WQ0010607_Regional Office Historical File Pre 2018

WELL CONSTRUCTION RECORD (GW-1)
1. Well Contractor Information:
Rich Lemire
Well Contractor Name
2593A
NC Well Contractor Certification Number
sAEDACCO, Inc
Company Name � /� �
2. Well Construction Permit #: v V R0300 07
List all applicable well construct -it permits (i.e. WC, County, Store, Variance, elk)
3. Well Use (check well use):
Water Supply Well:
(Heating/Cooling Supply)
Non -Water Supply Well:
E)NI tinlclpal/public
[)Residential Water Supply (single)
Residential Water Supply (shared)
iter Recharge
Groundwater Remediation
fifer Storage and Recovery
C)Salinity Barrier
ifer'l'est
13Stormwater Drainage
:rimental Technology
Subsidence Control
hermal (Closed Loop)
[3'1-racer
Return) QOther (explain under #21 Remarks
4. hate Well(s) Completed: 11 M.16 Well IDH R Y U-2A
ia. Well Location:
Catalent, Inc.
facility/Owner Name Facility IDM (if applicable)
2021 E. Roosevelt Blvd, Monroe, NC, 28112
Physical Address, City, and Zip
Union 09117004
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/min utes/secoads or decimal degrees:
(ifweIl field, one rat/long is sufficient)
34-980308 N 80.492322 W`~
6.Is(are) the well(s)Ox Permanent or 1117emporary
7. is this a repair to an existing well: []Yes or JgNo
lfthit is a repair, fill out known well construction otiar namn and explata the nurture afthe
repair under 721 remarks section or on the back of this first
S. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
construction; only 1 GW-I is needed. Indicate TOTAL NUMBER ofwells
drilled: o/a
9. Total well depth below land surface: 72.5 (tt)
Fix multiple wells list all depths ifdierent (example- 3 a Z00' mod 2 ttl100')
10. Static water level below top of casing: 30.30 (ft.)
lfwater level is above caving use -"
11. Borehole diameter: 12, 7-7/8, 6 (in.)
12. Well construction method; HSA to 14, air hammer to depth
(i.e_ auger, rotary, cable, direct push, etc.)
Print Form
For Itmal Use Only:
14. WATER ZONES
FROM
TO
I DFSCRIPrtON
ft
ft
ft
ft.
_--
15.OUT)iR CASING for multi -cased welts OR LINER (if a cable
FROM TO
DIAMETER
fit KIItESS
MA'r1,RtAI.
ft
in.
16. INN R CASING OR TUBING(geothermal closed -loop)
FROM
TO
DIAMETER I
THICKNESS
MATERIAL.
0
24.5 fL
6 in I
0.28-in
PVC
tf.
ft.
in.
_
17. SCR EN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
24.5 rid
72.5 ft
6 in.
nla
n/a
Open Rock
ft.
18. GROVT _._---
FROM
TO
MATERIAL
EMMACEMEN-r MErHOD & AMOUNT'
0
24.5 ft,
cement/bentonite
tremmie pipe, -90 gallons
ft
ft
19. SAN GRAYh`L PACK 1f a icable
FROM I
I TO
MATERIAL, 1
EMPLACEMENT MErHOD
IL
ft
nfa
tk
ft
20.DRILLING LOG attach additional sheets ifaecessa )
FROM
"ro
DF.SCRIPr[ON cob-, hardness, sodtmckt sae, etc.)
0 rL
14 It,
Orange Silty Clay
14
22.5 ft.
PWR Ar illite
Rock Blue Stone
22.5
72.5 ft'
ft.
-
fl.
ft
fl.
ft
ft
ft.
21. REM
RKS
I
P
Date
)Iv signing thiat'fcrntI'l hereby cerrify that the well(s) was (were) constructed in accordance
with 15A A -AC OA, .01049 or 15A NCAC 02C -0200 We!! Comtruction Standards and that a
copy of this! record has been provided to the well owner.
23. Site diagram or additional well details:
You may ilse the back of this page to provide additional well site details or well
construc4n details. You may also attach additional pages if uecessary.
24a. For All Wells: Submit this tbrm within 30 days of completion of well
construction to the following:
vision of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For lniectiou NVells: In addition to sending the form to the address in 24a
stove, also submit one copy of this form within 30 days of completion of well
constructiiin to the following:
Divisiain of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield (gpm) Method ortest: 24c. For water Supph* &c Inisction Wellg. In addition to sending the form to
the addre$,s(es) above, also submit one copy of this form `Within 30 days of
13h. Disinfection type: Amount: completion of well construction to the county health department of the county
where constructed.
Fortin G W-I Nwth Carolina Department of Environmental Quality . Oivision of Water Resources. Revised 2-22-2016

F
WELL CONS'fRUC` ION RECORD
n,s fro, can tr #-d k r single ae nab ipk %A "k
t. Well Contractor Information:
Rich Lemire
We'll C•tmrimr Mamc
2593A
'�C 1ttoCtCr��:earCcnit`�c:�t�rz'�wlabc*
SAEDACCO Inc
2. Well t enienetion Pelf
1 erf ui! r:�nlf.:rhlr ..rt! (tr.reri(+ rz I fiutnSr.'..SteeJ.•, l:uaa»t�, �. jr�lCd011 �h.1
3. W'elh i. w tcheck wdl awr
CIAg -(hurl r.lkftmi6pa?ubhr
t 141owthewnwA tHenting'Cooling StW%t 0Rcsi&ntial Water St"* tsingko
clfttduutiai Catnowrciakl E ilte idennal WaterSupph ishttvds
C:IAguifer R"harge
ClAgtlitet Stamp.ir aid Rccown
nAgsiikv T;.N
0ENpi:nnic tat rechool
DGemhenral (t kved LoVt
a
06mundWater RcinediXion
ITS21180 flamer
01.4o mw:lter Dminape
Cl5ltbsuk»cc C'emtml
O'TMVt
4Date WcRfr! Completed: 11-30-2016 Weli ID#RN-2A
Via. Well Location:
CATALENT PRARMA RN-2A
Fac elms '"x fm Xank Fxelst+ ttU t If mplicabk-s
2021 East Roosevelt Boulevard Monroe, NC 28112 Uni,
MONROE, NC, 28112 PhAvac;tl ;ytkltrs,; tits, 496 Zip
P.atee3trtsaalFtu;ttxwittia. fPt'ti1
�h. Latitude and Longitude in d t give ^minuteVseconds or decimal drove., :
{tis�rvlECsib tnlelat,7[aq{�m.tdlit:wae:
34R979625 N 80.492794
h.ta{anitbe�rll{rt: �t'rn»alee»t er _i'etetpArrar.
;. 1% tht% a repair to an c"irhng well^ %C% or KNO
h •hu At. if ea`}r car 141 •,trt ir:a><7! u r,f eam>:s� h.w eryirre.ral(a. nt artj erl xtr+ r n nu R��t r.( Na
rrtrcra.+ srerrfr» 8.'P nfrarrrls rr>#•m �tr rre tsar txr t n1 tlg: harm
U. Number or tteib conmracted: 1
F'R'MAJnrJ,e+, rEr n:-a,-,•rr,•t•N.,rrnFPtt'.VON, OUV r..•<.h rhr WMrt K<rrrsttlirlNHf ,...,,..,,'
F,YbAnrr''mr r0"n-
4. Total well deptb ",A la»d wrf,"V:. 72'
/'.,r frrsr(M.(..ir wrFCs It�r,rJd ��y�e rrtte!ysperrr.rt!aflyia•.. 7As?!r1'.•ai'�t(u;";."`"""".
Id. Static %fitter irtrl below top of cmAng; 42'
Ji nu!r( idi rl t. �Y,ri . ar+rrt;, a•a
t 1. Bnrcink diameter. 6 • (fn. i
Farinerlattt:x„�t,. 440766
! Il ti Ott y1)Nfti�..r.._a.•.ea,•-.......ow..,..om,.�-.F.�a..�_ �„-,_-.�,.v..�:�,....,m. �.....--.,....-.,a.�
iR11N ; tU
BIWRIr'tttlt
it. fi.
f
t5, QtrTr:'R C.iStl�cs.r
mom _ 7O
wrt1,> QR t.MERlif
at'i'arFM Tn1CA'VFS.' N.tTiP14U
~�
0 q, 24.5 ft
►r~ tail r1rx(, oR.niulw
t+A10
k ft fl
ft ft.
6• ill SCH40 PVC
; ®f YiYFlt iNICk.�R53' *A UtL
in
in.
S
�---
ft.
I9 GUM T
u_FitON TO 1t.hrUtt.U. ,y fyp ACENT:�TNt2'if110UtA�1t-UG4
tL tt J.
--------------
! 0 R. i 14
ft.
ORANGE SILTE CLAY
14' fl. 22'
it.
PNR j
i 22' fl. E 72'
p,
ROCK -� , I
8
i II. REMARKS
THIS IS A OPEN HOLE CASING TO 24.5'OPBN
TO 72
WQROS
ZL Certification: HUAUNAL (
411 +� '� 12/1/2016
Sign ®fC'rn . WzliCaA wor OJac
B. 1 inr bt ..'wlp. fbw (1fr YYTNa1 .cW Igr',!f ai'M_, IItM SaV 'R G xa+ryid®ty
a v(r i 5,t 4'r it t)T t1hiff w 1 t.A W, IC WC jV10) hi-fi f i+asir to taus Srre/tlr.rtl4.t1W *00
rfrs a(rAa. rr.,:an! l�.'3 irrrry ,nrr,rdZrd en a6.Avt: ,rarraYr.
23. Ske diagram or additi nAi well details -
You ttvtt ttae the ht<L of this page to pta%tde adthflrJlial wrll rate {let. -A (u well
ticrosttta ttun tktath. You twd'* 31w :ttlach 3"flonal paps'. at 1V'xSa:ar%
ltit4117"1:4t-IN-5F CTIONS
24a. Few AN W'a•Iba: Subrtnl this form lslthm Ott da,.s rf outpLtion of w li
:omtnKnon to the fnlMuing
Miklos of WAter Rewwrem Infurtuation Pntceming t: nit..
1617 Nad tiern'tee letter, Rakigh. N( 276"-161'
24b. F.iILj1!$'5.4 .-*#1 jt ON1,V: lit addinon to sending, itic', form to tkaddtem in
241pine also altbuatt a cite of thiS farm tsiihot W (lms of compktktn of well
12. Ueil efflWniction method. AIR DRILLED -_ Constnatton to the lollawutg
t r fli %I. wjn' ciffir flikX4 rust, Cta I
Dh imo of Water Ret/wrets. ltnderpwuund Injection Control ProRrattt.
FOR WATER SUPPLY WELLS ONLY: 1636 Mail tier* ice Center. Rakieb. NC 276".1636
13a. ti ►rid (gpml .__ - %Scdwd of ttU. ____ _ _ 24e. For Water So r elk finials. Welt.""--- Alas wbunt o t "" of this Calm witt»t at, dj%s tat 4txttplokNot ill
13b. Munfn-tion qlw. Amrwut: well cotestntction to the callow licahh defrartturnt of the ctatrttt %.here
constructed
l•:,rtntilt'-lutATtC;ntttn tkVta€rtarw,>iLaatcoattrtaandlwnaulR:soe}rs.s Ue+r>t�r«at;tuRe3tnsccs RsoIsi':dAtgust-,fie

PAT MCCRORY
Ciuvermn.
Water Resources
ENVIRONMENTAL QUALITY
November 16, 2016
Catalent Pharma Solutions
2725 Scherer Drive North
St. Petersburg, FL 33716-01016
Attention: Dina Kostakis, General Manager
Dear Ms. Kostakis:
DONALD R. VAN DER VAART
Secrerarr
S. JAY ZIMMERMAN
l )rrerlor
RE: Compliance Inspection Report
Groundwater Remediation
Permit No. WQ0010607
Catalent Pharma Solutions
(Former RP Scherer/Chelsea Labs)
2021 E. Roosevelt Ave., Monroe
Union County
The MRO would like to extend our thanks to Mr. Stan Golaski of Rogers & Callcott and to Mr. Jerry
Sullivan of Aqua -Trot for taking time to meet with us so we were able to review the remediation system
at the permitted facility.
On November 9, 2016, a compliance inspection was performed for the groundwater remediation system
of the Catalent Pharma Solutions groundwater remediation system at 2021 Roosevelt Avenue, Monroe,
Union County. During this inspection the recovery and treatment system were reviewed, the recovery
wells were checked for operational functionality and the treatment system was discussed with
representatives of Rogers & Callcott and Aqua -Trot, Inc. Please see the attached inspection report.
The permit expiration date is August 31, 2018. Per permit requirements, a renewal application is due
180 days prior to expiration.
Edward Watson
Hydrogeologist
Division of Water Resources
Water Quality Regional Operations Section
Cc: George Maalouf, Rogers & Calcott Engineers, Inc. POB 5655 Greenville, SC 29606
State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1 610 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115
704 663 1699

Compliance Inspection Report
Permit: WQ0010607 Effective: 09/01/09 Expiration: 08/31/18 Owner : Catalent Pharma Solutions LLC
SOC: Effective: Expiration: Facility: R P Scherer Corp -Chelsea Lab
County: Union 2021 E Roosevelt Blvd
Region: Mooresville
Monroe NC 28111
Contact Person: George Maalouf Title: Phone: [phone]
Directions to Facility:
from Charlotte take US-74E toward Monroe merge LT onto E. Roosevelt Blvd arrive at 2021.
System Classifications: PC1,
Primary ORC: Certification:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 11/09/2016 EntryTime: 11:OOAM
Primary Inspector: Edward Watson
Secondary Inspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Groundwater Remediation
Facility Status: Compliant Not Compliant
Question Areas:
Record Keeping Well inventory
Treatment Units Disposal units
Laboratory
(See attachment summary)
Exit Time: 12:20PM
Phone:
Phone:
Inspection Type: Compliance Evaluation
Wells
Sampling
Page: 1

Permit: WQ0010607
Inspection Date: 11/09/2016
Inspection Summary:
Owner - Facility: Catalent Pharma Solutions LLC
Inspection Type : Compliance Evaluation Reason for Visit: Routine
On Novemebr 9, 2016, a compliance inspection of the groundwater remediation system was performed by MRO staff. The
system was found to be in good operating order. A slight bacteria sheen was noticed in both the wet well and in the
holding tank. The wet well high water alarm was tested and was found to be in good working condition. The SCADA
system called the ORC to report a high water alarm condition.
The recovery wells appear to be in good working order and the outfall was clear of debris, foam, odor and color. The out fall
had been moved to a secured area inside the driveway of the loading dock.
Paperwork and laboratory data were found to be in good order an no compliance issues were noted during the site visit.
Page: 2

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Permit: WQ0010607 Owner - Facility: Catalent Pharma Solutions LLC
Inspection Date: 11/09/2016 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Field Observations
Do any surface water features appear to be adversely impacted by GW discharge?
Are flow rates less than permitted flow?
Are application rates adhered to?
Comment: The system discharges to a collection line throuqh a permit between the RP and the City of
Monroe The permit between Catalent and the City of Monroe VWVfP renews every three
years.
Monitorinq
Is GW monitoring being conducted?
Are MWs sampled for all required parameters, as required in permit?
Does monitoring data indicate that disposal of treated effluent is impacting GW quality?
Is GW-59A certification form completed for facility?
Yes No NA NE
❑ ❑ N ❑
Yes No NA NE
■❑❑❑
❑ ❑ ❑
■❑❑❑
■❑❑❑
Operating Records Yes No NA NE
Was operational log book reviewed? 0 ❑ ❑ ❑
Does data in log book correlate to operational status referenced in monitoring reports? 0 ❑ ❑ ❑
Are all recording units (flow, time, pressure) functional? If not, explain. ❑ ❑ ❑
Is operator performing as required? ❑ ❑ ❑
Do reports meet permit needs? 0 ❑ ❑ ❑
Comment: Operation records were reviewed and appear to be up to date. All reports are in compliance with
the permitted conditions for this site. Records are in good order.
System Operation Yes No NA NE
Flow rate at time of inspection (gpm):
Design capacity: 20000
Has system owner/operator noticed any abnormalities (turbidity, air in system, poor heating/cooling, etc) in ❑ 0 ❑ ❑
system operation?
Is system status consistent with that anticipated by inspector? M ❑ ❑ ❑
Page: 4

Permit: W00010607
Inspection Date: 11/09/2016
System Operation
Owner - Facility: Catalent Pharma Solutions LLC
Inspection Type : Compliance Evaluation
Describe inconsistencies between expected and observed operation/construction
The system is discharging at rates compliant with the 17,280 GPD limit as stipulated in the permit. Most
times this system does not discharge to daily maximum limits.
The system acts as a pre-treatment system which then is discharged into a SSO line owned by the City of
Monroe. This happens via a permit between the RP and the City of Monroe.
Well MW-2 is currently being used as a recovery well. The permitee has plans of installing a recovery well at
a location between the exisitng MW-2 and a nearby piezometer. at an approximate distance of 5 to 10 feet
between the well and the Piezometer.
Reason for Visit: Routine
Yes No NA NE
Page: 5

Rogers & Callcott
ENVIRONMENTAL
November 2, 2016
WPCSOCC
if. *
RECEIVEDINCDENR/DWq
NOV - 3 2016 Laboratory
wOROs Engineering
MOORES�/1� !.GIONAL OFFICE
Assessment
1618 Mail Service Center Remediation
Raleigh, North Carolina 27699-1618
(Delivered via Email: [e-mail]) Air Quality
Subject: New Backup Operator in Responsible Charge (ORC) Compliance
Catalent Pharma Solutions (Formerly R.P. Scherer)/Chelsea Laboratories Facility
Rogers & Callcott Project Number: 93-121
To Whom It May Concern:
Please find enclosed the Water Pollution Control System Operator Designation Form documenting a
new Backup ORC in accordance with NCAC 15A 8G.0201 for the subject site located at 2021 East
Roosevelt Boulevard in Monroe, Union County, North Carolina, 28112. Feel free to contact me at
864.232.1556([e-mail]) with any questions or concerns.
Sincerely,
ROGERS & CALLCOTT ENVIRONMENTAL
Stan Golaski
Assessment & Remediation Manager
Enclosure
\\RC-VMSRV03\Projects\14\93-121\2016\CORR
VU6 G O C a?(o Cj r7
dn���
PO Box 5655 1 Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 i fax [phone] rogersandeallcott.eom
an employee owned company

WATER POLLUTION CONTROL SYSTEM OPERATOR DESIGNATION FORM (WPCSOCC)
NCAC 15A 8G .0201
Press TAB to enter information
Permittee Owner/Officer Name: Catalent Pharma Solutions / Ms. Dina Kostakis
Mailing Address: 2725 Scherer Drive North —
city: St. Petersburg
Email Add re ostakiS@Ca t. om
Signature:— '
Facility Name: Catalent Pharma Solutions] Chelsea Laboratories Facility
County: Union
State: FL
Phone: [phone]
_ Zip.. 33716
- Date:
Permit # LP-001
YOU MUST SUBMIT A SEPARATE FORM FOR EACH TYPE AND CLASSIFICATION OF SYSTEM:
Facility Type: PC
Facility Grade: I
OPERATOR IN RESPONSIBLE CHARGE (ORC)
Print Full Name: Jerry Lane Sullivan _ Work Phone: [phone]
Certificate Type: Select — Certificate Grade: I Q Certificate #: 27897
Email Address: jefry•[e-mail]
— l�
Signature: Date:
"l certify that / agree to my designation as the Operator in Responsible Charge for the facility noted. 1 understand and will abide by the
rules and regulations pertaining to the responsibilities of the ORC as set forth in 15A NCAC 08G .0204 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
_ BACKUP ORC
Print Full Name: James Doric Sullivan-----_ _ Work Phone:[phone]
Certificate Type: Select Certificate Grade: 1 Q Certificate #:1003532
Email Address james.aquatrot gmail.com — —_
/p Date: / /
�� Signature: is Da,"/certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. 1 understand and wilt abide by
the rules and regulations pertaining to the responsibilities of the ORC as set forth in 15A NCAC 08G .0204 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Mail, fax or email WPCSOCC, 1618 Mail Service Center, Fax: [phone] Email: certadmin(wncdenr.gov
ORIGINAIto: Raleigh, NC 27699-1618
Mail or Fax Asheville
a COPY to: 2090 US Hwy 70
Swannanoa, NC 28778
Fax:[phone]
Phone:[phone]
Fayetteville
225 Green St., Suite 714
Fayetteville, NC 28301-5043
Fax:[phone]
Phone:[phone]
Mooresville
Raleigh
610 E. Center Ave., Suite 301
3800 Barrett Dr.
Mooresville, NC 28115
Raleigh, NC 27609
Fax:[phone]
Fax:[phone]
Phone:[phone]
Phone:[phone]
Washington Wilmington Winston-Salem
943 Washington Sq. Mall 127 Cardinal Dr. 45 W. Hanes Mall Rd.
Washington, NC 27889 Wilmington, NC 28405-2845 Winston-Salem, NC 27105
Fax:[phone] Fax:[phone] Fax:[phone]
Phone:[phone] Phone:[phone] Phone:[phone] Revmd412016

May 26, 2016
Ms. Dina Kostakis
Catalent Pharma Solutions
2725 Scherer Drive North
St. Petersburg, Florida 33716-1016
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Dear Ms. Kostakis:
CITY
OF
MONR OE
a herilage of progress
Please find enclosed herein Local Industrial User Permit No. LP-001 authorizing Catalent
Pharma Solutions / Chelsea Laboratories Facility located at 2021 East Roosevelt Blvd. to
continue to discharge treated ground water to the City of Monroe sewer system for further
treatment at the City of Monroe Wastewater Treatment Plant through June 30, 2019. All other
contract conditions remain unchanged and binding.
Consistent with the provisions of § 52.051 of the City's Sewer Use Ordinance, the terms and
conditions of this permit are binding upon the industrial user.
Should you require additional information please do not hesitate to contact me.
Respectfully,
—O- �oIQ�U�
Kevin Keesler
Pretreatment Coordinator
c: W WTP/IUP file
1: 8040 WWTP and collection/Pretreatment program/Industries/local permittees
City of rlrlonroc • 110 Box 69 •Monroe, NC 28111-0069
Tel: [phone] • Fax: [phone]
www.nionroenc.org

"EXHIBIT B"
City of Monroe WWTP
Municipal ily Name
hertaller in this permit to as the
Control Authority
LOCAL INDUSTRIAL USER PERMIT
Local Industrial User Permit (LIUP)
To Discharge Wastewater Under the
Industrial Pretreatment Program
LP-001
LIUP Number
In compliance with the provisions of North Carolina General Statute 143-215J, all other lawfid
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the City of Monroe Sewer Use Ordinance. The following Industry,
hereafter referred to by name or as the permittee:
Industry name, permiltee:
Catalent Pharma Solutions / Chelsea Laboratories
Facility
Facility Located at Street Address:
2021 East Roosevelt Blvd.
City
Monroe
State, Zip
North Carolina, 28110
is hereby authorized to discharge wastewater from the facility located at the above listed address into
the sanitary sewer collection system and the wastewater treatment facility of the City of Monroe
listed below:
RIP Control Authority WWTP name:
City of Monroe WWTP
NPDES Number:
NCO024333
WIVTP Address:
Post Office Box 69
State, Zip
Monroe, NC 28111-0069
in accordance with effluent limitations, monitoring requirements, and all other conditions set forth
in Parts I, II, and III of this Local Industrial User Permit (IUP).
Effective date, this permit and the authorization to discharge shall
become effective at midnight on this date:
July 1, 2016
Expiration date, this permit and the authorization to discharge shall
expire at midnight on this date:
June 30, 2019
t--' Date / Direetor of Water Resources
Page:1
Effective Datc: July 1, 2016

LIUP, Part 1
Industrial User (IU) Specific Conditions
IUP, PART I, OUTLINE:
A) LIUP Basic Information
B) LIUP Modification History
C) Authorization Statement
D) Description of Discharges
E) Schematic and Monitorurg Locations
F) Effluent Limits & Monitoring Requirements
G) Definitions and Limit Page(s) notes
A. LIUP Basic Liformation
Receiving POTW name:
POTW NPDESO:
City of Monroe Wastewater Treatment Plant
NCO024333
LIUP Name:
LIUP Number:
Catalent Pharma Solutions / Chelsea Labot-atories
LP-001
Facility
LIUP Effective date:
Pipe Numbers, list all regulated pipes:
July 1, 2016
01
LIUP Expiration date:
June 30, 2019
B. LIUP Histol :
Date Modified
Reason for & Description of modifications.
June 15, 2002
Permit Issued
Date Modified
February 21, 2003
Industry Name Change; Flow limit and
monitoring frequency change
Date Modified
June 15, 2007
Permit Issued; industry name change;
changed page 6 F) to G); changed verbiage
in PART II 2. a), b), c), 10., 13., 16., 25., 27.,
30.; changed verbiage in PART III 1.2., 1.3.
August 20, 2007
Industry name change
July 1, 2010
Permit issued; changed verbiage in PART
I G)
July 1, 2013
Permit renewal
July 1, 2016
Permit renewal
A Complete Permit modification Histo is required
LIUP# => LP-001
Page:2
Effective Date: July 1, 2016

LIUP, Part I
Industrial User (IU) Specific Conditions
C) Authorization Statement:
1) The Permittee is hereby authorized to discharge wastewater in accordance with the
effluent limitations, monitoring requirements, and all other conditions set forth in this
Local Industrial User Permit (LIUP) into the sewer collection system and wastewater
treatment facility of the City of Monroe.
2) The Permittee is hereby authorized to continue operation of and discharge wastewater
from the following treatment or pretreatment facilities. These facilities must correspond
to the treatment units listed on both the application and inspection forms.
IU Treatment Units
List all Treatment Units: Descriptions:
Air Stripping Air Stripping of Organics
Sedimentation Gravity Settling Tank
3) The Permittee is hereby authorized to, if required by the City of Monroe and after
receiving Authorization to Construct (A to C) from the City of Monroe, construct and
operate additional pretreatment units as needed to meet final effluent limitations.
D) Description of LIUP Discharge(s):
l . Describe the discharge(s) from all regulated pipes.
Pipe # 01 Description of Discharge:
Treated Ground Water
Pipe # 02 Description of Discharge:
N/A
LIUP# => LP-001
Page:3
Effective Date: July I, 2016

LIUP Part I
Industrial User (IU) Specific Conditions
P.) Schematic and Monitoring Locations:
The facility schematic and description of monitoring location(s) given below must show
enough detail such that someone unfamiliar with the facility could readily find and
identify the monitoring location(s) and connection to the sewer. Include and identify all
regulated pipes. See figures on Page 4A and 4B.
LIUP# => LP-001
Page: 4
Effective Date: July 1, 20t6

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LIUP, Part I, Section F: Receiving POTW name => City of Monroe LIU name=>Catalent Pharma Solutions
Effluent Limits and Monitoring Requirements Receiving POTW NPDES # _> NCO024333 LIUP # _> LP-001
Effective date for these Limits => 7/1/16 Pipe # _> 01
The permittee may discharge from this specific pipe Expiration date for these Limits => 6/30/19 40 CFR#=>
number according to these specific dates, effluent if not applicable put N/A
limits, and monitoring requirements. THE LIMITS ON THIS ARE, (Check one below):
LIMITS for ENTIRE permit period => X
INTERIM Limits for period # 1 =>
INTERIM Limits for period # 2 =>
FINAL Limits Page =>
Conventional
Concentration Limits
Mass -Based Limits
MonitoringFre uency
Sample
Required
Parameters'
Daily
Weekly
Units
Daily
Monthly
Units
by Industry
by POTW
Collection
laboratory
Max
Avg.
Max
Avg.
Method
Detection
(C or G)
Limits
Flow
0.01
MGD
Weekly 4
Tetra-
8.85
µg/l
1/month 2
Random
G
chloroethene
Tri-
81
µg/1
I/month
Random
G
chloroethene
EPA method
monitor
Quarterly 3
Random
G
8260 1,
only
pH
6 to 11
Std. Units
1/month
Random
G
' Parameters and Prohibitions not specified above are regulated and limited by the (See next section, LIUP, Part I, Section G.)
City of Monroe Sewer Use Ordinance. for Definitions and Limits Page(s) notes:
z 1/month shall be 1 sampling event taken each calendar month. LIUP, PART I, Page: 5
3 Quarterly sampling shall be during the months of February, May, August, November
4 Flow meter totalizer shall be recorded at least weekly.
Effective Date: July 1.2016

LIUP, PART I
Industrial User (IU) Specific Conditions
G) Definitions and Limit Page(s) notes:
In addition to the definitions in the City of Monroe Sewer Use Ordinance the following
definitions and requirements apply:
1. Composite Sample:
a) A composite sample for the monitoring requirements of this IUP, is defined as the
automatic or manual collection of a series of grab samples of constant volume, not less
than 100 ml, collected at equal time intervals ducting the entire discharge period on the
sampling day. The time interval between grab samples shall be no greater than once
per hour, or
b) a single, continuous sample collected over a 24 hour period proportional to the rate
of flow. Sampling day shall be a typical production, and discharge day.
2. Daily Monitoring Frequency
Daily Monitoring Frequency as specified in this LIUP shall mean each day of discharge.
3. Grab Sample
Grab sample for the monitoring requirements of this IUP, is defined as a single "dip and take"
sample collected at a representative point in the discharge stream over a period of time not
exceeding 15 minutes. The grab sample can be taken manually. Grab samples must be
representative of the discharge.
4. Instantaneous measurement
An Instantaneous measurement for the monitoring requirements of this LIUP is defined as a
single reading, observation, or measurement.
LIUP#=> LP-001
Page: 6
Effective Date: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
Outline of PART H,
1. Representative Sampling
2. Reporting
3. Test Procedures
4. Additional Monitoring by Permittee
5. Duty to comply
6. Duty to Mitigate
7. Facilities Operation, Bypass
8. Removed substances
9. Upset Conditions
10. Right of Entry
11. Availability of Records
12. Duty to Provide Information
13. Signatory Requirements
14. Toxic Pollutants
15. Civil and Criminal Liability
16. Federal and/or State Laws
17. Penalties
18. Need to Halt or Reduce
19. Transferability
20. Property Rights
21. Severability
22. Modification, Revocation, Termination
23. Reapplication
24. Dilution Prohibition
25. Reports of Changed Conditions
26. Construction of Pretreatment Facilities
27. Reopener
28. Categorical Reopener
29. General Prohibitive Standards
30. Reports of Potential Problems
1. Representative Sampling
Samples and measurements taken as required herein shall be representative of tyre volume and
nature of the monitored discharge. All samples shall be taken at the monitoring points specified
in this permit and, unless otherwise specified, before the effluent joins or is diluted by any other
wastestreanr, body of water, or substance. Monitoring points shall not be changed without
notification to, and approval by, the permit issuing authority.
2. Reporting
a) Monitoring results obtained by the permittee shall be reported on forms specified
by the City of Monroe, postmarked no later than the twentieth day of the month
following the month in which the samples were taken. Results based on laboratory
analysis shall include the laboratory report. If no discharge occurs during a reporting
period (herein defined as each calendar month) in which a sampling event was to have
occurred, a form with the phrase "no discharge" shall be submitted under the
signatory requirements of Part H, Section 13. Copies of these and all other reports
required herein shall be submitted to the City of Monroe to the following address:
Pretreatment Coordinator
City of Monroe
PO Box 69
Monroe, NC 28111
b) If the sampling performed by the permittee indicates a violation, the permittee shall
notify the City of Monroe within 24 hours of becoming aware of the violation. The
permittee shall also repeat the sampling and analysis and submit the results of the
repeat analysis to the City of Monroe within 30 days after becoming aware of the
violation.
LRJP#=> LP-001
Page:7
Effective Date: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
c) Laboratory reports shall include the following:
1. sample preparation - type and date(s) and time(s) performed;
2. analysis start dates and times;
3. analyst(s) initials;
4, analytical techniques and methods used;
5. results of the analyses;
6. chain of custody records which contain the following Information
a. sampling location;
b. date(s)/time(s) sample(s) taken;
c. sample type: composite (time, flow or hand) or grab
d. container type;
e. teflon liner and/or zero headspace, if applicable;
f. type of preservative used, if any;
g. sample iced upon receipt;
h. parameters to be run from that particular bottle;
i. individual(s) who performed the sampling and/or field measurements;
j. samples relinquished/received by who and when (date & time).
In addition, the laboratory performing the analysis shall maintain on file for up to three
years after the analysis all laboratory data taken and calculations during the analysis,
including dates and times, the analyst performing the work, and the data and
calculations from all quality assurance procedures and testing. This data shall be
available for inspection by personnel of the City of Monroe upon request.
3. Test Procedures
Test procedures for tine analysis of pollutants shall be performed by a North Carolina Certified
Wastewater Lab in accordance with the techniques prescribed in 40 CFR part 136 and
amendments thereto unless specified otherwise in the monitoring conditions of this permit. The
laboratory shall be certified by the State of North Carolina for each specific test parameter on
which their results are reported.
4. Additional Monitoring by Permittee
If tine permittee monitors any pollutant at the location(s) designated herein more frequently
than required by this permit, using approved analytical methods as specified above, the results
of such monitoring shall be submitted to the City of Monroe. The City of Monroe may require
more frequent monitoring or the monitoring of other pollutants not required in this permit by
written notification.
5. Duty to Comply
The permittee must comply with all conditions of this permit. Any permit noncompliance
constitutes a violation of the City of Monroe Sewer Use Ordinance and is grounds for possible
enforcement action; for Permit termination, revocation, and reissuance, or modification; or
denial of a Permit renewal application.
LIUP#=> LP-001
Page:8
Effective Date: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
6. Duty to Mitigate - Prevention of Adverse Impact
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation
of this permit which has a reasonable likelihood of adversely affecting human health, the
POTW, the waters receiving the POTW`s discharge, or the environment.
7. Facilities Operation, Bypass
The permittee shall at all times maintain in good working order anti operate as efficiently as
possible, all control facilities or systems installed or used by the permittee to achieve
compliance with the terms and conditions of this permit. Bypass of treatment facilities is
prohibited except when approved in advance by the City of Monroe. Bypass approval shall be
given only when such bypass is in compliance with 40 CFR 403.17. Treatment facilities shall be
as diagrammed in Figure 2.
8. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or
control of wastewaters shall be disposed of in a manner such as to prevent any pollutants from
such materials from entering the City of Monroe sewer system or the surface waters of the
State of North Carolina. The permittee is responsible for assuring its compliance with any
requirements regarding the generation, treatment, storage, and/or disposal of "Hazardous
Waste" as defined under the Federal Resource Conservation and Recovery Act. the permittee
shall maintain records of disposal of these substances for a minimum of three years.
9. Upset Conditions
An "upset" means an -exceptional incident in which there is an unintentional and temporary
noncompliance with the effluent limitations of this permit because of factors beyond the
reasonable control of the permittee. An upset does not include noncompliance to the extent
caused by operational error, improperly designed or inadequate treatment facilities, lack of
preventative maintenance, or careless or improper operations.
An upset may constitute an affirmative defense for action brought for the noncompliance. The
permittee has the burden of proof to provide evidence and demonstrate that none of the factors
specifically listed above were responsible for the noncompliance. Such evidence shall include
operating logs properly signed, or other relevant evidence that:
1. An upset occurred and that the permittee can identify the cause(s) of the upset;
2. The permittee facility was at the time being properly operated; and
3. tine permittee submitted notice of the upset as required in Part H, Section 30, of
this permit
4. The permittee complied with any remedial measures required under Part H,
Section 5, of this permit
LIUP#=> LP-001
Page: 9
Effective Dale: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
10. Right of Entry
The permittee shall allow the staff of the State of North Carolina Department of Environment
and Natural Resources, Division of Water Quality, the Regional Administrator of the
Environmental Protection Agency, the City of Monroe, and/or their authorized representative,
upon the presentation of credentials:
1. To enter upon the permittee's premises where a real or potential discharge is located
or in which records are required to be kept under the terms and conditions of this
permit; and
2. At reasonable times to have access to and copy records required to be kept under
the terms and conditions of this permit; to inspect any monitoring equipment or
monitoring method required in this permit; and to sample any discharge of pollutants.
11. Availability of Records and Reports
The permittee sl►all retain records of all monitoring information, including all calibration and
maintenance records as well as copies of reports and information used to complete the
application for this permit for at least three years. All records that pertain to matters that are
subject to any type of enforcement action shall be retained and preserved by the permittee until
all enforcement activities have concluded and all periods of limitation with respect to any and
all appeals have expired.
Except for data determined to be confidential under the Sewer Use Ordinance, all reports
prepared in accordance with terms of this permit shall be available for public inspection at the
City of Monroe. As required by the Sewer Use Ordinance, effluent data shall not be considered
confidential.
12. Duty to Provide Information
The permittee shall furnish to the Director of Water Resources or his/her designees, within a
reasonable time, any information which the Director, his/her designee, or the Division of Water
Quality may request to determine compliance with this permit. The permittee shall also
furnish, upon request, copies of records required to be kept by this permit.
13. Signatory Requirements
All reports or information submitted pursuant to the requirements of this permit must be
accompanied by the following certification by the Authorized representative:
"I certify under penalty of law that this document and all attachments were prepared under
my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for
LIUP##=> LP-001
Page:10
Eftective Date: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting
false information, including the possibility, of fine or imprisonment for knowing violations. "
The Authorized Representative shall be as defined by the City of Monroe Sewer Use
Ordinance. If the designation of an Authorized Representative is no longer accurate because a
different individual or position has responsibility for the overall operation of the facility, or
overall responsibility for environmental matters for the company, a new authorization
satisfying the requirements of this section must be submitted to the City of Monroe Water
Resources Director or his/her designee prior to or together with any reports to be signed by an
authorized representative.
14. Toxic Pollutants
If a toxic effluent standard or prohibition (including any schedule of compliance specified in
such effluent standard or prohibition) is established under Section 307(a) of the Federal Clean
Water Act for a toxic pollutant which is present in the discharge and such standard or
prohibition is more stringent than any limitation for such pollutant in this permit, this permit
may be revised or modified in accordance with the toxic effluent standard or prohibition and
the permittee so notified.
15. Civil and Criminal Liability
Nothing in this permit shall be construed to relieve the permittee from civil or criminal
penalties for noncompliance.
16. Federal and/or State Laws
Nothing in this permit shall be construed to preclude the institution of any legal action or
relieve the permittee from any responsibilities, liabilities, or penalties established pursuant to
any applicable Federal and/or State law or regulation.
17. Penalties
The Sewer Use Ordinance of the City of Monroe provides that any person who violates a per►nit
condition is subject to a civil penalty not to exceed $25,000 dollars per day of such violation.
Under state law, (NCGS 143-215.6B), under certain circumstances it is a crime to violate terms,
conditions, or requirements of pretreatment permits. It is a crime to knowingly make any false
statement, representation, or certification in any record or other document
submitted or required to be maintained under this permit, including monitoring reports or
reports of compliance or noncompliance. These crimes are enforced at the prosecutorial
discretion of the local District Attorney.
LIUP#=> LP-001
Page :11
Effective Date: duly I, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
The City of Monroe enforcement response will be in accordance with an Enforcement
Response Plan approved by the North Carolina Division of Environmental Management and
on file in the office of the Pretreatment Coordinator. However, the City reserves the right as
described in separate contract with R.P. Scherer, to require the permittee to immediately
discontinue all discharge of treated ground water to the City of Monroe system at the sole
discretion of the City of Monroe.
18. Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been
necessary to halt or reduce the permitted activity to maintain compliance with the conditions
of the permit.
19. Transferability
This permit shall not be reassigned or transferred or sold to a new owner, new user, different
premises, or a new or changed operation without approval of the City.
20. Property Rights
This permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
21. Severability
The provisions of this permit are severable and, if any provision of this permit or the
application of any provision of this permit to any circumstance is held invalid, the application
of such provision to other circumstances and the remainder of this permit shall not be affected
thereby.
22. Permit Modification, Revocation, Termination
This permit may be modified, revoked and reissued or terminated with cause in accordance
with the requirements of the City of Mouroe Sewer Use Ordinance and North Carolina General
Statute or implementing regulations.
23. Re -Application for Permit Renewal
The permittee is responsible for filing an application for reissuance of this permit at least 120
days prior to its expiration date. The permittee is not authorized to discharge after the
expiration (late of this permit if this re -application deadline has not been met.
24. Dilution Prohibition
The permittee shall not increase the use of potable or process water or in any other way attempt
to dilute the discharge as a partial or complete substitute for adequate treatment to achieve
compliance with the limitations contained in this permit.
LIUP#=> LP-001
Page:12
Effective Date: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
25. Reports of Changed Conditions
The permittee shall give notice to the City of Monroe of any planned significant changes to the
permittee's operations or system which might alter the nature, quality, or volume of its
wastewater at least 60 days before the change. Such changes, however, do not stay any
condition of this permit. If the changes require additions or modifications to pretreatment
facilities to comply with this permit, all such modifications shall be approved and constructed
before planned changes are made. The permittee shall not begin the changes until receiving
written approval from the City of Monroe. Also see PART H, 30 below for additional reporting
requirements for spill/slug issues.
26. Construction
No construction of pretreatment facilities or additions thereto shall be begun until Final Plans
and Specifications have been submitted to the City of Monroe and written approval and an
Authorization to Construct has been issued.
27. Reopener
The permit shall be modified or, alternatively, revoked and reissued to comply with any
applicable effluent standard or limitation for the control for any pollutant shown to contribute
to toxicity of the WWTP effluent or any pollutant that is otherwise limited by the POTW
discharge permit. The permit as modified or reissued under this paragraph may also contain
any other requirements of State or Federal pretreatment regulations then applicable.
28. Categorical Reopener
This permit shall be modified, or alternatively, revoked and reissued, to comply with any
applicable effluent standard or limitation issued or approved under Sections 302(b)(2)(C) and
(D), 304(b)(2), and 307(a)(2) of the Clean Water Act, if the effluent standard or limitation so
issued oe• approved:
1) contains different conditions or is otherwise more stringent than any effluent
limitation in this permit; or
2) controls any pollutant not limited in this permit.
The permit as modified or reissued under this paragraph shall also contain any other
requirements of the Act then applicable.
24. General Prohibitive Standards
The permittee shall comply with the general prohibitive discharge standards in 40 CFR
403.5(a) and (b) of the Federal pretreatment regulations, and shall comply with the prohibitive
discharge standards in §52.020 and §52.023 of the City Sewer Use Ordinance except as
specifically stated otherwise in this permit.
LIUP##=> LP-001
Page:13
Effective Dale: July 1, 2016

PART II
General Conditions
Local Industrial User Permit (LIUP)
30. Reports of Potential Problems
The permittee shall provide protection from accidential and slug discharges of prohibited
materials and other substances regulated by this permit. The permittee shall also notify the
City of Monroe immediately of any changes at its facility affecting the potential for spills and
other accidential discharge, discharge of a non -routine, episodic nature, a non -customary batch
discharge, or a slug load as defined in the City of Monroe Sewer Use Ordinance.
Additionally, the permittee shall notify by telephone the City of Monroe immediately of all
discharges that could cause problems to the POTW including any slug loadings as defined in
the Sewer Use Ordinance. If the permittee experiences such a discharge, they shall inform the
City of Monroe Pretreatment Coordinator, telephone number [phone], if no answer, the
Wastewater Treatment Plant, telephone number [phone] and [phone], if no
anwer, the Wastewater Treatment Plant Superintendent, telephone number [phone]
immediately upon the first awareness of the commencement of the discharge. Leaving a
message will not be acceptable until all phone numbers listed above have been attempted.
Notification shall include location of the discharge, type of waste, concentration and volume if
known and corrective actions taken by the permittee. A written follow-up report thereof shall
be filed by the permittee within (5) clays, unless waived by the City of Monroe.
LIUP##=> LP-001
Page:14
Effective Date: July 1, 2016

PART III
Special Conditions
Local Industrial User Permit (LIUP)
Flow Measurement
1. The Permittee shall provide and operate monitoring facilities for the inspection,
sampling and flow measurement of the permittee's process wastewater discharges.
2. The permittee shall maintain appropriate discharge flow measurement devices and
methods consistent with approved engineering and scientific practices to ensure the
accuracy and reliability of measurements of the volume of monitored discharges.
Devices installed shall be a continuous recording flow meter capable of measuring flows
with a maximum deviation of less than 5% from true discharge rates throughout the
range of expected discharge volumes.
3. The approved wastewater meter shall he installed, maintained, and calibrated once
every six months.
4. The wastewater meter must have a non-resettable mechanical totalizer that reads in
gallons.
5. Flow monitoring equipment and sampling point should be located in an area
accessible to the City of Monroe personnel without prior notification. The City of
Monroe must be supplied with any keys and/or other tools necessary to perform
the aforementioned.
6. There shall be no by-pass capability of the wastewater metering devices or the
sampling point.
7. The permittee shall maintain flow, maintenance, and calibration records for a
minimum of three years.
8. In the event of temporary unintentional failure of the flow meter, the permittee shall
notify the Pretreatment Coordinator as soon as possible, but in no case beyond 24 hours
after first becoming aware of the failure. Repair shall be under taken as quickly as
possible.
3. High Strength Surcharges
Notwithstanding any concentrations permitted for total suspended solids, 5 day BOD or
nitrogen ammonia stated in Part I, Section F of the Permit, the permittee shall be responsible
for the payment of high strength surcharges at rates that may be established in the future by
the Monroe City Council.
LIUP#ALP-001
Page: 15
Effective Date: July 1, 2016

&VA
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory
Governor
Catalent Pharma Solutions
2725 Scherer Drive North
St. Petersburg, FL 33716-0.1016
Attention: Dina Kostakis, General Manager
Dear Ms. Kostakis:
Donald van der Vaart
Secretary
RE: Compliance Inspection Report
Groundwater Remediation
Permit No. WQ0010607
Former RP Scherer/Chelsea Labs
2021 E. Roosevelt Ave., Monroe
Union County
——ne-MROwould like -to -extend -our -thanks -to -the -staff -of Rogers & Callcot-and-to-Nfi-l-erry-Sullivan --
Aqua-Trol for taking time to meet with us so we were able to review the remediation system at the permitted
facility.
On August 6, 2015, a compliance inspection was performed for the groundwater remediation system of the
former Catalent Pharma Solutions at 2021 Roosevelt Avenue, Monroe, Union County. During this
inspection the recovery and treatment system were reviewed, the recovery wells were checked for
operational functionality and the treatment system was discussed with representatives of Rogers &Callcott
and Aqua-Trol, Inc. Please see the attached inspection report.
The permit expiration date is August 31, 2018. Per permit requirements, a renewal application is due 180
days prior to expiration.
dward Watson
Hydrogeologist
Division of Water Resources
Water Quality Regional Operations Section
Cc: George Maalouf, Rogers & Calcott Engineers, Inc. POB 5655 Greenville, SC 29606
Mooresville Regional Office
610 East.CenterAvenue, Suite 301, Mooresville, North.Carolina 28115
Phone: [phone] / Fax: [phone] / Customer Service: 1-877-623-6748
Internet: www.ncdenr.gov
An Equal Opportunity1 Affirmative Action Employer— Made in part by recycled paper

rWatson, Edward M
From:
Rudder, James
Sent:
Wednesday, July 30, 2014 1:18 PM
To:
Bateson, James; Caulk, Kim; Doorn, Peter; Jesneck, Charlotte; Walch, John; Marks, Cheryl;
Mccarty, Bud; Jackson, Vance; Williford, Mike; Burch, Brent; Patterson, Jenny; Scott,
Michael; Watkins, Jason; Shackelford, Dennis; Bush, Ted; Zimmerman, Jay; Davidson,
Landon; Knight, Sherri; May, David; Barnhardt, Art; Pitner, Andrew; King, Morella s;
Andersen, Jan; Kromm, Carin; Bullock, Scott; Powers, Mark; Taraban, Ron; Day, Collin;
Ramey, David E; Alvalle, Miguel A
Cc:
Akroyd, Cathy R; Culpepper, Linda; Liggins, Shirley; Nicholson, Bruce; [e-mail];
[e-mail]
Subject:
Brownfields Program Initial Notification - Mac, LLC, Corrected Brownfields Project
Number
To DENR Cleanup Programs:
This is a repeat of the email Notification sent yesterday afternoon, but contains a corrected Brownfields Project
Number. Thank you.
This is an internal courtesy notice to inform your program that the DENR Brownfields Program is in receipt of a
Brownfields Property Application (BPA), submitted by Mac, LLC as prospective developer (PD), seeking entry into the
brownfields program for the following property:
Site Name: Former R.P. Scherer/Chelsea Labs
Address: 2021 E. Roosevelt Boulevard
City/County/Zip: Monroe, Union County 28110
Tax ID: 09117004
AKA: Give other regulatory site name(s), if applicable
Known Identifying Numbers:
NCD#: 981863228
GW Incident #: 9000
BF Number: 18034-14-090
Others? Non -Discharge Permit WQ0010607
We are now evaluating Mac, LLC,(and affiliates Royal Palm Pools, Inc.; Armor -Clad Fence, LLC) and the subject
property(s) for eligibility for entry into the Brownfields Program. Under the Brownfields Property Reuse Act, only
entities that did not cause or contribute to the contamination at the property are eligible to enter the program. The
applicant PD below has asserted that 1) it has not caused or contributed to the contamination at the property, and 2)
that it has substantially complied with laws, regulations, and rules for the protection of the environment. If you have
any information to suggest otherwise, please provide that information to me (via the contact information at the bottom
of this notice) by Tuesday, August 12, 2014.
Information regarding the applicant PD, Mac, LLC, including the primary PD contact person, is as follows:
PD:
Mac, LLC, Principal Officer is William MacTaggart, P.O. Box 985, Monroe, NC 28111
[e-mail], 704.661.3495
PD Contact:

10,resentative is Christopher Duggan,
cdu([e-mail], 704.776.9610
The Duggan Law Firm, PC, P.O. Box 481, Monroe, NC 28111
It is important to note that a Brownfields Agreement (BFA) has no legal effect on your agency's authority to regulate
or enforce against any and all parties who caused or contributed to the contamination at the property. A BFA only
provides liability protection to a non -causative redeveloper of the property. In fact, the BFA will require the developer
to provide access to the property to any party doing work under another DENR program, and the Brownfields Program
has several sites where another program is enforcing against a responsible party while we are working with the
developer on brownfields actions. The developer will only be required to make the property safe for its intended re-
use. That will not include cleanup to unrestricted use standards, unless that is consistent with the developer's
proposed use of the property.
If you have any questions, please don't hesitate to contact me. Thanks very much for your help.
Jim Rudder
James Rudder, P.G.
Project Manager
INC Department of Environment and Natural Resources
Division of Waste Management - Brownfields Program
Physical Address: 217 West Jones Street, Raleigh. 27603
Mailing Address: 1646 Mail Service Center, Raleigh, NC 27699-1646
Phone/Fax: [phone]
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.
James Rudder, P.G.
Project Manager
NC Department of Environment and Natural Resources
Division of Waste Management — Brownfields Program
Physical/Overnight Delivery Address: 217 West Jones Street, Raleigh, 27603
Mailing Address. 1646 Mail Service Center, Raleigh, NC 27699-1646
Phone/Fax: [phone]
Email correspondence to and from this address is subject to the Nroth Carolina Public Records Law and may be disclosed to third parties unless the
content is exempt by statute or other regulation.

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ROGERS & CALLCOTT
ENGINEERS, INC.
P.O. Box 5655, Greenville, SC 29606
Phone [phone] • FAX [phone]
March 16, 2004
Mr. Alan W. Klimek, P.E.
NCDENR, Div. of Water Quality
Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
AN EMPLOYEE -OWNED COMPANY
NC DEPT OF ENVIRONMENT
AND NATURAL RESOURCES
RECEIVED
MAR 1 R ?004
MOC-R F\" rE REGIONAL OFFICE
DWQ-GROUNDWATER SECTION
By Federal Express
Subject: Notification of Remediation System Restoration
Non -Discharge Permit VVQ0010607
Cardinal Health 409, Inc. (Formerly R.P.Scherer/Chelsea Laboratories)
Union County, NC
Dear Mr. Klimek:
An oil/water separator was added to the groundwater remediation system at the subject
site on April 1, 1998, to address diesel fuel encountered in one of the recovery wells (MW-
4). Subsequently, NCDENR issued an approval to discontinue monitoring for diesel fuel
constituents (EPA Method 625) on October 5, 1999, based on the absence of the
constituents in the monthly samples from the well since June 1998 and the absence of a
sheen or petroleum odor in the oil/water separator since November 1998. As a
precautionary screening measure for the possible recurrence of diesel fuel, we have
voluntarily continued to analyze the monthly effluent sample from the treatment system for
Oil & Grease and maintained routine visual inspections of the flow through the oil/water
separator. Based on the Oil and Grease data and weekly inspections, there has been no
indication of such a recurrence for more than five years.
At this time, we plan to discontinue testing for Oil & Grease and by-pass the oil/water
separator as these measures are no longer needed. Flow from MW-4 will be restored to
its original configuration by closing a valve to the separator. The oil/water separator will
remain connected to the system in the event it is needed in the future. An approximately
one -week system shutdown is tentatively scheduled for the week of April 19, 2004, for
system maintenance, including rust treatment of the air stripper and replacement of the
above ground galvanized piping and fittings. The proper valves needed to isolate the
oil/water separator will be installed at that time. After maintenance, the system will be
ENGINEERING
LABORATORY
HYDROGEOLOGY

Notification of Remediation System Restoration
Non -Discharge Permit WQ0010607
Cardinal Health 409, Inc. (Formerly R.P. SchererlChelsea Laboratories)
Union County, NC
March 16, 2004
restored to normal operation for the recovery and treatment of chlorinated VOCs as
originally designed.
The oil/water separator and Oil & Grease testing are not part of the Non -Discharge permit
and would not require any permit modification. If you have any questions or concerns,
please contact me at 864-232-1556.
Sincerely,
ROGERS & CALLCOTT ENGINEERS, INC.
George Y. Maalouf, P.G.
NC License No. 1129
Copy: DENR, DWQ, Groundwater Section, Central Files
DENR, DWQ, Water Quality Section, Central Files
DENR, Mooresville Regional Office, DWQ, Water Quality Section
DENR, Mooresville Regional Office, DWQ, Groundwater Section
DENR, Technical Assistance and Certification Unit
Union County Health Department, Monroe, NC
Mr. Russell Colbath, Director of Water Resources, City of Monroe
Mr. Victor San Agustin, R. P. Scherer
Mr. Jerry Sullivan, Aqua -Trot
Mr. Peter Holmes, Clark Hill
103-c:\clients\rpscherer\ Page 2 of 2 Rogers R Callcott Engineers. Inc.
Notification of Remediation System Restoration.doc

'OGERS & CALLCOTT
ENGINEERS, INC.
�lllfff�I I P.O. Box 5655, Greenville, SC 29606
o Phone [phone] • FAX [phone]
October 10, 2003
Ms. Peggy Finley
NC Dept. of Environment and Natural Resources
Division of Water Quality, Groundwater Section
919 North Main Street
Mooresville, NC 28115
AN EMPLOYEE -OWNED COMPANY
INC DEPT OF P-10RONMENT
AND NATUkwj. RESOURCES
RECEIVED
0C i 1 6 �003
MOORESVILLE REGIONAL OFFICE
DWQ-GROUNDWATER SECTION
Subject: Cardinal Health 409, Inc. (Formerly R. P. Scherer)/Chelsea Laboratories
2021 E. Roosevelt Blvd.
Monroe, Union County, North Carolina
Groundwater Remediation System Shutdown for Cleaning
Non -Discharge Permit #WQ0010607
Rogers & Callcott Project Number 93-121
Dear Ms. Finley:
As we discussed by telephone on October 3, 2003, we have temporarily shut down the
groundwater recovery and treatment system at this facility for cleaning. The system was
shut down on September 24, 2003, and will resume operation during the week of October
13" or 20tt
Over the last six years that the system has been in operation, scale has deposited in the
pipes and tanks that receive treated water from the air -stripper. The air stripper and
meters have been cleaned routinely, but this would be the first cleaning of the pipes and
tanks.
If you have any questions or comments, please call me at [phone].
Sincerely,
ROGERS & CALLCOTT ENGINEERS, INC.
George Y. Maalouf, P.G.
NC Registration #1129
Copy: Kyle Ketchum, City of Monroe
Victor San Agustin, Cardinal
Peter Holmes, Clark Hill PLC
Jerry Sullivan, Aqua -Trot (on -site file)

yV V ri`�
AUG 20 1999 J. L. Rogers. P.E.
ROGERS & CALLCOTT F. D. Cailcot[. P.E.
ENGINEERS, INC. S. W. Avery. Jr..
Laboraton Director
P.O. Box 5655, Greenville, SC 29606
Phone [phone] • FAX [phone]
August 19, 1999
Mr. Samar Bou-Ghazale / Mr. Rex Gleason
NC Dept. of Environment and Natural Resources
Division of Environmental Management
Water Quality Section
919 North Main Street
Mooresville, NC 28115
By Facsimile: [phone]
By Certified Mail: Z305095269
Ref: Five -Day Written Report of an Upset
NPDES Permit #NC0084344, Non -Discharge Permit #WQ0010607
R. P. Scherer/Chelsea Laboratories
2021 E. Roosevelt Blvd., Monroe, Union County, North Carolina
R & C Project Number 93-121
Gentlemen:
Please consider this letter as the five-day written report of an upset that may have occurred
in the groundwater remediation system at the subject site. A 24-hour verbal report and
written confirmation were submitted to your office on July 30, 1999, when we received the
first indication of a possible upset. Since then, the laboratory analyses were completed
and an analytical report was received on August 18, 1999.
As indicated in our written confirmation to the 24-hour verbal report, two repeat samples
of the effluent were collected for confirmation on July 30, 1999. The samples were
collected at the effluent sampling port and at the end of the pipe. The system was also
shut down temporarily on July 30, 1999 until results of the confirmation samples became
available to prevent any discharge that potentially could had any adverse effects.
Laboratory analysis of the initial effluent sample collected on July 21, 1999 indicated that
the upset had resulted in readings above the NPDES effluent daily maximum for
trichloroethene and tetrachloroethene. The detected levels were 160 and 590 ug/L,
compared with the daily maximum of 92.4 and 8.85 ug/L for each compound, respectively.
Other VOCs were detected but were not above any established daily maximums.
However, analysis of the repeat samples (collected on July 30, 1999) did not confirm the
results of the earlier sample. No VOCs were detected in the two repeat samples except
9

Five -Day Written Report of a Possible Upset
NPDES Permit #NC0084344, Non -Discharge Permit #WQ0010607
R. P. Scherer/Chelsea Laboratories
August 19, 1999
for tetrachloroethene at concentrations of 0.79 and 0.63 ug/L. These concentrations are
more than ten times below the daily maximum of 8.8 ug/L. Copies of the laboratory
analysis reports are attached. A Daily Monitoring Report (DMR) is being prepared and will
be submitted to the NCDENR by the end of August as required by the NPDES permit.
In an effort to identify the cause of the upset, Rogers & Callcott has interviewed the
operator and the manufacturer of the system. We have also closely reviewed the system
design, its operation and maintenance, sampling and analysis procedures and historical
data from the site. The evaluation confirmed that the system was properly designed, and
at the time was being properly operated and maintained. Enclosed are copies of the
operation and maintenance records for the last three months and a table and graph
showing the amount of VOCs recovered from the aquifer. Moreover, as the data submitted
in the monthly DMRs show, no significant changes have occurred in the influent
concentrations in July 1999. Therefore, it is apparent that the upset was due to factors
beyond our control that are unrelated to the system design, operation or maintenance.
Because the latest effluent data did not confirm the July 21, 1999 results, R. P. Scherer
plans to re -activate the remediation system as soon as possible. In my discussion with Mr.
Bou-Ghazale on August 18, 1999, R. P. Scherer was authorized to re -activate the system
on August 23, 1999. It is important to re -start the system in August to allow for the routine
influent/effluent and groundwater monitoring required by the permits for August.
We appreciate your attention to this matter. Please contact me if you have any concerns
or need additional information.
Sincerely,
J. L. ROGERS & CALLCOTT ENGINEERS, INC.
George Y. Maalouf, P.G.
Enclosures
Copy.- DEM, Water Quality Section, Central Files
DEM, Ground Water Section, Permits and Compliance Unit
Ms. Peggy Finley, Groundwater Section, Mooresville Office
Mr. Gregory Schurig, R. P. Scherer
Mr. Jerry Sullivan, Aqua -Trot
Mr. Peter Holmes, Clark Hill
gym-c:\clients\rpscherer\5dayupst 2 J. L. Rogers & Callcott Engineers, Inc.

f `
"OGERS & CALLCOTT J. L. Rogers, P.E.
ENGINEERS, INC. R C Q•' V F. D. Callcott, P.E.
S. W. Avery, Jr.,
pp� I' I d
P.O. Box 5655, Greenville, SC 29606 VQ b� �.. r�P D�tO R 7 Laboratory Director
Phone [phone] • FAX [phone]
CLIENT: RPS/CHELSEA Gr� PAGE 1
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999 DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56967
56968
PARAMETER
VOLATILE ORGANICS, µg/L
ACETONE
BENZENE
BROMOBENZENE
BROMOCHLOROMETHANE
BROMODICHLOROMETHANE
BROMOFORM
BROMOMETHANE
n-BUTYLBENZENE
sec-BUTYLBENZENE
tert-BUTYLBENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
2-CHLOROTOLUENE
4-CHLOROTOLUENE
1,2-DIBROMO-3-CHLOROPROPANE
DIBROMOCHLOROMETHANE
1,2-DIBROMOETHANE
DIBROMOMETHANE
CONTINUED ON PAGE 2
SAMPLE DESCRIPTION
INFLUENT (2,3,&5) GRAB ON 07/21/99 AT 1700
INFLUENT 4 GRAB ON 07/21/99 AT 1630
56967
INF. 2,3,5
<500
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
28
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
56968
INF. 4
<500
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
46
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0

CLIENT: RPS/CHELSEA
MONROE, NC
• C/O GEORGE MAALOUF
PAGE 2
DATE RECEIVED: 07/22/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56967
56968
PARAMETER
VOLATILE ORGANICS, µg/L
(CONTINUED)
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
cis-1,2-DICHLOROETHENE
trans-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
1,3-DICHLOROPROPANE
2,2-DICHLOROPROPANE
1,1-DICHLOROPROPENE
ETHYLBENZENE
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
p-ISOPROPYLTOLUENE
METHYLENE CHLORIDE
NAPHTHALENE
n-PROPYLBENZENE
STYRENE
1,1,1,2-TETRACHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
TOLUENE
1,2,3-TRICHLOROBENZENE
SAMPLE DESCRIPTION
INFLUENT (2,3,&5) GRAB ON 07/21/99 AT 1700
INFLUENT 4 GRAB ON 07/21/99 AT 1630
56967
INF. 2,3,5
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
200
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
< 5 . 0
<5.0
<5.0
7.9
<5.0
<5.0
<5.0
<5.0
<5.0
1100
<5.0
<5.0
56968
INF. 4
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
360
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
<5.0
7.4
<5.0
<5.0
<5.0
<5.0
<5.0
1700
<5.0
<5.0
CONTINUED ON PAGE 3

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
PAGE 3
DATE RECEIVED: 07/22/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
SAMPLE NUMBER
56967
56968
Iy-m-gra i�T111�:7
VOLATILE ORGANICS, µg/L
(CONTINUED)
1,2,4-TRICHLOROBENZENE
1,1,1-TRICHLOROETHANE
1,1,2-TRICHLOROETHENE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
1,2,3-TRICHLOROPROPANE
1,2,4-TRIMETHYLBENZENE
1,3,5-TRIMETHYLBENZENE
VINYL CHLORIDE
m/p-XYLENE
HEXANE
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE DESCRIPTION
INFLUENT (2,3,&5) GRAB ON 07/21/99 AT 1700
INFLUENT 4 GRAB ON 07/21/99 AT 1630
56967
INF. 2,3,5
<5.0
<5.0
<5.0
360
<5.0
<5.0
<5.0
<5.0
<5.0
<10
<5.0
56968
INF. 4
<5.0
<5.0
<5.0
790
<5.0
<5.0
<5.0
<5.0
<5.0
<10
<5.0
CONTINUED ON PAGE 4

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
PAGE 4
DATE RECEIVED: 07/22/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
PARAMETER
ACID/BASE NEUTRALS, µg/L
PHENOL
2-CHLOROPHENOL
2-NITROPHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
P-CHLORO-M-CRESOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROPHENOL
4-NITROPHENOL
4,6-DINITRO-O-CRESOL
PENTACHLOROPHENOL
BIS(2-CHLOROETHYL)ETHER
B I S( 2- CHLORO I SOPRO PYL) ETHER
HEXACHLOROETHANE
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
ISOPHORONE
BIS(2-CHLOROETHOXY)METHANE
HEXACHLOROCYCLOPENTADIENE
2-CHLORONAPHTHALENE
DIMETHYLPHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
CONTINUED ON PAGE 5
SAMPLE DESCRIPTION
INFLUENT 4 GRAB ON 07/21/99 AT 1630
56968
INF. 4
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
PAGE 5
DATE RECEIVED: 07/22/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
.•m
PARAMETER
ACID/BASE NEUTRALS, µg/L
(CONTINUED)
ACENAPHTHENE
2,4-DINITROTOLUENE
DIETHYLPHTHALATE
FLUORENE
4-CHLOROPHENYL PHENYL ETHER
DIPHENYLAMINE (N-NITROSO)
AZOBENZENE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYLPHTHALATE
BENZO(A)ANTHRACENE
3,3'-DICHLOROBENZIDINE
CHRYSENE
BIS(2-ETHYLHEXYL)PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B)FLUORANTHENE
BENZO (K) FLUORANTHENE
BENZO (A) PYRENE
SAMPLE DESCRIPTION
INFLUENT 4 GRAB ON 07/21/99 AT 1630
56968
INF. 4
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
CONTINUED ON PAGE 6

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
PAGE 6
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
laaan\ui�Illi�i:7
ACID/BASE NEUTRALS, µg/L
(CONTINUED)
INDENO(1,2,3-C,D)PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO (G, H, I) PERYLENE
SAMPLE DESCRIPTION
INFLUENT 4 GRAB ON 07/21/99 AT 1630
56968
INF. 4
<10
<lQ
<10
TENTATIVELY IDENTIFIED COMPOUNDS
COMPOUND
TETRACHLOROETHENE
*REFER TO METHOD 6210D RESULTS
RETENTION
°s FIT TIME, min.
94.6 4.000
DISCLAIMER FOR ALL TENTATIVELY IDENTIFIED COMPOUNDS
CONTAINED IN THIS REPORT
ESTIMATED
CONCENTRATION, µQ/L
THE COMPOUND NAMES REPORTED FOR CHROMATOGRAPHIC PEAKS THAT ARE NOT TARGET COMPOUNDS ARE ONLY BEST
SPECTRAL FITS DERIVED FROM A COMPARISON TO OUR 62,235 COMPOUND NIST SPECTRAL DATABASE. ESTIMATED
CONCENTRATIONS ARE BASED UPON THE TOTAL ION AREAS COMPARED TO THAT OF THE NEAREST INTERNAL STANDARD
ASSUMING A RESPONSE FACTOR OF ONE.
NOTE THAT THESE DATA ARE PROVIDED ONLY FOR ESTIMATING THE RINDS OF MATERIALS THAT MAY BE ASSOCIATED
WITH A PARTICULAR SAMPLE, AND SHOULD NOT BE CONSTRUED AS EVIDENCE THAT THE NAMED COMPOUNDS ARE
ACTUALLY PRESENT IN THAT SAMPLE.
CONTINUED ON PAGE 7

CLIENT, RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
PAGE 7
DATE RECEIVED: 07/22/1999 DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
SAMPLE NUMBER
56967
56968
PARAMETER
SURROGATE
VOLATILE ORGANICS
4-BROMOFLUOROBENZENE
1,2-DICHLOROETHANE-D4
ACID/BASE NEUTRALS
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE DESCRIPTION
INFLUENT (2,3,&5) GRAB ON 07/21/99 AT 1700
INFLUENT 4 GRAB ON 07/21/99 AT 1630
QUALITY CONTROL SUMMARY
56967 56968
INF. 2,3,5 INF. 4
% RECOVERY
104 (105) 108 (102)
95 (98) 98 (95)
NITROBENZENE-D5 ---- 86
2-FLUOROBIPHENYL ---- 79
TERPHENYL-D14 ---- 72
2-FLUOROPHENOL ---- 46
PHENOL-D5 ---- 33
2,4,6-TRIBROMOPHENOL ---- 82
NOTE: SURROGATE RECOVERIES ARE WITHIN CONTROL LIMITS UNLESS NOTED WITH AN ASTERISK
NOTE: NUMBERS IN PARENTHESIS ARE FOR SURROGATE RECOVERY REANALYSIS.
CONTINUED ON PAGE 8

CLIENT RPS/CHELSEA
MONROE, NC
+' C/O GEORGE MAALOUF
PAGE 8
DATE RECEIVED: 07/22/1999 DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER SAMPLE DESCRIPTION
56967 INFLUENT (2,3,&5) GRAB ON 07/21/99 AT 1700
56968 INFLUENT 4 GRAB ON 07/21/99 AT 1630
ANALYSES CHRONOLOGY
SAMPLE#
PARAMETER
DATE/TIME ANALYZED
56967
VOLATILES
07/30
@
0308
INF. 2,3,& 5
AND
07/30
@
0131
56968
VOLATILES
07/30
@
0202
INF. 4
AND
07/30
@
0043
ABN
08/08
@
0148
AND
07/23
REPORTED BY:
CC: NCDEHNR — GR UNDWAT SECT
GREGORY A. S (RP SCh
JERRY SULLIVAN (AQUA—TROL)
METHOD# ANALYST
6210D LYNCH
11 fl
6210D LYNCH
it to
625 "
. AVI�W, LABORATORY DIRECTOR

'110GERS & CALLCOTT
ENGINEERS, INC.
P.O. Box 5655, Greenville, SC 29606
Phone [phone] • FAX [phone]
J. L. Rogers, P.E.
F. D. Callcott, P.E.
S. W. Avery, Jr.,
Laboratory Director
CLIENT: RPS/CHELSEA PAGE 1
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999 DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
SAMPLE NUMBER
56969
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
PARAMETER
RESULT
DATE/TIME
METHOD#
ANALYST
ARSENIC, mg/L
<0.02
07/26 @ 1050
200.7
ASHLEY
LEAD, mg/L
<0.02
08/04 @ 1028
"
11
MERCURY, mg/L
<0.0002
08/03 @ 0850
245.1
LYNN
TOTAL OIL AND GREASE, mg/L
<5.0
07/26 @ 0820
413.1
SALLEY
VOLATILE ORGANICS, µg/L
ACETONE
<50
BENZENE
<0.50
BROMOBENZENE
<0.50
BROMOCHLOROMETHANE
<0.50
BROMODICHLOROMETHANE
<0.50
BROMOFORM
<0.50
BROMOMETHANE
<0.50
n-BUTYLBENZENE
<0.50
sec-BUTYLBENZENE
<0.50
tert-BUTYLBENZENE
<0.50
CARBON TETRACHLORIDE
<0.50
CHLOROBENZENE
<0.50
07/29 @ 2216
AND 08/03 @ 0001
AND 08/03 @ 0049
6210D LYNCH
tt
t� ,t
CONTINUED ON PAGE 2

CLIENT•: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
PAGE 2
DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56969
PARAMETER
VOLATILE ORGANICS, µg/L
(CONTINUED)
CHLOROETHANE
CHLOROFORM
CHLOROMETHANE
2-CHLOROTOLUENE
4-CHLOROTOLUENE
1,2-DIBROMO-3-CHLOROPROPANE
DIBROMOCHLOROMETHANE
1,2-DIBROMOETHANE
DIBROMOMETHANE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
DICHLORODIFLUOROMETHANE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE
cis-1,2-DICHLOROETHENE
trans-1,2-DICHLOROETHENE
1,2-DICHLOROPROPANE
1,3-DICHLOROPROPANE
2,2-DICHLOROPROPANE
1,1-DICHLOROPROPENE
ETHYLBENZENE
CONTINUED ON PAGE 3
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
RESULT DATE/TIME METHOD# ANALYST
<0.50
15
<0'.50
< 0 . 5 0
<0.50
< 0 . 5 0
<0.50
< 0 . 5 0
<0.50
<0.50
<0.50
<0.50
< 0 . 5 0
2.5
0.54
1.4
83
<0.50
<0.50
<0.50
< 0 . 5 0
< 0 . 5 0
< 0 . 5 0
07/29 @ 2216 6210D LYNCH
AND 08/03 @ 0001 if
AND 08/03 @ 0049 " It

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
PAGE 3
DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56969
PARAMETER
VOLATILE ORGANICS, µg/L
(CONTINUED)
HEXACHLOROBUTADIENE
ISOPROPYLBENZENE
p-ISOPROPYLTOLUENE
METHYLENE CHLORIDE
NAPHTHALENE
n-PROPYLBENZENE
STYRENE
1,1,1,2-TETRACHLOROETHANE
1,1,2,2-TETRACHLOROETHANE
TETRACHLOROETHENE
TOLUENE
1,2,3-TRICHLOROBENZENE
1,2,4-TRICHLOROBENZENE
1,1,1-TRICHLOROETHENE
1,1,2-TRICHLOROETHANE
TRICHLOROETHENE
TRICHLOROFLUOROMETHANE
1,2,3-TRICHLOROPROPANE
1,2,4-TRIMETHYLBENZENE
1,3,5-TRIMETHYLBENZENE
VINYL CHLORIDE
m/p-XYLENE
o-XYLENE
HEXANE
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
RESULT DATE/TIME
<0.50
<0.50
<0.50
1.2
<0.50
<0.50
<0.50
<0.50
<0.50
590
<0.50
<0.50
<0.50
<0.50
<0.50
160
<0.50
<0.50
<0.50
<0.50
<0.50
<1.0
<0.50
<0.50
07/29 @ 2216
AND 08/03 @ 0001
AND 08/03 @ 0049
METHOD# ANALYST
6210D LYNCH
If
CONTINUED ON PAGE 4

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
PAGE 4
DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56969
PARAMETER
ACID/BASE NEUTRALS, µg/L
PHENOL
2-CHLOROPHENOL
2-NITROPHENOL
2,4-DIMETHYLPHENOL
2,4-DICHLOROPHENOL
P-CHLORO-M-CRESOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROPHENOL
4-NITROPHENOL
4,6-DINITRO-O-CRESOL
PENTACHLOROPHENOL
B I S ( 2 - CHLOROETHYL) ETHER
BIS(2-CHLOROISOPROPYL)ETHER
HEXACHLOROETHANE
N-NITROSODI-N-PROPYLAMINE
NITROBENZENE
ISOPHORONE
BIS(2-CHLOROETHOXY)METHANE
HEXACHLOROCYCLOPENTADIENE
2-CHLORONAPHTHALENE
DIMETHYLPHTHALATE
ACENAPHTHYLENE
2,6-DINITROTOLUENE
CONTINUED ON PAGE 5
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
RESULT DATE/TIME METHOD# ANALYST
08/07 @ 2349
EXTRACTED 07/23/99
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
625 LYNCH

CLIENT': RPS/CHELSEA
,i MONROE , NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
PAGE 5
DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56969
PARAMETER
ACID/BASE NEUTRALS, µg/L
(CONTINUED)
ACENAPHTHENE
2,4-DINITROTOLUENE
DIETHYLPHTHALATE
FLUORENE
4-CHLOROPHENYL PHENYL ETHER
DIPHENYLAMINE (N-NITROSO)
AZOBENZENE
4-BROMOPHENYL PHENYL ETHER
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DI-N-BUTYLPHTHALATE
FLUORANTHENE
PYRENE
BUTYLBENZYLPHTHALATE
BENZO(A)ANTHRACENE
3,3'-DICHLOROBENZIDINE
CHRYSENE
BIS(2-ETHYLHEXYL)PHTHALATE
DI-N-OCTYLPHTHALATE
BENZO(B)FLUORANTHENE
BENZO(K)FLUORANTHENE
BENZO (A) PYRENE
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
RESULT DATE/TIME METHOD# ANALYST
08/07 @ 2349
EXTRACTED 07/23/99
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
<10
625 LYNCH
CONTINUED ON PAGE 6

CLIEN'P: RPS/CHELSEA
,- MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
PAGE 6
DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
56969
PARAMETER
ACID/BASE NEUTRALS, µg/L
(CONTINUED)
INDENO(1,2,3-C,D)PYRENE
DIBENZO(A,H)ANTHRACENE
BENZO(G,H,I)PERYLENE
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
RESULT DATE/TIME METHOD# ANALYST
08/07 @ 2349 625
EXTRACTED 07/23/99
<10
<10
<10
TENTATIVELY IDENTIFIED COMPOUNDS
COMPOUND
TETRACHLOROETHENE
*REFER TO METHOD 6210D RESULTS
RETENTION
FIT TIME, min.
93.2 3.990
DISCLAIMER FOR ALL TENTATIVELY IDENTIFIED COMPOUNDS
CONTAINED IN THIS REPORT
LYNCH
ESTIMATED
CONCENTRATION.
THE COMPOUND NAMES REPORTED FOR CHROMATOGRAPHIC PEAKS THAT ARE NOT TARGET COMPOUNDS ARE ONLY BEST
SPECTRAL FITS DERIVED FROM A COMPARISON TO OUR 62,235 COMPOUND NIST SPECTRAL DATABASE. ESTIMATED
CONCENTRATIONS ARE BASED UPON THE TOTAL ION AREAS COMPARED TO THAT OF THE NEAREST INTERNAL STANDARD
ASSUMING A RESPONSE FACTOR OF ONE.
NOTE THAT THESE DATA ARE PROVIDED ONLY FOR ESTIMATING THE RINDS OF MATERIALS THAT MAY BE ASSOCIATED
WITH A PARTICULAR SAMPLE, AND SHOULD NOT BE CONSTRUED AS EVIDENCE THAT THE NAMED COMPOUNDS ARE
ACTUALLY PRESENT IN THAT SAMPLE.
CONTINUED ON PAGE 7
L

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 07/22/1999
DATE REPORTED: 08/09/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
SAMPLE NUMBER
56969
SURROGATE
VOLATILE ORGANICS
4-BROMOFLUOROBENZENE
1,2-DICHLOROETHANE-D4
ACID/BASE NEUTRALS
NITROBENZENE-D5
2-FLUOROBIPHENYL
TERPHENYL-D14
2-FLUOROPHENOL
PHENOL-D5
2,4,6-TRIBROMOPHENOL
PAGE 7
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/21/99 AT 1600
QUALITY CONTROL SUMMARY
% RECOVERY
106 (103) (101)
86 (97) (96)
93
84
65
44
32
86
NOTE: SURROGATE RECOVERIES ARE WITHIN CONTROL LIMITS UNLESS NOTED WITH AN ASTERISK
NOTE: NUMBERS IN PARENTHESIS ARE FOR SURROGATE RECOVERY REANALYSIS.
REPORTED BY:
AWRY, LABORATORY DIRECTOR
CC: NCDERNR - GRO WATEly SECT
GREGORY A. SC P SCF]
JERRY SULLIVAN (AQUA-TROL)

n
ROGERS & CALLC®TT
CHAIN OF CUSTODY RECORD PAGE -(-OF , 2
ENGINEERS, INC.
'
P.O. Box 5655, Greenville, SC 29606
Filtered (Yes/Z{o)
Phone [phone] • FAX [phone]
Shipping Address: 718 Lowndes Hill Road
Refrigerated (Yes/bLO)
Greenville, S.C. 29607
hire
G
Container Type ce/�
Client Name
/�� !�
Container volume
Address
°'
Sample type (Qrob/composite)
Sample source (WW, GW, DW, other)
Report To:
r e
c
° c�
Preserved (Code)
Telephone No.
FAX No.
o
`
. y
A -None D-NaaH
B—HNo, E—HCL
u
E
4�
C—H,so. F—
PO No.
Project No.
Z
��Ns �/ N/UC;
Rogers & YrV
F N a l r�a.17 «
Callcott
Time Sample Description
E-°
Lab No. Date
O
COMMENTS:
9
i?oo
q
16�a
*
3
9�9
600
3
I
c 01 C 4
SAMPLER
Date/Time
Received by (Sig.)
Date/Time
HAZARDS ASSOCIATED WiM SAMPLES
Relin shed
Qt/_e�
zi�6
I
Shipper Name & #
Relinquished y (Sig.)
Date/Time
Receive y Z
®
D te/T1me
7 O�.�S-
Cd �
Shippe Name
-4 q
Relinquished by (Sig.)
Date/Time
Received
®
by (Sig.)
Date/11me
Receipt Total CL2_ mg/L Receipt pH
©
Shipper Name & Al
Subsequent Analysis: _Check)
Date Resubmitted
Seal at'chd b Recvd. Intact b Seal at'chd b Recvd. Intact byd
Form Revised June I`Jy4

1\ V�
ROGERS & CALLCOTT & dr °3ev1DI7 J. L. Rogers, P.E.
F. D. Callcott, P.E.
ENGINEERS, INC. 8 (/ /I i y A S. W. Avery, Jr.,
/ /
P.O. Box 5655, Greenville, SC 29606 Laboratory Director
Phone [phone] • FAX [phone]
CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 08/02/1999 DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER SAMPLE DESCRIPTION
PAGE 1
57617 EFFLUENT GRAB ON 07/30/99 AT 1430
57618 EFFLUENT (AT PIPE) GRAB ON 07/30/99
AT 1500
PARAMETER 57617 57618
EFF. GRAB EFF. AT PIPE
VOLATILE ORGANICS, µg/L
ACETONE
<0.50
<0.50
BENZENE
<0.50
<0.50
BROMOBENZENE
<0.50
<0.50
13ROMOCHLOROMETHANE
<0.50
<0.50
13ROMODICHLOROMETHANE
<0.50
<0.50
BROMOFORM
<0.50
<0.50
BROMOMETHANE
<0.50
<0.50
n-BUTYLBENZENE
<0.50
<0.50
sec-BUTYLBENZENE
<0.50
<0.50
tert-BUTYLBENZENE
<0.50
<0.50
CARBON TETRACHLORIDE
<0.50
<0.50
CHLOROBENZENE
<0.50
<0.50
CHLOROETHANE
<0.50
<0.50
CHLOROFORM
<0.50
<0.50
CHLOROMETHANE
<0.50
<0.50
2-CHLOROTOLUENE
<0.50
<0.50
4-CHLOROTOLUENE
<0.50
<0.50
1,2-DIBROMO-3-CHLOROPROPANE
<0.50
<0.50
DIBROMOCHLOROMETHANE
<0.50
<0.50
1,2-DIBROMOETHANE
<0.50
<0.50
DIBROMOMETHANE
<0.50
<0.50
CONTINUED ON PAGE 2

?CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 08/02/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER SAMPLE DESCRIPTION
PAGE 2
57617 EFFLUENT GRAB ON 07/30/99 AT 1430
57618 EFFLUFNT (AT PIPE) GRAB ON 07/30/99
AT 1500
PARAMETER 57617 57618
EFF. GRAB EFF. AT PIPE
VOLATILE ORGANICS, µg/L
(CONTINUED)
1,2-DICHLOROBENZENE
<0.50
<0.50
1,3-DICHLOROBENZENE
<0.50
<0.50
1,4-DICHLOROBENZENE
<0.50
<0.50
DICHLORODIFLUOROMETHANE
<0.50
<0.50
1,1-DICHLOROETHANE
<0.50
<0.50
1,2-DICHLOROETHANE
<0.50
<0.50
1,1-DICHLOROETHENE
<0.50
<0.50
cis-1,2-DICHLOROETHENE
<0.50
<0.50
trans-1,2-DICHLOROETHENE
<0.50
<0.50
1,2-DICHLOROPROPANE
<0.50
<0.50
1,3-DICHLOROPROPANE
<0.50
<0.50
2,2-DICHLOROPROPANE
<0.50
<0.50
1,1-DICHLOROPROPENE
<0.50
<0.50
ETHYLBENZENE
<0.50
<0.50
HEXACHLOROBUTADIENE
<0.50
<0.50
ISOPROPYLBENZENE
<0.50
<0.50
p-ISOPROPYLTOLUENE
<0.50
<0.50
METHYLENE CHLORIDE
<0.50
<0.50
NAPHTHALENE
<0.50
<0.05
n-PROPYLBENZENE
<0.50
<0.50
STYRENE
<0.50
<0.50
1,1,1,2-TETRACHLOROETHANE
<0.50
<0.50
1,1,2,2-TETRACHLOROETHANE
<0.50
<0.50
TETRACHLOROETHENE
0.79
0.63
TOLUENE
<0.50
<0.50
1,2,3-TRICHLOROBENZENE
<0.50
<0.50
CONTINUED ON PAGE 3

CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 08/02/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
PAGE 3
SAMPLE NUMBER
SAMPLE DESCRIPTION
57617
EFFLUENT GRAB
ON 07/30/99 AT 1430
57618
EFFLUENT (AT
PIPE) GRAB ON 07/30/99
AT 1500
PARAMETER
57617
57618
EFF. GRAB
EFF. AT PIPE
VOLATILE ORGANICS, µg/L
(CONTINUED)
1,2,4-TRICHLOROBENZENE
<0.50
<0.50
1,1,1-TRICHLOROETHANE
<0.50
<0.50
1,1,2-TRICHLOROETHANE
<0.50
<0.50
TRICHLOROETHENE
<0.50
<0.50
TRICHLOROFLUOROMETHANE
<0.50
<0.50
1,2,3-TRICHLOROPROPANE
<0.50
<0.50
1,2,4-TRIMETHYLBENZENE
<0.50
<0.50
1,3,5-TRIMETHYLBENZENE
<0.50
<0.50
VINYL CHLORIDE
<0.50
<0.50
O-XYLENE
<0.50
<0.50
m/p-XYLENE
<1.0
<1.0
HEXANE
<0.50
<0.50
CONTINUED ON PAGE 4

r CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 08/02/1999
PAGE 4
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
SAMPLE NUMBER
57617
57618
PARAMETER
SURROGATE
VOLATILE ORGANICS
4-BROMOFLUOROBENZENE
1,2-DICHLOROETHANE-D4
SAMPLE DESCRIPTION
EFFLUENT GRAB ON 07/30/99 AT 1430
EFFLUENT (AT PIPE) GRAB ON 07/30/99
AT 1500
QUALITY CONTROL SUMMARY
57617 57618
EFF. GRAB EFF. AT PIPE
% RECOVERY
81 95
80 94
NOTE: SURROGATE RECOVERIES ARE WITHIN CONTROL LIMITS UNLESS NOTED WITH AN ASTERISK
CONTINUED ON PAGE 5

* CLIENT: RPS/CHELSEA
MONROE, NC
C/O GEORGE MAALOUF
DATE RECEIVED: 08/02/1999
DATE REPORTED: 08/13/1999
N.C. LABORATORY CERTIFICATE NUMBER - 27
PERMIT #WQ0010607
R.P. SCHERER/CHELSEA LABS FACILITY
GROUNDWATER REMEDIATION FACILITIES
UNION COUNTY, NC
PAGE 5
SAMPLE NUMBER SAMPLE DESCRIPTION
57617 EFFLUENT GRAB ON 07/30/99 AT 1430
57618 EFFLUENT (AT PIPE) GRAB ON 07/30/99
AT 1500
ANALYSES CHRONOLOGY
SAMPLE# PARAMETER DATE/TIME ANALYZED METHOD# ANALYST
57617 VOLATILES 08/02 Q 1908 6210D LYNCH
EFF. GRAB
57618 VOLATILES
EFF. AT PIPE
REPORTED BY:
08/02 Q 2312 6210D LYNCH
AVXI�Y, LABORATORY DIRECTOR
CC: NCDERNR - GR UNDWATE SEC
GREGORY A. S IG RP SCH
JERRY SULLIVAN (AQUA-TROL)

ROGERS & CALLC®TT
CHAIN OF CUSTODY
RECORD PAGE Z OF .
ENGINEERS, INC.
P.O. Box 5655, Greenville, SC 29606
Filtered (les/tio)
Phone [phone] • FAX [phone]
Shipping Address: 718 Lowndes Hill Road
Refrigerated (yes/rLo)
Name
Greenville, S/.C�. 29607
� cA Q r L /
Container Type (P/S�
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Address
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B—HNO, E—HCL
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Project No.
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° 4
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Time Sample Description
Lab No. Date
COMMENTS:
C,6y:Q.=,,e
3
3
SAMPLER
%
Date/Time
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Date me
HAZARDS ASSOCIATED W1T}� SAMPLES
Relin (shed Y
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to me t%
q
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Date/Time
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do #
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Date/Time
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®
by (Sig
Date/Time
I
Receipt Total CL,_ mg/L Receipt pH
boo
Shipper No a ac4
�OZI 11 ��6a
Subsequent Analysis: _ (Check)
Date Resubmitted
Seal at'chd b Recvd. Intact b Seal at'chd b
Recvd. Intact b
Form Revised June 1994

JJN-93-99 THU 11:01 AM AQUA-TROL.INC. 704 882 3542 P.01
AQUA-TROL,INC.
RP SCHERER-CHELSEA PLANT
PH VALUES FOR THE EOLLOWING
DATE g PH VALUE
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J'JN-03-99 THU 11:02 AM AQUA—TROL.INC. 704 882 3542 P.02
CHELSEA WATER REMEDIATION
MONITORING REPORT FOR MONTH OF
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Surface
Discharge
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j'JN-03-99 THU 11:03 AM AQUA-TROL.INC. 704 882 3542 P.03
CHELSEA WATER REMEDIATION
MONITORING REPORT FOR WELLS
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* JUL!s09-99 FRI 11:28 AM AQUA—TROL.INC.
704 882 3542 P.01
DATE
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RP SCHERER-CHELSEA PLANT
PH VALUES FOR THE EOLLOWING
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AUG-03-99 TUE 12:40 PM AQUA—TROL,INC.
704 882 3542 P.01
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RP SCHERER-CHELSEA PLANT
PH VALUES FOR THE EOLLOWING
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AUG-03-99 TUE 12:41 PM AQUA—TROL.INC. 704 882 3542 P.02
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R.P. SCHERER/CHELSEA LABORATORIES FACILITY
MONROE, NORTH CAROLINA
GROUNDWATER CORRECTIVE ACTION
Month
May-97
Jun-97
Pounds of
VOCs
Recovered
from
Aquifer
1.14
I 5.98
Jul-97
5.81
Au -97
1.72
A r-98
4.85
Ma -98 ,
5.43
Jun-98
8.20
Jul-98 .
4.09
Au -98 ;
3.51
Se -98
2.68
Oct-98
3.15
Nov-981
2.57
Dec-98
4.05
Jan-99
2.03
Feb-99
2.57
Mar-99 .
2.60
A r-99
0.95
Ma -99
Jun-99
Jul-99
2.83
1.60
2.15
R.P. SCHERER/CHELSEA LABORATORIES FACILITY
MONROE, NORTH CAROLINA
111L"
May-97 Jul-97 Apr-98 Jun-98 Aug-98 Oct-98 Dec-98 Feb-99 Apr-99 Jun-99
Jun-97 Aug-97 May-98 Jul-98 Sep-98 Nov-98 Jan-99 Mar-99 May-99 Jul-99
MonthNear
gym-c-\clients\rpscherer\vocremov.wk4 08/19/99