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WQ0002712_Regional Office Historical File Pre 2018 (4)
RECEIVED/NCDENR/DWR IdAR v 9 2020 435 Williams Court, Suite 100 Baltimore, bID 21220 wwwsynagro.com FEBRUARY 21, 2020 NCDEQ Division of Water Resoures . Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2019 Annual Report for Permit No. WQ0002712 Dear NCDEQ: WOROS SYN Air ZONAL OFFICE Synagro is submitting one copy and one electronic copy of the above referenced report on behalf of the City of Lincolnton, NC. If you have any questions or need additional information, please do not hesitate to contact Robert Pearson at (704) 736-8940 or Alex Fox at (336) 703-8681. Sincerely, I L Derrick Shivar Environmental Compliance Manager Enclosures cc: Robert Pearson, City of Lincolnton Alex Fox, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD CITY OF LINCOLNTON, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0002712 2019 ANNUAL REPORT City of Lincointon, NC Residuals Land Application Program 2019 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: WO0002712 County Lincoln Year 2019 Facility Name (as shown on permit) City of Lincolnton WWTP and WTP NPDES No. NC0025496 & 0085588 Land Application Operator Svnagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 54 Total number of fields utilized for land application during the year: 11 Total amount of dry tons applied during the year for all application sites: 350.91 Total number of acres utilized for land application during the year: 165.7 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2019 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations.` 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit. were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Robert Pearson, Water Services Director Pe 'tee Name and Tit (type or print) Signature of Preparer* ate (if different from Permittee) afore of Permittpe Date 21> Signature of Land Applier Date (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2019 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC LINCOLNTON, NC "UNCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS January 2019 142,600.00 G 16.35 D 14.83 February 2019 186,000.00 G 21.33 D 19.35 March 2019 514,600.00 G 36.90 D 33.48 April 2019 582,800.00 G 41.81 D 37.92 May 2019 403,000.00 G 36.98 D 33.53 June 2019 229,400.00 G 21.05 D 19.09 July 2019 713,000.00 G 65.40 D 59.33 August 2019 595,200.00 G 54.62 D 49.52 September 2019 285,200.00 G 19.74 D 17.90 October 2019 291,400.00 G 20.18 D 18.30 December 2019 155,000.00 G 16.55 D 15.00 YEARLY TOTAL 4,098,200.00 G 350.91 D 318.25 1/30/2020 SECTION 2 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002712 Laboratory Facility Name: LINCOLNTON, NC Waypoint Analytical Virginia Inc. NPDES# : NCO025496 or WQ# (residual only) WWTP Name: LINCOLNTON WWTP Residuals Analysis Data Product Type LIQ LIQ LIQ LIQ Date Sampled (grab) or 03/25/19 05/01/19 08/28/19 10/29/19 Date Composited Percent Solids 1.72 2.20 1.66 2.56 PARAMETERS (mg/kg dry weight) Arsenic <5 5.68 7.42 <19.2 Cadmium <1 <1 <1 <3.85 Mercury 0.0338 <0.0157 0.0433 <0.569 Chromium 39.7 43 43.3 53.8 Copper 319 191 190 255 Lead 16.5 7.6 10.8 16.8 Molybdenum 4.67 3.85 4.93 <9.62 Nickel 45.7 12.4 11.4 13.1 Selenium <5 <5 <5 <19.2 Zinc 462 190 235 260 Total Phosphorus 18900 16100 17700 27000 TKN 81200 71400 72900 78500 Ammonia -Nitrogen 30000 17300 36500 30200 Nitrate and Nitrite <4 . 87 285 <4. 66 <182 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �v v X �• Date (SIGNATURE OF PREPARER) DENR FORM RSSF (5/2003) Printed: Thursday - February 6, 2020 at 14:05:00 for: 2161 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002712 Laboratory Facility Name: LINCOLNTON, NC Waypoint Analytical Virginia Inc. NPDES# : NCO025496 or WQ# (residual only) WWTP Name: LINCOLNTON WWTP Residuals Analysis Data Product Type LIQ LIQ LIQ LIQ Date Sampled (grab) or 03/25/19 05/01/19 08/28/19 10/29/19 Date Composited Percent Solids 1.72 2.20 1.66 2.56 PARAMETERS (mg/kg dry weight) Aluminum 7870 7090 9090 9230 Calcium 7950 6490 7130 10300 Magnesium 3720 3270 3440 4850 pH 6.80 6.70 6.90 7.00 Potassium 4860 4350 5230 8460 Sodium 1620 1570 1870 3400' "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pejilties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X_ (SI I URE OF PREPARER) NR - Data Not Reported or Data Not Required Date Z /,/Z DENR FORM RSSF-B (7/2002) Printed: Thursday - February 6, 2020 at 14:06:02 for: 2161 01 Waypointo ANALYTICAL 4/3/2019 Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-085-0204 Project Description: Lincolnton WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 3/26/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, &� V 6—r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida E871087 North Carolina 257 South Carolina 93007 ' r' Page 1 of 6 • W���®' ■ ■��. 7621 (2) Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table --eport Number: 19-085-0204 Client Project Description: Lincolnton WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00• 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 65576 Lincolnton WWTP Solids 03/25/2019 08:00 03/26/2019 WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 SM-4500-NH3C WTN 9045D WTN 4500NO3F-2011 WTN 6010D WTN SW-7471B WTN SM-4500-NH3C-TKN WTN SM-2540G WTN Page 2 of 6 RE Number: 19-085-0204 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 65576 Sample Id : Lincolnton WWTP • y� Wa ®int,M ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WWTP REPORT OFANALYSIS Date Sampled: 3/25/2019 08:00:00 Date Received: 03/26/2019 00:00 Date Reported: 04/03/2019 Total Solids " 1.72 17200 100.0 CJR 04/01/2019 14:08 Moisture * 98.30 100.0 CJR 04/01/2019 14:08 Total Kjeldahl Nitrogen 8.12 81200 250 CLP 03/29/2019 12:30 Phosphorus 1.89 18900 50.0 JTR 04/01/2019 23:08 Potassium 0.49 4860 250 JTR 04/02/201913:08 Sulfur 0.63 6280 50.0 JTR 04/01/2019 23:08 Calcium 0.80 7950 250 JTR 04/01/2019 23:08 Magnesium 0.37 3720 50.0 JTR 04/01/2019 23:08 Sodium 0.16 1620 250 JTR 04/01/2019 23:08 Iron 5840 50.0 JTR 04/01/2019 23:08 Aluminum 7870 50.0 JTR 04/01/2019 23:08 Manganese 279 5.00 JTR 04/01/2019 23:08 Copper 319 2.50 JTR 04/01/2019 23:08 Zinc 462 12.5 JTR 04/01/2019 23:08 Ammonia Nitrogen 3.00 30000 100 JPJ 04/01/2019 13:00 Organic N 5.12 51200 250 03/29/2019 12:30 Nitrate+Nitrite-N <4.87 4.87 ZBD 04/01/201915:57 SM-2540G SM-2540G SM-4500-NH3C-TKN 601 OD 601 OD 601 OD 6010D 601 OD 6010D 6010D 6010D 6010D 601 OD 6010D SM-4500-NH3C CALCULATION 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time ?W4 P 6ew Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric MCGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 3 of 6 RE Number: 19-085-0204 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 65576 Sample Id : Lincolnton WWTP Cadmium Chromium Nickel Lead Arsenic Mercury Selenium pH * Molybdenum Comments: • Waypoint ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 3/25/2019 08:00:00 Date Received: 03/26/2019 00:00 Date Reported: 04/03/2019 <1.00 1.00 JTR 04/01/2019 23:08 601OD 39.7 2.50 JTR 04/01/2019 23:08 601OD 45.7 2.50 JTR 04/01/2019 23:08 6010D 16.5 3.00 JTR 04/01/2019 23:08 6010D <5.00 5.00 JTR 04/01/2019 23:08 6010D 0.0338 0.0157 TJS 03/29/2019 15:43 SW-7471 B <5.00 5.00 JTR 04/01/2019 23:08 6010D 6.8 JSL 04/01/2019 08:22 9045D 4.67 2.50 JTR 04/01/2019 23:08 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time awf�4 X 64w Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 6 WayPA®intn. NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46467 Customer Name: Synagro Central LLC/ Lincolnton Report Number: 19-085-0204 Shipping Method 0 Fed Ex 0 US Postal 0 Lab UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? is Yes 0 No Sample containers intact? ID Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. • Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No • N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: 0 Yes No Signature: lBrandi Watson Date & Time: 03/26/2019 11:09:20 Page 5 of 6 SAMPLING LOG # CHAUM OF CUSTODY �,p�p /� CUSTOMER: S 1f 11�fAGRO ILI II�IIIIII�IIIIIIIIIIII��IIIIIII IIIIIII�IIII�II'II�III�IIIIIIII�II gVnaoroCentral LLC/Ltncohlon Lincolnton WWTP 19-085-0204 4646 zols 11:07:23 RECORD & AMW YS 3 RECORD PROJECT MANAGER: 1 `� (ti per field sampling procedures he collection of these samples. Phone: (3 , ) 7a3�� SAMPLER A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED ^.r- a v-4 t%,% l,;,w -b'5rt sir C-0 ,%„p 3 ZS A w, k c-c c les Relinquished by Sampler: Date Time Recieved by: REMARKS: 312s 3 -, oa Relinquished by: , ^ ( Date, Time Reciy) Relinquished by: d Dat+ Time SPECIAL INSTRUCTIONS: 515� For 1. 1 L monitoring purposes. Recieved by: PO#: SAMPLE ANALYSIS REQUEST I.D. SLI SL2 NH4-N NO3 N OrgNanic Cd ct Ni Pb As Hg Se PH eq. Volatile Solids Mo Cl NO2 lrtrr� lam'" R400 !f " k4 yveo 110 Kam' Loo !-' A�o Aeo boo SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Rarige Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 3/25/2019 3/1/2019-4/30/2019 0.4911 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (1620 x 1.7200) + 100 = 27.864 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (7950 x 1.7200) + 100 = 136.74 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3720 x 1.7200) + 100 = 63.984 Na meq = Na mg/I = Molec.Wgt.Na = 27.864 _ 23 = 1.21148 Ca meq = Ca mg/I = Molec.Wgt.Ca = 136.74 + 20 = 6.837 Mg meq = Mg m.g/I = Molec.Wgt.Mg = 63.984 _ 12 = 5.332 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.21148 _ SgrRoot[0.5(6.837+5.332)] = 0.491138 Page 1 Printed: 2/6/2020 09:35 Waypointo ANALYTICAL 5/10/2019 Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-123-0204 Project Description: Lincolnton WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 'Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 5/3/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, P"a. P c�- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Virginia 460014 Page 1 of 7 Wpointay ANALYTICAL Client: Synagro Central LLC/ Lincolnton Project: Lincolnton WVVfP Lab Report Number: 19-123-0204 Date: 5/10/2019 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 66214 Analyte: Aluminum QC Batch No: L435144 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Arsenic QC Batch No: L435144 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Potassium QC Batch No: L435144 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Selenium QC Batch No: L435144 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Page 2 of 7 Waypoint.(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table ._eport Number: 19-123-0204 Client Project Description: Lincolnton WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 66199 Lincolnton WWTP Solids 05/01/2019 10:00 05/03/2019 66199 Lincolnton WWTP Solids 05/01/2019 10:00 05/03/2019 SM-4500-NH3C WTN 66199 Lincolnton WWTP Solids 05/O1/2019 10:00 05/03/2019 9045D WTN 66199 Lincolnton WWTP Solids 05/01/2019 10:00 05/03/2019 4500NO3F-2011 WTN 66199 Lincolnton WWTP Solids 05/01/2019 10:00 05/03/2019 6010D WTN 66199 Lincolnton WWTP Solids 05/01/2019 10:00 05/03/2019 SW-7471B WTN 66199 Lincolnton WWTP Solids 05/01/2019 10:00 05/03/2019 SM-4500-NH3C-TKN WTN 66199 Lincolnton WWTP Solids 05/O1/2019 10:00 05/03/2019 SM-2540G WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 3 of 7 RE I Number: 19-123-0204 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 66199 Sample Id : Lincolnton WWTP Total Solids Moisture * Total Kjeldahl Nitrogen Phosphorus Potassium Sulfur Calcium Magnesium Sodium Iron Aluminum Manganese Copper Zinc Ammonia Nitrogen Organic N Nitrate+Nitrite-N D Waypoint( ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WWTP REPORT OF ANALYSIS 2.20 22000 100.0 CJR 97.80 100.0 CJR 7.14 71400 250 JPJ 1.61 16100 50.0 BKN 0.44 4350 50.0 BKN 0.54 5430 50.0 BKN 0.65 6490 250 BKN 0.33 3270 50.0 BKN 0.16 1570 250 BKN 5010 50.0 BKN 7090 50.0 KKM 248 5.00 BKN 191 2.50 BKN 190 12.5 BKN 1.73 17300 100 JPJ 5.41 54100 250 285 4.75 ZBD Date Sampled: 5/1/2019 10:00:00 Date Received: 05/03/2019 00:00 Date Reported: 05/10/2019 05/08/2019 14:34 05/08/2019 14:34 05/09/2019 10:00 05/08/2019 18:21 05/08/2019 18:21 05/08/2019 18:21 05/08/2019 18:21 05/08/2019 18:21 05/08/2019 18:21 05/08/2019 18:21 05/09/2019 18:37 05/08/2019 18:21 05/08/2019 18:21 05/08/2019 18:21 05/09/2019 12:00 05/09/2019 10:00 05/09/2019 12:47 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. SM-2540G SM-2540G SM-4500-NH3C-TKN 6010D 6010D 6010D 6010D 601 OD 601 OD 601 OD 601 OD 6010D 6010D 6010D SM-4500-NH3C CALCULATION 4500NO3F-2011 ?W�r- XV 610wr Pauric McGroary Agronomist Page 4 of 7 RE Number: 19-123-0204 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 66199 Sample Id : Lincolnton WWTP s WaypoitM ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WWTP REPORT OFANALYSIS Date Sampled: 5/1/2019 10:00:00 Date Received: 05/03/2019 00:00 Date Reported: 05110/2019 Cadmium <1.00 1.00 BKN 05/08/201918:21 601OD Chromium 43.0 2.50 BKN 05/08/201918:21 601OD Nickel 12.4 2.50 BKN 05/08/201918:21 601OD Lead 7.60 3.00 BKN 05/08/201918:21 6010D Arsenic 5.68 5.00 BKN 05/08/201918:21 6010D Mercury <0.0157 0.0157 TJS 05/08/2019 11:45 SW-7471 B Selenium <5.00 5.00 BKN 05/08/201918:21 6010D pH * 6.7 JSL 05/08/2019 07:50 9045D Molybdenum 3.85 2.50 BKN 05/08/201918:21 6010D Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time I�G il'�C GQ4Ny Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 5 of 7 WayPAoint.' NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46467 Customer Name: Synagro Central LLC/ Lincolnton Report Number: 19-123-0204 Shipping Method 0 Fed Ex 0 US Postal 0 Lab is UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 40 Yes 0 No Sample containers intact? 41 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr) 7 High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: lBrandi Watson Date & Time: 05/03/2019 14:06:04 Page 6 of 7 SAMPLING LOG # CUSTOMER: SiYNAGRO PROJECT MANAGER: �� 2L,�)ru Phone. (33fc 19-123-0204 05--03-2019 Svnaqro Central LLCI Lincolnton 14:03:38 Lincolnton VW11TP INC. CHAEN OF CUSTODY RECORD ac AMAILYSPS RECORD i attest that the proper field sampling procedures were used during the collection of these samples. l+ SAM R A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED Relinquished by Sampler: Date Time - Recleved by: REMARKS: S Z- (c A,,, Relinquished by: . 1DILte I Time Recieveot�-� Relinquished by: D to Time SPECIAL INSTRUCTIONS: U1 ^ �` tqor H C -- monitoring purposes. rcre-Mi Recieved by: To, P L(, r-OGc/5' PO#: j SAMPLE ANALYSIS REQUEST I.D. SLI SLB NH4-N NO3-N Organic N Cd CY Ni Pb As H9 Se PH CaCO3 equiv. Volatile Solids Mo. Cl NO2-N W"i-l< !�` J0'" lam" POOO ;000 S-40 9100 1-0 1100 1�0 Ao�o §AO Pao ;'" SLB: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc Page 7 of 7 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 5/1/2019 5/1/2019-8/30/2019 0.5860 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (1570 x 2.2000) _ 100 = 34.54 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (6490 x 2.2000) = 100 = 142.78 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3270 x 2.2000) = 100 = 71.94 Na meq = Na mg/I _ Molec.Wgt.Na = 34.54 = 23 = 1.50174 Ca meq = Ca mg/I = Molec.Wgt.Ca = 142.78 = 20 = 7.139 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 71.94 + 12 = 5.995 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.50174 = SgrRoot[0.5(7.139+5.995)] = 0.586018 Printed: 2/6/2020 Page 1 09:35 Waypoint.0 ANALYTICAL 9/9/2019 Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-241-0004 Project Description: LINCOLNTON WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 8/29/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, P,a' P &—/- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Virginia 460014 7yLr, 5 - Page 1 of 6 Wav O ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointana"cal.com Sample Summary Table ..eport Number: 19-241-0004 Client Project Description: LINCOLNTON WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 SM-4500-NH3C WTN 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 9045D WTN 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 4500NO3F-2011 WTN 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 6010D WTN 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 SW-7471B WTN 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 SM-4500-NH3C-TKN WTN 67994 LINCOLNTON WWTP Solids 08/28/2019 12:10 08/29/2019 SM-2540G WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 Re Number: 19-241-0004 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 67994 Sample Id: LINCOLNTON WWTP Total Solids Moisture * Total Kjeldahl Nitrogen Phosphorus Potassium Sulfur Calcium Magnesium Sodium Iron Aluminum Manganese Copper Zinc Ammonia Nitrogen Organic N Nitrate+Nitrite-N 1.66 98.30 7.29 1.77 0.52 0.58 0.71 0.34 0.19 3.65 3.64 o Wav poin� ANALYTICAL 72900 17700 5230 5780 7130 3440 1870 8600 9090 221 190 235 36500 36400 <4.66 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: LINCOLNTON WWTP REPORT OF ANALYSIS 250 50.0 50.0 50.0 250 50.0 250 50.0 50.0 5.00 2.50 12.5 100 250 4.66 ADM ADM JPJ JTR JTR JTR JTR JTR JTR JTR JTR JTR JTR JTR JPJ ZBD Date Sampled: 8/28/2019 12:10:00 Date Received: 08/29/2019 00:00 Date Reported: 09/09/2019 08/30/2019 15:57 08/30/2019 15:57 09/06/2019 09:00 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/05/2019 21:22 09/06/2019 14:30 09/06/2019 09:00 09/04/2019 15:17 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. SM-2540G SM-254OG SM-4500-NH3C-TKN 601OD 601 OD 601OD 601OD 601OD 601OD 601OD 601OD 601OD 601OD 601OD SM-4500-NH3C CALCULATION 4500NO3F-2011 Pauric McGroary Agronomist Page 3 of 6 Re Number: 19-241-0004 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 67994 Sample Id: LINCOLNTON WWTP Wav0 P01t. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: LINCOLNTON WWTP REPORT OF ANALYSIS Date Sampled: 8/28/2019 12:10:00 Date Received: 08/29/2019 00:00 Date Reported: 09/09/2019 Cadmium <1.00 1.00 JTR 09/05/2019 21:22 601 OD Chromium 43.3 2.50 JTR 09/05/2019 21:22 6010D Nickel 11.4 2.50 JTR 09/05/2019 21:22 601 OD Lead 10.8 3.00 JTR 09/05/2019 21:22 601 OD Arsenic 7.42 5.00 JTR 09/05/2019 21:22 6010D Mercury 0.0433 0.0151 TJS 09/04/2019 13:52 SW-7471 B Selenium <5.00 5.00 JTR 09/05/2019 21:22 6010D pH * 6.9 JSL 09/04/2019 06:13 9045D Molybdenum 4.93 2.50 JTR 09/05/2019 21:22 6010D Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond holding time !"C 1 011 f Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Agronomist Page 4 of 6 ( b Way �®' �� 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Cooler Receipt Form Customer Number: 46467 Customer Name: Synagro Central LLC/ Lincolnton Report Number: 19-241-0004 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: 4 Shipping container/cooler uncompromised? • Yes 0 No Number of coolers received F- Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample Iabel(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? IS Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F— High concentration container (48 hr) F— Low concentration EnCore samplers (48 hr) F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: IBrandi Watson Date & Time: 08/29/2019 13:57:21 Page 5 of 6 SAMPLING LOG # CUSTOMER: SYNAGR® 1111111111111111111111111111111111111111111111111111111 1646 1.0004 vnagro Central LLCI LinColnlon 1111118 4467 LINCOLNWWTP 13:54:34:5q;34TON 19 PROJECT MANAGER: _ Plex IL�� Phone:( 33 �, 7-0 3 A & L CUSTOMER SAMPLING SAMPLE LAB # SAMPLE I.D. LOCATION TYPE L-i/lia_IAfin tl(Alr J�L!l sCI num iquisneq oy sampler: C Relinquished by: Relinquished by: SPECIAL INSTRUCTIONS: blql Fnr monitoring purposes. Date Date Time I ;ja Time Time ABS, INC. MAN OF C US ©©v RECORD st that the proper field sampling procedures were sed during the collection of these samples. SAMP R # OF SAMPLING METHOD METHOD CONTAINERS DATE TIME PRESERVED SHIPPED T/Zk/c I L.Ib -tc-z' 1QPS Recieved by: S Recieved by: Recieved by: PO#: REMARKS: SAMPLE ANALYSIS REQUEST I.D. SL9 SL2 NHN N0N Or a 3Nnic Gd Cr Ni Pb As Hg Se PHCaCO3 Volatile Mo. Clequiv. Solids NO I z-N I I SI-1: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SLI plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum,Manganese, Copper and Zinc Page 6 of 6 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 8/28/2019 91112019-10/31/2019 0.5841 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (1870 x 1.6600) _ 100 = 31.042 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (7130 x 1.6600) _ 100 = 118.358 Mg mg/I = (mg mg/kg x % Solids) + 100 = (3440 x 1.6600) + 100 = 57.104 Na meq = Na mg/I + Molec.Wgt.Na = 31.042 = 23 = 1.34965 Ca meq = Ca mg/I + Molec.Wgt.Ca = 118.358 + 20 = 5.9179 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 57.104 _ 12 = 4.75867 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.34965 + SgrRoot[0.5(5.9179+4.75867)] = 0.584146 Printed: 2/6/2020 Page 1 09:36 Waypointo ANALYTICAL 11 /8/2019 Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-304-0001 Project Description: Lincolnton WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary -Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 10/31/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, F'Wi� 0 6, -0- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 Waypoeinto ANALYTICAL Client: Synagro Central LLC/ Lincolnton Project: Lincolnton WWTP Lab Report Number: 19-304-0001 Date: 11 /7/2019 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 69303 Analyte: Calcium QC Batch No: L462918 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 2 of 7 0 Waypoint ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table ..Sport Number: 19-304-0001 Client Project Description: Lincolnton WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 SM-4500-NH3C WTN 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 9045D WTN 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 4500NO3F-2011 WTN 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 6010D WTN 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 SW-7471B WTN 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 SM-4500-NH3C-TKN WTN 69302 Lincolnton WWTP Solids 10/29/2019 11:30 10/31/2019 SM-2540G WTN WTN: Waypoint Analytical - TN, Memphis, TN Page 3 of 7 Waypoi to ANALYTICAL 46467 Synagro Central LLC/ Lincolnton 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Mary Brewer Project Lincolnton WWTP Report Date : 11/08/2019 284 Boger Road Information : Received : 10/31/2019 Mocksville , NC 27028 60wr Report Number :19-304-0001 REPORT OPANALYSIS Pauric McGroary Agronomist Lab No : 69302 Matrix: Solids Sample ID : Lincolnton WWTP Sampled: 10/29/2019 11:30 Moisture 97.4 % 0.010 1 11/04/1917:15 ADM SM-254OG Selenium <19.2 mg/Kg - dry 19.2 1 11/05/19 00:18 JTR 6010D Total Solids 2.56 % 0.010 1 11/04/19 17:15 ADM SM-254OG Total Kjeldahl Nitrogen 78500 mg/Kg - dry 9620 1 11/06/19 10:00 JPJ iM-4500-NH3C-TKP Phosphorus 27000 mg/Kg - dry 192 1 11/05/19 00:18 JTR 6010D Potassium 8460 mg/Kg - dry 192 1 11/05/19 00:18 JTR 6010D Sulfur 8500 mg/Kg - dry 192 1 11/05/19 00:18 JTR 6010D Calcium 10300 mg/Kg - dry 962 1 11/05/19 00:18 JTR 6010D Magnesium 4850 mg/Kg - dry 192 1 11/05/19 00:18 JTR 6010D Iron 11000 mg/Kg - dry 192 1 11/05/19 00:18 JTR 6010D Manganese 245 mg/Kg - dry 19.2 1 11/05/19 00:18 JTR 6010D Copper 255 mg/Kg - dry 9.62 1 11/05/19 00:18 JTR 6010D Organic N 48100 mg/Kg - dry 9620 1 11/06/19 10:00 CALCULATION Nitrate+Nitrite-N <182 mg/Kg - dry 182 1 11/06/19 14:18 ZBD 4500NO3F-2011 Nickel 13.1 mg/Kg - dry 9.62 1 11/05/19 00:18 JTR 6010D Mercury <0.569 mg/Kg - dry 0.569 1 11/05/19 16:21 TJS SW-7471B pH 7.0 s.u. 1 11/05/19 06:18 JSL 9045D Qualifiers/ * Outside QC Limit B Analyte detected in blank Definitions C GCMS Confirmation Analysis E Result above cal range g GGA Outside QC Limits H Beyond holding time J Estimated value M Minimum value NA Not on Scope of Accreditation NC Not confirmed Q RPD >40% dual column results T Sample exhibits toxicity U Unconfirmed Refer to cover letter. Page 4 of 7 Waypointo ANALYTICAL 46467 Synagro Central LLC/ Lincolnton 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Mary Brewer Project Lincolnton VW TP Report Date : 11/08/2019 284 Boger Road Information : Received : 10/31/2019 Mocksville , NC 27028 pa�4 X Ge°'r Report Number : 19-304-0001 REPORT OFANAL YSIS Pauric McGroary Agronomist Lab No : 69302 Matrix: Solids Sample ID: Lincolnton WWTP Sampled: 10/29/2019 11:30 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 30200 mg/Kg - dry 3850 1 11/06/19 14:00 JPJ SM-4500-NH3C Aluminum 9230 mg/Kg - dry 192 1 11/05/19 00:18 JTR 6010D Arsenic <19.2 mg/Kg - dry 19.2 1 11/05/19 00:18 JTR 6010D Cadmium <3.85 mg/Kg - dry 3.85 1 11/05/19 00:18 JTR 6010D Chromium 53.8 mg/Kg - dry 9.62 1 11/05/19 00:18 JTR 6010D Lead 16.8 mg/Kg - dry 11.5 1. 11/06/19 17:14 KKM 6010D Molybdenum <9.62 mg/Kg - dry 9.62 1 11/05/19 00:18 JTR 6010D Sodium 3400 mg/Kg - dry 962 1 11/05/19 00:18 JTR 6010D Zinc 260 mg/Kg - dry 48.1 1 11/05/19 00:18 JTR 6010D Qualifiers/ B Analyte detected in blank H Beyond holding time Definitions Page 5 of 7 (D WayPA�int NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46467 Customer Name: Synagro Central LLC/ Lincolnton Report Number: 19-304-0001 Shipping Method 0 Fed Ex 0 US Postal 0 Lab • UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? ID Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. ® Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No ® N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No • N/A F— High concentration container (48 hr) F— Low concentration EnCore samplers (48 hr) F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 41 No Comments: Signature: lBrandi Watson Date & Time: 10/31/2019 12:57:54 Page 6 of 7 I i L: Cllrnt Nam,/Add,,„ h ,C�o (n Pro)ert OcstrYptlon Prol eri Number ANALYTICAL 76<1 Whltrl.mr NuaJ Ntc}unaad, VA f8t14) 271 �nd-0b C l+enl ProJen ManaC,rf[oiria+t Uilhng Inlortna6on - Prn)eq/sits tnratlan ftlty/statcJ NlIs11-AdOgionai Nlugee ..oVW N 0,4c ltl Non ,hn+il,J Dat, „LIMults Nc.deJ Pm)an. Manager Ph— a 3 3� - 7o Project Mnnagef Email SeA4�o .C-0 u � M Y g s Unlei, natal, all cnntatncn R Part � ¢ Y c IZZI perl able ll of `i0 CI E n 236. 2 � u Requii simpl,IArnti6Calinn � 1 l 1 Go A f6r La 6Ni a.r„y Ice Custody LatlCDmmenu Seals rr YIN I f 5 sampfXd IJ1amcz�/x rc7 > - Belinqulshed by: I t iATUREL Relinquished by: ISIGN TUR Relinquished by: (SIGNATUlIEj of?; onr t:ihorntory Use Only «' IIIIIIIIIIIIIIIIIIIIIIIIIIiIINIIIIIIIIIIIIINIIIIIIIIIIIIIIIIIII 7646 ¢°°°' Svnagro Central LLCI Lincolnfon 31 2019 3 Lincelnlon WWTP 12:57:30 Gient Remarks/Comments Time Recelved by: 2 Time I Re[elvedkY A Cao1•LG[na�RaltMivotkhl g Cnol . 6i w1stN PNc2 n None a.,wked [ Nagn PNY1t) F iNos olia2 G iKL PNa2 11 NIPn1 PRQ 1 Cool t. 6C NgIS103 `l Commen[slNotrs -Dste .Tlttie t: k.? - Date . Tltltc ?Date . T1tnc: �^ s Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 10/29/2019 11/112019-12/3112019 1.1033 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (3400 x 2.5600) = 100 = 87.04 Ca mg/1 = (Ca mg/kg x % Solids) _ 100 = (10300 x 2.5600) + 100 = 263.68 Mg mg/I = (mg mg/kg x % Solids) = 100 = (4850 x 2.5600) _ 100 = 124.16 Na meq = Na mg/I _ Molec.Wgt.Na = 87.04 + 23 = 3.78435 Ca meq = Ca mg/I + Molec.Wgt.Ca = 263.68 _ 20 = 13.184 Mg meq = Mg mg/I z- Molec.Wgt.Mg = 124.16 _ 12 = 10.3467 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.78435 = SgrRoot[0.5(13.184+10.3467)] = 1.10329 Printed: 2/6/2020 Page 1 09:36 SECTION 3 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LOYD OWNER: TURBYFILL PROPERTIES PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 10.83 SITE #: NC CA 00035 FIELD# : CA 00035 0002 A OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 4.90 ACRES PERMITTED: 4.90 Page Lime Applied *** Date Lbs/Ac Gallons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - ova Tons Cond. Precip, cation tili- ali- Ammonia Nitrate PAN Total Per Acre DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and m (pp ) Crop p Acre Source Moist Hours * Rate** Rate Nitrite 3/22/19 55,800.00 (G) 11387.755 1,72 0.817 LIL DRY 0-<1/211 SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE Mar-19 55,800.00 (G) 11,387.755 8/1/19 74,400.00 (G) 1 15183.6731 2.20 1.393 LIL DRY 0-<1/211 SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19715 FESCUE PASTURE Aug-19 74,400.00 (G) 15,183.673 1 ruLai vauons/Ac: Total Wet Tons/Ac: T..,...1 l'...L._ T 66,J / 1.41 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 96 0.024 0.004 0.185 1.053 0.048 <.001 0.018 0.109 0.022 1.284 75.73 Cumulative lbs/acre 0.372 0.166 5.760 18.743 1.623 0.053 0.562 1.895 0.345 31.975 Ji Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 F LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID x .1. 711014 C.9 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LOYD OWNER: TURBYFILL PROPERTIES PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 12.51 SITE #: NC CA 00035 FIELD# : CA 00035 0002 B OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40 Page Lime Applied *** Date Lbs/Ac Gallons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I Per Acre DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop Acre Source Moist Hours * Rate** Rate Nitrite 7/29/19 136,400.00 (G) 21312.500 2.20 1.955 LIL DRY 0-<I/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE Jul-19 136,400.00 (G) 1 21,312.500 1 i otai (tattons/Ac: Total Wet Tons/Ac: 21,312.50 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 77 0.022 0.004 0.168 0.747 0.030 <.001 0.015 0.048 0.020 0.743 62.96 Cumulative lbs/acre 0.397 0.174 5.762 19.472 1.753 0.056 0.589 1.998 0.351 34.558 f Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 140 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL=LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID �r X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LOYD OWNER: TURBYFILL PROPERTIES PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 27.87 SITE #: NC CA 00035 FIELD# : CA 00035 0002 C OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page Lime Applied *** Date LWAc allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I Per Acre DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Acre Source Moist Hours * Rate** Rate Nitrite 6/3/19 111,600.00 (G) 11272.727 2.20 1.034 LR DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE 6/4/19 117,800.00 (G) 11898.990 2.20 1.092 LIL DRY 0-<I/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE Jun-19 1 229,400.00 (G) 23,171.717 8/1/19 24,800.00 (G) 2505.051 12.20 0.231 LIL DRY 0-<I/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 I FESCUE PASTURE 8/2/19 49,600.00 (G) 5010-1011 2.20 0.460 LIL MOIST 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19751 FESCUE PASTURE Aug-19 74,400.00 (G) 7,515.152 Total Gallons/Ac: Total Wet Tons/Ac: 30,686.87 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 111 0.032 0.006 0.242 1.075 0.043 <.001 0.022 0.070 0.028 1.070 90.65 Cumulative lbs/acre 0.392 0.174 5.715 19.027 1.639 0.054 0.572 1.884 0.354 32.195 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ; 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0003 A RESIDUAL SOURCE(S): See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 82.25 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 41.60 ACRES PERMITTED: 41.60 Page Lune Applied *** Date Lbs/Ac Gallons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I Per Acre DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Acre Source Moist Hours * Rate" Rate Nitrite 4/24/19 86,800.00 (G) 2086.538 1.72 0.150 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE 4/25/19 130,200.00 (G) 3129.808 1.72 0.224 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE 4/26/19 130,200.00 (G) 3129.808 1.72 0.224 LIL. DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE 4/29/19 62,000.00 (G) 1490.385 1.72 0.107 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE Apr-19 409,200.00 (G) 9,836.539 7/3/19 124,000.00 (G) 2980.769 2.20 0.273 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19715 FESCUE PASTURE 7/5/19 130,200.00 (G) 3129.808 2.20 0.287 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE 7/10/19 136,400.00 (G) 3278.846 2.20 0.301 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 I FESCUE PASTURE 7/I1/19 93,000.00 (G) 2235.577 2.20 0.205 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 I FESCUE PASTURE 7/12/19 93,000.00 (G) 2235.577 2.20 0.205 LIL DRY 0-<I/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE Jul-19 576,600.00 (G) 13,860.577 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LOYD OWNER: TURBYFILL PROPERTIES PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 82.25 SITE #: NC CA 00035 FIELD# : CA 00035 0003 A OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 41.60 ACRES PERMITTED: 41.60 Page : 2 Lime Applied *** Date LbsAc Gallons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Site Inches Appli- Vola- Miner - oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I DATE or Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Per Acre Acre Source Moist Hours * Rate** Rate Nitrite G0,u7 /." Total Wet Tons/Ac: TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 86 0.022 0.004 0.165 0.936 0.043 <.001 0.016 0.096 0.020 1.135 67.61 Cumulative Ibs/acre 0.269 0.142 5.600 17.642 1.455 0.050 0.515 1.731 0.316 27.554 3 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 124 FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 i 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X -�0/� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LOYD OWNER: TURBYFILL PROPERTIES PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 12.45 SITE #: NC CA 00035 FIELD# : CA 00035 0003 B OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 8.80 ACRES PERMITTED: 8.80 Page Lime Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total Per Acre Acre Source Moist Hours * Rate** Rate Nitrite 4/27/19 124,000.00 (G) 14090.909 1.72 1.011 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE 4/29/19 49,600.00 (G) 5636.364 1.72 0.404 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 FESCUE PASTURE Apr-19 1 173,600.00 (G) 19,727.273 i mai uauons/Ac: Total Wet Tons/Ac: TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 71 0.014 0.003 0.112 0.903 0.047 <.001 0.013 0.129 0.014 1.307 53.48 Cumulative lbs/acre 0.292 0.138 5.159 26.917 1.466 0.050 0.480 1.744 0.295 26.149 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 1 375.0 89.0 2500.0 LIL=LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID LX /v z0 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LLOYD OWNER: CHUCK WATERS PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 57.42 SITE #: NC LT 00019 FIELD# : LT 00019 0001 A OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 21.00 ACRES PERMITTED: 41.80 Page Lnne Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I Per Acre DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Acre Source Moist Hours * ' Rate** Rate Nitrite 1/31/19 142,600.00 (G) 6790.476 2.75 0.779 LIL MOIST 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 FESCUE PASTURE Jan-19 142,600.00 (G) 6,790.476 2/1/19 186,000.00 (G) 8857.1431 2.75 1.016 LIL MOIST 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16921 FESCUE PASTURE Feb-19 186,000.00 (G) 8,857.143 9/12/19 68,200.00 (G) 3247.619 1.66 0.225 LIL DRY 0-<1/2" SUR 0.5 0.20 72,900. p 36,500.00 p 4.66 p 25535 FESCUE PASTURE 9/13/19 155,000.00 (G) 7380.952 1.66 0.511 LIL DRY 0-<1/2" SUR 0.5 0.20 72,900. p 36,500.00 p 4.66 p 25535 FESCUE PASTURE 9/16/19 62,000.00 (G) 2952.381 1.66 0.204 LIL DRY 0-<1/2" SUR 0.5 0.20 72,900. p 36,500.00 p 4.66 p 25535 FESCUE PASTURE Sep-19 285,200.00 (G) 13,580.952 Total Gallons/Ac: Total Wet Tons/Ac: 29,228.57 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 109 0.039 0.005 0.248 1.132 0.060 <.001 0.030 0.062 0.027 1.547 115.10 Cumulative lbs/acre 0.229 0.083 7.834 15.646 0.855 0.032 0.491 1.062 0.206 16.461 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop f _.- ....__. _._._..- 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 i 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 FACILITY NAME: LINCOLNTON, NC OWNER: CHUCK WATERS SITE #: NC LT 00019 FIELD# : LT 00019 0001 B RESIDUAL SOURCE(S): See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 53.08 OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.80 ACRES PERMITTED: 41.80 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I Per Acre DATE or Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Acre Source Moist Hours * Rate** Rate Nitrite 3120/19 186,000.00 (G) 8942.308 1.72 0.641 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 SORGHUM/SUDAN PASTURE 3/21/19 161,200.00 (G) 7750.000 1.72 0.556 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 SORGHUM/SUDAN PASTURE 3/22/19 111,600.00 (G) 5365.385 1.72 0.385 LIL DRY 0-<1/2" SUR 0.5 0.20 81,200. p 30,000.00 p 4.87 p 25245 SORGHUM/SUDAN PASTURE Mar-19 458,800.00 (G) 22,057.693 10/15/19 186,000.00 (G) 8942.308I 1.66 0.619 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,900. p 36,500.00 p 4.66 p 25535 I SORGHUM/SUDAN PASTURE 10/17/19 105,400.00 (G) 5067.308 1.66 0.351 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,900. p 36,500.00 p 4.66 p 25535 SORGHUM/SUDAN PASTURE Oct-19 291,400.00 (G) 14,009.616 Total Uallons/Ac: Total Wet Tons/Ac: 36,067.31 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 129 0.030 0.005 0.210 1.378 0.073 <.001 0.024 0.167 0.026 1.918 94.13 Cumulative lbs/acre 0.220 0.082 7.796 15.892 0.868 0.032 0.485 1.166 0.204 16.831 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 207 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 ( 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X A (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LLOYD OWNER: CHUCK WATERS PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 14.79 SITE #: NC LT 00019 FIELD# : LT 00019 0002 OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 12.70 ACRES PERMITTED: 12.70 Page Lime Applied *** Date Lbs Ac DATE or MONTH Gallons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm ) Crop p Total Per Acre Acre Source Moist Hours * Rate** Rate Nitrite 5/20/19 111,600.00 (G) 8787.402 2.20 0.806 LIL DRY 0-<I/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE 5/21/19 49,600.00 (G) 3905.512 2.20 0.358 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE May-19 161,200.00 (G) 12,692.914 Total Uallons/Ac: Total Wet Tons/Ac: 12,692.91 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 46 0.013 0.002 0.100 0.445 0.018 <.001 0.009 0.029 0.012 0.442 37.50 Cumulative lbs/acre 0.283 0.136 26.815 17.279 2.469 0.090 0.808 1.632 0.221 28.084 i Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 ? { 375.0 89.0 2500.0 " LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X 2/v Aa (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: .LINCOLNTON, NC PREDOMINANT SOIL SERIES: CECIL OWNER: JEFF LINGERFELT PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 40.95 SITE #: NC LT 00036 FIELD# : LT 00036 0002 OPERATOR: JEFF LINGERFELT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 17.50 ACRES PERMITTED: 17.50 Page Lime Applied *** Date Lbs/Ac DATE or MONTH allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop Total I Per Acre Acre Source Moist Hours * Rate** Rate Nitrite 8/12/19 111,600.00 (G) 6377.143 2.20 0.585 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE 8/13/19 148,800.00 (G) 8502.857 2.20 0.780 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE 8/16/19 117,800.00 (G) 6731.429 2.20 0.618 LIL MOIST 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE 8/19/19 68,200.00 (G) 3897.143 2.20 0.358 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 FESCUE PASTURE Aug-19 1 446,400.00 (G) 25,508.572 i otai vanonsiAc: Total Wet Tons/Ac: 15,5U8.57 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual Ibs/acre 92 0.027 0.005 0.201 0.894 0.036 <.001 0.018 0.058 0.023 0.889 75.35 Cumulative lbs/acre 0.105 0.034 2.967 5.745 0.249 0.009 0.184 0.448 0.095 6.9-7 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop 156 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 E.— 1339.0 267.9 15.0 I 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X .� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME : LINCOLNTON, NC PREDOMINANT SOIL SERIES: CECIL OWNER: JEFF LINGERFELT PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 17.43 SITE #: NC LT 00036 FIELD# : LT 00036 0003 OPERATOR: JEFF LINGERFELT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 8.60 ACRES PERMITTED: 8.60 Page Lime Applied *** Date Lbs/Ac Gallons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total I Per Acre DATE or MONTH Solids Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop Acre Source Moist Hours * Rate** Rate Nitrite 5/21/19 6,200.00 (G) 720.930 2.20 0.066 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 SOYBEANS 5/22/19 55,800.00 (G) 6488.372 120 0.595 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 SOYBEANS 5/23/19 55,800.00 (G) 6488.372 2.20 0.595 LIL, DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 SOYBEANS May-19 117,800.00 (G) 13,697.674 12/7/19 31,000.00 (G) 3604.651 12.56 1 0.385 LIL DRY "0-<l/2" SUR 0.5 0.20 78,500. p 30,200.00 p 182.00 p 24902 I WHEAT 12/9/19 31,000.00 (G) 3604.651 2.56 0.385 LIL, MOIST "0-<1/2" SUR 0.5 0.20 78,500. p 30,200.00 p 182.00 p 24902 WHEAT Dec-19 62,000.00 (G) 7,209.302 1 otal Gallons/Ac: 2U,91)6.98 Total Wet Tons/Ac: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 50 0.044 0.008 0.191 0.873 0.045 0.001 0.024 0.051 0.042 0.878 82.02 38 Cumulative lbs/acre 0.157 0.042 3.351 7.025 0.319 0.013 0.238 0.523 0.137 8.541 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 185 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID x 4 C�7-- 0?// kr 0/ez 0 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, 1NJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: CECIL OWNER: JOANNE LEATHERMAN PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 21.30 SITE #: NC LT 00036 FIELD# : LT 00036 0005 OPERATOR: JEFF LINGERFELT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S): See list at bottom of report ACRES UTILIZED: 13.50 ACRES PERMITTED: 13.50 Page Lime Applied *** Date +_Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Total Per Acre DATE or MONTH Solids per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptn) Crop Acre Source Moist Hours * Rate** Rate Nitrite 5/21/19 12,400.00 (G) 918.519 2.20 0.084 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 SOYBEANS 5/22/19 55,800.00 (G) 4133.333 2.20 0.379 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 SOYBEANS 5/23/19 55,800.00 (G) 4133.333 2.20 0.379 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 17,300.00 p 285.00 p 19755 SOYBEANS May-19 124,000.00 (G) 9,185.185 12/7/19 74,400.00 (G) 5511.111I 2.56 0.511 LIL DRY "0-<1/2" SUR 0.5 0.20 78,500. p 30,200.00 p 182.00 p 24902 I WHEAT 12/9/19 18,600.00 (G) 1377.778 2.56 0.147 LIL MOIST 110-<l/2" SUR 0.5 0.20 78,500. p 30,200..00 p 182.00 p 24902 WHEAT Dec-19 93,000.00 (G) 6,888.889 iorat (jartonsi.vc: Total Wet Tons/Ac: 16,U74.U7 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual Ibs/acre 33 0.038 0.007 0.152 0.697 0.038 <.001 0.021 0.040 0.037 0.703 66.85 37 Cumulative lbs/acre 0.149 0.041 2.582 6.326 0.289 0.011 0.211 0.434 0.128 8.097 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 185 50 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X �Ar " �/✓ �J (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2020 SECTION 4 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Alex Fox Project Name: Lincolnton Lot Number:U106072 Date Completed:09/26/2019 09/26/2019 4:56 PM Approved and released by: Lab Director - Greenville: Lucas Odom Q`� '�-- `9eORAroDODELAP ACCREDITED The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 13 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: U106072 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP The initial sample amount used for the following sample deviated from the standard procedure: U106072- 001. Due to a low amount of % solids, the initial amount of the samples were weighed out to about 3.0 g instead of 1.0g. The LOQ has been adjusted accordingly. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 13 Client:Synagro Laboratory ID:U106072-001 Description: Lincolnton WWTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 1.39 09/07/2019 0416 )ate Received: 09/0612019 Inorganic non-metals un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 09/07/2019 0416 MDD 28205 1 350.1 (Ammonia - N ) 350.1 20 09/13/2019 1525 DFR 28582 1 (Ignitability) 1010A 1 09/26/2019 1200 SLC 30162 1 (Nitrate - N) 9056A 1 09/17/2019 1644 GMH 29171 1 (Nitrite - N) 9056A 1 09/17/2019 1644 GMH 29240 1 (pH) 9045D 1 09/09/2019 2034 HET 28337 1 (Phosphorus) 365.1 5 09/17/2019 1411 DMA 09/16/2019 0926 29064 1 (Reactive Cya) 7.3.3 1 09/11/2019 2054 MSG 09/09/2019 0934 1 (Reactive Sul) 7.3.4 1 09/10/2019 1655 HET 09/09/2019 0934 1 351.4 (TKN) 351.2 1 09/12/2019 1037 DMA 09/11/2019 1806 28644 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 2540G 1.39 % 1 Ammonia - N (gas diffusion) 350.1 41000 1400 750 mg/kg 1 Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 0 o F 1 Nitrate - N (soluble) 9056A 52 36 1.8 mg/kg 1 Nitrite - N (soluble) 9056A 65 14 1.4 mg/kg 1 Soil pH measured in water @ 22.3 ° C 9045D 7.0 su 1 Phosphorus 7723-14-0 365.1 12000 1800 360 mg/kg 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 TKN 351.2 70000 1800 1800 mg/kg 1 TCLP Volatiles un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260D 10 09/14/2019 0316 JTH 28924 09/12/2019 1814 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 8260D ND 0.050 0.0040 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 0.020 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0.050 0.0040 mg/L 1 Chlorobenzene 108-90-7 8260D ND 0.050 0.0040 mg/L 1 Chloroform 67-66-3 8260D ND 0.050 0.0040 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 0.0040 mg/L 1 1,1-Dichloroethene 75-35-4 8260D ND 0.050 0.0040 mg/L 1 Tetrachloroethene 127-18-4 8260D ND 0.050 0.0040 mg/L 1 Trichloroethene 79-01-6 8260D ND 0.050 0.0040 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 0.0040 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight basis Daly Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 13 Client:Synagro Laboratory ID:U106072-001 Description: Lincolnton WWTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 1.39 09/07/2019 0416 Date Received:09/06/2019 Run 1 Acceptance urrogate Q % Recovery Limits —romofluorobenzene 106 70-130 1,2-Dichloroethane-d4 117 70-130 Toluene-d8 118 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 09/16/2019 1.606 JCG 09/13/2019 1657 28844 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND - 0.040 0.0050 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 0.0050 mg/L 1 Hexachlorobenzene 118-74-1 8270E ND 0.040 0.0050 mg/L 1 Hexachlorobutadiene 87-68-3 8270E ND 0.040 0.0050 mg/L 1 Hexachloroethane 67-72-1 8270E ND 0.040 0.010 mg/L 1 2-Methylphenol 95-48-7 8270E ND 0.040 0.010 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND 0.040 0.015 mg/L 1 Nitrobenzene 98-95-3 8270E ND 0.040 0.015 mg/L 1 Pentachlorophenol 87-86-5 8270E ND 0.20 0.020 mg/L 1 Pyridine 110-86-1 8270E ND 0.040 0.0050 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 0.0050 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits "-Fluorobiphenyl 63 37-129 -Fluorophenol 34 24-127 Nitrobenzene-d5 54 38-127 Phenol-d5 44 28-128 Terphenyl-d14 102 10-148 2,4,6-Tribromophenol 56 41-144 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 09/17/2019 0031 DAL1 09/15/2019 1406 28961 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 2,4-D 94-75-7 8151A ND 0.020 0.0050 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 0.0013 mg/L 1 Run 1 Acceptance Surrogate 9 Q % Recovery Limits DCAA 60 50-112 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight basis Daly Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 13 Client:Synagro Laboratory ID:U106072-001 Description: Lincolnton WWTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 1.39 09/07/2019 0416 Date Received:09/06/2019 TCLP Pesticides un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 09/18/2019 0509 DAL1 09/15/2019 1543 28959 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 0.00017 mg/L 1 Chlordane 57-74-9 8081B ND 0.0040 0.0015 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 0.00015 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 0.00015 mg/L 1 Heptachlor epoxide 1024-57-3 8081E ND 0.00040 0.00016 mg/L 1 Methoxychlor 72-43-5 8081B 0.00040 J 0.0016 0.00021 mg/L 1 Toxaphene 8001-35-2 8081B ND 0.0080 0.0030 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 80 20-131 Tetrachloro-m-xylene 76 26-132 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471 B 7471 B 1 09/10/2019 0953 KSH2 09/09/2019 1520 28269 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7471B ND 5.5 1.3 mg/kg 1 TCLP Metals _un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 6010D 1 09/12/2019 0254 LLL 09/11/2019 1726 28648 09/10/2019 2043 1 1311/7470A 7470A 1 09/13/2019 1317 KSH2 09/12/2019 1455 28691 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Arsenic 7440-38-2 6010D ND 0.15 0.025 mg/L 1 Barium 7440-39-3 6010D 0.070 J 0.25 0.031 mg/L 1 Cadmium 7440-43-9 6010D ND 0.050 0.0060 mg/L 1 Chromium 7440-47-3 6010D ND 0.10 0.013 mg/L 1 Lead 7439-92-1 6010D ND 0.10 0.047 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 0.00091 mg/L 1 Selenium 7782-49-2 6010D ND 0.20 0.085 mg/L 1 Silver 7440-22-4 6010D ND 0.10 0.021 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight basis Daly Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 13 Client:Synagro Laboratory ID:U106072-001 Description: Lincolnton WWTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 1.39 09/07/2019 0416 Date Received:09/06/2019 ICP-AES un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 09/13/2019 1205 LLL 09/12/2019 0834 28607 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429-90-5 6010D 12000 480 180 mg/kg 1 Arsenic 7440-38-2 6010D 6.3 J 18 5.9 mg/kg 1 Cadmium 7440-43-9 6010D ND 5.9 1.5 mg/kg 1 Calcium 7440-70-2 601OD 9500 5900 740 mg/kg 1 Chromium 7440-47-3 601OD 47 12 3.0 mg/kg 1 Copper 7440-50-8 601OD 210 12 5.3 mg/kg 1 Iron 7439-89-6 6010D 12000 120 54 mg/kg 1 Lead 7439-92-1 6010D 12 12 5.3 mg/kg 1 Magnesium 7439-95-4 6010D 5500 J 5900 740 mg/kg 1 Manganese 7439-96-5 6010D 250 18 7.0 mg/kg 1 Molybdenum 7439-98-7 6010D ND 48 12 mg/kg 1 Nickel 7440-02-0 6010D 13 J 48 12 mg/kg 1 Potassium 7440-09-7 6010D 12000 5900 740 mg/kg 1 Selenium 7782-49-2 6010D 9.7 J 24 9.7 mg/kg 1 Sodium 7440-23-5 6010D 3600 J 5900 740 mg/kg 1 Zinc 7440-66-6 6010D 250 59 15 mg/kg 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight basis :aly Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 13 Client:Synagro Laboratory ID:U106072-002 Description: Lincolnton WTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 3.03 09/07/2019 0416 Date Received:09/06/2019 Inorganic non-metals un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (% Solids) SM 2540G 1 09/07/2019 0416 MDD 28205 1 (Ignitability) 1010A 1 09/26/2019 1330 SLC 30162 1 (Paint Filter) 9095B 1 09/15/2019 1540 HET 1 (pH) 9045D 1 09/09/2019 2037 HET 28337 1 (Reactive Cya) 7.3.3 1 09/11/2019 2056 MSG 09/09/2019 0934 1 (Reactive Sul) 7.3.4 1 09/10/2019 1655 HET 09/09/2019 0934 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 2540G 3.03 % 1 Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 0 o F 1 Paint Filter Test 9095B Fail, H* pass/fail 1 Soil pH measured in water @ 22 o C 9045D 6.6 su 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 100 50 mg/kg 1 TCLP Volatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date 1 1311/5030B 8260D 10 09/14/2019 0340 JTH Batch Leachate Date 28924 09/12/20191814 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 8260D ND 0.050 0.0040 mg/L 2-Butanone (MEK) 78-93-3 8260D ND 0.10 0.020 mg/L r'arbon tetrachloride 56-23-5 8260D ND 0.050 0.0040 mg/L hlorobenzene 108-90-7 8260D ND 0.050 0.0040 mg/L _hloroform 67-66-3 8260D ND 0.050 0.0040 mg/L 1,2-Dichloroethane 107-06-2 8260D ND 0.050 0.0040 mg/L 1,1-Dichloroethene 75-35-4 8260D ND 0.050 0.0040 mg/L Tetrachloroethene 127-18-4 8260D ND 0.050 0.0040 mg/L Trichloroethene 79-01-6 8260D ND 0.050 0.0040 mg/L Vinyl chloride 75-01-4 8260D ND 0.010 0.0040 mg/L Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 110 70-130 1,2-Dichloroethane-d4 115 70-130 Toluene-d8 120 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 09/16/2019 1631 JCG 09/13/2019 1657 28844 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight basis :aly Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 13 Client:Synagro Laboratory ID: U106072-002 Description: Lincolnton WTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 3.03 09/07/2019 0416 Date Received:09/0612019 TCLP Semivolatiles Lin Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 09/16/2019 1631 JCG 09/13/2019 1657 28844 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 0.0050 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 0.0050 mg/L 1 Hexachlorobenzene 118-74-1 8270E ND 0.040 0.0050 mg/L 1 Hexachlorobutadiene 87-68-3 8270E ND 0.040 0.0050 mg/L 1 Hexachloroethane 67-72-1 8270E ND 0.040 0.010 mg/L 1 2-Methylphenol 95-48-7 8270E ND 0.040 0.010 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND 0.040 0.015 mg/L 1 Nitrobenzene 98-95-3 8270E ND 0.040 0.015 mg/L 1 Pentachlorophenol 87-86-5 8270E ND 0.20 0.020 mg/L 1 Pyridine 110-86-1 8270E ND 0.040 0.0050 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 0.0050 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 60 37-129 2-Fluorophenol 34 24-127 Nitrobenzene-d5 50 38-127 Phenol-d5 44 28-128 Terphenyl-d14 99 10-148 2,4,6-Tribromophenol 51 41-144 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 09/17/2019 0054 DAL1 09/15/2019 1406 28961 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 2,4-D 94-75-7 8151A ND 0.020 0.0050 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 0.0013 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 62 50-112 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 09/18/2019 0523 DAL1 09/15/2019 1543 28959 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 0.00017 mg/L 1 LOQ = Limit of Quantitation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL Out of holding time W = Reported on wet weight basis !aly Environmental Services, Inc. iuti Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 13 Client:Synagro Laboratory ID:U106072-002 Description: Lincolnton WTP Matrix: Solid Date Sampled:09/05/2019 % Solids: 3.03 09/07/2019 0416 Date Received: 0910612019 TCLP Pesticides un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081 B 1 09/18/2019 0523 DAL1 09/15/2019 1543 28959 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Chlordane 57-74-9 8081B ND 0.0040 0.0015 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 0.00015 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 0.00015 mg/L 1 Heptachlor epoxide 1024-57-3 8081B ND 0.00040 0.00016 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 0.00021 mg/L 1 Toxaphene 8001-35-2 8081E ND 0.0080 0.0030 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 77 20-131 Tetrachloro-m-xylene 72 26-132 TCLP Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 6010D 1 09/12/2019 0259 LLL 09/11/2019 1726 28648 09/10/2019 2043 1 1311/7470A 7470A 1 09/13/2019 1320 KSH2 09/12/2019 1455 28691 09/10/2019 2043 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Arsenic 7440-38-2 6010D ND 0.15 0.025 mg/L 1 Barium 7440-39-3 6010D 0.097 J 0.25 0.031 mg/L 1 r'admium 7440-43-9 6010D ND 0.050 0.0060 mg/L 1 hromium 7440-47-3 6010D ND 0.10 0.013 mg/L 1 -aad 7439-92-1 6010D ND 0.10 0.047 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 0.00091 mg/L 1 Selenium 7782-49-2 6010D ND 0.20 0.085 mg/L 1 Silver 7440-22-4 6010D ND 0.10 0.021 mg/L 1 Footnote(s): "Paint Filter: 64mL collected; LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL Out of holding time W = Rdported on wet weight basis ialy Environmental Services, Inc. 1 us Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9of13 Chain Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 13 ,Cn O 3 O N w w � a m �E3 �CD o� C, m C (. N N n 5 o p v N rn V N W ., i�ALY Chain of Custody Record Shealv En.rircnmontal SerS:icws, [no, 106 Vnriwge Point Drive 9°.rest Calumbiz?, South Cwclina 22-172 Telephone No. (1303;, 791-9700 Fax No. i.843j 7,91-9111 'rru�rsheal}la#:.cart Number Moir ;x-port to Conlaat •:ample: ;?rinte:; Tdar-roj u� quota No. Synagrn Flex' ox F1v>'Fox a arlrFus Telephone No. 1 Fax Nc, i Cnr2:l If-fay*'II Na. Page &M Clegur rRd, 3U 703 538.1 a• yr-sp).corr 1 ai Dlry IState JZIP Cats preservathlC 1 _ 1 NLMUcr of Cc itair5rs trl�ciw^F1U NO, 127, 02B 9, Unpras. 4, HUO3 ;. NaOF ^. Na��llr7r,A S, iC� I Bottle I°:cadNine I PrsamBlivc Lard: nlntun 4'e,'A'4N :!. I•I:?S(1� Ei. fda Thio. ,w p m = I a - n 1iIiU1:��1:�1��d711 Flr.•�e Y �`(lmiE:er P.0 wailer h,��i� _._.CL L^, J ? 2 $eIT %.D!L1r3SGr10iirJfP h t1C�nl.rar�Miur.t:ih arrt pr'nCrY1+C Lot_ Tire Lyr Zvi Clt1, 'rV',"d ti0 I- �c tL ' ° ej ('r i c ,,rbined an one line', r, r JO Q II.Dd n M 000 a- � 4-0 �s ' Lina;,kiton 514 4"u'TP I•r' G X X I NC Munitarltlg Kpl-; 17- T�+nl4+::�r+c Tiri�Re:lurrd [P,in• lo:Y� uppu,;il+ncul•e;l r�,rr.:+Ewdi:est T,�r, Ca,drpla Dispe�31 Cv Re�>,iretnents 11'aa�e u'r�clF�j PC:s�I� TI��tJ Id-rglti�atlCrr , EwA»lord a.qt sir (°Ir^,e EpaTy;+ 7 ca;rs a Lucks C Roturrt :o Client plapras5l by Lab SIC Cerftir -lion Non-Hazen �PL-rnrracta �Skn Irritant QPoiscn U a}:nam I 4 hFt> Y; viraplm Det j Tirnt; I „ 1, Rut�i,&a f y DatQri Iine ry 2. Relinquished by Dato Trim! Late Ti-no 3. polinquislwo LY Date T.-no ;. Roc::•.odCv r)aie TI'rtA 4. Relinquished 7� f Dag Tint ^ A. LaUarat ti~ c„awed hp I 1 L� r f Tyre `r NO—M: All sa.mplW5 are retained for six weeks from receipt unless other L.0.13 LASE 45�tL4r,/ nmce pl T np. Tert�. t3lanv arra arnonts are made : Re,oNsi Lin IV.(Ohock) []Y it a Ise PAO ,n-r,', ; ° C" i! Y �rt Effnuivc D'atu 90-27-2012 Cn M 0 Z 0 8 Cn ::F 0 (D rn (D -0 0 0 53 CD < Cn CD CD 0 CD Sn ET o P 3 3 hea.1y Environrnental Servic.-es, 1po. 106 Vant%e Poini Drily a Chain of Custody Record West Columbia, joule Qa, 4 na 2 P 172 Number (803; 7a1.91111 Cllent Ruport to Cwbtaot San ^tf). SynF@rD Fox Alex rcx Addref'... TDIBphDnI?N0, F-:K NLI. J FItInil VLIEgWIll No. Page 128-1 Br, -Rd, 2NO 703 DW nkxq.-Synagra. fxml Ci C: IN 17ICade Pm—'ertratin '41 j I N U n W C. 1; 0; t i I j MOCKS'Alo I 4, FINC3 7. NnOH 2. Nal)H,,ZIIA 5. HGL 00wo Projed NaMa Presemadva. LincalnEon'OPAM, 3. H 2-S C-11 S. He 7hlo. Ti PJI Numbor matflx GaM ple U 106072 'Cr intow,,"ns for cacli sample may be DaL- Time IL Dvk I It 3 LL zi Ix nmL D Inea an ant7. ]in C I g; Lu UZI -< )I LL UncoInton'Arl-P IC Y, x x x g NC Monitoring UnroInfon x pc • TUM -reurd rNP.- r-equif°'d 12barproval raqmirod %Ir wpW L-3dTA.7) iiequlrrernem (Please 13pedry) XI-wroiwc [] PjA�jpluvAjj SpEcei,, 7 dkly� pi Luris El Return go Meng 1),y Lob NO Cer.ific-mian nSkin Irritant j[]P4.kfjfI EJJnInvNn I.Relinquish vpy? TAno 1. ITime 2- R01nqulV--, htr Date Time 2. Rec-wed oy Dam Time by Time me 3. RemNed by Time 4. Relh - U �S V 4. L,=,:retc Recelved by y7f� /I q _JID31; Note." All samples are retained for six w4c-kq frarn receipt unless other 1AIR US E ONLY RFkiffpVTiwna. TArnp. R174nk.' of ran are made U Ice -,0hek.) E]y H ice fAaa,k .I E v S A X T1 P* z z 0 SHEALY ENVIRONMENTAL SERVICES, INC. .Shwilr Ea+'irtr.:nuvla Ken'irS9, [tie. Page 1 of 1 DOZ=UANw::her. 61F.00If•':.•.1= ItFfC::live �s�te; $•�;�ofI Sample receipt Checidist (SRC) CHUnt: Synazlro Cfjoh:r Inspected ;clrstc: ttis 1 1f6119 Lot : UI06072 M--ans of receipt: EJ SISI ❑ ('faent TJPS �] [ edF.x Cftlter- — o Fes [] 1No [_ �w'c re enstcldv s+:als aresenf On the cooler? _ Ye3l Q No NA 2- If custody seals Wcrc UMenL vwrc rhey imact and urt6ru[cc:i t �rH Strip [D: NA Chlorine Strip ID: NA Tested by, IN lCriginal temperature upon rep eiflt f l�erivecl(t<amected) tempt ratwrre ullcan rceeipt 9'oSalid Snap -Cup [i]11946 27.1 ,`27.1 ce NHS, ;-N.ev �(; _Nei /NA °( INA ? NA °C kfothod: [ATcmperature Blank RJAgainst &a[tles IR Gust ID: 5 IR Gun Correction Factor, _ IvIctlied r1f coolant: lee -Ice Facks Dry Icc ®None ® Yes Nn ElNA If temperature of any cook.'r exceeded 1 .t1`C, was Pr-Diect Mamagrer NOLif-tUd IPNI %vas I1'ofifrcd by: plione teniayr;' facto-fawfcire Ie tine). ®} es ❑ No ET NA d. is I cnnimemiai courier's packing, sLIP attachM to this firrm7 Yes ❑lib 5_ Were proU: r castody prncedure.s(rcUnquiIsltcd-`recei%rcd) FolluWrd? } Yes ❑ 2tiTcr b. Were sample IDs IE:5icd oil the COC? F'y ❑ �No 7. Were sample IDs lis[vd, on all sampic contairlc.�rs`T ® No R. Wascolitxtion date& time list�lan the C017 No 9. V��as collection date & time listed on aii sample contaititIN ❑ N;} �111D!edall container labt;] information (ID, da:, time) aSmte witct the Coca® Yes ❑ No ' e tests to be herfvrnted Iis lul ae1 the { QC? ® Ycy ®No 12, IDid all saunI an ivo in dle prt:[,•rr container-, for each test anCnr in good contiirirnt (unbroken. lids can, etc.)? 6o1 Yes No _ 13. Was ade late 3amp•Ityvolume lavai[able? Yes ❑ No 14, 'Were Il swuptes received within I,- the hold big V-11 yr48 hours, Whichever comes fimx? Ycs No I S. Wurc any samples i rurdainers missingt`excess ioirc[e or_o) samples Not Head on COO El •tis N© NA 16. For _ rOA and RSIti-175 samples, wen: bub:ales present = `pest -size" (�fa°'OI btttnl in Cilc3lt]etea) in an,,, of the VQA viala7 Ycs Yes Nn ® Nn NA 17. 'Je'ere all DR 0r1met31sinutriealt samples recL.ivc;d at a pH of< �? NA 'a'4`ere . -I S. all cyanide sare�plws t�ceiv. d1 at a )H = 12 and mrlfide Sarrtples r�ceitired at a yH 4r� El �'cs ®hr, I _ lV` all a l[bable NH;: N. a}anidc.'phenr)1 fi35 {•. t}.gmgr'L'} sarnp[es ticee ol`residual ®IVA pd1 �lllorine?' ❑ Yes EINo 2-0' lh•ers:tlient.timarks(refit gists ([.e: rdymsted dilutions, 41%%1817 designations, etc...) -orreet[y tratlscrihed front the COC inlu the C-0111rra.•nt section in UMS? Y 1�0 'Was -the 4uote nutnbcsr listed on the conlilirrs:r label? If;es, Que1lG 4 NIA 'ample Pre-4er vatioll (Mttst be coniplet=f fQr ar y santple(s) inc•nn-actlw pr4:scrved t1r with ]1�arlspace. j antrslc�(s) hd?I t sa[ttpl receiving -were racei+•cd incoarcctly press arvcd and tern adjusted srocordingly t'eitlt N, nil. of circle i:nc:1LSO4, I-lNO3, HU NadH using SR # NA Illw of pvseruation NA If mare !]tan tine preservative is needed, pbmse note in the comficnts below, NA were receiticd with lttlbbles� G m1t, in diameter. ,ycre received w4h TI C. ? 0.5 111911- (II'1i l 9 is no) and werc stacl accord;llgly in sample receiving with sodium thins0fate (Nays,t�;) with Shealy li): NA bareix[c labels applied by: 17V6, l Date: 9. 6.+19 cotttmt:nts: "I,.incolnlUn" bo-le fclrN&M exploded in coo[er. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 13 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WQ Permit Number: WQ 0002712 WWTP Name: Lincolnton WWTP NPDES Number: NC 0025496 Monitoring Period: From 01/01/19 To 03/31/2019 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed Class A or Class B complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 61' MPN MPN/g Coliform power per gram of total solids 4398 39970 95159 CFU/g 0 Quarterly Grab 9222D CFU SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 (VS reduction) X (40-day bench) Option/Alt. 5 Option/Alt. 6 (14-Day Aerobic) (Alk Stabilization) Option/Mt. 9 Option/Mt. 10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 Option/Alt. 4 Q0-day bench) (Spec. 02 uptake) Option/Alt. 7 Option/Alt. 8 (Drying — Stable) (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inc u ' fine an�prisonment." Director of Public Works 1 g. / YJ Pre rer Name and Ti ( type or print) Land Applier a e and Title (if applicable) (type or print) mow.--- ZI/Zv Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) SLUDGE Fecal Coliforms -See, Effluent Fecal Coliform Setup for QA Data o Method: 9222D SM 21st ad Temperatures are in. C Collection Date Time By Water Bath Setup < 8 hours after Grab Read 24 +/- 2 hours Setup Removal Time In By Temp Time Out By Temp Colony Count per Filter B Calculate Colonies per 100 mUFilter Colonies per 100 mUFilter C % TOTAL SOLIDS D Reportable Colonies per 9 C/D ml Used A 1 0.01 J��4��� "LE, 3d U�1 ' I/31� CFU 0.1 i 0.01 1 /J'� CFU 0.1 / 01 CFU 0.1 0.01 'Lq i (�r (� IL�) ° � Y CFU 0.1 0.01� Jj��� � I ��� CFU 0.1 I 0.01 V1,4i5C CFU 0.1 I 0.01 j 1 � � CFU 0.1 i ecnnician uuaner / Year SM 2540 B-2011, 2540 D -20.)1 NCO0254.96 All weighings are dome in grams ��.� €r�,n5 � � ; ro _r �k{�x � 'n�'�`�{/}'���' ,���� F2" �'ps(�}7*: -s ,Ka'Y`x"p���}��_�-jjz�'j� 2 �� .�"'•�" rr� �.:p+.f� �.,r r,} .r ,���.�`�[ -•y � c� a Time Collected Date Collected 2� —2 Z� Date/Time In L , Date / Time Out 3 — Z2 _� �, •� 1 O Total Wet Wgt Dish Wet Sludge Wgt (103-105°C) Dried Wgt 7 7 L(r gs l o Dist; �f r .Gl % 3 L% D j, 2 2 3 Dry Solids Wgt % Solids 3 zZ "� l r L/ l Ll AVG % Solids' Time In/Out 21 e -2 3 (103-105°C) Dried Wgt L /� [ �� ( /J `( tJ 37 550°C.Wt L� z10 0 r T l , Volatile Solids Wgt O—p D' y 2-3 % Volatile Solids AVG o /o Volatile.Solids v TS DAF =' ,q3 % TS Sludge = j , D % VS DAF = i % VS Slud e = G� % Total Solids Dry Solids Wgt _ . X 100 Wet Solids Wgt % Volatile Solids = (Volatile Solids Wgt) X 100 Dried Solids Wgt % Reduction _ (VS DAF - VS Sludge) X� 00 VS DAF - (VS DAF)(VS Sludge) q 31 ©�® ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WWTP Name: Lincolnton WWTP WQ Permit Number: WQ 0002712 NPDES Number: NC 0025496 Monitoring Period: From 04/01/19 To 06/30/2019 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Anaerobic Digestion Composting Aerobic Digestion If applicable to alternative performed Class A or Class B complete the following monitorin data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6th MPN . MPN/g Coliform power per gram of total solids CFU 37500 91179 237762 CFU/g 0 Quarterly Grab 9222D SM 1000 NUN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 (VS reduction) X (40-day bench) Option/Alt. 5 Option/Alt. 6 (14-Day Aerobic) (Alk Stabilization) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Mt. 3 Option/Alt. 4 (30-day bench) (Spec. 02 uptake) Option/Alt. 7 Option/Alt. 8 (Drying — Stable) (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are significant penalties for false certification inclyWing fine and imprisonment" Director of Public Works Pre arer Name and Title ( type or print) Land A 1' r Name and Title (if applicable) (type or print) Z Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) —See Effluent Fecal Coliform Setup for QA Data nno4hn 1. 0999n CM 91 of aH Temperatures are in.°C Collection Date Time By Water Setup < S hours after Grab Setup Time In By Temp Bath Read 24 +/- 2 hours Removal Time Out By Temp Colony Count per Filter Calculate Colonies per 100 mUFilter Colonies per 100 mUFilter % TOTAL SOLIDS Reportable Colonies per g ml Used A B C D CID ®101 .- ®�" �l� i�� 0.01 ��3U6© pC?4�. �� � G�� y CFU 0.1 0.01 .�i CFU 0.1 �i l i `1 .4 i%' 0.01 `� .��� c�),� G CFU 0.1� ��jOt7 XG�7 .dam 0 .01`lil/ !/( CFU 0.1�� L7 lVc� U`D �. • �'v1 l `� D'� �s✓i�� 0.01ar O O I) ��� . �a , t v CFU 0.1 to 0.01 CFU 0.1 / 7 o.016b 3 / CFU 0.1 �Q r SLUDGE Fecal Cofforms *—See Effluent Fecal Collform Setup for QA Data nnarti, r• a���n cnn �n& P� 0 v Temperatures are in.°C Collection Date Time By Water Bath Setup < 8 hours after Grab Read 24 +P 2 hours Setup Removal Time In By Temp Time Out By Temp Colony Count per Filter B Calculate Colonies per 100 mUFilter Colonies per 100 mUFiiter C� '/o TOTAL SOLIDS D Reportable Colonies per .g C/D ml Used A c .I V J 4q DOD G 7 t d` t J��p� *Ora_- . CFU 0.1 (_ J �+.,t 0.01 C�D ] (� �L i CFU 0.1 3-0 �y CGpG 0.01 CFU 0.1 0.01 CFU 0.1 0.01 CFU 0.01 CFU 0.1 0.01 CFU 0.1 Technician Quarter ! Year &-4 enn ncen o anal gcnn n_,)nai r%1r_nn7Z;AgA All wpinhince; ara done in crams :Yr S pY, 1 1'zgd �; �• -t.�� �!I � 't L � �.1,� 7fi , � R �xR�h � 5St 1 eS ..'N� ¢,c� i a,�.sc.,:. _.t' ,.r �S..Wr� Time Collected Z9 Date Collected Date / Time In L- f Date /Time Out Total Wet Wgt 31 Z-0 0( 6 Dish Wet Sludge Wgt `l 31 s� , �� 1 j [ L� Z2 (.i (103-10 gt Dried Disc; Z32 3 zd D Solids Wgt % Solids [ [ c AV G % Solids ,ct 7 Time In/Out (103-105°C) Dried Wgt o[ 36 i��f (��� 5500C Wt Volatile Solids Wgt i 11 i Q C� f L l 1 S % Volatile Solids c %� L} ? ®, 1 AVG %Volatile Solids (![�/�� -9, % TS DAF = a % TS Sludge = s /o VS DAF = �� a D �Z % VS Sludge = L % dotal Sol!da = Dry Solids Wgt % 90® Inlet Solids Wgt % Volatile Solids = (Volatile Solids Wgt) x 100 Dried Solids Wgt % Reduction _ (Vs DAF - VS Sludge) x 100 VS DAF - (VS DAF)(VS Sludge) Technician can 9AAn a-i 997. 9540 D -1997 S Quarter / Year All weighings are done in grams -. _. . 'a `*, 1, t., '•s w <t:: Y .. a:�"?'".t,.. ....�. > : ..... ,.� l... .. w. 'f: i S -. �. ... '..: .a '. " Y ti r, x ..«'.t.; a f i _ - .: ,:,- >z. ':� ��• S .7 �0. �v��®It VONF, K.. .e' .. <.:s:n .. �..- ... Time ,c�. �1 t� 0 Yd^D Collected '� - z3 � � � � - L�F. �I � ~ 2-5 "� � :� ® Date /✓ / � Collected J� l C �2 03-D� ( -r - �(1b� l0 Date Time In ����'� �� (r ( l .5 Q 3 Date/ y d 23 jppc7 �+ �t—Z� f � Ott L .2�✓j�j/� ,2(""I �O .z 1 � ��� Time Out Total (o ?7� A36L/D �f%,`(li� {i�,1(O23 �/ 3 ��,oy�3 /�7 ,5�>.`� ��b ��' �lzs �`��.2� �`� �(�� /Di.1 �.�,d�'�P l913.1Z' Wet Wgt /b a. 5 . Oj a1— o Dish� (° 1 g q GgeZ Cv�• s q-o r{ J 'IdS' �a67� j�r 6P0Z �)y° uj%`/� �Y� a aj?. C®o��G�-- qo °aiijj �l J� G� I7� qy °' Wet Sludge 5�(,$�� �f��1o23 �b �3°� 3� i�`�� 7��?l°3> ��� FP. %i,�•���% `�ti ��,�5®� ��a��� r{z,1j15`� I.tia'��oi ��,bo2b Wgt ��i� 1(��� ��� �ZCi q6, C2. 2 n �u��CJ l , �7 t )j01 Oe�o�l 7i2` i6 ^IYl,�li' (t°1�5& C�Ua 7r)3l ` 5�1a Ll (103-105°C) 3 2,?� Dried Wgt •j`&l�yJZ- Chn20?`� U c '�$s( 44, �.ZIF��a�l�!.Z���4 )��r.� 3�`f Dish P�3 �� 0-2- 1 �t 2, °tP1o3 �eDrySolids I Wgt %Solids Oi�L%°.C'� 3 �,,� b� %t� °�- ° � °�, 3 � Average ° I O l J % Solids V lJ 1 ��9 Da .13 RPD %'dotal Solids ® Dry Solids Wgt X 100 'Wet Solids Wgt technician Quarter /Year �t9 SM 2540 G-1997. 2540 D-1997 All weighings are douse in grams ' 1 C� ?.. <. } � , .`.. '- .., -.. ! F :. b rv',r f i. . _,. -. >,....r ...,Y .J. .... f .b3. V. t .., t, 1-J -'1� �a !.. •. i ;1.... Time Collected Date Collected--1 Date / Time In �+ l Date Time Out a Total Wet Wgt Dish°�e Wet Sludge Wgt (103-105°C) Dried Wgt Dish a q Dry Solids Wgt ®e c�-��'� ®d�63 % Solids o ®G B Average % Solids RPD d� % Total Solids m Dry Solids Wgt X I®® 'Wet Solids Wgt ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WQ Permit Number: WQ 0002712 WWTP Name: Lincolnton WWTP NPDES Number: NC 0025496 Monitoring Period: From 07/01/19 To 09/30/2019 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed Class A or Class B complete the following monitorin data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61h NUN MPN/g Coliform power per gram of total solids CFU 901 80170 227692 CFU/g 0 Quarterly Grab 9222D SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 (VS reduction) X (40-day bench) Option/Alt. 5 Option/Alt. 6 (I4-DayAerobic) (Alk Stabilization) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 Option/Alt. 4 (30-day bench) (Spec. 02 uptake) Option/Alt. 7 Option/Alt. 8 (Drying — Stable) (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inc ding fine air i imprisonment." Director of Public Works �1L m / $`5 Pre erg Name and Title pe or print) / Land App 'e Name a e (if applicable) (type or print) �ro �• ��! �® c ?� ignature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) r" �- Ole - SLUDGE Fecal CoMorms ...eve Fri ienf Feral Cniiform SetuD for QA Data Ua +h.,,i• cnn 99 + Al Temperatures are in °C Collection Water Bath Setup < 8 hours after Grab Read 24 +/- 2 hours Colony Count Calculate Colonies Colonies % TOTAL Reportable Colonies ml Used Date Time By Setup Removal Time In By Temp Time Out By Temp per Filter per 100 mL/Filter per 100 mUFilter SOLIDS per .9 pA B C D C/D �0.01 6 D?()o 0 oo ,h- 74(5 0 ��(� `'w- `t (�� ® � �� � J � s �j %� � CFU l a-L5 6� 0.1 �30 0 gC15' g J+A- qJS 0.01 4,9000 r[ Z�� CFU L� t�/�� d 7 6 0.1 l O Ii7®O ° �S�(0041� ®06fl /J CFU -rpre, _ _.— 0.1 G b 3� ,i"l �y� �Cjdv �5 �- o.01 D__ . `�pO�a0 °° l °' �? %C7 CFU 0.1 7 ,. CFU 0.1 ' n.� ®�ly ✓vt. 7 ®ri �� �- C 0.01 v V (o ��� 3.l C FU I�.®®° 0�3o � � 0.01 o o a0�•� ��CJOf0 �y �' l� CFU Technician 'i - Quarter / Year SM 2540 G-1997, 2540 D -1997 All weighings are done in grams SAMP ®iTime Collected C'• CJ i 1 �% (� 3 V C l D �i �+ Li C 00 O `{ Dat Collected 1 ! �1"��,l�j �Jr�C-Z.� �f� Z�✓�� -7�Da Timten /cr% ����l�U (�!®�(�0�(� 10 r� _ 2.7_-//r�}CG �—Z�-(��®�. Date! Time Out 1-! 7 - ( lv 5i } A ? l l �! 0 4� [7 . l v `�,9�®� !�"0 ®� r� ® ��yl�(i�JZU� 1 ?� �i� ! ��®�3� WTo ettWgt -Z-o CL °'01 Dish ����.3�U !-�y��f;�b ��.��3 3 �,��3Z �G,�3,/0� �1y.3��� y� `t`I',;�'",-• �` �{�35 �` Y3, WetSludge d l +~3 (Z �� 3 f � °���� �l �j`% `� �� ����� � (�� �6l§� L 65`F �� 01 �,�, �8: 21 d, ai (103-1050C) Dried Wgt v4 3� ``� t .i ,{� U j Q a'd✓Gi p )S&qa �q, Dish �t�. �U� `1 �1.� ��� qq p3 3ctc?`��' ��'Z��' y'la"lq'4,"33 y 3 ' ( Z-, 13 J �K°3�f ,��i�� zF,t-rt2 , Dry Solids Wgt %Solids 01gj Average % SolidseC RPD S ' l J % Total Solids ® Dry Solids Wgt x 100 Wet Solids Wgt Technician _ ��"-� (,luarror / Year J �Z� � r `: `9 sM 2540 B-2011, 2540 D -2011 NCO025496 All w►eighings are dove in grams Time Collected I C) I D 6) Date Collected Date /Time In Date /Time Out 2 (� 0 Total Wet Wgt� Dish ; Wet Sludge Wgt (103-1050C) Dried Wgtt(� ( L) J� Dish Ll L 5 � . Dry Solids Wgt y� ! z 1� � 2 % Solids ! ( 6,33 AVG % Solids Time In/Out (103-105°C) Dried Wgt�jrS��Tr/p3� 550°C Wt Z711�, qp Volatile Solids Wgt % Volatile Solids i I (9L S� AVG % Volatile Solids �3 % TS DAF = % TS Sludge = - Y70 � 22.?` fD ?�z0 �0 eq ?? T VS DAF Y > % VS Slud e = % Total Solids = Dry Solids Wgt X 100 Weft Solids Wgt % Volatile Solids = (Volatile Solids Wgt) X I fl0 Dried Solids Wgt % Reduction m (VS DA+F - VS Sludge) x 1100 VS OAF - (VS DAF)(VS Sludge) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WWTP Name: Lincolnton WWTP WQ Permit Number: WQ 0002712 NPDES Number: NC 0025496 Monitoring Period: From 10/01/19 To 12/31/19 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 6' MPN MPN/g Coliform power per gram of total solids 90 1189 3931 CFU/g 0 Quarterly Grab 9222D CFU SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Mt. 2 (VS reduction) X (40-day bench) Option/Alt. 5 Option/Alt. 6 (14-Day Aerobic) (Alk Stabilization) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Alt. 3 Option/Alt. 4 (30-day bench) (Spec. 02 uptake) Option/Alt. 7 Option/Alt. 8 (Drying — Stable) (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the athogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inc ding fine amprisonment." Director of Public Works Pre rer Name /and Tit%( type or print) / Land App ier Name and Title (if applicable) (type or print) I Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) SLUDGE Fecal CoNfoirms "*See Effluent Fecal Coliform Setup for QA Data o Method: 9222D SM 21st ed Temperatures are in. C Collection Water Bath Colony Calculate % Reportable Date Time By Setup < 8 hours after Grab Read 24 +1- 2 hours Setup Removal Count per Colonies per Colonies per TOTAL SOLIDS Colonies per ml Time In By Temp Time Out By Temp Used Filter 100 mL/Filter 100 mLlFilter .9 A B C D CID u 1'�L l Ll D � � � ✓" " � S 0.01 Z- ! ✓ � CFU --To a O t� �— t 0.1 I ¢ / �2 ` l q�1c, ®U-6J �/ O�q4 �v �% �� i D,�J ,1 �7' O'9fr1' � O %� �! Vd r �.� l g / L CFU L� CFU yo v 7J%� / �.S �!✓ d" CFU ✓rdo�7 10 iw r J ' 01 CFU A 3 cQ O4 G0.0 �^' '6�° ��3 � 'M' '•'�Y -a6.8� v � 2!� �� O� CFU v✓R,� �y Technician -ILA- SM 2540 G-1997,2540 D -1997 Quarter / Year All weighings are done in grams 0,� a 0— 5 Time Collected �00 C) C) Date Colle /,q- /cte 0 0 Date /V- -/7 Time In q 6) 4D Date 1,c2- /0 0 -la40-n-0- /0 Time Out 0 6DO L9 r, c) Ottep -4,() Totalgt WetWgt 1[16 109,3VY /09, 7963 �3�& 1L)I, o,719 5�, q f, SO 5W /00, l0q, 16q' Dish iq LI, 3 1,7 7✓ 1041 �i R3 Via, -3- q 3 52� q, 9,5-0) q6, 71 Ij 11)115� Nil,t-(-96o, S- q,/, J6 Y 6., 0- 78� 4 q4 590) WetWgt Sludge 0, 1612-- DjY' 5 -5120 -S'b"t'g�t) 31 Vb jq6 sa8j-s��lp�0 3 (I 03-1WC) DriedWgt L�VS ?353 11 _jq6. 900 , 10 qji.61 q&, q6,6 Dish q -1.5 r ItA q)-,Ci q& q3 tjsl qyqiP qq,5631 V 6, 194 33, cf� Dry Solids Wgt 3. 8,,- � V� o5' %Solids 66 &, 1,q 3- l I J,IU Average % Solids 3,15 % Total Solids Dry Solids Wgt —X 100 'Wet Solids Wgt I sM 2540 e--201;, 2640 o -2011 NCO025496 All weighiogs are done in grams J i Time Collected l 3 D Date Collected Date%Time-ln /p Date / Time Out Total Wet Wgt =¢f 1-7 f 0 " 010 Dish� ? t A_ Wet Sludge Wgt V, (103-105°C) Dried Wgt Dish `� Z Dry Solids Wgt % Solids I d ® d L! AVG % Solids, I )I L !' yo /16%lf�a Time In/Out L� V (103-10 gt Dried q nP u 2 ( rf IY 3 550°C Wt �% o `� Y 3 i 30 Volatile Solids Wgt % Volatile Solids AVG t 1 `G %'Volatile.Solids ___ - % TS DAF =• - - . I % VS DAF ` 3 % TS Sludge = % VS Sludge % Total Solids ® Day Solids Wgt X 100 Wet Solids Wgt % Volatile Solids = (Volatile Solids Wgt) X 100 Dried Solids Wgt % Reduction ® (VS DAF - VS Sludge) x 100 VS DAF - (VS DAF)(VS Sludge) �® SECTION 6 Agricultural Lime Application Log Year: 2019 Project: Lincolnton Field S01171 Lime Requirement Tons/Acre Date Applied (state -county -site -field) pH from soil anal sis Applied(CCE E .) UA-3b-2Ab /.IJ U.UI/HC. CA-35-2C 6.9 O.OT/Ac. CA-35-3AB 6.8 0.0 T/AC LT-1 9-1 6.6 O.OT/Ac. LT-1 9-2 6.3 O.OT/Ac. LT-1 9-7 6.1 O.OT/Ac. LT-36-1 6.3 O.OT/Ac. LT-36-2 6.5 O.OT/Ac. LT-36-3 6.1 O.OT/Ac. LT-36-4 6.7 O.OT/Ac. LT-36-5 6.2 O.OT/Ac. SECTION 7 NCDA&CS Ai >mic Division Phone: (919) 733-2655 Website: ww �,; ` �`+'f� Predictive "t r. ¢' 4}. Soil Report Mehlich-3 Extraction T. Links to Helpful Information Sampled: 09/10/2019 Received: 09/12/2019 Completed: 09/21/2019 Farm: NC-CA-35 Sample ID: 2AB Recommendations: Lime Crop (tons/acre) N P2O5 Lime History: 1 - Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.36 1.01 22.1 100 0.0 7.3 186 52 91 8 Sample ID: 2C Recommendations: Lime Crop (tons/acre) N P2O5 Lime History: 1 - Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.51 0.94 18.1 97 0.6 6.9 221 96 84 10 Sample ID: 3AB Recommendations: Lime Crop (tons/acre) N P2O5 Lime History: 1 - Fescue/OGrass/Tim, M 0.0 120-200 0 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.46 1.00 18.2 96 0.7 6.8 250 106 81 12 Norte Carolina er _ Tobacco Trust rin;tl Cminii%sloto igr.gov/agronomi/ Report No. '20-SL004629 Client: Laura / Jeff Elmore Advisor: Alex Fox Elmore Farms Synagro 4862 Range Ridge Road 284 Boger Rd Claremont, NC 28610 Mocksville, NC 27028 Sampled County: Catawba Client ID: 152466 Advisor ID: 501947 Nutrients (lb/acre) More Information K2O Mg S Mn Zn Cu B 40 0 0 pH$ 0 0 0 Note: 12 Note: Soil Class: Mineral S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 54 447 265 277 277 236 0.1 0 Nutrients (lb/acre) More Information K2O Mg S Mn Zn Cu B 0 0 0 pH$ 0 0 0 Note: 12 Note: Soil Class: Mineral S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 49 332 202 343 343 237 0.1 1 Nutrients (lb/acre) More K2O Mg S Mn Zn Cu B Information 0 0 0 pH$ 0 0 0 Note: 12 Note: Soil Class: Mineral S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 53 382 234 383 383 235 0.1 1 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. . - Steve Troxler. Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL004629 Laura / Jeff Elmore Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not M-0 N mineral -organic soil class nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmV/;f ind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-1, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm NCDA&CS Al. ►mic Division Phone: (919) 733-2655 Website: wwi igr.gov/agronomi/ Report No. 120-SL004621 Client: Chuck Waters Advisor: Alex Fox Predictive 3529 Killian Road S na ro Y 9 Soil Report Mehlich-3Extraction Lincolnton, NC 28092 284 Boger Rd Mocksville, NC 27028 Sampled County: Lincoln kx'�'"'•5'�" Links to Helpful Information Client ID: 409870 Advisor ID: 501947 Sampled: 09/10/2019 Received: 09/12/2019 Completed: 09/21/2019 Farm: NC-Lt-19 Sample ID: 01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 pH$ 0 0 0 Note: 12 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 1.01 11.1 93 0.8 6.6 80 81 60 29 38 690 422 403 403 314 0.1 1 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.08 8.5 88 1.0 6.3 108 24 59 28 36 1428 870 187 187 162 0.1 1 Sample ID: 07 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, M 0.0 120-200 70 70 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.71 0.99 8.5 84 1.4 6.1 28 34 69 13 40 1333 816 183 183 285 0.1 1 North Carolina rV?IIJ ixi TRISS Fwt-d cool1IA10%sioll Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL004621 Chuck Waters Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I M-0 manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NOs-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmtsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www• ncagr.gov1agronomi1uyrst.htm NCDA&CS Ai )mic Division Phone: (919) 733-2655 Website: wwi igr.gov/agronomi/ Report No. 120-SL004617 Client: Jeff Lingerfelt Advisor: Alex Fox Predictive 7338 W Hwy 27 Synagro Vale, NC 28168 284 Boger Rd NC 27028 Soil Report Mehlich-3 Extraction Mocksville, Sampled County: Lincoln Links to Helpful Information Client ID: 318761 Advisor ID: 501947 Sampled: 09/06/2019 Received: 09/12/2019 Completed: 09/21/2019 Farm: NC-Lt-36 Sample ID: 01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM%a WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.18 8.0 88 1.0 6.3 116 89 62 20 48 184 124 193 193 194 0.1 1 Sample ID: 02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3•; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.13 10.7 92 0.9 6.5 209 102 65 22 48 252 161 270 270 269 0.1 1 North Carolina �4}I?JL'C!� �ILI1� I-171iLj C111�}�LI$\yIS�IA Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler. Commissioner of Aqriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SL004617 Jeff Lingerfelt Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I M-0 manganese index mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm ind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi/uvrst.htm NCDA&CS Al >mic Division Phone: (919) 733-2655 Website: wmn igr.gov/agronomi/ Report No. '20-SL012711 �w�'`'' ""f• Client: Jeff Lingerfelt Advisor: Alex Fox ;, .�Y •`i. 'I Predictive 7338 W Hwy 27 Vale, NC 28168 Synagro 284 Boger Rd Mehlich-3 Extraction Mocksville, NC 27028 ' a'�� Soil Report Sampled County: Lincoln '`"�"'•y5"" Links to Helpful Information Client ID: 318761 Advisor ID: 501947 Sampled: 10/23/2019 Received: 10/30/2019 Completed: 11/08/2019 Farm: NC-Lt-36 Sample ID: 3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.0 120 - 160 0 40 0 0 0 0 0 0 Note: 3 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.71 1.15 8.8 85 1.3 6.1 258 54 62 20 40 177 121 261 261 193 0.1 1 Sample ID: 4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.0 0 0 40 0 0 pH$ 0 0 0 Note: 3 Note: 2 - 0.0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.51 1.13 9.7 91 0.9 6.7 196 49 67 21 43 156 93 228 228 128 0.1 1 Norlh Carolina A- J is311Joxt Tfllsl I lmd C1'14 11%4%% c>l0 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Trox/er, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY20-SLO12711 Jeff Lingerfelt Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not M-0 N mineral -organic soil class nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmitdsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncacrr.gov/agronomi/uvrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL027426 Client: Jeff Lingerfelt Advisor: � Predictive 7338 W Hwy 27 i f�- 'i, r Vale, NC 28168 ` Soil Report Mehlich-3 Extraction 'mot. Sampled County: Lincoln -'�k'ti7icAs Links to Helpful Information Client ID: 318761 Advisor ID: Sampled:03/15/2019 Received: 03/25/2019 completed: 04/04/2019 Farm: Sample ID: 10001 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain 0.0 120 - 160 60 70 0 0 0 0 0 0 Note: 3 2-Soybean 0.0 0 60 70 0 0 0 0 0 0 Note: 3 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.22 0.98 7.1 91 0.6 6.3 34 32 74 15 48 77 58 51 100 100 82 0.1 1 Sample ID: 20001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, E 0.0 50-70 0 30 0 0 pH$ 0 0 0 Note: 12 Note: 2- Fescue/OGrass/Tim, M 0.0 120-200 0 70 0 0 pH$ 0 0 0 Note: 12 Note: Test Results [units - WN in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 1.02 9.9 96 0.4 6.7 151 36 76 18 33 259 161 161 283 283 279 0.1 1 Sample ID: 30001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.0 0 0 50 0 0 pH$ 0 0 0 Note: 3 Note: 2 -Small Grain (SG) 0.0 80-100 0 50 0 0 pH$ 0 0 0 Note: 3 Note: Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.32 1.06 9.2 97 0.2 7.0 159 44 73 22 36 301 176 176 205 205 146 0.1 1 North Carolina F&A �� To i=o Trust Fu mijisslnn Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of AG `-- " ure NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomcl Report No. FY19-SL027426 Jeff Lingerfelt Page 2 of 4 Sample ID: 40001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, E 0.7 50-70 30 70 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, M 0.0 120-200 20 100 0 0 0 0 0 0 Note: 12 Test Results [units - W/V in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.04 5.2 82 0.9 6.1 55 19 64 16 45 169 111 117 73 73 60 0.1 2 Sample ID: 50001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, E 0.6 50-70 0 70 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, M 0.0 120-200 0 100 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.46 1.11 6.1 88 0.8 6.2 103 19 71 15 45 150 99 104 146 146 92 0.1 2 Sample ID: 60001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.0 0 0 10 0 0 pH$ 0 0 0 Note: 3 Note: 2 -Small Grain (SG) 0.0 80-100 0 10 0 0 pH$ 0 0 0 Note: 3 Note: Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.06 8.3 93 0.6 6.6 181 73 75 13 39 193 117 117 223 223 82 0.1 1 Sample ID: 70001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.0 0 0 30 0 0 pH$ 0 0 0 Note: 3 Note: 2 -Small Grain (SG) 0.0 80-100 0 30 0 0 pH$ 0 0 0 Note: 3 Note: Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 1.19 6.0 93 0.4 6.6 197 60 76 12 36 134 81 81 175 175 44 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SL027426 Jeff Lingerfelt Page 3 of 4 Sample ID: 80001 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.0 0 0 20 0 0 0 0 0 0 Note: 3 2 -Small Grain (SG) 0.0 80-100 0 20 0 0 0 0 0 0 Note: 3 Test Results [units - WN in g1cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.06 7.5 91 0.7 6.4 92 68 75 12 65 123 78 78 182 182 56 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY19-SLO27426 Jeff Lingerfelt Page 4 of 4 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn- mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmtsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index Zn-I zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm J 435 Williams Court, Suite 100 Baltimore, IOD 21220 wwwsynagro.com FEBRUARY 26, 2019 NCDEQ Division of, Water Resoures Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2018 Annual Report for Permit No. WQ0002712 Dear NCDEQ: RECEIVED/NCDENROUW MAR 18 2019 WQROS MOORESVIL.LE REGIONAL QFFICI;' RECEI\1EDINCDEQID�R FEB 2 7 2019 Non-Disch Un t Permitting Synagro is submitting one copy and one electronic copy of the above referenced report on behalf of the City of Lincolnton, NC. If you have any questions or need additional information, please do not hesitate to contact Robert Pearson at (704) 736-8940 or Erik Bruce at (336) 703-8681. Sincerely, Derrick Shivar Environmental Compliance Manager Enclosures cc: Robert Pearson, City of Lincolnton Erik Bruce, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD CITY OF LINCOLNTON, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0002712 2018 ANNUAL REPORT City of Lincolnton, NC Residuals Land Application Program 2018 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation- Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00002712 County Lincoln Year 2018 Facility Name (as shown on permit) City of Lincolnton WWTP and WTP NPDES No. NC0025496 & 0085588 Land Application Operator Synaaro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 54 Total number of fields utilized for land application during the year: 17 Total amount of dry tons applied during the year for all application sites: 609.69 Total number of acres utilized for land application during the year: 294.70 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water QualityX YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T A 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of owledge and beli ,true, accurate, and complete. am aware that there are significant penalties for submitting false infon ati cludin the possib' of fines and imprisonment for knowing violations." / Robert Pearson, Water Services Director li Permittee Name and Title (type or print) Signature o Permittee Date Signature ofPreparer* Date Signa e Apple ate (if different from Permittee) (if different fro ermittee and Pr arer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) LINCOLNTON, NC LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID DRY METRIC MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS January 2018 254,200.00 G 16.01 D 14.52 February 2018 638,600.00 G 40.22 D 36.47 March 2018 415,400.00 G 26.15 D 23.72 April 2018 502,200.00 G 58.42 D 53.00 May 2018 613,800.00 G 71.41 D 64.77 June 2018 682,000.00 G 79.35 D 71.96 July 2018 496,000.00 G 57.70 D 52.34 August 2018 508,400.00 G 60.22 D 54.60 September 2018 421,600.00 G 49.92 D 45.28 October 2018 328,600.00 G 37.68 D 34.17 November 2018 452,600.00 G 51.90 D 47.07 YEARLY TOTAL 5,313,400.00 G 548.98 D 497.90 LINCOLNTON, NC WATER PLANT LIQUID MONTH/YEAR AMOUNT UNIT DRY TONS UNIT April 2018 86,800.00 G 14.91 D May 2018 266,600.00 G 45.80 D YEARLY TOTAL 353,400.00 G 60.71 D DRY METRIC TONS 13.53 41.54 55.07 1 /25/2019 SECTION 2 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002712 Laboratory Facility Name: LINCOLNTON, NC Waypoint Analytical Virginia Inc. NPDES# : NCO025496 or WQ# (residual only) WWTP Name: LINCOLNTON WWTP Residuals Analysis Data Product Type LIQ LIQ LIQ LIQ Date Sampled (grab) or 01/25/18 04/20/18 08/22/18 11/30/18 Date Composited Percent Solids 1.51 2.79 2.84 2.75 PARAMETERS (mg/kg dry weight) Arsenic <3 4.21 5.4 7.03 Cadmium <2 <2 <1 <1 Mercury <0.4 <0.4 0.258 0.0476 Chromium 51.4 51.3 48.2 46.4 Copper 181 204 236 216 Lead 5.99 12.6 12.4 11.1 Molybdenum <5 <5 5.35 5.82 Nickel 7.7 14.6 9.09 11.4 Selenium <5 <5 <5 <5 Zinc 265 351 290 308 Total Phosphorus 18800 21200 20900 22800 TKN 72400 71400 107000 54600 Ammonia -Nitrogen 30900 18600 17800 20000 Nitrate and Nitrite <20. 7 2180 407 <4 . 66 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significaplenalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date TURE OF/PREPARE DENR FORM RSSF (5/2003) Printed: Saturday -January 26, 2019 at 17:19:10 for: 2161 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002712 Facility Name: LINCOLNTON, NC NPDES# : NCO025496 or WQ# (residual only) WWTP Name: LINCOLNTON WWTP Residuals Analysis Data Product Type Date Sampled (grab) or Date Composited Percent Solids Laboratory Waypoint Analytical Virginia Inc. LIQ LIQ LIQ LIQ 01/25/18 04/20/18 08/22/18 11/30/18 PARAMETERS (mg/kg dry weight) Aluminum Calcium Magnesium pH Potassium Sodium 1.51 2.79 2.84 2.75 5690 5730 10800 11100 8550 9850 10100 8990 2610 4040 3820 4740 7.90 7.30 7.10 7.90 3670 5850 5110 4190 1990 2180 1730 3290 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significan�etnalties for submitti false information, including the possibility of fines and imprisonment for knowing violations." X TURE OF PREPARER) NR - Data Not Reported or Data Not Required Date�����. DENR FORM RSSF-B (7/2002) Printed: Saturday - January 26, 2019 at 17:23:03 for: 2161 01 Page: 1 of 2 Report Number: 18-030-0209 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 58330 Sample Id : Lincolnton s Waypoinet.M ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 1/25/2018 09:30:00 Date Received: 01/30/2018 00:00 Date Reported: 02/07/2018 Total Solids * 1.51 15100 100.0 JM 01/30/2018 13:45 SM-2540G Moisture * 98.48 100.0 JM 01/30/2018 13:45 SM-2540G Total Kjeldahl Nitrogen 7.24 72400 50.0 R D 01/31/2018 09:30 SM-4500-NH3C-TKN Total Phosphorus 1.88 18800 100 MOS 02/02/2018 17:47 6010C Total Potassium 0.37 3670 100 MOS 02/02/2018 17:47 6010C Total Sulfur 0.70 7000 100 MOS 02/02/2018 17:47 6010C Total Calcium 0.86 8550 100 MOS 02/02/2018 17:47 6010C Total Magnesium 0.26 2610 100 MOS 02/02/2018 17:47 6010C Total Sodium 0.20 1990 100 MOS 02/02/2018 17:47 6010C Total Iron 5030 100 MOS 02/02/2018 17:47 6010C Total Aluminum 5690 100 MOS 02/05/2018 16:04 6010C Total Manganese 98.5 5.00 MOS 02/02/2018 17:47 6010C Total Copper 181 5.00 MOS 02/02/2018 17:47 6010C Total Zinc 265 5.00 MOS 02/02/2018 17:47 6010C Ammonia Nitrogen 3.09 30900 50.0 R D 01/31/2018 09:30 SM-4500-NH3C Organic N 4.15 41500 50.0 01/31/2018 09:30 CALCULATION Nitrate+Nitrite-N <20.7 20.7 MMT 02/01/201814:48 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. ors Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 18-030-0209 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 58330 Sample Id : Lincolnton Waypoint(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com e Project: Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 1/25/2018 09:30:00 Date Received: 01/30/2018 00:00 Date Reported: 02/07/2018 Total Cadmium <2.00 2.00 MOS 02/02/2018 17:47 6010C Total Chromium 51.4 5.00 MOS 02/02/2018 17:47 6010C Total Nickel 7.70 5.00 MOS 02/02/2018 17:47 6010C Total Lead 5.99 5.00 MOS 02/02/2018 17:47 6010C Total Arsenic <3.00 3.00 MOS 02/02/2018 17:47 6010C Total Mercury <0.400 0.400 MOS 02/06/2018 16:51 SW-7471 B Total Selenium <5.00 5.00 MOS 02/02/2018 17:47 6010C pH * 7.9 1.0 JM 01/31/2018 08:30 9045D Total Molybdenum <5.00 5.00 MOS 02/02/2018 17:47 6010C Comments: NC CERT#257, SC CERT#9300 7001 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 1/25/2018 1/112018-3/3112018 0.5920 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (1990 x 1.5100) _ 100 = 30.049 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (8550 x 1.5100) _ 100 = 129.105 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2610 x 1.5100) = 100 = 39.411 Na meq = Na mg/I = Molec.Wgt.Na = 30.049 _ 23 = 1.30648 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 129.105 _ 20 = 6.45525 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 39.411 = 12 = 3.28425 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.30648 + SgrRoot[0.5(6.45525+3.28425)] = 0.592037 Printed: 1/29/2019 Page 1 16:23 Page: 1 of 2 Report Number: 18-114-0212 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 60205 Sample Id : Lincolnton WWTP D Waypoint-( ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 4/20/2018 10:00:00 Date Received: 04/24/2018 00:00 Date Reported: 05/04/2018 Total Solids * 2.79 27900 100.0. R D 04/24/2018 14:30 SM-2540G Moisture * 97.20 100.0 R D 04/24/2018 14:30 SM-2540G Total Kjeldahl Nitrogen 7.14 71400 50.0 JM 04/25/2018 09:00 SM-4500-NH3C-TKN Total Phosphorus 2.12 21200 500 BKN 05/04/2018 01:05 6010C Total Potassium 0.59 5850 100 SMC 04/26/2018 19:23 6010C Total Sulfur 0.73 7270 100 SMC 04/26/2018 19:23 6010C Total Calcium 0.99 9850 500 BKN 05/04/2018 01:05 6010C Total Magnesium 0.40 4040 100 SMC 04/26/2018 19:23 6010C Total Sodium 0.22 2180 100 SMC 04/26/2018 19:23 6010C Total Iron 6030 100 SMC 04/26/2018 19:23 6010C Total Aluminum 5730 100 SMC 04/26/2018 19:23 6010C Total Manganese 139 5.00 BKN 05/04/2018 01:00 6010C Total Copper 204 5.00 BKN 05/04/2018 01:00 6010C Total Zinc 351 5.00 BKN 04/26/2018 19:23 6010C Ammonia Nitrogen 1.86 18600 50.0 R D 04/25/2018 09:00 SM-4500-NH3C Organic N 5.28 52800 50.0 04/25/2018 09:00 CALCULATION Nitrate+Nitrite-N 2180 2.35 MMT 04/27/2018 09:34 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 18-114-0212 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 60205 Sample Id : Lincolnton WWTP D Waypoin(ta ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project : Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 4/20/2018 10:00:00 Date Received: 04/24/2018 00:00 Date Reported: 05/04/2018 Total Cadmium <2.00 2.00 BKN 05/04/2018 01:00 6010C Total Chromium 51.3 5.00 BKN 05/04/2018 01:00 6010C Total Nickel 14.6 5.00 BKN 05/04/2018 01:00 6010C Total Lead 12.6 5.00 BKN 05/04/2018 01:00 6010C Total Arsenic 4.21 3.00 BKN 05/04/2018 01:00 6010C Total Mercury <0.400 0.400 SMC 04/25/2018 16:51 SW-7471 B Total Selenium <5.00 5.00 BKN 05/04/2018 01:00 6010C pH * 7.3 1.0 R D 04/25/2018 09:00 9045D Total Molybdenum <5.00 5.00 BKN 05/04/2018 01:00 6010C Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made i fi�'fL4 to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 4/20/2018 4/112018-7/31/2018 0.7775 DIGESTED LIQUID Na mg/1 = (Na mg/kg x % Solids) -= 100 = (2180 x 2.7900) _ 100 = 60.822 Ca mg/1 = (Ca mg/kg x % Solids) = 100 = (9850 x 2.7900) _ 100 = 274.815 Mg mg/I = (mg mg/kg x % Solids) + 100 = (4040 x 2.7900) _ 100 = 112.716 Na meq = Na mg/I = Molec.Wgt.Na = 60.822 _ 23 = 2.64443 Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 274.815 _ 20 = 13.7408 Mg meq = Mg mg/1 = Molec.Wgt.Mg = 112.716 = 12 = 9.393 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.64443 = SgrRoot[0.5(13.7408+9.393)] = 0.777544 Printed: 1 /29/2019 Page 1 16:23 Way nt-(2) P ANALYTICAL 9/5/2018 Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 18-236-0203 Project Description: Lincolnton WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 8/24/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pam. IV"r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida E871087 North Carolina 257 South Carolina 93007 1:e z Page 1 of 8 (D WayPA®intn NALYTICAL Client: Synagro Central LLC/ Lincolnton Project: Lincolnton WWTP Lab Report Number: 18-236-0203 Date: 9/4/2018 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 62454 Analyte: Al QC Batch No: L397771 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: As QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Ca QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Cu QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Fe QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: K QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Mg QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Mn Page 2 of 8 Waypoint(2) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Mo QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Ni QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: P QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Pb QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: S QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Se QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Zn QC Batch No: L397608 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Page 3 of 8 (D Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 18-236-0203 Client Project Description: Lincolnton WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 SM-4500-NH3C WTN 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 9045D WTN 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 4500NO3F-2011 WTN 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 6010D WTN 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 SW-7471B WTN 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 SM-4500-NH3C-TKN WTN 62425 Lincolnton WWTP Solids 08/22/2018 10:00 08/24/2018 SM-2540G WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 4 of 8 Report Number: 18-236-0203 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 62425 Sample Id : Lincolnton WWTP Waypoint.(D 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 8/22/2018 10:00:00 Date Received: 08/24/2018 00:00 Date Reported: 09/05/2018 Total Solids 2.84 28400 1000 CJR 08/27/2018 16:43 SM-2540G Moisture * 97.20 1000 CJR 08/27/2018 16:43 SM-2540G Total Kjeldahl Nitrogen 107000 478 CLP 08/29/2018 13:00 SM-4500-NH3C-TKN Phosphorus 2.09 20900 50.0 JTR 08/31/201818:52 6010D Potassium 0.51 5110 250 BKN 09/02/201814:06 601OD Sulfur 0.63 6300 50.0 JTR 08/31/201818:52 601OD Calcium 1.01 10100 500 BKN 09/02/201814:06 6010D Magnesium 0.38 3820 50.0 JTR 08/31/201818:52 6010D Sodium 0.17 1730 250 JTR 08/31/201818:52 6010D Iron 9110 50.0 JTR 08/31/201818:52 601OD Aluminum 10800 50.0 JTR 08/31/201818:52 6010D Manganese 224 5.00 JTR 08/31/201818:52 6010D Copper 236 2.50 JTR 08/31/201818:52 6010D Zinc 290 25.0 BKN 09/02/201814:06 6010D Ammonia Nitrogen 17800 25.0 ZBD 08/29/2018 09:30 SM-4500-NH3C Organic N 89200 478 08/29/2018 09:30 CALCULATION Nitrate+Nitrite-N 407 4.93 ZBD 08/281201814:39 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. pmf« m` G0r Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page 5 of 8 Report Number: 18-236-0203 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 62425 Sample Id : Lincolnton WWTP Cadmium Chromium Nickel Lead Arsenic Mercury Selenium pH Molybdenum Comments: •(2) 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 8/22/2018 10:00:00 Date Received: 08/24/2018 00:00 Date Reported: 09/05/2018 <1.00 1.00 JTR 08/31/201818:52 6010D 48.2 2.50 JTR 08/31/201818:52 6010D 9.09 2.50 JTR 08/31/201818:52 6010D 12.4 3.00 JTR 08/31/201818:52 601OD 5.40 5.00 JTR 08/31/201818:52 601OD 0.258 0.0144 TJS 08/29/2018 11:51 SW-7471 B <5.00 5.00 JTR 08131/201818:52 601OD 7.1 SAJ 09/04/2018 08:22 9045D 5.35 2.50 JTR 08/31/201818:52 601OD All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. ?Wic- #1 C 10*r1r Pauric McGroary Agronomist Page 6of8 Waypoint.Q) ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46467 Customer Name: Synagro Central LLC/ Lincolnton Report Number: 18-236-0203 Shipping Method 0 Fed Ex 0 US Postal 0 Lab UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? • Yes 0 No Number of coolers received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No ® Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. • Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes I* No Comments: Signature: lBrandi Watson Date & Time: 08/24/2018 14:16:20 Page 7 of 8 v m w 0 00 SAMPLING LOG # 3��( n �°+& I 7621 iiliilllntlillilllllllllllllillilllillllllllilllllllllllillllli 18 236-0203 46467 IN DIr� CUSTODY nagro Central LLC! Lmcolnton 2018 �Ll Li Lincolnton WWTP 14:13: 9R® & ANALYSES 14:13:50 CUSTOMER: SYNAGR® ° Rich 804/ ���®�® `� I`N C - I attest that the proper ltutu sampling procedures PROJECT MANAGER: ed during the collection of these samples. 3 Z, q/ � 7G 5 r7 `Q� Phone: IJ. SAMPLER A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAS ## SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED �iZZ tT Relinquished by Sam Date Time Recieved by: REMARKS: 8&3 , Iz'-cc f►' Relinquished by: Date Time Recieved by: Relinquished by: UPS A DatQ 41 � Time R�c�d by: SPECIAL INSTRUCTIONS: d V For monitoring purposes. SAMPLE ANALYSIS REQUEST SL1 SL2 NH4 N -NO3 N Or Nanic Cd Cr ' Ni Pb As Hg Se pH equiCaCOv3 Volati Solids Mo Cl NO2 N ko R'0�0 xl�o Ae�o Y'oo y'00 � ko k�o Y100 yoleo SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 8/22/2018 811/2018-9130/2018 0.6247 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (1730 x 2.8400) _ 100 = 49.132 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (10100 x 2.8400) + 100 = 286.84 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3820 x 2.8400) = 100 = 108.488 Na meq = Na mg/I = Molec.Wgt.Na = 49.132 _ 23 = 2.13617 Ca meq = Ca mg/I = Molec.Wgt.Ca = 286.84 = 20 = 14.342 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 108.488 _ 12 = 9.04067 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.13617 _ SgrRoot[0.5(14.342+9.04067)] = 0.624748 Printed: 1/29/2019 Page 1 16:24 WayPA®' nt.y e NALYTICAL 12/13/2018 Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 18-339-0209 Project Description: Lincolnton WTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 12/5/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, P,w (0 c-r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida E871087 North Carolina 2S7 South Carolina 93007 4 "Oeill,iaw!""' ,= Page 1 of 8 Waypoin(2)tn ANALYTICAL Client: Synagro Central LLC/ Lincolnton Project: Lincolnton WTP Lab Report Number: 18-339-0209 Date: 12/13/2018 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 6010D Sample 63830 Analyte: Aluminum QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Arsenic QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Calcium QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Iron QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Potassium QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Manganese QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Phosphorus QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Sulfur Page 2 of 8 (D WayPAoint- NALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Selenium QC Batch No: L412391 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Page 3of8 Waypoint.(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table Report Number: 18-339-0209 Client Project Description: Lincolnton WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 SM-4500-NH3C WTN 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 9045D WTN 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 4500NO3F-2011 WTN 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 6010D WTN 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 SW-7471B WTN 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 SM-4500-NH3C-TKN WTN 63832 Lincolnton WWTP Solids 11/30/2018 10:00 12/05/2018 SM-2540G WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 4of8 Report Number: 18-339-0209 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 63832 Sample Id : Lincolnton WWTP Waypoint.(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.wayp6intanalytical.com Project: Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 11/30/2018 10:00:00 Date Received: 12/05/2018 00:00 Date Reported: 12113/2018 Total Solids * 2.75 27500 100.0 CJR 12/06/2018 16:12 SM-2540G Moisture * 97.20 100.0 CJR 12/06/2018 16:12 SM-2540G Total Kjeldahl Nitrogen 5.46 54600 250 CLP 12/12/2018 14:30 SM-4500-NH3C-TKN Phosphorus 2.28 22800 50.0 KKM 12/10/2018 22:49 601 OD Potassium 0.42 4190 50.0 KKM 12/10/2018 22:49 6010D Sulfur 0.87 8730 50.0 KKM 12/10/2018 22:49 601 OD Calcium 0.90 8990 250 KKM 12/10/2018 22:49 601 OD Magnesium 0.47 4740 50.0 KKM 12/10/2018 22:49 601 OD Sodium 0.33 3290 250 KKM 12/10/2018 22:49 601 OD Iron 8880 50.0 KKM 12/10/2018 22:49 601 OD Aluminum 11100 50.0 KKM 12/10/2018 22:49 601 OD Manganese 257 5.00 KKM 12/10/2018 22:49 6010D Copper 216 2.50 KKM 12/10/2018 22:49 6010D Zinc 308 5.00 KKM 12/10/2018 22:49 6010D Ammonia Nitrogen 2.00 20000 100 ZBD 12/12/2018 14:00 SM-4500-NH3C Organic N 3.46 34600 250 12/12/2018 14:00 CALCULATION Nitrate+Nitrite-N <4.66 4.66 ZBD 12/11/201815:00 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Rffib #1C GQO/" Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pau ric McGroary to the work, the results, or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization. Agronomist Page 5 of 8 Report Number: 18-339-0209 Account Number: 46467 Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 D Waypoint( ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WWTP REPORT OF ANALYSIS Date Sampled: 11/30/2018 10:00:00 Lab Number: 63832 Date Received: 12/05/2018 00:00 Sample Id : Lincolnton WWTP Date Reported: 12/13/2018 RESULT RESULT QUANTITATION PARAMETER o• •. Cadmium <1.00 1.00 KKM 12/10/2018 22:49 6010D Chromium 46.4 2.50 KKM 12/10/2018 22:49 6010D Nickel 11.4 2.50 KKM 12/10/2018 22:49 6010D Lead 11.1 3.00 KKM 12/10/2018 22:49 6010D Arsenic 7.03 5.00 KKM 12/10/2018 22:49 6010D Mercury 0.0476 0.0134 TJS 12/10/2018 12:45 SW-7471 B Selenium <5.00 5.00 KKM 12/10/2018 22:49 6010D pH" 7.9 JSL 12/11/201808:50 9045D Molybdenum 5.82 2.50 KKM 12/10/2018 22:49 6010D Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. pwir' m` G01 Pauric McGroary Agronomist Page 6 of 8 Q) Wayp®int,,. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46467 Customer Name: Synagro Central LLC/ Lincolnton Report Number: 18-339-0209 Shipping Method 0 Fed Ex 0 US Postal 0 Lab • UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? • Yes 0 No Number of coolers received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No ® Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? is Yes 0 No COC agrees with sample label(s)? • Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? • Yes 0 No Sufficient sample volume for indicated test(s)? • Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No ® N/A Trip Blanks received with VOAs 0 Yes 0 No ® N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 41 No Comments: Signature: IMorgan Tichacek Date & Time: 12/05/2018 14:18:40 Page 7 of 8 UT 5 SAMPLING LOG # /L1 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII �. CKAUN OF fCUSYG®Y jam, Synagro Central LLC/ Lmcolnton 46406720189 RECORD & AMALYSES CUSTOMER: SY(�AGR® Lincointon WTP 14:16:08 RECORD PROJECT MANAGER: N« r QLLG0L <„u..ne proper field sampling procedures were used dune the collection of these samples. Phone: (334, `���6c7j 74� (?-ioiUfFe..@S�A05ro.co+� SAMPLER A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED Relinquished by Sampie1r, r Relinquished Relinquished by: \: Relinquished by: SPECIAL INSTRUCTIONS: For 0C. monitoring purposes. lSTAT9 Date Time Recieved by: VV IZ-06 Time Recieved by: Date Time Recieved by: PO#: jO" k� j 3 v' I C �rGf r REMARKS: SAMPLE ANALYSIS REQUEST I.D. SL1 SL2 NH4-N NO3 N Organic N Cd Ct' Ni Pb As H Se pH CaCO3 equiv, Volatile Solids Mo. CI NO2-N SLI: Total Solids (Moisture), Total Kleidahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc co 0 co m o_ Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2161 -01 -LIQ-NC LINCOLNTON, NC WWTP ANAEROB. 11/30/2018 1011/2018-12/3112018 1.1544 DIGESTED LIQUID Na mg/I = (Na mg/kg x % Solids) 100 = (3290 x 2.7500) _ 100 = 90.475 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (8990 x 2.7500) + 100 = 247.225 Mg mg/I = (mg mg/kg x % Solids) + 100 = (4740 x 2.7500) + 100 = 130.35 Na meq = Na mg/I = Molec.Wgt.Na = 90.475 = 23 = 3.9337 Ca meq = Ca mg/I = Molec.Wgt.Ca = 247.225 _ 20 = 12.3613 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 130.35 + 12 = 10.8625 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.9337 _ SgrRoot[0.5(12.3613+10.8625)] = 1.15438 Printed: 1 /29/2019 Page 1 16:24 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002712 Facility Name: LINCOLNTON, NC NPDES# : 01-55-010 or WQ# (residual only) WWTP Name: LINCOLNTON WTP Residuals Analysis Data Product Type WPL Date Sampled (grab) or 02/27/18 Date Composited Percent Solids 4.12 PARAMETERS (mg/kg dry weight) Arsenic 12 Cadmium <2 Mercury 0.0489 Chromium 112 Copper 1060 Lead 21.1 Molybdenum <5 Nickel 22.1 Selenium <5 Zinc 111 Total Phosphorus 5670 TKN 18900 Ammonia -Nitrogen 3390 Nitrate and Nitrite <2.43 Laboratory Waypoint Analytical Virginia Inc. certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pAlties for submittn Ise information, including the possibility of fines and imprisonment for knowing violations." X a'UC�6P L (SIGNATURE OF LK) Date ZaZle DENR FORM RSSF (5/2003) Printed: Saturday - January 26, 2019 at 17:19:26 for: 2161 02 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002712 Facility Name: LINCOLNTON, NC NPDES# : 01-55-010 or WQ# (residual only) WWTP Name: LINCOLNTON WTP Residuals Analysis Data Product Type WPL Date Sampled (grab) or 02/27/18 Date Composited Percent Solids 4.12 PARAMETERS (mg/kg dry weight) Aluminum 139000 Calcium 966 Magnesium 1180 pH 6.40 Potassium 1130 Sodium 201 Laboratory Waypoint Analytical Virginia Inc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant qd alties for submitt% false information, including the possibility of fines and imprisonment for knowing violations." X TURE OF PRE NR - Data Not Reported or Data Not Required DENR FORM RSSF-B (7/2002) Printed: Saturday - January 26, 2019 at 17:23:23 for: 2161 02 Page: 1 of 2 Report Number: 18-060-0207 Account Number: 46467 Submitted By: Erik Bruce Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 58890 Sample Id : Lincolnton WTP D Waypoin(t.. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WTP REPORT OF ANALYSIS Date Sampled: 2/27/2018 10:00:00 Date Received: 03/01/2018 00:00 Date Reported: 03/09/2018 Total Solids 4.12 41200 100.0 JM 03/01/2018 15:00 SM-2540G Moisture * 95.87 100.0 JM 03/01/2018 15:00 SM-2540G Total Kjeldahl Nitrogen 1.89 18900 50.0 JM 03/02/2018 08:30 SM-4500-NH3C-TKN Total Phosphorus 0.57 5670 100 SMC 03/06/2018 14:49 6010C Total Potassium 0.11 1130 100 SMC 03/07/2018 14:20 6010C Total Sulfur 0.33 3260 100 SMC 03/06/2018 14:49 6010C Total Calcium 0.10 966 100 SMC 03/06/2018 14:49 6010C Total Magnesium 0.12 1180 100 SMC 03/06/2018 14:49 6010C Total Sodium 0.02 201 100 SMC 03/06/2018 14:49 6010C Total Iron 51200 100 SMC 03/06/2018 14:49 6010C Total Aluminum 139000 100 SMC 03/06/2018 14:49 6010C Total Manganese 1860 5.00 SMC 03/06/2018 14:49 6010C Total Copper 1060 5.00 SMC 03/06/2018 14:49 6010C Total Zinc 111 5.00 SMC 03/06/2018 14:49 6010C Ammonia Nitrogen 0.34 3390 50.0 JM 03/02/2018 08:30 SM-4500-NH3C Organic N 1.55 15510 50.0 03/02/2018 08:30 CALCULATION Nitrate+Nitrite-N <2.43 2.43 MMT 03/06/201811:53 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. ?W�r- PIC �/ Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page: 2 of 2 Report Number: 18-060-0207 Account Number: 46467 Submitted By: Erik Bruce Send To: Synagro Central LLC/ Lincolnton Mary Brewer 284 Boger Road Mocksville , NC 27028 Lab Number: 58890 Sample Id : Lincolnton WTP • Waypoint-(2 ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: Lincolnton WTP REPORT OF ANALYSIS Date Sampled: 2/27/2018 10:00:00 Date Received: 03/01/2018 00:00 Date Reported: 03/09/2018 Total Cadmium <2.00 2.00 SMC 03/06/2018 14:49 6010C Total Chromium 112 5.00 SMC 03/06/2018 14:49 6010C Total Nickel 22.1 5.00 SMC 03/06/2018 14:49 6010C Total Lead 21.1 5.00 SMC 03/06/2018 14:49 6010C Total Arsenic 12.0 3.00 SMC 03/07/2018 14:20 6010C Total Mercury 0.0489 0.0133 KKM 03/06/2018 14:06 7471A Total Selenium <5.00 5.00 SMC 03/07/2018 14:20 6010C pH * 6.4 1.0 JM 03/02/2018 08:30 9045D Total Molybdenum <5.00 5.00 SMC 03/06/2018 14:49 6010C Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part. nor may any reference be made pofj4 #1C 6ewr to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2161-02-WPL-NC LINCOLNTON, NC WATER PLANT LIQUID 2/27/2018 1/1/2018-12/31/2018 0.2072 Na mg/I = (Na mg/kg x % Solids) _ 100 = (201 x 4.1200) = 100 = 8.2812 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (966 x 4.1200) + 100 = 39.7992 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (1180 x 4.1200) + 100 = 48.616 Na meq = Na mg/I _ Molec.Wgt.Na = 8.2812 = 23 = 0.360052 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 39.7992 + 20 = 1.98996 Mg meq = Mg mg/I + Molec.Wgt.Mg = 48.616 = 12 = 4.05133 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.360052 = SgrRoot[0.5(1.98996+4.05133)] = 0.207165 Printed: 1/29/2019 Page 1 16:40 SECTION 3 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0002 A RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 12.97 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 4.90 ACRES PERMITTED: 4.90 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/28/18 93,000.00 (G) 18979.592 1.51 1.195 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p F 23771 FESCUE PASTURE Feb-18 93,000.00 (G) 18,979.592 10/2/18 24,800.00 (G) 5061.224 2.75 0.580 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 I FESCUE PASTURE 10/3/18 37,200.00 (G) 7591.837 2.75 0.871 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 FESCUE PASTURE Oct-18 62,000.00 (G) 12,653.061 Total Gallons/Ac: 31,632.65 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual Ibs/acre 106 0.028 0.008 0.258 1.059 0.047 0.001 0.029 0.051 0.026 1.527 111.10 Cumulative Ibs/acre 0.348 0.162 5.575 17.689 1.575 0.053 0.544 1.786 0.323 30.691 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop "`77 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X Z IV I (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR-Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0002 B RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 20.19 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/24/I8 74,400.00 (G) 11625.000 2.84 1.377 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE Sep-18 74,400.00 (G) 11,625.000 10/2/18 99,200.00 (G) 15500.000 2.75 1.777 LIL I DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 FESCUE PASTURE Oct-18 99,200.00 (G) 15,500.000 1 1 Total Gallons/Ac: 27,125.00 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 135 0.040 0.006 0.298 1.418 0.074 <.001 0.035 0.066 0.032 1.893 138.60 Cumulative lbs/acre 0.375 0.170 5.594 18.725 1.723 0.056 0.574 1.949 0.331 33.815 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 147 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0ej LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X I� f (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0002 C RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 23.66 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 2/27/18 124,000.00 (G) 12525.253 1.51 0.789 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE PASTURE 2/28/18 37,200.00 (G) 3757.576 1.51 0.237 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE PASTURE Feb-18 161,200.00 (G) 16,282.829 10/2/18 6,200.00 (G) 626.263 2.75 0.072 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 I FESCUE PASTURE 10/3/18 111,600.00 (G) 11272.727 2.75 1.293 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16921 FESCUE PASTURE Oct-18 117,800.00 (G) 11,898.990 Total Gallons/Ac: 28,181.82 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 0.025 0.007 0.232 0.961 0.043 <.001 0.026 0.047 0.024 1.384 100.77 95 Cumulative lbs/acre 0.360 0.169 5.473 17.952 1.596 0.054 0.550 1.814 0.326 31.126 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 4s 162 e.� FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC W WTP ANAEROB. DIGESTED LIQUID X e� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0003 A RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 126.05 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 41.60 ACRES PERMITTED: 41.60 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/11/18 80,600.00 (G) 1937.500 2.79 0.225 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 5/14/18 186,000.00 (G) 4471.154 2.79 0.520 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE May-18 266,600.00 (G) 6,408.654 7/19/18 148,800.00 (G) 3576.923 2.79 0.416 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 29180.00 p 22040 I FESCUE PASTURE 7/20/18 161,200.00 (G) 3875.000 2.79 0.451 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400.p 18,600.00 p 2,180.00 p 22040 I FESCUE PASTURE 7/23/18 186,000.00 (G) 4471.154 2.79 0.520 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE Jul-18 496,000.00 (G) 11,923.077 9/25/18 136,400.00 (G) 3278.846 2.84 0.388 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE 9/26/18 148,800.00 (G) 3576.923 2.84 0.424 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE Sep-18 285,200.00 (G) 6,855.769 10/3/18 31,000.00 (G) 745.1921 2.75 0.085 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. T,000.00 p 4.66 p 16925 FESCUE PASTURE Oct-18 31,000.00 (G) 745.192 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0003 A RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 126.05 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 41.60 ACRES PERMITTED: 41.60 Page : 2 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids Total Gallons/Ac: 25,932.69 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 0.028 0.010 0.305 1.290 0.076 0.002 0.031 0.079 0.030 2.021 128.26 141 Cumulative lbs/acre 0.247 0.138 5.434 16.706 1.413 0.049 0.499 1.635 0.296 26.419 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop I 142 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X (� (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: TURBYFILL PROPERTIES SITE #: NC CA 00035 FIELD# : CA 00035 0003 B RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 23.90 OPERATOR: ELMORE JEFFERY CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.80 ACRES PERMITTED: 8.80 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/15/18 124,000.00 (G) 14090.909 2.79 1.639 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p FESCUE PASTURE May-18 124,000.00 (G) 14,090.909 F57 9/24/18 62,000.00 (G) 7045.455 2.84 0.834 LIL DRY 0-<I/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE Sep-18 62,000.00 (G) 7,045.455 10/2/18 18,600.00 (G) 2113.636 12.75 0.242 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16921 FESCUE PASTURE Oct-18 18,600.00 (G) 1 2,113.636 Total Gallons/Ac: 23,250.00 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 126 0.026 0.009 0.271 1.167 0.067 0.002 0.028 0.069 0.027 1.784 115.44 Cumulative lbs/acre 0.278 0.135 5.046 26.014 1.419 0.050 0.467 1.615 0.280 24.842 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop r 146 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID (SIGNATURE OF L APPLIER) DATE f "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: LEON LEONHARDT SITE #: NC CL 00005 FIELD# : CL 00005 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 21.86 OPERATOR: LEON LEONHARDT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 23.90 ACRES PERMITTED: 23.90 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/26/18 124,000.00 (G) 5188.285 1.51 0.327 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 I FESCUE PASTURE 1/27/18 130,200.00 (G) 5447.699 1.51 0.343 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE PASTURE Jan-18 254,200.00 (G) 10,635.984 2/1/18 93,000.00 (G) 3891.213 1.51 0.245 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE PASTURE Feb-18 93,000.00 (G) 3,891.213 Total Gallons/Ac: 14,527.20 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 43 0.005 0.004 0.094 0.331 0.011 <.001 0.009 0.014 0.009 0.485 34.39 17, Cumulative lbs/acre 0.036 0.017 0.577 1.922 0.086 0.003 0.054 0.141 0.042 2.312 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 156 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X l (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: LEON LEONHARDT SITE #: NC CL 00005 FIELD# : CL 00005 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 18.35 OPERATOR: LEON LEONHARDT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00 Page: 1 Lime Applied *** Date�:[ Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 2/1/18 43,400.00 (G) 2893.333 1.51 0.182 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE HAY 2/2/18 130,200.00 (G) 8680.000 1.51 0.547 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE HAY 2/3/18 117,800.00 (G) 7853.333 1.51 0.495 LIL MOIST 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE HAY Feb-18 291,400.00 (G) 19,426.666 Total Gallons/Ac: 19,426.67 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual Ibs/acre 58 0.007 0.005 0.126 0.443 0.015 <.001 0.012 0.019 0.012 0.648 45.99 Cumulative lbs/acre 0.043 0.021 0.650 2.198 0.098 0.004 0.068 0.147 0.053 2.831 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop 209 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X I (SIGNATURE OF L PLIER) DA E "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: LEON LEONHARDT SITE #: NC CL 00005 FIELD# : CL 00005 0005 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: PACOLET PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 33.90 OPERATOR: LEON LEONHARDT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 16.90 ACRES PERMITTED: 16.90 Page: 1 Lime Applied *** Date F LWA. DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/13/18 124,000.00 (G) 7337.278 2.79 0.854 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 6/14/18 93,000.00 (G) 5502.959 2.79 0.640 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 6/15/18 74,400.00 (G) 4402.367 2.79 0.512 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400.p 18,600.00 p 2,180.00p 22040 FESCUE PASTURE Jun-18 1 291,400.00 (G) 17,242.604 1 Total Gallons/Ac: 17,242.60 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 88 0.017 0.008 0.206 0.818 0.051 0.002 0.020 0.059 0.020 1.408 85.06 ,7 Cumulative lbs/acre 0.054 0.026 0.529 2.406 0.137 0.005 0.068 0.154 0.066 3.654 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop _;x. 100 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X 1� ► (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: LEON LEONHARDT SITE #: NC CL 00005 FIELD# : CL 00005 0007 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 18.75 OPERATOR: LEON LEONHARDT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.80 ACRES PERMITTED: 8.80 Page: 1 Lime Applied *** Date Lb./A. DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) ova Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/9/18 31,000.00 (G) 3522.727 2.79 0.410 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p F 22040 FESCUE PASTURE 6/11/18 62,000.00 (G) 7045.455 2.79 0.820 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 6/12/18 68,200.00 (G) 7750.000 2.79 0.902 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE Jun-18 1 161,200.00 (G) 18,318.182 Total Gallons/Ac: 18,318.18 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 94 0.018 0.009 0.219 0.870 0.054 0.002 0.021 0.062 0.021 1.496 90.36 Cumulative lbs/acre 0.052 0.025 0.688 2.507 0.132 0.005 0.074 0.178 0.062 3.575 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 111 142 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID x l� /19 (SIGNATURE OF LAND ER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: LEON LEONHARDT SITE #: NC CL 00005 FIELD# : CL 00005 0008 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 26.69 OPERATOR: LEON LEONHARDT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 13.30 ACRES PERMITTED: 13.30 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/9/18 55,800.00 (G) 4195.489 2.79 0.488 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p F 22040 FESCUE PASTURE 6/11/18 74,400.00 (G) 5593.985 2.79 0.651 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 6/12/18 80,600.00 (G) 6060.150 2.79 0.705 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 6/13/18 18,600.00 (G) 1398.496 2.79 0.163 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE Jun-18 229,400.00 (G) 17,248.120 Total Gallons/Ac: 17,248.12 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 88 0.017 0.008 0.206 0.819 0.051 0.002 0.020 0.059 0.020 1.409 85.08 Cumulative lbs/acre 0.049 0.024 0.663 2.407 0.126 0.005 0.071 0.171 0.059 3.456 , Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 142 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 i LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X < a- 1%'� � I V)9/o ' (SIGNATURE OF LAND APPLIER) DA E "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: LEON LEONHARDT SITE #: NC CL 00005 FIELD# : CL 00005 0011 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 58.43 OPERATOR: LEON LEONHARDT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 31.30 ACRES PERMITTED: 31.30 Page : 1 Lime Applied *** Date LWAc DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/18/18 111,600.00 (G) 3565.495 2.79 0.415 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 4/19/18 111,600.00 (G) 3565.495 2.79 0.415 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 4/20/18 111,600.00 (G) 3565.495 2.79 0.415 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 4/21/18 74,400.00 (G) 2376.997 2.79 0.277 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 4/30/18 93,000.00 (G) 2971.246 2.79 0.346 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE Apr-18 502,200.00 (G) 16,044.728 Total Gallons/Ac: 16,044.73 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 82 0.016 0.007 0.192 0.762 0.047 0.001 0.019 0.055 0.019 1.310 79.15 Cumulative lbs/acre 0.024 0.012 0.300 1.182 0.070 0.002 0.029 0.088 0.029 1.775 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop >' 3 F 152 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ` 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, [NJ - Injection, SUR N - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: CHUCK WATERS SITE #: NC LT 00019 FIELD# : LT 00019 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 117.71 OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 41.80 ACRES PERMITTED: 41.80 Page : 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/17/18 204,600.00 (G) 4894.737 1.51 0.308 LIL DRY 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE PASTURE 3/18/18 210,800.00 (G) 5043.062 1.51 0.318 LIL DRY 0-<1/2" SUR 0.5 0.20 72,400. p 30,900.00 p 20.70 p 23771 FESCUE PASTURE Mar-18 415,400.00 (G) 9,937.799 4/30/18 86,800.00 (G) 2076.555 4.12 0.357 LIWPL DRY 0-<I/2" SUR 0.5 0.40 18,900. p 3,390.00 p 2.43 p 7901 FESCUE PASTURE Apr-18 86,800.00 (G) 2,076.555 5/1/18 266,600.00 (G) 6377.990 4.12 1.096 LIWPL DRY 0-<I/2" SUR 0.5 0.40 18,900. p 3,390.00 p 2.43 p 7901 FESCUE PASTURE May-18 266,600.00 (G) 6,377.990 8/21/18 24,800.00 (G) 593.301 2.84 0.070 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 I FESCUE PASTURE 8/22/18 111,600.00 (G) 2669.856 2.84 0.316 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE 8/24/18 124,000.00 (G) 2966.507 2.84 0.351 LIL DRY 0-<I/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE Aug-18 260,400.00 (G) 6,229.664 FACILITY NAME: LINCOLNTON, NC OWNER: CHUCK WATERS SITE #: NC LT 00019 FIELD# : LT 00019 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: LLOYD PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 117.71 OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 41.80 ACRES PERMITTED: 41.80 Page: 2 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids Total Gallons/Ac: 24,622.01 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annuallbs/acre 0.047 0.010 0.461 3.654 0.087 0.001 0.029 0.087 0.028 1.082 70.84 93 Cumulative ]bs/acre 0.190 0.077 7.586 14.514 0.794 0.032 0.461 1.000 0.178 14.914 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop b 7 162 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID LIWPL = LINCOLNTON, NC WATER PLANT LIQUID X 7J (SIGNATURE OF L APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: LLOYD OWNER: CHUCK WATERS PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 36.63 SITE #: NC LT 00019 FIELD# : LT 00019 0002 OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 12.70 ACRES PERMITTED: 12.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/10/18 161,200.00 (G) 12692.913 2.79 1.477 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE 5/11/18 62,000.00 (G) 4881.890 2.79 0.568 LIL DRY 0-<1/2" SUR 0.5 0.20 71,400. p 18,600.00 p 2,180.00 p 22040 FESCUE PASTURE May-18 223,200.00 (G) 17,574.803 11/30/18 93,000.00 (G) 7322.835 2,75 0.840 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 FESCUE PASTURE Nov-18 93,000.00 (G) 7,322.835 Total Gallons/Ac: Total Wet Tons/Ac: Total Cubic Yds/Ac: u.uu TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 119 0.029 0.010 0.288 1.197 0.070 0.002 0.030 0.079 0.029 1.953 124.99 Cumulative lbs/acre 0.270 0.134 26.715 16.834 2.451 0.090 0.799 1.603 0.210 27.642 24,897.64 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop ;; 141 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X A ql (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: CHUCK WATERS SITE #: NC LT 00019 FIELD# : LT 00019 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: RIVERVIEW LOAM PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 29.37 OPERATOR: CHUCK WATERS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 13.20 ACRES PERMITTED: 13.20 Page: 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Solids Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pp-) Crop Total Per Acre MONTH 8/22/18 74,400.00 (G) 5636.364 2.84 0.668 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE 8/23/18 148,800.00 (G) 11272.727 2.84 1.335 LIL DRY 0-<1/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE 8/24/18 24,800.00 (G) 1878.788 2.84 0.223 LIL DRY 0-<I/2" SUR 0.5 0.20 107,00(p 17,800.00 p 407.00 p 27147 FESCUE PASTURE Aug-18 1 248,000.00 (G) 18,787.879 1 1 otal Gallons/AC: 18,787.88 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 121 0.024 0.004 0.214 1.050 0.055 0.001 0.024 0.040 0.022 1.291 93.01 Cumulative lbs/acre 0.136 0.065 6.023 9.954 0.690 0.030 0.402 0.746 0.166 13.759 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop �..,. _ 133 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 .-.. 1339.0 267.9 15.0 375.0 E 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X 1 (SIGNATURE OF L PLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 FACILITY NAME: LINCOLNTON, NC OWNER: JEFF LINGERFELT SITE #: NC LT 00036 FIELD# : LT 00036 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CECIL PERMIT #: WQ0002712 ANNUAL DRY TONS APPLIED: 14.93 OPERATOR: JEFF LINGERFELT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.60 ACRES PERMITTED: 8.60 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 11/28/18 117,800.00 (G) 13697.674 2.75 1.571 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 WHEAT 11/29/18 12,400.00 (G) 1441.860 2.75 0.165 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 WHEAT Nov-18 130,200.00 (G) 15,139.534 Total Gallons/Ac: 15,139.53 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 59 0.024 0.003 0.161 0.750 0.039 <.001 0.020 0.040 0.017 1.069 79.17 Cumulative lbs/acre 0.113 0.033 3.160 6.152 0.274 0.012 0.213 0.472 0.094 7.663 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 109 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X !� - -2-/k 5, ) 19 (SIGNATURE OF LAND APPLIER) DATE ` { "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: CECIL OWNER: JOANNE LEATHERMAN PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 4.27 SITE #: NC LT 00036 FIELD# : LT 00036 0004 OPERATOR: JEFF LINGERFELT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 24.10 ACRES PERMITTED: 24.10 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 11/29/18 37,200.00 (G) 1543.568 2.75 0.177 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 WHEAT Nov-18 37,200.00 (G) 1,543.568 Total Gallons/Ac: 1,543.57 Total Wet Tons/Ac: Total Cubic Yds/Ac: 0.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 6 0.002 <.001 0.016 0.076 0.004 <.001 0.002 0.004 0.002 0.109 8.07 Cumulative lbs/acre 0.035 0.013 1.687 2.555 0.111 0.005 0.092 0.217 0.029 2.987 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 99 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 = 1339.0 267.9 15.0 " _•< 375.0 89.0 2500.011 LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID X 1 (SIGNATURE O APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LINCOLNTON, NC PREDOMINANT SOIL SERIES: CECIL OWNER: JOANNE LEATHERMAN PERMIT #: W00002712 ANNUAL DRY TONS APPLIED: 22.04 SITE #: NC LT 00036 FIELD# : LT 00036 0005 OPERATOR: JEFF LINGERFELT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 13.50 ACRES PERMITTED: 13.50 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 11/28/18 55,800.00 (G) 4133.333 2.75 0.474 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600.p 20,000.00 p 4.66 p 16925 WHEAT 11/29/18 136,400.00 (G) 10103.704 2.75 1.159 LIL DRY 0-<1/2" SUR 0.5 0.20 54,600. p 20,000.00 p 4.66 p 16925 WHEAT Nov-18 192,200.00 (G) 14,237.037 1 'I otal Uallons/Ac: Total Wet Tons/Ac: Total Cubic Yds/Ac: 14,237.04 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop •. 99 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LIL = LINCOLNTON, NC W WTP ANAEROB. DIGESTED LIQUID X 2/t%i 9 (SIGNATURE OF L IER) DATE \ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2019 SECTION 4 r-",'VIROt,IM1EN'rilL T=-Cl4t4OLOt.'ES, WC; Arraiyttrrai L baraio6es August 19, 2014 Will Hodges Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Lincolnton WWTP Dear Will Hodges: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http:1Mvw.settek.com Order No.: 14080434 Summit Environmental Technologies, Inc. received 1 sample(s) on 8/6/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, W� Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, Califomia 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Pagel of 5 SunnnitEnvironmental Technologies, Inc. Workorder Rn SU101"Int 3310 Win St. Sample Summary f WRONhIEN`mL TECHWOLOtIES, WC; GryahogaFalls, Ohio 44223 tAnalktieal L-hangtvries TEL: (330) 253-8211 FAX.• (330) 253-4489 WO#: 14080434 Website: hQ:1Mvw.settek.com 19 Aug-l4 CLIENT: Synagro Project: Lincolnton WWTP Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14080434-001 Lincolnton WWTP 8/5/2014 9:45:00 AM 8/6/2014 9:55:00 AM Sludge Page 2 of 5 Summit Environmental Technologies, Inc. WO#: 14080434 SUMMIT r 1T r:Pi11R4�h1r�tENTI�L ._Ct:CdOL.dGJc'S, 1Pty 3310 Win St. Ct aho a Falls, Ohio 44223 tY g Date Reported 8/19/2014 AP,aiyfical Lpborarorle5 TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: htW:1A+nvw.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 8/6/2014 Project#: Lincolnton WW TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lincolnton WWTP 001 8/5/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 8/11/2014 VVK Lincolnton WWTP 001 8/5/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 8/11/2014 VVK Lincolnton WWTP 001 8/5/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 8/11/2014 VVK Lincolnton WWTP 001 8/5/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 8/11/2014 VVK Lincolnton WWTP 001 8/5/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 8/11/2014 VVK Lincolnton WWTP 001 8/5/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 8/11/2014 VVK Lincolnton WWTP 001 8/5/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 8/11/2014 VVK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lincolnton WWTP 001 8/5/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 8/11/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client EW Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lincolnton WWTP 001 8/5/2014 Chlordane, total 0.010 ND mg/L Sludge EPA 8081 B 1 0.030 8/18/2014 JBN Lincolnton WWTP 001 8/5/2014 Toxaphene 0.10 ND mg/L Sludge EPA 8081 B 1 0.50 8/18/2014 JBN Lincolnton WWTP 001 8/5/2014 Endrin 0.0020 ND mg/L Sludge EPA 8081 B 1 0.020 8/18/2014 JBN Lincolnton WWTP 001 8/5/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 8/18/2014 JBN Lincolnton WWTP 001 8/5/2014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 8/18/2014 JBN Lincolnton WWTP 001 8/5/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 8/18/2014 JBN Lincolnton WWTP 001 8/5/2014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 8/18/2014 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lincolnton WWTP 001 8/5/2014 1,1-Dichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 1,2-Dichloroethane 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Benzene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Carbon tetrachloride 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Chlorobenzene 0.10 ND mg/L Sludge EPA 8260 B 1 100 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Chloroform 0.10 ND mg/L Sludge EPA 8260 B 1 6.0 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Tetrachloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Trichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 Vinyl chloride 0.20 ND mg/L Sludge EPA 8260 B 1 0.20 8/11/2014 MES Lincolnton WWTP 001 8/5/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 200 8/11/2014 MES Page 3 of 5 An Summit Environmental Technologies, Inc. WO#: 14080434 3310 Win St. i=UVIRONMENTAL TECIiNOLOG; , Cuyahoga Falls, Ohio 44223 Date Reported 8/19/2014 r4naiyfics�l L harai�rie TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: http:1Avww.settek.con: Address: 284 Boger Rd. Mocksville NC 27028 Received: 8/6/2014 Project#: Lincolnton WW SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lincolnton WWTP 001 8/5/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 2,4,6-Trichlorophen ol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 8/10/2014 JRT butadiene Lincolnton WWTP 001 8/5/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 8/10/2014 JRT Lincolnton WWTP 001 8/5/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 8/10/2014 JRT SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lincolnton WWTP 001 8/5/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 8/15/2014 AMZ Lincolnton WWTP 001 8/5/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 8/15/2014 AMZ Page 4 of 5 SunnnitEnvironmental Technologies, Inc. WO#: 14080434 3310 Win St. LIJRWIRONMENTAL TEMPdOLOG1=_a, li Cuyahoga Falls, Ohio 44223 Date Reported $/19/2014 4rsiV tins; L.-boraforfe-,+ TEL: (330) 253-8211 FAX: (330) 253-4489 Company: Synagro Website: hho:/Ammsettek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 8/6/2014 Project#: Lincolnton WW Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Lincolnton WWTP 001 8/5/2014 Flashpoint (140°F) Lincolnton WWTP 001 8/5/2014 Total PCBs Lincolnton WWTP 001 Lincolnton WWTP 001 Lincolnton WWTP 001 8/5/2014 Cyanide, Reactive 8/5/2014 pH 8/5/2014 Sulfide, Reactive >140 °F Sludge EPA 1010 1 8/7/2014 TAH ND mg/Kg Sludge EPA 8082 1 0.20 8/18/2014 JBN ND ppm Sludge EPA 9014 1 0.50 8/7/2014 TIR 7.0 s.u. Sludge EPA 9045 D 1 8/7/2014 AYS 30 ppm Sludge EPA 9034 1 25 8/7/2014 TIR Page 5 of 5 Rev. 12 Date: 07/27/13 SLtr' nit Environmental Technologies, 5nc. Coder Receipt Form // ll initials of person inspecting cooler and samples: Client: s ` C_ t� _ Order IJumber: Date Received: tJ r ( Time Received: V 1 bate cooler(s) opsred and samples Inspacad:_C� lJ ( r Nue -Gf Coolers[Bcx ' NVA Shipper.,F6� UPS DHL Airborne US Postal Walk-in Pickup Other. Packaging: Peanuts '1 oWr f bhle ap) Pap e Foam None Cater: Tape on coolerlbOx Pt/�) N NIA Custody Seats ,ntact N NIA C-O•C in plastic . �' tt N NA Ica - slue ice Sample Temperature IR Gun A1602G459 CF�� �`C aresenp I abs nt I melOd f 11A �C °C NIA 1 RadMogical Testing Instrument serial P35127 isle page 2 for scan results) Y N "Use 9 sheet per sample for Radiological Testing. If sample is HOT, the Radiological Safety Officer must be nct fled immediately. C-O-C filled out properly x N IVA Sarnpies in separate bags C N sjV� NIA Sample containers intact' N CCJ� NIA '€f no, list broken sample(s): Sample lab'el(s) complete (ID, date, etc.) NIA. Label(s) agree with C-O-C �iC� � N N/A Corect containers used `ir Pl NIA Sufficient sample received ( Yf f" N N/A Butbles absent from 40 mL vials— Y N `_>IA " Samples with bubbles <omm are acceptable. Indicate bubble size if >6mm. Was client contacted about samples Y N Will client send new samples Y N Client contact: Logged in G QC SHAP.EMDocument Control Templates - Tracking\Gdoler receipt form P.Ev. 12 07-27-13.doc Page 1 bf 2 mI CL Summit Environmental Technologies, Inc. y 3310 Win St. Am IT 1�11 1lfAf C�SL+alL v,r tr,, Cuyahoga Falls, Ohio 44223 as axre f L „� rI TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httP.1Avww.settek.com July 29, 2015 Will Hodges Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Lincolnton WTP Dear Will Hodges: Order No.: 15072087 Summit Environmental Technologies, Inc. received 1 sample(s) on 7/21/2015 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, A-1-90 Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A21-A 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Comecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Minois 200061 and Reg.5, Indiana C-0H-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-0PH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New Yodr 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, OregonOH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDAIAPHIs P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 10 i. �?* SummiI Environmental Technologies, Inc.Narrative h ologies I Case 3310 Win St. ?s^:3 i fIT • i-' Wfi;d!4V EWr*AL Cuyahoga Falls, Ohio 44223 WO#: 15072087 TEL: (330) 253-8211 FIX.' (330) 253-4489 Website: hty.-11Www.settek.com Date: 7/29/2015 CLIENT: Synagro Project: Lincolnton WTP This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway Haddock, GA 31033 All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. Summit Environmental Technologies, Inc., holds the accreditation/certifications listed at the bottom of the cover letter that may or may not pertain to this report. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency. Any comments or problems with the analytical events associated with this report are noted below. Original Page 2 of 10 Summit Environmental Technologies, Inc. Case Narrative 3310 Win St. x F d� ] AT ��� 1 y�crLl��r � �� ` Cuyahoga Falls, Ohio 44223 Wp#; 15072087 TEL: (330) 253-8211 FAX: (330) 2534489 Website: hap://www.settek.com Date: 7/29/2015 CLIENT: Synagro Project: Lincolnton WTP j Analytical Comments for SVOC-BNA TCLP(8270), Sample LCS-14767, Batch ID 14767 : The BNA TCLP LCS (Batch 14767) exhibited poor recoveries for Hexachloroethane, Surrogate: 2- Fluorobiphenyl and Surrogate: p-Terphenyl-dl4. The MSD exhibited control. Analytical Comments for SVOC-BNA TCLP(8270), Sample LCS-14704, Batch ID 14704 : The BNA TCLP LCS (Batch 14704) exhibited a high recovery for Surrogate: p-Terphenyl-dl4. Original Page 3 of 10 - T Summit -Environmental Technologies, In Qualifiers and Acronyms 3310 Win S arr#at fil§3 atia3t .e= pLG Cuyahoga Falls, Ohio 442= WO#: 15072087 TEL: (330) 253-8211 FAX. • (330) 253-445 Website: htro://www.settekco. Date: 7/29/2015 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. X The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+), R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit NIB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quamitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit NISD Matrix Spike Duplicate MCI, Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextractlon CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data - Original Page 4 of 10 `} Summit Environmental Technologies, Inc. Workorder 3310 Win St. rh009AlxL.: t 9 t a111 xe; Cuyahoga Falls, Ohio44223 Sample Summary. TEL: (330) 253-8211 FAX. 253-4489 Wp#: 15072087 Website: hn .-11www.settek.com 30-Jul-I5 CLIENT: Synagro Project: Lincolnton WTP Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 15072087-001 Licolnton WTP 7/20/2015 10:00:00 .AM 7/21/2015 10:05:00 AM Sludge Page 5 of 10 Summit Environmental Technologies, Inc. Analytical Report -� 3310 Win St. 1 elrit;tylt,rt1 "* �U:v� „- Cuyahoga Falls, Ohio 44223 (base report) TEL: (330) 253-8211 FLY.• (330) 253-4489 WO#: 15072087 Website: hitp:/hvww.settek.com Date Reported: 7/29/2015 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 7/20/2015 10:00:00 AM Lab ID: 15072087-OOIA Project: Lincolnton WTP Client Sample ID Licolnton WTP Analyses Result RL Qual Units DF Date Analyzed :I RCI SW9045D i Analyst: MS PH (SW9045D) pH 6.48 s.u.@23.8 1 7/23/2015 3:59:00 PM Qualifiers . Value exMax ceeds irmmm Contammant Level E ve Value aboquantitadoa range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below MmhatmmCompound Limit N Tentatively identified compounds ND Not Detected at the Reporting Limit 0 RSDisgreaterthan RSDlimit ' P Second column confirmation exceeds PL Permit Limit Original � R RPD outside accepted recovery limits RL Reporting Detection Limit U Sables with C.IcW <MDL I Analyte detected below quandtation Imes Page 6 of 10 `' Summit Em�ironmental Technologies, Inc. wo#: 1so7zas7 u 5r rrar�r�t 1P,�}'" li"vtLt 3310 Win St. Cuyahoga Falls, Ohio 44223 Date Reported: 7/29/2015 ` TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Wehsite: httD://www.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 7/21/2015 Project#: Lincolnton WTP TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Licolnton WTP 001 7/20/2015 TCLP Arsenic(As) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 7/23/2015 WK Licolnton WTP 001 7/20/2015 TCLP Badum(Ba) 5.00 ND mg/L Sludge EPA 6010 C 1 100 7/23/2015 WK Licolnton WTP 001 7/20/2015 TCLP Cadmium(Cd) 0.100 ND mg/L Sludge EPA 6010 C 1 1.00 7/23/2015 WK Licolnton WTP 001 7/20/2015 TCLP Chromium(Cr) 0.200 ND mg/L Sludge EPA 6010 C 1 5.00 7/23/2016 WK Licolnton WTP 001 7/20/2015 TCLP Lead(Pb) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 7/23/2015 WK Licolnton WTP 001 7/20/2015 TCLP Selenium(Se) 0.500 ND mg/L Sludge EPA 6010 C 1 1.00 7/23/2015 WK Licolnton WTP 001 7/20/2015 TCLP Silver(Ag) 0.500 ND mg/L Sludge EPA 6010 C 1 5.00 7/23/2015 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Licolnton WTP 001 7/20/2015 TCLP Mercury 0.00200 ND mg/L Sludge EPA 7470 A 1 0.200 7/23/2015 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Licolnton WTP 001 7/20/2015 Chlordane, total 0.0250 ND mg/L Sludge EPA 8081 B 1 0.0300 7/27/2015 JBN Licolnton WTP 001 7/20/2015 Toxaphene 0.0500 ND mg/L Sludge EPA 8081 B 1 0.500 7/27/2015 JBN Licolnton WTP 001 7/20/2015 Endrin 0.00250 ND mg/L Sludge EPA 8081 B 1 0.0200 7/27/2015 JBN Licolnton WTP 001 7/20/2015 gamma-BHC 0.00250 ND mg/L Sludge EPA 8081 B 1 0.400 7/27/2015 JBN Licolnton WTP 001 7/20/2015 Heptachlor 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 7/27/2015 JBN Licolnton WTP 001 7/20/2015 Heptachlor epoxide 0.00250 ND mg/L Sludge EPA 8081 B 1 0.00800 7/27/2015 JBN Licolnton WTP 001 7/20/2015 Methoxychlor 0.00250 ND mg/L Sludge EPA 8081 B 1 10.0 7/27/2015 JBN Licolnton WTP 001 7/20/2015 Surr: Tetrachloro-m- 5-119 0 %REC Sludge EPA 8081 B 1 7/27/2015 JBN xylene Licolnton WTP 001 7/20/2015 Surr: DCB 5-119 0 %REC Sludge EPA 8081 B 1 7/27/2015 JBN Page 7 of W r + Summit Environmental Technologies, Inc. gi WO#: 15072087 1 rNC1(1ii��31a�L1IdL7L _,� 3310 Win St. Cuyahoga Falls, Ohio44223 Date Reported: P 7/29/2015 .. TEL: (330) 253-8211 FAX.• (330) 253-4489 Company: Synagro Website: htto:/Avww.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 7/21/2015 Project#: Lincolnton WTP VOC by GC/MS (8260)-TCLP Client EN Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF Re;Lvl Run Analyst Licolnton WTP 001 7/20/2015 1,1-Dichloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.700 7/23/2015 JCR Licolnton WTP 001 7/20/2015 1,2-Dichloroethane 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 7/23/2015 JCR Licolnton WTP 001 7/20/2015 MEK 2.00 ND mg/L Sludge EPA 8260 B 1 200 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Benzene 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Carbon tetrachloride 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Chlorobenzene 0.100 ND mg/L Sludge EPA 8260 B 1 100 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Chloroform 0.100 ND mg/L Sludge EPA 8260 B 1 6.00 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Tetrachloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.700 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Tdchloroethene 0.100 ND mg/L Sludge EPA 8260 B 1 0.500 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Vinyl chloride 0.200 ND mg/L Sludge EPA 8260 B 1 0.200 7/23/2015 JCR Licolnton WTP 001 7/20/2015 Surr: 4- 70-130 96.9 %REC Sludge EPA 8260 B 1 7/23/2015 JCR Bromofluorobenzene Licolnton WTP 001 7/20/2015 Surr: 70-130 105 %REC Sludge EPA 8260 B 1 7/23/2015 JCR Dibromofluoromethane Licolnton WTP 001 7/20/2015 Su.. Toluene-d8 70-130 98.0 %REC Sludge EPA 8260 B 1 7/23/2015 JCR SVOC 8270 TCLP BNA List Client ID# Lab EN Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst Licolnton WTP 001 7/20/2015 1,4-Dichlorobenzene 0.100 ND mg/L Sludge EPA 8270 C 1 7.50 7/28/2015 RLF Licolnton WTP 001 7/20/2015 2,4,5-Trichlorophenol 0.250 ND mg/L Sludge EPA 8270 C 1 400 7/28/2015 RLF Licolnton WTP 001 7/20/2015 2,4,6-Trichlorophenol 0.250 ND mg/L Sludge EPA 8270 C 1 2.00 7/28/2015 RLF Licolnton WTP 001 7/20/2015 2,4-Dinitmtoluene 0.100 ND mg/L Sludge EPA 8270 C . 1 0.130 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Cresols, Total 5.00 ND mg/L Sludge EPA 8270 C 1 200 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Hexachloro-1,3- 0.100 ND mg/L Sludge EPA 8270 C 1 0.500 7/28/2015 RLF butadiene Licolnton WTP 001 7/20/2015 Hexachlorobenzene 0.100 ND mg/L Sludge EPA 8270 C 1 0.130 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Hexachloroethane 0.100 ND mg/L Sludge EPA 8270 C 1 3.00 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Nitrobenzene 0.100 ND mg/L Sludge EPA 8270 C 1 2.00 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Pentachlorophenol 0.250 ND mg/L Sludge EPA 8270 C 1 100 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Pyridine 0.250 ND mg/L Sludge EPA 8270 C 1 5.00 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Surr: 2-Fluorophenol 5-109 46.3 %REC Sludge EPA 8270 C 1 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Surr: Phenol-d6 5-109 44.7 %REC Sludge EPA 8270 C 1 7/28/2015 RLF Licolnton WTP 001 7/20/2015 Sur.. Nitrobenzene- 19-120 51.0 %REC Sludge EPA 8270 C 1 7/2812015 RLF d5 Licolnton WTP 001 7/20/2015 Surr: 2,4,6- 10-120 40.1 %REC Sludge EPA 8270 C 1 7/28/2015 RLF Tribromophenol Licolnton WTP 001 7/20/2015 Surr: 2- 22-117 49.8 %REC Sludge EPA 8270 C 1 7/28/2015 RLF Fluorobiphenyl Licolnton WTP 001 7/20/2015 Surr: p-Terphenyl- 34-116 58.1 %REC Sludge EPA 8270 C 1 7/28/2015 RLF d14 Page 8 of 10 Summit Environmental Technologies, Inc. 3310 Win St. WO#: 15072087 A z. �itat]9i 7 4� __. Cuyahoga Falls, Ohio 44223 Date Reported: 7/29/2015 J -�� TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: htta://www.settekcom Address: 284 Boger Rd. Mocksville NC 27028 Received: 7/21/2015 Project#: Lincolnton WTP SVOC SW-846: 8321 Herbicides-TCLP Client EN Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Licointon WTP 001 7/20/2015 2,4-D 5.00 ND mg/L Sludge EPA 8321 A 1 10.0 7/24/2015 BJH Licointon WTP 001 7/20/2015 2,4,5-TP 0.500 ND mg/L Sludge EPA 8321 A 1 1.00 7/24/2015 BJH Licolnton WTP 001 7/20/2015 Surr: 2,4- - %REC Sludge EPA 8321 A 1 7/24/2015 BJH Dichlorophenylacetic acid Page 9 of 10 ZZ Summit Environmental Technologies, Inc. g` WO#: 15072087 3310 Win St. s £tl�€��l}e st1s�� r azsc5t>i_r s+: Cuyahoga Falls, Ohio 44223 Date Reported: 7/29/2015 TEL: (330) 253-82I1 FAX• (330) 253-4489 Company: Synagro Website: httn://www.settekcom Address: 284 Boger Rd. Mocksville NC 27028 ! i Received: 7/2112015 i Project#: Lincolnton WTP i Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Licolnton WTP 001 7/20/2015 Flashpoint (140°F) >140 °F Sludge EPA 1010 1 7/22/2015 TAH Licolnton WTP 001 7/20/2015 Total PCBs ND mg/Kg Sludge EPA 8082 1 1.95 7/27/2015 BJH Licolnton WTP 001 7/20/2015 Surr: Tetrachloro-m- 87.6 %REC Sludge EPA 8082 1 5-119 7/27/2015 BJH xylene Licolnton WTP 001 7/20/2015 Cyanide, Reactive ND mg/Kg Sludge EPA 9014 1 0.500 7/23/2015 MS Licolnton WTP 001 7/20/2015 Sulfide, Reactive ND mg/Kg Sludge EPA 9034 1 25.0 7/23/2015 MS Page 10 of 10 S�a.m6it Ehvitoijh. e�ital t'hnologles c; - z�,�. ,.ri. �ro��. ,04lyOs �equestl:, aj n,.of C * stc +dy se dw nd4e' I palpatu'ZIP.010 Sim e4x& wwq>. s;?Iqqnq VM Said was.j.,: it" said -Wes YIN VIN N ?Ian `% YIN :N WN 44 (�vp446jE.P4tdjj 4ja�diu. (s) dwe Oqu1. PRO D-O-Q. 'A aq pnwj9*Wo.Aj*pS 1.11* E (igif UU05 jca3 Zzoed aas) -IN4 VIN 3;--a 4? �.gzAwi- uoo.-si.wei" ci"dw I:el, ..0 gs :ViN Papaw I qp an YIN A AP 01,0 n**-z)*,. Dco�"Jow UO edeL. LIM13.4 �atap do NIPAA. lqsP8!M -SJfj' ,YIN 01 - OCC'IOJeqwrlN /14 pea-d-ISmdums pun pou�O (Spa., ra _O)T Well!) P- 141000 M4m—d 1000 *21ul ew.uqAIAU3 ;ttuwns SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WQ Permit Number: WWTP Name: Lincolnton WWTP NPDES Number: Monitoring Period: From 01/01/18 To 03/31/2018 WQ 0002712 NC 0025496 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlirnhle to alternative nerfnrmed (Class A nr Class Rl romnlete the fnllnwinu mnnitnrinv data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6` MPN MPN/g Coliform power per gram of total solids 22947 94837 281250 CFU/g 0 Quarterly Grab 9222D CFU SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Mt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." —RoA Pearson Water Sery,'c s Director P e r Na 6 2nd Tit ype or print) Land Applier Name and Title (if applicable) (type or print) Signature of Preparer at Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 22947 4.36 Min 79470 4.90 Max 83784 4.92 Geometric Mean 101,594 5.01 172535 5.24 91603 4.96 281250 5.45 Average 4.98 22947 281250 94837 Technician SM 2540 &1997. 2540 D 4 Quarter / Year l Q O-Lc) j All weighings are done in grams Q. Z-PL .. Time Collected T¢� C C1Q� Dsis—L—) Date Collected 11�J r G Date/Time In Date/Time Out Total Wet Wgt 1. lr*4 3 42LO Dish t44,,?0$s L16.6.0bt{ 2047 Wet Sludge Wgt (105-105°C) Dried w9t q?.29� 4?. may �}(A3ay Dish (�i� Lit. 20 4? Dry Solids Wgt d .SQO qa D .` n4 e, % Solids g 33% g a-3�� AVG % Solids O • d� r� - Time InlOut . (103-10�g) Dried q 7.294 +�?•5lS �( 41143 9-4 55o°cwt µto. SSla. LKO."toy 41.3Ito7 Volatile Solids Wgt 0� 44$0 b• h 0 •� 5 �r, % Volatile Solids Olt Q v L f-(01 AVG % Volatile Sollds TS DAF 3A % TS Sludge = a 1 % VS DAF = 6-4- (0 { % VS Slud e = / �O LI ` j4 it?V- p. oWo p .S-40 — 0. (05os "Sq % Total Solids = Dry Solids Wgt X 100 0.Oi to ? Wet Solids Wgt - ZO 0,1 a 0 ��ea Yo Volatile Solids .= (Volatile Solids Wgt) X 100 Dried Solids Wgt % Reduction w (VS DAF - VS Siudge) X 100 3 VS DAF - (VS DAF)(VS Sludge) ®�® Technician DS SM 2540GA997.2540D-19K Quarter Year All weighings are done in grams ns4z";* 53 zw� 14 t-� nr� �pp��-jIM:•+. "F, n WN" Time Collected 11o4 oq05 Date Collected 1748 k%--i C6� Date Time In Oct 'q llq[S- 0 et 3S-/133 t 12 S 5 -4 3 L--) Vrs'S G 4(0 1k1;a ZI? 10. %% D.X /IqOS- C) ej a / 1,4 lqo Date 1%r Is -,I% I- Ict- L I; I - 2- -b- t !a Time Out 0 (0 ca S7- L4 a Total VVet Wgt -63-1931 57.CA5'1 (pt? %qS 2 G1p,92o5 53.12'WZ STr.SWZ 77.7731 7pTSV .27 �.0(,Vj Dish - q (0.70-tc]6 q((,-fffl0(0qj ( Pt IVY f// US V 46- . 0&-7 01-205T 46-7010 41.&OqS- 4(..24,Frs Wet Sludge Wgt -7. 0'943 1 t -OY15' 10C&V '3A157;1co 20,�3S IVRTS'a IVRITIr 31Scqq 2(-DQir- 253Saf 31-7Tff'7 2.3,5153 30,025M (I 03-1051,C) Dried Wgt ZqA 2 . ,2 q*7.5,Sq t45.543-,: qj 2,pq q.-4tf Lj,7-q4t9 4. I&T '1 -4 , q555--jq q,7.31oq q2_05V. quoSY7 q(d.S-qSfr Dish 0 �I-ZO51 ql.Zoj ql.ZoqS q( Dry Solids Wgt o.5qC4 L-).elo?o 47 q wwj) G - ?G22, o,,5,q +3 0AP00 of, c).(P&zS o.r34,4 P-q542 % Solids 3 3.O(7 . 3. I q,ca 12, Average % Solids <6- - 'MOD RPID % Total Solids = Dry Solids Wgt X100 Wet Solids Wgt SLUDGE Fecal Coliforms —See Effluent Fecal Coliform Setup for QA Data Meth d 9222b SM 27 T ° - Collection Date The By Water Bath Setup < 8 hours after Grab Read 24 +/- 2 hours Setup Removal Time In By Temp Time Out By Temp o . Colony Count per Fflter B st ed Calculate Colonies per 100 mL/Fliter Colonies per 100 mL/Fliter C emperatures % TOTAL SOLIDS D are in C -Reportable Colonies per g CID ml Used A ," R"I$ ngSS ¢ oao�y 0 ` �i t � 4s o.o, 19 I Ito poa5 a 4�7 CFU 0.1 0,116 pq.. isGr pgL(o y�k5' OjLfS 0 aN°� ov° 3 oa`t �1� r �o CFU t _ox,',� ltoo cjc� O4�S y S 0.01 �� 310 000 000 Al �0 83,E CFU ("I $ ()%q7 VZ pQ(t,- d q45 o13 r qq, a.a1 51 5lofo o o 15 f o 5.09, g +� 1�►, CPU 7.4 ' � q 1 a l 't'7. S� p 7as c 0 Llq 0.01 . _i ` gaop LIQ°,000 °%vt5� �• t CFU 1-t b TA4 NT �- i . aq 0 ! 000 a _cot-� R I �03 , CFU °a. l3 Zb0000 0405 �is ba1S ��f s- 0.01 S� 5 oi��a 'Jr 401000 q'q �. 1 25a 2� j CFU ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WQ Permit Number: WQ 0002712 WWTP Name: Lincolnton WWTP NPDES Number: NC 0025496 Monitoring Period: From 04/01/18 To 06/30/2018 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlicable to alternative nerformed (Class A or Class R) cmmnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 611 MPN MPN/g Coliform power per gram of total solids 2616 25002 446808 CFU/g 0 Quarterly Grab 9222D CFU SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an _ explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Robert Pearson, Water Services Director Pr p rer Na ��e and T' (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 446808 5.65 Min 99291 5.00 Max 8721 3.94 Geometric Mean 5,194 3.72 17500 4.24 66378 4.82 2616 3.42 Average 4.40 2616 446808 25002 Technician .5M2909-1997,2540D-1997 Quarter/Year per & C3(0((s PJI weighings are done in grams P.N' 00%,'A"MI, man, ME M11 �S. - , - . — M, ln�,M, wl� Time Collected Date Collected Date I Time In Date I Time Out Total Wet Wgt Dish q&. 707G 2 ()Carr Wet Sludge Wgt 23.3 r2 ?-9 3o. (103-105°C) Dried Wgt q ss(oq 4-7-v14(, Dish 41 C4. Saari Dry Solids Wgt C) doss % Solids 0% AVG % Solids 0 3, 2, Time In/Out 0-755 (103-1050C) Dried Wgt q'7014 (o q2.00cp.3 51501)C Wt qq t. 3 Volatile Solids Wgt (0 ") % Volatile Solids -7(,P.?(-p -7G. co Ll 2,92 AVG "7(,o. % Volatile Solids % TS DAF = %TSS[udge= % VS DAF = Is q - a"? %VSS[udge= 71o.?a I -%- PQ C).-,6 -- & 1�V % Totaf Solids = C)LySollda Wgt -X 100 Wet Solids Wgt % Volatile Solids = (Volatile Solids Wgt) x 100 Dried Solids Wgt % Reduction .= (VS DAP - VS Sludge) A 100 VS DAF - (VS DAF)(VS Sludge) O & -7s, ?" 0 , 0 - o- SL Technician Ne SM 2540G-1997,2549D -1 970 Quarter Year Q E3 All welghlhgs are done in grams SO g 4;11 W gg 5 L tg Time Collected (:)q oltas 14 S Z),aqo Date Collected L)- Date Ic�RZLfoq33 Time In q,3-ts /4-61ck 4-114-1 �i 'A-10-t /D S'a-M 0431 t4-vo-t8/ Date I Time Out 9-14e/oG3T II /c*qS--(4-toAS-/q(A1 Ir 4* 11 7� Total Wet wgt r).q. 1(0.(40 6 VnMd (,,elfcsn"d (006 (.q2q 7 3.,jq-, 1 (09.(.0 ?9'(- 17?e>3SI j Dish 44—M At#--70-741 91-0- Vn tkM 4LLqW% q 6 (0 OEr *4-3ooO I 0. 7ol M04 qLL290i �?CNQ 301.0a? 4(,.-?lq7 q6-ito,09 Wet Sludge wg' 3q.ZGt7 24t.'%W 2,54US0 ;63541 7qA,2,l 2.1334I 7-339S-011 30-9Zf9' 2-LA.H31-2,4(,V,3 2.5.8M 30.S3Z.L) 23ASSS 22!i.996 (Tas-1o5°C) Dried Wgt LKLIo2- 41272 t/qe,0q-jq i/q.(,s(ot LILL"id q705,?(, qLtss(a? q7. tAL(979W LIS 12-20 40.OS3() 1'7.3'712, q-7. vs Dish 4LL7-fq qt,,.-70?j qLLU75 qQ .741" L14 4(o6l LILLuol 4f4.?07 qf .2j. rg qLC29 L1471qj 3 J. (.7()7 (A(...,7tq L4f Dry Solids w9t a.oq6,a O..S(,qte 0.,5�60j 035'9-1 C).q3-V(,o 0-q51LP 0-7-S(oSi o .3(Y7 0 0 G9frc 048frl 3 rY?- 3 O.U'Snl 0.-M" % Solids L)7 1.0047 Average % d Solls 0 '5,/, RPD D Y) -'5 % Total Solids = Dry Solids Wgt —X 100 Wet Solids Wgt: SLUDGE fecal Collforms —*See Effluent Fecal Collform Setup for QA Data .9 d Q C9C)18 Collection Date .Time By Water Bath Setup < 8 hours after Grab .Read 24 +/- 2 hours Setup Removal Time in By Temp Time Out By Temp ivicu iuu. yccw Colony Count per Filter aiw z'jsc ea Calculate Colonies per 100 mUFilter Colonies per 100 mUFilter i emperatures % TOTAL SOLIDS are in -C .Reportable Colonies per g ml Used A 9 C D CID .,4_a_ 1F3�S �a2 2s b��,�, S o,01 �f S4U Wv '�o�Uoo i. ��s`�b��y �' : CFU 0.1 j .© 0S_ �� o �n3qtjS Oq� ! °? �rrr c 0.01 ! 1 jc�p aov � j000 �."t1 V a l� _q 1 � CFU 0.1 -�-}-1 ���� bq �` C715CD V S� 0.01 l �� t7 15j © �-� �S 12 t 1 CFU 4(-q.AY O. {� d � � 1 Q ,�, \� Cj Ito���! Cq 23 ��.5 a.D1 10 no 5-qS�-I �% 5, 14 cFu V� 14�460 CFU 0.1 —1 ! ' r Wv 0� 1� l �� Q�S ! 6Qc (�. ��' 0.01 c3 io3 �n � -� to ��3? CFU 0.1 o _ . DO'S �� 0.01 0.1 �27 ?j .7$� Z (ter Co CFu �1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WWTP Name: Lincolnton WWTP NPDES Number: Monitoring Period: From 07/01/18 To 09/30/2018 WQ Permit Number: WQ 0002712 NC 0025496 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlirnhle to nlfernntive nerfnrmerl WInvz A nr (Inca R) rmmnlete the fnllnwinv mnnitnrino rint5v Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6ch MPN MPN/g Coliform power per gram of total solids 4132 35770 227728 CFU/g 0 Quarterly Grab 9222D CFU SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Robert Pearson, Water Services Director P arer Name anc ' le ( type or print) Cl � Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 4132 3.62 Min 4132 55556 4.74 Max 227728 15873 4.20 Geometric Mean 35770 91,716 4.96 111548 5.05 227728 5.36 8826 3.95 Average 4.55 SLUDGE Fecal Conforms —See Effluent Fecal Coliform Setup for QA Data 2 rri -.9Df8 nnea� s• oe�en cne oe�., t e, a ti.. an Collection Date Time By Water Bath Setup < 8 hours after Grab Read 24 +/- 2 hours Setup Removal Time In By Temp Time Out By Temp Colony Count per Filter Calculate Colonies per 100 mL/Fiiter Colonies per 100 ml lFilter % TOTAL SOLIDS Reportable Colonies per g ml Used A S C D CID qq dos �� � 0.01 a o �1 ? , _�8 L,l-z CFU 0.1 f1 q i 1$ o(B30 , � S Or�gS' t� s o.01 1 Co ,�o aoo 1 too 0�0 . �. $ 55, 551a CFU . 0.1 Oq D5 �s C) 90 a �- 1 2-01 U � 3 a aov �n�Do° l . �1 � 57 CFU 0q0 / � 0.01 3j �lv,o�� 3to,0u� 3 g� J,71co CFU 0.1 ^, A 0.01 CFU ' 0.1 '�` (�!f 5 �ti2� �Z� �C► �`'G`(S 0.01�'v 1 t � CFU 0.1 TV C- Ic �`' �) ���`f, �f•S' b i.� 0.01 CFU 0.1 I,a`l o as / SLUDGE Fecal C®li$®rms ***See Effluent Fecal Coliform Setup for CA Data n cnngli t wi Temperatures are in °C Collection Date Time By Water Bath Setup < B hours after Grab Read 24 +1- 2 hours Setup Removal Time In By Temp Time Out By Temp Colony Count per Filter B Calculate Colonies per 100 mUFilter Colonies per 100 mL/Filter C % TOTAL SOLIDS D Reportable Colonies per •9 CID ml Used A 1 � CFU 0.01 � _ ' �� � 4 0� l�?�� �' Y CFU VS ry 0.01 CFU 0.01—v1 �(i 'j ` �V , , CFU 0.1 I • 0,01 CFU 0,1 0.01 CFU 0.1 0.01 CFU 0.1 Technician Quarter iYear SM 2540 Ca-19974 500 -1997 All weighings; are done in grams g, KV. Time Collected If �10 83 (D 0 1�05 0os %-It E- Date Collected Date I Time In SIC 6qSs/ �-[H&Gqpo/ Date/ Time Out /rl-qo.<l Total wet wgt )I-S,(0LRP (0i-26111 -,I?v? Dish qq40o LIQ3o7q q 1.2a2S—qq_ q43a7 Wet Sludge w9t Ro-W-a 2-0,,2 ;)-7Sato aQ.95(o0 12 7, (103-105°C) Dried Wgt c j.lL1 Lo 4(.v.G'7q3 L15,2SILI q5.oi?cj Dish tALLq(j 1194� q (P. ZVI q I q 43alLf L1j.--zo3 q4.2271� LAO, 1) 1 w -3c? 0 44-30251ttfnv Dry Solids wgt (P1 0.41iq O.-?qqq C). ?7� 09 (8'0 ().(460(o 6.4qi? % Solids t1r? Z, 2 Average % Solids N 0 ram- i RPD IM, qD 2 �P:571 Ll .0 % Total Solids = Dry Solids Wgt —X 100 Wet Solids Wgt Technician Ll�� qM 2W G-1 997, 2540 0 -1 S97 z Quarter./ Year All weighings are done in grams Z. R M 0Mr •I M I .-.1 :ru . , , g-gw .,09 M M� UApgz Time Collected 'Al Date Collected Date I Time In -7 Date Time AJ;Ls H� /I Out -11 Total wet Wgt to3 mv 19-GiC.35, low Dish Wet Sludge Wgt Scj-JLt!t S-Caq Ltq.,) uy 50.112r 53. t,t ft Dried Wgt am? Litt.1qV "trj.(jy2 :41J.57S7 Dish LkJoW 1-o -),CJ9S5--, 't'i qq - 17W t 1, ICFTI 4 L --7 tITZ,11co-014 Dry Solids w9t :�l K- C, -Lt-n2, C, % Solids '0 c> 0 Average % Solids Olt, 0 RPD 0A C4 D C-) % Total Solids = Dry Solids Wgt x 100 'Wet Solids Wgt Technician - w r�� SM 2540 8-2011, 2540 D-2011 NCO025496 WuUl LVI I ► Cal 2 W %Lp- ¢.t �Y All weighings are done in grams sl ��� Time Collected Date Collected M v c( -30— j r,( Date I Time In r} —3 -� c�• / �3 O /� 3 S/ pate/Time Out/103� Total Wet Wgt b r�• �. � � q �,1. t t � 0 • � � �' Dish �-��..� i �l `jL( �.0t4 Wet Sludge Wgt ��75 53 � ` • % l q q (103-105°C) Dried- Wgt ? �� i1 t �f Dish lo, • log � � • l � �� Dry Solids Wgt 0 • ? 0. Solids AVG % Solids' o 4 '� / j zt•(D Time In/Out (103-1 Wgt) DriedLk 1 5500C Wt �• : 3�32 �t3.3z� Volatile Solids Wgt , d'-� �Z d , ;��{� a .0 3 `� i Volatile Solids r1 �i� b•3 3` a AVG %'Volatiie.Solids 4 6 1 ' % TS DAF = �� % TS Sludge %VS DAF= % VS Slud e = . L % Total Solids = Dry solids Wgt 100 Wet Solids Wgt i.•`63 �..3-.. •`117�� � 6.12(1 % Volatile Solids = (Volatile Solids Wgt) X 100 Dried Solids Wgt % Reduction (VS DAF - VS Sludge) X 100 S VS DAF - (VS DAF)(VS Sludge) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WWTP WQ Permit Number: WQ 0002712 WWTP Name: Lincolnton WWTP NPDES Number: NC 0025496 Monitoring Period: From 10/01/18 To 12/31/18 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlirahln *n al*arna*ivo narfnrmr(1 WNeQ A nr (NQQ R) rmmnh+tn tha fnllnwina mnnitnrina data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61h MPN MPN/g Coliform power per gram of total solids 449 7214 84586 CFU/g 0 Quarterly Grab 9222D CFU SM 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Mt. 3 Option/Alt. 4 (VS reduction) X (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Mt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Robert Pearson, Water Services Director Prep r Name and T' ( type or print) Ignature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) FECAL DATA SHEET Lab result Log 758 2.88 Min 449 73469 4.87 Max 84586 84586 4.93 Geometric Mean 7214 39,169 4.59 982 2.99 449 2.65 12500 4.10 Average 3.86 SLUDGE Fecal Colifforrms ***See Effluent Fecal Coliform Setup for QA Data NA.tr —1- ag,)gn Gnn gist arl Temperatures are in °C Collection Date Time By Water Bath Setup < 8 hours after Grab Read 241-/- 2 hours Setup Removal Time In By Temp Time Out By Temp Colony Count per Filter Calculate Colonies per 100 mL/Filter Colonies per 100 mL/Filter % TOTAL SOLIDS Reportable Colonies per 9 ml Used A B C D CID `� _�� `�l ���� f-•S U��U;, dam. �lY..� �� 1� � � D.o1 0,01 0 �13.3 o CFU 0.1 og30 �s 1359 tt�(� 0.01 `5 i �� • p3J ``�OlOov de�S 1 7 (m `� CFU v 0.1 .J l 1 0.01 -7 �r�—� b0� � �•b�( �GY`5�1 0 CFU 0.1 0.01 0.1 -__ :13 _ 0 O6 ) U i � y t �]4 b CFU 0.01` 6OS l U� CFU 0.1 LT c% ��� 4� (a �t l�• ti:� � �� E` GL� o.o 1-I �. 6 1.0�1 tCFUI ---tm 0.1 I ( rq 7 0 ;t.S V t "',9v CFU 0.1 Z- Technician &� SM 2540 B-2011, 2540 D -2011 NCO025496 Quarter / Year All weighings are done in grams 410 i6ll"�8 .?.. Time Collected t S 5 5 15t r Ca L Date Collected � P � 1 b Date / Time In Date / Time Out Total Wet Wgt �6 6 ®� ctw Dish Li 1%0 2— Wet Sludge Wgt � � • � b � � , � � � � � ` • ��� � (103-105°C) Dried Wgt �('� �1 t c� 'A 3. S z� LA ('0 Dish Ltl • �-1 V1 c,i � S 2— L� LA • a-:� Dry Solids Wgt 3` i l . to `t`l a . Li % 3 % Solids 01� (3 Lt �l . `fib AVG % Solids 1 r ® a/v Time In/Out (103-1 Dried Wgt 5500C Wt LQ - Volatile Solids Wgt Volatile Solids 2q� AVG % Volatile Solids n ®/ ` a"O�1 G 0 % TS DAF = 1 -0 1' 7 /0 %TSSlud e= ���6 e`0 % VS DAF = 3. 17 % VS Sludge = % 'dotal Solids Dry Solids Wgt 00 Wet solids Wgt -�33 — ®�atS % Volatile Solids s (Volatile Solids Wgt) X 100 Dried Solids Wgt % Reduction _ (VS DAF - VS Sludge) X 100 LATI VS DAF - (VS DAF)(VS Sludge) ��® ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lincolnton WQ Permit Number: WQ 0002712 WWTP Name: Lincolnton WTP NPDES Number: NC 0085588 Monitoring Period: From 01/01/18 To 12/31/2018 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens i aUjlal L.q Vlc LV 0.Rc1 ll [l LlYc f1 G11V1 UIGLL ll..I..a L V.. Y) 111U1LQLc 1 I VLOJJ LV 01g11111L[111L1J' XXVUULV 14LILUgUllb Exempt from meeting Pathogen and Vector Attraction Reduction per Permit. Option/Alt. 5 Option/Alt. 6 (14-Day Aerobic) (Alk Stabilization) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) Option/Mt. 7 Option/Alt. 8 (Drying — Stable) (Drying — Unstable) No vector attraction reduction alternatives were performed "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Robert Pearson, Water Services Director Aignatu, arer Nam pae and Title ( typeor print) Land Applier Name and Title (if applicable) (type or print) e of Prerer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) SECTION 6 Agricultural Lime Application Log Year: 2018 Project: Lincolnton Field Soil Lime Requirement Tons/Acre Date Applied (state -county -site -field) ::][: pH (from soil analysis) Applied(CCE Eq.) CA-35-2A 7.6 O.OT/Ac. CA-35-213 5.9 1.OT/Ac. CA-35-2C 7.2 O.OT/Ac. CA-35-3A 7.2 O.OT/Ac. CA-35-313 7.2 O.OT/Ac. CL-05-03 5.6 0.7T/Ac CL-05-04 5.9 0.8T/ac C L-05-05 6.3 CL-05-07 5.4 O.OT/Ac. 1T/Ac 12/17/17 C L-05-08 6.4 CL-05-11 5.7 0.5T/Ac LT-1 9-1 6.1 LT-1 9-2 6.5 LT-1 9-3 6.4 LT-36-3 6.3 LT-36-4 6.2 LT-36-5 6.4 *Lime will be applied when conditions improve SECTION 7 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY1B-SL035642 Predictive Client: Sidney Turbyfill Advisor: E Bruce 4AD,Cl7LTrJ �2NU 4300 Biggerstaff Rd Synagro Soil Rep®rt Mehlich-3Extractlon Maiden, NC28650 284Boger Rd o — Mocksville, NC 27028 •� �.� Links to Helpful Information Sampled: 03/01/2018 U DED Sampled County: Catawba Received: 05/18/2018 Farm: CA-35 Completed: 05/23/2018 Client ID: 285863 Advisor ID: 475821 Sample ID: 35-2A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 40 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.22 0.97 21.4 100 0.0 7.6 159 48 90 9 47 906 537 241 241 183 0.3 1 Sample ID: 35-2C Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.88 15.4 99 0.2 7.2 104 98 87 9 46 282 168 197 197 173 0.2 1 `North Carolina Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035642 Sidney Turbyfill Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or'in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not M-O N mineral -organic soil class nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.html sfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowners Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume 0 o The first seven values [soil class, HM /o, W/V, CEC, BS /o, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar c7ov/apronomi/uvrst.htm Page 1 of 1 Report Number: 19-018-0753 Account Number:46488 Waypoint Send To: SYNAGRO CENTRAL LLC/SALISBURY ANALYTICAL Mary Brewer "Every acre... Every year. ",m 284 BOGER RD MOCKSVILLE NC 27028 Farm: CA-35 SOIL ANALYSIS REPORT Date Received: 01/18/2019 Date Of Analysis: 01/21/2019 Date Of Report: 01/21/2019 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Sid Turbyfill Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertility Index Value OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Soil Ibs/A M3 K M g Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g megl100g 35-2B 24953 4.7 131 32 M 235 VH 261 H 922 M 30 VL 5.9 6.77 1.6 9.1 I MIN M NC = 27 NC = 120 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K M9 Ca Na H NOs N S Zn Mn Fe Cu B SS % % % % 0% ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 35-2B 6.6 23.9 50.7 1.4 17.6 15 L 2.9 M . 50 H 148 VH 1.4 M 0.3 VIL NC=31 NC=72.5 NC=313 NC=70.0 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Date Received: 01/18/2019 Date Of Report: 01/21/2019 Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypointAnalytical Virginia, Inc. Salts ms/cm x 640 = ppm. SOIL FERTILITY RECOMMENDATIONS by: pap is or 60wr Pauric McGroary Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Iti/A Ib/A Ib/A Ib/A Ib/A 35-2B Adjust pH to 6.0 0 1.0 0 0 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FYIS-SL035626 Predictive Client: Sidney Turbyfill Advisor: E Bruce AG�CULTUI�o 4300 Biggerstaff Rd Synagro Soil Report Mehlich-3 Extraction Maiden, NC 28650 284 Boger Rd o Mocksville, NC 27028 6. a ) Sampled County: Catawba .� ,. Links to Helpful Information CNDED Xa Sampled: 05/17/2018 Received: 05118/2018 Farm: CA-35 Completed: 05/23/2018 Client ID: 285863 Advisor ID: 475821 Sample ID: 35-3A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, M 0.0 120-200 0 20 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 0.99 19.2 99 0.2 7.2 133 66 88 10 50 327 195 267 267 161 0.2 1 North Carolina \ d Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035626 Sidney Turbyfill Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field,,crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the sotil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.govlagronomilobpart4.htmfsfind information that P-I phosphorus index may help you choose a comparable alternate. For`more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routine) Zn-I zinc index available)] indicate levels of plant nutrients or'other fertility measurement. Visit www•ncapr.aov/apronomiluvrst.htm Page 1 of 1 Report Number: 19-023-0996 Account Number: 46488 Waypoint Send To: SYNAGRO CENTRAL LLC/SALISBURY ANALYTICAL Mary Brewer "Every acre... Every year. "TM 284 BOGER RD MOCKSVILLE NC 27028 Farm: CA-35 SOIL ANALYSIS REPORT Date Received: 01/24/2019 Date Of Analysis: 01/25/2019 Date Of Report: 01/25/2019 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Sid Turbyfall Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NC = North Carolina Fertilitv Index Value OM wN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Soil IbslA M3 K M g Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate p H Index me 1100 q g me /100 q g 35-313 02711 8.3 150 212 VH 62 VL 179 L 3329 VH 24 VL 7.2 0.0 18.4 MIN VH NC = 177 NC = 32 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Sample ID Field ID K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 35-313 0.9 8.1 90.5 0.6 0.0 9 VL 9.2 VH 59 VH 65 VH 2.7 H 1.0 M NC=19 NC=230.0 NC=369 NC=135.0 Values on this report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Date Received: 01/24/2019 Date Of Report: 01/25/2019 Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: payria OF Gr (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalytical Virginia, Inc. SOIL FERTILITY RECOMMENDATIONS Pauric McGroary Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 35-3B Adjust pH to 6.0 0 0.0 0 0 0 1 � 7 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035643 G�GVLTV Predictive Client: Leon Leonhardt Advisor: E Bruce 3730 Fallston-Waco Rd Synagro Soil Report Mehlich-3 Extraction Lawndale, NC 28090 284 Boger Rd Mocksville, NC 27028 UWD �I��.Links to Helpful Information Sampled: 04/20/2018 Sampled County: Cleveland Received: 05/18/2018 Farm: CL-05 Completed: 05/23/2018 Client ID: 234620 Advisor ID: 475821 Sample ID: 05-03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.7 120-200 50 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cO; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.90 7.2 75 1.8 5.6 38 111 44 24 119 180 125 109 109 50 0.2 3 North Carolina Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035643 Leon Leonhardt Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed, and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-A11 Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not M-O N mineral -organic soil class nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.hnd information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Ian-AI2, Zn-I, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine[ Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/aaronomi/uvrst.htm Page 1 of 1 Report Number: 19-018-0751 ' Account Number:46488 Waypoint Send To: SYNAGRO CENTRAL LLC/SALISBURY ANALYTICAL Mary Brewer "Every acre... Every year. "TM 284 BOGER RD MOCKSVILLE NC 27028 Farm: CL-05 SOIL ANALYSIS REPORT Date Received: 01/18/2019 Date Of Analysis: 01/21/2019 Date Of Report: 01/21/2019 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalyticdl.com Grower: Leon Leonardt Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH NO = North Carolina Fertilitv Inriex Value OM w/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Field ID Lab Number ova Rate Soil Class lbs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate M g ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meq/100g meq/100g 05-04 24951 4.5 130 72 H 285 VH 197 H 708 L 21 VL 5.9 6.81 1.2 7.2 I MIN M NO = 60 NC = 146 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 05-04 10.1 22.8 49.2 1.3 16.7 28 H 3.1 M 19 M 151 VH 1.2 M 0.3 VL NC=58 NC=77.5 NC=119 NC=60.0 values on tins report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Date Received: 01/18/2019 Date Of Report: 01/21/2019 Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �Qyria (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalytical Virginia, Inc. (/ SOIL FERTILITY RECOMMENDATIONS Pauric McGroary Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 05-04 Adjust pH to 6.0 0 0.8 0 2 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, conceming crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL037941 Predictive Client: Leon Leonhardt Advisor: E Bruce �AG�UULTUllFµo 3730 Fallston-Waco Rd Synagro Soil Report Mehlich-3 Extraction Lawndale, NC 28090 284 Boger Rd o fi Mocksville, NC 27028 Links to Helpful Information Sampled: 06/13/2018 ED Sampled County :Cleveland Received: 06/28/2018 Farm: CL-05 Completed: 07/09/2018 Client ID: 234620 Advisor ID: 475821 Sample ID: 05-05 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 40 60 0 0 0 0 0 0 Note: 12 1.00 tons/acre; 12/2017 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na. ESP SS-1 NO3-N 0.46 1.07 8.1 89 0.9 6.3 42 39 56 30 40 83 62 104 104 50 0.2 2 Sample ID: 05-07 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 0 0 0 0 Note: 12 1.50 tons/acre; 12/2017 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC /BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.17 5.8 72 1.6 5.4 122 24 44 25 46 73 61 143 143 107 0.1 2 Sample ID: 05-08 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cn73; CEC and Na in meq/100 crn3; NO3-N in mgldrrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.05 11.5 91 1.0 6.4 293 135 56 30 46 163 109 458 458 130 0.2 2 -North Carolina e: Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Leon Leonhardt Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat( is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for freld crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.pov/acrronomi/obpart4.htmtltsfind information that may help you choose a comparable alternate. For more information, read A Homeowners Guide to Fertilize] Test Results The first seven values [soil class, HM%, W/V, CEC, BS%a, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-Al I, Mn-AI2, Zn-I, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine[ available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagr.gov/agronomi/uvrst.htm ;} Report No. FY18-SL037941 Page 2 of 2 Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-I potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035628 LTU(jE�O Predictive Client: Leon Leonhardt Advisor: E Bruce i PG,V w2° cO2"G 3730 Fallston-Waco Rd Synagro F Soil Report Mehlich-3 Extraction Lawndale, NC 28090 284 Boger Rd o — S Mocksville, NC 27028 ' Sampled County: Cleveland •� �.�� Links to Helpful Information UNDED \� Sampled: 04/15/2018 Received: 05/18/2018 Farm: CL-05 Completed: 05123/2018 Client ID: 234620 Advisor ID: 475821 Sample ID: 05-11 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.5 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.13 5.9 76 1.4 5.7 80 64 49 22 40 109 82 66 66 47 0.2 3 North Carolina Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035628 Leon Leonhardt Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE Ca%o % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is, needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM%o percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-AH Mn-availability index for crop 1Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients: Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit www3ncagr.govlagronomilobpart4.htmVlfsfind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-Al 1, Mn-Al2, Zn-[, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit v ww.ncagr.aov/aaronomiluyrst.htm NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035630 Predictive Client: Chuck Waters Advisor: E Bruce 4PG�CULTU/��o 3529 Killian Road Synagro F Soil Report Mehlich-3 Extraction Lincolnton, NC 28092 284 Boger Rd o Mocksville, NC 27028 Links to Helpful Information Sampled: 05/17/2018 Sampled County :Lincoln Received: 05/18/2018 Farm: LT-19,CA-17 Completed: 05/23/2018 Client ID: 409870 Advisor ID: 475821 Sample ID: 17-07 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 50 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/do]: Soil Class: Mineral' HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.27 0.94 24.1 100 0.0 7.5 97 47 93 6 70 419 245 522 522 346 0.2 1 Sample ID: 17-08 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 30 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units -W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.27 1.02 18.4 100 0.0 7.4 65 57 90 9 46 1315 785 319 319 256 0.2 1 Sample ID: 19-01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/do]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.00 9.9 85 1.5 6.1 117 4Q 58 25 50 577 361 346 346 217 0.2 2 North Carolina , Z Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035630 Chuck Waters Page 2 of 3 Sample ID: 19-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.0 120-200 0 70 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cm3; CEC and Na in meq/100 cnr3; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-1 Na ESP SS-1 NO3-N 0.51 1.02 10.0 87 1.3 6.5 123 34 57 29 48 962 587 347 347 265 0.2 2 Sample ID: 19-03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 40 80 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.51 0.98 8.8 88 1.1 6.4 42 31 56 30 44 532 330 113 113 181 0.2 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL035630 Chuck Waters Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.pov/agronomi/obpart4.htmsfind information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.00v/aoronomi/uvrst.htm Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-1 copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-AI1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index WN weight per volume Zn-AI zinc availability index Zn-I zinc index Page 1 of 2 Report Number: 18-348-0676 Account Number: 46431 Send To: Synagro Central LLC Marshal Puryear 284 Boger Rd Mocksville NC 27028 D Waypoint.( ANALYTICAL "Every acre... Every year. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.way p o i n t a n a l ytica I. c o m Grower: Jeff Lingerfelt LT-36 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH Date Received: 12/14/2018 Date Of Analysis: 12/17/2018 Date Of Report: 12/19/2018 NC = North Carolina Fertility Index Value Sample ID Field ID Lab Number OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 %Soil Rate Class Ibs/A M3 ppm Rate ppm Rate ppm Rate K ppm Rate M 9 ppm Rate Ca ppm Rate Na ppm Rate Soil PH Buffer Index H meq/100g meq/100g 03 07410 3.7 114 138 VH 61 L 166 H 863 M 27 VL 6.3 0.7 6.7 MIN M NC=115 NC=31 04 07411 3.4 103 157 VH 90 L 354 VH 1190 M 33 VL 6.2 1.3 10.6 MIN M NC =131 NC = 46 05 07412 4.3 125 141 VH 66 L 193 H 955 M 34 VL 6.4 0.7 7.4 MIN M NC=117 NC=34 Sample ID Field ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts K Mg Ca Na H NO, N S Zn Mn Fe Cu B SS % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate 03 2.3 20.6 64.4 1.8 10.4 14 L 7.4 H 15 M 173 VH 2.2 H 0.7 M NC=29 NC=185.0 NC=94 NC=110.0 04 2.2 27.8 56.1 1.4 12.3 22 M 18.5 VH 98 VH 128 VH 4.8 VH 0.7 M NC=46 NC=462.5 NC=613 NC=240.0 05 2.3 21.7 64.5 1 2.0 9.5 12 L 7.7 H 15 M 174 VH 2.0 H 0.7 M NC=25 NC=192.5 NC=94 NC=100.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. m� G� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypointAnalyfical Virginia, Inc. Pauric McGroary Page 2 of 2 Report Number: 18-348-0676 Account Number:46431 Send To: Synagro Central LLC Marshal Puryear 284 Boger Rd Mocksville NC 27028 Date Received: 12/14/2018 Date Of Report: 12/19/2018 • Waypoint. ANALYTICAL "Every acre... Every year "Tm SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Grower: Jeff Lingerfelt LT-36 Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P206 K20 Mg S Zn Mn Fe Cu B Field ID bu Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 03 Wheat 65 0.0 79 25 84 0 15 0 2 0 0 0.5 04 Wheat 65 0.0 80 0 79 0 6 0 0 0 0 0.5 05 Wheat 65 0.0 767 25 81 0 17 0 2 0 0 0.5 Comments: Sample(s) : 04,05 Crop: Wheat Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. Boron recommendations are on a broadcast basis. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." pM� Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary