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HomeMy WebLinkAboutNCG030056_Monitoring Report_22122020®i O Ljj LL _W W Q F— M CL �D O o � U J � J Q Q a. ^ LL 11. V O w 0 Q Q � L Uwcu 4) Cl)O LLI tli W a) Q Z CU � U WO _ 0 Z � O 2 F- .J Z Q 14cc U al L O r ov (f) O N p Rt (J C ❑ ❑ U U z z O Z O 0 Z U E O U) N 0 U a_ — Z N O U > tf (D U U C 0 U O O 0 LO N' LO co co 0 Z U � Z 4 C � U 73 O O = L.L U a. 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CD CD�- v v Q5 J C 0) Er N r r O O � O O a O U 00 :77- E ~ co ~ LO CY) CD o F •� CD a� cu V t U a coco N N C O E E r d� r m U �co O co L O 0- (U N O E }� 0 0 C 4— p L N fn O _L }� E CO C CD E cn O •— � O O +� i N C(6 C L N fn " O O v— � m C � O _O (� O O Q U N N .p E L �' N C: p L a) L (D Q� L G Q :3 O +� a) ; 4-- Q) Qi Q� O O O a) E Q cu 4- Q � � L •� E O (� O p U Y -O � L O_ U1 O 'D L O M L N O 0- O U L Q) 0 M C O O U \ U L O fl �. �-� E L 'O O Co cu >1 •� 0 ^w^, W 4— � J O c O U � ca � N O p O CL 70 0) .Y N - O O .- - �E 0)U U 2) m W 0 -0 co 0 in ryco � o Q N O U C J V N D NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DMR) Form for NCG030000 Metal Fabrication Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG031 0 10 15 16 Facility Name: Gilbarco inc Person Collecting Samples: John Burke Laboratory Name: Pace Facility County: Guilford 0 1 Laboratory Cert. No.: 12, 40, 633 Discharge during this period: ❑■ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions for any benchmark exceedances? ❑■ Yes ❑ No If so, which Tier (I, II, or III)? 1 D Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Parameter Outfall)01 Outfall02 Outfall03 Outfall Outfall Code N/A Receiving Stream Class 5 5 5 N/A Date Sample Collected MM/DD/YYYY 11/26/2020 11/26/2020 01/26/2020 46529 24-Hour Rainfall in inches 0.3 0.3 0.3 005S2 Non -Polar Oil & Grease in mg/L (15) <5.00 <5.00 <5.00 C0530 TSS in mg/L (100 or 50*) 136 8.4 17.7 00400 pH in standard units (6.0-9.0) 7.33 6.20 5.84 NCOIL New Motor/Hydraulic Oil Usage in gal/month 01119 Copper, total recoverable in mg/L 0.013 0.006 0.012 (0.010 FW, 0.005 SW) 01051 Lead, total recoverable in mg/L 0.005 <0.005 <0.005 (0.075 FW, 0.220 SW) 01094 Zinc, total recoverable in mg/ L (0.126 0.077 0.075 0.120 FW, 0.095 SW) 78141 Total Toxic Organics (TTO) in mg/L(1) SMP SMP SMP * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L. Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Permittee or Delegated Authorized Individual Date L O i .L. C 4- .E Q 0 N N N a E .Q N cu z N a ❑ ❑ � a„I z% O O Q O Ln F- s. ❑ai i-+ c� a cr L]❑ 3 5 O O a i o o ? 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U 0- U .� LO Ln � � ca Q � }' d• C CD E Q) CB +1 0 U U v O E `+ _ = o o+- a, � bn 0 N O } E O N 4- ,pp U QJ cn ' X c O U UO c: O O = a .D +� _ fB L 4- — v +E 4= O w O a N E Q) u bOA �O Y v _ +- W L w L _ o E m -O N +- = U a U C U tw N L 4- 4- QJ QJ a U OL U i' Q) O a — o -0 M U Z U a -&-- U -0 N U a U L i Ou a > O O N E L � N cn Q) m U o LnI N O > O a O O A O Q (O 4-0 r-I L a M N Q O E N _ O v O Q, L } +' 0 -0 s Z3LL U Z3 ap Q) U O E _ = c� = O L +-+ Off' cB -0 Q)O _ O a� C a a m O U= = bA c-I U � Qj L L a--+ C: O O QJ Q M = 4 U Q U O a t- Q Co t]A v - C O O C M U O ,- } U E m 4= N c (/7 In L C O v O 0 E = a QJ Q L L Q) to_O Q U 0-s � N) cn } C1lJ a — U Q — N .x : o O Q� - m cB Ln+� U' — OL 4-E D L QJ a +� a O t a O u C N " M 'cY ill w L u E 2 00 0 N c-1 c-I r-I N +-1 N `—° m Lr 4- � o N r -I r-I N O (V \ r-I m \ Ln O 00 r-I O N \ \ c-I c--I 1 c� 0 2 E v W/ L O O _ + _U L O () E Q) tO p �7-- + O 0 O O cn U Q) c X NO O O 4O Q . Ln `� • — co a) > O +� o L E _ O O c 41 Q) U — L n E Q' ro E L E N Q) C: p L i O Q L +-+ U C L U -a p p .N O N a U o Q N E �Q Q) Q) C- U) N 4- 4, + U +- O *� N O E N v oELO w +� O — U U L O U X Q) Q) C O U > U cn Q_ L Q) O E Q) O O- dA p + i O f0 U D O O aA 4 -, +- U U _O C - U }' c O O a C L ro O d — Q) ra U Q a cv E � Q) 0 +- L O on O +�Q) �O 3 > Q) Q LO v > E n3 ..Q O O p aA cn U Q O O N C . -, O °' L O a) u U a - L — U E L O O O N c� Ln n3 a C- a� E ++ Q) ° c L = cn L Q) +1 o i E o O Q O bn Q. O c E o .0 c m E Q) Q) cn Q) E o Q ptw O a fB tw cn L.- U 4-1v U O O U O O E a) > O LM i +' cn Q c� C U)O O M c M O } C o N U c CU O Q) m v> i n3 O O O ucx Ln 4-1 — > C c� > } Q) LnO L > Uo m ° O Ln - L, UL cB E a m 0 a- rZ O (B +�U_ U L +� QC) Q) E -0 4 Q) x 4 N 4— 4Q O O o� a E ' a L Ln IV � a) U o O O X C) X Qa 4- — Q) v •O � � M O z U o a X X Ln Ln m ~ n W E E Q O _O 44 � O QJ Q) U ��, co i •V O O CD Q) i L L O O ° �, >. a) o O � N O O O � z Qj QJ }i � -Q w m E E •%. 4- a) O O � a• + •u U U 0 O Q � Q o m L cu Q) O b\A U ++ o o. 0 +O+ cn C a) +, = • _ 44 (N E L 0 v bA i U � t o �. > � m +� 44 L O i E O fB z — — Z a O v�Ln ai s Z ❑ J Cl) E G) cn to O CL a L. m o ° O o ~ O Ln +, 0 FO— M \ U O J O >' = n m O C) 0 � o O L z a a) O = O O O O U U 'S z M v s! _ C O E m N N Ln O t �r N au U L 0 U a cu \ O' O ( N m o z m : O fu E r a m a Oo O N c--I r-I 4 i (om) Ln Q) 4.1 L i Ln i 2 m a o It N � N a v a, H Q) H O O Q Q) M i Q) O N� O) 1= H L 4Q _v O- E h 0 i` a t U v O H H O) U Qj c Q) ::I- O Q N Q � m \ a Ln Zn o a 00 {� CD L N O a v a � o Qj O L z °p- 00 c, o .L N •= Gj OO L 4-, O Q1 _0 .i a-1 c -p C E Q) N N O Q7 (A_0a U Z O L co m w (n N > o N a _E N cD U mcB M N p OLU a� N d 3 4Q a O U N � O O ._ L WJ LL LO -0 � v O F- O.. 41 Ov O- - LLU LU O L c m O m E Cn Z y .� O bA 0 (AO o Ln 0 'o Z z o •Z7i Q O co N _ W c/ W LLI p •+'� L L 4- O •� O ` t C N •U - \\ CD a Z G] O U -0 > O O LL N E ca w O +J I w w h O O N o = O -0 m d J � C Li-O O' D Z 3 Q N w w C w Z N Lu w Ln w p Lu i p W 0 p 0- N a w } a� } L m X r`. \ OC Ln L L Z F- Lil U Y 4) O O Q O a� 4- aLL Cw C a Lj- a NJ E 4LU •� O .0 Z U C) In C z Z i= m� tw O m Z Q o w cc Elf W 0 c w O O Z - kn H Lf) a w � O C7 w O 0 cD Q a� v 'i• w 3 �- o H a on \ 1 � U 0 2 0 = 0 bO L w Z U w p ++ L Z 4- fl0 p o- 4-4- 41 0Q�Uza O o u�Q� \�� o CIA z w z U a Lai O U U F- t +r rn o Z X _ � � U w i � � N an 4- O O N N O m Y w O O H ) L �' N a% LLJ U A v 00 I- w U}} Z a= ro o N Q> y 0 a a Lu sclm � � oUo Ll 4-WM Q. Z Z U cLijvi vi LL a Lu LL.ru •� p > v 4� a w X oC a m w Lu } O •L p U N O c/f 0 +�+ p a N H LL Q =? O '� Z i N \ L a z a o g"_4- Q� v, o cr- (� p oo� vvi ] u NO N c °oar° �- � C ao �n aceAnalytical www.pacelabs.com December 08, 2020 John Burke Gilbarco 7300 West Friendly Ave. Greensboro, NC 27410 RE: Project: Stormwater Sampler Pace Project No.: 92508405 Dear John Burke: Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, AMw_y4� Stephanie Knott stephanie.knott@pacelabs.com 336-996-2841 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 IaceAnalytical www.pacelabs.com Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalytical www.pacelabs.com Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 SAMPLE SUMMARY Project: Stormwater Sampler Pace Project No.: 92508405 Lab ID Sample ID Matrix Date Collected Date Received 92508405001 001 Outlet Water 11/26/20 06:10 11/30/20 11:18 92508405002 002 Outlet Water 11/26/20 06:00 11/30/20 11:18 92508405003 003 Outlet Water 11/26/20 05:50 11/30/20 11:18 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 aceAnalytical www.pacelabs.com Project: Stormwater Sampler Pace Project No.: 92508405 Lab ID Sample ID 92508405001 001 Outlet 92508405002 002 Outlet 92508405003 003 Outlet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-E = Pace Analytical Services - Eden SAMPLE ANALYTE COUNT Method SM 2540D-2011 EPA 1664B EPA 200.7 Rev 4.4 1994 SM 2540D-2011 EPA 1664B EPA 200.7 Rev 4.4 1994 SM 2540D-2011 EPA 1664B EPA 200.7 Rev 4.4 1994 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Analytes Analysts Reported MLS1 1 CJM 1 IDS 3 MLS1 1 CJM 1 IDS 3 MLS1 1 CJM 1 DS 3 Page 4 of 13 acice Analyfical www.pacelabs.com ANALYTICAL RESULTS Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Sample: 001 Outlet Parameters Lab ID: 92508405001 Collected: 11/26/20 06:10 Results Units Report Limit DF Received: 11/30/20 11:18 Matrix: Water Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 136 mg/L 5.3 1 12/01/20 08:27 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 12/08/20 08:35 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 0.013 mg/L 0,0050 1 12/05/20 01:37 12/06/20 17:18 7440-50-8 Lead 0.0050 mg/L 0.0050 1 12/05/20 01:37 12/06/20 17:18 7439-92-1 Zinc 0.077 mg/L 0.010 1 12/05/20 01:37 12/06/20 17:18 7440-66-6 Date: 12/08/2020 03:41 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 13 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Sample: 002 Outlet Lab ID: 92508405002 Collected: 11/26/20 06:00 Received: 11/30/20 11:18 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 8.4 mg/L 3.2 1 12/01/20 08:27 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 12/08/20 08:35 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 0.0058 mg/L 0.0050 1 12/05/20 01:37 12/06/20 17:21 7440-50-8 Lead ND mg/L 0.0050 1 12/05/20 01:37 12/06/20 17:21 7439-92-1 Zinc 0.075 mg/L 0.010 1 12/05/20 01:37 12/06/20 17:21 7440-66-6 Date: 12/08/2020 03:41 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 13 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Sample: 003 Outlet Lab ID: 92508405003 Collected: 11/26/20 05:50 Received: 11/30/20 11:18 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Eden Total Suspended Solids 17.7 mg/L 3.4 1 12/01/20 08:27 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 5.0 1 12/08/20 08:35 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper 0.012 mg/L 0.0050 1 12/05/20 01:37 12/06/20 17:37 7440-50-8 Lead ND mg/L 0.0050 1 12/05/20 01:37 12/06/20 17:37 7439-92-1 Zinc 0.12 mg/L 0.010 1 12/05/20 01:37 12/06/20 17:37 7440-66-6 Date: 12/08/2020 03:41 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 QC Batch: 583485 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92508405001, 92508405002, 92508405003 METHOD BLANK: 3084976 Matrix: Water Associated Lab Samples: 92508405001, 92508405002, 92508405003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 12/01/20 08:26 LABORATORY CONTROL SAMPLE: 3084977 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 242 97 90-110 SAMPLE DUPLICATE: 3085030 92508454001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 381 411 8 25 SAMPLE DUPLICATE: 3085031 92508461001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 405 370 9 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 QC Batch: 585226 Analysis Method: QC Batch Method: EPA 1664B Analysis Description: Laboratory: Associated Lab Samples: 92508405001, 92508405002, 92508405003 EPA 1664B 1664 SGT-HEM, TPH Pace Analytical Services - Charlotte LABORATORY CONTROL SAMPLE: 3093376 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 13.5 68 64-132 MATRIX SPIKE SAMPLE: 3093377 92509161001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 ND 2 64-132 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Stormwater Sampler Pace Project No.: 92508405 Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 QC Batch: 584771 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92508405001, 92508405002, 92508405003 METHOD BLANK: 3091372 Matrix: Water Associated Lab Samples: 92508405001, 92508405002, 92508405003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 12/06/2016:35 Lead mg/L ND 0.0050 12/06/2016:35 Zinc mg/L ND 0.010 12/06/2016:35 LABORATORY CONTROL SAMPLE: 3091373 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L 0.25 0.26 103 85-115 Lead mg/L 0.25 0.25 101 85-115 Zinc mg/L 0.25 0.25 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3091374 3091375 MS MSD 92507513001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Copper mg/L 212 ug/L 0.25 0.25 0.48 0.48 109 109 70-130 0 20 Lead mg/L ND 0.25 0.25 0.26 0.26 104 104 70-130 0 20 Zinc mg/L 61.0 ug/L 0.25 0.25 0.33 0.33 109 108 70-130 1 20 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3091376 MS 92508491001 Spike Parameter Units Result Conc. Copper mg/L 0.014 0.25 Lead mg/L 0.0052 0.25 Zinc mg/L 0.038 0.25 3091377 MSD Spike MS MSD MS MSD % Rec Max Conc. Result Result % Rec % Rec Limits RPD RPD Qual 0.25 0.29 0.28 109 108 70-130 1 20 0.25 0.27 0.27 105 105 70-130 0 20 0.25 0.31 0.31 107 107 70-130 0 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 aceAnalytical www.pacclabs.com QUALIFIERS Project: Stormwater Sampler Pace Project No.: 92508405 DEFINITIONS Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/08/2020 03:41 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 13 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 106 Short St. Kernersville, NC 27284 336-996-2841 Project: Pace Project No.: Stormwater Sampler 92508405 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92508405001 001 Outlet SM 2540D-2011 583485 92508405002 002 Outlet SM 2540D-2011 583485 92508405003 003 Outlet SM 2540D-2011 583485 92508405001 001 Outlet EPA 1664B 585226 92508405002 002 Outlet EPA 1664B 585226 92508405003 003 Outlet EPA 1664B 585226 92508405001 001 Outlet EPA 200.7 Rev 4.4 1994 584771 EPA 200.7 Rev 4.4 1994 584807 92508405002 002 Outlet EPA 200.7 Rev 4.4 1994 584771 EPA 200.7 Rev 4.4 1994 584807 92508405003 003 Outlet EPA 200.7 Rev 4.4 1994 584771 EPA 200.7 Rev 4.4 1994 584807 Date: 12/08/2020 03:41 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 13 ` m m r_ z O n cn m 0 0 c _mz _ 03 --u cnm -zj D n �- cn --i rs m -1 D > z < m m O C --I `� m -i p m cn — 1 m m .. I o o �. R o o �. - D 0 O co /m m 0 C,} c m t. D rn Dr i '� f �� o ('m� r� O Dz m C D r' m rn NO. OF CONTAINERS �/ verb n `DSO has �S �/0 pes�J e y 7� p 0 /TQ�J c< 74 c 0 71 e -.� -- 7Z OO � Q're Nr�,Pa C 74 �O /iLjef °J dseJ efQJ R1 /S `S/e G/C� ydr tiSQ ySQ � n/e � A qti/ aye a e O ss D c /o%o�tidQyJ Q m rn w `. ->m F: ,a c� Co cn i z N cn C/) c. �D s� �(2) rn CD l01 CL) rn� CD o CD o o �- CT) CD .• 9 M � m �_ Z cn ct • Ocn c Q t ® W a CA v• O C� X m n O v Page 13 of 13 GVR-226 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ a/3/ Lx t) / S--/ 6/ Facility Name: t County: c Coun �u ; � ��� � Phone No. Inspector: �'� i 4� Date of Inspection: k L Time of Inspection: Total Event Precipitation (inches): 0,30 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: of Permittee or Designee) 1. Outfall Description: Outfall No. 0 b Structure (pipe, ditch, etc.): D A--Z�4- Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): �j o,^/f 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: �v. 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. 8. 9. 10. 1 2 3°` 4 5 Is there any foam in the stormwater discharge? o Yes No. Is there an oil sheen in the stormwater discharge? 0Yes No. Is there evidence of erosion or deposition at the outfall? Yes O No. Other Obvious Indicators of Stormwater Pollution: List and describe ► �/i- (-,) .1-1 c i-�- U. '&o Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 GVR-226 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/enel-gy-mineral-land-resources/ np des-storinwater-gp s Permit No.: N/C/ or Certificate of Coverage No.: N/C/G/ 6131 Facility Name: 3 County: Gv L Phone No. 3 3 L S"Lj 7— S�'O a o Inspector: 07, VKJ Date of Inspection: Time of Inspection: (3 Total Event Precipitation (inches): All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. ......................................................................................................................................................................................................................................................................................................................................................................................................_.......................................................................... By tkjs signatu ce�t� y-that4hi&iz is accurate and complete to the best of my knowledge: (Signatilre of Permittee or Designee) 1. Outfall Description: Outfall No. 0 0 '�— Structure (pipe, ditch, etc.): kl� Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: �,� I—iy 14-Jy�-� S i 1�► L t�; S , LVfi- Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: L-T 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): �✓`��-- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 / 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: ;D 2 3 4 5 — 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: j 1 2 3 4 5 7. Is there any foam in the stormwater discharge? o Yes No. S. Is there an oil sheen in the stormwater discharge? OYes No. 9. Is there evidence of erosion or deposition at the outfall? U Yes XNo. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 . GVR-226 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.ne.gov/about/divisions/enel-gy-mineral-land-resources/ np des-stormwater-gp s Permit No.: N/C/ or Certificate of Coverage No.: N/C/G/ 61 / 6/ 6 / 6 / 6/ Facility Name: County: Phone No. Inspector: �i tfZ Date of Inspection: Time of Inspection: Fs L) Total Event Precipitation (inches): 0-,,3 0 All permits require qualitative monitoring to be perfonned during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. ............................................ _............................................................................................................................................. I ....................................... _... By this Signature, I certify that this report is accurate and complete to the best of my knowledge: of Permittee or Designee) 1. 'Outfall Description: Outfall No. 0 0 . Structure (pipe, ditch, etc.): � � G-��— Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: -TA,*C AL— 9AA1 C, % Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Li-16vr 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): N��z- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: /1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 2 3 4 5 7. 8. 9. Is there any foam in the stormwater discharge? O Yes No. a Is there an oil sheen in the stormwater discharge? QYes No. Is there evidence of erosion or deposition at the outfall? o Yes A No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 GVR-226 N---. Enidr-ommenta! Quality. Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://deq.ne.gov/about/divisions/energy-mineral-land-resources/ np des-storinwater-gp s Permit No.: N/C/ or Certificate of Coverage No.: N/C/G/ (3/3/ L�/ t� / 657% b/ Facility Name: r lbe-cam; <— County: U Phone No. 3 3 L �cl 7 S-0 i; Inspector: 07, Date of Inspection: Time of Inspection: `. Total Event Precipitation (inches): 0-10 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. ........................................................ ................................................................................................................................................................................................................................................................................................. .............................................. .... .................. ............. _...._ . By this sig-lature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Vermittee or Designee) 1. Out 11 Description: Outfall No. 0 , Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors:�� 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): N v,Ni�'w= 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: bl", 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: LI) 2 3 4 5 7. 8. 9. 10. Is there any foam in the stormwater discharge? o Yes Is there an oil sheen in the stormwater discharge? oYes Is there evidence of erosion or deposition at the outfall? o Yes Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 GVR-226 fntlironmental Quality. Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.ne.gov/about/divisions/energy-mineral-land-resources/ npdes -stortnwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 613 / of C5 / S / 6/ Facility Name: G r \ bc,, -Cz 3 County: Gu m Phone No. 3 3 LS"I 7 !� b 6 0 Inspector: VVj �.61 !& i (p` Date of Inspection: t k Time of Inspection:, Total Event Precipitation (inches): 0ti,3 D All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By thisAgaatur-@,—I-ee4i-fy-thaLthilreSort is accurate and complete to the best of my knowledge: Permittee or Designee) 1. Outfall Description: Outfall No. 00 Structure (pipe, ditch, etc.): P-Z-Vr- k, k-- Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C-1.- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: �- 6 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: d/.,. 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? 0 Yes S. Is there an oil sheen in the stormwater discharge? QYes No. No. 9. Is there evidence of erosion or deposition at the outfall? U Yes No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018 GVR-226 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https:Hdeq.ne.gov/about/divisions/energy-mineral-land-resources/ npdes-stormwater-gps Permit No.: N/C/ / / / / / / / or Certificate of Coverage No.: N/C/G/ 6/3/ 6/.45 / c- / b/ Facility Name: ic.,r- County: Phone No. 3 3 L ' S-cj % SA) i,' o Inspector: wo &�Aljtip. Date of Inspection: E � 1. � L I Time of Inspection: 6 r -3 Z) Total Event Precipitation (inches): All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. .............................................................................................................................................................................................. .. ._. By this signature, I certify that this report is accurate and complete to the best of my knowledge: of Permittee or Designee 1.'—'Outfall Description: Outfall No. 0 0 -( Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 06/01/2018 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (2-�) 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 02' 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (2) 3 4 5 7. 8. 9. Is there any foam in the stormwater discharge? O Yes No. Is there an oil sheen in the stormwater discharge? QYes No. Is there evidence of erosion or deposition at the outfall? Q Yes No. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 06/01/2018