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HomeMy WebLinkAboutWI0400106_REMEDIAL CONSTRUCTION COMPLETION REPORT_20110824ameO August 24, 2011 Mr. David Goodrich, Hydrogeologist Aquifer Protection Section — UIC Program NCDENR — Division of Water Quality 1636 Mail Service Center Raleigh, North Carolina 27699-1636 Subject: Remedial Construction Completion Report Former CMI Waste Water Treatment Plant Elkin, North Carolina Site ID NONCD 0001092 MACTEC Project 6228-08-4691 Dear Mr. Goodrich: In accordance with the requirements outlined in Injection Permit W10400106 issued to CMI Industries on April 7, 2011, AMEC Environment and Infrastructure (E&I) is please to submit this Remedial Construction Completion Report for the subject site. This report presents the "as -built" plans and specifications, a summary of major variances from the final design plans and a summary of problems that were encountered. Please note that a copy of this report was previously submitted to the Inactive Hazardous Sites Branch of the North Carolina Department of Environment and Natural Resources under separate cover on July 20, 2011. If you have questions concerning this report, please contact the undersigned at (704) 357-8600. Sincerely, MACTEC ENGIN AND CONSULTING, INC. Mark P. Fiiardi, P.G. ag&lark,/P .G. Senior Geologist Principal Geologist cc: NCDENR Aquifer Protection Section, WSRO Enclosures Correspondence: AMEC E&I, Inc. 2801 Yorkmont Road, Suite 100 www,amec.com Charlotte, North Carolina 28208 Tel 704-357-8600 Fax 704-357-8638 OMACTEC engineering and constructing a better tomorrow July 20, 2011 Mr. Kim Caulk, P.G. Inactive Hazardous Sites Branch Superfund Section — Division of Waste Management North Carolina Department of Environment and Natural Resources 401 Oberlin Road, Suite 150 Raleigh, North Carolina 27699 Subject: Remedial Construction Completion Report Former CMI Waste Water Treatment Pint NONCD 0001092 Elkin, North Carolina Surry County MACTEC Project 6228-084691 Dear Mr. Caulk: In accordance with the Registered Environmental Consultant -Directed Assessment and Remediation pursuant to N.C.G.S. 130A-310.9(c) and 15A NCAC 13C .0306(a), MACTEC Engineering and Consulting, Inc. (MACTEC) is pleased to submit this Remedial Construction Completion Report for the subject site. This Report presents the "as -built" plans and specifications, a summary of major variances from the final design plans and a summary of problems that were encountered. Please let us know if you have any questions or would like to discuss the project in greater detail. Sincerely, �ONSULTTNG, INC. Ze'NI'lar-rk. L.G., R M Principal Geologist NC License # 1748 MACTEC Engineering and Consulting, Inc. 2801 York mont Road, Suite 100 • Charlotte, NC 28208 • Phone: 704-357.8600 RECEIVED I DENR � AOUIFr=1?-R17t1Tr:r"TIr .�t ?c�ri1 www. mactec.com MACTEC Engineering and Consulting MACTEC �801 nt Read. Suitta 100 CHARLOTTE, NORTH CARDLINA 28208 Phonc:(704)357-8600 Fax:(7D4)357-8638 LETTER OF TRANSMITTAL TO: Mr. Kim Caulk, P.G. DATE: July 22, 2011 Inactive Hazardous Sites Branch PROJECT NO.: 6228-0"91 NCDENR PROJ. NAME: CMI Waste Water Treatment Plant 40I Oberlin Road, Suite 150 SUBJECT: Construction Completion Report Raleigh North Carolina 27699 WE TRANSMIT TO YOU: HEREWITH UNDER SEPARATE COVER SUBJECT: ❑DRAWINGS ❑ SPECIFICATIONS ❑CALCULATIONS ❑REPORT ❑COST ESTIMATE ®AS NOTED ACTION: ®FOR YOUR INFORMATION ❑FOR YOUR COMMENT OR APPROVAL ❑RETURNED FOR CORRECTION: RESUBMIT ❑APPROVED AS NOTED ❑AS REQUESTED SENT BY: ❑MAIL ❑CERTIFIED MAIL ❑EXPRESS (Fedex) []COURIER ❑HAND DELIVERED ❑FACSIMILE: pages. (includiniz transmittal sheet) COPIES DATE DESCRIPTION 1 7-20-1 I Paper copy of Final Remedial Construction Completion Report 1 7-20-11 CD of Final Remedial Construction Completion Report REMARKS: CC: Mr. Jim Ovendea By: File (1) L.G., Direct Phone: 704-357-5630 CONFIDENTIALITY NOTICE- This =ssage is intmdcd only for the use of the individual or entity to which it is addressed, and may contain information that is privileged, confidential, and exempt front disclosure under applicable law- if the reader orthis message is not the intended recipient, or the employee or agent responsible ror delivering the message to the intended recipient, you are hereby notified that any dissemination, distribution, or copying or this communication is strictly prohibited. lryou have received this communication in error, please notify us immediately by telephone and m am the original message to us at the above address via the U , S . Postal Service. Thank you, If trattsmission is not nreived in goal order, please cull Andy Clark at (704) 357-5622 gyp AOU1FP ,"CTiON AUG 25 2011 REC PROGRAM DOCUMENT C'FRTIFICATION FORM - PAGE I OF 2 1T1S13 SITE NAME CMI WWTP DATE & NAME OF DOCUMENT Ju)y 20, 2011 Remedial Construction Completion Report TYPE OF SUBMITTAL [cimk aii ❑rai apply]: Report, Workplan, Work Phase Comp, Statement, Schedule Change REMEDIATING PANTY DOCUMENT CERTIFICATION STATEMENT [.0306(B)(2)) "I certify under penalty of law that I have personally examined and am familiar with the information contained in this submittal, including any and all documents accompauying this certification, and that, based on my ingtuiry of those individuals immediately responsible for obtaining the information, the material and information contained herein is, to the best of my knowledge and belief, true, accurate and complete. i am aware that there are significant penalties for willfully submitting false, inaccurate or incomplete information." Naim of Rmncdiating Party igna ire of Rrmediat S Party _l -- IIase 3145 pr^ NOTARIZATION ���ner 3�u1 Cowry 11 ,ice t - Q S , a Notary Public of said County and State, do hereby certify that ]iiM4-1� OK�eAvkd-. did personally appear and sign before me d4 s day, produced proper identification in the form of - &wye --� p,u_, was duly Sworn or affirmed, and declared that, he or she is the duly authorized environmental consultant of the remediating party of -'the property referenced above and that, to the best of his or her knowledge and belief, after thorough investigation, the information contained in the above certifications is true and accurate, and he or she then signed these Certifications in my presence. WITNESS my hand and official seal this day of _. (OPFICIAt SPAL) pl6ry r �c - ure] My commission expires: 13� ;[ , ao 1q Document Certifrcution Form No. DC -1 (7evised 3I11) -., ��-j11 REC PROGRAM DOCUMENT CERTIFICATION FORM - PAGE 2 OF 2 IHSB SITE NAME CMI WWfP DATE & NAME OF DOCUMENT July 20, H11 Remedial Construction Completion_ Repoli TYPE OF SUBMITTAL (circle all that apply): Report, Workplan, Work Phase Comp. Statement, Schedule Change REGISTERED SITE MANAGER CERTIFICATION OF SIGNATURES As the Registered Environmental Consultant for the Site for which this filing is made, I certify that the signatures included herewith are genuine and authentic original handwritten signatures and/or true, accurate, and complete copies of the genuine and authentic original handwritten signatures of the persons who purport to sign for this filing. I further certify that I have collected through reliable means the originals and/or copies of said signatures from the persons authorized to sign for this filing who, in fact, signed the originals thereof. Those persons and I understand and agree that any copies of signatures have the same legally binding effect as original handwritten signatures, and I certify that any person for whom I am submitting a copy of their signature has provided me with their express consent to submit said copy. Additionally, I certify that I am authorized to attest to the genuineness and authenticity of the signatures, both originals and any topics, being submitted herewith and that by signing below, I do in fact attest to the genuineness and authenticity of all the signatures, both originals and copies, being submitted for this filing. Name of Regisived Site Mana er Signatu Registered Site Manager -ityt1 II Date REGISTERED SITE MANAGER DOCUMENT CERTIFICATION STATEMENT (.0306(b)(1)) "I certify under penalty of Jaw that I am personally familiar with the information contained in this submittal, including any and all supporting documents accompanying this certification, and that the material and information contained herein is, to the best of my knowledge and belief, true, accurate and complete and complies with the Inactive Hazardous Sites Response Act G.S. 130A- 310, et seq, and the remedial action program Rules 15A NCAC 13C .0340. I am aware that there are significant penalties for willfully submitting false, inaccurate or incomplete information." Name of Registered Site Manager _ '717,t Ott Signature of Registered Site Manager LJatr t{ Z'rp w+ NOTARIZATIONCmwkp-1 ter State) COUNTY I, . a Notary Public of said County and State, do hereby certify that did personally appear and sign before me this day, produced proper identification in the form of CWK �L,(&rye, was duly sworn or affirmed, and declared that, he or she is the duly authorized environmental consultant of the remediating party of the property referenced above and tbat, to the best of his or her knowledge and belief, after thorough investigation, the information contained in the above certifications is true and accurate, and he or she then signed thYcse Certifications in my presence. WITNESS my ha d and official seal this �l day of r (ICIAL SEAL) ary ubli { igna } My commission expires: 1L Howy Pubk Mrido"L q CW" Document Cerfification Form No. DC - LT CWd" s (Revised 3111) AUG 20- 1111j REC PROGRAM WORK PHASE COMPLETION FORM — PAGE ❑OF ❑ CONSTRUCTION COMPLETION CERTIFICATION 15A NCAC 13C.0306(b)(5)(D) Media (check all that apply): ❑ All Media ❑ Soil ❑ Ground water ❑ Surface water ❑Sediment Site Name CMI WVYfP Street Address Fabric Lane County Surry Site ID No. NCNCD 0001092 Elkin North Carolina The construction of the final remedy, which is the subject of this certification has, to the best of my knowledge, been completed in compliance with the Inactive Hazardous Sites Response Act G.S. 130A-310, et seq. and the remedial action program Rules 15A NCAC 13C .0300, and MACTEC Engineering and Consulting, Inc. LUZ Nataei is in compliance with Rules .0305(b)(2) and .0305(h)(3), of this section. I am aware that there are significant penalties for willfully submitting false, inaccurate or incomplete information. I(T-1 /fit 'gTrp►-+.• R Signature Date A:lN a &-e A rl�. RSM Name MACTEC Engineering and Consulting, Inc. 4021 Stirrup Creek Drive REC Name Mailing Address 00110 Durham, NC, 27703 REC No, City, State, ZIP NOTARIZATION Nl GW[W, (Enter State) �-COUNTY I, Kytqm W J. K", a Notary Public of said County and State, do hereby certify that did tt personally appear and sign before me this day, produced proper identification in the forth of 1CJr5 Ll(�PM�iPz`, was duly sworn or affirmed, and declared that, he or she is the duly authorized environmental consultant of the remediating party of the property referenced above and that, to the best of his or her knowledge and belief, after thorough investigation, the information contained in the above certification is true and accwate, and he or she then signed this Certification in my presence. WTTNESS my hand and official seal this day of tk p� o ry Fu • (signa[um) My commission expires: — Work Phase Completion Form No. WPC -- V (Revised 3111) (OFFICIAL SEAL) 11111"t.*4 Nftyw* tint pwirs RL-HivI_D I !!s I t VVQ AQUiTPP ;r�(N i ION AUG 25 2011 NCDENR — Remedial Cominiciion Comple[ion Report July 20 2011 MA CTEC Projeci 6628-08-4691 NONCD0001092 REMEDIAL CONSTRUCTION COMPLETION REPORT FORMER CMI WASTE WATER TREATMENT PLANT The Former CMI Waste Water Treatment Plant (W W 1P) is located on Fabric Lane in Elkin, North Carolina at a latitude / longitude of 36.245225" 1-80.842024' (Figure 1). The parcel is located within a larger textile manufacturing complex where historical disposal activities resulted in environmental impacts to soil and groundwater beneath the Site. The Site Plan with monitoring well locations is provided on Figure 2. Greater detail regarding historical operations and associated environmental impacts is provided in the Remedial Investigation Report dated March 9, 2007 prepared by others. This Remedial Construction Completion Report (Report) reviews the Remedial Action Plan development for groundwater and presents the remedial action implementation documentation. In so doing, the Report also presents the "as -built" plans and specifications, a summary of major variances from the final design plans and a summary of problems that were encountered. 1.0 REMEDIAL ACTION PLAN DEVELOPMENT Based on a review of soil, groundwater, and surface water quality data collected by others at the former CM1 WWTP, MACTEC Engineering and Consulting, Inc. (MACTEC) submitted a Remedial Action Plan (RAP), in accordance with the requirements of the North Carolina Department of Environment and Natural Resources (NCDENR) Registered Environmental Consultant (REC) Program, on January 14, 2009. As requested, a draft copy of the RAP was submitted to the NCDENR REC Program Director for review and approval prior to finalizing the document and providing public notice. Subsequent to public comments, MACTEC submitted a Response to Comments and Proposed Remedial Action Plan Completion Certification to NCDENR in correspondence dated May 8, 2009. The objective of the RAP was to cost-effectively reduce the concentrations of select volatile organic compounds (VOCs) at the site and promote longer term natural attenuation to meet established Remedial Goals; i.e., the NCDENR Groundwater Quality Standards as defined in 15A NCAC 03L.0202 (2L Standards). MACTEC conducted additional activities in support of the RAP, including test pit excavation and groundwater sampling, between June and August 2009. MACTEC evaluated the results and worked with our subcontractor to develop a cost-effective injection program to promote natural degradation of the chlorinated VOCs (CVOCs) identified in groundwater as described in the RAP. The results of these activities were summarized in a Remedial Action Pre -Construction Report (PCR) prepared by MACTEC and dated May 11, 2010. The PCR also presented a final engineering design for the Site that included injection of electron donor material (Regenesis' 3DMe) into six existing and 10 proposed RECavED / D NR i On I of 7 AQUIFP Ppnrr NCDENR - Remedial Cnnstnictlnn Conipletian Report July 20, 2011 Mrt CTEC Project 6628-08-4691 NONCDOON092 monitoring/injection wells screened across the shallow bedrock groundwater zone (approximately 25 to 85 feet below ground surface (bgs)). Between June and September 2010, MACTEC conducted a pilot test at the Site that included installation and yield testing of three of the 10 proposed injection wells. No significant fractures were encountered between the base of the surficial casing (set at 25 to 26 feet bgs) and the total depth of each well (approximately 120 feet bgs) during installation of the three injection wells. Subsequent well yield testing conducted in September 2010 indicated that while the injection wells produce water, they were not viable for injection, as water pumped into the packered intervals under pressure was unable to significantly penetrate into bedrock. To address this problem with injecting into bedrock, the injection program was modified to include in -situ chemical injection into the impacted shallow bedrock and saturated overburden zones at three areas of the Site identified as Areas "A", "B", and "C" on Figure 3. This modification was necessary to meet the RAP objective of cost-effectively reducing constituent concentrations while promoting longer term natural degradation of CVOCs in groundwater. Bedrock injection was proposed utilizing six existing monitoring wells and two proposed new injection wells. Injection into saturated overburden was proposed via approximately 150 direct -push temporary injection points covering an approximate area of 52,000 square feet. The modified injection plan was discussed with the NCDENR REC Program Director and summarized in the Remedial Action Plan — Addendum #2 prepared by MACTEC and dated January 3, 2011. Implementation of the modified injection plan and associated deviations are discussed in the following sections, 2.0 REMEDIAL ACTION IMPLEMENTATION A Modified Underground Injection Control (UIC) permit application was submitted to the NCDENR on January 26, 2011. Subsequent to approval of the Modified UIC permit application in correspondence dated April 7, 2011 (Appendix A), MACTEC commenced remedial action (RA) activities at the Site on April 15, 2011. 2.1 Pre -Injection Activities 2.2.1 Well Installation Between April 15 and 20, 2011, MACTEC installed the two proposed new injection wells (IW-12+A and IW-14f) and four sentinel monitoring wells (EBMW-29 through EBMW-32), MACTEC installed the 2 of 7 NCDENR — Remedial Construction Campletfon Report July 20. 2011 MACTEC Project 6628-08--4691 NONCDMI092 four sentinel monitoring wells to satisfy a condition of approval of the Modified UIC Permit. The previously installed pilot injection wells were abandoned during this field effort, as well. The purpose of the sentinel wells was to monitor potential injectate discharge and/or potential "flushing" of contaminated groundwater into the Yadkin River. Injection wells IW-12+A and IW-14+ were installed to approximately 40 feet bgs. Because the depths to competent bedrock were deeper in these locations than previously encountered (i.e., 28-38 feet bgs versus approximately 20 feet bgs), the wells were installed to 40 feet bgs to target the planned treatment zone of approximately 25-40 feet bgs instead of extending deeper into rock as originally proposed. Monitoring wells EBMW-29 through EBMW-32 were installed to the top of bedrock at depths ranging from 18 to 25 feet bgs. The locations of the newly installed injection and monitoring wells are shown on Figure 2. A summary of well construction details is presented in Table 1. Well construction/abandonment records for the wells installed and/or abandoned during the current remedial activities are included as Appendix B. 2.2.2 Well Sampling As a condition of approval of the Modified UIC permit, the NCDENR required sampling and analysis of metals in wells EBMW-10 and EBMW-18 prior to commencement of injection activities. Subsequent to installation of the new injection wells and sentinel wells discussed above, MACTEC sampled EBMW-10 and EBMW-18 on April 18, 2011. Although not required by the Modified UIC Permit, MACTEC also collected groundwater samples from wells EBMW-29 through EBMW-32 on May 5, 2011 to provide baseline data for comparison of pre- and post -injection groundwater quality in the sentinel wells. In accordance with the Modified UIC Permit, laboratory analyses were performed on the samples collected from EBMW-10 and EBMW-18 for the eight Resource Conservation and Recovery Act (RCRA) metals using United States Environmental Protection Agency (EPA) Methods 5010 and 7470. Laboratory analyses were performed on the samples collected from EBMW-29 through EBMW-32 for volatile organic compounds (VCCs) using EPA Method 8260. Concentrations of barium, chromium and silver were detected in the samples obtained from wells EBMW-10 and EBMW-18. However, only the concentration of chromium at 10.5 micrograms per liter (ug/L) reported in well EBMW-10 exceeded the 2L Standard of 10 ug/L. Chromium was not previously detected in a June 2009 groundwater sample from well EBMW-10. The chromium concentration will continue to be monitored during future sampling events in accordance with the post -injection activities described below. Concentrations of 1,1-dichlomethene, l,l-dichloroethane, 1,1,1-trichioroethane, tetrachloroethene, trichloroethene and vinyl chloride that exceeded the 2L Standards were reported in each of the samples collected from wells EBMW-29 through EBMW-32. A summary of laboratory analyses of the groundwater samples collected from the wells between April I8 and May 5, 2011 is 3 of 7 NCDENR — Remedial Construction Completion Report MAC'TEC P►nject 6628-084691 J211y 20, 2011 NONCD0001092 presented in Table 2. Groundwater sampling data sheets are included as Appendix C. A copy of the laboratory report is included as Appendix D. 2.2.3 Field Parameter Monitoring On May 16, 2011, MACTEC recorded depth to groundwater measurements and field parameter readings of temperature, pH, specific conductance, turbidity, dissolved oxygen, and oxidation reduction potential from select existing monitoring wells within 24 hours of the commencement of injection activities. The purpose of the field measurements was to provide baseline data at these locations to complement previous baseline data collected at the Site that was presented in the PCR. The baseline data will be used for comparing proposed post -injection readings to gauge the effectiveness of the injection event. A summary of depth to water measurements and field parameter readings obtained on May 16, 2011 is presented in Table 3. 2.3 Injection Activities As summarized in the RAP Addendum #2, remedial activities planned for the Site included injection of an electron donor compound (3DMe) into saturated overburden soils in three spatially distinct injection "areas" (Areas A, B and C) via a grid network of approximately 150 temporary injection points. Injection points were to be installed by track -mounted rig using direct push technology (DPI) and injection was proposed to occur at three vertical intervals ranging from approximately 15 to 21 feet bgs at each injection point. In addition, MACTEC proposed injection into the shallow bedrock zone via six existing wells (EBMW-5, EBMW-8, EBMW-9, EBMW-10, EBMW-18 and EBMW-22) and two proposed new injection wells (IW-12+A and IW-14+). The locations of temporary injection points advanced during the current remedial activities are shown on Figure 3. The injection field forms and an associated injection boring location plan are provided in Appendix E. Photographs of the injection activities are provided in Appendix F. Upon commencement of injection activities, several adjustments were made to the injection plan to accommodate changing site conditions and maximize efficiency of the injection event. Those adjustments are summarized in the sections below. 2, 3.1 Overburden Injection Prior to initiating the overburden injection activities the RAP Addendum #2 specified conducting four borings to evaluate the depth to top of rock at the site. This task was accomplished by installing the wells discussed above: the pilot injection wells (IW-1 through AV-3), the sentinel monitoring wells (EBMW-29 4 of 7 NCDENR — Remedial Construction Completion Report July 20. 2011 MACTEC Project 6628-08-4691 NDNCDO001092 through EBMW-32), and the newly installed injection wells IW-12+A and IW-W. Based on these well borings, the depth to top of rock ranges from 18 to 38 feet bgs beneath the site. Subsequent to conducting the drilling activities, overburden injection activities were implemented in general accordance with the RAP Addendum #2 and the Modified UIC Permit. Injection of 3DMe into saturated overburden soils was performed between May 16 and June 13, 2011. A total of approximately 30,915 gallons of 3DMe emulsion (20:1 water-to-injectate mix ratio) were injected into saturated overburden soils during these activities. This volume is consistent with the anticipated volume for Areas A and B presented in the RAP Addendum #2. A typical temporary injection point schematic is provided on Figure 4. A summary of overburden injection activities is presented on Table 4. The following variations were made to the overburden injection plan: 1. Area "C" was eliminated from the overburden injection plan prior to commencement of activities on May 16, 2011. The initial purpose of injection into groundwater in Area "C" was to inject 3DMe hydraulically up -gradient of the floodplain and associated impacted groundwater and allow the natural hydraulic gradient to carry injectate through the impacted area (i.e., Areas A and B) over time. During review of the Modified UIC permit, the NCDENR expressed a concern that injection activities in the floodplain would "flush" contaminated groundwater into the adjacent Yadkin River. Injection into Area "C" was eliminated to reduce the potential for flushing into the Yadkin River and to effectively focus the current injection activities on the contaminant mass that is primarily located beneath Areas A and B. In addition, MACTEC staged injection activities to begin with the row of points located closest to the river, working up -gradient toward the more - heavily contaminated areas to further reduce the potential for flushing of contaminated groundwater into the Yadkin River. 2. The total number of temporary injection points was reduced from approximately 150 points to 126 points, primarily due to the elimination of injection into Area "C", as discussed above. 3. The depth interval of injection was amended from the proposed interval of approximately 15-21 feet bgs to a vertical interval within the expected saturated zone, which was the intent of the proposed 15-21 foot bgs interval. The reason for this change was that bedrock was encountered deeper than expected (38 feet bgs) during installation of injection well IW-12+A, resulting in a thicker saturated zone (i.e. 14 feet thick at injection point A3) on the western portion of injection Area "A". Therefore, the target injection zone was amended in the field to maximize treatment efficiency in the overburden and shallow bedrock, assuming that much of the contaminant mass is concentrated near the saprolite-bedrock interface. 4. The injection grid rows were narrowed from the designed specification of 30-foot spacing between rows to an actual spacing of approximately 20 feet. The row spacing was narrowed based on field -verification of the locations of the Yadkin River, drainage ditch, and berm for the aeration basin. The modified injection grid covered the area originally contemplated for Areas A and B as described in the RAP Addendum #2. 2.3.2 Bedrock Injection Injection of 3DMe and HRC Primer into shallow bedrock monitoring wells was performed in general accordance with the RAP Addendum #2 and the Modified UIC Permit between June 7 and 13, 2011. A 5 of 7 NCDENR —,Remedial Construction Completion Report July 20, 2011 MACTEC Project 6628-08-4691 NONCD0001092 total of approximately 1,799 gallons of 3DMe emulsion (10:1 water-to-injectate mix ratio) and HRC Primer mix were injected into wells EBMW-5, EBMW-8, EBMW-9, EBMW-10,1W-12+A, and IW-144 . This volume is consistent with the anticipated volume for Areas A and B presented in the RAP Addendum #2. A summary of bedrock injection activities is presented on Table 4. The following adjustment was made to the bedrock injection plan; Similar to the overburden zone described above, Area C was eliminated for bedrock injection to effectively focus the injection activities on the contaminant mass located in shallow bedrock beneath Areas A and B. Therefore, bedrock wells proposed in the RAP Addendum #2 (EBMW- 18 and EBMW-29) were not included in the injection activities. Note that the because well EBMW-29 was not installed in Area C, this well name was used for the first sentinel well installed along the bank of the Yadkin River in accordance with the Modified UIC Permit. Also note that the RAP Addendum #2 inadvertently referred to well EBMW-22 as an injection well located in Area C. This well is actually located in Area B and injection was not contemplated in Ns well during the original RAP or the RAP Addendum #2 as this well is screened in deeper bedrock (105-125 feet bgs) below the zone anticipated for injection during preparation of the RAP. 2.3.3 Survey and Investigative Derived Waste Subsequent to the conclusion of injection activities, the locations of the temporary injection points, newly installed injection and monitoring wells, and select existing monitoring wells, as well as the drainage ditch and top of bank of the Yadkin River were surveyed by a certified North Carolina Land Surveyor. The surveyed locations of these features are shown on Figure 3. Investigative derived waste was containerized during the RA activities for subsequent offsite shipment by Garco, Inc. Complete waste manifest forms were not available at the time of this report and will be provided in the first remedial action progress report. 3.0 POST -INJECTION ACTIVITIES Pending availability of funds, periodic post -injection groundwater field monitoring and sampling will be conducted for the fast year following the completion of 3DMefHRC Primer application at select well locations, as specified in the RAP Addendum #2. In addition, the Modified UIC Permit requires analysis of ferrous iron, nitrate/nitrite, total organic carbon (TOC), chloride, sulfate, sulfide, alkalinity, and ethane in post -injection groundwater samples. The initial round of post -injection groundwater monitoring was completed on July 12, 2011. The results of this monitoring will be incorporated into the first remedial action progress report for the Site. 6of7 NCDENR — Remedial Construction Completion Report MACPEC Project 6628-08-4691 Attachments: July 20, 2011 1VONCDM1092 Table 1 Summary of Well Construction Details Table 2 Summary of Pre -Injection Groundwater Quality Data Table 3 Summary of Pre-Tnjection Field Parameter Measurements Table 4 Summary of As -Built Injection Plan Details Figure 1 Site Location Map Figure 2 Site Plan Figure 3 As -Built Injection Plan Figure 4 Typical Temporary injection Point Schematic Appendix A LIIC Permit Appendix B Well Construction/Abandonment Records Appendix C Groundwater Sampling Data Sheets for Pre -injection Sampling Appendix D Laboratory Report — Pre -Injection Groundwater Samples Appendix E Injection Field Forms and Location Plan Appendix F Photographs 7of7 NCDENR - Remedial Construction Completion Report MALT'ECProiecr 6628-08-4691 TABLES July 20, 2011 NONCD0001092 Table 1 Summary of Well Construction Details Former CMI WWTP Elkin, North Carolina MACTEC Project 6228-08-4691 Top of Casing Well ID Elevation' [MSt Rate Depth to Groundwater {ft below TOC} Water Table Elevation �MSL} Screened Interval {ft bgs) Constructed Well Depth tft bgs} Injection wells 1W-12+A 102.67 5116/11 17.92 84.75 25-40 40 IW-14 +. 97M 5/16/11 15A1 82.95 2540� 40 Monitoring Wells EBMW-5 94.29 5116/11 12.50 81.79 29-39 39 EBMW-8 96.52 5/16/11 12.56 83.96 22-32 32 EBMW-9 96.29 5116/11 NM3 NM 43-53 53 EBMW-10 97.18 5116/11 12.85 84.33 41-56 56 EBMW-29 103+16 5l501 18.48 84.68 15-25 25 EBMW-30 104.37 515111 20.77 8160 12-22 22 EBMW-31 99.05 515111 14.88 84.17 8-18 18 EBMW-32 97.10 5.15i11 14.07 83.03 10-20 20 Notes: 1. Elevations for existing wells surveyed previously by others; elevations for wells IW-12+A, IW-14+ and EBMW-29 through EBMW-32 surveyed by R.B. Pharr & Associates, P.A. on June 23, 2011. 2. Well completed as open -borehole rock well from 25-40 feet bgs. 3. Well could not be located during pre -injection field parameter monitoring event on June 16, 2011. MSL - feet above mean sea level TOC - top of rasing ft - feet bgs - below ground surface Prepared by: +DPP 11 x''+'' Checked by:-1Lvht Table 2 Summary of Pre -Injection Groundwater Quality Data Farmer CMI WWTP Efkin, North Carolina MACTEC Project 6228-08-4691 Well ID EBMW-10 EBMW-18 EBMW-29 EBMW-30 EBMW-31 EBMW-32 NCDENR 2L Sample Dale 4/18/2011 4/16/2011 515i2011 5l512011 5/5/2011 5/512011 Standard (ug/L) RCRA Metals Arsenic E5.17 <5.0 NA NA NA NA 10 Barium 31.6 67.8 NA NA NA NA 700 Cadmium <1.0 <1.0 NA NA NA NA 2 Chromium <5.0 10.5 ° NA NA NA NA 14 Lead <5.0 <5.0 NA NA NA NA 15 Selenium <10.0 <10.0 NA NA NA NA 20 Silver <5.0 9.6 NA NA NA NA 20 Mercury <0.20 <0.20 NA NA NA NA 1 VOCS 2-Butanone (MEK) NA NA <5.0 5.1 <5.0 <100 4,000 Chloroethane NA NA <1.0 2.6 44.0 <20.0 3,000 Chloroform NA NA <1.0 4A 13.8 <20.0 70 1,1-Dichloroethane NA NA 66.7 2,850 3,960 3,590 6 1,2-Dichloroethene NA NA <1.0 <1.0 15.6 <20.0 0.4 1,1-Dichloroethene NA NA 51.1 2,590 3,720 101 7 cis-1,2-Dichloroethene NA NA <1.0 <1.0 4.3 <20.0 70 p-Isoprop Iloluene NA NA <1.0 1.6 <1.Q <20.0 NS Tetrachloroethene (PCE) NA NA <1.0 3.7 48.1 <20.0 0.7 1,1.1-Trichloroethane NA NA 1 278 22,000 39,300 1,970 200 1,1,2-Trichloroethane NA NA < 1.0 4.9 24.8 <20.0 NS Trichloroethene (TCE) NA NA <1.4 5.9 11.6 <20-0 3 Vinyl chloride NA NA <1.0 2.7 1.9 <20.0 0.03 Notes: 1. Concentrations reported in micrograms per liter (ug/L). 2. Less than the laboratory reporting limit. 3. Not analyzed. 4. Concentrations in bold -face type exceeded the NCDENR 2L Standard. 5. Not specified by the NCDENR. RCRA - Resource Conservation and Recover Act VOCs - volatile organic compounds NCDENR 2L Standards - 15A NCAC Subchapter 2L Groundwater Classification and Standards, January 2014 Prepared by. Checked by: 7 1 r Table 3 Summary of Pre -Injection Field Parameter Measurements Former CMI WWTP Elkin, North Carolina MACTEC Project 6228-08-4691 Well I❑ Date Field Measurements Depth to Water Temp. bC CRP pH Specific Conductance Turbidity (ft btoc) 'C (m 1L) (mV) S.U. us/cm NTU EBMW-5 5/16/11 12.50 14.32 4.36 -18 6.48 0.993 5.4 EBMW-7 5/16111 11.76 13.01 2.99 223 5.12 0.171 463 EBMW-8 5116/11 12.56 13.96 5.0 184 6.14 0.518 393 EBMW-10 5M6111 12.85 13.79 4.75 166 6.52 0.322 5.5 EBMW-11 5/16/11 11.77 13.33 4.72 220 6.04 0.101 62.6 EBMW-12 5116/11 18.73 14.83 3.86 233 5.22 0.357 17.9 EBMW-13 5116/11 16.80 ' EBMW-14 5/16/11 14.67 12.70 5.57 287 4.69 0.439 8.8 EBMW-15 5/16/11 14.15 14.26 2.88 216 5.84 0.224 15.5 EBMW-16 5116111 12.35 14.12 3.29 261 4.83 0.113 204 EBMW-18 5/16/11 11.97 14.00 3.11 -11 6.83 1.57 7.8 EBMW-19 5/16/11 18.61 15.36 8.67 145 6.75 0.397 5A EBMW-21 5116/11 15.44 13.49 6.79 129 7.27 0.316 5.4 EBMW-22 5/16111 11.24 13.68 7.41 -49 8.33 0.462 5.6 EBMW-29 515111 18.48 15.12 3.86 283 5.32 0.458 360 EBMW-30 515111 20.77 14.68 3.12 57 5.92 0.720 521 EBMW-31 515111 14.88 13.13 4.84 260 4.66 0.311 420 EBMW-32 515111 14.07 12.90 5.15 315 4.69 0.514 NM IW-12+A 5/16/11 17.92 15.31 3.41 93 5.72 0.423 8.5 IWA4+ 5/16/11 15.01 14.15 3.76 101 6-77 2.17 6.1 FAMW-1 5/16/11 14.39 14.37 6.67 207 5.77 0.156 535 Notes: - Water quality meter not able to be lowered down well due to obstruction at 10 feet bgs. Could not locate wells EBMW-1 and EBMW-9 at the time of collecting the field measurements ft btoc - feet below top of casing ❑O - dissolved oxygen QRP - oxidation reduction potential 'C - degrees Celsius mg1L - milligrams per titer mV - millivolts S.U. - standard units uSlcm - microSiemens per centimeter NTU - nephelometric turbidty unit Prepared by. lzdJ Checked by:_2"riK 7/_z*/(f Table 4 Summary of As -Built Injection Plan Details Former CMI WWTP Elkin, North Carolina MACTEC Project 6228-08-4691 Temporary Injection Points Injection Wells Area A Area B EBMW-5 EBMW_8 EBMW-9 EBMW-10 IW-12+A IW-14+ Number of Injection 91 35 NA' NA NA NA NA NA Points Injection z 10-28' bgs 10-26' bgs 25-38' bgs 18-31' bgs 40-53' bgs 38-55' bgs 23-40' bgs 23-40' bgs Interval Injectate3 Volume 22,389 8,526 207 225 227 320 396 414 (gallons) Notes: 1. NA = Not Applicable; single injection well 2. Injection interval in Injection wells indicates packer depth (typically two feet above screen) to the base of the well screen; Injection Interval in Temporary Injection Points is range of maximum and minimum depths. Injectate was generally injected over three intervals: three feet above refusal depth, two feet above the first interval and two feet above the second interval. 3. Injectate = 3DME at a 20:1 ratio in the Temporary Injection Paints; 3DME at a 10:1 ratio and HRC Primer in the injection Wells. bgs - below ground surface Prepared by. N F -7 201 I I Checked by:_Anq_ 7("I t+ NCDENR — Remedial Construction Completion Report MACTEC Proiect 6628-08-4691 FIGURES July 20. 2011 NONCO0001092 .q E pP� O S v RA1�aN� �Rl+� a N CHATHAM INC. PROPERTY V� J J 1 � { t} l 1 • 1 .1 1 1 � � EBMW-4 } } } FAMW-2 L EBMW-23 EBMW-24 , E W-1I I ai EBMW-18 CHATNAM INC. PARCEL 2 PROPERTY CMI FLYASH DISPOSAL — -� AREA PROPERTY TRUCK TERMINAL EBMv-3 PARCEL 1 CMt WWTP PROPERTY A3 UWE O EEWW-2 INACTIVE FT SEWER LINE W-WEBMW-26 BRICKMWE-101 MANHOLE EBMW-1 s 55 EBMW-17 EBMW-16'0 MW�1 $fBMW-9 Y55 FPMW-5 Iw-14+03 EBMW-5 EBMW•-22 -fjG Mw�14 �BI4'tYE-$ EBMW-28 E gljyr_ 5= FAMW-I EBM EBUW-10 � RV 5i E MW-21 EBMW-7L W-12+ EBMW-2 ESMW-31 13 _55 SMw-�'' 1�pK9� MWE-2 l 10 RANG a�p5 �ss S_ SS � FPMW-3 45 FPMW-2 APPROXIMATE SCALE IN FEET FPMW- 100 50 0 130 NOTES: BASE MAP AFTER SPATCO EN4IROMENTAL SERVICES DRAWING No, 9-1790+ FIGURE 2 MONITORING WELL LOCATIONS AFTER DUNN ENGINEERING SURVEY MAP, PROJECT NO. 802D603. 6/8/04 (REVISED 10/24/05 and 10/02/05) SELECT MONITORING WELLS SURVEYED BY R.S. PHARR ON 6/23/11, ALONG WITH THE LOCATION OF ALL TEMPORARY INJECTION POtNTS. EBMIIIr-19 EBMW-30 � ~ MACTEC APPROXIMATE TOP of E7(PLANAT[QN JBANK OF YADKIN RIVER RAILROAD TRACKS OVERBURDEN MONITORING WELLS iv EA'cfwrmNC & C7NSW w. the. �•� CHARLOTTE, NORTH CAROLINA STREAM {13 BEDROCK MONITORING WELLS -- • — • • -- PROPERTY LINE PILOT TEST INJECTION WELLS (ABANDONED) SITE PLAN —SS-- SEWER UNE CMI WWTP — — — — APPROXIMATE TOP OF BANK ELKIN, SURRY COUNTY, NORTH CAROUNA BARED MQ� DAT� 14 It CHECK 0 DATE 7 I No. 6228-08-4691 FIGURE 2 l� MW-01-1 I 1l ` 1 1 l 1 � i i EBMW-4 L-� I � I A►fW-2 EBµw-23 AREA '\ C (NOT COMPLETE 4 EBMW-24 ti _ -2 EBMw7 s$ m EB1AW-1B m EBMW-11 _ ss E$s,IW-TQ � \�9 — OEBMW-12 EBMW-25 EBMW-21 E 1-7 � EBMW-20 Nw-13 s EBMW-30 APPROXIMATE TOP OF BANK OF YADKIN RIVER APPROXIMATE SCALE IN FEET 50 25 O 5D l EBMw-s f � - - STREAM (D OVERBURDEN WELLS - -- - PROPERTY LINE ffi BEDROCK WELLS —55 SEWER LINE E3 UPPER BEDROCK INJECTION WELL (25-45') - - — - APPROXIMATE TOP OF BANK PILOT TEST INJECTION WELLS (ABANDONED) TEMPORARY OVERBURDEN INJECTION POINT EBUW-17� FPM W-S$ NOTES: BASE MAP AFTER SPATCO ENVIROYENTAL SERVICES DRANANG No. 9-1790. FIGURE 2 MOMTORING WELL LOCATIONS AFTER BUNN ENGINEERING SURVEY NAP, PROJECT NO. B020601 6/8/04 (REVISED 10/24/05 and 10/02/06) SELECT MONITORING WELLS SURVEYED BY R.B. PHARR ON 6/23/11, ALONG WITH THE LOCAT4ON OF ALL TEMPORARY INJECTION POINTS, iwAil MACTEC EII NE RUG k CDAwA rm. WC CHARLOTTE, NORTH CAROLINA AS BUILT INJECTION PLAN CMI WWTP El KIN, SURRY COUNTY, NORTH CAROLINA PREPARED ❑ATE CHEC 0 DATE BY Mai itm 0I11 JOB NO- 6228-08-4691 FIGURE 3 DIRECT PUSH DRILL ROO, 2.25. O.D. RESIDUAL SOIL STIMATED WATER LEVEL Wit_-'. '•r -,r� ;:i • �' , ' ' :r•' PARTIALLY :•.`:' ...= 'w �.. WEATHERED ROCK SLOTTED INJECTION SOUN PROBE TO REFUSAL AND INJECT 30ME SLURRY AT THREE INTERVALS WITHIN THE ESTIMATED SATURATED ZONE WHILE EXTRACTING THE PROBE LEGEND j 3DME SLURRY PROBE RE USAIL (ESTIMAIM TOP OF RWO FIGURE TYPICAL OVERBURDEN IgJECT10N Parr fiMAETECSUITELai�iJE CMI c. 2s2oa ELKIN, SURRY COUNTY, NORTH CAROLINA 4 FlLE- 5 NL vm BY: I to I, CHE KED EM 71u it APPROVED BY. DATE JOB II{1: 7-19-1f 6228-08-4691 1VCDENR - Remedial Construction Completion Report MACTECProieet 6628-0$-4691 APPENDIX A UIC PERMIT Jtily 20,2011 NDNCDO001092 TXX �i MCDENR North Carolina Depariment of Environment and Natural Resource-, Division of Water Quality, Beverly Eaves Perdue Coieerr, K Sullins GOVernor Director April 7, 2011 James A. Ovenden. Trustee CMI-Industries - 219 Muirfield Drive Spartanburg, SC 29306 Ref: Issuance of Injection Permit W10400106 CMl Industries' Wastewater Treatment Plant Elkin, Surry County, North Carolina. Dear Mr. Ovenden: De_=reemar Secretar � In accordance with the application received on February 14, 2011, and the supporting data received March 16, 2011, we are forwarding permit number W10400106. This permit is to inject HRC 3DMe (Hydrogen Release Compound Primer with 3D Micro Emulsion) to remediate groundwater contaminated with chlorinated solvents at the facility referenced above. This permit shall be effective from the date of issuance until March 31, 2013, and shall be subject to the conditions -and limitations stated therein, including the requirement to submit a final project evaluation as stated in PART VII — MONITORING AND REPORTING REQUIREMENTS. Please note that some of the monitoring requirements have chanted from amour application. Please read the entire permit to ensure that you are aware of all compliance requirements of the permit. You will need to notify this office by telephone 48 hours rior to initiation of operation of the facility. In order to continue uninterrupted legal use of1hadmiection facility for the stated purpose, you must submit an application to renew the permit 120 days prior to i expiration date. Please contact me at (919) 715-6162 or david.goodrichr cdenr.gov if you have any questions about your permit. Best Regards, David Goodrich, fiydrogeologist cc: Sherri Knight. Winston-Salem Regional Office Mark P. Filardi, MACTEC Engineering and Consulting. Inc.. 2801 Yorkmont Road. Suite I00. Charletie. NC 282OF Janet MacDonald, NCDWM Superfund Section. 1646 Mail Service Center. Raleigh. NC 27699-1646 W10400106 Permit File AzYJi==_R FROT CM101: 3=71I A 1636 hAa� 55roce Center. Raieipl.. North Lxo na 276W.1BY iomwr.. 272E C.E ai! botiwarC. Ra0r.. hnrlr:.arorms P601 11' Pane. Qt6. 3 -3U' ;Ax ; 915-''..waBE. =kh i 5t5 1 -U4 asome Ssrv;.� . 1r= mzerr;c; wwx.norrarsroualm.n� ��]�;�'�.ilril;il;L NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH, NORTH CAROLINA PERMIT FOR THE CONSTRUCTION AND OPERATION OF A WELL FOR INJECTION In accordance with the provisions of Article 7, Chapter 87; Article 21. Chapter 143, and other applicable Laws, Rules, and Regulafions. PERMISSION IS HEREBY GRANTED TO CMI Industries FOR THE CONSTRUCTION OF 150 INJECTION WELLS AND OPERATION OF 158 TYPE 51 INJECTION WELLS, defined in Title 15A North Carolina Administrative Code 2C .0209(e)(3)(C), to inject HRC 3DMe and HRC Primer, for the stimulation of anaerobic bioremediation of chlorinated solvents and petroleum compounds. These injection wells/points will be located at the CMI Wastewater Treatment Plant, 304 East Main Street, Elkin, Surry County, North Carolina, and will be operated in accordance with the application submitted February 14, 2011, and in conformity with the specifications and supporting data submitted March 16, 2011, all of which are filed with the Department of Environment and Natural Resources and are considered a part of this permit. This permit is for Construction and Operation only, and does not waive any provisions of the Water Use Act or any other applicable Laws, Rules, or Regulations. Operation and use of an injection well shall be in compliance with Title 15A North Carolina Administrative Code 2C .0100 and .0200, and any other Laws, Rules, and Regulations pertaining to well Construction and use. This permit shall be effective, unless revoked, from the date of its issuance until March ' and shall be subject to the specified conditions and limitations set forth in Parts 1 through h hereof. Permit issued this the 7th day of April, 2011. j j; or Coleen H. Sullins, Director Division of Water Quality By Authority of the Environmental Management Commission. Permit No. W10400106 PAGE 1 OF Ver. Apri12011 A111111C-6 PART I - WELL CONSTRUCTION GENERAL CONDITIONS 1. The Permittee must comply with all conditions of this permit and with the standards and criteria specified in Criteria and Standards Applicable to Injection Wells (15A NCAC 2C .0200). Any noncompliance with conditions of this permit constitutes a violation of the North Carolina Well Construction Act and is grounds for enforcement action as provided for in N.C.G.S. 87-94. 2. This permit shall become voidable unless the facility is constructed in accordance with the conditions of this permit, the approved plans and specifications, and other supporting data. 3. This permit is valid only for construction of the number of injection wells described in the application -and other supporting data. Construction of additional injection wells must be approved in advance by the Aquifer Protection Section. 4. Each injection well shall not hydraulically connect separate aquifers. s. Each injection well shall be constructed in such a manner that water from land surface cannot migrate into the gravel pack or well screen. 6. Each injection well shall be secured to reasonably insure against unauthorized access and use. Each well shall be permanently labeled with a warning that it is for injection purposes and the entrance to each well must be secured with a locking cap. Each injection well 'shall be afforded reasonable protection against damage during construction and use. 8. Each injection well shall have permanently affixed an identification plate. 9. Within 30 days of completion of well construction, a completed Well Construction Record (Form GW-1) must be submitted for each injection well to: Aquifer Protection Section-UIC Program DENR-Division of Water Quality 1636 Mail Service Center Raleigh, NC 37699-1636 PART II - WELL CONSTRUCTION SPECIAL CONDITIONS At least forty-eight (48) hours prior to constructing each injection well, the Permittee shall notify the Aquifer Protection Section -Underground Injection Control (UIC) Central Office staff, telephone number 919-715-6162 and the Winston-Salem Regional Office Aquifer Protection Section Staff, telephone number (336) 771-5000. Permii No. WI0400106 PAGE , OF VM APW 201 1 APUC-6 PART III - OPERATION AND USE GENERAL CONDITIONS I. This permit is effective only with respect to the nature, volume of materials, rate of injection, and number of injection wells as described in the application and other supporting data. 2. This permit is not transferable without prior notice to, and approval by, the Director of the Division of Water Quality (Director). In the event there is a desire for the facility to change ownership, or there is a name change of the Permittee, a formal permit amendment request must be submitted to the Director, including any supporting materials as may be appropriate, at least 30 days prior to the date of the change. 3-. The issuance of this permit shall not -relieve the Per-mittee of the responsibility of complying with any and all statutes, rules, regulations, or ordinances which may be imposed by other local, state, and federal agencies which have jurisdiction. Furthermore, the issuance of this permit does not imply that all regulatory requirements have been met. PART IV - PERFORMANCE STANDARDS 1. The injection facility shall be effectively maintained and operated at all times so that there is no contamination of groundwater which will render it unsatisfactory for normal use. In the event that the facility fails to perform satisfactorily, including the creation of nuisance conditions or failure of the injection zone to adequately assimilate the injected fluid. the Permittee shall take immediate corrective actions including those actions that may be required by the Division of Water Quality such as the repair, modification, or abandonment of the injection facility. 2. The Permittee shall be required to comply with the terms and conditions of this permit even if compliance requires a reduction or elimination of the permitted activity. 3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface or groundwater resulting from the operation of this facility. PART V - OPERATION AND MAINTENANCE REQUIREMENTS 1. The injection facility shall be properly maintained and operated at all times. 2. The Permittee must notify the Division and receive prior written approval from the Director of any planned alterations or additions in the permitted facility or activity not specifically authorized by the permit. 3. At least forty-eight (48) hours prior to the initiation of the operation of the facility for injection, the Permittee trust notify by telephone the Aquifer Protection Section-UIC. Central ❑ffice staff, telephone number 919-715-6152. Notification is required so that Division staff can inspect or otherwise review the injection facility and determine if it is in compliance with permit conditions. Permit No. W104001 Q5 PAGE 3 OF 7 ver. April 2011 APR]IC-6 PART VI - INSPECTIONS Any duly authorized officer, employee, or representative of the Division of Water Quality may, upon presentation of credentials, enter and inspect any property, premises, or place on or related to the injection facility at any reasonable time for the purpose of determining compliance with this permit, may inspect or copy any records that must be maintained under the terms and conditions of this permit, and may obtain samples of groundwater, surface water, or injection fluids. ?. Department representatives shall have reasonable access for purposes of inspection, observation. and sampling associated with injection and any related facilities as provided for in-N.C.G.S. 87-90. I Provisions shall be made for collecting any necessary and appropriate samples associated with the injection facility activities. PART N1II - MONITORLNG AND REPORTING REQUIREMENTS 1. The proposed monitoring plan included in the application, along with additional wells and parameters cited herein, shall be followed. The additional wells shall be four shallow monitor wells presented on Figure 1 situated between Area A and the Yadkin River; wells EBMW-6 and EBMW-17 associated with Area B, and wells FPMW-4 and FPMW-5 associated with Area B. Additional laboratory parameters that will be performed concurrent with all other laboratory analyses will consist of the following: ferrous iron `s ehloride ''__� ethane nitrite/nitrate nitrogen ✓ sulfate sulfide Total Organic Carbon (TOC) alkalinity's Alkalinity shall be reported as Total Alkalinity and individual values shall be given for the concentrations of Bicarbonate, Calcium, and Magnesium. All sample results shall be submitted to the Aquifer Protection Section's Winston-Salem Regional Office and the Raleigh Central Office, Any monitoring (including groundwater, surface water, or soil sampling) deemed necessary by the Division of Heater Quality to ensure surface and ground water protection, will be established and an acceptable sampling reporting schedule shall be followed. 4. Pre -injection metals analysis of monitoring wells EBMW-10 and EBMW-1 S shall be submitted as soon as the results are available. 5. The Permittee shall submit an Injection Event Record within 30 days of completing each injection. Permit No. ►N10400106 PAGE 4 OF 7 ver. April 2011 - AP LJ1C-6 6. The Permittee shall produce a finai project evaluation within 9 months after completing all injection -related activity associated with this permit or produce a project interim evaluation before submitting a renewal application for this permit. This document shall assess the injection projects findings in a written summary. The final project evaluation shall also conWn monitoring well sampling data, contaminant plume maps and potentiometric surface maps. 7. The monitoring results and the final project evaluation shall be submitted to: and to: Aquifer Protection Secbon-1_IIC Program DENR-Division of Water Quality 1636 Mail Service Center Raleigh, NC 27699-1636 - Aquifer Protection Section DENR-DWQ Winston-Salem Regional Office 585 Waughtown Street Winston-Salem, NC 27107 8. The Permittee shall report by telephone, within 48 hours of the occurrence or first knowledge of the occurrence, to the Winston-Salem Regional Office, telephone number (336) 771-5000, any of the following: (A)Any occurrence at the injection facility which results in any unusual operating circumstances; (B) Any failure due to known or unknown reasons, that renders the facility incapable of proper injection operations, such as mechanical or electrical failures. 9. Where the Permittee becomes aware of an omission of any relevant facts in a permit application, or of any incorrect information submitted in said application or in any report to the Director, the relevant and correct facts or information shall be promptly submitted to the Director by the Permittee. 10. In the event that the permitted facility fails to perform satisfactorily, the Permittee shall take such immediate action as may be required by the Director. PART VXII - PERMIT RENEWAL In order to continue uninterrupted legal use of the injection facility for the stated purpose, the Permittee must submit an application to renew the permit 120 days prior to its expiration slate. PART IX - CHANGE OF MIELL STATUS i . The Permittee shall provide written notification within 15 days of any change of status of an injection well. Such a change would include the discontinued use of a well for injection. If a well is taken completely out of service temporarily, the Permittee must install a sanitary seal. If a well is not to he used for any purpose that well must be permanently abandoned according to 15A NCAC X .0314. Well Construction Standards. Permit No. W10400106 PAGE ; OF 7 Ver. April 2011 APIUK-4, 2. When operations have ceased at the facility and a well will no longer be used for any purpose, the Permittee shall abandon that injection well in accordance with the procedures specified in I5A NCAC 2C .0214, including but not limited to the following: (A) All rasing and screen materials may be removed prior to initiation of abandonment procedures if such removal will not cause or contribute to contamination of the groundwaters. (B) The entire depth of each well shall be sounder] before it is sealed to insure freedom from obstructions that may interfere with sealing operations. (C) The well shall be thoroughly disinfected, prior to sealing, if the Director determines that failure to do so could lead to the contamination of an underground source of drinking water. 4 (D)Drilled wells shall be completely filled with cement grout or bentonite grout, which shall be introduced into the well through a pipe which extends to the bottom of the well and is raised as the well is filled. (E) In the case of gravel -packed wells in which the casing and screens have not been removed, neat -cement, or bentonite grout shall be injected into the well completely filling it from the bottom, of the rasing to the top. (F) In those cases when, as a result of the injection operations, a subsurface cavity has been created, each well shall be abandoned in such a manner that will prevent the movement of fluids into or between underground sources of drinking water and in accordance with the terms and conditions of the permit. (G)The Permittee shall submit a Well Abandonment Record (Form GW-30) as specified in 15A NCAC 2C .0213(h)(1) within 30 days of completion of abandonment. 3. The written documentation required in Part IX (1) and (2) (G) shall be submitted to: Aquifer Protection Section-UIC Program DENR-Division of Water Quality 1636 Mail Service Center Raleigh, NC 27699-1636 PART X — WORKER PRECAUTIONS DURING APPLICATION 1. Ingestion may result in burn of the lips, tongue and mouth. Exposure to the eyes can cause distortion of cellular membranes, loss of corneal, conjunctival and lens epithelium. and loss of endothelium of the cornea and blood vessels. Inhalation may produce upper airway edema. respiratory failure, wheezing, pulmonary edema, and pne=onitis. Skin exposure may cause pain, redness, irritation and severe burns. Permit No. W10400106 PAG1r fi ❑F 7 ver. April 2011 APUC-6 `_'. if the product is released into the environment in a way that could result in a suspension of fine solid or liquid particles (e.g., grinding, blending, vigorous shaking or mixing), then proper personal protective equipment should be used. The application process should be reviewed by an industrial hygienist to ensure that the most appropriate personal protective equipment is used. 3. Persons working with these products should wear goggles or a face shield, gloves, and protective clothing. Face and body protection should be used for anticipated splashes or sprays. 4. Eating, drinking, smoking, handling contact lenses, and applying cosmetics should not be permitted in the applicationareaduring or immediately following application. 5. Safety controls should be in place to ensure that the check valve and the pressure delivery systems are working properly. d. The Material Safety Data Sheets should be followed to prevent incompatible or adverse reactions and injuries. 7. Access to the area of application should be limited to the workers applying the product. 8. Violent reactions or ignition could occur under the appropriate conditions with acids, alcohols, p-bis(1,3-dibromothyl) benzene, cyclopentadiene, germanium, hypnitrous acid, maleic anhydride, nitroalkanes, ?-tetrafluoropropanol, and thorium dicarbide. "Measures should be taken to prevent such reactions. Measures should be taken to prevent contamination of existing or future wells and surface waters that may be located near the application area. Permit No. V+'10400106 PAGE OF 7 vcr. April 2011 At' UIC -1, rA.crt 7 ti n,t_ la.YL'IRSY d3rPF rl YR( 7 ~ ` r r t i r.(wIYEMI I r�y� ou+r .ASV _ fflril•J �YfXKNVA VZZe.T6r /AFA (ISO POSH) _ rtrAgr ilsivo an J .� IOLE _- _ APr'RDXMA'rr SCALE DF MET � nYw_a. �••\ �-"�i�''=',[yHs-. 51 r l �.e am a lee •[aYq-ji Sl4w -fed • CO[1 a-:: rPVP�•5 _ l • I rr/ � I Oh, .�t 1 1TLF A (!Lx}'1 9ry �� 1rASOMO ,RAd.7 rNMI" r+rc tmm ip .�-e�-I I�t�f�r �+ ❑r'� ! ©vGrh:{ pL{ GR ��drf. fa,• {Jef! 5 . .cr: �[!•� a L.fcrw1^ •• N_z Wr r.crM[. 1, *.f09+ t.Gf M,c cOYNt L K. rlGu4i S. w*to t.rnr ov"M " ■MI lta.00. WnLs U."Q KDNM. -mg 25-40- tEx mul w.FlVtaerr K"ON ARTS RS-AS trm"'m Ur'rtrl aEQOXK HILLS (UM o t4[cr�ol row. IS rile ew 0 Bows 4VE5 PAIL ver Ar 111 1 Am A ErrYwolr[wl.{ sd.-rs P..w µ, .-�r.r. rwws 7 0a.101W4 wtu 109AWIS Arta "H.d P020.01 6/010i .[rrylP f./t.,my we LLKA*Od% e.[ A A1[. 1 &IMAICTEC I OM fnf7tFfw t {Cr4'.Enc Yc n RYg0lrt. MWW CAMOM INJECTION LOCAIM PLAN CIA, WWIP EVP . Sl IrMy COON I T. NORM CAROUWr pf ln.re I111, r0 627A-OS-iG81 NCDENR — Remedial Cons+nxtion Completion Report AM CTEC Project 6628-08-4691 APPENDIX B WELL CONSTRUCTION RECORDS July 20. 2011 NONCD0001092 1 ■ oN RLswNma WELLCONsTRuCTIoN RECUiiD North Carolina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACrOR CERTIFICATION # 2581 1. WELL CONTRACTOR: 13RIAN THOMAS Wen Contractor (IndiviJual) Name GEOLOGIC EXPLORATION, INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE BLVD STATESVILLE NC 28625 City or Town State Zip Code 7��- 872-7686 Area code- Phone number 2, WELL INFORMATION: SITE WELL tD #(it appficaNe) IW-3 STATE WELL PEHMITO(if applicable) DWQ or OTHER PERMIT #(if applicable) WELL USE (Check Applicable Sox) Monitoring F. Municipal/Public ❑ IndustriallCommercial ❑ Agricultural ❑ Recovery p Injection ❑ Irrigation❑ Other ❑ {fist use] OATF DRILLED 06/02/10 - 05104I10 TIME COMPLETED AM ❑ PM ❑ 3. WELL LOCATION: CITY: ELKIN COUNTY SURRY FABRIC LANE 28621 (Street Name, Numbers, Community, SubdIvision, Lol Ho-, Parcel. Zip Code} TOPOGRAPHIC I LAND SETTING: ❑Slope ❑Valley ❑Fiat ❑Ridge ❑ Other (check appropriate box) LATITUDE May be in dcp ees, minutes, seconds or LONGITUDE i n a decimal formal Latitudc/longitude source: ❑GPS ©'topographic map (loeatbn of we►must be shown on a USG topo map and attached to this fonn if not askig GPS) 4. FACILITY -Is the name of the busrnai%where the well is lacaxd- FACILITY ID tf(if applicable) NAME OF FACILITY CMI STREET ADDRESS FABRIC LANE ELKIN NC 28621 City or Town State Zip Code CONTACT PERSON CMI. INC MAfLI1NG ADDRESS 4399 CORPORATE ROAD CHARLESTON SC 29405 City of Town Slate Zip Code L�- Area code - Phone number S. WELL DETAILS: a. TOTAL DEPTH: 120-0 FEET b. DOES WELL REPLACE EXISTING WELL? YES Ll NO E c. WATER LEVEL Below Top of Casing: 18.0 FT (Use "+" if Above Top of Casing) d. TOP OF CASING IS 3-0 FT. Above Land Surface' 'Tap of casing terminated alloy below land surface may require a variance in accordance with ISA NCAC 2C .0118. e. YIELD (gpm) NfA METHOD OF TEST NIA 1. DISINFECTION: Type NIA Amount NIA g. WATER ZONES (depth): From To From To From To From To Frain To From To & CASING: Thicknessl Depth Di e�er WLgF�att Ma,01 It �i 0 PVC From O.0 To 26,0 Ft. 4 From To FL Fran To Ft- 7, GROUT: Depth Material Meth rd From 0'0 To 260 Ft. Port!" benlonee SLURRY Frcm To Ft. From To— Ft. 8. SCREEN: Depth Diameter Slot Size Material From To Ft, in, 41, From To— Ft. Im in. From Ta FL in. in. 9. SANOIGRAVEL PACK: Depth Sae Material From To Ft. From To FL From To FL 10. DRILLING LOG From TO Formation Description 0.0 7.0 GROWN SILTY CLAY 7-0 17.0 GRAY SANDY CLAY 1T 0 21.0 PARTIALLY WEATHERED ROCK 21,0 120,0 ROCS 11. REMARKS: OPEN HOLE FROM 26-0 To 120.0 FT I DO HE RE BY CE RTIFY THAT Ti RS WELL WAS CONSTRUCTED I N ACCORDANCE WITH t FC. WELL CONSTRUCTION STANDARDS, AND TWIT A COPY OF THIS t(,DR6 5 UEEEN PROVIDED TO THE OWNER. 06/15/10 MWAT U IED LL COWMAC T OR' DATE BRIAN THONAS PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b 1617 Mail Service Center— Raleigh, NC 27699-1617 Phone No. (919) 733-7015 ext 568. Rey, 7105 NONRESIDENTIAL WELL coNmuCTiON RECORD North Caroiina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2581 1. WELL CONTRACTOR: BRIAN THOMAS Web Contractor (Individual) Name GEOLOGIC EXPLORATION, INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE BLVD STATESVILLE NC 2a625 City or Town State zip Cade 7pi 4 �- 872-7686 Area code- Phone number 2. WELL INFORMATION: SITE WELL ID 9(d applicable) ICY-1 STATE WELL PER MIT#(if Applicable) DWD or OTHER PERMIT #(if applicable) WELL USE (Check Applicable Box) Moniloring @ Municipal/Public C] IndustriallComrrlercial ❑ Agricultural ❑ Reco+ery L} injection ❑ Irrigation❑ Other ❑ (list use) DATE DRILLED 06102110 - 06t04 110 TIME COMPLETED AM U Ph! ❑ 3. WELL LOCATION: CCiY; ELKIN COUNTY SURRY FABRIC LANE 28621 (Street Name, Numbers, Cornmunity, Subdivision, Lot No., Parcel, Zip Code) TOPOGRAPHIC 1 LARD SETTING: ❑ Slope []Valley ❑ Flat ❑ Ridge ❑ Other (check appropriate box) LATITUDE May be in degrees, minutes, seconds or LONGITUDE in a decimal format Latitude/longitude source: ❑ GPS ❑Topographic map (bcabbn of we® must be shown on a USG topo reap and attached to this form # net Using CPS) 4. FACILITY- Is the name or the business where the wet! rs to *d FACILITY ID #(if applicable) NAME OF FACiLIT'f CMI STREET ADDRESS FABRIC LANE ELKIN NC 28621 City or Town State Zip Code CONTACT PERSON CMI, INC MAILING ADDRESS 4399 CORPORATE ROAD CHARLESTON SC 29405 City or Town State Zip Code Area code - Phone number 5, WELL DETAILS: a. TOTAL DEPTH: 120.0 FEET b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO c, WATER LEVEL_ Below Top of Casing: 18 0 FT. (Use "+- If Above TDp of Casing) d, TOP OF CASING IS 3.0 FT. Above Land Surface' 'Top of casing tenninaled atfor below land surface may require a variance in accordance with 15A NCAC 2C .01 I & e. YIELD (gpm): NIA METHOD OF TEST NIA f. DISINFECTION: Type NIA Amount NIA 9. WATER ZONES (depth): From-1-0 From To From To From To From Tv From To 6. CASING: Thickness) Depth Diamr�eetter W hII Material From 0.0 To 25.0 Ft, 4 INi;Hi s' a6 PVC From To— Ft. From To Ft. T GROUT: Depth Material Method From 0.0 To 25.0 Ft. Portland bwn kx ile SLURRY From To Ft, From To Ft, 11 SCREEN: Depth Diameter Slot Size Material From To Ft. in. In. From To- F1. in. in, From To Ft. in. in. g. SANDIGRAVEL PACK: Depth Size Material From To FL From To Ft. From To Ft. 10. DRILLING LOG From To Formation Description 0.0 7.0 BROWN SILTY CLAY 7.0 17.0 GRAY SANDY CLAY 17.0 20,0 PARTIALLY WEATHERED ROCK 20.0 1200.ROCK 11. REMARKS: OPEN HOLE FROM 25.0 TO 120.0 FT i Do HEREBYCERTIFYTHAT THIS WELL WA CDNSTRUCTEO IN ACCORDANCE WITH 15Apr3 WELL CONSTR 0 CTIGN STANDAR AND THATA COPY OF THIS D riA EENrR[]VIpE6 TD TiiE JHER. 06/15110 SiGt URE'04Pr5?,6IFMDWEL1 CONTRACTOR DATE BRIANT THQ AS PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b 1617 Mail Service Center — Raleigh, NC 27699-1517 Phone No. (919) 733-7015 ext 668. Rev. 7105 .[ ■ ON � IESIDENTIA.L WF,LL CONSTR[ICTIO]V RECORD T fit' North Carolina Department of Envirarment and Natural Resources- Division of Water Quality •� WELL CONTRACTOR CERTIFICATION # 2581 1. WELL CONTRACTOR; SRIAN THOMAS Well Contractor (Indiudual) Name GEOLOGIC EXPLORATION. INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE OLVC STATESVILLE NC 28625 City or Tawas stale Zip Code 70� a J_ 872-7686 Area code- Phone number 2. WELL INFORMATION: SfTE WELL ID#(Wa*cabe) iW•2 STATE WELL PERMIT#t(tf applicable) DW4 or OTHER PERMIT #{if applicable) WELL USE (Check Applicable Box) Morrtering fl MumdpallPubhc L7 IndvstriallCommercial ❑ Agr{cullural (] RecoveryLl Injeclion I.a Irrigation❑ Other ❑ (iist use) DATE DRILLED W02110.0610010 TIME COMPLETED AM ❑ PM ❑ 3. WELL LOCATION: CITY; ELKIN COUNTY SORRY FABRIC LANE 20621 {Sae et !Jame, Numbers, Cammurtity, Subdivision, Lot No., Parcd, Zip Code! TOPOGRAPHIC 1 LAND SETTING: ❑ Slope ❑ Valley ❑ Flat ❑ Ridge Ll Other (Check appropnate box) LATITUDE Mey be in degrees, `— — minutes, seconds or LONGITUDE in a decimal format Ladtudellongitude source: ❑G11S ❑Topographic map (focaton of well must be shown on a USG5 ropo map and attached to this brm d not using GPS) 4- FACILITY- is thn name or Iha business where the weA is located. FACILITY ID #(it applicable) NAME OF FACILITY CMI STREET ADDRESS FABRIC LANE ELKIN NC 28621 City or Town State Zip Cade CONTACT PERSON CMI, INC MAILING ADDRESS 4399 CORPORATE ROAD CHARLESTON Sc 29465 City or Town Slate Zip Cade Area code - Phone number s. WELL DETAILS: a. TOTAL DEPTH: 120.0 FEET b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO El c. WATER LEVEL Bel ow Top of Casing: 18.0 Fr. [Use "+" if Above Top of Casing) d- TOP OF CASING IS 3-0 FT- Above Land Surface' 'Toµ of casing terminated attar below land surface may require a variance in accordance with 15A NCAC 2C +0118. C. YIELD (gpm). NIA METHOD OF TEST NIA t DISINFECTION: Type NIA Amount NIA g. WATER ZONES (depth): From To— From To From To From To From To From To 6. CASING: Thicknessl Depth From D.0 To 25•0 Dlaet�eter Wf< h; Malaria! Ft. d 1NGH Suva PVC From To FL From To Ft. 7, GROUT: Depth Material Method Frorn 0.0 To 25.0 Ft. Poruand bentonite SLURRY From To- Ft. From To Ft, 8. SCREEN; Depth Diameter Slot size Material From TO Ft. in. in. From To Ft, in, in. _ From To Ft. In. In. 9. SANDIGRAVEL PACK: Depth Size Material From To Ft. From —To— Ft, From To Fl- 10. DRILLING LOG From To Formation Description 0.0 7.0 BROWN SILTY CLAY 7.0 17-0 GRAY SANDY CLAY 17,0_ _ 20.0 PARTIALLY W£ATHERE0 ROCK 20.0 120.0 ROCK 11. REMARKS: OPEN HOLE FROM 25.0 TO 120-0 FT I DO HEREaY CERTIFY THAT THIS WEtd. WAS CONSTRUCTED IN ACC OfIOANCE WrTh 7�LL ONSTRU T ONE W_W AR -AND THAT A COPY Qf THIS R COi� EN P�OVIpEO TOTHEW ER. srs511❑ SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE BRIAN THOMAS PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the ❑ivision of Water quality within 30 dayS. Attn: Information Mgt., Form GW-1b 1617 Mail Service Center -- Raleigh, NC 27699.1617 Phone No. (919) 733-7015 ext 568. Rev. 7105 WELL ABANDONMENT RECORD North Carolina Depattlnent of Environment and Namrai Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2452 I. WELL CONTRACTOR: JERRY WATKINS Well Contractor {individual} Name GEOLOGIC EXPLORATION, INC. Weil Cuntraelor Company Name STREETADDRESS 176 COMMERCE BLVD_ STATESVILLE NC 28625 City or Town 7[ 04 - 872-7686 Area code - Phom number State 2. WELL INFORMATION: SITE WELL III # (ifapplicable) IWA STATE WELL PERMIT k (if applicable) COUNTY WELL PERMITN (i f appi icab It) DWQ or OTHER PERMIT # (ifapplicabit) Zip Code WELL USE (Check applicable use): JZ Monitoring ❑ Residential ❑ Municipal/Public ❑ lndustriallCommerciAl ❑ Agricultural ❑ Recovery ❑ Injection ❑ Irrigation ❑ Olber (list trse) 3. WELL LOCATION: COUNTY SURRY QUADRANGLE NAME NEAMTTOwN: ELKIN 104 FABRIC LANE 28621 (SizcetlRoed Narec, Number, Commruiity, Strhdivisirm, lot No., P=cl, Zap Code) TOPOGRAPHIC I LAND SETTING- ❑ Slope ❑ Valley []Fiat ❑ Ridge ❑ Dther (Check appropriaic setting) LATITUDE May be in degrees, minutes, sewndc, or in a LONGITUDE decimal fomut LafitutitAoagitrde source: ❑ GPS ❑Topographic map (Location of well must he shown on a U5GS taps mup and areached 10 this form if not using GPS) 4a. FACILITY- The name of the business where the well is teemed. Compleir 4a and4b. (If a re odenoat well, skip 4a: compl cic 4b, wctl owner information only,] FACILITY ID #(ifapplicahle) NAMEOFFACU Y CMI - WWTP STWEETADDRESS 104 FABRIC LANE ELKIN NC 28621 Cily cr Town State Zip Cade 4K CONTACT PERSONfWELL OWNER: NAME CMI, INC S•IT= ADD RESS 4399 CORPORATE ROAD CHARLESTON. SC 20406 6. WELL DETAILS: a. Total Depth: 100.0 ft. Diameter: 4.0 in. b, Watcr Level (Below Mmsuring Point): [L- Measuring point is ft above land surface. 6 CASLNG: Length Diameter a Casing Depth (if known). N/A ft. in. b. Casing Removed: /A ft. in- 7. DISINFECTION: NIA (Amaunl of 65W75%calciurn hypochlorite used) S. SEALING MATERIAL: Nest Cement Sfnd Crmrnt Cement - 1b Cernen: — Ili - Water `- gal. Water — gal- lien to n i tr Bentonite lb - Type: 0 Slurry ❑Pellets Water pi- th Sr Typt material PORTLAND BENTONITE SLURRY Amount 75-0 GALLONS 9. EXPLAIN METIIOD OF EMPLACEMENT OF MATERIAL: VIA TREMIE PIPE WITH PORT1ANO-BENIONIIE SLURRY 10. WELL DIAGRAM. Draw a detailed sketch of the well an the back of this Form showing total depth, depth and diameter of screens (if any) remaining in the well, gravel interval, intervals of casing perforations, and depths and types of fill materials used - Ill. DATE WELL ABANDONED 4/15111 I Do HEREBY CERTIFY THAT THIS WELL WAS ABANDONED I ACCORDANCE W fr}t 1 SA NCAC 2C, WELL CONMUCT10-4 STANDARD5, AND THAT A COPY OF THIS RECO D HAS SEEN PROVIDED To THE WELL OWNER {,/A.!{Ict" 04/27/11 SSG NATURV. OFC 'IF1EDWELL.CONTRA CTOtt DATE SIGNATt1REOF PRIVATE WELL OWNER ABANDONING THE WELL DATE (The Whale well owner must be an individual who gm2tiglly-abandons hishxr residonaal well in accordance with 15A NC AC 2C-0111] JERRY WATKINS PRINTED NAME OF PERSON ABANDONING THE WELL Submit it ropy to the owner and the origiml to the Division of Water Quality within 30 days. Form GW-30 Attn: Information Management, 1617 Mail Service Center - Raleigh, NC 27699-1617, Phone No. (919) 733-7015 cat 568. Rev. 59]6 WELL ABANDONMENT RECORD Norib Carolina 1Depubnent of Fnvironment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2452 1. WELL CONTRACTOR: JERRY WATKINS _ Well Contractor (individual) Name GEOLOGIC EXPLORATION, INC. Well Contractor Company Name STREETADDRFSS 176 COMMERCE BLVD. STATESVILLE NC 28625 _ City or Towns state Zip Code 7[ 04 y- 872-7686 Area code - Phone number 2. WELL INFORMATION: SITE WELL ID # (if applicable} LW-� STATE WELL PERMIT 4 (if applicable) COUNTY WELL PER STIT 11 (if applicable) DW Q or OTHER PERMIT 0 (if applicable] WELLUSE (Cbeckapplicable use}: 0 Monitoring ❑ Resideati:sl 0 Municipal/Public ❑ ]ndustriallCommercisl Lj Agricutlural ❑ Recovery ❑ Injection ❑ Irrigation [IOther(list use) 3. WELL LOCATION: COUNTY SURRY QUADRANGLENAMI: NEARESTTOwN: ELKIN 104 FABRIC LANE 28621 (Straa/Road Name, Number, Cotnrnuruty, Sutdivism, Lot No., Parcel, Tip Code) TOPOwURAPHIC / LAM] SETTING: ❑ Slopc ❑ Valley ❑ Flat ❑ Ridge ❑ Other (Check appropriate setting) LA,TT UDE May be m degrees, minutes, aroonds, nr in a LONGITUDE decimal Format LAtitudeAongitude source: ❑ GPS ❑Topographic map (LOCation Of well marl be shown on a USG5 (CPO map and attached so this form tf not using CPS) 411. FACILITY• The name 0Fthe business where the well is Iocrted Complete 4a and4b. (lFe residendat well, skip4a: complete 4b, well owner information only.) FACILITY ID 9(ifapphrable) NAMEOFFACILiTY CMI - WW7P STREET ADDRI=SS 104 FABRIC LANE ELKIN NC City or Town Stare 4b- CONTACT PERSONIWELL OWNER: NAME CMI, INC STREET ADDRESS 4399CORPORATE RDA CHARLESTON, SC 29405 28621 Zip Code 6. WELL DETAILS; a, Total Depth: 120.0 ft, Dmmeta: 4.0 b. Water Level (Below Measuring Point): ft. Measuring poi at is ft. above land surface- & CASING: Length Diameter a. Casing Depth (iI known): NIA ft. in. b, Casing Removed- N7K— ft- in. DISINFECTION: N/A (Amount of 65% 75% calci um hypochWte used) 8. SEALING MATERIAL: Nrat Crinrnt Sand Cement Cement — lb- Cement'- Ib Water -- gal. Water -- -gill. Bentonile Bentonite lb - Type: ©Slurry ❑ Pellets Water gal. Other Type mate ial PORTLAND BENTONITE SLURRY Amount 00.0 GALLONS 9. EXPLAIN METHOD OF E.MPLACENTE14T OF MATERIAL: VIA TRFMIE_PJEE WITH POBTLAND BENTQJ]ILTE-- SWRRY_ 10. WELL DIAGRAM. Draw a detailed sketch of the well on the back of this form showing total depth, depth and diameter of screens (if any) remaining in She we) 1, gravel interval, intervals of casing perforations, and depths and types of fill materials used. 11. DATE WELL ABANDONED 4/15/11 1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE W ITI4 t 5A NCAC 2C. W ELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RE RD HAS DEEN PROVIDED TO THE WELL OWNER. �01A" , 04/27/11 SIGN AT RE OF CERTIFIED IVELL CONTRA CFOR DATE SIGNATURE OF PRIVATE WELL, OWNER ABANDONING THE WELL DATE (The private well owner must be en individual who persoaal]yabandons his/her rrsidmiial well in ■awwdartee with 15A NCAC 2C .01 13.) JERRY WATKINS PRINTED NA141E OF PERSON ABANDONING THE WELL Submit a Copy to the owner and the original to the Division of Witter Quality within 30 days. Fort GW -30 Attn: Information MAnagetoen1, 1617 Mail Service Center - Raleigh, NC 27699-1617, Phone No. (919) 733-701S exi 569. Rev. SM6 WELL ABANDON —ENT RF,CORD Borth Carolina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICAT1ION #_ 2452 1. WELL CONTRACTOR: JERRY WATKINS Well Contractor (Individual) Name _G_EOLOGIC EXPLORATION, INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE BLVD. STATESViLLE NC 28625 City or Town State Zip Code 7[ 04 ] - 872-7686 Area code - Phone number 2. WELL INFORMATION: SITE WELL III # (ifapplirable) IW-3 STATE WELL PERMIT h (if applicable) - COUNTY WELL PERMIT # (if applicable) _ 0WQ or OTHER PER KIT # (if appiicabk) WELL USE (Check applicable use) ® Monitoring ❑ Residential ❑ Muniripal/Public ❑ Industrial/Cosnmercial ❑ Agricultural ❑ Recovery ❑ Injection ❑ Irrigation ❑ Other (list use) 3. WELL LOCATION. COUNTY SURRY QUADRANGLE NAME NEAREST TOWN: _ELKIN 104 FABRIC LANE 28621 (S!jrmV toad Nsnw, Number, Community, Subdivision, Lot No., Parcel, Zip Code) TOPOGRAPHIC 1 LAND SETTING; ❑ Slope ❑ ValIey ❑ Flat ❑ Ridge ❑ Othcr (Check appropriate setting) LATM DE May be in degnem. �. nines, seconds, or in a LONGITUDE let Tam nt Latitude/tongitude source: ❑ GPS ❑Topographic map (Locotinir of well wrusi be shown an a UUSGS ropo map and arcarhed to eels fornr if not zamg GPS) 4 a. FACILITY- The name of dw bwincss where the we is located. Cornplele 4a and4b. IIFa residential well, skip 4a; camplptc 4b, well owner information only. j FACILITY tit 9(ifapplicabla) NAME OF FACILITY CM? - WWfP STREETADDRFSS 104 FABRIC LANE ELKIN NC 28621 — City or Town State Zip Code 4b. CONTACTPERSONIIVELL OWNER: NAME CMI, INC STREET ADDRESS 4319 CORPORATE ROAD CFNRLESTON, SC 29405 5. WELL DETAILS: a. Total Depth: 120.0 R Diameter: 4.0 in. b. Water Lcvci (Below Measuring Point): __ ft. Measuring point is ft. above land surface. 6. CASING: Length Diameter a. Casing Depth (if known). NIA ft. 1r1 b. Casing Removed: -IVA! ft. in. 7. DISINFECTION. NIA (Amount of 65%75%calcinm hypochlorite used) & SEALING MATERIAL: Neat Cement S■nd Cement Cement lb. Cement— III. WSW -- gal. Water gel. nt nite Bentonite lb. Type: ® Slurry ❑Pellets Water gal. her Type material PORTLAND BENTONITE SLURRY Amount 90.0 GALLONS 9. EXPLAIN METIIOD OF EMPLACEMENT OF MATERIAL: VIA TREMIE PIPE WITH P1JLA,f10.aEN15NTE_ SLURRY 10. W'ELI. DIAGRAM; Draw a detailed sketch ofthe well on the back ofthis Form showing total depth, depth and diameter of screens (if any) remaining in the well, gravel interval, intervals of casing perforations, and depths and types of fill materialsu%ed. II. DATE WELL AUkNDONED 4115111 I DO HFREBY CERTIFY THAT THIS wE.L WAS ABANDONED IN ACCORDANCE WITH 15A NCAC 2C. WELL CONSTRUCTION STANDARDS, AIVD THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE W ELL OWNER. `'""'"'� w�, 04/27/11 $IGNATI FIE OF C TIFIED WELL CONTRACTOit DATE SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE (The privy tc well owner must be m individual who W r5onIIll.l abandons hiw'her residential well in ascendance wsth ISA NCAC 2C.0113-) JERRY WATKINS FRINT£D NAME OF PERSON ABANDONING Tilt WELL. Submit it copy to the owner and the original to the Division of Water Quslity within 30 days. Form GW -30 Attn-. Inrormation Ntanagement, 1617 Mail Srrvicr Center -- Raleigh, NC 27699-I6I7, Phone No. (919) 733-7015 ext 568. Rev. 5/06 NONRESIDENTIAL WELL CONSTRUCT]ON RECORD North Carolina Department of Environment and Natural Resources- Division of Waler Quality WELL CONTRACTOR CERTIFICATION # 2452 1. WELL CONTRACTOR: JERRY WATKINS Well Contractor (Individual) Name GEOLOGIC EXPLORATION, INC Well Conlractor Company Name 176 COMMERCE BLVD Street Address STATESVILLE NC 28625 City or Town Stale Zip Code Tau_ j 872-7686 Area code Phone number 2. WELL INFORMATION: WELL CONSTRUCTION PERMIT# NIA OTHER ASSOCIATED PERMIT#(i(applicable} SITE WELL ID #(if applicable) IW-12+A 3. WELL USE (Check One Box) Monitoring W MuricipallPubiic ❑ IndustriaVComrnercial u Agricultural [:1 Recovery C] Injection 1"afionLl Other [] (list use) DATE DRILLED 04/18/11 - 04120111 4. WELL LOCATION: 104 FABRIC LANE 28621 (Stre¢; Name, Numbers. Community. SubdivWon, Lot No., Par.,el, Zip Code) CITY: ELKIN COUNTY SURRY TOPOGRAPHIC I LAND SETTING- (check appropriate box) OSlope UValley []Flat CIRidge ❑Other LATITUDE ' DMS OR DD LONGITUDE �`�' " DMS OR DO LaMudeflongitude source: BPS j _Xopographlc map (location of well must be shown on a USGS topo map andattached to this farm if not using GPS) 5. FACILITY (Name of the business where the well is located.) CMI - WWTP --- NIA _ Facility Name _. Facility ID# (if applicable) 104 FABRIC LANE Street Address LKIN NC 28621 City or Town State Zip Code CIAL INC Contact Name 4399 CORPORATE ROAD Mailing Address _ CHARLESTON SC 29405 City or Town State Zip Cade u Area code Phone number d. TOP OF CASING IS 2.5 FT. Above Land Surface' 'Top of casing terminated atfor below Sand surface may require a variance in accordance with 15A NCAC 2C .0118. e. YIELD (gpm): N/A METHOD OF TEST NIA L DISINFECTION: Type h[IA Amount NIA : g. WATER ZONES (depth): Top Bottom Top Bottom Top Bottom Top Bottom Top Bottom Top Bottom Thicknessl 7. CASING: Depth Diameter Weight Material Top 0.0 Bottom 25.0 Ft, 4 INCH. SCH 40 PVC Top 0.0 Bottom 25.0 Ft. B 1n INCH 18H GALVANIZEC Top Bottom Ff.- B. GROUT: Depth Material Method Top 0.0 Bottom 10.0 Ft. PDRtlANDBEWTONTF SLURRY Top 0.0 Bottom 25.0 Ft. PORTLANDafRTOMITE SLURRY Top Bottom Ft. 9. SCREEN: Depth Diameter Slot Size Material Top 25.0 Bottom 40.0 Ft. 4.0-in. .010 in. PVC Top 6ottflrn FL in. in. m Top BottoFt. in. in. 7 O. SANDIG RAVE L PACK: Depth Size Top 22.0 Bottom 40.0 Ft. 20-40 Tap _Bottom Ft. Top Bottom Ft. 11. DRILLING LOG Tap Bottom 0.0 1 4.0 4.0 1 9.0 9.a 1 25.0 25.0 1 310 33.0 1 38.0 38.0 1 4D.0 1 I I t Z REMARKS: Material FINE SILICA SAND Formation Description BLACK SILTY CLAY TAN SILTY CLAY PARTIALLY WEATHERED ROCK ORANGE SILT PARTIALLY WEATHERED ROCK ROCK 6. WELL DETAILS: I W HER`c By CERTIFY THAT THIS Y42=L L WAS CONSTRUCTED IN ACC ORDANCE WITH " 15A" C YELL CONSTRUCTION STANDARDS. AND THAT A COPY ❑F THIS a. TOTAL DEPTH: 40.0 FEET : RECoRD EEN PROVIDED ;o3 w z rw,04/27/11 b. DOES WELL REPLACE E?CISTSNG WELL? YESC] NOG/ : SIGNATU RE OF CERTIFIED WELL CONTRACTOR DATE C. WATER LEVEL Below Top of Casing: 15.0 FT, JERRY WATKINS (Use "}" if Above Top of Casing) : PRINTED NAME OF PERSON CONSTRUCTING THE WELL '.Slit 16 t.vi dihilb days of com letion to: Oivfs10 of Water'QUaIit Information Proress1n , Form GW-1b Y P Y - 9 Rev_ zlos 16�7Aka 0 5ef�ticeGenter, Raleigh, NC 27699-161, Phone : (919) 807-6300 NONRESIDENTIAL WELL CONSTRUCTION RECORD North Care Iina Department of EnviTonment and Natural Resources- Division of Water [duality WELL CONTRACTOR CERTIFICATION # 2452 1. WELL CONTRACTOR: = d. TOP OF CASING IS 2.5 FT. Above Land Surface' JERRY WATKINS 'Top of casing terminated a below land surface may require Well Contractor (individual) Name a variance in accordance with 15A NCAC 2C -0118. GEOLOGIC EXPLORATION, INC : a. YIELD (gpm): NIA METHOD OF TEST NIA Well Contractor Company Name : 176 COMMERCE BLVa L DISINFECTION: Type NIA Amount NIA Street Address STATESVILLE NC 28525 City or Town Slate -Lip Code t 04 } 872-7586 Area code Phone number g. WATER ZONES (depth). Top __ Bottom Top Bottom Top Bottom Top Bottom Top Bottom Top Bottom Thickness/ 2. WELL INFORMATION: : 7. CASING: Depth Diameter Weight Material WELL CONSTRUCTION PERMIT# NIA = Top 0.0 Bottom 25-0 Ft. 4 INCH SCH ap PVC OTHER ASSOCIATED PERMIT#(if appitable) Top Bottom._ Ft. _ SITE WELL ID #(if appilcabie) IW-14+ Top Bottum Ft. 3. WELL USE (Check One Boxy Monitoring N( MunirapallPublic ❑ 8. GROUT: Depth Material Method Industrial/Commercial L Agricultural ❑ Recovery Cl Injection ❑ - Top 0.0 Bottom 25.0 Ft. POffr Moexwro:+'rF SLURRY IrrigationQ OtherLi (list use) _ : Top Bottom Ft - DATE DRILLED 04115/11 - 04120111 Top Bottom-- Ft. d, WELL LOCATION; 9, SCREEN, Depth Diameter Slat Size Material 104 FABRIC LANE 28621 ; Top Bottom Ft. In, in, ISrreet Name, Numbers. Community, Subdivision, Lot No.. Parcel, Zip Code) _ Top Bottom Ft. in- in, CITY. ELKIN COUNTY SURRY Top Bottom Ft. in- in. TOPOGRAPHIC 1 LAND SETTING: (check appropriate box) [']Slope []Valley fjFlat ❑Ridge ❑Other to. SANDIGRAVEL PACK: Depth Size Material LATITUDE _ 'DMS OR DD Top Bottom Ft. LONGITUDE ' DMS OR DD Top Bcnom Ft- Laliludello%ilude source: (BPS [Topographic reap : Top Bottom Fl. (loca(ion of well must be shown on a USG topo map andattacheor to this form if not using GPS) 11. DRILLING LOG 5. FACILITY ( Jame of the business Where the we II is located-} Top Bottom Formation Desriiption CM[ - W1NTP NIA = D.0 1 4.0 BLACK SILTY CLAY Facility Name Facility ID# (if applicable) 4.0 1 9.0 TAN SILTY CLAY 104 FABRIC LANE 9.0 1 23.0 PARTIALLY WEATHERED ROCK Street Address 23.0 1 44.0 ROCK ELKIN NC 28621 1 City or Town State Zip Code J CMI 1NIC 1 Contact Name 1 4399 CORPORA IL, ROAD : 1 Mailing Address 1 CHARLE TON SC 294 1 City or Town Slate Zip Code 12. REMARKS: OPEN HOLE FROM 25.0 TO 40-Q FT Area code Phone number 6. WELL DETAILS: I DO HEREBY CERTIFY THAT 7AS WELL WAS CONSTRUCTED IN ACCORDANCE W7H • t5A NCAC 2C, WELI CONST R UCT H7N STANDARDS, AND THAT A COPY OF THIS a. TOTAL DEPTH: 40.0 FEET RECo S SEEN PRCVIOFD TO THE WELL OWNER f G. DOES WELL REPLACE EXISTING WELL? YES L] NO p/ � (A _ 04127111 SIGN URE OF C E R TiF I ED VV ELL = NTRACTOR DATE c. WATER LEVEL Below Top of Casing: 15.0 FT. JERKY WATi4NS (Use °+' If Above Top of Casing) : PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit.* n':3 thiU'days of to: Division of Water duality InfolTnatioProcessIng, term GW-16 completion - in. Rev. 2109 1617 Mali Service Center, Raleigh, NC 27699.161, Phone : (919) 607-6300 ti r� 1, WELL CONTRACTOR: BRIAN THOMAS Well Contractor (Individual) Name GEOLOGIC EXPLORATION, INC Well Contractor Company Name 176 COMMERCE BLVD Street Address STATESVILLE NC 28525 City or Town State Zip Code 70� 4 872-7686 Area code Phone number 2. WELL INFORMATION: WELL CONSTRUCTION PERMIT#. NIA OTHER ASSOCIATED PERMIT#(dappri�cable) SITE WELL ID #(ir applicable} EBMW-29 3. WELL USE (Check One Box) Monitoring d MunidpaliPublic ❑ IndustriallCommerrial C7 Agricultural ❑ Recovery L1 injection ❑ Inigabonp Other ❑ (fist use} DATE DRILLED 04/15111 4. WELL LOCATION: 104 FABRIC LANE 28621 (Steel Name, Numbers, Community, Suodivislon. Lot No., Parce'., Zip Code) CITY: ELKIN COUNTY BURRY TOPOGRAPHIC i LAND SETTING: (check appropriate box) OStope [)Valley ❑Ral [)Ridge pother LATITUDE ' OMS OR OD LONGITUDE " OM5 OR DO Latiludeliongltude source: ❑GPS Qfopographic map (location of well must be shown on a USG topo map andaftached to this form if not using GPS) S. FACILITY (Name of the business where the well Is located.} CMI - WWTP NIA Facility Name Facility ID# (if applicable) 104 FABRIC LANE Street Address ELKIN NC 28521 City or Town State Zip Code CMI INC Contact Name 43S9--CORPORATE ROAD Mailing Address CHARLESTON 5C 29405 City or Town State _ Zip Code Area code Phone number .NONRESIDENTIAL WELL CONSTRUCTION RECORD North Carolina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2581 d. TOP OF CASING IS 2.6 FT. Above Land Surface' 'Top of rasing terminated atior below land surface may require a variance in accordance with 15A NCAG 2C .011 B. C. YIELD (gpm): NIA METHOD OF TEST NIA f. DISINFECTION: Type NIA Amount NIA g. WATER ZONES (depth): Top Bottom Top Bottom Top Bottom Top Bolom Top Bottom Top Bottom Thicknessr : 7. CASING: Depth Diameter Weight Material Top 0.0 Bottom 15.0 Ft, 2 INCH $CH 40 PVC Top Bottom FIL Top Bottom FL 8. GROLrT Depth Material Method Top 0.0 Bottom 10.0 Ft. vatrrA"D6EwrowTE SLURRY : Top Bottom Fl. Top Bottom Ft. 9. SCREEN: Depth Diameter Slot Size Material Top 15.0 Bottom 25.0 Ft. 2.0 In. .010 in. PVC Tap Bottom Fl. in. in. Top Bottom Ft in. in. 10. SANDIG RAVEL PACK: Depth size Material Top 13.0 Bottom 25.0 Ft. 20-40 FINE SILICA SAND Top Bottom Ft. Top Bottom^ _ Ft_ 11. DRILLING LOG Top Bottom Formation Description 0.0 1 4.0 BLACK SILTY CLAY 4.0 1 15.0 TAN SILTY CLAY 15.0 ! 25.0 PARTIALLY WEATHERED ROCK 1 1 1 1 r 1 r 12. REMARKS: RENTONITE SEAL FROM 10.0 TO 6, WELL DETAILS; :I DO HERCRY CERTIFY THAT THIS WELL WAS CONSTRUCTED rN ACCORDANCE WITH • 7 WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS a. TOTAL DEPTH: 25.0 FEET CORD I ££N PROVIDED TO THE HER. // b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO V Q4127I11 SIGNATURE O TIF D WELL CONTRA OR DATE c. WATER LEVEL Below Top of Casing: 18.0 FT. BRIAN THOMAS (Use'+" if Above Top of Casing) : PRINTED NAME OF PERSON CONSTRUCTING THE WELL Form GW-tb Submit withl"n"30 days of completion to: Division of Water Duality - Information Processing, Rev. 2109 1617 Mail Service Center, Raleigh, NC 27699.161, Phone : (919) 807-6300 1 ■ ONl►E.SIDENTIAL WELL CONSTRUCTION RECORD Earth Carolina Department of Environment and Natural Resources- Division of Water Quality .a,, �• WELL CONTRACTOR CERTIFICATION tl 2551 I. WELL CONTRACTOR BRIAN THOMAS Well Contractor (Individual) Name GEOLOGIC EXPLORATION, INC Well Contractor Company Name 176 COMMERCE BLVD Street Address STATESVILLE NC 28625 City or Town State Zip Code To[ 4 872-7686 Area code Phone number 2. WELL INFORMATION: WELL CONSTRUCTION PERMIT# NIA OTHER ASSOCIATED PERMIT#(it applicable) SITE WELL ID #(if applicable) EBMW-30 3. WELL USE (Check One Box) Monitoring W Municipal/Public ❑ IndustriallCommercial ❑ Agricultural ❑ Recovery I7 Injection ❑ Irrtgationn Other p (list use) DATE DRILLED] 0411 S111 4. WELL LOCATION: 104 FABRIC LANE 28621 {Street Name, Numbers, Community, Subdivision, Lot No„ Pane], Zip Code) CITy: ELKIN COUNTY SURRY TOPOGRAPHIC 1 LAND SETTING: (check appropriate box) n Slope [:]Valley ❑ Flat Q Ridge []Other LATITUDE " ❑MS OR DO LONGITUDE A"� " DMS OR ❑O Latitudeflongitude source: BPS aopographlc map (locaf on of well must be shown on a USGS topo map andettached to this form if not using GPS) 5. FACILITY (Name of the business where the well is located.) CMI - WWTP NIA Facility Name Facility ID# (if applicable) 104 FABRIC LANE Street Address ELKIN NC 28621 City or Town State Zip Code Contact Name 43CORPORATE ROAQ Mailing Address CHA LEST N SC 294D5 City or Town State Zip Code Area code Phone number & WELL DETAILS; a. TOTAL DEPTH: 22.0 FEET b. DOES WELL REPLACE EXISTING WELL? YES C NO d d. TOP OF CASING IS 2.5 FT. Above Land Surface' 'Top of casing terminated atlor below land surface may require a variance in accordance Wth 15A NCAC 2C .0118. e. YIELD (gpm): NIA METHOD OF TEST NIA f. DISINFECTION: Type NIA Amount NIA g. WATER ZONES (depth): Top Bottom Top Bottom Top Bottom Top Bottom : Top Bottom Top Bottom Thicknessl : 7, CASING: Depth Diameter Weight Material Top 0-0 Bottom 12.0 Ft. 2 INCH SCH 40 PVC Top Bottom Fl. : Top Bottom Ft GROUT: Depth Material Method Top D.0 Bottom TO Ft. PO�iIANDVE"To" Tr SLURRY Top Bottom Ft. Top Bottom Ft. 9. SCREEN: Depth Diameter Slot Size Material Top 12.0 Bottom�22.0 Ft. 2.0 In. .010 in. PVC Top Bottom Ft. In. in. : Top Bottom Ft- in- in, 10. SANDIGRAVEL PACK: Depth Size Material : Top 10.0 Bottom 22.0 Ft. 20-40 FINE SILICA SAND Top Bottom Ft. : Top Bottom Ft. 11- DRILLING LOG Top Bottom 0.0 1 4.0 4.0 1 9.0 9-0 1 22.0 12. REMARKS: Formation Description BLACK SILTY CLAY TAN SILTY CLAY PARTIALLY WEATHERED ROCK I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRLICTE D IN ACCORDANCE W1TK ,,-ti 5r3K2C, WELL CONSTRUCTiON STANDARDS, AND THAT A COPY OF THIS RC HAS SEEN PROVIDED TO L OWNER. 04/27/11 SIGNATURE F CEF�TiFIED WELL CONTF:A TOR DATE c. WATER LEVEL Below Top of Casing: 16.0 FT. BRIAN THOMAS {Llse '*' it Above Top of Casing] : PRINTED NAME OF PERSON CONSTRUCTING THE WELL Farm GW-Ih Submit Within 30'days of cvmpietion to: Division of Water quality - Inrormattoh Proc*"Ing, Rev. 2109 1617 Mail Service Center, Raleigh, INC 27699-161, Phvne'.(919),807-G300 fd �i STA3rV �=. NONRESIDENTIAL WELL CONSTRUCTION RECORD North Carolina Departriwal of Environment and Natural Resources- Division of Water Quajity WELL CONTRACTOR CERTIFICATION €k 2581 1. WELL CONTRACTOR: BRIAN THOMAS Weil Contractor (individual) Name GEOLOGIC EXPLORATION, INC Well Contractor Company Name 176 COMMERCE BLVD Street Address STATESVILLE NC 28625 City or Town State Zip Code 70[ 4 872-7686 Area code Phone number SCANNED d. TOP OF CASING IS 2.5 FT. Above Land Surface' 'Top of casing lerminated atlor below land surface may require a variance in accordance with 15A NCAC 2C -011 B. e. YIELD (gpm): NIA METHOD OF TEST NIA f. DISINFECTION: Type NIA Amount NIA g- WATER ZONES (depth): Tnp Bottom Top Bottom Top Bottom Top Bottom Top Bottom Top Bottom 2. WELL INFORMATION: : 7. CASING: Depth Diameter WELL CONSTRUCTION PERMIT# NIA : Top 0.0 Bottom 8-0 Ft. 2 INCH OTHER ASSOCIATED PERMITA(ifapplicaue) : Top Bottom Ft. SITE WELL ID #CeappilreWe) EBMW-31 : Top Bottom Ft. Thicknessr Weight Material SCH 40 PVC 3. WELL USE (Check One Box) Monitoring 5( MunicipattPublic ❑ : B. GROUT: Depth Material Method IndustriallCommerciai ❑ Agricultural ❑ Recovery ❑ Injection ❑ Top 0.0 Bottom 3-0 FL PORTLP06f"TwTE SLURRY IrTigation❑ Other,::) (list usel Top Bottom Ft. DATE DRILLED 041151i 1 : Top Bottom Ft. 4. WELL LOCATION: 104 FABRIC LANE 28621 (Street Narna, Numbers, Community, SVb<jlvision, Lot No-, Parml, Zip Code) CITY: ELKIN COUNTY SURRY TOPOGRAPHIC 1 LAND SETTING: (check appropriate box) ❑Slope QVellev ❑Flat ❑Ridge ❑Other LATITUDE _°`' " DMS OR DD LONGITUDE ' DMS OR DD Latitudellongitude source: MPS Qfopographic map (location of well must be shown on a USG5 topo map andattached to this form if not using GPS) 5. FACILITY (Name Wthe business where the well is located.) CMI - WWTP NIA Facility Name Facility D# (if applicable) 104 FABRIC LANE Street Address ELKIN NC 2B621 City or Town State Zip Code CMi IN Contact Name 4399 CORPORATE RA Mailing Address CHASLESTON SC 2945 _ City or Town _ State Zip Code Area code Phone number 6. WELL DETAILS: a. TOTAL DEPTH; 18.0 FEET b. DOES WELL REPLACE EXISTING WELL? YES ❑ NO IGV : 9. SCREEN: Depth Diameter Top 8,0 Botforn 18.0 Ft. 2.0 in. Top Bottom Ft. in. Tap Bottom Ft. in. 10. SANDIGRAVEL PACK: Depth Size Top 6.0 Bottom 18.0 Ft. 20-40 Top Bottom Ft. Top Bottom Fl. 11- DRILLING LOG Top 0.0 4.0 1 1 Bottom 4.0 13.0 13.0 1 1&0 I I 1 1 1 I 1 Slot Size Material .010 in. PVC tn. in. Material FINE SILICA SAND Formation Description BLACK SILTY CLAY TAN SILTY CLAY PARTIALLY WEATHERED ROCK 12. REMARKS: BENTONITE �jEAL FROM 3.0 TO 6 0 FEET I Od HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED 10ACCORDANCE WITH VHELL CONSTRUCTION STANWDS, AND THAT A COPY OF THIS rpplq BEEN PROVIDED TO THE ER. ^ _.� 04/27111 SIGNATLIRc D RTlrED WEEL COP) DATE C. WATER LEVEL Below Top of Casing: 13.0 FT. BRIAN THOMAS (Use'+" if Above Top of Casing] : PRINTED NAME OF PERSON CONSTRUCTING THE WELL Form GW-1a sdIatnitwitfiin 34 days ietion to: i]ivision.of Water• uali InForrnation:Pracessing, 1Y ' Rev. 2ra9 ql4 C 27699.151, PhonO = -esr Swtp ff � i. WELL CONTRACTOR: BRIAN THOMAS NONRESIDENTIAL WELL CONSi•RUMON RECORD North Carolina Department of Environment and Natural Resources- Division of Water Quali:7 WELL CONTIRACFOR CERTIFICA'I'IOiN # 2581 Well Contractor (Individual) Name GEOLOGIC EXPLORATION, INC Well Contractor Company Name 176 COMMERCE BLVD Street Address STATESVILLE NC 28625 City or Town Slate Zip Code 70� 4 a 872-7686 Area code Phone number 2. WELL INFORMATION: WELL CONSTRUCTION PERMIT* NIA OTHER ASSOCIATED PERMITS(if applicable) SITE WELL lD #{f appl;cabIa) EBMW-32 3. WELL USE (Check One Box) Monitoring d Municipal/Public C7 IndustriallCommercial ❑ Agricaiitural ❑ Recovery p Injection ❑ Irrigation❑ Other L} (list use) DATE DRILLED 04115M 1 4. WELL LOCATION: 104 FABRIC LANE 28621 (Street Name, Numbers, Commurvty, Subdivision, Lot No. Parcel, Zip Code) CITY: ELKIN COUNTY SURRY TOPOGRAPHIC 1 LAND SETTING: (check aparopnate box) ZlSlope ❑Valley 0Flat ❑Ridge CjOther LATITUDE �'� ' DMS OR DID LONGITUDE �' ` DMS OR DD Lalitudefloogitude source: [BPS UopographiC map (location of welt must be shown on a USGS tope map andattached to this form if not using GPS) 5. FACILITY (Name of the business where Itw well is located.} CM - WIN P NIA Facility Name Facility )D* (if applicable) 104 FABRIC LAN Street Address ELKIN NC 28621 City or Town State Zip Cade CMI INC Contact Name 4399 CORPORATE ROAD Mailing Address _ CHARLESTON SC 2940 City or Town State Zip Code Area code Phone number d. TOP OF CASING IS 2.5 FT. Above Land Surface' 'Top of casing terminated atlor below land surface may require a variance in accordance with 15A NCAC 2C .011S. e. YIELD (gpm): NIA METHOD OF TEST NIA f. DJSINFECTION:Type NIAAmount NIA g. WATER ZONES (depth): Top Bottom Top Bottom Top Bottom Top Bottom Top Bottom Top Bottom Thlcicriv%si 7, CASING: Depth Diameter Weight Material Top 0.0 Bottom_ 10.0 FL 2 INCH SCH 40 PVC Top Bottom Ft. Top Bottom Ft. 6. GROUT: Depth Material Method Top 0.0 Bottom 5.0 Ft, ten- l o -%TON- SLURRY Tap Bottom Ft, Top Bottom Ft. 9. SCREEN: Depth Diameter Slot Size Material Top 10.0 Bottom 20.0 Ft. 2,0 In. 010 in, PVC : Top Bottom Ft. In. _ in. Top Bottom Ft. in. in. 10. SANDIGRAVEL PACK: Depth size Top 8,0 Bottom 20.0 Ft. 20-40 Top Bottom Ft. Top Bottom Ft. 11. DRILLING LOG Top Bottom 0.0 1 4.0 4.0 i 11.0 11.0 1 20.0 1 1 1 1 1 12. REMARKS: —BLNTONITE,^1,EAL FF _ Material FINE SILICA SAND Formation Descriplion 81ACK SILTY CLAY TAN SILTY CLAY PARTIALLY WEATHERED ROCK 6. WELL DETAILS: ' I p0 H E R EBY CE RTI FY THAT THIS WELL WAS CONSTRLICTE4fNACCORDANCE WITH 2C. WELL CON57RL1CT1pN ST ROS, ANp THAT A COPY OF THIS a, TOTAL DEPTH: 20.0 FEET 5 Bpi �PROVIOEO TO F L pWNER. �.,r ate,_ 04/27/11 b. DOES WELL REPLACE EXISTING WELL? YE5{7 NOW : SIGNATURE dFCERTIFiEQ WELL CONTRAC QR DATE c. WATER LEVEL Below Top of Casing: 14.0 FT. BRIAN THOMAS (Use'+" if Above Top of Casing) 'PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit within 30 days of comp Ietion to: Division of Water Quality tnfarrnatfon Pracvsvn Form GW-1b Y P ". , 9 Rev. 2109 1617 Mail Service Center, Raleigh, NC 27699-161, Phone : (919) B07-6300 NCDENR - Remedial Construction Completion Report MACTEC Project 6628-08-4691 July 20, 2011 NOMCDOOV IO97 APPENDIX C GROUNDWATER SAMPLING DATA SHEETS FOR PRE -INJECTION SAMPLING AVMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-08-4691_ MONITORING WELL NUMBER EBMW-5 SITE NAME CM] WWTP DATE 51I6111 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag I drillers log -- circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (I>GW) IZ50 LENGTH OF WATER COLUMN (LWC) = TWD — DGW — CASING DIAMETER IN. ONE STANDING WELL VOLUME = gal, (NOTE %:" = 0.0102G/Fi': %" = 0.023 GIFT. 1 "= 0.041 G/FT: 2" = 0.163 GIFT: 4" = 0.653 G/FT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: WELL TYPE: FLUSH MOUNT I ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL GAL. YES NO X YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH COMMENTS In-wcll ter readin s Time Volume PH Cond. (A/cm) Turbidity (NTU) Dis.O= (mglL) Ternp CC) OR.P (Mv) Notes `-- 6.48 0.943 5.4 4.36 14.32 -18 Horiba U-22 JVMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSIIEET MACTEC PROJECT NUMBER 6228-08-069I MONITORING WELL NUMBER EBMW-7 SITE NAM>; CMi WWTP DATE 511611 l TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH OFWD) FT. (measured f well tag 1 drillers log — ruck one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (I?GW) _ 11.76 LENGTH OF WATER COLUMN (LWC) = TWD — DGW — CASING DIAMETER IN. ONE STANDING WELL VOLUME= al. (NOTE `h" = 0.0102GII'T: %" = 0.023 GIFT: 17= 0.041GfFT: 2" = 0.163 GfFT: 4"= 0.653 GIFT: 6" = 1.46 GfFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER f PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: WELT, TYPE: FLUSH MOUNT/ ABOVE GRADE GAL. LOCKING CAP YES X NO PROTECTIVE POSTIABUTMENT YES NO x NONPOTABLE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH COMMENTS In -well water quality reading Time Volume PH(1&cm) Cond. Turbidity (NTU) Dis.02 (mglL) Temp CC) ORP (mV) Notes — 5.12 0.171 463 2.99 13.01 223 Horiba U-22 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6229-084691 _ _ _ MONITORING WELL NUMBER EBMW-8 SITE NAME CMI WWTP DATE 5/16/11 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag 1 drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 12,56 _ LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = gal. (NOTE 'h" = 0.0102GIFT: 3/+" = 0.023 GIFT: I "= 0.041 GIFT: 2" = 4.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER / PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE. FLUSH MOUNT 1 ABOVE GRADE COMMENTS In -well water quality readings LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL ID PLATE WELL INTEGRITY SATISFACTORY YES NO x YES X NO YES X NO YES X NO WELL YIELD LOW MODERATE HIGH Time Volume pH Cond, (p&cm) Turbidity (NTU) Dis.O2 (mglL) Temp (°C) ORP (mV) Notes -- 6.14 0.518 39.3 5.0 13.96 184 Horiba U-22 AMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-08A691 _ MONITORING WELL NUMBER EBMW-10 SITENAME CMI WWTP DATE, 511611I TIME OF SAMPLE FIELD PERSONNEL Mike Flank WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag 1 drillers log -- circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTI-I TOC DEPTH TO GROUNDWATER (DGW) 12.85 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = dal. (NOTE %z" = 0.0102GIFT: %" = 0.023 GIFT: 1 "= 0.041 GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1 A6 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER I PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVER: GAL. WELL TYPE: FLUSH MOUNT / ABOVE GRADE COMMENTS , In-well_water_quality readings LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NON -POTABLE LABEL ID PLATE WELL INTEGRITY SATISFACTORY YES NO x YES X NO YES X NO YES X NO WELL. YIELD LOW MODERATE HIGH Time Volume pH Cond. (F&cm) Turbidity (NTU) Dis.02 (mW) Temp (°C) ORP (mV) Motes -- 6.52 0,322 5.5 4.75 13.79 166 Horiba U-22 AVMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6 -08-4 91 MONITORING WELL NUMBER EBMW-11 SITE NAME CMI WWTP DATE 5116II I TIME OF SAMPLE FIELD PERSONNEL Mice Flak _ WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag I drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DOW) 11,77 LENGTH OF WATER COLUMN (LWC) - TWD- DGW = CASING DIAMETER ONE STANDING WELL VOLUME = ��aL (NOTE''/"= 0.0102GIFT: %: = 0.023 GIFT: 1"= 0.041G/FT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: WELL TYPE: FLUSH MOUNT J ABOVE GMQE LOCKING CAP YES X NO PROTECTIVE POSTIABU"TMENT NONPOTABLE LABEL GAL. YES NO X YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES _XNO WELL YIELD LOW MODERATE HIGH COMMENTS In-w ll water uaI' readings Time Volume pH Cond. (01cm) Turbidity (NTLJ) Dis.O1 (mWL) Temp (°C) DRP I (mV) Notes -- 6.04 0.101 62.6 4.72 13.33 220 Horiba U-22 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-084691 MONITORING WELL NUMBER EBMW-12 SITE NAME CID WWTP DATE 5I16111 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDTFIONS TOTAL WELL DEPTH (TWD) I T. (measured I well tag 1 drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 18.73 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = at. (NO'T'E'/2" = 0.0102G/FT: Ye" = 0.023 GIFT: 1"= 0.041GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL, EVACUATION: BAILER 1 PUMP / OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL, WELL TYPE: FLUSH MOUNT 1 ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO X NONPOTABLE LABEL ID PLATE YES X NO YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH COMMENTS In -well water quality readin s Time Volume PH Cond. (pSJcm) Turbidity (NTU) Dis. Us (mg/L) Temp (°C) ORP (rnY) Notes -- 5.22 0.357 17.9 3.86 14.83 233 Horiba U-22 4VMACTEC MACTEC ENGHgEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-OSA691 MONITORING WELL NUMBER �HM -13 SITE NAME CMI WWTP DATE 5116111 TIME OF SAMPLE FIELD PERSONNEL Mike Flank WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag 1 drillers lag — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH. TOC DEPTH TO GROUNDWATER (DGW) 16.8 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = gal. (NOTE 14" = 0.0 IO2GIFT: %" = 0.023 G1FF: I"= 0.041 GIFT: 2" = 0.163 GIFT: 4" � 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION FIVE STANDING WELL VOLUMES = BAILER I PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL, WELL TYPE: FLUSH MOUNT 1 ABOVE GRADE COMMENTS In -well water quality readings LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LA13EL ID PLATE YES NO X YES X NO - YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH Time Volume pH Coed. Turbidity (NTU) Dis. ❑t (mg/L) Temp (C) ORP (mV) Notes40cm) `--past No measurements. Horiba cannot get 10' in well AMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228 S-4 91 MONITORING WELL NUMBER EBMW-14 SITENAME QbM WWTP DATE 5116111 TIME OF SAMPLE FIELD PERSONNEL Mike F aWk WEATHER CONDITIONS TOTAL WELL DEPTH MVD) FT. (measured / well tag 1 drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) i 14.67 - -- LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER ONE STANDING WELL VOLUME = dal. (NOTE h" = 0.0102G/FT: N" = 0.023 GIFT: 1 "= 0.041 GIFT: 2" = 0.163 G/FT: 4" = 0.653 GIFT: 6" - i .46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT 1 ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POSTIABUTMENT YES NO X NONPOTABLE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH COMMENTS In -well water quality readings Time Volume PH Cond. (µSlcm) Turbidity (NTU) Dis.O1 (mg/L) Temp (°C) ORP (MV) Notes `-- 4.69 0.439 8.8 5.57 12.70 287 Horiba U-22 AVMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 622808A691 _ MONITORING WELL NUMBER EBMW-15 SITE NAME CMI WWTP DATE Il 1 1 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH CTWD) FE (measured 1 well tag 1 drillers fog — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC ' Y DEPTH TO GROUNDWATER (DGW) 14.15 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME _ dal. (NOTE %," = 0.0102GIFT: X" = 0.023 G/FT: 1 "= 0.041 GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1 A6 G/FT) THREE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: FIVE STANDING WELL VOLUMES = BAILER 1 PUMP 1 OTHER: TOTAL VOLUME OF WATER REMOVED: WELL TYPE: FLUSH MOUNT 1 ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POSTIABUTMENI NONPOTABLE LABEL ID PLATE GAL. YES NO x YES X NO YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH TYPE COMMENTS In -well water quality readings Time Volume PR Cond. (µ51cm) Turbidity (NTU) Dis.O2 (mg/L) Temp CC) ORP (mV) Notes — 5.84 0.224 15.5 2.88 14.26 216 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORK.SHEET MACTEC PROJECT NUMBER 622MB-4691 MONITORING WELL NUMBER EBMW-! 6 T SITE NAME _ CMI WW`TP DATE_ 511611 l TIME OF SAMPLE FIELD PERSONNEL Mile Fla ik _ WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) _-_Tr. (measured / well tag 1 driflers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 12.35 LENGTH OF WATER COLUMN (LWQ = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = dal. (NOTE 'W' = 0.0 I42G/FT: 1/4" = 0.023 GIFT: 1 "= O.D4 I G/FT: 2" = 0.163 G/Fi": 4" = 0.653 GIFT: 6" = 1.46 G/F I") THREE STANDING WET I. VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP / OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT I ABOVE GRADE COMMENTS In --well water quality readings LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL YES NO x YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH Time Volume PA Cond. (Pglcm) Turbidity (NTU) Dis.O2 (mg/L) Temp CC) ORP (mom Notes `— 4.83 0.113 204 3.29 14.12 261 Horiba U-22 AVMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-08A691 MONITORING WELL NUMBER EBMW-18 SITE NAME CMI WWTP DATE 5/16/11 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured I well tag I drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 11.97 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = _gal. (NOTE '/a" = 0.0102GIFT: '/," = 0.023 GIFT: 1 "= 0.041 GIFT: 2" _ 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FTVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: 13AILER I PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT/ ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO X NONPOTABLE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH COMMENTS In -well wat uali readin Time Volume PR Cond. (µ.Slcm) Turbidity (NTU) Dis. Ux (mglL) Temp CC) ORP (mom Notes -- 6.83 L57 7.8 3.11 14 -11 Hariba U-22 AMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-OR-4691 MONITORING WELL NUMBER EBMW-19 SITE NAME ClV1I WWTP DATE 5116111 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik _ WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag i drillers log -- circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 18.61 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = a1. (NOTE %" = 0.0102GIFT: Y44" = 0.023 GIFT: 1 "= 0.041 GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT.- 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER i PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT I ABOVE GRADE COMMENTS In -well water quality readings LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL ID PLATE WELL INTEGRITY SATISFACTORY YES NO X YES X NO YES X NO YES X NO WELL YIELD LOW MODERATE HIGH Time Volume PH Cond. (µSlcm) Turbidity (NTM Dis.Ox (mg'L) Temp CC) ❑RP (mv) Notes -- 6.75 0.397 5.4 8.67 15.30 145 Horiba U-22 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-08-4691 _ _ MONITORING WELL NUMBER EBMW-21 SITE NAME CMI WWTP DATE 5116I11 TIME OF SAMPLE FIELD PERSONNEL _ Mike Flani c _- -- WEATHER CONDITIONS TOTAL WELL DEPTH (I'WD) FT. (measured I well tag I drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 15.44 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = dal. (NOTE %x" = 0.01020/FT: 3A" = 0.023 GIFT: 1 "= 0.041GIFT: 2" = 0.163 G/FT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT 1 A13OVE GRADE COMMENTS In -well water quality readings LOCKING CAP YES X NO PROTECTIVE POSTIABUTMENT YES NO X NONPOTABLE LABEL YES X NO IDPLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL. YIELD LOW MODERATE HIGH Time Volume PH Cond. (µ5lcrn) Turbidity (NTU) Dis.O2 (mg/L) Temp CC) ORP (mV) Notes `-- 7.27 0.316 5.4 6.79 13.49 129 Horiba U-22 JrMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACI"EC PROJECT NUMBER 6228-084691 MONITORING WELL NUMBER _ EBMW-22 SITENAME CMI WWTP DATE 5116/11 TIME OF SAMPLE FIELD PERSONNEL Mike Elanik WEATHER CONDITIONS TOTAL WELL DEPTH (i VD) FT. (measured I well tag 1 drillers log -- circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH C DEPTH TO GROUNDWATER (DGW) 11.24 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER 1N, ONE STANDING WELL VOLUME = gal. (NOTE W' = 0.0102G1FT: 11/."= 0.023 GIFT: 1"= 0.041GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES METHOD OF WELL EVACUATION: BAILER I PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT/ ABOVE QRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO X NONPOTAB LE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH COMMENTS In -well walter.quality readin s Time Volume PH Land. 01Slcm) Turbidity (NTL) Dis.OZ (mglL) Temp (°C) ORP (mV) Notes `-- 8.33 0.462 5.6 7.41 13.68 -49 Horiba U-22 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228:Q8-4691 MONITORING WELL NUMBER EBMW-29 SITENAME CMI WWTP DATE 515111 TIME OF SAMPLER 11.00 FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) 27 40 FT. measured / well tag / drillers log — circIe one) SCREENED INTERVAL MEASURING POINT FOR DEPTH, -T C DEPTH TO GROUNDWATER (DGW) 18.48 _ _ _ LENGTH OF WATER COLUMN (LWC) = TWD — DGW = 8,92 CASING DIAMFTER ONE STANDING WELL VOLUME = _— 1,45 seal. (NOTE IA" = 0.0102GIFP: N" = 0.023 GIFT: 1" = 0.041GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = 4.36 FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: 4.36 GAL. WELL TYPE: FLUSH MOUNT 1 ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL YES NO x YES X NO ID PLATE YES x NO WELL 1NTEGRi71Y SATISFACTORY YES x NO WELL YIELD LOW MODERATE x HIGH COMMENTS Time Volume pH Cond. (IiSlcm) Turbidity (NTU) Dis.O1 (m) (mom) Temp f C) ORP (jnV) Notes 1 4.97 0.484 191 5.94 15.22 371 Horiha U-22 2 5.17 0.467 162 4.45 15.13 325 3 5.32 0.459 360 3.86 15.12 283 OMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 622MS-4691 MONITORING WELL NUMBER ERMW-30 SITE NAME CMI WWTP DATE 5I5111 TIME OF SAMPLE 11:20 FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) 25.00 FT. measured I well tag 1 drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 2Q,77 LENGTH OF WATER COLUMN (LWC) = TWD — DG W = 4.23 CASING DI.A.METER 2 IN. ONE STANDING WELL VOLUME _ 0.68 al. (NOTE '%" = 0.0102G/FT: 'I," = 0.023 GIFT: I 0.041 GIFT: 2" = 0.163 G/FT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = 2.07 FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER I PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: 2.07 GAL. WELL TYPE: FLUSH MOUNT 1 ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO X NONPOTABLE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE X HIGH 16I016TlUVIAZIO Time Volume pH Cond. Wcmj Turbidity (NM Dis.O2 (M?)L) Temp (CC) ORP (MV) Notes 1 5.87 0.659 564 3.83 14.63 81 Horiba U-22 2 5.85 0.712 674 3.53 14.65 84 3 5.92 0.720 521 3.12 14.68 57 AMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSIIEET MACTEC PROJECT NUMBER 6228-08-4691 MONITORING WELL NUMBER ERMW-31 SITE NAME _CM WWTP DATE 5I ! 1 TIME OF SAMPLE 11:50 FIELD PERSONNEL Mike Flanik WEATHER CONDTTIONS TOTAL WELL DEPTH (TWD) 20.13 FT. (�� I well tag I drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 14.88 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = 5.25 CASING DIAMETER 2 IN. ONE STANDING WELL VOLUME = 0.86 eat. (NOTE `h" = 0.0102GIFT: V4" = 0.023 GIFT: 1"= O.Q4IGIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 G/F ) THREE STANDING WELL VOLUMES = 2.57 FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER I PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: 2J7 _ __ _ GAL. WELL TYPE: FLUSH MOUNT I ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO X NONPOTABLE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE X HIGH COMMENTS Time Volume pH Cond. (µSlcm) Turbidity (NTU) Dis. Di (mg L) Temp OC) ORP (mv) motes 1 5.36 0.242 220 6.04 13.12 196 Horiba U-22 2 4.88 0.215 343 5.66 13.04 234 3 4.66 0.311 420 4.84 13.13 260 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROTECT NUMBER 6228-084691 MONITORING WELL NUMBER EBMW-32 SITE NAME WWTP DATE 515/11 TIME OF SAMPLE �12:20 FIELD PERSONNEL Mike FlanA -- WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) 22.05 FT. measured 1 well tag I drillers log -- circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) I4.07 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = 7.98 CASING DIAMETER 2 IN. ONE STANDING WELL VOLUME = 1.3 gal. (NOTE!/2" = 0.0102GIFT: Y4" = 0.023 GIFT: I "= 0.041 GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = 3.9 FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER i PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: 3.9 GAL. WELL TYPE: FLUSH MOUNT i ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POSTIABUTMENT YES NO X NONPOTABLE LABEL YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE X HIGH COMMENTS Time Volume pH Cond. (µSlcm) Turbidity (NTM Dis.02 (mglL) Temp CC) ORP (mV) Motes 1 4.80 0.389 608 6.13 12.82 298 Horiba U-22 2 4.69 0.480 830 5.12 12.88 313 3 4.69 0.514 --- 5.15 12.90 315 4VMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-084691 MONITORING WELL NUMBER IW-12+A SITE NAME CMI WWTP DATE 5116111 TIME OF SAMPLE FIELD PERSONNEL. Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured / well tag 1 drillers log - circle one) SCREENED INTERVAL MEASURING POW I' FOR DEPTH DEPTH TO GROUNDWATER (DGW) 17.92 LENGTH OF WATER COLUMN (LWC) = TWD - DGW W CA -SING DIAMETER LIV. ONE STANDING WELL VOLUME _ gal. (NOTE %" = 0.0102GIFT: 3G" = 0.023 G11=T: i"= 0.041GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES - FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER 1 PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT/ ABOVE GRADE LOCKING CAP PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL ID PLATE WELL 1NTEGRITY SATISFACTORY COMM[ENTS In -well water quality readings YES X NO YES NO x YES X NO YES X NO YES X NO WELL YIELD LOW _MODERATE HIGH Time Volume PA Coad. (01cm) Turbidity (NTU) Dis.O1 (mglL) Temp (°C) ORP (mV) Notes `-- 5.72 0.423 8.5 3.41 15.33 93 Horiba U-22 A MACTEC N ACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228&8-4691 MONITORING WELL NUMBER IW-14+ SITE NAME CMI WWTP DATE 511 fill 1 TIME OF SAMPLE FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH 9WD) FT. (measured i well tag I drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 15.01 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = CASING DIAMETER IN. ONE STANDING WELL VOLUME = al. (NOTE h" = 0.0102GIFT: N" = 0.023 GIFT: 1"= 0.041GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: SAILER I PUMP I OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FLUSH MOUNT I ABOVE GRADE COMMENTS In -well water quality readings LACKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO x NONPOTA13LE LABEL YES --ANO iD PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH Time Volume pR Cond. (µSlcm) Turbidity (NTU) Dis.O1 (m1;fL) Temp CC) ORP (mV) Notes `- 6.77 2.17 6.1 3.76 14.15 101 Horiba U-22 AVMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 2 -08-4 91 MONITORING WELL NUMBER FAMW-1 SITE NAME CMI WWTP DATE 511611 i TIME OF SAMPLE FIELD PERSONNEL Mik-HoA __ WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) FT. (measured 1 well tag 1 drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 14,29 LENGTH OF WATER COLUMN (LWC) = TWD—DGW = CASING DIAMETER IN. ONE STANDING WELL. VOLUME _ dal. (NOTE 'li" = 0.0102GIFT: 'I." = 0.023 GIFT: 1 "= 0.041 GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER / PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: GAL. WELL TYPE: FI..USH MOUNT / ABOVE GRAPE COMMENTS In -well water quality readines LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL YES NO X YES X NO ID PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE HIGH Time Volume PA Cond. (0/cm) Turbidity (NTU) DIs.O2 (m91L) Temp CC) ORP (mV) Notes — 5.77 0.156 535 6.67 14.37 207 Horiba U-22 4rMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-08A691 MONITORING WELL NUMBER EBMW-10 SITE NAME WWTP DATE 411VI I TIME OF SAMPLE 15:00 FIELD PERSONNEL Mike Flanik WEATHER CONDITIONS TOTAL WELL DEPTH FWD) 55.34 FT.(measured / well tag / drillers log — circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 12.14 LENGTH OF WATER COLUMN (LWC) = TWD — DGW = 43.20 CASING DIAMETER 2 IN. ONE STANDING WELL VOLUME = 28.2 gal. (NOTE 'IN' = 0.0102GIFT: '/." � 0.023 G/F T: I"= 0.04I GIFT: 2" - 0.163 GIFT: 4" - 0.653 GIFT: 6" = 1.46 GIFT) THREE STANDING WELL VOLUMES = 84.6 FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER/ PUMP 1 OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: 28.2 GAL. WELL TYPE: FLUSH MOUNT/ ABOVE GRADE LOCKING CAP YES X NO PROTECTIVE POST/ABUTMENT YES NO X NONPOTABLE LABEL YES —,X—NO I D PLATE YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE X HIGH COMMENTS Time Volume PH Cand• (µStem) Turbidity (NTU) Dis.02 (mg/L) Temp cc) OItP (mV) Notes 0.33 7.36 0.302 44.4 3.72 15.17 64 0.66 7.22 0.278 48.4 2.69 14.36 69 l 7.11 0.281 48.7 3.10 14.30 71 4tMACTEC MACTEC ENGINEERING AND CONSULTING, INC. MONITORING WELL SAMPLING FIELD DATA WORKSHEET MACTEC PROJECT NUMBER 6228-08-4691 MONITORING WELL NUMBER EBMW-k 8 SITE NAME CMI WWTP DATE 4118111 TIME OF SAMPLE 14:00 FIELD PERSONNEL Mike Flani.k WEATHER CONDITIONS TOTAL WELL DEPTH (TWD) 79.7 FT.(measured / well tag/drillers log— circle one) SCREENED INTERVAL MEASURING POINT FOR DEPTH TOC DEPTH TO GROUNDWATER (DGW) 11.43 LENGTH OF WATER COLUMN (LWC) = TWD — DG W = 0-27 CASING DIAMETER 2 IN. ONE STANDING WELL VOLUME = 11.12 pal. (NOTE 'h" = 0.0102GIFT: %" = 0.023 GIFT: I "= 0.041 GIFT: 2" = 0.163 GIFT: 4" = 0.653 GIFT: 6" � 1.46 G/FI) THREE STANDING WELL VOLUMES = 33.36 FIVE STANDING WELL VOLUMES = METHOD OF WELL EVACUATION: BAILER / PUMP / OTHER: TYPE TOTAL VOLUME OF WATER REMOVED: 33.5 GAL, WELL TYPE: FLUSH MOUNT/ ABOVE GRADE LOCKING CAP PROTECTIVE POST/ABUTMENT NONPOTABLE LABEL 1D PLATE YES X NO YES NO X YES X NO YES X NO WELL INTEGRITY SATISFACTORY YES X NO WELL YIELD LOW MODERATE X HIGH COMMENTS Time Volume pH Cond. (NS/cm) Turbidity (NTU) Dis. Uz (mglL) Temp CC) ORP (mV) Motes 1 6.46 1.39 16.4 1.14 16.66 257 2 7.07 1.54 27.9 0.69 16.55 -165 3 7.07 1.59 31.5 0.68 16.34 -71 NCDENR — Remedial Construction Complelion Report July 20, 2011 MRCTEC Project 6628-08-4691 NOMCDO001092 APPENDIX D LABORATORY REPORT - PRE -INJECTION GROUNDWATER SAMPLES ace Analyfical9 +vww.pacdsas.cam April 26, 2011 Mr, Mark Filardi Mactec Charlotte 2801 Yorkmont Road Charlotte, NC 28208 Pace Analytical Services, Inc. 205 Eas! Meadow Road - Suil9A Eden, NC 27288 (336)W-a921 RE: Project: CMI WWTP Pace Project No.: 929225C Pace Analytical Services, Inc. 2225 Riverside Or. Ashev die. NC 288n4 (828)254-7176 Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 1 N Huntarsvile, NC 28078 (704)875,9092 Reviewed by MPF 715111 Dear Mr. Filardi: Enclosed are the analytical results for sample(s) received by the laboratory on April 18, 2011, The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. The samples were received outside of required temperature range. Analysis was completed upon client approval. If you have any questions concerning this report, please feel free to contact me. Sincerely, �r r Kevin Godwin kevin.godwin@pac,elabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, without the written consent of Paco Analytical Services. Inc.. L. if Page 1 of 15 _ aceAna",ol wwvraaradabam" Project: CMI WWTP Pace Project No.: 9292250 Pace Analytical Services, Inc. 205 East Meadow Road - SuIla A Eden, NC 27288 Charlotte Certification fDs 9800 Kincey Ave. Ste t00, Huntersville, NC 28078 LouisianalLEI-AP Certification #: W34 New Jersey Certification #: NCO12 North Carolina ❑rinking Water Certification # 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #. 12 Pennsylvania Certificalion #' 6a-007a4 South Carolina Certification #: 99006W1 Asheville Certification IOs 2225 Riverside Or., Asheville, NC 28804 Connecticut Certificalion #: PH-0106 Flarida/NELAP Certification #: E87648 Massachusetts Certification #: M•NCO30 New Jersey Certification #: NC011 North Carolina Bioassay Certification #: 9 Nnrth Cnrnfina 0rink Inc Water Certification #; 37712 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 26804 CERTIFICATIONS (828)254-7176 South Carolina Drinking water Celt. #-. 99ON003 Virginia Certification #: 00213 Connecticut Certification #: PH-0104 FloNatNELAP Certification #: E87627 Kentucky LIST Certificalion #: 84 Louisiana DHH Drinking Water # LA 100031 West Virginia Gertiflcatic n #: 357 North Carolina Wastewater Certification #: 40 Pennsylvania Certification #: 68-03578 South Carolina Bioassay Certification #: 99030002 South Carolina Certification #: 99030001 Virginia Certification #: OW72 West Virginia Certification #: 356 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, wi hout the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc, 98M Kincey Ave. Sulle 100 Huntersville, NC 2807E (704)875-9092 Page 2 of 15 aceAnalj&calr n Pdowsbs.mm Project: Choi WWTP Pace Project No.: 9292250 Lab 10 Sample I❑ 9292250001 ESIAW-18 9292250002 EBMW-10 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 272M (336)G23-8921 9292250003 DEVELOPMENT WATER 91 Pace Analytical Services, Inc. 2225 Rtversrde Or- Ashe nlie, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Method EPA 6010 EPA 7470 EPA 6010 EPA 7470 EPA6010 EPA 7470 EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not W reproduced, except In full, Wiithcut the written consent of Pa ce A natytical Services, Inc.- .. Pace Analytical Services, Inc. 9600 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)B75.9092 Analytes Analysts Reported Laboratory JMW 7 PASI-A SHB 1 PASI-A JMW 7 PASI-A SHB 1 PASI-A JMW 7 PASi-A SHE i PASi-A MCK 63 PASI-C Page 3 of 15 aC6malXicals >tiww.pea94bs cnm Project: Civil WWTP Pace Project No.- 929225D Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27286 (336)623-8921 Pace Analyticat Services, Inc, 2225 Riverside Or. Asheville, NC 28804 (828)254.7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9 800 Kn cey Ave. Suite 100 Huntersv+Ile, NC 25078 (704)876_a092 Sample: EBMW-18 Lab ID: 9292250001 Collected: 0411&11 14:00 Received. 0411&11 16A7 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND uglL 5.0 1 04/22/11 13:15 04/25111 21:00 7440-38-2 Barium 67.0 uglL 5.0 1 04/22111 13:15 04/25/11 21:00 7440-39-3 Cadmium NO uglL 1.0 1 04/22111 13:15 M25111 21:00 7440-43-9 Chromium 10.5 uglL 5.0 1 04r22111 1315 04125/11 21:00 7440-47-3 Lead ND ug1L 5.0 1 04/22/11 13.15 04/25111 21:00 7439-92-1 Selenium ND uglL 10.0 1 04/22/11 13:15 0412511121:00 7782-49-2 Silver 9.6 ugiL 5.0 1 04/22/11 1315 04/25111 21:00 7440-22-4 7470 Mercury Analytical Method: EPA7470 Preparation Method: EPA7470 Mercury NO uglL 0.20 1 04/21111 10:30 04/21/11 1523 7439-97.6 Sample: EBMW-10 Lab ID: 9292250002 Collected: 04118/11 15.00 Received: 04/18/11 16:47 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic NO ug1L 5.0 1 04122/11 13:15 04/25/11 21:06 7440-38-2 Barium 31.6 ug1 5.0 1 04122/11 13:15 0412"1 21:06 7440-39-3 Cadmium NO ug1L 1.0 1 04122/11 13:15 04/25/11 21:06 7440.43-9 Chromium. ND ul;& 5.0 1 04/22/11 13:15 0412601 21:06 7440-47-3 Lead NO ug1L 5.0 1 04/22111 13:15 04/25111 21:06 7439-92-1 Selenium NO ugyL 10.0 1 C4122111 1315 04/25/11 21:06 7782-49-2 Silver NO ug1L 5.0 1 04122/11 13.15 0412511121:06 7440-22.4 7470 Mercury Analytical Method. EPA 7470 Preparation Method: EPA 7470 Mercury NO uglL 0.20 1 04/21/11 10:30 (4121111 15:26 7439-97-6 Sample: DEVELOPMENT WATER #1 Lap ID: 9292250003 Collected: 04/18111 15:15 Received: 04/18111 16:47 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual $010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3010 Arsenic ND ug11 5.0 1 04/22111 13:15 4W25111 17;52 7440-38-2 Barium 386 uglL 5,0 1 04122J11 13:15 04/25/11 17:52 7440-39.3 Cadmium ND uglL 1-0 1 04122/11 13:15 04125/11 17:52 7440-43-9 Chromium 26.4 uglL 5.0 1 041M1 1315 0412501 17:52 7440-47-3 Lead 35.2 ug1L 5.0 1 04/22/11 13:15 04125/11 17:52 7439-92-1 Selenium ND uglL 10.0 1 04QW11 13:15 04/25111 17:52 7782.49-2 Silver ND uglL 5.0 1 04/22/11 13:15 04/25/11 17:52 7440-22-4 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury NO uglL 0.20 1 04/21/11 10:30 W21111 15:28 7439-97-6 Date: 04/26/2011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 4 of 15 This report shall not he reproduced, except in lull, without the written consent of Pace Analytical Services, Inc.. 1 �CidC aceAnalytical" w.rw.�eebs.cm+ Pace Anaiytltal Services, Inc. Z05 East U.Meacow Row - Suite A Eden, NC 272U (336)523.8921 Pace Analytical Services, inc. 2225 Rivem4e Dr. Asheville, NC 288N ANALYTICAL RESULTS (828)254-7176 Pace Analytical Services, Inc. 98DO t4nc4ay Ave. Suite 100 Huntersville, NC 28078 (704 W5-9092 Project: CMI WWTP Pace Proiect No. 9292250 Sample: DEVELOPMENT WATER #1 Lab Id: 9292250003 Collected: M18/11 15:15 Received: 04118111 16:47 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff 8260 MSV Low Level Analytical Method: EPA 8260 Acelone NO uglL 25.0 1 04122/11 17:35 67-64-1 Benzene NO ug1L 1.0 1 04/22/11 17:35 71-43-2 Bromicibenzena NO uglL 1.0 1 04122J11 17:35 108-86-1 Bromochloromethane NO ug1L 1.0 1 04122/11 17:35 74-97-5 Bromodichlofomethane ND uglL 1.0 1 04J22111 17:35 75-27-4 Bromoform ND u9k 1.0 1 04/22/11 17:35 75.25-2 Bromomethane ND ugR 2.0 1 04/22/11 17:35 74-83-9 2-Butamne (MEK) NO uglL 5.0 1 04/22/11 17:35 78-93-3 Carbon tetrachloride NO uglL 1.0 1 04/22/11 17:35 56-23-5 Chlorobenzene NO tKYL 1.0 1 04/22/11 17:35 108-90-7 Chloroethane 37.9 ugA- 1.0 1 04122/11 17:35 75-00-3 Chloroform 6.9 ugR 1.0 1 04/22/11 17:35 67-66-3 Chloromethane N❑ u91L 1.0 1 04/22111 17.35 74-87-3 2-Chlorotoluerte NO ugR 1.0 1 04/22/11 17:35 95AM 4-Chbrotoluene ND uglL 1.0 1 04/22111 17:35 106-43.4 1,2-Dibroma-3-chloropropane ND ug1L 5.0 1 04122111 17.35 96.12-8 Dlbromochlaromethane ND ug1L 1.0 1 04/22111 17:35 124-48.1 1,21)ibromoethane (EfDB) ND uglL 1.0 1 04/22/11 17:35 106-93-4 Dibromomethane ND uglL 1.0 1 04/22/11 17:35 74-95-3 1,2-Dichiorobenzene ND ug1L 1.0 1 04/22/11 17:35 95-50-1 1,3-Dichlorobenzene ND uglL 1.0 1 04/22/11 17:35 541-73-1 1,4-Dichtorobenzene NO uglL 1.0 1 D4122111 17:35 106-46-7 Dich4orodifVuoromethane ND ugR 1.0 1 M22/11 17,35 75-71-8 1,1-Dichloroelhane 2550 ugR 200 200 04/23111 21:56 75-34-3 1,2-Dichloroethane 4.1 uglL 1.0 1 04/22/11 17:35 107-06.2 1,1-01chloroetherne 1200 ug1L 200 200 04123/11 21:56 755-35--4 65-1,2-Dichloroethene ND ug1L 1.0 1 04122/11 17:35 156-59-2 trans-1,2-Dichloroethene NO uglL 1.0 1 04/22/11 17:35 156-60-5 1,2-Dichicropropane NO ug1L 1.0 1 04/22/11 17:35 78-87.5 1,3-Dichtoropropane ND uglL 1.0 1 041221i1 17:35 142-28-9 2,2-Dichloropropane ND ugR 1.0 1 04/22/11 17:35 594-20-7 1,1-Dichloropropene ND ug1L 1.0 1 04/22111 17;35 563-58-6 cls-1,3-Dichloroprapene ND ug1L 1.0 1 04122111 17:35 10061-01-5 trans- 1, 3-Dich lorop rape ne ND ug1L 10 1 04/22/11 17:35 10061.02-6 Diisopropyl ether NO ug1L 1.0 1 0W22111 17:35 108-20.3 Ethylbenzene ND uglL 1.0 1 04/22111 17.35 100-41-4 Hexachlofe-1,3-butadiene N❑ ug1L 1.0 1 04122Ji1 17:35 87-68-3 2-Hexanone ND ug1L 5.0 1 04122/11 17:35 591.78-6 p4sopropyltaluene N❑ ug1L 1.0 1 04122/11 17:35 99-87-6 Methylene Chloride NO ug1L 2.0 1 04122/11 17:35 75-09-2 4- Meth yl-2-pentanane (MIBK) ND ug1L 5.0 1 04/22/11 17:35 108-10-1 Methyl -tart -butyl ether NO ugfL 1.0 1 04122/11 17:35 1634-04-4 Naphthalene N❑ ug1L 1.0 1 04/22/11 17:35 91-20-3 Styrene 1.3 uWL 1.0 1 04122111 17:35 100-42-5 1.1,1,2-Tetachlorcelhane ND ug1L 1.0 1 04/22/11 17:35 530-20-6 1.1.2,2-Te1rachloroethane NO uglL 1.0 1 04/22111 17:35 79-34-5 Tetra chloroe th ene 14.7 ug1L 1.0 1 04/22/11 17:35 127-18-4 Date: 04126/2011 04.23 PM REPORT OF LABORATORY ANALYSIS Page 5 of 15 This report shall not be raproduted, except In Tull. wiftut the written consent of Pace AnaiyticaI Services, Inc.. [l_74=•_ ��H Pace Analytical Services, fne. Pace Analytical Se"kes, Inc. Pace Analytical Services, Inc. accAnalytical 205 Easl Meadow Roa4 - SuAeA 2225 Riverside Df 9NO Kincey Ave. Stile 100 paz%�s�rcnm Eden, NC 27288 Asheville. NC 288D4 Nunter5vile. NC 26078 (33W23-8921 (B2B)254-7176 f D4)675-9092 ANALYTICAL RESULTS Pro;ecl Cmi WVVTP Pace Prcject No.: 9292250 Sample: DEVELOPMENT WATER #1 Lab ID: 92M50003 Collected- 04/18/11 15:15 Received. 04118111 16747 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. "I B260 MSV Low Level Analytical Method: EPA 6260 Toluene 3.8 ugrL 1.0 1 04a2J11 17:35 10B-B8-3 1,2,3-Trichlorohenzene ND ug1L 1,0 1 04/22/11 17:35 87-61-6 12,4-T&h1orobenzene ND ug2 1,0 1 04/22/11 17:35 120-82-1 1,1,1-Trichic roethane 14300 ug1L 200 200 04123/11 21:56 71.55-6 1,1,2-Trichloroethane 11.9 uglL 1.0 1 04/22111 17:35 79-04.5 Trichloroethene 4.6 ug1L 1.0 1 04/22/11 17:35 79-01-6 Trichforonuoromethane NO uglL 1.0 1 D4122111 17:35 75-69-4 1,2,3-Tn&Iompropane ND ug1L 1,0 1 04/22/11 17:35 96-18-4 Vinyt acetate NO ugA- 2.0 1 04/22/11 1735 108.054 Vinyl chloride 4.0 uglL 1.0 1 04/22111 17:35 75-01-4 m&p-Xylene ND uA 2.0 1 04122/11 17:35 179601-23-1 o-Xylene NO ug1L 1.0 1 04122/11 17:35 95-47-6 4-BramofVuorobenzene (S) 98 °% 70-130 1 04/22/11 17.35 460-00-4 Oibromofluoromethane (S) 104 % 70.130 1 04/22/11 17:35 1668-53-7 1,2-0ichloroelhane-d4 (S) 142 % 70-130 1 04/22/11 17:35 17060-07-0 Toluene -dB (S) 100 % 70-130 1 04122/11 17:35 2037-26.5 Date. 04/2612011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 6 of 15 This reporl shall riot 6e reproduced, except to full, without the written consent of Pzce Analytical 9arvl er, {nc.. . 1 1GiGLC, aceAnalyticaie r�ncpare.'a5s-tm Pace Anatyticat Sory ice s, Inc. 205 Easl kleadaw Road - Suite A Eder, NC 27288 (336)623-8921 Pace An aIyrlcal Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 QUALITY CONTROL DATA Projecl- CMI WWTP Pace Project No.: 9292250 ❑C Batch: MPRP18230 Analysis Method- EPA 6010 QC Batch Method. EPA 3010 Analysis Des&plicn: 6010 MET Associated Lah Samples: 9292250p01, 9292250002 METHOD BLANK: 594902 Matrix: Water Associated Lap Samples: 9292250001, 9292250002 Blank Reporting Parameter LIPAS Resull Limit Analyzed Qualifiers Arsenic uglL ND 5.0 04)2511119:26 Barium uglL NO 5.0 0412511119:26 Cadmium uglL ND 1.0 0412511119:26 Chromium ug1L ND 5.0 04/2511119:26 Lead ug1L NO 5.0 04/25111 19:26 Selenium uglL NO 10.0 0412511119-26 Silver ug1L ND 5.0 04/2511119:26 Pace Analydcat Services, Inc- 9800 KinceyAve-Suite 100 Huntersvine, NC 28079 (704)875-"2 LABORATORY CONTROL SAMPLE- 594903 Spike LCS LCS to Rec Parameter Units Conc- Result % Rec Limits Qualifiers Arsenic uglL 500 503 101 80-120 Barium uglL 500 512 102 80-120 Cadmium ug1L 500 523 105 80-120 Chromium ug1L 500 505 101 80-120 Lead ug1L 500 509 102 80-120 Selenium uglL 511)(] 505 101 80-120 Silver ugA- 250 255 102 80-120 MATRIX SPIKE & MATRIX SPICE DUPLICATE: 594906 594907 MS MSD 9292183006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Llmils RPD Arsenic uglL ND 500 500 512 505 102 101 75-125 1 Barium uglL 88-7 500 500 605 695 103 101 75-125 2 Cadmium ug!L ND 500 500 519 507 104 101 75-125 2 Ghromium ug1L ND 500 S00 506 490 101 98 75-125 3 Lead uglL NO 500 500 509 497 102 99 75-125 2 Selenium ug1L NO 500 500 511 503 102 101 75-125 2 Silver uglL ND 250 250 255 251 102 100 75-125 2 Date: 04/26/2011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 7 of 15 This reprxt shall not i,e reproduced, except In full, without the wrilten consent of Pace Analytical Services, Inc-. ��aeAnalytical ww�+:yaa�zcvn Pace Artatyticai Services, Inc. 205 East Meaeuw Road - Suile A Eden, NC 27288 1336 )623-892 t Project: CM VWVTP Pace Project No.: 9292250 QC Batch: MPRP18231 QC Batch Method: EPA 3010 Associated Lab Samples. 9292250003 METHOD BLANK: 594910 Associated Lab Samples: 9292250003 Parameter Units Arsenic ug1L Barium ug11 Cadmium ug1L Chromium uq& Lead uglL Selenium ug)L Silver uglL LABORATORY CONTROL SAMPLE: 594911 Parameter Units Arsenic UA Barium uglL Cadmium uglL Chromium uglL Lead ug1L Selenium ug1L Silver ug1L Pace Analytical Services, Inc, 2225 Rwrslda Qr. AsfteVilie, NC 289A {820)254-71 >6 QUALITY CONTROL DATA Analysis Method: EPA 6010 Analysis Description: 6010 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04r2511117:45 NO 5.0 0412511117A5 NO 1.0 0412511117:45 ND 5.0 04QS11117:45 NO 5.0 0412511117:45 NO 10.0 04/25/11 17:45 ND 5.0 04/25/11 17:45 Pace Analytical Services, Inc. 9300 NhnceyAve. Suite 100 Huntersvite, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conic, Result % Rec Limits Qualifiers 50O 504 101 80-120 500 505 101 80-120 500 520 104 80-120 500 504 101 80-120 500 506 101 80-120 50O 494 99 80-120 250 252 101 80-120 MATRIX SPIKE SAMPLE: Parameter 594912 Units 9292250003 Result Spice Conc. MS Result MS % Rec % Rec Limits Qualifiers Arsenio u9fL NO 500 505 101 75-125 Barium uglL 386 500 861 95 75-125 Cadmium ug1L NO 500 493 99 75-125 Chromium ug1L 26.4 500 507 96 75-125 Lead uglL 352 500 502 93 75-125 Selenium ug1L NO 500 496 99 75-125 Silver uglL NO 250 246 98 75-125 SAMPLE DUPLICATE: 594913 9292003003 Dup Parameter Units Result Result RPO Qualifiers Arsenic uglL NO ND Barium uglL 78.1 77,8 Cadmium uglL NO NO Chromium ugii NO NO Lead uglL NO ND Date: 04126/2011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 8 of 15 This re part shall not be reproduced, except in full, millout Iha written consertl 01 PPaCee Analytical SBrviCes, Inc . ! 1 IG1QLl: x! 0 aceMaly aif >rww�oMehucoonr Prcjezt: CMI VVWTP Pace Project pia.' 9292250 SAMPLE DUPLICATE, 594913 Parameter Selenium Silver Pace Analytical Services. Inc. Paco AnakyUcW So micas, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite 2225 Riverside Or. 9800 KinceyAve. Suile 100 Eden, NC 27288 Asheville, NC 2$804 Huntarsville, NC 28078 (336)623-8921 (828)254-7176 (7n4)875-W92 QUALITY CONTROL DATA 9292003003 Dup Units Result Result ug/L ND NO ug1L NO ND RPD Qualifiers Date. 04/26/2011 04.23 PM REPORT OF LABORATORY ANALYSIS Page 9 of 15 This report shall not he reproduced, except in full, without the written cansml of I Pace Analytical Sarmces, Inc.. ek,. aceAnalyiical' �.Fan sb>ca Face Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (33fi)623-8921 Pace Analytical Servlc", Inc. 2225 PjVCr5ide Dr. Asheville, NC 2a804 (828)254-7176 QUALITY CONTROL DATA Project: CMI VW TP Pace Project Na.: 9292250 LAC Batch: MERP13418 Analysis Method: EPA 7470 QC Bata Method: EPA 7470 Analysis Description: 7410 Mercury Associated Lab Samples: 9292250001, 9292250002, 9292250003 METHOD SLAW 593389 Matrix: Water Associated Lab Samples: 9292250009, 9292250002. 9292250003 Blank Reporting Parameter Uniis Result Limit Analyzed Qualifiers Mercury U91L N❑ 0.20 04/2111114:30 Paco Analytical Sarvices. Inc. 9800 KinceyAve . Suite 100 HuntwsviAe, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 593390 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug1L 2.5 2.1 86 80-120 MATRIX SPIKE b MATRIX SPIKE DUPLICATE: 593391 593392 MS MSD 9292183006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Car1c. Cane. Result Result % Rec % Rec Limits RPD Quaff Mercury ug1L ND 2.5 2.5 2.0 2.1 79 83 75-125 5 Date 04126/2011 D4:23 PM REPORT OF LABORATORY ANALYSIS Page 10 of 1!� This report Shall nol W roproduCed, orc"l in full. withoul the written consent of Pace AnalyUcai Services, Inc.. aceRnavica( wrrw,papplap3-Cn,^ Project. CfUM1 WWTP Pace Project No.: 9292250 Pace Analytical Se rvl ces. Inc. 205 fast Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analyticat Services, Inc. 2225 Riverrrlda Dr Asheville, NC 28804 (8281254-7176 QUALITY CONTROL DATA QC Batch: MSVfl4900 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description; 8260 MSV Low Level Associated Lab Samples: 9292250003 METHOD BLANK- 595311 Matrix Water Associated Lab Samples: 9292250003 Parameter 1.1,1,2-Tetrachlam ethane ugfL 1.1.1-Trichloroethane ugfL 1,1,2,2-Telrachloroethane u9111- 1,1,2•Trichloroethane ugfL 1,1-Dichloroethane uglL 1,1-Dichlomethene ug1L 1,1-Dichloropropene uglL 1,2,3-Trrchlorobenzene uglL 1,23-Trichlompropane uglL 1,2,4-Teichlorobelizene uglL 1,2-Dibromo-3 -chic rapropane ug1L 1,2-Dibromoethane (EOH) ug1L 12-Dichiorobencene ug1L 1.2-Di chloroethane ug1L 1,2-Dichloropropane ug1L 1,3-1)ichIoroberizene ug1L 1,3-Dichloropropa ne ug/L 1,4-0ichlorobenzene ugll 2,2-Dichloropropane uglL 2-Butanone (MEK) ugfL 2-Chlarololuene ug1L 2-Hexanone ugfL 4-Chlorotoluene uglL 4-Methyl-2-pentanone (MIBK) UA Acetone ugli Benzene uglL Bromobanzene ugfL Bromochloramethane uglL Bromodichloromethane ugfL Bromoform ugfL Bromomethane ug1L Carbon tetrachloride ugA- Chlorobenzene uglL Chloroethane uglL Chloroform uglL Chlorametharte upfL cis-1,2-0ichloroethene uglL cis-1,3-Dichlaropropene ugfL Dibromochloromelhane uglL Dibromamethane ugfL DichlorodiSluoromethane ug1L Diisopropyl ether ug1L Elhyibenzene ug1L Oate 04/25/2011 04:23 PM Blank Units Result Reporting Limit Analyzed ND 1.0 041221111538 NO 1.0 0412211115:38 ND 1.0 04122J1115;38 NO 1.0 D412211115:38 NO 1.0 0412211115:38 ND 1.0 0412211115:38 ND 1,0 0412211115:38 ND 1.0 041220115:38 ND 1.0 0412211115:38 ND 1.0 04122/1115:38 ND 5.0 04122/11 1538 N❑ 1.0 04122/1115:38 N❑ 1.0 04/2211115:38 ND 1.0 0412211115,38 ND 1.0 0412211115:3B ND 1.0 0412211115:38 ND 1.0 0412211115:38 ND 1.0 04122/1115.38 ND 1,0 0412211115,38 ND 5.0 0412211115:38 NO 1.0 04122/11 15:38 N D 5.0 04122/11 15:38 ND 1.0 04122/1115:38 ND 5.0 0412211115:36 ND 25.0 0412211115:38 ND 1.0 0412211115:38 ND U 04/2211115.38 NO 1,0 04122J111538 ND 1.0 04/22111 15:38 N D 1.0 04/22111 15:38 ND 2.0 0412211115-38 ND 1.0 04122J1115:3B ND 1.0 04122/1115:38 ND 1.0 0412211115.38 N❑ 1.0 D111221111518 ND 1.0 041221111538 ND 1.0 0422J1115:36 ND 1.0 0412211115:38 ND 1.0 04/22/11 15:38 N0 1,0 0412211115:38 N ❑ 1.0 04122J11 15:38 ND 1.0 04122/1115:3B N❑ 1.0 04122J1115:38 REPORT OF LABORATORY ANALYSIS This report shall not be reproducea, except in lull, without the written consent of Pace Anatytical Services, Inc.. Qualifiers Pace Analytical Services, tnc. 9600 KincayAve. Suite 100 Hunlersville, NC 28078 (704)87-' -9092 Page 11 of 15 aceAnaiyticai* K*wP&'G4N,rm Pace Analytical Sarvices, Inc. 205 East Meadow Road - SOW A Eden. NC 21288 (336)673.8921 Pace Analytical 8arvices, Inc. 2225 Riverside 13r. Asheville, NC 28804 (828)254-717C QUALITY CONTROL DATA Project: CMI WWTP Pace Project No.: 9292250 METHOD BLANK: 595311 Matrix: Water Associated Lab Samples: 9292250003 Parameter Units Blank Result Reporting Limit Analyzed HexacNora- l,3-butad[an a uglL ND 1.0 0412211115:3B m&p-Xylene uglL ND 2.0 0412211115:38 Methyl-tert-butyl ether ug1L ND 1.0 OQ22111 15:38 Methylene Chloride ug1L NO 2.0 04/22/11 15:38 Naphthalene ug1L NO 1.0 04/22/1115:38 o-Xylene ug1L ND 1.0 0412211115,38 p-Isopropylloluene uglL NO 1.0 041221111518 Styrene KIL NO 1.0 0412211115:38 Tetrachloroethene U91L No 1.0 0412211115:38 Toluene uglL ND 1.0 0412211115:38 trans-1.2-Dichloroethene ug1L NO 1.0 0412211115:38 tran s- 1. 3- Di ch I oropropen e ug& ND 1.0 0412211115.38 Trichloroethene ug1L ND 1.0 0412211115.38 TrichloraAuoromeJlane uglL ND 1,0 0412211115:38 Vinyl acetate ug1L NO 2.0 04 MIll 15:38 Vinyl chloride uglL ND 1.0 D4122111 15:38 1,2-Dichloroelhane-d4 (S) % 98 70-130 04/22/11 15:38 4-Brornofluorobe»zene (S) % 98 70.130 04/22/11 15:38 Dibromo8uorornelhane. (S) % 101 70-130 04/22/11 15:38 Toluene-dB(S) % 101 70-130 04/22/11 15.38 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 595312 Units Spike Conc. LCS Result LCS % Rec % Rec Limlls 1,1.1.2-Tetrachtoroethane ugJL 50 49.5 99 70-130 1,1,1-Trlchlolvethane ug[L 50 49.5 99 70-130 1,1,2,2-Tetrachlomethane ug1L 50 48,6 97 70-130 1,1,2-Trichloroethane uglL 50 47.9 96 70-130 1,1-Dichloroelhane uglL 50 50.2 100 70-130 1,1-Dichloroethene uglL 50 48.6 97 70-132 1,1-Dichlompropene uglL 50 45.1 90 70-130 1,2.3-Trichtorobenzene ug1L 50 52.6 105 70-135 1,2,3-Trichloropropane uglL 50 48.7 97 70-130 1,2,4-7richtcrobenzene ug1L 50 54.2 108 70-134 1,2-Dibromo-3•chioropropane ug1L 50 52.0 104 70-130 1,2-Dibrcmoethane (EDB) ug1L 50 51A 102 70-130 1,2-Dichlorobenzene ug1L 50 50.7 101 70-130 1,2-Dichloroethane ug1L 50 48.5 97 70-130 1,2-Dichloropropane uglL 50 47.0 84 70-130 1,3-DicNioroberuene ug1L 50 497 99 70.130 1,3-❑ichloropropane uglL 50 48.5 97 70-130 IIA-Dichlorohenzene uglL 50 49.3 99 70-130 2.2-Di chloropropane ug1L 50 48.6 97 58-145 2-Butanone (MEK) uglL 100 95.5 96 70-145 2-Chlorotoluene ug1L 50 48.9 98 70-130 Pace Analytical Services, Inc. 9800 Kincey Ave. Suile 100 Hunlersvft, NG 28073 (704AT5-9092 Qualifiers Date- 04/26/2011 04,23 PM REPORT OF LABORATORY ANALYSIS Page 12 of 15 This repcul "11 n01 he repraduced, except in tull, w Mout the written consenI of Pa cee Analytical 5ervices, Inc... rrJ �L�LlL,: a Pace Analytical Ser Vices, lne. Pace Analytical Serrlces, Inc. /,❑ �17+ I a�cG a�r 1Clr j�r'al 205 East Meadow Read - Sutte A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 26a04 (336)623-B@21 t8281254.7176 QUALITY CONTROL DATA Project: C M I V1rWiP Pace Project No.: 9292250 LABORATORY CONTROL SAMPLE: 595312 Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2-1iexanone uglL 100 94.2 94 70-144 4-Chlorotoluene ug/L 50 52.5 105 70-130 4-Methyl-2-pentanone (MI8K) ug/L 100 99.7 100 70-140 Acetone ugfL 100 84.6 8s 50-175 Benzene ugfL 50 45.9 92 70-130 Sromobenzene LKA 50 50.3 101 70-130 Bromochloromethane LVL 50 48.8 98 70.130 Bromodichlaromethane ug/L 50 51.1 102 70-130 Brornoform uglL 50 52.8 106 70.130 Bromomethane VWL 50 53.9 108 54-130 Carbon tetrachloride ug/L 50 45.1 90 70-132 Chlorobenzene ug1L 50 46.7 93 70-130 Chioraethane ug/L 50 47.9 96 64-134 Chloroform ugtL 50 50.4 101 70.130 Chloromethane ug1L 50 46.7 93 E4-130 cis-1,2-❑ichloroethene ug/L 50 46.3 93 70-131 6s-1,3-Dichlorapropene ug/L 50 51.2 102 70.130 Dibromachlorornethane ug/L 50 50.7 101 70-130 Dibromomethane ug/L 50 49.5 99 70-131 Oich lo rodill uorome than a ug/L 50 46.9 94 56-130 Diisopropyl ether ug1L 50 48.2 96 70.130 Ethylbenzene ug/L 50 48.5 97 70-130 Hexachlom-13-hutadiene u911- 50 51.1 102 70.130 m&p-Xylene ug/L 100 95.8 97 70-130 Methyl-tert-butyl ether ug1L s0 51.7 103 70.130 Methylene Chloride uglL 50 45.9 92 63-130 Naphthalene uglL 50 54.8 110 70-138 o-Xyterie ugfL 50 50.5 101 70-13D p4sopropylloluene uglL 50 51.8 104 70-130 Styrene uglL 50 48.3 97 70-130 Tetrachloroethene ug1L 50 48.7 97 70-130 Toluene ug1L 50 45.3 91 70-130 trans-11,2-Dichloroetnene ug1L 50 47.0 94 70-130 trans-13-Dichloropropene u911- 50 49.7 99 70-132 Trichloroethene ug1L 50 47.4 95 70-130 Trlchlorafluorolnethane ug1L 50 49A 98 62-133 Vinyl acetate ug/L 100 105 105 66-157 Vinyl chloride ug/L 50 45.8 92 69-130 1,2-Dichlaroethane-d4 (S) % 97 74-130 4-Bromoftuorobenzene (S) % 98 70-130 ClibromcHuoromethane (S) % 101 70-130 Toluene-d8 (S) 115 99 70-130 Pace Ar,alyticaf Services, Inc. 9800 FGnceyAve. Suite 100 Huntersville, NC 28078 {704)875-9092 Qualifiers Date- 04/26/2011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 13 15 This report shah not be reproduced, oxcept m full, wilheuI the wntlen conso}n-tt of�Pecee Analyl"I Services, Inc.. '1 ICif�L': ;aceAnaVical- wwwc00"4'sw- Praject CMl VVINTP Pace Project No.: 9292250 Pace Analytical Services, Inc. 205 Easl 6iaadow Road - SuileA Eden, NC 27268 (336)62M921 Paca Analytical Services, Inc. 7225 Riverside Dr. Asheville, NC 26804 (828)254.7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9W Kin coy Ave. Suite 100 Nuntersville, NC 29078 (704)875.W92 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 595313 9292186009 Parameter Units Result MS Spike Conc. MSD Spike Conc. 595314 MS Result MSD Result MS °/, Rec MSD % Rec % Rec Limits RPD t,1-0ichloroe lhene uglL ND 50 50 52.5 51.7 105 103 70-166 2 Benzene ug/L ND 50 50 54.2 5&4 108 111 70-148 2 Chlorobenzene ug/L ND 50 50 58.3 57.4 113 115 70-146 2 Toluene ug14 ND 50 50 55.9 50.0 112 116 70-155 4 Trichloroethene uglL N❑ 50 50 57.3 58.9 115 118 69-151 3 1,2-Dichloraethane-N (S) % 104 1t74 70-130 4-Bromofluarabenzene (S) % 95 90 70-130 Dibromokwomethane (S) % 102 100 70-130 Toluene -dB [Sj % 97 99 70 i30 Qual Date: 04126/2011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 14 of 15 This report shall ool ha reproduced, except in lull. without the writlen consent of Pace AnalylicaI Services, Inc.. aceAnalXiical nwwpaesratrs CCO� Project: CMl VVWTP Pace Project No.: 9292250 DEFINITIONS Pare Analytical Services, Inc. 205 East Meadow Road - Suite A Eden NC 27288 (335)623.8921 QUALIFIERS Pace Analytical Services, lne. 2225 Riverside Dr. ASI-PWIle. NC 28804 (828)254-7178 Pace Analytical Services, inc. 9800 KlnceyAve- Suite 100 HuntersviEe, NC 28078 (704)875.9092 ❑F - 0iiufion Factor, if reported. represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MID -Adjusted Method Detection Limit. S - Surrogate 1.2-Diphenythydrazine (8270 listed analyte) decomposes toA/obenzene. Consistent with EPA guidelines, unrounded da(a are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Dupiicale RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but r of delectec. N-Nitrosodipherty{amine decomposes and cannot be separated from Diphenylamine using Method a270. The result reported for each analyle is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace Pfaf for the current list of accredited anaiytes. LABORATORIES PAST -A Pace Analytical Services - Asheville PAS)-C Pace Ana "cal Services - Charlotte Date:4412512011 04:23 PM REPORT OF LABORATORY ANALYSIS Page 15 of 15 This report shall nol be reproducad, except ir, full, wlthotll the wrilten mnEent oror PareAneyllcal SmiCas, Ino.. 1 R./Clll►. �- ; eAnaVical' CHAIN -OF -CUSTODY J Analytical Request Document The Chain -of -Custody IS a LEGAL DOCUMENT" All :elwant fmida miss[ be cnmpketed accuratnly. Pap.: of Section A Section B Section C 1475216 R.qulrrd fr1i.n1 Inky atm. Wquired Project Intnrmehonl knw��u In! --t—W Company i4apen To Attunklon: �/ _ -+f / r J -MI . F•¢j{ i 41-IFf Addreas! rs s-f��%�h✓ y f rT- �f/I Copy To. Campwv Noma: REGULATORY AGENCY D��i� • �f Address- - _ f F NPOES 1— GROUNDWATER j- DRINKING WATER r' UST RCRA �' OTHER E mad To. • r Purchase Order tlo." Dool �r Rdsn.+ Pnone. Fa.. Proj&u Name / ! aeL (j�[� Pau �v Site Locatlon j �r6� �� S TA TE: R.questarl Du. DalerTAT:� / J �1 Project FhulTher" Paco PrvAle i. } [� Requoltte afysis Filtarn IN) Sect.on D Ma via Godaa N4gvd-i!0i W.—Von bMTRM I CODE § COLLECTED Preservafivos x r f)rirw,N Waler DW Water W r ra Product ales WW Sakvsaid SL I j _ CCSTART TL LIkWtiiAU W o o "F r SAMPLE ID alp.W°LP '4 $ �, W Sample IDs MUST RE LINIDUE T65u. TS z Vl t ❑ U[ner OT x a p L 2 Ll O a O c) p S S c V 1 V V y F — r a H DATE TIME DAfE TIMEr c x x m 2 z m i a w a: a Pate Prolect No.l Lab i.n. 2 s p a 5 C 3-� s yap a: o 4 S -�• G; 8� 1E s 6 7 8 9 1 {I 11 12 ADDITIONAL CDMMENT3 REI-TNQUI SHED AY 7 "TION DATE TIME ACCEPTED HY 1 AFFRJAT ION DATE TIME SAMPLE CONDITIONS k Cghily IZ35 r I 13 3 mit Thr d., AkAk 1 6 ►�d Jmn Tf �r SAMPLER NAME AND SIGNATURE J �,/3 o L ORIGINAL U a n 2 PRINT Name of SAMPLER: eff a f A � SIGNATURE of SAMPLER: 11! tlM V • PDIVYI� r�/ 'tnparlanf Nale 9y slparp IhIs Fp rau al. her ps fq P.u'• NET 30 day paywwl wmi and aqr 1pp w Iafs chup.a of 1.5%par month for ary64"s rot paid vA1h1n 7O days - F-ALL-Q-020mv-OT, 15-May-2007 Sample Condition Upon Receipt Fko nalyfical _ Where Received: fl�Huntersville ❑ Asheville ❑ Eden Courier: ❑ Fed Ex ❑ UPS ❑ USPS Client ❑ Commercial ❑ Pace Other Custody Seal on CoolerlSox Present: ❑ m I no Seals intact: ❑ yes Packing Material: ❑ Bubble Wrap 013ubble Bags ❑ Non ❑Other (��(?, ;4 �C ❑ tional - ' ❑ no Proj: Due Date: Proj. Name: Thermometer Used: I Gun : T1101 Type of Ice: te) Slue None Samples on ice, cooling process has begun Tema Correction Factor: Add l Subtract a 'C Corrected Cooler Tern C Biological Ttssue Is Frozen: Ye too Date and 1 ti is f en mining P content Temp should be above freezing to 6*C Comments: Chain of Custody Present: res ❑No ❑NIA 1. Chain of Custody Filled Out: Yes ONO ❑NIA 2- 3 I. Chain of Custody Relinquished: res ❑l+to CA �g7 3- p Sampler Name & Si nature on COC: res ❑No ❑NIA 4- Samples Arrived within Hold Time: res ❑No ❑NIA 5- Short Hold Time Anal is (a72hr): ❑Yes VINa ❑NIA 6. Rush Turn Around Time Requested: Yes ❑No ❑NIA 7. Sufficient Volume: Yes ❑No El VA g. Correct Containers Used: dies �]No ❑NIA g, N` 7 R`"d-'- ("C' J -Pace Containers Used: Yes Nc El WA Containers Intact: Yes ❑No ❑NJA 10, Filtered volume received for Dissolved tests ❑Yes ❑No A 11. Sample Labels match COC: res ❑No ❑NIA 12, -Includes date/timePD/Anal sis Matrix: � C_ All containers needing preservation have been checked. Dyes ONO NiA 13. All containers needing preservation are found to be in Dyer, ❑Ho compliance with EPA recommendation. �N1A exceptions: VOA, coworm, TOC, O&G. WI-0RD (waver) ❑Yes ❑No Initial when completed Samples checked for dechlohnatlon: 0Yes ❑No 'NIA 1 C Headspace in VOA Vials (>6mm): Ores []No WA 15. Trip Blank Present: ❑Yes ❑No �WA 16. Trip Blank Custody Seals Present ❑Yes ❑No 1,WA Pace Trip Blank Lot # if purchased Client Notification/ Resolution Field Data RequireC7 y 1 N Person Contacted: �L Date(Time: T Commentsl Resolution: SCURF Review:l 12 4V► Coate: I YI SRF Review:_ .ff k _Date:I `fly Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina ❑EHNR Certification Office (i.e out of hold, Incorrect preservalive, out of temp, incorrect containers) F-CH R-CS-003-rev.03 13Apr2011 rw . • awe A lClpical t. WWK pe-Ara.z — May 11, 2011 Mr. Mark Filardi Mactec Charlotte 2801 Yorkmont Road Charlotte, NC 28208 Pace Analytical Services, Inc. 205 Eas, Meadow Road - Suite A Eden, NC 27288 (336)B23-8421 RE: Project: CMI Pace Project No.: 9293621 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville, NC 28804 j92Bj254-7176 Pace Analyticai Services, ins. 9800 KinceyAve. Sure 100 Hunlersville, NC 28070 (744)675-9092 Reviewed by MPF 715111 Dear Mr. Filardi: Enclosed are the analytical results for sample(s) received by the laboratory on May 06, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current NEL.AC standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS -his report shall not oe reproduced, mcopi in fuli- wnhout the written consent of Pace An alp ical Services, Inc. 6heb n: Page 1 of 17 2aceAnapical wtilw.pacda.hs.cr Project; Civil. Pace Project No.: 9293621 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 Charlgtte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvilla, NC 28078 LouisianalLELAP Certification #: 04034 New Jersey Certification #: NC012 Na1h Carolina Drinking Water Geflification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pennsylvania Certification #: 6a-00784 South Carolina Certification 4: 99008001 (336)a23-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28a04 140ffim107—Allbolt I (a29)254-7176 South Carolina Drinking Water Cent. #- 99006003 Virginia Certification #- 00213 Connecticut Certification M. PH-0104 FiaridaMELAP Certification #- E87627 Kentucky UST Certification 84 Louisiana EJHH Drinking Water # LA 100031 West Virginia Ceflification #. 3,57 REPORT OF LABORATORY ANALYSIS This report stlall not ha re pioduted, except in toll, without the written consent of Paco An alytical Services, Inc.. �r Pace Analytical Servlcea, Inc. 9600 Kincey Ave, Suft 100 Huntersviile, NC 25078 (704)875.9092 Page 2 of 17 1192cekaoicalA WW*_P8arle &=m Pac¢ Analytical Services, Inc. 205 East Meadow Rand - Suite A Eden, NC 27288 (536)623-8921 Pace Analytical Services, Inc. 2225 Rlverssde Or, AshevillP-, NC 28B04 (828)25,t-7176 SAMPLE ANALYTE COUNT Pace Analytical Survlces, Inc. 9800 Kficoy Av ri. Sulle 1 Do Nuntersville, NC 28078 (704)675-W92 Project: CN1I Pace Project No-! 9293621 Anal ytes Lab ED Sample ID Method Analysts Reported Laboratory 9293621001 EBMW-29 EPA 6269 MCK 63 PASI-C 9293621002 EBMW-30 EPA 6260 MCK 63 PASi-C 9293621003 EBMW-31 EPA8260 MCK 63 PASI-C 9253621004 EBMW32 EPA8260 MCK 63 PASI-C Page 3 of 17 1.2 aceArWj4ical lM>v� cvr, Project. CMI Pace Project No.: 9293621 Sample: EBMW•29 Parameters 8260 M S V Law Level Acetone Benzene Brornobenzene Bromochloromelhane B ro modi ch loro m e tha n e Bromoform Bramomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroelhane Chloroform Chleromethane 2-CHarotoluene 4-Chlorololuene 1,2-Dlbromo-3-chlorepropane Dibrome ch to ro m e tha ne 1,2-Dlbromoethane (FOB) Dibromomethane 12-Dichlorobenze ne 1,3•Oichlorobenzene 1,4-❑ichlcrobenzane Oic h lorod if] uarometh an e 1,1-Dichloroethane 1,2-Dichloroethane 11-Dichloroethene cis-1,2-Dichloroethene trans-1, 2- Di chloroet hene 1,2-Dichioropropane 1,3-Dlctiloropropane 2,2-Dichloropropane 1.1-Dichloropropene cls-1, 3-Dichlompropene trans-1, 3-D i chlo ropropen e Diisopropyi ether Ethylbenzene Hexachloro-1,3-buladiene 2-Hexanone p-Isopropyltoluene Methyfene Chloride 4-Methyl-2-penlanone (M18K) Methyf-lert-bulyl elher Naphthalene Styrene 1.1,1,2-Tetrachloroethe ne 1,1.2,2-Tetrachloroethe ne Telrachioroethene Pare Analytical Se"Icts, Inc. 206 East Meadow Road - Suita A Eden, NC 27288 Pace Anslytical5ervices, Inc. 2225 Riverside Dr. Ashaville, NC 28804 t828J254-7176 ANALYTICAL RESULTS Pace Analytical Services. Inc. 9800 Kincey Ave. Suite 100 HuntersvlNe, NC Z8078 (704)875 9092 Lab lD: 9293621001 Collected: 05105J11 11.00 Received: 05406111 14:55 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Analytical Method. EPA 8260 NO ug+L ND ugk NO uglL HD uglL NO ug1L NO ug1L NO uglL NO ug1L NO ug1L NO ug1L NO ug1L ND ug1L ND ug+'L NO ug1L N❑ uglL NO uglL NO ogIL NO ug1L NO ug1L NO ug1L NO ug1L NO uglL NO uglL 66.7 uglL NO ug - 51.1 uglL NO uglL ND uglL NO ug1L NO uglL NO uglL NO uglL NO uglL NO ug1L NO ug1L ND ug1L ND uglL ND vglt- NO uglL ND uglL NO uglL ND uglL NO uglL ND ugA- ND ugA- ND ug1L NO ug1L 25.0 1 05/07/11 1848 67 &4-1 1.0 1 0510711118,48 7143-2 1.0 1 05107/11 18:48 108-Wl 1.0 1 0540711118.48 74-97-5 1.0 1 05/07/11 18:48 75-27-4 1.0 1 0510711118:48 75-25.2 2.0 1 05107111 18:48 74-83-9 5.0 1 0510711118:48 78-93-3 1.0 1 05107111 18:48 56-23-5 1.0 1 05/07/11 18:48 108-90-7 1,0 1 05/0711118:4B 75-00-3 1.0 1 0510711116:48 67-66-3 1,0 1 051071111848 74-87-3 1.0 1 05107/1118.48 95-49-8 1.0 1 05/07/11 16:48 106.43.4 5.0 1 05M7/1118:48 96-12-8 1.0 1 05107/11 18:48 124-48-1 1.0 1 05M7111 18:48 106-93-4 1.0 1 0510711118-48 74.95-3 1.0 1 0510711118:48 95-50-1 1,0 1 0510711118:48 541-73-1 1.0 1 M07111 18:45 106-46-7 1.0 1 0510N1116:48 75-71-8 1.0 1 05/07/11 18:48 75-34-3 1.0 1 05/07111 18.48 107.06.2 1.0 1 GW71ll18:48 75-35-4 1.0 1 05107/11 18.48 156-59-2 1.0 1 05107111 18:48 156-60.5 1.0 1 05107111 18:48 78-87-5 1.0 1 05107/11 18748 142-29.9 1.0 1 0510711118:48 594-20-7 1.0 1 05107111 18:48 553-58.5 1.0 1 05/07/11 18!48 10061-01-5 1.0 1 ON07111 18:48 10061-02.5 1.0 1 05/07/11 1848 108-20-3 1,0 1 05/07/11 18:48 100-41-4 1.0 1 0510711118:48 87-68-3 5.0 1 05107111 18:48 591-78-6 1.0 1 0510711118:49 99-07-5 2.0 1 0510711118:48 75-09-2 5.0 1 05/07/11 18A8 105-10-1 1.0 1 05107111 18.48 1634-04-4 1.0 1 05/07111 18:48 91.20-3 1.0 1 05/07111 18:48 100-42-5 1.0 1 0510711118:48 630-20.6 1.0 1 05/0711118:48 79-34-5 1.0 1 OU07111 18:48 127-18-4 ❑ ;at Dale: 05/1112011 04 15 PM REPORT OF LABORATORY ANALYSIS Page 4 of 17 Thls report shall not be reproduced, except in full, without the written consent or Pace +ArOytical Services, Inc.. i IGiCiLr: 2ace Analytical Pace Analytical Services, Int. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Uc Asheville, NC 28804 (828)254.7176 ANALYTICAL RESULTS Paca Anatyucall 5ervicas, Inc. 9800 Kincay Ave. Suite 100 Huntersville. NC 2SO78 (704)875.9092 Project. CMt Pace Projed No.: 9293621 Sample: ERMW-29 Lab ID: 9293624001 Coilecled: 05M5111 11.00 Received- OW6111 14:55 Matrix: Water Parameters Resltlls units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Ana lyttcaI Me(hod. EPA 8260 Toluene ND uglL 1.0 1 05J07111 18:48 108-88-3 1,2,3-Trichlorobenzene ND uglL 1.0 1 05/07/11 18:48 87.61-6 1,2,4-Trichlorobenzene N❑ ug)L 1.0 1 05/07/11 18:48 120-82-1 1,1,1-TdcMoroethane 278 ug1L 10.0 10 05/08/11 10.36 71-55-6 1,1,2-TOChloroethane ND uglL 1.0 1 05M7111 18.40 79-00-5 Trichlorvelhene ND ug1L 1.0 1 05/07/11 18:48 79-01-6 Tdchlorofiuo€omethane ND uglL 1.0 1 05M7111 18:48 75.69.4 1.2,3-Trichloropropane NO uglL 1.0 1 OW7111 18:48 96.18-4 Vinyl acetate NO uglL 2.0 1 GEW07111 18:48 106-05-4 Vinyl chloride NO uglL 1.0 1 05/07/11 18:48 75-01-4 mSp-Xylene ND uglL 2.0 1 0,907111 18:48 179601.23.1 o-Xylene ND ug1L 1.0 1 05107/11 18.48 95-47-5 4-Bromoiluorobenzene (S) 93 °% 70-130 1 051071t1 18:48 460-00-4 Oibromofluoromethane (S) 131 % 70-130 1 05107/11 18.48 1868-53.7 S2 1,2-❑ichloroethane-d4 (S) 127 % 70-130 1 M07111 18:48 17060-07-0 Toluene-d8 (S) 102 °k 70-130 1 05/07/11 18:48 2037-26-5 Sample: EBMW-30 Lab ID' 9293621002 Collected: 05WIll 11.20 Received. 05106111 14.55 Matrix: Water Parameters Results Unils Report Limit OF Prepared Analyzed CAS No. Oual 8260 MSV Low Level Analytical Method: EPA 8260 Acelone ND uglL 25.0 1 05/07/11 19:13 67.64-1 Benzene NO uglL 1.0 1 M07111 19:13 71-43-2 Bromobenzene N❑ ug& 1.0 1 OW7111 19:13 108-86-1 Bromochloromethane NO ug1L 1.0 1 05/07/11 19:13 74-97-5 Bromadichloromethane NO uglL 1.0 1 05/07/11 19:13 75.27-4 Bmmoform NO uglL 1.0 1 05107/11 19:13 75-25-2 Bromomethane NO uglL 2.0 1 05107111 19:13 74-83-9 2-Butanone {MEK) 5.1 ug1L 5.0 1 05/07/11 19:13 78-93-3 Carlson tetrachloride NO uglL 1.0 1 05107I11 19:13 56-23-5 Chlarobenzene ND uglL 1.0 i OW7111 19:13 108-90-7 Chloroethane 2.6 LeglL 1.0 1 OW7111 19:13 75-00-3 Chloroform 4.4 ugA- 1.0 1 M07111 19:13 67.66-3 Chloromethane ND uglL 1.0 1 05/07/11 19.13 74.87-3 2-Chlorololuene NO uglL 1.0 1 05M7M 1 19:13 95-49-8 4-Chlorotoluene NO ug1L 1.0 1 051'07111 19:13 106-43-4 1,2-Dibromo-3-ch}oropropane NO uglL 5.0 1 05107/11 19:13 96-12-8 Dibromochloromethane NO uglL 1.0 1 05/07111 19:13 124-48.1 1,2-Dibromoethane (EDB) NO ug1L 1.0 1 05107/11 19:13 106-93-4 Dibromomethane NO uWL 1.0 1 OV07111 19,13 74.95-3 12-Dlchlarobenzene NO ug1L 1.0 1 05107I11 19:13 95-50.1 13•Dichlerobenzene ND ug1 IX 1 OW7111 19:13 541-73-1 1,4-Dichtorobe nzene NO uglL 1.0 1 05/07/11 1913 106-46.7 DiCh}orodiflucronnethane NO ug.rL 1.0 1 05/07/11 19:13 75-71-8 1,1-Dichloroethane 2850 uglL 250 250 05/08111 11 00 75-34-3 Date: 05/1112011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 5 of 17 This report shall riot ha rnproduG9d, uxcepl in full, without the written consent of Paco Analytical Services, Inc.. a Pace Ana"caI Services, Inc. Pace Analytical Services, trnc. Pace Analytical Sorvtees, Inc. aceAnalXical 205 East Meadow Road - Suite A 2225 Rivesside Dr. 9800 Kimey Ave. Suite 100 ~ bs-cam Eden. NO 2728a Asheville, NC 2B804 Hunterwi;ie, NO 28078 (336)6234WI (828)254-7176 (704)875.9092 ANALYTICAL RESULTS Project: CM! Pace Projecl No.: 9293621 Sample: EBMW-30 Lab !D: 9293621002 Collected: 051051i1 11,20 Received: 05106/11 14.55 Matrix: Wafer Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 M5V Low Level Analytical Method: EPA 8260 1,2-Dichlorpethane ND ug1L 1.0 1 05/07/11 19:13 107-06-2 1,1-Dichloroethene 2590 uglL 250 250 05/08/11 11:00 75-35-4 cis-1,2-1)ichlarcethene ND ug/L 1.0 1 M07111 19:13 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 05/07/11 19.13 156-60.5 1,2-Dichloropropane ND ug/L 1.0 1 05/07111 19:13 78-87-5 1,3-Dichioropropane ND ugrL 1.0 1 05/07/11 19:13 142.28.9 22-Dichloroprdpane NO ug/L 1.0 1 05/07/11 19:13 594-20-7 1,1-Dichloropropene NO ug/L 1.0 1 051071ll 19:13 563.5a-6 cis- 1.3•Dichloropropene NO ug/L 1.0 1 05/07/11 19:13 10061-01-5 trans- 1,3-Dlchlorapro perle NO ug/L 1.0 1 05/07111 19:13 10061-02-6 Diisopropyl ether NO ug/L 1.0 1 05/07/11 19:13 108-20-3 ETLylbenzene NO ug/L 1.0 1 05/07/11 19:13 100-414 Hexachloro-1,3-butadiene ND ug1L 1.0 1 05/07/11 19:13 87-68-3 2-Hexanone NO ug1L 5.0 1 05/07/11 19:13 591-78 6 p4sopropyltdoene 1.6 uglL 1.0 1 05/07111 19:13 99.87-6 Methylene Chloride NO ug/L 2.0 1 05/07/11 19:13 75.09.2 4-Methyl-2-penlanone (MIBIQ NO ug1L 5.0 1 05/07/11 19.13 108-10-1 Methyl-tert-butyl ether NO ugfL 1.0 1 05/07/11 19.13 1634-04.4 Naphthalene NO ug/L 1.0 1 05/07111 19:13 91-20-3 Styrene NO ug/L 1.0 1 05/07/11 19:13 100.42.5 1,1.1,2-Tatra chtoroethane ND ugX 1.0 1 05/07/11 19:13 630.20.6 1,1.2,2-Tatra chlorcethane NO uglL 1.0 1 05/07/11 19:13 79-34-5 Tetrachloroethene 3.7 uglL 1.0 1 05/07/11 19.13 127-18-4 Toluene ND uglL 1.0 1 05/07/11 19:13 108.88.3 1,2,3-Trichlorobenzene NO ug/L 1.0 1 05/07/11 19:13 87-61-6 12,4-Trichlorobenzene ND ug/L 1.0 1 05107/11 19:13 120-82-1 11,1-Trichloroethane 22000 ug1L 2511 250 05/08/11 11:00 71-55-6 1,1.2-Trichlore ethane 4.9 ug/L 1.0 1 05107/11 19:13 79-00-5 Trlchloroethene 5.9 ug/L 1.0 1 05/07/11 19:13 7"1-6 Trichlorolluommethane ND ug/L 11,0 1 M07111 19:13 75-69.4 1,2,3-Ttichlompropane N❑ ug/L 1.0 1 05/07/11 19:13 96-18-4 Vinyl acetate NO ug/L 2,4 1 05/07/11 19:13 108-05-4 Vinyl chloride 2,7 uglL 1.0 1 05/07/11 19:13 75-01-4 map-Xytene NO uA 2.0 1 05/07/11 19:13 179601-23.1 o-Xylene NO ug/L 1.0 1 05/07/11 19:13 95-47-6 4-Bromofluorcbenzene (S) 99 % 70-130 1 05/07111 19:13 460-00-4 Dibromofluoromethane (S) 77 % 70.130 1 05/07/11 19:13 t866-53-7 1,2-01chioroethane-d4 (S) 106 % 70-130 1 05/07111 19:13 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/07/11 1913 2037-26-5 Sample: EBMW-31 Lab 10. 92SJ621003 Collected: 05/05/11 11:50 Received: 05/06/11 14:55 Matrix. Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. 4ual 8260 MSV Low Level Analvlical Method- EPA B260 Acetone NO ugil- 25.0 05/07/11 19:38 67-64-1 Date:05111/2011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 6 of 17 This re pert shall not be reproduced, except in full, wilhput the wri"n consent of Pac�ee An2lyt:cal Services. Inc:., c Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace An atytica1 5ervlce5, Inc. ❑ �I + ac A! alXi .�+ al :� East Meadow Rood - SuheA 2225 Riverside Dr. WOO }GnceyAve. Suite 10U wwwpawos.. sI_ Eden. NC 27288 Asheville, NC 2WN Huntersville, NC 28078 (336)a23-8921 (828)254•7 t 76 (704)875-9092 ANALYTICAL RESULTS Project, CMl Pace Project No.: 9293621 Sample: ESMW�31 Lab ID: 9293621003 Collected: 05105111 11:50 Received. 05/06/11 14.55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 M5V Low Level Analytical Method: EPA 8260 Benzene NO uglL 1.0 1 05/07111 19:38 71-43-2 Bromobenzene NO uglL 1-0 1 M07111 19:38 108-86-1 8romochloromethane ND ugrL 1.0 1 05/07/11 19:38 74-97-5 Bromodlch;oromethane NO uglL 1.0 1 05/07/11 19!38 75.27-4 Bramoform ND ug1L 1.0 1 05107111 19:38 75-25-2 Bromomethane NO ug& 2.0 1 05/07111 19:38 74-83-9 2-Butanone (MEK) NO uglL 5.0 1 05107/11 19:3a 78.93.3 Carbon tetrachloride NO uglL 1.0 1 05107/11 1938 56-23-5 Chlorobenzene NO uglL 1.0 1 05107111 19:38 108-90-7 Chloroethane 44.0 ug1L 1.0 1 05107/11 19:38 75.00-3 Chloroform. 13.8 ug1L 1.0 1 05107i11 19:35 67-66-3 Chloromathane NO uglL 1.0 1 05107/11 19:38 74.87-3 2-Chlorotaluene NO uglL 1.0 1 05/07/11 19:38 95-49-8 4-Chlorotaluene NO uglL 1.0 1 05/07111 19:38 106-43-4 1,2-Dibromo-3-chloropropane NO tig1L 5.0 1 05/07/11 19:38 96-12-8 Dibromochloromettlane NO ug1L 1.0 1 05/07/11 19:38 124-48.1 1,2-Dibromoethane (EDB) NO uglL 1.0 1 05/07111 19:38 106-93-4 Dibromomethare NO uglL 1.0 1 06/07/11 19:38 74-95-3 1.2-Dichlorobenzene ND ug1L 1.0 1 05107/11 19:313 95-50-1 1,3-Dichlorobenzene NO u91L 1.0 1 05/07/11 19:38 541-73-1 1,4-Oichlorobenzene NO uglL 1.0 1 05107/11 19:38 106.46.7 Dichlorodifluoromelhane NO uglL 1.0 1 0&07111 19:38 75-71-8 1,1-Dichlorcethane 3960 uglL 1000 1000 05108/11 21:53 75-34-3 1.2-Dichloroethane 15.6 ug1L 1.0 1 05/07/11 19:36 107-06-2 1,1-Dichloroethene 3720 ug1L 1000 1000 05/08/11 21:53 75-35-4 ds-1,2-0ichloroethene 4.3 ug1L 1.0 1 M07111 19:38 156-59-2 trans-1,2-0Echloroothene NO ug1L 1.0 1 05/07/11 19:38 156-60-5 1,2-Dichloropropane ND ug1L 1.0 1 05/07/11 19,38 78-87-5 1,3-Dichlompropane NO uglL 1.0 1 05/07/11 19:38 142-28-9 2,2-Dichloropropane NO uglL 1.0 1 05107/11 19:38 594-20-7 1,1-Dichloropropene NO ug1L 1.0 1 05107/11 19:38 563-58-6 cis- 1,3-Dichioroprope ne NO uglL 1.0 1 05/07/11 19.38 10061-01-5 trans-1,3-Dichloropropene NO ug1L 1.0 1 05/071111938 10061-02-6 Dilsopropyl ether NO ug1L 1.0 1 05/07/11 19:38 108-20-3 Ethylbenzene NO uglL 1.0 1 05/07/11 19:36 100-41-4 Hexachloro-1,3-butadiene NO uglL 1.0 1 05/07/11 19:36 87-68-3 2-Hexanone NO ug1L 5.0 1 (15107111 19.35 591-78-6 p-150propylloluene NO uglL 1.0 1 05/07/11 19:38 99-87-6 Methylene Chloride NO ug1L 2.0 1 05r07111 19:38 75-09.2 4-Methyl-2-penlanone Q016K) NO ug1L 5.0 t 051071.11 19:38 108-10-1 Methyl-leR•butyl ether NO uglL 1.0 1 05107/11 19:38 1634-04-4 Naphthalene NO uglL 1.0 1 05107/11 19:38 91-20-3 Styrene NO uglL 1.0 1 OW7111 19738 100-42-5 1.1,1.2JelrachIoroethane NO uglL 1.0 1 05J07111 19:38 630-20-6 1.1,2,2Jet rachloroethane NO uglL 1.0 1 M07/11 19:36 79-34-5 Tatra ch loroeth e no 48.1 ug1L 1.0 1 05 V11 19:38 127.18-4 Toluene ND ug1L 1.0 1 05107)11 19:38 108.88-3 Date: 051111201104715 PM REPORT OF LABORATORY ANALYSIS Page 7 of 17 This report shalt rot"reproduced, oxcept in luil, wilhoul the written consent of Pace Ana lytica[ Services. Inc.. e Pace Analytical Services, Inc. Pace Analyucai Services, Inc. Pace Analytical Services, =nc. aeeAna f � i l 205 Eas: Meadow Road - Suite A 2225 Riverside Qr. 98flp Kincey Ave. Suite 100 WWW Pa blabs = Eden, NC 27288 Ashevike, NC 28W4 Huntersville, NC 28078 (336)623.8921 (828)254-7176 [704]875-9992 ANALYTICAL RESULTS Project: CMI Pace Project No.: 9293621 Sample: EBMW-31 Lab ID: 9293621003 Collected. 05/05111 11:50 Received: 05/06/11 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6260 MSV Low Level Analytical Method: EPA 8260 1,2,3-Trichlorobenzene NO UA 1.0 1 05/07111 19:38 87-61-6 1,2,4-Tdchlorobenzene NO ug1L 1.0 1 05/07/11 19:38 120-82-1 1,1,1-Trichloroethane 39300 ug/L 1000 1000 05/08/11 21:53 71-55-6 1,1,2-Trichloroethane 24.8 ug/L 1.0 1 05/07111 19:38 79-00-5 Trichloroethene 11.6 ug1L 1.0 1 0510711i 19:38 79-01.6 Tric h$of of] uo rome thane N❑ ug1L 1.0 1 05/07/11 19:38 75-69-4 1,2,3-Trichlorcpropane ND ugA- 1.0 1 0510711119:38 96-18-4 Vinyl acelate NO ug& 2.0 1 05/07/11 19:38 10"5-4 Vinyl chloride 1.9 ug1L 1.0 1 05107/11 19:38 75-01-4 m8,p-Xylene NO ug/L 2.0 1 M07111 19:38 179601-23-1 0-Xylerle NO ug/L 1.0 1 05/07/11 19:38 95-47-6 4-Bromoiluorobenzene (S) 98 % 70-130 1 05/07/11 19:35 480-00-4 Dibromoflumomethane (S) 45 °% 70-130 1 M07111 19:38 1156a-53-7 S2 1,2-Dichloroelhane-d4 (5) 96 % 70-130 1 05/07/11 19:38 1706D-07-0 Toluene-d8 (S) 96 °% 70-130 1 M7111 19:38 2037-26-5 Sample: EBM W-32 Lab III- 9293621004 Collected: 05/05/11 12.20 Received: 05106111 14 55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 500 20 05/08/11 12:13 67-64-1 Benzene NO ug/L 20.0 2D 05/08/11 12:13 71-43-2 Brornobenzene NO ug/L 20.0 20 05/08/11 12.13 108-86-1 Brornochloromelhane NO ugfL 20.0 20 05/08/1112:13 74-97-5 Bromodichloromelhane NO ug/L 20.0 20 05/08/11 1213 75-27-4 Bromoform ND uglL 20.0 20 05108/11 12:13 75-25-2 Bromomeihane NO ug/L 40.0 20 05108/11 12:13 74-83-9 2-Butarwne (MEIS) NO uglL 100 20 05/08/11 12.13 78-93-3 Carton tetrachloride NO ug/L 20.0 20 05/08/11 12:13 56-23-5 Chlorobenzene NO ug/L 20.0 20 05/08/11 12,13 108-90-7 Chloroethane NO ug/L 20.0 20 05/08/11 12:13 75.00-3 Chloroform NO u91L 20.0 20 05/05/11 12:13 67-66-3 Chiaromethane NO ug1L 20.0 20 0510B111 12:13 74-87-3 2-Chlorotoluene NO ug l- 20.0 20 05/08/11 12:13 95-49-8 4-Chlarotoluene NO ug/L 20.0 20 05108/11 12:13 106-43-4 1,2-Dlbromo-3-chloropropane NO ug/L 100 20 W0811112:13 96-12-8 ❑ibromechloromethane NO ug1L 20.0 20 0&08111 12:13 124-48-1 1,2-Dibrcmoethane (EDO) NO uglL 20.0 20 05/08111 12:13 106-93-4 Dibromomathane NO uglL 20.0 20 05/08/11 12:13 74-95-3 1,2-Dichlorobenzene ND ug1L 20.0 20 05/08111 12:13 95-50-1 1,3-Dichlorobenzene NO uglL 20.0 20 D5108/11 12:13 541.73.1 1,4-Dichlorobar,zene NO uglL 20.0 20 05/06/11 12:13 106-46-7 ❑ichlorodifluoromeihane NO ugA- 20.0 20 MOW11 12:13 75-71-8 11-Dichlooethane 3590 uglL 20.0 20 05/08111 12:13 75-34-3 1,2-Dichloroelhane NO u9I 20.0 2D 05/08/11 12:13 107-06-2 ❑file 05/11/2011 04:15 PM REPORT OF LABORATORY ANALYSIS 7h:5 report shall not be reproduced, except in full, withoul the written consent of Pace Analytical Services. Inc.. Page 8 of 17 e Paco An alyticM Services, Inc. Pace Analytical $ervIces, Inc. Pace Analytical Savicaa, Inc. aceAnaliXicai 205 Eas; Meradow Road - Sake 2225 Nvers da Dt. 9800 Kincey Ave. Suite 100 rw.p ca.sy• �� Eden, NC 272U Asheville, NC 28804 Huntersvlte, NC 28075 (336)623.0921 (828)254.7176 f704j875-9092 ANALYTICAL RESULTS Project: C'Ni Face Project No.: 9293621 Sample; EBMW-32 Lab ID: 9293621004 Collected: OM5111 12:20 Received: 05/06111 14:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 6260 MSV Low Level Analytical Method: EPA 8260 11-Dichloroethene 101 uglL 20.0 20 0510811112:13 75-35-4 cis-1,2-Dichloroethene ND uglL 20.0 20 05/08/11 12.13 156-59-2 trans-1.2-Dichlorcethene NO uq& 20.0 20 05108/11 12:13 156-60-5 1,2-Dichioropropane NO uglL 20.0 20 051081t1 12:13 78.87-5 1,3-Dichioropropane NO uglL 20.0 20 05/08/11 12:13 142-28-9 2,2-Dichkwopropane NO ug/L 20.0 20 05/08/11 12:13 594-20-7 i,i-Dichloropropene NO ug1L 20.0 20 05/08111 12:13 563-5&6 cis-1,3-Dichloropropene NO uglL 20.0 20 05/08/11 12:13 10081-01-5 trans -1,3-Dichlorapropeoe NO uglL 20.0 20 05/08/11 12:13 10061-02-6 Diisopropyl ether NO ug/L 20.0 20 05/08/11 12.13 108-20-3 Ethylbenzene NO u9I 20.0 20 05/08/11 12:13 100-41-4 liexachloro-1.3-butadiene NA uglL 20.0 ZO 05/08/11 12:13 67-68-3 2-Hexanone NO uglL 100 20 05108/11 12:13 591-78-6 p4sopropyitoluene NO u911- 20 0 20 05/08111 12:13 99-87-5 Methy(ene Chloride NO ug1L 40.0 20 05/08111 12:13 75-09-2 4-Methyl-2-pentanone (MIRK) NO ug/L i00 20 05108/11 12713 106-113-1 Methyl-tert-butyl ether NO ug/L 20.0 20 WOW 1 12:13 1634-04-4 Naphthalene NO ug/L 20.0 20 05108/11 t2.13 91.20-3 Styrene NO ug1L 20.0 20 05/08/11 12:13 100.42-5 1,1.1,2-Tetrachloroethane NO ug/L 20.0 20 05/08/11 12:13 630-20-6 1,1,22-Tetrachloroethane NO ug1>_ 20.0 20 051ff8111 12:13 79-34-5 Tetrachloroethene NO ugll 20.0 20 05/08111 12:13 127-18-4 Toluene NO ugA- 20.0 20 05/08/11 12:13 106-88.3 1,43-Trichlorobenzene NO ug/L 20.0 20 05/08/11 12:13 87-61.6 12,4-Tdchlorobenzene NO ug/L 20.0 20 05108/11 12:13 120-82-1 1,11-Trichloroethane 1970 ug1L 20.0 20 05/08/11 12:13 71-55-6 1,1,2-Trichloroethane NO ug/L 20.0 20 05/08/11 12:13 7MO-5 Trtchloroethene ND uglL 20.0 20 051081111213 79-01-6 Trichiorontioromethane ND ug/L 20.0 20 05108/11 12:13 75 69-4 1,2,3 -Trichloroprop ane N❑ ug/L 20.0 20 05/08/11 12:13 96-18-4 Vinyl acetate NO ug1L 40.0 20 WWI 12.13 108-05-4 Vinyl chloride NO uglL 20.0 20 05108/11 12:13 75-01-4 rn&p-Xylene NO ug1L 40.0 20 05108/11 12:13 179601-23-1 0-Xylene NO ug/L 20.0 20 05108111 12:13 95-47-6 4-Bromofluorobenzene (S) 98 % 70-130 20 05/08/11 12:13 460-00.4 ❑lbromofluoromethane (S) 108 % 70.130 20 05108111 12:13 1868-53-7 1,2-DicMoroethene-d4 (S) 112 °% 70-130 20 05/08/11 12:13 17060.07-0 Toluene -dB (S) 102 % 70-130 20 05/08/11 1213 2037.26.5 Rate: 05/11/2011 04.15 PM REPORT OF LABORATORY ANALYSIS Page 9 of 17 This report shall not be reproduced, except In lull. without the written consent or Pace An alytical Services, Inc.. ace Analytical Project: CtAl Pace Project Na.: 9293621 Pace Analytical Services, Inc. 205 East Meadow Roaa - Sulle A Eden. NC 2720 (336)62"921 Pace Analytical Services, Inc. 2225 Riverside Or, Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Balch: MSVII5147 Analysis Method: QC Batch Method: EPA 8260 Analysis Description: Associated Lab Samples: 9293621001, 9293621002, 9293621003 EPA 8260 8260 M5V Low Level METHOD BLANK: 602974 Matrix: Water Associated Lab Samples. 9293621001, 9293621002, 9293621003 Blank Reporting Parameter Units Result Limit Analyzed 1,1.1,2-Tatrachloraethane ug/L NO 1.0 05107/1114:59 1.1.1-Trichloroethana ug1L N❑ 1.0 05107/il14:59 1,1,2,2-Telrachtoroethane uglL NO 1.0 05/07/il 14:59 1.1,2-Trichloroethane uglL N❑ 1.0 05M711114759 1,1-Dichloroethane uglL N❑ 1.0 05J07/1114:59 1,1-Dichlorcalhene uglL NO 1.0 05/0711114�59 1,1-Mchtoropropene ug/L NO 1.0 05107/1114:59 1,2,3-Trichlorobenzene ug/L N❑ 1-0 0510711114:59 1,2,3-Trichioropropane ug/L NO 1.0 (1510711114:59 1,2,4-Trichlorobenzene ug1L ND 1.0 M0711114:59 1,2-0ibromo-3-chloropropane uglL ND 5.0 OSIC711114:59 1,2-Dibromoethane (EDB) uglL NO 1.0 05/07/11 14:59 1,2-Dichlombenzene ug(L ND 1.0 0510711114:59 f,2-Dichloroethane uglL ND 1.0 0510711114:59 1,2-Dichloropropane ug/L N❑ 1.0 0510711114:59 1,3-Dichlorobenzene ug/L N❑ 1.0 05107/1114;59 1,3-Dichk)ropropane ug/L ND 1.0 05107/1114:59 1,4-Dichlorobenzene uglL NO 1.0 0510711114:59 2,2-Dichloropropane ug/L ND 1.0 0510711114:59 2-Butanone (MEK) ug/L NO 5.0 05/07/11 14:59 2-Chlorotoluene ug/L NO 1.0 0510711114:59 2-Hexanone ug/L NO 5.0 0510-111114-59 4-Chlorotoluene ug/L ND 1.0 05107/1114:59 4-Methyi-2-pentanone (MIBK] ug/L ND 5.0 05/07/11 14:59 Acetone uglL ND 25.0 0610711114:59 Benzene ug/L ND 1.0 0510711114:59 Bromobenzene uglL NO 1.0 0510711114:59 Bromochlorometharte ug/L NO 1.0 0510711114:59 Bromodichloremethane uglL N❑ 1.0 05/07/11 14:59 Bromofonn ug(L NO 1.0 05107/1114:59 Bromomethane ug)L NO 2.0 0510711114:59 Carbon tetrachloride ug)L NO 1.0 05/07/11 14:59 Ch)orobenzene uglL ND 1,0 05/07/11 14:69 Chloroelhane uglL NO 1.0 05/0711114:59 Chloroform u91L NO 1.0 05/0711114.59 ChWomethane ug/L NO 1.0 05107/1114:59 cis-1,2-Dich[circa therie ug/L ND 1.0 0510711114:59 cis-1,3-Dichloropropene ug/L ND 1.0 0510711114:59 Dibromochtoromelhens ug/L ND 1.0 OW0711114:59 Dibromomethane ug1L NO 1.0 05107/1114:59 DichlorodlIluoromalhane ug/L NO 1.0 0510711114:59 Diisopropyl ether ug/L ND 1.0 0S107111 14:59 Ethytbenzene ug/L NO 1.0 M0711114.59 Date: 05111/2011 04:15 PM REPORT OF LABORATORY ANALYSIS his report shalt not be ro prod u[ed, except in ful,, withcul the written consent of Pace Analytical Services, Inc.. Qualifiers Pace Analytical Services, inc. 98W IGncay Ave, Suite 100 Hun}ersville, NC 28078 (704)875-9092 Page 10 of 17 1!;ac Analytical R W. WCWE'�'S CPT: P ac it Analytical Services, Inc. 206 East Meadow Road - Suite A Eden, HC 27288 (336)623.8921 Pace Analytirat SorWces, Inc. 2225 Riverside Dr. F,5hevilie, NC 25804 (828)254.7178 QUALITY CONTROL DATA Project: CMI Pace Project Noz 9293621 METHOD BLANK: 602974 Matrix: water Associated Lab Samples: 9293621001, 9293621002. M3621003 Blank Reporting Parameter Units Result Limit Analyzed Hexachloro-1,3-buladiene uglL N❑ 1.0 0510711114:59 m&p-Xylene ug1L N❑ 2.0 05/0711114:59 Methyl-lert-butyl ether ug1L ND 1.0 M07111 14:59 Methylene Chloride uglL NO 2.0 05/07/11 14:59 Naphthalene uglL NO 1.0 0510711114:59 o-Xyiene uglL ND 1.0 05107/1114:59 p-Isopropylloluene IJA ND 1.0 OW0711114:59 Styrene ug1L ND 1.0 0510711114:59 Telrachlorcethens ug1L NO 1.0 05107/1114:59 Toluene uglL ND 1.0 051071i114:59 trans-1,2-Dichloroetherie ugJL ND 1.0 0510711114:59 trans-11,3-Dichlaropropene uglL NO 1.0 0510711114:59 Trichloroelhene ugrl- N❑ 1.0 0510711114:59 Trichlorofluoromethane uglL NO 1.0 OW0711114:59 Vinyl acetate uglL ND 2.0 05/07/11 14:59 Vinyl chloride ug1L N❑ 1.0 OSM7111 14:59 1,2-Dichloroethane-d4 (S) % 120 70-130 05107/11 14:59 4-Bromofluorobenzene (S) % 95 70-130 M07111 14:59 Dibromofluoromethane (S) % 121 70-130 05/07/11 14:59 Toluene-d8 (S) 0i; 100 70-130 05/07/11 14;59 Qualifiers LABORATORY CONTROL SAMPLE. Parameter 502975 Units Spike Corte. LCS Result LCS % Rec % Rec Limlls 1,1,1,2-Telrachloroethane ug1L 50 57.5 115 70-130 1,1,1-Trichiorcethane uglL 50 55.8 112 70-130 1,1,2,2-Tetrachloroelhane uglL 50 54.5 109 70-l30 1,1,2-Trichloroelhane uglL 50 56.5 113 70-130 1,1-Dichloroethane uglL 50 56.8 114 70-130 1,1-Dichloroethane uglL 50 55.8 112 70.132 1,1-Dirhioropropene uglL 50 54.4 109 70-130 1,2,3-Trichlorobenzene uglL 50 52.7 105 70.135 1,2,3-Trichicropropane uglL 50 54.6 109 70.130 1,2,4-Trlchlorobenzene uglL 50 49.4 99 70.134 1,2-01bromo-3-chloropropane ug1L 50 50.6 101 70-130 1,2-Dibromoethane (EDB) ug1L 50 57.7 115 70-130 1,2-DichIorobenzene uglL 50 56.6 113 70-130 12-Dichloroethane uglL 50 54.7 109 70-130 1,2-Dichloropropane uglL 50 54.4 109 70-130 1,3-Dichlorobenzene ug1L 50 56.8 114 70.130 1,3-Dichioropropane ug1L 50 56.9 114 70-130 14•Dichhorobenzene ug)L 50 52.9 106 70-130 2,2-Dichlorepropane uglL 50 55.9 112 58-145 2-Butanone (MEK) u91L 100 110 110 70-145 2•Chlorotoluene uglL 50 58.6 117 70-130 Pace Analyllcaj Services, Inc. 9800 IGncey Ave. Suite 100 Huniersvdle, NO 28075 (704]875-9092 Qualifiers Date: 05/11/2011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 11 of 17 `n s report snail riot be reproduced, except Ln tuil, without the written wrisant of Pa ce Analytical Services, inc.. aceAna&lical WWW oxc kaAl =- Project- CM1 Pace Project No.. 92,33621 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27286 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Or. Ashevitle, NC 28604 (a28)254-7176 QUALITY CONTROL DATA LABORATORY CONTROL SAMPLE: Parameter 602975 Units Spike Canc. LCS Result 2-Hexanone ug1L !DO 97.0 4-Chlorotaluene ug+L 50 SO.D 4-Methyl-2-pentanone (Ml6K) uglL 100 97.0 Acetone uglL 100 107 Benzene uglL 50 55.4 Bromobenzene ugX 50 54.4 Bromochloromethane ug1L 50 55.0 Bromodiahbromethane uglL 50 57A Bromororm uglL 50 51-2 Bromomelhane ugk 50 44-5 Carbon tetrachloride uglL 50 53A Chtorobenzene uglL So 54.3 Chloroelhane uglL 50 60.0 Chloroform ugA- 50 54-7 Chloromethane uglL 50 42.5 cis-1,2-Dichioroethene ugA- 50 53.8 cis-1,3-Dichiaropropene uglL 50 50.D Dlbromachtoramethane ugA- 50 57.3 Dibromomethane uglL 50 55-2 DichlorcdMuoromethane uglL 50 47.1 Diisopropyl ether uglL 50 54.7 Ethylbenzene uglL 50 59.5 Hexachloro-1,3-butadiene uglL 50 54.5 m&p-Xylene ug1L 100 120 Methyl-tert-butyl ether uglL 50 55-9 Methylene Chtoride ug& 50 56.6 Naphthalene ug)L 50 50.0 o-Xylene uglL 50 54-6 p-Iscpropyltoluens uglL 50 54.6 Styrene ugIrL 5G 55.0 Tetrachtorcethene uglL 50 56.0 Toluene uglL 5o 54.6 trans-1,2-Dichloroethene uglL 50 55.0 trans-1,3-Dichloropropene uglL 50 49.7 Tdchloroethene uglL 50 58.8 Tdchlorofluoromethane ug1L 50 51-5 Vinyl acetate uglL 1 GO 106 Vinyl chloride uglL 50 51.6 1,2-Dichloroethane-d4 (S) % 4-Bromofluoroberrzene (S) % Dibromafluoromethane (S) % TOluene-dS (S) % LCS % Rec % Rea Limits 97 70-144 120 70-130 97 70-140 107 50-175 111 70-130 109 70-130 110 70-130 115 70-130 102 70-130 89 54-130 106 70-132 109 70-130 120 64-134 109 70-130 85 64-130 108 70-131 100 70-130 115 70-130 110 70-131 94 56-130 109 70-130 119 70.130 109 7G-130 120 70.130 112 70-130 113 63-130 1GO 70-138 109 70-130 109 70-130 110 70-130 112 70.130 109 70-130 110 70-130 99 70-132 118 70-130 103 62-133 106 66-157 103 69-130 96 70-130 102 70-130 98 70-130 100 70.130 Pace Analytical Services, Inc- 9300 Klrrcey Ave. Suite 100 Hunters0e, NC 280743 (704)875-t3092 Qualifiers Date: 05/11/2011 04:15 P110 REPORT OF LABORATORY ANALYSIS Page 12 of 17 This report shall not be reproduced, except In full, without the wrl tie consent of Pace An alyllcal Services, Inc.. . � •i l lG�1rr aceAnaiXiCal� www.:ep7.�6s �.,m Project. CMI Pace Project No.: 9293621 Pace Analytical Services, Inc. 205 Easi Meadow Road - SuitoA Eden. NC 2728E (335)623•8921 Pace Analytical Services, Inc. 2225 Riverside Or A5hevile, NC 28W4 (B28)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincr ryAve. Suite 100 i-luniersville, NC 23078 (704)67Fr9092 MATRIX SPIKE & MATRIX SPIKE DUPLICAM. 602976 602977 NIS MSD 92916480111 Spike Spike MS MS❑ MS MST] %Rec Parameter LIMS Result Conc. Conc. Result Result % Rec % Rec Limits RPD Rua[ 1,1-Dichloroethene uglL ND 50 50 58.5 62.9 117 125 70-166 7 Benzene ug/L 0.84J 50 50 52.6 57.0 103 112 70-148 8 Chlorobenzene ug/L ND 5o 50 53.6 57A 107 114 70-146 7 Toluene uglL ND 50 50 53.9 57.3 108 115 70-155 6 Tridliorcethene ug/L 0.511 50 50 49.2 52A 97 105 69-151 7 1,2-DicNorcethane-d4 (S) % 114 114 70-130 4-Bromofluomberzene (S) % 92 90 70-130 Dibromofluorometharle (S) % 111 114 70-130 Touene-d8 (S) % 93 93 70-130 Date: 05/11/2011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 13 of 17 This report shall not be reproduced, except in full, without the written consent of Pace An aIyticai Services, 1nc.. / a 2 aceAnalyfical wwx:yyuain:s ^:,.r Project: CMI Pace Project No.: 9293621 Pace Analytical Semites, Inc. 205 East Meadow Read - Suite A Eden, NC 27288 (338)623-882l Pace Anarocal Servicai, Inc. 2225 Riverside Dr. Asheville. NC 2UO4 (828)251-7178 QUALITY CONTROL DATA Pace Analyttcai Services, ioc. 9800 Kincey Ave. Suite 1 DO Huntersvillo, NC 28078 (704)875-9092 QC Balch. MSV115148 QC Batch Method. EPA 8260 Associated Lab Samples:/3293621004 Analysis Method. Analysis Description: EPA 8260 8260 MSV Low Level METHOD BLANK: 603096 Matrix: Water Associated Lab Samples: 9293621004 Blank Reporting Parameier Units Result Lund Analyzed Qualirpers 1,1,1,2-Tetrachloroelhane ug[L N❑ 1.D 051081tl 09A8 1,1,1-Tdchioroelhane ug/L NO 1.0 0510811109.48 1,1,2,2-Telrachloraethane ug1L ND 1.0 0510811109:48 1.1,2-Trichloroothana ug/L ND 1.0 0510811109:48 1,1-Dichloroethane ug1L ND 1.0 0510811109:48 1,1-Dichloroethene ug1L ND 1.0 05/0811109:48 1,1-Dichloropropene ug/L NO 1.0 05/0811109:48 1,2,3-Trichlorobenzene ug/L NO 1.0 0510811109:48 1,2,3-Trichloropropane ug/L ND 1.0 0510811109:48 1,2,4-Trichlorobenzane uglL ND 1.0 051a811109:48 1,2-Dibrorno-3-chloropropane ug/L N❑ 5.0 05108/1109:48 1,2-0ibromoelhane (EDB) ug/L ND 1.0 05/08/11 09AB 1,2-Dichlorvbenzene uglL NO 1.0 OSM811109:48 1,2-❑ichlomethane ug/L ND 1.0 05/0811109:48 1,2-Dichloropropane ug/L ND 1.0 0510811109:48 1,3-Dichlorobenzene ug/L NO 1.0 0510811109:48 1,3-Dichloropropane t4L NO 1.0 0510811109A8 1,4-Dichlorobenzene ug1L NO 1.0 0510B11109AB 2,2-01 chi oropropane ug1L NO 1.0 05/08/1109:48 2-Butanone (MEK) ug/L ND 5.0 05/08/11 09.48 2-Chlcroloiuene ug)L NO 1.0 0510811109.48 2-Hexanone ug/L ND 5.0 0510811109:43 4-Chlorololuene ug1L NO 1.0 05/0811109:48 4-Melhyl-2-pentanane (MIBK) uglL ND 5.0 051a6111 09:48 Acetone ug1L ND 25.0 051DB/l 1 09:48 Benzene ug/L N❑ 1.0 0510811109:48 Bromobenzene ug1L ND 1.0 05(0011109:48 Bromochlommethane ug/L ND 1.0 0510811109:48 Bromedichloromethane ug/L ND 1,0 0510BJll09:48 Bromcfarm ug1L NO 1.0 05MEVIl09.48 Bromomethane uglL NO 2.0 0510B11109A8 Carbon tetrachloride ug/L NO 1.0 0510811109:48 Chlorobenzene ug ND 1.0 0510811109.48 Chloroethane uglL NJ) 1.0 0510811109:48 Chloroform ug/L ND 1.0 05108/1109,48 Chlaromelhane ug/L NO 1.0 0510811109:48 cis-1,2-0ichloroethene ug/L NO 1.0 0510811109:48 cis-1,3-Dichiorepropene ug/L ND 1.0 051081110948 ❑ibromochimmethane ug/L N❑ 1.0 0510811109748 Dibromomethene uglL ND 1.0 05108/1109.-48 Dichiorodiiluommethone uglL N❑ 1.0 0510811109:48 Diisopropyl ether uglL NO 1,0 05/08/11 09AS Ethylbenzene uglL ND 1.0 0510811109A8 Date: 05/11/2011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 14 of 17 This *por; shall net be ruproouced, excapl In full, without the written consent of Pace Analytical $eMces, Inc.. -�aceAnalytrca,t www.pe0H9bs.cem Project. CMI Pace Project No.: 9293621 Pace Anal yticaf 5"ices, Inc. 205 Fast Meadow Road - Suite A Caen. NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. AOeville, NC 28804 (r328)254.7176 QUALITY CONTROL DATA METHOD SLINK: 603096 Associaled Lab Samples: Parameter 9293621004 Units Matrix: Water Blank Reporting Result Limit Analyzed Hex achIcro-1,3-butadlene ug/L NO 1.0 05/t! 8!11 09:48 m&p-Xylene ug/L ND 2.0 05/08/11 %48 Methyl-tert-butyl ether ug/L NO 1.0 05/08/11 09:48 Methylene Chloride ug/L NO 2.0 05/08/11 09!48 Naphihalene ug)L ND 1.0 0510811109,48 O-Xylene ugJL NO 1.0 0510811109:48 P-Isopropylloluene ug& NO 1.0 05M/1109:48 Styrene ugIL NO 1,0 05108/1109A8 Tetrachloroethene tiglL NO 1.0 05/0811109:48 Toluene uglL NO 1.0 0510811109A8 trans-1.2-Dichloroethene UA N❑ 1.0 05108/1109:48 trans-1,3-❑ichloropropene ug1L No 1.0 0510811109748 Trichloroethene ug1L ND 1.0 0510811109748 Trichlorofluoromethane ug/L ND 1.0 0510811109:48 Vinyl acetate ug/L ND 2.0 05108/11 09:48 Vinyl chloride ug1L ND 1.0 05)09111 0948 1.2-DieNoroethane-d4 (S) % 115 70-130 05IM11 09:48 4-Sromalluorobenzene (S) % 97 70-130 05/08/11 09:48 Dibromofluoromethane (S) % 110 70-130 05/08/11 09.48 Toluene-d8 (S) % 100 70-130 05/08/11 09:48 Qualifiers V+BQRATORY CONTROL SAMPLE: Parameter 603097 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachlorcethane ug1L 50 55.0 110 70-130 1, 1, 1 -Trichloroetha no ug/L 50 55.2 110 70-130 1.1.2,2-Tetrachloroethane ug/L 50 52.3 105 70-130 1,1,2-Trichloroethane ug1L 50 51.8 104 70-130 1,1-Di0ioroethane uglL 50 54.2 108 70.130 1,1-Dichloroelhene uglL 50 56.4 113 70-132 1,1-Dichlaropropene uglt 50 48.7 97 70-130 1,2,3-Trichlorobenzene ug/L 50 58.1 116 70-135 1,2,3-Trichloroproparle ug1L 50 51.1 102 70.130 1,2,4-Trichlorobenzene ug/L 50 54.6 109 70-134 1,2-Dibromo-3-chloropropane ug1L 50 58.3 117 70.130 1,2-Dibromoethane (EDS) ug/L 50 52.5 105 70-130 1.2-Dichlorobenzene uglL 50 50.1 100 70-130 1,2-Dichlomethane uglL 50 55.1 110 70-130 1,2-1)ichloropropane uglL 50 49.9 100 70-130 1,3-Ol0lorobenzene ug/L 50 50.6 101 70-130 1,3-Dichloropropane ug/L 50 51.4 103 70-130 1,4-Dichlornbenzene ug1L 50 49.4 99 70.130 2,2-Dlchloropropane uglL 50 57.0 114 58-145 2-Buianone (MEK) uglL 100 116 116 70-145 2-Chlorotoluene ugfL 50 50.6 101 70-130 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvttle, NC 28078 (704)875.9092 Qualifiers Date: 05/11/2011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 15 of 17 This report shall not be reproduced, except In full, without the written consent a Pace Analytical Services, Inc.. aceAnalytcal w wp&-&%r6s.ma Pace AnatylieaI Services, Inc. 205 East M8adow Road - Suila A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Rivers de Dr. Asheville, NC 28804 {828}254.1116 QUALITY CONTROL DATA Project: CMI Pace Project No.: 9293621 LABORATORY CONTROL SAMPLE. 603097 Spike LCS LCS °I Rec Parameter Emits Conc. Result Yo Rec Limits 2-Hexanone 4L 100 114 114 70-144 4-Chloratoluene uglL 50 54.5 109 70-130 4-Methyl-2-pentanone (MIBK) uglL 100 109 109 70-140 Acetone ug1L 100 123 123 50-175 Benzene uglL 50 48.8 96 70-130 Bromobenzene uglL 50 51.3 103 70-130 Bromachloromethane ug(L 50 50.6 101 70-130 Bromodichloromethane uglL 50 54.8 110 70-130 Bromeform ug)L 50 56.3 113 70-130 Bromemethane ug1L ra0 61.3 123 54-130 Carbon tetrachloride uglL 50 53.2 106 7D-132 Chlorobenzene uglL 50 50.1 100 70-130 Chloroethane 4L 50 51.3 103 64-134 Chloroform uglL 50 54.7 109 70.130 Chloromethane u911- 50 52.4 105 64-130 cis-1,2-Oichlaroethene uglL 50 52.1 104 70-131 cis- 1,3-Dichlempropene uglL 50 55.7 111 70-130 Dibramochloromelhane ug1L 50 54A 109 70-130 Dibrom,omethane ug& 50 52.8 106 70-131 DicNorodifluoromethane uglL 50 51,3 103 56-130 ❑iisopropyl ether ugA- 50 52.1 104 70-130 Ethylbenzene ugll- 50 52.0 104 70-130 Hexacbloro-11.3-butadiene uglL 50 49.4 99 70-130 m&p-xylene ug1L 100 105 105 70-130 Methyl-tert-butyl ether uglL 50 54.3 109 TG-130 Methylene Chloride uglL 50 50.3 101 63-130 Naphthalene uglL 50 60.2 120 70-138 o-Xylene ugA- 50 54.2 108 70-130 p-tsopropylloluene uglL 50 53.9 108 70-130 Styrene tig1L 50 50,1 100 70130 Tetrachloroethene uglL 50 54.1 108 70-130 Toluene uglL 50 45$ 97 70-130 trans-1,2-Oichtoruethene ug1L 50 52.3 105 70-130 trans-1,3-Dichloropropene ugll_ 50 53A 106 70-132 T6chlorcethene ug1L 50 52.6 105 70-130 Trichlorofluoromelharie uglL 50 56.5 113 62-133 Vinyl acetate ug& 100 120 120 66-157 Vinyl chloride uglL 50 52.0 104 69-130 1,2-Dichloreelhane-d4 (S) % 102 70-130 4-Bromoftuarobenzene (S) % 102 70-130 Dibromoftuoromethane {S) % 101 70-130 Toluene-0 (S) % 99 70-130 Pace Analytical Serv1cws, Inc. 9800 Kincey Ave. Suite 1 W Hunlersville, NC 28078 (704}875-9092 Qualifiers Dale 05/11/2011 04:15 PM REPORT OF LABORATORY ANALYSIS Page 16 or 17 This report shall nat be reproduced, ekcept in full, wil hoot She written consent or Pace Analytical services, Inc.. ,xe;� www Pa�6:aSs.[:m Project CMI Pace Project No.: 9293621 DEFINITIONS Pace Analytical Services, inc. 205 East Meadow Road - Suite A Eden, NC 272BB (338)623-952: QUALIFIERS Pace AnatyIle at 5"icer, Inc. 2225 Riverside Dr. Asheville, NC 28W (828)254.7176 Pace Analytical Services, Inc. %00 KnceyAve. Suits 100 Hun!ersville, NC 28078 (704)875-W92 bF - Dilution Factor, If reported, represents the fa et or applied I the reported data due to changes in sample preparation, ditulion of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting Dmit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-13lphenylhyidrazine (8270 listed analyze) decomposes to Azobenzene. Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RP values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Lip U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylarnine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Ana lyztcaI is NELAP accred Ile d. Contact your Pace PM for the current list of accrediled analyzes. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS S2 Surrogate recovery outside laboratory control limits due to matrix interferences {confirmed by similar results from sample re -analysis}. Date- Ob111/2011 04 15 PM REPORT OF LABORATORY ANALYSIS Page 17 of 17 TInLs report shag: not be rapraiiucod, oxcap: in full, wilhdui the written consent of Pace Analyllcal Services, Inc,. a i�,��4 :. '�. 2ceAnal4ical - CHAIN -OF -CUSTODY I Analytical Request Document The Chain -&-Custody is a LEGAL DOCUMENT. All rclovant fields must he completed acaaataiy. i� . --- -...,- Page: of 3ectt�n A Section B Section C 1478471 R.qr. ad Giant Infomimon. Required Proiaci I'NomW!tOn� Invo.ce lnlo a lone ny: Repod To Anern on. core L T r L .4ddre s! f r � 1 p� Cagy TO; n ++ L fin S Ar-tT� � m Company Name: REGULATORY AGENCY G F NPDE3 r GROUND WATER i— DRINKING WATER UST RCRA r OTHER Email o: �P. C Pvchase Drd ra 14".. Pace 9uwc t a�eo�e; P Fax PrOprl Name P" Proj.cl Site Locsllon Manager: R. ud pu. DitalFAT: h p Prv1eC Nutn.bar ,L tfD , `�`- P Prono s. .2 -7 7 Requested Analysis Fl[tered (YIN) ��I SI-vn "' D Madt. Coda0 x a t.wcaw�+l mhmrwm �ryTH % , cr.,F 8 COLLECTED Prosorvnlhrus � Drantt7 Water OW g V Water WTWaste $ ci tcurvane Product !IK e y �p cn«rc3i*e STMT kNWiJNa w SvWSaud SL 0 rn SAMPLE ID ow L ? LA•Z, 0-91: Y Alf AR Sample 16s MUST 9E UNlgllE TS ❑w❑ ❑ � w n fi C y l41 !c Other Dr ou,.r x w 'wv L> Q uo 4 0 W DATE TIME DATE TIME x z z mi D T Pace Project No./ Lam I.O. 2 >.� , tia � 6t�ti•- - �Z ��La 3 6 7 B 9 16 1t l2 ADDITIONAL COMMENTS RELIN,]LOSHM BY (AFFILIATION DATE TIME AC D AFIt T1oN D E TIME SAMPLE CONDIMN5 t 6 V A A VA 411 3 _ 6 L.c SAAAPLER NAME AND VGNATURE a ORIGINALr y V z PLAINT Nam. of SAMPLER; i SIGNATURE of SAMPLER: ` DATE -Y w—v -- aam yar .r0 acropw* rara's NEf W my pwMw lem,. and .pmNrq tv lat. urge. w 1.6%p6r moeln for any ewaa.. bt paid _Vd. 30 d.y.. F-ALL •Q-naflr.w R7 - . . so ■ • - ^, .. �Face.4nalyfrcal -- - . -- - - - - Client Name: �— Project # � 2`3(c, z Where Received: Zuntersville ❑ Asheville ❑ Eden Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ C mercial Pace Other Optional - Custody y no Seals intact: ❑ yes ❑ no Projy flue,Date- T-- Sea! an Cooler/Box Present: ❑ pro.w Packing Material: ❑ Bubble Wrap ubble Bags ❑ None ❑Other Thermometer Used: lR Gun : T1101 Type of lie: a Blue None Samples on ice, cooling process has begun Temn rnrrA.rfinn Farfnr- Add f Suhtmet n •r- Corrected Cooler Temp.: C $lolo Biological Tissue Is Frozen: Yes No S Date and Initial of p e Ining contents: Temp should he above freezing to VC Comments: Chain of Custody Present: ye ❑No DMA 1. Chain of Custody Filled Out: yes No ❑wA 2- Chain of Custody Relinquished: res ONo OwA 3, Sampler Name & Signature on CDC: yes No ❑NIA 4. Samples Arrived within Hold Time: res ❑No ❑NiA 5- Short Hold Time Analysis (e72hr)- Dyes No ❑wA 6. Flush Turn Around Time Requested: Oyes ON- C311A 7, Sufficient Volume: res ❑No ©TA g. Correct Containers Used: yes ❑No ❑NIA g. -Pace Containers Used: .Gres ❑No ❑NIA Containers Intact: Elyes ONO OMAA 0- Filtered volume received for Dissolved tests Dye s No fA 11, Sample Labels match COC: 51(CII< s o ❑wA 12. 0-- q r7R3 tlra �¢ -Includes dateltimellalAnalysis Matrix: All containers needing preservation have been checked. es ONO ©NIA 13. All containers needing preservation are found to be in es ❑Na ❑N1A compliance with EPA recommendation- exception9' VOA, coliform, TOC. OdG, WI•DRO (water) Dyes ❑No Initial when compketed Samples checked for dechlorination: Dyes ❑Na OINIA 14. Headspace in VOA Vials f >6mmj: Dyes 2<o ❑NA 15, Trip Blank Present: Dyes ❑No !A 16. Trip Blank Custody Seals Present Oyes ❑No A Pace Trip Blank Lot # (if purchased): Client Notification) Resolution: Field Data Required? Y r' N Person Contacted: Date/Time: Comments' Resolution: SCURF Review;,_1 Date; .�!— t SRF Reviev Note: Whenever tt a discrepancy affecting North Carolina compliance samples, a copy Certification Office ( Le out of hold, incorrect preservative, out of temp, Incorrect containers) form wilf be sent to the North Carolina DEHNR F-C H R-CS-003-rev.03 13Apr2011 NCDENR — Remedial Construction Completion Repon July 20, 2011 MAC7EC Project 6628-08-4691 NVNCDOOM92 APPENDIX E INJECTION FIELD FORMS AND LOCATION PLAN ►4 1 - i �AIAW-2 �' EBMW-15 i. ARE/\ C (NOT COMPLETED)` — ,. / /- mm EBMW-23 BRICK MANHO 8-x6 h M'�!E r x •S_�y �ss Ty— EBIrW—I� a -is vil_es EBMW-24 A_a, • \ �•� _H, 6-xa EBMW--16 e_i l$s ~ k t A-9O Se H-9 A 6x• A-i7 A-66 fi� 14 F / EBMw-27 EBMw-18 W 5 I �rss EBMw-11 S �' r. A-7 "-On F-a' -pH 0-+7 B-+' a-�� a-;x s_,� Lit EBMw-22 a-,i0-5 34 9-1 0-1 lEBMw-28 A-;s � � � � A-'% N. BMW-14 •, a-� i a-i Q-] EBMw-6� 1 A- xI r A41 A-71 , � \ Jj+1 _ A 48 A_73 MW 4Wl,1 qf.A , AG A. ��'• A -By f6� A-x7 - AREA B _Sy�-� A-" EBMw-10 \�,. F-2t . EBMw-21 E W-7 N OEBMW-12 y I�I� A-]s EB1Aw-25 A-% A-iA ♦. �[j]y ]6 A A--7y T� A•30 A-xy 1*1 A-62 `�• A-6 IW A_-12+A A-yx is A-A5 -59 A-w •-IQ A-i9 A-U A�j.l + A A-36 A_x+ A-• t A 16A A..i A -ix EBMW-3 NO7£S: .-As A-aT EBMW-3 . AREA A BASE MAP AFTER SPATCO ENVIROMENTAL SERVICES A-50 1-14 A-/7 A-jx A-07 A-N F-{{ A-;/ -91 AAI F-4 A-10 fl3 EBMW-13 A-b — IV A-11 — — A-1 A:y A-3 I -5./ •-. — EBMW-30 mmEBMw-19 6TT A ] -� I A-1 YADM )rTGP OI 6AInf K / rAppl 9n"ER I � L EXPLANATION DRAWING No. 9-179D. FIGURE 2 ytiR MONITORING WELL LOCATIONS AFTER BLlNN ENGINEERING SURVEY MAP, PROJECT NO. 8020603 fLpw 6/6/04 (REWISED 10/24/05 and 10102106) SELECT MONITORING WELLS SURVEYED BY R.B. PHARR ON 6123111, ALONG WITH THE LOCATION OF ALL TEMPORARY INJECTION POINTS. STREAM OVERBURDEN WELLS - — — - PROPERTY LINE E BEDROCK WELLS —a— SEWER LINE UPPER BEDROCK INJECTION WELL (25-45•) — — — — APPROXIMATE TOP OF BANK I PILOT TEST INJECTION WELLS (ABANDONED) A-/ TEMPORARY OVERBURDEN INJECTION POINT APPROXIMATE SCALE IN FEET IMACTEC MON EK TCTAC A CASK Mr AC. CHARLOTTE• HARM CAII"A AS BUILT INJECT10N PLAN CMI WWTP ELKIN, SURRY COUNTY. NORTH CAROLINA FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: �- Date Drilled: J' /G - Borehole Depth: �y Date Borehole Date Injected: Abandoned: Time Start injection: Time Finish Injection: Lin 1 Lift 2 Lift 3 Notes Lift depth - a0d D3' - 17' Gals Solution CYS, i-�_ Pumping Rate 575 7 S $� COMMENTS: Field Rep-: Yh • k� - Borehole Number: A- 0 Date Drilled: Borehole Depth: { Date Borehole Date Injected: 1t; - I! Abandoned: S •� I r Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth D6 - a Gals Solution 9_5 Pumping hate COMMENTS: Field Rep-: r''' Borehole Number: 1�)- Date Drilled: Borehole Depth! Date Borehole Date Injected: Abandoned: S -17- Il Tirne Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 9 : Z)-7' Gals Solution Pumping Rate �• COMMENTS: Field Rep-: M EC FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: ' Hate Drilled: 5-- / 7 - I ( Borehole Depth 6 Date Borehole Date Injected: S 17- II Abandoned: .S- I V- II Time Start Injection: Time Finish Injection: Uf! 1 Lift 2 Lift 3 Notes Lift Depth 06 Gals Solution Pumping Rate COMMENTS: Field Rep.: - in-` K - Borehole Number: r Date Drilled: 1 7 Borehole Depth: a�S Date Borehole Date injected. Abandoned: '9-12. II Time Start Injection: Time Finish Injection: Lift 1 laft 2 Uf# 3 Notes Lift Depth Gals Solution a �S Pumping Rate S:.S` COMMENTS: Field Rep.: a Borehole Number: fit- 6 Date Drilled: Borehole Depth: _ Date Borehole Date Injected: J' J 7� Abandoned: 'S 47 P Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lilt 3 Notes Lift Depth g1 = ��� �` - f 7' 1;7' Gals Solution Pumping Rate COMMENTS: Field Rep.: l�'1 6,ev. ItP : t4�--'7 4. ff = Z�f-zo �1�7 I rl (i•�j.oF �k a►a�v� Z y ZC!-17 F- S� FIELD FORM - SOIL BORING AND INJECTION RECORD hg"� ?/I C1 r I Borehole Number: Date Drilled: �j -%� /� Borehole Depth: 00 Date Borehole Dateinjected: Abandoned: Time Start Injection: Time Finish injection: Lift I Lift 2 Litt 3 Notes Lift Depth a�v1- / �' 19 - / /'7 Gals Solution 1? Pumping Rate $T•S" COMMENTS: Field Rep.: �t - Borehole Number. Date Drilled:. '/ I� Borehole Depth: Date Borehole Date Injected: rr- f, Abandoned: J ' /,f- Time Start Injection: Time Finish Injection: Lit 1 Lift 2 Litt 3 Notes Lift Depth 3 - a n% fl' - ) 7 /7•' I Gals -Solution Pumping Rate {� COMMENTS. Field Rep.: � • kL Borehole Number: /+-/o Date Drilled: it Borehole Depth: Date Borehole Date Injected: Abandoned: Time Start Injection: Time Finish injection: Lift I Lift 2 Lift 3 Notes Lift Depth ;;)3• P3 p'- /7' 17 1 Gals Solution Pumping Rates COMMENTS: Field Rep.: �1 �. FIELD FORM - SOIL BORING AND INJECTION RECORD AWL--, (M Il Boreho her: - fl Date Drilled: Il Borehole Depth: Date Borehole Date Injected: Abandoned: Time Start Injection: Time Finish _1vidTom Lill 1 Lift 2 Notes Lift Depth Gals Solution Pumping Rate COMMENTS: field Rep_: YV\ % Borehole Number: - g Date Drilled: P Borehole Depth: Date Borehole Date Injected: Abandoned: Il Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 04�-- 0 1 /7- / Gals Solution Ps Pumping Rate if 5� COMMENTS: Field Rep.: Borehole Number: Date Drilled: ' 1 rr- I Borehole Depth: a _ Date Borehole Date Injected: - / Fr- p Abandoned. - Time Start Injection: Time Finish Injection: Litt 1 Lift 2 Lift 3 Notes Lift Depth a t% - [ al'/7 /P /�/_ Gals Solution Pumping Rate, 5` COMMENTS: Field Rep.: t FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: /3 Date Drilled: �`'g. I t Borehole Depth: Jq Date Borehole Date Injected: 1 Abandoned: A9-I1 Time Start Injection: Time Finish injection: Lift I Lilt 2 Lifr33 Notes Lift Depth 1 1-7- 17 Gals Solution �s �S rr Pumping Rate 6-. S COMMENTS: Field Rep.: WI ►�� Borehole Number: Date Drilled: Borehole Depth: Date Borehole Date Injected:- /9- !L Abandoned: J/ Time Start Injection: Time Finish Injection: Lill 1 Lift 2 Lift 3 Notes Lift Depth I of - 17 f J / y Gals Solution 'Ps- Pumping Rate <_ 3r COMMENTS: Field Rep.: ft,\ Borehole Number: ] - f Date Drilled: 5 19 - It Borehole Depth: 96 Date Borehole Date Injected: Abandoned: Time Start injection: Time Finish injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 6 - da - f ,y %,?- Gals Solution i Pumping Rate COMMENTS: Field Rep.: FIELD FORM - SOIL BORING AND INJECTION RECORD - Borehole Number: - ( Date Drilled: I`P' I Borehole Depth: 0471 + Date Borehole Date Injected: Abandoned: j J ef- f1 Time Start injection: Time Finish Injection: Lift 1 Lift 2 Litt 3 Notes Lift Depth - do 901 /6 161 /� Gals Solution Pumping Rate �. COMMENTS: Field Rep_: Borehole Number: A - &/'7 Date Drilled: 19 ' d Borehole ❑epth: ov Date Borehole Date Injected: Abandoned: 9 Time Start injection: Time Finish injection: Lift 1 Lift 2 Litt 3 Notes Lift Depth Q' '% ' f i - 1 S �--- Gals Solution Pumping Rate K COMMENTField Rep._ Borehole Number: Date Drilled; Borehole Depth: Date Borehole • Date injedted::.. - 11 Abandoned: 5--1,9 — r+ Time Start Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Sol Pumpin ' S r COMMENT& - Field Rep.: (� •� µ_. FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: /9-�� Borehole Depth: COO, Date Borehole Date Injected: Abandoned: <_ Time Start Injection: Time Finish injection - Lift 1 Litt 2 Lift 3 i Notes Lift Depth Do -!r-7' 12 - Pr Gals Solutions j Pumping Rake 6 • S 6. S sr 5- COMMENTS: Field Rep.: Borehole Number. A- ao Date Drilled: Borehole Depth: go ` Date Borehole Date injected: - I Abandoned:- 19 it Time Start Injection: Time Finish injection: Lift l Litt 2 Ld 3 Notes Lift Depth j- )'7 IT— A - Gals Solution r%0 9S Pumping Rate %,,r % 6. COMMENTS: Field Rep_: >� kQ- Borehole Number: Date Drilled: I l Borehole Depth: Date Borehole Date Injected: S QQ�- I t Abandoned' S'' a b' it Time Star! Injection: Time Finish Injection: Lift t Lift 2 Lrfl 3 Notes Lift Depth Gals Solution Pumping Rate �. COMMENTS: Field Rep.: Y►'L L FIELD FORA! - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: , a - It Borehole Depth: Date Borehole Date Injected: 1/ Abandoned: -)-0 - It rime Start Injection: Time Finish Injection: Lift 1 Lift 2 Lill 3 Notes Lift Depth aj - 17 17 • /� /S I� Gals Solution Pumping Rate COMMENTS: Field Rep.: Borehole Number: Date Drilled_ - ao • 1 Borehole Depth: Date: Borehole Date Injected: - aJ - ) I Abandoned: r Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Ui! 3 Notes Lift Depth Q p' _ 1-7 "- J<- /S - 13 Gals Solution Pumping Rate f �• COMMENTS: Field Rep.: Borehole number: Date Drilled: 'S" O o - A Borehole Depth: Date Borehole Date Abandoned. aa. N ime Start injection: Time Finish Injection: Lift 1 Lift 2 LiR 3 Notes Lilt Depth Gals Solution Pumping Rate Sr COMMENTS: Field Rep.: L FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: v Date Drilled: — Borehole Depth CP1 Date Borehole Date Injected: Abandoned: '�-- -)0- Time Start Injection: Time Finish injection: Lift t Ltft 2 taH 3 Motes Lift Depth c-� 1- 1 F ! ,F- 15 I s Gals Solution Pumping Rate ,f • S COMMENTS: Field Rep-: k - Borehole Number. Date Drilled: i4 Borehole Depth: Date Borehole Date Injected: S- as - IJ Abandoned: Time Start Injection: Time Finish Injection: Litt 1 Lift 2 Litt 3 Notes Lift Depth ce�o Gals Solution Pumping Rate S• COMMENTS: Field Rep.: -q— Borehole Number: Date Drilled: $- Jc>- Borehole Depth: Date Borehole Date Injected: 5" a o _ JJ Abandoned: S • Ji Time Start Injection: Time Finish Injection: Lift 1 Litt 2 Lift 3 Notes Lrft Depth / L /6 - A/ /V /a Gals Solution Pumping Rate s COMMENTS: �j �,� �������� �,� Field Rep.: ti� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: A, Date Drilled: Borehole Depth: (3 Date Borehole Date Injected: Abandoned: C- �!, • ( Time Start Injection: Time Finish Injection: Lift I Lift 2 Uft 3 Notes Lift Depth . 17 %7. 1 /S- /_7" Gals Solution IV 9< Pumping Rate 7. v ri. 1-- 5' COMMENTS: Field Rep-: -��- Borehole Number: Date Drilled: 0 - j j Borehole Depth: ' Date Borehole Date Injected: j*J Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 tr Notes Litt Depth 14-7'1� Jd -Iy Gals Solution �r Pumping Rate ;? �S COMMENTS: Field Rep.: t•ti��c �- Borehole Number: A Date Drilled: Borehole depth: C90 ` Date Borehole Date Injected: 5 -+j Abandoned: 5-:) j1 Time Start Injection: Time Finish Injection: Lift'I Lift 2 Lift 3 Notes Lift Depth Gals Solution $ 7 Ibr f1 Pumping Rate COMMENTS: Field Rep.: I'�• �k�- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: A- 3! Date Drilled: Borehole Depth: I Date Borehole Date Infected: Abandoned: Time Start Injection: Time Finish Injection: Lift i Lift 2 LA 3 Notes Lit Depth 01 - 18 - A & Gals Solution �j K_ Q Pumping Rate COMMENTS: r , Field Rep.: f*,r..c.-rlg/r. Borehole Dumber: Date Drilled: - a3 ' tl Borehole Depth: 00i Date Borehole Date Injected: 5- �3• �� Abandoned: 'T"a7- ime Start Injection: Time Finish Injection: Lift i Lift 2 [A 3 Notes Lift Depth 0 - 19 lr l-? Gals Solution 9� 17�_ Pumping Rate yr S COMMENTS: Field Rep.:'"�� Borehole Number: A-22 Date Drilled: Borehole Depth: Date Borehole Date Injected: S' �s�' l Abandoned: ime Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 dotes Lift Depth 00 f ]? / • 1 I S - !-? Gals Solution Xr Pumping Rate COMMENTS; Field Rep.: �"•� t� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number Date Drifted: S - - f Borehole Depth: �d Date Borehole Dateinjected: Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Litt 3 Notes Uff Depth oQD— 1 Gals Solution CY0 0 Pumping Rate COMMENTS: + '� Field Rep.: �• ��wov%4 Borehole Number Date Drilled: 5 =- j! Borehole Depth: ZZ _ Date Borehole Date injected: Abandoned: Time Start Injection: Time Finish Injection: Litt 1 Litt 2 Litt 3 Notes Lift Depth (9.;) - 0 19 • ? 17- /S Gals Solution _ Pumping Rate COMMENTS: Field Rep.: ,k s_7�qr It Borehole Number: (A-f Date Drilled: { Borehole Depth- .2-q Date Borehole Date Injected: It Abandoned: Time Start Injection: Time Finish Injection: Lift I Lift 2 Lift 3 Motes Lift Depth /7 Gals Solutions Pumping Rate -7-( �f S COMMENTS: Field Rep.: iY\ �� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: A - Date Drilled: Borehole Depth: Date Borehole Date injected: S -c-) q - j Abandoned: Time Start Injection: Time Finish injection: Lift 1 Lift 2 UR 3 Notes Litt Depth q- a r I7 Gals Solution -! t.Irl+r Pumping Rate COMMENTS: Field Rep._ - ►� Borehole Number, Date Drilled: S'ad' Ji Borehole Depth: Date Borehole Date Injected: j .J- JJ Abandoned. 5-,D4- P Time Start Injection: Time Finish injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 2 go_ I Gals Solution 11__6_ r J" Pumping Rate 9 f COMMENTS- Field Rep.: 4 Borehole Number: -A- Date Drilled: Borehole Depth: 3 Date Borehole Date Injected: - I Abandoned: Time Start injection: Time finish Injection: Lift 1 !'rift 2 Lift 3 Notes Litt Depth IF- K Gals Solution Pumping Rate COMMENTS: Field Rep.: k`"��- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole plumber: Date Drilled: I rl Borehole Depth: a y Date Borehole Date Injected: S - C� y- ] Abandoned: Time Start Injection: Time Finish injection: Lift 1 Lift 2 Lift 3 Notes Licit depth V -; I 9 i-% 9 I Q" Gals Solution Pumping Rate COMMENTS: Field Rep.: > /� 1 Borehole number: A � Date Drilled: S - � Borehole Depth: �-�- Date Borehole Date injected: Abandoned: A- ime Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Z?rl'f814 rj 1 17-/ Gals Solution Pumping Rate r7 s� S S• S COMMENTS: Field Rep.: Borehole Number: jl� - c) Date Drilled:- fr Borehole Depth: cgz/ Date Borehole Date lnjeated: d- P Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Litt 2 Lift 3 Notes Lift Depth cf - 1 1(91- /`F 1 /? • -7 Gals Solution '► ! r Pumping Rater COMMENTS: Field Rep_: .. +� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number:-40 1/.; Date Drilled: Borehole Depth: Date Borehole Date injected: Abandoned: S- J - 11 Time Start Injection: Time Finish Injection: Lift t Litt 2 Litt 3 Notes Lift Depth 27-Z 1`rZY- Zy 1$' t� Gals Solution 1-5- Pumping Rate {, COMMENTS: Field Rep_: Borehole Number: -� Date Drilled: Borehole Depth: 07 Date Borehole Dale Injected: Abandoned: 6 — d - fl Time Start Injection: _ Time Finish Injection: Lift i Lift 2 Litt 3 Notes Lift Depth -i tv) �+ Gals Solution Pumping Rate 5'r G COMMENTS: Field Rep.: t1 "Z - 1� l -_ .61 Borehole Number: JS y- Date Drilled: �� �r `Borehole Depth: 1,q "Lsr Rate Borehole Date Injected: j - - tl Abandoned: Time Start Injection: Time Finish Injection: Lift l Lilt 2 Lilt 3 dotes Litt Depth a - 14 Iq'- t7 Gals Solution F_ .�� �.• '� �/� �`: Pumping Rate COMMENTS: Field Rep.: ���-L FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: A- q6 Date Drilled. i�-aS-1f Borehole Date Borehole Date Injected: S-alb _ i Abandoned: Time Start Injection: Time Finish Injection: Litt 1 Lift 2 Lit 3 Notes Lift Depth �Z-�'F �g—r7 Gals Solution fS Pumping Rate g COMMENTS: Field Rep.: C- - Borehole Number: Date Drilled: S^ a!� - 1t Borehole Depth:,Pf--, I Date Borehole [late Injected: � � �T ' l i Abandoned: l Time Start Injection: Time Finish Injection: Lift 1 Litt 2 Lift 3 Notes Lift Depth ZZ-11 L-7-� 1 --17 A--K-Y 7f-1 Gals Solution 19;s- § Pumping Rate F COMMENTS: Field Rep.: OA Borehole Number: A - Date Drilled: Borehole Depth Date Borehole Date Injected: Abandoned: S X ` ( l Time Start Injection: Time Finish injection: Lift i Lift 2 UR 3 Notes Lift Depth - jG JF- 16 Gals Solution Pumping Rate 6 COMMENTS: Field Rep.: Pri y In FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Humber: �- �� Date Drilled: Borehole Depth: �t Date Borehole Date Injected: t) Abandoned: S-as- ri Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth a I - / V l F - 16 16 - Gals Solution 157s- Pumping Rate COMMENTS: Field Rep-: Borehole Number: A -s o Date Drilled: S--QS- A Borehole Depth: Date Borehole Date Injected: Abandoned:-c75' tl Time Start Injection: Time Finish Injection: Lift i Lift 2 Lift 3 Notes Lift Depth f - / �_ 1v - IG Jd - /S/ Gals Solution SS �,rArL Pumping Rate it COMMENTS: Field Rep_: r ,k� Borehole Number: A-:5-t Date Drilled: Borehole Depth -- Date Borehole Date Injected: - ' 11 Abandoned: S - S' 0 ime Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth a1- IF- IG e• 1 Gals Solution rn- Pumping Rate COMMENTS: Field Rep_: 1,•._., � FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole dumber: - v� Date Drilled: C 75 i k Borehole Depth: Date Borehole Date Injected: S Abandoned: Time Start:ln}ection: Time Finish tnjecbon: Lift t Lift 2 Lift 3 Notes Lift Depth Gals Solution F5 �Sr Pumping Rate 6. COMMENTS: Field Rep.: - Borehole Number: f-1- t; Date Drilled: J S -I I Borehole Depth: Date Borehole Date Injected: S - ! I Abandoned: Time Start Injection: Time Finish Injection: Lift i Lift 2 Lift 3 Notes Lift Depth qwax-jv Gals Solution R 7 9- &5f` Pumping Rate 6 COMMENTS: Field Rep_: Ir�t :x Borehole Number: q Date Drilled: S-- a S - j{ Borehole Depth: �3 Date Borehole f Date Injected: �• �$' - It Abandoned: 6- ime Start Injection: Time Finish Injection: Lift 1 Lift 2 Lilt 3 Notes Lift Depth F A Gals Solution T4 Pumping Rate COMMENTS: Field Rep.:•c FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: date Drilled: S-- r II Borehole Depth: Date Borehole Date injected: Abandoned: S ar' ll Time Start Injection. Time Finish Injection. - Lift ? Litt 2 Lift 3 Notes U t depth i- 1k )r-16 16 1 Gals Solution S Pumping Rate .714110 -+1IV I' COMMENTS: Field Rep.: - Borehole Number: - !�-G Date Drilled: 6 ' �.E Borehole Depth: �Q Date Borehole Date Injected: Abandoned: Time Start Injection: Time Finish Injection: Lilt f Lift 2 Lftt 3 Notes Lift Depth ao- Gals Solution !�T f f Pumping Rate r% 7. ] 6 y COMMENTS: Field Rep.: l� l K � Borehole NumberA- S7 Date Drilled: Borehole Depth: Date Borehole Date Injected: Abandoned: S-c_�G - Time Start Injection: Time Finish Injection: Lift I Lift 2 Lift 3 Notes Lift Depth 's 2 � a d - at ;A - 1 I Gals Solution b Pumping Efate II COMMENTS: Field Rep.:��-� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: 14 Spa Elate Drilled: �'- P-C I Borehole Depth: 911 Date Borehole Date Injected: -99 - I t Abandoned: s- aG- 11 Time Start Injection: Time Finish Injection: Litt 1 Lift 2 Lift 3 Notes Lift Depth 0�1 - i4 /?- ) ? 1-7- 14 Gals Solution Pumping Rate 7.5 COMMENTS: Field Rep-: f-y\ Borehole Number. Date Drilled: c)b- I Borehole Depth: t Date Borehole Date Injected: S--ab- 1 Abandoned: rime Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth /?_ 15 Gals Solution ¢ 9r Pumping Rate ] 7, d COMMENTS- Field Rep.: A_ Borehole Number: Hate Drilled: Borehole Depth: t Date Borehole Date Injected: Abandoned: Time Start lnjeCbDn: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth [ - — r f Gals Solution ? Pumping Rate COMMENTS: i f Field Rep_: i'►\ ►�� t. rt�� n FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number.-0 Date Drilled: S"af • jl Borehole Depth: Date Borehole Date Injected: Abandoned: Time Start Injection: Time Finish Injection: Lift t Lift 2 Lilt 3 Notes Lift Depth at- I is- It ]- Gals Solution la o IDa Pumping Rate 7 S 7•f 6 COMMENTS: Field Rep.: Borehole Number: fA' - Date Drilled: �5 -a6 - [ Borehole Depth: Date Borehole Date Injected: 9�_- 44 - t l Abandoned: Tin* Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 4 I 1 Gals Solution Pumping Rate t7, 7. { COMMENTS: Field Rep-: 'c- Borehole Number: - (, Date Drilled: JG - t Borehole Depth: a Date Borehole Date Injected: �5_- aG - i t Abandoned: Time Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth )I- j7 17-15 Gals Solution Pumping Rate 9. � COMMENTS: Field Rep-: ern A< -A-- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: 1 ` ^ "4 Date Drilled: 6 - �� Borehole Depth: Date Borehole Date Injected: S- j 1 Abandoned: It Time Start Injection: Time Finish Injection: Litt t Lift 2 Lin 3 Notes Lift Depth c4f - j 9 M ' 1? Gals Solution 0 J�o Pumping Rate COMMENTS: Field Rep.: Borehole Number: f - C5 Date Drilled: Q16 - Jt Borehole Depth: Date Borehole Date Injected: S- 11 Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Litt 2 Lift 3 Notes Lift Depth aQ a-0 - I N- 16 Gals Solution pb J i'b f D b Pumping Rate 7.S s $ COMMENTS: Field Rep.: Borehole Number: Date Drilled: S - 26 - kL Borehole Depth: Date Borehole Date Injected: a6 - IL Abandoned: $'� ZG• [t Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 7 - - r- IG Gals Solution S { Pumping Rate ? 7►t C COMMENTS: Field Rep-: FIELD FORM - SOIL BORING AND INJECTION RECORD C-7G-r/ Borehole Number: - { Date Drilled: Borehole Depth -- Date Borehole /� e{ Date injected: -ZG-f1 Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth ,Q - 1-7 j 7 --1 C5, 5"- 1 -711V I� Gals Solution Pumping Rate COMMENTS: Field Rep.: - Borehole Number: - b% Date Drilled: rj Borehole Depth: Date Borehole Date injected: Abandoned: Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 2 I- f 44P Gals Solution Pumping Rate COMMENTS: Field Rep-: Borehole Number: Date Drilled: IBorehole Depth: j9 Date Borehole + l Date injected: -4-?-f I Abandoned: Z- 7 Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 1 Notes Lift Depth /Li - f '-L- -71 M1 t i Gals Solution Pumping Rate COMMENTS: Field Rep.: ' k-G FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number; i" ' { ~ Date Drilled: S Z7 ! I Borehole Depth: Date Borehole Date Injected: S- 1� 1 Abandoned. y [ r r Awe- -7 rtv/// Time Start Injection: Time Finish Injection: Lift i Lift 2 Uit 3 Notes Lift Depth 1 9 - l G —f 1 "r �— J v%4-- -7 1134,11 Gals Solution W4 Pumping Rate COMMENTS: field Rep_: Borehole Number: P� -r][ Date Drilled: S 1.27I1► Borehole Depth: Date Borehole Date injected: rl 77 1 f Abandoned: -7 t ic-1 y Time Start Injection: Time Finish Injection: Lift I Lift 2 Lift 3 Notes Lift Depth /fn -( 'f Icy —1 Z Vv '_ /(t-/ rI Gals Solution c r Pumping Rate COMMENTS: Field Rep.: Borehole Number: Date Drilled: 5 / Z7/1 f Borehole Depth: Date Borehole7 �Irl� b Date Injected: C-Z -11 ►► Abandoned: ] [ 2, 7 / 1 1 ime Start injection: Time Finish injection: Lift I Lift 2 Lift 3 Notes Lift Depth r* rT - l if 4 i Z 1 7 tirl `+ Gals Solution F Pumping Rate i COMMENTS: - Field Rep_: rf�e- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: rA^ 13 DateDrilled- ��Z { rl Borehole Depth: b � Date Borehole Date Injected: S rf Z '7 1 Abandoned' 577 7 f Time Start Injection: Time Finish injection: Lift 1 Litt 2 Lift 3 Notes Lift Depth /& r r 3 13 r r Gals Solution J)- Pumping Rate COMMENTS: ( r Field Rep.: - r' dA"-f- 'f, �q* Borehole Number: Date Drilled: Z-7 r' + Borehole Depth: �$ Date Borehole Date injected: -7 1 1 Abandoned: yam/ g-P I I Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals SoMion S Pumping bate OMMENTS: Field Rep-: Borehole Number: -- DateDrilled. Borehole Depth: I -E-7 - y v Date Borehole �r 3 a Dateinjected: _ i Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lilt 3 Notes Lilt Depth isr —i T r— us I �j t► Gals Solution Si m 1fid 1, Pumping Rate COMMENTS: Field Rep.: 1�� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: 3i f r Borehole Depth: Date Borehole � 1�8"{ t► Date Injected: C' 3 Z; I { Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth I Ir r► , (5- "3 iv- ( k Gals Solution f Pumping Rate COMMENTS: Field Rep_: I- �— Borehole Number: A _ ?`� Date Drilled: �'")� t ' Borehole Depth: b Date Borehole Date Injected: Abandoned: 5,0 r 1 ­7 r or LL, Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth f jr- 1 { S— 17 ) 3— 1 ► xt- - 71►r1►. Gals Solution Pumping Rate COMMENTS: Field Rep.: AiA Borehole Number: 7 Date Drilled: t of 3'RIK Borehole Depth: f q Date Borehole Rate Injected: j 13011► Abandoned: SD (I ({ {� Time Start Injection: 'Fiore Finish Injection: Lift 1 Lift 2,J 3 Notes Lift Depth �� {i — % T /JUft J 7 rI z Gals Solution Pumping Rate COMMENTS: Field Rep_: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: 5 R Borehole Depth' Date Borehole Date Injected: - - 11 Abandoned: 5' 1 Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth I `1 t q F� 14 ID Gals Solution �,rj V Pumping Rate G COMMENTS: Field Rep-: •' T''�� Borehole Number: - 0 Date Drilled: - l - t Borehole Depth: Date Borehole Date Injected: r, - 3 i - iAbandoned: 5-s - t Time Start Injection: Time Finish injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth i' j S 1 13, It Gals Solution 9( Pumping Rate 6 COMMENTS: Field ReP-Y'��� Borehole Number: A Date Drilled: - P' it Borehole Depth: ` Date Borehole Date Injected: S - 3 j Abandoned: �g- 21-11 Time Start Injection: Time Finish injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth a )?- f ' J a IT Id-1 Gals Solution 07 fr Pumping Rate Y 6 COMMENTS: Field Rep.:-- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Q. Date Drilled: Borehole Depth: f Date Borehole Date Injected: S- 3 f ' If Abandoned: Time Start Injection: Time Finish Injection: Lilt 1 Lift 2 Lilt 3 Notes Lift Depth q - a Gals Solution a P Pumping Rate COMMENTS: Field Rep_: +� eW A .�` r S-• Borehole Number: Date Drilled: Borehole Depth: J9' Date Borehole Date Injected:- �1. ji Abandoned: S`-_;(-)1 Time Start Injection: Time Finish Injection: Lift 1 Lilt 2 Lift 3 Notes Lift Depth 19 IG 16 . Jq I�" I'� Gals Solution 950 Pumping Rate 7 S 7 r 6 COMMENTS: Field Rep.: V, \\+— Borehole Number: - Dale Drilled: Borehole Depth: 6 ' Date Borehole 1 Date Injected: Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Litt Depth A- 2- r?1 'Fr Gals Solution 7W II Pumping Rate �� 7•� 6 COMMENTS: Field Rep.: Y, � � FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: - �J- lr* Borehole Depth: Date Borehole Date Injected: Jy • N Abandoned: S_- Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Litt 3 Notes Lift Depth 7 Gals Solution �j ��� •y'�Cri l t Pumping Rate '7�_ COMMENTS: Field Rep-:, Borehole Number: C- S Date Drilled: L Borehole Depth: Date Borehole Date injected: S - 31 - II Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lilt 3 Notes Lift Depth 14 0 - P 17. 15 Gals Solution J Pumping Rate S S ;7 S COMMENTS.- Field Rep.: r- Borehole Number: - Date Drilled: S---?I- A Borehole Depth: l 9 Date Borehole Date Injected: Abandoned: Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Solution t Pumping Rate 6 COMMENTS: Field Rep.: ?^" +-�- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: - `] Date Drilled: Borehole De r-- -?I- !� pth: Date Borehole Date Injected: Abandoned: __ W_ /I Time Start Injection: Time Finish injection: Lift I Lift 2 lift 3 Notes Lift Depth 9i • 17 )T I S iS - 13 Geis Solution 1-If Pumping Rate COMMENTS: Field Rep.: N - Borehole Number: Date Drilled: Borehole Depth: Date Borehole Date Injected: 1- t Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Litt 3 Notes Lift Depth d - r7 Z- 15 15 - Gals Solutions Pumping Rate 6 COMMENTS: Field Rep.: 114 . Borehole Number: Date Drilled: 6 - f ' i1 Borehole Depth'. Date Borehole Date Injected: - Abandoned: 6 - j Time Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth Q- 1 ? - I S Gals Solution ?s GS Pumping Rate 7 S ? G COMMENTS: Field Rep.: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Dumber: L] - l'd Date Drilled: G -1- Ir Borehole Depth: �V Date Borehole Date Injected: ( I- 1 Abandoned_ 6- Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Litt 3 Notes Lift Depth 19 A:IEf?-I,? Ac-/� Gals Solution d �� Pumping Rate COMMENTS: Field Rep.: -� - Borehole Number: �' �� Date Drilled. f Borehole Depth: + Date Borehole Date Injected: ❑` 1- 11 Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 I1R 3 Notes Lift Depth d 5- - a3 - 1 `1 1 `I ' 1? Gals Solution �7 Pumping Rate COMMENTS: Field Rep.: Y"'A�' �- Borehole Number: Date Drilled: y - J Borehole Depth: C -al Date Borehole Date Injected: G - l i Abandoned: Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Litt Depth ac7 - I? 1;?- r S- IS - /'.? Gals Solution �p Pumping Rate COMMENTS: Field Rep.: i►'�►�-� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number:Date Drilled: 6 - 1-i i' Borehole Depth: Date Borehole Date Injected: - J - 11 Abandoned: 6 - Id ( Time Start Injection: Tune Finish injection: Lit i Lift 2 Lift 3 Notes Left Depth 9- C G - N N-1 d2 Gals Solution �7 Pumping Rate r% tS 64, COMMENTS: Field Rep_: Borehole Number: "�� Date Drilled: t4 i'+ 1r► Borehole Depth: Date Borehole Date Injected: " Abandoned: 1, Time Start Injection: Time Finish injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth da- 19 / T ]2 l7 /:�_ Gals Solution 4; � & Pumping Rate 7 f COMMENTS: Field Rep.: Borehole Number: - s hate Drilled: G 1; I I Borehole Depth: Date Borehole Date Injected: 6-1- )1 Abandoned ,(' I - Time Start Injection: Oo r.. Time Finish Injection: LM 1 Lift 2 Lift 3 Notes Lift Depth 15 l§ • 1�? _?• 1( Gals Solution $' 'J 0 7U rb Pumping Rate 7 S 9, < COMMENTS: Field Rep.- ■`(mot FIELD FORM - SOIL BORING AND INJECTION RECORD i Borehole Number: - r!6 Date Drilled: 6- J - j Borehole Depth: Date Borehole Date injected: Abandoned: 6 - f - 1 r Time Start Injection: Time Finish Injection: Lift 'I Lift 2 Lift 3 Notes Lift Depth J q- 16 Gals Solution �c? Pumping Rate 7 i G COMMENTS: Field Rep.=-.,�•—� Borehole Number: • Date Drilled: G - !t Borehole Depth: /� Date Borehole Date injected: G • a- e i Abandoned: Time Start Injection: Time Finish injection: Litt i tiff 2 Lift 3 Notes Lift Depth Q- 6 1� • 1� �� la Gals Solution �d d Pumping Rate � f 7 t; f7, f COMMENTS: Field Rep.: �`•'L Borehole Number: Date Drilled: �-- 1+' Borehole Depth: 16P, Date Borehole Date Injected: Abandoned: 6 t{ Time Start Injection- Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth 1S Gals Solutions �d Pumping Bate�- COMMENTS: Field Rep-: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: L5 ' [ Date Drilled: G -a' l l Borehole Depth: p ' Date Borehole Date Injected: G-1- ll Abandoned: G •Q- /I Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Solution �D Pumping Rate 6X % 6 COMMENTS: Field Rep_: - �-- Borehole Number: >_k Date Drilled: 6 - -, - 1 ( Borehole Depth: J if Date Borehole Date injected: 6- a- t{ Abandoned: G-ate It Time Start Injection: Time Finish injection: Lift 1 Litt 2 Lift 3 Notes Lift Depth i'S ) S - r3 3. H Gals Solution RZ) 90 Pumping Rate 6, � COMMENTS: Field Rep.: ►' \1<1 � Borehole Number: Date Drilled: 6 -�- 11 Borehole Depth: Hate Borehole Date Injected: - ai - I Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth TT - / Gals Solution Pumping Rate `% 6 COMMENTS: Field Rep.: v_ •�` FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: A- Date Drilled: G - ox . I Borehole Depth: Date Borehole Date Injected: 6 - a - It Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Litt 2 lift 3 Notes Lift Depth /If - 15 /S - ! /V - 11 Gals Solution Pumping Rate 7 rf G COMMENTS: Field Rep.: -' Y►� t� Borehole Number. -A- 'R6 Date Drilled: G - j i Borehole Depth: 7 Date Borehole Date injected: 6-,� - 1 Abandoned: 6-a- j ime Start injection: Time Finish Injection: Lit 1 Lift 2 U# 3 Notes Lift Depth 7- L Ia Gals Solution Pumping Rate 9 7 COMMENTS: Field Rep.: Borehole Number: - Date Drilled: Borehole Depth: I d Date Borehole Date Injected: _ a- I L Abandoned: G- 3- I C Time Siam Injection- Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth /_?, Il Gals Solution Pumping Rate COMMENTS: Field Rep.: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: A' 90 Date Drilled: G - a - 1 1 Borehole Depth: ' Date Borehole Date Injected- (p t 7,t u Abandoned: (oo L. Time Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Holes Ulf Depth f %-1 Y - Gals Solution IFS A Pumping Rate (. s- 6 .S G COMMENTS: Field Rep.: Borehole Number: Date Drilled: 6,- -7- P Borehole Depth: J% Date Borehole Date Injected- G - Abandoned: 6 --?" Il Time Start Injection: ,'Q% Time Finish Injection: Lift 1 Lift 2 Litt 3 Notes Lift Depth 7- Gals Solution r] fit} �a Pumping Rate (, COMMENTS: Field Rep_- G2 Borehole Number: &Cx) Date Drilled: . f Borehole Depth: Date Borehole Date Injected: 4131m Abandoned: 60r3J11 Time Start Injection: 0 SI Time Finish Injection: 10; 11 Lift t Lift 2 Lift 3 Notes Lift Depth Ir? V - I Gals Solution �V Pumping Rate COMMENTS: Field Rep.: r- FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole number: -o13 Date Drilled: 6-2- // Borehole Depth: Id Date Borehole Date Injected: Abandoned: 6'-_�- Time Start Injection: /0;5 Time Finish Injection: /1` 37 Litt 1 Lift 2 Lstt 3 Notes Lift Depth IJ IS" -lam I~?-11 Gals Solution Irb &gb go Pumping Rate 1 (. ,S . C: COMMENTS: Field Rep-: - - Borehole Number: �'�I Date Drilled: Borehole Depth: / rr Date Borehole Date Injected: Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Solution 60 Pumping Rate c COMMENTS: Field Rep.: Borehole Number: 0 - X Date Drilled: ' }' 11 Borehole Depth: 1� Date Borehole Date Injected: - �- >{� Abandoned: G - 2 ' 1� Time Start InjectioTime Finish Injection: Lift 1 Lift 2 Lift 3 Notes Litt Depth ��- ►� 1S- 1� l� -1� Gals Solution Pumping Rate �• C• COMMENTS: Field Rep.: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: 'dp Date Drilled: 6---? Ir Borehole Depth: Date Borehole date Injected: Abandoned. - Time Start Injection: ." Time Finish Injection: Lift 1 2 Litt 3 Notes Lit Depth �9 I't `tit X- /7 1L1 Iv� Gals Solution frO� Pumping Rate 6 G COMMENTS: Field Rep.: Borehole Number: �- Date Drilled: Borehole Depth: Date Borehole Date Injected: - - II Abandoned: Time Start Injection: r�: Time Finish injection: Lilt 1 Lift 2 Lift 3 Notes Lift Depth fs - K Gals Solution Pumping Rate '�f G COMMENTS: Field Rep.: Borehole Number: • v Date drilled: �- l� Borehole Depth: I I Date Borehole Date Injected. � = - t; '�- j l Abandoned: C- 6, t 1 Time Start injection: • 5-5 Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth i- 16 rI T ' /,;� Gals Solution M Pumping Rate I % ^ 5 6 COMMENTS: Field Rep_: G r!�— FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: o1q Date Drilled: 6-6- Borehole Depth: Date Borehole Date Injected' - A Abandoned: 6.6 - Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Motes Lift Depth r 6 (f-w Gals Solution d �d Pumping Rate G• tr COMMENTS: Field Rep.: 1►ti��� ■ Borehole Number: ►� �� Date Drilled: 6 6 - 1{ Borehole Depth: Date Borehole Date Injected: 6- 6 - I( Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth a_7/ J 1(_ 1�-1 q 14� Z Gals Solution .+4431— 3 D 4z: Ip -7 ",g-/�� Pumping Rate 6. 6 COMMENTS: Field Rep.: Borehole Number: Number: Q ' pate Drilled: (, • G - U Borehole Depth: Date Borehole Date Injected: G - G - { Abandoned: G - 6 1� Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Solution Pumping Rate G [, COMMENTS: Field Rep.: �-c� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: �-�a[ Date Drilled: G-G- I/ Borehole Depth: If Date Borehole Date Injected: G • G ! t Abandoned: - 6- Time Start Injection: Time Finish Injection: Lift 1 Litt 2 Lilt 3 Notes Litt Depth Gals Solution Pumping Rate COMMENTS: Field Rep.: •�:-� Borehole Number: A- Date Drilled6- If Borehole Depth: /01-- � Date Borehole Date Injected: Abandoned: 6• G• K Time Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth • x 1 --12 13 - f l Gals Solution 0- v Pumping mate 6�% G COMMENTS: Field Rep.:-�- Borehole Number: ] - Date Drilled: 6- 7- t I Borehole Depth: Date Borehole Date Injected: jI Abandoned: 6- �• �D Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Solution Pumping Rate 6.5 COMMENTS: Field Rep.: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number. - Date Drilled: G - 7- j 1 Borehole Depth: ! D Date Borehole Date Injected: Abandoned: 6• Time Start Injection: Time Finish Injection: Lift t Lift 2 Lift 3 Notes Lift Depth '�. �� K - r.? 13 I i Gals Solution} Pumping Rate COMMENTS: Field Rep.: I Borehole Number: Date Drilled: 6- f%- Borehole Depth: Date Borehole Date Injected: 6-q- Abandoned: 6- r%• �� Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Uft 3 Notes Lift Depth J5 - - 0 / ,?- j R Gals Solution Pumping Rate COMMENTS- Field Rep.: ►t''���`� r Borehole Number: Date Drilled: Borehole Depth: 17 Date Borehole Date Injected: 1 - - Abandoned: 6• 7- It Time Start Injection: Time Finish Injection: Lift t Lift 2 Ltft 3 Notes t-"rft Depth Gals Solution L. If/g14 Pumping Hate GOMMENTS: Field Rep-: FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: 6-/? // Borehole Depth: Date Borehole Date Injected: 1.7- /1 Abandoned: C-13. 11 Time Start Injection: Time Finish injection: Litt 1 Lift 2 Litt 3 Notes Lift Depth Gals Solution Pumping Rate COMMENTS: Field Rep.: k� - Borehole dumber: Date Drilled: 6I1 Borehole Depth: Date Borehole Date Injected: [, - I?- It Abandoned: Time Start Injection: Time Finish injection: Lift 1 Lift 2 Litt 3 Dotes Lift Depth _ 17 17 /T Gals Solution c1 : Pumping Rate COMMENTS: Field Rep.: Kk1< [- Borehole Number: Date Drilled: 6, 13 It Borehole Depth: Date Borehole Date Injected: /Y. fI Abandoned: d• /-i'- [� Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth Gals Solution 7 100 Pumping Rate 7• S' r r COMMENTS: Field Rep.: 14�� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number-XW-14 + Date Drilled: Borehole Depth:Ir+oR,b.a,,;, Date Borehole Date Injected: t; g-ir !f Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 0S - C/ C> Gals Solution 41 q Pumping Rate 1, `a COMMENTS: r �^ S Field Rep_: In G �' � �� l Borehole Number: EM""" Date Drilled: Borehole Depth -- Date Borehole Date Injected. G- g7- It Abandoned: Time Start injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth�LS'� Gals Solution Q c l Pumping Rate 6 6' COMMENTS: �S r} Field Rep_: f'^•�� Borehole Number: 0 + A Date Drilled: Borehole Depth: Date Borehole Date Injected: Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth- q) Gals Solution I Pumping Rate COMMENTS: Field Rep.: 1+��� FIELD FORM - SOIL BORING AND INJECTION RECORD Borehole Number: Date Drilled: 6 Borehole Depth: Date Borehole Date Injected: 6- Abandoned: Time Start Injection, Time Finish Injection: Lift 1 Lift 2 Lift 3 Notes Lift Depth 53 Gals Solution Pumping Rate COMMENTS: Field Rep.: - - Borehole Number: >LTt--.P - ]d Date Drilled: Borehole Depth: 5 Date Borehole Date Injected: 1 Abandoned: Time Start Injection: Time Finish Injection: Lift 1 Litt 2 Uf# 3 Notes Lift Depth qf Gals Solution Dd Pumping Rate 6. j COMMENTS: + Field Rep.: �c 0 '�t 0'e 36 4 Borehole Number: €ovo - Date Drilled: Borehole Depth: _75— Date Borehole Date Injected: [ - ! Abandoned: Time Start Injection: Time Finish injection: Lift I Lift 2 Lift 3 Notes Lift Depth Gals Solution v1o1S Pumping Rate COMMENTS: Field Rep.: I P � E NCDENR — Remedial Construction Completion Report July 20. 2011 MACTF_C Project 6628-08-4691 NONCD000109Z APPENDIX F PHOTOGRAPHS NCDENR - Remedial Construction Completion Report AMCTEC Project 662&08-4691 Photograph 3: Injection into newly installed injection well. Judy 20, 2011 MOrNCDM01092 APPENDIX E Underground Injection Control Permit Application li)[o 'van f d G amec January 13, 2012 Mr. Kim Caulk, P.G. - Inactive Hazardous Sites Branch Superfund Section - Division of Waste Management North Carolina Department of Environment and Natural Resources 401 Oberlin Road, Suite 150 Raleigh, North Carolina 27699 Subject: Second Quarterly Groundwater Monitoring and Remedial Action Progress Report and Fourth Quarter 2011 Status Report CMI Waste Water Treatment Plant Site NONC❑ 0001092 Elkin, Surry County, North Carolina MACTEC Project 6228-08-4691 Dear Mr. Caulk: In accordance with 111,E of the Administrative Agreement For Registered Environmental Consultant -Directed Assessment and Remedial Action pursuant to N.C.G.S. 130A-310.9(c) and 15A NCAC 13C .0300, AMEC Environment & Infrastructure, Inc. (AMEC) is pleased to submit this Second Quarterly Groundwater Monitoring and Remedial Action Progress Report and Fourth Quarter 2011 Status Report. The planned work is progressing in a manner to achieve the mandatory work phase completion deadlines set out in 15A NCAC 13C.0302(h) as modified to accommodate project delays as previously discussed with you and summarized in our Quarterly Reports. Quarterly Status Report Previous Quarter (Fourth Quarter 2011) ■ Received analytical results from Month 3 groundwater sampling activities. + Performed Month 6 groundwater field parameter monitoring on December 6, 2012. Current Quarter (First Quarter 2012) ■ Conduct Month 9 groundwater sampling event in March 2012. Correspondence: AMEC Environw"t R Infrastructure, Inc. 2801 Yorkwont Road, Suite 100 Charlotte, North Carolina 28209 www.tunre,rann Tel 704-357-8600 Fax 703-357-8638 Second Quarterly Groundwater Monitoring arrd Remedial Action Progress Reporl January 13, 2012 and Fount) Quarter 2011 Status Report Page 2 CMI Waste Water Treatmeni Plant Site (NONCD 0001092) AMEC Prefect No.: 6228-08-4691 • Pursue land Use Restriction of property to limit exposure at the Site, as funding allows. • Discuss project status with NCDENR related to limited remaining funds. 2nd Quarterly Groundwater Monitoring and Remedial Action Progress Report Pursuant to 15A NCAC 13C (.0306) (o) and in general accordance with the Groundwater Monitoring Procedures and Reporting correspondence dated September 28, 2011, AMEC provides the following post -injection performance monitoring evaluation. O&M Results The remedial action implemented at the site consisted of in -situ chemical injection (Regenesis 3DMe and HRC) into overburden soils and shallow bedrock via a network of existing and newly installed injection and monitoring wells, and temporary injection points. As such, operation and maintenance (O&M) of a remedial system is not applicable. Performance Evaluation Results Performance evaluation of the groundwater injection activities includes implementation of the proposed groundwater monitoring program as specified in the Groundwater Monitoring Procedures and Reporting correspondence dated September 28, 2011. The monitoring program includes collection of field geochemical parameters on a quarterly basis, as well as collection of groundwater samples for laboratory analysis of volatile organic compounds and natural attenuation parameters at months 3,6,9 and 18 after injection and pending available funds. To date, baseline, Month 1, Month 3, and Month 6 monitoring activities have been completed in May, July, October, and December 2011, respectively. Evaluation of field parameter data (pH, conductivity, turbidity, dissolved oxygen, temperature and oxidation reduction potential) indicates generally favorable conditions for dechlorination of chlorinated volatile organic compounds (CVOCs) in groundwater at the Site. Additional discussion of monitoring results for select field parameters is presented below. A summary of field parameter measurements recorded during the four monitoring events is presented in Table 1. Dissolved Oxygen It is generally accepted that dissolved oxygen (DO) is one of the most thermodynamically favored electron acceptors used by microbes for the degradation of organic carbon. ❑O Second Quarterly Groundwater Monitoring and Remedial Action Progress Report January 13, 2012 and Foarth Quarter 2011 Statas Report Page 3 CMI Waste Water Treatment Plant Site (NONGO 0001092) AMEC Project No.: 6228-08-4691 concentrations of less than 5 milligrams per liter (mglL) are considered acceptable for reductive dechlorination while concentrations of less than 0.5 mg1L are considered highly favorable. A significant reduction in DO levels was observed in the data collected during the Month 1 post -injection monitoring event. Prior to injection, ❑O levels were generally measured between 3 and 5 mg/L. ❑O levels measured during the Month 1 post -injection event were generally less than 1 mg/L. Rebound of D❑ levels was observed in some wells during the Month 6 post -injection monitoring event; however, the levels were still generally below 5 mg1L. Oxidation Reduction Potential Oxidation reduction potential (ORP) is a measure of electron activity in groundwater, which influences rates of biological degradation. Biological reduction of TCA, 1,1-DCA, and 1,1- ❑CE can be achieved by various anaerobic bacteria over a wide range of ORP (+50 millivolts [mV] to -400 mV); however, for complete dechlorination to ethane or ethane, the ideal ORP range is between -100 and -225 mV. In general, ORP measurements obtained during the Month 9 activities indicated favorable conditions for reductive dechlorination. PH A pH range of 5 to 9 is considered to be optimum for reductive dechlorination, Comparison of pre- and post -injection pH levels also indicate favorable conditions for reductive dechlorination in the majority of wells measured at the Site. Field and Laboratory QA/QC Procedures In accordance with T15A NCAC 13C .0300, AMEC personnel performed the following general quality assurance/quality control (QAIQC) protocols in the field during field parameter monitoring and groundwater sampling. • Measurement and sample collection beginning with less contaminated wells and moving toward more highly contaminated wells; • Dedicated disposable nitrile gloves were used at each well; • Dedicated sampling tubing was used at each well; • Down -well instruments (i.e. water level meter, submersible pump) were decontaminated between wells using a 3-stage process that included separate LiquinoxOldistilled water, distilled water, and distilled water rinses in series; and, Containerization of well purging and decontamination water in 55-gallon drums for subsequent disposal when samples were collected for laboratory analysis. Second quarterly Groundwater Monitoring and Remedial Action Progress Report January 13, 2012 anor Fourth Quarter 20 11 Status Report Page 4 CMI Wasle Water Treatment Plant Site (NONCD 0001092) AMEC Proiect No.; 6228-08-4691 In addition to field QA/QC protocols, AMEC also submitted the following QAIQC samples to the laboratory for analysis of VOCs using SW-846 Method 8260B during the Month 3 post - injection sampling event: One equipment rinse blank per event; • One field duplicate sample per event; and, ■ One trip blank per laboratory cooler (for a total of three samples). No target analytes were detected in the trip blank samples (TRIP BLANK 1, TRIP BLANK 2, and TRIP BLANK 3y, indicating that contaminants of concern were not introduced during shipping/transport and field handling procedures. No target analytes were detected in the rinsatelequipment blank (RB-1) sample, indicating that adequate decontamination of non - dedicated sampling equipment (i.e. submersible pump) was acheived during the sampling event. The field duplicate sample (DUPLICATE) was collected from well EBMW-15. Comparison of the analytical data between the standard and duplicate samples collected from EBMW-15 yielded almost identical results. Based on these results and associated laboratory quality control procedures, the results are considered acceptable for their intended purpose of evaluating groundwater quality at the Site. Sampling Results To date, AMEC has conducted one groundwater sampling event (Month 3 — October 2011) subsequent to injection. The next groundwater sampling event is scheduled for March 2012. As such, comparison of pre- and post -injection groundwater quality data is considered pre- mature. An evaluation of these data, including data obtained during the planned March 2012 sampling event, will be included in the 4`�' Quarterly Monitoring Report. For reference, groundwater quality data obtained from select monitoring and injection wells at the Site to date are shown on Table 2. The laboratory analytical reports are attached to this report. Map A site map showing groundwater monitoring and injection wells within and in the vicinity of the treatment area is attached to this report, Second Quarterly Groundwater Monitoring and Remedial Action Progress Reporl January 13, 2012 and Fourth Quarter 2011 Status Report Page 5 CMl Waste Water Treatment Plant Site (NOMCa 0001092) AMEC Project No.: 6228-08-4691 The Remediating Party and Registered Site Manager Certification Statements are attached in accordance with 15A NCAC 13C.0306(h). Sincerely, MACTEC ENGIN WNGrAN CONSULTING, INC. - I Mark P. Filardi, P.G. dre lark, L.G. Senior Geologist Principal Geologist Cc: Mr. David Goodrich, Aquifer Protection Section, 1636 Mail Service Center, Raleigh, NC 27699 Enclosures: REC Certifications Tables Figure Month 3 Laboratory Analytical Reports REC PROGRAM CERTIFICATION REC PROGRAM DOCUMENT CERTIFICATION FORM - PAGE 1 OF 2 IHSB SITE NAME CMI Waste Water Treatment Plant Site DATE & NAME OF DOCUMENT 2nd gqalterly Groundwater Monitoring and RA Progreso 1/11/2012 TYPE OF SUBMITTAL (chyle an that apply lR-eport Work plan, Work Phase Comp. Statement, Schedule Change RE, MEDIATING PARTY DOCUMENT CERTIFICATION STATEMENT (.0306(B)(2)} "I certify under penalty of Iaw that I have personally examined and am familiar with the information contained in this submittal, including any and all documents accompanying this certification, and That, based on my inquiry of those individuals immediately responsible for obtaining the information, the material and information contained herein is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant pen olties for willfully submitting false, inaccurate or incomplete information." Jaynes A. Ovenden Name of Rmnediating Party Si ilHC o Reme 5aturg Panty pate NOTARIZATION 'Sak 1111 1 y, (F.iiter Slate) Gn COUNTY TM CWl!����7 'bbn a Notary Public of said County and State, de hereby certify that S. t 0 -6-, N1 -t°,6-1 did personally appear and sign before me this day, produced proper identification in the form ofwas duly sworn or affirmed, and declared that, to the best of his or her knowledge and belief, after thorough investigation, the information contained in the above certification is trite and accurate, and he or she Bien signed this Certification in my resenee. �h SS my hand and official seal this 10 day of oUli ota Pu 5�;�� SEAL.} ry (signature) k�•�,GEy PLe,q /Y Qp . • , •.. , +4g . 01, My connnission expires:tytJTA� J- PuquG ,� •. Document Certification Form No. DC -I (J?euised 8111) REC PROGRAM DOCUMENT CERTIFICATION FORM - PAGE 2 OF 2 IHSB SITE NAME CMI Waste Water Treatment Plant Site DATE & NAME OF DOCUMENT Second gjuVerly Groundwater Monitoring and Remedial Pd 1 3 2 11 TYPE OF SUBMITTAL (circle all that apply). AOpa , Work plan, Work Phase Comp. Statement, Schedule Change REGISTERED SITE MANAGER CERTIFICATION OF SIGNATURES As the Registered Environmental Consultant for the Site for which this filing is made, I certify that the signatures included herewith are genuine and authentic original handwritten signatures and/or true, accurate. and complete copies of the genuine and authentic original handwritten signatures of the persons who purport to sign for this filing. I further certify that I have collected through reliable means the originals and/or copies of said signatures from the persons authorized to sign for this filing who, in fact, signed the originals thereof. Those persons and I understand and agree that any copies of signatures have the same legally binding effect as original handwritten signatures. and I certify that any person for whom I am submitting a copy of their signature has provided me with their express consent to submit said copy. Additionally, I certify that I am authorized to attest to the genuineness and authenticity of the signatures, both originals and any copies, being submitted herewith and that by signing below, I do in fact attest to the genuineness and authenticity of all the signatures, both originals and copies, being submitted for this filing. Andrew M. Clark ltiia Eta ' t d Site Manager r' 1 ature oTftegistered Site Manager bate REGISTERED SITE MANAGER DOCUMENT CERTIFICATION STATEMENT (.0306(b)(1)) "I certify under penalty of law that I am personally familiar with the information contained in this submittal, including any and all supporting documents accompanying this certification, and that the material and information contained herein is, to the best of my knowledge and belief, true, accurate and complete and complies with the Inactive Hazardous Sites Response Act G.S. 130A- 310, et seq, and the remedial action program Rules 15A NCAC 13C .0300. I am aware that there are significant penalties for willfully submitting false, inaccurate or incomplete information." Andrew M. Clark Name of d Si anager Sign atugis to Manager NOTARIZATION Q1;il A-914EnI LT SLate] (( 1�()Z pate COUNTY I, LAL a Notary Public of said County and State; do hereby certify that (Ja did personally appear and sign before me this day, produced proper identification in the form of C [IV i i mcp- , was duly swam or affirmed, and declared that, he or she is the duly authorized environmental consultant of the remediating party of (lie property referenced above and that, to the best of his or her knowledge and belief. after thorough investigation, the information contained in the above ceiiifications is true and accurate, and lie or she then signed these Certifications in my presence. WITNESS rru hand and official seal this day of (OFF14L SFA 1. ) Nolary lic ignat y wstp L (tang My commission expires! _.NawyN �>r Mottle cook& Document Certification Form No. DC- 11 (Revised 8/1 l) Table 1 Performance Monitoring Water Quality parameters and Monitored Natural Attenuation Parameters Former CMI WWTP Elkin, North Carolina AMEC Project; 6228.08-4691 Well ID Date Depth to Water bt0c} (ft Temperature {`C] Turbidity {NTIJ] Canducli�ity [US1cm] Total Hardness (mglL] Total Dissolved Solids (mglL) oxygen Reduction Potential �mV] pH Alkalinity (total) as Ca CD, (mgfL} Ferrous Iron {mglL] Manganese [pgR] Calcium [pg1L} Methane (poll-) Dissolved OxygenOxygen Nitrate [mglL] Nitrite [mglL] Sulfate (mglL) Sulfide {mg1L] Chloride (mg1L) Ethane [}7g1L) Ethane (pg1L) TOC [mgll ] EBMW-1 8125=09 13.02 2240 NM -•• NM 0.970 1,10 _ 1.06 NA NA NA NA _ 533 NA 91 6,87 455o NO NA NA _ NA _ 2.69 NA NA NA 4,15 NO NO 79.7 NO 83.4 NO ND 50,2 512011 •• -_ ..-- NA NA NA NA NA NA NA NA NA NA NA NA NA W1212011 14.96 1C10 634 NA -9 6.95 NA NA NA NA 1,20 NA NA NA NA NA NA NA NA 10/3/2011 WAS 15.15 0.00 464 NA 127 7.11 447.0 0.50 156 0,188 1,93 40.20 -o.10 6.9 C0.10 712 <10D <10,0 7.3 12/8/2011 15,59 15.91 3,90 -110 B.47 NA NA NA NA 2.42 NA NA NA NA NA NA NA NA EBMW-5 8128MM 12AS 17.90 NM NM 0.993 1.13 1,44 NA NA NA -49 5,95 139,0 10,8 NA NA NA NA 0,14 ND NO NO NO 182.0 NO NO 24,8 W16I2o11 12,50 14.32 5,40 NA -IS &48 NA NA NA NA 4,36 NA NA NA NA NA NA NA 7/12/2011 13.69 54.99 -999 NA NA -119 4.64 NA NA NA NA NA 0.11 NA NA NA NA NA NA NA _NA NA 1012DII - NA' 12AMI1 12,54 Imo 195 NA NA -464 5.43 NA NA NA NA NA 2.03 NA NA NA NA NA NA NA E13MW-6 5116I2011 NM NM NM NM NM NA NA NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA 711212011 NM NM NM NA NA NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA 10=11 NA NA 12JU2-01 -IT 12.65 15.49 137 1,26 NA NA .233 6,71 NA NA NA NA NA 0.19 NA NA NA NA NA NA NA NA 8129/2009 17.35 17.0D NM NM NA NA 176 4.81 6.7 NO NA NA NA 132 1.9 No 19.5 NO 34A NO NO 2.0 5+1812Q71 1136 13,01 463 0.171 NA NA 223 5.12 NA NA NA NA NA 2.99 NA NA NA NA NA NA NA EB1�AW-7 7112t2011 19,32 13,87 0A0 0,96 NA NA -236 6.09 NA NA NA NA NA 1.26 NA NA � NA NA NA NA NA NA 1014011 19.95 18,99 527 1,22 345 838 -93 SAO 34,0 81.9 1.48 103 0.0486 IA2 40.20 uii 5-0 o.58 91.1 ii0.0 s10.0 425,0 12/8/2011 16.36 16.13 0,00 1,07 NA NA -222 8.11 NA NA NA NA NA 1.47 NA NA NA NA NA NA NA NA &2812009 i1.90 19,60 NM NM NA NA -7 5.98 86.1 31 NA NA NA 0.34 NO NO 18.7 NO 105.0 NO ND ml 5116i2011 12.58 13.69 39.30 0.518 NA NA 184 6.14 NA NA NA NA NA 5.00 NA NA NA NA NA NA NA NA EBMW$ 7112/2011 i3,48 14,63 136 EL49 NA NA 230 2.58 NA NA NA NA NA 9.2e NA NA NA NA NA NA NA NA 12B12011 14.23 1587 208 5,73 NA NA 223 3.14 NA NA NA NA NA 0,41 NA NA -NA NA NA NA NA NA 8)2612DD9 14,81 16.60 NM NM NA NA -w 6.30 136.17 24A NA NA NA 0.20 ND NO 6.5 NO 197.0 NO NO 362 512011 NA NA •• » NA NA NA NA NA •• NA _ NA _ NA NA NA NA NA NA EBMW-9 V1212011 1&49 ie,34 aggg 3,74 NA NA 10 3.76 NA NA 0,74 NA NA NA NA NA NA NA NA 1012011 NA NA NA 12W2011 14,37 15,49 ` 20.40 8.49 NA NA -407 3,61 NA NA NA NA NA 1,51 NA NA NA NA NA NA NA NA &+3012009 12.52 i8.36 NM NM NA NA -26 5,98 12D,0 NO NA NA NA OA8 t7 NO 1&6 NO 30A No NO 45,0 Ulwo11 12,85 13.79 5.50 0.322 NA NA 166 eZ7 NA NA NA NA NA 4J5 NA NA NA NA NA NA NA NA EBMW.10 7/12/2011 13.01 14,17 589 0.900 NA NA 309 2,89 NA NA NA NA NA 0,51 NA NA' NA NA T NA NA NA NA 1012011 1216f2011 14.55 15,77 487 0413 NA NA 289 3,2D NA NA NA NA NA 0.63 NA NA NA NA NA NA NA NA 541612011 11.T7 13,33 62,60 0,101 NA NA 220 6.04 NA NA NA NA NA 432 NA NA NA NA NA NA NA NA EBMW-11 7112=11 12.12 16.45 76.80 GA17 NA NA 297 4,89 NA NA NA NA NA 1.32 NA NA NA NA NA NA NA NA 10121211 NM NM NM NM NM NM NM NM NA NA NA NA NM NA NA NA NA NArjok NA NA 1V&=1 13.23 15.48 81,37 0.12 NA _ NA 264 4,91 NA NA _NA _ - NA NA NA 1-46 NA NA NA NA NA NA NA 5/16/2011 18-73 14.93 17.90 0,357 NA NA 233 522 NA NA NA NA NA 3.86 NA NA NA NA NA NA NA EBMW-12 71t2gD11 19.32 15,93 fief 0-607 NA NA -72 &63 NA NA NA NA NA 0,40 NA NA NA NA NA NA l NA 101201 i NM NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA 1216/2011 i7.93 16.47 675 0.93 NA NA -63 &56 NA NA NA NA NA 0,32 NA NA NA NA NA NA NA EBMW-13 5/16/2011 16.80 NM NM NM NM NM NM_ W NM NA NA NA NA NA NM NA NA NA NA NA NA NA 7/12/2011 20.89 NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA 1012DII I NM NM NM NM NM NN1 NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA 1216/2011 1 20,37 NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA &2BI2009 16.25 21,20 NM NM NA NA 187 4.54 7,3 ND NA NA NA 2.40 30,7 1 NO 3&9 NO 13A NO NO 6.9 &1812011 14.67 12.70 8,80 01439 NA NA 287 4,69 NA NA NA NA NA 5.57 NA NA NA NA NA NA NA NA EBMW-14 7112I2011 17.20 14.09 0.80 0.688 NA NA •105 6.00 NA NA NA NA NA 0,21 NA NA NA NA NA NA NA NA 101412DII 18,D6 16,07 0.00 0.811 48.90 482 451 6.64 223-0 63,0 7Z5 10.0D 0.201 2A7 aD,ZO 0.33 ea() Z025 38.4 410.0 410.0 63.6 1216/2011 16.59 15,45 233 1.07 NA NA -205 6.58 NA NA NA NA NA Z47 NA NA NA NA NA NA NA _- �NA 5116I2011 14.15 1626 15M 0,224 NA NA 216 5.84 NA NA NA NA NA 2AS NA NA NA NA NA NA NA NA EBMW-i5 7172I2011 15.28 NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA 10/4/2011 16.53 16.69 1 0,00 0,837 161 350 78 8.1e 290-0 40.50 182 3&40 cA73 2.14 40.2D 40.10 15A 40.10 60.9 410,0 410.0 15.6 121 Ml1 1 &54 16.33 209 1.25 NA NA -32 6.58 NA NA NA NA NA 0.75 NA NA NA NA NA NA NA NA 5116I2011 12,35 14.12 204 0,113 NA NA 261 4.83 NA NA NA NA NA 3.29 NA NA NA NA NA NA NA NA EBMW-16 7/12/2011 13.53 I&DO 10,20 0,3430 NA NA �aD 5.36 NA NA NA NA NA 0.65 NA NA NA NA NA NA NA NA 1216*1311 14,25 16.31 999 0,93 NA NA -96 5.90 NA NA NA NA NA 1.42 NA NA NA NA NA NA NA NA 612011 NM NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA EBMW-17 7=11 NM NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA 10/412011 15.95 15.41 0.00 0.407 52.20 213 -71 9,07 1410 c0.50 0,D537 18.90 0,016 2,02 1.7 t0,10 12.8 0.10 55.0 410,0 15,3 20.4 12/812011 19,90 15.67 253 0,45 NA NA -158 9.48 NA NA NA NA NA 0.53 NA NA NA NA NA NA NA NA 613012009 9,45 km NM NM NM NM •141 5-41 1 TU ND NA NA NA 0.46 NO 6.3 ND 310.0 DA 0.2 33.9 $11612011 11,97 _ 14,00 7.80 1,57 NA NA -11 6,83 NA NA NA NA NA 3.11 NA NA NA NA NA NA NA EBMW-18 7/1212011 12,54 IK 2 0,00 1,440 NA NA -111 7.18 NA NA NA NA NA 0.27 NA JTII NA NA NA NA NA NA 50/412011 13.51 _7399 iK517 000 060 1.61 604 1030 -94 7.35 217.0 -0.50 0,134 2110 0.026 2.19 411.20 __5.4 NA Nq e0.10 348.0 BDD an 43.6 12161201t 13.36 1,56 NA N -Us 7.26 NA NA NA NA NA 047 NA NA NA NA NA NA Table 1 Performance Monitoring Water Quality Parameters and Monitored Natural Attenuation Parameters Farmer CMI WWTP Elkin, North Carolina AMEC Project: 6228.06.4691 Well ID pate Depth to Water (ft bloc) Temperature ('C) Turbidity (NTII) Conductivity ({1SIcm) Total Hardness (mgfL) Total Dissolved Solids (mg1L) Oxygen Reduction Potential (mV) pH Atka Iinity (fatal) as CaCO3 (mglL) Ferrous Iron (mglL) Manganese (pg1L1 Calcium [pgk) Methane (pg1L) Dissolved Oxygen (mg1Lj Nitrate [mg1L) Nltrile [-OfO Sulfate (mg/L) Sulfide (mgfL) Chloride {mglL) Ethane (pglL) Ethene (pgIL) TOC (mg1L) EBMW-19 V112009 16.29 I8,20 _ 15.30 15.22 _NM _ 5.40 458 NM _ NM NA NA 144 NA tVM NA NA 323 NA -100 145 7,53 _ 140.p NO NA NA _ NA NA 028 NO NA NA ND NA NA 125.0 0.1 NO NP NO 6.5 5f1812011 13.51 U97 6,75 NA NA NA NA 8.67 8.17 NA NA NA NA NA NA 711212011 19.33 0.434 42 6.98 NA NA KA NA NA NA NA NA NA NA NA i07312011 10.90 19.83 _ 0.015 0,624 30 8,05 151.0 c0.50 0.41 34,60 <0'010 7,27 c0.23 1.1 146.0 <0.25 <5.0 r10.0 �10.0 21A 12MMI1 20.08 1&92 >g9y 0,65 -89 6.77 NA NA NA NA NA 0.92 NA NA FLA NA _ NA NA NA NA EBMW-21 812W2D09 11AD 20.80 NM NM NM_ KA _ NA 112 _ NA _ NM NA NA Z08 NA 52 7.50 156,0 NO NA NA NA 6,15 NO NO No NO 22$ NO NA NO 5-1 y16f2011 15.44 13.49 5.40 0.316 129 7.27 NA NA NA NA NA 6,79 NA NA _wi NA NA NA NA 7112J2011 16.D9 _ 1&36 >m 0,348 282 6.30 NA NA NA NA NA 3.28 _ NA NA NA NA NA NA NA NA 1014=11 721612Q11 13,87 18.16 0.00 0,442 -92 7.15 77.1 <0,50 0.0318 36,W 0,021 2.71 cO,20 <0.10_ 5.8 <0.10 s5.0 �10.0 NA 0OX 16,0 15.95 15.32 0.00 0,38 -145 6.66 NA NA NA NA NA 0.86 NA NA NA NA NA NA NA 6IM2009 y1612011 5.65 18.70 NM NM NM NM -3 9.89 76.8 NO NA NA NA 5.38 NO NO 12&0 NO 26A NO 0,0 11,6 1124 13.6E 5.60 0.462 NA NA :9 8.33 NA NA MA NA NA 7,41 NA _ NA NA NA NA NA NA NA EBMW-22 7112Y1011 12.15 15.84 911 0.527 NA NA -72 9.04 14A NA NA NA NA O,d4 NA NA NA NA NA NA NA NA 10/3/2011 18,36 0.00 2,780 1140 480 -82 12.21 735.0 <0,5D 0,45 401 0,D474 2,81 <D.20 c0.10 136.D c0,10 1919 ■10.0 45.4 9.0 12/6/2011 _13.18 13.8d 15.81 W.40 _ 0.57 NA NA -369 9.05 NA NA NA NA _ NA 0.58 NA NA I NA NA NA NA NA NA EBMW-23 71V2009 16.88 19.20 NM NM NM NM 122 5.45 35.7 NO NA NA NA 6.98 1,0 NO 84,0 NO 24.4 NO NO 2.5 &512511 19.48 15.12 360 D.45a NA NA 783 5.32 NA NA NA NA NA 3,85 NA NA NA NA NA NA NA NA EBMW-29 711=011 19.22 15.73 483 0.457 NA NA -20 5,65 NA NA NA NA NA 0,48 NA NA NA NA NA NA NA NA SQ1312011 20.76 21,72 0.00 0.594 80.30 159 170 _ -196 67.5 1.3 7AS 21,40 0.0136 1,82 <0.20 eGAD 813 <0J0 c5.0 Z10.0 a10.0 9A 12/6/2011 20.40 16.10 95.70 13 7m NA NA _5.49 6,07 NA NA NA NA NA 3,12 NA NA NA NA NA NA NA NA 51512Q11 2077 20,77 521 0,72D NA NA 57 5.92 NA NA NA NA NA 3,12 NA NA NA NA NA NA NA NA EBMW-30 711212011 21.66 15.30 557 0.753 NA NA 145 6.05 NA NA NA NA NA 0.45 NA NA NA NA NA NA NA__ NA 1015fZQ11 22.40 NM NM NM _ 182 _ 392 NM NM 175.0 18.7 7.00 41.50 0.01$4 NM <0.20 0.46 <50 1 0.56 83.0 c10.0 c0_0 1 26.5 NA IM2011 21,52 15.99 693 0,92 -- -- NA NA -203 B-15 tJA NA NA NA NA 2.65 NA NA NA NA NA NA NA 51512Q11 14,a8 13.13 420 0.311 NA NA 250 4,66 NA NA NA NA NA 4.84 NA NA NA NA NA NA NA NA EBMW-31 7112/2011 1&30 14.37 >qw BA33 NA NA 40 5.47 NA NA NA NA NA i,80 NA NA NA NA NA NA NA NA 10/512011 18,13 NM NM NM 322 - 624 NM NM 41.7 58.4 6.34 71.OD 0.0147 NM �0.20 0.14 <5L &0,10 292.0 c10,0 00.0 4&5 12/6/2011 18.78 15.62 359 1.25 NA NA -72 5,47 NA NA NA NA NA 3,54 NA NA NA NA NA NA NA NA 5/512011 14.07 12.90 NM 0.514 NA NA 315 4.69 NA NA NA NA NA 5.15 NA NA NA NA NA NA NA NA EBMW-32 7/12/2011 16,02 14,33 >999 0.725 NA NA -24 &25 NA NA NA NA NA - 038 NA NA NA� NA NA NA NA NA_ IQ1812011 lam NM_ �15.30 _ NM 16.10 NM 1.39 281 NA 708 NM -111 NM 5.65 719 ~fJA 77.9 3.28 79.90 OA423 NM cO,20 6.11 <5.0 c0,10 269A �10.Q �10.0 54.1 IZV2011 `l&22 _ NA - NA NA. NA NA 2.45 NA - - NA NA NA NA NA NA _ NA IW-12aA 51161W011 17.92 15,31 8.50 0.423 NA NA 93 5.72 NA NA NA ... _ NA NA NA 3.41 NA NA NA NA NA NA NA NA NA 711212Q71 _ 26.59 16.61 _ 597 - - 617 I.340 NA NA 170 3.78 NA NA NA NA 1,56 NA NA NA NA NA NA Nfi _ 121612011 23.47 15.89 --- 1.476 NA NA 209 3.56 NA NA NA NA NA 1.37 NA NA NA NA NA MA NA NA FW-14+ SI161Z011 15.01 14.15 6AC 2.17 NA NA 101 _ 5.77 NA NA NA NA _ - -NA NA NA 3.76 _ 0.2Z NA_ NA NA NA NA NA NA NA NA 7112/2011 _ 16,52 14.89 >999 Z360 NA NA -43 5.34 NA NA NA - NA NA NA NA NA NA NA 12161201, 1&63� 15.35 >999 08 NA NA 119 3,31 NA NA NA NA NA 2,02 NA NA NA NA NA NA NA NA 5/16/2011 14.39 14.37 535 0.156 NA NA 207 5.77 NA NA NA NA NA 5167 NA NA NA NA NA NA NA NA FAMW-1 7I2011 « .. .. « .. .. 1012017 .. .. .. .. .. « .. .. .. .. - « .. 1216/2011 16.44 16,28 >999 0,178 NA NA 285 5.42 NA NA NA NA NA 3.31 NA NA NA NA NA NA NA NA 5f2D15 NM NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA NA NA FPM 71Z011 NM NM NM NM NM NM N NM NM � NM NA NA NA N0. NA NM NA NA NA NA NA NA NA NA 10=11 NM NM _ NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA _ NA NA NA NA 12mmi1 NM NM NM NM NM NM NM NM I NA NA NA NA NA NM NA I NA NA NA NA NA NA NA SM11 NM NM NM NM NM NM NM NM NA NA NA NA NA, NM NA NA NA NA NA NA NA NA FPMW-5 712411 NM NM NM NM NM NM NM NM NA NA NA NA NA NM NA NA NA NA NA NA _ 'NA lVA f015YLQ11 15.81 16.34 0.00 1.11 184 302 133 7.83 292 11 1.43 65,40 cDAIO 209 �20 c0110 14 0 <GA0 es'o s10.0 c10.0 14.6 t2f612011 13.51 15A5 7d.80 0.573 NA NA 103 5.55 NA _ NA NA NA MA 727 NA NA NA NA _NA NA NA NA Notes Pre-uryecWn measurements - May 2011 1-m0rdh Ptrsi-injection meaaurmenls = JOl 2011 3-month posl•injecW measurem ent5 = Oclaber 2011 rt bloc = feet be)ow top of casvtg ystem = mk r[rsiemens Per cart-eter NTV = neprldomelric turbrdily units mg = militg rams per liter 'C = degrees celous mV = millivolts = Inject" presem in well, f ald wamemem not measured or anal gzea [Auld not locate well at tlma of %8m play NM - Not measured EEMW13 - ObsWeled and ins of ,dent vol urn es 10 called measuram ems EBMW-30. 31. 32 - Wells band dry, a ererbre waler quality measummems cat measured FPMW-4 - Well obsmxled. measrremmts not collected NA = Not Analyzed Prepared BylOate' 13/p_ 1,z Table 2 Summary of Well Construction Details and Recent Groundwater Quality Data VOC Analyses Former CMI WWTP Elkin. North Carolina Well Construction Details CDC Concentrations Top of Well !D Casing Screened Constructed Sampling 1,1.1- 1,1,2- Vinyl Elevation Interval Well Depth Aquifer pate TCA TCA 1,i-DCA 1,1-DCE PCE TC8 Chloride (MSL) Lft bgsj ift 5gsj Injection Wells 10/5/2006 183,000 NO 15,800 14,000 NO N❑ ND 189,000 16,100 EBMW-5 94.29 29-39 39.0 SBR 12/17/2007 NO 16.500 <10,000 <10.000 <10,000 280,000 NO NO 6/26/2009 57.5 43.8 49.6 15.1 NS 10/2011 NS NS NS NS NS NS 10/1012006 87,200 NO 4,800 5,500 N❑ NO ND 240,000 EBMW-8 96.52 21.7-31.7 36.7 SBR 12/18/2007 ND 11,200 10,600 <10.000 <10,000 <10,000 109,000 4,810 6/26/2009 47 8,530 35.1 98.0 5.7 NS 10/2011 NS NS NS NS NS NS 10/4/2006 184,000 ND 9,920 13,000 ND ND ND 214,000 16,300 EBMW-9 96,29 45-55 55.0 SBR 1211W2007 ND 10,400 <10,000 <10,000 <10,000 327,000 ND 18,900 6/26/2009 61.2 11.6 39.3 8.5 NS NS 1012011 NS NS NS NS NS 10/10/2006 202,000 ND 9,650 7,800 ND ND ND 73,000 EBMW-10 97.18 40-55 55.0 SBR 12/18/2007 ND ND NO - <16,000 <16,00.0 <16,000 23,200 6/30/2009 8.4 ND- NO 44.4- 8.2 1_.1 NS 10/2011 NS NS NS NS NS NS IW-12+A 102.67 25-40 40.0 SBR 10/2011 NS NS NS NS NS NS NS tW-14+ 97A6 25-40` 40.0 SBR 10/2011 NS NS NS NS NS NS NS Monitorin Wells 10/4/2006 3,000 N❑ 3,340 1,160 ND ND NO EBMW 1 98.61 23,5-33,5 33.5 SBR 12/18/2007 6,100 NO 5,810 3,070 <160 <160 <160 6/25/2009 2,490 3A 4,190 1,330 <1.0 2.1 1.2 10/3/2011 796 <20.0 2 260 818 <20.0 <20.0 <20.0 EBMW-6 94.39 10-20 20.0 SBR 10/2011 NS NS NS NS NS NS NS 10/10/2006 71,000 ND 10,800 3,930 ND ND ND EBMW-7 100.83 10.5-20.5 20.5 OVB 12/18/2007 80,100 NO 11,400 4,480 <4,000 <4,000 <4,000 6/29/2009 5,830 5 2,580 ND 22.9 8.1 <1.0 10/3/2011 8,900 <50.0 29,400 2290 <50.0 63.5 <50.0 EBMW-13 101 A 8 12-22 22.0 OVB 10/2011 NS NS NS NS NS NS NS 10/5/2006 34,200 NO 832 1,080 N❑ ND ND 12/17/2007 110,000 N❑ ND N❑ <5,000 <5,000 <5,000 EBMW-14 98.64 8.5-18.5 18.5 OVB 6/26/2009 17,600 ND 696 802 31.8 4_9 2,.2 10/4/2011 88,100IND 19,300 3,120 166 <100 <100 EBMW-15 100.87 8-18 18.0 OVB 10/4/2011 7.8 4A 9.1 <1.0 <1.0 <1.0 EBMW-16 98.77 8-18 18.0 OVB 10/2011 NS NS NS NS NS NS EBMWA7 95.58 75-90 90.0 SBR 10/4/2011 <1.0 2.7 1.0 <1.0 <1.0 <1A 10/10/2006 348,0003�0 fi,900 ND ND ND 309,00048,500 EBMW-18 97.43 68-78 78.0 DBR 12/18/2007 ND <16,000 <16,000 <16,000 104,000 39,200 6/30/2009 ND 7,620 <50.0 <50.0 103 42�400 10/4/2011 <500 54100 3,500 <500 <500 <500 10/10/2006 54.9 NO 5.2 3.3 NO ND ND EBMW-19 103,25 90-100 100.0 DBR 12/18/2007 11 A NO 4.7 NO -- <1 r1 <1 7/1/2009 2.6 NO 2.5 ND <1.0 <1.0 <1-0 10/312011 <1.0 <11.0 1.4 <1.0 <1.0 <1.0 <1.0 10/9/2006 2,580 ND 136 90.0 N❑ ND EBMW-21 100.94 110-125 125.0 DBR 12/18/2007 1,540 ND 61 50.5 <50 _ND -<50 <50 6/29/2009 4,360 NO 1,190 280.0 3.7 <1.0 1.8 10/4/2011 341 <2.0 234 45.5 <2.0 <2.0 <2.0 10/5/2006 10,800 ND 1,820 1,050 ND N❑ ND 5,160 EBMW-22 96.67 105125 125.0 ❑BR 12M9/2007 ND 772 500 <400 <400 <400 6/25/2009 5,080 ND 2,230 1,090 <1.0 1,1 3 10/3/2011 2,860 <20.0 2,640 741 <20.0 <20.0 <20.0 EBMW-29 103.16 15-25 25.0 OVB 515/2011 278 <1.0 66.7 51.1 <1.0 <U t1.0 10l312011 234 <1.0 79.8 48.4 <1.0 <1.0 <1.0 EBMW-30 104.37 12-22 22.0 OVB 5/5/2011 22,000 4.9 2,850 2,590 3_7 5_9 2_7 32 700 10/5/2011 <200 32,800 fi 330 <200 <200 <200 EBMW-31 99.05 8-18 18,0 OVB 5/5/2011 39,300 24.8 3,960 3,720 48.1 11.6 1_9 221.000 1014/2011 <200 22.600 19.600 <200 <200 <200 EBMW-32 97.1 10-20 20.0 OVB 5/5/2011 1.970 <20.0 3,590 101 <20.0 <2U <20.0 10/4/2011 28,300 53.4 30 300 3 980 <20.0 29.0 21.5 FAMW-1 101.87 4.8-14.8 14.8 OVB 1012011 NS NS NS NS NS NS NS FPMW-4 96,12 6-16 16.0 OVB 1012011 FPMW-5 1 95.02 6-16 16.0 OVB 1015/2011 <1.0 t1.0 9.8 <1.0 <1.0 <1.o <1.0 2L Standards 200 - 70 7 0,7 3 0.03 Notes: 1. Concentrations reported in units of ug1L. 2. Concentrations in bold -face underlined type exceeded the 2L Standards. 3. Groundwater quality data from 2005-2006 adapted from Table 3 of Supplementary Phase 11 Test Pit and Monitoring Well Explorations and Soil, Groundwater, Stream, Sediment, and Surface Water Sampling Report, dated January 29, 2007 and prepared by Trigon Engineering Consultants, Inc. 4. Groundwater quality data from 2007 adapted from Table 3-4 of 2007 Annual Groundwater Monitoring Report, dated May 2008 and prpared by Sevee & Maher Engineers, Inc. 5. Injection completed June 13, 2011, 6. NS = Not Sampled. 7- Well IW-14+ installed as an open -borehole bedrock well. 8. Wells EBMW-5,6,8,9,10,13 and 16 had injectat present and were not sampled in October 2011. 9. Wells FAMW-1 cout not be located during Otober 2011. 10. Well FPMW-4 has a down well obstruction and can not be sampled. 11. SBR = Shallow Bedrock. 12. DBR = Deep Bedrock. 13, OVB = Overburden. Frepared hy: _3r .1,3110� P:18228 Ernironmerilalljvhsl2D0818228 f1&d697 CMI WW P RFCEEPjIRAP Implemerkal anlPasi-Injection MonitvringlPerfvrmance Montoring VpCs, WO, and MNA Checked hy: 4;1 � i ��� FIGURE .I . 1 1 ,` 11 FLYASH BASIN 1 I 1 ` EBMW-4 I _Ji- YAMW-x i / 1 AREA c (NOT core EBMw-23 1 EBMW-24 \ t. / ti 1 �" \ss � ass~ • ' —ss EBMW-2 7 EBMW-18 � � f fl3EBMW-22 M E8Mw-11 -- � r \'F <BiAW-14 - � J r EBAAW +EBMW-28 AREA• E EBMW-21 f13 EB►aw-7 \` :FAMW-1 'AEB>d EBMW-12 W-25Fm \ . EBMW-3 -'� EB�AW-32 AREA A -f EBMW-.20 � EBMW-13 EBMW-30 �EBM•W-19 - . � .. APPROXIMATE TOP OF . BANK OF YADKIN RIVER y EXPLANATION STREAM OVERBURDEN WELLS — — PROPERTY LINE BEDROCK WELLS —SS— SEWER LINE UPPER BEDROCK INJECTION WELL (25-45•) APPRID MATE SCALE IN FEET — — — APPROXIMATE TOP OF BANK PILOT TEST INJECTION WELLS (ABANDONED) TEMPORARY OVERBURDEN INJECTION POINT 50 25 0 50 FPMW-50. NOTES: BASE MAP AFTER SPATCO ENVIROMENTAL SERVICES DRAWING No. 9-179o. FIGURE 2 MONITORING WELL LOCATIONS AFTER BUNN ENGINEERING SURVEY MAP, PROJECT NO. B020603. 6/8/04 (REVISED 10/24/05 and 10/02/06) SELECT MONITORING WELLS SURVEYED BY R.H. PHARR ON 6/23/11, ALONG WITH THE LOCATION OF ALL TEMPORARY INJECTION POINTS. a MONTH 3 LABORATORY ANALYTICAL REPORTS 1!aceAnalylical4 wwwpaCefaks,471P October 12, 2011 Mr. Mark Filardi AMEC-Chariotte 2801 Yorkmont Road Charlotte, NC 28208 PaceAna lytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27286 (336P3-8921 RE: Project: CM WWTP 6228-08-4691 Pace Project No.: 92103587 Pace Analytical Services, Inc. 2 22 5 Riverside ❑r. Asheville, NC 28804 {826y254.7176 Received by MPF 10/12/11 Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Nuntersville, NC 28078 (704)875.9092 Dear Mr. Filardi: Enclosed are the analytical results for samples} received by the laboratory on October 04, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. It you have any questions concerning this report, please feel free to contact me. Sincere#y, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Ana10cal Services, Inc.. Page 1 of 40 e Pace Analytical Services, Inc. Pace Analytical Services, Inc. _ acemalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. j' www.puefabs.wm Eden, NG 272U Asheville, NC 28804 (336)62"921 (828)254-7176 CERTIFICATIONS Project: CMI WWTP0228-08-4691 Pace Project No.: 92103587 Minnesota Certification IDs 1700 Elm Street SE Suite 200, Minneapolis, MN 55414 A2LA Certification #: 2 926. 01 Alaska Certification #: UST-078 Alaska Certification #MN00064 Arizona Certification #: AZ-0014 Arkansas Certification #: 88.0680 California Certification #. 01155CA EPA Region 8 Certification #: Pace FloddalNELAP Certification #: E87605 Georgia Certification #: 959 Idaho Certification #: MN00064 Illinois Certification #: 200011 Iowa Certification #: 368 Kansas Certification #: E-10167 Louisiana Certification #: 03086 Louisiana Certification #: LA080009 Maine Certification #: 2007029 Maryland Certification #: 322 Michigan DEQ Certification #: N09 Minnesota Certification #: 027.053.137 Charlotte Certification IDs 9800 Kincey Ave. Ste 100. Huntersville, NC 2 807 8 North Carolina prinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Cerlificatlon #: 99006001 South Carolina Drinking Water Geri. #: 99008003 Virginia Drinking Water Certification #: D0213 Asheville Certification IDs 2225 Riverside Dr., Asheville. NC 28804 Florida/NELAP Certification #: E87648 Massachuselts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Mississippi Certification M Pace Montana Certification M MT CERT0092 Nebraska Certification M Pace Nevada Certification M MN_00064 New Jersey Certification #: MN-002 New Mexico Certification #; Pace New York Certification M 11647 North Carolina Certification #: 530 North Dakota Certification #: R-OM North Dakota Certification #: R-036A Ohio VAP Certification #: CL101 Oklahoma Certification #: D9921 Oklahoma Certification #: 9507 Oregon Certification #: MN200DO1 Pennsylvania Certification #: 68-00563 Puerto Rico Certification Tennessee Certification #: 02818 Texas Certification #: T 1047 04192 Washington Certification #: C764 Wisconsin Certification #: 999407970 Connecticut Certification #: PH•0104 FloridafNELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana D H H Drinking Water # LA 1OD031 West Virginia Certification #: 357 MrginiaNELAP Cer ifcation #: 46D144 South Carolina Certification #: 99030001 Virginia Certification #: 00072 West Virginia Certification #. 356 VirginaNELAP Certification #: 460147 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent a Pace Analytical Services, Inc.. pace Analytical Services, Inc. 'aft() Kincey Ave. Suite 100 HunterWile, NC 28078 (704)875-9092 Page 2 of 40 Pace Analytical Services, Inc- Pace Analytical Services, Inc. Pace Analytical Services, tnc. a'OAnalyllcal 205 East Meadow Road • Suite A 2225 Riverside Dr 9800 Kincey Ave. Suite 100 nwwpa�l scam Eden, NC 27288 Asheville, NC 28804 Huntersville, NG 29078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project CMI WW7P6228-08-4691 Pace Project No.. 92103587 Analytes Lab ID Sample I❑ }Method Analysts Reported Laboratory 92103587001 EBMW4 RSK 175 SK4 3 PASI-M SM 23408 JMW 1 PASI-A EPA6010 JMW, SHB 2 PASI-A EPA 8260 MCK 63 PASI-G SM 23208 AES 2 PASI-A SM 2540C GW1 1 PASI-A SM 3500-Fe 0#4 LEP 1 PASI-A SM 4500-S2C AES 1 AASI-A EPA 300-0 SAJ 1 PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A 92103587002 EBMW-22 RSK 175 SK4 3 PAS!-M SM 2340B JMW 1 PASI-A EPA 6010 JMW, SHB 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320E AES 2 PASI-A SM 25400 GW1 1 PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S2D AES 1 PASI-A EPA300.0 SAJ i PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 53108 SAJ 1 PASI-A 92103587003 EBMW-19 RSK 175 SK4 3 PASI-M SM 2340B JMW 1 PASI-A EPA6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 23208 AES 2 PASI-A SM 2540C GW1 1 PASI-A SM 3500-Fe D04 LEP 1 PASI-A SM 4500-S2D AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DIVIN 2 PASI-A SM 4500-0I-E JDA 1 PAS [-A SM 5310B SAJ 1 PASI-A 92103587004 EBMW-29 RSK 175 SK4 3 PASI-M REPORT OF LABORATORY ANALYSIS Page 3 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dt. worwp"ahs arm Eden, NC 27288 A5hevtlle, NC 26804 (336)623-8921 (828)254.7176 SAMPLE ANALYTE COUNT Project: CMI WWTP6228-08-4691 Pace Project No.: 92103587 Lab ID Sample ID 92103587005 EBMW-7 92103587006 Trip Blank Pace Analytical Services, Inc, 9800 Kineey Ave. Suite 100 Hunkusville, NC 28078 (704)875-9092 Method Analysts Analytes Reported Laboratory SM 2340B JMW 1 PASI-A EPA 6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PASI-A SM 2540C GW1 1 PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S20 AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JRA 1 PASI-A SM 5310B SAJ 1 PASI-A RSK 175 SK4 3 PAS]-M SM 2340B JMW 1 PASI-A EPA6010 JMW, SHB 2 PASI-A EPA 8260 MCK 63 PAS]-C SM 2320B AES 2 PASI-A SM 254OG GW 1 1 PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S2D AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 ❑MN 2 PASI-A SM 4500-GI-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A EPA 8260 MCK 63 PASI-C REPORT OF LABORATORY ANALYSIS Page 4 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. PaceAnalytical Services, Inc. Pace Analytical Services, Ime. aceMalytical 205 East Meadow Road - Svile A 2225 Riverside Dr. 9800 KinceyAve. Suite 100 Kwwpamfabs.com Eden, NC 27288 Asheville, NC 28804 Huntersvilie, NC 28078 (336)623-8g21 (8281254.7176 (704)875.9092 ANALYTICAL RESULTS Project. CM WWTP 6228.08-4691 Pace Project No.: 92103587 Sample: EBMW-1 Lab ID: 92103587001 Collected: 10/03/11 10:20 Received: 1D104111 11A9 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug& 10.0 1 10/07/11 127D0 74-84-0 Ethene ND ug)L 10.0 1 10107/11 12:00 74-85-1 Methane 188 ug/L 10.0 1 10/07/11 12:W 74-82-8 2340E Hardness, Total (Calc) Analytiral Method: SM 2340B Total Hardness 464 mg)L 6.5 10 10110/11 1fi:55 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 156000 ug/L 1000 10 10/06/11 10:15 10/10/11 16:55 7440-70-2 Manganese 2690 ug1L 5.0 1 10/06/11 10:15 10/08/11 00:51 7439.96.5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug1L 500 20 10/05/11 14:54 67-64-1 Benzene ND ug/L 20.0 20 10/05/11 14:54 71-43-2 Bromobenzene ND ug/L 20.0 20 10/05/11 14:54 108-86-1 Bromochlvromethane ND ug/L 20.0 20 10/05/11 14:54 74-97-5 Bromodichloromethane ND ug/L 20.0 20 1W05111 1454 75-27-4 Bromoform ND ug/L 20.0 20 10/05/11 14:54 75-25-2 Bromomethane ND ug/L 40.0 20 101051i1 14.54 74-83-9 2-Butanone (MEK) ND ug/L 100 20 10105/11 14754 78-93-3 Carbon tetrachloride ND ug/L 20.0 20 10/05/11 14:54 56-23-5 Chlorobenzene ND ug/L 20.0 20 10/05/11 14:54 108-90-7 Chloroethane 63.6 ug/L 20.0 20 1010511i 14:54 75-00-3 Chloroform ND ug/L 20.0 20 10105(11 14:54 67-66-3 Chloromethane ND ug/L 20.0 20 10/05/11 14:54 74-87-3 2-Chlorotoluene ND ug/L 20.0 20 10/05/11 14:54 95-49-8 4-Chlorotoluene N❑ ug/L 20.0 20 10/05/11 14:54 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 100 20 10/05/11 14:54 96-12-8 Dibromvchloromethane ND ug/L 20-D 20 10/05/11 14:54 124-48-1 1,2-Dibromoethane (ED8) ND ug/L 20.0 20 10/05/11 14:54 106-93-4 Dibrornornelhane ND ug/L 20.0 20 10/05/11 14:54 74-95-3 1.2-Dich)Drobenzene ND ug/L 20.0 20 10105/11 14:54 95-50-1 1,3-Dichlorobenzene ND ug/L 20.0 20 10/05/11 14:54 541-73.1 i,4-Dichforobenzene ND ug/L 20.0 20 10/05/11 14:54 106-46-7 Dichlorodifluoromethane ND ugIL 20.0 20 10/05111 14:54 75-71-8 1,1-Dichtoroethane 2260 ug1L 20.0 20 10/05111 14:54 75-34-3 1,2-Dich#oroethane ND ug/L 20.0 20 10/05/11 14:54 107-06-2 i,'I-Dichloroethene 818 ug/L 20.0 20 10105/11 14:54 75-35-4 cis-1,2-Dichloroethene ND ug/L 20.0 20 10/05/11 14:54 156.59.2 trans-1,2•Dichloroethene ND ug/L 20.0 20 10/05111 14:54 156-60-5 1,2-Dichloropropane ND ug/L 20.0 20 10105111 14:54 78-87-5 1,3-Dichtoropropane ND uglL 20,0 20 10/05/11 14:54 142-28-9 2,2-Dichioropropane ND ug/L 20.0 20 10105/11 14:54 594-20-7 1,1-Dichloropropene ND ug/L 20.0 20 10/05111 14:54 563-58-6 cis- 1.3-Dichloroprapene ND ug/L 20.0 20 10/05111 14:54 10061-01-5 (ran s-1,3-Dichloropropene ND ug/L 20.0 20 10/05141 14:54 10061-02-6 Date. 10/12/2011 D1:55 PM REPORT OF LABORATORY ANALYSIS Page 5 of 40 This report shall not be reproduced, except In Tull, without the written consent of Pace Analytical Services, Inc.. 4P aceAnapical K"pamtab&com Pace Analytical Services. Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Anaiyilcall Services, Inc 2225 Riverside Dr Asheville, NG 28004 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Klncey Ave Suite 100 Huntersville, NC 28078 (704)875.9092 Project: C M I WWTP6228-0B-4691 Pace Project No.: 921D3587 Sample: EI3MW-1 Lab ID: 92103587001 Collected: 10103/11 10-20 Received: 10104/11 11:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. ❑ual 8260 MSV Low Level Analytical Method: EPA 8260 Diisopropyl ether ND ug1L 20.0 20 10/05/11 14:54 108-20-3 Ethylbenzene ND ug1L 20.0 20 10/05/11 14:54 IDD-41-4 Hexachloro-1,3-butadiene N❑ ug1L 20.0 20 10105/11 14:54 87-68-3 2-Hexanone ND uglL 1D0 20 10105/11 14:54 591-78-6 p-Isopropyltoluene ND uglL 20.0 20 10/05/11 14,54 99-87.6 Methylene Chloride ND uglL 40.0 20 10/05/11 14:54 75-09-2 4-Methyl-2-pentanone (MI13K) ND uglL 100 20 10/05/11 14:54 108-10-1 Methyl-tert-butyl ether ND uglL 20.0 20 10/05/11 14:54 1634-04-4 Naphthalene ND ugll_ 20.0 20 10/05/11 14:54 91-20-3 Styrene ND uglL 20.0 20 10105/11 14:54 100-42-5 11,1,2-Tetrachloroethane ND ug1L 20,0 20 10105111 14;54 630-2D-8 1,1,2,2-Tetrachloroethane ND uglL 20.0 20 10/05/11 14:54 79-34-5 Tetrachloroethene ND uglL 20.0 26 10/05/11 14:54 127-18-4 Toluene ND tiglL 20.0 20 10/05/11 14:54 108-88-3 1,2,3-Trichlorobenzene ND uglL 20.0 20 10/05/11 14:54 87-61-6 1,2,4-Trichlorobenzene ND uglL 20.0 20 10/05/11 14:54 120-82-1 1,1,1-Trichloroethane 796 uglL 20.0 20 10105/11 14:54 71-55-6 1,1,2-Trichloroethane ND uglL 20.0 20 10/05/11 14:54 79-00-5 Trichloroethene ND uglL 20.0 20 1010&11 14:54 79-01-6 Trichlorofiuoromethane ND uglt. 20,0 20 10/05/11 14:54 75-69.4 1,2,3-Tfichloropropane ND uglL 20.0 20 10/05/11 14:54 96-18-4 Vinyl acetate ND uglL 40,0 20 10/05/11 14:54 1W05-4 Vinyl chloride ND uglL 20.0 20 10/05/11 14:54 75-01-4 m&p-Xylene ND uglL 40.0 20 10/05/11 14:54 179601-23-1 o-Xylene ND uglL 20.❑ 20 10105/11 14:54 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 20 10/05/11 14:54 460-00-4 Dibromofluoromethane {Sj 88 % 70-130 20 10105M1 14-54 1868-53-7 1,2-Dichloroethane-d4 (S ) 90 % 70.130 20 10/05/11 14:54 17060-07-0 Toluene-d8 {S) 101 % 70-130 20 10/05/11 14:54 2037-26.5 2320B Alkalinity Analytical Method: SM 2320B Alkalinily,Bicarbonate (CaCO3) 447 mglL 5.0 1 10/09/11 16:20 Alkalinity, Total as CaCO3 447 mg1L 5.0 1 10/09/11 16:20 2540C Total Dissolved Solids Analytical Method: SM 254DG Total Dissolved Solids 533 mg1L 25.D 1 10/05/11 15A1 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron, Ferrous ND mg1L 0.50 1 10/10/11 16:50 4500S2D Sulfide Water Analytical Method: SM 450D-S2D Sulfide ND mglL 0.10 1 1010W11 12:00 18496-25-8 300.0 1C Anions 28 Days Analytical Method: EPA 300,0 Sulfate 8.9 mg1L 5.0 1 10/05/11 1726 14808-79-8 H1.N2 Date: 10/1212011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 6 or40 This report shall not he reproduced, except In Full, without the written consent of Pace Ana lyllcaI Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 1�;a'ce A nalXical 705 East Meadow Road - Suite A 2225 Riverside Dr. 9800 KinceyAve . Suite 100 nnw.pamerabs.Czn Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-6921 (8261254-7176 t704j875-9092 ANALYTICAL RESULTS Project: C M I WWTP6228-08-4691 Pace Project No.: 92103587 Sample: EBMW-1 Lab ID: 92103587001 Collected, 10/03/11 10:20 Received; 10/04111 11.-49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mg1L 0.20 1 10/04/11 23:18 Nitrogen, Nilrite NO mg1L 0.10 1 10/04/11 23A8 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 73.2 mg1L 25.0 5 10/07/11 14:44 16887-00-6 5310B TQC Analytical Method: SM 53103 Total Organic Carbon 7.3 mg1L 1.0 1 10/07/11 15:32 7440-44-0 Sample: EBMW-22 Lab 10: 92103587002 Collected: 10/03/11 12:00 Received: 10/04/11 11:49 Matrix: Water Parameters Results units Report Limit OF Prepared Analyzed CAS No, Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO uglL 10.0 1 10/07/11 12:11 74-84-0 Ethene 46.4 ug1L 10.0 1 i0107111 12;11 74-85-1 Methane 47.4 uglL 10.0 1 10107111 12:11 74-82-8 234DB Hardness, Total (Calc.) Analytical Method: SM 2340B Total Hardness 1140 mg1L 6.5 10 10/10/11 17:16 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 401000 ug/L 1000 10 101D6111 10:15 10/10/11 17:16 7440-70-2 Manganese 453 uglL 5.0 1 10106111 1015 10/08/11 00:57 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO uglL 5D0 20 10105111 23:26 67-64-1 Benzene NO ug1L 20.0 20 10/05/11 2126 71-43-2 Bromobenzene NO uglL 20.0 20 10/05/11 23:26 108-86-1 Bromochloromethane NO uglL 20.0 20 10/05111 23:26 74-97-5 Sromodichloromethane NO ug1L 20.0 20 10/05111 23;26 75-27-4 Bromolorm NO uglL 20.0 20 10/05111 23:26 75-25-2 Bromomethane N❑ ug1L 40.0 20 10/05/11 23:26 74-83-9 2-Butanone (MEK) ND uglL 100 20 1U05111 2326 78-93-3 Carbon tetrachloride ND ug1L 20.0 20 10/05/11 23:26 56-23-5 Chlorobenzene ND uglL 20.0 20 10/0501 23:26 108-90-7 Chloroethene N❑ ug1L 20.0 20 10/05/11 23:26 75-00-3 Chloroform NO ug1L 20.0 20 10/05/11 2126 67-66-3 Chtoromethane NO ug1L 20.0 20 10/05/11 23:26 74-87-3 2-Chlorotoluene NO ug1L 20.0 20 10ID5111 2326 95-49-8 4-Chlorotvluene NO ug1L 20.0 20 10/05/11 2126 106-43-4 1,2-Dibromo-3-chloropropane NO ug1L 100 20 10/05/11 23:26 96-12-6 Dibromochloromethane ND uglL 20.0 20 10/05111 23-26 124 48 1 1,2-Dibromcethane (EDB) ND ug1L 20.0 20 10105111 23:26 106-93-4 Dibromomethane NO ug1L 20.0 20 1 D105111 23:26 74-95-3 Date: 10/1222011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 7 of 40 This report shall not be reproduced, except in full, without the written consent or Pace Analytical Services, Inc. o Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. acema4dical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 1 WAWPacelab.s.avn Eden, NC 27288 Asheville, NC 28804 Huntersvllle, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: CM WWTP6228-08-4691 Pace Project No.: 02103587 Sample: EBMW-22 Lab ID: 92103587002 Collected: 10103/11 12:00 Received: 10/04111 11:49 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oval 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dichlorobenzene NO uglL 20.0 20 10/05/11 23:26 95-50-1 1,3-Dichlorobenzene NO ug1L 20.0 20 10/05/11 23:26 541-73.1 IA-Dichlorobenzerie N❑ uglL 20.0 20 10/05/11 23:26 106-46.7 Dichiorodinuoromethane NO uglL 20.0 20 10/05/11 23:26 75-71-8 1,1-Dichloroethane 2640 ug1L 20.0 20 10/05/11 23:26 75-34-3 1,2-Dichloroethane ND ug1L 20.0 20 10/05/11 23:26 107-06-2 1,1-Dichloroethene 741 uglL 20.0 20 10105/112126 75-35-4 cis-1,2-Dichloroethene NO ug1L 20.0 20 10/05/11 23:26 156-59-2 trans-1,2-Dichloroethene ND ug1L 20.0 20 10/05/11 23:26 156-60-5 1,2- Dichloro propane ND ug1L 20.0 20 10/05/11 23:26 78-87-5 1,3-Dichloropropane NO uglL 20.0 20 10105111 23:26 142-28-9 2,2-Dichloropropane ND ug1L 20.0 20 1 D105111 2126 594-20-7 1,1-Dichloropropene ND ug1L 20.0 20 10/05/11 2316 563-58-6 cis-1,3-Dichloropropene NO uglL 20.0 20 10105/11 23:26 10061-Dl-5 trans-1,3-Dichloropropene ND uglL 20.0 20 10/05111 23:26 10061-132.6 Diisopropyl ether NO ug1L 20.0 20 10/05/11 23:26 108-20-3 Ethylbenzene ND uglL 20.0 20 1010W11 23:26 100-41-4 Hexach loro- 1 .3- b utadlen e NO uglL 20.0 20 10/05/11 23:26 87-68-3 2-Hexanone ND uglL 100 20 10/05/11 23:26 591-78-6 p4sopropyltoluene ND uglL 20.0 20 10/05/11 23:26 99-87-6 Methylene Chloride NO ugIL 40.0 20 10/05/11 23:26 75-09-2 4 -Methyl-2-penta none (MIBK) 109 uglL 100 20 10/05/11 23:26 108-10-1 Methyl-tert•butyl ether NO uglL 20.0 20 10/05/11 2126 1634-04-4 Naphthalene NO ug1L 20.0 20 10/05/11 23:26 91-20-3 Styrene NO uglL 20.0 20 10/65/11 23:26 100-42-5 1,1,1,2-Tetrachloroe lhane ND ug1L 20.0 20 10105/11 23:26 630-20.6 1,1.2,2-Tetrachlaroe lhane N❑ uglL 20.0 20 10/05/11 23:26 79-34-5 Tetrachforoethene ND uglL 20.0 20 10/05111 23:26 127-18-4 Toluene ND uglL 20.0 20 10105/11 2126 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 20 10105/11 23:26 87-61-6 1,2,4-Trichlorobenzene ND uglL 20.0 20 10105/11 23:26 120-82-1 1. 1. 1 -Trich loroethan e 2860 ug1L 20.0 20 10/05/11 23:26 71-55-6 1,1,2-Tdchloroethane ND ug1L 20,0 20 10/05/11 23:26 79-60-5 Trichlaroethene ND uglL 20.0 20 10/05/11 23:26 79-01-6 Trichlorolluoromethane NO uq& 20.0 20 10/05/11 23:26 75-69-4 1,2,3-Tdchloropropane ND ug1L 20.0 20 10/05/11 23:26 96-18-4 Vinyl acetate NO uglL 40.0 20 10/05/11 23:26 108-05-4 Vinyl chloride ND ug1L 20.0 20 10105/11 23:26 75-01-4 m&p-Xylene ND ug1L 40,0 20 10/05/11 23:26 179601-23-1 o-Xylene ND uglL 20.0 20 10/05/11 23:26 95-47-6 4-Bromotiuorobenzene (S) 95 % 70-130 20 10/05/11 23:26 460-00-4 Dibromoi uoromethane (S) 114 % 70.130 20 10/05/11 23:26 1868-53-7 1,2-Dichloroethane-d4 (S) 114 % 70-130 20 10/05/11 23:26 17060-07-0 Toluene-d8 (S) 99 eta 70-130 20 10/05/11 23:26 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinily,Bicarbonate (CaG03) 535 mg1L 5.0 1 10/09/11 16:20 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page Ent 40 This report shaft not be reproduced, except in Fui1. without the written son sent of Pace Analytical Services, InC.. /7;5'ce A nalj4ical� www.paoefahs.mm PaceAnalyticalServices, Inc. 205 East Meadow Road - SuIte A Eden, NC 27288 R338y623-8921 Pace Analytical Services, Inc, 2225 Riverside ❑r Asheville, NC 28804 I8281254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Sulte 100 Huntersville, NC 28078 (704)875-9092 Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 Sample: F-BMW22 Lab ID: 92103587002 Collected: 10/03/11 12:00 Received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed GAS No. dual 2326E Alkalinity Analytical Method. SM 2320B Alkalinity, Total as GaCO3 735 mg1L 5.0 1 10/09111 16Q0 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 486 mg1L 25.0 1 1(/05/11 15A1 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron, Ferrous ND mg1L 0.50 1 10/10/11 16:53 H1,N2 4500S2D Sulfide Water Analyticat Method: SM 4WD-S2D Sulfide ND mg1L 0.10 1 10/08/11 12:00 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 138 mglL 50.0 10 10/06/11 15:09 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mg1L 0.20 1 10/04/11 23:20 Nitrogen, Nitrite NO mglL 0.10 1 10/04/11 23:20 4500 Chloride Analytical Method: SM 450D-CI-E Chloride 19.9 mglL 5.0 1 10/07/11 14:35 16887-00-6 5310B TOC Analytical Method: SM 53106 Total Organic Garton 9.0 mg1L 1.0 1 10/07/11 15:52 744044-0 Sample: EBMW19 Lab TD; 92103587003 Collected: 10103/11 13:30 Received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS Na. Quai RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO ug1L 10.0 1 10/07/11 12:22 74-84-0 Ethene ND uglL 10.0 1 10107/11 12:22 74-85-1 Methane NO ug1L 10.0 1 10/07/11 12:22 74-82-8 2340B Hardness, Total (Catc.) Analytical Method: SM 2340B Total Hardness 1" mg)L 0.65 1 10/08/11 01:04 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 34600 uglL 100 1 10/06/11 1015 10/08/11 01:04 7440-70-2 Manganese 409 ug1L 5.0 1 10/06/11 10:15 10/08/11 01:04 7439-96-5 8260 MSV Law Level Analytical Method: EPA 8260 Acetone NO ug1L 25.0 1 10/05/11 15:45 67-64-1 Benzene 1.6 uglL 1.0 1 10/05/11 15:45 71-43-2 Bromobenzene NO uglL 1.0 1 10/05/11 15 45 108-86-1 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 9 of 4D This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services. Inc e Pace Analytical Services,ti Inc. Pace Analytical Services, Inc. Pace Analycal Services, Inc. r� r� J �{,,a /"11 ipica 205 East Meadow Road - Suite A 2225 Riverside Of 9800 KlnceyAve. Suite 1W wxnvpacelahacnm Eden. NC 27288 Asheville, NC 28804 Huntersville, NC 28078 [338)623.8921 (828)254.7176 (704)875-9092 ANALYTICAL RESULTS Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 Sample: ERMW-19 Lab ID: 92103587003 Collected: 10/03/11 13:30 Received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Ltuai 8260 MSV Low Level Analytical Method: EPA 8260 Bromochloromethane NO uglL 1.0 1 10/05/11 15:45 74-97-5 Bromodichioromethane NO uglL 1.0 1 10/05/11 15:45 75-27-4 Bromoform NO uglL 1.0 1 10/05/11 15:45 75-25-2 Bromomethane NO ug1L 2.0 1 10/05/11 15:45 74-83-9 2-Butanone (MEK) ND ug)L 5.0 1 10/05/11 15:45 78.93-3 Carbon tetrachloride NO uglL 1.0 1 10105/11 15:45 56-23-5 Chlorobenzene ND uglL 1.0 1 10/05/11 15:45 108-90-7 Chloroethane ND uglL 1.0 1 10/05/11 15:45 75-00-3 Chloroform ND uglL 1.0 1 10/05111 15:45 67-66-3 Chloromethane N❑ ug)L 1.0 1 10/05/11 15:45 74-87-3 2-Chlorotoluene ND uglL 1.0 1 10105/11 15:45 95-49-8 4-Chlorotoluene NO uglL 1.0 1 10/05111 15:45 106-43-4 1,2-Dibromo-3-chloropropane NO uglL 5.0 1 10/05/11 15:45 96-12-8 Dibramochloromethane NO ug)L 1.0 1 10/05111 15:45 124-48-1 1,2-Dibromoethane (EOB) NO uglL 1.0 1 10/05111 15:45 106-93-4 Dibromomethane NO uglL 1.0 1 10/05/11 15:45 74-95-3 1,2-Dichlorobenzene NO uglL 1.0 1 10105111 15;45 95-50-1 1,3-Dichlorabenzene NO uglL 1.0 1 10/05111 15:45 541-73-1 1,4-Dichlorobenzene NO uglL 1.0 1 10/05/11 15:45 106-46-7 Dichicrodinuoramethane NO uglL 1.0 1 10/05111 15.45 75-71-8 1,1-Dichloroethane 1.4 uglL 1.0 1 10/05111 15:45 75-34-3 1,2-Dichloroethane NO uglL 1.0 1 10/05111 15:45 107-06-2 1.1-Dichloreethene NO uglL 1.0 1 10105111 15:45 75-35-4 cis-1,2-Dichloroethene ND uglL 1.0 1 10/05/11 15:45 156-59-2 trans-1,2-Dichlaroethene NO uglL 1.0 1 10/05111 15:45 156-60-5 1,2-Dichloropropane NO uglL 1.0 1 10/05111 15745 78-87-5 1,3-DichIwo propane NO uglL 1.0 1 10105/11 15:45 142-28-9 2,2-Dichloropropane NO uglL 1.0 1 10/05111 15:45 594-20-7 1,1-Dichloropropene NO uglL 1.0 1 10/05/11 15:45 563-58-6 cis-1,3-Dichloropropene NO uglL 1.0 1 10/05111 15:45 10061-01-5 trans-1.3-Dichloropropene NO uglL 1.0 1 10/05111 15A5 10061-02-6 Oiisopropyl ether ND uglL U 1 10/05111 15:45 108-20-3 Ethylbenzene ND ug1L 1.0 1 10/05/11 15:45 10041-4 Hexachiaro-1,3-butadiene ND ug1L 1.0 1 10/05/11 15A5 87-68-3 2-Hexanone ND uglL 5.0 1 10/05111 15:45 591-78-6 p-Isopropyltoluene ND uglL 1.0 1 10/05/11 15:45 99-87-6 Methylene Chloride ND uglL 2.0 1 10/05/11 15:45 75-09-2 4- M ethyl -2-pe nta none (MIBK) ND ug1L 5.0 1 10/05/11 15:45 108-10-1 Methyl-tert-butyl ether N❑ ug1L 1.0 1 10/05/11 15:45 1634-04-4 Naphthalene NO ug1L 1Z 1 10/05/11 15:45 91-20-3 Styrene ND ug1L 1.0 1 10/05/11 15A5 100-42-5 1.1,1,2-Tetrachloroethane ND uglL 1.0 1 10/05/11 15A5 630-20-6 1,1,2,2-Tetrachloroethane N❑ ug1L 1.0 1 10/05111 15:45 79-34-5 Tetrachloroethene ND uglL 1.0 1 10/05/11 15:45 127-18-4 Toluene 3.9 uglL 1.0 1 10105/11 15:45 108-88-3 1,2,3-Trichlorohenzene NO ug1L 1.0 1 10/05111 15:45 87-61-6 1,2,4-Trichlorohenzene ND uglL 1.0 1 10/05/11 15:45 120-82-1 Date: 10/12/2011 01:55 PM REPORT ❑F LABORATORY ANALYSIS Page 10 of 40 This re part shall not be reproduced, except in Full, without the written consent or Pace Analytical Services, Inc.. n aceRnalytical xxw�celabs.cum Pace Analytical Services, IAC. 205 Past Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc, 2225 Riverside Or. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KInceyAve. Sulte 100 fiuniersville, NC 28078 (704)875.W92 Project CMI WWTP6228-08.4691 Pace Project No.: 92103587 Sample: EBMW-19 Lab ID: 921035B7003 Collected: 10/03/11 13:30 Received: 10/04/11 11A9 Matrix, Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 1.1,1-Trichtoroethane IN uglL 1.0 1 10/05111 15:45 71-55-6 1,1,2-Trichioroethane ND ug/L 1.0 1 10/05/11 15:45 79.00-5 Trichloroethene ND uglL 1.0 1 10/05/11 15:45 79-01-6 Trichlorofiuoromethane ND ug1L 1.0 1 10/05/11 15A5 75-69-4 1,2,3 Trichloropropane ND ug1L 1.0 1 10/0-9111 15:45 96.18-4 Vinyl acetate ND uglL 2.0 1 10105/11 15:45 108-05-4 Vinyl chloride ND uglL 1.0 1 10105/11 15:45 75-01.4 m&p-Xylene ND ug1L 2.0 1 10105111 15A5 179601-23-1 o-Xylene ND uglL 1.0 1 10105/11 15:45 95-47.6 4•Bromoikuorobenzene (S) 94 % 70-130 1 10/05/11 15:45 460-00-4 Dibromofluoromethane (S) 86 % 70-130 1 10/05/11 15A5 1868-53-7 1,2-13ichioroethan e-d4 (S) 89 % 70-130 1 10/05/11 15:45 17060-07.0 Toluene-d8 (S) 102 % 70-130 1 10/05/11 15A5 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity,Bicarbonate (CaCO3) 151 mglL 5.0 1 10/09/11 16-20 Alkalinity, Total as CaCO3 151 mg1L 5.0 1 10/09/11 16.20 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 323 mg1L 25.0 1 10/05111 15:41 Iron, Ferrous Analytical Method: SM 3500-Fe 0#4 Iron, Ferrous N0 mg1L 0.50 1 i0110111 16:55 1­11,192 450052D Sulfide Water Analytical Method: SM 4500-S20 Sulfide ND mglL 0.25 2.5 10/08/11 12:00 18496-25-8 D3 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 146 mg1L 50.0 10 10106/11 1523 14808.79-8 353.2 Nitrogen, N021NO3 unpres Analytical Melhod: EPA 353.2 Nitrogen, Nitrate ND mg)L 0.20 1 10/04/11 2131 Nitrogen, Nitrite 1.1 mg1L 0,10 1 10/04/11 23:31 4500 Chloride Analytical Method: SM 4500-CI-E Chloride NO mg1L 5.0 1 10/07/11 14.36 16837-00-6 5310E TQC Analytical Method: SM 5 310 B Total Organic Carbon 21.6 mglL 1.0 1 10/07/11 16 08 7440-44-0 Dale: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 11 of 40 This report shall not be reproduced, except in Tull, without the written consent of Pace Analytical Services, Inc.. a, Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Analytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 0iceyAve, Suite 100 wimpace.Jahs.cam Eden. NC 27288 Asheville, NC 28804 Huntersville, NC 28078 t336j623-B921 (828)254-7176 (704)875.9092 ANALYTICAL RESULTS Project: Civil WWTP 6228-08-4691 Pace Project No.: 92103587 Sample: EBMW-29 Lab ID: 92103587004 Collected: 10103111 14:40 Received: 10/04/11 11:49 Matrix: Water ace Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO uglL 10,0 1 10/07/11 12:33 74-84-0 Ethane NO ug/L 10.0 1 1OM7111 12:33 74-85-1 Methane 13.6 ug1L 10.0 1 10/07/11 12:33 74-82-8 2340B Hardness, Total (Calc.j Analytical Method: SM 2340B Total Hardness 80.3 mg1L 0,05 1 10/08/11 01:07 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 21400 uglL 100 1 10/06/11 10:15 10/08/11 01:07 7440-70-2 Manganese 7860 ug/L 5.0 1 10/06/11 10:15 10/08/11 01:07 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND uglL 25,0 1 10/10/11 19!50 67-64-1 Benzene NO ug/L 1,0 1 10110/11 19:50 71-43-2 Bromobenzene ND ug1L 1.0 1 1011001 19:50 108-86-1 Bromochtoromethane NO ug/L 1.0 1 10/10/11 19:50 74-97-5 Bromodichloromethane NO ug/L 1.0 1 10/10/11 19:50 75-27-4 Bromoform ND ug/L 1.0 1 10/10/11 19:50 75-25-2 Bromomethane ND ug1L 2,0 1 10/10/11 19:50 74-83-9 2-Butanone (MEK) N❑ ugIL 5,0 1 10/10/11 19:50 78-93-3 Carbon tetrachloride ND ugIL 1.0 1 10/10111 19:50 56-23-5 CNorobenzene NO uglL 1,0 1 10/10111 19:50 108-9D-7 Chloroethane 2.9 uglL 1.0 1 10/10/11 19:50 75-00-3 Chloroform NO ug1L 1.0 1 10/10/11 19:50 67-66-3 Chloromethane NO ug/L 1.0 1 10/10/11 19:50 74-67-3 2-Chlorotoluene NO ug/L 1.0 1 10/10/11 19:50 95-49-8 4-Chlorotoluene NO uglL 1.0 1 10/10/11 19:50 106-43-4 1,2-Dibromo-3-chioropropane NO ug1L 5,0 1 10/10/11 19:50 96-12.8 Dibromochloromethane NO ug1L 1.0 1 10/10/11 19:50 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 1.0 1 10/10/11 19:50 106-93-4 Dibromomethane NO ugIL 1.0 1 10/10/11 19.50 74.95-3 1,2-Dichlorobenzene NO ugIL 1.0 1 10M0111 19:50 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 10/10111 19:50 541-73-1 1,4-❑ichlorobenzene NO ug1L 1.0 1 10110111 19:50 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 10/10/11 19:50 75-71-8 1,1-Dichloroethane 79.8 ug1L 1.0 1 10/10/11 19:50 75-34-3 1,2-Dichloroethane NO ugIL 1.0 1 40110111 19:50 107-06-2 1,1-Dichlaroethene 48.4 ug1L IZ 1 10110/11 19:50 75-35-4 cis-1,2-Dichloroethene NO uglL 4.0 1 10/10/11 19:50 156-59-2 trans- l,2-Dichloroeth one NO uglL 1.0 1 10/10/11 19:50 156-60-5 1,2-Dichloropropane NO uglL 1.0 1 10/10/11 19:50 78-87-5 1,3-Dichloropropane NO uglL 1.0 1 10/10/11 19:50 142-28-9 2,2-Dichloropropane NO ug1L 1.0 1 10/10/11 19:50 594-20-7 1,1-Dichloropropene NO uglL 1.0 1 10/10/11 19.50 563-58-6 cis-1,3-Dichloropropena NO ugIL 1,0 1 10/10/11 19.50 10061-01-5 trans-1,3-Dichloropropene NO uglL 1.0 1 10/10/11 19.50 10061-02-6 Date: 1011212011 01,55 PM REPORT OF LABORATORY ANALYSIS Page 12 of 40 This report shall not be reproduced, except in full, without the written consent of Pace An atytical Services, Inc.. Pace Analytical Services, Inc. Pase Analytical Services, Inc. ace Ana lXiea1 205 East Meadow Road - Suite A 2225 Riverside Dr. nww.pacela6s.cam Eden. NC 27288 Asheville, NC 2B804 (336)623-8921 t828j254-7176 ANALYTICAL RESULTS Project. CMI WWTP 6228-08-4691 Pace Project No.: 92103587 Pace Analytical Services, Inc. U800 Kincey Ave. Suite 100 Huntersville, NC 28078 {704)875-9092 Sample: EBMW-29 Lab ID: 92103587004 Collected: 16/03111 14:40 Received; 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 8260 MSV Low Level Analytical Method- EPA 8260 Diisopropyl ether NO u91L 1.0 1 10/10/11 19:50 108.20-3 Ethylbenzene NO ugIL 1.0 1 10/10/11 19:50 100-41-4 Hexachloro-1.3-butadiene NO ug1L 1.0 1 10/10/11 19:50 87-68-3 2-Hexanone NO uglL 5.0 1 10/10/11 19:50 591-78-6 p-Isopropyltoiuene NO ug1L 1.0 1 10/10/11 19:50 99.87•6 Methylene Chloride NO uglL 2.0 1 10110/11 %50 75-09-2 4-Methyl-2-pentanone (MIRK) NO uglL 5.0 1 10/10111 19:50 108-10-1 Methyl-tert-butyl ether NO ug1L 1.0 1 101i0111 19:50 1634-04-4 Naphthalene NO ug1L 1.0 1 10/10/11 19:50 91-20-3 styrene NO ug1L 1.0 1 10/16111 19:50 100-42-5 1.1.1,2-Tetrachloroethane ND ug1L 1.0 1 1DI10111 19:50 630-20-6 1,12,2-Tetrachloroethane ND ug1L 1.0 1 10/10/11 19.50 79-34-5 Tetrachloroethene N❑ ug1L 1,0 1 10/10/11 19:50 127-18-4 Toluene ND ug1L 1.0 1 10/16/11 19:50 108-88-3 1,2,3-Trichlarobe naene ND uglL 1.0 1 10/10/11 19.50 87-61-6 1,2,4-Trichlorobenzene ND ug1L 1.0 1 10/10/11 19;50 120-82-1 1,1,1-Trichloroethane 234 ug1L 10.0 10 10111/11 12:56 71-55-6 1,12-Trichloroethane NO ug1L 1.0 1 10/10/11 19750 79-00-5 Trichloroethene NO ug1L 1.0 1 10/10/11 19:50 79-01-6 Tdchlorofluoromethane NO ug)L 1.0 1 10/10/11 %50 75-69-4 1,2,3-Trichlaropropane NO ugli- 1.0 1 10/10/11 19,50 96-18-4 Vinyl acetate NO ug/L 2.0 1 10/10/11 19:50 108-05-4 Vinyl chloride NO ug1L 1.0 1 10/10/11 19:50 75-01-4 m&p-Xyiene NO ug1L 2.0 1 10110/11 19.50 179601-23-1 o-Xylene NO uglL 1.0 1 10110/11 19:50 95-47-6 4-Sromofluorobenzene (S) 94 % 70-130 1 10/10/11 19:50 460.004 Dibromolluoromethane (S) 130 % 70-130 1 10/10/11 19:50 1868-53-7 1,2-Dichloroethane-d4 (S) 126 % 70-130 1 10/10/11 19:50 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 10/10/11 19750 2037-26-5 2320E Alkatirill ty Analytical Method: SM 2320B Atkalinity,Bicarbonate (CaCO3) 67.5 mg1L 5.0 t 10/09/11 16:20 Alkalinity, Total as CaCO3 67.5 mg1L 5.0 1 10/09/11 16:20 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved solids 159 mglL 25.0 1 10105/11 15:42 Iron, Ferrous Analytical Method: SM 3500-Fe 0#4 Iron, Ferrous 1.3 mg1L 0,50 1 10/10/11 16155 4500S2D Sulfide Water Analytical Method: SM 4500-S20 Sulfide NO mglL 0.10 t 10/08111 12:00 18496.25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 81.3 mg1L 25.0 5 10/06/11 15:36 14808-79-8 H1,N2 Date: 10112/2011 01;55 PM REPORT OF LABORATORY ANALYSIS Page 13 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. fi aceAnalylical .pawabs.ton) Pace Analytical 5ervices, Inc. 205 E a A Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28904 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersvllla, NC 28078 (704)875-9092 Project: CM WVVTP 6228-08-4691 Pace Project No.: 92103587 Sample: EBMW-29 Lab ID: 92103587004 Collected: 10/03/11 14.40 Received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mglL 0.20 1 10J04)11 23:35 Nitrogen, Nitrite ND mglL 0.10 1 10/04/11 23:35 4500 Chloride Analytical Method: SM 4500-CI-E Chloride NO mglL 5.0 1 10107/11 14:37 16887-00-6 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 9.4 mglL 1.0 1 10/07111 16:18 7440-44-0 Sample: EBMW-7 LabID: 92103587005 Collected: 10103111 16:00 Received: 10/04/11 il;49 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO ug1L 10.0 1 10107111 13:35 74-84-0 Ethene NO ug1L I 1 10/07/11 13:35 74-85-1 Methane 48.6 uglL 10.0 1 10/07111 13:35 74-82-8 2340E Hardness, Total (Calc.) Analytical Method: SM 2340B Total Hardness 345 mg1L 6.5 10 10/10/11 17:22 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 103000 uglL 1000 10 10/06/11 10:15 10/10111 17:22 7440-70-2 Manganese 1480 uglL 5.0 1 10/06/11 1015 10/08/11 0111 7439-96-5 8260 INSV Low Level Analytical Method: EPA 8260 Acetone NO uglL 1250 50 10/05111 16:36 67-64-1 Benzene NO ug1L 50-D 50 10/05/11 16:36 71-43-2 Bromobenzene NO ug1L 50.0 50 10/05/11 16:36 108-86-1 Bromochloromethane NO ug1L 50.0 50 10/05/11 16:36 74-97.5 Bromodichioromethane NO ug1L 50.0 50 10/05/11 16:36 75-27-4 Bromoform NO ug1L 50.0 50 10/05/11 16:36 75-25-2 Bromomethane NO ug1L 100 50 10/05/11 16:36 74-83-9 2-Buianone (MEK) NO ug1L 250 50 10/05/11 16:36 78-93-3 Carbon tetrachloride NO ug1L 50.0 50 10/05/11 16:36 56-23-5 Chlorobenzene NO uglL 50.0 50 10/05/11 16:36 108-90.7 Chloroethane 130 ug1L 50.0 50 10/05/11 16;36 75-00-3 Chloroform NO uglL 50.0 50 10/05/11 16:36 67-66-3 Chloromethane NO ug1L 50.0 50 10/05/11 16:36 74-87-3 2-Chlorotoiuene NO ug1L 50.0 50 101D5111 16:36 95.49-8 4-Chiorotoluene NO ugli. 50.0 50 10/05/11 16:36 106-43-4 1,2-Dibromo-3-chloropropane NO uglL 250 50 10105/11 16:36 96-12-8 Dibromochloromethane NO uglL 50.0 50 10/05/11 16:36 124-48-1 1,2-Dibromoethane (EDB) NO uglL 50.0 50 10/05/11 16:36 106-93.4 Dibromomethane NO uglL 50.0 50 10/05/11 16:36 74-95-3 ❑ate: 10112)2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 14 of 40 This report shad not be reproduced, except in full, without the written consent cFPace AnaIyticaI 5ervices, Inc.. e Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. a e*alytical 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 Klncey Ave. Suke 100 wtisw.pacefaLs.ram Eden, NC 27298 Asheville, NC 28804 Huntersville, NC 28078 (336)623.8921 (828)254.7176 (704)875-9092 ANALYTICAL RESULTS Project: CM} WW'rP 6228-08-4691 Pace Project No.- 92103587 Sample: EBMW7 Lab ID: 92103587005 Collected: 10103/11 15.00 received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Cual 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dichlorobenzene NO ug1L 50.0 50 10/05111 16:36 95-50-1 1,3-Dichlorobenzene ND uglL 50.0 50 10/05/11 %36 541-73-1 1,4-Dichlarobenzene ND ug1L 50.0 50 10/05/11 16:36 106-46-7 Dichlorodiflucromethane ND uglL 50.0 50 10/05/11 16:36 75-71-8 1,1-Dichloroethane 29400 ug/L 250 250 10/06/11 11:48 75-34-3 1,2-Dichloroethane N❑ ug1L 50.0 50 10/05/11 16:36 107-06-2 1,1-Dichloroethe ne 2290 uglL 50.0 50 10/05/11 16:36 75-35-4 cis-1,2-Dichlorcethene ND ug1L 50.0 50 10/05/11 16:36 156-59-2 trans-1,2-Dichlomethene N❑ uglL 50.0 50 10/05/11 16:36 156-60-5 1,2-Dchloropropane ND uglL 50.0 50 10/05/11 16.36 78-87-5 1,3-Dichloropropane ND ug1L 50.0 50 10/05/11 16:36 142-28-9 2,2-Dichieropropane NO ug1L 50.0 50 10/05/11 16:36 594-20-7 11-Dichloropropene N❑ ug1L 50.0 50 10/05/11 16:36 563-58-6 cis-1,3-Dichloropropene ND uglL 50.0 50 10/05111 16:36 10061-01-5 Ira ns-1,3-Dichloropropene ND ug1L 50.0 50 10/05/11 16:36 10061-02-6 ❑iisopropyl ether N❑ ug1L 50.0 50 10/05/11 16:36 108-20-3 Ethylbenzene NO ug1L 50.0 50 10/05111 16:36 100-41-4 Hexachloro-1,3-butadiene NO ug1L 50.0 50 10/05/11 16:36 87-68-3 2-Hexanone NO ug1L 250 50 10/05/11 16:36 591-78-6 p-Isopropyltaluene ND ug1L 50.0 50 10/05/11 16:36 99-87-6 Methylene Chloride ND ug1L 100 50 10/05/11 16:36 75-09-2 4-Methyl-2-pentanone (M18K) ND ug1L 250 50 10/05111 16:36 108-10.1 Methyl-terl-butyl ether ND ug1L 50.0 50 10/05111 16:36 1634-04-4 Naphthalene NO ug1L 50.0 50 10/05/11 16:36 91-20-3 Styrene NO ug1L 50.0 50 101051111 16:36 100-42-5 1,1,1,2-Tetrachloroethane ND ug1L 50.0 50 10/05/11 16,36 630-20-6 1,1,2,2-Tetrachloroethane ND uglL 50.0 50 10/05/11 16:36 79-34-5 Tetrachiaroethene ND ug1L 50.0 50 10105/11 16:36 127-18-4 Toluene ND ug1L 50.0 50 10/05/11 16.36 108-88-3 1,2,3-Trichlorobenzene N❑ ug1L 50.0 50 10/05/11 16-36 87-61-6 12,4-Trichlorobenzene NO ug1L 50.0 50 10/05/11 16:36 120-82-1 1, 1, 1 -Tric hloroethane 8900 ug1L 50.0 50 10/05/11 16:36 71-55-6 1,1,2-Trichloroethane ND uglL 50.0 50 10/05/11 16:36 79-00-5 Trichloroethene 63.5 uglL 50.0 50 10/05/11 16:36 79-01-6 Trichlorolluoromethane NO ug1L 50.0 50 10/05111 16:36 75-69-4 1,2,3-Tdchloropropane ND uglL 50.0 50 10/05/11 16:36 96-18-4 Vinyl acetate NO uglL 100 50 10/05/11 16:36 108-05-4 Vinyl chloride NO uglL 50.0 50 10/05111 16:36 75-01-4 m&p-Xylene NO uglL 100 50 10105111 16:36 179601-23-1 a-Xylene NO uglL 50.0 50 10/05/11 16:36 95-47-6 4-Bromofiuorobenzene (S) 94 °% 70-130 50 10/05/11 16:36 460-00-4 Dibromofluoromethane (S) 91 °% 70-130 50 10105/11 16:36 1868-53-7 1,2-Dichiorcethane-d4 (S) 91 % 70-130 50 10105M1 16:36 17060-07.0 Toluene-d8 (S) 105 °% 70-130 50 1 D105111 16,36 2037-26-5 2320E Alkalinity Analytical Method: SM 23208 Alkalinity,6icarbonate (CaCO3) 346 mg1L 5.0 1 10/09/11 16:20 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 15 at 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. d PaceAnalyticaI Services, Inc. Pace Analytical Services, Inc. �IeAnalyfica f 205 East Meadow Road - Suite A 2225 Riverside 0r. awwpaeelahs rem Eden, NC 27288 Asheville, NC 28604 (336)62M92l (B28)254-7176 ANALYTICAL RESULTS Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 Pace Analytical Services, Ine, 9800 KinceyAve. Suite f0o Huntersville, NC 28078 (704)875-9092 Sample: EBMW7 Lab ID: 92103587005 Collected_ 10/03111 16-00 Received: 10/04/11 11:49 Matrix. Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2320E Alkalinity Analytical Method: SM 2320E Alkalinity, Total as CaCO3 346 mg1L 5.0 1 10/09/11 16:20 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 835 mglL 25.0 1 10/05/11 15:42 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iran, Ferrous 81.9 mglL 5.0 10 10/10/11 18:12 H1,N2 4500S21) Sulfide Water Analyticat Method: SM 4500-S2D Sulfide 0.58 mglL 0.10 1 10108/11 12:00 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg1L 5.0 1 10/05/11 18:47 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mg1L 0.20 1 101051110114 Nitrogen, Nitrite 0.16 mglL 0.10 1 10/05/11 01:14 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 91.1 mglL 25.0 5 10/08/11 14:23 16887-00-5 5310E TOC Analytical Method: SM 53103 Total Organic Carbon 425 mglL 10.0 10 10/07/11 16:28 7440-44-0 Sample: Trip Blank LabID: 92103587006 Collected, 10/03/11 00:00 Received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low level Acetone Benzene Bromobenzene Bra mochloromethane Bromodichloromethane Bromofarm Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloramethane 2-Chlorotoluene 4-Chlorotoluene Analytical Method: EPA 8260 ND uglL NO ugll NO uglL NO uglL NO uglL ND uglL ND uglL NO uglL N❑ uglL ND uglL ND uglL ND uglL ND ug1L ND uglL ND ug1L 25.0 1 10105/1114:28 67-64-1 1.0 1 1010511114:28 71-43-2 1.0 1 10/05/11 14:28 108-86-1 1.0 1 1010511114:28 74-97.5 1.0 1 1010511114:28 75-27-4 1,0 1 1010511114:28 75-25-2 2.0 1 1010511114:28 74-83-9 5.0 1 10/05/1114:28 78-93-3 1.0 1 10105/1114:28 56-23.5 1.0 1 10/05111 14:28 108-90-7 1,0 1 10/05/1114:28 75-00-3 1,0 1 101051111428 67-66-3 1.0 1 10/05/11 14:28 74-87-3 1.0 1 101051111428 95-49-8 1.0 1 10/05111 1418 100-43-4 Date: 1Off 2/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 16 of 40 Tnis report shall not be reproduced, except in full, without the written con seal of Pace AnalylicaI Services, Inc.. q. Pace Analytical Services, Inc, Pace AnalytFcaI Services, Inc. 2fl5 East Meadow Road - Suite A 2225 Riverside Dr. aceAnalytical nrK.pacelahs.aun Eden, NC 27288 Asheville, NC 28804 (33W23-8921 (828)254-7176 ANALYTICAL RESULTS Project. CMi WWTP 6228-08-4691 Pace Project No.. 92103587 Pace Analylical Servieas, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Trip Blank Lab ID: 92103587OD6 Collected: 10/03/11 00:00 Received. 10/04/11 11 A9 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level 1,2-Dibromo-3-chlaropropane Dibromochlorom ethane 1,2-Dibromoethane (EDS) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dic hlorodifl uorom eth a ne 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1, 2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropen e Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyttoluene Methylene Chloride 4 -Meth yl-2- pen ta no ne {MIRK} Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Telrachloroethene Toluene 1.2, 3-Trichlo robe nzene 1,2,4-Trichlorobenzene 1,1,1-Trichiorcethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethan e 1,2,3-Trichtore propane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-SromoBuorobenzene (S) Dibromofluoramethane (5) 1,2-Dichloroethane-d4 (S) Analytical Method: EPA 8260 ND uglL &0 1 10/05/11 14:28 96-12-8 NO uglL 1.0 1 10/05/11 14:28 124-48-1 NO ugA- 1.0 1 10105111 14:28 106-93.4 ND uglL 1.0 1 10105/11 14:28 74-95-3 NO uglL 1.0 1 10/05/11 14:28 95-50-1 ND uglL 1.0 1 10105111 14:28 541-73-1 NO ug1L 1.0 1 10/05111 14.28 106-46-7 NO uglL 1.0 1 101D5111 14:28 75-71-8 ND uglL 1.0 1 10/05/11 14,28 75-34-3 NO uglL 1.0 1 10105111 14:28 107-06-2 NO ug1L 1.0 1 10/05/11 14.28 75-35-4 NO uglL i.0 1 10105/11 14:28 156-59-2 ND ug1L 1.0 1 10/05111 14:28 156-60-5 ND uglL 1.0 1 10/05/11 14:28 78-87-5 NO uglL 1.0 1 1OW11 14:28 142-28-9 ND ug1L 1.0 1 10/05/11 14:28 594-20-7 NO uglL 1.0 1 10/05/11 14:28 583-58-8 ND ug1L 1.0 1 10/05/11 1428 10061-01-5 NO ug1L 1.0 1 10/05/11 14:28 10061-02-6 ND uglL 1.0 1 10/05/11 14:28 108-20-3 NO ug1L 1.0 1 10/05111 14:28 1D0-41-4 NO ug1L 1.0 1 10/05/11 14:28 87-68-3 NO uglL &0 1 10105/11 14:28 591-78-6 NO ug1L 1.0 1 10/05/11 14:28 99-87-6 NO ug/L 10 1 10/05/11 14:28 75-09-2 ND uglL 5.0 1 10/05/11 14:28 108-10-1 ND ug/L 1.0 1 10/05/11 1428 1634-04-4 NO uglL 1,D 1 10/05/11 14:28 91-20.3 NO uglL 1.0 1 10/05/11 1428 100-42-5 ND uglL 1.0 1 10/05/11 1428 030.20-6 NO ug1L 1.0 1 10/05/11 14:28 79-34-5 NO uglL 1.0 1 10/05/11 1428 127-18-4 NO uglL 1.0 1 10/05/11 14:28 108-88-3 NO uglL 1.0 1 10/05/11 1428 87-61-6 NO uglL 1,0 1 10/05/11 14:28 120-82-1 ND uglL 1.0 1 10/05/11 14:28 71-55-6 ND ug1L 11,10 1 10105/11 14.28 79-OG-5 ND ug1L 1.0 1 10/05/11 14,28 79-01-6 ND ug1L 1.0 1 10M5111 14:28 75-69-4 ND ug1L 1.D 1 10/05/11 1428 96-18-4 NO uglL 2.0 1 10/05/11 14:28 108-05-4 NO ug1L 1.D 1 10105/11 14:28 75.01-4 ND uglL 2.0 1 10/05/11 14:28 179601-23-1 ND uglL 1.0 1 10/05/11 14:28 95-47-6 94 % 70-130 1 i0105111 14:28 460-00-4 87 % 70-130 1 10/05/11 14:28 1868-53-7 89 ❑1❑ 70-130 1 10/05/11 14:28 17060-07-0 Dale: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 17 o►40 This report shall not be reproduced, except In full, without the written consent of Pace Analylical Services, Inc.. a Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 205 East Meadow Road - Sufie A 2225 Riverside dr. 9800 KfnceyAve. Suite 100 K%w.pacelahs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623.8921 (828)254-7176 (704)875.9092 ANALYTICAL RESULTS Project: CMI WWTP6228-08.4691 Pace Project No.: 92103587 Sample: Trip Blank Lab ID: 92103587006 Collected. 101011 00:00 Received: 10/04/11 11:49 Matrix: Water Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8200 Toluene -dB (S) 101 °% 70-130 1 10/05/11 14:28 2037-26-5 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 18 of 40 This report shall not be reproduced, except in full, without the written Lonsent of Pace Analyticaf Services, Inc.. a Pace Analytical Services. Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ll�aceAnalXical 205 East Meadow Road - Suile A 2225 Riverside Dr. 9800 KlnceyAve. Suite 100 w pace s axn Eden, NC 27288 Asheville, NC 28604 Huntersvilie, NC 28078 [336]623 8921 1828)254-7178 (704)875-9092 QUALITY CONTROL DATA Project: CMI WWTP6228-08-4691 Pace Project No.: 92103587 QC Balch: AIR113302 Analysis Method: RSK 175 QC Batch Method; RSK 175 Analysis Description: RSK 175 AIR HEADSPACE Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004 METHOD BLANK: 1070404 Matrix: Water Associated Lab Samples. 92103587001, 92103587002, 92103587003, 92103587004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethane uglL ND 10.0 10/0711110:03 Ethene ug1L ND 10.0 1010711110:03 Methane ug1L ND 10.0 10107/1110:03 LABORATORY CONTROL SAMPLE & LCSD: 1070405 10704DG Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethane ug1L 114 124 118 109 104 70-130 5 30 Ethene ug1L 106 117 112 110 106 70-130 4 30 Methane uglL 60.7 68.7 66.8 113 110 70-130 3 30 SAMPLE DUPLICATE: 1070875 Parameter Ethane Ethene Methane 259463002 Dup Units Result Result ug1L NO N❑ ug1L ND NO uglL ND 15.8 RPD Qualifiers Dale: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 19 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ® Pace An atytic aI Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. . aceAnaly#1ca1 205 East Meadow Raad - Suite A 2225 Riverside Dr. 9$00 KInceyAve . Suite 100 nnw.pacelahs.rnm Eden, NC 27?B8 Asheville, NC 28804 Hontersvilla. NC 28076 (336)623-8921 (828)254-7176 (704)875.9092 QUALITY CONTROL DATA Project: CM WWTP 6228-06-4691 Pace Project No.- 92103587 QC Batch: AIR/13308 Analysis Method: RSK 175 QC Batch Method: RSK 175 Analysis description: RSK 175 AIR HEADSPACE Associated Lab Samples: 92103587D05 METHOD BLANK: 1070641 Matrix: Water Associated Lab Samples: 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Qualifers Ethane uglL NO 10.0 10/07/11 12:57 Ethane uglL NO 11D.0 10/07/11 12:57 Methane uglL NO 1 D.0 10/07/11 12:57 LABORATORY CONTROL SAMPLE & LCSD: 1070642 1070643 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc, Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethane uglL 114 118 128 104 113 70-130 8 30 Ethane uglL 106 112 120 106 113 70-130 7 30 Methane ug)L 60.7 66.8 6813 110 113 70-130 2 30 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072586 1072587 MS MSD 10171559003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD oval Ethane uglL ND 114 103 120 130 106 126 30-150 8 Ethene uglL ND 1D6 96A 113 118 106 122 30-150 4 Methane uglL 0.088 60.7 55.1 120 143 53 99 30-150 17 mg/L SAMPLE DUPLICATE. 1072585 Parameter Ethane Ethene Methane 259463003 Dup Units Result Result uglL NO NO uglL ND ND ug1L ND ND RPD Qualifiers Date 10112/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 20 o140 This report shall not be reproduced, except in full, without tha written consenl of Pace Analytical Services, Inc. e Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. acemalxical 205 Easi Meadow Road - Suite A 2225 Riverside ❑r. 9800 Kincey Ave. Suite 100 nnwpa adscflm Eden, NC 27288 Asheville, NC 2BB04 Huntersville, NC 28078 (336)623-8921 (928)254-7176 (7Q4)875-9092 QUALITY CONTROL DATA Project C M I WWTP 6228-08-4691 Pane Project No.: 92103587 OC Batch; MPRP19159 Analysis Melhod: EPAWO QC Batch Method: EPA 3010 Analysis description: 6010 MET Associated Lab Samples: 92103587001, 92103587002. 921035870D3, 92103587004, 92103587005 METHOD BLANK: 669016 Matrix: Water Associated Lab Samples; 92103587001, 92103587002, 92103587003, 92103587004, 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Cluali iers Calcium uglL NO 100 10/08/11 00:44 Manganese ug/L NO 5.0 1010811i 00A4 LABORATORY CONTROL SAMPLE' 669017 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Calcium ug/L 5000 5080 102 80-120 Manganese ug/L 500 488 98 80-120 MATRIX SPIKE SAMPLE- 669018 92103587001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Calcium ug/L 156000 5000 167000 216 75-125 M6 Manganese ug/L 2690 500 3190 99 75-125 SAMPLE DUPLICATE: 669019 92103587002 Dup Parameter Units Result Result RPO Qualifiers Calcium ug1L 401000 394000 2 Manganese ug1L 453 447 1 Date: 10112J2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 21 of 40 This report shall not be reproduced, except in Full, without the written consent of Pace Ana IocaI Services, Inc.. a. Pace Analytical Services, Inc. Pace Analytical 5ervices, Inc. 1�;a'ceAnalyfical 205 Ease Meadow Road - 50e A 2225 Riverside Dr wxwpmWahscom Eden, NC 27288 AsheVille, NC 28804 (336)623.8921 (828)254.7176 DUALITY CONTROL DATA Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 QC Batch: MSV116888 Analysis Method: EPA 8260 UC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103587001. 92103587002, 92103587003, 92103587005, 92103587006 METHOD BLANK: 668548 Matrix: Water Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587005. 92103587006 Blank Reporting Parameter Units Result Limit Analyzed 1,1.1,2-Tetrachloroethane uglL ND 1.0 1010511114:02 1,1,1-Tdchloroethane uglL ND 1,0 10/05/1114:02 1.1.2.2-Tetrachloroethane uglL ND 1.0 1010511114:02 1,1,2-Trichloroelhane uglL ND 1.0 10105M114:02 1,1-Dichloroethane uglL ND 1.0 1010511114:02 1,1-Dichloroethene ug1L ND 1.0 10/05/1114:02 1,1-Dichloropropene ug1L N❑ 1.0 1010511114:02 1,2,3-Tdchlorobenzene uglL ND 1,0 10105/1114:02 1,2,3-Trichloropropane uglL ND 1.0 1010511114:02 1,44-Trichlorobenzene ug1L ND 1A 1010511114:02 1,2-Dibromo-3-chioropropane uglL ND 5.0 1010511114:02 1,2-Dibromoethane (EDB) ug1L ND 1.0 IW05/11 14:02 1,2-Dichlorobenzene uglL ND 1.0 1010511114:02 1,2-Dichloroethane uglL ND 1.0 10/05/1114:02 1,2-Dichloropropane ug1L ND 1.0 10/0511114:02 1,3-Dichlorobenzene ug1L ND 1.0 10105/1114:02 1,3-Dichloropropane ug1L ND 1.0 1010511114.02 1,4-Dichlorobenzene u911- ND 1.0 10/0511114:02 2,2-Dichloropropane uglL ND 1.0 10105/1114:02 2-Butanone (MEK) ug1L ND 5.0 10/05111 14:02 2-Chlorotoluene uglL ND 1.0 10/05/1114:02 2-Hexanone ug1L N❑ 5.0 1010511114:02 4-Chiarotoluene ug1L ND 1.0 10/05/1114:02 4-Methyl-2-pentanone (MiBK) uglL ND 5.0 10/05/11 14:02 Acetone ug1L ND 25.0 10105/1114:02 Benzene ug1L ND 1.0 10/05/1114:02 Bromobenzene ug1L NO 1.0 1010511114:02 Bromochloromethane uglL ND 1.0 10105/1114:02 Bromodichloromethane uglL ND 1,0 10105(1114:02 Bromoform uglL ND 1.0 10105/1114:02 Bromomethane ug1L ND 2.0 10105M114:02 Carbon tetrachloride uglL ND 1.0 10/05/11 14:02 Chiorobenzene uglL ND 1.0 10105/1114:02 Chioroethane uglL ND 1.0 1010511114:132 Chloroform uglL ND 1.0 10105/1114-02 Chioromethane uglL ND 1.0 10105/1114-02 cis-1,2-Dichloroethane ug)L ND 1.0 1010511114:02 cis-1,3-Dichloropropene uglL ND 1.0 10/0511114-02 Dibromochloromethane uglL ND 1.0 1010511114:02 Dibromomethane ug)L ND 1.0 1010511114:02 Dichlorodifluoromethane uglL ND 1.0 1010511114-02 Diisopropyl ether uglL ND 1.0 10/05/11 14:02 Ethylbenzene uglL ND 1.0 10105/1114:02 Dale. 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pa0aAnalylical Services, Inc - Qualifiers Pace Analytical ServtC@S, Inc. 9500 KinceyAVe. Suite 100 HuntersvIlle, NC 28078 (704)875-9092 Page 22 of 40 a Pace Analytical Services, Inc. Pace Analytical Services, Inc. `aceAnalt I ica f 205 East Meadow Road - Suite A 2225 Riverside Dr. - �L w�m'W�s.cam Eden. NC 272B8 Asheville, NC 28804 (336)623-8921 (828y254-7176 QUALITY CONTROL DATA Proiect: C M I WWTP6228-D8-4691 Pace Project No.: 92103587 METHOD BLANK: 668548 Associated Lab Samples: Parameter Matrix: Water 92103587001, 92103587002, 92103587003, 92103587005, 92103587006 Blank Reporting Units Result Limit Analyzed Hexachloro-1.3-butadiene uglL ND 1.0 1010511114:02 m&p-Xyiene ug1L ND 2.0 1010511114:02 Methyl -tent -butyl ether ug1L ND 1.0 10105/11 14:02 Methylene Chloride ug1L ND 2.0 10/05/11 14:02 Naphthalene uglL ND 1.0 1010511114:02 o-Xyiene uglL ND 1.0 101051il14:02 p-isopropyitoluene uglL ND 1.0 1010511114:02 Styrene ug1L ND 1.0 1010511114:02 Tetrachloroethene ug1L ND 1.0 1010511114:02 Toluene ug1L ND 1.0 1010511114:02 trans-1,2-Dichloroethene uglL ND 1.0 1010511114:02 trans-1,3-13ichloropropene uglL ND 1.0 1010511114:02 Trichlaroethene ug1L ND 1.0 1010511114:02 Trichloroiluoromethane uglL ND 1.0 1010511114:02 Vinyl acetate vg1L ND 2.0 10/05/11 14:02 Vinyl chloride uglL N❑ 1.0 10/05/11 14:02 1,2-Dichloroethane-d4 (S) % 89 70-130 10/05/11 14:02 4-Bromottuorobenzene (S) % 93 70-130 10/05/11 14:02 Dibromotluoromethane (S) % 87 70-130 10/05/11 14:02 Toluene -dB (S) % 99 70-130 10/05/11 14:02 Qualifiers LABORATORY CONTROL SAMPLE- Parameter 668549 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug1L 50 53.5 107 70-130 1,1,1-Trichloroelhane uglL 50 42.4 85 70-130 1,1,2,2-Tetrachloroethane uglL 50 53.1 106 70-130 1,1,2-Trichloroethane uglL 50 52.2 104 70-130 1,1-Dichloroethane uglL 50 42.1 84 70-130 1,1-Dichloroelhene uglL 50 43.8 88 70-132 1,1-Oichloropropene ug1L 50 45.4 91 7D-130 1,2,3-Trichlorobenzene ug1L 50 50.6 101 70-135 1,2,3-Trichloroproparte uglL 50 52.3 105 70-130 1,2,4-Trichlorobenzene ug1L 50 48.0 96 70-134 1,2-Dibromo-3-chloropropane ug1L 50 52.0 104 70-130 1,2-Dibromoelhane (EOB) uglL 50 54.4 109 70-130 1,2-Dichlorobenzene ug1L 50 52.9 106 70-130 1,2-Dichloroethane uglL 50 473 95 70-130 1,2-Dichloropropane ug1L 50 5Z8 106 70-130 1,3-Dichlorobenzene uglL 50 52.0 104 70-130 1,3-Dichloropropane ug1L 50 54.1 108 70-130 1,4-Dichlorobenzene uglL 50 49.6 99 70-130 2,2-Dichloropropane ug1L 50 43.7 87 58-145 2-Butanone (MEK) uglL 100 108 108 70-145 2-Chlorotoluene uglL 50 53.8 108 70-130 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in Full, withvvt the written consent of Pace Analytical Services, inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 Clual iers Page 23 of 40 Pace Analytical Services, Inc. Pace Analytical Services, Inc. /// aceAnalyfical 205 East Meadow Road - Su teA 2225 Riverside dr. wrKwwcelabs.mm Eden, NC 27286 Asheville, NC 28804 (336)623.8921 {828)254.7176 QUALITY CONTROL DATA Prcjecl� CMI WW7P6228-08-4091 Pace Project No.: 921 G3587 �l'ie3i�•1Le]i�'L�Ie7.11.�eIE.1�1��i1;1�� I��I���: Parameter Units Spike Conc. LC5 Result LCS % Rec % Rec Limits 2-Hexanone ugll- 100 97.1 97 70-144 4-Chlorotoluene uglL 50 55.5 111 70-130 4-Methyl-2-pentanone [MIBK) uglL 100 99.8 100 70-140 Acetone ug1L 100 111 111 50-175 Benzene uglL 50 50.9 102 70-130 Bromobenzene uglL 50 50.0 10D 70-130 Bromochloromethane uglL 50 45.0 90 70-130 Bromodichloromethane uglL 50 52.0 104 70-130 Bromororm uglL 50 46.1 92 70-130 Bromomethane ug1L 5o 27.4 55 54-130 Carbon tetrachloride ug1L 50 49.8 100 70-132 Chlorobenzene ug1L 50 50.1 100 70-130 Chloroethane ug1L 50 45.3 91 64.134 Chloroform ugll- 50 5Z6 105 70-130 Chloromethane ug1L 50 491 99 64-130 cis-1,2-Drhloroethene uglL 50 41.7 83 70-131 cis-1,3-Dichloropropene ug1L 50 50.2 100 70-130 Dlbromochloromethane uglL 50 53.0 106 70-130 Dibromomethane ug1L 50 51.8 104 70-131 Dichioroditiuoromethane ug1L 50 59.7 119 56-130 Diisopropyl ether uglL 50 44.4 89 70-130 Ethylbenzene uglL 50 52.6 100 70-130 Hexachloro-1,3-butadiene uglL 50 51,6 103 70-130 m&p-Xylene uglL 100 111 ill 70-130 Methyl-tert-butyl ether uglL 50 46.4 93 70-130 Methylene Chloride uglt. 50 51.8 104 63-130 Naphthalene uglL 50 51.2 102 70-138 o-Xylene ug1L 5o 48,9 98 70-130 p-isopropyitoiuene uglL 50 49.7 99 70-130 Styrene uglL 50 50.5 101 70-130 Tetrachioroathene uglL 5o 60.3 101 70-130 Toluene ugh- 50 51.1 102 70-130 trans- l,2-Dichioroethene uglL 50 42,9 86 70-130 trans- 1,3-Dichloropropene ug& 50 50.0 100 70-132 Trichloroethene uglL 50 54.9 110 70.130 Trichloronuoromethane uglL 50 51.5 103 62-133 Vinyl acetate ug)L 100 86.6 87 66-157 Vinyl chloride ug1L 50 49,6 99 69-130 1,2-Dichioroethane-d4 (5) % 90 70-130 4-Sromofluorobenzene (5) % 99 70-130 DibromoTluoromethane (S) % 89 70-130 Toluene-d8 (S) % 100 70-130 Pace Analytical Services, Inc. 9800 KinCey Ave. Suite 100 Hunlersville, NC 28078 Qualifiers i(704)875-9092 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 24 of 40 This report shall not GB reproduced, except in full, without the written consent of Paca Analytical Services, Inc.. x Pace AnalyticaI services, Ina. Pace Analytical Services, Inc. aceAnalytica j 205 East Meadow Road - Suite A 2225 Riverslde Or, wmwpa_eJaSs.ccnr Eden. NC 27288 Asheville, NC 28804 (336)523.8921 (828)254.7176 QUALITY CONTROL DATA Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 Pace Analytical Services. Inc. 9800 KlnceyAve . Suite 100 Hunlersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 668550 668551 MS MSD 92103245024 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1.1-❑ichloroethene ug/L N❑ 50 50 49.1 48.5 98 97 M16B 1 Benzene uglL ND 50 50 36.9 39.5 74 79 70-148 7 Chlorobenzene ug/L ND 50 50 42.4 42.5 85 85 70-146 0 Toluene uglL N❑ 50 5D 42.4 42.4 85 85 70-155 0 Trichioroethene ug/L 8.5 50 50 48.1 47.2 79 77 69-151 2 1,2•Dichloroelhane-d4 (S) % 115 118 7D-130 4-Sromofluorobenzene {S) % 91 90 70.130 Dibromol7uoromethane (S) % 114 115 70-130 Toluene -dB (5) % 92 93 70-130 Date10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 25 of 40 Thls report shall not be reproduced, except In full, without the written consent of Pace Analytica I Services, Inc.. Pace Anatytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc, 205 East Meadow Road - Suite A 2225 Riverside Dr 9800KinceyAve. Suiteloo 1!;a'ceAna1j4ica1" trww.parefabs.rnm Eden, NC 27286 Asheville, NC 28804 Huntersville, NC 28078 (336)62"921 (828)254-7176 (704)875-9092 DUALITY CONTROL DATA Project: Civil WWTP6228.08-4691 Pace Project No.: 92103587 QC Balch: MSV116914 Analysis Method: EPA 8260 QC Batch Method EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103587004 METHOD BLANK_ 670089 Associated Lab Samples: 92103587004 Parameter Matrix: Blank Units Result Water Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ugiL ND 1.0 1011011113:00 1.1.1 Trichloroethane ugiL ND 1-0 10/10/11 13:00 1,1,2,2-Tetrachloroethane ug1L ND 1.0 1011011113:00 1,1,2-Trichloroethane ugiL ND 1.0 1011o11113:00 1,1-Dichloroethane ugiL NO 1.0 1011011113:00 1,1-Dichloroethene ugiL ND 1.0 1011011113:00 1.1-Dichloropropene ugiL ND 1.0 10110/1113:00 1,2,3-Trichlorobenzene ugiL ND 1.0 1D1i011113:00 1,2,3-Trichlaropropane ugiL NO 1.0 10/1oil 113:00 1,2,4-Trichlorobenzene ugiL NO 1.0 10/1D11113:00 1,2-Dibromo-3-chloropropane ugiL ND 5.0 1011011113:00 1,2-Dibremoethane (EDB) ugiL NO 1.0 10/10/11 13:00 1,2-Dichlorobenzene ugiL NO 1.0 10/10/11 13:00 1,2-Dichloroethane ugiL ND 1.0 1011011113:D0 1,2-Dichloropropane ugiL NO 1.0 1011011113:00 1,3-Dichlorobenzene ugiL NO 1.0 10110/1113:D0 1,3-Dichloropropane ugiL NO 1.0 10110/1113-00 1,4-Dichlorobenzene ugiL ND 1.a 10110/1113:00 2,2-Dichloropropone ugiL NO 1.0 1011011113:00 2-Butanone (MEK) ugiL NO 5.0 10/10/11 13:00 2-Chlorototuene ugiL ND 1.0 1D11Dill 13:00 2-Hexanone ug1L NO 5.0 1011011113:00 4-Chlorotoluene ug1L NO 1.0 10/1011113:00 4- Moth yl-2-pentanone (MlBK) ugiL ND 5.0 10/10/11 13:00 Acetone ugiL NO 25.0 1011011113:00 Benzene ug1L NO 1.0 1011011113-00 Bromobenzene ug1L ND 1.0 10110/1113:00 Bromochloromethane ugiL ND 1.0 10/10/1113:00 Bromodichlaromethane ugiL NO 1.0 1011011113:00 Bromaform ugiL NO 1.0 10/1011113:00 Bromomethane ug1L ND 2.0 10/10/1113:00 Carbon tetrachloride ugiL ND 1.0 10MOIll 13;00 Chlorobenzene ugiL ND 1.0 10110/1113:00 Chloroethane ugiL ND 1 A 10/10/11 13:00 Chloroform ugiL ND 1.0 10110/1113:00 Chloromethane ugiL ND 1.0 10110/1113,00 cis-1,2-Dichloroe thene ugiL ND 1.0 10/10I1113:00 cis- 1,3-Dichloropropene uglL NO 1.0 10110/1113:00 Dibromochloromethane ugiL ND 1.0 10110/1/ 13:00 Dibromamethane ugiL ND 1.0 1011011113:00 Dichiorodit]ucromethane ugiL ND 1.0 10/10/11 13 00 Diisopropyl ether ugiL NO 1.0 10/10/11 1100 Elhyibenzene ugiL ND 1.0 1011011113:00 Date: 1011212011 01.55 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 26 of 40 �_ Pace Analytical Services, Inc. Pace Analytical Services, Inc. l aceRnalytical 205 Easl Meadow Road - Suite A 2225 Riverside Dr. xx�r.pa rlabs.onm Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254.7176 QUALITY CONTROL. DATA Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 METHOD BLANK: 670089 Associated Lab Samples: Parameter 92103587004 Units Matrix: Blank Result Water Reporting Limit Analyzed Hexachloro-1,3-butadiene ug)L NO 1,0 101101111100 m&p-Xylene ugIL ND 2.0 1011011113:00 Methyl-tert-butyl ether ug/L NO 1.0 10/10/11 13:00 Methylene Chloride ug)L ND 2.0 10/10/11 13:00 Naphthalene ug/L ND 1.0 1011011113:00 a-Xylene ug)L NO 1.0 10/10/11 13:00 p-tsopropyltoluene uglL NO 1.0 10/10/11 13:00 Styrene ug/L NO 1.0 10/10/11 13:00 Tetrachloroethene ug)L NO 1.0 1011011113:00 Toluene ug1L ND 1.0 10110/1113:00 trans-1,2-Dichloroethene ug/L ND 1.0 10/10/1113:00 trans-1,3-Dichloropropene ug/L ND 1.0 1011011113:00 Trichloroethene ug1L ND 1.0 1011011113:00 irichiorollucromethane ug/L NO 1.0 10/10/11 13 00 Vinyl acetate ug1L ND 2.0 10/10/11 13;00 Vinyl chloride ug/L ND 1.0 10/10/11 13:00 1,2-Dichloroethane-d4 (S) % 118 70-130 10110/11 13:00 4-Bromofiuoroberizene (S) % 95 70-130 10/10/11 13:00 Dibromofluaromethane (S) % 116 70-130 10110/11 13:00 Toluene-d8 {S) % 102 70-130 10/10/11 13:00 Qualifiers LA13DRATORY CONTROL SAMPLE: Parameter 670090 units Spike Canc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Telrachlorcelhane uglL 5D 53.4 107 70-130 1,1,1-Trichloroelhane uglL 50 45.5 91 70.130 1,1,22-Tetrachloroethane ug/L 5D 51-9 104 70-130 1,1,2-Trichtoroe lhane ug1L 50 51.2 102 70-130 11-Dichlaroethane uglL 50 44.7 8g 70-130 1,1-Dichlorcethene ug/L 50 45.5 91 70-132 i,1-Dichloropropene ug/L 50 47.5 95 70-130 1,2,3-Trichlorobenzene uglL 50 47.9 96 70-135 1,2,3-Trichloropropane uglL 50 50.15 101 70-130 1,2,4-Trichlorobenzene ug/L 50 47.0 94 70-134 1,2-Dibromo-3-chloropropane ug/L 50 53.5 107 70-130 1,2-Dibromoethane (EDB) ug/L 50 53.7 107 70-130 1,2-Dichlnrobenzene ug/L 50 50.5 101 70-130 1,2-Dichloroethane ug/L 50 51.2 102 70-130 1,2-Dichioroprapane ug/L 50 53.0 106 70-130 1,3-Dichlorobenzene ug/L 50 50.1 100 70.130 1,3-Dichloropropane ug/L 50 53.6 107 70-130 1,4-Dichiorobenzene ug/L 50 47.4 95 70-130 2,2-Dichloropropane ug/L 50 48.3 97 58.145 2-Butanone (MEK) ug/L 10t] 116 116 70-145 2-Chiorotoluene ug/L 50 51.7 103 70-130 Pace Analytical Services, Inc. 9800 Kincey Ave. Suile 100 Huntersvllle. NC 28078 (704)875-9092 Qualifiers Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 27 of 40 This report shall not be reproduced, except in UT, without the written consent of Pace Analytical Services, Inc.. z Pace AnalybeaI Services, Inc. Pace Analytical Services. Inc. 205 East Meadow Road - SulteA 2225 Riverside Or1!2eAnaOical WWW paCvW5 car" Eden. NC 27288 Asheville, NC 28804 (336)023.8921 (828)254-7176 QUALITY CONTROL DATA Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 Pace Analytical Serrvlces, Inc. 9300 Kincey Ave. Suite 100 Huntemville, NC 28076 LABORATORY CONTROL SAMPLE: Parameter 670090 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Hexanone ug/L 100 102 102 70-144 4-Chlorotoluene ug/L 50 53.6 107 70-130 4-Methyl-2-pen La none (MIBK) ug/L 100 102 102 70-140 Acetone ug/L 100 127 127 50-175 Benzene ug/L 50 43.2 86 70-130 Bromobenzene ugIL 50 48.7 97 70-130 Bromochloromethane ug/L 50 47.9 96 70-130 Bromodichloromethane uglL 50 51.9 104 70-130 Bromoform uglL 50 47.8 96 70-130 Bromomethane uglL 50 19.7 39 54-130 LO Carbon tetrachloride uglL 50 48.6 97 70.132 Chlorobenzene uglL 50 49.2 98 70-130 Chloroethane uglL 50 46.0 92 64-134 Chloroform uglL 5o 55.5 111 70-130 Chloromethane uglL- 50 55.1 110 64-130 cis-1,2-Dichioroethene uglL 50 43.7 87 70-131 cis-1,3-Dichloropropene uglL 50 51.1 102 70-130 Dibromochloromethane ug)L 50 54.0 108 70-130 Dibromomethane uglL 50 52.3 105 70-131 DichiorodiPuoromethane uglL 50 64.6 129 56-130 Diisopropyl ether uglL 50 47.6 95 70.130 Ethyibenzene ug/L 50 51.4 103 70-130 Hexachloro-1,3-butadiene ug1L 50 49.8 100 70-130 m8p-Xylene ug/L l00 106 106 70-130 Methyl-tert-butyl ether ug/L 50 51A 102 70-130 Methylene Chloride uglL 50 52.9 106 63-130 Naphthalene ugIL 50 49.9 1D0 70-138 o-Xylene ug/L 50 48A 97 70-130 p-Isopropyltoluene ug/L 50 48.1 96 70-130 Styrene ugIL 50 49.3 99 70-130 Tetrachlorceihene ug/L 50 49.6 99 70-130 Toluene ug/L 5o 50.3 101 70-130 Ira ns•1.2-0ichloroethane ugIL 50 44.4 89 70-130 trans-1,3-0ichloropropene ugIL 5o 50.5 101 7D-132 Trichloroethene uglL 50 54.2 108 70-130 Tfichlorofluoromethane ug/L 50 54.3 109 62.133 Vinyl acetate ug/L 100 92.1 92 66-157 Vinyl chloride ug1L 5o 53.9 108 69-130 1,2-Dichloroethane-d4 (S) % 96 7D-130 4-Bromofluorobentene (S) % 102 70-130 Dibromofluoromelhane (S) % 94 70-130 Toluene-d8 (S) % 99 70-130 Date: 10/12/2011 01-55 PM REPORT OF LABORATORY ANALYSIS This reporl shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 28 of 40 R aceAnalytical - rrwwpace7ahswm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (338 )523-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, INC 28804 {828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 HunSersville, NC 28070 (704)875-9092 Projects CM WWTP 6228-08-4691 Pace Project No.: 92103587 MATRIX SPIKE & MATRIX SPIKE DUPLICATE, 670091 670092 MS MSD 92103399016 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conn. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1-Dichloroethene uglL 21.2 50 50 63,7 64A 85 86 70-166 1 Benzene ug/L ND 50 50 53.9 55.3 108 111 70-148 3 ChlDrobenxene ug1L ND 50 50 60A 61.8 120 124 70.146 3 Toluene ug1L ND 50 50 55.9 57A 112 114 70-155 2 Trichloroethene uglL ND 50 50 50.6 51.2 101 102 69-151 1 1,2-Dichloroethane-0 (S) % 119 118 70-130 4-Bromofluorobenxene (5) % 94 96 70-130 DihromoFluoromethane (S) % 113 112 70-130 Toluene-d8 (S) % 89 90 70-130 Date: 1011W2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 29 of 40 This report shall not be reproduced, except in full, without the written consent at Pace Analytical Services, Inc.. ,, r�s Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAl7alytical 205 East Meadow Road - Suite A 2225 Riverside Ur. 9800 KinceyAve . Suite 100 n%,a,psce1aha cam Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (338)623-8921 (828)254-7176 R704j875-9092 QUALITY CONTROL DATA Project: CMI WVVTP 6228.08-4691 Pace Project No.: 92103587 OC Balch: WET118181 Analysis Method: SM 2320B QC Balch Method. SM 2320B Analysis Description: 2320B Alkalinity Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004, 92103587005 METHOD BLANK: 670489 Matrix: Water Associated Lab Samples: 92103587001, 92103587002. 92103587003, 92103557004, 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg1L ND 5.0 10/09/11 16:20 Alkalinity,Bicarbonate, (CaCO3) mg1L ND 5.0 10/09/11 16:20 LABORATORY CONTROL SAMPLE: 670490 Spike LCS LCS % Rec Parameter Units Conc. Result % Rea Limits Qualifiers Alkalinity, Total as CaCO3 mg1L 50 50.1 i00 90-110 Alkalinity,Bicarbonate (CaCO3) mglL 9.0 SAMPLE DUPLICATE 670491 92103587001 Dup Parameter Units Resell Result RPD Qualifiers Alkalinity. Total as CaCO3 mg1L 447 420 6 Alkalinity,Bicarbonale (CaCO3) mg1L 447 420 6 SAMPLE DUPLICATE: 670492 92103544013 Dup Parameter Units Result Result RPD Qualifiers Alkalinity, Total as CaCO3 mg1L 16.9 19.0 12 Aikalinity,Bicarbonate (CaCO3) mg1L 16.9 19.0 12 Dale: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 30 of 40 This report shall not be reproduced, except in full, without the written consent 01 Pace Ana Iyhcal Services, Inc . Pace Analytical Services, Inc, Pace Analytical Services, Inc. Pace Analytical Services, Inc. aeeAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980O KinceyAve. Suite 100 • riww.parelabs.wm Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28076 (336)623.8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project; GMI WWTP 6228-08.4691 Pace Project No.: 92103587 QC Batch: WET118132 Analysis Method: SM 2540C QC Batch Method; SM 2540C Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004, 921035870D5 METHOD BLANK: 668680 Matrix: Water Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004, 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg1L ND 25.0 10/05/11 115:38 LABORATORY CONTROL SAMPLE: 668681 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg)L 250 246 98 80-120 SAMPLE DUPLICATE: 668682 92103519001 Dup Parameter Units Result Result RPO Qualifiers Total Dissolved Solids mgJL 947 961 1 Date: 10/1212011 01;55 PM REPORT OF LABORATORY ANALYSIS Page 31 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Ino.. aceAnalyticalCS nwkpacrJahs.cnm Pace Analytical Services, Inc. 205 East Meadow Road - Suile A Eden, NC 27288 (336)623.8921 Project: CMi WWTP 6228-08-4691 Pace Project No.: 92103587 Pace Analytical 5arvices, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DUALITY CONTROL DATA QG Batch: WET118158 Analysis Method: SM 35D0-Fe D#4 QC Batch Method: SM 3500-Fe D#4 Analysis Description: Iron, Ferrous Associated Lab Samples: 92103587001. 92103587002. 92103587003, 92103587004, 92103587D05 METHOD BLANK: 669771 Matrix: Water Associated Lab Samples: 92103587001. 92103587002, 92103587003, 92103587004. 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Iron, Ferrous mg1L NO 0,50 10/10/11 16:48 N2 Pace Analytical Services, Inc. 9800 I(incey Ave. Suite 700 Huntersville, INC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 669772 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec. Limits Qualifiers )ron, Ferrous mg1L 1.5 1.6 105 90-110 N2 SAMPLE DUPLICATE: 669773 Parameter Iron, Ferrous 92103587001 Dup Units Result Result mg1L NO NO RPD Qualifiers N2 Date: 10/1212011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 32 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. e Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAna f ` fical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 KinceyAve. Suhe l00 xxw.pa[s?a6s.c�m Eden, NC 27288 Asheville, NC 28804 HuntersWle, NC 28078 (336)623.8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Projecl. CMI VVWfP 6228-08-4691 Pace Project No.: 92103587 QC Batch: WET118178 Analysis Method: SM 4500-S2Q QC Batch Method: SM 4500-S2D Analysis Description: 450oS2❑ Sulfide Water Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004, 92103587005 METHOD BLANK: 670418 Matrix; Water Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004, 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide mglL ND 0.10 1010811112:00 LABORATORY CONTROL SAMPLE: 670419 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide mglL 5 0.52 104 90-110 MATRIX SPIKE SAMPLE: Parameter 670420 Units 92103587001 Result Spike NIS MS % Rec Cone. Result % Rec Limits Qualifiers Sulfide mg1L ND 5 0.39 78 75-125 SAMPLE DUPLICATE. 670421 92103587001 Dup Parameter Units Result Result RPD Qualifiers Sulfide mg1L ND ND Date: 10/1212011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 33 of 40 This report shall not he reproduced, except in full, without the written consent of Pace An aIytical Services, Inc.. e Pace Analytical Services, Inc. Pare Analytical Services. Inc. Pace Analytical Services. Inc. aeeAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 we pacetabswm Eden, NC 27288 Asheville, NC 28604 Huntersvllle, NC 28078 (336)623-8921 (828)254-7176 [704]875-9092 QUALITY CONTROL DATA Project: CMI WWTP 6228-08-4091 Pace Project No.: 92103587 QC Batch: WETA110673 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples., 92103587001. 92103587002. 92103587003, 92103587004, 92103587005 METHOD BLANK: 668009 Matrix: Water Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103,987004, 921035B70G5 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg1L ND 5.0 1010511116:59 LABORATORY CONTROL SAMPLE: 068010 Spike LCS LCS °% Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mglL 20 19A 97 90-110 MATRIX SPIKE SAMPLE: 668011 92103587001 Spike MS MS % Rec Parameter Units Result Conc. Result °% Rec Limits Qualifiers Sulfate mg/L &9 20 28.9 100 90-110 MATRIX SPIKE SAMPLE; 668013 92103519005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mglL 37.0 20 50.7 68 90-110 MI SAMPLE DUPLICATE: 668012 92103587001 Dup Parameter Units Result Result RPD Qualifiers Sulfate mg1L 8.9 8.9 0 SAMPLE DUPLICATE: 668014 92103519005 Dup Parameter Units Result Result RPD Qualifiers Sulfate mglL 37.0 37.0 0 Gate: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 34 of 40 This report shall not be reproduced, except in full, without the written consent 0f Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAna1j4ica1205 East Meadow Road - SuIle A 2225 Riverside ❑r. 9800 Kincay Ave. Suite 100 Kx�r.pareJabs,com Eden, NC 27288 Asheville, NC 20804 Hontersvllle, NC 28078 (336)623-8921 (828)254-7176 (744)875-9092 QUALITY CONTROL DATA Project. CMI WWTP 6228-08-4691 Pace Project NO.' 92103587 QC Batch: WETA110677 Analysis Method: EPA 353,2 QC Batch Method: EPA 353,2 Analysis Description; 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004 METHOD BLANK: 668289 Matrix: Water Associated Lab Samples: 92103587001, 92103587002, 92103587003. 92103587004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg]L NO 0.20 10/04/11 22;59 Nitrogen, Nitrite mg/L ND 0A0 10104111 22:59 LABORATORY CONTROL SAMPLE' 668290 Spike LCS LCS %, Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.0 100 90-1i❑ Nitrogen, Nitrite mg1L 1 1.0 102 90-110 MATRIX SPIKE SAMPLE: 668291 92103666002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 33.3 5 36.5 64 90-110 MB Nitrogen, Nitrite mg/L N❑ 1 1.3 113 90-110 M1 MATRIX SPIKE SAMPLE: 668293 92103667002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg1L 7.6 5 14.7 142 90-110 Mi Nitrogen, Nitrite mg/L NO 1 1.1 110 90-110 SAMPLE DUPLICATE: 668292 92103666002 Dup Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mg1L 33.3 33.8 2 Nitrogen, Nitrite mg1L NQ ND SAMPLE DUPLICATE: 668294 92103667002 Dup Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mglL 7.6 7,8 3 Nitrogen, Nitrite mg1L ND ND Date, 10/12/2011 01,55 PM REPORT 0IF LABORATORY ANALYSIS Page 35 of 40 This report shall not be reproduced, except in full, without the wriEfen consent of Pace Analytical services, Inc.. a Paca Analytical Servicas, lac. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside ter. 9800 KioceyAvs Suite Soo aceAnaiy icaJ wo pacera>yamm Eden, NC 27288 Asheville, NC 28804 Huhtersvilte, NC 28078 (336)623-8921 (828)254.7176 (704)875-9092 QUALITY CONTROL DATA Project: CM WWTP 6228-08-4691 Pace Project No.: 92103587 QC Hatch: WETA110678 Analysis Method: EPA 353.2 QC Batch Method: EPA 353,2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92103587005 METHOD BLANK: 668295 Matrix: Water Associated Lab Samples: 92103587005 Blank ReporUng Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg1L ND 0,20 10104/11 23:39 Nitrogen, Nitrite mg/L N❑ 0.10 10/04/11 23:39 LABORATORY CONTROL SAMPLE; 668296 Spike LOS LCS °% Rec Parameter Units Conc. Result °% Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 4.5 90 90-110 Nitrogen, Nitrite mg1L 1 1,0 103 90.110 MATRIX SPIKE SAMPLE: 668297 92103620003 Spike MS MS °% Rea Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mglL ND 5 5.9 117 90-110 M1 Nitrogen, Nitrite mg1L NO 1 1.2 115 90-110 M1 SAMPLE DUPLICATE: 668298 92103620003 Dup Parameter Units Result Result RPO Qualifiers Nitrogen, Nitrate mg1L NO NO Nitrogen, Nitrite mg1L NO NO Date: 10112/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 36 of 40 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc . a Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical5ervlces, Inc. aceAnalX cal 205 East Meadow Read - Suite A 2225 Riverside ❑r 9800 Kincey Ave. Suite 100 nKwpaselaGs.Gnm Eden, NC 27265 Asheville, NC 25804 Huntersville, NC 28078 (336)623-8921 (828)254.7176 (704)875.9092 QUALITY CONTROL DATA Project: CMI WWTP 6228-08-4691 Pace Project No.: 92103587 QC Batch: WETA110698 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500•CI•E Analysis Description: 4500 Chloride Associated Lab Samples: 92103587001. 92103587002, 92103587003, 92103587004 METHOD BLANK: 669945 Matrix: Water Associated Lab Samples: 92103587001. 92103587002, 92103587003, 92103587004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mglL NO 5.0 1010711114:20 LABORATORY CONTROL SAMPLE: 669946 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mglL 20 20.0 100 90-110 MATRIX SPIKE SAMPLE: 669947 92102974001 Spike MS Nis % Rec Parameter Units Result Conc. Result °I° Rec Limits Qualifiers Chloride mglL 18400 uglL 20 37.3 94 75-125 SAMPLE DUPLICATE: 669948 92102974002 Dup Parameter Units Result Result RP❑ Qualifiers Chloride mglL 23600 ug)L 23.8 1 Date; 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 37 of 40 This report shall not be reproduced, except in full, without She written consent of Pace Analytical Services, Inc.. 4P Pace Analytical services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 205 East Meadow Road - SuiteA 2225 Riverside Dr. 9800 KfnceyAve. Suite 100 1%rn.pacefab&C0M Eden. NC 27288 Ashevllle, NC 28H04 Huntersville, NC 28076 1 (336)623-8921 (828)254-7178 (704)875-9092 QUALITY CONTROL DATA Project: C M I WWTP6228-48-4691 Pace Project No.: 92103587 QC Batch: WETA110712 Analysis Method: SM 4500-CI-E QC Batch Method. SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 92103587005 METHOD BLANK: 670430 Matrix: Water Associated Lab Samples: 92103587005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg1L ND 5.0 1010811113:44 LABORATORY CONTROL SAMPLE: 670431 Spike LCS LCS % Rec Parameter Units Canc. Result % Rec Limits Qualifiers Chloride mg1L 20 20.7 103 90-110 MATRIX SPIKE SAMPLE: 670432 92103587005 Spike MS MS % Rec Parameter Units Result Canc. Result % Rec Limits Qualifiers Chloride mg1L 91.1 20 109 90 75-125 SAMPLE DUPLICATE: 670433 92103486002 Dup Parameter Units Result Result RPD Qualifiers Chloride mglL 14.7 15.3 4 Date: 10/12/2011 01.55 PM REPORT ❑F LABORATORY ANALYSIS Page 38 of 40 This report shall not be reproduced, except in full, without }ate written consent of Pace Analytical Services, Inc.. x Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalXical 205 East Meadow Road - SuiteA 2225 Riverside Dr. 9800 Klncey Ave. Suite 100 nxx,yacotaLs.wm Eden, NC 27288 Asheville, NC 28804 Huntersvllle, NC 28078 [336]623-8921 (828)254.7176 (704)875.9092 QUALITY CONTROL DATA Project: CMI WWTP6228-08-4691 Pace Project No.: 92103587 QC Batch: WETA110684 Analysis Method-. SM 53106 OC Batch Method. SM 5310B Analysis Description: 5310B TOC Associated Lab Samples: 92103587001, 92103587002, 92103587003, 92103587004. 92103587005 METHOD BLANK: 668627 Matrix; Water Associated Lab Samples: 92103587001, 92103587002. 92103587003, 92103587004, 92103587005 Blank Reporting Parameter Units Result Limit Analyzed ❑ualifiers Total Organic Carbon mglL NO 1.0 10/07/11 15;01 LABORATORY CONTROL SAMPLE: 668628 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers TOW Organic Carbon mg1L 25 22A 90 90-110 MATRIX SPIKE SAMPLE: 668629 92103587001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg1L 7,3 25 29.7 90 75-125 MATRIX SPIKE SAMPLE: 668631 92103336005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg1L 1.6 25 25.8 97 75-125 SAMPLE DUPLICATE: 668630 92103587002 Dup Parameter Units Result Result RPD Qualifiers Total Organic Carbon mg1L 9.0 9.1 1 SAMPLE DUPLICATE: 668632 92103336006 Dup Parameter Units Result Result RPD Qualifiers Total Organic Carbon mg/L 1.6 1.6 3 Date: 10/12/2011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 39 of 40 This report shall not be reproduced. except in full, without the written consent of pace Analytical Services, 1nc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analyticat Services, Inc. G'e �14�fG' f 205 Ease Meadow Road - Suite A 2225 Riverside Dr. 9800 kinceyAve. Suite 100 _ xxwpaJceta6` sram Eden. NC 27288 Asheville, NC 28804 Huntersville. INC 28078 (336)623.8921 (828)254.7176 (704)875-9092 QUALIFIERS Project: CM WWTP 6228-08-4691 Pace Project No.: 92103587 DEFINITIONS OF - Dilution Factor. if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution or the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. S - Surrogate 142-DOhanylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RP values. LCS(D) - Laboratory Control Sample (Duplicate) MS�Dj - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NO - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed Tor, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each anaiyte is a combined concentration. Acid preservation may not be appropriate for 2-Chioroethyivinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited anal ytes. LABORATORIES PAS I -A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-M Pace Analytical Services • Minneapolis ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. H1 Analysis conducted outside the EPA method holding lime. LO Ana lyte recovery in the laboratory control sample (LCS) was outside 0C limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. N2 The tab does not hold TNI accreditation for this parameter. Date: IOft 212011 01:55 PM REPORT OF LABORATORY ANALYSIS Page 44 of 40 Th-s report shall not be reproduced, except in full. without the written consent of PaceAnalvtical Services. Inc... ;a?ceAnaVica1' CHAIN -OF -CUSTODY / Analytical Request Document Th8 Chajn-0f-Custody is a LEGAL DOCUMENT- All relevant Gelds must be camplelad accuratoly- Pager: ❑f Section A Sectlon B Section C 150365 2 Re gat red Chen In forma Lori- Required Project Inlormation: In"m Informatian- Company: Report To: Ahonrion, Addr �} Gppy Tp- Company Name: REGULATORY AGENCY 7`dJ [i4 AJ < Address: [- NPI)ES GROUND WATER I- DRINKING WATER [- UST RCRA r OTHER E it To- Purchase Order No : Pace auorc fterorenae: Phone: F;sz. Project Name �r Paca Prgacl Site LOG7tivn C./+"+L- s TA rjE: Requested Due Dala/TAT- t F Project Number: �- }� ll Pace Profilo 9 ^] -7 �, C� L Requested Analysis Filtered (YIN) Section D Matrtx Codes a x Roq ulrod Client lnfomm bw MATRjX r CgOE n COLLECTED Preservatives i pdrrking I(4 ali]f DW O [] x O Water WTpp V COMPOGiTe CW.rr'OSIT[ P Waste Water WW v m ,TART IZKMGFu V = Product P �. SoiVSolid S1. g [a ❑ rn " '� SAMPLE ID Wipe " w � WP A-,-, D.g 1 .} Air AR o w a 2 ~ { H a r^7 Sample IDs MUST 8E UNIQUE �se TS C) J I b N rY u_ ti d T 0 c`-i M tJ S W Q C q fl a N . _ V a m DATE TIME DATE TIME w V.] z r z z z `r O a Pace Project No.1 Lab I.D. J v ✓ D 2 n oo v " d129 ii tiI U V d� 7 s W 3 v V `� 7 B 9 ,o tt 12 ADDITIONAL COMMENTS RELIN ISH BY !AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION HATE TIME SAMPLE CONDITIONS ISM p plqlj SAMPLER NAME AND SIGNATURE OP.iGINAL PRINT Name of SAMPLER- a )= m r m m m -" cc m �. `m n E SIGNATURE pf SAMPLER: DATE 5lgned (' J (MMIDDrYY)! [ +� w ar--owwnt NOLO; cw 56Qn09 vas rvrm roe are s Vlknq Pace's NeT 30 rrav caymenl InmA and Veep+. - r:,v. charge, 1 11 -rer men"- r-----'nvoir s 'I rw N r I L-O-C '. , 5-1 Document Name: Document Revised: July 29, 2011 f 2eAnjVical Sample Condition Upon Receipt (SCUR) Pace 1 of 2 Document Number: Issuing Authority: F-CHR-CS-03-rev,05 Pace Huntersville Quality Office C ' nt Name: Project # ��� 3�k 7 Where Received: Huntersville ❑ Asheville ❑ Ede Courier; ❑Fed Ex ❑ UPS❑ LISPS❑ Client❑ G martial Pace tither Q-tlOnal�:- Praj�d,laepateft"I , Custody Seal on CoalerlBox Present: ❑ yes no Seals intact. ❑yes ❑ no Proj.NaiieWt . Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None Ll Other Thermometer Used: IR Gun T1102 Type of Ice Blue None Samples on ice, cooling process has begun Temo Correction Factor Add / Subtract 0 'C Corrected Cooler Tem. D C Temp.: Biological Tissue Is Frozen: Yes No NIA Date and Initial of er ning contents: l� '� �� Temp should be above freezing to 6'C Comments: Chain of Custody Present: Leles No ❑NIA 1. Chain of Custody Filled Out: es No ❑NIA 2, Chain of Custody Relinquished: EfY.s ❑No ❑NIA 3. Sampler Name & Signature on COG: L24 ONO ❑NIA 4. Samples Arrived within Hold Time: es No ❑NIA 5. Short Hold Time Analysis <72hr : Yes ONO NIA g, Rush Turn Around Time Requested: Dyes No ❑NIA 7. Sufficient Volume: k< No ❑NIA 8. Correct Containers Used: Yes No ❑WA 9. _ -Pace Containers Used: es No ❑NIA Containers Intact: ErYes ❑No ❑NIA O. Filtered volume received for Dissolved tests ❑Yes No NIA 11. Sample Labels match COC: Oles ONO ©NIA 12. -Includes date/time/ID/Analysis Matrix: 7- All containers needing preservation have been checked. es ON- ❑NIR 1 3- All containers needing preservation are found to be in 61Y compliance with EPA recommendation. rrrr���� ONO ❑NIA exceptions: VOA, coliform, TOC, O&G, WI -SRO (water) ❑Yes ❑No Inilial Men completed Samples checked for dechlodnatlon: Yes El No ❑NIA 14. Headspace in VOA Vials { a6mm): E)Yej ONo ❑NIA 15. Trip Blank Present: Y ONO ❑NIA 16. Trip Blank Custody Seals Present Yes ONO ONIA Pace Trip Blank Lot # {if purchased): Client Notification) Resolution: Field Oata Required? Y 1 N Person Contacted: DateMme: Comments/ Resolution: SCURF Review: Y Date: I SRF Review: � Qate: ra Y Note: Wheneve is-, discrepancy affecting North Carolina compliance samples, a cop is form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers) aceAnapical wwwpaceraes.oam October 14, 2011 Mr. Mark Filardi AMEC-Charlotte 2801 Yorkmont Road Charlotte, NC 28208 Pace Analytic aI Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 RE: Project: CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 2225 Riverside dr. Asheville, NC 28804 (826)254.7175 Received by MPF 10/14/11 Pace Analytical Services, Inc. 9800 Kincey Ave. suite 1DO Huntersville, NC 26078 (704y875-WW Dear Mr. Filardi: Enclosed are the analytical results for samples} received by the laboratory on October fly, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, "Z-- Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 67 aceAnalytrcals nxw.parelabsmm Project: CMI WWTP Pace Project No. 92103792 Minnesota Certification lDs 1700 Elm Street 5E Suite 200, Minneapolis, A2L4 Certification #: 2926.G1 Alaska Certification M UST-078 Alaska Certification #MN00064 Arizona Certification #: AZ•0014 Arkansas Certification M 88-0680 California Certification M 01155CA EPA Region 8 Certification #. Pace Flo6da/NELAP Certification #: E87605 Georgia Certification #: 959 Idaho Certification #: MN00064 Illinois Certification #: 200011 Iowa Certification #: 368 Kansas Certification #: E-10167 Louisiana Certification #: 03086 Louisiana Certification #: LA080009 Maine Certification M 2007029 Maryland Certification #: 322 Michigan DEQ Certification #: 9909 Minnesota Certification M 027-053-137 Pace Analytical Services, tnc. 2D5 East Meadow Road - Suite A Eden, NC 27288 [336)823.8921 Pace Analytical Services, Inc. 2225 Riverside Dr - Asheville. NC 28804 (828]254-7176 CERTIFICATIONS MN 55414 Mississippi Certification #: Pace Montana Certification #: MT CERT0092 Nevada Certification #: MN 00064 Nebraska Certification #: Pace New Jersey Certification #: MN-002 New Mexico Certification #: Pace New York Certification M 11647 North Carolina Certification M 530 North Dakota Certification M R-036 North Dakota Certification #: R-036A Ohio VAP Certification M CL101 Oklahoma Certification #: D9921 Oklahoma Certification M 9507 Oregon Certification #. MN200001 Pennsylvania Certification M 68-00563 Puerto Rico Certification Tennessee Certification #; 02818 Texas Certffication #; T104704192 Washington Certification #: C754 Wisconsin Certification M 999407970 Charlotte Certification Ids 9800 Kincey Ave. Ste 100. H u ntersvi I le, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #; 99006003 Virginia prinking Water Certification M. 00213 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Connecticut Certification #: PH-0104 FloridalNELAP Certification #: E87627 Kentucky UST Certification M 84 Louisiana DHH Drinking Water # LA 1 D0031 West Virginia Certification M 357 VrgtnialVELAP Certification #: 460144 South Carolina Certification #: 99030001 Virginia Certification #: 00072 West Virginia Certification #: 356 VrginafVELAP Certification #: 460147 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace AnalyticaI Services, Inc. 9800 KinceyAve. Suite 100 Huntersvllle, NC 28078 [704]875-9092 Page 2 of 67 aceAnalyticala wNw.pacefabs.com Project: CMI WWTP Pace Project No.: 92103792 Lab ID Sample ID 92103792001 EBMW-14 92103792002 EBMW-15 92103792003 EBMW-17 92103792RD4 EBMW-18 pace Analytical Services, Inc. 205 Fast Meadow Road - SuiteA Eden, NC 27288 [336]523.8921 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kir"y Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Method Analysts Anatytes Reported Laboratory RSK 175 SK4 3 PASI-M SM 2340B JMW 1 PASI-A EPA SD10 JMW 2 PASI•A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PASI-A SM 2540C GW1 1 PASi-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S21D AES 1 PASI-A EPA 300.0 SAJ i PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 5310E SAJ 1 PASI-A RSK 175 SK4 3 PAS I-M SM 2340B JMW 1 PASI-A EPA 6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PASI-A SM 2540C GW1 1 PASi-A SM 3500-Fe D#4 LEP 1 PASI-A SM 450D-S2D AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 ❑MN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 53106 SAJ 1 PASI-A RSK 175 SK4 3 PASI-M SM 23408 JMW 1 PASI-A EPA 6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PASI-A SM 2540C GW1 1 PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S21D AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DMN 2 PAS I -A SM 4500-CI-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A RSK 175 SK4 3 PASI-M REPORT OF LABORATORY ANALYSIS Page 3 of 67 This report shall not he reproduced, except in full, without the written consent of Pace Ana lyllcal Services, Inr _ acemaly lcal W1rN.pdoC1a65. p7m Project: CMI WWTP Pace Project No.: 92103792 Lab ID Sample ID 92103792005 EBMW-21 92103792006 EBMW-30 92103792007 EBMW-31 Pace Analytical Services, tne. 205 East !Meadow Road - Suite A Eden, NC 27288 t336j623.8921 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville, NC 28804 [828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 KInceyAve . Suite 100 Hunlersville, NC 28078 (704)875-9092 Method Analysts Analytes Reported Laboratory SM 2340B JMW 1 PASI-A EPA6010 JMW, SNB 2 PAST -A EPA 8260 NICK 63 PASI-C SM 2320B AES 2 PASI-A 5M 2540C GW1 1 PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S2D AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SIA 5310E SAJ 1 PASI-A RSK 175 SK4 3 PASI-M SM 2340B JMW 1 PAS! -A EPA6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PASI-A SM 25400 GW1 i PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S2D AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A RSK 175 SK4 3 PASI-M SM 2340B JMW 1 PASI-A EPA 6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PASI-A SM 2540C GW1 1 PASI-A SM 3500-Fe 0#4 LEP 1 PASI-A SM 4500-S21] AES 1 PASI-A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A RSK 175 SK4 3 PASI-M SM 2340B JMW 1 PASI-A REPORT OF LABORATORY ANALYSIS Page 4 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc aceAnalytical www.Paaeiabs.mm Project: CMI WWTP Pane Project No.: 92103792 Lab ID Sample ID 92103792008 EBMW32 92103792009 FPMW5 92103792010 DUPLICATE 92103792011 RB-1 92103792012 TRIP BLANK 2 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside ❑r. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace AnaIytleaI Services. Inc. 9800 Xincey Ave. Suite 100 HuntersWW, NC 28078 (704)875-9P92 Method Analysts Ana}ytes Reported Laboratory EPA 6010 JMW 2 PASI-A EPA 8260 MCK 63 PASI-C SM 2320B AES 2 PAS [-A SM 25400 GW1 1 PAS [-A SM 3500-Fe D#4 LEP 1 PASk-A SM 4500-S2D AES 1 PA51-A EPA 300.0 SAJ 1 PAS I -A EPA 353.2 DMN 2 PASI-A SM 4500-Ci-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A RSK 175 SK4 3 PASI-M SM 2340E JMW 1 PASI-A EPA6010 JMW 2 PASI-A EPA 8260 MCK 63 PA51-C SM 2326E AES 2 PASI-A SM 2540C GW 1 1 PASI-A SM 3500-Fe D#4 LEP 1 PASI-A SM 4500-S2D AES 1 PAS I -A EPA300.0 SAJ 1 PAS I -A EPA353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI-A SM 5310B SAJ 1 PASI-A RSK 175 SK4 3 PASI-M SM 2340B JMW 1 PASI-A EPA6010 JMW 2 PASI-A EPA 8260 MCK 63 PAS I-C SM 2320B AES 2 PASI-A SM 2540C GW1 1 PASI-A SM 3500-Fe D#4 LEP 1 PAST -A SM 4560-S2D AES 1 PAS I -A EPA 300.0 SAJ 1 PASI-A EPA 353.2 DMN 2 PASI-A SM 4500-CI-E JDA 1 PASI•A SM 5310S SAJ 1 PASI-A EPA 8260 MCK 63 PASI-C EPA 8260 MCK 63 PASI-C EPA 6260 MCK 63 PASI-C REPORT OF LABORATORY ANALYSIS Page 5 of 67 This report shall not he reproduced, except to Full, without the written consent of Pace Analytical Services, Inc aceAnalytrcale' -- www.paceWbs,com Project- CMI WWTP Pace Project No.: 92103792 Lab IQ Sample I❑ 92103792013 TRIP BLANK 3 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 21288 (336)623-8921 Pace Analytical Services, tnc. 2225 Riverside or. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Method EPA 8260 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fun, without tha written consent of Pace Analytical Services, Inc.. Analysts MCK Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersviile, NC 28078 (704)875.9092 Analytes Reported Laboratory 63 PA$I-C Page 6 of 67 aceAnalyiicala www.paceiabs-cw Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside 0r. Asheville, NC 28804 (82$)2$4-717$ ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KlnceyAve. Suite 100 Hunter5ville, NC 2807E (704)875-9092 Project: CMI WWTP Pace Project No.: 92103792 Sample: EBMW-14 Lab tD: 92103792001 Collected: 10/04/11 09:55 Received: 10105/11 16.35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual R5K 175 AtR Headspace Analytical Method: RSK 175 Ethane NO uglL 10.0 1 10/10/11 16:10 74-84-0 Ethene NO uglL 10.13 1 10/10/11 16:10 74-85-1 Methane 201 uglL 10.0 1 10/10/11 16:10 74-82-8 2340E Hardness, Total (Calc.)l Analytical Method. SM 2340B Total Hardness 48.9 mg1L 0,65 1 1010&11 02:D4 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 10000 uglL 100 1 10/06/11 10:15 1010&11 02 04 7440-70-2 Manganese 7550 uglL 5.0 1 10/06/11 10:15 10/08/11 02:04 7439-96-5 8260 MSV Low Level Analytical Method- EPA 8260 Acetone ND uglL 2500 100 10110/11 20 42 67-64-1 Benzene N❑ uglL 100 100 10110/11 20:42 71-43-2 Bromobenzene N❑ uglL 100 100 10/10/11 20:42 108-86-1 Bromochivromelhane N❑ uglL 100 100 10/10/11 20:42 74-97-5 Bromodichloromethane ND ug)L 100 100 10/10/11 20:42 75-27-4 Bromoform ND uglL 100 100 10110111 20.42 75-25-2 Bromomethane ND uglL 200 100 10/10/11 20:42 74-83-9 2-Bulanone (MEK) ND uglL 500 100 10/10/11 20:42 78-93-3 Carbon tetrachloride NO uglL 1DO 100 10MOIll 20A2 56-23-5 Chlorobenzene ND uglL 100 100 10/10/11 20A2 108-90-7 Chioroethane 291 ug)L 100 100 10/10/11 20A2 75-00-3 Chloroform NO uglL 100 100 1011OM1 20A2 67-66-3 Chloromethane ND uglL 100 100 10/10/11 20:42 74-67-3 2-Chlorotoluene ND ug1L 100 100 10/10/11 20:42 95-49-8 4-Chlorotoluene ND uglL. 100 100 10/10/11 20:42 106-43-4 1,2-Dibromo-3-chloropropane N❑ uglL 500 100 10/10/11 2DA2 96-12-8 Dibromochloromethane ND uglL 100 100 10/10/11 20.42 124-48-1 1,2-Dibromoethane (EDB) NO uglL 100 1DO 10/10/11 20:42 106-93-4 Dibromomethane ND uglL 100 100 10110/11 20,,42 74-95-3 1,2-Dichlorobenzene ND uglL 100 100 10/10/11 20A2 95-50-1 1,3-Dichlorabenzene ND uglL 100 100 10P0111 20A2 541.73-1 1,4-Dichlorabenzene NO uglL 100 100 10/10/11 20:42 106-46.7 DichiorodiFluoramethane NO ug1L 100 100 10/10/11 20:42 75-71-8 1,1-Dichlarcethane 19300 ug1L 100 100 10/10/11 20:42 75-34-3 1,2-01chloroethane NO ug1L 100 100 10/10/11 20:42 107.06-2 1,1-Dichloroelhene 3120 ug1L 100 100 10/10/11 20:42 75-35-4 cis-1,2-Dichlaroethana ND ug1L 100 100 10/10/11 2042 156.59-2 trans-1,2-Dichloroethene ND ug1L 1O0 100 10110/11 2DA2 156-60-5 1,2-Dichloropropane ND ug1L 100 100 10/10/11 20:42 78-87-5 1,3-Dichloropropane ND ug1L 100 ion 10/10/11 20:42 142-28-9 2,2-01chloropropane NO uglL 1DO 100 10/10/11 20:42 594-20-7 1,1-Dichloropropene NO uglL 100 100 10/10/11 20:42 563-58.6 cis-1,3-Dichloropropene N❑ uglL 100 100 10/10/11 20.42 1OD61-01-5 trans-1,3-Dichloropropene ND uglL 100 100 10/10/11 20A2 1OD61-02-6 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 7 of 67 This report shall nal be reproduced, except In Full, without She written consent of Pace Analytical Services, Inc.. /�;a'cie Analyfical w WWWpace738s.wm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27268 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ProjmL CM WWTP Pace Project No. 92103792 Sample: EBMW-14 Lab ID: 92103792001 Collected: 10/04/11 09:55 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 8260 MSV Law Level Analytical Method: EPA 8260 Diisopropyl ether N❑ ug/L 100 100 Ethylbenzene ND ug1L 100 100 Hexachloro-1,3-butadiene ND ug/L 100 100 2-Hexanone ND ug/L 500 100 p-Isopropyltoluene ND ug1L 100 100 Methylene Chloride ND ugIL 200 100 4- Meth yl-2-pentanone (MIRK) ND uglL 5o0 100 Methyl-tert-butyl ether ND ug)L 100 100 Naphthalene N❑ ug& 100 100 Styrene ND ugIL 1D0 100 1,1,1,2-Tetrachloroethane ND ugIL 100 100 1,1,2,2-Tetrachloroethane ND ug/L 100 1D0 TetrachIcroethene 166 ug/L 100 1D0 Toluene ND ug/L 100 100 1,2,3-Trichlorobenzene ND ug/L 100 100 1,2,4-Trichiorobenzene N❑ ug/L 100 100 1,1,1-Tdchloroethane 88100 ug/L 1000 10DO 1,1,2-Tdchloroethane ND ug1L 100 100 Trichloroethene ND ug/L 100 100 Tdchlorofluoromethane ND ug/L 100 100 1,2,3-Tdchloropropane N❑ ug1L 100 100 Vinyl acetate ND uglL 200 100 Vinyl chloride ND ug)L 100 100 m&p-Xylene ND ugIL 200 100 o-Xylene ND ug/L 100 100 4-Bromafluorobenzene (S) 92 °% 70.130 100 Dibromofluoromethane (S) 130 °% 70.130 100 1,2-Dichloroethane-d4 (S) 129 °% 70-130 1D0 Toluene-d8 (S) 102 °% 70.130 100 2320E Alkalinity Analytical Method: SM 2320B At ka linity, B ica rbon ate {CaCO3) 223 mglL 5.0 1 Alkalinity, Total as CaCO3 223 mg1L 5.0 1 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 482 mglL 25.0 1 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron. Ferrous 63.0 mg1L 5.0 10 4500S21) Sulfide Water Analytical Method: SM 4500-S2D Sulfide ND mg1L 0.25 2.5 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg1L 5.0 1 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, wilhoul the written consent of Pace Analytical Services, Inc.. 10/10/11 20 A2 108-2D-3 10/10/11 20:42 100.41-4 1 D110111 20A2 87-68-3 10/10/1120A2 591-78-6 10/1011120:42 99-87-6 10110/11 20:42 75-09-2 10 / 10111 2 0: 42 108-10-1 10110 / 11 2 0: 4 2 16 34-04 -4 10/10/1120:42 91-20-3 10110/11 2 0: 42 100-42-5 1011011120:42 630-20-6 10/1011120-42 79-34-5 10/10/11 20:42 127-18-4 1011011120:42 108-88-3 10110/11 20:42 87.61.6 10/10/11 20; 42 120-82.1 10/12/1102:35 71-55-6 1011011120:42 79-00-5 10/1011120;42 7MI-6 10/10/1120:42 75-69-4 1011011120:42 96-18-4 10/ 10/ 11 20: 42 108-05- 4 1011011120:42 75-01-4 10110/11 20 A2 179601-23-1 10/10/112042 95.47-6 10110/1120A2 460-00-4 10 / 10111 2 0: 4 2 1868-53.7 10110 / 11 2 0: 4 2 1706 0-07-0 10110/1120,42 2037-26-5 10/11/11 10:30 10/11/11 10:30 10/07/11 16:33 100011118:13 H1,N2 1010W1112:00 18496-25-8 D3 10107 / 11 16:16 14 806-7 9-8 Page 8 of 67 aceAnalytical Kxw.a4CefBGS.[am Pace Analytical Services, Inc. 205 East Meadow Road - Suite Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 r828]254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800KinceyAve. SuitefUO Huntersville, NC 28078 (704 $75.9092 Projecl: CMI WWTP Pace Project No.: 92103792 Sample: EBMW-14 Lab ID: 92103792001 Collected: i0104111 09;55 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual. 353.2 Nitrogen. N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mglL 0.20 1 101051il 22:27 Nitrogen, Nitrite 0.33 mg1L 0.10 1 10/05/11 22:27 4500 Chloride Analytical Method- SM 4500-CI-E Chloride 38.4 mg1L &0 1 10/08/11 13:52 16887-00.6 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 63,8 mg1L 5.0 5 10/11/11 09:53 7440-44-0 Sample: EBMW-15 Lab ID: 92103792002 Collected- 10104111 14:30 Received; 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO ug1L 10.0 1 10/10/11 16:21 74-84-0 Ethene NO ug1L 10.0 1 10/10/11 16 21 74-85-1 Methane 473 uglL 10.0 1 10/10/11 16:21 74.82-8 2340E Hardness, Total {Calc.) Analytical Method: SM 2340B Total Hardness 161 mg1L 0.65 1 10/08/11 02 07 6010 MET ICP Analytical Method. EPA 6010 Preparation Method: I- PA 3010 Calcium 38400 uglL 100 1 10/06/11 10.15 10/08111 02:07 7440-70-2 Manganese 3820 uglL 5.0 1 10/06/11 10:15 10/08/11 02:07 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO uglL 25.0 1 10/12/11 08:07 67-64-1 Benzene NO ug1L 1.0 1 10/12/11 08:07 71-43-2 Bromobenzene NO uglL 1.0 1 10/12111 08.07 108-86-1 Bromochloromethane NO ug1L 1.0 1 10/12/11 08:07 74-97-5 Bromodichloromethane NO ug)L 1.0 1 10/12/11 0&07 75-27-4 Bromoform NO uglL 1.0 1 10/12/11 08:07 75-25-2 Bromomethane NO uglL 2.0 1 10/12/11 08:07 74-83-9 2-Butanone (MEK) NO uglL 5.0 1 10/12/11 08:07 78-93.3 Carbon tetrachloride NO uglL 1.0 1 10/12/11 08:07 56-23-5 Chlombenzene 11.9 uglL 1.0 1 10/12/11 08:07 108-90-7 Chloroelhane NO uglL 1.0 1 10112111 08:07 75-00-3 Chloroform NO uglL 1.0 1 10112/11 08 07 67-66-3 Chloromethane NO uglL 1.0 1 10/12/11 08:07 74-87-3 2-Chlorotoluene ND ug1L 1.0 1 10112/11 08:07 9549-8 4-Chlorotoluene NO uglL 1.0 1 10/12/11 08:07 106-43-4 1,2-❑ibromo-3-chioropropane NO uglL 5.0 1 10112/11 08:07 96-12-8 Dibromochloromethane NO uglL 1.0 1 10112A1 08:07 124-48-1 1,2-Oibromoethane (ED8) NO uglL 1.0 1 101121il 08:07 106-93.4 Dihromomethane NO uglL 1.0 1 10112111 08:07 74-95-3 Date: 10/14/2011 09 06 AM REPORT OF LABORATORY ANALYSIS Page 9 of 67 This report shall not be reproduced, except in full, without the written consent of PaceAnalytkal Services, 1nc„ 1�;a'ceAnalj4ical- wwwPWelabsMm Project: CM WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. Pace Analytical Services, toc. 205 East Meadow Road - SuiteA 2225 Riverside Dn Eden, NC 27288 Asheville, NC 28804 (336)623.8921 (828)254-7176 ANALYTICAL RESULTS Paco Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2807E Sample: EBM1N-15 Lab ID: 92103792002 Collected: 10/04/11 14.30 Received: 10/05111 16:35 Matrix: Water Parameters Results units Report Limit DF Prepared Anatyzed CAS No 8260 MSV Low Level Analytical Method: EPA S260 (704)875-9092 1,2-Dichlorobenzene NO uglL 1.0 1 10/12/11 08:07 95-5(-1 1,3-Dichlorobenzene NO uglL 1.0 1 10112/11 08:07 541-73-1 1,4-Dichlarobenzene 2.9 uglL 1.0 1 10/12/11 08:D7 106-46-7 Dichlorodifiuoromethane NO ugJL 1.0 1 10/12/11 08:07 75-71-8 1.1-Dichioroethane 4.4 uglL 1.0 1 10112/11 08:07 75-34-3 1.2-Dichloroethane ND ug1L 1.0 1 10/12111 08:07 107-06-2 1,1-Dichloroethene 9.1 uglL 1.0 1 10/12/1108-07 75-35-4 Cis-1,2-Dichioroethene NO uglL 1,D 1 10112111 08:07 156-59-2 trans- 1, 2- Dich loroeth ene NO ug1L 1.0 1 10/12/11 08:07 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 10/12111 08:07 78-87-5 1,3-Dichloropropane IN ug1L 1.0 1 10/12111 08:07 142-28-9 2,2-Dichloropropane N❑ ug1L 1.0 1 10/12/11 08:07 594-20-7 i,1-Dichloropropane N❑ ug1L 1.0 1 10/12/11 08:07 563-58-6 cis- 1,3-Dichloropropene NO ug1L 1.0 1 10/12/11 08:07 10061-01-5 Iran s-1,3-Dichloropropene N❑ ug1L 1.0 I 10/12/11 08:07 10061-D2-6 Dilsopropyl ether N❑ ug1L 1.0 1 10/12/11 0&07 108-20-3 Ethylbenzene NO ug1L 1.0 1 10/12/11 08:07 100-41-4 Hexachloro-1,3-butadiene NO ug1L 1.0 1 10/12/11 08:07 87-68-3 2-Hexanone NO ug1L 5.0 1 10/12/11 08:07 591-78-6 p-isopropyltoluene NO ug1L 1.D 1 10/12/11 08:07 99-87-6 Methylene Chloride NO ug1L 2.0 1 10/12/11 08.07 75-09-2 4-Methyl -2-pentanone (MIBK) N❑ ug/L 5.0 1 10/12/11 08:07 108-10-1 Methyl -tert-butyl ether NO uglL 1.0 1 10/12/11 08:07 1634-04-4 Naphthalene ND ug1L 1.0 1 10/12/11 08:07 91-20-3 Styrene NO ug1L 1.0 1 10/12/11 08:07 1130-42-5 1,1,1,2-Tetrachloroethane NO ug1L 1.0 1 10/12/11 08:07 630-20-6 1,1.2,2-Tetrachloroethane ND ug/L 1.0 1 10/12/11 08:07 79-34-5 Tetrachloroethene NO ug1L 1.0 1 10)12111 08:07 127-18-4 Toluene NO ug1L 1.0 1 10/12/11 08:07 108.88-3 1,2,3-Trichlorobenzene NO ug1L 1.0 1 10/12/11 08:07 87-61-6 1,2,4-Trichiarobenzene NO ug1L 1.0 1 10/12/11 08:07 120-82-1 1.1,1-Trichloroethane 7.8 ug1L 1.0 1 10/12/11 0807 71-55-6 1.1,2-Trichloroethane NO ug1L 1.0 1 1011211i 08:07 79-00-5 Trichloroethene NO ug1L 1.0 1 10/12/11 08:07 79-01-6 Trichlarofluoromethane NO ug1L 1.0 1 10/12/11 08.07 75-69-4 1.2,3-Trichloropropane N❑ ug1L 1.0 1 10/12/11 08:07 96-18.4 Vinyl acetate NO ug1L 2.0 1 10/12/11 0&07 103-05-4 Vinyl chloride ND ug1L 1.0 1 10/12/11 08:07 75-01-4 m&p-Xylene NO ug1L 2.0 1 10/12/11 0&07 179601-23-1 o-Xylene NO ug1L 1.0 1 10/12/11 0&07 95-47-6 4-Bromofluorobenzene (S) 93 % 70-130 1 10/12/11 08:07 460-OD-4 Dibramo6uoromethane (S) 129 % 70-130 1 10/12/11 08 07 1868-53-7 1,2-Dichloroethane-d4 (S) 129 % 70-130 1 10/12/11 08:07 17060-07-0 Toluene-d8 (S) 105 % 70-130 1 10/12/11 0&07 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity,Bicarbonate (CaCO3) 290 mg1L 5.0 1 10M1111 10:30 Qual Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 10of 67 This report shall not be reproduced, except in Full, without the written can sent or face Analytical Services, Inc.. ace Analydlcal a. " w.pacv+ahs.mm Project: CMI WWTP Pace Project No.: 92103792 Pace Anaiyllcal Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)023.8921 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville. NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: EBMW-15 Lab IA: 92103792002 Collected: 10/04/11 14:30 Received: 10/05/11 16:35 Maldx: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual 2320E Alkalinity Analytical Method SM 2320B Alkalinity, Total as CaCO3 290 mg1L 5.0 1 10/11111 10:30 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 350 mg1L 25.0 1 10/07/11 16:34 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron, Ferrous ND mg1L 0.50 1 10/10/11 17:10 1-11.N2 450OS20 Sulfide Water Analytical Method: SM 4500-S21) Sulfide ND mg1L 0.10 1 10/08/11 12:00 18496-25-8 300.01C Anions 28 Days Analytical Method. EPA 300.0 Sulfate 6A mglL 5.0 1 10/07/11 16:56 14808-79.8 353.2 Nitrogen, N021NO3 unpres Analytical Method EPA 353.2 Nitrogen, Nitrate ND mg1L 0.20 1 10/05/11 22:36 Nitrogen, Nitrite ND mg1L 0.10 1 10/05/11 22:36 4500 Chloride Analytical Melhod: SM 4500-CI-E Chloride 50.9 mg)L 25.0 5 10/08/11 14:36 16887-00-6 5310E TOC Analytical Mel hod: SM 5310B Total Organic Carbon 15.6 mglL 1.0 1 10/10/11 15.31 7440-44-0 Sample: EBMW-17 Lab ID: 92103792003 Collected: 10/04/11 16:30 Received: 10/05/11 18735 Matrix: Water Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No. Dual RSK 175 AIR Headspace Ethane Ethane Methane 2340E Hardness, Total (Calc.) Total Hardness 6010 MET ICP Calcium Manganese 8260 MSV Low Level Acetone Benzene Sromobenzene Date7 10114/2011 09 06 AM Analytical Method: RSK 175 ND ug/L 10.0 1 10/11/11 15:01 74-84-0 15.3 uglL 10.0 1 10/11/11 15:01 74-85-1 16.2 uglL 10.0 1 1001111 15701 74-82-8 Analytical Method: SM 2340B 52.2 mg1L 0.65 1 1010811102:10 Analytical Method- EPA 6010 Preparation Method- EPA 3010 18900 ugfL 100 1 10/06/11 10:15 10108/11 02:10 7440-70.2 63.7 uglL 5.0 1 10/06/11 10,15 10/08/11 0210 7439-96-5 Analytical Method: EPA 8260 ND uglL 25.0 1 10/11/11 04:47 67-64-1 NO uglL 1.0 1 10111 /11 04.47 71-43-2 ND uglL 1.0 1 10MI111 04A7 108-86-1 REPORT OF LABORATORY ANALYSIS Page 11 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. a0Analyfrcal www.pacelabscom Project: CMI WWTP Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28bD4 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 Pace Project No.: 92103792 Sample: EBMW-17 Lab ID: 92103792003 Collected: 10/04/11 16:30 Received: 10/05/11 16:35 Matdx: Water (704)875.9092 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. oval 8260 MSV Low Level Analytical Method,. EPA 8260 Bromochloromethane ND uglL 1.0 1 10/11/11 04:47 74-97-5 Bromodichloromethane ND uglL 1.0 1 10/11/11 04:47 75-27-4 Bromoform N❑ ug1L 1.0 1 10/11/11 04:47 75-25-2 Bromornethane ND uglL 2.0 1 10/11111 04:47 74-83-9 2-Butanone (MEK) ND ug1L &0 1 10/11/11 04:47 78-93-3 Carbon tetrachloride ND uglL 1.0 1 10/11/11 04:47 56-23-5 Chlorobenzene ND uglL 1.0 1 10/11/11 04:47 108-90-7 Chloroethane ND ug1L 1.0 1 10/11/11 04:47 75-OD-3 Chloroform ND uglL 1.0 1 10/11/11 04:47 67-66-3 Chloromethane ND uglL 1.0 1 10/11/11 D4:47 74-87-3 2-Chlorotoluene ND uglL 1.0 1 i0111111 04:47 95-49-8 4-Chlomtoluene ND uglL 1.0 1 10/11/11 04:47 106-43-4 1,2-Dibromo-3-Ghloropropane ND uglL 5.0 1 10/11/11 04:47 96-12-8 Dibromochloromethane ND uglL 1.0 1 10/11/11 D4:47 124-48-1 1,2-Dibromoethane (EDB) ND uglL 1.0 1 10P1111 04:47 106-93-4 Dibromvmethane ND uglL 1.0 1 10/11/11 04:47 74-95-3 1,2-Dichlorobenzene ND uglL 1.0 1 10111/11 04:47 95-50-1 1,3-Dichlorobenzene NO uglL 1.0 1 10/11/11 D4:47 541-73-1 1,4-Dichlorobenzene ND uglL 1.0 1 10/11/11 04:47 106-46-7 Dichlorodinuoromethane ND uglL 1.0 1 10111/11 04:47 75-71-8 1,1-Dichloroethane 2.7 uglL 1.0 1 10/11/11 04:47 75-34-3 1,2-Dichloroethane NO uglL 1.0 1 10/11/11 D4:47 107-06-2 1,1-Dichloroethene 1.0 uglL 1.0 1 1011101 04:47 75-35-4 cis- 1,2-Dichloroethene NO uglL 1.0 1 113/11/11 04:47 156-59-2 trans- 1. 2 -Dich loroet hene ND uglL 1.0 1 10/11/11 04:47 156-t30-5 1,2-Dichloropropane NO uglL 1Z 1 10/11/11 04:47 78-87-5 1,3-Dichloropropane N❑ ug1L 1.0 1 10/11/11 04:47 142-28-9 2.2 -Dichl oro propane ND uglL i.0 1 10/11/11 04:47 594-20-7 1,1-Dichloropropene N❑ uglL 1.0 1 10/11/11 04:47 563-58-6 cis-1,3-Dichloropropene ND ug1L i.D 1 10/11/11 04:47 10061-01-5 trans-1,3-Dichloropropene ND uglL 1.0 1 10/11/11 04:47 10061-02-6 Diisopropyl ether NO uglL 1.0 1 10/11/11 04:47 108-20-3 Ethyibenzene NO uglL I'D 1 10111/11 04:47 100-41-4 Hexachlora-1,3-butadiene ND ug1L 1.D 1 1D111111 04:47 87-68-3 2-Hexanone ND uglL 5.0 1 10/11/11 04:47 591-78-6 p-Isopropyltoluene ND uglL 1.0 1 10/11/11 04:47 99-87-6 Methylene Chloride NO ug1L 2.0 1 10/11/11 04:47 75-09-2 4- Meth yl-2-pentanone (MIBK) ND uglL 5.0 1 10/11/11 04:47 108-10-1 Methyl-tert-butyl ether ND uglL 1.0 1 i011111i 04:47 1634-04-4 Naphthalene 3.6 uglL 1.0 1 10JI1111 04:47 91-20.3 Styrene ND uglL 1.0 1 10/11/11 04,47 100-42-5 1,1,1,2-Tetrachloroethane ND ug1L 1.0 1 10111/11 D4:47 630-20-6 1.1.2,2-Tetrachloroethane ND uglL 1.0 1 10/11/11 04:47 79-34-5 Tetrachloroelhane ND uglL 1.0 1 10/11/11 04:47 127-18-4 Toluene ND ug1L 1.0 1 10/11/11 04:47 108-88-3 1,2.3-Trichlorobenzene NO uglL 1.0 1 10/11/11 04:47 87-61-6 1,2,4-Trichlorobenzene NO uglL 1.0 1 10111/11 04:47 120-82-1 Dale: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 12of67 This rapers shall not be reproduced, except in full, wilhoul the written consent of Pac a Analyiical Services, Inc., 1!;a1C6Ana1jdica1' www.pa&ahs.com Pace Analytical SerVIres, Inc. 205 East Meadow Road - Suile A Eden, NC 2728a (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 980o KinceyAve . Suite 100 Huntersville, INC 28078 (704)875.9092 Project CMI WWFP Pace Project No.: 92103792 Sample: EBMW-17 Lab ID: 92103792003 Collected: 10/04/11 1630 Received: 10/05111 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 I,ASV Low Level Analytical Method: EPA 8260 1,1,1-Trichloroethane ND ug1L 1.0 1 10/11/11 04A7 71-55-6 1,1,2-Trichloroethane ND ugIL 1.0 1 10/11/11 04:47 79.MS Trichloroethene ND ug/L 1.0 1 10/11/11 04:47 79-01-6 Trichlorofluoromethane ND ug1L 1,0 1 10/11/11 04:47 75-69-4 1,243-Trichloropropane ND ug/L 1.0 1 10/11/11 04:47 96-18-4 Vinyl acetate ND ug1L 2.0 1 10/11/11 04:47 108-05-4 Vinyl chloride ND ug1L 1.0 1 10111)11 04:47 75-01-4 m&p-Xylene ND ug1L 2.0 1 10/11/11 04:47 179601-23-1 o-Xylene ND ug1L 1.0 1 10/11/11 04:47 95-47-6 4-Bromofluorobenzene (S) 95 % 70-130 1 10/11/11 04:47 460-00-4 Dibromofluoromethane (S) 118 % 70-130 1 10/11/11 04:47 1868-53-7 1,2-Dichloroethane-d4 (S) 120 % 70-130 1 i0111111 04:47 17060-07-0 Toluene -dB (S) 101 % 70-130 1 10/11/11 04A7 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity,Bicarbonate (CaCO3) 82.3 mg1L 5.0 1 10/11/11 10:30 Alkalinity, Total as CaCC3 143 mg/L 5.0 1 10/11/11 10:30 2540C Total Dissolved Solids Analytical Method. SM 2540C Total Dissolved Solids 213 mg/L 25.0 1 10/07/11 16:34 Iron, Ferrous Analytical Method. SM 3500-Fe D#4 Iron, Ferrous ND mg/L 0.50 1 10/10/11 17:10 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide 0.10 mg1L 0.10 1 10/08/11 12:00 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate 12.6 mg1L 5.0 1 10107111 17:10 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 1.7 mg/L 0.20 1 10/05/11 22:37 Nitrogen, Nitrile NO mg)L 0.10 1 10/05/11 22:37 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg1L 5.0 1 10/08/11 13:53 16887-00-6 5310B TOC Anatytir I Method: SM 531013 Total Organic Carbon 20.4 mg/L 1.0 1 10/10111 15:52 7440-44-0 Date: 1011412DII 09:06AM REPORT OF LABORATORY ANALYSIS Page 13 of 67 This report sha[I not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAna lyfrcaI a WWW pacel ft cam Project: CMI WWTP Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 Oast Meadow Road - Suite A 2225 Riverside Dr - Eden, NC27288 Ashevliie, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Sulte 100 Huntersvflle, NC 28078 Pace Project No.: 92103792 Sample: EBMW-18 Lab 10: 92103792004 Collected; 10/04/11 08:35 Received: 10/05/11 16:35 Matrix: Water (704)875-9092 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane 800 ug1L 110 1 10/11/11 15:12 74-84-0 Ethene 222 uglL 10.0 1 10/11/11 15;12 74-85-1 Methane 25.9 uglL 10.0 1 10/11/11 15:12 74-82.8 2340E Hardness, Total (Calc.) Analytical Method: SM 2340B Total Hardness 604 mglL 6.5 10 10110N 1 17:26 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 200000 uglL 1000 10 10/06/11 10:15 10/10/11 17:26 7440-70-2 Manganese 134 ug1L 5.0 1 10/06/11 1015 10/08/11 0214 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug1L 12500 500 10112111 15:29 67.64-1 Benzene ND ug1L 500 500 10/12/11 15:29 71-43.2 Bromobenzene ND uglL 500 500 10/12111 15:29 108-86-1 Bromochloromethane ND ug1L 500 500 10112/11 15:29 74-97-5 Bromadichioromethane ND ug1L 500 500 10/12/11 15:29 75-27-4 Bromoform ND ug1L 500 500 10112/11 15:29 75-25-2 Bromomethane ND uglL 1000 500 10112/11 15:29 74-83-9 2-Butanone (MEK) ND uglL 2500 500 10112/11 15:29 78-93-3 Carbon tetrachloride NO ug1L 500 500 10112/11 15:29 56.23-5 Chlorobenzene NO ug1L 500 500 10/12/11 15:29 108-90-7 Chloroethane 1200 uglL 500 500 10112/11 15:29 75-00-3 Chloroform NO ug1L 500 500 1011211 15.29 87-66-3 Chloromethane NO uglL 500 500 10/12/11 15.29 74-87-3 2-Chlorotoiuene NO ug1L 500 500 10/12111 15:29 95-49.8 4-Chlorotoluene NO uglL 500 500 10/12/11 15:29 106-43-4 1,2-Dibromo-3-chloropropane NO uglL 2500 500 10/12/11 15:29 96-12-8 Dibromochloromethane ND uglL 500 500 10/12/11 15:29 124-48.1 1,2-Dibromoethane (EDB) NO ug1L 500 500 10/12/11 15:29 1DS-93-4 Dibromomethane ND ug1L 500 500 10/12/11 15:29 74-95-3 1,2-Dichlorobenzene NO uglL 500 500 10/12/11 15:29 95-50-1 15-131chlorobenzene IN ug1L 500 500 10/12/11 15:29 541-73-1 1,4-Dichlorobenzene ND uglL 500 500 10/12/11 15:29 106-46-7 Dichlorodifluoromethane NO ug1L 500 500 10/12/11 15:29 75-71-8 1,1-Dichloroethane 54100 ug1L 500 500 10/12/11 15:29 75-34-3 12-Dichloroethane ND ug1L 500 500 10/12/11 15:29 107-06-2 11-Dichloroethene 3500 uglL 500 500 10/12/11 15:29 75-35-4 cis-1,2-Dichloroetnene NO uglL 500 500 10/12/11 15:29 156-59-2 trans-1,2-Dichloroethene ND ug1L 500 500 10/12/11 15:29 15MO-5 1,2-Dichloropropane NO uglL 500 500 10/12/11 15.29 78-87-5 1,3-Dichloropropane ND uglL 500 500 10/12/11 15:29 142-28-9 2,2•Dichloropropane NO ug1L 500 500 10/12/11 15:29 594-20-7 1,1-Dichloropropene NO uglL 500 500 10/12/11 15:29 563-58-6 cis-1,3-Dichloropropene ND ug1L 500 500 10/12/11 15:29 10061.01-5 bans-1,3-Dchloropropen e ND ug1L 500 500 10/12/11 15:29 10061-02-6 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 14 of 67 This report shall not be reproduced, except in full, without the written consentaf Pa ce Analytical Services. Inc.. 1!;a'cleAnalyfical Www.pacerahs.rOm Pace Analytical Services, Inc. 205 East Meadow Road - Suite Eden, NC 27288 t33(1}623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9600 Kincey Ave. Suite 100 Huntersville. NC 28078 ;704)875-9492 Project CMI WWTP Pace Project No.: 92103792 Sample: EBMW-18 Lab ID: 92103792004 Collected: i0104111 08.35 Received: 10/05/11 16:35 Matrix' Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No 4ual 8260 MSV Low Level Analytical Method: EPA 8260 Diisopmpyl ether NO uglL 500 500 10/12111 15:29 1 D8-20-3 Ethylbenzene NO uglL Soo 50o 10/12/11 15:29 100-41-4 Hexachloro-1,3-butadiene NO uglL 500 500 10/12/11 15:29 87-68-3 2-Hexanone NO uglL 2500 500 10/12/11 15:29 591-78-6 p-lsopropyltoluene ND uglL 500 500 101121il 15:29 99-87-6 Methylene Chloride ND ug1L 1000 50D 101121il 15,29 75-09-2 4-Methyl -2- penta none (MIBK) NO uglL 2500 500 10/12/11 15,29 108-10-1 Methyl-tert-butyl ether NO uglL 500 500 10/12/11 15:29 1634-04-4 Naphthalene ND ug1L 500 5D0 10/12/11 15:29 91-20-3 Styrene ND uglL 500 500 10112J11 15-29 100-42-5 1,1,1,2-Tetrachloroethane NO ug1L 500 500 10112J11 15:29 630-20-6 1,1,2,2-Tetrachloroethane ND uglL 500 500 10/12111 15:29 79-34-5 Tetrachloroethene ND uglL 500 500 10/12/11 15:29 127-18-4 Toluene NO ug1L 500 500 10/12/11 15:29 108-88-3 1,2,3-Trichlorobenzene ND uglL 500 500 10112111 15,29 87-61-6 1,2,4-Tmhlorobenzene ND ug1L 500 500 10112/11 15:29 12D-82-1 1,1,1-Trichloroethane 42400 ug1L 500 500 10/12/11 15:29 71-55-6 1,1,2-Trichloroethane ND uglL 5D0 500 10/12/11 15,29 79-00-5 Trichloroethene N❑ uglL Soo 500 10/12111 15.29 79-01-6 Trichlorofluoromethane N❑ ug1L 500 500 10/12/11 15.29 75-69-4 1,2,3-Trichloropropane ND uglL 500 500 10/12/11 15:29 96-18-4 Vinyl acetate NO uglL 1000 500 10/12/11 15:29 108-05-4 Vinyl chloride NO uglL 500 500 10/12/11 15:29 75-01-4 m&p-Xyiene NO ug1L. 1000 500 10112J11 15:29 179601-23-1 ❑-Xylene NO uglL 500 500 10/12/11 15-29 95-47-0 4-Bromofluorobenaene (S) 92 % 70-130 500 10/12/11 15:29 460-00-4 Dibromofluoromethane (S) 126 % 70-130 500 10/12/11 15:29 1868-53-7 1,2-Dichloroethane-d4 (S) 126 °% 70-130 500 10112/11 15:29 17060-07-0 Toluene-d8 (S) 102 % 70-130 500 10/12/11 1529 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Bicarbonate (CaCO3) 217 mglL 5.0 1 10/11111 10:30 Alkalinity, Total as CaCO3 217 mg1L 5.0 1 10/11/11 10:30 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 1030 mg1L 25.0 1 1010701 16,34 Iron, Ferrous Analytical Method. SM 3500-Fe D#4 Iron, Ferrous NO mg1L 0.50 1 10/10/11 16.58 4500S2D Sulfide Water Analytical Method: SM 4500-S2❑ Sulfide NO mglL 0.10 1 10/08/11 12A0 18496--25-8 300.0 IC Anions 28 Days Analytical Method. EPA 300.0 Sulfate ND mg1L 5.0 1 10/07/11 17:23 14808-79-8 HS,N2 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 15 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. aceAnalytrcal WWw.pacefabs.rarrr Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27280 (336)623-8921 Pare Analytical Services, Inc. 7225 Riverside Or Asheville, NC 28804 (828)254.7176 ANALYTICAL RESULTS Pace Analytical 5ervices, Inc, 9800 KIncey Ave. Suile l00 Huntersville, NC 28078 (704)875-9092 Project: CMi WWTP Pace Project No.: 92103792 Sample: EBMW-18 Lab IQ: 92103792004 Collected 10/04/11 08:35 Received: 10/05111 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Oual 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mglL 0.20 1 10/05/11 22:21 Nitrogen, Nitrite ND mglL 0.10 1 10/05/11 22:21 4500 Chloride Analyticai Method: SM 4500-CI-E Chloride 348 mg1L 50.0 10 10/08/11 14:38 16887-00-6 5310E TOC Analytical Method: SM 531013 Total Organic Carbon 43.6 mg/L 2.0 2 10111/11 10:21 744D-44-0 Sample: EBMW-21 Lab ID: 92103792005 Caliected: i01D4111 12:30 Received: 10/05/11 16,35 Matrix: Water Parameters RSK 175 AIR Headspace Ethane Ethene Methane 2340E Hardness, Total (Galt.) Total Hardness 6010 MET ICP Calcium Manganese 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethan e Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chiorololuene 4-Chlorotoluene 1,2-Dlbromo-3-chloropropane Di brom oc hl o ro methan e 1,2-Dibromoethane (EDB) Dibromomethane Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ Analytical Method: RSK 175 NO uglL 10.0 1 10/10/11 10:36 74-84-0 NO uglL 10.0 1 10110/11 10:36 74-85-1 21.0 uglL 10.0 1 10/10/11 10:36 74-82-8 Analytical Method: SM 2340B 112 mg/L 0.65 1 10/08/11 02:17 Analytical Method: EPA 6010 Preparatlan Method: EPA 3010 36800 uglL 100 1 10/06/11 10:15 10/08/11 02:17 7440-70-2 31.8 uglL 5.0 1 10/06/11 10:15 1010&11 02:17 7439-96-5 Analytical Method: EPA 8260 NO uglL 50.0 2 10/12111 13:21 67-64-1 NO ug1L 2.0 2 10/12/11 13:21 71-43-2 NO uglL 2,0 2 10/12/11 1121 108-86-1 N❑ ug1L 2.0 2 10/12/11 13:21 74-97-5 NO uglL 2.0 2 10/12/11 13:21 76-27-4 NO ug/L 2.0 2 10/12/11 13.21 75-25-2 NO uglL 4,0 2 10/12/11 13:21 74.83-9 NO uglL 10.0 2 10112/11 13:21 78-93-3 NO ug)L 2.0 2 10/12/11 13:21 56-23-5 NO uglL 2.0 2 10/12/11 13:21 108-90-7 NO uglL 2.0 2 10/12/11 13:21 75-00.3 ND ug)L 2.0 2 1011 M 113.21 67-66-3 ND uglL 2.0 2 10112i11 13:21 74-87-3 No ug)L 2.0 2 10/12/11 13-21 95.49.8 NO ug)L 2.0 2 10/12/11 13:21 106-43-4 NO ug1L 10.0 2 10/12/11 13�21 96-12-8 NO ug)L 2.0 2 101121il 13:21 124-48-1 NO uglL 2.0 2 10/12/11 13-21 106-93A NO uglL 2.0 2 10112/11 1121 74-95-3 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 16 of 67 This report shall not be reproduced, except In full, without the written Consent of Pa ce Ana lytical Services, Inc.. e aceAnalytical w+sw.pace�3ds.:om Project: CMI VVWTP Pace Analyticar Services, Inc, Pace Analytical Services, Inc. 205 East trleadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)523-8921 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave Suite 100 Huntersviile, NC 28079 Pace Project No,i 92103792 Sample: EBMW-21 Lab ID: 92103792005 Collected: 101041il 12:30 Received: 10/05/11 16:35 Matrix. Water (704)875-9092 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Grua! 8260 MSV Low Level AnalylicaI Method- EPA 8260 1,2-Dichtarobenzene ND uglL 2.0 2 10/12/11 1311 95-50-1 1,3-Dichlorobenzene ND uglL 2.0 2 10/12/11 13:21 541-73-1 1,4-Dichiarobenzene ND ug)L 2.0 2 10/12/11 13.21 1D6-46-7 Dichlorodifluoromethane ND ug1L 2Z 2 10/1 2/1 1 13:21 75-71-8 1,1-Dichloroethane 234 uglL 2.0 2 10/12/11 13:21 75-34-3 1,2-Dichloroethane ND uglL 2.0 2 10/12/11 13:21 107-06-2 1,1-Dichloroethene 45.5 uglL 2.0 2 10/12/11 13:21 75-35-4 cis•1,2-Dichloroethene NO uglL 2.0 2 1OM2111 13:21 156-59-2 trans-1,2-Dichloroethene ND uglL 2,0 2 10/12/11 113:21 156-60-5 1,2-Dichloropropane NO uglL 2.0 2 10/12/11 13:21 78-87-5 1,3-Dichloropropane NO uglL 2.0 2 1(/12/11 13:21 142-28-9 2,2-Dichloropropane ND uglL 2.0 2 10JI2111 13:21 594-20-7 1,1-Dichloropropane ND ug1L 2.0 2 1002111 13:21 563-58-6 cis-1,3-Dichloropropane NO uglL 2.0 2 10/12/11 13:21 10061-01.5 trans-1,3-Dichlaropropene ND ug1L 2.0 2 10/12/11 13:21 10061-02.6 Dilsopropyl ether NO uglL 2.0 2 10/12/11 13:21 108-20-3 Ethylbenzene NO ug1L 2.0 2 10/12111 13.21 100-41-4 Hexachloro-1,3-butadiene ND ug1L 2,0 2 10112JI1 13:21 87-08-3 2-Hexanone NO uglL 10.0 2 10/12/11 13:21 591-78.6 p4sopropylloluene NO uglL 2.0 2 10/12111 13:21 99-87-6 Methylene Chloride N❑ uglL 4.0 2 10/12/11 13:21 75-09-2 4 -M ethyl-2-penta none (MIRK) NO ug1L 10.0 2 10112111 1121 108-10.1 Methyl-tert-butyl ether NO uglL 2.0 2 10112J71 13721 1634-04-4 Naphthalene NO uglL 2.0 2 10112/11 13:21 91-20-3 Styrene NO ug1L 2.0 2 10/12/11 13:21 100-42-5 1,1.1,2-Telrachloroethane N❑ ug1L 2.0 2 10112M1 13:21 630-20d6 1,1,2,2-Tetrachloroethane NO ug1L 2.0 2 10/12/11 13:21 79-34-5 Tetrachlorcethene ND ug1L 2.0 2 i0112111 1121 127-18-4 Toluene NO ug1L 2.0 2 10/12/11 13:21 108-88-3 1,2,3-Trichlorobenzene NO ug1L 2.0 2 1002111 13:21 87-61-6 1,44-Trichlorobenzene NO ug1L 2.0 2 10/12/11 13:21 120-82-1 1,1,1-Trichloroethane 341 ug1L 2.0 2 10/12/11 13.21 71-55-6 11,2-Trichloroethane ND ug1L 2.0 2 10/12111 13:21 79-00-5 Trichloroethene ND ug1L 2.0 2 10/12/11 13:21 79-0t-6 Trichlorofluoromethane NO ug1L 2.0 2 10/12/11 1321 75-69-4 1,2,3-T6chloropropane NO ug1L 2.0 2 10/12/11 13:21 96-18-4 Vinyl acetate NO ug)L 4.0 2 10/12/11 13:21 108-05-4 Vinyl chloride ND uglL 2,0 2 10112/11 13:21 75-01-4 m8p-Xylene NO uglL 4.0 2 10112/11 13:21 179601-23-1 o-xylene 3A uglL 2.0 2 10112M1 13:21 95-47-6 4-Bromonuorobenzene (S) 88 % 70-130 2 10/12/11 13:21 460-00-4 Dibromofluoromethene (S) 124 % 70.130 2 10/12/11 13:21 1868-53-7 1,2-Dichloroethane-d4 (S) 124 % 70-130 2 10/12/11 13:21 17060-07-0 Toluene-d8 (S) 101 % 70-130 2 10/12/11 13:21 2037-26-5 2320B Alkalinity Analytical Method: SM 23208 Alkali nily,Bicarbonate (CaCO3) 77.1 mg1L 5.0 1 10/11/11 10:30 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 17 of 67 This report shall not be reproduced, except in full, without the written consent of pace Analytical Services, Inc.. aceAnalytical xnnv.pace7ebs.cam Project: CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside ❑r. Asheville, NC 28804 (628)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 i{incey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Sample: EBMW-21 Lab ID: 92103792005 Collected: 10/04/11 12:30 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua! 2320E Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 77.1 mg1L 510 1 10/11/11 10:30 2540C Total Dissolved Solids Analytical Method SM 2540C Total Dissolved Solids 208 mglL 25.0 1 10/07111 16:35 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron, Ferrous NO mg1L 0-50 1 10/10/11 17:05 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2D Sulfide NO mglL 0A a 1 10108/11 12:00 18496-25-8 300.0 IC Anions 28 Days Analyt]caI Method: EPA 300,0 Sulfate 5.8 mglL 5.0 1 10/07/11 17:37 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mg1L 0.20 1 10/05/11 22:28 Nitrogen, Nitrite NO mglL 0.10 1 10/05/11 22:28 4500 Chloride Analytical Method: SM 4500-CI-E Chloride NO mg1L 5.0 1 10/08/11 13:54 16887-00-6 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 16.0 mglL 1.0 1 10/10/11 16:12 7440-44-0 Sample: EBMW-30 Lab ID: 92103792006 Collected: 10105/11 12:50 Received. 10105/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO ug1 10.0 1 10/11/11 15:22 74-84-0 Ethene NO ug1L 10.0 1 10/11/11 15:22 74-85-1 Methane 16.4 ug1L 10.0 1 10/11/11 15:22 74-82-8 2340B Hardness, Total [Calc.) Analytical Method: SM 2340B Total Hardness 182 mglL 0.65 1 10112/11 00:40 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 41500 uglL i00 1 10/07/11 10.50 10)12111 00:40 7440-70-2 Manganese 7000 uglL 5.0 1 10/07/11 1 M50 10)12111 00:40 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND uglL 5000 200 10/12/11 13:47 67-64-1 Benzene NO uglL 200 200 10/12/11 13:47 71-43-2 Bromobenzene ND ug1L 200 200 10/12/11 13:47 108-86-1 Date: 10/14/2011 09:06AM REPORT ❑F LASORATORY ANALYSIS Page 18 of 67 This report shall not be reproduced, except in full, wilhout the written consent of P ace A nalytiml Services. Inc ace Anal j4jcal a ,� _ w,�w.paceraAs.w+r+ i Pace Analytical Services, Inc. 205 East Meadow Raad - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc, 2225 Riverside [fir. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Anatyllcal Services, Inc 9800 Kinney Ave, Sulte 100 Huntersville, NC 28078 (704)875-9092 Project. CMl WWTP Pace Project No.: 92103792 Sample: EBMW-30 Lab 10: 92103792006 Collected: 10/05/11 12.50 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual 8260 MSV Low Level Analytical Method. EPA 8260 Bromochloromethane NO ug1L 200 200 10/12111 13:47 74-97-5 Bromodichioromethane NO ug1L 200 200 10/12111 13:47 75-27-4 Bromoform NO ug1L 200 200 10/12/11 13:47 75-25-2 Bromomethane ND ug1L 400 200 10/12/11 13:47 74-83-9 2-Sulanone (MEK) NO ug1L 1000 200 10/12/11 13:47 78-93-3 Carbon tetrachloride NO ug1L 200 200 101121il 13A7 56-23-5 Chlorobenzene ND ug1L 200 200 10/12/11 13:47 108-90-7 Chloroethane 643 ug1L 200 200 10/12/11 13:47 75-00-3 Chloroform NO ug1L 200 200 10/12111 13:47 67-66-3 Chloromethane N❑ ug1L 200 200 10/12/11 13:47 74-87-3 2-Chlorotoluene NO ug1L 200 200 10/12/11 13;47 95-49-8 4-Chlorotoluene NO ug1L 200 200 10117J11 13:47 106-43-4 12-Dibromo-3-chloropropane NO ug1L 1000 200 10/12/11 13:47 96-12-8 Dibromochloromethane ND ug1L 200 200 10/12/11 13:47 124-48-1 1,2-Dibromoethane (EDS) NO ug1L 200 200 1Of12111 13:47 106-93-4 Dibromomethane NO ug1L 200 200 10/12/11 13A7 74-95.3 1,2-Dichioroberizene ND ug1L 200 200 10/12/11 13:47 95-50-1 1,3-Dichiorobenzene N❑ ug1L 200 200 10112/11 13:47 541-73.1 1,4-Dichlorobenzene NO ug1L 200 200 10/12111 13:47 106-46-7 Dichlorodinuoromethane NO uglL 200 200 10/12/11 13:47 75-71-8 1,1-Dichloroethane 32800 ug1L 200 200 10/12/11 13:47 75-34-3 1,2-Dichloroethane ND uglL 200 200 1GM2111 13:47 1D7-06-2 1,1-Dichloroethene 6330 uglL 200 200 10/12/11 13:47 75-35-4 cis- 1,2-Dichloroethene ND ug)L 200 200 10/12/11 13:47 156-59-2 trans- 1,2-Dichloroethene N❑ uglL 200 200 10/12/11 13:47 156-60-5 1,2-Dichloropropane ND ug)L 200 200 10/12/11 13:47 78-87-5 1,3-Dichloropropane ND uglL 200 200 10/12/11 13A7 142-28-9 2,2-❑ichioropropane ND ug)L 200 200 10/12/11 13:47 594-20.7 1,1-Dichloropropene ND uglL 200 200 10/12111 13A7 563-58-6 cis-13-Dichloropropene ND uglL 200 200 10112111 13:47 10061-01-5 trans- 1,3-Dichloropropene ND uglL 200 20 10/12111 13,47 10061-02-6 Dlisopropyl ether NO ug)L 200 200 10112111 1147 108-2D-3 E<thylbenzene ND uglL 200 200 101i2111 13:47 100-41-4 Hexachloro-i,3-buladiene ND uglL 200 200 10/12/11 13,47 87-68-3 2-Hexanone ND uglL 1000 200 10/12/11 13:47 591-78-6 p-Isopropyltoiuene ND uglL 200 200 10/12/11 13747 99-87-6 Methylene Chloride NO ug1L 400 200 10/12/11 13:47 75-09-2 4-Methyl-2-pentanone (MIBK) NO uglL 1000 200 10/12/11 13:47 108-10-1 Methyl-tert-butyl ether NO uglL 200 200 10112/11 13.47 1634-04-4 Naphthalene ND uglL 200 200 10/12/11 13:47 91-20.3 Styrene ND ug1L 200 200 10/12111 13:47 100-42.5 1,1,1,2-Tetrachloroethane N❑ ug1L 200 200 1N12111 13:47 630-20-6 1.1,2,2-TetrachIaroethane N❑ ug1L 200 200 10/12/11 13:47 79-34-5 Tetrachloroethene ND ug1L 200 200 10/12/11 13:47 127-18-4 Toluene N❑ ug1L 200 200 10112Ji1 13:47 108-88-3 12,3-Trichiorobenzene N❑ ug1L 200 200 10)12111 13:47 87-61-6 1,2,4-TriChlorobenzene NO ug1L 200 200 10/12/11 13A7 120-82-1 Date: 10/1412011 09.06 AM REPORT ❑F LABORATORY ANALYSIS Page 19 of 67 This report shall not be reproduced, except In full, wilhoul the written Consent of Pace Analytical Services. Inc.. 7aceAnalXical werwoacelabs.4= PaceAnalylical Services, Inc, 205 East Meadow Road-SuiteA Eden, NC 27298 (3361623-8921 Pace Analytical Services, Inc. 2225 Rlverside Or. Asheville, NC 28804 (628)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite 100 Huwersville. NC 28078 (704)875-9D92 Project: CMi WWTP Pace Project No.: 92103792 Sample: EBMW-30 Lab ID: 92103792006 Collected. 10/05/11 12:50 Recelved: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. {dual 8260 MSV Low Level 1,1, i-Trichioroethane 1,1,2-Trichloroethane Trichloroethene Trich loran uoromethan e 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m8,p-Xylene o-Xyiene 4-Bromofluorobenzene {S) Dibromoflucromethane tSj 12-Dioh1oroethane-0 (S) To4uene-d8 (S) 2320E Alkalinity Alkaiinity,Bicarbonate (CaCO3) Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids Iron, Ferrous Iron, Ferrous 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 353.2 Nitrogen, N07IN03 unpres Nitrogen, Nitrate Nitrogen, Nitrite 4500 Chloride Chloride 5310E Tt7C Total Organic Carbon Analytical Method: EPA 8280 32700 ug/L 200 200 10112A 1 13A7 71-55-6 ND ug1L 200 200 10/12/11 13:47 79-00-5 ND ug1L 200 200 10112/11 13:47 79-01-6 ND u9JL 200 2D0 10/12/11 13:47 75-69-4 ND ug1L 200 200 10/12/11 13:47 96-18-4 ND ug/L 400 200 10/12/11 13:47 108-05-4 ND ugIL 200 200 10/12/11 13:47 75-01-4 N4 ug/L 400 200 10/12/11 13:47 179601-23-1 ND ug/L 200 200 10/12/11 13:47 95-47.6 91 % 70.130 200 1(/12/11 13:47 460-00-4 128 % M130 200 10/12/11 13:47 1868-53-7 128 % 70-130 200 10/12/11 1147 17060-07-0 101 % 70.130 200 10112Ji113:47 2037-26-5 Analytical Method: SM 2320B 175 mg/L 5.0 1 10/11/11 10:30 175 mg/L 5.0 1 10111/11 10 30 Analytical Method: SM 2540C 392 mg1L 25.0 1 10107/11 16:35 Analytical Method- SM 3500-Fe D#4 18.7 mg1L 5.0 10 10/10/11 18:23 Analytical Method: SM 4500-S2D 0.55 mg/L 0.10 1 10/08/11 12:00 18496-25-8 Analytical Method: EPA 300.0 N❑ mg1L 5.0 1 10/07/11 17:51 14808.79-8 Analytical Method: EPA 353.2 ND mg/L 0.20 1 10/06/11 22:42 0.48 mg1L 0.10 1 101001 22:42 Analytical Method: SM 4500-CI-E 83.0 mg/L 25.0 5 10108/11 14AD 16887-00-6 Analytical Method: SM 5310B 26.5 mg/L 10 1 10/10/11 16.22 7440-44-0 H1,N2 Dale: 10)14/201109:06AM REPORT OF LAB ORATO RY ANA LYS I S Page 2Dof67 This report shall not be reproduced, except in Full, without the written consent of Pace Analytical Services, Inc. _ aceanalytrcal "w_pace}a6s. mm Pace An alyticaI Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-$921 Pace AnaIyt+cal Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828]254.7176 ANALYTICAL RESULTS Pace AnalylicaI Services, Inc. 9800 KlnceyAve- Suile 100 Hunlersville, NC 28078 (704)875.9092 Project: CM WWTP Pace Project No.: 92103792 Sample: EBMW-31 Lab ID: 92103792007 Collected. 10/04/11 13 15 Received: 10105/11 16'35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane ND ug)L 10.0 1 10/10111 10:47 74-84-0 Ethene ND uglL 10.0 1 10110/11 10A7 74-85-1 Methane 14.7 uglL 10.0 1 10/10/11 10A7 74-82.8 2340E Hardness, Total (Cale.) Analytical Methods 5M 23403 Total Hardness 322 mg1L 0,65 1 10112/11 00:49 6010 MET ICP Analytical Method: EPA 6010 Prep era lion Method: £PA 3010 Calcium 71000 ug1L 100 1 10/07/11 10.50 10/12/11 00:49 7440-70-2 Manganese 8340 uglL 5.0 1 10/07/11 10:50 10/12111 00:49 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug1L 5000 200 10/12/11 06:50 67-64-1 Benzene ND ug1L 200 200 10/12/11 06:50 71-43-2 Bromobenzene NO uglL 200 200 10/12111 06:50 108-86-1 Bromochloromethane ND uglL 200 200 10/12/11 06:50 74-97-5 Bromodichloromethane ND uglL 200 200 10/12/11 06:50 75-27-4 Bromoform ND uglL 200 200 10/12/11 06:50 75-25-2 Bromomethane ND ug1L 400 200 10112/11 06:50 74-83-9 2-Butanone (MEK) ND uglL 1000 200 10/12/11 06:50 78-93-3 Carbon tetrachloride ND ug1L 200 200 10/12/11 06:50 56-23-5 Chlorobenzene ND uglL 200 200 10112/11 D6:50 108-90-7 Chloroethane 488 uglL 200 200 10/12/11 06,50 75-00-3 Chloroform ND uglL 200 200 10/12/11 06:50 67-66-3 Chloromethane ND uglL 200 200 10/12/11 06:50 74.87-3 2-Chlorotoluene ND uglL 200 200 10112)11 06-50 95-49-8 4-Chlorotoluene ND uglL 200 200 1011211106:50 106-43-4 1,2-01bromo-3-chloropropane ND uglL 1000 200 1011211106:50 96-12-8 Dibromochloromethane N❑ ug1L 200 200 10/12/11 06:50 124-48-1 1,2-Dibromoethane (EDB) ND uglL 200 200 1011211106:50 106-93-4 Dibromomethane ND ug1L 200 200 10112/11 06.50 74-95-3 1,2-Dichlorobenzene ND uglL 200 200 10/12/11 06:50 95-50-1 1,3-91Ctllorobenzene NO uglL 200 200 1011211106:50 541-73-1 II A-Dichlorobenzene ND uglL 200 200 1011211106:50 106-46-7 Dichlorodifluoromethane ND uglL 200 200 1011211106:50 75-71-8 1,1-Dichloroethane 226DO uglL 200 200 1D112111 06:50 75-34-3 1,2-Dichloroelhane ND uglL 200 200 10/12/11 06:50 107-06-2 1,1-Dichloroethene 19600 uglL 200 200 10112111 06:50 75-35-4 cis-1,2-Dichloroethene N❑ ug1L 200 200 10/12/11 06:50 156-59-2 trans-1,2-Dichloroethene NO ug)L 200 200 10112/11 06:50 156-60-5 1,2-Dichloropropane ND uglL 200 200 10/12111 003 50 78.87-5 1,3-Dichloropropane ND ug(L 200 200 10112111 06:50 142-28-9 2,2-Dichloropropane ND uglL 200 200 10112111 W:50 594-20-7 1,1-Dichloropropene Na ug)L 200 200 10412111 O6:50 563-58-6 cis-1,3-Dichloropropene NO uglL 200 200 10112/14 06,50 10061-01.5 trans-1,3-Dichloropropene ND uglL 200 200 10112111 DUO 10061-02.6 Date-. 10/1412011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 21 of 67 This report shall not be reproduced, except in full, without the written consent of Pace An aIyticai Services, Inc. ace Analytical www.pacelabs.mm Project CMl WWTP Pace Project No.: 92103792 Sample: EBMW-31 Parameters 8260 MSV Low Level Diisopropyl ether Ethylbenzene Hexachlord-1,3-butadiene 2-Hexanone p-Isopropylloluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl -tent -butyl ether Naphthalene Styrene 1,1,1.2-Tetrachloroethane 1.1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Tdchlorobenzene 1,2,4-Trichlorobenzene 1.1,1-Trichloroethane 1,1,2-Trichlorcelhane Trichlorcethene Trichlo roiluorome tha n e 1,2,3-Trichloroproparie Vinyl acetate Vinyl chloride m&p-Xyiene o-Xylene 4-Bromofluorobenzene (S) Dibromofiuoromethane (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320E Alkalinity Alkalinily,Bicarbonate (CaCO3) Alkalinity, Total as CaCO3 2540C Total dissolved Solids Total Dissolved Solids Iron, Ferrous Iron, Ferrous 4500S21) Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate Pace Analytical Services, Mc. 205 East Meadow Road - SuiteA Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, lie. 9800 Kincey Ave. Suite 100 Hvrntersville, NC 28078 t704j875.9092 Lab ID: 92103792007 Collected: 10/04/11 13:15 Received: 10/05/11 16:35 Malrix. Water Results Units Report Limit DF Prepared Analyzed CAS No, Dual Analytical Melhod: EPA 8260 NO ug/L 200 200 ND ug1L 200 200 ND ug/L 200 200 ND uglL 1000 200 NO ug/L 200 200 NO ug1L 400 200 ND uglL 1000 200 NO uglL 200 200 ND uglL 200 200 NO ug1 200 200 NO uglL 200 200 ND uglL 200 200 ND ug& 200 200 ND uglL 200 200 ND ug)L 200 200 N❑ uglL 200 200 221000 ugIL 2500 2500 ND uglL 200 200 N❑ ug)L 200 200 N❑ ug/L 200 200 ND ug/L 200 200 ND ug1L 400 200 ND ug1L 200 200 ND ug1L 400 200 ND ug1L 200 200 96 % 70.130 200 125 % 70.130 200 129 % 70.130 200 103 %v 70.130 200 Analytical Method- SM 2320B 41.7 mglL 5.0 1 41.7 mglL 5,0 1 Analytical Method: SM 2540C 624 mglL 25.0 1 Analytical Method: SM 3500-Fe D#4 58.4 mglL 5.0 10 Analytical Method: SM 4500-S2D ND mg/L 0.10 1 Analytical Method- EPA 300.0 ND mg/L 5.0 1 10112/1106:50 108-20-3 10/ 12111 06: 50 100-41-4 10112/1106:50 87-68-3 10/12/11 06:50 591-78.6 10/1211106:50 99-87-6 10/1211106:50 75-09-2 10 / 12111 06:5 0 108-10.1 10/12/11 06:50 1634-04.4 10/12/11 06:50 91-20-3 10 / 12111 06:50 100-4 2 -5 1011211106-50 630-20.6 1011211106:50 79-34-5 10/12/11 06:50 127-18-4 10/12/11 06:50 108-88-3 10112/11 06:50 87-61-6 10/12/11 06:50 120-82-1 1011211115:55 71-55-6 1011211106:50 79-00-5 10112/1106:50 79-01-6 10112/1106:50 75-69.4 1011211106!50 96-18-4 10/12/11 06;50 108-05-4 1011211106:50 75-01-4 10/12/11 06!50 179601-23-1 10112/1106:50 95-47-6 10112/1106:50 460-00-4 10/12/11 06:50 1868-5 3-7 10112/1106:50 17060-07 -0 1011211106,50 2037.26-5 10/11/11 10:30 10/11111 10:30 14107111 16:35 10110111 181-16 H1,N2 10/0811112:00 18496-25-8 D3 1010 7111 18,31 14808-7 9-8 Dale: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 22 of 67 This report shall not be reproduced, except in full, wilheut the written con senI of Pace AnalyticaI Services, Inc.. e aceAnalj4ical �I vww.pace7abs.r�m Pace Analytical Services, Inc. 205 East Meadow Read . Suite A Eden, NC 27288 (336M3.8921 Pace Analytical Services. Inc, 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinwyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GMI WWTP Pace Project No,: 02103792 Sample: EBMW-31 tab lD: 92103792007 Collected: 10/04/11 13:15 Received: 10/05/11 16:35 Matrix. Water Parameters Results Units Reporl Limit DF Prepared Analyzed CAS No. Qual 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mg1L 0.20 1 10)05/11 22:33 Nitrogen, Nitrite 0.14 mglL 0.10 1 10105/11 22:33 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 292 mg1L 50.0 10 10/08111 14:42 16887-00-6 53108 TOC Analytical Method SM 5310B Total Organic Carbon 45.5 mg1L 2.0 2 10111IM1 10:31 7440-44-0 Sample: EBMW-32 Lab ID: 92103792008 Collected: 10104/11 14.00 Received: 10/05/11 16:35 Matrix. Water Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual RSK 175 AIR Headspace Analytical Method. RSK 175 Ethane ND ug1L 10.0 1 101101i1 10:57 74-84-0 Ethene ND ugll- 10.0 1 10/10111 10:57 74-85-1 Methane 42.3 uglL 10,0 1 10110/11 10:57 74-82-8 2340B Hardness, Total (Catc.) Analytical Method: SM 2340B Total Hardness 281 mg1L 0.65 i 10112/11 00:58 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 79900 uglL 100 1 10/07/11 10:50 10112/11 00:58 7440-70-2 Manganese 3280 uglL 5.0 1 10/07/11 10:50 10/12/11 00:58 7439-96-5 8260 MSV Low Level Analytical Mel hod: EPA8260 Acetone ND uglL 500 20 10/12/11 07:16 67-64-1 Benzene ND uglL 20.0 20 10112/11 07:18 71-43-2 Bromobenzene NO uglL 20.0 20 10/12/11 07,16 108-86-1 Bromoch to rom ethane ND ug1L 20.0 20 101121110716 74-97-5 Bromodichloromethane NO ug1L 20.0 20 10112/11 07:16 75-27-4 Bromoform ND uglL 20.0 20 10/12/11 07;16 75-25-2 Bromomethane NO ug1L 40.0 20 10112/11 0716 74-83-9 2-Butanone (MEK) ND ug1L 100 20 10112/11 07:16 78-93-3 Carbon tetrachloride ND uglL 20.0 20 10/12111 07:16 56-23-5 Chlorobenzene ND ug1L 20.0 20 10/12/11 07:16 108-90-7 Chlvroethane 1390 ug1L 250 250 10112/1118:54 75-0D•3 Chloroform ND ug1L 20.0 20 10/12111 07;16 67-66-3 Chioromethane ND ug1L 20,0 20 1092/11 07:16 74-87-3 2-Chlorotoiuene NO uglL 20.0 20 10/12/11 07:16 95-49-8 4-Chiorotoluene NO uglL 20.0 20 10/12111 07-16 106-43-4 1,2-Dibromo-3-chloropropane NO uglL 100 20 10/12/11 07:16 96-12.8 Dibromochloromethane NO ug1L 20.0 20 10112/11 07:16 124-48-1 1,2-Dibromoethane (EDB) NO ug1L 20.0 20 10112/11 07'16 106-93-4 Dibromomethane NO ug1L 20.0 20 10/12111 07:16 74-95-3 Dale: 10114/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 23 of 67 This report shall not be reproduced, except in full, with out the written consent of Pace Analytical Services, Inc.. 1aceAnalj4ical wvrwpacera6xwm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 21288 (3n)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc, 9800 Kincey Aye. Suite 100 Huntersville, NC 28076 (704)875.9092 Project: CMI WWTP Pace Project No.: 92103792 Sample: EBMW-32 Lab ID: 92103792008 Ccllected: 10/04/11 14:00 Receivers: 10/05111 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 M5V Low Level Analytical Method: EPA 8260 1,2-Dichlorobenzene ND ug1L 20.0 20 i0112111 07:16 95-50-1 1,3-Dichlorobenzene ND ug1L 20.0 20 10/12/11 07:16 541-73-1 1,4-13ichlorobenzene ND ug1L 20.0 20 10112/11 07:16 106.46-7 Dichlorodiflucromethene ND uglL 20.0 20 10112111 07:16 75-71-8 1,1-Dichloroethane 30300 ug1L 250 250 10/12/11 18:54 75-34-3 12-Dichlaroethane 56A ug1L 20.0 20 10112/11 07:16 107-06-2 1,1-Dichloroethene 3980 ug1L 20.0 20 10/12/11 07:16 75-35-4 cis-1,2-Dichloroethene NO ug1L 20.0 20 10/12/11 07:16 156-59-2 trans-1,2-Dichloroethene NO uglL 20.0 20 1011211107:16 156-60-5 1,2-Dichloropropane NO ug1L 20.0 20 10/12/11 07:16 78-87-5 1,3-Dichloropropane NO uglL 20.0 20 1011211107:16 142-28.9 2,2-Dichloropropane ND uglL 20.0 20 10/12/11 07:16 594-20-7 1,1-Dichlaropropene NO uglL 20.0 20 10/12/11 07:16 563-58-6 cis-1,3-Dichlaropropene NO ug1L 20.0 20 10/12/11 07;10 10061-01-5 trans- 1, 3- 0 ich loropro pene ND uglL 20.0 20 10/12/11 07:16 10061-02-6 Diisopropyl ether NO uglL 20.0 20 10/12/11 07:16 108-20-3 Ethylbenzene NO ugJL 20.0 20 10/12/11 07:16 100-41-4 Hexachloro-1,3-hutadiene NO uglL 20.0 20 1002111 07:16 87-58-3 2-Hexanone NO uglL 100 20 10/12/11 07:16 591-78-6 p-lsopropyiloluene NO uglL 20.0 20 10/12/11 07:16 99-87-6 Methylene Chloride ND uglL 40.0 20 10/12/11 07:16 75-09-2 4-Meth yl-2- pen tanon e (MIRK) 154 uglL 100 20 10/12/11 07:16 108-10-1 Methyl -tent -butyl ether ND ug1L 20.0 20 10M2111 07:16 1634-04-4 Naphthalene NO uglL 20.0 20 1DJ12MI 07:16 91-20-3 Styrene NO ug1L 20.0 20 10/12/11 07:16 100-42-5 1. 1, 1,2-Tetrach loroethane ND uglL 20.0 20 10M2/11 0716 630-20-6 1,1,2,2-Tetrachloroethane NO uglL 20,0 20 10/12/11 07:16 79-34-5 Tetrachloroethene IN ug1L 20.0 20 10112/11 07:16 127-18.4 Toluene ND ug1L 20.0 20 10/12/11 07:16 108-88.3 1,2,3-Trichlorobenzene N❑ uglL 20.0 20 10112111 07:16 87-61-6 1,2,4-Trichlorohenzene N❑ ug1L 20.0 20 10/12/11 07:16 120-82-1 1,1,1-Trichloroe thane 28300 ug1L 250 250 10/12111 18:54 71-55-6 1,1.2-Trichloroethane 53.4 uglL 20.0 20 10/12/11 07 16 79-00-5 Trichloroethene 29.0 uglL. 20.0 20 10/12111 DT 16 79-01-6 Trichlorofluoromethane ND ug1L 20.0 20 10/12/11 07:16 75-69-4 1,2,3-Trichloropropane ND uglL 20.0 20 10/12/11 07:16 96-18-4 Vinyl acetate ND ug1L 40.0 20 10/12111 07:16 108-05.4 Vinyl chloride 21.5 uglL 20.0 20 10112111 07;16 75-01-4 m&p-Xylene ND uglL 40.0 20 10112/11 07!16 179601-23-1 o-xylene ND uglL 20.0 20 10/12/11 07:16 95-47-6 4-Bromofluorobenzene (S) 96 % 70-130 20 101121110716 460-DO-4 Dibromofluoramethane (S) 126 % 70-130 20 10112111 07:16 1868-53-7 12-Dichloroethane-d4 (S) 127 % 70-130 20 10/12/11 07:16 17060-07-0 Toluene-d8 (S) 103 % 70-130 20 10/12/11 07:16 2037-26-5 2320E Alkalinity Analytical Method: SM 23208 Alkalinity,Bicarbonate (CaG03) 72.9 mg1L 5.0 1 10/11/11 10:30 Date: 10/14/2011 09TBAM REPORT OF LABORATORY ANALYSIS Page 24 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc ■ aceAnalytical nKx.yare+ahs.rac: Projecl CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - SulteA Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Or. Ashevilie. NC 28804 (B28)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9082 Sample: EBMW-32 Lab ID: 92103792008 Collected: 10/04/11 14.00 Received. 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2320B Alkalinity Analytical Method: SM 23203 Alkalinity. Total as CaCO3 72.9 mglL 5.0 1 10/11/11 10:30 2540C Total Dissolved Solids Analytical Method: SM 2540C Total Dissolved Solids 708 mglL 25.0 1 10/07111 16:35 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron, Ferrous 77.9 mg1L 0.50 1 10/10111 13:30 H1,N2 4500S2D Sulfide Water Analytical Method: SM 4500-S2❑ Sulfide NO mglL 0.10 1 10/08/11 12:00 18496-25-6 300,0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate NO mg(L 5.0 1 10/07/11 18:45 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate NO mg1L 0.20 1 10/05/11 22:35 Nitrogen, Nitrite 0.11 mg& 0.10 1 10/05/11 22:35 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 269 mg1L 50.0 10 10/08111 14 45 16887-00-6 53108 TOG Analytical Method. SM 53108 Total Organic Carbon 54.1 mgIL 2.0 2 10111/11 10:41 7440-44-0 Sample: FPMW5 Lab ID: 92103792009 Collected: 10/05/11 09:00 Received. 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit DP Prepared Analyzed CAS No. Qual RSK 175 AIR Headspace Analytical Method: RSK 175 Ethane NO ug1L 10.0 1 10/11111 14.29 74.84.0 Ethene NO ug/L 10.0 1 10)11/11 14:29 74-85-1 Methane ND ug1L 10.0 1 10/11111 14:29 74.82-8 2340B Hardness, Total jCatc.j Analytical Method: SM 2340B Total Hardness 184 mglL 0,65 1 10/12/11 02.32 60110 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Calcium 65400 uglL 100 1 10/07/11 %50 10/12/11 02:32 7440-70-2 Manganese 1430 uglL 5.0 1 10/07/11 10 50 10/12/11 02:32 7439-96-5 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO uWL 25.0 1 10111111 08:50 67.64-1 Benzene NO ug/L 1.0 1 10/11/11 06:50 71-43-2 Bromobenzene NO ug)L 1.0 1 10/11/11 06:50 108-86-1 Date- 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 25 of 67 This report. shall not be reproduced, except in full, w11110ut the written consent of Pace Analytical Services, Inc aCMnalytical Kwwpaceiabs.cam Project: CMI WWTP Pace Project No-: 92103792 Sample: FPMW-5 Parameters 8260 MSV Low Level Brornachloromethane B ramodich Ior❑m ethane Brornoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloramethane 2-Chlorotoluene 4-Chloratoluene 1, 2-D ibromo-3-eh ioropropane D ibrom och lorom eth ane 1,2-Dibromaethane (EDS) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene D ichlorod ifl uorom eth a ne 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene ci s-1, 2-Dichloroeth ene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichlaropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MI6K) Methyl -tort -butyl ether Naphthalene Styrene 1.1.1, 2- Telrach loroeth a ne 1.1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2, 3-Trcchlorobenzene 1,2,4-Trichlorobenzene Pace Analytical Services, Inc. 205 East Meadow Read - Suite A Eden, NC 27288 (336)823.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9809 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID: 92103792009 Collected: 10/05111 09:00 Received. 10/05111 16:35 Matrix: Water Results Units Report Limit ❑F Prepared Analyzed CAS No. Qual Analytical Method: EPA 8260 ND ug1L IN uglL ND uglL ND ug1L NO uglL NO ug1L NO ug1L NO uglL ND uglL NO uglL NO uglL ND ug1L ND uglL NO q1 ND uglL ND uglL ND uglL ND uglL NO uglL NO uglL 9.8 uglL N❑ ug)L NO uglL NO ugll- NO uglL NO uglL ND uglL NO uglL ND ug1L NO uglL ND uglL ND ug1L NO ug1L N❑ uglL NO ug1L ND uglL NO ug1L ND ug1L NO ug1L ND ug1L ND ug1L NO ug/L NO uglL NO uglL NO ug& NO ug)L NO uglL 1.0 1 10111111 M50 74-97.5 1.0 1 10/1111106:50 75-27-4 1.0 1 1011111106:50 75-25-2 2.0 1 1011111106:50 74-83.9 5.0 1 1011111106:50 78-93-3 1.0 1 1011111166:50 56-23-5 1.0 1 10111/11 176:50 108-90-7 1.0 1 10M111106:50 75-00-3 1.0 1 1 D111111 06:50 67-66-3 1.0 1 10/11/11 D6:50 74-87-3 1.0 1 10111/1106:50 95-49-8 1.0 1 1 D111111 06:5D 106-43-4 &0 1 10/11/14 06:50 96-12-8 1.0 1 1011111106,50 124.48-1 1.0 1 10/11/11 06:50 106-93-4 1.0 1 10111/1106:50 74-95-3 1.0 1 10111/1106:50 95-50-1 1.0 1 10/1111106:5D 541-73-1 1.0 1 10/11/11 06:50 106-46-7 1.0 1 10111/1106:50 75-71-8 1.0 1 1011111106:50 75-34-3 1.0 1 10111 /11 06.50 107-06-2 1.0 1 10111/1106:50 75-35-4 1.0 1 10/11/11 06:50 156-59-2 1.0 1 10/11/11 06.50 158-60-5 1.0 1 1011111106:50 78-87-5 1.0 1 101111110&50 142-28-9 1.0 1 10/11/11 06:50 594-20-7 1.0 1 10111/1106:50 563-58-6 1.0 1 10/11/11 06: 50 10061-01-5 1.0 1 10/11/11 06:50 10061-02-6 1.0 1 10111/11 06:50 108-20-3 1.0 1 10/11/11 06:50 1 OD-41-4 1.0 1 10/11/11 06:50 87-68-3 5.0 1 10/11/11 06:50 591.78-6 1.0 1 10/11/11 06:50 99-87-6 2.0 1 10/1111106:50 75-09-2 5.0 1 10/11/11 D6:50 108-10-1 1-0 1 10111/11 06:50 1634-04-4 1.D 1 10/11/11 06:50 91-2D-3 1.0 1 1 DI11111 06:50 100-42.5 1.0 1 1011111106-50 630-20-6 1-0 1 10/11/11 06:50 79-34-5 1-0 1 10111/1106:50 127-18-4 1.0 1 10/11/11 06-50 108-86-3 1-0 1 10/11/11 D6:50 87-61-6 1-0 1 10111 / 11 D6:50 120-82-1 Date: 10M412011 09:06AM REPORT OF LABORATORY ANALYSIS Page 26 of 67 This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ace RnaPical rnsw.�ace'a6s.cam Project CMI WWTP Pace Project No. 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville. NC 29804 028)254-7176 ANALYTICAL RESULTS Pace Analytical Services. Inc. 9800 Klncey Ave. Suite 100 Huntersvilie, NC 28078 (704)675.9092 Sample: FPMW5 Parameters Lab ID: 92103792009 Collected: 10/05/11 09:00 Results Units Report Limit DF Received: 11WO5111 16:35 Matrix. Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 1,1,1-Trichloroethane ND ugIL 1.0 1 10/11/11 06:50 71-55-6 1,1,2-Tdchloroethane ND ugIL 1.0 1 10/11/11 06:50 79-00-5 Trichloroethene ND ugIL 1.0 1 1DJ11111 06:50 79-01-6 Trichloroiluoromethane ND ug)L 1.0 1 10/11/11 06.50 75-69-4 1,2,3-Trichloropropane ND ugIL 1.0 1 10/11111 06:50 96-18-4 Vinyl acelate NO ug1L 2,0 1 10/11/11 06:50 108-05-4 Vinyl chloride ND ugJL 1 A 1 10/11/11 06:50 75-01-4 m&p-xylene ND ugIL 2,0 1 10/11/11 06:50 179601-23-1 a-Xylene ND ugIL 1.0 1 10/11/11 06:50 95-47-6 4-Bromofluorobenzene [S) 101 °% 70-130 1 10)11111 06:50 460-00-4 Dibromofluoromethane (S) 100 °% 70-130 1 10/11/11 06.50 1B68-53-7 1,2-Dichloroethane-d4 (S) 110 °% 70-130 1 10/11/11 06:50 17060-07-0 Toluene-d8 (S) 102 °% 70-130 1 10/11/11 06:50 2037-26-5 2320E Alkalinity Analytical Method: SM 2320B Alkalinity,Bicarbonate (CaCO3) 29.2 mg1L 5.0 1 10/11/11 10:30 Alkalinity, Total as CaCO3 29.2 mg1L 5.0 1 10/11/11 10:30 2540C Total Dissolved Solids Analytical Method: SM 25400 Total Dissolved Solids 302 mg1L 25.0 1 10/07/11 16:36 Iron, Ferrous Analytical Method: SM 3500-Fe D#4 Iron, Ferrous 3.1 mg1L 1.0 2 10/10/11 17:36 H 1, N2 4500S2❑ Sulfide Water Analytical Method: SM 4500-S2❑ Sulfide N❑ mg1L 0.10 1 10/08/11 12,00 18496.26-8 300.0 IC Anions 28 Days Analytical Method- EPA 300,0 Sulfate 146 mg1L 50.0 10 10/08111 11:21 14808-79-8 353.2 Nitrogen, NO2IN03 unpres Analytical Method: EPA 353,2 Nitrogen, Nitrate N❑ mg1L 0,20 1 10/06/11 22:26 Nitrogen, Nitrite ND mg/L D.11) 1 10106/11 22:26 4500 Chloride Analytical Method: SM 45DO-CI-L Chloride ND mg/L 5.4 1 10/08/11 13:57 16887-00-6 53108 TDC Analytical Method: SM 5310B Total Organic Carbon 14.6 mg1L 1.D 1 10/10111 16:54 7440-44-0 Date- 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 27 of 67 This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, Inc.. ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 205 East Meadow Road • Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 1o0 aes Eden, NC 27288 Asheville, NC 28804 H untersvi Ile, NC 28078 (335)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: CMI WWTP Pace Project No.: 92103792 Sample: DUPLICATE Lab ID: 92103792010 Collected: 101D4111 14:35 Received: 10105111 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NO uglL 25.0 1 10/10/11 21:33 67-64-1 Benzene NO ug1L 1.0 1 10/10111 21:33 71-43-2 Bromobenzene ND uglL 1.0 1 10/10/11 21:33 108-86.1 Bromochloromethane NO ug1L 1.0 1 10/10111 21:33 74-97-5 Bromodichloromethane NO ug1L 1.0 1 10/10/11 21:33 75-27-4 Bromoform NO uglL 1.0 1 10/10/11 21:33 75-25-2 Bromomethane NO uglL 2.0 1 10/10111 21:33 74-83-9 2-Butanone (MEK) NO uglL 5.0 1 10110111 21:33 76-93-3 Carbon tetrachloride NO ug1L 1.0 1 10/10/11 21:33 56-23-5 Chiorobenzene 11,9 ug1L 1.0 1 10110/11 21:33 108-90-7 Chloroethane ND ug1L 1.0 1 10/10/11 21:33 75-00-3 Chloroform NO ug1L 1.0 1 10/10/11 21M 67-66-3 Chloromethane NO ug1L 1.0 1 10/10/11 21M 74-87-3 2-Chlarotoluene NO ug1L 1.0 1 10110/11 21:33 95-49-8 4-Chiarotoluene NO ug1L 1.0 1 10/10/11 21:33 106-43-4 1.2-Dibromo-3-chloropropane NO ug1L 5.0 1 10/10/11 21:33 96-12-8 Dibromochloromethane ND ug1L 1.0 1 10/10/11 21:33 124-48-1 1,2-Dibromoethane (EDB) NO ug1L 1.0 1 10/10/11 21:33 106-93-4 Dibromomethene NO ug1L 1.0 1 10110111 21:33 74-95-3 1,2-❑ichlarobenzene NO uglL 1.0 1 10/10/11 21:33 95-50-1 1,3-Dichlorobenzene NO uglL 1,0 1 10/10/11 21,33 541-73-1 IA-Dichlorobenzene 3.0 ug1L 1.0 1 10/10/11 21M 106-46-7 Dichlorodifluoromethane NO ug1L 1.0 1 10/10/11 21:33 75-71-8 1,1-Dichloroethene 4.4 ug1L 1.0 1 10/10/11 21:33 75-34-3 1,2-Dichloroethane NO ug1L 1.0 1 10/10/11 21:33 107-D6.2 1,1-Dichloroethene 9.5 ug1L 1.0 1 101101112133 75-35-4 cis-1,2-Dichloroethene NO uglL 1.0 1 10/10/11 21,33 156-59-2 trans-1,2-Diohioroethene NO uglL 1.0 1 10/10/11 21:33 156-60-5 1,2-Dichloropropane NO ug1L 1.0 1 10/10/11 21:33 78.87-5 1,3-Dichloropropane NO ug1L 1.0 1 10/10/11 21.33 142-28.9 2,2-Dichloropropane NO ug1L 1.0 1 10/10/11 21:33 594-20-7 11,1-Dichloropropene N❑ ug1L 1.0 1 10/10/11 21:33 563-58.6 cis-1,3-Dichloropropene NO uglL 1.0 1 10/10/11 21:33 10061-01-5 trans-1,3-Dichioropropone N❑ ug1L 1.0 1 10/10/11 21:33 10061-02-6 Diisopropyl ether ND uglL 1.0 1 10/10/11 21:33 108-20-3 Ethylbenzene NO uglL 1.0 1 10/10/11 21:33 100-41-4 Hexachloro-1.3-butadiene ND uglL 1.0 1 10/10/11 21:33 67-68-3 2-Hexanone ND uglL 5.0 1 10/10/11 21:33 591-78-6 p-Isopropylioiuene NO ug1L 1.0 1 10/10/11 21:33 99-87-6 Methylene Chloride NO ug1L 2.0 1 10/10/11 21:33 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug1L 5.0 1 10/10/11 21:33 108-10-1 Methyl-terl-butyl ether NO ug1L 1.0 1 10/10/11 21:33 1634-04-4 Naphthalene NO uglL 1.0 1 10/10/11 2i:33 91-20-3 Styrene NO ug1L 1.0 1 10/10/11 21:33 100-42-5 1.1,1,2-Tetrachloroethane ND ug1L 1.0 1 10/10/11 21.33 630-20-6 1,1,2,2-Tetrachloroethane ND uglL 1.0 1 10/10/11 21:33 79.34-5 Tetrachloroethene N❑ uglL 1.0 1 101101112133 127-18-4 Date-. 10114/2011 09:06 AM REPQRT ❑F LABORATORY ANALYSIS This report shall not ba reproduced, except in full, without the written consent of Pace Analytical Services, inc. Page 28 of 67 a• /7;a'ce Ana lj&aI wawpace7ahs.cam Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dt Asheville, NC 28604 (0281254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Huntersvllle, NC 28078 (7041875-9092 Project CMI WWTP Pace Project No.: 92103792 Sample: DUPLICATE Lab ID: 92103792010 Collected: 10/04/11 14:35 Received: 10)05111 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quat 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug)L 1.0 1 10110/11 21:33 108-88-3 1.2,3-Trichlorobenzene N❑ ug1L 1.0 1 10/10/11 21:33 87-61-6 1,2,4-Trichlorobenzene ND uglL 1.0 1 10/10/11 21:33 120-82-1 1.1,1-Trichloroethane 7,9 ug1L 1.0 1 10/10/11 21:33 71-55-6 1,1,2-Trichlaroethane ND uglL 1.0 1 10/10/11 21:33 79-00-5 Trlchloroethene ND uglL 1.0 1 10110/11 21:33 79-01-6 Trlchloroflueromethane ND uglL 1.0 1 10/10111 21:33 75-69-4 1,2,3-Trichloropropene ND uglL 1.0 1 10110/11 21:33 96-18-4 Vnyl acetate NO uglL 2.0 1 10/10/11 21:33 1M05-4 Vinyl chloride ND uglL 1.0 1 10/10/11 21:33 75-01-4 m&p-Xylene ND uglL 2.D 1 10110/11 21.-33 179601-23-1 o-xylene ND ug1L 1.0 1 10/10111 21:33 95-47-6 4-Bromonuarobenzene (S) 91 % 70-130 1 10/10/11 21:33 40D-00.4 ❑ibromatluoromethane (S) 130 % 70-13D 1 10/10/11 21.-33 1868-53-7 1,2•Dichloreethane-d4 {S) 130 % 70-130 1 1Of10111 21:33 17060-07.0 Toluene-d8 (S) 102 % 70-130 1 10/10/11 21:33 2037-26-5 Sample: RB•1 Lab ID: 92103792011 Collected: 10/05/11 09:30 Received: 10ID5111 16:35 Matrix: Water Parameters Results Units Report Llmit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone N❑ ug1L 25.0 1 10/10/11 23:41 67-64-1 Benzene NO uglL 1.0 1 10/10111 23:41 71-43-2 Bromobenzene NO uglL 1.0 1 10/10111 23:41 108-86-1 Bromochloromethane NO uglL 1.0 1 10/10111 23:41 74-97-5 Bromodichloromethane NO uglL 1.0 1 10/10/11 23:41 75-27-4 Bromororm ND ug)L 1.0 1 10/10/11 23A1 75-25-2 Bromomethane ND uglL 2.o 1 10/10/11 23:41 74-83-9 2-Butanone (MEK) ND uglL 5.0 1 10/10/11 23:41 78-93-3 Carbon tetrachloride ND uglL 1.0 1 10/10/11 23:41 56-23-5 Chlorobenzene N❑ uglL 1.0 1 10/10/11 23:41 108-90-7 Chloroethane NO uglL 1.0 1 10/10/11 23AI 75-OD-3 Chloroform ND uglL 1.0 1 10/10/11 23:41 67-66-3 Chloromethane ND ug1L 1.0 1 10/10/11 23:41 74-87-3 2-Chlorotoluene ND uglL 1.0 1 10/10/11 23:41 9549-8 4-Chlorotoluene N❑ ug1L 1.0 1 10/10/11 23:41 106-43-4 1,2-01bromo-3-chloropropane N❑ ug1L 5.0 1 10/1(V11 23:41 96-12-8 Dibromochloromethane NO ug1L 1.0 1 10/10111 23:41 124-48-1 1,2-Dibromoethane (EDS) ND ug1L 1.0 1 10/10/11 23.41 106-93-4 Dibromomethane NO uglL 1.0 1 10/10/11 23:41 74-95-3 1.2-Dichlorobenzene ND ug1L 1.0 1 10/10/11 23:41 95-50-1 1,3-Dichlorobenzene ND uglL 1.0 1 10/10/11 23:41 541-73-1 1,4-Dichlorobenzene ND ug1L 1.0 1 10/10/11 23A 1 106-46-7 Dichlorodifluoromethane NO uglL 1.0 1 10/10/11 23:41 75-71-8 1,1-Mchloroethane ND ug)L 1.0 1 10110/11 23:41 75-34-3 Date: 1011412011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 29 of 67 This report shall not be reproduced. except In full, without the written consent of Pace Analytical Services, Inc.. /�;alceAnalyticalo invw.pacerabs.curr, Project. CMI WWfP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside W. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KimeyAve. Suite 100 Huriters0e, NC 28078 [704)875-9092 Sample: RB-1 Lab ID: 92103792011 Collected. 10/05/11 09:30 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quai 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dichloroethane ND ug1L 1.0 1 10/10/11 2141 107.06-2 1,1-Dichloroethene NO uglL 1.0 1 10/10111 23:41 75-35-4 cis•1,2-Dichloroethene NO uglL 1.0 1 10/10111 23:41 156-59-2 trans-1.2-Dichloroethene NO ug/L 1,0 1 10110/11 23:41 156-60-5 1,2-Dichloropropane ND ug/L 110 1 10110/11 23:41 78-87-5 1,3-01chloropropane ND ug/L 1.0 1 10/10/11 2141 142-28-9 2,2-Dichloropropane ND uglL 1.0 1 10/10/11 23:41 594-20-7 1,1-Dichloropmpene NO ug/L 1.0 1 10110/11 23:41 563-58-6 cis- 1,3-Dichloropropene ND ug/L 1.0 1 10/10/11 23:41 10061-01-5 trans-1,3-Dichloropropene NO uglL 1.0 1 10/10/11 23:41 10061-02.6 Diisopropyt ether NO ug1L 1,0 1 10/10/11 23:41 108-20-3 Ethylbenzene NO ug/L 1.0 1 10/10/11 23:41 100-41-4 Hexachloro-1,3-butadiene NO ug/L 1.0 1 10/10111 23:41 87-68-3 2-Hexanone NO ug)L 5,0 1 10/10/11 23:41 591-78.6 p-Isopropyltoiuene NO uglL 1.0 1 10/10/11 23:41 99-87-6 Methylene Chloride NO uglL 2.0 1 10/10111 23AI 75-09-2 4•Methyl-2-pentanone (MISK) N❑ uglL 5.0 1 10110/11 23:41 108-10-1 Methyl -tent -butyl ether NO ug/L 1.0 1 10/10/11 23:41 1634-04-4 Naphthalene ND ug/L 1.0 1 10110/11 2141 91-20-3 Styrene ND ug/L 1.0 1 1011011i 23:41 100.42-5 1.1,1,2-Telrachloroethane ND ug/L 1.0 1 10/10/11 23:41 630-20-6 1,1,2,2-Tetrachloroelhane ND ug/L 1.0 1 10/10/11 23:41 79-34-5 Tetrachloroethene ND ug/L 1.0 1 10110)11 23:41 127-18-4 Toluene NO ug/L 1.0 1 1011 D111 23,41 1 DS-88-3 11,2,3-Trichlorobenzene, NO ug1L 1.0 1 10M0111 23:41 87-61-6 1,2,4-Trichlorobenzene NO ug1L 1.0 1 10/10/11 23A1 120-82-1 1,1,1-Trichloroethane NO uglL 1.0 1 10/10/11 23:41 71-55-6 1,1,2-Trlchloroethane NO uglL 1.0 1 10110/11 23:41 79-00-5 Trichioreethene ND uglL 1,0 1 10/10/11 2141 79-01-6 Trichlorofluoromethane NO uglL 1.0 1 10110/11 23:41 75-69-4 1,2,3-Tichooropropane NO ug/L 1,0 1 10/10/11 23:41 96-18-4 Vinyl acetate NO uglL 2.0 1 10/10/11 23:41 108-05-4 Vinyl chloride NO ug/L 1.0 1 10/10/11 23:41 75-01-4 m&p-Xylene ND ug/L 2.0 1 10/10/11 23:41 179601-23-1 o-Xylene NO ug/L I.0 1 10/10/11 23:41 95-47-0 4-Bromofluombenzene (S) 93 % 70-130 1 10110/11 2141 460-00-4 Dibromofluoromethane (S) 126 % 70-130 1 10/10/11 23:41 1868-53-7 1,2-Dichloroethane-d4 (S) 125 % 70-130 1 10/10/11 23:41 17060-07-0 Toluene-d8 (S) 102 01 70-130 1 10/10/11 23,41 2037-26.5 Sample: TRIP BLANK 2 Lab ID: 92103792012 Collected. 10/05/11 00:00 Received 10/05111 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 10111/11 00:06 67-64-1 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 30 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. inc- 1!�2 aceAnalpical nxm.Aarelabs,cam Projecl: CMI WWfP pace Analytical Services, Inz. PaceAnalyticaI Services, Inc. 205 East Meadow Read - Sulte A 2225 Riverside Dr. Ellen, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc 9800 KinceyAve. Sulte 100 H u ntersvil la, NC 28076 Pace Project No-: 921037132 Sample: TRIP BLANK 2 Lab ID: 92103792012 Collected: 10/05/11 0D:D0 Received: 10/05/11 1&35 Matrix: Water (704)875.9092 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Quai 8260 MSV Low Level Analytical Method: EPA 8260 Benzene NO ug1L 1.D 1 10/11111 00:06 71-43-2 Bromobenzene NO uglL 1.0 1 10111/11 00:06 108-86-1 Bromochloromethane NO ug1L 1.0 1 10/11/11 00!06 74-97-5 Bromodichloromethane NO ug/L I.0 1 10111/11 00:06 75-27-4 Sromotorm ND ug1L 1.0 1 10/11/11 00:D6 75-25-2 Bromomettlane ND uglL 2.0 1 10/11/11 00:06 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 10/11/11 D0:06 78-93-3 Carbon tetrachloride NO uglL 1.0 1 10/11/11 00:06 56-23-5 Chlorobenzene NO uglL 1.0 1 10/11/11 D0:06 108-90-7 Chloroethane NO uglL 1.0 1 10/14/11 00:06 75-00-3 Chloroform NO uglL 1.0 1 10111111 00:08 67-66-3 Chloromethane NO uglL 1.0 1 10/11/11 D0:06 74-87-3 2-Chlorotoluene NO ug1L 1.0 1 10/11/11 00:06 95-49-8 4-Chlorotoluene NO uglL 1.0 1 10111/11 00:D8 106-43-4 1,2-Dibromo-3-cnloropropane NO uglL 5.0 1 10/11/11 00:06 96-12-8 Dibromochloromethane NO uglL 1.0 1 10/11/11 00:D6 124-48-1 1,2-Dibromoethane (EDB) No uglL 1.0 1 10/11/11 00:06 106-93-4 Dibromomelhane NO uglL 1.0 1 10111/11 00:06 74-95-3 12-01chlorobenzene NO ug1L 1.0 1 10/11/11 D0:W 95-50-1 1,3-Dichlorobenzene NO uglL 1.0 1 10/11/11 00:06 541-73.1 1.4-Dichlorobenzene NO uglL 1.0 1 i0111111 00.06 106-46-7 Dichlorodifluaromethane NO ug1L 1.0 1 W111111 00:06 75.71.8 1,1-Dichloroethane NO uglL 1.0 1 10/11/11 00:06 75-34-3 1.2-Dichloroethane NO uglL 1.0 1 10/11/11 00:06 107-06-2 1,1-Dlchloroethene ND ug1L 1.0 1 10111/11 00.06 75-35-4 cis-1.2-Dichiorcethene ND uglL 1.0 1 10/11/11 00:06 156-59-2 trans- l,2-Dichloroethene NO uglL 1.0 1 10111/11 00:06 156-6D-5 1,2-Dichloropropane NO uglL 1.0 1 10/11/11 00:06 78-87-5 1,3-Dichloropropane NO ug)L 1.0 1 10/11/11 00:06 142-28-9 2,2-Dichloropropane NO ug1L 1.0 1 10/11/11 00:06 594-20-7 1,1-Dichloropropene ND uglL 1.0 1 10/11/11 00:06 563-58-6 cis- 1,3-Dichioropropene NO ug1L 1.0 1 10/11/11 00:06 10061-01-5 trans- l,3-Dichloropropene NO uglL 1.0 1 10/11/11 00:06 10061-02-6 Diisopropyl ether ND uglL 1.0 1 10/11/11 00:06 108-20.3 Ethytbenzene NO uglL 1.0 1 10/11/11 00:136 100-41-4 Hexachlorc-1,3-butadiene N❑ uglL 1.0 1 10/11/11 00:06 87-68-3 2-Hexanone NO uglL 5.0 1 10/11/11 00:06 591-78-6 p4sopropyitoluene NO uglL 1.0 1 10/11/11 00:06 99-87-6 Methylene Chloride ND uglL 2.0 1 10111/11 00 D6 75-09-2 4-Methyl-2-pentanone {MIBK) ND uglL 5.0 1 10/11/11 00:06 108-10-1 Methyl -tent -butyl ether ND uglL 1.0 1 10/11111 00:06 1634-04-4 Naphthalene ND ug1L 1.0 1 10/11/11 00:06 91-20-3 Styrene NO uglL 1.0 1 10111/11 00:06 100-42-5 1.1.1.2-Tetrachloroethane ND uglL 1.0 1 10111/11 00:06 630-20-6 1,1,22-Tetrachloroethane N0 ug1L 1.0 1 10111111 00:06 79-34-5 Tetrachloroethene ND ug)L 1.0 1 10/11/11 00.06 127-18-4 Toluene NO uglL 1.0 1 10/11/11 00:06 108-88-3 Date: 10/14/2011 09.06AM REPORT OF LABORATORY ANALYSIS Page 31 of 67 This report shall not be reproduced, exGapt in Tull. without the written consent of Pace Analytical Services, Inc.. aceAnalytical � wrrw.AacefaLs.mm Project: CM WWfP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (338)623.8921 Pace Analytical Services, Inc_ 2225 Rivers lde Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL. RESULTS Pace Analytical Services, Inc. 19800 KinceyAve. Sulte 1{10 Hunlersviiie, NC 28078 (704)875.9092 Sample: TRIP BLANK 2 Lab ID: 92103792012 Collected: 10/05/11 00:00 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level 1,2,3-Trichlorabenzene 1,2,4-Trichlorabenzene 1,1,1-Trichloroethane 11,2-Trichlorcethane Trichloroethene Trich lorofiu orom eth a ne 1,2,3-Trichlaropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofiuoromethane (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Analytical Method: EPA 8260 NO ug1L ND uglL N❑ uglL ND ug1L ND uglL N❑ uglL ND ug1L ND ug1L ND ug1L ND ug1L NO uglL 93 % 123 % 123 % 103 % 1.0 1 10/11/11 00:06 87-61-6 1.0 1 10/11/11 00-06 120-82-1 1.0 1 10111/1100.06 71-55-6 1.0 1 1011111100;06 79-DO-5 1.0 1 10/11/11 00-06 79-01-6 1.0 1 1011111100:06 75-69-4 1.D 1 1011111100;06 96-18-4 2.0 1 10/11/11 00:06 108-05-4 1,0 1 10/11/11 00:06 75-01-4 2.0 1 10/11/11 OD'06 179601-23-1 1.0 1 10111/1100-06 95-47-6 70-130 1 10111/1100:06 460-00-4 70-130 1 10/11/11 DD:06 1868-53-7 70-130 1 10/11/11 00:06 170W07-0 70-130 1 1011111100:06 2037-26-5 Sample: TRIP BLANK 3 Lab ID: 92103792013 Collected: 10/05/11 00:00 Received: 10/05/11 16:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Quaff 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane S rom od ich lorom etha ne Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobanzene Chloroethane Chloroform Chlorometheme 2-Chlorotofuene 4-Chlorotofuene 1,2-Dibromo-3-chloropropane Di bromoch lorometha n e 1,2-Dibromoethane (EDB) Dibromcmethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlo rod i fl uo ro metha ne 1,1-Dichloroethane 1,2-Dichloroethane Analytical Method: EPA 8260 ND ug1L 25,0 1 ND uglL 1.0 1 NO uglL 1.0 1 ND ug1L 1.0 1 ND ug1L 1.D 1 NO ug1L 1.0 1 N❑ ug1L 2.0 1 NO uglL 5.0 1 NO uglL 1.0 1 ND uglL 1.0 1 ND ug1L 1.0 1 ND ug1L 1.0 1 N❑ ug1L 1,0 1 NO uglL 1.0 1 ND uglL 1.0 1 NO uglL 5.0 1 ND uglL 1.0 1 ND uglL 1.0 1 ND uglL 1.0 1 NO ug1L 1,0 1 ND ug1L 1.0 1 ND ug)L 1.0 1 ND uglL 1,0 1 ND ug)L 1,0 1 NO uglL 1.0 1 1011111100:32 67-64-1 10/11/11 00:32 71-43-2 10/11/11 00:32 108-86-1 10/11/11 00:32 74-97-5 1011111100'32 75-27-4 10/11/11 0D:32 75-25-2 1011111100:32 74-83-9 1011111100:32 78-93-3 1011111100:32 56-23-5 10/11/11 00:32 108-90-7 1011111100:32 75-DO-3 1011111100,32 67-66-3 10/11/11 00:32 74-87-3 10/11/11 00-32 95-49-8 10/11/11 00:32 106-43-4 10/1111100.32 96-12-8 10111/11 00:32 124-48-1 10111 / 11 00: 32 106-9 3-4 10/1111100-32 74-95-3 1011111100:32 95-50-1 101110100:32 541-73-1 10/11/11 00:32 106-46-7 10/11/11 OD:32 75-71-8 10/1111100;32 75-34-3 10111/11 00:32 107-06-2 Date: 10114/2011 09:06AM REPORT DF LABORATORY ANALYSIS Page 32 of 67 This report shall not be reproduced, except In full, without the written consent cI Pace Analytical Services, Inc.. aceAnalXical smwrocelabs.com Projecl CMI WWTP Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Sulie A 2225 Rlversde Dr Eden, NC 27288 Asheville, NC 28804 (336)623.8921 (828)254.7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinoeyAve- Suite 100 Huntersville, NC 20078 Pace Project No.: 92103792 Sample: TRIP BLANK 3 Lair ID: 92103792013 Collected 10105/11 00 00 Received: 10105/11 16:35 Matrix Water (704)875-9092 Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 1,141ehloroethene ND ug1L 1.0 1 10/11/11 00,32 75-35-4 cis-1,2•Dichloroethene N❑ ug1L 1.❑ 1 1D111111 00:32 156-59-2 trans-1,2-Dichloroethene ND ug1L 1.0 1 10/11/11 00:32 156-60-5 1,2-Dichloropropane ND ug1L 1.0 1 101i1111 00:32 78-87-5 1,3-Dichloropropane NO ug1L 1.0 1 i0111111 00:32 142-28-9 2,2-Dichioropropane ND uglL 1.0 1 10/11111 00:32 594-20-7 1,1-Dichloropropene ND uglL 1.0 1 10111/11 00:32 563-58-6 cis-1,3-Dichloropropene ND uglL 1.0 1 10/11/11 00:32 1D061.01.5 trans- l,3-Dichloropropene ND uglL 1.0 1 i(W11111 00:32 ID061-02-6 Diisopropyl ether NO ug& 1.0 1 101i1111 00.32 108-20-3 Ethylbenzene NO uglL 1.0 1 10/11111 00:32 100-41.4 Hexachloro-1,3-butadiene ND uglL 1.0 1 UN11111 00:32 87-68-3 2-Hexanone NO uglL 5.0 1 10/11/11 00.32 591-78-6 p-Isopropyltoluene N❑ uglL 1.0 1 10/11/11 00:32 99.87-6 Methylene Chloride NO ug)L 2,0 1 10/11/11 00:32 75-09-2 4-Mclhyl-2-pentanone(MIBK) ND uglL 5.0 1 10/1111100;32 108-1D-1 Methyl-tert-butyl ether NO uglL 1.0 1 10/11/11 00:32 1634-04-4 Naphthalene NO ug)L 1.0 1 10/11/11 00:32 91-2D-3 Styrene ND ug)L 1.0 1 10/11111 00.32 1OD-42-5 1,1,1.2-Telrachlor(>e1hane ND uglL 1.0 1 10/11/11 00:32 530-20-6 1,1,2,2-Tetrachloroethane ND ug1L 1.0 1 10)11/11 00:32 79-34-5 Tetrachloroethene NO uglL 1.0 1 10/11/11 00:32 127-16-4 Toluene ND ug1L 1.0 1 10/11/11 00,32 108-88-3 1,2,3-Trichiorobenzene NO ug1L 1.0 1 10/11/11 00:32 87-61-6 1,2A-Trichiorobenzene NO uglL 1.0 1 10111/11 00:32 120-82-1 1,1,1-Trichloroethane NO uglL 1.0 1 10/11/11 D0:32 71-55-6 1,1,2•Trichloroethane ND ug1L 1,0 1 10/11/11 00:32 79-00-5 Trichloroethene ND ug1L 1.0 1 10/11111 00:32 79-01-6 Trichlorofluoromethane ND uglL 1.0 1 10/11/11 00:32 75-69-4 1,2,3-Trichlompropane ND ug1L 1.0 1 10111/11 00:32 96-18.4 Vinyl acetate ND ug1L 2.0 1 10/11/11 00:32 108-05-4 Vinyl chloride NO ug1L 1.0 1 10/11/11 00:32 75.01-4 m&p-Xylene ND ug1L 2.0 1 10/11/11 00:32 179601-23-1 o-Xylene NO uglL 1.0 1 10/11/11 00:32 95-47-6 4-Bromofluoroben7ene (S) 94 % 70-130 1 10/11/11 00:32 4604ff0-4 Dibromailuoromethane (S) 127 % 70-130 1 10/11111 00:32 1868-53-7 1,2-Dichloroethane-d4 (S) 128 % 70-130 1 10/11/11 00,32 17060-07.0 Toluene-d8 (S) 102 % 70-130 1 10111111 00,32 2037-26-5 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 33 of 67 This report shall not be reproduced, except in Full, without the written consent of Pace Analytical Services, Inc.. aceAnalAcal wmr.pacefa8s.conr Pace Analytical Services, Inc. 205 East Meadow Road - SuiteA Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DUALITY CONTROL DATA Project: CMI WWTP Pare Project No.: 92103792 QC Batch: AIR113315 Analysis Method: RSK 175 QC Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE Associated Lab Samples: 92103792005, 92103792007, 92103792008 METHOD BLANK: 1070993 Matrix- Water Associated Lab Samples: 92103792005, 92103792007, 92103792008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethane uglL ND 10.0 1011011109:53 Ethene uglL ND 10.0 10/1011109:53 Methane uglL N❑ 10.0 10110/1109:53 Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE & LCSD; 1070994 1070995 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc, Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethane uglL 114 114 118 100 104 70-130 4 30 Ethene ug1L 106 108 112 102 105 70-130 3 30 Methane uglL 60.7 64.9 65.8 107 108 70-130 1 30 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1072836 1072837 M5 MSD 10171803003 Spike Spike MS MSD M5 MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Ethane ug/L NO 103 108 120 127 116 118 30-150 6 Ethene uglL NO 96.4 101 107 112 111 111 30-150 5 Methane ug/L 1.2 55.1 57.8 5490 5470 7780 7390 30-150 A P6 mg/L SAMPLE DUPLICATE: 1072747 Parameter Ethane Ethene Methane 92103883010 Dup Units Result Result ug/L 12.5 10.9 uglL ND N❑ ug1L 12000 10100 RPD Qualifiers 14 17 E Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 34 of 67 This report shall not be reproduced, except in full, without the written consent or Pace Analytical Sarvica5, Inc.. y Pace Analytical Services, Inc, Pace Analytical Services, Inc. Pace Analytical Services, Inc. 17a'ceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 KImey Ave. Suite 100 nww.Fa�efa6s.cam Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: CMI WWTP Pace Project No.: 92103792 QC Batch: AIR113316 Analysis Method: RSK 175 OC Batch Method: RSK 175 Analysis Description: RSK 175 At HEADS PACE Associated Lab Samples: 92103792001, 92103792002 METHOD BLANK: 1071005 Matrix: Water Associated Lab Samples: 92103792001, 92103792002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethane uglL NO 10.0 10110/1115:12 Ethene ug/L ND 10.0 10110/1115:12 Methane ugA_ ND 10.0 1011011115,12 LABORATORY CONTROL SAMPLE & LCSD: 1071006 1071D07 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Quallfiers Ethane ug1L 114 118 124 104 109 70-130 5 30 Ethene ug/L 106 112 116 105 109 70-130 4 30 Methane ug1L 60.7 65.8 65.2 108 107 70-130 .9 30 SAMPLE DUPLICATE: 1073335 10171803004 Dup Parameter Units Result Result RPD Qualifiers Ethane ug/L NO ND Ethene uglL ND ND Methane ug1L 0.16 mg/L 102 46 R1 SAMPLE DUPLICATE: 1073337 92103909001 Dup Parameter Units Result Result RPD Qualifiers Ethane ug1L NO NO Ethene ug1L NO NO Methane ug/L ND NO Dale: 10/14/2011 09.06AM REPORT OF LABORATORY ANALYSIS Page 35 of 67 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. 1:;5'ceAnaljdical'�' wwparefehs.cam i Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 2 72 88 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside ❑r. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project. CMl WWTP Pace Project No.: 92103792 OC Balch: AIR113317 Analysis Method; RSK 175 QG Batch Method: RSK 175 Analysis Description: RSK 175 AIR HEADSPACE Associated Lab Samples: 92103792003, 92103792004, 92103792006, 92103792009 METHOD BLANK: 1071009 Matrix: Water Associated Lab Samples: 92103792003, 92103792004, 92103792006, 92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethane ug/L NO 10.0 1011111109:30 Ethene ug)L NO 10.0 10/11111 09:30 Methane ug1L NO 10.0 10111/1109:30 Pace Analytical ServFces, Inc, 9800 Kinsey Ave. Suile 10o Huntersvilte, NC 28078 (7D4)875-9092 LABORATORY CONTROL SAMPLE & LCSD; 1071010 1071011 Spike LCS LCS❑ LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Ethane ug/L 114 99.7 122 88 108 70-130 21 30 Ethene ug1L 106 92.4 115 87 108 70-130 22 30 Methane uglL 60.7 57.1 65.6 94 108 70.130 14 30 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1073565 MS MSD 5053524003 Spike Spike Parameter Units Result Conc, Conc, 1073566 MS Result MSD Result MS MSD % Rec % Rec % Rec Limits RPD Qual Ethane ug1L NO 114 120 112 104 99 87 30-150 7 Ethene ug1L NO 106 112 106 100 100 90 30-150 6 Methane ug1L NO 60.7 618 65.0 56-0 97 78 30-150 15 SAMPLE DUPLICATE: 1073567 92103947001 pup Parameter units Result Result RPD Qualifiers Ethane ug1L NO ND Ethene ug1L NO ND Methane ug1L 29,9 23.4 24 Date: 1011412011 09 06 AM REPORT OF LABORATORY ANALYSIS Page 36 of 67 Thls report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ace Ana 1picaI • titiww.wrcfahs.Com Project. CMl WVYTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Sidle A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc, 2225 Riverside ❑r, Asheville, INC 28804 (828)254.7176 QUALITY CONTROL DATA QC Batch. MPRP19159 Analysis Method; EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associaled Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005 METHOD BLANK: 669016 Matrix: Water Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005 Blank Reporting Parameter Units Resull Limit Analyzed Calcium ug1L NO 100 10/08/11 00:44 Manganese ug1L NO 5.0 10/0811100:44 LABORATORY CONTROL SAMPLE: 669017 Qualifiers Pace Analytical Services, Inc. 9800 KinceyAve . Suite 100 Huntersvilte, NC 28078 (704)875-9092 Spike LCS LCS % Ree Parameter Units Cane. Result % Rec Limits Qualifiers Calcium uglL 5000 5080 102 80-120 Manganese ug1L 500 488 98 80-120 MATRIX SPIKE SAMPLE: Parameter 669018 Units 92103587001 Result Spike Cone. MS MS Result % Rec % Rec Limits Qualifiers Calcium ug1L 156000 5000 167000 216 75-125 M6 Manganese uglL 2690 500 3190 99 75-125 SAMPLE DUPLICATE: 669019 92103587002 ❑up Parameter Units Result Result RPD Qualifiers Calcium uglL 401000 394000 2 Manganese ugJL 453 447 1 Date: 10114/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 37 of67 This report shall not be reproduced, except in full. without the written consent or Pace Analytical Services, tnc.. lacieAnalytical "W,pacews. WM Project: CM WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)62"921 Pace Analytical SerWces, Ine. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800KinceyAve . Suite 100 Hunlersviile, NC 28078 {704)875-9092 OC Batch: MPRP19166 Analysis Method: EPA 6010 OC Batch Method: EPA 3010 Analysts Description: 6010 MET Associated Lab Samples: 92103792006, 92103792007, 92103792D08, 92103792009 METHOD BLANK: 669296 Matrix: Water Associated Lab Samples: 92103792006, 92103792007, 92103792008, 92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Calcium uglL ND 100 10112/1100:31 Manganese uglL N❑ 5.0 10112/1100-.31 LABORATORY CONTROL SAMPLE: 669297 Spike LGS LGS °I° Rec Parameter Units Conc. Result % Rec Limits Qualifiers Calcium uglL 5000 5220 104 80-120 Manganese ug)L 500 496 99 80-120 MATRIX SPIKE SAMPLE; Parameter 669298 Units 9210379200E Result Spike Conc. MS MS Resul! % Rec % Rec Limits Qualifiers Calcium ug1L 41500 5000 45100 72 75-125 M1 Manganese ug1L 7000 500 7170 33 75-125 M1 SAMPLE DUPLICATE: 669299 92103792007 Dup Parameter Units Result Result RPD Qualifiers Calcium uglL 71000 70500 1 Manganese ug1L 8340 8240 1 Date: 10/14/2011 09:06AM REPORT OR LABORATORY ANALYSIS Page 38 of 67 This report shall not be reproduced, exeept in full, without the written consent or Pace Analytical Services, Inc.. i aceAnalytical www. pacefabs-m n Project. CM1 WWTP Pace Project No.: 921C3792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc, 2225 Riverside ❑r. AshevKe, NC 26804 (828)254-7179 QUALITY CONTROL DATA OC Batch- MSVIIBP14 Analysis Method: OC Batch Method: EPA 8260 Analysis Description: Associated Lab Samples- 92103792001. 92103792010 EPA 8260 8260 MSV Low Level METHOD BLANK- 670089 Matrix: Water Associated Lab Samples: 9210379200i, 92103792010 Blank Reporting Parameter Units Result Limit Analyzed 1.1,1.2-Tetrachloroethane ug1L N❑ 1.0 1011011113.00 1, 1, 1 -Trichto roethan a ug1L ND 1.0 10110/1113:00 1,1,2,2-Teirachloroethane uglL N❑ 1.0 10fi o111 13:00 1,1,2-Trichloroethane uglL N❑ 1.0 10/10/1113:00 1,1-Dichloroethane uglL ND 1-0 1011011113100 1,1-Dichloroett'ene ug1L ND 1.0 1011011113:00 1,1-❑ichloropropene ug1L N❑ 1.0 1G11D11113:00 1,2,3-Trichlorobenzene ugf- ND 1.0 1011011113:00 1,2,3-Trichloropropane ug1L ND 1.0 1011011113:00 1,2,4-Trichlorobenzene uglL ND 1.0 10110/1113:00 1,2-Dibromo-3-chloropropane uglL ND 5.0 10110/1113:00 1,2-Dibromoethane (EDB) ug1L ND 1.0 10/10/11 13:00 1,2-Dichlorobenzene ugll_ ND 1,0 10/1011113,00 1,2-Dichioroethan e ug& ND 1.0 10/1011113:00 1,2-Dichloropropane uglL ND 1.0 10110/1113:00 1,3-Dichlorobenzene uglL ND 1.0 1011011113:00 1,3•Dichloropropane ug1L ND 1.0 1011011113:00 1,4-Dichlorobenzene uglL ND 1.0 1011011113:00 2,2-DichlDropropane uglL ND 1.0 1011011113:00 2-Butanone (MEK) uglL ND 5.0 10/10111 13:00 2-Chlorotoluene ug1L ND 1.0 113110/1113:00 2-Hexanone ug1L ND 5.0 1011011113:00 4-Chlorotoluene uglL ND 1.0 10/10/1113:00 4•Methyl•2•pentanone (MIRK) ug1L ND 5-0 i0110/11 13:00 Acetone uglL ND 25.0 10/1011113:00 Benzene ug1L ND 1.0 1Oil 0/1113-00 Bromobenzene ug1L ND 1.0 10110/1113:00 Bromachloromethane ug1L ND 1.0 1D11011113:00 Bromodichloromethane ug1L ND 1.0 10/10/1113:00 Bromoform uglL ND 1.0 10110/1111-00 Bromomethane uglL ND 2Z 10/1011113:00 Carbon tetrachloride ug1L ND 1.0 10/10/11 13:00 Chlorobenzene ug1L ND 1.0 1oil D11113-DO Chloroethane ug1L ND 1.0 1011011113:00 Chloroform uglL ND 1.0 1011011113:00 Chloromethane ug1L ND 1.0 1011011113:00 ds•1,2-Dichloroethene uglL ND 1.0 1011011113:00 cis-1,3-Dichloropropene ug1L ND 1.0 1011011113:00 Dibromochlorometharie ug1L ND 1.0 1011011113:00 Dibromomethane ug1L ND 1.0 10/1011113:00 Dichlorodifluoromelhane ug1L ND 1.0 1011011113:00 Diisopropyl ether ug1L ND 1.0 10/10111 13:00 Ethylbenzene ug1L ND 1.0 1Oil (VI 113:00 Date: 101141201109:06AM REPORT OF LARORATORYANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Pace Analytical Services, Inc. 9800 Ifincey Ave. Suile 100 Huntersville, NC 28078 (704)875.9092 Page 39 of 67 aceAnalyllcalr www.pacefabs.mm Pace Analytical Services. Inc. Pace Analytical Services, Inc 205 East Meadow Road - Stifle A 2225 Riverside Or Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254.7176 QUALITY CONTROL DATA Project: CMI WWTP Pace Project No.: 92103792 METHOD BLANK: 670089 Matrix: Water Associated Lab Samples: 921 D3792001, 92103792010 Blank Reporting Parameter Units Result Limit Analyzed Hexachloro-1,3-butadiene ug1L NO 1.0 1011011113:00 m&p-Xylene ug1L ND 2.0 10/1011113:00 Methyl-tert-butyl ether ug1L NO 1.0 10/10/11 13:00 Methylene Chloride ug1L ND 2.0 10/10/11 13:00 Naphthalene ug1L ND 1.0 10/1011113:00 o-Xylene ug1L ND 1.0 10/1011113:00 p-lsopropylioluene ug1L ND 1.0 10/10/11 13:00 Styrene uglL N❑ 1.0 1011011113:00 Tetrachloroethene ug1L ND 1.0 10/10/1113:0 Toluene ug1L ND 1.0 1011011113:00 trans- 1,2-0ichloroethene uglL ND 1.0 10/10/11 13:00 trans-1,30chloropropene u91L ND 1,0 10/10/11 13:00 Trichloraethene ug1L ND 1.0 10110/1113:00 Trichicrofluoromethane uglL ND 1.0 10110/1113:00 Mnyl acetate uglL ND 2,0 10N D111 13:00 Vinyl chloride uglL ND 1.0 10/10/11 13:00 1,2-Dichloroethane-d4 (S) % 118 7D-130 10/10/11 11100 4-Bromoftuorobenzene (S) % 95 7D-130 10/10111 13:00 Dibromofluaromettlane (5) % 1i6 7D-130 10/10111 13:00 Toluene-d8 (S) % 102 70-130 10/10/11 13:00 LABORATORY CONTROL SAMPLE: 670090 Qualifiers Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersviile. NC 28078 Parameter Units Spike Conc. LCS Result LC5 % Rec % Rec Limits Qualifiers 1,1,1.2-Tetrachloroethane ug1L 50 53.4 107 70-130 1.1.1 Trichloroethane ug1L 50 45.5 91 70.130 1.1.2,2-Tetrachloroethane ug1L 50 61.9 104 70.130 1,1,2-Trichloroethane ug1L 50 51.2 1D2 70-130 1,1-Dichioroethane ug1L 50 44.7 89 70-130 1,1-Dichioroethene ug1L 50 45.5 91 70-132 1,1-Dichloropropene ug1L 50 47.5 95 70-130 1,2,3-Trichlorobenzene uglL 50 47.9 96 70-135 1,2.3-Trichiaropropane ug1L 50 50.6 101 70-130 1,2,4-Trichlarobenzene ug1L 50 47.0 94 70-134 1,2-Dibromo-3-chloropropane uglL 50 53.5 107 70-130 1,2-Dibromoethane (EDB) uglL 50 53.7 107 70-130 1,2-Dichlorobenzene ug1L 50 50.5 101 70-130 1,2-Dichiaroethane uglL 50 51.2 102 70-130 1,2-Dichloropropane ug1L 50 53.0 106 70-130 1,3-Dichlorobenzene ug1L 50 50.1 100 70-130 1,3-Dichloropropane ug1L 50 516 107 70.130 1,4-Dichiorobenzene ug1L 50 47.4 95 70-130 2,2-Dichloropropane uglL 50 48.3 97 58-145 2-Butanone (MEK) ug1L 100 116 116 70-145 2-Chlorotoluene ug1L 50 513 103 70-130 Date: 1D114/2011 09:06AM REPORT OF LABORATORYANALYSjS This report shall not he reproduced, eXcept in full, wqhout the written consenT of Pace AnalylicaI Services, Inc.. (704)875-9092 Page 40 of 67 aceAnalyfical W%W-paC9�ab4. C4 7M Project CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (335)623-8921 Pace Analytical Services, Inc. 2225 Riverside Or. Ashevilie, NC 28804 (828)254.7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 HinceyAve. SuiSe 10e Honterwille, NC 28078 (7D4)875-9092 LABORATORY CONTROL SAMPLE. Parameter 670090 Units Spike Conc. LCS Result LCS In Rec % Rec Llmils Qualifiers 2-Hexanone ug/L 100 102 102 70-144 4-Chlorotoluene ug/L 50 53.6 107 70-130 4-Methyl-2-pentanone (MIRK) ug/L 100 102 102 70.140 Acetone ug1L 100 127 127 50-175 Benzene uglL 50 43.2 86 70-130 Bromobenzerle iiglL 50 48.7 97 70-130 Bromochloromethane uglL 50 47.9 96 70.130 6romodichloromethane ugIL 50 51.9 104 70-130 Bromoform uglL 50 47.8 96 70-130 Bromomelhane uglL 50 19.7 39 54-130 LO Carbon tetrachloride uglL 50 48.6 97 70-132 Chlorobenzene uglL 50 49.2 98 70.130 Chioroelhane uglL 56 46.0 92 64-134 Chloroform uglL 50 55.5 Ill 70.130 Chloromethane UgIL 50 55.1 110 64-130 cis- 1,2-Dichloroelhene ug1L 50 43.7 87 70-131 cis•1,3•Dichloropropene ug/L 50 51.1 102 70-130 ❑lhromochloromethane ug1L 50 54.0 108 70-130 ❑ibromomelhane ug/L 50 52.3 105 70-131 Dichlorodlffuoromelhane ug/L 50 64.6 129 56-130 ❑iisopropyl ether ug1L 50 47.6 95 70.130 Ethylbenzene ug1L 50 51.4 103 M130 Hexachtoro-1,3-butad iene ug/L 50 49.8 1O0 70.130 m&p-Xylene ug1L 100 106 106 70-130 Methyl-tert-butyl ether ugIL 50 51.1 102 70-130 Methylene Chloride ug/L 50 52.9 106 53-130 Naphthalene ug/L 50 49.9 100 70-138 o-xylene ug1L 50 48.4 97 70-130 pAsopropyltoluene ug/L 50 48A 96 70.130 Styrene ugIL 50 49.3 99 70-130 Tetrachlaroethene ugIL 50 49.6 99 70-130 Toluene uglL 50 50.3 101 70-130 trans- 1.2-Dichloroethene ug1L 50 44.4 89 70-130 trans- 1,3-Dichioropropene ugIL 50 50.5 101 70-132 Trichtoroethene ug/L 50 54.2 108 70-130 Trichiorafluoromelhane ug/L 50 54.3 109 62-133 Vinyl acetate ug/L 100 92.1 92 66-157 Vinyl chloride ug1L 50 53.9 108 69-130 1,2-Dichloroethane-d4 (S) % 96 70-130 4-Bromofluorobenzene (S) °% 102 70-130 Dibromolluoromethane (S) % 94 70-130 Toluene -dB (S) % 99 70-130 Dale, 10/14/2011 W06 AM REPORT ❑F LABORATORY ANALYSIS Page 41 of 67 Thls report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, Inc.. /72eAnalytical" n'n'wpacelahs.cam Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, lnc 2225 Rivers lde Dr Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 1(incey Ave. Suite 100 Huntersville. NC 28078 t704)875.9092 Project: CMI WWTP Pace Project No.: 92103792 MATRIX SPIKE & MATRIX SPIKE DUPLICATE- 670091 670092 MS MSD 92103399016 Spike Spike MS MSD MS MSD °% Rec Parameter Units Result Cone, Cone. Result Result % Rec °% Rec Limits RPD Qual 1,1-Dichloroethene ug/L 21.2 50 50 63.7 64.1 85 86 70-166 1 Benzene uglL ND 50 50 53.9 55.3 108 111 70-148 3 Chlorohenzene ug/L ND 50 50 60.1 61.8 120 124 70-146 3 Toluene uglL ND 50 50 55.9 57.1 112 114 70-155 2 Trichloroethene ug1L ND 50 50 50.6 51.2 101 102 69-151 1 1,2-Dichloroethane-d4 (S) % 119 118 70-130 4-Bromotluorobenzene (S) °% 94 96 70-130 Dibromoiluoromethane (S) °% 113 112 70-130 Toluene-cI8 (S) % 89 90 70-130 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 42 of 67 This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 1!;a'ceAnalyfical' wnw.Aacefahs.cwn Project: CMI WWTP Pace Project No.. 92103792 Paco Analytica! Services, Inc. Pace Analytical Services, Inc. 205 East Meadow (toad - Suite A 2225 Riverside Dr Eden. INC 27288 Asheville, NC 28804 (336)623.8921 1828j254-7176 QUALITY CONTROL DATA OC Balch: MSVI16917 Analysis Method; EPA 8260 OC Batch Method: EPA 8260 Analysis Descrtption: 8260 MSV Low Level Associated Lab Samples. 92103792003, 92103792D11, 92103792012, 921D3792013 METHOD BLANK: 670245 Matrix Water Associated Lab Samples: 92103792003, 921D3792011, 92103792012, 92iD3792013 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.6 1011011123:15 1,1,1-Trichlorcethane uglL ND 1.0 10110/112115 1,1.2.2-Tetrachloroelhane uglL ND 1.0 10/1011123.15 1,12-Trichloroethane ugIL ND 1-0 1011011123:15 1,1-Dichloroethane ugIL ND 1,0 1D11D11123:15 1,1-Dichloroethene ug)L ND 1.0 10110/1123:15 1,1-Dichloropropane ug)L ND 1-0 1011011123:15 1,2,3-Tfichlorobenzene ug/L NO 1.0 1D110/1123.15 1,2,3-Trichioropropane ug/L NO 1.0 10110/1123:15 1,244-Trichlorobenzene u91 ND 1-0 10/10/1123:15 1,2-0ibromo-3-chloropropane ug1L NO &0 10/1011123-15 1,2•Dibromoethane (EDBj ug1L ND 1.0 10/10/11 23:15 1,2-0ichlorobenzene ugIL NO 1.0 10110/1123:15 1,2-Dichloroethane ug1L NO 1.0 10110/1123:15 1,2-Dichloropropane ug1L NO 1.0 1011011123:15 1,3-Dichlorobenzene ug1L N❑ 1.0 10110/1123-15 1,3-Dichloropropane ug/L ND 1.0 1011011123:15 1,4-Dichlorobenzene ugIL NO 1.0 1011011123:15 2,2-Dichloropropane ug/L N❑ 1.6 10/1011123-15 2•Sutanone (MEK) ug1L ND 5.0 10/10/11 23:15 2-Chlorotoluene ugIL NO 1.0 10/1011123:15 2-Hexanone ugIL N❑ 5.0 1011011123,15 4-Chlorotoluene ugIL N❑ 1.0 1011011123:15 4-Methyl-2-pentanone (MIBK) ug)L ND 5.0 10/10/11 23:15 Acetone ugll- ND 25.0 10/1011123:15 Benzene ug)L ND 1.0 1011011123:15 Bromobenzene ug)L N❑ 1.0 1011011123:15 Bromochloromethane uglL ND 1.0 10/1011123:15 Bromadichloromelhane uglL ND 1.0 1011011123:15 Bromoform uglL ND 1.0 1011011123:15 Bromomethane ugIL ND 2.0 1011011123:15 Carbon tetrachloride ug)L ND 1.0 10/10/11 23:15 Chlorobenzene ug1L NO 1.0 1011011123715 Chloroalhane uglL ND 1.0 1011011123:15 Chloroform ugIL ND 1.0 10/10/1123:15 Chloromethane ug/L NO 1.0 1011011123:15 cis-1.2-Dichloroethene ugIL N❑ 1.0 10110/1123:15 cis•i,3•Dichloroprvpene ug1L ND 1.0 1011011123:15 Dibromochloromethane ug1L NO 1.0 10/10/1123.15 Dibromomethane ug1L N❑ 1.0 1011011123-15 Dichlorodifiuoromethane ugIL NO 1.0 101101112315 Diisopropyl ether ug/L ND 1.0 10110/11 23:15 Elhylbenzene ug1L ND 1.0 10110/1123:15 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Pace Analytical Services, Inc 9800 Kincey Ave. Suite 100 Huntersville, INC 28076 {704)875.9052 Page 43 of 87 11eAnalyfical" wtinv.paealaDxram Project. CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, tnc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA METHOD BLANK: 670246 Associated Lab Samples: Parameter Matrix- Water 92103792003, 92103792011, 92103792012, 92103792013 Blank Reporting Units Result Limit Analyzed Hexachloro-1,3-butadiene uglL NO 1.0 10/10/112315 m&p-Xylene ug1L ND 2.0 10/1011123:15 Methyl-tert-butyl ether ug1L NO 1.0 10/10/11 23:15 Methylene Chloride ug1L NO 2.0 10/10111 23:15 Naphthalene ug1L ND 1.0 101101112V5 o-Xylene uglL NO 1.0 10/1011123:15 p-Isopropyltoluene ug/L NO 1.0 101101112115 Styrene ug/L NO 1.0 1011011123:15 Tetrachloroethene uglL NO 1.0 1011011123:15 Toluene uglL NO 1.0 1011011123:15 trans-1,2-Dichloraethene uglL NO 1.0 1011011123:15 trans-1,3-Dichloropropene uglL NO 1.0 1011011123:15 Trichloroethene uglL ND 1.0 10110/1123:15 Trichforofluoromethane uglL N❑ 1.0 10/1011123:15 Vinyl acetate uglL ND 2.0 1011011123:15 Vinyl chloride uglL ND 11.0 10/10/11 23:15 1,2-Dichloroethane-d4 (S) % 123 70-130 1011011123:15 4-Sromofluorobenzene (S) % 94 70-130 10/10/11 23:15 Dibromofluoromethane (S) % 123 70-130 10/10/11 23:15 Toluene -dB (S) % 100 70-130 10110/11 23:15 Qualifiers LABORATORY CONTROL SAMPLE; Parameter 670247 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane uglL 50 53.2 106 70-130 1,1,1-Trichloroethane ugll- 50 46.4 93 70-130 1,122-Tetrachloroethane uglL 50 53.9 108 70-130 1,1,2-T0chloroethane ug1L 50 53.4 107 70-130 141-Dichloroethane uglL 50 46A 93 70-130 141-Dichloroe1hene uglL 50 47.6 95 70-132 1,1-Dichloropropene uglL 50 49A 98 70-130 1,2,3-Trichlorobenzene ugll- 50 48.6 97 70-135 1.2,3-Trichloropropane ug/L 50 52.3 105 70-130 1,2,4-Trichlorobenzene ug1L 50 46.1 92 70-134 12-01bromo-3-chloropropane ugll- 50 53.6 107 70-130 1,2-❑ibromaethane (EDB) ug/L 50 54.5 109 70-130 1,2-Dichlorobenzene uglL 50 51.3 103 70-130 1.2-1)ichloroethane uglL 50 54.3 109 70-130 1,2-Dichloropropane uglL 50 55A 110 70-130 1,3-Dichlorobenzene uglL 50 50.3 101 70-130 1,3-Dichloropropane uglL 50 54.5 109 70-130 1.4-Dichlarobenzene ug/L 50 47.9 96 70-130 2,2-Dichloropropane uglL 50 40_5 81 58-145 2-Butanone (MEK) uglL 100 129 129 70-145 2-Chlorotoluene uglL 50 5i,9 iO4 70-130 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Ana lyticaI Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suile 100 Hunlersville, NC 28078 (704$75-9092 Qualifiers Page 44 of 67 ;ac e Ana Ij / tica / " wwwv.paceiabs.ra-i Project. CMI WVVTP Pace Project No.: 92103792 PaceAnaiylical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)823.8921 Pace Analytical Services, Inc- 2 225 Riverside dr. Asheytne, NC 28804 (828)254.7176 QUALITY CONTROL DATA Pace AnalyIIca I Services. Inc. 9800 KlnceyAye Suite 100 Huntersville, NC 28078 t704y875-9092 LABORATORY CONTROL SAMPLE: Parameter 670247 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Hexanone uglL 100 99.5 100 70-144 4-Chlorotoluene uglL 50 54.3 109 70-130 4-Methyl-2-pentanone (MIBK) uglL 100 104 104 70-140 Acetone uglL 100 115 115 50-175 Benzene uglL 50 44.6 89 70-130 Bromobenzene uglL 50 49.7 99 70.130 Bromochtoromethane uglL 50 50.5 101 70-130 Bramodichloromethane uglL 50 53.0 106 70-130 Bromoform ug]L 50 47.0 94 70-130 Bromomethane ug/L 50 23.1 46 54-1301C,L0 Carbon tetrachloride ug/L 50 48.8 98 70-132 Chlarobenzene ug1L 5o 50.1 100 70-130 Chloroethane ug(L 50 51.2 102 64-134 Chloroform ugfL 5o 57.7 115 70-130 Chloromethane ug& 50 58.6 117 64-130 cis-1,2-Dichloreethene uglL 50 45.9 92 70-131 cis- 1,3-Dichloroproper e ugIL 50 49.8 100 70-130 Dibromochloromethane uglL 50 53.3 107 70-130 Dibromomethane uglL 50 53.0 106 70-131 Dichlorodifluoromethane uglL 50 64.1 128 56-130 Diisapropyl ether ug)L 50 48.0 96 70-130 Ethyibenzene uglL 50 52.8 106 70-130 Hexachloro-1,3-butad iene ug)L 50 47.6 95 70.130 m8p-Xylene uglL 100 111 111 70-130 Methyl-tert-butyl ether ug1L 50 51.0 102 70-130 Methylene Chloride ug1L 50 56A 113 03-130 Naphthalene uglL 50 50.8 102 70-138 o-xylene uglL 50 49.4 99 70-130 p-IsopropyltolUene ugll- 50 47.5 95 70-130 Styrene uglL 50 50.5 101 70-130 Tetrachloroethene uglL 50 48.7 97 70-130 Toluene uglL 50 52A 105 70.130 trans-1,2-Dichloroethene uglL 50 47.0 94 70-130 trans-1,3-Dichloropropene uglL 50 49.3 99 70-132 Trichloroeihene ug1L 5o 55.8 112 70-130 TrichlorofEuoromethane uglL 50 55.3 t11 62-133 Vinyl acetate uglL 1Dt1 90.9 91 66-157 Vinyl chbride uglL 50 56.9 114 69-130 1,2•Dichloroefhane-d4 (S) % 98 70-130 4-Bromaflucrobenzene (S) % 99 70-130 Dibromofluoromethane (S) % 95 70-130 Toluene-d8 (S) % 99 70-130 Date: 10/14/2011 MMAM REPORT OF LABORATORY ANALYSIS Page 45 of 67 This report shall not he reproduced. except in full, wit}tout the written consent of Pace Analytical Services, Inc iceAnalytical" "Wpacelahs.mm Project: CMI WWTP Pace Project No.: 92103792 Pace Analylical Services, Inc. 205 East Meadow Road - SuiteA Eden, NC 27288 (336)623.8921 Pace Analytical Services, Inc. 2 22 5 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KlnceyAve . Suite 100 Huntersyllle, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 670248 610249 MS MSD 92103792003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Quaff 1,1-0ichloroethene ugJL 1.0 50 50 66.2 64.4 130 127 70-166 3 Benzene uglL NO 50 50 48.0 48.2 96 96 70-148 0 Chlorobenzene uglL NO 50 50 55.0 54.2 110 108 70-146 1 Toluene uglL NO 50 50 57.5 56.5 115 113 70-155 2 Trichloroethene uglL NO 50 50 49.7 48.3 99 97 69-151 3 1,2-DichIcroethane-d4 (S) % 118 120 70-130 4-Bromonuorobenzene (S) % 90 91 70-130 Dibromofluoromethane (S) % 116 118 70-130 Toluene-d8 (S) % 93 92 70-130 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 46 of 67 This report shall not he reproduced, except in Full, without the written consent of Pace Analytical Services, Inc.. e /A ? mAnalytrcal � n�+w.p8cC18A9-Cam Project CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27268 1336j623-0921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 I828)254-7176 QUALITY CONTROL DATA QC Batch: MSV116929 Analysls Method: EPA 8260 OC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 921037920D9 METHOD BLANK: 670724 Associated Lab Samples: 92103792009 Parameter Matrix: Water Blank Reporting Units Result Limit Analyzed 1.1.1,2-TetracNoroe lhane ug1L ND 1.0 10110/1122:43 1,1,1-Trichloroethana ug1L N❑ 1,0 101101112243 1,1,2,2-Tetrachloroethane ug1L ND 1.0 1011011122,43 1.1,2Trichloroethane ug1L ND 1.0 10/10/1122:43 1,1•Dlchloroethane ug1L ND 1,0 1011011122:43 1,1-Dlchloroethene ug1L ND 1.0 10/1011122743 1,1-Dichloropropene ug1L ND 1.0 1011011122:43 1,2,3-Trichlorobenzene u911- ND 1,0 10110/1122:43 142,3-Trichloropropane uglL N❑ 1.0 10110/1122:43 1,2,4-Trichlorobenzene uglL ND 1.0 1011011122:43 1,2-1)14romo-3-chforopropane uglL ND 5,0 1011011122:43 1,2-Dibromoethane (EDB) ug1L ND 1.0 10/10/11 22:43 1,2-Dichlorobenzene ug1L ND 1.0 1011011122:43 1,2-Dichloroethan e uglL ND 1,0 10/1011122:43 1,2-Dichloropropane uglL ND 1.0 10110/1122:43 1,3-Dichlorobenzene uglL ND 1.0 1011011122-43 1,3-Dichloropropane uglL ND 1.0 1011011122:43 1,4-Dichlorobenzene uglL ND 1.0 1011011122:43 2,2-Dichloropropane ugll_ ND 1.0 10/1011122:43 2-Bulanone (MEK) uglL ND 5.0 10/10/11 22:43 2•Chlorotoluene uglL ND 1.0 1011011122:43 2-Hexanone uglL ND 5.0 1WI011122:43 4-Chlorotoluene ug/L ND 1,0 10/1011122:43 4-Methyl-2-pentanone (MIRK) ug1L ND 5.0 10/10/11 22:43 Acetone ug1L N❑ 25.0 1011011122:43 Benzene uglL ND 1.0 1011011122,43 Bromobenzene ug1L ND 1.0 1011011122:43 Bromochloromethane ug1L ND 1.0 1011011122:43 Bromodichloromethane ug1L N❑ 1.0 1011011122:43 Bromoform ug1L ND 1.0 1011011122:43 Bromomethane uglL ND 2.0 10/1011122:43 Carbon tetrachloride ug1L N❑ 1.0 10/10/11 22:43 Chlorobenzene uglL ND 1.0 10110/1122:43 Chloroethane uglL ND 1.0 10/1011122:43 Chloroform ug1L N❑ 1.0 10/10/1122-.43 Chloromethane uglL N❑ 1.0 10/1011122:43 cis-1.2-Dichloroelhene u91L ND 1.0 1011011122:43 cis- 1,3-Dichloropropene uglL ND 1.0 10/1011122:43 Dibromochloromethane u911. ND 1.0 10/1011122:43 Dibromomethane ug1L N❑ 1.0 1011011122:43 Dichlorodifiuoromelhane uglL ND 1.0 10/1011122-43 Diisopropyl ether uglL ND 1.0 1011011122:43 Elhylbenzene ug1L ND 1.0 1 D110111 22:43 Dale: 10/14/2011 09.06 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of pace Analytical Services, Inc.. Qualifiers PaceAnatyticaI Services, Inc_ 9800 Kincey Ave. Suite 100 Huntersvllle, NC 28078 (794)075.%92 Page 47 of 67 aceAnaij4ical Www.pa:elsrSs.Cnm Project: CM WWTP Pace Project No.: 92103792 METHOD BLANK 670724 Associated Lab Samples: 92103792009 Pate Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336M3.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Matrix: Water Parameter Units Blank Result Hexachloro-1,3-butadiene uglL 1.2 m&p-Xylene uglL N❑ Methyl-terl-butyl ether uglL ND Methylene Chloride ug1L ND Naphthalene ug1L ND o-Xylene ug1L ND p-Isopropyltoluene ug1L ND Styrene ug1L ND Teirachloroethene uglL ND Toluene ug1L ND trans-1,2-Dichloroethene ug1L ND trans-1,3-Dichloropropene uglL ND Trichloroethene ug1L ND TricMorofluoromethane ug1L ND Vinyl acetate uglL ND Vinyl chloride ug1L ND 1,2-Dichloroethane-d4 (S) % 114 4- Bromoflu oro benzene (S) % 99 Dibromofluoromethane (S) % 103 Toluene-d8 (S) % 105 LABORATORY CONTROL SAMPLES 670725 Parameter 1,1,1.2-Tetrachloroethane 1,1,1-Trichloroethane 1,1.2,2-TeIra chloroethane 1,1,2-Trichloroethane 11-Dichloroethane 1,1-Dichloroethene 1,1 •flichloropropene 1,2,3-Trichlorobenzene 1,2,3-Tdchloropropane 1,2,4-Trich1orobenzene 1,2-Dibroma-3-chloropropane 1,2-Dibromoethane (EDB) 12-DiOlorobenzene 1,2-Dichtoroethane 1,2-Dichloropropane 1,3-Dichtorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlarotoluene 10mr-.A[i[iTf[}PZFii[rk]iT:TTi►.I Reporting Limit Analyzed Qualifiers 1.0 10110/1122A3 B- 2,0 10/10/11 22A3 1.0 10110/11 22A3 2A 10/1011122A3 1.0 10/10/11 22:43 1.0 10110/11 22:43 1.0 10110/11 22A3 1.0 10/10/11 22:43 1.0 10/10/11 22A3 1.0 10/10/11 22:43 1.0 10/10/11 22:43 1.0 10/10/11 22.43 1.0 10/10/11 22:43 1.0 101101112243 2.0 10/10/11 22:43 1.0 10/10/11 22A3 70-130 10/10/11 22A3 70-130 10/10/11 22:43 70-130 10/10/11 22:43 70-130 10/10/11 22:43 Units Spike Conc. LCS Result LC5 % Rec % Rec Limits uglL 5Q 57.1 114 70-130 uglL 50 47.3 95 70-130 uglL 50 59.6 119 70-130 uglL 50 53.8 108 70-130 uglL 50 51.0 102 70.130 uglL 50 52.3 105 70-132 uglL 50 52.5 105 70-130 ug1L 50 54.9 110 70-135 uglL 50 55.1 110 70-130 ug1L 50 53.3 107 70-134 ug1L 50 60.6 121 70-130 ug1L 50 55.8 111 70-130 uglL 50 54.1 108 70-130 uglL 50 59.6 119 70-130 ug1L 50 58.6 117 70-130 uglL 50 54.5 109 70-130 ug1L 50 56.2 112 70-130 uglL 50 51.2 102 70-130 uglL 50 48.9 94 58-145 ug1L 100 111 111 70-145 uglL 50 55.8 112 70-130 REPORT ❑F LABORATORY ANALYSIS This re part shall not be reproduced, except in full, without the written consent of Pam Arra lytical Services, tnc.. Pace AnatyticaI ServIcas. Inc. 9800 KIncey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Qualifiers Page 48 of 67 a Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 1!;a'ceAnalytical 205 East Meaduw Road - Suite A 2225 Rlverside Dr. 9 80 0 KlnceyAve. Su Re 100 nvns.parefaL�.cwrr Eden, NC 27268 Asheville, NC 28804 Huntemville, INC 28078 (336)623-8921 (8281254-7176 (704)875.9092 QUALITY CONTROL DATA Project; CMI WWTP Pace Project No.: 92103792 LABORATORY CONTROL SAMPLE; 670725 Parameter Units Spike Conc_ LCS Result LCS % Rec °% Rec Limits Qualifiers 2-Hexanone ug/L 100 110 110 7D-144 4-Chlarotoluene ug1L 50 58.5 117 7D-130 4-Methyl•2-pentanone (MtBK) uglL 100 107 107 70-140 Acetone ug1L 100 112 112 50-175 Benzene ug1L 5D 58.4 117 70-130 Bramobenzene ug1L 50 54.3 109 7D-130 Bromochloromethane ug/L 50 49.7 99 70-130 Bromodichloromelhane ug/L 50 53.3 107 71H 30 Bromoforrn uglL 50 52.6 105 70-130 Bromomelhane ug/L 50 54.7 109 54-130 Carbon tetrachloride uglL 50 53.8 108 70-132 Chlorobenzene uglL 50 55.1 110 7D-130 Chloroethane ug1L 5o 64.7 129 64-134 Chloroform ug/L 50 50.8 102 70-130 Chloromethane ug/L 50 53.3 107 64-130 cis- 1,2-Dichloroethene ug1L 50 51.0 102 70-131 cis-1,3-Dichloropropene ug1L 50 59.1 118 70-130 Dibromochloromethane ug1L 50 53.6 107 70-130 Dibromomethane uglL 50 52.7 105 70-131 Dichlorodifluoromethane ug/L 50 54.4 109 56-130 Diisopropyl ether ug1L 50 52.9 106 70-130 Ethylbenzene ug1L 50 55.2 110 70-130 Hexachlaro-1,3-butadiene ug/L 50 53.6 107 70-130 m&p-Xyiene ug1L 100 110 110 70-130 Melhyl-tert-butyl ether ug1L 50 53.2 106 70-130 Methylene Chloride uglL 50 57,0 114 63-130 Naphthalene uglL 50 50.1 100 70-138 a-Xylene ug1L 50 56.6 113 7D-130 p-Isopropyltoluene uglL 50 55.6 111 70-130 Styrene ug1L 50 59.4 119 70-130 Tetrachloroelhene ug1L 50 51.3 103 70.130 Toluene ug1L 50 53.7 107 7D-130 trans-1,2-Dichloroethene ug1L 50 49.5 99 7D-130 trans-1,3-Dichloropropene uglL 50 59.6 120 70-132 Trichloroethene uglL 50 58.0 116 70.130 Trichlorofiuoramethane uglL 50 54.0 108 62-133 Vinyl acetate uglL 100 101 101 66-157 Vinyl chloride u91L 50 57.3 115 69-i30 1,2-Dichloroelhane-dill (S) % 105 70-130 4-Bromonuorobenzene (S) % 104 70-130 Dibromonuorometharie (S) % 94 70-130 Toluene-d8 (S) % 102 70-130 Date? 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 49 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. e Pace Analytical Services, Inc. Pace Analytical Services, Inc - Pace Analytical Services, Inc aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr 9800 KinceyAve. SuNa 100 ammpirrlabs com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623.8921 (828)254-7178 (704)875.9092 QUALITY CONTROL DATA Project: CMI WWTP Pace Project No.: 92103792 OC Batch: MSV116939 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples; 92103792002, 92103792007, 92103792008 METHOD BLANK: 671139 Matrix: Water Associated Lab Samples: 92103792002, 92103792007, 92103792008 Parameter Blank Units Result Reporting Limit Analyzed 1.1,1,2-TeIre chloroethane ug/L ND 1.0 1011211100-.02 1,1,1-TricNoroethane uglL ND 1.0 10/1211100:02 1,1.2,2-TeIra chloroethane ug/L ND 1.0 10/1211100:02 11,2-Trichlaroethane ug/L ND 1.0 1011211100:02 1,1-Dichloroethane uglL ND 1-0 10/1211100:02 1,1-Dichloroethene ug1L NO 1.0 10/1211100,02 1,1-Dichloropropene ug/L NO 1.0 1011211100:02 1,2,3-Trichlorobenzene uglL NO 1.0 10/12/1100:02 1,2,3-Trichloropro pane uglL NO 1.0 10/12/1100:02 1,2,4-Trichlorobenzene ug/L ND 1.0 10/1211100:02 1,2-Dibromo-3-chlorapropane uglL NO 5.0 10/12/1100,02 1,2-Dibramoethane (EDB) uglL NO 1-0 10/12/11 00:02 1,2-Dichicrobenzene ug/L NO 1.D 10/1211100:02 1,2-Dichloroethane uglL NO 1.0 10/1211100:02 1,2-Dichloropropane uglL NO 1-0 1011211100:02 1,3-Dichiorobenzene uglL NO 1,10 10/1211100:02 1,3-Dichloropropane ug/L NO 1.0 10/12/1100:02 1,4-Dichlorobenzene ug/L NO 1.0 1011211100:02 2,2-Dichloropropane ug)L NO 1.0 1011211100:02 2-Butanone (MEK) ug/L NO 5-0 10/12/11 00:02 2-Chlorotoluene ug/L NO 1-0 10/12/1100:02 2-Hexanone uglL ND 5.0 10112/1100:02 4-Chlorotoluene uglL NO 1.0 10/121-1100.02 4- Methyl -2-pentanon e (MIRK) ug/L N❑ 5.0 1D(12111 00:02 Acetone ug1L NO 25-0 10/12/1100:02 Benzene ug/L ND 1.0 10112/1100:02 Bromobenzene uglL NO 1.0 101ID1100:02 Bromochloromethane ug)L ND 1.0 10/12/1100:02 Bromodichloromethane uglL ND 1.0 1011211100:02 Bromoform ug/L NO 1.0 1011211100:02 Bromomethane ug1L NO 2.0 1011211100:02 Carbon tetrachloride uglL ND 1.0 10/1211100:02 Chlorobenzene uglL NO 1.0 10/1211100:02 Chloroethane uglL NO 1.0 10/1211100:02 Chloroform ugJL ND 1.0 10/1211100:02 Chloromethane uglL ND 1.0 10/1211100.-02 cis-1,2-Dichloroethene uglL NO 1-0 1011211100:02 cis- 1, 3- Dich loropropene uglL NO 1.0 1011211100:02 Dibromochloromethane uglL ND 1.0 1011211100.02 Dibromomethane uglL NO 1.0 1DJ1211100:02 Dichlorodinuoromethane ug1L NO 1-0 1011211100.02 Diisapropyl ether uglL NO 1,0 10(12/11 00:02 Ethylbenzene uglL ND 1-0 10)1211100:02 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS ThIs report shall not be reproduced, except in Full, without the written consent of Pace Analytical Services, Inc Qualifiers Page 50 of 67 aceAnalyllcala xuw.pa;el.b.q-C m Project CM I wwrP Pace Project No.. 92103792 Pace Analytical Services, Inc. 205 East M ea dow Road - Suite A Eden, NC 27288 (3381523-8921 Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC28804 (828)254-7176 QUALITY CONTROL DATA METHOD BLANK' 671139 Associated Lab Samples: Parameter Matrix: 92103792002. 92103792007, 92103792008 Blank Units Result Water Reporting Limit Analyzed Hexachtoro-1.3-butadlane uglL NO 1.0 1011211100:02 m&p-Xylene ug1L ND 2.0 1011211100:02 Methyl-terl-bulyl ether ug1L ND 1.0 10/12111 00:02 Methylene Chloride uglL NO 2.0 10/12/11 00:02 Naphthalene u91L ND 1.0 10112/1100;02 o-Xyiene ugll_ N❑ 1.0 10112J1100:02 p-Isopropyltoluene uglL N❑ 1.0 1011211100:02 Styrene ug/L ND 1.0 1011211100,02 Telrachloroethene uglL NO 1.0 10/12111 00:02 Toluene ug1L NO 1.0 1011211100:02 trans- l,2-Dichiaroethene uglL ND 1.0 1011211100,02 trans- l,3-Dichloropropene uglL N❑ 1.0 10/1211100:02 Trichloroethene ug1L ND 1.0 1011211100:02 Trichlarofluoromethane ug1L ND 1.0 10112/1100:02 Vinyl acetate ug1L ND 2.0 10/12111 00,02 Vinyl chloride uglL ND 1.0 10/12/11 00:02 1,2-Dichloroethane-64 (S) % 123 70-130 10/12/11 00:02 4-Bromofluorobenzene [S] % 95 70-130 10/12/11 OQ02 Dibromonuoromethane (5) % 122 70-130 10/12/11 00:02 Toluene-d8 (S) % 100 70-130 10/12/11 00:02 Qualifiers LABORATORY CONTROL SAMPLE- Parameter 671140 Units Spike Conc. LCS Result LCS °% Rec °% Rec limits 1.1,1,2-Tetrachloroethane ug1L 50 52.6 105 70-130 1,1,1-Trichloroethane uglL 50 45.5 91 70-130 1,1,2,2-Tetrachloroethane uglL 50 54.0 108 70-130 1,1,2-Tdchloroethane uglL 50 53.5 107 70.130 1,1-Dichloroetharie ug1L 50 45.8 92 70-130 1,1-Dichloroethene uglL 50 47.3 95 70-132 1,1-Dichloropropene uglL 50 47.9 96 70-130 1,2,3-Tdchlorobenzene uglL 50 48.4 97 70-135 1,2,3-Tdchloropropane ug1L 50 51.9 104 70-130 12,4-Trichlorobenzene ug1L 50 45.4 91 70-134 12-Dibromo-3-chloropropane uglL 50 53.1 106 70-130 1,2-Dibromoethane (EDS) ug1L 50 54.1 108 70-130 1,2-Dichlorobenzene ug1L 50 51.1 102 70-130 1,2-Dichloroethane uglL 50 53.7 107 70-130 1,2-Dichloropropane ug1L 50 54.1 1D8 70-i30 1,3-Dichlorobenzene ug1L 50 50.2 100 70-130 1,3-Dichloropropane uglL 50 54.4 109 70-130 1,4-Dichlorobenzene ug1L 50 47.7 95 70-130 2,2-Dichloropropane ug/L 50 38.9 78 58-145 2-Butanone (MEK) uglL 100 112 112 70-145 2-Chlorotoluene ug1L 50 51.9 104 70.13D Date. 10/14/2011 09-06AM REPORT OF LABORATORY ANALYSIS This report shall nut be reproduced. except In full. without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc P800 KinceyAve, Suite 1t70 Huntersvitle, NC 28078 (704)875.9092 Qualifiers Page 51 of 67 a Pace Analytical Services, He. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalyflcal 265 fast Meadow Road - Suite A 2225 Riverside Dr 98ot} KinceyAve. Suite 100 emn.pacelats Eden. NIC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623.8521 (828)254-7170 (704)875-9092 QUALITY CONTROL DATA Project: CM I WYVTP Pace Project No.: 92103792 LABORATORY CONTROL SAMPLE: 671140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec. Limits Qualifiers 2-Hexanone uglL 100 97.4 97 70-144 4-Chlorotoluene ug1L 50 53.9 108 70-130 4-Methyl-2-pentanone (MIRK) ug1L 100 103 103 70-140 Acetone uglL 100 107 107 50-175 Benzene ug1L 50 44.8 90 70-130 Bromobenzene uglL 50 49.1 98 70-130 Bromochloromethane uglL 50 49.8 100 70-130 Bromodichloromethane ug1L 50 52.3 105 70-130 Bromofarm uglL 50 46.4 93 70-130 Bromomethane ug1L 50 30.1 00 54-130IC Carbon tetrachloride ug1L 50 47.8 96 70-132 Chlorobenzene uglL 50 50.2 100 70-130 Chloroelhane uglL 50 53.7 107 64-134 Chloroform uglL 50 57.5 115 70.130 Chloromethane uglL 50 59.9 120 64-130 cis-1,2-Oichloroethene uglL 50 45A 90 70-131 cis-1,3-0ichloropropene uglL 50 49.6 99 70.130 Dibromochloromethane uglL 50 52.9 106 70-130 Dibromomethane uglL 50 53.0 106 70-131 Dichlorodinuoromethane uglL 50 68.8 138 56-130 LO Dlisopropyl ether uglt 50 46.7 93 70-130 Ethylbenzene uglL 50 52,5 105 70-130 Hexachloro-1,3-butadiene ug1L 50 46.6 93 70-130 m&p-Xylene uglL 100 108 108 70-130 Methyl-teri-butyl ether uglL 50 49.6 99 70-130 !Methylene Chloride ug1L 50 55.6 111 63.130 Naphthalene ug1L 50 50.6 101 70-138 o-Xylene ug1L 50 48.5 97 70-130 p-Isopropyltaluene uglL 50 47.5 95 70-130 Styrene uglL 50 50.0 100 70-130 Tetrachloroethene uglL 50 48.2 96 70-130 Toluene uglL 50 52.2 104 70-130 trans•1,2-Dichloroethene ug1L 50 45.9 92 70-130 trans- 1,3•Dichloropropene uglL 50 49.0 98 70-132 Thchloroethene uglL 50 55.8 112 70-130 Trichlorofluoromelhane ug1L 50 55.2 110 62-133 Vinyl acetate uglL 100 88.4 88 66-157 Vnyl chloride uglL 50 57.2 114 69-130 i,2-01chloroethane-d4 (S)i % 96 70-130 4-Bromoiluorobenzene (S) %c 99 70-130 Dibromonuoromelhane (S) % 93 70-130 Toluene-d8 (S) %c 100 70-130 Dale: 1011412 01109.06 AM REPORT OF LABORATORY ANALYSIS Page 52 of 67 This report shalt nol he reproduced, except in full, without the writlem Consent of Pace Analytical Services, Inc aCeAnalyllca(' nxw,pace+a65.com Project: CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc, 9800 I[insey Ave. Suite 100 Huntersville, NC 25078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 671141 671142 MS MSD 92103911003 Spike Spike MS MSD MS MSD % Rec. Parameter Units Result Cane, Cone. Result Result % Rec % Rec Limits RPD Qua) 1,1-Dichloroethene uglL ND 50 50 51.5 54.7 103 109 70-160 6 Benzene uglL GAW 50 50 40.0 42.0 79 83 70-148 5 Chlorobenzene ugJL 4.0 50 50 48_8 52.9 90 98 70-146 8 Toluene uglL ND 50 50 44.5 49.1 89 98 70-155 10 T6chlaroelhene uglL ND 50 50 37A 41.5 75 83 69-151 11 1,2-Dichloroethane-d4 (S) % 121 120 70-130 4-Bromofluorobenzene (S) % 89 88 70-130 Dibromotluoromethane (S) % 118 117 70-130 Toluene-d8 (S) % 93 92 70.130 Date- 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 53 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services. Inc.. aceRnaly ical- www.pac0abs.eom Project: CMI WW-TP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Sul teA Eden, NC 27288 (336)623-6921 Pace Analyfical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 [QUALITY CONTROL DATA QC Batch: MSV116943 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Law Level Associated Lab Samples: 92103792004, 92103792005, 92103792006 METHOD BLANK 6711589 Matrix: Water Associated Lab Samples: 92103792004, 92103792005, 92103792006 Blank Reporting Parameter Units Result Limit 1,1.1,2-Tetrachloroethane ug/L ND 1,1,1-Trichloroethane ug/L ND 1,1,2.2-Tetrachtoroethane ug/L N❑ 1,1,2-Trichloroethane ug/L N❑ 1,1-Dichloroethane u91L ND 1,1-Dichloroethene ug/L ND 1.1-Dichloropropane ug/L ND 1,2,3-Trichlorobenzene ug1L ND 1,2,3-Tdchloropropane ug/L N❑ 1,2,4-Tdchiorobenzene ug/L ND 1,2-Dibromo-3-chloropropane ug/L ND 1,2-Dibromoethane (EDB) ug/L ND 1,2-Dichlorobenzene ug/L ND 1,2-Dichloroethane ug/L N❑ 1,2-Dichloropropane ug/L ND 1,3-Dichlorobenzene uglL ND 1,3-Dichloropropane ug/L ND 1,4-Dichlorobenzene ug/L ND 2,2-Dichloropropane ug/L ND 2-Butanone (MEK) uglL ND 2-Chlorotoluene uglL ND 2-Hexanone ug/L ND 4-Chlorotoluene uglL ND 4-Methyl-2-pentanone (MIBK) uglL ND Acetone uglL ND Benzene ug/L ND Bromobenzene uglL ND Bromochloromethane uglL ND Bromodichloromethane ug1L ND Sromotorm ug/L ND Bromomethane ug/L ND Carbon tetrachloride ug/L ND Chiorobenzene ug1L ND Chloroethane ug/L ND Chloroform ug/L N❑ Chloromethane ug/L ND cis-1,2-Dichloroethene ug1L ND cis-1,3-Dichloropropene uglL ND Dibromochloromethane uglL ND Dibromomethane ug/L ND Dichlorodifluorometharle ug1L ND Diisopropyl ether ug/L ND Ethylbenzene ug/L ND Analyzed 1.0 10/12/11 12:04 1.0 10/12/11 12:04 1.0 10/12/11 12:D4 1.0 10//2111 12:04 1.0 10/12/11 12;04 1.0 10/12/11 12:04 1.0 1 D112111 12:04 1,0 10/12/11 12:04 1.0 10/12111 12:04 1,0 10/12/11 12:04 5.0 10/12/11 12:04 1.0 10/12/11 12:04 1.0 10/12/11 12:04 1.0 10/12/11 12:04 1-0 10/12/11 12:04 1.0 10112/11 12:04 1.0 10/12/11 12:04 1-0 10/12/11 12:04 1.0 10112/11 12:04 5.0 10112/11 12:04 1.0 10/12/11 12:04 5.0 10/12/11 i 2:04 1.0 10/12/11 12:04 5.0 10/12/11 12:04 25,0 10112/11 12:04 1.0 10/12/11 12.04 1.0 10/12/11 12:04 1.0 10112/11 12:04 1.0 10/12/11 12:04 1.0 10112/11 12-04 2.0 10112/11 12:04 1.0 10/12/11 12:04 1,0 10/12/11 12.04 1.0 10/12/11 12:04 1.0 10/12111 12:04 1.0 10/12/11 12:04 1.0 10/12/11 12:04 1.0 10112111 12:04 1.0 10/12/11 12,04 1.0 10112/11 12:04 1.0 10112/11 12:04 1.0 10/12/11 12,04 1-0 10/12/11 12:04 Oualiliers Pace Analytical Services, Inc. 9800 KInceyAve. Suite 700 i-luntersvlle, NC 28078 (704)875-9092 Dale: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 54 of 67 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. 1!;a'ce Analytical nwn.parele5s.ra.n Pace Analytical Services. Inc. 205 East Meadow Road - SVke A Eden, NC 27288 (3M)623-8921 Pace Analyticat Services, Inc. 2225 RiversWe Or Ashev 31e, NC 28&D4 (828)254-7176 QUALITY CONTROL DATA Project CMI WWTP Pace Project No.: 92103792 METHOD BLANK671689 Matrix: Water Associated Lab Samples: 92103792004, 92103792005, 92103792006 Blank Reporting Parameter Units Result Limit Analyzed Hexachloro-1,3-buladiene uglL NO 1.0 1011211112:04 m&p-Xylene uglL NO 2.0 1011211112:04 Methyl-tert-butyl ether uglL NO 1.0 10/12/11 12:04 Methylene Chloride uglL NO 2.0 10/12/11 12704 Naphthalene uglL NO 1.0 10/12/11 12:04 o-Xylene uglL NO 1 X 101121l1 12:04 p-lsopropylioluene uglL NO 1.0 10/12111 12:04 Styrene ug1L NO 1.0 10/12/11 12 04 Tetrachlorcethene uglL NO 1.0 10112/11 12:D4 Toluene uglL NO 1.0 10/12/11 12,04 trans-1,2-Dichloroethene ug/L ND 1.0 10112/1112�04 trans-1,3-Dichiaropropene uglL NO 1.0 10/1211112:04 Trichloroethene uglL NO 1.0 1011211112:04 Trichloronuoromethane uglL ND 1.0 1011211112A4 Vinyl acetate uglL NO 2.0 10/12/11 12:04 Vinyl chloride uglL NO 1.0 10/12/11 12:04 1,2-Dichloroethane-d4 (S) % 118 70.130 10/12/11 12:04 4-Bromofluorobenzene (S) % 94 70-130 10/12/11 12.04 Oibromofluoromethane (S) % 115 70.130 10112/11 12:04 Toluene-d8 (S) % 100 7D-130 10/12/11 12:04 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 071690 Units Spike Cone. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane uglL 50 53.2 106 70-130 11,1-Trichloroethane uglL 50 45.0 90 70.130 1,1.2,2-Tetrachloroethane uglL 50 54A 108 70-130 1,1,2-TricNoroethane uglL 50 51A 103 70-130 11-Dichloroelhane uglL 50 44.9 90 70-130 1,1-Dichloroethene uglL 50 46.0 92 70-i32 1,1-Oichloropropene uglL 50 47.5 95 70-130 1,2.3-Trichlorobenzene uglL 50 49.2 98 70-135 1,2,3-Trichloropropane uglL 50 51.8 104 70-130 1,2,4-Trichlorobenzene uglL 50 47.5 95 70-i34 1,2-Dibromo-3-chloropropane uglL 50 53.2 106 70-130 1,2•Dibromoethane (EDB) ug)L 50 54.0 108 70-130 1,2-Dichlorobenzene uglL 50 52.7 105 70-130 1,2-Dichloroelhane uglL 50 51.5 103 70-130 1,2-Dichloropropane uglL 50 52.6 105 70.130 1,3-Dichlorobenzene uglL 50 51.9 104 70-130 1,3-Dichlompropane uglL 50 54.1 108 70-130 1,4-Dichlorobenzene uglL 50 49.8 100 70-130 2,2•Dichloropropane ug1L 50 45.3 91 58-145 2-Butanone (MEK) ug1L 100 113 113 70-145 2-ChlorotDluene ug1L 50 54.2 108 70-130 Pace Analytical 5arvices. Inc. 9800 KinceyAve . Suite 100 Huntersv3e, NC 28076 (704)675-9D92 Qualifiers Date* 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 55 of 67 This report shall not be reproduced, except in full, wlthoul the written Consent of Pace Analytical Servlce5, 1nt.. �. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 11�aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside dr 9800 KinceyAve. Suile 100 aww.pacetabs.mm Eden, NC 27288 Asheville, NC 28804 Huntersvllle, NC 26078 (336)623-8921 (828)254.7176 (704)875-9092 QUALITY CONTROL DATA Project: Cm WW P` Pace Project No.: 92103792 LABORATORY CONTROL SAMPLE: 671690 Parameter units Spike Canc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Hexanone siglL 100 96,7 97 70-144 4-Chlorotoluene uglL 50 55,8 112 70.130 4-Methyl-2-pentanon e (MIBlt) uglL 100 98.7 99 70-140 Acetone uglL 100 119 119 50-175 Benzene uglL 50 46.8 94 70-130 Bromobenzene uglL 50 50.5 101 70-130 Bromochloromethane uglL 50 48A 96 70-130 Bromodichloromethane uglL 50 51.1 102 70-130 BromoforM uglL 50 46.5 93 70-130 Bromvmethane uglL 50 31.2 62 54.130 Carbon tetrachloride uglL 50 47.4 95 70-132 Chlorobenzene uglL 50 50.5 101 70-130 Chloroethane uglL 50 50.7 101 64-134 Chloroform uglL 50 55.8 112 70-130 Chloromethane uglL 50 56.8 114 64-130 cis-1,2-Dichloroethene uglL 50 44.5 89 70-131 cis-1,3-Dichloropropene uglL 50 49.5 99 70-130 Dibromochloromethane uglL 5fl 52.7 105 70-130 Dibromomethane u911- 50 50.7 101 70-131 Dichlorodifluoromethane uglL 50 67.3 135 56-130 L3 Diisopropyl ether uglL 50 45.7 91 70-130 Ethylbenzene uglL 50 52.6 105 70-130 Hexachloro-1,3-butadiene ugll- 50 50.7 101 70-130 m&p-Xylene uglL 100 110 110 70-130 Methyl -tent -butyl ether uglL 50 48.0 96 70-130 Methylene Chloride uglL 50 53,9 108 63-130 Naphthalene uglL 50 51.0 102 70-138 o-Xylene uglL 50 48.5 97 70-130 p-Isopropylloluene uglL 50 49.4 99 70-130 Styrene uglL 50 50.7 101 70-130 Tetrachlorcethene uglL 50 49,6 99 70-130 Toluene uglL 50 51.1 102 70-130 trans-1,2-Dichloroethene uglL 50 44.8 90 70-130 trans- 1,3-Dichloropropene uglL 50 49,2 98 70-132 Trichloroethene uglL 50 53.7 107 70-130 Trichlorofluoromelhane uglL 50 55.4 111 62-133 Vinyl acetate uglL 100 9U 90 66-157 Vinyl chloride uglL 50 55.5 ill 69-130 1,2-Dichloroethane-d4(6) % 97 70-130 4-Bromofluorobenzene (S) 0/0 99 70-130 Dibromofluoromelhane (S) % 95 70-130 Toluene-d8 (S) % 99 70-130 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 56 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAna1j4ical www. pace abs. wrr Project: CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East hie"ow Road - Suite A Eden, NC 27288 (336)623-892 i Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 QUALITY CONTROL DATA Pace Analytical Services. Inc. 9800 KlnmyAve. Suile 10t3 Hvntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE- 671691 071692 MS MSD 92103924002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Conc. Result Result % Rec % Rec Limits RPD oval 1,1-Dichloroethene ug/L ND 50 50 56.4 58.1 113 116 70-166 3 Benzene ug1L ND 50 50 51.9 46.5 104 93 70-148 11 Chlorobenzene ug1L ND 50 50 5316 52M 107 106 70-146 1 Toluene ug/L N❑ 50 50 53.4 52.6 107 105 70-155 1 Trichloroethene ug/L N❑ 50 50 49.9 481 100 97 69.151 2 1,2-01chloroethane-& (S) % ill 116 70-130 4-8romofluorobenzene (S) % 92 91 70-130 Dibromofluoromethane (S) % 105 109 70-130 Toluene-d8 (S) % 93 92 70-130 Date: 10/14/2011 09-.06AM REPORT OF LABORATORY ANALYSIS Page 57 of 67 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc. s. aceAnalXical � nxwpacelabs.mm Pace Analytical Services, Inc. 205 East Meadow Road - Suile A Eden, NC 27289 (335)823.8921 Pace Analytical Services, Inc. 2225 Riverside Cr Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Hunlersville, NC 28078 (704)875.9092 Project: CMI WWTP Pace Project No..- 92103792 OC Batch: WET118187 Analysis Method: SM 2320B OC Balch Method: SM 2320B Analysis Description: 2320B Alkalinity Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792006. 92103792007, 92103792008.92103792009 METHOD BLANK: 670819 Matrix: Water Associated Lab Samples7 921037132001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792006, 92103792007, 92103792008,92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L NO 5.0 10/11/11 10:30 Alkalinity,81carbonate (CaCO3) mg1L NO 5.0 10/11/11 10:30 LABORATORY CONTROL SAMPLE-. 670820 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaG03 mg1L 50 50.0 100 90-110 Alkalinity,Bicarbonate (CaCO3) mglL 8.3 SAMPLE DUPLICATE: 670821 Parameter Units Alkalinity, Total as CaCO3 mg1L Alkalinily,Bicarbonale (CaCO3) mg1L 92103486002 Qup Result Result RPD Qualifiers 335 339 1 339 1 SAMPLE DUPLICATE: 670822 92103792008 Dup Parameter Units Result Result RPD ❑ualiflers Alkalinity, Total as CaCO3 mg/L 72.9 66.7 9 Alkalinity,Biearbonate (CaG03) mg1L 72.9 66.7 9 Date: 10114/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 58 of 67 This report shall riot he reproduced, except in full, wilhoul the written consent or Pace Analytical Services. Inc.. 117;'a'ceAnalyfical www.pacefa8s.cnm Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27208 (336)623.8921 Pace Analytical Services, tnc. 2 22 5 Riverside ❑r. Asheville, NC 28804 (828)254.7176 DUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 K[ ncey Ave. Suite TOO Huntersville, NC 28078 (704)875-9D92 Project: CMI WWTP Pace Project No. 92103792 QC Batch: WET118171 Analysis Method; SM 2540C ❑C Batch Method: SM 2540C Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792006, 92103792007, 92103792008,92103792009 METHOD BLANK: 670263 Matrix: Water Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792006, 92103792007, 92103792008,92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg1L NO 25.0 10107/11 16-33 LABORATORY CONTROL SAMPLE: 670264 Spike LCS LC5 % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg1L 250 256 102 80-120 SAMPLE DUPLICATE: 670265 Parameter Total Dissolved Solids 92103792001 pup Units Result Result mg1L 482 479 RPD (Qualifiers 1 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 59 of 67 This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 1!;a'c le Analyfica / " • Mom'-AdCElabs. FOm Pace Analytical Services, Mr. 205 East Meadow Road - Suite Eden, NC 2 72 88 (336)623.8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1o0 Hunlersville, NC 28078 (704)875-9092 Project: CMI WWTP Pace Project No.: 92103792 CC Batch: WET118158 Analysis Method: SM 3500-Fe D#4 QC Batch Method. SM 35D0-Fe D#4 Analysis Description: Iron, Ferrous Associated Lab Samples: 92103792001, 92103792002. 92103792D03, 92103792004. 92103792005, 92103792006, 92103792007, 92103792008,921037920D9 METHOD BLANK 669771 Matrix: Water Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 921037920D6, 921037920D7, 92103792008,92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Iron, Ferrous mg/L ND d.50 10/10/11 16A8 N2 LABORATORY CONTROL SAMPLE: 669772 Spike Parameter Units Conc. Iron, Ferrous mg/L 1.5 SAMPLE DUPLICATE: 669773 Parameter Iron. Ferrous LCS LCS % Rec Result °% Rec Limits Qualifiers 1.6 105 90-110 N2 92103587001 Dup Units Result Result mg/L NO ND RPD Qualifiers N2 Date: 10/14/2011 09 06 AM REPORT OF LABORATORY ANALYSIS Page 60 of 67 This report shall not be reproduced, except In Full, wilhoul. the wrltten consernl or Face Ana local Services, inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. /'ceAnalyfical"' a205 Easl Meadow Road - 5uite A 2225 Riverside Dr. 9800 KinceyAve. Suite ili0 www.pacetabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254.7176 t704j875.9092 QUALITY CONTROL DATA Project: CMI WWTP Pace Project No.. 92103792 QC Batch: WET11817a Analysis Method: SM 45fl0-S2❑ ❑C Batch Method: SM 4500-52D Analysis Description, 450DS2D Sulfide Water Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792006. 92103792007, 92103792008,92103792009 METHOD BLANK: 670418 Matrix: Water Associated Lab Samples: 92103792001, 92103792D02, 92103792003. 92103792004, 92103792005, 92103792006, 92103792007. 92103792008,92i03792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide mg/L ND 0A 0 10/08/11 12:00 LABORATORY CONTROL SAMPLE: 670419 Spike LC5 LCS % Rec Parameter Units Canc. Result % Rec Limits Qualifiers Sulfide mglL .5 0.52 104 90-110 MATRIX SPIKE SAMPLE: 670420 92103587001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfide mg1L NO .5 0.39 78 75-125 SAMPLE DUPLICATE, 670421 92103587001 Dup Parameter Units Result Result RPiD Qualifiers Sulfide mg1L ND ND Date. 10114/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page 61 of 67 This report shall not he reproduced, except In full, without the written consent of Pare Analytical Services, Inc.. ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical 5ervices, Inc. 117aceAnalytreal 205 Easl Meadow Road - Suite A 2225 Riverside Dr. 9800 KinceyAve. Suite 100 paselQAstnrr Eden, NC 27288 Asheville, NC 28804 Huntersviile, PVC 28078 WWW(336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: CMl WWTP Pace Project No.: 92103792 QC Batch. WETAI10688 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004. 92103792005, 92103792006, 92103792007, 92103792008,92103792009 METHOD BLANK: 669157 Matrix: Water Associated Lab Samples: 92103792001, 92103792002, 92103792003. 92103792004, 92103792005, 92103702006, 02103792007, 92103792008,92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L NO 5.0 10/0711115:48 LABORATORY CONTROL SAMPLE: 669158 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mg/L 20 19A 97 90-110 MATRIX SPIKE SAMPLE: 669159 92103792001 Spike MS MS °% Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg1L NO 20 20.9 97 90-110 MATRIX SPIKE SAMPLE: 669101 92103698002 Spike MS MS % Rec Parameter Units Result Conc- Result °% Rec Limits Qualifiers Sulfate mg1L 117 20 175 289 90-110 M6 SAMPLE DUPLICATE- 669160 92103792001 ❑up Parameter Units Result Result RPD Qualifiers Sulfate mglL ND ND SAMPLE DUPLICATE: 669162 92103698002 ❑up Parameter Units Result Result RPD Qualifiers Sulfate mg1L 117 117 0 Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 62 of 67 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc-. - aceAnaVica1" wwwpaceiaLs.cnm i Project: CMI WWTP Pace Project No.: 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, INC 272B8 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kin cey Ave. Suite 100 Huntersville, NC 28018 t7041875-9092 OC Batch: WLTA110687 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres, Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792007, 92103792008 METHOD BLANK: 668983 Matrix: Water Associated Lab Samples: 92103792001, 92103792002. 92103792003, 92103792004, 92103792005, 92103792007, 92103792008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg1L ND 0,20 10/05111 22:18 Nitrogen, Nitrite mg/L ND 0,10 10/05/11 22:18 LABORATORY CONTROL SAMPLE: 668984 Parameter Units Nitrogen, Nitrate mg1L Nitrogen, Nitrite mg1L MATRIX SPIKE SAMPLE: 668985 Parameter Units Nitrogen, Nitrate mg1L Nitrogen, Nitrite mg1L SAMPLE DUPLICATE: 668986 Parameter Nitrogen, Nitrate Nitrogen, Nitrite Spike LCS LCS % Rec Gonc. Result % Rec Limits Qualifiers 5 5.0 101 90-110 1 1.0 102 90-110 92103792004 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND 5 5,4 109 90-110 ND 1 'iA 105 90-110 92103792004 pup Units Result Result mg/L ND N❑ mg/L ND ND RPD Qualifiers Date: 10/14/2011 09:06AM REPORT OF LABORATORY ANALYSIS Page 63 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Servlces, Inc. e Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc, aceAnapical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kinsey Ave. Suite loo wwwpaceiaba mm Eden. NC 27288 Asheville, NC 28804 Hvntersville, NC 28078 (336)623-8921 (828)254.7176 (704)875-9092 QUALITY CONTROL DATA Project: CM WWTP Pace Project NO.' 92103792 QG Batch: WETA110693 Analysis Method: EPA 353.2 QC Batch Method: EPA 353,2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 92103792006, 92103792009 METHOD BLANK: 669563 Matrix: Water Associated Lab Samples: 92103792006, 92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mglL NO 0.20 10/06/11 22:18 Nitrogen, Nitrite mg1L NO 0.10 10/06/11 22:18 LABORATORY CONTROL SAMPLE: 669564 Spike LGS LCS % Rec Parameter Units Conc. Result % Res Limits Qualifiers Nitrogen, Nitrate mg1L 5 5.1 102 90-110 Nitrogen, Nitrite mglL 1 1.0 100 90-110 MATRIX SPIKE SAMPLE: 609565 92103730D03 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg1L 7,5 5 11.8 84 90-110 M1 Nitrogen, Nitrite mg1L ND i 1.1 106 90-110 MATRIX SPIKE SAMPLE: 669567 92103792009 Spike M5 MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg1L NO 5 5.0 99 90-110 Nitrogen, Nitrite mglL NO 1 1.0 102 90-110 SAMPLE DUPLICATE. 669566 92103730003 Dup Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mg1L 7.5 7.6 1 Nitrogen, Nitrite mglL ND NO SAMPLE DUPLICATE_ 659568 92103792009 Dup Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mg1L NO NO Nitrogen, Nitrite mg1L NO NO Dale-. 10/14/2011 09:06 AM REPORT Of LABORATORY ANALYSIS Page 64 of 67 This report shall not be reproduced, except in fvll, without the written coraent of Pace Analytical Services, Inc, a aceAnalytical �nrw,paoelatrscvrrr Project: CMI WWTP Pace Project No.. 92103792 Pace Analytical Services, Inc. 205 East Meadow Road - SuiteA Eden, NC 27298 (335)523.8921 Pace Analytical Services, Inc. 2225 Riverside Or. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1 GO Huntersville, NC 28078 (704)875-9092 OC Batch. WETAl10712 Analysis Method; SM 4500-CI-E QC Batch Method: SM 4500-C1-E Analysis Description: 4500 Chloride Associated Lab Samples- 92103792001, 92103792002, 92i03792003, 92103792004, 92103792005, 92103792006, 92103792007, 92103792008,92103792009 METHOD BLANK: 670430 Matrix- Water Associated Lab Samples: 92103792001, 92103792002.92103792003, 92103792004, 92103792005, 92103792006, 92103792007, 92103792008,92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg1L ND 5.0 10108/1113:44 LABORATORY CONTROL SAMPLE; 670431 Spike LCS LCS % Rec Parameter Units Conc- Result % Rec Limits Qualifiers Chloride mg1L 20 20.7 103 90-110 MATRIX SPIKE SAMPLE: Parameter 670432 Units 92103587005 Result Spike MS MS % Rec Conc. Result % Rec Limits Qualifiers Chloride mglL 91-1 20 109 90 75-125 SAMPLE DUPLICATE: 670433 92103486002 Dup Parameter Units Result Result RPD Qualifiers Chloride mg1L 14.7 15.3 4 Date: 10/14/2011 09!06AM REPORT OF LABORATORY ANALYSIS Page 65 of 67 This report shall not be reproduced, except in full. without the written consent of PaCe Analytical Services, Inc.. 7ac', e Pace Analytical Services, Inc, Pace Analytical Services, Inc. Pace Analytical Services. Inc. Analytical 205 East Meadow Road - Suite A 2225 Riverside ❑r. 9800 KlnceyAve. Suite 100 p�e7aL�wm Eden, NC 27288 Asheville, NC 28804 Huotersvllle, NC 28078 (336)623.8921 (828)254-7176 (704)875.9092 QUALITY CONTROL DATA Project. CMI WWTP Pace Project No.: 92103792 QC Batch: WETA110702 Analysis Method: SM 5310B QC Balch Method: SM 5310B Analysis Description; 5310B TOC Associated Lab Samples: 92103792001. 92103792002, 92103792003, 92103792004, 92103792005, 92103792D06, 92103792007, 92103792008.92103792009 METHOD BLANK: 670021 Matrix: Water Associated Lab Samples: 92103792001, 92103792002, 92103792003, 92103792004, 92103792005, 92103792006, 92103792007, 92103792008,92103792009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mglL NO 1.0 10/10/11 14:44 LABORATORY CONTROL SAMPLE: 670022 Spike LCS LCS % Rec Parameter Units Cone. Result ❑% Rec Limits Qualifiers Total Organic Carbon mglL 25 23.9 96 90-110 MATRIX SPIKE SAMPLE: 670023 92103792001 Spike MS MS % Rec Parameter Units Result Cane. Result °% Rec Limits Qualifiers Total Organic Carbon mg1L 63,8 25 84.2 81 75-125 MATRIX SPIKE SAMPLE: 670025 92103440016 Spike MS MS ❑/❑ Rec Parameter Units Result Conc. Result '% Rec Limits Qualifiers Total Organic Carbon mg1L 27.0 25 6.5 -82 75-125 Mi SAMPLE DUPLICATE; 670024 92103792002 Dup Parameter Units Result Result RPD Qualifiers Total Organic Carbon mg/L 15A 15.2 3 SAMPLE DUPLICATE: 67DO26 9210344DO33 Dup Parameter Units Result Result RPD Qualifiers Total Organic Carbon mg1L 1.5 1.5 2 Date: 10/14/2011 09:06 AM REPORT OF LABORATORY ANALYSIS Page fib of 67 This report shall not be reproduced, except In full, without the written consent of Pane Analytical Services, Inc.. aceAnalytical" www.pa:&bs.ram Project. CMI WWTp Pace Project No.� 92103792 GI:111K11W141,21V Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254.7176 Pace Analytical Services, Inc 9600 hincey Ave. Suite 100 Huntersvllle, NC 28076 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-0iphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent wish EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicales the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TN accrediled. Contact your Pace PM for the current list of accredited analytes. l�•Li+1:7�ia1.�1�9 PASI-A Pace Analytical Services -Asheville PAS I C Pace Analytical Services - Charlotte PASI-M pace Analytical Services - Minneapolis ANALYTE QUALIFIERS 13- Analyte detected In method blank but was not detected in the associated samples. D3 Sample was diluted due to the presence of high levels of non -target anaiyles or other matrix interference. E Analyte concentration exceeded the calibration range. The reported result is estimated. H1 Analysis conducted outside the EPA method holding time. IC The initial calibration for this compound was outside of method control limits. The result is estimated. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaivaled against control limits due to sample dilution, N2 The lab does not hold TNt accreditation for this parameter. P6 Matrix spike recovery andlor matrix spike duplicate recovery was outside laboratory control limits. Sample amount is 83.15 times larger than the spiked amount. P6 Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the spike level. R1 RPD value was outside control limits. Date: loll 412011 09;06AM REPORT OF LABORATORY ANALYSIS Page 67 of 67 This report shall not" reproduced, except in full. without the written consent of Pace Analytical Services, inc... ' 2"l!eAnalytical' ul , eem CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-0t-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 5 Section C Pape. 1 oI Required Client Information: Required Project Information: Invoice IMormatlan: Company Report To: Anenilnn: 1503653 Address: L Copy To: Company Name; REGULATORY AGENCY C em u' F NPIDES GROUNDWATER r DRINKING WATER f IJST RCRA j' OTHER Emall To: Purchase Order No.: Para Owke Reference: Phone: Fax: Project Name: Pace Pmj wA Manager. Site Location STA TE. I '� Raqueslod Due DatslTAT; Project Number. & q Y Paco Prvefe A "j' ! I7 LS—Requested Analysts Fitt red [Y1N] 3nctlon D µelr{x Godes T PAgUIMACLent lntdmetion L= COLLECTED PresefV80ves 1 Drinkin7 Water DW 0 O Water wT $ 7 WasteWater WW Product p v A corwosrre srAM7 cowPosrre EnwCrtw v J z S01115olid SL SAMPLE lD W a w Wi e (A-Z. Aire AR LLra w as F o Sample IDs MUST BE UNIQUE Tissue TS O q w F w m L7 Other OT x w .F i LL a [[; Q V i L vC y N ~ DATE TIME GATE TIME 7 Z Z 2 Z Q pace Project Nol Lab I.O. , Innw-1L4 I VV q 19 1 2 SG 10/4Se- IU 3 f�ti+Lw— s ►�- � �s 5 a I/11y 1 D 7 w— V I B WI ILI< w ov 4 t"r - 5 9 y x Y y Y)c Y e +a t v ! 3 12 1►P ADDITIONAL COMMENTS REY NQUISNED BY 1 AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS AIM SAMPLER NAME AND SIGNATURE ORIGINAL 3 x_ PRINT Name of SAµI E m $ n DATE Signed l LL� SIGNATURE of SAMPLER: r P O m n (MMIDDlYY): •Impanam Note: By synNg Inrs form yet, are aceapbng Paca's NET 30 day payment wrens and agraoing to late cnargos of t.5% per mvntn Ior any 1—cea not paid within 30 days. I F-ALL-0-020rev,07, 15-May-2007 'OzAnalyflcal - CHAIN-aF-CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must he compleled accurately. Page: 12-- of Section A Section B Section C A 1503654 Required Client Information: Raqulred Projoct lnfc Lien: Inm" Information: Company: Report To: Anoniion: f R w vT ► Address: ��( /. i Copy To: Company Name REGULATORY AGENCY �{ LL Address: i- NPOES GROUNDWATER r DRINKING WATER UST RCRA j-' OTHER Email 7o: Purchase Order No.: Pace QwQ'e Reference: ;1Fwnu: Fax: Protect Name: r' n ,� ' ` pBGe Projoci glte Location LJ:' V L L/V hranager.� STA TE. Raquosled Due DatorfAT:w^Y Project Number, pr P �R�� Requested Analysis Filtered [Y!N] Suction D Matrlx Codes E,z y Requlr.acnem Inlumauon-VATRU! r CODE $ COLLECTED Preservatives 3- Drinking Wairr DW [i0,1 O Water WT [] Wasto weer Wv s m sr,.Rs"E c or w c+ w Product P Sod+Sorld SL ? x Y SAMPLE !D 041 OP �_ ° Ir (A-Z. Da : Y Air AR o ui a }�.. ❑ Sample IDs MUST BE UNIQUE Tissue TS ❑ C. w ;- Omer GP a OM-Z a❑ ❑ O L n 2 '-' 1 ~ N DATE TIME GATE TIMEN 7 T 2 2 2 O tY Pace Project Na. La 2 3 4 5 S 7 a 9 7o 1T 12 ADDITIONAL COMMENTS REUNOUISHED AY IAFFILIATION GATE TIME ACCEPTED BY f AFFILL0knON DATE TIME SAMPLE CON VMONS i- SAMPLER NAME AND SIGNATURE 'm 9 ORIGINAL C v a PRINT Name of SAMPLER! .n 3 c m = m 9 v = U N E N SIGNATURE of SAMPLER: DATE Slgnad. ! U � jMMIDDlYY): •—extant u.w. n. . j�a In.. e...... u ire : - .__•.__ ^uca 6 kFT an n Fyy ,....n..__ _.� e_....... [rWr�- _... , pnr rtw •__ -i-1- __• _. ' Walm . - . I r I ' LL.O_.. 17, 15 - 77 1.2ce,ak7ry 1Ca1' Document Name: Sample Condition Upon Recei Document Number: F-CHR-CS-03-rev.05 Client Name: Where Received: {untersville ❑ Asheville ❑ Eden 7e ,nt Revised: July 29, 2011 Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Project # 9 ?wa 3 72 ?— Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Clien Commercial❑ Pace Other Custody Seal on Cooler/Box Present: ❑ yes ❑ no Seals intact: ❑ yes ❑ no Packing Material: ❑ Bubble Wrap ❑ ble F gs ❑ None [] Other Thermometer Used: I Gun T1102 Type of ice: et Blue None Temo Correction Factor Add 1 Subtract 0 'C Pio};;aue. `- ry; amples on ice, cooling process has begun Corrected Cooler Temp.: �' C Temp should be above freezing to 6'C Biological Tissue Is Frozen: Yes No NIA Comments: Date and Initials of persor�exa i g contents: Chain of Custody Present: Yes ON. ON/A 1, Chain of Custody Filled Out: es ONO ❑NIA 2• Chain of Custody Relinquished: es ❑No ❑wA 3, Sampler Name & Signature on COC: s ONO ❑NIA 4. Samples Arrived within Hold Time: __-Elfe's ONO ❑NIA 5, Short Hold Time Analysis (a72hr): -!!�_Ye, [IN. ❑NIA 6. Rush Turn Around Time Requested: ❑resel�,'IJwA 7. Sufficient Volume: es ❑Ne ❑NIA g. Correct Containers Used: -Pace Containers Used: Yes ❑No Yes ❑No ❑NIA ❑NIA 9- Containers Intact: es ❑No ❑7wA 10. Filtered volume received for Dissolved tests ❑Yes ❑Na i 1, Sample Labels match COG: 64 -Includes dateltimellD/Anal sis Math ` ❑Yes - I^' ❑NIA 12 �C if n �.- - { t r Alt containers needing preservation have been checked. Alf containers needing preservation are found to be in compliance v th EPA recommendation. exceptions: VOA, coliform,'roc, O&G, WI-dRO (water) _ es ON. es ❑No ❑Yes ONO ❑NIA ©NIA �, 5 L, 13 � 1 _ i� d^ C'D ' Initial when completed Samples checked For dechlorination: es ❑No ❑NIA f 4. Headspace in VDA Vials t >6mmJ: es El NO ❑NIA 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # {if purchased), des ❑No _—PYe's ❑No ❑NIA ❑NIA 1C�. JV t L—' f tr l I �} La (c cy �. Client Notification) Resolution: Field Data Required? Y I N Person Contacted: /`j- K r,1¢.�.' _ Dateffime: 10 7 " Comments) Resolution: �rK ►` S7fa k � �42 rLs.-, A /f��rr�S � � Pe1G,r-5' SCURF Review: ! :ram Date: SRF Review: .� Date: Note: Whenever they a discrepancy aFTecling North Carolina compliance samples, a cap this form will be sent to the North Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers)