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Home My WebLink AboutWQ0010607_Regional Office Historical File Pre 2018 (4)Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf(Rogers & Callcott) 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Groundwater - Monroe NC 6100451 10/07/2016 07:45 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on October 07, 2016. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Lauren Woodrum, your Project Manager, at lauren.woodrum@rogersandcallcott.com or (864)-232-1556 if you have any questions about this report. Permit #W00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski (Rogers & Callcott) Report Approved By. 4�vyp�zl� Lauren Woodrum Project Manager This report may not he reproduced. except in full. without written pennission from Rogers & Callcou. Inc. PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.I556 1 fax 864.232.6140 rogersandcal Icott.com --- an employee -owned company Page 1 of 38 go, =f Rogers & Callcott ENVIRONMENTAL South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 Certificate of A n a l v s i s North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Client Catalent Pharma Solutions Project: Groundwater - Monroe NC C/O George Maalouf(Rogers & Callcott) Work Order: 6100451 2021 E. Roosevelt Blvd. Received: 10/07/2016 07:45 Monroe, NC 28110 Sample Number Sample Description Matrix Sampled Type 6100451-01 MW7 PDB 45' Ground Water 10/06/16 12:09 Grab 6100451-02 MW I PDB 32' Ground Water 10/06/16 12:20 Grab 6100451-03 MW 12 PDB 42' Ground Water 10/06/16 12:33 Grab 6100451-04 MW 10 PDB 66' Ground Water 10/06/16 12:45 Grab 6100451-05 MW8 PDB 2T Ground Water 10/06/16 12:55 Grab 6100451-06 MW9 PDB 29' Ground Water 10/06/16 13:08 Grab 6100451-07 MW6 PDB 52' Ground Water 10/06/16 13:19 Grab 6100451-08 MW I 1 PDB 72' Ground Water 10/06/16 13:29 Grab 6100451-09 MW3A PDB 106' Ground Water 10/06/16 13:43 Grab 6100451-10 PZI PDB 29' Ground Water 10/06/16 14:42 Grab 6100451-11 Trip Blank Ground Water 1,0/06/16 08:55 Grab 6100451-12 PDB Blank Ground Water 10/06/16 09:02 Grab 6100451-13 MW7 PDB 45' Ground Water 10/06/16 12:09 Grab 6100451-14 MW I PDB 32' Ground Water 10/06/16 12:20 Grab 6100451-15 MW 12 PDB 42' Ground Water 10/06/16 12:33 Grab 6100451-16 MW 10 PDB 66' Ground Water 10/06/16 12:45 Grab 6100451-17 MW8 PDB 27' Ground Water 10/06/16 12:55 Grab 6100451-18 MW9 PDB 29' Ground Water 10/06/16 13:08 Grab 6100451-19 MW6 PDB 52' Ground Water 10/06/16 13:19 Grab 6100451-20 MW I l PDB 72' Ground Water 10/06/16 13:29 Grab 6100451-21 Field Blank at MW 11 Ground Water 10/06/16 13:33 Grab 6100451-22 MW3A PDB 106' Ground Water 10/06/16 13:43 Grab 6100451-23 MW5 Ground Water 10/06/16 14:02 Grab 6100451-24 MW4 Ground Water 10/06/16 14:12 Grab 6100451-25 MW3 Ground Water 10/06/16 14:23 Grab 6100451-26 MW2 Ground Water 10/06/16 14:34 Grab 6100451-27 PZI PDB 29' Ground Water 10/06/16 14:42 Grab PO Box 5655 1 Greenville. SC 29606 1 426 fairforest VVay I Greenville, SC 29607 1 main 864.232.1556 1 fax 864,232.6140 rogersandcallcott.eom an employee- )wned-_cmpany 10 20 2016 1433 This report mqv not be reproduced. except in full, without written permission from Rogers & Cullcon. Inc. Page 2 Of 38 Rogers &Callcott . ENVIRONMENTAL Catalent Phatma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number Sample Description Matrix Sampled Type 6100451-28 MW5 Ground Water 10/06/16 13:58 Grab 6100451-29 MW5 Ground Water 10/06/16 14:02 Grab 6100451-30 MW4 Ground Water 10/06/16 14:10 Grab 6100451-31 MW4 Ground Water 10/06/16 14:12 Grab 6100451-32 MW3 Ground Water 10/06/16 14:21 Grab 6100451-33 MW3 Ground Water 10/06/16 14:23 Grab 6100451-34 MW2 Ground Water 10/06/16 14:31 Grab 6100451-35 MW2 Ground Water 10/06/16 14:34 Grab PO Box 5655 ': Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned Company 10 20 2016 14:33 This report may not be reproduced, except in full, without written permission from Rogers & Callcott. Inc Page 3 Of 3H Jk Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Data Sample Number 6100451-01 Sample Description MW7 PDB 45' collected on 10/06/16 12:09 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 24.25 0.00 Ft 1.00 10/06/16 12:09 JHF B00268 Temperature 21.1 0.0 °C 1.00 10/06/16 12:09 Field Screen JHF B6J0268 Sample Number 6100451-02 Sample Description MW l PDB 32' collected on 10/06/16 12:20 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 27.22 0.00 Ft 1.00 10/06/16 12:20 JHF B00268 Temperature 20.1 0.0 °C 1.00 10/06/16 12:20 Field Screen JHF B6J0268 Sample Number 6100451-03 Sample Description MW 12 PDB 42' collected on 10/06/16 12:33 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 24.67 0.00 Ft 1.00 10/06/16 12:33 JHF B6J0268 Temperature 21.5 0.0 °C 1.00 10/06/16 12:33 Field Screen JHF B6J0268 Sample Number 6100451-04 Sample Description MW 10 PDB 66' collected on 10/06/16 12:45 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 32.12 0.00 Ft 1.00 10/06/16 12:45 JHF B6J0268 Temperature 22.4 0.0 °C 1.00 10/06/16 12:45 Field Screen JHF B6J0268 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way I Greenville. SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an I— c^moar; 10 20 2016 l •l:33 This report muv not be reproduced, except in full. without written permission from Rogers & Collcoll. Ina Page 4 Of 3 H Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-05 Sample Description MW8 PDB 27collected on 10/06/16 12:55 Reporting Parameter Result Limit t nits DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 16.85 0.00 Ft 1.00 10/06/16 12:55 JHF B6J0268 Temperature 20.8 0.0 1.00 10/06/16 12:55 Field Screen JHF B6J0268 Sample Number 6100451-06 Sample Description MW9 PDB 29' collected on 10/06/16 13:08 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 25.63 000 Ft 1 00 10/06/16 13:08 JHF B6J0268 Temperature 19.4 0 0 °C 1.00 10/06/16 13:08 Field Screen JHF B6J0268 Sample Number 6100451-07 Sample Description MW6 PDB 52' collected on 10/06/16 13:19 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 27.10 0.00 Ft 1.00 10/06/16 13:19 JHF B6J0268 Temperature 20.7 0 0 °C L00 10/06/16 13:19 Field Screen JHF B6J0268 Sample Number 6100451-08 Sample Description MW 1 I PDB 72' collected on 10/06/16 13:29 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 32.42 0.00 Ft 1.00 10/06/16 13:29 JHF B6J0268 Temperature 19.8 0.0 °C 1.00 10/06/16 13:29 Field Screen JHF B6J0268 Sample Number 6100451-09 Sample Description MW3A PDB 106' collected on 10/06/16 13:43 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 26.85 0.00 Ft 1.00 10/06/16 13:43 JHF B6J0268 Temperature 19.5 0.0 °C 1.00 10/06/16 13:43 Field Screen JHF B6J0268 PO Box SW I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax %4.232.6140 rogersandcalleott.eom anen t)")/e?-("A-nOd _nmpIfly 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & C'allcou. Inc. Page 5 G13H Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-10 Sample Description PZ 1 PDB 29' collected on 10/06/16 14:42 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 26.56 0.00 Ft 1.00 10/06/16 14:42 JHF 136J0268 Temperature 19.5 &0 °C 1.00 10/06/16 14:42 Field Screen JHF 136J0268 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report mqv not be reproduced except in full, without written permission from Rogers & Callcorr. Inc. Page 6 Of 38 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-11 Sample Description Trip Blank collected on 10/06/16 08:55 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 I3:09 EPA 8260B LBW 136J0579 l,l-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 1,1-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW 136J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260E LBW B6J0579 Chloroform ND OS ug/L 1.00 10/10/16 13:09 EPA 8260E LBW B6J0579 cis-1,2-Dichlorcethene ND 0.5 ug/L 1.00 10/10/t6 13:09 EPA 8260B LBW B6J0579 Ethylbenzene ND OS ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 lsopropylbenzene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW 136J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 13:09 EPA 8260E LBW 136J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 13:09 EPA 8260E LBW 136J0579 n-Butylbenzene ND 0.5 ug/L. 1.00 10/10/16 13:09 EPA 8260E LBW B6J0579 n-Propylbenzene ND OS u9fL 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 o-Xylene ND OS ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 see -Butyl benzene ND 2.0 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW 136.10579 Styrene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 tent-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260E LBW B6J0579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0 5 ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Trichloroethene ND OS ug/L 1.00 10/10/16 13:09 EPA 8260B LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 13:09 EPA 8260E LBW B6J0579 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 95 70-130 4-Bromo/luorobenzene 100 70-130 Toluene-d8 99 70-130 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way I Greenville. SC 29607 1 main 864.232.1556 1 tax 864.232.6140 rogersandeallcott.eom an employee -owned company 10 20 2016 14:33 This report may not be reproduced, except in full. without written permission from Rogers & Callcon, Inc. Page 7 Of 38 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-12 Sample Description PDB Blank collected on 10/06/16 09:02 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND Q5 ug/L 1.00 10/10/16 13:39 EPA9260B LBW 136J0579 1,1-Dichloroethane ND 0.5 ug/L. 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 1,1-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW 136J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW 136J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 Chloroform ND OS ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 lsopropylbenzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW 136J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW 136.10579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW 136J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW 136J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Tetrachloroethene ND 0.5 U91L 1.00 10/10/16 13:39 EPA 8260E LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0 5 ug/L 1.00 10/10/16 13:39 EPA 8260B LBW 136.10579 Trichloroethene ND U ug/L 1.00 10/10/16 13:39 EPA 8260B LBW B6J0579 Vinyl chloride ND 05 ug/L 1.00 10/10/16 13.39 EPA 8260B LBW B6J0579 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 93 70-130 4-Bromofluorobenzene 99 70-130 Toluene-d8 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom an employee -owned company 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written pennission from Rogers & C'allcon. Inc. Page 8 Of 3 H Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-13 Sample Description MW7 PDB 45' collected on 10/06/16 12:09 Parameter Result Rel mLing I unit Units DF lnal zed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 1,1-Dichloroethane ND 05 ug/L 1.00 10/10/16 14:09 EPA 9260B LBW B6J0579 1,1-Dichloroethene ND 05 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 9260B LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW 136J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.3 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 lsopropylbenzene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 9260B LBW B6J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16..14:09 EPA 8260B LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/I6 14:09 EPA 8260B LBW B6J0579 n-Butylbenzene ND OS ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260B LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 9260B LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 U91L 1.00 10/10/16 14:09 EPA 9260B LBW B6J0579 Trichloroethene ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 8260E LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 14:09 EPA 9260B LBW B6J0579 Surrogates % REC % REC Limits Flag 1.2-Dichloroeihane-D4 93 70-130 4-Brom9luorobenzene 98 70-130 Toluene-dR 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville. SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an emo ov-P-nv;ned-omcar, 10 20 2016 14:33 This report may not be reproduced, except in full, without written pertnissionfrom Rogers & Callcon. Inc. Page 9 of 38 iH Rogers & Callcott -- ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-14 Sample Description MW I PDB 32' collected on 10/06/16 12:20 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 1, 1 -Dichloroethane ND 0.5 ug/L 1.00 10/10/16 14:40 EPA8260B LBW B6J0579 1,1-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA9260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 c is- 1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Hexane ND l.0 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Isopropylbenzene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 m,p-Xylene ND 10 ug/t. 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 n-Butylbenzene ND 0.3 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 n-Propylbenzene ND 0.3 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B610579 Styrene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B SI LBW B6J0579 Toluene ND 0.5 ug/L L00 10/10/16 14:40 EPA 8260E LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Trichlomethene ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260B LBW B610579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 14:40 EPA 8260E LBW B6J0579 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 93 70-130 4-Bromofluorobenzene 99 70-130 Toluene-d8 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville. SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company 10 20 2016 14:33 This report muv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page l O Of 3H Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-15 Sample Description MW 12 PDB 42' collected on 10/06/16 12:33 Parameter Result Reporting Limit t nits DF Analyzed Method Flag Analyst Batch N olatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 1,1-Dichloroethane ND 0 5 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6JO579 l,l-Dichloroethee ND 0 5 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW 136J0579 1,2,4-Trimethylbenzene ND OS ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6J0579 1,2-Dichloroethane ND OS ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 Acetone ND 20.0 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 Benzene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 u8/t. 1.00 10/10/16 16:11 EPA 8260E LBW B6JO579 Chloroform ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6J0579 cis-1,2-Dichloroethee ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6J0579 Ethylbenzene ND OS ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6J0579 Hexane ND 1.0 ug/L I.00 10/10/16 16:11 EPA 8260B LBW B6J0579 lsopropylbenzene ND 05 ug/L 1.00 10/10/16 16:11 EPA9260B LBW B6JO579 m,p-Xylene ND LO ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6JO579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW B6JO579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 tent-Butylbenzene ND 0.5 us/L 1.00 10/10/16 16:11 EPA 8260B LBW B6JO579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethee ND 0.5 ug/L 1.00 10/10/16 16: l l EPA 8260E LBW B6J0579 Trichloroethene ND 0.5 u8/L 1.00 10/10/16 16:11 EPA 8260E LBW B6JO579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 16:11 EPA 8260E LBW 136J0579 Surrogates %REC %REC Limits Flag 1.2-Dichloroethane-D4 92 70-130 4-Bromofluorobenzene 100 70-130 Toluene-d8 103 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom an employee -owned company 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 11 Of 38 t� = z Rogers & Callcott ♦ ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample `umber 6100451-16 Sample Description MWIO PDB 66 collected on 10/06/16 12:45 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND OS ug/L 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 1,1-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 1,1-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA9260B LBW 136J0579 1,2,4-Trimethylbenzene ND 0.5 u8/1. 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 16.42 EPA 8260B LBW B6JO579 Acetone ND 20.0 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW 136J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW 136J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW 136J0579 cis-1,2-Dichloroethene ND OS ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 Etylbenzene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 Hexane ND 1.0 u9/1. 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 Isopropylbenzene ND 05 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW 136J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 o-Xylene ND 0.5 ue/L 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW 136J0579 Styrene ND 0.5 us/L 1.00 10/10/16 16:42 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6J0579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW B6J0579 Toluene ND OS ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6JO579 Trichloroethene ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260B LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 16:42 EPA 8260E LBW B6J0579 Surrogates %REC % REC Limits Flag 1,2-Dichloroethane-D4 91 70-130 4-Bromofluorobenzene 98 70-130 Toluene-d8 102 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 12 Of 38 WRogers &Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-17 Sample Description MW8 PDB 27collected on 10/06/16 12:55 Parameter Result Reporting ' Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1,1,1-Trichloroethane ND 0.5 ug/L 1.00 10/10/I6 17:12 EPA 8260B LBW B6JO579 1, 1 -Dichloroethane ND 0.5 ug/L 1.00 10/10/16 17:12 EPA9260B LBW B6J0579 1,1-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 u8/L 1.00 10/10/16 17:12 EPA 8260E LBW 136J0579 1,2-Dichloroethane ND 0.5 us/L 1.00 10/10/16 17:12 EPA 8260B LBW B6JO579 Acetone ND 20.0 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 Benzene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6JO579 Chloroform ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 Hexane ND 1.0 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 lsopropylbenzene ND 0.5 us/L 1.00 10/10/16 17:12 EPA 8260B LBW B6J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 17.12 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 17:12 EPA 82608 LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6JO579 n-Butylbenzene ND 0.5 ug/L 100 10/10/16 17:12 EPA 8260B LBW B6JO579 n-Propylbenzene ND OS ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 tert-Butylbenzene ND 0 5 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 Tetrachloroethene 0.9 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6JO579 Toluene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6JO579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260B LBW B6J0579 Trichloroethene ND 05 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 17:12 EPA 8260E LBW B6JO579 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 93 70-130 4-Bromojluorobenzene 99 70-130 Toluene-d8 102 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an en oti )ve_ .. ed -emG-iry 10 20 2016 14:33 This report mqv not be reproduced, except infill, ll, without written permission from Rogers & C'allcou. Inc. Page 13 Of 38 Rogers & Cakott # ENVIRONMENTAL Catalent Phatma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-18 Sample Description MW9 PDB 29' collected on 10/06/16 13:08 Rcportin,, Parameter Result l unit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 1,1-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 1,1-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA8260B LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 cis-1,2-Dichloroethene ND 0.5 ug/L 1,00 10/10/16 17:43 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Isopropylbenzene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 m,p-Xylene ND 1.0 u9/1- 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Naphthalene ND 1.0 u8/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260E LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260E LBW B6J0579 sec-Butylbenzene ND 2.0 u8/1- 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 0.5 u8/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Tetrachloroethene ND OS ug/L 1.00 10/10/16 17:43 EPA 8260E LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0 5 ug/L 1.00 10/10/16 17:43 EPA 8260E LBW B6J0579 Trichloroethene ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260B LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 17:43 EPA 8260E LBW B6J0579 Surrogates %REC %REC Limits Flag 1,2-Dichlomeihane-D4 92 70-130 4-Bromofluorobenzene 96 70-130 Toluene-dS 101 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax 864.232.6140 rogersandealleott.eom an employee -owned --ompany 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcon. Inc. Page 14 of 38 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-19 Sample Description MW6 PDB 52' collected on 10/06/16 13:19 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 I,1-Dichloroethane ND 0 5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 I,l-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0 5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 1,2-Dichloroethane 1.7 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Benzene ND OS ug/L 1.00 10/10/16 18:13 EPA 8260E LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 u8/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Chloroform 0.6 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 cis-1,2-Dichloroethene 1.7 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Isopropylbenzene ND 0.5 u8/l. 1.00 10/10/16 18:13 EPA 8260E LBW B6J0579 m,p-Xylene ND LO ug/L 1.00 10/10/16 18.13 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 18:13 EPA 8260E LBW B6J0579 n-Butylbenzene ND 05 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 n-Propylbenzene ND OS ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260E LBW B6J0579 sec -Butyl benzene ND 2.0 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Tetrachloroethene 0.6 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Toluene ND 0 5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Trichloroethene ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260E LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 18:13 EPA 8260B LBW B6J0579 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 92 70-130 l-BromoJluorobenzene 98 70-130 Toluene-dS 103 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom in 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 15 Of 3H Rogers & Callcott - ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-20 Sample Description MW I I PDB 72' collected on 10/06/16 13:29 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 1,1-Dichloroethane 0.6 0.5 ug/L 1.00 10/10/I6 18:44 EPA 8260B LBW B6J0579 1,l-Dichloroethene 3.8 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 19:44 EPA 8260B LBW B6J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 cis-1,2-Dichloroethene 3.5 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Isopropylbenzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Naphthalene ND LO ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Toluene ND 0.5 u8/L 1.00 10/10/16 18A4 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Trichloroethene 1.6 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 18:44 EPA 8260B LBW B6J0579 Surrogates %REC %REC Limits Flag 1,2-Dich1oroethane-D4 92 70-130 4-BromoJluorobenzene 96 70-130 Toluene-d8 102 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SG 29607 1 main 864.232.1556 1 fax %4.232.6140 rogersandeallcott.eom an employee -owned Company 10 20 2016 14:33 This report may not be reproduced, except in full, without written permission from Rogers & Callcon. Inc Page 1 6 Of 3H = Rogers & Cakott ENVIRONMENTAL Catalent Phartna Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-21 Sample Description Field Blank at MW 11 collected on 10/06/16 13:33 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 1, 1 -Dichloroethane ND 0.5 ug/L I.00 10/10/16 19:14 EPA 8260B LBW B6J0579 1, 1 -Dichloroethene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 9260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 19:14 EPA 8260E LBW B6J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Isopropylbenzene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 19.14 EPA 8260B LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 n-Buylbenzene ND 0.5 u8/1. 1.00 10/10/16 19:14 EPA 9260B LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 sec-Buylbenzene ND 2.0 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 tert-Bthylbenzene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Tetrachloroethene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 9260B LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Trichloroethene ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 19:14 EPA 8260B LBW B6J0579 Surrogates %REC %REC Limits Flag 1, 2-Dichloroethane-D4 91 70-130 4-Bromofhiorobenzene 95 70-130 Toluene-dS 101 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom an employee -owned company 10 20 2016 14:33 This report muv nor be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 17 Of 38 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-22 Sample Description MW3A PDB 106' collected on 10/06/16 13:43 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 1,1-Dichloroethane 3.8 0.5 ug/L L00 10/10/16 19:45 EPA 8260B LBW B6J0579 1,1-Dichloroethene 0.9 0.5 ug/L L00 10/10/16 19:45 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW 136J0579 Acetone ND 20.0 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW 136J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Chloroform ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260E LBW B6J0579 cis-1,2-Dichloroetltene 9.0 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Ethylbenzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 lsopropylbenzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 m,p-Xylene ND 1.0 ug/L 1,00 10/10/16 19:45 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 u8/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Naphthalene ND 1.0 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260E LBW B6J0579 o-Xylene ND OS ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 19:45 EPA 8260E LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260E LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Tetrachloroethene 2.5 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW 136.10579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Trichloroethene 8.1 0.5 ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Vinyl chloride ND OS ug/L 1.00 10/10/16 19:45 EPA 8260B LBW B6J0579 Surrogates %REC % REC Limits Flag I, 2-Dichloroethane-D4 91 70-130 4-BromgJluorobenzene 97 70-130 Toluene-dR 103 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 18 of 38 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-23 Sample Description MW5 collected on 10/06/16 14:02 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane l,l-Dichloroethane l,l-Dichloroethene 1,2,4-Trimethylbenzene 1,2-Dichloroethane Acetone Benzene Bromomethane (Methyl Bromide) Chloroform cis-1,2-Dichloroethene Ethylbenzene Hexane lsopropylbenzene m,p-Xylene Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Toluene trans-1,2-Dichloroethene Trichloroethene Vinyl chloride Rebatch Sample Number: 6100151-23RE1 Tetrachloroethene Surrogates ND 0.5 U91L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 20.0 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW 136J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 2.1 0.5 u8/L. 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 5.7 0.5 u8/1- 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 1.0 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 1.0 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 2.0 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 1.0 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 u811- 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 2.0 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260B LBW B6J0579 15.2 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 20:15 EPA 8260E LBW 136J0579 58.5 1.0 ug/L 2.00 10/12/16 10:07 EPA 8260E LBW B6J0581 %REC %REC Limits Flag 1. 2-Dichloroethane-D4 93 70-130 4-Bromq luorobenzene 97 70-130 Toluene-dS 101 70-I30 Rebatch Sample Number: 6100451-23RE1 1,2-Dichloroethone-D4 89 70-130 4-Bromo/luorobenzene 87 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax %4.232.6140 rogersandealleott.eom an emoin,;ee-erred-cmnarl. 10 201016 14:33 This report muv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 19 Of 38 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-23RE1 Sample Description MW5 collected on 10/06/16 14:02 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates % REC %.REC Limits Flag Rebatch Sample Number: 6100451-23RE1 Toluene-& 94 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned Company 10 201016 14:33 This report muv not be reproduced, except in full, without written permission from Rogers & Callcou. Inc. Page 20 Of 38 t. Rogers & Callcott 0 ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample.Number 6100451-24 Sample Description MW4 collected on 10/06/16 14:12 Parameter Result Reporting limit t nits DF Analyzed Method Flag Analyst Batch Volatile Organics l,l,l-Trichloroethane ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 l,l-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 1,1-Dichloroethene 0.6 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 0.5 118/L 1.00 10/10/16 20:46 EPA 82608 LBW B6J0579 1,2-Dichloroethane ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Acetone ND 20.0 u8/1- 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Benzene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260E LBW B6J0579 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Chloroform 1.1 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260E LBW B6J0579 cis-1,2-Dichloroethene 14.1 0.5 u8/L 1.00 10/10/16 20:46 EPA 8260E LBW B6J0579 Ethvlbenzene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Hexane ND 1.0 ug/L 1.00 10/10/16 20:46 EPA 8260E LBW 1300579 Isopropylbenzene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260E LBW B6J0579 m,p-Xylene ND 1.0 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Methylene chloride ND 2.0 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B00579 Naphthalene ND 1.0 u91L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 n-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 n-Propylbenzene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 o-Xylene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 2.0 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Styrene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Tetrachloroethene 45.0 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Toluene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260E LBW B6J0579 Trichloroethene 35.8 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260B LBW B6J0579 Vinyl chloride ND 0.5 ug/L 1.00 10/10/16 20:46 EPA 8260E LBW B6J0579 Surrogates %REC % REC Limits Flag 1,2-Dichloroethane-D4 90 70-130 4-BromoJluorobenzene 95 70-130 Toluene-d8 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned corncary 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 21 of 38 Ok Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-25 Sample Description MW3 collected on 10/06/16 14:23 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane 1, 1 -Dichloroethane l,l-Dichloroethene 1,2,4-Trimethylbenzene 1,2-Dichloroethane Acetone Benzene Bromomethane (Methyl Bromide) Chloroform Ethylbenzene Hexane Isopropylbenzene m,p-Xylene Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Toluene trans-1,2-Dichloroethene Vinyl chloride Rebatch Sample Number: 6100451-25RE1 cis-1,2-Dichloroethene Tetrachloroethene Trichloroethene Surrogates ND 0.5 ug/L 1.00 10/10/16 21:16 EPA8260H LBW 136J0579 1.8 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 1.3 0.5 ug/L L00 10/10/16 21:16 EPA 8260B LBW 136J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 20.0 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260E LBW B6J0579 9.8 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 1.0 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND LO ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 2.0 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 1.0 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 2.0 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260B LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260E LBW B6J0579 ND 0.5 ug/L 1.00 10/10/16 21:16 EPA 8260E LBW B6J0579 152 5.0 u9/1- 10.0 10/12/16 10:38 EPA 8260E LBW B6J0581 235 5.0 ug/L 10.0 10/12/16 10:38 EPA 8260B P1,S1 LBW B6J0581 312 5.0 ug/L 10.0 10/12/16 10:38 EPA 8260B PI,SI LBW 136.10581 %REC % REC Limits Flag 1.2-Dichloroethane-D4 92 70-130 4-Bromojluorobenzene 97 70-130 Toluene-dR 100 70-130 Rebatch Sample Number: 6100451-25RE1 1.2-Dichloroethane-D4 90 70-130 4-BromoJluorobenzene 85 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandea.11eott.eom an employee -owned company 1010 2016 14:33 This report muv not be reproduced, except in full, without written permission from Rogers k Callcott. Inc. Page 22 Of 3S v. Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-25RE1 Sample Description MW3 collected on 10/06/16 14:23 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC % REC Limits Flag Rebatch Sample Number: 6100451-25RE1 Toluene-d8 95 70-130 PO Box 5655 Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report may not be reproduced. except in full, without written permission from Rogers & Callcott. Inc. Page 23 3838 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-26 Sample Description MW2 collected on 10/06/16 14:34 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane 1, 1 -Dichloroethane 13-Dichloroethene 1,2,4-Trimethylbenzene 1,2-Dichloroethane Acetone Benzene Bromomethane (Methyl Bromide) Chloroform cis-1,2-Dichloroethene Ethylbenzene Hexane lsopropylbenzene m,p-Xylene Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Toluene trans-1,2-Dichloroethene Vinyl chloride Rebatch Sample Number: 6100451-26RE1 Tetrachloroethene Trichloroethene Surrogates ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260E LBW 136J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 200 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW 136.10579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW 136J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 139 5.0 u9/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 722 5.0 u6/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260E LBW B6J0579 ND 10.0 ug/L 10.0 10/10/16 21:46 EPA 8260E LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260E LBW B6J0579 ND 10.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 20.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 10.0 ugJL 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 u8/1- 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 20.0 u9/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260E LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 ND 5.0 ug/L 10.0 10/10/16 21:46 EPA 8260B LBW B6J0579 5070 50.0 ug/L 100 10/12/16 12:11 EPA 8260B LBW 136J0581 2120 50.0 ug/L 100 10/12/16 12:11 EPA 8260B LBW B6J0581 %REC % REC Limits Flag 1.1-Dichloroethane-D4 90 70-130 4-Broinofluorobenzene 96 70-130 Toluene-d8 95 70-130 Rebatch Sample Number: 6100451-26RE1 1.1-Dichloroeihane-Da 86 70-130 4-Bromofluorobenzene 89 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report may not be reproduced except in full, without written permission from Rogers & Callcon. Inc. Page 24 Of 38 Rogers & Cakott -.. --. ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-26RE1 Sample Description MW2 collected on 10/06/16 14:34 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 6100451-26RE1 Toluene-d8 100 70-130 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an empoyee-owned company 10 20 2016 1 a:33 This report mqv not be reproduced, except in full, without written pennission from Rogers & Callcott. Inc. Page 25 Of 3S Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-27 Sample Description PZI PDB 29' collected on 10/06/16 14:42 Parameter Result Reporting Limit Units DF Analyzed Nlethod Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 1, 1 -Dichloroethane ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 l,l-Dichloroethene 15.4 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 1,2,4-Trimethylbenzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 1,2-Dichloroethene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260E LBW B6J0579 Acetone ND 500 ug/L 25.0 10/10/16 22:17 EPA 8260E LBW B6J0579 Benzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260E LBW B6J0579 Bromomethane (Methyl Bromide) ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 cis-1,2-Dichloroethene 291 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Ethylbenzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Hexane ND 25.0 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Isopropylbenzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW 136J0579 m,p-Xylene ND 25.0 u8/L 25.0 10/10/16 22:17 EPA 8260B LBW 136J0579 Methylene chloride ND 50.0 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Naphthalene ND 25.0 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 n-Butylbenzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 n-Propylbenzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 o-Xylene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 sec-Butylbenzene ND 50.0 u8/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Styrene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 tert-Butylbenzene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Toluene 14.7 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260E LBW B6J0579 trans-1,2-Dichloroethene ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW B6J0579 Trichloroethene 570 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW 136J0579 Vinyl chloride ND 12.5 ug/L 25.0 10/10/16 22:17 EPA 8260B LBW 136J0579 Rebatch Sample Number: 6100451-27RE1 Chloroform 3180 250 ug/L 500 10/10/16 12:38 EPA 8260B LBW 136J0579 Tetrachloroethene 13200 250 ug/L 500 10/10/16 12:38 EPA 8260B LBW B6J0579 Surrogates %REC %REC Limits Flag 1.1-Dichloroethane-D4 90 70-130 -l-Bromofluorobenzene 99 70-130 Toluene-dR 91 70-130 Rebatch Sample Number: 6100451-27RE1 1.1-Dichloroethane-D4 94 70-130 !-Bromojluorobetizene 99 70-130 PO Box 5655 r Greenville. SC 29606 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom an e nafcvec-, n,r..-ed 'cmcam,: 10 20 2016 14:33 This report muv not be reproduced, except injull, without written pennissionfrom Rogers & ('allcott. Inc. Page 26 Of 38 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-27RE1 Sample Description PZI PDB 29' collected on 10/06/16 14:42, Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC % REC Limits Flag Rebatch Sample Number: 6100451-27RE1 Toluene-d8 98 70-130 Sample Number 6100451-28 Sample Description MW5 collected on 10/06/16 13:58 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 58.12 0.00 Ft 1.00 10/06/16 13:58 JHF B6J0268 Sample Number 6100451-29 Sample Description MW5 collected on 10/06/16 14:02 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.1 0.1 pH Units 1.00 10/06/16 14:02 Field Screen JHF B6J0268 Specific Conductance at 25 C 560 10.0 umhos/cm 1.00 10/06/16 14:02 Field Screen JHF B6J0268 Temperature 21.7 0.0 °C 1.00 10/06/16 14:02 Field Screen JHF B6J0268 Turbidity (Field) ND 5.0 NTU 1.00 10/06/16 14:02 Field Screen JHF B6J0268 Sample Number 6100451-30 Sample Description MW4 collected on 10/06/16 14:10 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 35.90 0.00 Ft 1.00 10/06/16 14:10 JHF B6d0268 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville. SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 /4:33 This report muv not be reproduced, except in full, without written permission from Rogers & Callcon. Inc. Page 27 Of 3$ Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-31 Sample Description MW4 collected on 10/06/16 14:12 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.3 0.1 pH Units 1.00 10/06/16 14:12 Field Screen JHF 136.10268 Specific Conductance at 25 C 489 10 0 umhos/cm 1.00 10/06/16 14:12 Field Screen JHF B6J0268 Temperature 23.2 0 0 °C 1.00 10/06/16 14:12 Field Screen JHF 136J0268 Turbidity (Field) ND 5.0 NTU 1.00 10/06/16 14:12 Field Screen JHF B6J0268 Sample Number 6100451-32 Sample Description MW3 collected on 10/06/16 14:21 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 53.50 0.00 Ft 1.00 10/06/16 14:21 JHF 136J0268 Sample Number 6100451-33 Sample Description MW3 collected on 10/06/16 14:23 Repnrtin,_, Parameter Result I unit I nit, 1) F analyzed Method Flag Analyst Batch Field Parameters pH 6.5 0.1 pH Units 1.00 10/06/16 14:23 Field Screen JHF B6J0268 Specific Conductance at 25 C 450 100 umhos/cm 1.00 10/06/16 14:23 Field Screen JHF 136J0268 Temperature 21.9 0.0 °C 1.00 10/06/16 14:23 Field Screen JHF 136J0268 Turbidity (Field) ND 5.0 NTU 1.00 10/06/16 14:23 Field Screen JHF B6J0268 Sample Number 6100451-34 Sample Description MW2 collected on 10/06/16 14:31 Reporting Parameter Result Limit Units DF Analyzed Method Fla-, Anat>st Batch Field Parameters Depth to Water 33.40 0.00 Ft 1.00 10/06/16 14:31 B6J0268 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville. SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.com an employee -owned compare 10 20 2016 la 33 This report may not be reproduced except in full, without written permission from Rogers & C'allcon. Inc. Page 28 383 H Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Sample Number 6100451-35 Sample Description MW2 collected on 10/06/16 14:34 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.2 0. I pH Units 1.00 10/06/16 14:34 Field Screen JHF B6J0268 Specific Conductance at 25 C 469 10.0 umhos/cm 1.00 10/06/16 14:34 Field Screen JHF B6J0268 Temperature 23.3 0.0 °c 1.00 10/06/16 14:34 Field Screen JHF B6J0268 Turbidity (Field) 19.5 5.0 NTU 1.00 10/06/16 14:34 Field Screen JHF B6J0268 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report may not be reproduced, except in full, without written permission from Rogers & C'allcott. Inc. Page 29 of 88 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result '%,REC Limits RPD Limit Flags Batch B6JO579 - EPA 5030 Blank (B6.10579-BLK1) 1,1,l-Trichloroethane ND 0.5 ug/L 1,1-Dichloroethane ND 0.5 ug/L Ll-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 0.5 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND LO ug/L Isopropylbenzene ND 0.5 ug/L m,p-Xylene ND LO ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 1.0 ug/L n-Butylbenzene ND 0.5 ug(L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Butylbenzene ND 2.0 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate: 1. 2-Dic hl o methane-D,t Surrogate: -l-BromoJluorohenzene Surrogate: Toluene-d8 LCS (86J0579-BSI) 9- -0-130 98 :0-130 9- -0-130 1, 1, 1 -Trichloroethane 20.2 0.5 ug/L 20.0 101 70-130 Ll-Dichloroethane 22.0 0.5 ug/L 20.0 110 70-130 Ll-Dichloroethene 19.7 0.5 ug/L 20.0 99 70-130 1,2,4-Trimethylbenzene 21.5 0.5 ug/L 20.0 108 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 ! fax 864.232.6140 rogersandealleott.eom an employee owned company 10 20 2016 14:33 This report may not be reproduced, except in full, without written permission from Rogers & Callcort Inc Page 30Of 3H Rogers & Callcott ENVIRONMENTAL Catalent Phartna Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe. NC 28110 Reported: 10/20/16 14:33 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B6J0579 - EPA 5030 LCS (B6.10579-111SI) 1,2-Dichloroethane 22.6 0.5 u8/L 20.0 113 70-130 Acetone 103 20.0 ug/L l00 103 60-140 Benzene 21.6 0.5 ug/L 20.0 109 70-130 Bromomethane (Methyl Bromide) 16.5 0.5 ug/L 20.0 83 60-140 Chloroform 21.0 0.5 ug/L 20.0 105 70-130 cis-1,2-Dichloroethene 22.5 0.5 ug/L 20.0 112 70-130 Ethylbenzene 19.7 0.5 ug/L 20.0 99 70-130 Hexane 24.0 1.0 ug/L 20.0 120 70-130 Isopropylbenzene 21.6 0.5 ug/L 20.0 108 70-130 m,p-Xylene 43.4 1.0 ug/L 40.0 108 70-130 Methylene chloride 20.8 2.0 ug/L 20.0 104 70-130 Naphthalene 20.5 1.0 ug/L 20.0 103 70-130 n-Buylbenzene 20.5 0.5 ug/L 20.0 102 70-130 n-Propylbenzene 21.0 0.5 u8/L 20.0 105 70-130 o-Xylene 2L3 0.5 u8/L 20.0 106 70-130 sec-Butylbenzene 20.7 2.0 ug/L 20.0 103 70-130 Styrene 21.7 0.5 u8/L 20.0 108 70-130 tert-Butylbenzene 21.4 0.5 118/1- 20.0 107 70-130 Tetrachloroethene 21.9 0.5 ug/L 20.0 109 70-130 Toluene 20.9 0.5 ug/L 20.0 104 70-130 trans-1,2-Dichloroethene 22.4 0.5 ug/L 20.0 112 70-130 Trichloroethene 22.7 0.5 ug/L 20.0 114 70-130 Vinyl chloride 21.9 0.5 u8/1. 20.0 109 60-140 Surrogate:l.2-Dichlomeihane-Da 108 70-130 Surrogate: 4-Bromqfluoroben_ene 95 70-130 Surrogate: Toluene-d8 !Ol 70-130 Matrix Spike (B6J0579-MS1) Source: 6100451-14 I,1,1-Trichloroethane 23.4 0.5 ug/L 20.0 ND 117 70-130 l,l-Dichloroethane 22.2 0.5 ug/L 20.0 ND ill 70-130 LI-Dichloroethene 24.9 0.5 u8/L 20.0 ND 125 70-130 1,2,4-Trimethylbenzene 22.6 0.5 ug/L 20.0 ND 113 70-130 1,2-Dichloroethane 21.3 0.5 ug/L 20.0 ND 107 70-130 Acetone 85.6 20.0 u8/L 100 ND 86 60-140 Benzene 23.3 0.5 ug/L 20.0 ND 116 70-130 Bromomethane (Methyl Bromide) 19.8 0.5 ug/L 20.0 ND 99 60-140 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report muv not be reproduced, except in full, without written permission from Rogers & Callcon. Inc Page 31 3838 WRogers &Cakott ENVIRONMENTAL Catalent Phartna Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result '9 REC Limits RPD Limit Flags Batch B6J0579 - EPA 5030 Matrix Spike (B6J0579-MS1) Source: 6100451-14 Chloroform 21.9 0.5 ug/L 20.0 ND 110 70-130 cis-1,2-Dichloroethene 23.8 0.5 ug/L 20.0 ND 119 70-130 Ethylbenzene 22.4 0.5 ug/L 20.0 ND 112 70-130 Hexane 21.9 1.0 ug/L 20.0 ND 109 70-130 Isopropylbenzene 24.5 0.5 ug/L 20.0 ND 123 70-130 m,p-Xylene 48.7 1.0 ug/L 40.0 ND 122 70-130 Methylene chloride 21.4 2.0 ug/L 20.0 ND 107 70-130 Naphthalene 20.2 1.0 ug/L 20.0 ND 101 70-130 n-Butylbenzene 22.7 0.5 ug/L 20.0 ND 113 70-130 n-Propylbenzene 23.6 0.5 ug/L 20.0 ND 118 70-130 o-Xylene 23.4 0.5 ug/L 20.0 ND 117 70-130 sec-Butylbenzene 23.3 2.0 ug/L 20.0 ND 116 70-130 Styrene 22.8 0.5 ug/L 20.0 ND 114 70-130 tert-Butylbenzene 22.7 0.5 ug/L 20.0 ND 114 70-130 Tetrachloroethene 26.4 0.5 ug/L 20.0 ND 132 70-130 sl Toluene 23.7 0.5 ug/L 20.0 ND 119 70-130 trans-1,2-Dichloroethene 23.1 0.5 ug/L 20.0 ND 116 70-130 Trichloroethene 24.9 0.5 ug/L 20.0 ND 125 70-130 Vinyl chloride 22.7 0.5 ug/L 20.0 ND 113 60-140 Surrogate: 1.2-Dichloroethane-D4 104 70-130 Surrogate: 4-8mmofluorohen_ene 97 -0-130 Surrogate: Toluene-& 114 70-130 Matrix Spike Dup (136,10579-MSD1) Source: 6100451-14 1,1,1-Trichloroethane 21.5 0.5 ug/L 20.0 ND 108 70-130 8 20 I,1-Dichloroethane 20.4 0.5 ug/L 20.0 ND 102 70-130 8 20 IJ-Dichloroethene 21.5 0.5 ug/L 20.0 ND 108 70-130 15 20 1,2,4-Trimethylbenzene 21.0 0.5 ug/L 20.0 ND 105 70-130 7 20 1,2-Dichloroethane 21.3 0.5 ug/L 20.0 ND 106 70-130 0.4 20 Acetone 94.2 20.0 ug/L 100 ND 94 60-140 10 20 Benzene 21.6 0.5 ug/L 20.0 ND 108 70-130 7 20 Bromomethane (Methyl Bromide) 19.9 0.5 ug/L 20.0 ND 100 60-140 0.8 20 Chloroform 20.7 0.5 ug/L 20.0 ND 104 70-130 6 20 cis-1,2-Dichloroethene 22.1 0.5 ug/L 20.0 ND 111 70-130 7 20 Ethylbenzene 20.8 0.5 ug/L 20.0 ND 104 70-130 7 20 Hexane 19.2 LO ug/L 20.0 ND 96 70-130 13 20 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 train 864.232.1556 1 tax 864.232.6140 rogersandealleott.eom an employee -owned _ompany 10 20 2016 14:33 This report mqv not be reproduced, except in full, without written pennission from Rogers & Callcott. Inc. Page 32 Of 38 Rogers &Cakott - ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Lc'el Result %REC Limits RPD Limit Flags Batch B6J0579 - EPA 5030 Matrix Spike Dup (B6J0579-MSD1) Source: 6100451-14 Isopropylbenzene 22.8 0.5 ug/L 20.0 ND 114 70-130 7 20 m,p-Xylene 44.8 1.0 ug/L 40.0 ND Ill 70-130 8 20 Methylene chloride 20.4 2.0 ug/L 20.0 ND 102 70-130 5 20 Naphthalene 20.3 1.0 ug/L 20.0 ND 102 70-130 0.7 20 n-Butylbenzene 20.6 0.5 ug/L 20.0 ND 103 70-130 9 20 n-Propylbenzene 21.9 0.5 ug/L 20.0 ND 109 70-130 8 20 o-Xylene 21.7 0.5 ug/L 20.0 ND 109 70-130 7 20 sec-Butylbenzene 21.4 2.0 ug/L 20.0 ND 107 70-130 9 20 Styrene 21.7 0.5 ug/L 20.0 ND 108 70-130 5 20 tert-Butylbenzene 20.9 0.5 ug/L 20.0 ND 105 70-130 8 20 Tetrachloroethene 23.9 0.5 ug/L 20.0 ND 119 70-130 10 20 Toluene 22.1 0.5 ug/L 20.0 ND 111 70-130 7 20 trans-1,2-Dichloroethene 21.1 0.5 ug/L 20.0 ND 105 70-130 9 20 Trichloroethene 22.4 0.5 ug/L 20.0 ND 112 70-130 11 20 Vinyl chloride 20.2 0.5 ug/L 20.0 ND 101 60-140 11 20 Surrogate:ll-Dichloroethane-Ua 104 -0-130 Surrogate:4-BromoJluorohen_ene 92 70-130 Surrogate: Toluene -A 107 70-130 Batch BU0581 - EPA 5030 Blank (B6J0581-BLKI) cis-1,2-Dichloroethene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L LCS (B6J0581-BSI) cis-1,2-Dichloroethene 22.4 0.5 ug/L 20.0 112 70-130 Tetrachloroethene 25.7 0.5 ug/L 20.0 128 70-130 Trichloroethene 25.0 0.5 ug/L 20.0 125 70-130 Matrix Spike (B6J0581-NISI) Source: 6100451-25RE1 cis-1,2-Dichloroethene 380 5.0 ug/L 200 152 114 70-130 Tetrachloroethene 501 5.0 ug/L 200 235 133 70-130 CI Trichloroethene 566 5.0 ug/L 200 312 127 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax 664.232.6140 rogersandealleott.eom an employee -owned company 10 20 2016 14:33 This report muv not be reproduced, except in full, without written permission from Rogers & Cullcott. Inc. Page 33 of 38 jRogers &Callcott Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe, NC 28110 Reported: 10/20/16 14:33 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result '% REC Limits RPD Limit Flags Batch B6J0581 - EPA 5030 Matrix Spike Dup (136.10581-NISDI) Source: 6100451-25RE1 cis-1,2-Dichloroethene 336 5.0 Tetrachloroethene 400 5.0 Trichloroethene 450 5.0 ug/L 200 152 92 70-130 12 20 ug/L 200 235 82 70-130 22 20 PI ug/L 200 312 69 70-130 23 20 PI, St PO Box 5655 I Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864,232.6140 rogersandcallcott.eom an employee -owned company 10 20 2016 14:33 This report mqv not be reproduced, except injull, without written permission from Rogers & Callcon, Inc. Page 34 Of 3H Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater - Monroe NC 2021 E. Roosevelt Blvd. Work Order: 6100451 Monroe. NC 28110 Reported: 10/20/16 14:33 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference P I The RPD between the sample / duplicate or matrix spike / spike duplicate was not within control limits due to matrix interference. S 1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. PO Box 5655 ' Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.com an employee -owned company 10 20 2016 1 a:33 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 35 of 38 �I= CHAIN Rogers & Ca Cott OF CUSTODY STODY RECORD WORK ORDER e I UU`15► � ENVIRONMENTAL N Filtered (Yes/No) — Y Cooled (Yes/No) Mailing PO Box 5655 Shipping 426 Fairforest Way 215B Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 G Container Type Llastic/Glass) Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 ao Container Volume (mL) Catalent Client Name G Sample Type (Grab/Composite) MonroeNC Address , GW Sample source (WW, GW, DW, SW, S, Other) Re ort To: P 41 c Preservation Code(s) u° A — None E — HCl I — Zn Acetate Email Address o B—HNO3 F—Na25203 1—H3POa Tele hone # P E +� Pq o N C — H2SOa G —Boric Acid K - MCAA D— NaOH H— Ascorbic Acid L- PO # Project # 93-121 � z ca 0 ar E ` 19 ao h a °" R&C WORK ORDER YRIb DATE TIME SAMPLE DESCRIPTION COMMENTS I /b/b 0%5;S !�� i �/� *3 vials unpres, 1 HCl L/ sAlw7PD6 ys y �� i 1 Z20 M w, pD r 32, Field Data Collected 'I IZ 3 Pit 6 -2- Ll --01 -� 1245 -, `l -35 -�� 1255 PI VT P-913 ZZ Y y - 308 hv-,9 PP6 29 -� 132 Mw►l PDT 77- `'IT-, INQUISHED BY: SA VC— 1 DATE/TIME: D / �L RECEIVED BY: 2 L�%U(� n �G '71' DATE/TIME: `00 �0 1-W Composite Start Date: Composite Start Time: RELI ISHEpD BY: DATE/TIME: RECEIVE Y: DATE/TIME: p (�� 3 ��I l I'1� 4 Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED B DATE/TIE: �D -"4 N yJ 5. 6 Temperature of blank or representative sample At time of collection 'C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7. 8, At time of lab receipt 61 L( "C Possible Hazards associated with samples: nNon-HazardFlammable ❑Skin Irritant Poison DUnknown ❑Other Form Revised July, 2014 Page 1 Page 36 of 38 .r CHAIN Rogers &Ca Cott OF CUSTODY RECORD WORK ORDER U (004S I ENVIRONMENTAL N Filtered (Yes/No) Y Cooled (Yes/No) Mailing PO Box 5655 Shipping 426 Fairforest Way 215E Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 G Container Type (Plastic/Glass) Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 40 Container Volume (ml.) Catalent Client Name G Sample Type (Grab/Composite) Address Monroe, NC In ow Sample Source (WW, GW, DW, SW, 5, Other) Cu c Re ort To: p 'co c v + Preservation Codes) u A — None E — HCI I — Zn Acetate Email Address o h > B — HNO3 F — Na25203 J — H3PO4 Telephone # v E 45 as N C—H2SO4 G—Boric Acid K-MCAA D— NaOH H —Ascorbic Acid L- PO # Project # 93-1.21 z 0 E a w R&C WORK ORDER YR ' DATE TIME SAMPLE DESCRIPTION COMMENTS It b 1333 c 1 '• etitp1. 1;., k m v i( Y Cl *3 vials unpres, 1 HC1 ti 13�3 taw3A,1,5 labs ft 2 s l 2 M w 1,J L] Field Data Collected 3 L/ w ��1 r BIZ CZ-1 POP 29 Y SAMP REL HED BY: 1 DATE/TIME: JW RECEIVED BY: 2. SeC.v,(i Ayem, DATE/TIME: Composite Start Date: 10 614 Composite Start Time: RELI UISHED B ATE/TIME: RECEI E BY: DATE/TIME: 3. �cUN� e6" 4. Z( D•1 •lto 1`4- Time or Flow (Circle one) Initials: RELINQUISHED BY:. DATE/TIME: RECEIVED BY: DATE/TIME: Temperature of blank or representative sample S. 6. At time of collection °C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7, g_ At time of lab receipt °C Possible Hazards associated with samples: ® Non -Hazard ❑Flammable Skin Irritant 0 Poison 0Unknown ❑other Form Revised July, 2014 Page Page 37 of 38 Rogers &�Caticott ENVIRO,NKENTAL Sample Receipt Verification Date Work Client: L '( 81,15TJ T Received: to, -7. (ta Order: (e 100' j 5 Carrier Name: Client FedEx UPS US Mail Courier Field Servic Other: Tracking Number: Receipt Criteria Y e s u A Comments Shipping container / cooler intact? 1 Damaged Leaking Other: Custody seals intact?J COC included with samples? x COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? . VOA vials free of headspace (<6mm bubble)? Samples cooled? Temp at receipt recorded on COC p Temp measured with IR thermometer - SN: 97050067 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. v oc Ck.0 { l Gh Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? X If in-house preservation used — record Lot # HCL H3PO4 HZSO4 NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or INo) Non -Conformance issue other than noted above: Revised July 2014 Completed by: XJEU Paae 38 of 38 Catalent PDB Temperature Field Sheet DATE TIME Monitoring Well Water Level (ft below TOC TEMP. °C SAMPLER 10/6/2016 1209 MW7PDB 45' 24.25 21.1 JHF/JCK 10/6/2016 1220 MW1PDB 32' 27.22 20.1 JHF/JCK 10/6/2016 1233 MW12PDB 42' 24.67 21.5 JHF/JCK 10/6/2016 1245 MW10PDB 66' 32.12 22.4 JHF/JCK 10/6/2016 1255 MW8PDB 27' 16.85 20.8 JHF/JCK 10/6/2016 1308 MW9PDB 29' 25.63 19.4 JHF/JCK 10/6/2016 1319 MW6PDB 52' 27.10 20.7 JHF/JCK 10/6/2016 1329 MW11PDB 72' 32.42 19.8 JHF/JCK 10/6/2016 1343 MW3APDB 106' 26.85 19.5 JHF/JCK 10/6/2016 1442 PZ1 PDB 29' 26.56 19.5 JHF/JCK COMMENTS: Temp Probe-RR1-17122 \\RC-VMSRV03\ProjedsN4\93-121\2016\DATA\Field Data\10.6.16\Catalent PDB Field Sheet xis ❑ Development FIELD DATA LOG FOR GROUNDWATER SAMPLING f3 Purging by Volume ❑ Low Flow -) Q Rogers CaCleott Well Identification or Number: MW5 .& El Micro -Purge ENVIRONMENTAL Date: 1016/16 Field Personnel: JHF/JCK Site Name/Location: Catalent Weather Conditions/"'Temp: Mostly cloudy / 73 °F Page 2 of 7 Method of Well Evacuation or Sample Collection Water Volume Calculations Circle One that Applies Pump Bailer Initial Depth to Ground Water (a): 58.12 @ 1358 Measuring Point: ❑ Grundfos ❑ Non Disposable Teflon Total Depth of Well (b): Riser Material: ❑ Submersible [I Disposable Teflon Length of Water Column in We - 8.12 Steel Pro ecti asing? ❑ Peristaltic ❑ Disposable Poly Well Casing Diameter (inches): i� lards? ❑ Bladder ❑ Dedicated Teflon Depth to Immiscible Layer: NA 1• . I h Mount? ❑ Waterra S Continuous (Recovery Well) El One Volume Multiplier (gal/ft) = n rz h (7.48) (r in feet) Well Diameter(gal/ft.) I"=0.041; 2"=0.163; 3"=0.367 4"= 0.653; 6"= 1.470 Water f2Pmnval / Fipld Analvsis Data # of Casings Gallons to be Total Gallons Removed Removed 1 Casing Vol = 0.00 (b-a) x Multiplier 3 Casing Vol 0.00 1.00 I Loc ed? W II Padlie di ion? l g? W�II I4e ri�c ry? Vegetation: Light Date Time Increment Removal Rate ferallm)or (ml m) Water Level (feet) Water Volume Removed I or (ml) pH (+/-0.1) (Stabilization) Temp VC) Conductivity (us/cm) 5% Dissolved Oxygen (mg/L) DRIP (mV01ts) Odor (Subj•) Turbidity (NTUs) Other Parameter or Comments 10/6/16 1402 na 58.12 1.0 6.11 21.7 560.0 NA NA 1 <5.0 1 3 4 5 6 7 0u0/ec[rve (1/ rvunr (Z/ .wynr (s/ rvwoerurr (4/ �uuny Well Yield: High Sample Clarity: clear Precipitate: None Fe+z mg/L= NA Sample Collection Time: VOCS-1402 Co Revised 1-10-13 FIELD DATA LOG FOR GROUNDWATER SAMPLING Well Identification or Number: MW4 Date: 10/6/16 Field Personnel: JHF/JCK ❑ Development M Purging by Volume ❑ Low Flow ❑ Micro -Purge Rogers &Callc Ott ENVIRONMENTAL Site Name/Location: Catalent Weather Conditions/Temp: Mostly cloudy / 73 °F Page 3 of 7 Method of Well Evacuation or Sample Collection Pump Bailer ❑ Grundfos ❑ Non Disposable Teflon ❑ Submersible ❑ Disposable Teflon ❑ Peristaltic ❑ Disposable Poly ❑ Bladder ❑ Dedicated Teflon ❑ Waterra 111 Continuous (Recovery Well) One Volume Multiplier (gal/ft) = it rz h (7.48) (r in feet) Well Diameter (gal/ft.) 1"= 0.041; 2"= 0.163; 3"= 0.367 4"= 0.653; 6"= 1.470 Water Removal / Field Analysis Data Water Volume Calculations Initial Depth to Ground Water (a): 35.90 @ 1410 Total Depth of Well (b): Length of Water Column in We 1(b-a): -35.90 Well Casing Diameter (inches): Depth to Immiscible Layer: NA # of Casings Gallons to be Total Gallons Removed Removed 1 Casing Vol = 0.00 (b-a) x Multiplier 3 Casing Vol 0.00 1.00 Circle One that Applies g Point: �t;"ateriai: eel tive Casing? B Ilar s? ush u t? el LbJ✓ L II C ndition? ell Tag? Well Integrity Satisfactory? Vegetation: Light Date Time Increment Removal Rate al m)or (in, m) Water Level (feet) Water Volume Removed )or(ml) pH (+/-0.1) (Stabilization) Temp (•C) Conductivity (US/CM) 5% Dissolved Oxygen (mg/L) ORP (mvolts) Odor (Subj•) Turbidity I Other Parameter or Comments (NTUs) 10/6/16 1412 na 35.90 1.0 6.27 23.2 488.6 NA NA 1 <5.0 i 3 4 AV 5 "i 6 7 Well Yield: LOW Sample Collection Time: VOCS-14 Comments: . Subjective (I) None (2) Slight (3) Moderate (4) Strong Sample Clarity: clear Precipitate: None Fe+2 mg/L= NA Revised 1-10-13 FIELD DATA LOG FOR GROUNDWATER SAMPLING ❑ Development 8 Purging by Volume Well Identification or Number: MW3 ❑ tow Flow ❑ Micro -Purge Rogers'&:Callcott Date: 10/6116 Field Personnel: JHF/JCK * E N V I R O N M E N TA L Site Name/Location: Catalent Weather Conditions/ —Temp: Mostly cloudy / 75 OF Page 4 of 7 Method of Well Evacuation or Sample Collection Water Volume Calculations Circle One that Applies PUMP Bailer Initial Depth to Ground Water (a): 53.50 @ 1421 Suring Point: ❑ Grundfos ❑ Non Disposable Teflon Total Depth of Well (b): / gglser n eal: ❑ Submersible ❑Disposable Teflon Length of Water Column in We : -53.50 /_ \ S P L ctive Casl ? ❑ Peristaltic ❑ Disposable Poly Well Casing Diameter (inches): _ �j B Ilards? ❑ Bladder ❑ Dedicated Teflon Depth to Immiscible Layer: NA I,ount? ❑ Waterra 0 Continuous (Recovery Well 173 One Volume Multiplier (gal/ft) = n rl h (7.48) (r in feet) Well Diameter (gal/ft.)1"=0.041; 2"=0.163; 3"=0.367 4"= 0.653; 6"= 1.470 Water Removal / Field Analvsis Data # of Casings Gallons to be Total Gallons Removed Removed 1 Casing Vol = (b-a) x Multiplier 0.00 J! 3 Casing Vol 0.00 1.00 I II cked? 1 ell P d Condition? Well Tag? Well Integrity Satisfactory? Vegetation: Light Date Time Increment Removal Rate _Lgallm) (ml m) Water Level (feet) Water Volume Removed q or (rnl) pH (+/-0.1) (Stabilization) Temp (`C) Conductivity (US/CM) 5% Dissolved Oxygen (mg/L) ORP (mV01ts) Odor (Subi•) Turbidity (NTUs) Other Parameter or Comments 10/6/16 1423 na 53.50 1.0 6.54 21.9 449.8 NA NA 1 <5.0 1 2 3 4 5 6 7 Well Yield: High Sample Collection Time: VOCs-1 Comm Sample Clarity: "Subjective (1) None (2) Slight (3) Moderate (4) Strong Precipitate: None Fern mg/L= NA Revised 1-10-13 FIELD DATA LOG FOR GROUNDWATER SAMPLING Well Identification or Number: MW2 Date: 10/6116 Field Personnel: JHF/JCK Site Name/Location: Catalent Method of Well Evacuation or Sample Collection P- ump Bailer ❑ Grundfos ❑ Non Disposable Teflon ❑ Submersible ❑ Disposable Teflon ❑ Peristaltic ❑ Disposable Poly ❑ Bladder ❑ Dedicated Teflon ❑ Waterra E Continuous (Recovery Well) One Volume Multiplier (gal/ft) = n r2 h (7.48) (r in feet) Well Diameter (gal/ft.) 1"= 0.041; Z"= 0.163; 3"= 0.367 4"= 0.653; 6"= 1.470 Water Removal / Field Analysis Data ❑ Development 8 Purging by Volume Tyr ❑ Low Flow1�111 Rogers & Callcott ❑ Micro -Purge ENVIRONMENTAL Weather Conditions/Temp: Mostly Cloudy / 74 of Page_5 of 7 Water Volume Calculations Initial Depth to Ground Water (a): 33.40 @ 1431 Total Depth of Well (b): Length of Water Column in Well (b-a): -33.40 Well Casing Diameter (inches): 2" Depth to Immiscible Layer: NA a of Casings Gallons to be Total Gallons Removed Removed 1 Casing Vol = -5.44 (b-a) x Multiplier 3 Casing Vol -16.33 0.50 Circle One that Applies Measuring Point: TOC Riser Material: Steel Steel Protective Casing? Yes Bollards? No Flush Mount? No Well Locked? Yes Well Pad Condition? OK Well Tag? OK Well Integrity Satisfactory? OK _ Vegetation: Light Date Time Increment Removal Rate I m) or (ml m) Water Level (feet) Water Volume Removed or (ml) pH W- 0.1) (Stabilization) Temp CC) Conductivity (us/cm) 5% Dissolved Oxygen (mg/L) ORP (mV01ts) Odor (Subj•) Turbidity (NTUs) Other Parameter or Comments 10/6/16 1434 na 33.40 0.5 6.20 23.3 469.1 NA NA 1 19.5 1 3 4 5 6 7 Well Yield: LOW Sample Collection Time: Sample Clarity: ' Subjective (1) None (2) Slight (3) Moderate (4) Strong Precipitate: None Fe'z mg/L= NA Revised 1-10-13 6 of z Rogers and Callcott Environmental Client: Catalent Date: 10/6/16 Field Meter Calibration Record Conductivity Calibration - EPA 9050A Meter Make / Model: Orion Star A325 SN: G04166 Probe: RR1-17122 Time: 0904 Analyst: JHF Cell Constant 0.483 Chemical Inventory Conc. of Standard, µmhos/cm @25°C Actual Reading of Standard, µmhos/cm @Temperature, °C P603493 10.14 10.58 21.5 P603495 100.5 100.2 21.8 P603499 999 1027 21.6 P603518 I SSS conc: 1447 458.4 1 21.7 Temperature compensation for pH / conductivity meter: 0.0 p H Calibration = EPA 9040C Meter Make / Model: Orion Star A325 Probe: UX1-16637 Time: 0855 Analyst: JHF Slope: 99•4 Chemical Inventory Conc. of Buffer, units Actual Reading of Buffer, units P604773 4.0 4.02 P602655 7.0 7.02 P601774 10.0 10.05 P604668 SSS conc: 7.0 7.03 Turbidity Meter. Calibration lw Field -Screen Method Meter Make / Model: Hach 2100P 5N: 130200023551 Date of most recent calibration: 10/3/16 Time: 0908 Analyst: JHF Chemical Inventory Assigned Conc. of Standard, NTU Actual Reading of Standard, NTU P605075 5.33 5.46 P605076 55.1 53.5 P605077 555 553 Reviewed by: Date: Revised 01/21/13 7Of 7 Rogers and Callcott Environmental Client: Catalent Continuing Calibration Verification Date: 10/6/16 _ Conductivity Meter EPA 9050A Meter Make/Model: Orion StarA325 SN: G04166 Probe: RR1-17122 Time Analyst Conc. of Standard, Actual Reading of Standard, µmhos/cm @25°C µmhos/cm 1349 JHF 999 1039 @ 21.5 °C 1445 JHF 100.5 102.7 @ 25.1 °C pH Meter., EPA.9640C . Meter Make / Model: Orion Star A325 Probe: UX1-16637 Time Analyst Conc. of Buffer, Actual Reading of Buffer, units units 1349 JHF 7.0 6.97 1445 JHF 1 4.0 1 4.09 Turbidity Meter . :.Field Screen Method Meter Make / Model: Hach 2100P or 2100Q SN: 130200023551 Time Analyst Assigned Conc. of Standard, Actual Reading of Standard, NTU NTU 1349 JHF 555 548 1445 JHF 5.33 5.21 Field Duplicate _ Well ID: MW5 Time Analyst Conductivity, pH, Turbidity, Temperature, µmhos/cm units NTU °C 1405 JHF 562.0 6.20 <5.0 22.0 Note: Refer to daily calibration log for instrument calibration and chemical inventory information / documentation. Reviewed by: Date: Revised 01/21/13 ow Rogers & Callcott ENVIRONMENTAL Laboratory Report Client Catalent Pharma Solutions Project: C/O George Maalouf (Rogers & Callcott) Work Order: 2021 E. Roosevelt Blvd. Received: Monroe, NC 28110 Dear Client: Effluent 6090335 09/08/2016 07:55 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on September 08, 2016. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Lauren Woodrum, your Project Manager, at lauren.woodrum@rogersandeallcott.com or (864)-232-1556 if you have any questions about this report. Permit #WQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski (R&C) Report Approved By 4AJI�zl� Lauren Woodrum Project Manager This report may not be reproduced, except in full, without written pennission from Rogers & Callcott. Inc. PCB Box 5655 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcal Icott.com --- an employee -owned company Page 1 of 11 ENVIRONMENTALRogers &Callcott Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf (Rogers & Callcott) 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 6090335-01 Effluent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Effluent Work Order: 6090335 Received: 09/08/2016 07:55 Matrix Sampled Type Ground Water 09/07/16 13:00 Grab PO Box 5655 '• Greenville, SC 29606 1426 Fairforest Way ! Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom an employee -owned company 09 14 2016 08:51 This report mqv not be reproduced, except infull, without written permission from Rogers & Callcou. Inc Page 2 Of Rogers & callcott i._ ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe, NC 28110 Reported: 09/14/16 08:51 Sample Data Sample Number 6090335-01 Sample Description Effluent Grab collected on 09/07/16 13:00 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 8.0 0.1 pH Units 1.00 09/07/16 13:00 Field Screen SWG 13610252 Temperature 25.6 0.0 °C 1.00 09/07/16 13:00 Field Screen SWG 13610252 Volatile Organics 1, 1, l-Trichloroethane ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B6I0415 1,1-Dichloroethane ND 05 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B6I0415 1,1-Dichloroethene ND OS ug/L 1.00 09/09/16 17:01 EPA 8260B P2 LBW B6I0415 1,2,4-Trimethylbenzene ND 0.5 ag/L 1.00 09/09/16 IT01 EPA 8260E LBW B610415 1,2-Dichloroethane ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B610415 Acetone ND 20.0 ue/L 1.00 09/09/16 17:01 EPA 8260E LBW B6I0415 Benzene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW 13610415 Bromomethane (Methyl Bromide) ND 1.0 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW 13610415 Chloroform ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW B6I0415 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW B6I0415 Ethylbenzene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B6I0415 Hexane ND 1.0 ug/L 1.00 09/09/16 17:01 EPA 8260B P2 LBW B6I0415 Isopropylbenzene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW B610415 m,p-Xylene ND 1.0 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B6I0415 Methylene chloride ND 2.0 ug/L 1.00 09/09/16 17:01 EPA 826013 LBW B6I0415 Naphthalene ND 2.0 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B6[0415 n-Butylbenzene ND 1.0 ug/L 1.00 09/09/16 17:01 EPA 8260B P2 LBW B610415 n-Propylbenzene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B610415 o-Xylene ND OS ug/L 1.00 09/09/16 17:01 EPA 8260E LBW 13610415 sec-Butylbenzene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW B6I0415 Styrene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW B6I0415 tert-Butylbenzene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260E LBW 13610415 Tetrachloroethene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B P2 LBW B610415 Toluene ND 0.5 U91L 1.00 09/09/16 17:01 EPA 8260B LBW B6I0415 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B61[0415 Trichloroethcne ND 0.5 ug/L 1.00 09/09/16 17:01 EPA 8260B LBW B6I0415 Vinyl chloride ND 0 5 ug/L 1.00 09/09/16 17:01 EPA 8260E P2 LBW B6I04IS Surrogates %REC % REC Limits Flag 1,2-Dichloroethane-D4 100 70-130 4-Bromofluorobenzene 96 70-130 PO Box 5655 i Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 i main 864.232.1556 i fax 864.232.6140 rogersandealleott.eom an employee -owned company 09 14 2016 08:51 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 3 Of Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe, NC 28110 Reported: 09/14/16 08:51 Sample Number 6090335-01 Sample Description Effluent Grab collected on 09/07/16 13:00 Reporting Parameter Result Limit I nits DF Analyzed Method FLtg analyst Batch Volatile Organics Surrogates %REC % REC Limits Flag Toluene-dR 100 70-130 PO Box 5655 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax %4.232.6140 rogersandcalleott.eom an employee owned company 0914 2016 08:51 This report muv not be reproduced, except in full, without written permission from Rogers & Callcon. Inc. Page 4 Of 1 � Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe, NC 28110 Reported: 09/14/16 08:51 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B610415 - EPA 5030 Blank (B6[0415-BLKI) 1,1,1-Trichloroethane ND 0.5 ug/L 1,1-Dichloroethane ND 0.5 ug/L 1,1-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 1.0 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L Isopropylbenzene ND 0.5 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 2.0 ug/L n-Butylbenzene ND 1.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ugfL Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate:l.2-Dieltloroethane-D4 95 70-130 Surrogate: 4-Bromciluoroben-ene 100 70-130 Surrogate: Toluene-& 99 -0-130 LCS (B6[0415-BSI) 1,1,1-Trichloroethane 23.6 0.5 ug/L 20.0 118 70-130 1,1-Dichloroethane 22.4 0.5 ug/L 20.0 112 70-130 1,1-Dichloroethene 23.3 0.5 ug/L 20.0 116 70-130 1,2,4-Trimethylbenzene 2L8 0.5 ug/L 20.0 109 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax 864.232.6140 rogersandealleott.eom an emplovee-owned company 0914 2016 08:51 This report nmv not be reproduced, except in full, without written permission from Rogers & ('allcott. Inc. Page 5 of 1 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe. NC 28110 Reported: 09/14/16 08:51 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B610415 - EPA 5030 LCS (B610415-BS 1) 1,2-Dichloroethane Acetone Benzene Bromomethane (Methyl Bromide) Chloroform cis-1,2-Dichloroethene Ethylbenzene Hexane Isopropylbenzene m,p-Xylene Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene Trichloroethene Vinyl chloride 21.1 0.5 ug/L 20.0 105 70-130 85.3 20.0 ug/L 100 85 60-140 22.5 0.5 ug/L 20.0 113 70-130 15.7 1.0 ug/L 20.0 78 60-140 21.1 0.5 ug/L 20.0 106 70-130 23.0 0.5 ug/L 20.0 115 70-130 22.1 0.5 ug/L 20.0 111 70-130 25.0 1.0 ug/L 20.0 125 70-130 22.1 0.5 ug/L 20.0 Ito 70-130 45.8 1.0 ug/L 40.0 115 70-130 20.3 2.0 ug/L 20.0 102 70-130 18.1 2.0 ug/L 20.0 91 70-130 23.6 1.0 ug/L 20.0 118 70-130 21.2 0.5 ug/L 20.0 106 70-130 21.3 0.5 ug/L 20.0 107 70-130 24.1 0.5 ug/1. 20.0 120 70-130 21.7 0.5 ug/L 20.0 l08 70-130 21.2 0.5 ug/L 20.0 106 70-130 22.2 0.5 ug/L 20.0 111 70-130 21.0 0.5 ug/L 20.0 105 70-130 23.1 0.5 ug/L 20.0 116 70-130 23.2 0.5 ueL 20.0 116 70-130 19.1 0.5 ug/L 20.0 95 60-140 Surrogate: 1.1-Dichloroe/hone-D4 Surrogate: a-Bromofluoroben_ene Surrogate: Toluene-d8 Matrix Spike (B610415-MSI) Source: 6090335-01 102 70-130 91 70-130 108 70-130 1,I,I-Trichloroethane 25.2 0.5 ug/L 20.0 ND 126 70-130 l,l-Dichloroethane 23.7 0.5 ug/L 20.0 ND 119 70-130 I,1-Dichloroethene 24.6 0.5 ug/L 20.0 ND 123 70-130 1,2,4-Trimethylbenzene 22.6 0.5 ug/L 20.0 ND 113 70-130 1,2-Dichloroethane 23.6 0.5 ug/L 20.0 ND 118 70-130 Acetone 112 20.0 ug/L 100 ND 112 60-140 Benzene 21.4 0.5 ug/L 20.0 ND 107 70-130 Bromomethane (Methyl Bromide) 17.4 1.0 ug/L 20.0 ND 87 60-140 PO Box 5655 . Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax %4.232.6140 rogersandeallcott.eom an employee-o�:ned compam, 09 14 2016 08:51 This report may nor be reproduced, except in full, withour written permission from Rogers & Callcott Inc. Page 6 of 1 � Rogers & Callcott FW; ENVIRONMENTAL Catalent Phanna Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe, NC 28110 Reported: 09/14/16 08:51 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch BQ0415 - EPA 5030 Matrix Spike (8610415-MSl) Source: 6090335-01 Chloroform 20.4 0.5 ug/L 20.0 ND 102 70-130 cis-1,2-Dichloroethene 24.6 0.5 ug/L 20.0 ND 121 70-130 Euylbenzene 22.2 0.5 ug/L 20.0 ND 111 70-130 Hexane 24.3 LO ug/L 20.0 ND 122 70-130 Isopropylbenzene 22.3 0.5 ug/L 20.0 ND 112 70-130 m,p-Xylene 47.9 1.0 ug/L 40.0 ND 120 70-130 Methylene chloride 19.0 2.0 ug/L 20.0 ND 95 70-130 Naphthalene 18.8 2.0 ug/L 20.0 ND 93 70-130 n-Butylbenzene 22.0 LO ug/L 20.0 ND 110 70-130 n-Propyibenzene 21.6 0.5 ug/L 20.0 ND 108 70-130 o-Xylene 21.2 0.5 ug/L 20.0 ND 106 70-I30 sec-Butylbenzene 24.9 0.5 ug/L 20.0 ND 125 70-130 Styrene 22.5 0.5 ug/L 20.0 ND Ill 70-130 tert-Butylbenzene 21.6 0.5 ug/L 20.0 ND 108 70-130 Tetracirloroethene 21.7 0.5 ug/L 20.0 ND 108 70-130 Toluene 21.8 0.5 ug/L 20.0 ND 109 70-130 trans-1,2-Dichloroethee 24.7 0.5 ug/L 20.0 ND 124 70-130 Trichloroethene 24.1 0.5 ug/L 20.0 ND 119 70-130 Vinyl chloride 19.0 0.5 ug/L 20.0 ND 95 60-140 Surrogate: 1.2-Dichloroethane-D4 115 70-130 Surrogate: 4-Bromofluorohenzene 98 70-130 Surrogate: Toluene-& 114 70-130 Matrix Spike Dup (136I0415-MSDI) Source: 6090335-01 1.1,l-Trichloroethane 20.6 0.5 ug/L 20.0 ND 103 70-130 20 20 I,l-Dichloroethane 20.4 0.5 ug/L 20.0 ND 102 70-130 15 20 1,1-Dichloroethee 19.9 0.5 ug/L 20.0 ND 100 70-130 21 20 P2 1,2,4-Trimethylbenzene 19.6 0.5 ug/L 20.0 ND 98 70-130 14 20 1,2-Dichloroethane 22.7 0.5 ug/L 20.0 ND 114 70-130 4 20 Acetone 117 20.0 ug/L 100 ND 117 60-140 5 20 Benzene 18.1 0.5 ug/L 20.0 ND 90 70-130 17 20 Bromomethane (Methyl Bromide) 15.0 1.0 ug/L 20.0 ND 75 60-140 15 20 Chloroform 17.9 0.5 ug/L 20.0 ND 90 70-I30 13 20 cis-1,2-Dichloroethee 22.2 0.5 ug/L 20.0 ND I10 70-130 10 20 Etylbenzene 18.6 0.5 ug/L 20.0 ND 93 70-130 18 20 Hexane 18.5 1.0 ug/L 20.0 ND 93 70-130 27 20 P2 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax 864.232.6140 rogersandeallcott.eom an employee -owned company 09 141016 08:51 This report mqv not be reproduced, except infull, without wrinen permission from Rogers & Callcott. Inc. Page 7 OP y g , Rogers &Callcott '-- ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe, NC 28110 Reported: 09/14/16 08:51 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B6I0415 - EPA 5030 Matrix Spike Dup (11610415-MSD1) Source: 6090335-01 Isopropylbenzene 18.7 0.5 ug/L 20.0 ND 94 70-130 18 20 m,p-Xylene 40.9 1.0 ug/L 40.0 ND 102 70-130 16 20 Methylene chloride 17.1 2.0 ug/L 20.0 ND 86 70-130 10 20 Naphthalene 18.3 2.0 ug/L 20.0 ND 90 70-130 3 20 n-Butylbenzene 17.6 1.0 ug/L 20.0 ND 88 70-130 22 20 P2 n-Propylbenzene 18.0 0.5 ug/L 20.0 ND 90 70-130 18 20 o-Xylene 18.1 0.5 ug/L 20.0 ND 90 70-130 16 20 sec-Butylbenzene 20.8 0.5 ug/L 20.0 ND 104 70-130 19 20 Styrene 20.4 0.5 ug/L 20.0 ND 102 70-130 10 20 tert-Butylbenzene 18.2 0.5 ug/L 20.0 ND 91 70-130 17 20 Tetrachloroethene 17.4 0.5 ug/L 20.0 ND 87 70-130 22 20 P2 Toluene 18.5 0.5 ug/L 20.0 ND 92 70-130 16 20 trans-1,2-Dichloroethene 20.5 0.5 ug/L 20.0 ND 102 70-130 19 20 Trichloroethene 20.0 0.5 ug/L 20.0 ND 99 70-130 19 20 Vinyl chloride 14.2 0.5 ug/L 20.0 ND 71 60-140 29 20 P2 Surrogate: 1.2-Dichloroeihane-D4 110 -0-130 Surrogate:4-Bromofluoroberr_ene 88 70-130 Surrogate: Toluene-d8 100 70-130 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom an employee -owned company 09 14 2016 08:51 This report muv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 8 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 6090335 Monroe, NC 28110 Reported: 09/14/16 08:51 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference P2 The RPD between the matrix spike / spike duplicate exceeded the control limits; however, both spike recoveries were within control limits. PO Sox 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom an employee -owned company 09 14 2016 08:51 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 9 Of Rogers CallCOtt CHAIN OF CUSTODY RECORD ENVIRONMENTAL " Y Mailing Po Box 5655 Shipping 426 Fairforest Way 2158 Stoneridge Drive Address Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 G Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Caiitlelli Client Name 40 G Address Monroe, NC GW c Report To: U Email Address 0 Telephone # Tele p cu E oo PO # Project # 93-121 Z E 7 R&C YR�{p WORK ORDER DATE TIME SAMPLE DESCRIPTION O F' � t� p��5'o► • � �3r� F _ SAMP — JyfffI ED BY: DATE%1-IM : RECEI D BY: DATE/TIME: % Y: _ RELINQUISHED B%; DATE/TIME: 3. 4. RELINQUISHED BY: DATERIVIE: RECEIVED BY: 5. 6. RELINQUISHED BY: DATE/TIME: RECEIVED BY: 7. 8. Possible Hazards associated with samples: Non -Hazard ❑Flammable ❑Skin Irritant FiPoisonFlUnknowm IDDther DATE/TIME: WORK ORDER Filtered (Yes/No) Cooled (Yes/No) Container Type (Plastic/Glass) Container Volume (ml) Sample Type (Grab/Composite) Sample Source (WW, GW, DW, SW, S, Other) — Preservation Codes) A — None E — HCI I — Zn Acetate B—HNO3 F—Na1S203 1—H3PO4 C — H2SO4 G — Boric Acid K - MCAA D — NaOH H — Ascorbic Acid L - COMMENTS *3 vials unpres, 1 HC1 Effluent L�0C4 (J ')`' ()1 pH - .,TB Collected on� 6@l3ou Temp -z .(, °(' by Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: Temperature of blank or representative sample DATE/TIME: At time of collection -.—°C At time of lab receipt G • S- °C Form Revised July, 2014 Page __� Page 10 of 11 Rogers &-C611cott ENVIRONMENTAL Sample Receipt Verification Date Work Client: CA --I Rt�ENT Received: j Order: (QQ O33 S' Carrier Name:. Client FedEx UPS US Mail Courier Field Services Other: Tracking Number: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample 1D on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? ' VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on CoC Samples cooled? Temp measured with IIt thermometer - SN: 97050067 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. V 0 G G Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot # HCL HIP04 H2SO4 NaOH HN01 Other Comments: Were non-conformance issues noted at sample receipt? Yes or � No , Non -Conformance issue other than noted above: Revised July 2014 Completed by: y X _ U Page 11 of 11 = Rogers & Callcott - ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf (Rogers & Callcott) 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Laboratory Services Influent 6090336 09/08/2016 07:55 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on September 08, 2016. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Lauren Woodrum, your Project Manager, at lauren.woodrum@rogersandcallcott.com or (864)-232-1556 if you have any questions about this report. Permit #WQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski (R&C) Report Approved By: 4AVYI�zl� Lauren Woodrum Project Manager This report may not be reproduced eccept in full, without wrillen permission from Rogers & Callcott. Inc. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 train 864.232.1556 1 fax 864.232.614o rogersandealleott.eom an employee -owned company Page 1 of 11 Rogers &Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf (Rogers & Callcott) 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 6090336-01 Influent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Influent Work Order: 6090336 Received: 09/08/2016 0755 Matrix Sampled Type Ground Water 09/07/16 13:15 Grab PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way 1 Greenville. SC 29607 1 main 864.232.1556 1 tax %4.232.6140 rogersandealleott.eom an empioyee-owned companv 09 14 2016 09:01 This report mqv not be reproduced, except in full, without written permission from Rogers & C'allcou. Inc. Page 2 Of Rogers & Callcott - ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Sample Data Sample Number 6090336-01 Sample Description Influent Grab collected on 09/07/16 13:15 Parameter Result Reporting Limit Units DF Analyzed Nlethod Flag Analyst Batch Volatile Organics 1,1,1-Trichloroethane ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B610415 I,1-Dichloroethane 1.2 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B610415 I,l-Dichloroethene 1.2 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 1,2,4-Trimethylbenzene ND OS ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 1,2-Dichloroethane ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW 13610415 Acetone ND 20.0 us/L 1.00 09/09/16 11:50 EPA 8260E LBW B6I0415 Benzene ND 0.5 u8/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 Bromomethane (Methyl Bromide) ND 1.0 ug/L 1.00 09/09/16 11:50 EPA 9260B LBW B6I0415 Chloroform 8.4 0.5 ug/L 1.00 09/09/16 11:50 EPA 9260B LBW B6I0415 c is- 1,2-Dichloroethene 72.9 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B610415 Ethylbenzene ND OS ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 Hexane ND 1.0 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B610415 Isopropylbenzene ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260E LBW 13610415 m,p-Xylene ND LO ug/L 1.00 09/09/16 11:50 EPA 8260E LBW B6I0415 Methylene chloride ND 2.0 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 Naphthalene ND 2.0 119/1. 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 n-Butylbenzene ND LO ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 n-Propylbenzene ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW 13610415 o-Xylene ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260E LBW B6I0415 sec-Butylbenzene ND 0.5 ug/L 100 09/09/16 11:50 EPA 8260B LBW B6I0415 Styrene ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260E LBW B6I0415 tert-Butylbenzene ND OS ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 Toluene ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260E LBW B6I0415 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 Vinyl chloride ND U ug/L 1.00 09/09/16 11:50 EPA 8260B LBW B6I0415 Rebatch Sample Number: 6090336-OIRE1 Tetrachloroethene 88.6 2.5 ug/L 5.00 09/09/16 18:32 EPA 8260E LBW B6I0415 Trichloroethene 99.9 2.5 ug/L 5.00 09/09/16 18:32 EPA 8260E LBW B6I0415 Surrogates % REC %REC Limits Flag 1,2-Dichloroethene-D4 98 70-130 4-Bromojluombenzene 99 70-130 Toluene-ds 96 70-130 Rebatch Sample Number: 6090336-01RE1 1.2-Dichloroetbane-D4 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way Greenville. SC 29607 1 main 864.232.1556 1 far 864.232.6140 rogersandealleott.eom ar �n,G ;sae ;wrnd -crroa,, 09 14 2016 09:02 This report may not be reproduced, except in, full, without written permission from Rogers & Callcott. Inc. Page 3 Of Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Sample Number 6090336-OIRE1 Sample Description Influent Grab collected on 09/07/16 13:15 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 6090336-OIREI 4-Bromofluorobenzene 96 70-130 Toluene-dR 99 70-130 PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 09 14 2016 09:02 This report mqv not be reproduced, except in full, without written permission from Rogers & C'allcott. Inc. Page 4 Of PK Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit t nits Level Result % REC Limits RPD Limit Flags Batch B610415 - EPA 5030 Blank (B61041 S-BLK1) 1,1.1-Trichloroethane ND 0.5 ug/L I,l-Dichloroethane ND 0.5 ug/L I,l-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 1.0 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L lsopropylbenzene ND 0.5 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 2.0 ug/L n-Butylbenzene ND 1.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate: 1.2-Dichloroethane-D4 Surrogate: 4-Bromofluoroben_ene Surrogate: Toluene-& LCS (B6[0415-BSI) 95 70-130 100 70-130 99 -0-130 1, 1, 1 -Trichloroethane 23.6 0.5 ug/L 20.0 118 70-130 I,l-Dichloroethane 22.4 0.5 ug/L 20.0 112 70-130 1,1-Dichloroethene 23.3 0.5 ug/L 20.0 116 70-130 1,2,4-Trimethylbenzene 21.8 0.5 ug/L 20.0 109 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax 864.232.6140 rogersandealleott.eom an employee -owned company 09 14 2016 09:02 This report may not be reproduced, except in full, without written permission from Rogers & Callcon. Inc. Page 5 Of NUL/ 'f M. Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Volatile Organics Quality Control Summary Reporting Spike Source %REC RI'D (Parameter Result Limit Units Level Result %REC Limits RPD Limit F'la<,. Batch B610415 - EPA 5030 LCS (B610415-BSI) 1,2-Dichloroethane 21.1 0.5 ug/L 20.0 105 70-130 Acetone 85.3 20.0 ug/L 100 85 60-140 Benzene 22.5 0.5 ug/L 20.0 113 70-130 Bromomethane (Methyl Bromide) 15.7 1.0 ug/L 20.0 78 60-140 Chloroform 21.1 0.5 ug/L 20.0 106 70-130 cis- 1,2-Dichloroethene 23.0 0.5 ug/L 20.0 115 70-130 Ethylbenzene 22.1 0.5 ug/L 20.0 111 70-130 Hexane 25.0 1.0 ug/L 20.0 125 70-130 Isopropylbenzene 22.1 0.5 ug/L 20.0 110 70-130 m,p-Xylene 45.8 1.0 ug/L 40.0 115 70-130 Methylene chloride 20.3 2.0 ug/L 20.0 102 70-130 Naphthalene 18.1 2.0 ug/L 20.0 91 70-130 n-Butylbenzene 23.6 1.0 ug/L 20.0 118 70-130 n-Propylbenzene 21.2 0.5 ug/L 20.0 106 70-130 o-Xylene 2 L3 0.5 ug/L 20.0 107 70-130 sec-Butylbenzene 24.1 0.5 ug/L 20.0 120 70-130 Styrene 21.7 0.5 ug/L 20.0 108 70-130 tert-Butylbenzene 21.2 0.5 ug/L 20.0 106 70-130 Tetrachloroethene 22.2 0.5 ug/L 20.0 111 70-130 Toluene 21.0 0.5 ug/L 20.0 105 70-130 trans-1,2-Dichloroethene 23.1 0.5 ug/L 20.0 116 70-130 Trichloroethene 23.2 0.5 ug/L 20.0 116 70-130 Vinyl chloride 19.1 0.5 ug/L 20.0 95 60-140 Surrogate: 1.1-Uichloroethane-L)4 102 70-130 Surrogate: 4-BromoJluoroben_ene 91 70-130 Surrogate: Toluene-& 108 70-130 Matrix Spike (B6[0415-MS1) Source: 6090335-01 1, 1, 1 -Trichloroethane 25.2 0.5 ug/L 20.0 ND 126 70-130 1,1-Dichloroethane 23.7 0.5 ug/L 20.0 ND 119 70-130 I,I-Dichloroethene 24.6 0.5 ug/L 20.0 ND 123 70-130 1,2,4-Trimethylbenzene 22.6 0.5 ug/L 20.0 ND 113 70-130 1,2-Dichloroethane 23.6 0.5 ug/L 20.0 ND 118 70-130 Acetone 112 20.0 ug/L 100 ND 112 60-140 Benzene 21.4 0.5 ug/L 20.0 ND 107 70-130 Bromomethane (Methyl Bromide) 17.4 1.0 ug/L 20.0 ND 87 60-140 PO Box 5655 i Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom an emolovee owned company 09 141016 09:01 This report mqv not be reproduced, except in fid/, without written permission from Rogers & C'allcott. Inc. Page 6 of 1 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B6I0415 - EPA 5030 Matrix Spike (B6I0415-MSl) Source: 6090335-01 Chloroform 20.4 cis-1,2-Dichloroethene 24.6 Ethylbenzene 22.2 Hexane 24.3 Isopropylbenzene 22.3 m,p-Xylene 47.9 Methylene chloride 19.0 Naphthalene 18.8 n-Butylbenzene 22.0 n-Propylbenzene 21.6 o-Xylene 21.2 sec-Butylbenzene 24.9 Styrene 22.5 tert-Butylbenzene 21.6 Tetrachloroethene 21.7 Toluene 21.8 0ans-1,2-Dichloroethene 24.7 Trichloroethene 24.1 Vinyl chloride 19.0 Surrogate: 1.2-Dichloroethane-D4 Surrogate: 4-Bromojluoroben_ene Surrogate: Toluene-& Matrix Spike Dup (B610415-MSDI) Source: 6090335-01 0.5 ug/L 20.0 ND 102 70-130 0.5 ug/L 20.0 ND 121 70-130 0.5 ug/L 20.0 ND Ill 70-130 1.0 ug/L 20.0 ND 122 70-130 0.5 ug/L 20.0 ND 112 70-130 1.0 ug/L 40.0 ND 120 70-130 2.0 ug/L 20.0 ND 95 70-130 2.0 ug/L 20.0 ND 93 70-130 1.0 ug/L 20.0 ND 110 70-130 0.5 ug/L 20.0 ND 108 70-130 0.5 ug/L 20.0 ND 106 70-130 0.5 ug/L 20.0 ND 125 70-130 0.5 ug/L 20.0 ND 112 70-130 0.5 ug/L 20.0 ND 109 70-130 0.5 ug/L 20.0 ND 108 70-130 0.5 ug/L 20.0 ND 109 70-130 0.5 ug/L 20.0 ND 124 70-130 0.5 ug/L 20.0 ND 119 70-130 0.5 ug/L 20.0 ND 95 60-I40 Hi 70-130 98 70-130 114 70-130 1,1,l-Trichloroethane 20.6 0.5 ug/I, 20.0 ND 103 70-130 20 20 1,1-Dichloroethane 20.4 0.5 ug/L 20.0 ND 102 70-130 15 20 I,1-Dichloroethene 19.9 0.5 ug/L 20.0 ND I00 70-130 21 20 P2 1,2,4-Trimethylbenzene 19.6 0.5 ug/L 20.0 ND 98 70-130 14 20 1,2-Dichloroethane 22.7 0.5 ug/L 20.0 ND 114 70-130 4 20 Acetone 117 20.0 ug/L 100 ND 117 60-140 5 20 Benzene 18.1 0.5 ug/L 20.0 ND 90 70-130 17 20 Bromomethane (Methyl Bromide) 15.0 LO ug/L 20.0 ND 75 60-140 15 20 Chloroform 17.9 0.5 ug/L 20.0 ND 90 70-130 13 20 cis-1,2-Dichloroethene 22.2 0.5 ug/L 20.0 ND 110 70-130 10 20 Ethylbenzene 18.6 0.5 ug/L 20.0 ND 93 70-130 18 20 Hexane 18.5 1.0 ug/L 20.0 ND 93 70-130 27 20 P2 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 ! fax 864.232.6140 rogersandealleott.eom an emp'o`iee owned :`ornpany 09 14 2016 09:02 This report muv not be reproduced, except in full, without written permission from Rogers & C'aBeott, Inc. Page 7 Of 1 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Volatile Organics Quality Control Summary Reporting Spike Source % REC RPD Parameter Result Limit t nits Level Result % REC Limits RPD Limit Flags Batch B610.115 - EPA 5030 Matrix Spike Dup (B610415-NISD1) Source: 6090335-01 Isopropylbenzene 18.7 0.5 ug/L 20.0 ND 94 70-130 18 20 m,p-Xylene 40.8 1.0 ug/L 40.0 ND 102 70-130 16 20 Methylene chloride 17.1 2.0 ug/L 20.0 ND 86 70-130 10 20 Naphthalene 18.3 2.0 ug/L 20.0 ND 90 70-130 3 20 n-Butylbenzene 17.6 LO ug/L 20.0 ND 88 70-130 22 20 P2 n-Propylbenzene 18.0 0.5 ug/L 20.0 ND 90 70-130 18 20 o-Xylene 18.1 0.5 ug/L 20.0 ND 90 70-130 16 20 sec-Butylbenzene 20.8 0.5 ug/L 20.0 ND 104 70-130 18 20 Styrene 20.4 0.5 ug/L 20.0 ND 102 70-130 10 20 tert-Butylbenzene 18.2 0.5 ug/L 20.0 ND 91 70-130 17 20 Tetrachloroethene 17.4 0.5 ug/L 20.0 ND 87 70-130 22 20 P2 Toluene 18.5 0.5 ug/L 20.0 ND 92 70-130 16 20 trans-1,2-Dichloroethene 20.5 0.5 ug/L 20.0 ND 102 70-130 19 20 Trichloroethene 20.0 0.5 ug/L 20.0 ND 99 70-130 19 20 Vinyl chloride 14.2 0.5 ug/L 20.0 ND 71 60-140 29 20 P2 Surrogate: 1.2-Dichloroethane-D4 110 -0-130 Surrogate: a-Bromofluorohen_ene 88 70-130 Surrogate: Toluene-d8 100 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.2316140 rogersandealleott.eom an employee -owned company 09 14 2016 09:02 This report mnv not be reproduced, except in full, without written permission from Rogers & Callcott Inc. Page 8 of 11 Rogers & Callcott - ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 6090336 Monroe, NC 28110 Reported: 09/14/16 09:02 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference P2 The RPD between the matrix spike / spike duplicate exceeded the control limits; however, both spike recoveries were within control limits. PO Box 5655 1 Greenville. SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax 864.232.6140 09 14 2016 09: 02 This report mqv not he reproduced except in full, H ithout written penni lion from Rogers & Callcott. Inc. rogersandcal Icott.com an employee -owned company Page 9 of 19 Rogers &Callcott CHAIN OF CUb I UUY KELM) WORK ORDER ENVIRONMENTAL N Filte . d yes/No) Cooled (yes/No) y Mailing Po Box 5655 Shipping 426 Fairforest Way 2158 Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 6 Container Type (plastic/glass) Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Catalent 40 Container Volume (ml-) Sample Type (grab&omposite) Client Name Address Monroe, N(' OW Sample Source (WW, GW, DW, SW, S, Other) 4) Report To: .G M 41 C 0 Preservation Code(s) U A — None E — HCI I — Zn Acetate Email Address 0 B — HNO3 F — Na5201 J — H3PO4 Telephone # Z, X a) S C — H2SO4 G -- Boric Acid K - MCAA E .6.1 a) " D — NaOH H — Ascorbic Acid L - PO # Project # 93-121 D Z 1 E R&C YR WORK ORDER DATE TIME SAMPLE DESCRIPTION M i7- COMMENTS -------- ----------- *3 vials unpres, I HC1 Lf Effluent 0 PH - Collected on lle Temp - 'C by SA MP�Ef7,," *Qljl�*ED BY: DATEMM, L RECEI�q[) BY: 2. DATE/TIME: Composite Start Date: RELINQUISHED BY: T E /T DATEJ21� --Y. -��CFIAD DATEJTIME: Composite Start Time: 1 4. Time or Flow (Circle one) Initials: RE(INQUISHED BY: DATE/TIME: RECEIVED BY: DATUTIME: 5. 6. Temperature of blank or representative sample At time of collection C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7_ 8. At time f b it ------- C me olab receipt. 1--- Possible Hazards associated wth samples: FlNon-Hazard [7]Flammable EDSIdn Dther irritant Poison FlUnknown EIL — ------------- — Form Revised July, 2014 e 10 of 11 Page —, RogersCallcott ENVIRONMENTAL Sample Receipt Verification. Date Work Client: Ch-TftLg1\,J'r Received: G[. . ((p Order: f Q U 3 (a Carrier Name: Client FedEx UPS US Mail Courier Field Servi Other: Tracking Number. Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date I time on COC agree with label on bottie(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? ' VOA vials free of headspace (<6mm bubble)? Samples cooled? Temp at receipt recorded on COC Temp measured with IR thermometer - SN: 97050067 X[ / \ Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. i� C Ch Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? �/ X .� If in-house preservation used — record Lot # HCL H3PO4 HZSO4 NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or � No Non -Conformance issue other than noted above: Revised July 2014 Completed by: A U Paae 11 of 11 NON -HAZARDOUS 1. Generator ID Number 2. Paget of 3. Emergency Response Phone 4. Waste Tracking Numbe / �6''`` WASTE MANIFEST � 5. Generator's Name and Mailing Address Generators Site Address (H different than mailing a Cataterd Pharrrta 2021 East Roosevelt Bird Monroe, NC 28112 Generators Phone: 6. Transporter 1 C U.S. EPA ID Number r 7. Transporter 2 Company Name U.S. EPA ID Number 8. Designated Facility Name and Site Address U.S. EPA ID Number A&D Environmental Serdices y,C il f 2713 llwhaMe Road Archdale, NC 27263 USA Facilil 's Phone: 10. Containers 11. Total 12. Unit 9. Waste Shipping Name and Description Quantity WtJVol. No. Type _ 1 Non -Hazardous Materials N.O.S. (Process Wastewater wnn 01 TT ^y O ao� Iron/Manganese Scale) a J W z W 2 0 3. 4. 113. Special Handling Instructions and Additional Information A&D Proflle# 14. GENERATOR'SIOFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are filly and accurately described above by the proper shipping name, and are classified, packaged, marked and labeled/placarded, and are in all respects in proper condition for transport according to applicable international and national governmental regulations. GeneratoeslOfferoes Printe liTyped Name Signal r Month Day Year �C��avvtrH L, 1&� etL*r ;.,�.... - 15. Internatill56al Shipments ❑ Import to U.S. ❑ Export from U.S. Port of entry/exit: Transporter Signature for exports only): Date leaving U.S.: CC16. Transporter Acknowledgment of Receipt of Materials WTransporter 1 dritedlTyped NNaa�e Signature Month Day Year N✓' h a Transporter 2 Printedrryped Name Signature Month Day Year 17. Discrepancy tla. Discrepancy Indication Space ❑ Quantity ❑ Type ❑ Residue ❑ Partial Rejection ❑ Full Rejection Manifest Reference Number: 17b, Alternate Facility (or Generator) U.S. EPA ID Number J U u`l Facility's Phone: 17c. Signature of Alternate Facility (or Generator) Month Day Year Z 183 Desgnated Facility Owner or Operator. Certification of receipt of materials covered by the manifest except as noted in Item 17a PrintadR Signature Month aye Y 169-BLC-0 5 11977 (Rev. 9/09) DESIGNATED FACILITY TO GENERATOR ® A&D Environmental Services Bill of Lading / Material Manifest A&D Job No: 7 (, 2 Generator ID Number Page 1 of 1 Emergency Response Phone 25&3924-MIS0007961 Tracking Number 26154 Generator's Name and Mailing Address Generator's site address (if different from mailing address) Cahierlt Phomta Solutions 2021 East Roosevelt BNd Monroe, INC 28112 USA 884-414.0862 Transporter 1020 Company Name A&D Environmental Services, Inc. US EPA ID No: NCD986232221 Transporter 1 li 12❑ Company Name A&D Environmental Services (SC), LLC US EPA ID No: SCD987598331 Designated Facility A&D Environmental Services, Inc. 2718 Uwharrie Road Archdale, NC 27263 336-434-7750 NCD986232221 Designated Facility A&D Environmental Services, Inc. 3149 Lear Drive Burlington, NC 27215 336-229-0058 NCR000138628 Designated Facility A&D Environmental Services (SC), LLC 1741 Calks Ferry Road Lexington, SC 29073 803-957-9175 SCD987598331 Designated Facility A&D Environmental Services (SC), LLC 1321 White Horse Road, Suite C Greenville, SC 29605 864-234-6055 HM Hazardous Materials Shipping Name and Description (if applicable) No. Type CITY Wt/Vol Profile Number Non -Regulated Material (Iron & Manganese Scale) DM 0 P ao/5'D,S-0s Petroleum Products for Recycle No. Type QTY Wt/Vol Profile Number X NA1993, Diesel fuel, 3, III ERG# 128 X NA1993, Fuel oil (No.1,2,4,5 or 6), 3, III ERG# 128 X UN1203, Gasoline, 3, II ERG# 128 USED OIL (Not a USDOT Hazardous Material) Petroleum Contact Water (Not a USDOT Hazardous Material) Universal Waste Lamps, Batteries, Ballasts, and Electronics for Recycle HM No. Type Est. Wt. Count Shipping Name and Description (if applicable) Common Name Discrepancy X RQ, UN2809, Mercury contained in manufactured articles, 8, III ERG# 172 Mercury Containing Articles X RQ, UN3432, Polychlorinated biphenyls, solid, 9, 11 ERG# 171 TSCA Exempt PCB Lamp Ballasts X UN2800, Batteries, wet, nonspillable, 8, III ERG# 154 Sealed Lead Acid Batteries X UN2794, Batteries, wet, filled with acid, 8, III ERG# 154 Lead Acid Batteries X UN2795, Batteries, wet, filled with alkali, 8, 111 ERG# 154 Wet NiCad Batteries X UN3090, Lithium batteries, 9, II ERG# 138 Lithium Batteries X UN3028, Batteries, dry, containing potassium hydroxide solid, 8, 111 ERG# 154 Alkaline Batteries X UN3028, Batteries, dry, containing potassium hydroxide solid, 8, 111 ERG# 154 NiCad Batteries Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) Fluorescent lamps 4' or < Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) Fluorescent lamps 4' Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) Circular/U-tube lamps Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) Compact Lamps Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) Shattershleld Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) HID/MV/UV Lamps Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e) Incandescent lamps Non -PCB Light Ballasts for Recycle (Not DOT -Regulated) Non -PCB Light Ballasts Electronic Equipment for Recycle (Not DOT -Regulated) Electronics Generator's Certification: This is to certify that the above -named materials are properly classified, described, packaged, marked, and labeled, and are In proper condition for transportation according to the applicable regulations of the Department of Transportation. I further certify that none of the materials described above are a hazardous waste as defined by EPA 40CFR Part 261 or any applicable state law, and unless specifically identified above the materials contain less than 1,000 ppm total halogens and do not contain quantifia levels (2ppm) of PCBs as defined by EPA 40 CFR Parts 279 and 761. Generator's/Offeror's Printed/Typed Name Signature Month Day Year Transporter 1 Printed/Typed Name Signatur4 Month Day Year Transporter 2 Printed/XW Name Signature Month Day Year Discrepancy Indication /Additional Information: Designated Facility Certification: I hereby acknowledge receipt of the materials covered by this manifest except for any discrepancy indicated above. Printed/Typed Name Signature Month Day Year DESIGNATED FACILITY TO GENERATOR Catalent. �, July 10, 2015 Catalent Pharma Solutions 2725 Scherer Drive North St Petersburg, FL 33716 T 727.803.2100 F 727.803.2419 www.catalent.com Mr. Kyle Ketchum City of Monroe WWTP 775 Treeway Drive Monroe, North Carolina 28110 Subject: Effluent Discharge Report — LIUP # LP-001 Treated Groun water Catalent Pharma Solutions (Formerly R. P. Scherer)/Chelsea Laboratories Facility 2021 East Roosevelt Blvd., Monroe, North Carolina 28112 Dear Mr. Ketchum: Enclosed are the June 2015 effluent discharge and laboratory analysis reports for the referenced facility. No non -conformances were reported. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted Is, to the best of my knowledge and belief, true, accurate and complete. I am aware there are significant penalties for submitting false information, including the possibility of fine or imprisonment for knowing violations. If you have any questions or concerns, please contact Jeffery Rogers at 727-803-2282 (email: Jeffery. Rogers@catalent.com) or Stan Golaski of Rogers & Callcott at 864-335-4984 (email: stan.golaski@rogersandcallcott.com). Sincerely, atatent Pharma Solutions Dina Kostakis General Manager Enclosures Date 0-fs cc with attachments: Stan Golaski, Rogers & Callcott Environmental Jerry Sullivan, Aqua -Trot (on -site file) Receiving POTW NPDES #: NCO024333 Effective Date for these Limits: 7/1/13 Expiration Date for these Limits: 6/30/16 LILIP #: LP-001 Pipe #: 01 Reporting Period: June 2015 Date i� Time of Reading Days Between Readings Meter Reading (gal) Weekly Flow (gal) 1 Weekly Average (mgpd)2 Tetrachloro- ethene (ug/L) Trichloro- ethene (ug/L) 82603 (ug/L) pH (units) Comments 5/27/15 7:30 1,077,412 6/2/15 7:30 6.00 1,113,780 36,368 0.006061 0.6 0.6 1.2 8.2 6/9/15 19:30 7.50 1,157,945 44,165 0.005889 6/11/1510:30 1.63 1.164,866 6,921 0.004259 6/16/15 7:00 4.85 1,174,645 9,779 0.002015 Sample and pH 6/23/15 7:30 7.02 1.211,973 37,328 0.005317 collected on 6/30/15 7:30 7.00 1,253,191 41,218 0.005888 June 11, 2015. Monthly Total 175,779 Maximum 0.006061 Minimum 0.002015 Sample Type Grab Grab Grab Grab Permit Limits 0.010000 8.85 81 monitor only 6 to 11 Flow between Meter Readings 2 Weekly Average = Weekly Flow / Days Between Readings 3 Value represents total 8260 volatile organic compounds. BRDL= Below Reportable Detection Limits 11RC-VMSRV031Proie=%14193121\2015\RPTS\POTW ReportsUune 20151 Juno 2015 POTN FormAu 7/10/2015 Rogers & Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf- Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Laboratory Services Effluent 5060491 06111/2015 14:51 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on June 11. 2015. Rogers and Callcott maintains n formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. 77ie analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Jason Swinger, your Project Manager, at jason.sivanger a.rogersandcallcottcom or (864)-335-4997 ifyou have any questions about this report. Permit #WQ0010607 Catalent Pharma Solutions'Chelsen Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: 0 Jason Swanger Project Manager PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 sniln 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom an employee -owned company 77iis report nug- not be reproducers except in full, n Ithout irritten permission jrvm Rogerx R t'allcott, bic. rf age 1 of 6 Rogers &Callcott �1 t+[� ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions CIO George hirwour- Rogers and Callcott 2021 E- Roosevelt Blvd. Monroe, NIC 28110 Sample Number Sample Nscription 50M491-01 Effluent Grab South Carolina Greenville Laborvloty klentlftcation 2310S South Carolina ColumblaLaboratoty Menlification 40572 North Carolitut Laboratory Certification Number 27 North C'arolitur Drinking Meter fifth Number 4.1710 NGLAP Utah Cerltficule Arumber SC000042014-1 Georgitt Drinking Metter Lob JD 830 Project: Effluent Work Order: 5060491 Received: 06/11/2015 14:51 Matrix Samplcd 'Type Ground Rater 06l11115 11:20 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 nuin 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com ---------- an employee owned company 07,90 2015 0339 Thir report nury, not be reprothice,( except in full, without written parodrsion from Rogers R Collcotl, Du. Page 2 of 6 -"�! Rogers &Callcott 1_ _tt!�jj ENVIRONMENTAL Calalent Pharma Solutions Project: Effluent 202I L. Roosevelt Blvd. Work Order: 5060491 Monroe, NC 28110 Reported: 07/10/15 08:19 Sample Data Sample Number 5060491-01 Sample Description Effluent Grab collected on 0&11115 11:20 Parameter Result Reporting Limit Units DF Anal) -Zed Method Flag Analyst Batch Field Parameters pH 8.2 0.1 PH Units 1.00 06/11/15 11:20 EPA904DC RIF 1351`0448 Temperature 25.1 0.0 °C 1.00 06/11/15 11:20 SM255OB-2010 Rip B51`0448 Volatile Organics 1,41-Trichioroethane ND LO ug/L 1.00 06/17/15 18:58 EPA 6260E ARM B5GO240 41-Dichloroethane ND 1.0 ug/L 1.00 06/17/15 18:58 EPA 9260B ARM B5G0240 1,1-Dichloroethene ND 0.5 ug/L 1.00 06/17/15 18:58 EPA 8260B 112 ARM B5G0240 1,2,4-Trimethylbenzene ND 0.5 us/L 1.00 06/17/15 18:58 EPA 8260B ARM B5GO240 1,2-Dichloroethane ND 0.5 ug/L 1.00 06/17/15 18:58 EPA 9260B % ARM 135GO240 Acetone ND 20.0 ue/L 1.00 06!17/15 18:58 EPA 8260B ARM 135G0240 Benzene ND 0.5 u9/1. 1.00 06/17/15 18:58 EPA 9260B ARM 13500240 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 06/17/15 18:58 EPA 9260B ARM 135GO240 Chloroform ND 1.0 ug/L 1.00 06/17/15 18:58 EPA 8260B ARM BSG0240 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 06/17/15 18:58 EPA 8260B ARM B5G0240 Ethylbenzene ND 1.0 ug/L t.00 06/17/15 18:58 EPA 9260B ARM BSG0240 Hexane ND LO ug/L 1.00 06/17/15 18:58 EPA 9260B P, S ARM B5GO240 ni,p-Xylene ND 1.0 ug/L 1.00 06/17/15 18:58 EPA 8260B ARM B5GO240 Methylene chloride ND 2.0 ug/L LOO 06/17/13 18:58 EPA 8260B ARM BSG0240 Naphthalene ND 2.0 ug/L 1.00 007/15 18:58 EPA 8260B ARM B5GO240 n-Butylbenzene ND 2.0 ug/L 1.00 06/17/15 18:58 EPA 826013 P2 ARM H5GO240 n-Propylbenzene ND 0.5 ug/L L00 06/17/15 18:58 EPA 8260B ARM B5GO240 o \ylene ND 1.0 ug/L L00 06/17/15 18:58 EPA 8260B ARM B5GO240 sec-Butylbenzene ND 0.5 u8n• 1.00 0617/15 18:58 EPA 8260B P2 ARM 135G0240 Styrene ND 1.0 ug/L 1.00 06/17/15 18:58 EPA 8260E ARM 135GO240 ten-Butylbenzene ND 0.5 u8/1• 1.00 06/17/15 18:58 EPA 8260E ARM 135G0240 Tetrachloroethene 0.6 0.5 ug/L 1.00 06/17/15 18:58 EPA 8260B P2 ARM B5G0240 Toluene ND 0.5 ugtl. IkO 06/17/15 18:58 EPA 8260E ARM 135GO240 trans-1,2-Dichloroelhene ND 0.5 us/L 1.00 06/17/15 18:58 EPA 8260B ARM B5GO240 Trichloroethene 0.6 0.5 u9/11 1.00 06!17/15 18:58 EPA 8260B ARM B5GO240 Vinyl chloride ND 0.5 ug/L 1.00 06117/15 18:58 EPA 8260B P2, Za ARM B5GO240 Surrogates %REC %REC Limits Flag 1,2-Dieh1oroe1"&,-D1 90 70-130 4-Bromofhtorohemew 92 70-130 Toluen.,43 91 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 ` mrin 864.232.1556 1 fax 864.232.6140 rogersandeallcomcom __ a ,�.._,_ _ _ ._ _ _ _.___ �_ .__ _-._ _ anemployee•avnedcompany 0T10 2015 OS:19 Ihir report nut not be reproduced, except hifull, it dow uviuon permission from Rogers & C'ollcou, Ire. Page 3 of 6 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work- Order: 5060491 Monroe, NC 28110 Reported: 07/10/15 08:19 Data Qualifiers and Definitions ND Analyte NOT DFI'FCTED at or above the reporting limit NR Not reported P The RPD between the sample / duplicate or matrix spike / spike duplicate e.ts not within control limits P2 The RPD between the matrix spike / spike duplicate exceeded the control limits; however, both spike recoveries were within control limits. S The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits. The Laboratory Control Sample (LCS) was within control limits. Z h4DL is 0.05; No peak detected. Za hiDL is 0.06; No peak detected. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom -------- -- - an employee-ovvnedcompany 0"0 2015 0s:19 17w report may not be reproduces{ except to full, without u•niten permtsslon front Rogers R Calicott In Page 4 of 6 T Rogers & Callcott CHAIN ENVIRONMENTAL vlalling PO Box 5655 Shipping 426 Falrforest Way 215B Stoneridge Drive %ddress: Greenville, SC29606 Address: Greenville,SC29W7 Columbia, SC29210 Phone (864) 232-SS56 Fax (864) 232-6140 Phone (803) S09-8999 Pent Name ��d. � L Address Report To: Email Address Telephone# PO # Project # 93'� Z- ( OF WU > I UUY Kt(-UKU WORK ORDER d a`> =3 Z N yv -"- ° c, N F a if Filtered (Yes/No) Cooled (Yes/No) Container Type (Plastic/Glass) Container Volume (rnL) Sample Type Lrab/Compcsite) Sample Source (WW, CW, DW, SW, S, Other) Preservation Codes) A -None E-HCI I - ZnAcetate B-HNO3 F-Na3S203 J-H3POa C-H2S0. G - Boric Acid K -MCAA D -NaOH H-Ascorbic Add L- R&C WORK ORDER yR�s DATE nmE I SAMPLE DESCRIPTION COMMENTS B,Z1 C��la CJ(ZU o/) I i SAMPL UISHED BY: S ATE/TIME: 7RECEIVEDB D E/�YIME I ( Composite Start Date: Start Time: Time or Flow (Circle one) Initials: RELIN UISHED BY: 3, DATE/TIME: DATE/TIME:Composite RELINQUISHED BY: S. DATE/71ME: RECEIVED BY:— 6. DATEJTIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt D °C RELINQUISHED BY: 7. DATEITIME: RECEIVED BY: S. DAT E/rIME: Possible Hazards associated with samples: 1-�71 Non -Hazard orl3rnrn3ble "Skin Irritant U Poison "Unknown L"Dther Form Revised July, 2014 Page f of i Rogers &Cattcott ENVIRONMENTAL OSample Receipt Verification P �Date IIj<Work Client: Received: Order: Carrier Name: Client FedEx Tracking Number: UPS US Mail Courier Field Service � n Receipt Criteria Y e s N o N A Comments Shipping container/ cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Samples cooled? Temp at receipt recorded on COC Temp measured with IR themrometcr - SN: 970SM67 F ce Col Pac Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be prescr ed upon receipt in the lab Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot N HCL H3POa H2SO4 NaOH HNO, Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: I — Revised July 2014 Completed by;, Page 6 of 6 Rogers and Callcott Environmental Client: Date: J► lS Field Meter Calibration Record Conductivity Calibration - EPA 9050A Meter Make/Model: Orion StarA325 SN: 6 0 706 Probe: Time: C Analyst: Cell Constant Chemi Conc. of Standard, µmhos/cm @25°C Actual Reading of Standard, µmhos/cm @ Temperature,'C SSS conc: Temperature compensation for pH / conductivity meter : pH Calibration -EPA 9040C Meter Make /Model: Orion Star A325 Probe: Z SC�S Time: 0,939 Analyst: ( Slope: 91e, L/ Chemical Inventory Conc. of Buffer, units Actual Reading of Buffer, units PSoly V? 4.0 3,9 5 015,61 7.0 . 7 P.SGI'-g 10.0 )0'o 5 02-2]Z- SSS conc. 7 v 3 -9 Turbidity Meter Calibration Field Screen Method Meter Make / Model: Hach 2100P SN: Time: Analyst: Date of most recent calibration: Chemical Inventory Assigned Conc. of Standard, NTU Actual Reading of Standard, NTU Reviewed by: Date: Revised 01/21/13 Rogers and Callcott Environmental Continuing Calibration Verification Meter Make / Model: Orion Star A325 Client: L-"ni-. /" Conductivity Meter EPA 9050A SN: & o Z% 0 6 Probe: Date: Time Analyst Conc. of Standard, µmhos/cm @25'C Actual Reading of Standard, µmhos/cm T @ •c •C Meter Make / Model: Orion Star A325 pm mewl 'PA 90401 Probe: Syl^ ! 2,5 a-S Time Analyst Conc. of Buffer, units Actual Reading of Buffer, units 1179 , G, Meter Make / Model: Hach 2100P Turbidity Meter Field Screen Method d'al Analyst —77 Assigned Conc. of Standard, NTU I Actual Reading of Standard, NTU Field Duplicate Well ID:S�- Time Analyst Conductivity, µmhos/cm pH, units Turbidity, NTU Temperature, •C A- $. o >k Note: Refer to daily calibration log for Instrument calibration and chemical Inventory information / documentation. Revised 01/21/13 Reviewed by: Date: 7 Rogers & Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Laboratory Services P92 Im14:51 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on June 11, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Tiffany Kay, your Project Manager, at tiffany.kay@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit 11WQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Tiffany Kay Project Manager PO Box 5655 : Greenville, SC 29606 ! 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 I-0ger-Sandeal1cott.COm ---- an employee -owned company This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 1 of 7 r Rogers & Callcott g e� ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5060492-01 Influent Grab South Carolina Greenville Laboratoty Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratoty Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Influent Work Order: 5060492 Received: 06/ 11 /2015 14:51 Matrix Sampled Type Ground Water 06/11/15 11:34 Grab PO Box 5655 1 Greenville, SC 29606 i 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.com an employee -owned company 0710612015 10: 07 This report may not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Page 2 of 7 71 4 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5060492 Monroe, NC 28110 Reported: 07/06/15 10:07 Sample Data Sample Number 5060492-01 Sample Description Influent Grab collected on 06/11/15 11:34 Parameter Result Reporting Limit Units DF Analvzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5F0834 I,1-Dichloroethane 0.8 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5F0834 1,1-Dichloroethene 0.9 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5170834 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW 135170834 1,2-Dichloroethane 0.5 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260E LBW 1351`0834 Acetone ND 20.0 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW 135F0834 Benzene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260E LBW 135F0834 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260E LBW 135F0834 Chloroform 6.9 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW BSF0834 cis-1,2-Dichloroethene 67.2 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5170834 Ethylbenzene ND 1.0 ug/L 1.00 06/18/15 16:20 EPA 8260E LBW B5170834 Hexane ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5170834 Isopropylbenzene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B51`0834 m,p-Xylene ND 1.0 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW 135170834 Methylene chloride ND 2.0 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5F0834 Naphthalene ND 5.0 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW BSF0834 n-Butylbenzene ND 2.0 ug/L 1.00 06/18/15 16:20 EPA 8260E LBW B5F0834 n-Propylbenzene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260E LBW B5170834 o-Xylene ND 1.0 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5F0834 sec-Butylbenzene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5170834 Styrene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5170834 tert-Butylbenzene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW 135170834 Toluene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B5F0834 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW B51`0834 Vinyl chloride ND 0.5 ug/L 1.00 06/18/15 16:20 EPA 8260B LBW 1351`0834 Rebatch Sample Number: 5060492-01RE1 Tetrachloroethene 172 2.5 ug/L 5.00 06/19/15 20:06 EPA 8260B LBW 135170832 Trichloroethene 135 2.5 ug/L 5.00 06/19/15 20:06 EPA 8260B LBW B5F0832 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 76 70-130 4-BromoJluorobenzene 95 70-130 Toluene-d8 83 70-130 Rebatch Sample Number: 5060492-01RE1 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 ' main 864.232.1556 1 tax 864.232.6140 rogersandcallcott.com -- - an employee owned company 0710612015 10: 07 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 3 of 7 r Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5060492 Monroe, NC 28110 Reported: 07/06/15 10:07 Sample Number 5060492-01 Sample Description Influent Grab collected on 06/11/15 11:34 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5060492-OIRE1 1,2-Dichloroethane-D4 77 70-130 4-Bromojluorobenzene 94 70-130 Toluene-d8 87 70-130 PO Box 5655 I Greenville, SC 29606 426 Fairforest Way I Greenville, SC 29607 main 864.232,1556 I fax 864.232.6140 rogersandealleott.com an employee -owned company 0710612015 10: 07 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 4of7 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5060492 Monroe, NC 28110 Reported: 07/06/15 10:07 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported PO Box 5655 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 fax 864.232.6140 rogersandcalleott.eom ----- an employee -owned company 0710612015 10: 07 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 5 of 7 v m n m M 0 0 AiiiiimiRogers & Callcott CHAIN OF CUSTODY RECORD WORK ORDER _ ENV I R O N MENTAL ` — /✓ Filtered (Yes/No) Mailing PO Box 5655 Shipping 426 Fairforest Way 2158 Stoneridge Drive Y Cooled (Yes/No) (�- Container Type (Plastic/glass) Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Container Volume (mL) Client Name Cad, Address (j Sample Type (Grab/Composite) ��✓ Sample Source (WW, GW, DW, SW, S, Other) /t%dtfc�j .A/C. Report To: Email Address c o v o 1& Preservation Code(s) A —None E —HCI I — ZnAcetate B—HNO3 F—Na2S203 J—H3PO4 ) Telephone # p PO # Project # 9j / Z. I ) Z l E a p oo C — — Boric Acid K - MCAA H2SO4 d? D — NaOH H — Ascorbic Acid L - R& c WORK ORDER YR j s DATE TIME SAMPLE DESCRIPTION COMMENTS I'DI 6 /r 12-0 1/ .3 `ilap Co �r'ti L 1 2v o 1 SAMPL — UISHED BY: 1. ATE/TIME: d �/ is / y / ECEIVE 2 Dt?ME (( <' Composite Start Date: Composite Start Time: RELIN UISHED BY: DATE/TIME: RECEIVED B DATE/TIME: 3. 4. Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY:.v DATE/TIME: 5. 6• Temperature of blank or representative sample At time of collection °C RELINQUISHED BY: DATEITIME: RECEIVED BY: DATE/TIME: 7. 8. At time of lab receipt /, D °C Possible Hazards associated with samples: Non -Hazard Flammable "Skin Irritant "Poison ElUnknown ED:)ther Form Revised July, 2014 Page �_ of I j Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Q�� Date Work IIJ! Z Client: V^� Received: I Order: [•� Carrier Name: Client FedEx UPS US Mail Courier Field Services Other: Tracking Number: Receipt Criteria Y e s N o N A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? 01 VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples COOIed? Temp measured with IR thermometer - SN: 97050067 1 e Cold cks Dry Ice None Samples requiring pH preservation at proper pH? Note. Samples for metals analysis may be preserved upon receipt in the lab. 1 I� Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot # HCL H;PO4 HZSO, NaOH HNO, Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: F j Revised July 2014 Completed by: Page 7 of 7 i Catalent. June 8, 2015 Catalent Pharma Solutions 2725 Scherer Drive North St. Petersburg, FL 33716 T 727.803.2100 F 727.803.2419 wimcatalent.com Mr. Kyle Ketchum City of Monroe WWTP 775 Treeway Drive Monroe, North Carolina 28110 Subject: Effluent Discharge Report LIUP # LP-001 Treated Gro n water Catalent Pharma Solutions (Formerly R. P. Scherer)/Chelsea Laboratories Facility 2021 East Roosevelt Blvd., Monroe, North Carolina 28112 Dear Mr. Ketchum: Enclosed are the May 2015 effluent discharge and laboratory analysis reports for the referenced facility. No non -conformances were reported. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware there are significant penalties for submitting false information, including the possibility of fine or imprisonment for knowing violations. If you have any questions or concerns, please contact Jeffery Rogers at 727-803-2282 (email: Jeffery.Rogers@catalent.com) or Stan Golaski of Rogers & Calicott at 864-335-4984 (email: stan.golaski@rogersandcalicott.com). Sincerely, to ent Pharma o cations Dina Kostakis General Manager Enclosures Date cc with attachments: Stan Golaski, Rogers & Callcott Environmental Jerry Sullivan, Aqua -Trot (on -site file) Effluent Discharge Report Local Industrial User Permit (LIUP) Receiving POTW Name: City of Monroe LIU Name: Catalent Pharma Solutions (formerly R.P. Scherer)/Chelsea Receiving POTW NPDES #: NCO024333 LIUP #: LP-001 Effective Date for these Limits: 7/1/13 Pipe #: 01 Expiration Date for these Limits: 6/30/16 Reporting Period: May 2015 Date & Time of Reading Days Between Readings Meter Reading (gal) Weekly Flow (gal)' Weekly Average (mgpd)2 Tetrachloro- ethene (ugL) Trichloro- ethene (ug/L) 82603 (ug/L) pH (units) Comments 4/27/15 10:00 901,792 5/7/15 10:00 10.00 962,713 60,921 0.006092 <0.5 <0.5 BRDL 8.1 5/13/15 12:00 6.08 997,150 34,437 0.005661 1 5/14/15 11:00 0.96 1,002,664 5,514 0.005754 Sample and pH 5/20/15 12:30 6.06 1,038,008 35,344 0.005830 5/27/15 7:30 6.79 1,077,412 39,404 0.005802 collected on May 7,2 015. Monthly Total 175,620 21M, Maximum 0.006092 Minimum ,� . . .... 0.005661 Sample Type Grab Grab Grab Grab Permit Limits 0.010000 8.85 81 monitor only 6to 11 Flow between Meter Readings 2 Weekly Average = Weekly Flow I Days Between Readings 3 Value represents total 8260 volatile organic compounds. SRDL= Below Reportable Detection Limits X\RC-VMSRVC3\ProjectsII4\93-121\20151RP'rSWOTW RGpor%XWy 20151 May 2015 P07W FormAsx 6AMI 5 Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions CIO George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: NVork Order: Received: LoLorotoly Services Effluent 5050321 05/07/2015 17:40 Rogers and Cal lcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on May 07, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNl standard. The analyses met the QAIQC confidence interval for each test method unless otherwise qualified_ Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara hrkach@rogersandcallcott.com or (864)-3354956 ifyou have any questions about this report. Perot #11r00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Ka� dV6 Kara Hrkach Project Manager Has reporl nray nol he reproduee4 excepi Infill, rriiitoul rrrillen permission from Rogers k Collcoa, Lra PO Box 5655 1 Greenville, SC 29606 1 426 Falrforest Way I Greenville, SC 29607 1 nuin 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee owned company Page 1 of 11 z t ' ` Rogers & Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George hlaalouf- Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe., NC 28110 Sample Number Sample Description 5050321-01 Effluent Grab Sbmnh Caralitra Greenville Laboratory ldentifteation 23105 South Carolina Columbia Laborator, kleniif cation 40571 Korth Carolina Laborenory Certification Number 27 north Carolina Drinking Dater hob Number 43710 NGLAP Utah CertificateNunberSC00004201d-1 Georgia Drinking Witter Lob ID 880 Project: Effluent Work Order: 5050321 Received: 05/07/2015 17:40 hlatrtc Sampled Type Ground Water 05/07/15 11:35 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott,com an employee -owned company 06.OI12015 13: 43 77ds report may not he reproduced except in fi ll, trldwuf u•ritlen pernnrssion fronm Rogers R CnUcot! be. Page 2 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5050321 Monroe, NC 28110 Reported: 06/01/15 13:43 Sample Data Sample Number 5050321-01 Sample Description Effluent Grab collected on 05/07/15 11:35 Reporting Parameter Result Limit Units DF Anal)zed Method Flag Analyst Batch Field Parameters PH 8.1 0.1 PH Units 1.00 05/07/15 11:35 EPA9040C S1VG B5E0272 Temperature 23.2 0.0 °C 1.00 05/07/15 11:35 SM255OB-2010 SWG B5E0272 Volatile Organics 1,1,1-Trichloroethane ND 1.0 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5E0734 1,1-Diehloroethane ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 9260B LBW B5130734 l,l-Dichloroethene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 9260D LBW B5E0734 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5E0734 1,2-DiclAorocthane ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 8260B Z LBW BSE0734 Acetone ND 20.0 u9/1. 1.00 05/12/15 15:21 EPA 9260B LBW BSF0734 Benzene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5F0734 Brontontelhane (Methyl Bromide) ND 2.0 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5F.0734 Chloroform ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 9260B LBW B5130734 cis-1,2-Dichloroethene ND 0.5 ug/l• 1.00 05/12/15 15:21 EPA 826011 L13W B5130734 Ethylbenzene ND 1.0 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5E0734 Hexane ND 1.0 ugn- 1.00 05/12/15 15:21 EPA 8260B LBW BSE0734 Isopropylbcnzene ND 0.5 U91L 1.00 05/12/15 15:21 EPA 9260B LBW B51-0734 m,}rXyfenc ND 1.0 ug/L LGO 05/12/15 15:21 EPA 8260B LBW B5E0734 Methylene chloride ND 2.0 ug/L 1.00 05/12/15 1521 EPA 8260B LBW B5F0734 Naphihnlcne ND 2.0 ug/L 1.00 05/12/15 15:21 EPA 9260B LBW B5F0734 n-Bulylbettzene ND 2.0 ug/L 1.00 05/12/15 1521 EPA 8260D LBW B5130734 n-Propylbenzene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 8260D LBW B5130734 o-Xylene ND 1.0 ug/L 1.00 05/12/15 15:21 EPA 8260D LBW B5E0734 sec-Butylbenzene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5E0734 Styrene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 826013 LBW B5E0734 tert-Butylbenzene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 9260B LBW B5E0734 Telrachloroethene NO 0.5 ug/L 1.00 05/12/15 13:21 EPA 8260B LBW B5E0734 Toluene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA826013 LBW B5E0734 trans-42-Dichloroethene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 8260B LBW B5E0734 Trichloroethene ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 82608 LBW B5E0734 Vinyl chloride ND 0.5 ug/L 1.00 05/12/15 15:21 EPA 9260B Za LBW B5E0734 Surrogates 9GREC %RECLimils Flag 1,2-D1eh1oroe/hose-D4 83 70-130 4-Bromofluorobenzene 103 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Falrforest Way I Greenville, SC 29607 1 rnain 864.232.1556 1 tax 864.232.6140 rogersandcallcott.com --- - - an employee -owned company 06 012013 13: i3 This report nury not be reproduced except Lt full, 01hout trrilteu permission from Rogers h Cal/col4 Inc Page 3 of t 1 Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Effluent 2021 G. Roosevelt Blvd. Work Order. 5050321 Monroe, NC 28110 Reported: 06/01/15 13:43 Sample Number 5050321-01 Sample Description Effluent Grab collected on 05/07/15 1 L35 Reporting Parameter Result Limit Units DF Analyzed Method Flag Anetyst Batch Volatile Organics surrogates %REC %RECLimlis Flag Tolurne43 91 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Cafrforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcoti .Com anemployee-owned company 0610112015 13:43 77rts report mrry rat be reproduce.{ except Infill. trlllwut a ripen ptmisston from Rogen R Caltcatt, Lk. Page 4 of 19 Rogers &Callcott ENVIRONMENTAL Catalent Phafma Solutions Project: Fi7lucllt 2021 F. Roosevelt Blvd. Work Order: 5050321 Monroe, NC 29110 Reported: 06/01/15 13:43 Volatile O!•gauics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit units Lerei Result %REC Limits RPD limit Rags Batch B5EO734 - EPA 5030 Blank (BSE0734-BLICI) 1,1,1-Trichloruethane 1,1-Dichlofoeth2ne l,l-Dichloroethene 1,2,4-Trimelhyllxnzeoe 1,2-Dichlotoethane Acetone Benzene Brotnome0rane (Methyl Bromide) Chlorofomt cis-1,2-Di chloroethene Ethyibenzene ilexane Isopropylbennane m,p-Xylnte hlethylenechloride Naphthalene n-Butylbenzene n-Propylbcnzenc o-Xylenc sec-Bulylbeozene Styrene tert-Butylbenwne Tetmchlor"thene Toluene trafss-1,2-Dichloroethe ne Trichloroethene Vinylchlori& LCS (135F0734-hSI) NID ND ND ND ND h'D ND NO No TTJ ND ND ND N➢ IdD A'D ND A'D A'D ND ND ND ND ND ND ND ND Surrogole: 1, 2-Dichlorvel)xnx-DI Surrogote: 4-Rromoflrwrobenzene Surrogrve: Tohtene-rl3 1.0 0.5 0.5 0.5 0.5 20.0 0.5 2.0 0.5 0.5 1.0 1.0 0.5 1.0 20 20 20 0.5 1.0 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 ug/L ug/L ug/L ug/L ug/L ugh, ug/L ugli. ug/L ug/l, ugtl, ug/L ug/L ug/L ug/L ug/I. ug/L ug/L ug/L ugtL uSIL ugtL ug/L ug/L ug/L ug/L 82 70-130 101 70-130 92 70-130 1,1,1-Trichlofoethane 17.7 1.0 ug/L 20.0 88 70-130 1,1-Diddoroedtane 18A 0.5 ug/L 20.0 92 70-130 I,1-Dichloroethene 22.5 0.5 ug/L 20.0 112 70-130 1,2,4 Trimethylbenzmc 22.3 0.5 ug/L 20.0 112 70.130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com - - -- --- - --•- - an employee -owned company 06'011201S 13:43 Thisreportmuynorbereproduced, excepthrfull,u•ldxrut;rottenpernvssionfroniRagershCollcon,Ire. Page 5 of 11 ./ Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Bird. York Order: 5050321 Monroe, NC 28110 Reported: 06/01/15 13:43 Volatile Organics Quality Control Sununary Reporting Spike Source %REC lull) Parameter Result Limit 111nin Level Restdt %REC Limits "D Limlt Flags Batch B5E0734 - EPA 5030 LCS (WE0734-13SI) 1,2-Dichloroethane 19.3 0.5 ug/L 20.0 96 70.130 Acetone 106 20.0 ug/L too 106 60-140 Benzene 18.7 0.5 ug/L 20.0 93 70.130 Bromomethane (Methyl Bromide) 21.6 2.0 ng/L 20.0 IN 60-140 Chloroform 18.2 0.5 ug/I, 20.0 91 70.130 cis-1,2-Dichloroethene 222 0.5 ug/L 20.0 111 70.130 rthylbenzene 20.3 1.0 ug/L 20.0 102 70-130 Hexane 21.7 1.0 ug/L 20.0 los 70-130 lsopropylbenzene 21.5 0.5 ug/L 20.0 107 70-130 m,p-Xylene 40.8 1.0 ug/L 40.0 102 70-130 lmfethylene chloride 18.1 2.0 ug/L 20.0 90 70-130 Naphthalene 17.3 2.0 ug/L 20,0 86 70-130 n-But3,ibcnzcnc 20.9 2.0 ug/L 20.0 104 70.130 n-Propylbenzene 22.6 0.5 ug/L 20.0 113 70.130 o-Xylene 20.0 1.0 ug/L 20.0 100 70-130 sec-Butylbenzene 22.9 0.5 ug/L 20.0 114 70.130 Styrene 20.5 0.5 109/1. 20.0 103 70-130 tert-Buydbenune 20.4 0.5 ug/1. 20.0 102 70.130 Tetrachloroethene 19.8 0.5 ug/L 20.0 99 70.130 Toluene 19.6 0.5 ug/L 20.0 98 70.130 trans-1,2-Dichloroethene 20A 0.3 ug/L 20.0 102 70-130 Trichloroethene 19.2 0.5 ugR. 20.0 96 70-130 Vinyl chloride 19.6 0.5 ug/L 20.0 98 60.140 Surrogate. 1.2-Dirbloroedrane Da 93 70.130 Surrogate: d-Bromofluorobenzew, 101 70430 Surrogate:7oluene-d8 99 70-130 Alatric Spike(BSE0734-AISI) Source:5050209-15 0,1-Trichlorocthane 974 50.0 ug/L 1000 54.7 92 70-130 l,l-Dichloroethane 1160 25.0 ug/L 1000 176 99 70.130 1,1-Dichloroethene 1870 25.0 uglL 1000 685 118 70.130 1,2,4Trimethylbenzene 1140 25.0 ug/L 1000 ND 114 70-130 1,2-Dichtoroethane 1040 25.0 ug/L 1000 ND 104 70-130 Acetone 5060 1000 USA- 5000 ND lot 60-140 Benzene 961 25.0 uStL 1000 ND 96 70-130 Dunnomethane (kfelhyl Bromide) 1160 100 ug/L 1000 ND 116 60-140 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main $64.232.1556 1 fax 864.232.6140 rogersandcaUcott.com -- --- - - --- --- --- - - anemployee-owned company 06 0112015 13:43 17ils rzpon nm ynmor be reproduced. except In jrll, . Page 6 of 11 I Rogers & Callcott ENVIRONMENTAL Catelent Phtlrma Solutions Project: Fffluent 2021 E. Roosevelt Blvd. Work Order: 5050321 Monroe, NC 28110 Reported: 06/01/15 I3:43 Volatile Organics Quality Control SlInunary Reporting Spike Source %REC RPD Parameter Result limit Units Level Result %R.EC Limits RPD Limit Flags Batch B5EO734 - EPA 5030 Dlatrix Spike (RSE0734-DISI) Source:5050209-15 Chlorofomr 938 25.0 ug/L 1000 ND 94 70-130 cis-1,2-Dichlorcethene 1140 25.0 ug/L 1000 ND 114 70.130 Etylbenzene 1060 50.0 ug/L 1000 ND 106 70.130 Hexane 996 50.0 ug/L 1000 ND 100 70-130 Isopropylbenzene 1120 25.0 ug/1. 1000 ND 112 70.130 m,p .Yylene 2200 50.0 ug/L 2000 ND 110 70-130 Methylene chloride 938 100 ug/L 1000 ND 88 10.130 Naphthalene 388 100 ug/L 1000 ND 85 70-130 n-Butylbenzene 1080 100 ug/L 1000 ND 108 70-130 n-Propylbenzene 1160 23.0 ug/L 1000 ND 116 70.130 o-\ylene 1060 50.0 ug/L 1000 ND 106 70.130 set-Butylbenzene 1160 25.0 ug/L 1000 ND 116 70-130 Styrene 1070 25.0 ug/L 1000 ND 107 70-130 tert-Butylbenzene 1100 25.0 ug/L 1000 ND 110 70-130 Tetrachloroethene 1030 25.0 ug/L 1000 ND 103 70.130 Toluene 1010 25.0 u2x 1000 ND 101 76.130 trans-1,2-Dichlorothene 1070 25.0 u9n. 1000 ND 107 70-130 Triehloroelhene 1140 25.0 ug/L 1000 134 101 70-130 Vinyl chloride 1090 25.0 ug/L 1000 N'D 109 60-140 Surrogole:l,2-Dichlaroeilmma-DI 10J 70-130 Surrogate: d-Bromofluorobenzene 101 70-130 Surrogole: Taluenz-JS 102 70-130 Matrix Spike Dup (B5E0734-EISDI) Source: 5050209-15 1,1,1-Trichloroethane 942 50.0 ug/L 1000 54.7 89 70-130 3 20 1,1-Dichlorocthanc 1110 25.0 u9/1- 1000 176 94 70-130 5 20 IJ-Dichlorothene 1710 25.0 ug/L 1000 635 102 70-130 9 20 1,2,4-Trimethylbenzene 1120 25.0 ug/1- 1000 ND 112 70-130 2 20 1,2-Dichlorcethane 088 25.0 ug/L 1000 ND 99 70-130 5 20 Acetone 5130 1000 ug/L 5" ND 103 60440 1 20 Benzene 950 25.0 119/1- 1000 ND 95 70-130 I 20 Brotuametrane(htethylBfomide) 1040 100 ug/L low ND 104 60-140 11 20 Chlorofomr 936 25.0 ug/L 1000 ND 94 70-130 02 20 cis-1,2-Dichlorcethene 1100 25.0 ugR, 1000 ND 110 76-130 4 20 Elhylbenzene 1030 50.0 uBQ, I000 ND 103 70-330 3 20 Hexane 940 50.0 ug/L 1000 ND 94 70-130 6 20 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com --- --- ---^- --- anemployee-owned company 06`01/2015 13:43 Th1srapor!nur3rwtbereproduced,ezccpJiu�r71,aitlwuJariuenprrniissfaajromRogersRCnllrall,Irt. Pago 7 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5050321 Monroe, NC 28110 Reported: 06/01/15 13:43 Volatile Organics Quality Control Sunnual-Y Reporting Spike Source %IIEC RED Parameter Result Limit Units Level Result %BEC Limits RPD Limit Flags Batch BSE0734 - EPA 5030 Matrix Spike Dup (WE07344DISDl) Source: 5050209-15 lsopropylbenzene 1070 25.0 ugtl, 10D0 ND 107 70-130 5 20 ns,p-Xylene 2050 50.0 119/1- 2000 ND 102 70.130 7 20 Methylene chloride 930 100 113/1. IODD NTD 87 70-130 0.9 20 Naphthalene 9-49 100 ugtL low ND 91 70-130 7 20 n-Bulylbenunc 1060 100 uA 1000 ND 106 70-130 2 20 n-Propylbenune 1150 25.0 ug/L 1000 ND 115 70-130 0.9 20 o-X)lene 1020 50.0 uA 1000 ND 102 70-130 3 20 5ec-Bu(ylben2ene 1130 25.0 u91L 1000 ND 113 70.130 2 20 Styrene 1020 25.0 ug/i, 1000 ND 102 70-130 5 20 tert-Butylbenzene 1060 25.0 ug/l, 1000 ND 106 70-130 4 20 Tetrachloroethene 969 25.0 ug/L 1000 ND 97 70.130 6 20 Tolurne 992 25.0 ug/L 1000 ND 99 70-130 2 20 trans-1,2-Dichloroethene 1030 23.0 ugtL Iwo ND 103 70-130 4 20 Trichioroelhene 1070 25.0 ugtL 1000 134 94 70-130 6 20 vinyl chloride 992 25.0 uA 1000 ND 99 60.140 9 20 Surrogare: 1, 2Dichloroetrxme-D I Surrogate. 4-Rrotua luorobereew Surrogate: 7oluen a-elS 101 70.130 103 70.130 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.Com --- ------------ - --- --- -- an employee -owned company 06'01 n201S 13:43 7hts report nw), not be reproduce) ttcepr lu full, a flhad uri/pen permission from Rogan X Callcol/, Lk. Page 8 of i 1 `r 56 Rogers & Cakott , .: t.t ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5050321 Monroe, NC 28110 Reported: 06/01/15 13:43 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting lintit NR Not reported RPD Relative Percent Difference Z Nil)). is 0.17 ug/L - No peaks detected 7�a h4DL is 0.18 ug/L - No peaks detected PO Box 5655 1 Greenville, SC 29606 1 426 hirforesc Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com ---- �- - --- -- - ---- — an employee -owned company 06,4112015 13: d3 77ris report nuo rwt be reproduced except hifill, Wtlwut written permission from Rogers R CaUcort, bx•. page 9 Of 11 rm m Rogers &Calcott CHAIN OF CUSTODY RECORD WORK ORDER ENVIRONMENTAL N Filtered Les/No) Y Cooled LYes/No) Mailing POBOX 5655 Shipping 426FafrforestWay 215BStonerldgeDrive G Container Type (PlastiC/Glass) Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 732-1556 Fax (864) 232-6140 Phone (803) 509-8999 40 Container Volume (ml.) Client Name Catalent G Sample Type (Grab/Composite) Address Monroe, NC GW Sample Source (WW, (3W, DW, SW, S, Other) c ReportTo: Preservation Code(s) Email Address U o N u Oj A —None E—HCI I — ZnAcetate B—HNO3 F—NazSzOa J—H3POa Telephone# v $ C—H7.SO4 G—Boric Acid K-MCAA PO # Project # 93-121 Z E D—NaOH H—Ascorbic Add L- c � ft&C YRa WORK ORDER DATE nME SAMPLE DESCRIPTION COMMENTS 1C" s } iG "3 vials unpres, 1 HC1 Effluent pH-J Collected on S ,-W@u Temp - 23.1. by 5, j Su�;o3a1-o SAMPLE tELI QUISHED BY: DATE/TIME: CEIV pql Composite Start Date: Composite Start Time: RELINQUISHED BY: DATE/TI . RECEIVED DATE/TIME: 3 4. Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 5. 6. Temperature of blank or representative sample At time of collection °C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7 8. At time of lab receipt r °C ossible Hazards associated with samples: Non Hazard ❑Flammable Skin Irritant Ofti= Unknown [DOther form Revised July, 2014 Page of 11 t� Rogers & Cattcott 1, t ENVIRONMENTAL Sample Receipt Verification Date Work Client: Cu� �((� L �� Received: Order: �CU3dj Carrier Name: Client Fedit UPS US Mail Courier Meld Service Other: Tracking Number: Receipt Criteria .Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other; Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding lime? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Samples cooled? Temp at receipt recorded on COC p Tcmp measured with IR thermometer - SN: 9705OD67 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for melals analysis may be preserved upon receipt in the lab. Samples dechlorinated for parameters requiring chloride removal at the time of sample collection? If in-house preservation used — record Lot # HCL H1PO4 H2SO4 NaOH I NOJ Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by:_� V Page l l of t t 11 a Rogers and Callcott Environmental client: Date: Field Meter Calibration Record Conductivity Calibration - EPA 9050A, " Meter Make / Model: Orion Star A325 SN: Probe: Time: Analyst: Cell Const - Chemical Inventory Conc of Standard µmh °C Actual Reading of Standard, mhos/cm @ Temperature, °C SSS cone Temper, compensation for pH / conductivity meter: pH Calibration = i:PA 9040C Meter Make / Model: Orion Star A325 Probe: 1 Time: 06,-z Analyst Slope: Chemical Inventory Conc. of Buffer, units Actual Reading of Buffer, units 4.0 3. 7.0 S F31i 10.0 2 !a Olo� SSS Conc: Turbidity Meter. Calibration Field Screen Method. Meter Make / Model: Hach 2100P SN: Date of most recent calibration: Time: Analyst: Chemical Inventory Assigned Conc. of Standard, ing of Standard, - NTU NTU Reviewed by Date- Revised 01/21/13 I Rogers and Callcott Environmental Client: �,.,��-'' Date: Continuing Calibration Verification ,. •'CanductivityMetei • ••EPA9050A,. Meter Make/Model: Orion StarA325 SN: Probe: Time Analyst Conic Actual Reading of Standard, µmhos/cm @25'C µmhos/cm @ 'C °C pH Meter EPA 9040C: Meter Make/Model: Orion StarA325 Probe: �1iy� ,f7r/ Time Analyst Conc, of Buffer, units Actual Reading of Buffer, units tI : Vd '� C6.0 ld, O Z_ .:Turbidity' Meter Field Screen Method Meter Make / Model: Hach 2100P SN: Time An igned Conc. of Standard, NTU Actual Reading of Standard, NTU Field Duplicate. Well ID: Time Analyst Conductivity, pH, µmhos/cm units Note: Refer to daily calibration log for instrument calibration and chemical Inventory information /documentation. Turbidity, Temperature, NTU "C Reviewed by. Dom: Revised 02/21/1.3 Rogers &Callcott ENVIRONMENTAL Laboratory Report Client Catalent Pharma Solutions Project: C/O George Maalouf- Rogers and Callcott Work Order: 2021 E. Roosevelt Blvd. Received: Monroe, NC 28110 Dear Client: vp 10W:40 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on May 07, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com rogersandcallcott.com or (864)-3354956 if you have any questions about this report. Permit #W00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: ) �' &I e, rX&' f Kara Hrkach Project Manager 7his report may not be reproduced, except in full, without written permission from Rogers K Callcon, Inc. PO Box 5655 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalicott.com — an employee -owned company Page 1 of 12 Rogers & Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5050322-01 Influent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Influent Work Order: 5050322 Received: 05 /0 7/2015 17: 40 Matrix Sampled Type Ground Water 05/07/15 11:25 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.colll an employee -owned company 0610112015 13:55 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 2 of 12 P. Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Sample Data Sample Number 5050322-01 Sample Description Influent Grab collected on 05/07/15 11:25 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 1.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 I,1-Dichloroethane 0.8 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 1,1-Dichloroethee 1.1 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 1,2-Dichloroethane 0.7 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 Acetone ND 20.0 u911- 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 Benzene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 Chloroform 8.1 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 cis-1,2-Dichloroethee 74.8 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW 135E0734 Ethylbenzene ND 1.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW 135E0734 Hexane ND 1.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 Isopropylbenzene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 m,p-Xylene ND 1.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW BSE0734 Methylene chloride ND 2.0 u9/1- 1.00 05/13/15 00:28 EPA 8260E LBW B5E0734 Naphthalene ND 2.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 n-Butylbenzene ND 2.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 n-Propylbenzene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 o-Xylene ND 1.0 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 sec-Butylbenzene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 Styrene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 tert-Butylbenzene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5EO734 Toluene ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 trans-1,2-Dichloroethee ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260B LBW B5E0734 Vinyl chloride ND 0.5 ug/L 1.00 05/13/15 00:28 EPA 8260E LBW B5EO734 Rebatch Sample Number: 5050322-OIRE1 Tetrachloroethene 179 2.5 ug/L 5.00 05/14/15 12:13 EPA 8260B LBW B5E0735 Trichloroethene 120 2.5 ug/L 5.00 05/14/15 12:13 EPA 8260B LBW B5EO735 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 81 70-130 4-Bromofluorobenaene 104 70-130 Toluene-& 87 70-130 Rebatch Sample Number: 5050322-OIRE1 1,2-Dichloroethane-D4 79 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 06'01/2015 13:55 This report muv not be reproduced, except in full, without written pennissionfrom Rogers & Callcott, Inc. Page 3 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Sample Number 5050322-OIREI Sample Description Influent Grab collected on 05/07/15 11:25 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5050322-OIRE1 4-BromoJluorobenzene 98 70-130 Toluene -A 87 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom an employee -owned company 0610112015 I3: SS This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 4 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Phatma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5E0734 - EPA 5030 Blank (B5E0734-BLKI) 1, 1, 1 -Trichloroethane ND 1.0 ug/L 1,1-Dichloroethane ND 0.5 ug/L 1,1-Dichloroethee ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 2.0 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethee ND 0.5 ug/L Ethylbenzene ND 1.0 ug/L Hexane ND 1.0 ug/L Isopropylbenzene ND 0.5 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 2.0 ug/L n-Butylbenzene ND 2.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 1.0 ug/L sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate:l,2-Dichloroethane-D4 82 70-130 Surrogate: 4-BromoJluorobenzene 104 70-130 Surrogate: Toluene-& 92 70-130 LCS (B5E0734-BS1) 1, 1, 1 -Trichloroethane 17.7 1.0 ug/L 20.0 88 70-130 l,l-Dichloroethane 18.4 0.5 ug/L 20.0 92 70-130 l,l-Dichloroethene 22.5 0.5 ug/L 20.0 112 70-130 1,2,4-Trimethylbenzene 22.3 0.5 ug/L 20.0 112 70-130 1,2-Dichloroethane 19.3 0.5 ug/L 20.0 96 70-130 Acetone 106 20.0 ug/L 100 106 60-140 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 iax 864.232.6140 rogersandcallcott.com a i employee -owned company 0610112015 13:55 This report may not be reproduced, except in full, without written permission from Rogers & Callcon. Inc. Page 5 of 12 J Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit fla s Batch B5E0734 - EPA 5030 LCS (B5E0734-BS1) Benzene 18.7 0.5 ug/L 20.0 93 70-130 Bromomethane (Methyl Bromide) 21.6 2.0 ug/L 20.0 108 60-140 Chloroform 18.2 0.5 ug/L 20.0 91 70-130 cis-1,2-Dichloroethee 22.2 0.5 ug/L 20.0 111 70-130 Ethylbenzene 20.3 1.0 ug/L 20.0 102 70-130 Hexane 21.7 1.0 ug/L 20.0 108 70-130 Isopropylbenzene 21.5 0.5 ug/L 20.0 107 70-130 m,p-Xylene 40.8 1.0 ug/L 40.0 102 70-130 Methylene chloride 18.1 2.0 ug/L 20.0 90 70-130 Naphthalene 17.3 2.0 ug/L 20.0 86 70-130 n-Butylbenzene 20.9 2.0 ug/L 20.0 104 70-130 n-Propylbenzene 22.6 0.5 ug/L 20.0 113 70-130 o-Xylene 20.0 1.0 ug/L 20.0 100 70-130 sec-Butylbenzene 22.9 0.5 ug/L 20.0 114 70-130 Styrene 20.5 0.5 ug/L 20.0 103 70-130 tert-Butylbenzene 20.4 0.5 ug/L 20.0 102 70-130 Toluene 19.6 0.5 ug/L 20.0 98 70-130 trans-1,2-Dichloroethee 20.4 0.5 ug/L 20.0 102 70-130 Vinyl chloride 19.6 0.5 ug/L 20.0 98 60-140 Surrogate:l,2-Dichloroethane-D4 98 70-130 Surrogate: 4-Bromofluomhenaene 101 70-130 Surrogate: Toluene-& 99 70-130 Matrix Spike (B5E0734-MS1) Source: 5050209-15 1,1,1-Tichloroethane 974 50.0 ug/L 1000 54.7 92 70-130 1,1-Dichloroethane 1160 25.0 ug/L 1000 176 99 70-130 1,1-Dichloroethee 1870 25.0 ug/L 1000 685 118 70-130 1,2,4-Trimethylbenzene 1140 25.0 ug/L 1000 ND 114 70-130 1,2-Dichloroethane 1040 25.0 ug/L 1000 ND 104 70-130 Acetone 5060 1000 ug/L 5000 ND 101 60-140 Benzene 961 25.0 ug/L 1000 ND 96 70-130 Bromomethane (Methyl Bromide) 1160 100 ug/L 1000 ND 116 60-140 Chloroform 938 25.0 ug/L 1000 ND 94 70-130 cis-1,2-Dichloroethee 1140 25.0 ug/L 1000 ND 114 70-130 Ethylbenzene 1060 50.0 ug/L 1000 ND 106 70-130 Hexane 996 50.0 ug/L 1000 ND 100 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com a i employee -owned company 0610112015 13:55 This report may not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. Page 6 of 12 Rogers &Callcott l_ ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5E0734 - EPA 5030 Matrix Spike (B5E0734-MS1) Source: 5050209-15 Isopropylbenzene 1120 25.0 ug/L 1000 ND 112 70-130 m,p-Xylene 2200 50.0 ug/L 2000 ND 110 70-130 Methylene chloride 938 100 ug/L 1000 ND 88 70-130 Naphthalene 888 100 ug/L 1000 ND 85 70-130 a-Butylbenzene 1080 100 ug/L 1000 ND 108 70-130 n-Propylbenzene 1160 25.0 ug/L 1000 ND 116 70-130 o-Xylene 1060 50.0 ug/L 1000 ND 106 70-130 sec-Butylbenzene 1160 25.0 ug/L 1000 ND 116 70-130 Styrene 1070 25.0 ug/L 1000 ND 107 70-130 tert-Butylbenzene 1100 25.0 ug/L 1000 ND 110 70-130 Toluene 1010 25.0 ug/L 1000 ND 101 70-130 trans-1,2-Dichloroethene 1070 25.0 ug/L 1000 ND 107 70-130 Vinyl chloride 1090 25.0 ug/L 1000 ND 109 60-140 Surrogate: 1,2-Diehloroethane-D4 105 70-130 Surrogate: a-BromoJluoroben--ene 101 70-130 Surrogate: Toluene-& 102 70-130 Matrix Spike Dup (B5E0734-MSD1) Source: 5050209-15 1,1,1-Trichloroethane 942 50.0 ug/L 1000 54.7 89 70-130 3 20 1,1-Dichloroethane 1110 25.0 ug/L 1000 176 94 70-130 5 20 1,1-Dichloroethene 1710 25.0 ug/L 1000 685 102 70-130 9 20 1,2,4-Trimethylbenzene 1120 25.0 ug/L 1000 ND 112 70-130 2 20 1,2-Dichloroethane 988 25.0 ug/L 1000 ND 99 70-130 5 20 Acetone 5130 1000 ug/L 5000 ND 103 60-140 1 20 Benzene 950 25.0 ug/L 1000 ND 95 70-130 1 20 Bromomethane (Methyl Bromide) 1040 100 ug/L 1000 ND 104 60-140 11 20 Chloroform 936 25.0 ug/L 1000 ND 94 70-130 0.2 20 cis-1,2-Dichloroethene 1100 25.0 ug/L 1000 ND 110 70-130 4 20 Ethylbenzene 1030 50.0 ug/L 1000 ND 103 70-130 3 20 Hexane 940 50.0 ug/L 1000 ND 94 70-130 6 20 Isopropylbenzene 1070 25.0 ug/L 1000 ND 107 70-130 5 20 m,p-Xylene 2050 50.0 ug/L 2000 ND 102 70-130 7 20 Methylene chloride 930 100 ug/L 1000 ND 87 70-130 0.9 20 Naphthalene 949 100 ug/L 1000 ND 91 70-130 7 20 n-Butylbenzene 1060 100 ug/L 1000 ND 106 70-130 2 20 n-Propylbenzene 1150 25.0 ug/L 1000 ND 115 70-130 Q9 20 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com -- an employee -owned company 061OL12015 13:55 This report may not be reproduced, except m full, without written permission from Rogers & Callcott, Inc. Page 7 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Volatile Organics Quality Control Summary Reporting Spike Source % RE( RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit lla�s Batch B5E0734 - EPA 5030 Matrix Spike Dup (B5E0734-MSDI) Source: 5050209-15 o-Xylene 1020 50.0 ug/L 1000 ND 102 70-130 3 20 sec-Butylbenzene 1130 25.0 ug/L 1000 ND 113 70-130 2 20 Styrene 1020 25.0 ug/L 1000 ND 102 70-130 5 20 tert-Butylbenzene 1060 25.0 ug/L 1000 ND 106 70-130 4 20 Toluene 992 25.0 ug/L 1000 ND 99 70-130 2 20 trans-1,2-Dichloroethene 1030 25.0 ug/L 1000 ND 103 70-130 4 20 Vinyl chloride 992 25.0 ug/L 1000 ND 99 60-140 9 20 Surrogate: 1,1-Dichloroethane-D4 101 70-130 Surrogate. 4-BromoJluoroben_ene 103 70-130 Surrogate: Toluene-& 99 70-130 Batch B5E0735 - EPA 5030 Blank (B5E0735-BLK1) Tetrachloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Surrogate:l.l-Dichloroethane-D4 78 70-130 Surrogate:4-BromoJluoroben_ene 95 70-130 Surrogate: Toluene-d8 87 70-130 LCS (B5E0735-BS1) Tetrachloroethene 20.9 0.5 ug/L 20.0 105 70-130 Trichloroethene 19.4 0.5 ug/L 20.0 97 70-130 Surrogate:l,1-Dichloroethane-Da 99 70-130 Surrogate: a-BromoJluorobenzene 94 70-130 Surrogate: Toluene-d8 100 70-130 Matrix Spike (B5E0735-MS1) Source: 5050466-04 Tetrachloroethene 20.4 0.5 ug/L 20.0 ND 102 70-130 Trichloroethene 19.0 0.5 ug/L 20.0 ND 95 70-130 Surrogate: 1,2-Dichloroethane-D4 98 70-130 Surrogate:4-Bromq/luorobenzene 96 70-130 Surrogate: Toluene-d8 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company 0610112015 13:55 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 8 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5E0735 - EPA 5030 Matrix Spike Dup (B5E0735-MSDI) Source: 5050466-04 Tetrachloroethene 19.8 0.5 ug/L 20.0 ND 99 70-130 3 20 Trichloroethene 18.0 0.5 ug/L 20.0 ND 90 70-130 5 20 Surrogate: 1,1-Dichloroethane-D4 Surrogate: 4-Bromofluorobenzene Surrogate: Toluene -A 93 70-130 96 70-130 97 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0610112015 13:55 This report may not be reproduced, except in full, without written permission from Rogers k Callcott, Inc. Page 9 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5050322 Monroe, NC 28110 Reported: 06/01/15 13:55 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 06 012015 13:55 This report may not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. Page 10 of 12 I v m -' Rogers & Calleott CHAIN OF CUSTODY RECORD WORK ORDER ENVIRONMENTAL N Filtered (Yes/No) v Cooled (Yes/No) Mailing PO Box 5655 Shipping 426 Fair -forest Way 215B Stoneridge Drive G Container Type (Plastic/Glass) Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (903) 509-8999 40 Container Volume (mL) Catalent Client Name G Sample Type (Grab/Composite) Address Monroe, NC Gw Sample Source (WW, GW, DW, SW, S, Other) v c Report To: �� o Preservation Codes)) U A— None E — HCI I — Zn Acetate Email Address o N Oj B—HNO3 F—Na2S203 1—H3PO4 Telephone# v o C—H2SO4 G — Boric Acid K -MCAA PO # Project # 93-121 E Z +� E h D—NaOH H— Ascorbic Acid L- � p � J " R&C WORK ORDER YRa DATE TIME SAMPLE DESCRIPTION COMMENTS S'}'+s *3 vials unpres, 1 HCl /I Zs— l^�F Effluent pH - 8 Collected on �� @(/ S Temp -13. - (by SoSo3a I- o SAMPLEELINQUISHED BY: DATE/TIME: CEIV pq E/ IM �I Composite Start Date: 2 I Composite Start Time: RELINQUISHED BY: DATE/TI RECEIVED DATE/TIME: 3. 4. Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: Temperature of blank or representative sample At time of collection 4 a C 5. 6. RELINQUISHED BY: DATEJTIME: RECEIVED BY: DATE/TIME: 7 g. At time of lab receipt °C ossible Hazards associated with samples: 0Non-Hazard Ellarnmable Skin Irritant 0 Poison ❑Unknown ❑Dther Form Revised July, 2014 Page of Rogers & Callcott +T ENVIRONMENTAL Sample Receipt Verification Date _ Work Client: P((,WT Received: % `� Order: Carrier Name: Client FedEx UPS US Mail Courier Field Service Other: Tracking Number: Receipt Criteria A e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled? Temp measured with IR thermometer - SN: 97050067 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. �l Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? `, [ If in-house preservation used - record Lot # HCL H,PO, H,SO, NaOH HNO, Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by: �-)K I Page 12 of 12 Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Laboratory Services Groundwater 5041044 04/28/2015 16:35 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on April 28, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit #WQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Kara Hrkach Project Manager This report may not he reproduced, except in full, without written permission from Rogers & Callcott, Inc. PO Box 5655 4 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 fix 864.232.6140 rogersandcallcott.com ---- an employee -owned company Pagel of 42 Rogers & Callcott 0 ENVIRONMENTAL South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 Certificate of Analysis North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Client Catalent Pharma Solutions Project: Groundwater C/O George Maalouf- Rogers and Callcott Work Order: 5041044 2021 E. Roosevelt Blvd. Received: 04/28/2015 16:35 Monroe, NC 28110 Sample Number Sample Description Matrix Sampled Type 5041044-01 MW7 Ground Water 04/27/15 13:48 Grab 5041044-02 MW7 Ground Water 04/27/15 14:30 Grab 5041044-03 MW 12 Ground Water 04/27/15 14:44 Grab 5041044-04 MW12 Ground Water 04/27/15 15:25 Grab 5041044-05 MW10 Ground Water 04/27/15 15:38 Grab 5041044-06 MW10 Ground Water 04/27/15 16:14 Grab 5041044-07 MWI1 Ground Water 04/27/15 16:25 Grab 5041044-08 MWII Ground Water 04/27/15 17:11 Grab 5041044-09 MW8 Ground Water 04/27/15 17:47 Grab 5041044-10 MW8 Ground Water 04/27/15 18:19 Grab 5041044-11 MW9 Ground Water 04/28/15 08:13 Grab 5041044-12 MW9 Ground Water 04/28/15 08:44 Grab 5041044-13 MW6 Ground Water 04/28/15 09:03 Grab 5041044-14 MW6 Ground Water 04/28/15 09:32 Grab 5041044-15 MW1 Ground Water 04/28/15 10:00 Grab 5041044-16 MW1 Ground Water 04/28/15 10:36 Grab 5041044-17 MW3A Ground Water 04/28/15 10:55 Grab 5041044-18 MW3A Ground Water 04/28/15 11:55 Grab 5041044-19 MW5 Ground Water 04/28/15 11:16 Grab 5041044-20 MW5 Ground Water 04/28/15 11:20 Grab 5041044-21 MW3 Ground Water 04/28/15 11:30 Grab 5041044-22 MW3 Ground Water 04/28/15 11:32 Grab 5041044-23 MW4 Ground Water 04/28/15 11.38 Grab 5041044-24 MW4 Ground Water 04/28/15 11:40 Grab 5041044-25 MW2 Ground Water 04/28/15 11:59 Grab 5041044-26 MW2 Ground Water 04/28/15 12:01 Grab 5041044-27 PZ1 Ground Water 04/28/15 12:06 Grab PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05; 21 2015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number Sample Description Matrix Sampled Type 5041044-28 PZ1 Ground Water 04/28/15 12:23 Grab 5041044-29 Trip Blank Ground Water 04/27/15 09:20 Grab 5041044-30 Equipment Blank Ground Water 04/27/15 13:43 Grab 5041044-31 MW7 Ground Water 04/27/15 14:29 Grab 5041044-32 MW12 Ground Water 04/27/15 15:24 Grab 5041044-33 MW10 Ground Water 04/27/15 16:13 Grab 5041044-34 Field Blank Near MW 11 Ground Water 04/27/15 16:40 Grab 5041044-35 MW 11 Ground Water 04/27/15 17:10 Grab 5041044-36 MW8 Ground Water 04/27/15 18:18 Grab 5041044-37 MW9 Ground Water 04/28/15 08:43 Grab 5041044-38 MW6 Ground Water 04/28/15 09:31 Grab 5041044-39 MW1 Ground Water 04/28/15 10:37 Grab 5041044-40 MW5 Ground Water 04/28/15 11:20 Grab 5041044-41 MW3 Ground Water 04/28/15 11:32 Grab 5041044-42 MW4 Ground Water 04/28/15 11:40 Grab 5041044-43 MW3A Ground Water 04/28/15 11:54 Grab 5041044-44 MW2 Ground Water 04/28/15 12:01 Grab 5041044-45 PZ1 Ground Water 04/28/15 1222 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax 864.232,6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not he reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers • ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Data Sample Number 5041044-01 Sample Description MW7 collected on 04/27/15 13:48 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 13.61 0.00 Ft 1.00 04/27/15 13:48 CGW B5D1036 Sample Number 5041044-02 Sample Description MW7 collected on 04/27/15 14:30 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.2 0.1 pH Units 1.00 04/27/15 14:30 EPA 9040C CGW B5D1036 Specific Conductance at 25 C 117 10.0 umhos/cm 1.00 04/27/15 14:30 EPA 9050A CGW B5D1036 Temperature 21.2 0.0 °C 1.00 04/27/15 14:30 SM255OB-2010 CGW B5131036 Turbidity (Field) 69.3 5.0 NTU 1.00 04/27/15 14:30 Field Screen CGW B5D1036 Sample Number 5041044-03 Sample Description MW 12 collected on 04/27/15 14:44 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 19.47 0.00 Ft I.00 04/27/15 14:44 CGW B5D1036 Sample Number Sample Description Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 7.1 0.1 pH Units 1.00 04/27/15 15:25 EPA9040C CGW B5D1036 Specific Conductance at 25 C 4W 10.0 umhos/cm 1.00 04/27/15 15:25 EPA 9050A CGW B5D1036 Temperature 21.0 0.0 °C 1.00 04/27/15 15:25 SM255OB-2010 CGW B5D1036 Turbidity (Field) ND 5.0 NTU 1.00 04/27/15 15:25 Field Screen CGW B5D1036 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 Pax %4.232.6140 rogersandcallcott.com an employee -owned company 05121 2015 1 a: d2 This report may not be reproduced, except in fadl, without written permission front Rogers & Callcott, Inc. Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-05 Sample Description MW 10 collected on 04/27/15 15:38 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 27.79 0.00 Ft 1.00 04/27/15 15:38 CGW B5D1036 Sample Number 5041044-06 Sample Description llected on 04/27/15 16:14 40W Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.7 0.1 pH Units 1.00 04/27/15 16:14 EPA9040C CGW B5D1036 to . low 10.0 umhos/cm 1.00 04/27/15 16:14 EPA9050A CGW B5131036 Temperature 21.3 0.0 °C 1.00 04/27/15 16:14 SM 2550B-2010 CGW BSD1036 Turbidity (Field) 8.6 5.0 NTU 1.00 04/27/15 16:14 Field Screen CGW 135D1036 Sample Number 5041044-07 Sample Description MW 11 collected on 04/27/15 16:25 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 28.08 0.00 Ft 1.00 04/27/15 16:25 CGW B5D1036 Sample Number 44-08 Sample Description - collected on 04/27/15 17:11 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 8 0.1 pH Units 1.00 04/27/15 17:11 EPA9040C CGW B5D1036 v_ liti7 3" .•� 10.0 umhos/cm 1.00 04/27/15 17:11 EPA9050A CGW B5D1036 Temperature 20.1 0.0 °C 1.00 04/27/15 17:11 SM2550B-2010 CGW B5131036 Turbidity (Field) 15.1 5.0 NTU 1.00 04/27/15 17:11 Field Screen CGW B5D1036 Sample Number 5041044-09 Sample Description MW8 collected on 04/27/15 17:47 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 7.80 0.00 Ft 1.00 04/27/15 17:47 CGW 135D1036 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way € Greenville, SG 29607 1 main 864.232.1556 1 fax 864.232,6140 rogersandcallcott.eom an employee -owned company 05.71.2015 14:41 This report may not he reproduced, except in full, without written permission from Rogers & C'allcon, Inc. Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-10 Sample Description MW8 collected on 04/27/15 18:19 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.6 0.1 pH Units 1.00 04/27/15 18:19 EPA 9040C CGW 135D1036 Specific Conductance at 25 C 179 10.0 umhos/cm 1.00 04/27/15 18:19 EPA 9050A CGW 135D1036 Temperature 17.6 0.0 °C 1.00 04/27/15 18:19 SM255OB-2010 CGW 135D1036 Turbidity (Field) >1000 5.0 NTU 1.00 04/27/15 18:19 Field Screen CGW 135D1036 Sample Number 5041044-11 Sample Description MW9 collected on 04/28/15 08:13 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 20.58 0.00 Ft 1.00 04/28/15 08:13 CGW 135D1036 Sample Number Sample Description 44 kiwin� Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 7.0 0.1 pH Units 1.00 04/28/15 08:44 EPA 9040C CGW 135D1036 SNMI 10.0 umhos/cm 1.00 04/28/15 08:44 EPA9050A CGW 135D1036 Temperature 15.5 0.0 °C 1.00 04/28/15 08:44 SM2550B-2010 CGW 135D1036 Turbidity (Field) 9.4 5.0 NTU 1.00 04/28/15 08:44 Field Screen CGW 135D1036 Sample Number 5041044-13 Sample Description MW6 collected on 04/28/15 09:03 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 16.22 0.00 Ft 1.00 04/28/15 09:03 CGW 135D1036 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main $64.232.1556 1 fax W.232.6140 rogersandcallcott.com a i employee -owned company 05,21,2015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers & callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-14 Sample Description MW6 collected on 04/28/15 09:32 Reporting Parameter Result Limit units DF Analyzed Method Flag Analyst Batch Field Parameters pH 5.8 0.1 pH Units 1.00 04/28/15 09:32 EPA 9040C CGW BSD1036 Specific Conductance at 25 C 114 10.0 umhos/cm 1.00 04/28/15 09:32 EPA 9050A CGW B5D1036 Temperature 19.0 0.0 °C 1.00 04/28/15 09:32 SM255OB-2010 CGW B5D1036 Turbidity (Field) 85.4 5.0 NTU 1.00 04/28/15 09:32 Field Screen CGW B5D1036 Sample Number 5041044-15 Sample Description MW 1 collected on 04/28/15 10:00 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 10.12 0.00 Ft 1.00 04/28/15 10:00 CGW B5D1036 Sample Number 5041044-16 Sample Description MW 1 collected on 04/28/15 10:36 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.2 0.1 pH Units 1.00 04/28/15 10:36 EPA 9040C CGW B5D1036 Specific Conductance at 25 C 188 10.0 umhos/cm 1.00 04/28/15 10:36 EPA 9050A CGW B5D1036 Temperature 18.6 0.0 °C 1.00 04/28/15 10:36 SM255OB-2010 CGW B5D1036 Turbidity (Field) ND 5.0 NTU 1.00 04/28/15 10:36 Field Screen CGW 135D1036 Sample Number 5041044-17 Sample Description MW3A collected on 04/28/15 10:55 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 23.01 0.00 Ft 1.00 04/28/15 10:55 CGW B5D1036 PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way € Greenville, SC 29607 € main 864.2311556 1 fax W.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. , w Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-18 Sample Description aw ollected on 04/28/15 11:55 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 7.3 0.1 pH Units 1.00 04/28/15 11:55 EPA9040C CGW B5D1036 10.0 umhos/cm 1.00 04/28/15 11:55 EPA9050A CGW B5D1036 Temperature 20.5 0.0 °C 1.00 04/28/15 11:55 SM 255OB-2010 CGW B51)1036 Turbidity (Field) 6.5 5.0 NTU 1.00 04/28/15 11:55 Field Screen CGW B5D1036 Sample Number 5041044-19 Sample Description MW5 collected on 04/28/15 11:16 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 56.43 0.00 Ft 1.00 04/28/15 11:16 CGW B5D1036 Sample Number 5041044-20 Sample Description 04/28/15 11:20 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 0.1 pH Units 1.00 04/28/15 11:20 EPA 9040C CGW 135D1036 Specific Conductance at 25 C 10.0 umhos/cm 1.00 04/28/15 11:20 EPA 9050A CGW 135D1036 Temperature 21.2 0.0 °C 1.00 04/28/15 11:20 SM2550B-2010 CGW B5D1036 Turbidity (Field) ND 5.0 NTU 1.00 04/28/15 11:20 Field Screen CGW B5D1036 Sample Number 5041044-21 Sample Description MW3 collected on 04/28/15 11:30 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 58.54 0.00 Ft 1.00 04/28/15 11:30 CGW B5D1036 PO Box 5655 1 Greenville, SC 296% 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05 21 '2015 14: 42 This report may not he reproduced, except in full, without written permission from Rogers & Callcott, Inc. }' Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5 Sample Description lowd on 04/28/15 11:32 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 7.0 0.1 pH Units 1.00 04/28/15 11:32 EPA 9040C CGW B5D1036 Slecific Conductance at 25 C 10.0 umhos/cm 1.00 04/28/15 11:32 EPA 9050A CGW B5D1036 Temperature 20.5 0.0 °C 1.00 04/28/15 11:32 SM255OB-2010 CGW B5D1036 Turbidity (Field) ND 5.0 NTU 1.00 04/28/15 11:32 Field Screen CGW B5131036 Sample Number 5041044-23 Sample Description MW4 collected on 04/28/15 11:38 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 58.51 0.00 Ft 1.00 04/28/15 11:38 CGW B5D1036 Sample Number 5041044-24 Sample Description on 04/28/15 11 A0 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.6 0.1 pH Units 1.00 04/28/15 11:40 EPA 9040C CGW 135D1036 Specific Conductance at 25 C 10.0 umhos/cm 1.00 04/28/15 11:40 EPA 9050A CGW 135D1036 Temperature 20.5 0.0 °C 1.00 04/28/15 11:40 SM255OB-2010 CGW B5D1036 Turbidity (Field) 16.5 5.0 NTU 1.00 04/28/15 11:40 Field Screen CGW B5131036 Sample Number 5041044-25 Sample Description MW2 collected on 04/28/15 11:59 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 30.76 0.00 Ft 1.00 04/28/15 11:59 CGW B5D1036 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.2311556 1 fax W.232.6140 rogersandcallcott.com an employee -owned company 05 212015 14:42 This report may not be reproduced, eccept in full, without written permission from Rogers & Callcon, Inc. Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-26 Sample Description 04/28/15 12:01 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 6.7 0.1 pH Units 1.00 04/28/15 12:01 EPA9040C CGW 135D1036 Specific Conductance at 25 C - 10.0 umhos/cm 1.00 04/28/15 12:01 EPA 9050A CGW B51)1036 Temperature 21.6 0.0 °C 1,00 04/28/15 12:01 SM 2550B-2010 CGW B5D1036 Turbidity (Field) 14.3 5.0 NTU 1.00 04/28/15 12:01 Field Screen CGW B5D1036 Sample Number 5041044-27 Sample Description PZ1 collected on 04/28/15 12:06 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters Depth to Water 22.07 0.00 Ft 1,00 04/28/15 12:06 CGW B5D1036 Sample Number ,5,4�0�4 Sample Description PZ`l b /28/15 12:23 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 0.1 pH Units 1.00 04/28/15 12:23 EPA 9040C CGW B51)1036 Specific Conductance at 25 C 10.0 umhos/cm 1.00 04/28/15 12:23 EPA 9050A CGW B5D1036 Temperature 18.4 0.0 °C 1.00 04/28/15 12:23 SM 255OB-2010 CGW B5D1036 Turbidity (Field) 156 5.0 NTU 1.00 04/28/15 12:23 Field Screen CGW B5D1036 PO Box 5655 ; Greenville, SC 296% 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05'21 2015 1 a: 42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-29 Sample Description Trip Blank collected on 04/27/15 09:20 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 1,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW BSE0368 l,l-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 9260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 9260B LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260E LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260E LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 15:47 EPA 9260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 u8/L 1.00 04/29/15 15:47 EPA 8260E LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260E LBW B5E0368 o-Xylene ND 1.0 u8/L 1.00 04/29/15 15:47 EPA 8260E LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 u8/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW BSE0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260E LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 15:47 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 83 70-130 4-Bromofluorobenzene 96 70-130 Toluene-d8 87 70-130 PO Box 5655 ' Greenville, SC 29606 1426 Fairforest Way l Greenville. SC 29607 i main 864.232.1556 1 fix 864.232.6140 rogerSandcallcott.com an employee -owned company 05/21/2015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 11 of 42 Rogers &Caticott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number Sample Description Parameter 5041044-30 Equipment Blank collected on 04/27/15 13:43 Reporting Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 1,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 1,1-Dichloroethene ND 0.5 118/1, 1.00 04/29/15 16:18 EPA 9260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 118/1, 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Acetone ND 10.0 U91L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 16,18 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260E LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 9260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ng/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 16:18 EPA 8260E LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 16:18 EPA 9260B LBW B5E0368 n-Propylbenzene ND 0.5 n8/L 1.00 04/29/15 16:18 EPA 9260B LBW B5E0368 o-Xylene ND 1.0 118/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 118/L 1.00 04/29/15 16:18 EPA 8260B LBW BSE0368 Styrene ND 0.5 119/1, 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260E LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260E LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 9260B LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 16:18 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,1-Dichloroethane-D4 84 70-130 4-BromoJ&rorobenzene 96 70-130 Toluene-& 84 70-130 PO Sax 5655 1 Greenville, SC 296M 1 426 Fairforest Way Greenville, SC 29607 1 main 864.232.1556 ! fax 864,232.6140 rogersandcallcott.com - an employee -owned company 0512112015 14:41 This report may not be reproduced, except in full, without written permission from kogers & Callcou, Inc. Page 12 of 42 NKe Rogers & • ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-31 Sample Description MW7 collected on 04/27/15 14:29 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 1,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW BSE0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW 135E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 9260B LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 cis-1,2-Dichloroethene ND 05 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Ethylbenzene ND OS ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 Naphthalene ND 2.0 ng/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 n-Butylbenzene ND 1.0 ue/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 tert-Butylbenzene ND 0.5 u8/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260E LBW B5E0368 Toluene ND 0.5 ng/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW BSE0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 16:49 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 91 70-130 4-BromoJfuorobenzene 106 70-130 Toluene-d8 91 70-130 PO Box 5655 i Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 fax 864.232.6140 rogersandcalICOtt.com -� r--- an employee -owned company 0512112015 14: 41 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 13 of 42 Rogers&Callcott �._ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-32 Sample Description MW 12 collected on 04/27/15 15:24 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 1, 1 -Dichloroethane ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 9260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW BSE0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 9260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1,00 04/29/15 17:19 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 9260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 Styrene ND 0.5 ug/L 1,00 04/29/15 17:19 EPA 8260E LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ng/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260E LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 17:19 EPA 8260B LBW B5E0368 Surrogates %REC %RECLimits Flag 1,2-Dichloroethane-D4 91 70-130 4-Bromoflaorobenzene 103 70-130 Toluene-& 91 70-130 Po Box 5655 Greenville, SC 29606 1426 Fairforest Way E Greenville, SC 29607 1 main 864.232.1556 1 fax W,232.6140 rogerSalldcallcott.col71 -- an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 14 of 42 Rogers &Callcott sr_ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-33 Sample Description MW10 collected on 04/27/15 16:13 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1,1,1-Trichloroethane ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 1, 1 -Dichloroethane ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 1,1-Dichloroethene ND 0.5 118/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 9260B LBW BSE0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW BSE0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 9260B LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW BSE0368 Toluene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260E LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 17:50 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Diehloroethane-D4 91 70-130 4-Bromoflaorobenzene 102 70-130 Toluene-& 93 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way i Greenville, SC 29607 I main 864.232.1556 1 fax 864,232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-34 Sample Description Field Blank Near MW 11 collected on 04/27/15 16:40 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1,1,1-Trichloroethane ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 1, 1 -Dichloroethane ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260E LBW B5E0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW BSE0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 18:21 EPA 8260E LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 u8/L 1.00 04/29/15 18:21 EPA 8260E LBW BSE0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 18:21 EPA 8260E LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/l. 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 u8/L 1.00 04/29/15 18:21 EPA 8260B LBW BSE0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 u8/L 1.00 04/29/15 18:21 EPA 8260B LBW BSE0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260E LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW BSE0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260E LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 u8/L 1.00 04/29/15 18:21 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 91 70-130 4-BromoJlttorobenzene 104 70-130 Toluene-d8 95 70-130 PO Box 5655 Greenville, SC 2%% 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 fax 864.232,6140 rogersandcallcott.Com an employee -owned company 05/21/2015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 16 of 42 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044- Sample Description 0 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1,1,1-Trichlor ethane 1,2,4-Trimethylbenzene 1,2-Dichloroethane Acetone Benzene Bromomethane (Methyl Bromide) Chloroform Ethylbenzene Hexane Isopropylbenzene m,p-Xylene Methylene chloride Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-l2-Dichloroethene Vinyl chloride Surrogates ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ug/L 1.00 04/29/15 18:51 EPA 9260B LBW B5E0368 ug/L 1.00 04/29/15 18:51 EPA 8260B S1 LBW BSE0369 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 10.0 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 0.5 ug/L. 1.00 04/29/15 18:51 EPA 9260B LBW B5E0368 ND 1.0 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 1.0 ug/L 1.00 04/29/15 18:51 EPA 826013 LBW B5E0368 ND 2.0 ug/L 1.00 04/29/15 18:51 EPA 9260B LBW B5E0368 ND 2.0 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 1.0 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 1.0 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 9260B LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 9260B LBW BSE0368 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ug/L 1.00 04/29/15 18:51 EPA 8260E LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 18:51 EPA 8260B LBW BSE0368 %aREC %REC Limits Flag 1,2-Dichloroethane-D4 85 70-130 4-Bromoflaorobenzene 93 70-130 Toluene-& 84 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 17 of 42 Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number Sample Description Parameter 5041044-36 04/27/15 18:18 Result Reporting Limit units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW BSE0368 I,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW BSE0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260E LBW BSE0368 Acetone ND 10.0 ug/L 1.00 04/29/15 20:23 EPA 8260E LBW 135E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Chloroform ND 0.5 ❑g/L 1.00 04/29/15 20:23 EPA 8260E LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Hexane ND 1.0 ut,/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA9260B LBW B5E0368 m,p-Xylene ND 1.0 u8/L 1.00 04/29/15 20:23 EPA 8260E LBW 135E0368 Methylene chloride ND 2.0 u8/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 us/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 u8/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 u8/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260E LBW B5E0368 tert-Butvlbenzene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260E LBW B5E0368 hloroeth= ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260E LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 Ug/L 1.00 04/29/15 20:23 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 83 70-130 4-Bromofhtorobenzene 102 70-130 Toluene-& 87 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax 864,232.6140 rogersandcallcott.com a t employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. page 18 of 42 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 50410 Sample Description Parameter n 04/28/15 08:43 Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichl oroethane ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 I,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260E LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L. 1,00 04/29/15 20:53 EPA 8260B LBW B5E0368 Etylbenzene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L L00 04/29/15 20:53 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260E LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ❑g/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Styrene ND 0.5 u9/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260E LBW B5E0368 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260B LBW B5E0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260E LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 20:53 EPA 8260E LBW B5E0368 Surrogates % REC % REC Limits Flag 1,1-Dichloroethane-14 84 70-130 4-Bromoflnorobenzene 100 70-130 Toluene-d8 85 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05212015 14: 41 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-38 Sample Description 04/28/15 09:31 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW BSE0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 I,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 9260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 Acetone 10.0 ug/L 1.00 04/29/15 21:24 EPA 8260E LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 9260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW BSE0368 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 tsstl. a ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260E LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260E LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260E LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260E LBW BSE0368 Styrene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 Tetrachloroethene 1.0 0.5 ti ug(L 1.00 04/29/15 21:24 EPA 8260E LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 8260B LBW BSE0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 21.24 EPA 8260E LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 21:24 EPA 9260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 86 70-130 4-Bromofluorobenzene 99 70-130 Toluene-d8 86 70-130 PC) Box 5655 Greenville, SC 29606 ! 426 Fairforest Way 1 Greenville, SC 29607 1 main $64.232.1556 ' fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcon,, Inc. Page 20 of 42 0•iAh 0 • Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-39 Sample Description MW I collected on 04/28/15 10:37 Parameter Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 I,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA9260B LBW BSE0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 Acetone ND 10.0 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW 135E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW 135E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 9260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260E LBW 1315E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW 135E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 21:55 EPA 8260E LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 Styrene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 Tetrachloroethene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW 135E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 Trichloroethene ND 0.5 ug/L 1.00 04/29/15 21:55 EPA 8260B LBW BSE0368 Vinyl chloride ND 0.5 ng/L 1.00 04/29/15 21:55 EPA 8260B LBW B5E0368 Surrogates % REC % REC Limits Flag 1,2-Dichlaroethane-D4 85 70-130 4-Bromofhrorobenzene 98 70-130 Toluene-d8 84 70-130 PO Sox 5655 1 Greenville, SC 29606 l 426 Fairforest Way € Greenville, SC 29607 i main 864.232.1556 1 fax 864.232.6140 rOgerSandCaliCOtt.COfli __�...... an ernployee-owned company 05 21.2015 14:41 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 21 of 42 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-40 Sample Description Parameter 8/15 11:20 Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW BSE0368 1,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260E LBW BSE0368 1,1-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW BSE0368 1,2,4-Trimethy�ene IM ug/L 1.00 04/29/15 22:25 EPA 8260B LBW BSE0368 ug/L 1.00 04/29/15 22:25 EPA 8260E LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 22:25 EPA 8260E LBW B5E0368 Benzene ND 0.5 ue/L 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 low oft u8/L 1.00 04/29/15 22:25 EPA 8260E LBW B5E0368 T 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 Ethylbenzene INIMug/L 0. ug/L 1.00 04/29/15 22:25 EPA 8260E LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 22:25 EPA 9260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 9260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW BSE0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 22:25 EPA 9260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW BSE0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 9260B LBW BSE0368 o-Xylene ND 1.0 118/L 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260E LBW BSE0368 tert-Butylbenze � u8/L 1.00 04/29/1S 22:25 EPA 8260B LBW BSE0368 m* ug/L 1.00 04/29/15 22:25 EPA 8260E LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 22:25 EPA 8260B LBW BSE0368 transtransroethene ug/L 1.00 04/29/15 22:25 EPA 9260B LBW B5E0368 MoMe � ug/L 1.00 04/29/15 22:25 EPA 8260B LBW 135E0368 Vinyl chloride ND 0.5 118/1- 1.00 04/29/15 22:25 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 84 70-130 4-Bromofluorobenzene 97 70-130 Toluene-& 83 70-130 PO Box 5655 I Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax 8".232.6140 rogersandcallcott.com --- -- a i employee -owned company 05 212015 14: 42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 22 of 42 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5 044-41 Sample Description Parameter 4/28/15 11:32 Result Reporting Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1,1,1-Tnchloro ane ugL 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 ug/L 1.00 04/30/15 00:28 EPA 8260E LBW B5E0368 1 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW BSE0368 1,2-Dichloroethane 0.9 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0. ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260E LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW BSE0368 Naphthalene ND 2.0 ug/L 1.00 04/30/15 00:28 EPA 8260E LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW BSE0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 9260B LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260E LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/30/15 00:28 EPA 8260B LBW B5E0368 Rph umber:5041044-41RE1 ug/L 5.00 05/05/15 19:33 EPA 8260B ARM B5E0369 ug/L 5.00 05/05/15 19:33 EPA 8260B ARM B5E0369 vim ug/L 5.00 05/05/15 19:33 EPA 8260B ARM B5E0369 Surrogates %REC % REC Limits Flag 1,1-Uichloroethane-D4 94 70-130 4-Bromojluorobencene 112 70-130 Toluene-d8 92 70-130 Rebatch Sample Number:.5041044-41REI 1.2-Uichloroethane-U4 87 70-130 4-BromoJluorobenzene 99 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 tax 864.232.6140 rogersandcalleott.eom an employee -owned company 05 212015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers & callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-41RE1 Sample Description MW3 collected on 04/28/15 11:32 Reporting Parameter Result Limit units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC % REC Limits Flag Rebatch Sample Number: 5041044-41RE1 Toluene-d8 92 70-130 PO Box 5655 1 Greenville, SC 2960E 1 426 Fairforest Way i Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.E l40 rogersandcallcott,com an employee -owned company 05, 21 2015 14: 42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-42 Sample Description MW4 collected on 04/28/15 11:40 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1,00 04/29/15 22:56 EPA 8260B LBW BSE0368 1,1-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 1 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 NNW 0.5 u8/L 1.00 04/29/15 22:56 EPA 9260B LBW B5E0368 Acetone ND 10.0 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Wthylbeo.ene ow0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260E LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 22:56 EPA 8260E LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260E LBW 135E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 22:56 EPA 8260B LBW B5E0368 Rebatch S mber: 504104442REI 5.0 ug/L 5.00 05/05/15 20:03 EPA 8260E ARM B5E0369 5.0 ug/L 5.00 05/05/15 20:03 EPA 8260B ARM B5E0369 5.0 ug/L 5.00 05/05/15 20:03 EPA 8260B ARM BSE0369 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 92 70-130 4-Bromofluorobenzene 111 70-130 Toluene-& 84 70-130 Rebatch Sample Number: 5041044-42RE1 1,2-Dichloroethane-D4 86 70-130 4-Bromofluorobenzene 96 70-130 PO Box 5655 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 l main 864.232.I556 1 fax 864.232.6140 rogersandcallcott.com --�--------- an employee -awned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission front Rogers & Callcott, Inc. Page 25 of 42 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-42RE1 Sample Description MW4 collected on 04/28/15 11:40 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates % REC % REC Limits Flag Rebatch Sample Number: 5041044-42RE1 Toluene-d8 93 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 ! fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc h, ;t" sa Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-43 Sample Description MW3A collected on 04/28/15 11:54 Parameter Result Reporting Limit Units DFi Analyzed Method Flag Analyst Batch Volatile Organics 1,1,1-Trichloroethane ND 0.5 u8/L 1.00 04/29/15 23:27 EPA 8260B LBW BSE0368 1,1-Dichloroethane 6.0 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 1,1-Dichloroethene 1.6 0.5 us/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 1,2-Dichloroethane ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Acetone ND 10.0 U9(L 1.00 04/29/15 23:27 EPA 8260E LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Chloroform ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 cis-1,2-Dichloroethene 39.0 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Ethylbenzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260E LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260E LBW B5E0368 m,p-Xylene ND 1.0 u8/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/29/15 23:27 EPA 9260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 9260B LBW B5E0368 o-Xylene ND 1.0 us/[. 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260E LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Toluene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260E LBW B5E0368 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260B LBW B5E0368 Vinyl chloride ND 0.5 ug/L 1.00 04/29/15 23:27 EPA 8260E LBW BSE0368 Rebatch Sample Number: 504104443RE1 Tetrachloroethene ND 0.5 ug/L 1.00 05/05/15 22:51 EPA 8260B LBW B5E0180 Trichloroethene 0.7 0.5 ug/L 1.00 05/05/15 22:51 EPA 8260B LBW B5E0180 Surrogates %REC % REC Limits Flag 1,2-Dichloroethane-D4 84 70-130 4-BromoJluorobenzene 99 70-130 Toluene-d8 86 70-130 Rebatch Sample Number: 5041044-43RE1 1,2-Dichloroethane-D4 85 70-130 4-Bromojfuorobenzene 115 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way ! Greenville, SC 29607 1 main 864-232.1556 fax 864.232.6140 rogersandcalleott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 27 of 42 Rogers • Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-43RE1 Sample Description MW3A collected on 04/28/15 11:54 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates % REC % REC Limits Flag Rebatch Sample Number: 504104443RE1 Toluene-& 98 70-130 PO Box 5655 Greenville, SC 29606 1 426 Fairforest Way i Greenville, SC 29607 i main 864.232.1556 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14: 41 This report may not be reproduced, except in full, without written permission from Rogers & C'allcott, Inc. Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number Sample Description Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics da0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW BSE0368 ,1-Dichloroethane ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260E LBW B5E0368 0.5 ug/L 1.00 04/30/15 00:59 EPA826oB LBW B5E0368 Acetone 0 ND 10.0 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 Benzene ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 Bromomethane (Methyl Bromide) ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260E LBW B5E0368 + 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 Hexane ND 1.0 ug/L 1.00 04/30/15 00:59 EPA 8260E LBW B5E0368 Isopropylbenzene ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 m,p-Xylene ND 1.0 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 Methylene chloride ND 2.0 ug/L 1.00 04/30/15 00:59 EPA 8260E LBW B5E0368 Naphthalene ND 2.0 ug/L 1.00 04/30/15 00:59 EPA 8260E LBW B5E0368 n-Butylbenzene ND 1.0 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 n-Propylbenzene ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260E LBW B5E0368 o-Xylene ND 1.0 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 0.5 ug/L 1.00 04/30/15 0059 EPA 8260E LBW B5E0368 Styrene ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 tert-Butylbenzene ND 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 ® 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 0.5 ug/L 1.00 04/30/15 00:59 EPA 8260B LBW B5E0368 Rebatch Sample Number: 5041044-44RE1 100 ug/L 100 05/05/15 20:33 EPA 8260B ARM B5E0369 -hene -1�bb0 100 ug/L 100 05/05/15 20:33 EPA 8260B ARM B5E0369 5260 100 ug/L 100 05/05/15 20:33 EPA 8260B ARM B5E0369 100 ag/L 100 05/05/15 20:33 EPA 8260B ARM BSE0369 Surrogates %REC % REC Limits Flag 1,2-Dichloroethane-D4 77 70-130 4-Bromofluorobenzene 103 70-130 Toluene-d8 76 70-130 Rebatch Sample Number: 5041044-44RE1 1,2-Dichloroethane-D4 88 70-130 4-Brotno luoroben_ene 94 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom a i employee -owned company 05 212015 14:41 This report may not be reproduced, except in fill, without written permission from Rogers & Callcott, Inc. Page 29 of 42 Rogers & callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-44RE1 Sample Description MW2 collected on 04/28/15 12:01 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5041044-44RE1 Toluene-d8 } 90 70-130 1 PO Box 5655 Greenville, SC 29606 426 Fair€orest Way I Greenville, SC 29607 main 864.232.1556 1 fax 864.232,6140 rogersandcallcott.com - — — an employee -awned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Rogers & Calicott ENVIRONMENTAL Catalent Pharrna Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-45 Sample Description PZ I collected on 04/28/15 12:22 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics �f 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 1,1-Dichloroeth ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW 135E0368 1,2,4-Trimethylbenzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW B5E0368 1,2-Dichloroethane ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 Acetone ND 100 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW 135E0368 Benzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW 135E0368 Bromomethane (Methyl Bromide) ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW 135E0368 y enzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW B5E0368 Hexane ND 10.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW B5E0368 Isopropylbenzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW B5E0368 m,p-Xylene ND 10.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 Methylene chloride ND 20.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW 135E0368 Naphthalene ND 20.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW 135E0368 n-Butylbenzene ND 10.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW B5E0368 n-Propylbenzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 9260B LBW B5E0368 o-Xylene ND 10.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 sec-Butylbenzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 Styrene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW 135E0368 tert-Butylbenzene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW 135E0368 Toluene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260E LBW B5E0368 trans-1,2-Dichloroethene ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW B5E0368 in 5.0 ug/L M0 04/30/15 01:29 EPA 8260B LBW B5E0368 Vinyl chloride ND 5.0 ug/L 10.0 04/30/15 01:29 EPA 8260B LBW 135E0368 Rebatch Sample Number: 504104445RE1 250 ug/L 500 04/29/15 23:57 EPA 8260B LBW B5E0368 e 4A 250 ug/L 500 04/29/15 23:57 EPA 8260B LBW B5E0368 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 70 70-130 4-Bromofluombencene 108 70-130 Toluene -dB 88 70-130 Rebatch Sample Number: 504104445RE1 1,2-Dichloroethane-D4 85 70-130 4-Bromofluorobenaene 97 70-130 PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05 212015 14: 41 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Sample Number 5041044-45RE1 Sample Description PZ1 collected on 04/28/15 1222 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates % REC % REC Limits Flag Rebatch Sample Number: 5041044-45RE1 Toluene-d8 84 70-130 PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main M.232.1556 I fax M.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, eccept in full, without written permission fmm Rogers & Callcott, Inc. Page 32 of 42 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5E0180 - EPA 5030 Blank (B5E0180-BLK1) Tetrachloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Surrogate:l,1-Dichloroethane-D4 79 70-130 Surrogate:4-Bromofluorobenzene 114 70-130 Surrogate: Toluene-& 97 70-130 LCS (B5E0180-BSl) Tetrachloroethene 21.8 0.5 ug/L 20.0 109 70-130 Trichloroethene 21.1 0.5 ug/L 20.0 106 70-130 Surrogate:l,2-Dichloroethane-D4 106 70-130 Surrogate: 4-Bromofluorobenzene 110 70-130 Surrogate: Toluene-d8 108 70-130 Matrix Spike (B5E0180-MS1) Source: 5050076-13 Tetrachloroethene 21.9 0.5 ug/L 20.0 ND 110 70-130 Trichloroethene 21.9 0.5 u91L 20.0 ND 105 70-130 Surrogate:l,2-Dichloroethane-D4 106 70-130 Surrogate:4-Bromofluorobenzene 114 70-130 Surrogate: Toluene-d8 110 70-130 Matrix Spike Dup (B5E0180-MSD1) Source: 5050076-13 Tetrachloroethene 20.5 0.5 ug/L 20.0 ND 102 70-130 7 20 Trichloroethene 20.9 0.5 ug/L 20.0 ND 99 70-130 5 20 Surrogate:l,2-I)ichloroethane-D4 102 70-130 Surrogate: 4-Bromofluorobenzene 111 70-130 Surrogate: Toluene-& 107 70-130 Batch B5E0368 - EPA 5030 Blank (B5E0368-BLK1) 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1,1-Dichloroethane ND 0.5 ug/L 1,1-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 10.0 ug/L Benzene ND 0.5 ug/L PO Box 5655 1 Greenville, SC 29606 1 426 Fairtorest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.eom --- an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & C'allcort, Inc. Page 33 of 42 Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5E0368 - EPA 5030 Blank (B5E0368-BLK1) Bromomethane (Methyl Bromide) ND 0.5 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L Isopropylbenzene ND 0.5 ug/1. m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 2.0 ug/L n-Butylbenzene ND 1.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate: 1, 2-Dichloroethane-D4 Surrogate: 4-Bromq/luorobenzene Surrogate: Toluene-d8 LCS (B5E0368-BSI) 83 70-130 99 70-130 86 70-130 1, 1. 1 -Trichloroethane 20.6 0.5 ug/L 20.0 103 70-130 1,1-Dichloroethane 20.7 0.5 ug/L 20.0 104 70-130 1,1-15ichloroethene 23.7 0.5 ug/L 20.0 119 70-130 1,2,4-Trimethylbenzene 22.6 0.5 ug/L 20.0 113 70-130 1,2-Dichloroethane 20.6 0.5 ug/L 20.0 103 70-130 Acetone 102 10.0 ug/L 100 102 60-140 Benzene 20.7 0.5 ug/L 20.0 104 70-130 Bromomethane (Methyl Bromide) 15.7 0.5 ug/L 20.0 79 60-140 Chloroform 18.1 0.5 ug/L 20.0 91 70-130 cis-1,2-Dichlomethene 22.8 0.5 ug/L 20.0 114 70-130 Ethylbenzene 18.0 0.5 ug/L 20.0 90 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report miry not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. - Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5E0368 - EPA 5030 LCS (WE0368-BSI) Hexane 25.1 1.0 ug/L 20.0 125 70-130 Isopropylbenzene 18.4 0.5 ug/L 20.0 92 70-130 m,p-Xylene 47.2 1.0 ug/L 40.0 118 70-130 Methylene chloride 17.3 2.0 ug/L 20.0 86 70-130 Naphthalene 20.5 2.0 ug/L 20.0 102 70-130 n-Butylbenzene 23.9 1.0 ug/L 20.0 119 70-130 n-Propylbenzene 22.4 0.5 ug/L 20.0 112 70-130 o-Xylene 17.6 0.5 ug/L 20.0 88 70-130 sec-Butylbenzene 22.9 0.5 ug/L 20.0 115 70-130 Styrene 23.2 0.5 ug/L 20.0 116 70-130 tert-Butylbenzene 22.8 0.5 ug/L 20.0 114 70-130 Tetrachloroethene 20.6 0.5 ug/L 20.0 103 70-130 Toluene 18.7 0.5 ug/L 20.0 94 70-130 trans-1,2-Dichloroethene 21.8 0.5 ug/L 20.0 109 70-130 Trichloroethene 21.3 0.5 ug/L 20.0 107 70-130 Vinyl chloride 20.5 0.5 ug/L 20.0 103 60-140 ,Surrogate: 1,2-Dichloroethane-D4 107 70-130 Surrogate: 4-Bromgfluorobenzene 104 70-130 Surrogate: Toluene-dS 101 10-130 Matrix Spike (B5E0368-MS1) Source: 5041044-35 1,1,1-Trichloroethane 21.9 0.5 ug/L 20.0 ND 109 70-130 1,1-Dichloroethane 22.9 0.5 ug/L 20.0 0.6 112 70-130 1,1-Dichloroethene 28.9 0.5 ug/L 20.0 2.1 134 70-130 S1 1,2,4-Trimethylbenzene 23.5 0.5 ug/L 20.0 ND 118 70-130 1,2-Dichloroethane 21.7 0.5 ug/L 20.0 ND 109 70-130 Acetone 93.0 10.0 ug/L 100 ND 93 60-140 Benzene 22.1 0.5 ug/L 20.0 ND 110 70-130 Bromomethane (Methyl Bromide) 16.0 0.5 ug/L 20.0 ND 80 60-140 Chloroform 19.2 0.5 ug/L 20.0 ND 96 70-130 cis-1,2-Dichloroethene 26.3 0.5 ug/L 20.0 2.2 121 70-130 Ethylbenzene 19.0 0.5 ug/L 20.0 ND 95 70-130 Hexane 23.9 LO ug/L 20.0 ND 119 70-130 Isopropylbenzene 19.5 0.5 ug/L 20.0 ND 98 70-130 m,p-Xylene 49.9 1.0 ug/L 40.0 ND 125 70-130 Methylene chloride 17.7 2.0 ug/L 20.0 ND 89 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05121 2015 14:42 This report may not be reproduced, except in full, without written permission front Rogers d• Callcort, Inc. r1"_5==WM Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch BSE0368 - EPA 5030 Matrix Spike (B5E0368-MSI) Source: 5041044-35 Naphthalene 21.0 2.0 ug/L 20.0 ND 105 70-130 n-Butylbenzene 25.1 1.0 ug/L 20.0 ND 126 70-130 n-Propylbenzene 23.6 0.5 ug/L 20.0 ND 118 70-130 o-Xylene 18.4 0.5 ug/L 20.0 ND 92 70-130 sec-Butylbenzene 24.3 0.5 ug/L 20.0 ND 122 70-130 Styrene 24.5 0.5 ug/L 20.0 ND 122 70-130 tert-Butylbenzene 24.1 0.5 ug/L 20.0 ND 121 70-130 Tetrachloroethene 21.6 0.5 ug/L 20.0 ND 108 70-130 Toluene 19.8 0.5 ug/L 20.0 ND 99 70-130 trans-1,2-Dichloroethene 23.9 0.5 ug/L 20.0 ND 120 70-130 Tichloroethene 24.6 0.5 ug/L 20.0 1.7 114 70-130 Vinyl chloride 22.9 0.5 ug/L 20.0 ND 114 60-140 Surrogate: 1,2-Dichloroethane-D4 113 70-130 Surrogate:4-Bromofluorobenzene 107 70-130 Surrogate: Toluene-d8 107 70-130 Matrix Spike Dup (B5E0368-MSDI) Source: 5041044-35 1, 1, 1 -Trichloroethane 20.4 0.5 ug/L 20.0 ND 102 70-130 7 20 1,1-Dichloroethane 21.1 0.5 ug/L 20.0 0.6 103 70-130 8 20 1,1-Dichloroethene 25.7 0.5 ug/L 20.0 2.1 118 70-130 11 20 1,2,4-Trimethylbenzene 22.8 0.5 ug/L 20.0 ND 114 70-130 3 20 1,2-Dichloroethane 20.8 0.5 ug/L 20.0 ND 104 70-130 4 20 Acetone 91.6 10.0 ug/L 100 ND 92 60-140 l 20 Benzene 21.1 0.5 ug/L 20.0 ND 105 70-130 5 20 Bromomethane (Methyl Bromide) 15.0 0.5 ug/L 20.0 ND 75 60-140 6 20 Chloroform 18.4 0.5 ug/L 20.0 ND 92 70-130 4 20 cis-1,2-Dichloroethene 25.2 0.5 ug/L 20.0 2.2 115 70-130 4 20 Etylbenzene 19.1 0.5 ug/L 20.0 ND 90 70-130 5 20 Hexane 21.6 1.0 ug/L 20.0 ND 108 70-130 10 20 Isopropylbenzene 18.5 0.5 ug/L 20.0 ND 93 70-130 5 20 m,p-Xylene 47.1 1.0 ug/L 40.0 ND 118 70-130 6 20 Methylene chloride 17.1 2.0 ug/L 20.0 ND 86 70-130 3 20 Naphthalene 22.0 2.0 ug/L 20.0 ND 110 70-130 5 20 n-Butylbenzene 24.3 LO ug/L 20.0 ND 121 70-130 3 20 n-Propylbenzene 22.8 0.5 ug/L 20.0 ND 114 70-130 3 20 o-Xylene 17.8 0.5 ug/L 20.0 ND 89 70-130 3 20 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232,1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 05,212015 14:41 This report may not be reproduced, except in full, without written permission from Rogers & C'allcon, Inc. �wn6 Rogers &Callcott -�; ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5E0368 - EPA 5030 Matrix Spike Dup (B5E0368-MSD1) Source: 5041044-35 sec-Butylbenzene 23.2 0.5 ug/L 20.0 ND 116 70-130 5 20 Styrene 23.4 0.5 ug/L 20.0 ND 117 70-130 4 20 tert-Butylbenzene 22.9 0.5 ug/L 20.0 ND 114 70-130 5 20 Tetrachloroethene 19.9 0.5 ug/L 20.0 ND 100 70-130 8 20 Toluene 19.1 0.5 ug/L 20.0 ND 96 70-130 3 20 trans-1,2-Dichloroethene 21.9 0.5 ug/L 20.0 ND 110 70-130 9 20 Trichloroethene 22.6 0.5 ug/L 20.0 1.7 104 70-130 9 20 Vinyl chloride 19.9 0.5 ug/L 20.0 ND 99 60-140 14 20 Surrogate:l,2-Dichloroethane-D4 107 70-130 Surrogate:4-Bromofluorobenzene 106 70-130 Surrogate: Toluene-& 103 70-130 Batch B5E0369 - EPA 5030 Blank (B5E0369-BLKl) Chloroform cis-1,2-Dichloroethene Tetrachloroethene Trichloroethene ND ND ND ND 0.5 0.5 0.5 0.5 ug/L ug/L ug/L ug/L Surrogate:l,2-Dichloroethane-D4 94 70-130 Surrogate:4-Bromofluorobenzene 92 70-130 Surrogate: Toluene-d8 91 70-130 LCS (B5E0369-BSl) Chloroform 20.8 0.5 ug/L 20.0 104 70-130 cis-1,2-Dichloroethene 21.9 0.5 ug/L 20.0 109 70-130 Tetrachloroethene 19.5 0.5 ug/L 20.0 98 70-130 Trichloroethene 21.5 0.5 ug/L 20.0 107 70-130 ,Surrogate: 1,2-Dichloroethane-D4 111 70-130 Surrogate:4-Bromofluorobenzene 94 70-130 Surrogate: Toluene-& 99 70-130 Matrix Spike (B5E0369-MS1) Source: 5041134-08 Chloroform 22.5 0.5 ug/L 20.0 1.2 106 70-130 cis-1,2-Dichloroethene 23.1 0.5 ug/L 20.0 ND 116 70-130 Tetrachloroethene 21.9 0.5 ug/L 20.0 ND 109 70-130 Trichloroethene 23.0 0.5 ug/L 20.0 ND 115 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 rnain 864,232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproducer,, except in full, without written pennission from Rogers & Callcott, Inc. Page 37 of 42 pg,'Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5E0369 - EPA 5030 Matrix Spike (B5E0369-MS1) Source: 5041134-08 Surrogate: 1,2-Dichloroethane-D4 110 70-130 Surrogate:4-Bromojluorobenzene 98 70-130 Surrogate: Toluene-d8 107 70-130 Matrix Spike Dup (B5E0369-MSD1) Source: 5041134-08 Chloroform 20.2 0.5 ug/L 20.0 1.2 94 70-130 11 20 cis-1,2-Dichloroethene 20.6 0.5 ug/L 20.0 ND 103 70-130 11 20 Tetrachloroethene 17.6 0.5 ug/L 20.0 ND 88 70-130 22 20 P2 Trichloroethene 19.6 0.5 ug/L 20.0 ND 98 70-130 16 20 Surrogate: 1, 2-Dichloroethane-D4 Surrogate: 4-BromoJluorobenzene Surrogate: Toluene-& 104 70-130 91 70-130 92 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforw Way I Greenville, SC 29607 1 main 864.232.1556 , fax 864.232.6140 rogersandcallcott.com an emolovee-owned comoanv 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Groundwater 2021 E. Roosevelt Blvd. Work Order: 5041044 Monroe, NC 28110 Reported: 05/21/15 14:42 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference P2 The RPD between the matrix spike / spike duplicate exceeded the control limits; however, both spike recoveries were within control limits. S 1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0512112015 14:42 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 39 of 42 Rogers & Callcott CHAIN OF CUSTODY RECORD N ENVIRONMENTAL Y Mailing PO Box 56S5 Shipping 426 Fairforest Way 215E Stoneridge drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 G Phone (864) 232-1S56 Fax (864) 232-6140 Phone (803) 509-8999 40 Client Name Catalent G Address Monroe, NC N v GW c ReportTo: c u Email Address `v > Telephone # E D m PO # Project # 93-121 z c a2 d i R&C WORK ORDER YR( DATE TIME SAMPLE DESCRIPTION _)A `f a�- z,J 13�3 r'( e t �lanK Q 4i"-X LIP 1-\w 1 M� t �D`AO �,e� ►� �c�v MwLt 's}10 M Li IlIT iB16 M w 's q AM LER — RELI QUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 2. R NQUISHED BY: DA E/TIME: RECEIVED BY: DATE/TIME: 3. 4 RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 5. 6. RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7, 8. 4 — ossible Hazards associated with samples: 1-1 Non -Hazard Flammable ❑Skin Irritant FlPoison K Unknown apther WORKORDER Soy logy Filtered (Yes/No) Cooled (Yes/No) Container Type (Plastic/Glass) Container Volume (mL) Sample Type (Grab/Composite) Sample Source (WW, GW, DW, SW, S, Other) Preservation Code(s) A —None E—HCI I — ZnAcetate B — HNO3 F — Na2S203 1— H3PO4 C — H2SO4 G — Boric Acid K - MCAA D — NaOH H — Ascorbic Acid L - COMMENTS *3 vials unpres, 1 HCI Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: Temperature of blank or representative sample At time of collection °C At time of lab receipt 1.1 °C Form Revised July, 2014 Page [ of D- q AM LER — RELI QUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 2. R NQUISHED BY: DA E/TIME: RECEIVED BY: DATE/TIME: 3. 4 RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 5. 6. RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7, 8. 4 — ossible Hazards associated with samples: 1-1 Non -Hazard Flammable ❑Skin Irritant FlPoison K Unknown apther WORKORDER Soy logy Filtered (Yes/No) Cooled (Yes/No) Container Type (Plastic/Glass) Container Volume (mL) Sample Type (Grab/Composite) Sample Source (WW, GW, DW, SW, S, Other) Preservation Code(s) A —None E—HCI I — ZnAcetate B — HNO3 F — Na2S203 1— H3PO4 C — H2SO4 G — Boric Acid K - MCAA D — NaOH H — Ascorbic Acid L - COMMENTS *3 vials unpres, 1 HCI Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: Temperature of blank or representative sample At time of collection °C At time of lab receipt 1.1 °C Form Revised July, 2014 Page [ of D- ossible Hazards associated with samples: 1-1 Non -Hazard Flammable ❑Skin Irritant FlPoison K Unknown apther WORKORDER Soy logy Filtered (Yes/No) Cooled (Yes/No) Container Type (Plastic/Glass) Container Volume (mL) Sample Type (Grab/Composite) Sample Source (WW, GW, DW, SW, S, Other) Preservation Code(s) A —None E—HCI I — ZnAcetate B — HNO3 F — Na2S203 1— H3PO4 C — H2SO4 G — Boric Acid K - MCAA D — NaOH H — Ascorbic Acid L - COMMENTS *3 vials unpres, 1 HCI Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: Temperature of blank or representative sample At time of collection °C At time of lab receipt 1.1 °C Form Revised July, 2014 Page [ of D- Rogers & Callcott CHAIN OF CUSI VUY KtLUKu WORKORDER `w"I►U" 1� N Filtered (Yes/No) ENVIRONMENTAL Y Cooled (Yes/No) Mailing PO Box 5655 Shipping 426 Fairforest Way 215E Stoneridge Drive G Container Type Llastic/Glass) 4ddress: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 ao Container Volume (ml) Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Client Name Catalent G Sample Type (Grab/Composite) Address Monroe, NC 121 GW Sample Source (WW, GW, DW, SW, 5, Other) v c M Preservation Codes) V Report To: 0 U A -None E -HCI I - ZnAcetate Email Address o O B-HNO3 F-Na2S203 J-H3PO4 a� m C - H2SO4 G - Boric Acid K - MCAA Telephone # E }; ° D — NaOH H —Ascorbic Acid L - PO # Project # 93-121 z m a COMMENTS co U a ti R & C WORKORDER YR l� DATE TIME SAMPLE DESCRIPTION 3'1 yea Od M W *3 vials unpres, 1 HCl 346 O rn W (D L . 1 l Qv-�- f 1 4 11?o 113a �nw3 � I 1140 N3 1cslE 1'2-o \ M W -}— I--- S PLER -RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: Composite Start Date: 7ndck.l�o� 2; �D�s 2. Composite Start Time: RELINQUISHED BY: DATE/TIME: RECEIVED Y: DATE/TIME: 3 4. Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: Temperature of blank or representative sample 6. S. At time of collection "C At time of lab receipt 1• `F 'C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7. 8. Possible Hazards associated with samples: EINon-Hazard ❑Flammable ❑Skin irritant Poison Unknown El}ther Form Revised July, 2014 Page of o1� Rogers &Callcott ENVIRONMENTAL Sample Receipt Verification Date Client: (' R (,�Iy7" Received: . oZ • l Carrier Name: Client FedEx Tracking Number: UPS US Mail Courier Work Order: 50 H [ O y y field Services Other: Receipt Criteria Y e o A Comments s Shipping container / cooler intact? X Damaged Leaking Other: Custody seals intact? v COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled. Ice Cold Packs Dry Ice None Temp measured with IR thermometer - SN: 97050067 Samples requiring pH preservation at proper pH? No Note: Samples for metals analysis may be preserved upon receipt in the lab. i �C Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot # HCL H3PO4 HZSO4 NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by: !{ t ) (§§[§§§§§[}}[(§@ \ § § )(()§§} ® |R 2VVVV ="vV§`\ {( ) 7IV :! )(§§§ ® \ k § §;2==§§§§(.®.©!^ ;k:„ ( f=§§§[(§§(§§§_!§ k\ §_§§(§(([(§§§§!» !§ ) K :_)(():§ e IQ LQ IQ Vl 6 M6Ili ' ;�lR \| kk\§##%###§§&§■' q;i.6 p; f 2 ! ! Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: VOO2 am 16:32 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on April 14, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TM standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hkach@rogersandeallcott.com or (864)-335-4956 if you have any questions about this report. Permit #WQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Kara Hrkach Project Manager This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. PO Box 5655 1 Greenville, SC 29606 1 426 Pairforest Way I Greenville, SC 29607 1 main W.232.1556 I fax 864.232.6140 rogersandealleott.com an employee -owned company Page 1 of 11 P y Rogers & Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5040602-01 Influent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 17 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Influent Work Order: 5040602 Received: 04/14/2015 16:32 Matrix Sampled Type Ground Water 04/14/15 12:34 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0412812015 09: 23 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 2 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Sample Data Sample Number 5040602-01 Sample Description Influent Grab collected on 04/14/15 12:34 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 1.0 ug/L 1.00 04/16/15 16:08 EPA 9260B LBW 135130894 1,1-Dichloroethane 0.9 05 ug/L 1.00 04/16/15 16:08 EPA 8260E LBW B5D0894 1,1-Dichloroethene 1.2 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 1,2-Dichloroethane 0.8 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260E LBW B51)0894 Acetone ND 20.0 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 Benzene ND 0.5 u8/L 1.00 04/16/15 16:08 EPA 8260E LBW B5D0894 Bromomethane (Methyl Bromide) ND 2.0 u8/1- 1.00 04/16/15 16:08 EPA 8260B LBW B5130894 Chloroform 10.0 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260E LBW B5130894 cis-1,2-Dichloroethene 78.5 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 Ethylbenzene ND 0.5 u8/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 Hexane ND 1.0 ug/L 1.00 04/16/15 16:08 EPA 8260E LBW B5I30894 Isopropylbenzene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 m,p-Xylene ND 1.0 us/L 1.00 04/16/15 16:08 EPA 8260B LBW B5I30894 Methylene chloride ND 2.0 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5D0894 Naphthalene ND 3.0 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5130894 n-Butylbenzene ND 1.0 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5130894 n-Propylbenzene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5130894 o-Xylene ND 1.0 u5/1- 1.00 04/16/15 16:08 EPA 8260B LBW B51)0894 sec-Butylbenzene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260E LBW B5D0894 Styrene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260E LBW B5130894 tert-Butylbenzene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 9260B LBW 135DO894 Toluene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 9260B LBW B5130894 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 04/16/15 16:08 EPA 8260B LBW B5130894 Vinyl chloride ND 0.5 u8/L 1.00 04/16/15 16:08 EPA 8260B LBW B5130894 Rebatch Sample Number: 5040602-01RE1 Tetrachloroethene 182 2.5 ug/L 5.00 04/16/15 19:14 EPA 8260B LBW B5D0894 Trichloroethene 151 2.5 u8/1- 5.00 04/16/15 19:14 EPA 8260B LBW B5130894 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 92 70-130 4-BromoJluorobenzene 92 70-130 Toluene-d8 81 70-130 Rebatch Sample Number: 5040602-01RE1 1,2-Dichloroethane-D4 90 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way i Greenville. SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandealleott.eom an employee -owned company 0412812015 09:23 This report may not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. Page 3 of 11 D Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Sample Number 5040602-OIRE1 Sample Description Influent Grab collected on 04/14/15 12:34 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5040602-OIRE1 4-Bromofluorobenzene 95 70-130 Toluene-d8 87 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 tax 864.232.6140 rogersandcallcott.eom an employee -owned company 0412812015 09: 23 This report muv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 777 11 i y � Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Volatile Organics Quality Control Summary Reporting Spike Source %REC RI'D Parameter Result Limit Units Level Result %REC Limits RPD Limit Ih"S Batch B5D0894 - EPA 5030 Blank (B5D0894-BLKI) 1,1,1-Trichloroethane ND 1, I-Dichloroethane ND 1,1-Dichloroethene ND 1,2,4-Trimethylbenzene ND 1,2-Dichloroethane ND Acetone ND Benzene ND Bromomethane (Methyl Bromide) ND Chloroform ND cis-1,2-Dichloroedrene ND Ethylbenzene ND Hexane ND Isopropylbenzene ND m,p-Xylene ND Methylene chloride ND Naphthalene ND n-Buylbenzene ND n-Propylbenzene ND o-Xylene ND sec-Buylbenzene ND Styrene ND test-Buylbenzene ND Tetrachloroethene ND Toluene ND trans-1,2-Dichloroethene ND Trichloroethene ND Vinyl chloride ND Surrogate: 1,1-Diehloroethane-D4 Surrogate: 4-Bromofluorobeaaene Surrogate: Toluene-& LCS (B5D0894-BSl) 1.0 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 20.0 ug/L 0.5 ug/L 2.0 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 1.0 ug/L 0.5 ug/L 1.0 ug/L 2.0 ug/L 3.0 ug/L 1.0 ug/L 0.5 ug/L LO ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 0.5 ug/L 88 70-130 90 70-130 86 70-130 1,1,1-Trichloroethane 15.6 1.0 ug/L 20.0 78 70-130 l,l-Dichloroethane 19.9 0.5 ug/L 20.0 100 70-130 I,l-Dichloroethene 23.8 0.5 ug/L 20.0 119 70-130 1,2,4-Trimethylbenzene 18.3 0.5 ug/L 20.0 91 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax &A.232.6140 rogersandcalleott.com an employee -owned company 0412812015 09.23 This report ma y not be reproduced, except in full, H ithout written pennissionJrom Rogers & Cal/cat, Inc. Page 7 11 Rogers &Callcott ENVIRONMENTAL Catalent Phartna Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit 1'nits Level Result % REC Limits RPD Limit Flags Batch B5D0894 - EPA 5030 LCS (B5D0894-BSI) 1,2-Dichloroethane 19.8 0.5 ug/L 20.0 99 70-130 Acetone 136 20.0 ug/L 100 136 60-140 Benzene 21.4 0.5 ug/L 20.0 107 70-130 Bromomethane (Methyl Bromide) 25.0 2.0 ug/L 20.0 125 60-140 Chloroform 20.0 0.5 ug/L 20.0 100 70-130 cis-1,2-Dichloroethene 22.3 0.5 ug/L 20.0 112 70-130 Ethylbenzene 20.4 0.5 ug/L 20.0 102 70-130 Hexane 18.4 1.0 ug/L 20.0 92 70-130 lsopropylbenzene 19.2 0.5 ug/L 20.0 96 70-130 m,p-Xylene 40.8 1.0 ug/L 40.0 102 70-130 Methylene chloride 19.6 2.0 ug/L 20.0 98 70-130 Naphthalene 16.8 3.0 ug/L 20.0 84 70-130 n-Butylbenzene 19.3 1.0 ug/L 20.0 97 70-130 n-Propylbenzene 18.5 0.5 ug/L 20.0 93 70.130 o-Xylene 17.3 1.0 ug/L 20.0 87 70-130 sec-Butylbenzene 17.8 0.5 ug/L 20.0 89 70-130 Styrene 19.4 0.5 ug/L 20.0 97 70-130 tert-Butylbenzene 18.9 0.5 ug/L 20.0 94 70-130 Tetrachloroethene 19.6 0.5 ug/L 20.0 98 70-130 Toluene 19.4 0.5 ug/L 20.0 97 70-130 trans-1,2-Dicbloroethene 21.6 0.5 ug/L 20.0 108 70-130 Trichloroethene 22.7 0.5 ug/L 20.0 114 70-130 Vinyl chloride 21.7 0.5 ug/L 20.0 109 60-140 Surrogate: 1,2-Dichloroethane-D4 100 70-130 Surrogate:4-Bromojluorobenzene 87 70-130 Surrogate: Toluene-& 96 70-130 Matrix Spike (B5D0894-MS1) Source: 5040500-11 1, 1, 1 -Trichloroethane 154 10.0 ug/L 200 ND 77 70-130 1,1-Dichloroethane 239 5.0 ug/L 200 34.1 102 70-130 I,l-Dichloroethene 314 5.0 ug/L 200 79.4 117 70-130 1,2,4-Trimethylbenzene 184 5.0 ug/L 200 ND 92 70-130 1,2-Dichloroethane 204 5.0 ug/L 200 ND 102 70-130 Acetone 1410 200 ug/L 1000 ND 141 60-140 sl Benzene 224 5.0 ug/L 200 ND Ill 70-130 Bromometime (Methyl Bromide) 256 20.0 ug/L 200 ND 128 60-140 PO Box 56SS I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom -- an employee -owned company 0412812015 09:13 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 6 of 11 I ORogers &Callcott W ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Volatile Organics Quality Control Summary Reporting Spike Source % RE(RI'D Parameter Result Limit Units Level Result %REC Limits RI'D Limit Flags Batch B5D0894 - EPA 5030 Matrix Spike (B5D0894-MS1) Source: 5040500-11 Chloroform 200 5.0 ug/L 200 ND 100 70-130 cis-1 2-Dichloroethene 213 5.0 ug/L 200 ND 107 70-130 Ethylbenzene 206 5.0 ug/L 200 ND 103 70-130 Hexane 192 10.0 ug/L 200 ND 96 70-130 Isopropylbenzene 192 5.0 ug/L 200 ND 96 70-130 m,p-Xylene 395 10.0 ug/L 400 ND 99 70-130 Methylene chloride 190 20.0 ug/L 200 ND 95 70-130 Naphthalene 168 30.0 ug/L 200 ND 78 70-130 n-Butylbenzene 199 10.0 ug/L 200 ND 100 70-130 n-Propylbenzene 190 5.0 ug/L 200 ND 95 70-130 o-Xylene 172 10.0 ug/L 200 ND 86 70-130 sec-Butylbenzene 181 5.0 ug/L 200 ND 90 70-130 Styrene 194 5.0 ug/L 200 ND 97 70-130 tert-Butylbenzene 193 5.0 ug/L 200 ND 97 70-130 Tetrachloroethene 194 5.0 ug/L 200 ND 97 70-130 Toluene 190 5.0 ug/L 200 ND 95 70-130 trans-1,2-Dichloroethene 219 5.0 ug/L 200 ND 110 70-130 Tichloroethene 232 5.0 ug/L 200 ND 114 70-130 Vinyl chloride 223 5.0 ug/L 200 ND 111 60-140 Surrogate: 1.2-Dichloroethane-D4 105 70-130 Surrogate:4-BromoJluoroben_ene 86 70-130 Surrogate: Toluene-d8 93 70-130 Matrix Spike Dup (BSD0894-MSDI) Source: 5040500-11 1,1,1-Tichloroethane 146 10.0 u9/1, 200 ND 73 70-130 5 20 1,1-Dichloroethane 224 5.0 ug/L 200 34.1 95 70-130 6 20 1,1-Dichloroethene 292 5.0 ug/L 200 79.4 106 70-130 7 20 1,2,4-Trimethylbenzene 174 5.0 ug/L 200 ND 87 70-130 6 20 1,2-Dichloroethane 195 5.0 ug/L 200 ND 98 70-130 4 20 Acetone 1440 200 ug/L 1000 ND 144 60-140 2 20 SI Benzene 210 5.0 ug/L 200 ND 105 70-130 6 20 Bromomethane (Methyl Bromide) 234 20.0 ug/L 200 ND 117 60-140 9 20 Chloroform 196 5.0 ug/L 200 ND 98 70-130 2 20 cis-1,2-Dichloroethene 206 5.0 ug/L 200 ND 103 70-130 3 20 Ethylbenzene 198 5.0 ug/L 200 ND 99 70-130 4 20 Hexane 177 10.0 ug/L 200 ND 89 70-130 8 20 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 I main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com -- an employee -owned company 04,12812015 09:23 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 7 of 11 i Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5D0894 - EPA 5030 Matrix Spike Dup (B5D0894-MSDl) Source: 5040500-11 Isopropylbenzene 185 5.0 ug/L 200 ND 92 70-130 4 20 m,p-Xylene 373 10.0 ug/L 400 ND 93 70-130 6 20 Methylene chloride 187 20.0 ug/L 200 ND 93 70-130 2 20 Naphthalene 178 30.0 ug/L 200 ND 83 70-130 6 20 n-Butylbenzene 193 10.0 ug/L 200 ND 96 70-130 3 20 n-Propylbenzene 183 5.0 ug/L 200 ND 91 70-130 4 20 o-Xylene 169 10.0 ug/L 200 ND 84 70-130 2 20 sec-Butylbenzene 172 5.0 ug/L 200 ND 86 70-130 5 20 Styrene 187 5.0 ug/L 200 ND 93 70-130 4 20 tert-Butylbenzene 180 5.0 ug/L 200 ND 90 70-130 7 20 Tetrachloroethene 185 5.0 ug/L 200 ND 93 70-130 5 20 Toluene 187 5.0 ug/L 200 ND 93 70-130 2 20 trans-1,2-Dichloroethene 204 5.0 ug/L 200 ND 102 70-130 7 20 Trichloroethene 214 5.0 ug/L 200 ND 105 70-130 8 20 Vinyl chloride 214 5.0 ug/L 200 ND 107 60-140 4 20 Surrogate: 1.2-Dichloroethane-D4 99 70-130 Surrogate: 4-Bromofluorobenzene 85 70-130 Surrogate: Toluene-d8 92 70-130 PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 296077 1 main 864.232.1556 1 fax 864.232.6140 rogersandcalleott.com an employee -owned company 0412812015 09:23 This report may not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Page 8 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5040602 Monroe, NC 28110 Reported: 04/28/15 09:23 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference S1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232,6140 rogersandcallcott.com an employee -owned company 0412812015 09:23 This report mnv not be reproduced except in full, without written permission from Rogers & Callcott, Inc. Page 9 of 11 Rooprs 1, CA CHAIN OF CUSTODY RECORD WORK ORDER ENVIRONMENTAL !✓ Filtered (Yes/No) Cooled (Yes/No) Mailing PO Box 5655 Shipping 426 Fairforest Way 215E Stoneridge Drive Container Type Llastic/Glass) Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 �'D Container Volume (ml-) J Client Name ti s Sample Type (Grab/Composite) Address Sample Source (WW, GW, DW, SW, S, Other) qJ Report To: p 0 o Preservation Code(s) Email Address u o A —None E—HCI I — ZnAcetate V B—HNO3 F—Na2S203 J—H3PO4 Telephone# °J N 5) C—H2SO4 G — Boric Add K-MCAA z E D —NaOH H—Ascorbic Acid L- PO # Project # 93-/ Z p n) R&C WORK ORDER YR DATE TIME SAMPLE DESCRIPTION COMMENTS c�-I�1�o►�0l y �� 2-117 1C11J- 50— 3 v f- sJ_' j z��lQT >e, ,, v74 14cL, SO4 OU0 1 -0 1 f 12P - 7Z3 e Zi,I SAMP —reED BY: PAE/TIME: RECEIV BY: DATE/TIME: 1 //s 1632_ 2 Composite Start Date: ,! I Composite Start Time: RELI UIS EDGY: DATE/TIME: RECEI ED Y: DATE/TIME: 3. 4• Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 5. 6. Temperature of blank or representative sample At time of collection °C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7. 8. At time of lab receipt 316 °C Possible Hazards associated with samples: Non -Hazard Flammable ❑Skin Irritant Poison Unknown �ther Form Revised July, 2014 Page of j r Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Date u Work Client: CAReceived: Order: S 0 A p 73�. Carrier Name: Client FedEx Tracking Number: -T T UPS US Mail Courier field Service Other: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)7 Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of hcadspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled? Temp measured with IR thennometer - SN: 97050067 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. V 0 Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot # HCL II3PO4 HISO4 NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by: \ 10 Page 11 of 11 Catalent. May 11, 2015 Catalent Pharma Solutions 2725 Scherer Drive North St. Petersburg, FL 33716 T 727.803.2100 F 727.803.2419 %Ywmcatalent.com Mr. Kyle Ketchum City of Monroe WWTP 775 Treeway Drive Monroe, North Carolina 28110 Subject: Effluent Discharge Report LIUP # LP-001 Treated Groun water Catalent Pharma Solutions (Formerly R. P. Scherer)/Chelsea Laboratories Facility 2021 East Roosevelt Blvd., Monroe, North Carolina 28112 Dear Mr. Ketchum: Enclosed are the April 2015 effluent discharge and laboratory analysis reports for the referenced facility. No non -conformances were reported. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware there are significant penalties for submitting false information, including the possibility of fine or imprisonment for knowing violations. If you have any questions or concerns, please contact Jeffery Rogers at 727-803-2282 (email: Jeffery. Rogers@catalent.com) or Stan Golaski of Rogers & Cailcott at 864-335-4984 (email: stan.golaski@rogersandcalicott.com). Sincerely, Catalent Pharma Solutions Dina K akis V. /lesr,¢,rets General Manager Enclosures OS-/3 Date cc with attachments: Stan Golaski, Rogers & Callcott Environmental Jerry Sullivan, Aqua-Trol (on -site file) Receiving POTW NPDES #: NCO024333 Effective Date for these Limits: 7/1/13 Expiration Date for these Limits: 6/30/16 LIUP #: LP-001 Pipe#: 01 Reporting Period: April 2015 Date & T I ime of Reading Days Between Readings Meter Reading (gal) Weekly Flow (gal) Weekly Average (mgpd)' Tetrachloro- ethene (ug/L) Trichloro- ethene (ug/L) 82603 (ug/L) pH (units) Comments 3123/15 13:00 689,010 4/1/15 7:00 8.75 742,400 53,390 0.006102 4/6/15 13:00 525 776,867 34,467 0.006565 4/14/15 11:30 7.94 824,934 48,067 0.006056 <0.5 <0.5 BRDL 7.8 4/21/15 14:00 7.10 869,480 44.546 0.006270 Sample and pH 4/27/15 10:00 5.83 901,792 32,312 0.005539 collected on April 14,2015. Monthly Total 212,782 Maximum 0.006565 Minimum = 0.005539 Sample Type Grab Grab Grab Grab Permit Limits . . ....... . , - I 0.0100001 8.85 81 1 monitor only 6 to 11 'Flow between Meter Readings 2 Weekly Average = Weekly Flow / Days Between Readings 3 Value represents total 8260 volatile organic compounds. BRDL= Below Reportable Detection Limits 1\3C-VMSRV031Projects114193-121120151RPTS1POTW ReportMApri 2015N April 2015 POTW Form.xisx 5111/2016 Rogers &Callcott ENVIRONMENTAL Client Catatent Pharma Solutions C/O George Maalouf- Rogers and Callcott 2021 F. Roosevelt Blvd. Monroe, NC 29110 Dear Client: Laboratory Report Project: Work Order: Received: Effluent 5040601 04/14/2015 16:32 Rogers and Callcott appreciates the opporttmity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that %vere received on April 14, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard- The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at karahrkach it rogersaodealleott.com or {864}335-4956 if you have any questions about this report. Permit #WQ0010607 Catalent Pharma Solutions/Chelsea Lobs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers mid Callcott Report Approved By: Kae""_ abl* Kara Hrkach Project Manager ]his report may not be reproduced, except in fidl, it !flout it riuen pe»utssion jinni Rogers R Collrott, Im. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 nufn 864.232.1556 1 fax 864.232.6140 rogersalldCallCOtt.001Tf ---- — ----- - -- -- ---- --------------------- an employee onmedcompany 1 Page 1 of 11 Rogers & Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maaiouf - Rogers and Callcott 2021 F. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5040601-01 Effluent Grab QCY.� South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identificallmn 40572 North Carolina Inboralory Certification Number 27 North Carolina Drinking Wetter Lab Nimibcr 45710 NLL4P Utah Certificate Number SC000042014-1 Georgia Dr-inkiug Water Lob /D RS0 Project: Effluent Work Order: 5040601 Received: 04/14/2015 16:32 Matrix Sampled Type Ground Water 04/14/15 12:18 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 rruin 864,232,1556 1 fax 864.232.6140 rogersandcallcott.com ... ... - --. .�_-.__.., ----- --- _.... ...--- ._------------------------- -...._ an employee -owned company 0128,2015 07:07 210s rei vri nta), rot be reproduced., except in fall, tirlttrutrl vriuertlumrisston jram Rogers R Cantor., Inc. Page 2 of 1 t Rogers &Callcott 114",i. ENVIRONMENTAL Catalent Pharnla Solutions Project: Effluent 2021 1- Roosevelt Blvd, Work Order: 5040601 Monroe, NC 28110 Reported: 04/28/15 09:07 Sample Data Sample Number 5040601.01 Sample Description Effluent Grab collected on 04/14/15 12:18 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst hatch Field Parameters pff 7.8 0.1 pit Units 1.00 04/14/15 12:18 EPA 9040C JHF B5110524 Temperature 21.1 0.0 T 1.00 04/14/15 12:19 SM 233OB-2010 JFTF BSD0524 Volatile Organics 1,1,1-Trichloroethane ND 1.0 ugR. L00 04116.115 15:37 EPA 8260B LBW 145DO894 l,l-Dichloroethane ND 0.5 ugQ• I 04/16/15 15:37 EPA 8260B I.BW BSM894 1,1-Dichloroethene ND 0.5 u8R• 1.00 04/16/15 15:37 EPA 8260E LBW B5W894 1,2,4-Tiimethylbenzene ND 0.5 ugQ. 1.00 04116./15 15:37 EPA 8260B LBW BSM894 1,2-Dichloroelhane ND 0.5 ugQ. 1.00 04/16/15 15:37 EPA 9260B Z LBW B51)0894 Acetone ND 20.0 ugR- 1.00 04/16/15 15:37 EPA 8260B LBW B500894 Benzene ND 0.5 ugQ. 1.00 04/16/15 15:37 EPA9260B LBW B500894 Bromomethane (Methyl Bromide) ND 2.0 ugQ. 1.00 04/16/15 15:37 EPA 8260E LBW B51x1894 Chloroform ND 0.5 ug/l• 1.00 04/16/15 15:37 EPA 8260B LBW B5W894 cis-1,2-Dicliloroethene ND 0.5 ugQ. 1.00 04/16/15 15:37 EPA 8260B I.BW B5D0894 Ethylbenzene ND 0.5 ug/L 1.00 04/16/15 15:37 EPA 8260E I.BW B5110894 Hexane ND 1.0 ug/L 1.00 04/16/15 15:37 EPA9260B 1.BW B5130894 lsopropylbenzene ND 0.5 ug/L 1.00 04/16/15 15:37 EPA 8260B LBW B51X1894 ni,p-\ylene ND LO ug/L. 1.00 04/16/15 15:37 EPA 8260B 1.13W BSD0894 Methylene chloride ND 2.0 ug/L 1,00 04/16/15 15:37 EPA8260B LBW B5D0894 Naphthalene ND 3.0 ug/L 1.00 04/16/15 15:37 EPA 8260B LBW B5D0894 n-Butylbenzene ND 1.0 ug/L 1.00 04/16/15 15:37 EPA 8260B LBW BSD0894 n-Propylbenzene ND 0.5 ug/L 1.00 04/16/15 15:37 EPA$26013 LBW ➢5130894 o-Xylene ND 1.0 ug/L 1.00 04/16/15 15:37 EPA3260D LBW B5130894 sec-Butylbenzene ND 0.5 ug/L 1.00 04/16115 15:37 EPA8260B LBW B5D0894 Styrene ND 0.5 ug/L 1.00 04/16/15 15:37 EPA 8260B LBW B5130894 lert-Butylbenzene ND 0.5 ugQ. 1.00 04/16/15 15:37 EPA8260D LBW BSD0894 Tetrichloroethene ND 0.5 ug/L 1.00 04/16/15 15:37 EPA 8260B LBW B5D0894 Toluene ND 0.5 ug/L 1.00 04116//5 15:37 EPA 8260D LBW BSD0894 trans-1,2-Dichloroethene ND 0.5 ugQ• 1.00 04116!15 15:37 EPA 82608 LBW 135WS94 Trichloroethene ND 0.5 ugQ. 1.00 04/16/15 15:37 EPA 8260E LBW B5130894 Vinyl chloride AID 0.5 ugQ. 1.00 04116/15 15:37 EPA8260H %a LBW BSD0894 Surrogates %RF.0 %REC Limits Flag 1, 2-Dichloroethrnk-D4 91 70-130 4-Rramjlrmroheruene 92 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 nuin 864.232.1556 I. (ax 864.232.6140 rogersandcallcott.com --------- an an employee -owned company 04.28,2015 09.07 This report stay not he reprauat( except infull. without trrittenpormission front Rogersk Callcott, Irk. Page 3 0111 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5040601 Monroe, NC 28110 Reported: 04/28/15 09:07 Sample Number 5040601-01 Sample Description Effluent Grab collected on 04/14/15 12:18 Reporting Parameter Result Unvit Units DF Anal)ztd Alelhod Flag Analyst Batch Volatile Organics Surrogates %REC %RECLimits Flag 7ohrene-d4 86 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 ' main 864.232.1556 1 iax 864.232.6140 rogersandcall eott.com an employee -owned company 01 ,28.2015 09:07 ThJs r<7wr1 may twl be reproJuce<1, excepl in full, ultleonl irrrrten perntisslmt jram Rogers X Calkolt, Irk. Page 4 of 11 l 4: Rogers & Callcott !I I� ENVIRONMENTAL Cataleut Pharma Solutions Project: Effluent 2021 F. Roosevelt Blvd. Work Order: 5040601 Monroe, NC 28110 Reported: 04/28/15 09:07 Volatile Organics Quality Control Sun1»lary Reporting Spike Source %REC RPD parameter Result Limit Units Level Result %REC rJmits RPD Lindt Flags Batch B5D0894 - EPA 5030 Blank (B5D0894-BI,KI) 1,1,1-Trichlorotthane ND 1.0 ug/L 7,4Dichloroctlmc ND 0.5 ug/L 1J.Dichloroalicne ND 0.5 ug/L 1,2,4-Tritnethylbenzene ND 0.5 ug/l. 1,2-Dichloroethane ND 0.5 ug/L Acctonc NO 20.0 ug/L Benzene ND 0.5 ug/L Drotnomethane (Methyl Bromide) ND 2.0 ug/L Chlorofortu ND 0.5 ug/L cis-1,2-Dichloroethene ,W 0.5 ug/L E(hylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/1 Isoptopylbenzene ND 0.5 ug/L m,p-Xylene ND 1.0 ug/L hlethylene chloride ND 2.0 ug/L Naphthalene ND 3.0 ug/L n-Butylbenzene ND 1.0 ug/L n-Prop)lbenzene ND 0.5 uga. aXylene ND 1.0 ug/l. sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbcnzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/l. Toluene ND 0.5 118/1, trans-1,2-I31chloroediene ND 0.5 ug/L Trichlorocthene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate: 1, 2-Dichlonudme-Dd Surrogate: 4-BramoJl uorohenzew Surrogate: 2'alueim-d8 LCS (B5D0894-BSI) 88 70-130 90 70-130 86 70-130 1,1,1-Trichloroethane 15.6 1.0 ug4, 20,0 78 70-130 l.l-Dichtotoethane 19.9 0.5 ug/L 20.0 100 70.130 1,1-Dichlorocthtne 23.8 0.5 ug/L 20.0 119 70-130 1,2,4-Triniethylbenzene 18.3 0.5 ug/L 20.0 91 70-130 PO Box 56S5 I Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 twin 864.232.1556 i fax 864.232.6140 rogersandcallcott.com anemployee-awned company 04-28 2015 09:07 This report nuror not he repnxhuno� except in full, without a ritten pomiisslon from Rogers R 0dicati, Ine. Page 5 of 11 Rogers & Callcott ENVIRONMENTAL Cataletit Pharina Solutions Project: Effluent 2021 F. Roosevelt Blvd. Work Order: 5040601 Monroe, NC 28110 Reported: 04/28/15 09:07 Volatile Organics Quality Control Sunimary Reporting Spike Source •/.REC RPD Parameter Result Lintit Units Level Result •/.REC Umits RPD Limit Flags Batch B5D0894 - EPA 5030 LCS (B5D(31894-BSI ) 1,2-Dichlorocthanc 19.8 0.5 ug/L 20.0 99 70.130 Acetone 136 20.0 ug/L 100 136 60-140 Benzene 21.4 0.5 ug/L 20.0 107 70-130 Bromomethane (,Methyl Bromide) 25.0 2.0 ug/L 20.0 125 60-140 Chloroforro 20.0 0.5 u9/1. 20.0 100 70.130 cis-1,2-Dichloroethene 22.3 0.5 ug/L 20.0 112 7D-130 Ethylbenzene 20.4 0.5 ug/L 20.0 102 70-130 Hexane 18.4 1.0 ug/L 20.0 92 7D-130 tsopropylbenzene 19.2 D.5 U94- 20.0 96 70.130 m,p-Xylene 40.8 LO ug/I. 40.0 102 70.130 hiethylene chloride 19.6 2.0 ug/L 20.0 98 70.130 Naphthalene 16.8 3.0 ug/L 20.0 84 70-130 n-Butylbenzene 19.3 LO ug/L 20.0 97 70-130 n-Propylbenzene 18.5 D.5 119/1. 20.0 93 70-130 o-Xylcne 17.3 1.0 ug/L 20.0 87 70.130 sec-Butylbenzene 17.8 0.5 ug/L 20.0 89 70-130 Styrene 19.4 0.5 ug/L 20.0 97 70-130 tert-Butplbenzene 18.9 0.5 uZIL 20.0 94 70-130 Tetrachloroethene 19.6 0.5 ug/L 20.0 98 70-130 Toluene 19.4 0.5 ug/L 20.0 97 70-130 trans-1,2-Dlchloroctbene 21.6 0.5 ug/L 20.0 103 70-130 Trichloroethene 22.7 0.5 ug/L 20.0 114 70-130 Vinyl chloride 21.7 0.5 ug/L 20.0 109 60-140 Surrogate: 42-Dichlorow1hruK-DI 100 70-130 Surrogate: f-Brontufuoroben2ew, 87 70-130 Surrogate: Toluetx-M 96 70-130 Matrix Spike (B5130894-51S1) Source: 5040500-11 41,11-Trichlorocthanc 154 10.0 ug/l. 200 NO 77 70-130 1,1-Dichlotoethane 239 5.0 ug/L 200 34.1 102 70-130 1,1-Dichlorathene 314 5.0 ug/L 200 79.4 117 70-130 1,2,4 Trunethylbenzene 194 5.0 ug/L 200 NO 92 70-130 1,2-Dichtoroethane 204 5.0 ug/L 200 NO 102 70-130 Acetone 1410 200 ug/t. 1000 NO 141 60-140 SI Benzene 224 5.0 ug9. 200 ND 112 70-130 Broniontethme (,Methyl Bromide) 256 20.0 ug/L 200 NO 128 63440 PO Box 56S5 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 msin 664.232.IS56 I fax 864.232.6140 rogersandcallcott,com --------an employee -owned company 01,28,2015 09: 07 Tilts report twgj not be reprrulueeri, except in full, n ilhout i rillen p milesiou front Rogan & Calleotl Ere. Page 6 of 11 { Rogers & Callcott _ ENVIRONMENTAL Calaleut Pharnla Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5040601 Monroc, NC 28110 Reported: 04/28/15 09:07 Volatile Organics Quality Cot►trol Summaiy Reporting Spike Source %ILEC lull) Pammeter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5D0894 - EPA 5030 Matrix Spike (DSD0894-NISI) Source: 5040500-11 Chloroform 200 5.0 ugH. 200 ND 100 70-130 cis-1,2-Dichloroethene 213 5.0 ug/l. 200 ND 107 70.130 Ethylbenzene 206 5.0 ug/L 200 ND 103 70.130 litxane 192 10.0 ug/L 200 ND 96 70-130 Isopropylbenzene 192 5.0 ug2 200 ND 96 70-130 m,p \ylenc 395 10.0 ug/f. 400 ND 99 70-130 \lethylene chloride 190 20.0 ug/L 200 ND 95 70-130 Naphthalene 169 30.0 1192 200 ND 78 10-130 n-Butylbenzene 199 10.0 ug/L 200 ND 100 70-130 n-Propylbenzene 190 5.0 u92 200 ND 95 70-130 o-\ylene 172 10.0 ug2 200 ND 86 70-130 sec-Dutylbenzcne 181 5.0 ug/L 200 ND 90 70-130 Styrent 194 5.0 ug/L 200 NO 97 70-130 tort-Butylbenzene 193 5.0 ug/L 200 ND 97 70-130 Tetrachlorocthene 194 5.0 ug2 200 ND 97 70-130 Toluene 190 5.0 ug/l. 200 ND 95 70-130 (rans-1,2-Dichloroelhene 219 5.0 ug/L 200 ND 110 70.130 Trichloroethene 232 5.0 ug/L 200 ND 114 70-130 Vinyl chloride 223 5.0 ug/L 200 ND 111 60.140 Surrogate: 1,2-Dichloroedxnk-D4 105 70-130 Surrogate:4-Bromofluorobearene 86 70-130 Surrogate: Toluene-& 93 70-130 hlatri-c Spike Dup (135D0894-DISDI) Source: 504050D-ll 1,1,1-Trichloroethaoe 146 10.0 ug/L 200 ND 73 76d30 5 20 1,1-Dichlorocthane 224 5.0 ugR. 200 34.1 95 70-130 6 20 1,1-Dichlormthene 292 5.0 ug/L 200 79.4 106 70-130 7 20 1,2,4-Trimethylbenzene 174 5.0 USA- 200 ND 87 70-130 6 20 1,2-f)lehleroetbane 195 5.0 ug/l, 200 ND 98 70-130 4 20 Acetone 1440 200 ug2 1000 ND 144 60.140 2 20 S1 Benzene 210 5.0 ug/L 200 ND 105 70.130 6 20 Brornomethme(Methyl Bromide) 234 20.0 ug2 200 ND 111 60.140 9 20 Chloroform 196 5.0 u92 200 ND 98 70.130 2 20 cis-1,2-Dichloroethene 206 5.0 u82 200 ND 103 70-130 3 20 Eihylbenzcne 198 5.0 ug/l. 200 ND 99 70-130 4 20 Hexanc 177 10.0 ug/L 200 ND 89 70-130 8 20 PO Box 56S5 1 Greenville, SC 29606 1 426 Fairforesc Way 1 Greenville, SC 29607 main 864.232.1556 1 fax 864.232.6140 rogersandcalicott.com --- -- ------- -- - -- _._.._,__.. ------. - - - ---- ---- - an employee -owned company 041S,2015 09:07 Tbir rrport maj awl he reproduced, ercrpl in jdl, u•illaut a riltcn lvmission from Rogers 8• Callcoq Inc. Page 7 of 11 Rogers &Callcott ENVIRONMENTAL Catalent P1lanua Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5040601 Monroe, NC 29110 Reported: 04/28/15 09:07 Volatile Organics Quality Conh•01 Sunullary Reporting Spike Source % REC RFD Parameter Result Linttt Units Level Result %REC Limits RID Limit Flags --] Batch B5D0894 -)CPA, 5030 Matrix Spike Dup (115D0894-DISDI) Source: 5040500-11 lsopropylbenzene 185 5.0 ugll. 200 ND 92 70.130 4 20 nt,p-Xylene 373 10.0 ug/l. 400 ND 93 70-130 6 20 hlethylenc chloride 187 20.0 uglL 200 Nll 93 70-130 2 20 Naphthalene 178 30.0 ug/L 200 ND 83 70-130 6 20 n-Butylbenzene 193 10.0 ug/L 200 ND 96 70-130 3 20 n-PropyIbenzene 183 5.0 ug/L 200 ND 91 70-130 4 20 o-\ylcne 169 10.0 ug/I. 200 ND 84 70.130 2 20 sec-Butylbcnzene 172 5.0 ug/L 200 ND 86 70-130 5 20 Styrene 187 5.0 ug/L 200 ND 93 70-130 4 20 tort-Butylbenzene 180 5.0 ug/L 200 ND 90 70-130 7 20 Tetrachloroethene 185 5.0 ttg9. 200 ND 93 70-130 5 20 Toluene 137 5.0 ug/1. 200 ND 93 70.130 2 20 trans-1,2.Dichloroethene 204 5.0 ug/L 200 NO 102 70-130 7 20 Trichlaroethene 214 5.0 ug/L 200 ND 105 70430 8 20 Vinyl chloride 214 5.0 ug/L 200 ND 107 60-140 4 20 Surrogate: 1,2-Dialrloraedw ne-DI Surrogale: a-BroaroJluorobenzene Surrogare: ToluenrdS 99 70-130 85 70-730 92 70-130 PO Box 5655 i Greenville, SC 29606 1 426 Fairtorest Way I Greenville, SC 29607 1 main 864.232.1556 j fax 864.232.6i40 rogersandcallcott.conl an employee -owned company 0l48,2015 09:07 17iis rapvrr raa}• rwl be rrpralucr� rcrcapt to full, n idwur u•rtuaaDrrmisslat from Rogan r( Callcatl, Lx. Page 8 of 1 i Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 F. Roosevelt Blvd. Work Order: 5040601 Monroe, NC 28110 Reported: 04/28/15 09:07 Data Qualifiers and Definitions ND Analyte N07' DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference Sl 'rhe matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. 'rhe Laboratory Cmitcol Sample (LCS) was within control limits. Z A4DL is 0,17 ug/L - No peaks detected Za hiDL is 0.18 ug/L - No peaks detected PO Sox 5655 1 Greenville, SC 29606 1 426 fairforest Way I Greenville, SC 29607 1 mein 864,232.1556 1 fax 864.232.6140 t'OgersandcallcomcOm --- .-_. — ------ - --- ----- - ---._._.__._.-. ---- -._- — -- -- --- - -- ---- an employee -owned company 04,28,2013 09.07 Aels reporttruo, not he reproduced, except in jAl, without a ritten permission front Rogers & Calicoll, Irn. Page 9 of 11 v n 0 0 UJ Rogers &.Cakott CHAIN ENVIRONMENTAL Mailing PO Box 5655 Shipping 426 Falrforest Way 215BStoneridge Drive Address: GreenvOle,SC29606 Address: Greenville, SC29607 Columbia,SC29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 d ) Client Name �(� Address p �C Report Email Address Telephone #? PO # Project # 93-1 Z- 1 OF CUSTODY RECORD WORK ORDER v c m o u v E v E [✓ filtered Yes/No) Cooled (Yes/No) ContalnerType(Plastic/Glass) 1/0� p Container Volume {mL} iT Sample TypeLGrab/Composite) Sample Source (NMI, GW, DW, SW, S, Other) Preservation Code(s) A —None E—Hq I—ZnAcetate B—HNO3 F—NazSiO3 J—HaPO4 C — HxSO< G — Boric Acid K - MCAA D—NaOH H—Ascorbic Add L- v M R & C WORK ORDER YR DATE TIME SAMPLE DESCRIPTION COMMENTS rJ�l�teol--o1 y m I lZa /,J_ 03 V/ _ r1<' � / 1 Sew fah �L og OUo1- } G4.P-7q.3021.1�C SAMP rED BY: 1. PATE/TIME: / /s / 63 Z. RECEIV BY: a. DATE/TIME: .1 .r Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: RELIN UIS ED BY: 3. DATE/TIME: RECEI ED Y: 4• DATE/TIME. RELINQUISHED BY: S. DATE/TIME: RECEIVED BY: 6. DATE/T1ME: Temperature of blank or representative sample At time of collection °C At time of lab receipt 31% -C RELINQUISHED BY: 7, DATE/TIME: RECEIVED BY: B. DATE/TIME: Possible Hazards associated with samples: UqNon-Hazard ❑FI minable 1:11cinlrritant ElPolson Elldnkmmn ❑Other Form Revised July,2014 Page I of i Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Date Work Client: Received: Order: '5Cg0U0 j Carrier Name: Client FedRx UPS US Mail Courier Qield Services Other: Tracking Number: Receipt Criteria Y c s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? x VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on Coe Samples Booted? Temp measured with 1R thermometer - SN: 47050M7 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the tab. fit' Samples dech[orinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot N HCL 1ip04 H2SO4 NaOH HNO,3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other titan noted above: —� Revised July 2014 Completed by: page 11 of 11 Rogers and Callcott Environmental Client: Date: Field Meter Calibration Record i Conductivity Calibration - EPA 9050A Meter Make / Model: Orion Star A325 SN: : %2.76G Probe: Time: Analyst: Cell Constant Conc. of Standard, Actual Reading of Standard, 25"C µmhos/cm @ Temperature, "C SSS Conc: Temperature compensation for pH / conductivity meter: pH Calibration.- EPA 9040C Meter Make / Model, Orion Star A325 Probe: Time: 025 5 Analyst: -1574.1` Slope: Tj0,3 Chemical inventory Conc. of Buffer, units Actual Reading of Buffer, units 561b 4.0 r o2- 5$/ 7.0 71c3 50/ v Y 10.0 >6.63 P%63'-1 y SSS conc: 7,o Tlroo Turbidity Meter Calibration. Field Screen Method Meter Make / Model: Hach 2100P SN: Date of most recent calibration: Tir ie: Analyst: Chemical Inventory Assigned Conc. of Standard, j Actual Reading of Standard, I NTu Reviewed by: Date: Revised 01/21/13 Rogers and Callcott Environmental Client: Date:J15%lS Continuing Calibration Verification Conductivity. Meter EPA 9050A Meter Make / Model: Orion Star A325 SN: 4-0 7-706 Probe: Time Analyst Conc. of Standard, Actual Reading of Standard, µmhos/cm @25°C µmhos/cm @ °C 'C PH Meter EPA 9040C. Meter Make/ Model: Orion StarA325 Probe: GZ ! Time Analst y Conc. of Buffer, units Actual Reading of Buffer, units , c,2 Meter Make / Model: Hach 2100P Well ID: Turbidity Meter. Field Screen Method SN: Time Assigned Conc. of Standard, Actual Reading of Standard, NTU Field Duplicate Time Analyst Conductivity, pH, Turbidity, Temperature, µmhos/cm units NTU °C 12 �� Sir- h- 7 59 14 1,tom Note: Refer to daily calibration log for Instrument calibration and chemical inventory information / documentation. Reviewed by: Date: Revised 01/21/23 Catalent_ 10, April 9, 2015 Catalent Pharma Solutions 2725 Scherer Drive North St. Petersburg, FL 33716 T 727.803.2100 F 727.803.2419 w%mcatalent.com Mr. Kyle Ketchum City of Monroe WWTP 775 Treeway Drive Monroe, North Carolina 28110 Subject: Effluent Discharge Report LIUP # LP-001 Treated Groun water Catalent Pharma Solutions (Formerly R. P. Scherer)/Chelsea Laboratories Facility 2021 East Roosevelt Blvd., Monroe, North Carolina 28112 Dear Mr. Ketchum: Enclosed are the March 2015 effluent discharge and laboratory analysis reports for the referenced facility. No non -conformances were reported. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware there are significant penalties for submitting false information, including the possibility of fine or imprisonment for knowing violations. If you have any questions or concerns, please contact Jeffery Rogers at 727-803-2282 (email: Jeffery. Rogers@catalent.com) or Stan Golaski of Rogers & Callcott at 864-335-4984 (email: stan.golaski@rogersandcallcott.com). Sincerely, Catalent Pharma Solutions Dina Kost kis A —*A V. Date General Manager Enclosures cc with attachments: Stan Golaski, Rogers & Callcott Environmental Jerry Sullivan, Aqua-Trol (on -site file) Receiving POTW NPDES #: NCO024333 Effective Date for these Limits: 7/1/13 Expiration Date for these Limits: 6/30/16 LIUP #: LP-001 Pipe #: 01 Reporting Period: March 2015 Date &Time of Reading Days Between Readings 9 Meter Reading (gal) Weekly Flow 1 (gal) Weekly Average 2 (mgpd) Tetrachloro- ethene u /L (9 ) Trichloro- ethene u /L (9 ) 3 8260 (ug/L) pH (units) Comments 2/23/15 17:00 10,739,232 3/3/1511:00 7.75 10,760,502 21,270 0.002745 3/6/1510:30 2.98 10,776,193 15,691 0.005267 <0.5 <0.5 BRDL 7.9 3/9/15 12:00 3.06 10,796,843 20,651 0.006743 3/17/15 12:30 8.02 10,847,079 50,236 0.006263 Sample and pH 3/23/1513:00 6.02 689,010 39,250 0.006519 collected on March 6, 2015. Monthly Total 147,097 Maximum 0.006743 Minimum 0.002745 Sample Type Grab Grab Grab Grab Permit Limits 0.010000 8.85 81 monitor onlv 6 to 11 Flow between Meter Readings 2 Weekly Average = Weekly Flow / Days Between Readings 3 Value represents total 8260 volatile organic compounds. BRDL= Below Reportable Detection Limits Calibrated city effluent meter was installed on March 17, 2015. Reading at time of installation was 649,760. \\RC-VMSRV03\Projects\14\93-121\2015\RPTS\POTW Reports\March 2015\ March 2015 POTW Form.xlsx 4/9/2015 Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf- Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Laboratory r?y .der -vices Effluent 5030280 03/06/2015 15:08 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on March 06, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit NW00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: r ) a e, C///p /0 61� Kara Hrkach Project Manager This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. PO Box 5655 I Greenville, SC 29606 ; 426 Fairforest Way Greenville, SC 29607 main 864.232-1556 fax 864.2316140 rogersandeallcott.com -- an employee -owned company Page 1 of 11 Rogers & Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5030280-01 Effluent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Effluent Work Order: 5030280 Received: 03/06/2015 15:08 Matrix Sampled Type Ground Water 03/06/15 11:45 Grab PO Box 5655 1 Greenville, SC 29606 ; 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 fax 864,232.6140 rogersarldeallcott.com __ ..._ an employer owned company 03 27 2015 09:49 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 2 of 11 Rogers & Callcott ENVIRONMENTAL. Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Sample Data Sample Number 5030280-01 Sample Description Effluent Grab collected on 03/06/15 11:45 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 7.9 0.1 pH Units 1.00 03/06/15 11:45 EPA 9040C JHF BSCO250 Temperature 15.3 0.0 oC 1.00 03/06/15 11:45 SM255OB-2010 JHF B5CO250 Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 1,1-Dichloroethane ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW BSCO729 1,1-Dichloroethene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 1,2-Dichloroethane ND 0.5 u8/1- 1.00 03/13/15 11:58 EPA 8260B Z LBW B5C0729 Acetone ND 20.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Benzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW BSCO729 Chloroform ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260E LBW B5C0729 Ethylbenzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 9260B LBW B5C0729 Hexane ND 1.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW BSC0729 Isopropylbenzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 m,p-Xylene ND 1.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW BSCO729 Methylene chloride ND 2.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Naphthalene ND 1.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 n-Butylbenzene ND 1.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 n-Propylbenzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 o-Xylene ND 1.0 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW BSC0729 sec-Butylbenzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW BSCO729 Styrene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 tert-Butylbenzene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Tetrachloroethene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Toluene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260E LBW B5C0729 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Trichloroethene ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B LBW B5C0729 Vinyl chloride ND 0.5 ug/L 1.00 03/13/15 11:58 EPA 8260B Za LBW B5C0729 Surrogates % REC % REC Limits Flag 1,2-Diehloroethane-D4 85 70-130 4-BromoJluorobenzene 110 70-130 PO Box 5655 1 Greenville, SC 29606 426 Fairtorest Way Greenville, SC 29607 main 864.232.1556 fax 864,2326140 rogersandeallcott,com - an empInypp owniod company 03,12712015 09:49 This report may not be reproduced, except infull, without written permission from Rogers & Callcott, Inc. Page 3 of 11 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Sample Number 5030280-01 Sample Description Effluent Grab collected on 03/06/15 11:45 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC % REC Limits Flag Toluene-d8 97 70-130 Po Box 5655 1 Greenville, SC 29606 426 Fair forest Way Greenville, SC 29607 1 main 864.232.1S56 tax 864,232.6140 rogersandealleott.eom -- —.— an employee.owned company 0312712015 09: 49 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 4 of 11 #� Rogers & Ca«cott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Fags Batch B5C0729 - EPA 5030 Blank (B5C0729-BLK1) 1,1,1-Trichloroethane ND 0.5 ug/L l,l-Dichloroethane ND 0.5 ug/L l,l-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 2.0 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Etylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L lsopropylbenzene ND 0.5 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 1.0 ug/L n-Butylbenzene ND 1.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 1.0 ug/L sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate: 1,2-Diehloroedume-D4 81 70-130 Surrogate: 4-Bromgfluorobenzene 112 70-130 Surrogate: Toluene-& 96 70-130 LCS (B5C0729-BSI) 1,1,1-Trichloroethane 15.9 0.5 ug/L 20.0 80 70-130 1,1-Dichloroethane 17.4 0.5 ug/L 20.0 87 70-130 1,1-Dichloroethene 21.8 0.5 ug/L 20.0 109 70-130 1,2,4-Trimethylbenzene 22.9 0.5 ug/L 20.0 115 70-130 PO Box 5655 I Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.2321556 fix 864,232.6140 rOgerSandcallcott.cOm an employee owned company 0312712015 09:49 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 5 of 11 Rogers &Callcott j ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5C0729 - EPA 5030 LCS (B5C0729-BS1) 1,2-Dichloroethane 19.6 0.5 ug/L 20.0 98 70-130 Acetone 113 20.0 ug/L 100 113 60-140 Benzene 18.6 0.5 ug/L 20.0 93 70-130 Bromomethane (Methyl Bromide) 23.3 2.0 ug/L 20.0 116 60-140 Chloroform 17.8 0.5 ug/L 20.0 89 70-130 cis-1,2-Dichloroethene 21.9 0.5 ug/L 20.0 110 70-130 Ethylbenzene 19.4 0.5 ug/L 20.0 97 70-130 Hexane 20.1 1.0 ug/L 20.0 101 70-I30 Isopropylbenzene 20.0 0.5 ug/L 20.0 100 70-130 m,p-Xylene 41.3 1.0 ug/L 40.0 103 70-130 Methylene chloride 17.1 2.0 ug/L 20.0 85 70-130 Naphthalene 17.3 LO ug/L 20.0 86 70-130 n-Butylbenzene 19.4 1.0 ug/L 20.0 97 70-130 n-Propylbenzene 21.6 0.5 ug/L 20.0 108 70-130 o-Xylene 21.0 1.0 ug/L 20.0 105 70-130 sec-Butylbenzene 22.6 0.5 ug/L 20.0 113 70-130 Styrene 20.8 0.5 ug/L 20.0 104 70-130 tert-Butylbenzene 22.1 0.5 ug/L 20.0 111 70-130 Tetrachloroethene 19.1 0.5 ug/L 20.0 96 70-130 Toluene 21.3 0.5 ug/L 20.0 106 70-130 trans-1,2-Dichloroethene 19.4 0.5 ug/L 20.0 97 70-130 Trichloroethene 18.8 0.5 ug/L 20.0 94 70-130 Vinyl chloride 20.5 0.5 ug/L 20.0 102 60-140 Surrogate:l,2-Dichloroethane-D4 100 70-130 Surrogate:4-BromoJluorobenzene 102 70-130 Surrogate: Toluene-& 104 70-130 Matrix Spike (B5C0729-MS1) Source: 5030410-05 1,1,1-Trichloroethane 198 5.0 ug/L 200 40.5 79 70-130 1,1-Dichloroethane 305 5.0 ug/L 200 155 75 70-130 1,1-Dichloroethene 690 5.0 ug/L 200 576 57 70-130 Sl 1,2,4-Trimethylbenzene 247 5.0 ug/L 200 ND 123 70-130 1,2-Dichloroethane 200 5.0 ug/L 200 ND 98 70-130 Acetone 1120 200 ug/L 1000 ND 112 60-140 Benzene 200 5.0 ug/L 200 ND 100 70-130 Bromomethane (Methyl Bromide) 232 20.0 ug/L 200 ND 116 60-140 PO Box 56SS i Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.iS56 fax 864.232-6140 rogersandealleott.com an employee -owned company 03/17/2015 09:49 This report may not be reproduced except in full, without written permission from Rogers & Callcott, Inc. Page 6 of 11 IW9�x Rogers &Callcott Z ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Volatile Organics Quality Control Summary Reporting Spike Source %RE ( RI'D Parameter Result Limit Units Level Result %REC Limit, RI'D Limit lla,s Batch B5C0729 - EPA 5030 Matrix Spike (B5C0729-MSI) Source: 5030410-05 Chloroform 192 5.0 ug/L 200 ND 96 70-130 cis-1,2-Dicbloroethene 213 5.0 ug/L 200 ND 102 70-130 Ethylbenzene 204 5.0 u9/1. 200 ND 102 70-130 Hexane 167 10.0 ug/L 200 ND 83 70-130 Isopropylbenzene 199 5.0 ug/L 200 ND 100 70-130 m,p-Xylene 423 10.0 ug/L 400 ND 106 70-130 Methylene chloride 190 20.0 ug/L 200 ND 86 70-130 Naphthalene 184 10.0 ug/L 200 ND 92 70-130 n-Buylbenzene 219 10.0 ug/L 200 ND Ito 70-130 n-Propylbenzene 245 5.0 ug/L 200 ND 122 70-130 o-Xylene 228 10.0 ug/L 200 ND 114 70-130 sec-Buylbenzene 240 5.0 ug/L 200 ND 120 70-130 Styrene 213 5.0 ug/L 200 ND 106 70-130 tert-Butylbenzene 225 5.0 ug/L 200 ND 113 70-I30 Tetrachloroethene 193 5.0 ug/L 200 ND 94 70-130 Toluene 219 5.0 ug/L 200 ND 109 70-130 trans-1,2-Dichloroethene 185 5.0 ug/L 200 ND 93 70-130 Trichloroethene 272 5.0 ug/L 200 117 77 70-130 Vinyl chloride 204 5.0 ug/L 200 ND 102 60-140 Surrogate: 1,2-Diehloroethane-D4 101 70-130 Surrogate: 4-Bromofluorobenzene 111 70-130 Surrogate: Toluene-& 105 70-130 Matrix Spike Dup (B5C0729-MSD1) Source: 5030410-05 1, 1, 1 -Trichloroethane 193 5.0 ug/L 200 40.5 76 70-130 3 20 1,1-Dichloroethane 287 5.0 ug/L 200 155 66 70-130 6 20 S1 1,1-Dichloroethene 629 5.0 ug/L 200 576 26 70-130 9 20 SI 1,2,4-Trimethylbenzene 242 5.0 ug/L 200 ND 121 70-130 2 20 1,2-Dichloroethane 195 5.0 ug/L 200 ND 95 70-130 3 20 Acetone 1130 200 ug/L 1000 ND 113 60-140 0.5 20 Benzene 178 5.0 ug/L 200 ND 89 70-130 12 20 Bromomethane (Methyl Bromide) 214 20.0 ug/L 200 ND 107 60-140 8 20 Chloroform 179 5.0 ug/L 200 ND 90 70-130 7 20 cis-1,2-Dichloroethene 210 5.0 ug/L 200 ND 100 70-130 2 20 Ethylbenzene 192 5.0 ug/L 200 ND 96 70-130 6 20 Hexane 165 10.0 ug/L 200 ND 82 70-130 1 20 PO Box 5655 1 Greenville, SC 29606 ; 426 Fair(orest Way Greenville. SC 29607 ' main 864.232.IS56 fax 864,232.6140 rogersandeallcott.eom an employee -owned company 03,12712015 09:49 This report may not be reproduced, except in full, without written permission from Rogers & Callcoll, Inc. Page 7 of 11 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Volatile Organics Quality Control Summary Reporting Spike Source %REC RI'11 Parameter Result Limit Units Level Result %REC Limits Rill) Limit Fla�s Batch B5C0729 - EPA 5030 Matrix Spike Dup (B5C0729-MSDI) Source: 5030410-05 Isopropylbenzene 193 5.0 ug/L 200 ND 96 70-130 3 20 m,p-Xylene 398 10.0 ug/L 400 ND 100 70-130 6 20 Methylene chloride 180 20.0 ug/L 200 ND 81 70-130 6 20 Naphthalene 201 10.0 ug/L 200 ND 100 70-130 9 20 n-Butylbenzene 207 10.0 ug/L 200 ND 104 70-130 6 20 n-Propylbenzene 233 5.0 ug/L 200 ND 116 70-130 5 20 o-Xylene 213 10.0 ug/L 200 ND 106 70-130 7 20 sec-Butylbenzene 234 5.0 ug/L 200 ND 117 70-130 2 20 Styrene 208 5.0 ug/L 200 ND 104 70-130 2 20 tert-Butylbenzene 223 5.0 ug/L 200 ND 112 70-130 1 20 Tetrachloroethene 182 5.0 ug/L 200 ND 89 70-130 6 20 Toluene 210 5.0 ug/L 200 ND 105 70-130 4 20 trans-1,2-Dichloroethene 174 5.0 ug/L 200 ND 87 70-130 6 20 Trichloroethene 249 5.0 ug/L 200 117 66 70-130 9 20 SI Vinyl chloride 195 5.0 ug/L 200 ND 98 60-140 5 20 Surrogate:l,2-Dichloroethane-D4 95 70-130 Surrogate:4-BromofJuoroben_ene 109 70-130 Surrogate: Toluene-& 103 70430 PO Box 5655 I Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 fax 864,232.6140 rogersandcaIICott.Co171 -- - in ernployee•owned company 0312712015 09: a9 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 8of11 Rogers & Callcott ENVIRONMENTAL. Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5030280 Monroe, NC 28110 Reported: 03/27/15 09:49 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference S 1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. Z MDL is 0. l7ug/L - No peaks detected Za MDL is 0.18ug/L - no peaks detected PO Box 56S5 I Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 , main 864.232.IS56 %u 864,232.6140 rogersandealleott.eom — an employee -owned company 03 27 2015 09: 49 This report mqy not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 9 of 11 Rogers &Callcott CHAIN ENVIRONMENTAL Mailing PO Box 5655 Shipping 426 Fairforest Way 215E Stoneridge Drive Address: Greenville, SC 29696 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Client Name ��+++ Address A oe 1I/C— ReportTo: Email Address Telephone# PO # Project # 93-) 2,) OF CUSTODY RECORD WORK ORDER c 'ro o u o n E z p H Li cu E ro Filtered (Yes/No) y Cooled Les/No) G— Container Type LPlastic/Glass) 'yo Container Volume (mQ 6— Sample Type Lrab/Composite) v✓ Sample Source (WW, GW, DW, SW, S, Other) i Preservation Code(s) A— None E—HCI 1—ZnAcetate B—HNO3 F—Na2S203 J—H3PO4 C—H2SO4 G—Boric Acid K-MCAA D — NaOH H —Ascorbic Acid L - p (. ? a tl R&C WORK ORDER YRJ— DATE TIME SAMPLE DESCRIPTION COMMENTS • — izv j 1/1f71� G q, o,.316 lsC ItYS 3 vr,ls SAMPR E SHED BY: 1• DATE/TIME: G /5 !Sd [IRE�CEnYtW Z D E IM I/!°� Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: RE QUISHED BY: 3. ATE/TIME: RECEIVE Y: 4. ATE/TIME: RELINQUISHED BY: 5. DATE/TIME: RECEIVED BY: 6. DATE/TIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt t, °C RELINQUISHED BY: 7. DATE/TIME: RECEIVED BY: 8. DATE/TIME: Possible Hazards associated with samples: Non -Hazard ElFlammableElkin Irritant Poison Y ZUnknown ❑Other Form Revised July, 2014 Page Rogers & Caticott ENVIRONMENTAL Sample Receipt Verification Date Work Client: Received: I Order: Carrier Name: Client FedEx Tracking Number: UPS US Mail Courier Field Services Qther: Receipt Criteria Y e s 0 A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled? Temp measured with iR thermometer - SN: 97050067 Ice Cold Packs D ce None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. t �{ Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? x \V_ If in-house preservation used — record Lot # HCL H3PO4 HZSO4 NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or kio Non -Conformance issue other than noted above: Reviscd July 2014 Completed by: Page 11 of 11 Rogers and Callcott Environmental Client: Date: 22611 S Field Meter Calibration Record Conductivity Cal! ration EPA 9050A Meter Make / Model: Orion Star A325 SN: 2-7 D% Probe: Time: Analyst: Cell Constant Chemical Inventory Conc. of Standard, µmhos cm Actual Reading of Standard, µmhos/cm @ Temperature, °C SSS conc: Temperature compensation for pH / conductivity meter : 0,0 pH Calibration EPA 9040C' Meter Make/ Model Orion Star A325 Probe: Time: GS5 / Analyst: -T li-- Slope: i Chemical Inventory Conc. of Buffer, units Actual Reading of Buffer, units 5v1v 4.0 y,v�-/ 7.0 7, c ,6) Y0 Lj s 10.0 l 0 r C)2- v637 `i SSS conc: -7.v r7,cv0 Turbidity Metei Field Screen Meter Make / Model: Hach 2100P SN: Time: Analyst: :alibration 7ethod Date of most recent calibration: Chemica nv Assigned Conc. of Standard, NTU Actual Reading of Standard, NTU Reviewed by: Date: Revised 01/21/13 Rogers and Callcott Environmental Continuing Calibration Verification Client: 4!:�.: i - /11 +— Conductivity Meter EPA 9050A Meter Make / Model: Orion StarA325 SN: (,OZ7G6 Probe: Date: I 6//S Time Analyst Conc. of Standard, Actual Reading of Standard, µmhos/cm @25°C µmhos/cm @ ,C @ °C pH Meter EPA 9040C Meter Make / Model: Orion Star A325 Probe: Ql-llCr- Ti me Analyst Conc. of Buffer, units Actual Reading of Buffer, units 1152 Turbidity Meter Field Screen Method Meter Make / Model: Hach 2100P SN: Time Assigned Conc. of Standard, Actual Reading of Standard, NTU NTU 1 Field Duplicate Well ID: Time Analyst Conductivity, pH, Turbidity, Temperature, µmhos/cm units NTU °C 1IL17 j 1,i F kl - 719 9 iS, I Note: Refer to daily calibration log for instrument calibration and chemical inventory information / documentation. Reviewed by: Date: Revised 01/21/13 Rogers & Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Lubloratory services 3'S# 8 61 5:08 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on March 06, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit #W00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Kara Hrkach Project Manager This report may not be reproduced, except in full, without written permission from Rogers & Callcoll. Inc. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcal Icott.com — an employee -owned company Page 1 of 12 Rogers & Callcott iv ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5030281-01 Influent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water lab ID 880 Project: Influent Work Order: 5030281 Received: 03/06/2015 15:08 Matrix Sampled Type Ground Water 03/06/15 12:01 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax U4.232.6140 rogersandeallcott.eom an employee -owned company 0312712015 10:05 This report may not be reproduced, except infull, without written pertnissionfrom Rogers & Callcoti, Inc. Page 2 of 12 ` Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Sample Data Sample Number 5030281-01 Sample Description Influent Grab collected on 03/06/15 12:01 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 03/13/15 12:28 EPA9260B LBW B5C0729 1,1-Dichloroethane 0.6 0.5 us/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 1, 1 -Dichloroethene 1.0 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW 135C0729 1,2,4-Trimethylbenzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 1,2-Dichloroethane 0.8 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Acetone ND 20.0 ug/L 1.00 03/13/15 12:28 EPA 8260E LBW B5C0729 Benzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Chloroform 19.7 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Euylbenzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW BSC0729 Hexane ND I.0 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Isopropylbenzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 m,p-Xylene ND 1.0 ug/L 1.00 03/13/15 12:28 EPA 8260E LBW B5C0729 Methylene chloride ND 2.0 ug/L 1.00 03/13/15 12:28 EPA 8260E LBW B5C0729 Naphthalene ND 1.0 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 n-Butylbenzene ND 1.0 us/1- 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 n-Propylbenzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 o-Xylene ND 1.0 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 sec-Butylbenzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Styrene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 tert-Butylbenzene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260B LBW B5C0729 Toluene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260E LBW B5C0729 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 03/13/15 12:28 EPA 8260E LBW B5C0729 Vinyl chloride ND 0.5 ug/L 1,00 03/13/15 12:28 EPA 8260B LBW B5C0729 Rebatch Sample Number: 5030281-01RE1 cis-1,2-Dichloroethene 60.2 2.5 ug/L 5.00 03/10/15 16:20 EPA 8260E LBW B5C0554 Tetrachloroethene 202 2.5 ug/L 5.00 03/10/15 16:20 EPA 8260E LBW B5C0554 Trichloroethene 118 2.5 ug/L 5.00 03/10/15 16:20 EPA 8260B LBW B5C0554 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 84 70-130 4-Bromofluorobenzene 110 70-130 Toluene-d8 91 70-130 Rebatch Sample Number: 5030281-OIREI 1,2-Dichloroethane-D4 84 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232,6140 rogersandcallcott.eom an employee -owned company 0312712015 10:05 This report may not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 3 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Sample Number 5030281-OIRE1 Sample Description Influent Grab collected on 03/06/15 12:01 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5030281-OIRE1 a-BromoJluorobenzene 111 70-130 Toluene-d8 102 70-130 PO Box 5655 ; Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandeallcott.eom an employee -owned company 0312712015 10:05 This report muv not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 4 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC Rill) Parameter Result Limit Units Level Result %REC Limits RI'D Limit Flays Batch B5C0554 - EPA 5030 Blank (B5C0554-BLKl) cis-1,2-Dichloroethene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Surrogate: 1,2-Dichloroethane-D4 81 70-130 Surrogate: 4-Bromofluorobenzene 111 70-130 Surrogate: Toluene-& 96 70-130 LCS (B5C0554-BS1) cis-1,2-Dichloroethene 20.4 0.5 ug/L 20.0 102 70-130 Tetrachloroethene 19.7 0.5 ug/L 20.0 99 70-130 Trichloroethene 18.1 0.5 ug/L 20.0 91 70-130 Surrogate:l,2-Dichloroethane-D4 98 70-130 Surrogate:4-BromoJluorobensene 106 70-130 Surrogate: Toluene-& 103 70-130 Matrix Spike (B5C0554-MS1) Source: 5030281-01RE2 cis-1,2-Dichloroethene 97.9 0.5 ug/L 20.0 76.5 107 70-I30 S3 Tetrachloroethene 268 0.5 ug/L 20.0 245 118 70-130 S3 Trichloroethene 161 0.5 ug/L 20.0 145 79 70-130 S3 Surrogate: 1,2-Dichloroethane-D4 94 70-130 Surrogate:4-Bromofluoroben--ene 110 70-130 Surrogate: Toluene-& 100 70-130 Matrix Spike Dup (B5C0554-MSD1) Source: 5030281-01RE2 cis-1,2-Dichloroethene Wo 0.5 ug/L 20.0 76.5 97 70-130 2 20 S3 Tetrachloroethene 252 0.5 ug/L 20.0 245 36 70-130 6 20 S3 Trichloroethene 150 0.5 ug/L 20.0 145 28 70-I30 7 20 S3 Surrogate:l,2-Dichloroethane-D4 94 70-130 Surrogate: 4-Bromofluorobenzene 105 70-130 Surrogate: Toluene-& 97 70-130 Batch B5C0729 - EPA 5030 Blank (B5C0729-BLK1) 1,1,1-Trichloroethane ND 0.5 ug/L I,1-Dichloroethane ND 0.5 ug/L 1,1-Dichloroethene ND 0.5 ug/L PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0312712015 10:05 This report may not be reproduced, except in full, without written permission from Rogers & Callcoq, Inc. Page 5 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5C0729 - EPA 5030 Blank (B5C0729-BLK1) 1,2,4-Trimethylbenzene ND 0.5 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 2.0 ug/L Chloroform ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND LO ug/L lsopropylbenzene ND 0.5 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 1.0 ug/L n-Butylbenzene ND 1.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 1.0 ug/L sec-Butylbenzene ND 0.5 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate:1,2-Diehloroethane-D4 82 70-130 Surrogate: 4-Bromojluorobenaene 112 70-130 Surrogate: Toluene-& 96 70-130 LCS (B5C0729-BS1) 1, 1, 1 -Trichloroethane 15.9 0.5 ug/L 20.0 80 70-130 1,1-Dichloroethane 17.4 0.5 ug/L 20.0 87 70-130 1,1-Dichloroethene 21.8 0.5 ug/L 20.0 109 70-130 1,2,4-Trimethylbenzene 22.9 0.5 ug/L 20.0 115 70-130 1,2-Dichloroethane 19.6 0.5 ug/L 20.0 98 70-130 Acetone 113 20.0 ug/L 100 113 60-140 Benzene 18.6 0.5 ug/L 20.0 93 70-130 Bromomethane (Methyl Bromide) 23.3 2.0 ug/L 20.0 116 60-140 Chloroform 17.8 0.5 ug/L 20.0 89 70-130 Ethylbenzene 19.4 0.5 ug/L 20.0 97 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.614o rogersandeallcott.eom an employee -owned company 0312712015 10:05 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 6 of 12 c Rogers & Cakott ENVIRONMENTAL Catalent Phanna Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit l la s Batch B5C0729 - EPA 5030 LCS (B5C0729-BSl) Hexane 20.1 1.0 ug/L 20.0 101 70-130 Isopropylbenzene 20.0 0.5 ug/L 20.0 100 70-130 m,p-Xylene 41.3 1.0 ug/L 40.0 103 70-130 Methylene chloride 17.1 2.0 ug/L 20.0 85 70-130 Naphthalene 17.3 1.0 ug/L 20.0 86 70-130 n-Butylbenzene 19.4 1.0 ug/L 20.0 97 70-130 n-Propylbenzene 21.6 0.5 ug/L 20.0 108 70-130 o-Xylene 21.0 1.0 ug/L 20.0 105 70-130 sec-Butylbenzene 22.6 0.5 ug/L 20.0 113 70-130 Styrene 20.8 0.5 ug/L 20.0 104 70-130 tert-Butylbenzene 22.1 0.5 ug/L 20.0 Ill 70-130 Toluene 21.3 0.5 ug/L 20.0 106 70-I30 trans-1,2-Dichloroethene 19.4 0.5 ug/L 20.0 97 70-130 Vinyl chloride 20.5 0.5 ug/L 20.0 102 60-140 Surrogate: 1,2-Diehloroethane-D4 100 70-130 Surrogate:4-BromoJluorobenzene 102 70-130 Surrogate: Toluene-d8 104 70-130 Matrix Spike (B5C0729-MS1) Source: 5030410-05 1,1,l-Trichloroethane 198 5.0 ug/L 200 40.5 79 70-130 I,I-Dichloroethane 305 5.0 ug/L 200 155 75 70-130 1,1-Dichloroethene 690 5.0 ug/L 200 576 57 70-130 sl 1,2,4-Trimethylbenzene 247 5.0 ug/L 200 ND 123 70-130 1,2-Dichloroethane 200 5.0 ug/L 200 ND 98 70-130 Acetone 1120 200 ug/L 1000 ND Ill 60-140 Benzene 200 5.0 ug/L 200 ND 100 70-130 Bromomethane (Methyl Bromide) 232 20.0 ug/L 200 ND 116 60-140 Chloroform 192 5.0 ug/L 200 ND 96 70-130 Ethylbenzene 204 5.0 ug/L 200 ND 102 70-130 Hexane 167 10.0 ug/L 200 ND 83 70-130 Isopropylbenzene 199 5.0 ug/L 200 ND 100 70-130 m,p-Xylene 423 10.0 ug/L 400 ND 106 70-130 Methylene chloride 190 20.0 ug/L 200 ND 86 70-130 Naphthalene 184 10.0 ug/L 200 ND 92 70-130 n-Butylbenzene 219 10.0 ug/L 200 ND 110 70-130 n-Propylbenzene 245 5.0 ug/L 200 ND 122 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company 0312712015 10:05 This report mw not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 7 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5C0729 - EPA 5030 Matrix Spike (B5C0729-MS1) Source: 5030410-05 o-Xylene 228 10.0 ug/L 200 ND 114 70-130 sec-Butylbenzene 240 5.0 ug/L 200 ND 120 70-130 Styrene 213 5.0 ug/L 200 ND 106 70-130 tert-Butylbenzene 225 5.0 ug/L 200 ND 113 70-130 Toluene 219 5.0 ug/L 200 ND 109 70-130 trans-1,2-Dichloroethee 185 5.0 ug/L 200 ND 93 70-130 Vinyl chloride 204 5.0 ug/L 200 ND 102 60-140 Surrogate: 1,2-Dichloroethane-D4 101 70-130 Surrogate: 4-BromoJluorobenzene 111 70-130 Surrogate: Toluene-d8 105 70-130 Matrix Spike Dup (B5C0729-MSDI) Source: 5030410-05 1, 1, 1 -Trichl oroethane 193 5.0 ug/L 200 40.5 76 70-130 3 20 1,1-Dichloroethane 287 5.0 ug/L 200 155 66 70-130 6 20 S1 l,l-Dichloroethee 629 5.0 ug/L 200 576 26 70-130 9 20 S1 1,2,4-Trimethylbenzene 242 5.0 ug/L 200 ND 121 70-130 2 20 1,2-Dichloroethane 195 5.0 ug/L 200 ND 95 70-130 3 20 Acetone 1130 200 u9/1. 1000 ND 113 60-140 0.5 20 Benzene 178 5.0 ug/L 200 ND 89 70-130 12 20 Bromomethane (Methyl Bromide) 214 20.0 ug/L 200 ND 107 60-140 8 20 Chloroform 179 5.0 ug/L 200 ND 90 70-130 7 20 Ethylbenzene 192 5.0 ug/L 200 ND 96 70-130 6 20 Hexane 165 10.0 ug/L 200 ND 82 70-130 1 20 lsopropylbenzene 193 5.0 ug/L 200 ND 96 70-130 3 20 m,p-Xylene 398 10.0 ug/L 400 ND 100 70-130 6 20 Methylene chloride 180 20.0 ug/L 200 ND 81 70-130 6 20 Naphthalene 201 10.0 ug/L 200 ND 100 70-130 9 20 n-Butylbenzene 207 10.0 ug/L 200 ND 104 70-130 6 20 n-Propylbenzene 233 5.0 ug/L 200 ND 116 70-130 5 20 o-Xylene 213 10.0 ug/L 200 ND 106 70-130 7 20 sec-Butylbenzene 234 5.0 ug/L 200 ND 117 70-130 2 20 Styrene 208 5.0 ug/L 200 ND 104 70-130 2 20 tert-Butylbenzene 223 5.0 ug/L 200 ND 112 70-130 1 20 Toluene 210 5.0 ug/L 200 ND 105 70-130 4 20 trans-1,2-Dichloroethee 174 5.0 ug/L 200 ND 87 70-130 6 20 Vinyl chloride 195 5.0 ug/L 200 ND 98 60-140 5 20 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0312712015 10: 05 This report mqv not be reproduced, except in full, without written pennission from Rogers & Callcon, Inc. Page 8 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result GUREC Limits RPD Limit Flags Batch B5C0729 - EPA 5030 Matrix Spike Dup (R5C0729-MSD1) Source: 5030410-05 Surrogate:l.2-Diehloroethane-Da 95 70-130 Surrogate:4-Bromofluorobenzene 109 70-130 Surrogate: Toluene-& 103 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company 0312712015 10:05 This report mqv not be reproduced, except m full, without written permission from Rogers & Callcou, Inc. Page 9 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5030281 Monroe, NC 28110 Reported: 03/27/15 10:05 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference S l The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. S3 Estimated value - the spike result exceeded the calibration range. The spike recovery was not evaluated against the control limits. PO Box 5655 i Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com a i employee -owned company 0312712015 10: 05 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 10 of 12 Rogers & Ca([cott CHAIN OF CUSTODY RECORD WORK ORDER =i 4.0 ENVIRONMENTAL Al Filtered Les/No) Mailing PO Box 5655 Shipping 426 Falrforest Way 2156 Stonerldge Drive y Cooled (Yes/No) 6- Container Type (Plastic/Glass) Address: Greenville, SC 296D6 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Container Volume (mL) Client Name Sample (�- Type (Grab/Composite) Address i^% Sample Source (WW, GW, DW, SW, S, Other) RU-V d2 AI C— c Report To: o Preservation Code(s) Email Address v A —None E—HCI I—ZnAcetate 0o B—HNO3 F—Na2S203 J—H3PO4 Telephone# °J C °� N `1 C—H2SO4 G — Boric Acid K-MCAA PO # Project # 93-12-) z E V > D—NaOH H—AswrbicAcid L- cc r`o jL R & C WORK ORDER YR _L5 DATE TIME SAMPLE DESCRIPTION COMMENTS APO 'o 1 3 '-94,d 7. 9$ �e/14i-�o,j16 1Y-S s- wia n SAMPR E ISHED BY: DATE/TIME: RECE Y D E IM 1' t/ �S 1SLg' 2 ((j�p Composite Start Date: Composite Start Time: RE QUISHED BY: ATE/TIME: RECEIVE Y: ATE/TIME: 3. 4. Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 5. 6. Temperature of blank or representative sample At time of collection °C RELINQUISHED BY: DATE/TIME: RECEIVED BY: DATE/TIME: 7. 8. At time of lab receipt C Possible Hazards associated with samples: I —I Non -Hazard LiFlammable uSkin Irritant o Poison Unknown ElDther Form Revised July, 2014 Page Rogers &Caltcott ENVIRONMENTAL Sample Receipt Verification Date Work (� Client: Received: 1 Order: U Carrier Name: Client FedEx UPS US Mail Courier field Services Other: Tracking Number: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples Cooled? Temp measured with 1R thermometer - SN: 97050067 Ice Cold Packs Dr ce None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot # HCL H,POa HZSOa NaOH HNO, Other Comments: Were non-conformance issues noted at sample receipt? Yes or t�o Non -Conformance issue other than noted above: Revised July 2014 Completed by: Page 12 of 12 Catalent Pharma Solutions 2725 Scherer Drive North St. Petersburg, FL 33716 T 727.803.2100 r 727.803.2419 vrvrmcatalent.com March 9, 2015 Mr. Kyle Ketchum City of Monroe WWTP 775 Treeway Drive Monroe, North Carolina 28110 Subject: Effluent Discharge Report LIUP # LP-001 Treated Groundwater Catalent Pharma Solutions (Formerly R. P. Scherer)/Chelsea Laboratories Facility 2021 East Roosevelt Blvd., Monroe, North Carolina 28112 Dear Mr. Ketchum: Enclosed are the February 2015 effluent discharge and laboratory analysis reports for the referenced facility. The primary effluent sample was collected on February 5, 2015. A confirmation sample for analysis of volatile organic compounds only was collected on February 18, 2015. No non -conformances were reported. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete. I am aware there are significant penalties for submitting false Information, including the possibility of fine or imprisonment for knowing violations. If you have any questions or concerns, please contact Jeffery Rogers at 727-803-2282 (email: Jeffery.Rogers@catalent.com) or Stan Golaski of Rogers & Callcott at 864-335-4984 (email: stan.golaski @rogersandcallcott.com). Sincerely, Catalent Pharma Solutions Cc 2 Dina Kodakis General Manager Enclosures 03 -13 -1.5 Date cc with attachments: Stan'Golaski, Rogers & Callcott Environmental Jerry Sullivan, Aqua -Trot (on -site file) Receiving POTW NPDES #: NCO024333 Effective Date for these Limits: 7/1/13 Expiration Date for these Limits: 6/30/16 LIUP #: LP-001 Pipe #: 01 Reporting Period: February 2015 Date &Time Days Meter Reading Weekly Flow Weekly Tetrachloro- Trichloro- 3 8260 pH of Reading Between (gal) (gal)1 Average 2 ethene ethene (ug/L) (units) Comments Readings 9 (mgpd) (9/L u ) u (9/L ) 1 /26/15 10:00 10,615,128 2/4/15 10:30 9.02 10,648,168 33,040 0.003663 Sample and pH 2/5/15 16:00 1.23 10,653,239 5,071 0.004125 2.6 1.2 3.8 8.0 collected on 2/10/15 18:00 5.08 10,675,043 21,804 0.004289 February 5, 2/16/1515:00 5.88 10,699,365 24,322 0.004140 3.4 1.7 5.8 -- 2015. 2/23/1517:00 7.08 10,739,232 39,867 0.005628 Confirmation Monthly Total 124,104 Maximum 0.005628 sample collected February 18, Minimum 0.003663 2015. Sample Type Grab Grab Grab Grab Permit Limits 0.010000 8.85 81 monitor onlv 6 to 11 1 Flow between Meter Readings 2 Weekly Average = Weekly Flow / Days Between Readings 3 Value represents total 8260 volatile organic compounds. BRDL= Below Reportable Detection Limits \\RC-VMSRV03\Projects\14\93-121\2015\RPTS\POTW Reports\February2015\ February 2015 POTW Form.xlsx 3/9/2015 r ' Rogers & Callcott ENVIRONMENTAL PCWp Laboratory Report Client Catalent Pharma Solutions Project: C/O George Maalouf - Rogers and Callcott Work Order: 2021 E. Roosevelt Blvd. Received: Monroe, NC 28110 Dear Client: Laboratory Services Effluent 5020285 02/05/2015 16:21 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on February 05, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit #W00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: ) " & 6, - C/ %1/9d z Kara Hrkach Project Manager This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. PO Box 5655 I Greenville, SC 29606 Ir 426 Fairforest Way Greenville, 5C 29607 main 864.232.1556 tax 864,232.6140 rogersandcallcOLC.com an employee -owned company Page 1 of 11 Rogers &Callcott ENVIRONMENTAL South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 Certificate of Analysis North Carolina Laboratory Certification Number27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Client Catalent Pharma Solutions Project: Effluent C/O George Maalouf- Rogers and Callcott Work Order: 5020285 2021 E. Roosevelt Blvd. Received: 02/05/2015 16:21 Monroe, NC 28110 Sample Number Sample Description Matrix Sampled Type 5020285-01 Effluent Grab Ground Water 02/05/15 12:02 Grab 5020285-02 Effluent Grab Ground Water 02/05/15 12:02 Grab PO Box 5655 1 Greenville, SC 29606 426 Fairtorest Way Greenville, SC 29607 main 864.232.1556 f.w 864,232.6140 rogersandeallcott.com _..._ ... -.--_--------- an empinyew-owned company 02124,2015 15: 05 This report may not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Page 2 of 11 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Sample Data Sample Number 5020285-01 Sample Description Effluent Grab collected on 02/05/15 12:02 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Field Parameters pH 8.0 0.1 pH Units 1.00 02/05/15 12:02 EPA 9040C JHF B5B0234 Temperature 15.1 0.0 °C 1.00 02/05/15 12:02 SM255OB-2010 JHF B5B0234 Sample Number 5020285-02 Sample Description Effluent Grab collected on 02/05/15 12:02 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 1.0 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 1,1-Dichloroethane ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 1,1-Dichloroethene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 1,2,4-Trimethylbenzene ND 1.0 ug/L 1.00 02/09/15 20:50 EPA 8260E LBW B5B0719 1,2-Dichloroethane ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B Za LBW B5B0719 Acetone ND 20.0 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Benzene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW BSB0719 Bromomethane (Methyl Bromide) ND 1.0 ug/L 1.00 02/09/15 20:50 EPA 8260E LBW B5B0719 Chloroform ND 1.0 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Ethylbenzene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 9260B LBW B5B0719 Hexane ND I.0 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Isopropylbenzene ND 1.0 ug/L 1.00 02/09/15 20:50 EPA 8260E LBW B5B0719 m,p-Xylene ND 1.0 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Methylene chloride ND 2.0 u8/1. 1.00 02/09/15 20:50 EPA 8260B LBW 135B0719 Naphthalene ND 4.0 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 n-Butylbenzene ND 2.0 ug/L 1.00 02/09/15 20:50 EPA 8260E LBW B5B0719 n-Propylbenzene ND 0.5 u8/1- 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 o-Xylene ND 0.5 ug/I, 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 sec-Butylbenzene ND 1.0 u9/1. 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Styrene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260E LBW B5B0719 tert-Butylbenzene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Tetrachloroethene 2.6 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Toluene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 Trichloroethene 1.2 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B LBW B5B0719 PO Box 5655 I Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 . main 864.232.1556 fax 864,232.6140 rogersandealleott.eom an employee -owned coml .vw 0212412015 15: 05 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Page 3 of 11 u Rogers & Cakott ENVIRONMENTAL. Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Sample Number 5020285-02 Sample Description Effluent Grab collected on 02/05/15 12:02 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Vinyl chloride ND 0.5 ug/L 1.00 02/09/15 20:50 EPA 8260B Z LBW B5B0719 Surrogates %REC % REC Limits Flag 1,2-Dichloroethane-D4 80 70-130 4-BromoJluorobenzene 98 70-130 Toluene-& 89 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way Greenville, SC 29607 ' main 864.232.1556 fax $64,232.6140 rogersalldcallcott.com an employee -owned company. 02 24.2015 15: 05 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 4 of 11 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Volatile Organics Quality Control Summary Reporting Spike Source %RF,C RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5B0719 - EPA 5030 Blank (B5B0719-BLK1) 1,1,1-Trichloroethane ND 1.0 ug/L l,l-Dichloroethane ND 0.5 ug/L I,1-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 1.0 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 1.0 ug/L Chloroform ND 1.0 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Etylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L Isopropylbenzene ND 1.0 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 4.0 ug/L n-Butylbenzene ND 2.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Butylbenzene ND 1.0 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate: 1,1-Dichloroethane-D4 Surrogate: 4-Bromofluorobenzene Surrogate: Toluene-& LCS (B5B0719-BS1) 75 70-130 101 70-130 87 70-130 l,l,l-Trichloroethane 22.4 1.0 ug/L 20.0 112 70-130 1, 1 -Dichloroethane 19.7 0.5 ug/L 20.0 98 70-130 l,l-Dichloroethene 23.2 0.5 ug/L 20.0 116 70-130 1,2,4-Ttimethylbenzene 22.5 1.0 ug/L 20.0 112 70-130 PO Box 5655 , Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 ! main 864.232.1556 fax 864.232.6140 rogersandealleott.com __ __ _ -- - _ • - -- an employe- ownpel Con,, , 02124,12015 15: 05 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 5 of 11 J Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RFD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5B0719 - EPA 5030 LCS (B5B0719-BSI) 1,2-Dichloroethane 20.0 0.5 ug/L 20.0 100 70-130 Acetone 91.6 20.0 ug/L 100 92 60-140 Benzene 19.6 0.5 ug/L 20.0 98 70-130 Bromomethane (Methyl Bromide) 23.1 1.0 ug/L 20.0 115 60-140 Chloroform 19.4 1.0 ug/L 20.0 97 70-130 cis-1,2-Dichloroethene 21.9 0.5 ug/L 20.0 110 70-130 Ethylbenzene 21.0 0.5 ug/L 20.0 105 70-130 Hexane 24.1 1.0 ug/L 20.0 121 70-130 Isopropylbenzene 22.1 1.0 ug/L 20.0 110 70-130 m,p-Xylene 40.1 1.0 ug/L 40.0 100 70-130 Methylene chloride 19.5 2.0 ug/L 20.0 97 70-130 Naphthalene 17.9 4.0 ug/L 20.0 90 70-130 n-Butylbenzene 25.2 2.0 ug/L 20.0 126 70-130 n-Propylbenzene 22.6 0.5 ug/L 20.0 113 70-130 o-Xylene 21.0 0.5 ug/L 20.0 105 70-130 sec-Butylbenzene 23.2 1.0 ug/L 20.0 116 70-130 Styrene 19.6 0.5 ug/L 20.0 98 70-130 tert-Butylbenzene 21.4 0.5 ug/L 20.0 107 70-130 Tetrachloroethene 20.6 0.5 ug/L 20.0 103 70-130 Toluene 20.8 0.5 ug/L 20.0 104 70-130 trans-1,2-Dichloroetlrene 22.0 0.5 ug/L 20.0 110 70-130 Trichloroethene 21.5 0.5 ug/L 20.0 108 70-130 Vinyl chloride 20.9 0.5 ug/L 20.0 104 60-140 Surrogate: 1,2-Diehloroethane-D4 97 70-130 Surrogate: 4-Bromojluoroben_ene 101 70-130 Surrogate: Toluene-d8 101 70-130 Matrix Spike (B5B0719-MS1) Source: 5020286-01 1, 1, 1 -Trichloroethane 24.3 1.0 ug/L 20.0 ND 121 70-I30 1,1-Dichloroethane 22.1 0.5 ug/L 20.0 0.6 108 70-130 1,1-Dichloroethene 25.3 0.5 ug/L 20.0 0.9 122 70-130 1,2,4-Trimethylbenzene 22.7 LO ug/L 20.0 ND 114 70-130 1,2-Dichloroethane 21.8 0.5 ug/L 20.0 0.8 105 70-130 Acetone 97.7 20.0 ug/L 100 ND 98 60-140 Benzene 21.2 0.5 ug/L 20.0 ND 106 70-130 Bromomethane (Methyl Bromide) 25.3 1.0 ug/L 20.0 ND 126 60-140 PO Box 5655 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 lax 864.232.6140 rogersandcallcott.eom an employee -owned company 0212412015 15: 05 This report may not be reproduced except in full, without written permission from Rogers & Callcott, Inc. Page 6 of 11 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RI'D Parameter Result Limit Units Level Result %REC Limits Rill) Limit Flags Batch B5B0719 - EPA 5030 Matrix Spike (B5B0719-MSI) Source: 5020286-01 Chloroform 28.8 1.0 ug/L 20.0 8.2 103 70-130 cis-1,2-Dichloroethee 67.9 0.5 ug/L 20.0 43.9 120 70-130 Ethylbenzene 21.5 0.5 ug/L 20.0 ND 107 70-130 Hexane 27.2 1.0 ug/L 20.0 ND 136 70-130 S1 Isopropylbenzene 22.9 1.0 ug/L 20.0 ND 115 70-130 m,p-Xylene 43.8 1.0 ug/L 40.0 ND 109 70-130 Methylene chloride 19.9 2.0 ug/L 20.0 ND 99 70-130 Naphthalene 18.8 4.0 ug/L 20.0 ND 89 70-130 n-Buylbenzene 24.7 2.0 ug/L 20.0 ND 124 70-130 n-Propylbenzene 22.9 0.5 ug/L 20.0 ND 114 70-130 o-Xylene 21.7 0.5 ug/L 20.0 ND 108 70-130 sec-Butylbenzene 23.3 1.0 ug/L 20.0 ND 116 70-130 Styrene 20.2 0.5 ug/L 20.0 ND 101 70-130 tert-Buylbenzene 23.1 0.5 ug/L 20.0 ND 115 70-130 Tetrachloroethene 172 0.5 ug/L 20.0 145 136 70-130 S3 Toluene 21.3 0.5 ug/L 20.0 ND 106 70-130 trans-1,2-Dichloroethee 24.1 0.5 ug/L 20.0 ND 120 70-130 Trichloroethene 120 0.5 ug/L 20.0 96.4 120 70-130 Vinyl chloride 23.9 0.5 ug/L 20.0 ND 120 60-140 Surrogate: 1,2-Dichloroethane-D4 102 70-130 Surrogate: 4-BromoJluoroben_ene 104 70-130 Surrogate: Toluene-& 104 70-130 Matrix Spike Dup (B5B0719-MSD1) Source: 5020286-01 1,1,1-Trichloroethane 21.6 1.0 ug/L 20.0 ND 108 70-130 12 20 1,1-Dichloroethane 19.6 0.5 ug/L 20.0 0.6 95 70-130 12 20 1,1-Dichloroethee 22.1 0.5 ug/L 20.0 0.9 106 70-130 13 20 1,2,4-Trimethylbenzene 21.4 1.0 ug/L 20.0 ND 107 70-130 6 20 1,2-Dichloroethane 21.2 0.5 ug/L 20.0 0.8 102 70-130 3 20 Acetone 99.6 20.0 ug/L 100 ND 100 60-140 2 20 Benzene 18.4 0.5 ug/L 20.0 ND 92 70-130 14 20 Bromomethane (Methyl Bromide) 22.3 1.0 ug/L 20.0 ND 111 60-140 13 20 Chloroform 26.0 1.0 ug/L 20.0 8.2 89 70-130 10 20 cis-1,2-Dichloroethee 63.4 0.5 ug/L 20.0 43.9 98 70-130 7 20 Ethylbenzene 19.7 0.5 ug/L 20.0 ND 98 70-130 9 20 Hexane 24.1 1.0 ug/L 20.0 ND 120 70-130 12 20 PO Box 5655 ' Greenville. SC 29606 426 Fairforest Way ' Greenville. SC 29607 ` main 864.232.1556 fax 864,232.6140 rogersandcallcott.com __- _ _ an employee owned company 0212412015 15: 05 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 7 of 11 Rogers &Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5B0719 - EPA 5030 Matrix Spike Dup (B5B0719-MSDI) Source: 5020286-01 Isopropylbenzene 20.3 1.0 ug/L 20.0 ND 102 70-130 12 20 m,p-Xylene 40.0 1.0 ug/L 40.0 ND 100 70-130 9 20 Methylene chloride 18.6 2.0 ug/L 20.0 ND 93 70-130 6 20 Naphthalene 20.4 4.0 ug/L 20.0 ND 97 70-130 8 20 n-Butylbenzene 22.0 2.0 ug/L 20.0 ND 110 70-130 12 20 n-Propylbenzene 20.9 0.5 ug/L 20.0 ND 104 70-130 9 20 o-Xylene 19.7 0.5 ug/L 20.0 ND 98 70-130 10 20 sec-Butylbenzene 21.2 1.0 ug/L 20.0 ND 106 70-130 9 20 Styrene 19.2 0.5 ug/L 20.0 ND 96 70-130 5 20 tert-Butylbenzene 21.0 0.5 ug/L 20.0 ND 105 70-130 9 20 Tetrachloroethene 154 0.5 ug/L 20.0 145 41 70-130 12 20 S3 Toluene 19.5 0.5 ug/L 20.0 ND 98 70-130 9 20 trans-1,2-Dichloroethene 21.4 0.5 ug/L 20.0 ND 107 70-130 12 20 Trichloroethene 106 0.5 ug/L 20.0 96.4 45 70-130 13 20 S3 Vinyl chloride 21.1 0.5 ug/L 20.0 ND 106 60-140 12 20 Surrogate: 1, 2-Diehloroethane-D4 Surrogate: 4-BromoJluorobenzene Surrogate: Toluene-& 96 70-130 99 70-130 96 70-130 PO Box 5655 P Greenville, SC 29606 + 426 Fairtorest Way Greenville, SC 29607 , main $64.232.1556 fax 864.232.6140 rogersandcallcott.COl71 an employee -owned company 02 242015 15:05 This report may not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Page 8 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020285 Monroe, NC 28110 Reported: 02/24/15 15:05 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference S 1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. S3 Estimated value - the spike result exceeded the calibration range. The spike recovery was not evaluated against the control limits. Z MDL = 0.09ug/L - no peaks detected Za MDL = 0.16ug/L - no peaks detected PO Box 5655 1 Greenville, SC 29606 426 Fairfores€ Way Greenville, SC 29607 main W.232.IS56 fax 864,232.614o rogerSandcallcott.COm an employee -owned company 0212412015 15: 05 This report may not be reproduced, except in full, without written permission from Rogers & Callcoll, Inc. Page 9 of 11 m rm Rogers & Callcott CHAIN E N V I R O N M E N TA L Mailing PO Box 5655 Shipping 426 Fairforest Way 215E Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 2921D Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Catalent Client Name Address Monroe, NC Report To: Email Address Telephone # PO # Project # 93-121 OF CUSTODY RECORD WORK ORDER a c o c� o E Z 0 N Y G ao G GW _ ° m Y 00 E LLCOMMENTS Filtered (Yes/No) Cooled (Yes/No) Container Type (Plastic/Glass) Container Volume (mL) Sample Type (Grab/Composite) Sample Source (WW, GW, DW, SW, S, Other) Preservation Code(s) A —None E—HCI I — ZnAcetate B—HNO3 F—Na2S203 J—H3PO4 C — H2SO4 G — Boric Acid K - MCAA D — NaOH H —Ascorbic Acid L - R&C WORKORDER YR 1 DATE TIME SAMPLE DESCRIPTION q*3 vials unpres, I HCI 'p —0 �Z1 ��1�•� [ Effluent 5uac) - o pH - � r p"L Collected on ZI5 IS @ 12v Temp - I by r SA ISHED BY: 1. A E/TIME: Z _S �� l�Z 1 REC ED BY: 2. DATE/TIME: Composite Start Date: Composite Start Time: Time or Flow (Circle one) initials: RE QUISHED BY: 3. ATE/TIME: RECEIV D BY: 4• DATE/TIME: RELINQUISHED BY: 5. DATE/TIME: RECEIVED BY: 6. DATEITIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt 0 • L °C RELINQUISHED BY: DATE/TIME: RECEIVED BY: g DATE/TIME: ossible Hazards associated with samples: ❑ Non -Hazard EFI.mmable DSkin Irritant 0 Poison Unknown EDDther Form Revised July, 2014 Page �_ of Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Date Work Client: C jNt em-F Received: 1 S Order: rjUaoa�S Carrier Name: Client FedEx UPS US Mail Courier Field Services Other: Tracking Number: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? x COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? �( Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? X Sample volume sufficient for analysis? k VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled? Temp measured with IR thermometer - SN. 97050067 ("712eCold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. VU Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? u If in-house preservation used — record Lot # HCL H3POI HZSO4 NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by:v�_j Page l l oI 11 Rogers and Callcott Environmental Client: Cvd d— Date: Z/shs Field Meter Calibration Record Conductivity Calibration - EPA 9050A Meter Make / Model: Orion Star A325 SN: 027 OG Probe: Time: Analyst: Cell Constant Chemical Invento Conc. of Standard, Actual Reading of Standard, µmhos/cm @25°C µmhos/cm @ Temperature, *C SSS conc77 Temperature compensation for pH / conductivity meter: pH Calibration - EPA 9040C Meter Make / Model: Orion Star A325 Probe: Time: Q&39 Analyst: �} �- Slope: Chemical Inventory Conc. of Buffer, units Actual Reading of Buffer, units P11 D y S% 6 4.0 L' C> P653 7.0 7,o1 VC) V13 y I 10.0 /'D.UZ i�j � 3 L/ `� SSS conc: � d 3,99 Meter Calibration Field Screen Method Meter Make / Model: Hach 2100P SN: Date of most recent calibration: Time: Reviewed by: Date: Revised 01/21/13 Rogers and Callcott Environmental Continuing Calibration Verification Meter Make / Model: Orion Star A325 Client: ('-ec �^ 1,�— Conductivity Meter EPA 9050A SN: (702- 70 6 Probe: Date: 2 L,5h—s e Analyst Conc. of Standard, Actual Reading of Standard, mhos/cm @25°C µmhos/cm @ °C @ °C PH Meter EPA 9040C Meter Make / Model: Orion Star A325 Probe: 5Z I E'I ar 107 Time Analyst Conc. of Buffer, units Actual Reading of Buffer, units 2 i 14- % c� 7,07 Meter Make / Model: Hach 2100P Well ID: Turbidity Meter Field Screen Method SN: e Analyst Assigned Conc. of Standard, NTU Actual Reading of Standard, NTU Field Duplicate Time Analyst Conductivity, pH, Turbidity, Temperature, µmhos/cm units NTU °C I S-lI P-Al - 15_0 Note: Refer to daily calibration log for instrument calibration and chemical inventory information / documentation. Reviewed by: Date: Revised 01/21/13 Rogers & Callcott 6 ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: Loborat-ory Services Effluent 5020686 02/18/2015 16:55 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on February 18, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit NWQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: ame�- (VVM Kara Hrkach Project Manager This report may not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. PO Box 565S i Greenville, SC 29606 ` 426 Fairforest Way Greenville, SC 29607 s main 864.232.1556 fax 864.232.6140 rogersandCailcott.com an ernployee-owned company Page 1 of 10 Rogers & Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalc of - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5020686-01 Effluent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Effluent Work Order: 5020686 Received: 02/18/2015 16:55 Matrix Sampled Type Ground Water 02/18/15 13:55 Grab PO Boat $655 1 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 Fax 864,2326140 roger$andcallC©tt.com ..._.� v ._. an empioyaa..owned company 03 0612015 08:43 This report may not be reproduced, except in full, without written permissionfrom Rogers & Callcott, Inc. Page 2 Of 1 O Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020686 Monroe, NC 28110 Reported: 03/06/15 08:43 Sample Data Sample Number 5020686-01 Sample Description Effluent Grab collected on 02/18/15 13:55 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 1,1-Dichloroethane ND 0.5 u8/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 1, 1 -Dichloroethene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 1,2,4-Trimethylbenzene ND 1.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 1,2-Dichloroethane ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B Z LBW B5C0072 Acetone ND 20.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Benzene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 02/25/15 17:58 EPA 8260E LBW B5C0072 Chloroform ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260E LBW B5C0072 cis-1,2-Dichloroethene 0.7 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Ethylbenzene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Hexane ND 1.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Isopropylbenzene ND 1 0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 m,p-Xylene ND 1.0 ug/1. 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Methylene chloride ND 2.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Naphthalene ND 4.0 ug/L 1.00 02/25/15 17:58 EPA 8260E LBW B5C0072 n-Butylbenzene ND 2.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 n-Propylbenzene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B500072 o-Xylene ND 1.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 sec-Butylbenzene ND 1.0 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Styrene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW BSCO072 tert-Butylbenzene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Tetrachloroethene 3.4 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Toluene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Trichloroethene 1.7 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B LBW B5C0072 Vinyl chloride ND 0.5 ug/L 1.00 02/25/15 17:58 EPA 8260B Za LBW B5C0072 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 84 70-130 4-Bromofluorobenzene 108 70-130 Toluene-& 103 70-130 PO Box 5655 I Greenville, SC 246M s 426 Fair(orest Way Greenville, SC 29607 main 864.232.1556 864,232.6140 rogerSandcallcott.com __ - an employee -owned company 03,10612015 08:43 This report may not be reproduced, except in full, without written permission from Rogers & Callcon, Inc. Page 3 of 10 Rogers &VCallcott ENRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020686 Monroe, NC 28110 Reported: 03/06/15 08:43 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5C0072 - EPA 5030 Blank (B5C0072-BLKI) 1,1,1-Trichloroethane ND 0.5 ug/L l,l-Dichloroethane ND 0.5 ug/L l,l-Dichloroethee ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 1.0 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 2.0 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethee ND 0.5 119/1. Ethylbenzene ND 0.5 ug/L Hexane ND 1.0 119/1. Isopropylbenzene ND 1.0 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 4.0 ug/L a-Butylbenzene ND 2.0 119/1. n-Propylbenzene ND 0.5 ug/L o-Xylene ND 1.0 ug/L sec-Butylbenzene ND 1.0 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-12-Dichloroethee ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate:l,2-Dichloroethane-D4 87 70-130 Surrogate: 4-Bromofluoroben;ene 101 70-130 Surrogate: Toluene-& 93 70-130 LCS (B5C0072-BSI) 1,1,1-Trichloroethane 16.2 0.5 ug/L 20.0 81 70-130 1,1-Dichloroethane 20.1 0.5 ug/L 20.0 100 70-130 l,l-Dichloroethee 20.2 0.5 ug/L 20.0 101 70-130 1,2,4-Trimethylbenzene 22.4 1.0 ug/L 20.0 112 70-130 PO 0wt 5655 Greenville, SC 29606 426 Fairforest way Greenville, SC 29607 main 864.232.1556 fax 864,232.6140 rOgerSandcallcott.com an employes -owned company 03106,12015 08:43 This report may not be reproduced, except in full, without written permission from Rogers & Callcotl, Inc. Page 4 of 10 Rogers &Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020686 Monroe, NC 28110 Reported: 03/06/15 08:43 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5C0072 - EPA 5030 LCS (B5C0072-BSI) 1,2-Dichloroethane 20.8 0.5 ug/L 20.0 104 70-130 Acetone 96.9 20.0 ug/L 100 97 60-140 Benzene 21.2 0.5 ug/L 20.0 106 70-130 Bromomethane (Methyl Bromide) 25.2 2.0 ug/L 20.0 126 60-140 Chloroform 19.2 0.5 ug/L 20.0 96 70-130 cis-1,2-Dichloroethene 20.6 0.5 ug/L 20.0 103 70-130 Ethylbenzene 19.0 0.5 ug/L 20.0 95 70-130 Hexane 22.7 1.0 ug/L 20.0 113 70-130 Isopropylbenzene 19.0 1.0 ug/L 20.0 95 70-130 m,p-Xylene 41.7 1.0 ug/L 40.0 104 70-130 Methylene chloride 17.0 2.0 ug/L 20.0 85 70-130 Naphthalene 18.3 4.0 ug/L 20.0 91 70-130 n-Butylbenzene 20.6 2.0 ug/L 20.0 103 70-130 n-Propylbenzene 22.5 0.5 ug/L 20.0 112 70-130 o-Xylene 21.2 1.0 ug/L 20.0 106 70-130 sec-Butylbenzene 22.0 1.0 ug/L 20.0 110 70-130 Styrene 20.5 0.5 ug/L 20.0 103 70-130 tert-Butylbenzene 22.0 0.5 ug/L 20.0 110 70-130 Tetrachloroethene 19.0 0.5 ug/L 20.0 95 70-130 Toluene 21.0 0.5 ug/L 20.0 105 70-130 trans-1,2-Dichloroethene 21.6 0.5 ug/L 20.0 108 70-130 Trichloroethene 19.6 0.5 ug/L 20.0 98 70-130 Vinyl chloride 21.0 0.5 ug/L 20.0 105 60-140 Surrogate: 1,2-Dichloroethane-D4 104 70-130 Surrogate: 4-Bromofluoroben--ene 100 70-130 Surrogate: Toluene-d8 99 70-130 Matrix Spike (B5C0072-MS1) Source: 5020685-18 1,1,1-Trichloroedme 3440 100 ug/L 4000 ND 86 70-130 1,1-Dichloroethane 4050 100 ug/L 4000 ND 101 70-130 1,1-Dichloroethene 4250 100 ug/L 4000 ND 106 70-130 1,2,4-Trimethylbenzene 4560 200 ug/L 4000 ND 114 70-130 1,2-Dichloroethane 4080 100 ug/L 4000 ND 102 70-130 Acetone 19200 4000 ug/L 20000 ND 96 60-140 Benzene 4380 100 ug/L 4000 ND 109 70-130 Bromomethane (Methyl Bromide) 4890 400 ug/L 4000 ND 122 60-140 PO Box 56SS Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 fax 864,232.6140 rogersandcallcott.com an employee -owned company 0310612015 08:43 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 5 of 10 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020686 Monroe, NC 28110 Reported: 03/06/15 08:43 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5C0072 - EPA 5030 Matrix Spike (B5C0072-MSI) Source: 5020685-18 Chloroform 3940 100 ug/L 4000 ND 98 70-130 cis-1,2-Dichloroethene 8400 100 ug/L 4000 4190 105 70-130 Ethylbenzene 4090 100 ug/L 4000 ND 102 70-130 Hexane 4600 200 ug/L 4000 ND 115 70-130 Isopropylbenzene 3970 200 ug/L 4000 ND 99 70-130 m,p-Xylene 8580 200 ug/L 8000 ND 107 70-130 Methylene chloride 3460 400 ug/L 4000 ND 86 70-130 Naphthalene 3520 800 ug/L 4000 ND 86 70-130 n-Butylbenzene 4280 400 ug/L 4000 ND 106 70-130 n-Propylbenzene 4730 100 ug/L 4000 ND 118 70-130 o-Xylene 4460 200 ug/L 4000 ND 111 70-130 sec-Butylbenzene 4600 200 ug/L 4000 ND 115 70-130 Styrene 4150 100 ug/L 4000 ND 104 70-130 tert-Butylbenzene 4490 100 ug/L 4000 ND 112 70-130 Tetrachloroethene 4000 100 ug/L 4000 ND 100 70-130 Toluene 4380 100 ug/L 4000 ND 110 70-130 trans-1,2-Dichloroethene 4410 100 ug/L 4000 ND 110 70-130 Trichloroethene 10800 100 ug/L 4000 6950 96 70-130 Vinyl chloride 4210 100 ug/L 4000 ND 105 60-140 Surrogate: 1,2-Dichloroethane-D4 102 70-130 Surrogate:4-Bromofluorobenzene 102 70-130 Surrogate: Toluene-& 104 70-130 Matrix Spike Dup (135420072-MSD1) Source: 5020685-18 1,1,1-Trichloroethane 3340 100 ug/L 4000 ND 83 70-130 3 20 1,1-Dichloroethane 3650 100 ug/L 4000 ND 91 70-130 10 20 1,1-Dichloroethene 3890 100 ug/L 4000 ND 97 70-130 9 20 1,2,4-Trimethylbenzene 4520 200 ug/L 4000 ND 113 70-130 0.8 20 1,2-Dichloroethane 3850 100 ug/L 4000 ND 96 70-130 6 20 Acetone 19500 4000 ug/L 20000 ND 97 60-140 1 20 Benzene 3890 100 ug/L 4000 ND 97 70-130 12 20 Bromomethane (Methyl Bromide) 4400 400 ug/L 4000 ND 110 60-140 10 20 Chloroform 3680 100 ug/L 4000 ND 92 70-130 7 20 cis-1,2-Dichloroethene 8080 100 ug/L 4000 4190 97 70-130 4 20 Ethylbenzene 3890 100 ug/L 4000 ND 97 70-130 5 20 Hexane 4300 200 u9/1- 4000 ND 107 70-130 7 20 PC) Box 5655 ; Greenville. SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 hx 864,2316140 rogersandcallcott.com __... an employee -owned rornpanv 0310612015 08:43 This report may not be reproduced, except in full, without written permission from Rogers & Callcou, Inc. Page 6 of 10 Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020686 Monroe, NC 28110 Reported: 03/06/15 08:43 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5C0072 - EPA 5030 Matrix Spike Dup (B5C0072-MSDI) Source: 5020685-18 Isopropylbenzene 3820 200 ug/L 4000 ND 95 70-130 4 20 m,p-Xylene 8230 200 ug/L 8000 ND 103 70-130 4 20 Methylene chloride 3290 400 ug/L 4000 ND 82 70-130 5 20 Naphthalene 3800 800 ug/L 4000 ND 93 70-130 8 20 n-Butylbenzene 4040 400 ug/L 4000 ND 100 70-130 6 20 n-Propylbenzene 4530 100 ug/L 4000 ND 113 70-130 4 20 o-Xylene 4240 200 ug/L 4000 ND 106 70-130 5 20 sec-Butylbenzene 4490 200 ug/L 4000 ND 112 70-130 2 20 Styrene 4100 100 ug/L 4000 ND 103 70-130 1 20 tert-Butylbenzene 4410 100 ug/L 4000 ND 110 70-130 2 20 Tetrachloroethene 3690 100 ug/L 4000 ND 92 70-130 8 20 Toluene 4220 100 ug/L 4000 ND 105 70-130 4 20 trans-1,2-Dichloroethene 3950 100 ug/L 4000 ND 99 70-130 11 20 Trichloroethene 9870 100 ug/L 4000 6950 73 70-130 9 20 Vinyl chloride 4190 100 ug/L 4000 ND 105 60-140 0.6 20 Surrogate: 1,2-Dichloroethane-D4 Surrogate: 4-Bromojluorobenzene Surrogate: Toluene-d8 94 70-130 101 70-130 103 70-130 PO Box 5655 ! Greenville, SC 29606 s 426 Nirforest Way Greenville, SC 29607 ` main 864.232.1556 fax 864,232.614Q rogersandcallcott.com an employ2e-nwned romnany 03/062015 08: d3 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 7 of 10 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5020686 Monroe, NC 28110 Reported: 03/06/15 08:43 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference Z MDL is 0.17ug/L - No peaks detected Za MDL is 0.18ug/L - No peaks detected PO Box 56SS 1 Greenville, SC 29606 426 Nit -forest Way Greenville, SC 29607 ,Hain 864.232.1556 f.,w 864,232-6140 rogersandcallcott.001T1 0310612015 08: d3 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 8 of 10 Rogers & Callcott CHAIN ENVIRONMENTAL Mailing PO Box 5655 Shipping 426 FairfWay 215E Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Client Name �d lam, Address 'ye CK_ i N C- Report To: Email Address Telephone # PO # Project # �3' 1Z OF CUSTODY RECORD WORKORDER 50)-tDCOW (U ry v 0. 3 :' ai QJ E M CL Filtered (Yes/No) � YN Cooled (yes/No) ) (r Container Type (Plastic/Glass) `/ d Container Volume (mQ Sample Type (Grab/Composite) G V✓ Sample Source (WW, GW, DW, SW, S, Other) -- - Preservation Codes) A— None E — HCI I — Zn Acetate B - HNO3 F - Na2S203 J - H3PO4 C-H2SOa G - Boric Acid K -MCAA D- NaOH H-Ascorbic Acid L �� P . R&C WORK ORDER yR/S DATE TIME SAMPLE DESCRIPTION COMMENTS SAMPLE — R ED BY: 1 f� RELINQ (SHED BY: 3 DATE/TIME: 6 DATE/TIME: RECEIVED BY: z. RECEIVED BY: 4. DATE/TIME: I ),� DATE/TIME: Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: RELINQUISHED BY: DATE/TIME: RECEIVED BY: 6. DATE/TIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt �, L' °C ELINQUISHED BY: DATE/TIME: RECEIVED BY: 8• DATE/TIME: o sible Hazards associated with samples: Non -Hazard ❑Flammable ❑Skin Irritant 1-1 Poison ElUnknown EDDther Form Revised July, 2014 Page ___L of I 0 Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Date Client: CR'((kL-eP- '- Received: �2 116 Carrier Name: Client FedEx Tracking Number: UPS US Mail Courier Work Order: g 50 oZ0(Q `6l0 (eld Service 1 Other: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? �( COC included with samples? COC signed when relinquished and received? X Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? X Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? X Samples received within holding time? X Sample volume sufficient for analysis? X VOA vials free of headspace (<6mm bubble)? Samples cooled? Temp at receipt recorded on COC Temp measured with IR thermometer - SN: 97050067 \ . IceCold Packs Dry Ice None Samples requiring pH preservation at proper pH? (Vote: Samples for metals analysis may be preserved upon receipt in the lab. � �V1 ( jo Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? { dr If in-house preservation used — record Lot # HCL H,pO, H,SOa NaOH HNO, Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by: Page 10 of 10 Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: Laboratory Report Project: Work Order: Received: L0001 OLUI Y Services M51 INW6:45 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on January 09, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit 4WQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: X / 1119 )ae' 6/ � Kara Hrkach Project Manager This report may not be reproduced, excepl in full, without writlen permission from Rogers & Callcott, Inc. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company Page 1 of 11 Rogers &Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf- Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5010477-01 Influent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratory Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab 1D 880 Project: Influent Work Order: 5010477 Received: 01 /09/2015 16:45 Matrix Sampled Type Ground Water 01/09/15 11:32 Grab PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0112312015 11:18 This report may not be reproduced, except in full, without written permission from Rogers c& Callcon. Inc. page 2 Of 11 a Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Sample Data Sample Number 5010477-01 Sample Description Influent Grab collected on 01/09/15 11:32 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analvst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 1.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 1, 1 -Dichloroethane 1.0 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW BSA0702 l,l-Dichloroethene 1.2 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 1,2,4-Trimethylbenzene ND 1.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 1,2-Dichloroethane 1.2 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Acetone ND 20.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Benzene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260E LBW B5A0702 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Chloroform 11.4 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260E LBW B5A0702 Ethylbenzene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Hexane ND 1.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Isopropylbenzene ND 1.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 m,p-Xylene ND 1.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Methylene chloride ND 2.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Naphthalene ND 4.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 n-Butylbenzene ND 2.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW BSA0702 n-Propylbenzene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 o-Xylene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW 135A0702 sec-Butylbenzene ND 1.0 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Styrene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 tert-Butylbenzene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 Toluene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW B5A0702 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260B LBW BSA0702 Vinyl chloride ND 0.5 ug/L 1.00 01/12/15 13:03 EPA 8260E LBW B5A0702 Rebatch Sample Number: 5010477-01RE1 cis-1,2-Dichloroethene 71.9 2.5 ug/L 5.00 01/12/15 20:41 EPA 8260B LBW B5A0702 Tetrachloroethene 154 2.5 ug/L 5.00 01/12/15 20:41 EPA 8260B LBW B5A0702 Trichloroethene 131 2.5 ug/L 5.00 01/12/15 20.41 EPA 8260B LBW B5A0702 Surrogates % REC % REC Limits Flag 1,2-Dichloroethane-D4 85 70-130 4-BromoJluorobenzene 89 70-130 Toluene-d8 79 70-130 Rebatch Sample Number: 5010477-01RE1 1,2-Dichloroethane-D4 79 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 01,12312015 11:18 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 3 of 11 , Rogers & Cakott ENVIRONMENTAL Catalent Phanna Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Sample Number 5010477-OIRE1 Sample Description Influent Grab collected on 01/09/15 11:32 Reporting Parameter Result Limit CTnits DIP Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5010477-01RE1 J-Bromofluorobenzene 92 70-130 Toluene-d8 84 70-130 PO Box 5655 1 Greenville, SC 29606 ' 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 ': fax 864.232.6140 rogersandcallcott.eom an employee -owned company 0112312015 11:18 This report may not be reproduced, except in full, without written permission from Rogers & Collcon, Inc. Page 4 of 11 OW Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5A0702 - EPA 5030 Blank (B5A0702-BLK1) 1,1,1-Trichloroethane ND 1.0 ug/L 1,1-Dichloroethane ND 0.5 ug/L 1,1-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 1.0 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 2.0 ug/L Chloroform ND 0.5 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L Isopropylbenzene ND 1.0 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 4.0 ug/L n-Butylbenzene ND 2.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Buylbenzene ND 1.0 ug/L Styrene ND 0.5 ug/L tert-Buylbenzene ND 0.5 ug/L Tetrachloroethene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L Surrogate:l,2-Drehloroethane-D4 94 70-130 Surrogate: 4-Bromo luorobemene 77 70-130 Surrogate: Toluene-& 81 70-130 LCS (B5A0702-BSI) 1,1,1-Trichloroethane 18.4 1.0 ug/L 20.0 92 70-130 1,1-Dichloroethane 19.2 0.5 ug/L 20.0 96 70-130 1,1-Dichloroethene 19.4 0.5 ug/L 20.0 97 70-130 1,2,4-Trimethylbenzene 18.8 1.0 ug/L 20.0 94 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way Greenville, SC 29607 ' main 864.232.1556 (fax 864.232.6140 rogersandcallcott.eom an employee -owned company 0112312015 11:18 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott. Inc. Page 5 of 11 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5A0702 - EPA 5030 LCS (B5A0702-BSI) 1,2-Dichloroethane 20.6 0.5 ug/L 20.0 103 70-130 Acetone 82.5 20.0 ug/L 100 82 60-140 Benzene 21.3 0.5 ug/L 20.0 107 70-130 Bromomethane (Methyl Bromide) 18.3 2.0 ug/L 20.0 92 60-140 Chloroform 20.6 0.5 ug/L 20.0 103 70-130 cis-1,2-Dichloroethene 18.9 0.5 ug/L 20.0 95 70-130 Ethylbenzene 20.9 0.5 ug/L 20.0 104 70-130 Hexane 21.0 1.0 ug/L 20.0 105 70-130 Isopropylbenzene 21.4 1.0 ug/L 20.0 107 70-130 m,p-Xylene 40.6 1.0 ug/L 40.0 102 70-130 Methylene chloride 18.1 2.0 ug/L 20.0 91 70-130 Naphthalene 14.1 4.0 ug/L 20.0 71 70-130 n-Butylbenzene 17.2 2.0 ug/L 20.0 86 70-130 n-Propylbenzene 21.1 0.5 ug/L 20.0 106 70-130 o-Xylene 19.9 0.5 ug/L 20.0 99 70-130 sec-Butylbenzene 17.8 1.0 ug/L 20.0 89 70-130 Styrene 20.2 0.5 ug/L 20.0 101 70-130 tert-Butylbenzene 20.5 0.5 ug/L 20.0 102 70-130 Tetrachloroethene 20.4 0.5 ug/L 20.0 102 70-130 Toluene 18.8 0.5 ug/L 20.0 94 70-130 trans-1,2-Dichloroetliene 20.7 0.5 ug/L 20.0 103 70-130 Trichloroethene 23.0 0.5 ug/L 20.0 115 70-130 Vinyl chloride 22.3 0.5 ug/L 20.0 112 60-140 Surrogate: 1,2-Diehloroethane-D4 102 70-130 Surrogate:4-Bromofluorobenzene 87 70-130 Surrogate: Toluene-& 101 70-130 Matrix Spike (B5A0702-MS1) Source: 5010302-10 1,I,1-Trichloroethane 19.3 1.0 ug/L 20.0 ND 96 70-130 1,1-Dichloroethane 19.0 0.5 ug/L 20.0 ND 95 70-130 1,1-Dichloroethene 22.8 0.5 ug/L 20.0 ND 114 70-130 1,2,4-Trimethylbenzene 21.0 1.0 ug/L 20.0 ND 105 70-130 1,2-Dichloroethane 19.8 0.5 ug/L 20.0 ND 99 70-130 Acetone 85.1 20.0 ug/L 100 ND 85 60-140 Benzene 16.6 0.5 ug/L 20.0 ND 83 70-130 Bromomethane (Methyl Bromide) 19.2 2.0 ug/L 20.0 ND 96 60-140 PO Box 5655 Greenville, SC 29606 1 426 Fairforest Way i Greenville, SC 29607 1 main 864.232.1556 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0112312015 11:18 This report may not be reproduced, except in full, without written permission from Rogers & Callcolt, Inc. Page 6 of 11 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5A0702 - EPA 5030 Matrix Spike (B5A0702-MSl) Source: 5010302-10 Chloroform 17.3 0.5 ug/L 20.0 ND 86 70-130 cis-1,2-Dichloroethene 22.5 0.5 ug/L 20.0 ND 112 70-130 Ethylbenzene 17.5 0.5 ug/L 20.0 ND 87 70-130 Hexane 21.0 1.0 ug/L 20.0 ND 105 70-130 Isopropylbenzene 21.1 1.0 ug/L 20.0 ND 106 70-130 m,p-Xylene 42.2 1.0 ug/L 40.0 ND 106 70-130 Methylene chloride 16.0 2.0 ug/L 20.0 ND 80 70-130 Naphthalene 14.9 4.0 ug/L 20.0 ND 74 70-130 n-Butylbenzene 17.9 2.0 ug/L 20.0 ND 90 70-130 n-Propylbenzene 21.2 0.5 ug/L 20.0 ND 106 70-130 o-Xylene 16.4 0.5 ug/L 20.0 ND 82 70-130 sec-Buylbenzene 20.9 1.0 ug/L 20.0 ND 104 70-130 Styrene 20.6 0.5 ug/L 20.0 ND 103 70-130 tert-Buylbenzene 23.0 0.5 ug/L 20.0 ND 115 70-130 Tetrachloroethene 19.6 0.5 ug/L 20.0 ND 98 70-130 Toluene 16.3 0.5 ug/L 20.0 ND 82 70-I30 trans-1,2-Dichloroethene 21.1 0.5 ug/L 20.0 ND 106 70-130 Trichloroethene 20.2 0.5 ug/L 20.0 ND 101 70-130 Vinyl chloride 21.7 0.5 ug/L 20.0 ND 109 60-140 Surrogate:1,2-Diehloroethane-D4 97 70-130 Surrogate: 4-Bromojluorobenzene 94 70-130 Surrogate: Toluene48 97 70-130 Matrix Spike Dup (B5A0702-MSD1) Source: 5010302-10 1,1,1-Trichloroethane 17.3 1.0 ug/L 20.0 ND 86 70-130 11 20 1,1-Dichloroethane 17.4 0.5 ug/L 20.0 ND 87 70-130 9 20 1,1-Dichloroethene 19.8 0.5 ug/L 20.0 ND 99 70-130 14 20 1,2,4-Trimethylbenzene 19.6 1.0 ug/L 20.0 ND 98 70-130 7 20 1,2-Dichloroethane 19.3 0.5 ug/L 20.0 ND 97 70-130 2 20 Acetone 87.0 20.0 ug/L 100 ND 87 60-140 2 20 Benzene 15.6 0.5 ug/L 20.0 ND 78 70-130 6 20 Bromomethane (Methyl Bromide) 17.8 2.0 ug/L 20.0 ND 89 60-140 7 20 Chloroform 16.2 0.5 ug/L 20.0 ND 81 70-130 6 20 cis-1,2-Dichloroethene 20.6 0.5 ug/L 20.0 ND 103 70-130 9 20 Ethylbenzene 16.4 0.5 ug/L 20.0 ND 82 70-130 6 20 Hexane 18.7 1.0 ug/L 20.0 ND 93 70-130 12 20 PO Box 5655 1 Greenville, SC 29606 1 426 Faitforest Way Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company 0112312015 11:18 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc Page 7 of 11 Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result % REC Limits RPD Limit Flags Batch B5A0702 - EPA 5030 Matrix Spike Dup (B5A0702-MSD1) Source: 5010302-10 Isopropylbenzene 19.5 1.0 ug/L 20.0 ND 98 70-130 8 20 m,p-Xylene 38.3 1.0 ug/L 40.0 ND 96 70-130 10 20 Methylene chloride 15.3 2.0 ug/L 20.0 ND 77 70-130 5 20 Naphthalene 16.7 4.0 ug/L 20.0 ND 83 70-130 11 20 n-Butylbenzene 16.3 2.0 ug/L 20.0 ND 81 70-130 10 20 n-Propylbenzene 19.6 0.5 ug/L 20.0 ND 98 70-130 8 20 o-Xylene 15.7 0.5 ug/L 20.0 ND 78 70-130 5 20 sec-Butylbenzene 19.0 1.0 ug/L 20.0 ND 95 70-130 9 20 Styrene 19.5 0.5 ug/L 20.0 ND 98 70-130 5 20 tert-Butylbenzene 20.7 0.5 ug/L 20.0 ND 104 70-130 10 20 Tetrachloroethene 17.6 0.5 ug/L 20.0 ND 88 70-130 11 20 Toluene 15.3 0.5 ug/L 20.0 ND 76 70-130 7 20 trans-1,2-Dichloroethene 19.0 0.5 ug/L 20.0 ND 95 70-130 10 20 Trichloroethene 18.2 0.5 ug/L 20.0 ND 91 70-130 10 20 Vinyl chloride 19.2 0.5 ug/L 20.0 ND 96 60-140 12 20 Surrogate: 1, 2-Dichloroethane-D4 Surrogate: 4-Bromofluoroben_ene Surrogate: Toluene-d8 95 70-130 92 70-130 91 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 ': fax 864.232.6140 rogersandcallcott.com an employee -owned company 0112312015 11:18 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 8 of 11 Rogers & CaRcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5010477 Monroe, NC 28110 Reported: 01/23/15 11:18 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com - an employee -owned company 0112312015 11:18 This report may not be reproduced except in full, without written permission from Rogers & Callcott, Inc. Page 9 of 11 Rogers & Callcott CHAIN E N V I R O N M E N TA L Mailing PO Box 5655 Shipping 426 Fairforest Way 215B Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (903) 5D9-8999 Catalent Client Name Address Monroe, NC Report To: Email Address Telephone# PO # Project # 93-121 OF CUSTODY RECORD WORK ORDER v c m o u o � Z M ~ N Filtered (Yes/No) Y Cooled (Yes/No) G Container Type (Plastic/Glass) 40 Container Volume (mL) G Sample Type (Grab/Composite) GW Sample Source (WW, GW, DW, SW, 5, Other) Preservation Code(s) A — None E — HCI I — Zn Acetate B—HNO3 F—Na2Sz03 J—H3PO4 C—HzSO4 G — Boric Acid K -MCAA D — NaOH H — Ascorbic Acid L - u 0j WORK ORDER DATE TIME SAMPLE DESCRIPTION COMMENTS SOlOIh W-p )8 ) 115 �C; �_l *3 vials unpres, 1 HC1 Effluent 5 01 04— (,O —01 pH - %'3 Collected on )/y�/3 @ W5 Temp - 13, ZtbY TM F SAMP R�HED BY: 1 (/19 DATE/TIME: /S10'S2 D " I P� XPTMj� � omposite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: RELItfQUISHED BY: 3. ATE/TIME: RECEIVED W 4• I DATE/TIME: RELINQUISHED BY: 5. DATE/TIME: RECEIVED BY: 6. DATE/TIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt `/, Z °C RELINQUISHED BY: T DATE/TIME: RECEIVED BY: 8. DATE/TIME: Possible Hazards associated with samples: 7Non-Hazard 7FIammable Skin Irritant Poison FlUnknown El?ther Form Revised July, 2014 Page r Rogers & Callcott - ENVIRONMENTAL Sample Receipt Verification Date Work Client: C %LgP,1-c Received: L, C1 . 1157 Order: 4S_0 [y(J-7"7 Carrier Name: Client FedEx UPS US Mail Courier Field Services Other: Tracking Number: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled? Temp measured with IR thermometer - SN: 97050067 Ice Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. C C C Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? If in-house preservation used — record Lot # HCL H3P0, H2S0, NaOH HNO3 Other Comments: Were non-conformance issues noted at sample receipt? Yes or ( No 1 Non -Conformance issue other than noted above: Revised July 2014 Completed by: V (�[ Page 11 of 11 Rogers &Callcott ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Dear Client: qe� Laboratory Report Project: Work Order: Received: Laboratory s 5020286 9006:21 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on February 05, 2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request. Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Hrkach, your Project Manager, at kara.hrkach@rogersandcallcott.com or (864)-335-4956 if you have any questions about this report. Permit #W00010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Kara Hrkach Project Manager This report may not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. PO Box 5655 1 Greenville, SC 296% 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee -owned company Page 1 of 12 j Rogers &Callcott ENVIRONMENTAL Certificate of Analysis Client Catalent Pharma Solutions C/O George Maalouf - Rogers and Callcott 2021 E. Roosevelt Blvd. Monroe, NC 28110 Sample Number Sample Description 5020286-01 Influent Grab South Carolina Greenville Laboratory Identification 23105 South Carolina Columbia Laboratory Identification 40572 North Carolina Laboratot Certification Number 27 North Carolina Drinking Water Lab Number 45710 NELAP Utah Certificate Number SC000042014-1 Georgia Drinking Water Lab ID 880 Project: Influent Work Order: 5020286 Received: 02/05/2015 16:21 Matrix Sampled Type Ground Water 02/05/15 12:16 Grab PO Box 56S5 1 Greenville, SC 29606 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0310212015 14:39 This report may not be reproduced, except in full, without written pennission from Rogers & Callcou, Inc. Page 2 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Sample Data Sample Number 5020286-01 Sample Description Influent Grab collected on 02/05/15 12:16 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analvst Batch Volatile Organics 1, 1, 1 -Trichloroethane ND 1.0 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW 135110719 1,1-Dichloroethane 0.6 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW BSB0719 1,1-Dichloroethene 0.9 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5B0719 1,2,4-Trimethylbenzene ND 1.0 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW B5130719 1,2-Dichloroethane 0.8 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW 115110719 Acetone ND 20.0 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 Benzene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 Bromomethane (Methyl Bromide) ND 1.0 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5110719 Chloroform 8.2 1.0 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5B0719 cis-1,2-Dichloroethene 43.9 0.5 us/L 1.00 02/09/15 14:40 EPA 9260B LBW B5B0719 Ethylbenzene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5110719 Hexane ND 1.0 u8/1- 1.00 02/09/15 14:40 EPA9260B SI LBW B5110719 Isopropylbenzene ND 1.0 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW 115110719 m,p-Xylene ND 1.0 -911- 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 Methylene chloride ND 2.0 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5B0719 Naphthalene ND 4.0 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 n-Butylbenzene ND 2.0 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW 115130719 n-Propylbenzene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW 135130719 o-Xylene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 sec-Butylbenzene ND 1.0 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5B0719 Styrene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW 115110719 tert-Butylbenzene ND 0.5 U911- 1.00 02/09/15 14:40 EPA 8260B LBW 115110719 Toluene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 trans-1,2-Dichloroethene ND 0.5 ug/L 1.00 02/09/15 14:40 EPA 8260E LBW B5B0719 Vinyl chloride ND 0.5 us/L 1.00 02/09/15 14:40 EPA 8260B LBW B5B0719 Rebatch Sample Number: 5020286-01RE1 Tetrachloroethene 117 2.5 ug/L 5.00 02/12/15 20:43 EPA 8260B LBW B5B0934 Trichloroethene 88.6 2.5 ug/L 5.00 02/12/15 20:43 EPA 8260E LBW B5B0934 Surrogates %REC %REC Limits Flag 42-Dichloroethane-D4 77 70-130 4-BromoJluorobenzene 101 70-130 Toluene-d8 85 70-130 Rebatch Sample Number: 5020286-01RE1 1,2-Dichloroethane-D4 74 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 fax 864.232.6140 rogersandcalicott.com an employee -owned company 0310212015 14:39 This report mqv not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. Page 3 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Sample Number 5020286-01RE1 Sample Description Influent Grab collected on 02/05/15 12:16 Reporting Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch Volatile Organics Surrogates %REC %REC Limits Flag Rebatch Sample Number: 5020286-01RE1 4-Bromo luorobenzene 102 70-130 Toluene-D8 85 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairtorest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0310212015 I4: 39 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 4 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5B0719 - EPA 5030 Blank (B5B0719-BLK1) 1,1,1-Trichloroethane ND 1.0 ug/L 1,1-Dichloroethane ND 0.5 ug/L 1,1-Dichloroethene ND 0.5 ug/L 1,2,4-Trimethylbenzene ND 1.0 ug/L 1,2-Dichloroethane ND 0.5 ug/L Acetone ND 20.0 ug/L Benzene ND 0.5 ug/L Bromomethane (Methyl Bromide) ND 1.0 ug/L Chloroform ND 1.0 ug/L cis-1,2-Dichloroethene ND 0.5 ug/L Ethylbenzene ND 0.5 ug/L Hexane ND 1.0 ug/L Isopropylbenzene ND 1.0 ug/L m,p-Xylene ND 1.0 ug/L Methylene chloride ND 2.0 ug/L Naphthalene ND 4.0 ug/L n-Butylbenzene ND 2.0 ug/L n-Propylbenzene ND 0.5 ug/L o-Xylene ND 0.5 ug/L sec-Butylbenzene ND 1.0 ug/L Styrene ND 0.5 ug/L tert-Butylbenzene ND 0.5 ug/L Toluene ND 0.5 ug/L trans-1,2-Dichloroethene ND 0.5 ug/L Vinyl chloride ND 0.5 ug/L .Surrogate:l,2-Diclrloroethane-D4 75 70-130 Surrogate: 4-Bromofluorobenzene 101 70-130 Surrogate: Toluene-d8 87 70-130 LCS (B5B0719-BSI) 1,1,1-Trichloroethane 22.4 1.0 ug/L 20.0 112 70-130 1,1-Dichloroethane 19.7 0.5 ug/L 20.0 98 70-130 1,1-Dichloroethene 23.2 0.5 ug/L 20.0 116 70-130 1,2,4-Trimethylbenzene 22.5 1.0 ug/L 20.0 112 70-130 1,2-Dichloroethane 20.0 0.5 ug/L 20.0 100 70-130 Acetone 91.6 20.0 ug/L 100 92 60-140 PO Box 5655 1 Greenville, SC 29606 i 426 Fairforest Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0310212015 14:19 This report mqv not be reproduced, except in full, without written pennission from Rogers & Callcott, Inc. Page 5 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Phartna Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Yarametcr Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5B0719 - EPA 5030 LCS (B5B0719-BS1) Benzene 19.6 0.5 ug/L 20.0 98 70-130 Bromomethane (Methyl Bromide) 23.1 1.0 ug/L 20.0 115 60-140 Chloroform 19.4 1.0 ug/L 20.0 97 70-130 cis-1,2-Dichlomethene 21.9 0.5 ug/L 20.0 110 70-130 Ethylbenzene 21.0 0.5 ug/L 20.0 105 70-130 Hexane 24.1 1.0 ug/L 20.0 121 70-130 Isopropylbenzene 22.1 1.0 ug/L 20.0 110 70-130 m,p-Xylene 40.1 1.0 ug/L 40.0 100 70-130 Methylene chloride 19.5 2.0 ug/L 20.0 97 70-130 Naphthalene 17.9 4.0 ug/L 20.0 90 70-130 n-Butylbenzene 25.2 2.0 ug/L 20.0 126 70-130 n-Propylbenzene 22.6 0.5 ug/L 20.0 113 70-130 o-Xylene 21.0 0.5 ug/L 20.0 105 70-130 sec-Butylbenzene 23.2 1.0 119/1. 20.0 116 70-130 Styrene 19.6 0.5 ug/L 20.0 98 70-130 tert-Butylbenzene 21.4 0.5 ug/L 20.0 107 70-130 Toluene 20.9 0.5 ug/L 20.0 104 70-130 trans-1,2-Dichloroethene 22.0 0.5 ug/L 20.0 110 70-130 Vinyl chloride 20.9 0.5 ug/L 20.0 104 60-140 Surrogate: 1.2-Dichloroethane-D4 97 70-130 Surrogate: 4-Bromofluorobenzene 101 70-130 Surrogate: Toluene-d8 101 70-130 Matrix Spike (B5B0719-MS1) Source: 5020286-01 1,1,1-Trichloroethane 24.3 LO ug/L 20.0 ND 121 70-130 1,1-Dichloroethane 22.1 0.5 ug/L 20.0 0.6 108 70-130 l,l-Dichloroethene 25.3 0.5 ug/L 20.0 0.9 122 70-130 1,2,4-Trimethylbenzene 22.7 1.0 ug/L 20.0 ND 114 70-130 1,2-Dichloroethane 21.8 0.5 ug/L 20.0 0.8 105 70-130 Acetone 97.7 20.0 ug/L 100 ND 98 60-140 Benzene 21.2 0.5 ug/L 20.0 ND 106 70-130 Bromomethane (Methyl Bromide) 25.3 1.0 ug/L 20.0 ND 126 60-140 Chloroform 28.8 1.0 ug/L 20.0 8.2 103 70-130 cis-1,2-Dichloroethene 67.9 0.5 ug/L 20.0 43.9 120 70-130 Ethylbenzene 21.5 0.5 ug/L 20.0 ND 107 70-130 Hexane 27.2 1.0 ug/L 20.0 ND 136 70-130 s I PO Box 5655 1 Greenville, SC 29606 1 426 Fairiorest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864,232.6140 rogersandcallcott.eom an employee-ovvned company 0310212015 14:39 This report mqy not be reproduced, except in full, without written permission, from Rogers & Callcon. Inc. Page 6 of 12 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5B0719 - EPA 5030 Matrix Spike (115110719-MSI) Source: 5020286-01 Isopropylbenzene 22.9 1.0 ug/L 20.0 ND 115 70-130 m,p-Xylene 43.9 LO ug/L 40.0 ND 109 70-130 Methylene chloride 19.9 2.0 ug/L 20.0 ND 99 70-130 Naphthalene 18.8 4.0 ug/L 20.0 ND 89 70-130 n-Butylbenzene 24.7 2.0 ug/L 20.0 ND 124 70-130 n-Propylbenzene 22.9 0.5 ug/L 20.0 ND 114 70-130 o-Xylene 21.7 0.5 ug/L 20.0 ND 108 70-130 sec-Butylbenzene 23.3 1.0 ug/L 20.0 ND 116 70-130 Styrene 20.2 0.5 ug/L 20.0 ND 101 70-130 tert-Butylbenzene 23.1 0.5 ug/L 20.0 ND 115 70-130 Toluene 21.3 0.5 ug/L 20.0 ND 106 70-130 trans-1,2-Dichloroethene 24.1 0.5 ug/L 20.0 ND 120 70-130 Vinyl chloride 23.9 0.5 ug/L 20.0 ND 120 60-140 Surrogate: 1,2-Diehloroethane-D4 102 70-130 Surrogate: 4-Bromofluorobenzene 104 70-130 Surrogate: Toluene-& 104 70-130 Matrix Spike Dup (115110719-MSDI) Source: 5020286-01 1,1,1-Trichloroethane 21.6 1.0 ug/L 20.0 ND 108 70-130 12 20 l,l-Dichloroethane 19.6 0.5 ug/L 20.0 0.6 95 70-130 12 20 1,1-Dichloroethene 22.1 0.5 ug/L 20.0 0.9 106 70-130 13 20 1,2,4-Trimethylbenzene 21.4 1.0 ug/L 20.0 ND 107 70-130 6 20 1,2-Dichloroethane 21.2 0.5 ug/L 20.0 0.8 102 70-130 3 20 Acetone 99.6 20.0 ug/L 100 ND 100 60-140 2 20 Benzene 18.4 0.5 ug/L 20.0 ND 92 70-130 14 20 Bromomethane (Methyl Bromide) 22.3 1.0 ug/L 20.0 ND 111 60-140 13 20 Chloroform 26.0 1.0 ug/L 20.0 8.2 89 70-130 10 20 cis-1,2-Dichloroethene 63.4 0.5 ug/L 20.0 43.9 98 70-130 7 20 Ethylbenzene 19.7 0.5 ug/L 20.0 ND 98 70-130 9 20 Hexane 24.1 1.0 ug/L 20.0 ND 120 70-130 12 20 Isopropylbenzene 20.3 1.0 ug/L 20.0 ND 102 70-130 12 20 m,p-Xylene 40.0 1.0 ug/L 40.0 ND 100 70-130 9 20 Methylene chloride 18.6 2.0 ug/L 20.0 ND 93 70-130 6 20 Naphthalene 20.4 4.0 ug/L 20.0 ND 97 70-130 8 20 n-Butylbenzene 22.0 2.0 ug/L 20.0 ND 110 70-130 12 20 n-Propylbenzene 20.9 0.5 ug/L 20.0 ND 104 70-130 9 20 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way Greenville, SC 29607 1 main 864.232.1556 I fax 864.232,6140 rogersandcallcott.eom an employee -owned company 03102/2015 14:39 This report may not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 7 of 12 0& Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Volatile Organics Quality Control Summary Reporting Spike Source % REC RI'D Parameter Result Limit Units Level Result %REC Limits Kill) Limit Flags Batch B5B0719 - EPA 5030 Matrix Spike Dup (B5B0719-MSDl) Source: 5020286-01 o-Xylene 19.7 0.5 ug/L 20.0 ND 98 70-130 10 20 sec-Butylbenzene 21.2 1.0 ug/L 20.0 ND 106 70-130 9 20 Styrene 19.2 0.5 ug/L 20.0 ND 96 70-130 5 20 tert-Butylbenzene 21.0 0.5 ug/L 20.0 ND 105 70-130 9 20 Toluene 19.5 0.5 ug/L 20.0 ND 98 70-130 9 20 trans-1,2-Dichloroethene 21.4 0.5 ug/1. 20.0 ND 107 70-130 12 20 Vinyl chloride 21.1 0.5 ug/L 20.0 ND 106 60-140 12 20 Surrogate:l,2-Dichloroethane-D4 96 70-130 Surrogate:4-Bromofluorobenzene 99 70-130 Surrogate: Toluene-d8 96 70-130 Batch B5B0934 - EPA 5030 Blank (B5BO934-BLK1) Tetrachloroethene ND 0.5 ug/L Trichloroethene ND 0.5 ug/L Surrogate:l,2-Dichloroethane-D4 70 70-130 Surrogate:4-Bromofluorobenzene 99 70-130 Surrogate: Toluene-D8 85 70-130 LCS (B5B0934-BSl) Tetrachloroethene 19.7 0.5 ug/L 20.0 98 70-130 Trichloroethene 22.1 0.5 ug/L 20.0 110 70-130 Surrogate:l,2-Dichloroethane-D4 90 70-130 Surrogate: 4-Bromofluorobenzene 94 70-130 Surrogate: Toluene-D8 99 70-130 Matrix Spike (B5B0934-MSl) Source: 5020286-OIRE1 Tetrachloroethene 215 2.5 ug/L 100 117 98 70-130 Trichloroethene 189 2.5 ug/L 100 88.6 99 70-130 Surrogate: 1.2-Dichloroethane-D4 99 70-130 Surrogate:4-Bromofluorohenzene 97 70-130 Surrogate: Toluene-D8 100 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.eom an employee owned company 03102,2015 14:39 This report muy not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 8 of 12 Rogers &Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Volatile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags Batch B5B0934 - EPA 5030 Matrix Spike Dup (B5B0934-MSD1) Source: 5020286-01RE1 Tetrachloroethene 199 2.5 ug/L 100 117 82 70-130 8 20 Trichloroethene 175 2.5 ug/L 100 88.6 86 70-130 7 20 Surrogate: 1, 2-Diehloroethane-D4 Surrogate: 4-Bromo luorobenzene Surrogate: Toluene-D8 94 70-130 93 70-130 94 70-130 PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.COm w an employee -owned company 03.10212015 14:39 This report mqv not be reproduced, except in full, without written permission from Rogers & Callcott, Inc. Page 9 of 12 Rogers & Cakott ENVIRONMENTAL Catalent Pharma Solutions Project: Influent 2021 E. Roosevelt Blvd. Work Order: 5020286 Monroe, NC 28110 Reported: 03/02/15 14:39 Data Qualifiers and Definitions ND Analyte NOT DETECTED at or above the reporting limit NR Not reported RPD Relative Percent Difference S 1 The matrix spike and / or the matrix spike duplicate sample recovery was not within control limits due to matrix interference. The Laboratory Control Sample (LCS) was within control limits. PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -owned company 0310212015 14:39 This report may not be reproduced, except in full, without written permission from Rogers & Callcotl, Inc. Page 10 of 12 Rogbrs & Callcott CHAIN E NV I R O N M EN TA L Mailing PO Box 5655 Shipping 426 Fairforest Way 2158 Stoneridge Drive Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, SC 29210 Phone (864) 232-1556 Fax (864) 232-6140 Phone (803) 509-8999 Client Name Catalent Address Monroe, NC Report To: Email Address Telephone # PO # Project # 93-121 OF CUSTODY RECORD WORK ORDER c 0 o Z +� �0 v Et; 12 'K F Filtered (Yes/No) Y Cooled (Yes/No) G Container Type (Plastic/Glass) 40 Container Volume (ml-) G Sample Type (Grab/Composite) GW Sample Source (WW, GW, DW, SW, S, Other) Preservation Code(s) A — None E — HCI I — Zn Acetate B—HNOs F— NazSzOa J—H3POn C—Hzso, G—Boric Acid K-MCAA D — NaOH H — Ascorbic Acid L - c Im a R&C WORK ORDER YRj` DATE TIME SAMPLE DESCRIPTION COMMENTS '25pW 215'OZ *3 vials unpres, 1 HCl "op.nop. p -o 1216 2(�i� Y Effluent 5uac�a�5 - o pH - t, uZ Collected on J20' Temp - is by SA QUISHED BY: A E/TIME: REC I ED BY: 2. �J , DATE/TIME: Composite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: RE QUISHED BY: 3 ATE/TIME: RECEIV D BY: 4. DATE/TIME: RELINQUISHED BY: i S DATEITIME: RECEIVED BY: 6' DATE/TIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt 0 , `� °C RELINQUISHED BY: 7. DATE/TIME: RECEIVED BY: 8• DATE/TIME: ssible Hazards associated with samples: Non -Hazard ❑Flammable Skin Irritant ElPoison DUnknown EDDther Form Revised July, 2014 Page �_ of Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Date Work Client: CA 'j prt-6- i- Received: • S 1 S Order: c)-d'U ast"o Carrier Name: Client FedEx UPS US Mail Courier Field Service Other: Tracking Number: Receipt Criteria Y e s N o N A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? Y_ COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample ID on COC agree with label on bottle(s)? X Date / time on COC agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? X Sample volume sufficient for analysis? VOA vials free of headspace (<6mm bubble)? Samples cooled? Temp at receipt recorded on COC Temp measured with IR thermometer- SN: 97050067 1 lce Cold Packs Dry Ice None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. V0 C cl-�VFYI Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? x If in-house preservation used — record Lot # HCL H,PO, I_ SO4 NaOH 1 IIVO, Other Comments: Were non-conformance issues noted at sample receipt? Yes or No Non -Conformance issue other than noted above: Revised July 2014 Completed by:v_�K-o Page 12 of 12 Cata le nf February 11, 2015 Catalent Phorma Solutions 2725 Scherer Drive North St. Petersburg, FL 33716 T 727.803.2100 F 727.803.2419 rlvrn.catalent.com Mr. Kyle Ketchum City of Monroe WWTP 775 Treeway Drive Monroe, North Carolina 28110 Subject: Effluent Discharge Report — LIUP # LP-001 Treated Groun wa err Catalent Pharma Solutions (Formerly R. P. Scherer)/Chelsea Laboratories Facility 2021 East Roosevelt Blvd., Monroe, North Carolina 28112 Dear Mr. Ketchum: Enclosed are the January 2015 effluent discharge and laboratory analysis reports for the referenced facility. No non -conformances were reported. Totalizer readings from the certified effluent flow meter were anomalously low from January 9 to January 13 (12 gallons) and January 19 to January 26 (91 gallons). Consequently, site personnel cleaned the flow meter on January 13 and the flow meter and associated filter on January 26. Flow measurements recorded on the enclosed flow report for these two periods represent the total flow recorded by the individual flow meters for each of the recovery wells. These measurements are within the normal range for the system. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate and complete, I am aware there are significant penalties for submitting false information, including the possibility of fine or imprisonment for knowing violations. If you have any questions or concerns, please contact Jeffery Rogers at 727-803-2282 (email: Jeffery. Rogers@catalent.com) or Stan Golaski of Rogers & Callcott at 864-335-4984 (email: stan.golaski@rogersandcallcott.com). Sincerely, Cata) nt Pharm�SoJutions (2//JJ 11 r Dina Kostakis ' General Manager Enclosures Date cc with attachments: Stan Golaski, Rogers & Callcott Environmental Jerry Sullivan, Aqua -Trot (on -site file) Receiving POTW NPDES #: NCO024333 Effective Date for these Limits: 7/1113 Expiration Date for these Limits: 6/30/16 LILIP #: LP-001 Pipe #: 01 Reporting Period: January 2015 Date &Time of Reading Days Between Readings g Meter Reading (gal) Weekly Flow 1 (gal) Weekly Average 2 (mgpd) Tetrachloro- ethene u /L (9 ) Trichloro- ethene u /L (9 ) 82603 (ug/L) pH (units) Comments 12/30/14 14: 00 10,576,072 1/9/151D:30 9.85 10,600,287 24,215 0.002457 j 1/13/1516:00 4.23 10.600,299 20,2051 0,004778 1/19/15 12:00 5.83 10,615,037 14,738 0.002527 <0.5 <0.5 BRDL 7.8 Sample and pH 1126/15 10:00 6.92 10,615,128 33,5974 0.004857 collected on January 9, 2015. Monthly Total 92,755 Maximum 0.004857 Minimum 1 0.002457 Sample Type I I Grab Grab Grab Grab Permit Limits 1 0.010000 8.85 1 81 monitor only 6 to 11 Flow between Meter Readings 2 Weekly Average = Weekly Flow / Days Between Readings Value represents total 8260 volatile organic compounds. BRDL= Below Reportable Detection Limits 4 Calculated based on total flow recorded by individual flow meters for each of the recovery wells. \\RC-VMSRV03\Projects\14\93-121\2015\RPTSIPOTW Reportsuanuary 2015\ January 2015 POTW Form.xlsx 2111/2015 Rogers & Callcott . ENVIRONMENTAL Client Catalent Pharma Solutions C/O George Maalouf- Rogers and Callcott 2021 E. Roosevelt Blvd. Monroc, NC 28110 Dear Client-. Laboratory Report Project: Nark Order: Received: Effluent 5010476 01/09/2015 16:45 Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of custody for samples that were received on January 09, 2015. Rogers and Callcott maintains a format QAIQC program. Unless otherwise noted, all analyses performed under NELAP certification have complied with all the requirements for the'rNI standard The analyses met the QA/QC confidence interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request - Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee, or the person responsible for delivering to the person addressed, you may not copy or deliver this message to anyone else. If you receive this message by mistake, please notify Rogers and Callcott immediately. We strive to provide excellent service to our clients. Please contact Kara Much, your Project Manager, at karahrkach@rogersandcallcoti-com or (864)-335-4956 if you have any questions about this report. Perot 4%VQ0010607 Catalent Pharma Solutions/Chelsea Labs Facility Groundwater Remediation Facilities Union County, NC CC: Stan Golaski - Rogers and Callcott Report Approved By: Kara Hrkach Project Manager This npori may nal be reproduces{ exceplinfsdl, Itiilumut u'rinen pernrissionjroni Rogers h Galleon, Inc. PO Box 56SS Greenville, SC 29606 s 426 Fairforest Way I Greenville, SC 29607 ' nuin 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com anemployee-owned company Page 1 of 11 Rogers & Callcott Ii „! ENVIRONMENTAL Certificate of Analysis 4 South Carolina Greenville Laboratory Identification 23105 South Carolina Caltunbia Laboretlory Ideni f cation 40572 A'orlb Carolina Labomroq Certification Number 27 Xor/h Carolbut Drinking fVater Lub Manher 45710 N6LAP Utah Cerliftcale Ahmtber SC000042014-1 Georgia Drinking fSnter Lah ID 810 Client Catalent Pharma Solutions Project: Effluent C/O George Manlouf-Rogers and Callcott Work Order: 5010476 2021 E. Roosevelt Blvd. Received: 01/09/2015 16:45 Monroe, NC 28110 Sample Number Sample Description \lams Sampled "I)pe 5010476-01 Effluent Grab Ground Water Ol/09/15 11:15 Grab 5010476-02 P luent Grab Ground Water 01/09/15 11:15 Grab PO Box 56SS I Greenville, SC 29606 1 426 hirforest Way 1 Greenville, SC 29607 ma;n 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com an employee -wined company 01.23 2015 10-39 Thlr mpmt may nor he reproduced except In joll, ulrlxua mrltrcnpermissron from Rogers t<CNleolr, Ine. Page 2 of 11 Rogers &VCallcott Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5010476 Monroe, NC 28110 Reported: O1/23/15 10:59 Sample Data Sample Number 5010476-01 Sample Description Effluent Grab collected on 0 1109/1 5 11:15 Reporting Parameter Result Limit Units OF Analyzed Method Flag Anatyst Batch Field Parameters pH 7.8 0A pit Units 1.00 OU09115 11:15 EPA9040C JHF BSA0311 Temperature 13.2 0.0 "C 1.00 01/09/15 11:15 SM25508-2010 ]lIF BSA03I1 Sample Number 5010476-02 Sample Description Effluent Grab collected on 0 U09/15 11:15 Reporting Parameter Result Limit Units OF Analyzed Alethod Flag Analyst Batch Volatile Organics 1,1,1-Trichloroethane ND 1.0 ug/L 1.00 01/12/15 20:11 EPA 8260B LBW B5A0702 1,1-Dichloroethane ND 0.5 ugrL 1.00 01/12115 20.11 EPA 9260B LBW B5AO702 1,1-Dichloroedtcne ND 0.5 ugtL 1.00 01/12/15 20:11 EPA9260B LBW B5AO702 1,2,4-Trimethylben7ene ND 1.0 ug/L 1.00 01/12115 20:11 EPA 8260B LBW B5A0702 1,2-Dichtorocthane ND 0.5 ugn- 1.00 01/12/15 20:11 EPA9260B La LBW BSA0702 Acetone ND 20.0 ug/L 1.00 01/12/15 20.11 EPA 9260E LBW B5A0702 Benzene ND 0.5 ug/L 1.00 01/12/15 20:11 EPA 826011 LBW BSA0702 Bromomethane (Methyl Bromide) ND 2.0 ug/L 1.00 01/12/15 20:11 EPA 8260B LBW BSA0702 Chloroform ND 0.5 ug/L L00 01/12/15 20:11 EPA 8260E LBW BSA0702 cis-1,2-Dichloroethene ND 0.5 ug/L 1.00 01/12/15 20:11 EPA9260B LBW MOM Ethytbenzene ND 0.5 ug/L 1.00 01/12/15 20:11 EPA9260B LBW BSA0702 Hexane ND L0 IJA 1.00 01/12/15 20.11 EPA9260B LBW B5A0702 Isopropylbenzene ND 1.0 ug/L 1.00 01112/15 20AI EPA92608 LBW B5AO702 tn,p-Xylene ND 1.0 UVL 1.00 01/12/15 20:1t EPAS260B LBW 135A0702 Methylene chloride ND 2.0 ug1L 1.00 01/12/15 20:11 EPAS260B LBW B5AO702 Naphthalene ND 4.0 ugtL 1.00 01/12/15 20:11 EPA 8260B LBW B5A0702 n-Butylbenzene ND 2.0 ugtL 1.00 01/12/15 20:11 EPA 8260B LBW BSA0702 n-Propylbenzene ND 0.5 ug/L 1.00 01/12/15 20:11 EPA9260B LBW BSA0702 o-Xylene ND 0.5 ug/L 1.00 01/12/15 20:11 EPA 8260B LBW BSA0702 sec-Butylbenzene ND 1.0 ug/L 1.00 01//2115 20:11 EPA 9260E LBW B5A0702 Styrene ND 0.5 ugiL 1.00 01/12/15 20:11 EPA 8260E LBW B5AO702 tert-Butylbenzene ND 0.5 ugJL 1.00 01/12/15 20:11 EPA 8260B LBW B5A0702 Tetrachloroethene ND 0.5 118/1. 1.00 01/12/15 20:11 EPAS260B LBW B5AO702 Toluene ND 0.5 118/1- 1.00 01/12/15 20:11 EPA8260B LBW B5A0702 trans-1,2-Dichloroediene ND 0.5 ugil. 1.00 01/12/15 20:11 EPA 8260B LBW B5A0702 Trichioroethene ND 0.5 ugR• 1.00 01/12/15 20.11 EPA 8260B LBW BSA0702 PO Box 5655 Greenville. SC 29606 ' 426 Fairforest Way Greenville, SC 29607 maln 864.232.1556 ; lax 864.232.6140 rogersandcallcott.com an employee termed company OR23.1015 10.19 77dr repo" nteo, tot be reproducett except in full, Wtlout irratatln r nissimt front Rogers R Calleou, bk. Page 3 of 11 Rogers & Callcott `> ENVIRONMENTAL Catalent Phanna Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5010476 Monroe, NC 28110 Reported: 01/23/15 10:59 Sample Number 5010476.02 Sample Description Effluent Grab collected on 01/09/15 11:15 Iteporling Parameter Itessdt Limit Units DF Analyzed Method Flag Analpt Balch Volatile Organics Vinyl chloride ND 0.5 nsn- 1.00 01/12/15 20:11 EPA 8260a Z LBW 135A0702 Surrogates %REC %REC Limits Flag 1,2-DichloroetAmx-D4 78 70-130 a-Lrom,Wuorohetnetro 95 70-130 Toluene-& 86 70-130 PO Box 5655 ! Greenville. SC 29606 ' 426 Fairforest Way ' Greenville. SC 29607 main 864.232.1556 ' fax 864.232.6140 rogersandeallcott.com an employee -caned company 0123 201S 10:59 7hir report mrrp flat he reprodrrced, except in fall, is ltlntut it riven p was0on from Rogers d• Cnilcon, hk. Page 4 of 11 Rogers & Callcott ENVIRONMENTAL Catatent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5010476 Monroe, NC 28110 Reported: 01/23/15 10:59 Volntile Organics Quality Control Summary Reporting Spike Source %REC RPD Parameter Result Limit Units Level Result •/REC limits RPD Limit Flags Batch B5A0702 - EPA 5030 Blank (115A0702-111,K1) 1,1, I•Trichloroethatte 1,1-Dichloroethane I,1-Dichtoroethene 1,2,4-Trimelhyl be%c nc 1,2-Dichlorocthane Acetone Benzene Bromomethane (hfelhyl Bromide) Chloroform cis- 1,2-Dichloroethene Ethylbenzene Hexane Isopropylbcnzcnc m,p ..\ylene Mohylene chloride Naphthalene n-Butylbenzene n-Propylbeazene o-aylene sec-Butylbenzene Styrene teft•Butylbenzene Tetrachloroethene Toluene trans-1,2-Dicldoroethene Tfichlorocthene Vinyl chloride LCS (135A0702-BSI ) NO NO NO NO NO NO NO NO A'D NO NO NO NO NO NO NO NO NO NO NO NO NO NO A'D NO NO NO Surrogate: 1, 2-Dichloroetluax-DJ Surrogate: 4-17rarna luarohewene Surrogate: rohtene45 1.0 0.5 0.5 1.0 0.5 20.0 0.5 2.0 0.5 0.5 0.5 1.0 1.0 1.0 2.0 4.0 2.0 0.5 0.5 LO 0.5 0.5 0.5 0.5 0.5 0.5 0.5 ug/1, ug/L ug/L ug/l, ug/L ug/L U91L u9fL ugq. ug/L ug/L ug/L ug/L us/L ug/L ug/L ug/L USIL ug1f. ug/L ug/L ug/L ugtl. ug11. ug/L ugfL ug/L 94 70-130 77 70-130 81 70-130 I,I,1-Trichloroethane 18.4 1.0 ug/L 20.0 92 70-130 1,1-Dichlorocthanc 19.2 0.5 ug/L 20.0 96 70-130 1,1-Dichloroethene 19.4 0.5 uyl. 20.0 97 70-130 1, 2,4 -Tri are thy] benzene 19.8 1.0 ug/1. 20.0 94 70.130 PO Box 5655 Greenville, SC 29606 1 426 Fair forest Way ' Grcenville, SC 29607 fm;n 864.232.1556 i fax 864.232.6140 rogersandcallcott.co111 an employee o;medcompany 0123 2015 10:59 Als report nlay trot he reprorhtied, except in full, without a rifnw p erndssionjront Rugerr rt Callcorf, Me. Page 5 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 F. Roosevelt Blvd. Work Order: 5010476 Monroe, NC 28110 Reported: O U23115 10:59 Volatile Organics Qualit}, Control SRninlary Reporting Spike Source •/.REC RPD Parameter Result Limit Units 1-tvel Result %REC Limits MID Limit Flags Batch B5A0702 - EPA 5030 LCS (115A0702-DSI) 1,2-Dichlomethane 20.6 0.5 ugtL 20.0 103 70-130 Acetone 82.5 20.0 Usti- too 82 60-140 Benzene 21.3 0.5 ug2 20.0 107 70-130 Bromomethane (Methyl Bromide) 18.3 2.0 ug/L 20.0 92 60-140 Chloroform 20.6 0.5 ug2 20.0 103 70-130 cis-1,2-Dithloroethene 18.9 0.5 ug/L 20.0 95 70-130 Ethylbenzene 20.9 0.5 ug/L 20.0 104 70-130 Hevaum 21.0 LO u92 20.0 105 70-130 Isopropylbenzene 21.4 1.0 1194. 20.0 107 70-130 m,p.Xylene 40.6 1.0 ug4. 40o 102 70-130 Methylene chloride 18.1 2.0 u92 20.0 91 70-130 Naphthalene 14.1 4.0 ug/L 20.0 71 70-130 n-Butylhenzene 17.2 2.0 ug4. 20.0 86 70.130 n-Propylbenzene 21.1 0.5 u92 20.0 106 70-130 o-Xylene 19.8 0.5 ug/L 20.0 99 70-130 sec-Butyllrenzene 17.8 1.0 ug2 20.0 89 70-130 Styrene 20.2 0.5 ug4. 20.0 101 70-130 ten-Butylbemcne 20.5 0.5 ug4. 20.0 102 70-130 "reuacldoroethene 20.4 0.5 ug/L 20.0 102 70-130 Toluene 18.8 0.5 ug/L 20.0 94 70-130 trans-1,2-Dichloroethene 20.7 0.5 ug/L 20.0 103 70-130 Trichloroethene 23.0 0.5 ug4. 20.0 115 70.130 Vinyl chloride 22.3 0.5 ug4. 20.0 112 60-140 Surrogate.- 1,2-D1ch1orx71uuw-DI 102 70-130 Surrogate: a-BromoJluoroMizene 87 70-130 Surrogate: Tohrerre-rIS 101 70-130 Alalriz Spike(B5A0702-MS1) Source:5010302-10 1,1,1-Trichlorocthane 11.3 1.0 ug/L 20.0 ND 96 70-130 I,l-Dichloroethane Mo 0.5 ug4. 20.0 ND 95 70-130 l,l-Dichloroethene 22.8 0.5 ug/L 20.0 ND 114 70-130 1,2,4-Trimethylbenzene 21.0 1.0 ug/L 20.0 ND 105 70-130 1,2-Dichlorocthane Ms 0.5 u92 20.0 ND 99 70-130 Acetone 85.1 20.0 ug/L 100 ND 85 60-140 Benzene 16.6 OS 1182 20.0 ND 83 70-130 Bromoniethane (Methyl Ilromide) 19.2 2.0 ug/L 20.0 ND 96 60-140 PO Box 5655 1 Greenville, SC 29606 426 fairtorest Way � Greenville, SC 29607 rmin 864.232.1556 1 fax 864.232.6140 rogersandcallcott.Com an employee -wined company 0123 2015 10:59 77dr repurr nrny rwt he reproduced,, exeepf rnJtll, U idwrrt trrfnen permission from Rogers h C bdeott, Inc. Page 6 of 11 Rogers & Callcott ENVIRONMENTAL Catalent Phanna Solutions Project: E111uent 2021 E. Roosevelt Blvd. Work Order: 5010476 Monroe, NC 28110 Reported: 01/23/15 10:59 Volatile OI-ganies Quality Control Sunllnary Reporting Spike Source % RFC RPD Parameter Result Limit Units level Result %RFC Lhnits RPD Until Flags Batch B5A0702 - EPA 5030 Ninlriz Spike (n5A0702-il1S1) Source: 50I0302-10 Chlorofomt t7.3 0.5 ug/L 20.0 No 86 70.130 c is. 1,2-Dichloroethene 22.5 0.5 ug/L 20.0 ND 112 70-130 Ethylbenzene 17.5 0-5 ug/l. 20.0 No 87 70-130 hexane 21.0 1.0 ug/l, 20.0 ND 105 70.130 Isopropylbenzene 21.1 1.0 ug/L 20.0 ND 106 70-130 m,p-\ylcnc 42.2 1.0 ug/L 40.0 ND 106 70-130 Methylene chloride 16.0 2.0 ug/L 20.0 ND 80 70-130 Naphthalene 14.9 4.0 ug/L 20.0 ND 74 70-130 n-Butylbenzene 17.9 2.0 ug/L 20.0 ND 90 70-130 n-Propylbcnzcne 21.2 0.5 ug/L 20.0 ND 106 70430 o-aylcnc 16.4 0.5 119/1. 20.0 ND 82 70-130 sec-Butylbenzene 20.9 1.0 ug/L 20.0 ND 104 70-130 Styrene 20.6 0.5 ue. 20.0 ND 103 70-130 tert-❑utylbenzene 23.0 0.5 ug/L 20.0 ND 115 70-130 Telrachloroethene 19.6 0.5 ug/L 20.0 ND 98 70430 Toluene 16.3 0.5 ugn. 20.0 ND 82 70-130 trans-1,2-Dichloroethene 21.1 0.5 ugfL 20.0 ND 106 70-130 Trichloroethene 20.2 0.5 ug/L 20.0 ND 101 70-130 Vinyl chloride 21.7 0.5 ug/L 20.0 ND 109 60-140 S'urrogate:1,2-Diehlorwilme-Dl 97 70-130 Surrogate: d-BromoJluoroh mene 94 70-130 Surrogare:7ohtene-dS 97 70.130 Alatrix Spike Dup (WA0702-JISDI) Source: 5010302-10 1.1, 1-Ttichlorocthanc 17.3 1.0 ug/L 20.0 ND 86 70.130 II 20 1,1-Dichlotoethane 17.4 0.5 ug/L 20.0 ND 87 70-130 9 20 M-Dichlotoethene 19.8 0.5 uaQ. 20.0 ND 99 70.130 14 20 1,2,4-Trimethylbenzene 19.6 Lo uSIL 20.0 ND 98 70-130 7 20 1,2-Dichloroethaae 19.3 0.5 ugrl, 20.0 ND 97 70-130 2 20 Acetone 87.0 20.0 ug/L 100 ND 87 60-140 2 20 Benzene 15.6 0.5 ug/L 20.0 ND 78 70-130 6 20 Bronlomethanc (Melhyl Bromide) IT8 2.0 ug/L 20.0 ND 89 60-140 7 20 Chloroform 16.2 0.5 ug/l. 20.0 ND 81 70-130 6 20 cis-1,2-Dichloroethene 20.6 0.5 ug,L 20.0 ND 103 70.130 9 20 Ethylbenzene 16.4 0.5 ugrL 20.0 ND 82 70-130 6 20 Hexane 18.7 1.0 ugfL 20.0 ND 93 70-130 12 20 PO Box 5655 i Greenville, SC 29606 ; 426 Fairforest Way Greenville, SC 29607 unln 864.232.1556 fax 864.232.6140 rogersandcallcott.com an employee-o•emed company 01431015 10:59 Mir report nuo, not he repnkh eJ, e.rcepi in fill, 101hold wNflenl¢massionfrom Rogers & Galleon, fire. Page 7 of 11 Rogers & callcott ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. Work Order: 5010476 Monroe, NC 28110 Reported: 01/23/15 10:59 Volatile Organics Quality Control Summary Reporting Spike Source %Rr.0 RI4a Parameter Result limit Units lxvel Result %REC Limits RPD Limit Flags Batch 115A0702 - EPA 5030 Matrix Spike Dup (115A0702-AISD1) Source: 5010302-10 lsopropylbenzene 19.5 1.0 ug/L 20.0 ND 98 70-130 8 20 m,p-Xylene 39.3 1.0 ug/L 40.0 ND 96 70.130 10 20 hiethylene chloride 15.3 2.0 ug/L 20.0 ND 77 70-130 5 20 Naphthalene 16.7 4.0 ug/L 20.0 ND 83 70-130 11 20 n-liutylbenrene 16.3 2.0 149/1. 20A ND 81 70-130 10 20 n-Propylbeazeue 19.6 0.5 ug/L 20.0 ND 98 70-130 8 20 o-Xylene 15.7 0.5 ug/L 20.0 ND 78 70.130 3 20 scc-Butylbenzene 19.0 1.0 ug/L 20.0 ND 95 70-130 9 20 Styrene 19.5 0.5 ug/L 20.0 ND 98 70-130 5 20 tert-nutylbenzene 20.7 0.5 ugiL 20.0 ND 104 70-130 10 20 Tetracldoroelhene 17.6 0.5 ugtl- 20.0 ND 88 70-130 11 20 Toluene 15.3 03 ugR. 20.0 ND 76 70-130 7 20 t(ans-1,2-Dichlomethene 19.0 0.5 ue/L 20.0 ND 95 70-130 t0 20 Trichloroethene 18.2 0.5 uglL 20.0 ND 91 70-130 10 20 Vinyl chloride 19.2 0.5 ug/L 20.0 ND 96 60-140 12 20 S)rrrogate: 1,1-Dichloroetlraru-D4 Surrogate: 1-BrontoJluorohein-ene Surrogate: Toluene-dS 95 70-130 92 70-130 91 70-130 PO Box 5655 i Greenville, SC 29606 426 Fairforest Way ' Greenville, SC 29607 ruin 864.232.1556 ' tar 864.232.6140 rogersandcallcott.com an ernpioye e -ter: ned <otnpa ny 0123 2015 10:59 This nynur ma} tw1 he reprothicet{ except In full, arttlxna u,rrrten rwi rirrion front Rogers R Callcoll. hh. Page 8 of 11 14, Rogers &CaLlcott t if ENVIRONMENTAL Catalent Pharma Solutions Project: Effluent 2021 E. Roosevelt Blvd. York Order: 5010476 Monroe, NC 28110 Reported: 01/23/15 10:59 Data Qualifiers and Definitions ND Analyte NOT DHTHCI'F.D at or above the reporting limit NR Not reported RPD Relative percent Difference Z MDL is 0.09ug/L - No peaks detected Za MDL is 0.16ugll, - No perils detected PO Box 5655 ' Greenville, SC 29606 ' 426 fairforest Way i Greenville. SC 29607 nnln 864.232.1556 ' fax 864.232.6140 rogersandcallcott.com an employee -o fined company 0123 2015 10:59 MY report nw), not he nPrnOueed ereept In frill, urlrlam u•r/nen permiulnn from Rogers & Caflen0, hw. Page 9 of 11 Rogers &Cat[COtt CHAIN E N V I r2 Q N M E N TA L Mailing PO Box 56SS Shipping 426 Fairforest Way 215E Stonerldge Dove Address: Greenville,SC29606 Address: Greenviile,SC29607 Columbia, SC29210 Phone (864)Z32-1556 Fax (864(232-6140 Phone (803)509.8999 Client Name Catalent Address Mon -roc, NC Report TO: Email Address Tele hone p PO # Project # 93-121 OF CUSTODY RECORD WORK ORDER aj o o o E z p a`, aj E ca °°75 Filtered Les/No) Y Cooled (Yes/No) G Container Type (Plastic/Glass) as Container Volume(mL) G Sample Type Lrab/Composite} GW Sample Source (WW, GW, DW, SW, S, Other) Preservation Code(s) A —None E —HCI I — ZnAcetate 8—HNO3 F—Na2S203 1—H3PO4 c—H:SOi G — Boric Add K-MCA4 D— NaOH H— Ascorbic Acid L- > a R&C j YR WORK ORDER DATE nME SAMPLE DESCRIPTION COMMENTS ;VtID'Al 'lf� )! )) �S � �� — "3 vials unpres, 1 HCl Effluent rj D1 Oy-Z tp -Ui PH - % j Collected on )/V/3 @ )�15 Temp - i 3. ZtbY .3-14 F Au SAMIJ&Z6HJ ' HED 8Y: DATE/TIME: /5 %6`!S R _ D1 omposite Start Date: Composite Start Time: Time or Flow (Circle one) Initials: RELI QUISHED BY: 3• ATE/TIME: RECEIVED W G. DATE/TIME: RELINQUISHED BY: S. DATE/'TIME: RECEIVED BY: 6. DATE/TIME: Temperature of blank or representative sample At time of collection °C At time of lab receipt y. Z 'C RELINQUISHED BY: 7, DATEITIME: RECEIVED BY: g. DATE/TIME: Possible Hazards associated with samples: Non -Hazard ❑Flammable Skin Irritant Poison FlUnknown ED]ther Form Revised July, 2014 Page Rogers & Callcott ENVIRONMENTAL Sample Receipt Verification Date Work Client:Received: • 4t • Is Order:1 OLI `l to Carrier Name: Client FedEx UPS US Mail Courier Field Services Other: Tracking Number: Receipt Criteria Y e s o A Comments Shipping container / cooler intact? Damaged Leaking Other: Custody seals intact? COC included with samples? COC signed when relinquished and received? Sample bottles intact? Damaged Leaking Other: Sample 1D on COC agree with label on bottle(s)? Date / time on COG agree with label on bottle(s)? Number of bottles on COC agrees with number of bottles received? Samples received within holding time? Sample volume sufficient for analysis? VOA vials free of hcadspace (<6mm bubble)? Temp at receipt recorded on COC Samples cooled. Temp measured with IR thermometer- SN: 97050D67 Dry Ice Cold Packs D lee None Samples requiring pH preservation at proper pH? Note: Samples for metals analysis may be preserved upon receipt in the lab. 6 e Samples dechlorinated for parameters requiring chlorine removal at the time of sample collection? \/ l� If in-house preservation used — record Lot h HCL H3PO4 H2SO4 NaOH HNO3 Other Were non-conformance issues noted at sample receipt? Yes or No ' Non -Conformance issue other than noted above: Revised July 2014 Completed by: Page l l oft 1 Rogers and Calicott Environmental Client: C, Date: Continuing Calibration Verification Conductivity Meter EPA 9050A Meter Make / Model: Orion Star A325 SN: G-02 7, 6 Probe: Time Analyst Conc. of Standard, Actual Reading of Standard, l,imhos/cm @25°C µmhos/cm @ °C @ °C pH Meter EPA 9040C Meter Make / Model: Orion Star A325 Probe: AQi-/IP—A Time Analyst Conc. of Buffer, units Actual Reading of Buffer, units 7.0 7,67 Meter Make / Model: Hach 2100P Well ID: Turbidity Meter Field Screen Method SN: Time Analyst Assigned Conc of Standard, NTU Actual Reading of Standard, NTU Field Duplicate Time Analyst Conductivity, pH, Turbidity, Temperature, mhos/cm units NTU °C ii17 5 v 7,94 Note: Refer to daily calibration log for instrument calibration and chemical inventory information /documentation. Reviewed by: Date: Revised O1/21/13 Rogers and Callcott Environmental Client: ".,.,� �}— Date: Field Meter Calibration Record Conductivity Calibration - EPA 9050A Meter Make / Model: Orion Star A325 SN: Z- 02-7 U 6 Probe: Time: Analyst: Cell Constant Chemica 7 Conc. of Standard, µmhos/cm @25'C Actual Reading of Standard, µmhos/cm @ Tern perature, 'C r- SSS conc: Temperature compensation for pH / conductivity meter :Ci r PH Calibration - EPA 9040C Meter Make / Model: Orion Star A325 Probe: Time: 0,633 Analyst: Slope: Ufa r 99,2- Chemical Inventory Conc. of Buffer, units Actual Reading of Buffer, units `lo 4.0 3,99 0.5 Y 7.0 7 Uo yv IL/f 10.0 /o,Gr `/b G .) LI SSS conc: 7, v (,, 9 Meter Make / Model: Time: Reviewed *. Hach 2100P SN: Analyst: Chemical Inventory Date: Turbidity Meter Calibration Field Screen Method Date of most recent calibration: Assigned Conc. of Standard, Actual Reading of Standard, NTU /- I NTU Revised 02/21/13