROUNDWATER SECTION
Lab Number
0 Date Received I Time
Rec'd by: rom: Bu ourie , Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
Purpose:
_ Baseline, Complaint, Compliance LUST P
Owner CO oA) urisone)'
esticide Study, Federal Trust, Other:
G��Q� (�
pHSpec._Spec. Cond.94 at 250 C Location or site u: e 7 a,
Tem oC Odor o A)E / D'`
p'r , Description of sampling point �,51
Appearance Sampling Method
Field Analysis By: Remarks (Puma. �l�. eiic_ Sample Interval
LAB RAT0 RY :AN E Ownrlo�firvill.akImp. etc.)
BOD, 310 ,, 7 1 1 I_ _ .
A P A
ater o.utine
❑ Soil ❑ Emergency
❑ Other
Report To: ARO, FRO, , RRO, WaRO, WiRO,[[.[D16hain of Custody
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus, r and Del., Other-
Collector(s): Date 11'�S �17 Time
I q
yU H)gn 340 mg/I
tOpl. Low 335 /I
oliform: MF Fecal 31616 1 I
Coliform: MF Total 31 /1 I
TOC 680 m I
Turbidity 76 NTU
Residue., Suspended 530 mg/I
pH 403
unit
Alkalinity to pH 4.5 410
mg)
Alkalinity to pH 8.3 415
mg/
Carbonate 445
mg/
Bicarbonate 440
m /
Carbon dioxide 405
mg/
Chloride 940
Mg/I
Chromium: Hex 1032
ug/I
Color: True 8o
CU
Cyanide 720
mg/I
Lab Comments:
GW-54 REV. 7/9r' For Dissolved Analysis - submit filtered sample and write "DIS" in blo,
Pesticides
rus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCB's
Semivolatile Organics
TPH - Diesel Range
Volatile Organics (VOj
TPH - Gasoline Rang
TPH - BTEX Gasoline

EHNR/DWQ LABORATORY LAB NO. 7G2548
1 REPORTED BY VOLATILE ANALYTICAL REPORT
q� J,
CHECKED BY SUPERVISOR�C'1�
REVIEWED BY DATE y_.
SAMPLE TYPE
WATER
ENTERED B
ANALYSIS
RESULTS
DATE
CAS#
VOA TARGET COMPOUND
CL
DETECTEI3 :
QAS#
—
>
vER TARG�7;COMP(7E3Np
#
ETEGTEp
--
--
09
ug(L
75-35-4
1,1-Dichloroethene
0.75
U
75-09-2
Methylene Chloride
10
96-18-4
1,2,3-Trichloropropane
0.25
U
156-60-5
trans- 1,2-Dichloroethene
0.75
U
108-86-1
Bromobenzene
1
U
75-34-3
1, 1 -Dichloroethane
0.25
U
95-49-8
2-Chlorotoluene
0.25
U
590-20-7
2,2-Dichloropropane
0.25
U
106-43-4
4-Chlorotoluene
0 25
U
156-59A
cis-1,2-Dichloroethene
0.25
U
541-73-1
1,3-Dichlorobenzene
0.25
U
67-66-3
Chloroform
0.25
U
106-46-7
1,4-Dichlorobenzene
0 25
U
74-97-5
8romochloromethane
0.75
U
95-50-1
1,2-Dichlorobenzene
0.25
U
71-55-6
1. 1, 1 -Trichloroethane
0.25
U
96-12-8
1,2-0ibromo-3-Chloropropane
1
U
563-58-6
1. 1 -Dichloropropene
0.25
U
120-82-1
1,2,4-Trichlorobenzene
0.25
U
56-23-5
Carbon Tetrachloride
0.75
U
87-68-3
Hexachlorobutadiene
p 25
U
107-06-2
1,2-Dichloroethane
0.25
U
87-61-6
1,2,3-Trichlorobenzene
0.75
U
79-01-6
Trichloroethene
U
1634-04-4
Methyl-lert-butyl ether
5
U
78-87-5
1,2-Dichloropropane
0.25
0.25
U
71-43-2
Benzene
1
U
75-27-4
Bromodichloromethane
0.25
U
108-88-3
Toluene
1
U
74-95-3
Dibromomethane
1
U
100-41-4
Ethyl benzene
1
U
10061-01-5
cis-1,3-Dichloropropene
025
U
108-38-3
m,p-Xylenes
2
U
10061-02-6
trans- 1.3-Dichloropropene
0.25
U
U
95-47-6
o-Xylene
1
U
79-00-5
1.1,2-Trchloroethane
0.25
U
100-42-5
Styrene
1
U
127-18-4
Tetrachloroethene
0.25
98-82-8
Isopropylbenzene
1
U
142-28-9
1,3-Dichloropropane
0.25
U
103-65-1
n-Propylbenzene
1
U
124A8-1
Dibromochloromelhane
0.75
U
108-67-8
1.3,5-Trim ethyl benzene
1
U
106-93-4
1,2-Dibromoethane
1
U
98-06-6
tert-Butylbenzene
1
U
108-90-7
Chlorobenzene
0.25
U
95-63-6
1,2,4-Trimethylbenzene
1
U
630-20-6
1. 1, 1,2-Tetrachloroethane
0.25
U
135-98-8
sec-Butylbenzene
1
U
75-25-2
Bromoform
0.5
U
99-87-6
p-isopropyltoluene
1
U
79-34-5
1,1,2,2-Tetrachloroethane
0.75
U
104-51-8
n-Butylbenzene
1
U
U
91-20-3
Naphthalene
1
U
TQL- Target Quantilation Limit- Subject to
change due to instrument sensitivity
T- Tentatively Identified, not confirmed
E- Estimated Value
U- Samples analyzed for this compound but not detected
N- Sample not analyzed for this compound
D- Detected below quantitation limit
M- GC/MS Analysis performed
COMMENTS:
mg/L mg/L
iasoline Range Estimated Total Petroleum Hydrocarbon 0.25
Ithorn nki—
(up to 10 highest peaks) V U ug/L d
ug/L
NO VOLATILE ORGANIC COMPOUNDS
DETECTED BY GC/ELCD/PID.

REPORTED BY
CHECKED BY
REVIEWED BY
SAMPLE TYPE: WATER
62.53-3
108-95-2
11 1-44-4
95.57-8
541-73.1
106-46-7
100-51-6
95-50-1
95-48-7
108.60-1
106.44.5
621-64-7
67-72-1
98-95-3
78-59-1
88-75.5
105-67-9
65-85-0
111-91-1
120.83-2
120-82-1
91-20-3
106.47.8
87-68-3
59-50-7
91-57.6
77-47-4
88-06.2
95.95-4
91-58-7
88.74-4
131-11-3
208-96-8
ANILINE
PHENOL
BIS(2-CHLOROETHYL) ETHER
2-CHLOROPHENOL
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
BENZYL ALCOHOL
1,2-DICHLOROBENZENE
2-METHYL PHENOL
BIS(2-CHLOROISOPROPYL) ETHER
4-METHYL PHENOL
N-NITROSO-DI-N-PROPYLAMINE
HEXACHLOROETHANE
NITROBENZENE
ISOPHORONE
2-NITRO PHENOL
2,4-DIMETHYL PHENOL
BENZOIC ACID
BIS(2-CHLOROETHOXY) METHANE
2,4-DICHLORO PHENOL
1,2,4-TRICHLOROBENZENE
NAPHTHALENE
4-CHLOROANILINE
HEXACHLOROBUTADIENE
4-CHLORO-3-METHYL PHENOL
2-METHYL NAPHTHALENE
HEXACHLOROCYCLOPENTADIENE
2,4,6-TRICHLORO PHENOL
2,4,5-TRICHLORO PHENOL
2-CHLORO NAPHTHALENE
2-NITROANILINE
DIMETHYL PHTHALATE
ACENAPHTHYLENE
EHNR/DWQ LABORATORY
SEMI -VOLATILE ANALYTICAL REPORT
ANALYSIS RESULTS
10
U
606-20-2
10
2,6-DINITROTOLUENE
10
U
99-09-2
3-NITROANILINE
10
U
83-32 -9
ACENAPHTHENE
10
U
51-28-5
2,4-DINITRO PHENOL
10
U
100-02-7
4-NITRO PHENOL
20
U
132-64-9
DIBENZOFURAN
10
U
121-14-2
2,4-DINITROTOLUENE
10
U
84-66-2
DIETHYL PHTHALATE
10
U
7005-72 -3
4-CHLOROPHENYL PHENYL ETHER
10
U
86-73-7
FLUORENE
10
U
100-01-6
4-NITROANILINE
10
U
534-52-1
4,6-DINITRO-2-METHYL PHENOL
10
U
86-30-6
N-NITROSODIPHENYLAMINE
10
U
101-55-3
4-13ROMOPHENYL PHENYL ETHER
10
U
118-74-1
HEXACHLOROBENZENE
10
U
87-86-5
PENTACHLORO PHENOL
50
U
85-01-8
PHENANTHRENE
10
U
120-12-7
ANTHRACENE
10
U
84-74 -2
DI-N-BUTYL PHTHALATE
10
U
206-44-0
FLUORANTHENE
10
U
129-00-0
PYRENE
20
U
85.68-7
BUTYLBENZYL PHTHALATE
10
U
91-94-1
3,3'-DICHLOROBENZIDINE
20
U
56-55-3
BENZO(A)ANTHRACENE
10
U
218-01-9
CHRYSENE
10
U
U
117-81-7
BIS(2-ETHYLHEXYL) PHTHALATE
10
117-84 -0
DI-N•OCTYL PHTHALATE
10
U
205-99-2
BENZO(B)FLUORANTHENE
10
U
U
207-08-9
BENZO(K)FLUORANTHENE
50
U
50-32-8
BENZO(A)PYRENE
10
U
193-39-5
INDENO(1,2,3-CD)PYRENE
10
U
53-70.3
DIBENZO(A,H)ANTHRACENE
191-24-2
BENZO(G,H,I)PERYLENE
LAB NO. 7G2548
SUPERVISOR
DATE j t
ENTERED BY
DATE 7
10
50
10
50
50
10
10
10
10
10
50
50
10
10
10
50
10
10
10
10
10
10
20
10
10
10
10
10
10
10
10
10
10
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U

SEMIVOLATILE ORGANICS REPORT - DWQ LAB PAGE 2 LAB NO. 7G2548
} S�rri=�ltitati es cor;paintis refecttl >;:>'�ie�ttl
up to 20 jtigiiest peaks} g
NO BASE/NEUTRAL OR ACID EXTRACTABLE ORGANICS
DETECTED BY GC/MS.
TQL- Target Quantitation Limit- Subject to
change due to instrument sensitivity
T- Tentatively Identified, estimated concentration
E- Estimated Value
U- Samples analyzed for this compound but not detected
N- Sample not analyzed for this compound
D- Detected below quantitation limit
H- Holding time exceeded
COMMENTS: FOUR OF SIX SURROGATE STANDARDS
ABOVE QC LIMITS . SIX OF ELEVEN
MATRIX SPIKE STANDARDS ABOVE QC
LIMITS.

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF LABORATORY SERVICES
N.C. DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
306 N. WILMINGTON ST. — P.O. Box 28047, RALEIGH, 27611-8047
INORGANIC CHEMICAL ANALYSES -PRIVATE WATER SYSTEM
Complete
All Items Above Heavy Line
N
(See Instructions on Reverse Side)'t5
NOV 2 41997
E �
Name of
System JN'ee Dc,)
I }-----�--
Source of Water:
i;,:;'•..'•' ir30.Nl HEAt7m ^
Address - / r A �.
�tt'
(X 1 Ground
( ) Surface
( )
Purchased
�r%�<✓� /—'
ZIP
-L
Source of Sample:
County (J �J ( D LJ
( 1 House Tap
l X 1 Well Tap
Report To:
Type of Sample:
�OfCOtMlYiEAIlNt>E!N!}�
( ) Raw
( 1
Treated
Address:
SIX)MiiNWASE
Type of Treatment:
( ) None
( 1
Lime
( ) Chlorinated
( 1
Soda Ash
ZIP _
( ) Fluoridated
( 1
Polyphosphate
Filtered_
-( )
Water Softener
Collected By: 62W do e lei a
So<)
( ) Alum
( )
Other
AM
Type of Analysis Desired:
Date Collected: f — l[- �i; % Time: "`
Regular Parameters ', ( )
Parameters
Both
Location of Sampling Point: '
( 1 Optional
Remarks:(Z)uS Pec CC vi`a.�w..r t C^�l iaGry i f�G ► Ct4` " i� ' i\ l �izC;�� .
Regular Parameters
Results
Optional Parameters (List as needed — See SCOPE)
r Results i
pH
units
Arsenic
mg/I
Lead
mg/1
Iron
mg/I
Manganese
mg/I
0 S
,
Copper
mg/I
Zinc
mg/I
Calcium
mg/I
Magnesium
mg/I
Hardness-CaCO3 (Ca, Mg)
mg/I
Alkalinity-CaCO3
mg/I
Chloride
mg/I
Fluoride
mg/I
Date Received
Date Analyzed
DEHNR - 1441 (Rev. 1/93)
Laboratory Services
Date Reported ' Reported By
Laboratory Number

R
INSTRUCTIONS
Using typewriter or ball point pen, fill in all requested information on the top portion of form front.
Please pri^t legibly if typewriter is not available.
SAMPLE COLLECTION
1) Remove the one 1-quart plastic container and inflate by mouth, if uninflated.
2) Let the water (to be sampled) run for 5 minutes to assure that the water is from the distributior.
system.
3) Rinse the plastic container two or three times, and discard the water.
4) After rinsing, fill the containerto within approximately one inch of top of the sampling container.
Then cap the container securely.
SAMPLE SHIPMENT:
1) After collection of the sample, place the one 1-quart sampie into the cardboard box along with
the report form, then seal.
2) Mail immediately to the State Laboratory using the supplied labe?.
RECOMMENDED LIMITS FOR DRINKING WATEF ARE LISTED BELOW:.
ph Not less than 6.5 units : a?c:... Nc estabiished limiis
Alkalinity No established limits ivlacnesium N-0 estab?isne'd limits
Hardness No established limits Fluoride ^ mc.'i
Iron 0.30 mg;! Arsenic 0.05 mg.Y r
Manganese 0.05 mg."I Lead 0.016 mg -'I
Chloride 250 mg/l Zinc 5.0-0 m5'
Coppe; 1.3 mg;'I
FOR LABORATORY USE ONLY
r

ICC. DEff. OF HEALTH
.,
RaWNMENT,
h NATURAL RUSOU"
DEC 4 1997 �otth M a!n s
r
o �rth0
UnionConnt h G�,oN 011
J �
Health Department oC"
704/283-3553
c�
NC ?
December 2, 1997
Jerry Gordon
5516 Pageland Highway
Monroe, North Carolina 28112
Dear Mr. Gordon:
The purpose of this letter is to inform you that the water
sample that you requested was collected on November 19, 1997 from
the well system serving the Gordon residence located at 5516
Pageland Highway, Monroe, NC. The sample was examined by the Union
County Health Department laboratory for the presence of coliform
bacteria. The P/A (presence/absence) test indicated that this
sample was positive for the presence of coliform bacteria. The
further examination of this sample with ultraviolet fluorescence
indicated that the sample was positive for the presence of
E. Coli, which are associated with fecal contamination.
The presence of coliform bacteria exceeds current
Environmental Protection Agency Drinking Water Standards. Any
water which exceeds these standards should be disinfected or boiled
prior to use for drinking or cooking.
If you have any questions, you can reach me at 292-2548
generally between 8 and 9:00 a.m., Monday through Friday.
Sincerely,
� CJ iMk
David J. uneycut
Environmental Health Specialist
Environmental Health Division
DJH/mme
CC: Chuck Pippen, Mooresville Groundwater Division

JAMES B. HUNT JR.
GOVERNOR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
March 17, 1998
Gerald Hargette
3017 High Ridge Church Road
Marshville, North Carolina 28103
RE: Groundwater Investigation
Dear Mr. Hargette:
On February 16, 1998, I sampled your well and Mr. Gordon's new well. Both
well water samples showed that nitrates (NO3+NO2) were present at the time of sampling.
The nitrate levels in your well were 26 parts per million and those in Mr. Gordon's well
were 4.4 parts per million. The drinking water standard for nitrate is 10 parts per million.
I have enclosed an access agreementfor per" is ion to install monitoring wells on
your property. The monitoring wells will try to determine the source for the nitrate
contamination. I believe the high levels of nitrates in the groundwater are a result of
either cumulative applications of chicken liter to the surrounding fields or the nitrates
have infiltrated through the chicken house floor to the groundwater table. The sample
results from the monitoring wells should provide enough information to determine if the
nitrates are coming from a point source (i.e. the chicken house) or from the application of
chicken liter to the surrounding fields. Presently, I do not believe the hog lagoon is the
source for the nitrate contamination of the groundwater, since hog wastes are much lower
in nitrate concentrations than chicken wastes; however, I have not ruled the hog lagoon
out.
Upon receipt of the access agreement I will schedule a date for the state's drill
crew to come to the site and begin work. I will keep you informed of the drilling date and
any sample results. Should you have any questions please call me at 704-663-1699 ext.
268.
Sincerel
Chu ippm, P.G.
Hydrogeologic Technician
cgp/hargette.1tr
enclosure: Access Agreement, Site Map
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 28115
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Chuck Pippin
Hydrogeologic Technician
DENR/DEM/Groundwater Section
919 North Main Street
Mooresville, North Carolina 28115
RE: Agreement for the Use of a Site for a
Groundwater Investigation
Gerald Hargete Property
Hargette Road, Monroe
Union County, N.C.
Dear Mr. Pippin:
I/We am/are the owner(s) of a parcel of property, as described in Attachment 1,
and hereby permit the Department of Environment and Natural Resources (henceforth
referred to as the Department) to enter upon the groundwaters under the authority of G.S.
143-215.3(a)2.
I/We am/are granting permission with the understanding that:
1. The investigation shall be conducted by the Groundwater Section of the
Department's Division of Water Quality.
2. The costs of construction and maintenance of the site and access shall be
born by the Department. The Department shall protect and prevent
damage to the surrounding lands.
3. Unless otherwise agreed, the Department shall have access to the site by
the shortest feasible route to the nearest public road. The Department may
enter upon the land at reasonable times and have full right of access during
the period of the investigation.
4. At the end of the investigation, unless otherwise provided for by prior
written agreement, the Department shall remove from the site all structures
placed or erected by it and shall permanently abandon all wells constructed
by it.
5. Any claims which may arise against the Department shall be governed by
Article 31 of Chapter 143 of the North Carolina General Statutes, Tort
Claims Against State Departments and Agencies, and as otherwise
provided by law.
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 281 15
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/1 O% POST -CONSUMER PAPER

Gerald Hargette Property Investigation
Page 2
6. The information derived from the investigation shall be made available to
the owner upon request and is a public record, in accordance with G.S.
132-1 et sea.
7. The activities to be carried out by the Department are for the primary
benefit of the Department and of the State of North Carolina and any
benefits accruing to the owner are incidental. The Department is not and
shall not be construed to be an agent, employee, or contractor of the owner
of the land.
I/We agree not to interfere with, remove or in any way damage the Department's
well(s) and equipment during the investigation.
Sincerely,
(Signature)
(Type or Print Name of Owner or Agent)
(Date)
(Address)
cgp/hargette.agr

• .y
/i
'�t •�1r.+
r
7*V "•mar.
sr
•
•
•
3 -

1
,off
2C� +�' ' 30.0
.�
Q7r
,()� 9' `
y 536
ll6` is
v
Distributed in furtherance
of the Acts of Congress
of May 8 and June 30, 1914.
Employment and program
opportunities are offered to
all people regardless of
race, color, national origin,
sex, age, or disability. North
Carolina State University,
North Carolina A&T State
University, U.S. Department
of Agriculture, and local
governments cooperating.
SoilFacts
Poultry Manure as a
Fertilizer Source
Poultry manure is an excellent source of nutrients and can be incorporated into most
fertilizer programs. Those using manures must practice sound soil fertility management
to prevent nutrient imbalances and associated animal health risks, as well as surface -
water and groundwater contamination. The key to successful management is to match
the nutritional requirements of the crop with nutrients available in the manure. The
value of poultry manure varies not only with its nutrient composition and availability,
but also with management and handling costs.
Nutrient Composition and
Sampling Procedure
The nutrient composition of poultry manure
varies with the type of bird, the feed ration,
the proportion of litter to droppings, the
manure handling system, and the type of litter
Consequently, all manures should be sampled
and analyzed for specific nutrient content
before you apply them to the land. Waste
samples can be analyzed for $4 by the North
Carolina Department of Agriculture (NCDA),
Agronomic Division, Plant Analysis Lab, P.O.
Box 27647, Blue Ridge Road Center, Raleigh,
NC 27611. Other qualified private laborato-
ries can also perform the analysis (fees vary).
Collecting a representative manure sample
is essential to reliable nutrient analysis. The
nutrient value of litter varies greatly within
the poultry house. To reduce sample variabil-
ity, collect subsamples of broiler, turkey, and
duck litter in 6 to 12 areas of the house.
Samples taken around waterers, feeders, and
brooders should be proportionate to the space
these areas occupy in the house. At each
location, collect litter by digging an area
down to the earth; be careful, however, not to
include soil. Place the subsamples in a plastic
bucket, mix thoroughly, and put 2 to 3 pounds
of the mixture in a sample container. Samples
from stockpiled litter should be taken from at
least 6 locations around the pile, all at depths
of at least 18 inches. Subsamples should be
Table 1. Average Nutrient Composition ablillroiler Manures
Manure Type
Total
N
Ammonium
NH,
Phosphorus
Pz05
Potassium
K20
lb/ton
Fresh (no litter)
26
10
17
11
Broiler house litter'
72
11
78
46
Roaster house litter'
73
12
75
45
Breeder house litter'
31
7
54
31
Stockpiled litter'
36
8
80
34
'Annual manure and litter accummulabon; typical litter base is sawdust, wood shavings, or peanut hulls
Source: Biological and Agricultural Engineering Department, NCSU.
a�;=•� North
Carolina
Cooperative Extension Service
NORTH CAROLINA STATE UNIVERSITY
COLLEGE OF AGRICULTURE & LIFE SCIENCES

SoilFacts
mixed and submitted as suggested
for litter from poultry houses.
Table 2. Average Nutrient Composition OfNIAINWauras
r
To increase sample uniformity in
, .
poultry manure slurries and lagoon
Manure Total Ammonium Phosphorus
Potassium
sludges, stir them before sampling.
Type N NH4 N P2O5
KO
Within an anaerobic lagoon, liquids
lb/ton
are relatively uniform above the
Fresh (no litter) 26 6 22
11
sludge zone; nevertheless, take
Undercage scraped' 28 14 31
20
several subsamples and combine
them.
Highrise stored 38 18 56
30
If you cannot have the manure
Ib/1,000 gallons
analyzed, use the mean nutrient
Liquid slurry3 62 42 59
37
values for your specific type of
Anaerobic
poultry manure found in Tables 1
lagoon sludge 26 8 92
13
through 4. Table 5 gives the average
values for the secondary and micro-
lb/acre-inch
nutrients ordinarily listed in the
Anaerobic
manure analysis report.
lagoon liquid 179 154 46
266
When using mean values for
'Manure collected within two days.
manure nutrient composition, exer-
Annual manure accummulation on unpaved surfaces.
cise caution to avoid over- or under-
Six-12 months' accummulation of manure, excess water usage, and
rainfall surplus; does not include fresh water for flushing.
storage -surface
fertilization. Also, after several
years, elements such as copper or
Source: Biological and Agricultural Engineering Department, NCSU.
zinc may accumulate and reach very
high levels. To avoid these problems,
take an annual plant tissue and a
Table 3. Average Nutrient Composition olV My`anures
biennial soil sampl., to monitor
nutrient levels.
Manure Total Ammonium Phosphorus
Type
Potassium
N NH4 N P,O,
K�O
Nutrient Availabilities
_ lb/ton
Except for nitrogen, the availability
of most nutrients in poultry manures
is fairly consistent. Nitrogen can
occur in several forms, each of which
can be lost when subjected to differ-
ent management or environmental
conditions.
Nitrogen in poultry wastes comes
from uric acid, ammonia salts, and
organic (fecal) matter. The predomi-
nant form is uric acid, which readily
transforms to ammonia (NH), a
gaseous form of nitrogen that can
evaporate if not mixed into the soil.
When it is thoroughly mixed, the
ammonia changes to ammonium
(NH4`), which can be temporarily
held on clay particles and organic
matter. Thus, soil mixing can reduce
nitrogen losses and increase the
amount available to plants.
Table 6 lists the first -year nutri-
ent availability coefficients for
Fresh (no litter) 27 8 25 12
Brooder house litter' 45 9 52 32
Grower house Iitter2 57 16 72 40
Stockpiled litter3 36 8 72 33
'Based on cleanout after each flock.
'Based on annual cleanout after full production.
'Based on annual house accummulation removed to uncovered stockpile to be
spread within six months.
Source: Biological and Agricultural Engineering Department, NCSU.
Table 4. Average Nutrient Composition o&D uak,, lAenvres
Manure Total Ammonium Phosphorus
Type N NH4 N P,05
Potassium
K�O
lb/ton
Fresh (no litter) 28 5 23
17
House litter' 19 3 17
14
Stockpiled Iitter2 24 5 42
22
'Annual manure and litter accummulation; typical litter base is wood shavings.
'Annual house accummulation removed to uncovered stockpile to be spread
within
six months.
Source: Biological and Agricultural Engineenng Department, NCSU.
2

Poultry Manure as a Fertilizer Source
Table 5.,Average Secondary and Micronutrient Content of Poultry Manures
Manure Type Ca Mg S Na Fe Mn B MO Zn Cu
Undercage scraped
43.0
Highrise stored
86.0
lAr
Broiler house
41.0
Roaster house
43.0
Breeder house
94.0
Stockpiled
54.0
er
Brooder house
28.0
Grower house
42.0
Stockpiled
42.0
djj@Wtter
Duck house
22.0
Stockpiled
27.0
Liquid slurry
35.0
Lagoon sludge
71.0
Lagoon liquid
lb/ton
6.1
7.1
4.5
0.52
0.27
0.050
0.00390
0.32
0.036
6.0
8.8
5.0
1.8
0.52
0.046
0.00038
0.37
0.043
8.0
15.0
13.0
1.3
0.67
0.054
0.00085
0.63
0.45
8.5
14.0
13.0
1.6
0.74
0.049
0.00082
0.68
0.51
6.8
8.5
8.6
1.3
0.57
0.035
0.00048
0.52
0.21
8.0
12.0
6.2
1.5
0.59
0.041
0.00069
0.55
0.27
5.7
7.6
5.9
1.4
0.52
0.047
0.00081
0.46
0.36
7.0
10.0
8.4
1.3
0.65
0.048
0.00092
0.64
0.51
6.8
9.5
6.4
1.5
0.62
0.047
0.00095
0.56
0.34
2.7 3.1 2.8 .98 0.31 0.021 0.00040 0.26 .056
4.4 5.6 8.8 1.2 0.47 0.030 0.00030 0.47 .050
Ib/1,000 gallons
6.8 8.2 5.3 2.9 0.42 0.040 0.018 0.43 0.080
7.2 12.0 4.2 2.2 2.3 0.082 0.014 0.80 0.14
lb/acre-inch
25.0 7.4 52.0 51.0 2.0 0.24 0.37 0.020 0.70 0.19
various poultry manures. Determine indicates that phosphorus movement
the available nutrients by multiplying off -site can lead to eutrophication of
these values by the nutrient composi-
surface waters. In nondesignated
tion values listed on the waste analy-
areas, phosphorus movement can be
sis report or in Tables 1 through 4.
adequately controlled with conserva-
The NCDA's Agronomic Division
tion measures such as grass field
calculates available nutrients and
borders, grassed waterways, contour
lists them in its report.
planting, and reduced tillage, which
minimize soil and residual manure
Application Rate
movement. Leaching of phosphorus
is extremely limited on mineral soils
Land application rates are generally
and should not contribute to ground -
determined by matching the avail-
water contamination.
able nitrogen or phosphorus content
Nitrogen recommendations for
of the waste to the nutrient require-
various crops are listed in Table 7.
ments of the crop. In most cases,
Use these rates as guidelines with
nitrogen requirements determine the
realistic yield capabilities for the
application rate, unless the area is
crop and field. With feed and forage
designated "nutrient sensitive" and
crops, excessive manure application
can produce high nitrate concentra-
tions, which can harm livestock
(through nitrate poisoning) and
promote nutrient imbalances that
may lead to grass tetany. If loading
rates are to be based on phosphorus,
apply the amount suggested by soil -
test recommendations. Because the
manure may not supply adequate
amounts of all the other nutrients
required by the crop, be sure to take
a soil test and, if necessary, supple-
ment with commercial fertilizer.
In addition to monitoring nutri-
ents, be sure to maintain an adequate
soil pH, which will help to maximize
crop yields and nutrient availability
3

Distributed in furtherance
of the Acts of Congress
of May 8 and June 30, 1914.
Employment and program
opportunities are offered to
all people regardless of
race, color, national origin,
sex, age, or disability. North
Carolina State University,
North Carolina A&T State
University, U.S. Department
of Agriculture, and local
governments cooperating.
SoilFacts
Swine Manure as a
Fertilizer Source
Swine manure can be an excellent source of nutrients for crop production. The key
to proper management is determining the nutrient content of the manure, the
percentages of those nutrients that are available to the plant, and the nutrient
requirements of the plant. Considered together, these three factors will help you
apply the proper amount.
Nutrient Content of the Manure
Because the nutrient content of swine ma-
nure varies among operations and over time,
the manure must be analyzed before you
apply it to the land. Waste samples can be
analyzed for $4.00 by contacting the North
Carolina Department of Agriculture
(NCDA), Agronomic Division, Plant and
Waste Analysis Lab, P.O. Box 27647, Blue
Ridge Road Center, Raleigh, NC 27611.
Other qualified private laboratories are also
available (fees vary).
Samples collected for analysis should be
representative of the pit or lagoon. If the
waste is to be applied as a slurry, the storage
pit or basin should be agitated before sam-
pling. Collect approximately 3/4 of a pint of
material in an expandable container, being
sure to leave air space.
If you cannot have a sample analyzed,
determine the application rate by using the
average nutrient values for different swine
manure systems shown in Table 1. Table 2
shows the average amounts of secondary and
Table 1. Nutrient Composition of Swine Manure
Manure
Total
Ammonium Phosphorus
Potassium
Type
N
NH N P,O,
K20
lb/ton
Fresh
12
7 9
9
Scraped'
13
7 12
9
Ib/1,000 gallons
Uquid slurry2
31
19 22
17
Anaerobic
lagoon sludge
22
6 49
7
lb/acre-inch
Anaerobic
lagoon liquid
136
111 53
133
Source: Abridged from North Carolina Agricultural Chemicals Manual.
'Collected within 1 week.
2Six-12 months accumulation of manure, urine, and excess water usage; does not include fresh water for
flushing or lot runoff.
` North Carolina
_ ,.:� }_ = ,; _ Cooperative Extension Service
3�} r <•. NORTH CAROLINA STATE UNIVERSITY
_ ..., �.
COLLEGE OF AGRICULTURE & LIFE SCIENCES

PPilFacts
micronutrients present in swine
manures. These values can be used
as planning guidelines, as long as
you realize that they are not as
accurate as a sample analysis.
Nutrient Availabilities
The total nutrient content reported
on a manure analysis report (or the
levels shown in Tables 1 and 2) is
not immediately available to the
crops when the manure is applied.
Some elements are released when
the organic matter is decomposed by
soil microorganisms. Other elements
can combine with soil constituents
and be made unavailable. Nitrogen
may also be lost to the atmosphere
through volatilization or denitrifica-
tion, depending on the application
method and soil moisture levels.
Table 3 lists the proportion of
nutrients available for crop use
during the first year of application
for given application methods.
When determining the application
rate, refer to the availability coeffi-
cient for the appropriate application
method, and then multiply that
number by the corresponding nutri-
ent value on the waste analysis
report (or by the values shown in
Tables 1 and 2). Waste analysis
reports from the NCDA's Agro-
nomic Division show the nutrient
availabilities for the first crop.
The most recently applied waste
is not the only source of nutrients;
they are also available from previ-
ous applications of manures or from
Table 3. First -Year Availability Coefficients for Swine Manure
Manure
Type
Soil
Injection' Incorporation Broadcast' Irrigation
P 2 0 5 and K20 availability coefficients
All manure types
0.8 0.8 0.7 0.7
N availability coefficient
Scraped
paved surface
- 0.6 0.4 -
Liquid
manure slurry
0.8 0.7 0.4 0.3
Anaerobic
lagoon liquid
0.9 0.8 0.5 0.5
Anaerobic
lagoon sludge
0.6 0.6 0.4 0.4
'Manure injected directly into soil and immediately covered.
'Surface -spread manure plowed or disked into soil within two days
'Surface -spread manure uncovered for one month or longer.
`Sprinkler -irrigated liquid uncovered for one month or longer.
legumes crops. With the exception
of nitrogen, updated soil tests are
the best means of determining
nutrient reserves from manure
applications. Table 4 can be used to
estimate available nitrogen carry-
over from legumes.
Application Rates
Land application rates of manure are
generally determined by matching
the available nitrogen or phosphorus
content of the wastes to the nutrient
requirements of the crops. In most
cases, nitrogen determines the
application rate unless the area is
designated "nutrient sensitive" and
indicates that phosphorus movement
Table 2. *G,d VJar+t)rV&W, Lint Qb#ter1t,�0f 8;Nt 1"1g,�MSnur
off -site could contaminate surface
waters. In areas not designated as
nutrient sensitive, phosphorus
movement can be adequately con-
trolled with conservation methods
that minimize soil and nutrient
runoff. The conservation methods
include grass field borders, grassed
waterways, contour planting, and
reduced tillage. Leaching of phos-
phorus is extremely limited on
mineral soils and should not contrib-
ute to groundwater contamination.
Nitrogen recommendations for
various crops are listed in Table 5.
Use these rates as guidelines with
the realistic yield capabilities for
each crop and field. With feed and
forage crops, excessive manure
ManureType Ca Mg S Na Fe Mn B Mo Zn Cu
lb/ton
Fresh 7.9 1.7 1.8 1.6 0.39 0.04 0.074 0.00066 0.12 0.029
Paved lot scraped 12.0 2.3 2.2 1.6 1.03 0.19 0.015 0.00007 0.35 0.15
Ib/1,000 gallons
Liquid slurry
Lagoon sludge
8.6 2.9 4.7 3.7 0.69 0.15 0.069 0.0011 0.39 0.11
15.8 4.5 8.3 2.9 1.8 0.28 0.023 0.0095 0.67 0.23
lb/acre-inch
Lagoon liquid 25.5 8.3 10.0 57.7 2.4 .34 0.18 0.0045 1.5 0.3
Source: Biological and Agricultural Engineering Department. NCSU.

S
Dairy Manure as a
Fertiliser Source
Dairy manure and wastewater are excellent sources of nutrients for most agro-
nomic, horticultural, and silvicultural crops. Proper management of these manures
�e... as nutrient sources is critical to promoting optimum plant growth and yield while
protecting the environment. Optimum management of this resource includes
■ Handling and treating waste properly
■ Testing soil and manure regularly
■ Setting realistic yield goals
■ Applying manure in a uniform and timely fashion
■ Practicing soil conservation and environmental sustainability.
Nutrient Content of Dairy
Manures
Tables 1 and 2 show average nutrient values
for four dairy manure types. Table 1 also
shows the range in concentrations that make
up the average. Note the variability! Because
nutrient values vary considerably over time,
it is important to have a manure sample
analyzed for nutrient content before applying
the manure to the land. Because of the nature
of manure slurry systems, it may not always
be possible to have a sample analyzed before
land application. However, analysis results
received after the slurry application will
indicate whether there is a need for supple-
mental fertilizer. Samples can be sent to the
North Carolina Department of Agriculture
(NCDA), Agronomic Division, Plant and
Tablerdpiutripnt Composition of Dairy Manure
Total Nitrogen Ammonium Phosphorus
. Potassium
Manure Type N
NHS N P2O5
KO
Lot -scraped manure (lb/ton) 10
3 6
9
range (3 to 20)
(2 to 15) (0.6 to 13)
(2 to 20)
Liquid manure slurry (lb/1,000 gal) 22
9 14
21
range (8 to 50)
(4 to 13) (0.2 to 38)
(0.7 to 50)
Distributed in furtherance
of the Acts of Congress
Anaerobic la g
lagoon
of May 8 and June 30,1914.
sludge* (lb/1,000 gail) 15
6 22
8
Employment and program
range (3 to 42)
(1 to 12) (2 to 64)
(2 to 20)
opportunities are offered to
all people regardless of
Anaerobic lagoon
race, color, national origin,
liquid (lb/acre-inch) 137
88 77
195
sex, age, or disability. North
Carolina State University,
to 268 17 a
range ( ) (22 to 130) (10 to 233)
(13 to 571)
North Carolina A8T State
University, U.S. DepartmentSource:
Biological & Agricultural Engineering Department, North Carolina State University, 1980 to 1990.
of Agriculture, and local
*No manure solids removed before lagoon input
governments cooperating.
North Carolina
Cooperative Extension Service
NORTH CAROL.INA STATE UNIVERSITY
COLLEGE OF AGRICULTURE & LIFE
SCIENCES

Table &-,,A rerage Secondary and Micronutrient C*nte(nt'of 1Y8 rV Manure
Manure
Ca
Mg
Se
Na
Fe
Mn
B
Zn
Cu
CI
Lot -scraped manure (lb/ton)
5
2.2
1.7
1.3
0.9
0.1
0.01
0.1
0.02
3.3
Liquid manure (lb/1,000 gal)
10
4.8
3.1
3.2
1.8
0.2
0.02
0.2
0.05
6.1
Lagoon sludge* (lb/1,000 gal)
12
4.5
3.6
1.4
1.5
0.3
NR
0.4
0.4
2.3
Lagoon liquid (lb/acre-inch)
69
35
25
48
12
1.3
0.15
2.0
0.3
67
Note: Ca = Calcium, Mg = Magnesium, Se = Selenium, Na = Sodium, Fe = Iron, Mn = Manganese, B= Bordn, Zn = Zinc,
Cu = Copper, CI = Chloride
NR = Not reported.
Source: Biological & Agricultural Engineering Department, North Carolina State University.
*No manure solids removed before lagoon input.
Waste Analysis Lab, P.O. Box
27647, Blue Ridge Road Center,
Raleigh, NC 27611; phone: (919)
733-2655. The current charge is $4
per sample. Many private laborato-
ries can also perform manure
analyses.
Because the accuracy of the
analysis depends on a representative
sample, take several subsamples
from different locations in the
manure pile or the lagoon and mix
them together in a plastic bucket.
After mixing the subsamples in the
bucket, place approximately 3/4 of a
pint of the manure material in a
nonmetallic, flexible container,
leaving some air space for gas
expansion. If possible, refrigerate or
ice the sample, and deliver it to the
lab promptly.
Samples of liquid manure
slurries are more difficult to obtain
because the manure basin must be
thoroughly agitated before a
representative sample can be taken.
For liquid manure slurry systems
take samples as the slurry material
is being pumped out of the lagoon.
The agitation caused by the removal
of the slurry will provide a represen-
tative sample. Record the analysis
results to develop a representative
farm average as a guide for future
slurry applications.
Land Application
Nutrient Availability
Only a portion of the nutrients in
dairy manure are available immedi-
ately after application for use by the
crop. Some of the nutrients are part
of the manure's organic structure
and require microbial decomposi-
tion to release them. In general, only
about 50 percent of the organically
bound nitrogen (N) and 70 to 80
percent of the other nutrients
become available to a crop during
the year of application. With solid
and slurry manures, the remaining
organically bound nitrogen can be
released in subsequent years and
should be accounted for in fields
where manure is applied annually.
Ammonium and urea are readily
available forms of nitrogen that are
present in many manures. Both of
these forms, however, can change
into ammonia, which evaporates
readily. When surface -applied
manure is not incorporated for one
month or longer, as much as 75
percent of the ammonia can be lost
to the atmosphere. Incorporating the
manure within 48 hours reduces
losses to about 25 percent; with
direct soil injection all but 5 percent
of the ammonia is retained.
Coefficients are used to estimate
nutrient availabilities and to account
for different manure types and
methods of land application. These
"availability coefficients" are
multiplied by the total nutrient
concentration for each element as
reported in the manure analysis
report or, if no sample was taken or
no analysis is available, they are
multiplied by the average manure
values listed in Table 1. The sum of
these values is the nutrient concen-
trations available to plants. Avail-
ability coefficients are listed in
Table 3. If manure samples are sent
to the NCDA Agronomic Division,
analysis results will report both total
nutrient concentrations and plant -
available nutrients using these same
availability coefficients.
Application Rate
Land application rates should be
based on the nutrient requirements
of the crop being grown. Manure
can be applied at a rate to supply
any of the recommended nutrients.
Be careful, however, that the
application rate chosen to meet one
specific nutrient requirement does
not result in either excessive or
inadequate application of other
nutrients that can negatively impact
water quality or the crop's health. If

COUNTY:
UNION
QUAD NO:
REPORT TO
NIRO
COLLECTOR(S) :
FINLEY
DATE:
10/1 12000
TIME:
PURPOSE:
LABORATORY ANALYSIS
Regional Office
BOD310 m /L
COD High 340 m / L
COD Low 335 m / L
Coliform: MF Fecal 31616 / loom]
Coliform: MF Total 31504 / 100ml
rOC mg/ I
Turbititv NTU
Residue., Suspended 530 m /L
TolaI Suspended solids mg/L
PH units
Alkalinih, to PH 4.5 m / L
Alkalinity to pH 8.3 m / L
Carbonate mg/ L
Bicarbonate mg/ L
Carlpondioxide mg/ L
Chloride m /L
Chromium: Hex 1032 ug/ L
Color: Tru 80 c.u.
Cyanide 720 m / L
COPINIEN'rS :
Owner.
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
H.c- ; or
[)]CPT
DIVISION OF WATER QUALITY INMOR1bIEJy.I,
, REALTrt
Chemistry Laboratory Reporl / Ground Water Quality ` NA� �'�s.L RESOURC&
SAMPLE PRIORITY
ROUTINE EMERGENCY NOV 20 2000
❑ CHAIN OF CUSTODY
4MON OF
W❑ SAMPLE TYPE MOORINI[c
HARGETTEFARMS
Diss. Solids 70300 m /L
Fluoride 951 m /L
Hardness: total900 m /L
Hardness: non-carb 902 m /L
Phenols32730 u /L
.Specific Cond. 95 umhos/cm2
Sulfate m /L
Sulfide 745 m / L
MBAS m /L
Oil and Grease m / L
Silica m /L
Boron
Formaldehyde mg/ L
•
NH3 as N 610 0.03 m /L
r
TKN as N 625 0.4 m /L
r
NO2 +NO3 as n 630 m / L
S
P: Total as P 665 0.02 m /L
PO4 m /L
A-Silver46566 u /L
AI -Aluminum 46557 u /L
As-Arsenic46551 u /L
Ba-Barium46558 u /L
Ca-Calcium46552 mg/ L
Cd-Cadium46559 1 u /L
Cr-Chromium46560 u /L
Cu- Copper 1042 u / L
Fe- Iron 1045 u / L
H - Mercury 71900 u / L
K-Potassiurn46555 mg/ L
h1 - Magnesium 927 mg/ L
Mn-Manganese 1055 u /L
Na- Sodium 929 mg/ L
Ni-Nickel u /L
Pb-Lead 46564 u /L
Se -Selenium u /L
Zn_Zinc 46567 u /L
Lab Number
YG1571
Date Received :
10/122000
Time Received :
9:00 AM
Received By :
JG
Released By : DS
Date reported: 10/312000
Organochlorine Pesticides
Organophosphorus Pesticides
I I Acid Herbicides I
Gasoline
YG1571 As

PV
vL,AM Of CUSTODY North Cprolltla
F10UNDWA'1 EIS FIELD/LAD FO(�M �J ��,,jj CUSTODY Ileparlrnenl of Envlronrnertl, IIC(IIII1, pll(I NalU(UI ne50UfCeS
DIVISION OF WATEn QUALITY - G110UNDWATEII SECTION
counly sAIAELE TYPE SAMPLE P1110111TY
Quad No Sedal No. Water ignoullne
o �7 1-2- ❑ Soil ❑ Emergency
Lat. -�Z Z � i � Long. S❑ Olhcr
Lab Number
Date 7ecelved / U�aZ-OU1"line
nec'd From: l r s
011ie[:
id Del.,
fleporl To: ARO, f=R�F3 �nRO, WaRO, Wino. ,rk+ Chain of Custody Data Enlry By: Cl(:
WSRO Klnslon FO, F Trust Central Oil., Olhe1: Dale neporlod:
Shipped by: Dus, o j r, I land Del., Other
y Purpose: ,
Collector(s): - Dale oe Baseline, Complainl, Compliance r�rWST, Peslicide Sludy, Federal Trust, Olher.
HELD ANALYSES Owner /��.r� �
pl-I400 �• 3 Spec. Cond.94 3.3 al 25o C Location or site
Temp.10 / 8 • Z- oC Odom — Description of sampling poin fs�
Appearance Sampling Melhod Sample Interval
Field Analysis y sis D : '� , Ilenlalks", m`r�,'
.— -
LABORATORY ANALYSES omni,ilnplmo. nciuny;i� i,�O"
BOD, 310 11lc1/1
COD I IigI13,1u Ing/I
_
_
COD Low 335 Ing/I
Colllorm: MF Fecai 31616 /1001111
_
Colilonn: MF Total 31504 11001111
TOC 660 mg/I
Turbldily 76 I'llU
_
nesidue., Suspended 530 nlg/I
pl I 'tu3 unk
Alkalinity to pl 1 4.5 410 Ing/I
_
_
Alkalinity to pl 1 6.3 415 Inull
4,15 mull
_
_Calbonale
Blcatbonalo 44U nlcl/I
_
Calbon dioxide 405 nigh
_
Chlolldo 94U mull
_
_
Chlonlicnn: Ilex 1032 ug/I
Colo(: 11ue ou ICU
_
Cynnldo 72.0 mg/1
Lab Conrinenl—
IIDiss. Solids 70300 No/l
Hardness (non-calb) 902 111r1/1
Phenols 32730 ug/)_
Specific Cond. 95 u I o c LL
Sullale 945 nut/l
Sulfide 745 nl(I/I
Oil and Grease nlq/l
1411, as N U 10 11_n/l
L _ K14 as 14 s25 tuUlL
140,1 11 as I,1 630 IncLI
P: l olal ns P 665 11lc1/1
At - AluminunI 4G557 Uu/I
As - Arsenic 46551 1]q/1
Ba - Barium 46558 u0/I
Cr - Chromium 46560
ug/I
Cu - Copper 46562
ug/I
Fe —Iron 46563
uU/1
I Ig - Mercury 7190U
ug/I
K - Polassiurn 16555
Ing/
Mu - Ivlaanestum 46554
mu/'
- Manganese 46565 u
- Sodium 1655G It
1 ! - I,I nml
uMu
Pb - Lead i65G•t
ud/I
So - Selenium
ucL
ZII - Z1110 4o5G7
U11/1
_ Organoclllorillo Pesticides
_ Organophosphorus Pesticides
_ IJlllogen Pesticides
_ Acid I letblcides
PCB's
Semivolalile Organics
TPI I - Diesel nanUe
VoInIllo Organics (VOA bollle)
Till I - Gasollno jgg1Ia
I PI I- B f EX Gasollir n

DIYIS ON ENrr WA'E'F'iEE
Chemistry Laboratory Report / Ground Water Quality
Lab Number
YG0457
Dale Received
4/12/00
COUNTY: UNION
SAMPLE PRIORITY
Time Received
9:30 AM
QUAD NO:
®ROUTINE
EMERGENCY
Received By
JG
REPORT TO : MRO
Regional Office
®R
CHAIN OF CUSTODY
COLLECTOR(S) : M FINLEY
Released By :
JC
DATE: 4/11/2000
ow
SAMPLE TYPE
Date reported :
5/1/00
TIME:
PURPOSE:
Owner:
HARGETTE ROAD
Location or Site:
Description of sampling point_
Sampling Method:
Remarks:
LABORATORY ANALYSIS
BOD 310 m
COD High 340 mg/1-
COD Low 335 mgfL
Coliform: MF Fecal 31616 /100mI
Coliform: MF Total 31504 /100ml
TOC mgfl
Turbitity NTU
Residue., Suspended 530 mgfL
Total Suspended solids m
H units
.Alkafinity to pH 4.5 m
lAlkalinity to PH8.3 m
Carbonate m
Bicarbonate m
Carbon dioxide m
Chloride rat
Chromium: Hex1032 u
Color: True 80 C.U.
C anide 720 rat L
COMMENTS:
Diss. Solids 70300 m
Fluoride 951 m
Hardness: total 900 m
Hardness: (non-carb) 902 m
Phenols 32730 u
Specific Cond. 95 umhos/cm2
Sulfate m
Sulfide 745 mgJL
MBAS m
Oil and Grease m
Silica m
Boron
Fonnaldeh de m
X
N113asN610 0.06 m
TKN as N 625 m
X
NO2 +NO3 as n 630 7.0 m
X
P: Total as P 665 0.04 m
PO4 m
A -Silver 46566 u
AI -Aluminum 46557 ugfL
As -Arsenic 46551 ugIL
Ba-Barium 46558 u
Ca -Calcium 46552 m
Cd-Cadium 46559 u
Cr-Chromium 46560 u
Cu- Copper 1042 u
Fe -Iron 1045 u
H - Mercury 71900 u
K-Potassium 46555 m
Mg- Magnesium 927 m
Mn-Manganese 1055 u
Na- Sodium 929 m L
Ni-Nickel ugfL
Pb-Lead 46564 u
Se -Selenium ugfL
Zn Zinc 46567 u
H-
I
Or anochlorine Pesticides
Or ano hos horus Pesticides
I Nitrogen Pesticides
I I Acid Ilerbicides I
Gasoline
PEAL:. L AWE. W
IptyJA014MENT, MALTU
b MAMMAL R'EW)URCM
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TWA
twA-
NCDENR
JAMES B. HUNT JR
GOVERNOR
NORTH CAROLING F
ENVIRONMENT AND NAiOPYRES
MOORESVILLE REGIONAL OFFICE
DIVISION OF WATER QUALITY
Groundwater Section
August 16, 1999
Gerald Hargette
3017 High Ridge Church Road
Marshville, North Carolina 28103
RE: Water Well Sample Results
Hargette Farm
Union county
Dear Mr. Hargette:
On July 14, 1999, I sampled the well at your farm on Hargette Road. A sample
was collected for nitrate and nitrite. This is a continuation of Chuck Pippin's
investigation of the elevated nitrate levels in your well.
Laboratory results from the sample indicate at the time of sampling that nitrate
and nitrite which were tested for were present at a concentration of 20 mg/L or parts per
million. This is still above the safe drinking water standard of 11 parts per million (10
for nitrate and one part per million for nitrite). Enclosed is a copy of the results.
Should you have any questions, please feel free to call me at 704/663-1699, ext.
238. I plan to sample the well again in October.
Sincerely,
Margaret A. Finley
Hydrogeological Technician
Enclosure: Lab results
cc: Union County Environmental Health
MAF/hargett.lab
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 261 15
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER

DIVISION OF NVA7'ER QUALITY
Chemistry Laboratory Report / Ground Water Quality
COUNTY:
UNION
SAMPLE PRIORITY
QUAD NO:
FIROUTINE EMERGENCY
REPORT'TO
IRO
Regional Office
a CI JAIN OF CUSrODY
COLLEC'rOR(S) :
FINLEY
DATE:
7/14/99
W❑ SAMPLE TYPE
TIME:
PURPOSE:
Owner:
GERALD DARGETTE
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
LABORATORY ANALYSIS
BOD310 m /L
COD High 340 m /L
COD Low 335 m / L
Cohform: NIF Fecal 31616 /100m1
Coliform: MF Total 31504 / 100ml
TOC m / I
Turbititv NTU
Residue., Suspended 530 mg/ I,
1'otalSuspended solids mg/ L
Alkalinitv to pH 4.5 in /L
Alkalinity to pli 8.3 m /L
Carbonate in /L
Bicarbonate an /L
Carbon dioxide m /L
Chloride m /L
Chromium: Hex 1032 a /L
Color:'rrue 80 C.U.
Cyanide 720 in /L
CONINIF.NTS :
Diss. Solids 70300 mg/ L
Fluoride951 mg/ L
Hardness: total900 mg/ I,
Hardness: non Garb 902 m /L
Phenols32730 u /L
Specific Cond. 95 umhos/cm2
Sulfate mg/ L
Sulfide745 mg/ L
MBAS m /L
Oil and Grease m /L
Silica m /L
Boron
Formaldehyde m /L
N113asN610 0.01 mg/ L
TKN as N 625 m / L
X
NO2 +NO3 as n 630 20 m / L
P: Total as P 665 m /L
PO4 mg/ L
A Silver46566 u /L
AI-Aluminum46557 u /L
As-Arsenic46551 u /L
Ba-Barium 46558 u L
Ca -Calcium 46552 m /L
Cd-Cadium46559 u /L
Cr-Chromium46560 u /L
Cu- Copper 1042 u / L
Fe- Iron 1045 u /L
H - Mercury 71900 u /L
K-Polassium46555 m /L
Mg- Magnesium 927 m /L
Mn-Manganese 1055 u /L
Na- Sodium 929 m /L
Ni-Nickel u /L
Pb-Lead 46564 u /L
Se -Selenium u /L
Zn_Zinc 46567 u /L
Fl-
Lab Number
9G 1314
Date Received
7/15/99
Time Received :
9;00
Received By
DS
Released By :
DS
Dale reported:
8/4/99
Or anochlorine Pesticides
Or ano hos horns Pesticides
Nitrogen Pesticides
Acid Herbicides
7'PH-Gasoline Range
TPH-BTEX Gasoline Ranee
9G1314 JUL

-'
/ 11 orIIt Carolina
01,t;' T�Wl11 cn riE--I_D/I_A,13 ronM Dell omanl of Envlroninenl, Ilealth, and Nalitral Ilesourr.es
mvisim or WATEII WAI_ITY - (,IIOUNDWATEII SECTION
s�h1('hI=_1=YL'S ;�nt�fYla�L'lll��lll(_Y.
my �'„-�� �' (_ab Number _
V I_ Water Ilaullnn V
;u Nc / / Srllal No. Daln nere erl �� (�Tlrne_.
(_I Soll (_) I:nter(lenry
I. e? L iyLnnrf. 'L 7 I I] olllr.r need by: from: nII ouric , 1
011lcr:
poi To: Ano, MO MITO nn0, Wano, Wino, - Clialn of Ctislndy Dala Enlry ITy: Clc
A10, I(Itishm FO, Find. Trtisl, Cnnital Off., Olher: ----�- !lain neltorlod:
•II►Ped by: nits, Couller, I land Del., 011ler•
/ I'url►nsa:
.Ilerint(s): Pain 7 7 `FI `�`� 1111m Z 7 �o Ilrlselina, Cnmplalnl, Coml►Ilancr. 11IST, Poslirlrlo Sindy, I'arleral Trusl, Olher:
n _ n II u(w anal
III % O Sllec. Cond.s4 Sf al 2Ja C Locallon or site H�Y.c�:�'l� .� -i i122o07/'nC�
°nit•te ZO . 3 aC Odor '''�`'��- DesclIplion of sampling poi -rill ��e a-'� QU"'r� ��� ��► ¢'
ilesirance � Saillpfind Melhod Samplo Inlerval _
,Id Analysis fly: ��"`� �i-�--� nernarics �,,_�� �-, 01 ^'7,-�"�
_HOP. 910
Inrlll
_CO_D I_ligh .140
COO Low 335
111r1/I
nld/I
Collforne MI' Fecal 31616
Colilonn: IM Tolal 315114
/Inn1111
/1001111
T OC bon
mull
Tulbidily 76
1111 U
11eshluo., Suspended 5:10
111(l/1
l►I 14na
unlll.
Alkalinlly IFLO1.4.5 41n
Alkalinlly to pi I HA 415
Carbanalo_ 445
Ilicarbonalo 441)
Calbon clioxido 405
na1/1
ntq/1
not/1
Inrlll
nul/l
Chlarlde 040
nui/l
Chtondum: Ilex 1032
uq/I
Color: Toro on
CU
Cyanide 720
Ilig/I
n►nenis
DIss Solicds 70:100 lncl/l_
Plourido n51 rnrin-
I��ic1l�ssJ ol�l fort rll0/l_
I la►dness (nnn_carl►) �02 rnrin
�'lhlhl t �3Ln It( n_
ilh&II14S41) rur) 1lh1il45hltl'_
Sidlalo 945 rnrin
S_WIldn 745 mr /I
Afl_Silver 46566 u111
AI Aluntlnum 4rr557
_As - Arsenlc 46551 110
Ila - Markup 465511 u(1/I
Ca`Calrtlim 46552 rnrlrl
Gd - Gadmirim 4f559 (lr]/l
Cr - Chromiun14G5_GO lig/l
Gil - Co p•icr 465112
I'o - Iron 46563 111111
_
—
_
_
—
_
Oil and Grease Inrlll
- - - ----
1Iq - mrrru►y I loon uq/l
I( - Polasshtnl 46555 111j1/1
Mrl_Idnrinoslu111 46554 111(1/1
Nil) LL- mallmillosrl 4f►5fi5 Iir1/I
Mil - Sodilllil 465513--- 1119/1
_ill-fliclscl UU/I
_Ph - Lead 46564 urin
_So - Scletiirirn urd/I
Zn`Zinc 46567 llr]/I
—
—
I'll I, —as N r,in 11111/1
:11St1�s.N_G25 nmll.
No, + NO, ns 1,1 rmn mir 11
1'_f olal as P 665 rnrin_
--
_
—
—
—
—
- -
V. 7/00. For Dissolved Alntlysls - sidmill Mimed s;nnl►III and Wrilo "I11S" In block.
O lanochiorino r'eslicidw; r
Orrlanophosllhorus Peslicii ir:•• _
Nilrogen Peslicides
_
_
Acid l loibicidos
_
PCII's _
Srnllvolnlllo Oruanlcs -
T PI I - Diesel flantle
—
_Volaliln Orrlanlc_s (VOA hntt�.
TI'll_G_asollrlo Ilarlllo
TPII - UTEX Gasolltn Ilimoo
_

Gerald Hargette
3017 High Ridge Church Road
Marshville, North Carolina 28112
Subject:
Dear Mr. Hargutt,
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
Division of Water Quality
March 17, 1998
Well Water Sample Results
On February 16, 1998, I sampled the water suppy well located at 5516 Paigeland
Road, Monroe, North Carolina. The well water sample was tested for nitrates. The
sample results represent conditions in the well at the time of sampling. The level of
nitrates (NO3+NO2) in the well water sample was 26 parts per million. The drinking
water standard for nitrates is 10 parts per million. I am continuing my investigation of
the groundwater in the area. I will keep you informed of any new information. Should
you have any questions please call me at 704-663-1699 ext. 268.
Sincerel
Chuck Pippin, P.G.
Hydrogeologic Technician
enclosure: Sample Results
919 NORTH MAIN STREET, MOORESVILLE, NORTH CAROLINA 28115
PHONE [phone] FAX [phone]
AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/I 0% POST -CONSUMER PAPER

PPPPF,P,
COUNTY:
QUAD NO:
UNION
REPORT TO : NIRO Regional Office
COLLECTOR(S) C.PIPPIN
DATE: 2/16/93
TIME:
LABORATORY ANAI.YCIc
BOD 310 mg/L
COD High 340 mg/L
COD Low 335 mg/L,
X
Colifarm: MF Fecal 31616 <1 /IOOmI
X
Coliform: MFToW 31504 1 /loom]
TOC mg/1
Turbitity NTU
Residue., Suspended 530 mg/L
Total Suspended solids mg/L
pH units
Alkalinity to pH 4.5 mg/L
Alkalinity to pH 8.3 mg/L
Carbonate mg/L
Bicarbonate mg/L
Carbon dioxide mg/L
Chloride mg/L
Chromium: Hex 1032 ug/L
Color: True 80 C.U.
Cyanide 720 mg/L
C0111MENTS :
Owner:
Location or Site
Description of sampling point
Sampling Method:
Remarks:
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Ground Water Quality
SAMPLE PRIORITY
X❑ROUTINE EMERGENCY
l CHAIN OF CUSTODY
l SAMPLE TYPE ❑
GERALDHARGETE
Diss. Solids 70300 mg/L
Fluoride 951 mg/L
Hardness: total 900 mg/L
Hardness: (non -cub) 902 mg/L
Phenols 32730 ug/L
Specific Cond. 95 umhos/cm2
Sulfate mg/L
Sulfide 745 mg/L
MBAS mg/L
Oil and Grease mg/L
Silica mg/L
Boron
Formaldehyde mg/L
NH3 as N 610 <0.01 mg/L
TKN as N 625 0.2 mg/L
X
NO2 +NO3 as n 630 26 mg/L
P: Total as P 665 mg/L
PO4 mg/L
Ag-Silver 46566 ug/L
AI -Aluminum 46557 ug/L
As -Arsenic 46551 ug/L,
Ba-Barium-46558 ug/L
Ca -Calcium 46552 mg/L
Cd-Cadium 46559 ug/L,
Cr-Chromium 46560 ug/L,
Cu- Copper 1042 ug/L
Fe- Iron 1045 ug/L
Hg- Mercury 71900 ug/L
K-Potassium 46555 mg/L
Mg- Magnesium 927 mg/L
Mn-Manganese 1055 ug/L
Na- Sodium 929 mg/L
Ni-Nickel ug/L,
Pb-Lead 46564 ug/L
Se -Selenium ugh
Zn_Zinc 46567 ug/L
ENVI14c , : ` `
& NATL'::,,i
Lab Numbcr 8G040'
Date Received 2/17/98
Time Received 9:00 AM
Received "Fivic,f SuF
,sl
4w�
Released By : DS
Datc reported : 3/10/98
Organochlorine Pesticides
Organophosphoms Pesticides
Nitrogen Pesticides
Acid Herbicides I
ITPH-Diesel Range
Gasoline
12 t°0A
RNTRI . ,, ,:aMT
Bfliiii AI BM&[
a(30405YEB

North Carolina
OUNDWATER FIELD/LAB FORM CO rDepartment of Environment, Health, and Natural Resources
1- W5 f6/D url�) DIVISION OF WATER QUALITY - GROUNDWATER SECTION
County / / �(/ �( Mate�r
AMP
Quad Nov /� Serial No. Routine
Lat. Yt 52 -*-Z4" Long. C % 1-2, 3� ❑ Soil ❑ Eme.gency
❑ Other
Repor', To: ARO, FRO, RRO, WaRO, WiRO, IL ❑ Chain of Custody
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
— 0
Shipped by: Bus, o , Hand Del., Other -
Lab Number
Dale Receivtf—�From:Bus,
Time 61
Rec'd by: ouri Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
Collectors : Purpose:
() Date �—/6� Time Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
l
FIELD ANALYSES T��9� (circle one)
� �/� Z 6�7
PH400 Spec. Cond'94 at 250 C Location or site _ a1126E
Temp.10 oC Odor Description of sampling point
Appearance Sampling Method
Field Analysis By: Remarks _ /� '7W1-4rl]
LABORATORY ANALYSES
(PumPiny limo, an lomp. elc )
Sample Interval
BOD 310 m /1
COD High 340
Diss. Solids 70300 m /I
A - Silver 46566 u /I
Oryanochlorine Pesticides
m /l
9
COD -ow 335 rn /I
Flouride 951 m /I
At - Aluminum 46557 u /I
Crganophosphorus Pesticides
Coliform: MF Fecal 31616 /100ml
Hardness: Total goo m /I
As - Arsenic 46551 u /I
Nitrogen Pesticides
Coliform: MF Total 31504 /100m1
Hardness non-carb 902 m /I
Ba - Barium 46558 u /I
Acid Herbicides
TOC 68o
Phenols 32730 u /I
Ca Calcium 46552 m /1
PCB's
m /I
Turbidity 76 NTU
ifi n Mh rn'
Cd - Cadmium 46559 u /I
Residue., Suspended 530 m /I
9
Sulfate 945 m /I
Cr - Chromium 46560 u /l
Sulfide 7a5 rn /I
Cu - Copper 46562 uc /I
Fe - Iron 46563 u /I
Sernivolatile Organics
pH 403
Oil and Grease m /l
Hg - Mercury 71900 ug/I
TPH - Diesel Range
unit
Alkalinity to pH 4.5 410 mg/I
K - Potassium 46555 rng/l
Alkalinity to pH 8.3 415 mg/I
M - Magnesium 46554 m /l
445 mg/I
BicarbCarboonate
Bicarbonate 440 rn /I
NH as N 610 m /I
TKN as N us nur/I_
Mn - Manganese 46565 u /I
Na - Sodium 46556 m /l
�i Nickel
Volatile Organics (VOA bottle)
TPH - Gasoline Range
Carbon dioxide 405 nlg/I
NO + NO as N 630 nl /I
ram[(
Pb -Lead 46564
Chloride 940 mg/I
u /I
TPH - BTEX Gasoline Range
P: Total as P 665 m /I
Se -Selenium u /I
Chromium: Hex 1032 ug/I
Color: True 8o CU
Zn -Zinc 46567 u /I
Cyanide 720 mg/I
�uu V— IIIIGI IIJ.
GW-54 REV. 7/9F For Dissolved Analysis - submit filtered sample and write "DIS" in blr

Division of Environmental Nlanagemenr
GROUNDWATER SECTION
CHAIN OF CUSTODY RBECORD
For Investigation of Incident No.
Samples collected and GW-54 forms completed by:
Lab Only
Lab o.
Ouad
No.
-
Location
Data -
7lrne
No. of
Con;ainers
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FPI.
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Rec. by
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I /
Rel.
Rec. by
/
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Method of Shipment:
_ ----=ro3n b.y:
0 Cp Ji v
;!_1-aIIL�a71.11 WA
Lab ;;c.
From 7hr u h (
+tio.
Containers
Analysis
Palinquished by I Received by I
Date / 7ine
/
I/
/
White copy - Gvv meaoquariers . canary COPY - Lao , rinK Copy - r1060wil

Division of Environmental Management
GROUNDWATER SECTION
CHAIN OF CUSTODY RECORD
For Investigation of ",f—' I--- --- Incident No,
'JUL 19 1'
Samples collected and GW-54 forms
completed by:
Lab Only
Lab No.
Quad
No.
Location f
Date I
Time
No. of
Containers
�s
I
Relinquished by(S/ign�a2ture):•
ce d by(S'g
u e):
at / 'me
Rel.
Rec. by
/
Rel.
Rec. by
/
Rel.
Rec. by
/
Method of Shipment: Gam
Seal
Security Type and Condition: Lock
by:
by:
Broken by:
Open by:
1 AR IISF (')NI Y
Lab No.
From Through
No.
Containers
I Analysis
I Relinquished by
Received by
Date / Time
/
/
/
/
White copy - GW Headquarters , Canary copy - Lab , Pink copy - Region
GW-63 Revised 9/87

,• ,U1 C � ••�. 1 P
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3MOUNDWATEn rIL"I_U/LA.D 1=011M DcIlrlillllMII Of FlIVIIOmmnol, Ilell!111, told IIIIIINl Ilesolur.es
DIVISI011 OF WATCII 011A1_I1Y - (;IIOUNDWATG11 SCCI ION
rllllly
+,ul No 7Serinl No.
I -I--- 2 G / 5/Loll!l. Nv Z! / Z-
Lnh Nurnher
Dnlo rlecelvecl rime
Ilec'cl by: From: fills, Coullel. I
-- I _
Iulll To: Ar10, r=no 1llll ,'0, Wtlf10, wino,III Cllabu.^. t of CInlly OtherII DaIn Enlly 11y: Clc:
.I10, IUrlslorl 1:0, Fed. •I lust, C(!Ilbtll Off., 0111 r: ----- 1)n10 Ilepollncl:
'illlrcl I,y: 11us, purl �I Inntl Dcl., Olbor•
S,/ // f!w Ihulnwa:
Ilnrlor(s1: ' I)alo oo lltno / .CJ— linsrlinn, Cnlnlllnitll, Comidlcnlr:rl LIIST' f nslirlcln ,Iluly, rvat rnl lrusl, O!hor.
:I.I?_llhl�l Y�I�sI (Iw,Ic11 �-stc'vT _ .
Spec. ConcL94 1'7 LL rcl 25c' C Lornllon or 5110 _ Aj 2c-:- .0e r•
"C O(lor *'-_= 1)escllpllon of smoplinll IullnlImmance �R� �•�` •{�'�1 t�i� —ice' �, e-.=ems f'
>rinlplinll Method ���n Samplo Interval
-Id Annlysls Oyu:/� ��7�-i o'� i- �•z*--(lrmn►Ics _ ,n • .� jz��"" -,...Ste I
/ ;
�►�onn���I ALIA_i5� Ir,uryJiQ rin...Y IOdk,Ole•..-
�z
_ _IIUi), 11n
COI) I Mill 1•111
- -COI) Low 315
nth/l
nip/l
_ Colllolrn: MF Fecnl 3i6167
11061_l
Colllornl: MF 1olof 11504
T CIQ coo
/1001111
null
Tulhlcllly 70
PIIU
11rsldua:, Suspelldecl 51n
slitll
Ill 14n:1
anti:
Allmllolly I11111.4.5. 4111
AIIcnlInlly to (tl I I1.J 415
C_Olt,uonlu 4-Is
nut/l
nl!t/I
silt/1
IIICOII,arinlo 440
Crilbon cllolcl 10 405
rntl/l
IngA
_C111011 le 946.
mil/l
Cluonllunl: Ilex 1e12
uq/l
Color, 71110 0o
Cu
Cynnllle 720
out/l
Colnrnonls
SAMPLE-T_YL'r AMPLhL111IM11LY
W Wnler rloullim
I_I soli I_I Gmerflellcy
1--1 OUlar
—
Ulss SMIcIsio1n11 Ifnf./I—
rhl,llllo n?1 11111M
IIL,IdII,a2jmulI_g(,II HIM.
Rattiness (►Ion _rtlllll rot Inlln_
-SII�GIIISeStLl!lL L ] Illyllfu51mfit
S1111,110 045 rlulll_
Art —Silver 4r56(1 arts
Al - Alundnunl 46551 ails
ns_nl5ellk;46551 ails
Ila�llarhlm 4055" Ilrr/I
Cn`Cnlrallnl 46552 ftlrlll
-Gll_C(IIIrI1111111 4G55!! LIII/l
Cr=CCllroIII IInl 45561) url-ll
1,11 - Collper 4651112 Ifu l
FO boll4G5G1 1,r�ll
_I Iu_L�1rrruly 7llltlo Ilpll
K - Volnushl111 40555 liltlll
_LI(t_I4rlt)IIOSIIIIII 46554 111(lll
fAll - Hanlllllloso 46565 all/l
I In - fl ,(lllllll •16550
_III=1•llchla usvl
-I'h�Lrnll 46564 url!1
_Su - SOlcrllurll ubll
Zo ZZInr.4r5o7 lull)
—
—
_
—
_
—
—
_
SIIIIIc10 745
OII null clrease Inp►I
-_ — ---
—
—
_
(Is lI_U III 111(lll
-ilsr��,s-r1_o2� mclll.
�JO! + JJO� ns j1 ran f!!rf�
1': 7alnl as 1' rr5 rnrl/I
_
—
)ie,
—
—
I11:V• /Itm I`rn Illssulvnrl Annlysin - sulunll Illlurnrl si,iulrlu nnrl wills "I11(�" In I,Inr.l-
Orr anocblollno I'e511cicles
_ Urllononlloshllorus f �silchll___-
_ f•lilro�on I'osllciclos
_ _Acid Ilarlllciclos
I'CII's
SC1111VOIa1110 Oruanlcs
T III I - I)lesel Ilnnlle
_ _VOlnlllo Ulllnnlrs (VOA In ow)
TI'I I - Gasollne Mangle _
Tf 11 - []TCX Onsollrn Itnlltln

COUNTY :
UNION
QUAD NO:
REPORTTO
NIRO
COLLECTOR(S) :
FINLEY
DATE:
8/24199
TIME:
PURPOSE:
LABORATORY ANALYSIS
Regional Office
BOD310 m /L
COD High 340 m / L
COD Low 335 m L
X
Coliform: hIF Fecal31616 <1 /100ml
X
Coliform: hIF Total31504 <1 /100ml
TOC m /I
Turbititv NTU
Residue., Suspended 530 m /L
Total Suspended solids m /L
H units
Alkalinity to PH 4.5 m / L
Alkalinity to pit8.3 to /L
Carbonate mg/ L
Bicarbonate m /L
Carbon dioxide mn /L
Chloride m /L
Chromium: I lex 1032 at./I.
Color: True 80 C.U.
Cyanide720 in /L
COMMENTS:
Owner:
Location or Site:
Description of sampling point
Sampling Method:
Remarks:
DIVISION OF WATER QUALITY
Chemistry Laboratory Report / Ground Water Quality
SAMPLE PRIORITY
FIROUTINE EMERGENCY
X❑ CHAIN OF CUSTODY
Fl,-vl SAMPLE TYPE
GERALDIIARGETTE
Diss. Solids 70300 mg/ L
Fluoride951 mg/ L
Hardness: total900 m /L -
Hardness: non-carb 902 m /L
Phenols32730 u /L
Specific Cond. 95 umhos/cm2
Sulfate mg/ L
Sulfide745 mg/ L
MBAS mg/ L
Oil and Grease m /L
Silica m /L
Boron
Formaldehyde mg/L_
NH3 as N 610 m /L
TKN as N 625 mg/ L
NO2 +NO3 as n 630 m /L
P: Total as P 665 m /L
PO4 to / L
A-Sdver46566 u /L
AI-Aluminum46557 u /L
As -Arsenic 46551 u /L
Ba-Barium46558 u /L
Ca-Calcium46552 m /L
Cd-Cadium 46559 u /L
Cr-Chromium 46560 u /L
Cu- Copper 1042 u / L
Fe- Iron 1045 u / L
H - Mercury 71900 u /L
K-Potassium 46555 mg/ L
Mg- Magnesium 927 m / L
Mn-Manganese 1055 u /L
Na- Sodium 929 m /L
Ni-Nickel u /L
Pb-Lead 46564 a /L
Se -Selenium u /L
Zn_Zinc 46567 a /L
Lab Number 9G 1671
Date Received
8/25/99
Time Received :
9;30
Received By
JG
Released By : DS
Date reported : 9/8/99
Or anochlorine Pesticides
Or ano hos horus Pesticides
Nilroeen Pesticides
Acid
I IT'PH-BTEX Gasoline Ranee I
9G1671 AUG

F, North Carolina
TER FIELD/LAB FORM �� fi ` �, i q Department of Environment, Health, and Natural Resources
. ` `• "-DIVISION OF WATER QUALITY -GROUNDWATER SECTION
yj'/ �.'-
2 L /4
Serial No.
Long. So Z-2 i 2-
SAMPLE TYPE SAMPLE PRIORITY
® Water _]�] Routine
❑ Soil ❑ Emergency
❑ Other
Report To: ARO, FRO, v 6 , hno, WaRO, WIRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus ourieF> Hand Del., Other
Colleclor(s): J-� Date FIzZ159 Time
FIELD ANALYSES
pH400 Gam. F Spec. Cond.94 3 at 250 C
Temp.10 Zv oC Odom--��
Appearance c 'e - C •y ems-.- ��
Field Analysis. By:
Chain of Custody
61
Lab Number
Date Received &257 � Time
Redd by: From: Bu ,Courier, and Del.,
Other:
Data Entry By:_
Date Reported:.
Ck:
3,0 Purpose:
f'^ Baseline, Complaint, CompliancerhLUST, Pesticide Study, Federal Trust, Other:
Owner - -- L;' 1-4 - r-.Q c,-fte-
Location or site /d c_-_._q e_-&-e�- K_',,/ /--"7 r.17 .1 k:..
Description of sampling point -tQ4 G/-7 t c-A", c
Sampling Method 4 o Sample Interval
Remarks � i., *"A, " .-►� baiter. e'`.
LABORATORY ANALYSES " s / � "Te,ehtemp. e'a.'
- w Ec I'ts .tG.�
BOD 310 m /I Diss. Solids 70300 m A A - Silver 46566 u /I Organochlorine Pesticides
COD High 340 mgA
COD Low 335 m /I
Flouride 951 m /1
Hardness: Total 900 MOM
At - Aluminum 46557 u A
As - Arsenic 46551 u A
Organophosphorus Pesticides
Nitrogen Pesticides
Colilorm: MF Fecal 31616 1100ml
_
Hardness (non-carb) 902 mall
Ba - Barium 46558 uq/I
Acid Herbicides
Colilorm: MF Total 31504 /100ml
Phenols 32730 ugn
Ca - Calcium 46552 m /I
PCB's
TOC 680 rn A
—
Specific Cond. 95 uMhos/cm2
Cd - Cadmium 46559 u /I
Turbidity 76 NTU
Sulfate 945 mq/I
Cr - Chromium 46560 uq/I
Residue., Suspended 530 mg/I
_
Sulfide 745 mq/I
Cu - Copper 46562 ugA
Fe - Iron 46563 u A
Semivolatile Organics
pH 403 unit
Oil and Grease mall
Hg - Mercury 71900 ug/I
K - Potassium 46555 mg/I
TPH - Diesel Range
Alkalinity to pH 4.5 410 mg/I
Mg - Magnesium 46554 mq/I
Alkalinity to pH 8.3 415 mg/I
Mn - Manganese 46565 u /I
Carbonate 445 mg/I
Bicarbonate 440 m A
NH as N 610 m A
Na - Sodium 46556 m /l
- Nickel ugA_1TPH
Volatile Organics (VOA boltie)
- Gasoline Range
Carbon dioxide 405 mgA
Chloride 940 mg/I
NO + NO as N 630 m A
P: Total as P 665 m A
Pb - Lead 46564 u A
Se - Selenium u A
TPH - BTEX Gasoline Range
Chromium: Hex 1032 ug/I
Zn - Zinc 46567 u A
Color: True 80 CU
Cyanide 720 mg/l
Lab Comments:
GW-54 REV. 7/96 For Dissolved Analysis - submit filtered sample and write "DIS" In block.

UNION COUNTY HEALTHDEPT. LABORATORY
500 N. ;MAIN STREET MOINROE, N.C.
NAME: �Cirr�C�"dQn C�S�eC�
551Apfoe-
S/A�MP,LLIIN.G �POINT
T n
DATE COLLECTED �
PRIVATE' PUBLIC
TIME COLLECTED - I I
TIME DELIVERED_
TIME RUN 1111
l�a0J rfliLk
ENVIRONMENTAL HEALTH SPECIALIST
LAB NO. y�o--
WATER ANALYSIS
PRESENCE/ABSENCE (PA)
Coliforms
PRESENT ABSENT
U.V. FLUORESCENCE
(E. COIi)
POSITIVE
NEGATIVE
Signed: &l�
Laboratorian
Date:

Page 1 of 1
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Laney Oil Company, Inc.
April 16, 1998
Page III
Your prompt attention to the items described herein is required. Failure to comply
with the state's rules in the manner and time specified, may result in the -assessment of
civil penalties and /or the use of other enforcement mechanisms available to the State.
Each day that a violation continues may be considered a separate violation
Please note that performing assessment and cleanup work that is not required
under 15A NCAC 2L.0115 is not reimbursable from the Commercial or Noncommercial
Leaking Petroleum Underground Storage Tank Cleanup Funds.
If you have any questions regarding the actions that must be taken or the rules
mentioned in this letter, please contact Chuck Pippin of the Mooresville Regional Office
at the letterhead address and/or at 704-663-1699 ext. 268. If you have any questions
regarding trust fund eligibility or reimbursement, please colitact the Groundwater Section
at [phone].
Sincerely,
Barbara S. Christian, P.G.
Acting Regional Supervisor
cc: Ted Bush - Central Office
Union County Health Department
Janet Tucker - Union County Emergency Management
cpg/laney.nor

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