WQ0006245_Regional Office Historical File Pre 2018 (11)

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February 18, 2016
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service -Center
Raleigh, North Carolina 27699-1636
RE: Annual Reports for 2015
Alkaline Stabilization (WQ0006245)
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FEB 11 2016
OWR SECTION
YNA ORMATJON PROCESSING UNIT
RECEIVED/NCDENR/DWR
FEB. 2 2 2016
WOROS
MOORESVILLE REGIONAL OFFICE
Dear Mr. Hardee:
Enclosed, you will find 1 original and 2 copies of the required forms and lab data for the Alkaline
Stabilization program. Permit # WQ0006245.
This permit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
felAndi
WWupervisor, Fourth Creek WWTP

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2015
PERMIT NO. WQ0006245 .
FACILITY NAME: Fourth Creek WWTP NPDES NC0031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: L.F. "Joe" Hudson Jr., Director
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Andy Smith
Plant Supervisor . -
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

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of
4•tatjesutflt
I rx 1111 9 i*tateaufflc. Nort# &rvtina 2868
February 18, 2016
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Reports for 2015
Third Creek Monofil (WQ0004040)
Dear Mr. Hardee:
Enclosed, you will find 1 original and 2 copies of the required forms and lab data for the Third
Creek Monofil. Permit # WQ0004040. This monofil is currently closed and not being used for bio-solids
disposal.
This permit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
n y,
Andy Smith
WW P Supervisor, Fourth Creek WWTP

GENERAL INFORMATION
BIOSOLIDS REPORT
CALENDER YEAR 2015
THIRD 'CREEK MONOFILL
PERMIT NO. WQ0004040
FACILITY NAME:
Third Creek WWTP-NPDES NCO020591
LOCATION:
444 Third Creek Road
MAILING ADDRESS:
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL:
L. F. "Joe" Hudson, Jr., Director
Water Resources
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR:
Scott Austin
Plant Supervisor -
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC
Andy Smith
Residuals Supervisor
P.O.Box IIII
Statesville, NC 28687-1111
[phone]
APPLICATION:
Surface disposal unit.
This unit was not used for biosolids
disposal in 2015, and has completed
closure activities. The permit is
maintained for well sampling and
reporting.

Management Practices Description
Third Creek WWTP Sludge Monofill (Surface Disposal Unit)
NPDES No. NCO020591
40 CFR 503.24
Non -Discharge Permit WQ0004040
THREATENED OR ENDANGERED SPECIES: No known threatened or endangered species
occupy or frequent the disposal site.
BASE FLOOD FLOW RESTRICTION: The site is located above the flood plain.
LOCATION OF GEOLOGICAL STABLE AREA: Soil consists of tight red clay on high ground
and the site has had no history of movement or shifting due to saturation with rainwater or
seismic conditions. No known faults exist in the area.
WETLANDS LOCATION: Not a wetland location.
RUNOFF COLLECTION: Trenches are constructed as to prevent disposed material from exiting
as a part of any runoff. Berming and swales are constructed to contain erosion. Finished trenches
are domed with clean earth to allow shedding of water out and away from filled trenches. A
"green belt" is maintained and encouraged to grow around the entire area.
LEACHATE COLLECTION: As a liner is not used, leachate collection is not required.
METHANE GAS MEASUREMENTS: Periodic checks of air with electronic air monitors reveal
that methane is not escaping the surface disposal area.
CROP PROHIBITION: Crops are not grown on the site.
GRAZING PROHIBITION: Grazing is not permitted on the site. -
PUBLIC ACCESS RESTRICTED: Chain link fencing encloses the site property. NO
TRESPASSING signs are posted.
AQUIFER CONTAMINATION: Monitoring well samples for this calendar year show no danger
of aquifer contamination.
No disposal activities occurred in 2015.

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0004040
Facility Name: Third Creek WWTP Monofill
Residual Source WQ # or NCO020591
NPDES #:
WWTP Name:
Laboratory: 1) Prism Labs
2)
3)
4).
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
12/21/15
:{
Percent Solids (%)
NA
17.4
Arsenic
75
<0.050
Cadmium
85
<0.025
Copper
4,300
Chromium
NA
<0.25
Lead
840
<0.050
Mercury
57
<0.010
Molybdenum
75
Nickel
420
No
Residuah
disposed
of in
pennitted
Selenium
100
<0.10
unit
2015
Zinc
7,500
Total Phosphorus
NA
TKN
NA
Ammonia -Nitrogen
NA
Nitrate and Nitrite
NA
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under -penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
1pealt s for subm�tt' g false information, including the possibility of fines and imprisonment for knowing violations."
Signatu a of Preparer * Date
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0006245 FACILITY NAME: Fourth Creek Alkaline Stabilization '
PHONE: [phone] COUNTY: Iredell OPERATOR: Ray Wyrick ?-
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B,:and C)
Was the facilitv in operation durine the oast calendar vear? Yes 0 No ❑ --► If No skip carts A. B. C and certifv form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
.--
Volume (dry tons)
Intended use(s)
January
4th Creek WWTP
13
102
115
Various Farmers
120
Farmland
February
NPDES# NCO031836
17
88
105
Various Farmers
0
Personal & Farm
March
4th Creek WWTP
23
350
373
Various Farmers
491
Farmland
April
NPDES# NCO031836
15
148
1.63
Various Farmers
141
Farmland
May
4th Creek WWTP
13
74
87
Various Farmers
11
Turf
June
NPDES# NCO031836
9
92
101
Various Farmers
0
Farm/Garden
July
4th Creek WWTP
17
73
90
Various Farmers-
122
Farmland
August
NPDES# NCO031836
10
- . 75
85
Various Farmers
0
Farmland
September
4th Creek WWTP
0
0
0
Various Farmers
0
Landscaping
October
NPDES# NCO031836
0
0
0
Various Farmers
358
Farmland
November
4th Creek WWTP
0
0
0
Various Farmers
0
Farmland
December
NPDES# NCO031836
0
0
0
Various Farmers
0
Farmland
Total from FORM DMSDF (sup)
_ Q-
0...
i
0
...................
Totals:
Annual (d tons):
` 117.
1002
1119 '
1243 ;
...................
Amendments used- Bulking Agent(s) used: Lime Kiln Dust
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No No If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, laccurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisgnmej for knowing violations."
//II �� �� . 1n
• ignature of Permittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature tf Preparer**
(if differght from Permittee)
Date

A
AT
I: lqk:�'ttlj of
M. 1x 1111 0 —*tattsville,Xvrt4 Tarefina28687
4th CREEK& 3rd CREEK WWTP'SLUDGE NARRATIVE
Andy Smith
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered
using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process
area where the biosolids are set aside for contract land application off of the plant site. The contractor is
Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids disposal is the N-
Viro process and that permit # is WQ0006245.

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: q•, 7- 16
Removal From Bin Date: 5_=V.-%4
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH' 63
Start Time/Date/Temp
70'
CL�
Corrected pH: 17
_ Acj;
�j
Final pH: jL?
'
End Time / Date / Temp
v
7S
(, S
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
BIN # _.
Setup Date: y^2&- /6
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg..0 For 12 Hrs.
Operator
: d
Initial pH:
Start Time/Date/Temp
e — z
Lt✓�
Corrected pH: / ,a
Final pH:
End.Time/Date/ Temp
72 G
Corrected pH:
Has 12 Hour Temp Criteria Been Met? (Y) N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date: 57-,3 --/6
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
p
Initial pH: 0. fl
Start Time/Date/Temp
v
�
/ !
Corrected pH: J�...�5'
'
Final pH: 1 rah
End Time/Date/Temp
701,
P (j
Corrected pH: /� ,
Has 12 Hour Temp Criteria Been Met? N
72 Hour pH Criteria Been Met? N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
­>294
Initial pH: IRJP
StartTime/Date/Temp
IrYo
Corrected pH: la,3 7
';
Final pH: la a
/
End Time/Date/Temp
`7 °
1
15
Corrected pH: ,
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? v1 N
BIN.#s ;, .-...,,. ,....
Setup.Date:, �-./,-., ;,. _
IZemoval:From..BinDate:
Date -'
-`Time-
~Operator
-d-&
o M
Initial pH:
,,�
Start Time/Date/Temp
Corrected pH:
,3(�
Final pH: G
End Time/Date/Temp
7
Corrected pH- 02�QS
Has 12 Hour Temp Criteria Been Met? Y. N.
Has 72 Hourp Criteria Been- Met?- N -

City/ Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: (4 - -7-14
Removal From Bin Date: y-11-14
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
+7-16
Initial
10: 304
pH .?o
Start Time/Date/Temp
Corrected pH: )3.0)-
y-11 jla
j :0Q A
Final pH:
End Time/Date/Temp
73 °
i�LW
Corrected pH: )07.aa
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? N
BIN # r]
Setup Date: 'I-7-lb
Removal From Bin Date: y- //-16
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10 : 30;t
Initial pH: .)
Start Time/Date/Temp
171 ©
L
Corrected pH: 1,
i . ,1
:0D k
Final pH: 112, 1
End Time/Date/Temp
0
6.5
Corrected pH: j�, ,3
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10',10A
Initial pH: 1 ,Q
Start Time/Date/Temp
6
Ri LO
Corrected pH: j
07JJA
Final pH: l j 7
+
End Time / Date / Temp
V0
1' LLB'
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? ... N.
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Y4,94
O `; 0 fi-
Initial pH: j ,a
Start rime IDate JTemp
0
Corrected pH:
Li-1 lt
I: q8p
Final pH: ja, 1 1
End Time/Date/Temp
ICorrectedpH: 12,0q
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
Setup Date:
Removal From Bin -Date:
Date
Time
pH:>12'.0'For'72 Hrs. "
TEMP: >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Start Time/Date/Temp
L
Corrected pH: I
1(9
C%: 0(a iti
Final pH: 01163
End Time/Date/Temp
612
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72.Hour pH. Criteria. Been M6t?

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 7
Setup Date: k-10.16
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
A6IW A
Initial pH: /12.,r`6
Start Time/Date/Temp
— 0
A LA-0
Corrected pH: p
�'-/.S'l6' 1
` "2UL¢
Final pH: U
End Time / Date / Temp
%
I
Corrected pH: 12,71
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
BIN # - , '
Setup Date:
Removal From Bin Date: -/ ,14
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
'Co in
Initial pH: /a, j /
Start Time/Date/Temp
Corrected pH: /a:%D
ff /�
7.`-V/1-
Final pH: •(oa
End Time/Date/Temp
d
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? (JY N
BIN #
Setup Date: e-J 74
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�s -f
, 00
Initial pH:
StartTime/Date/Temp
l'
Corrected pH: 1,2, `7o
; ODk
Final pH:
End Time/Date/Temp
lCorrected pH: / a .
Has 12 Hour Temp Criteria Been Met? N
p Has -72 Hour H Criteria Been Met?: ., Y N_
BIN # j
Setup Date: /-7- 14
Removal From Bin Date: •f
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
rf /%/�
F-' J( "'
Initial pH: J /
r Start Time/Date/Temp
J
PLO
Corrected. pH: /'� •%D
i3'/�
%Q•Gb
pH: / f
End Time/Date/Temp
Y7
0al
rrected pH: /TY/
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
Setup. Date:.....�fc,�,._., ,...;,......;
Removal -From Bin. Date- . .-
"Date
' Thyme% '
. _.;..- pH `>12:fl F-or 72'Hrs `"` -
-`TEMP:: 5SZDeg:'Cfor'12,Hrs:`
=Operator
Initial pH: I
Start Time/Date/Temp
�
� pp
W
Corrected pH: _ ('
II
041Q4�
A
Final pH: �a,
End Time/Date/Temp
/
t
1.
Corrected pH: ra • % I
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour -ply Criterla.:Been� Met . ,, y. ,,.,.,N...

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: ,,;) f -/4
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: 13V
Start Time/Date/Temp
c
R uaJ
Corrected pH:
Final pH:
End Time/Date/Temp
� �
LLI)
Corrected pH: 0,33
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
BIN # . �7
Setup Date: 5%,;iq-14
Removal From Bin Date: _5-,,? j'. /L
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: L2,03Start
Time/Date/Temp
/
C-(,j
Corrected pH:
_27./
�;(;�
Final pH:
End Time / Date / Temp
ev _
PL�
Corrected pH:
Has 12 Hour Temp Criteria Been Whet? N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date: - '�yl �-
Removal From Bin Date: -, y -/4
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH' 1. 70
Start Time/Date/Temp
O
` �
Corrected pH:
;45-/t'
Final pH:
End Time / Date / Temp
%�
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
RIIU"it i
Cptnn Dntp: -7 /y //
lRemoval From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
. T-C
Initial pH: I I , ]�
Start Time/Date/Temp
R �.�
Corrected pH:
,) ( ./G
JJOP lCorrected
Final pH: /
End
y Time
6 Ll.r✓
pH: /
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
J
Setup'Date:- " "' f �� /
Removal From Bin Date: / -
Date
Time
pH >12'ffFor 72 Hrs:
TEMP: >52 Deg. C For 12 Hrs.'
Operator.
Sop
Initial pH: 60
StartTime/Date/Temp
9
L
Corrected pH: ( 3,9
a • 16
Final pH:
End Time/Date/Temp
On
71 z�
A LG
Corrected pH:
Has 12 Hour Temp Criteria Been Met? Y IV
- Has 7°2 our H Cri eria- Been:Mi t? " Y -..:;N
P

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACEDISPOSAL CERTIFICATION.AND SUMli ARY..FORM-:.
WQ PERMIT #: WQ0006245 FACILITY NAME: Fourth Creek Alkaline Stabilization
PHONE: [phone] COUNTY: Iredell OPERATOR: Ray Wyrick
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
R1 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in oneration during the east calendar vear? Yes R1 No ❑ ----► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
4th Creek WWTP
0
0
0
Various Farmers
0
Farmland
February
NPDES# NCO031836
0
0
0
Various Farmers
0
Personal &Farm
March
4th Creek WWTP
0
0
0
Various Farmers
0
Farmland
April
NPDES# NCO031836
59.73
82.5
139.24
Various Farmers
129.6
Farmland
May
4th Creek WWTP
238.92
330
556.97
Various Farmers
346.8
Turf
June
NPDES# NCO031836
10.86
12
22.32
Various Farmers
442
Farm/Garden
July
4th Creek WWTP
16.29
22.5
37.98
Various Farmers
27.2
Farmland
August
NPDES# NCO031836
38.01
52.5
88.61
Various Farmers
64.6
Farmland
September
4th Creek WWTP
86.88
112.5
195.04
Various Farmers
139.46
Landscaping
October
NPDES# NCO031836
0
0
0
Various Farmers
136
Farmland
November
4th Creek WWTP
135.75
187.5
316.46
Various Farmers
178.5
Farmland
December
NPDES# NCO031836
54.3
75
126.59
Various Farmers
166.6
Farmland
Total from FORM DMSDF (sup)
0
0
0
1
0
........... I........
Totals:
Annual (dry tons):
640.74
874.5
1483.21
1630.76
Amendment(s) used: Bulking Agent(s) used: Lime Kiln Dust
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and impriongrpnt for knowing vigations."
;Z41� •? /G 1 %
Signature of Permittee Date
(if d
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
of Preparer**
it from Permittee)
AD

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name .Third Creek WWTP Monofill, WQ Permit Number: WQ0004040
WWTP Name Third Creek WWTP. NPDES Number: NC0020591 `
Monitoring Period: From: 1/1/2015 To 12/31/2015
D.,+l,. --- 7?nrin m+;nn rdn VVP 463_321 _ Please indicate level achieved and alternative. performed:
1 [1 L11V�r11 1�.+a�uvuav�a
Class A:
•v. �.� �� -. ..�.��� - _-__-_
Alternative 113
_— --- _
Alternative 2 ❑
-
Alternative 3 ❑
"
Alternative 4' El
Alternative 5 ❑
Alternative 6 ❑
......................
If applicable to alternative .performed (Class A only) indicate "Process to Further Reduce Pathogens":
..........
Compost ❑
Heat -Drying ❑
Heat Treatment ❑
Thermo hilic ❑
::.:.:::.:.:.:.:.:.:.:
Beta Ray ❑
By
Ray0
ati
Pasteurization ❑
as
P
Class B:
' e
Ahernativ 1 ❑
e2
A rn ati ❑
lte
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying[] Composting E3 I Aerobic Digestion ❑
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Allowable Level Pathogen Density
Excee- Number o Frequency Sample AnaTech-
Parameter
in Sludge inimu Geo. Mean MaximumUnits
of Analysis Type,
dences yp ru ue
2 x 10 to the MPN
.6th power
per gram of
CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry No Residuals disposed
of in
permitted
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
unit
@
2015
coliform)
weight)
Vpptnr Attraetinn Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. Oz uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable)
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)-
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement. attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Name andcTitlp (type or print)
Land Applier Name and Title (if applicable)(type or print)
3ignatur of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

AT-
ttij 1
4th CREEK & 3rd CREEK WWTP SLUDGE NARRATIVE
Andy Smith
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester, and dewatered
using a belt press. After dewatering, the residuals are transferred to the N-Viro lime stabilization process
area where the biosolids are set aside for contract land application off of the plant site. The contractor is
Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids disposal is the N-
Viro process and that permit # is WQ0006245.

KI
City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 8
Setup Date: J-.a$-15
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1.?. 9 7
o
0
RIM
Corrected PH: 13. 1
Final PH: jl.,7h
Corrected PH: 13.
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 'I
Setup Date: d - 3 - / S.
Removal From Bin Date:,- 4e- /5
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1,5
p
12 : H o "'
Initial PH: 1 2. 7'J
706
Corrected PH: /,) . qy
5
9! yo,�
Final PH: /i., FIV ::4
0
121.
Corrected PH: / 3. O
Has 72 Hour & PH Criteria Been Met? Y FN
BIN # 1
Setup Date:
Removal From Bin Date: 2-7-15
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
`�. y_ } �-
p
U. y n""'
Initial PH: /.Z;75.
o
90
RAC w
Corrected PH: 12. 96"
-7_15
A
09:33�.,
Final PH: frS
900.R�.w
Corrected PH: /3.0
Has 72 Hour & PH Criteria Been Met? Y N
BIN #-_. $
Setup Date: 3- a-_1-5
Removal From Bin Date: 3- 5 -15. - -
Date
Time.,,.
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-.t-15
1 PM
Initial PH: i2.1 o
9 00
Rz W
Corrected PH: 12.9
PM
Final PH: j
`1 ®
RJ, vw
Corrected PH: 13, 0,1
Has 72 Hour & PH Criteria Been Met? (Y) N
BIN # `7
Setup Date:,3-3 - /S
Removal From Bin Date: 3 - 6-- /S
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3_3.-1:5.. ,
04; 35
Initial PH: 12. S5
"�i� °:
/11,-w
Corrected PH: /3.02
.
3- �- l3
/a a,o�
Final PH: /2.q 3
0 o
R�Mr
Corrected PH: 13.1
Has 72 Hour &. PH Criteria Been Met? UY
N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
.BIN # $
Setup Date: 1-
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
►_ S- 1�
10� 47
Initial PH: la, 73
©
®`
RI•Vi
Corrected PH:-12.g3
o4' S6
Final PH: U. S3
cm 0
R A, W
Corrected PH: 13, 0
Has 72 Hour & PH Criteria Been Met? Y N
BIN # ,�
Setup Date: /- 13-1
Removal From Bin Date: 1.5
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
A"'
Initial PH: 12. g O
O o
Rk
Corrected PH: /,', Q 9
Final PH: /;J, 10
Goo
o
Corrected PH: 13,1
Has 72 Hour & PH Criteria Been Met? Y N
BIN # •3
Setup Date: /-�0-15
Removal From Bin Date: /-.13-15
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: I . 7-5
Corrected PH: 1,2, 95
I-1F-IS
1.2ioaPM
Final PH: / �. �
q ®�
( kVV
Corrected PH: 13 ,0
Has 72 Hour & PH Criteria Been Met? TY� N
BIN # Y
Setup Date: /-A1-15
Removal From Bin Date: /-did-15
Date
Time
PH >12.0 For 72 Hrs.;,,
TEMP. >52 Deg. C For 12 Hrs.
Operator
I 0 m �*a
Initial PH: 19. 7S
900
RAW
Corrected PH: 14 ,q.5
�_ 1
1- .
/X 4 3 Prn
Final PH: /.2, kS
Corrected PH: 13.0
Q 0
R kv r
Has 72 Hour & PH Criteria Been Met? V N
BIN## S
Setup Date: /-,2C- IS
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
i-1 is
ld Ara
Initial PIS: 14. ?d�
o
®_ ...
�:..
Corrected PH: .13. 1
Final PH: III
� d a
l
Corrected PH: 13.1
Has 72 Hour & PH Criteria Been Met? UY N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # y
Setup Date: 3-17-15
Removal From Bin Date: 3-ao-►5
.
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-17- 13
/1 a0�rn
Initial PH: /a,YS
0
9d
R�(W
Corrected PH: l.Z, 65
q
08•"So"%
Final PH:7a, ss
Corrected PH: /.2.73
Has 72 Hour & PH Criteria Been Met? Y N
BIN # bl
Setup Date: 3 .Z3- /S
Removal From Bin Date: 3-.71- /5
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3- ;3- /5
1:3o P
Initial PH:
0 d
Corrected PH: /Z
3-3o-)
Is-,ao lCorrected
Final PH:
lJ
PH: j
Has 72 Hour & PH Criteria Been Met? Y 7N
BIN # 7
Setup Date: 3- aq- IS
Removal From Bin Date: 3- 2 7-
IS
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
A
S4 tn
Initial PH: .I,d • �(y
R k W
Corrected PH-
- a•�v
Final PH:
0
%�i
/
CC am"
Corrected PH:
Has 72 Hour & PH Criteria Been Met? rYTN
BI_N_#_
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

l
�-
City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
.BIN
#
Setup Date: Ll - 2 /, Ij
Removal From Bin Date: 4/-,;l �{_ /
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
14- - is-
14 Icy
Initial PH: )a., 4S
Corrected PH:
L�
Final PH: , $ S-
Corrected PH: a , 7 S '
Has 72 Hour & PH Criteria Been Met? N
BIN #
Setup Date: [� a _ ) r
Removal From Bin Date: /S
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1,2,'7f
5
Corrected PH: 1",,
.2 jf-►�
�jg; p(j
Final PH: I ,L ,, S
Corrected PH: 3, U
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: y-2y /y
Removal From Bin Date: /_ IS -
_-
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
13'
Initial PH: /2. q
°
Corrected PH: ,:
Final PH:
6O
Corrected PH: ij. 5
Has 72 Hour & PH Criteria Been Met.? Y N
BIN #_ _ l
Setup Date:_ .5'-9
Removal From Bin Date:
_.
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Od
Initial PH: y.!;,
o
0
Corrected PH:
Final PH: 1�
o
'
Corrected PH: 1
Has 72 Hour. & PH Criteria Been Met? Y N
RIN # Z
ISetur)Date: S =,rf-t F'
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
�d
//-fY-
Final PH:
l%
I Corrected PH: l a.c 7S`
Has 72 Hour & PH Criteria Been Met? 'N

City Of Statesville Alkaline Stabilization Record For .
Process To Further Reduce Pathogens (PFRP)
BIN #
SetupDate: 5.15, .�>
Removal From Bin Date: S = fig-Jj
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
FDa:te::F
Initial
PH:Corrected
PH:
d
+
Final PH:
b
D
�.✓'
Corrected PH: J 3, C�
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH :>12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
'15
f cf 30
Initial PH:
Corrected PH: t 2 •�%
-0/5
1 S'oo
Final PH: �r
n �
�y
Corrected PH: �
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 7- . 1
Removal From Bin Date: %- $ -
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12. Hrs.
Operator
Initial PH: Ja_ ff
a.
Id
e A
CJ+'
Corrected PH: 13: I:
(A2
i-IT
Final PH: 1�2rQ
ID �
Corrected PH: ,
Has 72 Hour & PH Criteria, Been Met? Y N
BIN-#_
Setup Date:
Removal From Bin Date:
Date
Time
=PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs,
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C.For 12 Hrs.
Operator
Initial PH:
Corrected PIS:
Final PH:
Corrected PH:
Has .72 Hour & PH Criteria Been Met? Y N

City Of. Statesville Alkaline Stabilization Record For .
Process To Further Reduce. Pathogens (PFRP)
.BIN # 1
Setup Date: g-
Removal From Bin Date: S- lo- 15
Date
Time.
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For. 12 Hrs.
Operator
`" 15
1 o Am
Initial. PH:' 1?. 87
CT o .0 __...
Ric w
Corrected PH: 13,1
('
Final PH: ►j.q 8
0
Corrected PH: 13. ,a .
' Has 72 Hour & PH Criteria Been Met? Y N
BIN # 6' Setup Date: $-9-15 Removal From Bin Date: 6-11-15
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs..
Operator
V-7 15
12NO
Initial PH: /a, 7'/
90
Corrected PH: /4.9Y
9 •'t 0,,,
Final PH: ,
Q 0
R�
Corrected PH: /3, p
Has 72 Hour & PH Criteria Been Met? OY N
BIN #k 1
Setup Date: 8-/k-15
Removal From Bin Date: 8-111-15
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
f -1q-15
/a : Na 'rr►
Initial PH: 12,175
.700
R�GJ
Corrected' PH: /,2 , 95
-19-1 S
0 9; 33,s,10
Final PH: /.I. *-S
6
JP� f;✓
[Corrected PH: / 3, O
Has 72 Hour & PH Criteria Been Met? -
Y � N
BIN_#. 7-_.
Setup- Date: 8-17-IS
Removal From Bin Date: 8-IQ-IT
Date
Time
PH. >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 17, Hrs.
Operator
8-17-IS
I P m
Iriitial PH: /2. f
c
0
A W
Corrected PH: -%.?,
fir'-19-13
P
•2: 5�,►
Final PH:
Corrected PH: /_9. O'/
Has -72 Hour & PH Criteria Been Met? Y N
BIN # 8
Setup Date: 8-.2y /S
Removal From Bin Date: ,7y-/5
Date
Time
.PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial
60
Cotrected pk: 13,0
P
Final PH: J.?. 9 3
80
Corrected PH: /3, 1
Has 72 Hour. & PH Criteria Been Met? Y N

REn t,i lSM
DIN7LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No.Case Narrative
SC Certification No. 990 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No.460211 01/21/2015
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Quarterly Parameters)
Lab Submittal Date: 01/12/2015
Prism Work Order: 5010167
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VL-
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash For Robbi A. Jones
VP Laboratory Services
MC - Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference .
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/5.29-6364 - Fax: [phone] Page 1 Of 8

Full -Service Analytical & Sample Receipt Summary
/&RISM
I Environmental Solutions 01/21/2015
IAeOaATOFIES ING
Prism Work Order: 5010167
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime 5010167-01 Solid 01/12/15 01/12/15.
Samples were received at 13.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 Of 8

City of Statesville
Mr. Andy Smith
Post Office Box 1111
Statesville NC, 28687-1111
*MICRO:BAC@
Fayetteville Division
Certificate of Analysis
Project: Sta-lime/Sludge Sample - 4th Creek W VTP
Date Reported: 10/01/15
Date Received: 09/22/15
Date Sampled: 09/22/15
Sampled By: Smith
Sta-lime Sample, Grab
K5I0532-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Baltimore
% Solids 94.99 % by Weight 09/25/15 07:17 LCR SM 2540 G-11
Salmonella <0.027 MPN/4g dry 09/26/15 10:00 RKT EPA 1682
QC Batch Run - (Microbac Laboratories, Inc. -Baltimore)
Analyte
Result
Units
Source
RPD
Limit
% Solids
19.26
% by Weight
15I1706
4.25
5
%a Moisture
97.13
% by Weight
1511706
0.0337
5
% Solids
2.87
V. by Weight
1511706
1.13
5
% Moisture
78.02
% by Weight.
1511706
1.36
5
%a Solids
21.98
% by Weight
15I1706
4.99
5
% Moisture
72.71
% by Weight
1511706
2.18
5
% Solids
27.29
% by Weight
1511706
5.58
5
%a Moisture
96.94-
-`- %o by Weight =
1511706
0.0636
5
% Solids
3.06
% by Weight
1511706
2.04
5
% Moisture
80.74
% by Weight
1511706
0.989
5
Notes and Definitions
RI Sample Duplicate RPD was out of acceptance limits.
State Certifications:
NCDNR #11
NCDOH #37714
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. We invite your feedback on our level ofservfce to you. Please contact the Division Manager, Rob Dermer at 910-864-1920 with any
uestioirs` You in ' also' contact' J. Trevor'Bo' ' e Presiden(af retiide»t murobadcom
Microbac Laboratories, Inc.
Page 1 of 2
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division 2592 Hope Mills Road —Fayetteville, NC 28306 [phone] / 864-8i
'�'� 1 �':u6 R.0-B- C-.-"- *K510532*
,,, IIIIVIII�IIIIIIII
CHAIN OF CUSTODY RECORD �III�IIIIIIII
PAG:
CLIENT NAME BADDRESS:
PO it _
TYPE
OF
ANALYSIS
PRE5ERVAIIUNV I.;UUC
.................................
>ropE; A N'66' : :
City oi. Statesville
y
13343Creek
TPROJECTILOCATION:
WWTP
CONTACTPERSON:
}
693 Be11 Farm Road
y
J
iii iiB .=EI SIO3: IiS2.'(EVg°CiiiiiiiEEEEiiEi'.:EEEiiiEE
............................[P........)..............:.,.......................
StateJille NC 28677
Mr. And Smith
..(P....,;.,..)......................................
O
Z
::::.+✓.:#?!l:isi.,.:::::::::.
PHONE:
704-878_3438
a
6iZ-N€Aa'W .....a.
s.mPl.a ey:
�v
_
.�.iii:isi:::�:Isis::::::��ii�::::::::?�:iii::::::
..............::::.:.:................................
DATE METHOD OF SHIPMENT:
.
Andy Smith
9/22/15 UPS Next Day Air
C
E
CO
..... ..
€=So �i Tfiii ' .................................
LAB ID #
SAMPLE
TYPE
DATE
TIME
COMP
GRAB
PH
FLOW
TEMP °C
RES.
CHLORINE
SULFIDE
1—
Sta-Lime
9/22/15
10:00
X
1
A
Lab Initials--p.
Turnaround time: REGULAR RUSH
Comments or Special Hazards:
Relinquished by:
Date
Time
Received by: (Signature)
Dot.
Time
And Smith 1
09/22/15
10:45
2
Relinquished by:
Date
Time
Received by: (Signature)
Data
Time
3
4
Relinquished by:
Date
Time
Received by: (Signature)
Data
Time
5
6
pH Field :
pre Field:
water Level *1
Temp Field 1:
Temp Field 2:
Water Level #2
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:
Page 2 of.2.

Laboratory Report
r= Full -Service Analytical 8
%? I Environmental Solutions 01/21/2015
�� u= LABORATORIES, INC.
City of Statesville, NC Project: StaLime (Quarterly Client Sample ID: StaLime
Attn: Andy Smith Parameters) Prism Sample ID: 5010167-01
P.O. Box 1111 Prism Work Order: 5010167
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/12/15 10:05
Time Submitted: 01/12/15 15:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
540
mg/kg
380
32
5
*Calculation
1/16/15 11:04
CLB
[CALC]
Solids
73.7
% by
0.100
0.100
1
*SM2540 G
1/15/15 17:15
IVIJO
P5A0211
Weight
Nitrate/Nitrite as N
13
mg/kg dry
6.8
0.75
1
*SM4500-NO3 F
1116/15 11:04
CLB
PSA0179
Phosphorus -Total
2300
mg/kg dry
68
15
20
*SM4500-P F
1/19/15 8:23
CLB
P5A0196
Total Kjeldahl Nitrogen
2300
mg/kg dry
1700
140
5
*351.2
1/16/15 8:25
CLB
PSA0185
Ammonia as N
140
mg/kg dry
6.8
1.6
1
*SM4500-NH3 G
1/15/15 8:45
CLB
PSA0165
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
1/13/15 10:00
MES
P5A0189
Total Metals
Mercury
0.12
mg/kg dry
0.029
0.0048
1
*7471B
1116/15 9:28
JAB
P5A0156
Arsenic
7.9
mg/kg dry
0.34
0.048
1
*6010C
1/14/15 22:31
BGM
PSA0149
Cadmium
BRL
mg/kg dry
0.34
0.048
1
*6010C
1/14/15 22:31
BGM
P5A0149
Copper
30
mg/kg dry
0.67
0.12
1
*6010C
1114115 22:31
BGM
PSA0149
Lead
14
mg/kg dry
0.34
0.051
1
*6010C
1/14/15 22:31
BGM
P5A0149
Nickel
160
mg/kg dry
1.3
0.17
1
*6010C
1/14/15 22:31
BGM
PSA0149
Potassium
5200
mg/kg dry
840
53
50
*6010C
1/21/15 12:17
BGM
P5AM49
Selenium
BRL
mg/kg dry
0.67
0.080
1
*6010C
1/14/15 22:31
BGM
P5A0149
Sodium
880
mg/kg dry
17
3.3
1
*6010C
1/14/15 22:31
BGM
P5A0149
Zinc
62
mg/kg dry
3.4
0.74
1
*6010C
1114115 22:31
BGM
PSA0149
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 8

Level II QC Report
/�FI S n i� Full -Service Analytical � 1/21/15 "
("� 'v � Environmental Solutions
5y "DORATORIE$ ING.
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 5010167
Attn: Andy Smith Time Submitted: 1/12/2015 3:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5A0149 - 3050B
Blank (HA0149-BLK1)
Prepared & Analyzed: 01/14/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P5A0149-BSI)
Prepared & Analyzed: 01/14/15
Arsenic
23.8
0.25
mg/kg wet
25.00 95
80-120
Cadmium
23.6
0.25
mg/kg wet
25.00 95
80-120 .
Copper
25.7
0.50
mg/kg wet
25.00 103
80-120
Lead
23.3
0.25
mg/kg wet
25.00 93
80-120
Nickel
23.8
1.0
mg/kg wet
25.00 95
80-120
Potassium
514
12
mg/kg wet
500.0 103
80-120
Selenium
23.7
0.50
mg/kg wet
25.00 95
80-120
Sodium
522
12
mg/kg wet
500.0 104
80-120
Zinc
23.8
2.5
mg/kg wet
25.00 95
80-120
Batch P5A0156 - 7471 B
Blank (P5A0156-BLK1) _ Prepared: 01/14/15 Analyzed: 01/16/15
Mercury BRL 0.020 mg/kg wet
LCS (P5A0156-BS1) Prepared: 01/14/15 Analyzed: 01/16/15 _
Mercury 0.466 0.020 mg/kg wet 0.4167 112 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 8

AL�l'
Level II QC Report
� Full -Service Analytical 1/21/15
R ISM
I Environmental Solutions
s
a` LABORATORIES INa
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 5010167
Attn: Andy Smith Time Submitted: 1/12/2015 3:10:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5AO165 - NO PREP
Blank (P5AO165-BLK1) Prepared & Analyzed: 01/15/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (PM0165-13SI) Prepared & Analyzed: 01/15/15
Ammonia as N 132 5.0 mg/kg wet 125.0 106 80-120
Matrix Spike (P5AO165-MS1) Source: 5010167-01 Prepared & Analyzed: 01/15/15
Ammonia as N 342 6.8 mg/kg dry 169.6 141 119 80-120
Matrix Spike Dup (P5AO165-MSD1) Source: 5010167-01 Prepared & Analyzed: 01/15/15
Ammonia as N 338 6.8 mg/kg dry 169.6 141 117 80-120 1 20
Batch P5AO179 - NO
Blank (P5A0179-BLK1) Prepared & Analyzed: 01/16/15
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P5AO179-BS1) Prepared & Analyzed: 01/16/15
Nitrate/Nitrite as N 51.8 5.0 mg/kg wet 50.00 104 80-120
Matrix Spike (P5AO179-MS1) Source: 5010167-01 Prepared & Analyzed: 01/16/15
Nitrate/Nitrite as N 73.6 6.8 mg/kg dry 67.84 13.1 89 80-120
Matrix Spike Dup (PSA0179-11VISD1) Source: 5010167-01 Prepared & Analyzed: 01/16/15
Nitrate/Nitrite as N 74.8 6.8 mg/kg dry 67.84 ' - 13.1 91 80-120 2 20
P5AO185 - 351.2
Blank(P5A0185-BLK1) Prepared: 01/15/15 Analyzed: 01/16/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 8

6 �43
a Full Service Analytical &
I S M Environmental Solutions
�.m� ,S;iLADORATONIE& INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Level II QC Report
1/21/15
Project: StaLime (Quarterly Parameters) Prism Work Order: 5010167
Time Submitted: 1/12/2015 3:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5AO185 - 351.2
LCS (P5A0185-BS1) Prepared: 01/15/15 Analyzed: 01/16/15
Total Kjeldahl Nitrogen 500 100 mg/kg wet 500.0 100 90-110
Batch P5AO196 - SM4500-PB5
Blank (P5AO196-BLK1) Prepared: 01/16/15 Analyzed: 01/19/15
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P5AO196-BSI) Prepared: 01/16/15 Analyzed: 01/19/15
Phosphorus -Total 101 2.5 mg/kg wet 100.0 - 101 90-110
Matrix Spike (P5A0196-MS1) Source: 5010167-01 Prepared: 01/16/15 Analyzed: 01/19/15
Phosphorus -Total 2230 68 mg/kg dry 135.7 2350 NR 80-120 MC
Matrix Spike_Dup (P5AO196-MSD1) Source: 5010167-01 Prepared: 01/16/15 Analyzed: 01/19/15
Phosphorus -Total 2210 68 mglkg dry 135.7 2350 NR 80-120 0.9 20 MC
Batch P5AO211 - Solids Dry Weight
Blank (P5AO21 1 -BLK1) Prepared & Analyzed: 01/15/15
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 Of $

Level II QC Report
�PFu11-Service Analytical& 1/21/15
P�R i S M I Environmental Solutions
a"'�-�--^�LgeOPpNPIES, ING
City of Statesville, NC Project: Stal-ime (Quarterly Parameters) Prism Work Order: 5010167
Attn: Andy Smith Time Submitted: 1/12/2015 3:10:00PM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits _ RPD Limit Notes
Batch P5A0189 - NO PREP
Blank (P5A0189-BLK1) Prepared & Analyzed: 01/13/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample. Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Daterrime
5010167-01
P5A0185
0.05 g 25 mL 01/15/15 10:30
Prep Method: SM4500-PBS
Lab Number
Batch
Initial Final Date/rime
5010167-01
P5A0196
1 g 50 mL 01/16/15 10:45
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial Final Daterrime
5010167-01
P5A0211
30 g 30 g 01/15/15 17:15
Prep Method: 3050B
Lab Number
Batch
Initial Final Daterrime
5010167-01
P5A0149
2.02 g 50 mL 01/14/15 ' 8:05
5010167-01
P5A0149
2.02 g 50 mL 01/14/15 8:05
Prep Method: 7471B
Lab Number
Batch
Initial Final Daterrime
5010167-01
P5A0156
0.56 g 50 mL 01/15/15 14:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 8

CHAIN OF cusTODY RECORD
.
.....
Full -Service Analytical &
R I Environmental Solutions
I
/A
00
0
LABORATOBIES, WC.
PAGE Or QUOTE # TO ENSURE PROPER BILLUNG:
pp'
Aecelved ON ET , ICE .
oo
449 Springbrook Road • P.O. Box 240543 •Charlotte, NC 2822 4-0543
Project Name:
.. .......
S_ ',' d I d ?5
PROPMPRESERY,�Tly.E_ in ICP,�'L
0)1
Phone: 704/52q-6364 • Fax: [phone]
Short Hold Analysis: (Yes) (No) LIST Project: (Yes) (No)
�Rbcelved;WITHIN HOLDING -TIMES? ­);
Name:
Client Company Na
*Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
C0STQDY�SEALS1NT
provisions and/or OC Requirements
,­___n
Report To/Contact Name:
Invoice To:
Reporting Address:
Address:
Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date C] I Day ❑0 2 Days ❑0 3 Days ❑CI 4 Days C3 5 Days
Certification: NELAC USACE FL
NC
EDD Type: PDF_ Excel —Othe
"Working Days" Q 6-9 Days C] Standard 10 days 0 Rush Work Must Be
Pre
Site Location Name:
-Approved
Samples received after 15:00 will be processed next business day.
so OTHER N/A
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— NO
(SEEREVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
MATRIX
(SOIL,
WATER OR
SAMPLE CONTAINER
'TYPE Kin SIZE
PRESERVA-
TIVES
ANALYSES REQUESTED
REMARKS
PRISM
LAB
ID NO.
Samr
Upon
sub
FIR "
Z
RelZ
MethoE
HOURS SLUDGE) SEE BELOW
(A ra
10!0JA .11 P
C
cu
Sampled By (Print Nam
this Chain of Ctuistody is your authorization for Prism to pri
to the Prism Project Manager. There will be charges for ai
Receive Ty: na}
RecelvffBy: (Signat
Affiliation
with the analyses as requested above. Any changes must be
nges after analyses have been initialized.
141� ils�o
P 11 <
FA
TA
SAMPLES ARE NOT ACEPTED AND VERIFIED AGAINST COC UNTILAECEIVED AT THE LABORATORY.
QFedEx DUPS C3 Hand -delivered risrri Fleld Service
C1 Other
NPDES: 1 UST: I GROUNDWATER: I
DRINKING WATER' SOLID WASTE:
RCRA.'
C ERCLA LANDFILL
OTHER:
0 NC ❑ SG C3 NC ID SC I C1 NC Q SC
C3
U NC Cj SC 0 NC El SC
121 N C C3 SC
�
0 NC 0 SC Ci NC C3 SC
C3 NC 0 SC
:1 LI
[3
C] —
0
Additional Comments:
Site Arrival T
Site Departure Tltpe
'77 Field T c
0
*i1nh1TA1r11F=92 TVDF= Cr1nr=4z- A - A-h., (' - ('1— ('- - ('-f— P - pi-fi- T1 - Tofln-1 in -A (:an \tr)A - \/nImflim ("ir-nine A -kicic (7arn 1-1-1 Qn­`i

NC Certification No.
990 Case Narrative
trnl
SC Certification No. 99012
n�Full-Service Analytical R NC Drinking Water Cert No. 37735S I V 1 IO2/17/2015
.��lEnvironmental Solutions vAcertification No. 4so211
fa'v eoaAToaiES INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (60 Day/7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 02/09/2015
Statesville, NC 28687 Prism Work Order: 5020175
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of T 3

Full -Service Anal tical & Sample Receipt Summary
Environmental So utions 02/17/2015
R ISM
�'��` ��°+IA90PATOaIES INC
Prism Work Order: 5020175
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime (and Fecal 1)
5020175-01
Solid
02/09/15
02/09/15
Fecal #2
5020175-02
Solid
02/09/15
02/09/15
Fecal #3
5020175-03
Solid
02/09/15
02/09/15
Fecal #4
5020175-04
Solid
02/09/15
02/09/15
Fecal #5
5020175-05
Solid
02/09/15
02/09/15
Fecal #6
5020175-06
Solid
02/09/15
02/09/15
Fecal #7
5020175-07
Solid
02/09/15
02/09/15
Samples were received in good condition at 1.3 degrees C unless otherwise noted.
This report should not be reproduced, exceptin its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13

R 0 S Laboratory Report
Full -Service Analytical &
IR Environmental Solutions 02/17/2015
l �U' L O6 TOnlm Ma
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: StaLime (ancl Fecal 1)
Attn: Andy Smith
Prism Sample ID: 5020175-01
P.O. Box 1111
Prism Work Order: 5020175
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
68.2
% by
0.100
0.100
1 'SM2540 G 2/13115 16:35
MJO
P5B0286
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 'SM9221 E 2/10/15 12:05
MES
P560239
Total Metals
Mercury
0.17
mg/kgdry
0.027
0.0045
1 `7471B 2/13/15 12:07
JAB
PSB0259
Arsenic
5.5
mg/kg dry
0.37
0.052
1 `6010C 2/12115 6:15
BGM
P5B0206
Cadmium
BRL
mg/kg dry
0.37
0.052
1 '6010C 2/12/15 6:15
BGM
P5B0206
Copper
30
mg/kg dry
0.73
0.13
1 `6010C 2/12115 6:15
BGM
PSB0206
Lead
13
mg/kg dry
0.37
0.056
1 '6010C 2/13/15 16:38
BGM
P5B0206
Nickel
120
mg/kg dry
1.5
0.19
1 '6010C 2/12/15 6:15
BGM
P5B0206
Selenium
BRL
mg/kg dry
0.73
0.088
1 '6010C 2/13/15 16:38
BGM
P5130206
Zinc
60
mg/kg dry
3.7
0.81
1 '6010C 2/12115 6:15
BGM
P5B0206
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] rage 3 Of 13

�TR Full -Service Analytical &
/11 '
,1 �'d IS Environmental Solutions
�� UBORATORIEq ING
Laboratory Report,
02/17/2015
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: Fecal #2
Attn: Andy Smith
Prism Sample ID: 5020175-02
P.O. Box 1111
Prism Work Order: 5020175
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids
70.2 % by
0.100 0.100
1 ASM2540 G 2/13/15 16:35 MJO P5B0286
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 2/10/15 12:05 MES P5B0239
Q
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 13

r
� R ISM Full -Service Analytical Environmental Solutions
`J".�iJ"t�v �"• UBOPATORwa-
Laboratory Report
02/17/2015
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #3
Attn: Andy Smith Prism Sample ID: 5020175-03
P.O. Box 1111 Prism Work Order: 5020175
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 70.0 % by 0.100 0.100 1 'SM2540 G 2/13/15 16:35 MJO PSB0286
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 2110115 12:05 MES P5130239
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

,F
Laboratory Report
r� � Full -Service Analytical &
M
'Ir l Environmental Solutions
02/17/2015
.�� IABORATORIEQ ING '
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: Fecal #4
Attn: Andy Smith
Prism Sample ID: 5020175-04
P.O. Box 1111
Prism Work Order: 5020175
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter Result
Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 66.3
% by
0.100 0.100
1 'SM2540 G 2113/15 16:35 MJO
P5B0286
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 2110/15 12:05 MES
P5B0239
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 Of 13

� I S Environmental
Analytical
r Environmental Solutions
VIAaONA Slgs. ING.
Laboratory Report
02/17/2015
City of Statesville, NC
Project: Stal-ime (60 Day/7 Fecal)
Client Sample ID: Fecal #5
Attn: Andy Smith
Prism Sample ID: 5020175-05
P.O. Box 1111
Prism Work Order: 5020175
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids
68.7 % by
0.100 0.100
1 *SM2540 G 2/13/15 16:35 MJO P5B0286
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 2110/15 12:05 MES P5130239
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 13

r.� Full -Service Analytical 8
,/rh,R ISM I Environmental Solutions
"VI-rATOHIE$ING � �'+
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/17/2015
Client Sample ID: Fecal #6
Prism Sample ID: 5020175-06
Prism Work Order: 5020175
Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 71.9
% by
0.100
0.100 1
*SM2540 G 2/13/15 16:35 NIJO
P5B0286
Weight
Microbiological Parameters .
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 2/10/15 12:05 MES
P5B0239
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 13

Full -Service Analytical &
O R I S M Environmental Solutions
l LAOORATORIE9, ING
Laboratory Report
02/17/2015
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #7
Attn: Andy Smith Prism Sample ID: 5020175-07
P.O. Box 1111 Prism Work Order: 5020175
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/09/15 12:20
Time Submitted: 02/09/15 17:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 67.0 % by 0.100 0.100 1 'SM2540 G 2113/15 16:35 MJO PSB0286
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 2/10/15 12:05 MES P580239
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 13

Level II QC Report
--r®R I S � /j EnviService Analytical 2/17/15
3. � �/ � Environmental Solutions
`4 -son To.'E9, I Q
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 5020175
Attn: Andy Smith Time Submitted: 2/9/2015 5:15:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5B0206 - 3050B
Blank (PSB0206-BLK1)
Prepared: 02/11/15 Analyzed: 02/12/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL.
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P5BO206-BS1)
Prepared: 02/11/15 Analyzed: 02/12/15
Arsenic
19.9
0.25
mg/kg wet
25.00 80
80-120
Cadmium
20.0
0.25
mg/kg wet
25.00 80
80-120
Copper
20.8
0.50
mg/kg wet
25.00 83
80-120
Lead
22.4
0.25
mg/kg wet
25.00 90
80-120
Nickel
20.0
1.0
mg/kg wet
25.00 80
80-120
Selenium
22.4
0.50
mg/kg wet
25.00 90
80-120
Zinc
20.0
2.5
mg/kg wet
25.00 80
80-120
Batch P5130259 - 7471 B
Blank (P5B0259-BLK1)
Prepared & Analyzed: 02/13/15
Mercury
BRL
0.020
mg/kg wet
LCS (P5B0259-BS1)
Prepared &Analyzed: 02/13/15
Mercury
0.460
0.020
mg/kg wet
0.4167 110
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 13

t Full -Service Analytical &
Environmental Solutions
LA90RAT 1R 1Na
City of Statesville, NC Project: StaLime (60 Day/7 Fecal)
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality.Control
Level II QC Report
2/17/15
Prism Work Order: 5020175
Time Submitted: 2/9/2015 5:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5BO286 - Solids, Dry Weight
Blank (P5B0286-BLK1) Prepared & Analyzed: 02/13/15
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] =Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 13

Lt4
�I SM n Full -Service Analytical &
' I Environmental Solutions
LA60HATOfl M ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime (60 Day/7 Fecal)
Level II QC Report
2/17/15
Prism Work Order: 5020175
Time Submitted: 2/9/2015 5:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5BO239 - NO PREP
Blank (P51B0239-BLK1) Prepared & Analyzed: 02/10/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Daterrime
5020175-01
P580286
30
g 30 g
02/13/15
16:35
5020175-02
P5130286
30
g 30 g
02/13/15
16:35
5020175-03
P51310286
30
g 30 g
02/13/15
16:35
5020175-04
P5B0286
30
g 30 g
02/13/15
16:35
5020175-05
P5B0286
30
g 30 g
02/13/15
16:35
5020175-06
P5130286
30
g 30 g
02/13/15
16:35
5020175-07
P5130286
30
g 30 g
02/13/15
16:35
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
5020175-01
P580206
2 g
50 mL
02/11/15 8:40
5020175-01
P5130206
2 g
50 mL
02/11/15 8:40
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
5020175-01
P5B0259
0.65 g
50 mL
02/13/15 7:40 -
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 0f 13

° Full -Service Analytical &
l yoCHAR OF CUSTODY RECOM
10 I Environmental Solutions PAGE _ of _ ouove m TO erasuat PROPER BILLIraq:
x+
s
taaoas.TORies, INC. Project Name:
449 St�ringbrook Road ^ P.O. Box 240543 ^Charlotte, NC 28224-0543 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Phone:[phone] Fax:[phone]
.� y 9.�' �,{.�.��, � �, s I �' � `Please ATTACH any project specific reporting (OC LEVEL I II III IV)
Client Company Name: provisions and/or QC Requirements
Report To/Contact Name- A tog x�'`�' ' Invoice To:
Reporting Address: Address:
Phone:7Q�f -$7 9-'3b3 Fax' es (No):�7�' 3dJ Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC_
Rush Work Must Be
EDD Type' PDF_ Excel _Other "Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ Pre -Approved SC_ OTHER N/A
Site Location Name:
{�u r - Cr c C C 1 LO 7 P Samples received after 15:00 will be processed next business day.
NO
�C � � VO'r`"B �'' � Turnaround time is based on business days, excluding weekends and holidays, Water Chlorinated: YES—
Site Location Physical Address: 6�YES_
— —
y) (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES ____ NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
ANALYSES REQUESTED PRISM
TIME MATRIXPSEE
AMPLE CONTAINER LAB
CLIENT DATE COLLELITCTED (SOIL, PRESERVA- j % REMARKS ID NO.
TIVES /
SAMPLE DESCRIPTION COLLECTED MHOURSY SLUDGE)LOWNO. SIZE (�:rt
> l . f j �.��'�Or2i�1 TriiaSr„rFA7 Dr . As
E-ram -`. /r :: rrD _e.—. r^^—.—.— --- —� -- � -- -- --- --- --- — — -- y
C14 No IV C
L'
Sampler's Signature „W� �' Sampled By (Print Name) Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proc ed ith the analyses as requested above. Any changes must 5besubmitted In writing to the Prism Project Manager. There will be charges fora changes after analyses have been initialized. =7
Date MAdd'Itienal Comments:
eceive .Sign ' e)
R 1i wished By: (Slgnat )
yJt dui. /� f�C�' G•C` . Receive By:(SI azure) Dat6
Re (shed By: (Signature) q
r Received For Prl aboratorrI4 By! Date h C
Reiny: (Sign atu 4
r
COS
N ATE: ALL SAMPLE COOLERSHUT WITH CUS DY SEALS FOR TRANSPORTATIO
Method o Shipment: S SHOULD BE TAPED
TO THE LABORATORY. COC G oup No.
/ S MPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNT) RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑UPS Hand -delivered ❑ Prism Field Service ❑ Other. / ) t
NPDES
: f UST: GROUNDWATER: DRINKING
WATER: SOLID WASTE: I RCRA: I ICE
RCLA I LANDFILL OTHER:
❑NC ❑c ❑NC ❑SCI ❑NC ❑SC ❑NC CSC I ❑NC CSC ❑NC ❑SC ❑NC ❑SC'} ❑NC ❑, ❑❑NC ❑SC
❑ ❑ — - ❑ _ — — — — ❑ — — — — — ❑ — — — ❑ — — ❑ — — — I ❑ —
.nnnrrneorcD rroF r_rant=Sr A =Amber C =Clear G =Glass P =Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
„.SEE'REVERSE FOR -a„
TERMS & CONDITIONS

�} h I S Full -Service Analytical &
Environmental Solutions
��.`•.' LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC'Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD FLAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 02/23/2015
Prism Work Order: 5020417
Case Narrative
03/02/2015
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VL•
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
)��_ a_. (_
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 8

Sample Receipt Summary
! �L. Full -Service Analytical &
�1r S I environmental Solutions 03/02/2015
� L--OFATORIM INC.
Prism Work Order: 5020417
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 5020417-01 Solid 02/23/15 02/23/15
Samples were received in good condition at 1.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety,.without-the written.consent of.Prism Laboratories„ Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 Of 8

Laboratory Report
,�f t.
* I S M
Full -Service Analytical &
Environmental Solutions
03/0212015
i�1�160RATOflIES, ING
.
City of Statesville, NC Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 5020417-01
P.O. Box 1111
Prism Work Order: 5020417
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 02/23/15 13:20
Time Submitted: 02/23/15 14:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
74.8
% by
0.100
0.100
1
'SM2540 G
2/26/15 16:05
MJO
PSB0511
Weight
Microbiological Parameters '
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
2/24/15 10:45
EGC
P5130483
Total Metals
Mercury
0.082
mglkg dry
0.026
0.0043
1
'7471B
2/27115 13:05
JAB
P580506
Arsenic
3.4
mg/kg dry
1.0
0.14
3
"6010C
2125115 20:01
BGM
P5130463
Cadmium
BRL
mg/kg dry
1.0
0.14
3
'6010C
2/25/15 20:01
BGM
P5B0463
Copper
17
mg/kg dry
2.0
0.37
3
'6010C
2125/15 20:01
BGM
P5B0463
Lead
10
mg/kg dry
1.0
0.15
3
"6010C
2/25/15 20:01
BGM
PSB0463
Nickel
110
mg/kg dry
4.1
0.52
3
'6010C
2/25115 20:01
BGM
P5B0463
Selenium
BRL
mg/kg dry
2.0
0.24
3
'6010C
2/25/15 20:01
BGM
P5B0463
Zinc
41
mg/kg dry
10
2.2
3
'6010C
2125/15 20:01
BGM
1`5130463
This_ re ort should not be„re roduced,, exce t m it entirety, without the written consent of Prism Laboratories, Inc
449 Springbrook Road -'P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free.Number: 1-800/529-6364 - Fax: [phone] Page 3 Of 8

�, n ISM I Full -Service Analytical s
. �r-'.,'i Environmental Solutions
T ra_'_ - I 80MT0MES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
P5BO463 - 3050B
Project: StaLime
Reporting
Result Limit Units
Level 11 QC Report
3/2/15
Prism Work Order: 5020417
Time Submitted: 2/23/2015 2:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P5B0463-BLK1)
Prepared & Analyzed: 02/25/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (PSB0463-BSI)
Prepared &Analyzed: 02/25/15
Arsenic
25.7
0.25
mg/kg wet
25.00 103
80-120
Cadmium
25.6
0.25
mg/kg wet
25.00 102
80-120
Copper
26.9
0.50
mg/kg wet
25.00 108
80-120
Lead
25.5
0.25
mg/kg wet
25.00 102
80-120
Nickel
25.7
1.0
mg/kg wet
25.00 103
80-120
Selenium
25.7
0.50
mg/kg wet
25.00 103
80-120
Zinc
25.8
2.5
mg/kg wet
25.00 103
80-120
Batch P5BO506 - 7471 B
Blank (P5BO506-BLK1) Prepared & Analyzed: 02/27/15
Mercury BRL 0.020 mg/kg wet
LCS (PSB0506-BS1) Prepared & Analyzed: 02/27/15
Mercury 0.443 0.020 mg/kg wet 0.4167 106 80-120
Matrix Spike (P5BO506-MS1) Source: 5020417-01 Prepared &Analyzed: 02/27/15
Mercury 0.597 0.027 mg/kg dry 0.5570 0.0823 92 80-120
:This.report.should not be reproduced„except. in its;entirety,;without the written, consent of, Prism,Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364- Fax: [phone] Page 4 of 8

,,,, Full -Service Analytical &
P
. �1[...R R I S M Environmental Solutions
�! LABORATCNIEa INC.
Level II QC Report
3/2115
City of Statesville, NC Project: StaLime Prism Work Order: 5020417
Attn: Andy Smith Time Submitted: 2/23/2015 2:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5130506 - 7471 B
Matrix Spike Dup (P5B0506-MSD1) Source: 5020417-01 Prepared & Analyzed: 02/27/15
Mercury 0.615 0.027 mg/kg dry 0.5665 0.0823 94 80-120 3 20
This report should not be reproduced, except in.its entirety, -without the written consent.of Prism. Laboratories,.:lnc.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 8

PI S Full -Service Analytical &
t�sa Environmental Solutions
= �"ueoanroaiEs, we
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
3/2/15
Prism Work Order: 5020417
Time Submitted: 2/23/2015 2:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P560511 - Solids Dry Weight
Blank (P5130511-131-K1) Prepared &Analyzed: 02/26/15
% Solids 100 0.100 % by Weight
_ This report should not,be reproduced, except in its entirety, without the written consent of Prism Laboratories„Inc_ ..:. . ... .... _.. _
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 8

Level 11 QC Report
g
Pgi S M
Full -Service Analytical&
I Environmental Solutions
3/2/1.5
aR
TM'LABORATORIES INQ
City of Statesville, NC
Project: StaLime Prism Work Order: 5020417
Attn: Andy Smith
Time Submitted: 2/23/2015 2:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5BO483 - NO PREP
Blank (P5B0483-BLK1)
Prepared &Analyzed: 02/24/15
Fecal Coliforms
BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number I Batch
Initial Final Daterrime
5020417-01 P5130511 30 g 30 g 02/26/15 1 6:05
Prep Method: 3050B
Lab Number Batch Initial Final Date/lime
5020417-01 P5130463 1.98 g 50 mi- 02/25/15 9:10
Prep Method: 7471B
Lab Number Batch Initial Final Daterrime
5020417-01 P5B0506 0.61 g 50 mL 02/27/15 8:30
>
449 Springbrook Road - P.O. Box 240543 - Cifarlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 8

8 4 0-9?-3Y3$" Fax es (No):MI-97r8'-W
Phone: �Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (NO) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC
EDD Type: PDF_ Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑Rush Work Must Be
Pre -Approved SC OTHER N/A ;
Site Location Name: io,,-4h Lre. A w- r _ P Samples received after 15:00 will be processed next business day.
Site Location Physical Address:473 -&� "7 Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
SG4esV41l lw NC RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED PRISM
CLIENT DATE COLLECTED_ (SOIL, PRESERVA- \/ �zy / LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR "TYPE TIVES ��' y+� REMARKS ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE �• ��
1)Ye+ro;wtFilY�
P
S�ntu�a
�S
_.
B:txeAJyCR
r
�3
J
-
-
..._
Z.1,
_
Sampler's Signature O- Ce!' "� Sampled By (Print Name) f1 a ZJI r^ r K Affiliation
Upon relinquishing, this Chain of ustody is your authorization for Prism to pr ceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for ny changes after analyses have been initialized.
Rel'nq�ished By: (Signalq) Receiv : (Si ature) Date Military/Hours Additional Comments:
�t / v
/r g .�,tu1?2v1Lf fi. �i lt�
Reli ished By: (Signature) Rece ed By: ( ignature) D e
Relinqul : (Signature) , I Received For P ' Laborato jes B Date
' '
f '
o
Site Arrival Tlme
Slte DepartureTtn]e
- =
Field Tech Fee
Mlleag:
•�
Method of S pment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH C ODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMP ES ARE NOT ACCEPTED AND VERIFIED AGAINST COC U -C RECEIVED AT THE LABORATORY, _
❑ Fed Ex ❑ UPS ❑ Hand-dellvered 'sin Field Service ❑ Other
NPDES: UST: CERCLA LANDFILL OTHER:
❑NC ❑SC CI ❑SC ❑NC ❑SC GROUNDWATER: I ❑NC ❑SC I ❑NC ❑SC DRINKING WATER: SOLID WASTE: RCRA: ❑NC ❑SC ❑NIX
NC ❑SC ❑NC ❑SC ❑NC ❑SC
n r_1 r-) ❑ - - - i ❑ . _— ❑ — _.— ❑ ❑ _ . - i ❑
t_cF"iii,yii•Jr":._
'CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VUA = voiame urganlcs Analysis (ceru nedu opdue)

NC Certification No.402 Case Narrative
SC Certification No. 99012
P I SM Full Service Analytical & NC Drinking Water Cert No 37735 03/17/2015
Environmental Solutions VA Certification No. 460211
Iu; tneoaAToaiEs, iNa bob ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 03/09/2015
Prism Work Order: 5030142
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 Of 7

Sample Receipt Summary
R f S� n I Full -Service Analytical &
-- 0 V f Environmental solutions 03/17/2015
LAeORATORIE$ ING
Prism Work Order: 5030142
Client Sample ID Lab Sample ID. Matrix Date Sampled Date Received
StaLime 5030142-01 Solid 03/09/15 03/09/15
Samples were received in good condition at 3.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 7

Report
Full -Service
Analytical
SLaboratory
�➢ � ISM Environmental Solutions
03/17/2015
-opxro-& INC.
City of Statesville, NC
Project: StaLime
Client Sample ID: StaLime
Attn: Andy Smith
Prism Sample ID: 5030142-01
P.O. Box 1111
Prism Work Order: 5030142
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 03/09/15 13:46
Time Submitted: 03/09/15 14:55
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
FactorDate/Time
ID
General Chemistry Parameters
% Solids
73.6
% by
0.100
0.100 .
1 *SM2540 G 3/11/15 16:10
MJO
P5CO219
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 3/10/15 12:10
EGC
P5CO236
Total Metals .
Mercury
0.18
mg/kg dry
0.027
0.0045
1 *7471B 3/11/15 10:45
JAB
PSCO183
Arsenic
6.1
mg/kg dry
1.0
0.15
3 *6010C 3116115 13:43
BGM
P5CO201
Cadmium
BRL
mg/kg dry
1.0
0.15
3 *6010C 3/16/15 13:43
BGM
P5CO201
Copper
23
mg/kg dry
2.0
0.37
3 *6010C 3/16115 13:43
BGM
P5CO201
Lead
24
mg/kg dry
1.0
0.16
3 *6010C 3116115 13:43
BGM
PSCO201
Nickel
160
mg/kg dry
4.1
0.53
3 *6010C 3116/15 13:43
BGM
PSCO201
Selenium
BRL
mg/kg dry
2.0
0.25
3 *6010C 3/16/15 13:43
BGM
P5CO201
Zinc
60
mg/kg dry
10
2.3
3 *6010C 3/16/15 13:43
BGM
P5CO201
This report should not be reproduced, except in its entirety, without the written.consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC.28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Of 7

Level II QC Report'"
i IS Full -Service Analytical 3/17/15
Environmental Solutions
, . LABORATORIES. INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P5C0183 - 7471 B
Project: StaLime
Reporting
Result Limit Units
Prism Work Order: 5030142
Time Submitted: 3/9/2015 2:55:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P5C0183-BLK1) Prepared &Analyzed: 03/11/15
Mercury BRL 0.020 mg/kg wet
LCS (P5C0183-BS1) Prepared & Analyzed: 03/11/15
Mercury 0.407 0.020 mg/kg wet 0.4167 98 80-120
Batch P5CO201 - 3050B
Blank (P5CO201-BLK1)
Prepared & Analyzed: 03/12/15
_
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
L_C_S (P5CO201-BS1)
Prepared &Analyzed: 03/12/15
_
Arsenic
23.4
0.25
mg/kg wet
25.00 94
80-120
Cadmium
23.9
0.25
mg/kg wet
25.00 96
80-120
Copper
24.7
0.50
mg/kg wet
25.00 99
80-120
Lead
23.6
0.25
mg/kg wet
25.00 94
80-120
Nickel
23.6
1.0
mglkg wet
25.00 94
80-120
Selenium
23.5
0.50
mg/kg wet
25.00 94
80-120
Zinc
23.5
2.5
mg/kg wet
25.00 94
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 7

®I FullService Analytical E
�"'� SM
Environmental Solutions
6 w:; ��L'^:*�, LABOgATOPIE&INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
3/17/15
Prism Work Order: 5030142
Time Submitted: 3/9/2015 2:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC . Limits RPD Limit Notes
Batch MOM - Solids, Dry Weight
Blank(P5CO219-BLK1) Prepared &Analyzed: 03/11/15
Solids 100 0.100 % by Weight ------------------ ---- --_---
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 7

R //�� alyLevel II QC Report
�-- l I S i V 1 Full -Service Antical s - _
Environmental Solutions 3/17/15 -
6"�5. uk LABORATORIES INa
City of Statesville, NC Project: Stal-ime Prism Work Order: 5030142
Attn: Andy Smith Time Submitted: 3/9/2015 2:55:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %DREG RPD
Analyte Result Limit Units Level Result %REC Limits RPD . Limit Notes
Batch P5CO236 - NO PREP -
Blank (P5CO236-BLK1) Prepared & Analyzed: 03/10/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Datelrime
5030142-01
P5CO219
30 g
30 g
03/11/15 16:10
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Daterrime
5030142-01
P5CO201
1.99 g
50 mL
03/12/15 8:45
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DatelTime
5030142-01 P5C0183
0.6 g 50 mL 03/11/15 9:26
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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CHAMN F CUSTODY RECORD
: L
,
dr
P R I I V
I Full -Service Analytical
f �-
�
Y S� NO
�•�
N/A,
Environmental Solutions
PAGE _ OF _ QUOTE d TO ENSURE P9ROP�ER BILLING:
�. l �--•
•'Sam Samples INTACTU on arrival.
p p
i
o
•- LABORATORIES, INC.
-
Received ON WET ICES Temp
—
4§9 Spluzgbroo{t Road ^ P.U. Box 240543 e Charlotte, NC 28224-0543
Project Name:.
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
PROPER PRESERVATIVES indicated?
-
o
Phone. 704/ r29-6364 Far: 704/525-0409
�' a ¢' � Ale
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
' .Received WITHIN HOLDING TIMES?.
�
r
�
Client Company Name: .�.y e +3.�r 5 vo;
" �p
provisions and/or QC Requirements
CUSTODY SEALS INTACT?
VOLATILES W/OUT HEADSPACE?
'!
Report To/Contact Name: v ti'
Invoice To:
rec'd
.:
Reporting Address:
Address:
PROPER CONTAINERS used?
_.
Phone: 10'1-8 V_ 3q 3,� Fax`Yes (No): 704- M'- FZ' 5
purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING
PERSONNEL
(Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL
NC
IEDD Type: PDF_ Excel _Other _
Name: r".,A Cf etr: k. �� t
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushWork Must Be pproved
business day.
SC OTHER
N/A
Site Location
Site Location Physical Address: 03 8C-11 r r m 171.
Samples received after 15:00 will be processed next
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES _ NO
PVC
(SEE REVERSE RENDERED BY PRRTERMS & CONDITIONS ISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
Sample
NO
TIME
COLLECTED
MATRIX
SAMPLE CONTAINER
PRESERVA-
ANALYSES REQUESTED
! % /
PRISM
CLIENT
DATE
(SOIL,
v°�
i REMARKS
SAMPLE DESCRIPTION
COLLECTED
MILITARY
SLUDGE)
SEE BE OW "NO.
SIZE
TIVES
/ /
ID NO.
Upon
re
f, this Chain of Custi
ig to the Prism Proje
ure) 0
_.. _ RAJ
�L 1�
cY Sampled By (Print Name) 0l t%' r Cl� Affiliation
dy is your authorization for Prism to Pr coed with the analyses as requested above. Any changes must be
A Manager. There will be charges for 7y changes after analyses have been initialized.
1 _1ri)` s I di , 3
Re ed By: (51 Q lure) nto v?.
rs I Additional Comments:
(- r i SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTI REC�.II/ED AT THE LABORATORY.
I \f
❑ Fed Ex ❑UPS ❑ Hand -delivered ❑ Prism Field Service ❑ Other
NPDES: I UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC El SC ❑NC ❑SC ❑NC ❑SC. ❑NC ❑SC ❑NC ❑SC Ci oNC ID SC
"CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402
Jg. SC Certification No. 99012 Case Narrative
MFull -Service Analytical & NC Drinkinq Water Cert No. 3773503/30/2015
Environmental Solutions VA Certification No. 460211
v eoRAroaies INC. DoFLAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 03/23/2015
Statesville, NC 28687 Prism Work Order: 5030389
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
1
Reviewed By. Terri W. Cole For Robbi A. Jones
Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 10

M
Full-Service Analytical sEnvironmental SolutionsnnOr-OR
Sample Receipt Summary
03/30/2015
Prism Work Order: 5030389
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 5030389-01 Solid 03/23/15 03/23/15
Samples were received at 19.9 degrees C. See case narrative for further information
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 10

P R I S M Full -Service Analytical 8
Environmental Solutions
..-al LABORATORIES INO
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime
Sample Matrix: Solid
Laboratory Report
03/30/2015
Client Sample ID: Sta-Lime
Prism Sample ID: 5030389-01
Prism Work Order: 5030389
Time Collected: 03/23/15 09:15
Time Submitted: 03/23/15 12:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
820
mg/kg
380
32
5
*Calculation 3130/15 8:07
CLB
[CALC]
Solids
71.6
% by
0.100
0.100
1
*SM2540 G 3126/15 16:00
EGC
P5C0454
Weight
Nitrate/Nitrite as N
8.0
mg/kg dry
7.0
0.77
1
*SM4500-NO3 F 3/30115 8:07
CLB
P5C0478
Total Kjeldahl Nitrogen
3700
mg/kg dry
1700
150
5
*351.2 3127115 7:48
CLB
PSC0450
Ammonia as N
110
mg/kg dry
7.0
1.6
1
*SM4500-NH3 G 3/26115 8:07
CLB
P5C0435
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 3123/15 13:45
EGC
P5C0401
Total Metals
Mercury
0.11
mg/kg dry
0.027
0.0044
1
SAR Soil Preparation
Complete
g
1
SAR Percent Moisture
46.6
% by
0.100
0.100
1
Weight
Arsenic
3.8
mg/kg dry
3.5
0.49
10
Sodium Absorption Ratio
0.84
[blank]
0.30
0.016
1
Cadmium
BRL
mg/kg dry
3.5
0.49
10
Calcium
2100 B
mg/L
50
4.2
500
Copper
24
mg/kg dry
6.9
1.3
10
Lead
10
mg/kg dry
3.5
0.52
10
Magnesium
1.0
mg/L
1.0
0.0070
10
Nickel
120
mg/kg dry
14
1.8
10
Selenium
BRL
mg/kg dry
6.9
0.83
10
Sodium
140
mg/L
5.0
0.074
10
Zinc
47
mg/kg dry
35
7.6
10
*7471B
3/25115 11:32
JAB
P5C0413
*2-78-054
3125/15 7:40
JAB
P5C0395
*2-78-054
3/25/15 9:00
JAB
P5C0440
*6010C
3/25/15 3:26
BGM
P5C0386
*2-78-054
3/26115 20:41
BGM
P5C0410
*6010C
3/25/15 3:26
BGM
P5C0386
*6010C
3126/15 20:41
BGM
P5C0410
*6010C
3/25/15 3:26
BGM .
. PSC0386
*6010C
3/25115 3:26
BGM
P5C0386
*6010C
3125/15 22:48
BGM
P5C0410
*6010C
3/25/15 3:26
BGM
P5C0386
*6010C
3/25/15 3:26
BGM
P5C0386
*6010C
3/25115 22:48
BGM
PSC0410
*6010C
3125115 3:26
BGM
P5C0386
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 10

Level II QC Report '
I Full -Service Analytical 3/30/15
Environmental Solutions
YC LABOFATOFIE$ NG
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime Prism Work Order: 5030389
Time Submitted: 3/23/2015 12:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5CO386 - 3050B
Blank (P5C0386-BLK1)
Prepared: 03/24/15 Analyzed: 03/25/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
0.731
0.50
mg/kg wet BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
L_CS (P5C0386-BS1)
Prepared: 03/24/15 Analyzed: 03/25/15
Arsenic
21.9
0.25
mg/kg wet
25.00
88
80-120
Cadmium
21.9
0.25
mg/kg wet
25.00
88
80-120
Copper
24.2
0.50
mg/kg wet
25.00
97
80-120
Lead
21.9
0.25
mg/kg wet
25.00
88
80-120
Nickel
22.5
1.0
mg/kg wet
25.00
90
80-120
Selenium
21.7
0.50
mg/kg wet
25.00
87
80-120
Zinc
22.0
2.5
mg/kg wet
25.00
88
80-120
Matrix Spike (P5C0386-MS1)
Source: 5030389-01
Prepared:
03/24/15
Analyzed: 03/25/15
Arsenic
29.4
3.4
mg/kg dry
34.06
3.79
75
75-125
Cadmium
23.6
3.4
mg/kg dry
34.06
BRL
69
75-125
MI
Copper
48.4
6.8
mg/kg dry
34.06
23.8
72
75-125
MI
Lead
33.6
3.4
mg/kg dry
34.06
10.1
69
75-125
MI
Nickel
144
14
mg/kg dry
34.06
124
60
75-125
MI
Selenium
20.2
6.8
mg/kg dry
34.06
BRL
59
75-125
MI
Zinc
69.9
34
mg/kg dry
34.06
47.3
66
75-125
MI
Matrix Spike Dup (P5CO386-MSD1)
_ _ Source: 5030389-01
Prepared:
03/24/15
Analyzed: 03/25/15
Arsenic
31.2
3.4
mg/kg dry
34.40
3.79
80
75-125
6
20
Cadmium
24.7
3.4
mg/kg dry
34.40
BRL
72
75-125
5
20
MI
Copper
49.7
6.9
mg/kg dry
34.40
23.8
75
75-125
3
20
Lead
34.8
3.4
mg/kg dry
34.40
10.1
72
75-125
3
20
MI
Nickel
150
14
mg/kg dry
34.40
124
77
75-125
4
20
Selenium
23.4
6.9
mg/kg dry
34.40
BRL
68
75-125
14
20
MI
Zinc
69.4
34
mg/kg dry
34.40
47.3
64
75-125
0.7
20
MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 0

®I S n � I Full -Service Analytical 8
®®�+ I'-"t ' � I Environmental Solutions
LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P5C0386 - 3050B
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
3/30/15
Prism Work Order: 5030389
Time Submitted: 3/23/2015 12:15:OOPM
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit
Notes
Post Spike (P5C0386-PSI)
Source: 5030389-01
Prepared: 03/24/15 Analyzed: 03/25/15
Arsenic
0.847
mg/L
1.000 0.108 74 80-120
MI
Cadmium
0.751
mg/L
1.000 0.00392 75 80-120
MI
Copper
0.944
mg/L
1.000 0.681 26 80-120
MI
Lead
0.776
mg/L
1.000 0.289 49 80-120
MI
Nickel
1.10
mg/L
1.000 3.54 NR 80-120
MI
.Selenium
0.813
mg/L
1.000-0.0773 81 80-120
Zinc
0.942
mg1L
1.000 1.36 NR 80-120
MI
Batch P5CO410 -
Blank (P5C0410-BLK1)
Prepared & Analyzed: 03/25/15
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium
0.204 0.10 mg/L BH
Magnesium
BRL 0.10 mg/L
Sodium
BRL 0.50 mg/L BH
Batch P5CO413 - 7471 B
Blank (P5C0413-BLK1) Prepared & Analyzed: 03/25/15
Mercury BRL 0.020 mg/kg wet
LCS (P5C0413-BS1) Prepared & Analyzed: 03/25/15
Mercury 0.432 0.020 mg/kg wet 0.4167 104 80-120
Batch P5CO440 - NO PREP
Blank (P5CO440-BLK1) Prepared & Analyzed: 03/25/15
SAR Percent Moisture BRL 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 10

'J
A0=111
L�' n n Full -Service Analytical &
I v' Environmental Solutions
w.�..,i. LARORATORIM INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Level II QC Report
3/30/15
Prism Work Order: 5030389
Time Submitted: 3/23/2015 12:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5CO440 - NO PREP
Duplicate (P5C0440-D1UP1) Source: 5030389-01 Prepared & Analyzed: 03/25/15
SAR Percent Moisture 46.2 0.100 % by Weight 46.6 0.9 200
0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
r
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 10

����//// Level II QC Report
PR I S Full -Service Analytical 3/30/15
z,._ Environmental Solutions
IARORATORIE1% INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 5030389
Time Submitted: 3/23/2015 12:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5CO435 - NO PREP
Blank (P5CO435-BLK1) Prepared & Analyzed: 03/26/15
Ammonia as N BRL 5.0 mg/kg wet
L_CS (P5C0435-BS1) Prepared & Analyzed: 03/26/15
Ammonia as N 126 5.0 mg/kg wet 125.0 101 80-120
Matrix Spike (P5C0435-MS1) Source: 5030389-01 Prepared & Analyzed: 03/26/15
Ammonia as N 278 7.0 mg/kg dry 174.6 112 95 80-120
Matrix Spike Dup (P5CO435-MSD1) Source: 5030389-01 Prepared & Analyzed:. 03/26/15
Ammonia as N 276 7.0 mg/kg dry 174.6 112 94 80-120 0.7 20
Batch P5C0450 - 351.2
Blank (P5C0450-BLK1)
Prepared: 03/26/15 Analyzed: 03/27/15
Total Kjeldahl Nitrogen
BRL 25 mg/kg wet
LCS (P5C0450-BS1)
Prepared: 03/26/15 Analyzed: 03/27/15
Total Kjeldahl Nitrogen
472 100 mg/kg wet
500.0 94 90-110
Matrix Spike (P5CO450-MS1)
Source: 5030389-01
Prepared: 03/26/15 Analyzed: 03/27/15
Total Kjeldahl Nitrogen
11200 3500 mg/kg dry
6982 3710 107 90-110
Matrix Spike Dup (P5C0450-MSD1)
Source: 5030389-01
Prepared: 03/26/15 Analyzed: 03/27/15
Total Kjeldahl Nitrogen
10800 3500 , mg/kg dry
6982 3710 101 90-110 4 20
Batch P5CO454 - Solids. Dry Weiqht
Blank (P5CO454-BLK2) Prepared & Analyzed: 03/26/15
% Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 10

RI S r V G I Full -Service Analytical Environmental Solutions
9 UB0flATOn1—INC.
Level II QC Report
3/30/15
City of Statesville, NC Project: Stal-ime Prism Work Order: 5030389
Attn: Andy Smith Time Submitted: 3/23/2015 12:15:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5C0478 - NO PREP
Blank (P5C0478-BLK1) Prepared & Analyzed: 03/30/15
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P5C0478-BS1) Prepared & Analyzed: 03/30/15
Nitrate/Nitrite as N 50.4 5.0 mg/kg wet 50.00 101 80-120
Matrix Spike (P5C0478-MS1) Source: 5030389-01 Prepared & Analyzed: 03/30/15
Nitrate/Nitrite as N 68.2 7.0 mg/kg dry 69.82 7.96 86 80-120
Matrix Spike Dup (P5CO478=MSD1) Source- 5030389-01. Prepared & Analyzed: 03/30/15
Nitrate/Nitrite as N 69.0 7.0 mg/kg dry 69.82 7.96 87 80-120 1 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 10

;r. Level II QC Report
Full -Service Analytical & 3/30/15
,R I S M Environmental Solutions
�"- —OnATos'mlNC.
City of Statesville, NC Project: StaLime Prism Work Order: 5030389
Attn: Andy Smith Time Submitted: 3/23/2015 12:15:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5C0401 - NO PREP
Blank (P5CO401-BLK1) Prepared & Analyzed: 03/23/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch . Initial Final Date/Time
5030389-01 P5C0450
Prep Method: Solids, Dry Weight
Lab Number Batch
0.05
Initial
g
25 mL
Final
03/26/15 12:00
Date/Time
5030389-01
P5C0454
30
g
30 g
03/26/15 16:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
5030389-01
P5C0410
50
mL
50 mL
03/25/15 9:00
5030389-01
P5C0410
50
mL
50 mL
03/25/15 9:00
5030389-01
P5C0410
50
mL
50 mL
03/25/15 9:00
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
5030389-01 P5C0386 2.02 g 50 mL 03/24/15 8:50
Prep Method: 7471B
Lab Number Batch Initial Final Daterrime
5030389-01 P5C0413 0.63 g 50 mL 03/25/15 8:35
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Daterl ime
5030389-01 P5C0395 250 g 250 g 03/24/15 7:40
I
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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CHAON OF CUSTODY RECORD
C:)
Full -Service Analytical &
Ism I Environmental Solutions
y N0 N/A
Or QUOTE fl TO ENSURE PROPER BILLING:
INTACT upon rriv l?­
arrival?
0
ABORMORIES, INC.
T
R eceiyed ON WET ICE? Temp-
C:)
449 Springbrook Road P.O. Box 240543 -� Charlotte, NC 26224-0543
Project Name:
PROPERPRIESERVATIVESindl ated?
c
a)
Phone: [phone] Fax: [phone] Short Hold Analysis: (Yes) (NO) UST Project: (Yes) (No)
.' :, . . - �I "I
-Fl eceivedWITHIN HOLG DINTIMES7:.
Client Company Name: C,,-I>L 04' 344,3i,,,fir *Please ATTACH any project specific reporting (QC LEVEL 111111
_c68t6by SEALS
Report To/Contact Na me: A n A y
provisions and/or QC Requirements
INTACT?
Reporting Address:
Invoice To:
'PROPER"CONTAINERS LIS'e' di.
Address:
Phone: 70 1 -'8'7 ?- -�3q 3 3' Fax gCeD (No): 70 Y- 97 9- MS
Purchase Order No./Billing Reference TO
BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date 0 1 Day 0 2 Days 0 3 Days C1 4 Days 0 5 Days
Certification: NELAC—USACE—FL—
INC
EDO Type: PDF_ Excel —Other "Working Days" EJ 6-9 Days 0 Standard 10 days ❑ Rush Work Must Be
Site Location Name: C%; T P Pre -Approved
Sc OTHER
NIA
Samples received after 15:00 will be processed next business day.
Site Location Physical Address:03 Bell/ Fall RA Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_, NO
S4J4e.5J,,4fie VC!
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
:S
TIVE
REMARKS
ID NO.
HOURS
SLUDGE)
SEE BELOW
3­,234-6
01: 1:5
S
P
A)
A
C-1 P4 IV
Z4
Sampler's Signature Sampled By (Print Name) a /(Jy ell Affiliation
Upon relinquishing, this Chain oMustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be qarges for any changes after analyses have* been initialized.
Relinquished By: (Signature) Re id By: (S(�natu D Military/Hours
Additional Comments:
_Y_
Reli,"hed By:, (Sig 3--, ReCle'lved By: (Signature) Date
Relihcru(sfied By: (Signaturd) Received Fcrrlsrn Laboraton'W By:, Date
0)hy
SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST COC rL RECEIVED AT THE LABORATORY.
0 Fed Ex El UPS C3 Hand -delivered I rism Field Service 0 Othe
NPDES: 1 UST: 1 GRObNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
0 NC 13 SC!, C] NC C1 SC ONC OSC 0 NC :1 SC 0 NC C, SC 00 NC 0 SCI Q NC
C3 SC 0 NC 0 SC C3 NC OSC
I
Q C1 D 0
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Site Arrival Time..
Ste Departure Time:
Field t6c'h F6 . Q:
-,Mileage:

®I Full -Service Analytical &
Environmental Solutions
LA6ORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. Case Narrative
SC Certification No. 990 99012
NC Drinking Water Cert No. 37735
VA Certification No.460211 - 04/21/2015
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Qtrly, Biweekly, 60Day 7 Fecal)
Lab Submittal Date: 04/06/2015
Prism Work Order: 5040074
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V L..
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A MB greater than one half of the RL, but it is less than 5% of the regulatory limit.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 -
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 Of 18

1 lIS �/' Fullironmee AnalyticalsEnvironmental SolutionsAoiiilP=s�a��.'LFBCfi RIE$INC. '
Sample Receipt Summary
04/21 /2015
Prism Work Order: 5040074
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Stal-ime (and Fecal 1)
5040074-01
Solid
04/06/15
04/06/15
Fecal #2
5040074-02
Solid
04/06/15
04/06/15
Fecal #3
5040074-03
Solid
04/06/15
04/06/15
Fecal #4
5040074-04
Solid
04/06/15
04/06/15
Fecal #5
5040074-05
Solid
04/06/15
04/06/15
Fecal #6
5040074-06
Solid
04/06/15
04/06/15
Fecal #7
5040074-07
Solid
04/06/15
04/06/15
Samples were received at 26.1 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 2 Of 18

Pia Laboratory Report
Full -Service Analytical
Environmental Solutions
04/21/2015
��-'�^i LA80ifATORIE$ ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Stal-ime (and Fecal 1)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 5040074-01
P.O. Box 1111 Prism Work Order: 5040074
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor .
DaterTime
ID
General Chemistry Parameters
Plant Available Nitrogen
710
mg/kg
160
13
2
*Calculation
4/10/15 7:49
CLB
[CALC]
Solids
69.3
% by
0.100
0.100
1
*SM2540 G
419115 17:10
MJo
P5D0127
Weight
Nitrate/Nitrite as N
10
mg/kg dry
7.2
0.79
1
*SM4500-NO3 F
418115 9:01
CLB
P5D0079
Phosphorus -Total
2000
mg/kg dry
72
19
20
*SM4500-P F
4/13/15 7:38
CLB
P5D0129
Total Kjeldahl Nitrogen
3300
mg/kg dry
720
61
2
*351.2
4110/15 7:49
CLB
P5D0109
Ammonia as N
180
mg/kg dry
7.2
1.6
1
*SM4500-NH3 G 4/9115 9:34
CLB
P5D0097
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
4/6/15 15:30
EGC
P5D0084
Total Metals
Mercury
0.13
mg/kg dry
0.029
0.0048
1
*7471B
4/13/15 12:23
JAB
P5D0150
SAR Soil Preparation
Complete
g
1
*2-78-054
4/9/15 9:05
JAB
P5D0123
SAR Percent Moisture
48.2
% by
0.100
0.100
1
*2-78-054
4/10/15 8:05
JAB
PSD0125
Weight
Arsenic
6.1
mg/kg dry
1.8
0.26
5
*6010C
4116/15 20:48
BGM
P5D0107
Sodium Absorption Ratio
0.89
[blank]
0.30
0.016
1
*2-78-054
4/20/15 15:46
BGM
P5D0124
Cadmium
BRL
mg/kg dry
1.8
0.25
5
*6010C
4/16/15 20:48
BGM
P5D0107
Calcium
2200
mg/L
1.0
0.085
10
*6010C
4/20/15 15:46
BGM
P5D0124
Copper
32 A
mg/kg dry
0.72
0.13
1
*6010C
4116/15 20:19
BGM
P5D0107
Lead
15
mg/kg dry
1.8
0.27
5
*6010C
4/16115 20:48
BGM
P5D0107
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010C
4/20/15 15:46
BGM
P5D0124
Nickel
200
mg/kg dry
7.2
0.93
5
*6010C
4/16115 20:48
BGM
P5D0107
Potassium
6000
mg/kg dry
90
5.7
5
*6010C
4116/15 20:48
BGM
P5D0107
Selenium
BRL
mg/kg dry
3.6
0.43
5
*6010C
4/16/15 20:48
BGM
P5D0107
Sodium
150
mg/L
5.0
0.074
10
*6010C
4/20/15 15:46
BGM
P5D0124
Sodium
810
mg/kg dry
90
18
5
*6010C
4/16/15 20:48
BGM
P5D0107
Zinc
71
mg/kg dry
18
4.0
5
*6010C
4/16/15 20:48
BGM
P5D0107
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 18

Laboratory Report
,,",® I S M Full -Service Analytical 8
'"'-� Environmental Solutions 04/21/2015
.:�i LABORATORIE41NG
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #2
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 5040074-02
P.O. Box 1111 Prism Work Order: 5040074
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Daterrime ID
General Chemistry Parameters
Solids 69.6 % by 0.100 0.100 1 'SM2540 G 4/9/15 17:10 NIJO P5D0127
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 4/6/15 15:30 EGC P5D0084
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 18

- P ISFull-Service Analytical � Environmental Solutions
---T'-' LABORATORIES INC
Laboratory Report
04/21 /2015
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #3
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 5040074-03
P.O. Box 1111 Prism Work Order: 5040074
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 68.4 % by 0.100 0.100 1 'SM2540 G 419115 17:10 MJO P5D0127
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 4/6/15 15:30 EGC P5D0084
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18

P`� ISM Full Service Analytical 6
®®® �, � Environmental Solutions
LABORATOME9, INC.
Laboratory Report
04/21 /2015
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #4 .
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 5040074-04
P.O. Box 1111 Prism Work Order: 5040074
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 70.6 % by 0.100 0.100 1 "SM2540 G 419/15 17:10 MJO P5D0127
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 4/6/15 15:30 EGC P5D0084
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 18

Laboratory Report
Full -Service
AsIRRISM
Analytical &
Environmental Solutions
04/21/2015
u UBOF-FES, ING
-
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Fecal #5
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 5040074-05
P.O. Box 1111
Prism Work Order: 5040074
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
69.3 % by
0.100 0.100
1 `SM2540 G 419/15 17:10 MJO
P5D0127
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 4/6/15 15:30 EGC
P5D0084
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 1

f I Full -Service Analytical & - Laboratory L®Iy Report
i I Environmental Solutions 04/21/2015
��.w'..$ ' LABORATORIES ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #6
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 5040074-06
P.O. Box 1111 Prism Work Order: 5040074
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
Solids 68.7 % by 0.100 0.100 1 *SM2540 G 419/15 17:10 MJO P5D0127
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 'SM9221 E 4/6115 15:30 EGC P5D0084
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 8 of 18

Laboratory Report
n Full -Service Analytical 8
p.1 V I I Environmental Solutions 04/21/2015
C£ LAaORATORIE$ ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #7
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 5040074-07
P.O. Box 1111 Prism Work Order: 5040074
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/06/15 00:00
Time Submitted: 04/06/15 13:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 69.8 % by 0.100 0.100 1 'SM2540 G 419115 17:10 MJO P5D0127
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 4/6/15 15:30 EGC P5D0084
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 -.Fax: [phone]
Page 9 of 18

PRISM Full -Service Analytical
Environmental Solutions
-60nA 0-r, I.Q.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch MOM - 3050B
Level II QC Report
4/21115'.
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 5040074
7 Fecal) Time Submitted: 4/6/2015 1:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank(P5DO107-BLK1)
Prepared:04/09/15 Analyzed: 04/16/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
9.65
0.50
mg/kg wet
A
Lead
0.385
0.25
mg/kg wet
BH
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
BH
LCS (P5D0107-BSI)
_
_
Prepared: 04/09/15 Analyzed: 04/16/15
Arsenic
24.6
0.25
mg/kg wet
25.00 98 80-120
Cadmium
24.0
0.25
mg/kg wet
25.00 96 80-120
Copper
28.5
0.50
mg/kg wet
25.00 114 80-120
Lead
24.2
0.25
mg/kg wet
25.00 97 80-120
Nickel
24.4
1.0
mg/kg wet
25.00 98 80-120
Potassium
510
12
mg/kg wet
500.0 102 80-120
Selenium
24.4
0.50
mg/kg wet
25.00 98 80-120
Sodium
536
12
mg/kg wet
500.0 107 80-120
Zinc
25.3
2.5
mg/kg wet
25.00 101 80-120
Matrix Spike (P5D0107-MS1)
Source: 5040074-01 _
Prepared: 04/09/15 Analyzed: 04/16/15
Arsenic
43.1
0.36
mglkg dry
36.08 6.07 103 75-125
Cadmium
26.6
0.36
mg/kg dry
36.08 0.664 72 75-125
MI
Copper
66.4
0.72
mg/kg dry
36.08 31.8 96 75-125
Lead
38.0
0.36
mg/kg dry
36.08 15.1 64 75-125
MI
Nickel
215
1.4
mg/kg dry
36.08 201 38 75-125
MC
Potassium
7540
18
mg/kg dry
721.5 6030 209 75-125
MC
Selenium
38.0
0.72
mg/kg dry
36.08 BRL 105 75-125
Sodium
1660
18
mg/kg dry
721.5 809 118 75-125
Zinc
111
3.6
mg/kg dry
36.08 70.7 111 75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 18
r

r
n q Full -Service Analytical
R I S
I ' V' Environmental Solutions
"�a UOORATONIE$ INC.
Level II QC Report
4/21 /15
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 5040074
Attn: Andy Smith 7 Fecal) Time Submitted: 4/6/2015 1:10:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P51010107 - 3050B
Matrix Spike Dup (P5D0107-MSD1)
Source: 5040074-01
Prepared: 04/09/15 Analyzed: 04/16/15
Arsenic
45.5
0.36
mg/kg dry
35.72 6.07 110
75-125
5
20
Cadmium
27.4
0.36
mg/kg dry
35.72 0.664 75
75-125
3
20
Copper
70.4
0.71
mg/kg dry
35.72 31.8 108
75-125
6
20
Lead
39.7
0.36
mg/kg dry
35.72 15.1 69
75-125
4
20
MI
Nickel
226
1.4
mg/kg dry
35.72 201 70
75-125
5
20
MI
Potassium
7790
18
mg/kg dry
714.4 6030 246 .
75-125
3
20
MC
Selenium
40.7
0.71
mg/kg dry
35.72 BRL 114
75-125
7
20
Sodium
1690
18
mg/kg dry
714.4 809 123
75-125
1
20
Zinc
117
3.6
mg/kg dry
35.72 70.7 131
75-125
6
20
MI
Post Spike (P5D0107-PS1)
_Source:
5040074-01
Prepared: 04/09/15 Analyzed: 04/16/15
Arsenic
1.23
mg/L
1.000 0.168 107
80-120
Cadmium
0.760
mg/L
1.000 0.0184 74
80-120
MI
Copper
1.93
mg/L
1.000 0.882 105
80-120
Lead
1.09
mg/L
1.000 0.418 67
80-120
MI
Nickel
5.99
mg/L
1.000 5.57 42
80-120
MC
Potassium
204
mg/L
20.00 167 184
80-120
MC
Selenium
1.13
mg/L
1.000 -0.480 113
80-120
Sodium
46.3
mg/L
20.00 22.4 119
80-120
Zinc
3.10
mg/L
1.000 1.96 114
80-120
Batch P5D0123 - SAR 2-78-054
Blank (P5D0123-BL_K1) _
Prepared & Analyzed: 04/09/15
SAR Soil Preparation
Complete
g
This report should not be reproduced, except in its entirety, without the written consent of Prism. Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 18

Level II QC Report
R I S M I Full -Service Analytical
5� 0.-, environmental solutionss
4/21/15
IABORATORIE$ INC.
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 5040074
Attn: Andy Smith 7 Fecal) Time Submitted: 4/6/2015 1:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units Level Result %REC Limits RPD Limit Notes
Batch P5D0124 - 3010A
Blank (P5DO124-BLK1)
Prepared: 04/10/15 Analyzed_: 04/20/15 _
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
Batch P5D0125 - NO PREP
Blank (P5D0125_BLK1) Prepared & Analyzed: 04/10/15
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (P5D0125-DUP1) Source: 5040074-01 Prepared & Analyzed: 04/10/15
SAR Percent Moisture 48.6 0.100 % by Weight 48.2
Batch P5D0150 - 7471 B
Blank (P5D0150-BLK1) _ Prepared &Analyzed: 04/13/15
Mercury BRL 0.020 mg/kg wet
LCS (P5D0150-_B_S1) _ __ _ _ Prepared & Analyzed: 04/13/15
Mercury 0.424 0.020 mg/kg wet 0,4167 102
0
-9 ---200 -- --
80-120 - -
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-6543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 11 $

Full -Service Analytical 8 Level II QC Report
4/21/15
Environmental Solutions
- � n�..,L��LA60PATORIE$ INC. ,
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P5130079 - NO PREP
Project: StaLirrte (Qtrly, BiWeekly, 60Day Prism Work Order: 5040074
7 Fecal) Time Submitted: 4/6/2015 1:10:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P5D0079-BLK1) _ Prepared & Analyzed: 04/08/15
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P5D0079-BS1) Prepared & Analyzed_ 04/08/15 —
Nitrate/Nitrite as N 50.5 5.0 mg/kg wet 50.00 101 80-120
Matrix Spike (P5D0079-MS1) — Source: 5040074-01 Prepared & Analyzed: 04108/15
Nitrate/Nitrite as N 71.6 7.2 mg/kg dry 72.15 10.2 85 80-120
Matrix Spike Dup (P5D0079-MSD1) Source: 5040074-01 Prepared & Analyzed: 04/08/15
Nitrate/Nitrite as N 71.8 7.2 mg/kg dry 72.15 10.2 85 80-120 0.3 20
Batch P5130097 - NO PREP
Blank (P5D0097-BLK1) Prepared & Analyzed: 04/09/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (P5D0097_BS1) — Prepared & Analyzed: 04/09/15
Ammonia as N 123 5.0 mg/kg wet 125.0 98 80-120
Matrix Spike (P5D0097-MS1) — _Source: 5040074-001 Prepared & Analyzed: 04/09/15
Ammonia as N 381 7.2 mg/kg dry 180.4 175 114 80-120
Matrix Spike Dup (P5D0097-MSD1) Source: 5040074-01 Prepared & Analyzed: 04/09/15
Ammonia as N 388 7.2 mg/kg dry 180.4 175 118 80-120 2 20 '
Batch P5D0109 - 351.2
Blank (P5D0109-BLK1) - Prepared: 0_4/09/15 Analyzed: 0.4_/10/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 Of 18

,� B fl Level II QC Report
V I Full -Service Analytical 8
"'"" Environmental Solutions 4/21/15
• ' LABORATORIES INa
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P5DO109 - 351.2
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 5040074
7 Fecal) Time Submitted: 4/6/2015 1:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P5DO109-BS1) _ _ _ _ _ Prepared: 04/09/15 Analyzed: 04/10/15
Total Kjeldahl Nitrogen 505 100 mg/kg wet 500.0 101 90-110
Matrix Spike (P5D0109-MS1) _ Source: 5040074-001 Prepared_04109/15 Analyzed: 04/10/15
Total Kjeldahl Nitrogen 10900 1800 mg/kg dry 7215 3260 106 90-110
Matrix Spike Dup (P5D0109-MSD1) _ Source: 5040074-01 Prepared: 04/09/15 Analyzed: 04/10/15
Total Kjeldahl Nitrogen 13300 1800 mg/kg dry 7215 3260 139 90-110 19 20 MI
Batch P5DO127 -Solids, Dry Weight
Blank (P5DO127-BLK1) Prepared & Analyzed: 04/09/15
B/ Solids 100 0.100 % by Weight
Batch P5DO129 - SM4500-PB5
Blank (P5D0129-BLK1) _ Prepared_ 04/10/15 Analyzed: 04/13/15
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P5D0129-BS1)� _ Prepared: 04/10/15 Analyzed: 04/13/15
Phosphorus -Total 98.4 2.5 mg/kg wet 100.0 98 90-110
Matrix Spike (P5D0129-MS1) _ _ Source: 5040074-01 _ Prepared: 04/10/15 Analyzed: 04/13/15
Phosphorus -Total 2010 72 mg/kg dry 144.3 1990 9 80-120 MC
Matrix Spike Dup (P5D0129-MSD1) _ Source: 50400.74-01 Prepared_ 04/10/15 Analyzed: 04/13/15
Phosphorus -Total 2070 72 mg/kg dry 144.3 1990 52 80-120 3 20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-636 4 - Fax: [phone] Page 14of 18

Level II QC Report
wG eee
�-R I S y` ,p
s _ , ' V'
Full -Service Analytical
Environmental Solutionss
4/21/15
a F' LABORATORIES INC.
City of Statesville, NC
Project: StaLime (Qtrly, Biweekly,
60Day Prism Work Order: 5040074
Attn: Andy Smith
7 Fecal)
Time Submitted: 4/6/2015
1:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality
Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD
Limit Notes
Batch P5D0084 - NO PREP
Blank (P5DO084-BLK1)
_
Prepared & Analyzed: 04/06/15
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0109
0.05 g
25 mL
04/09/15 12:30
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0129
1 g
50 mL
04/10/15 11:15
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0127
30 g
30 g
04/09/15 17:10
5040074-02
P5D0127
30 g
30 g
04/09/15 17:10
5040074-03
P5D0127
30 g
30 g
04/09/15 17:10
5040074-04
P5D0127
30 g
30 g
04/09/15 17:10
5040074-05
P5D0127
30 g
30 g
04/09/15 17:10
5040074-06
P5D0127
30 g
30 g
04/09/15 17:10
5040074-07
P5D0127
30 g
30 g
04/09/15 17:10
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0124
50 mL
50 mL
04/10/15 9:16
5040074-01
PSD0124
50 mL
50 mL
04/10/15 9:16
5040074-01
P5D0124
50 mL
50 mL
04/10/15 9:16
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0107
2.01 g
50 mL
04/09/15 8:30
5040074-01
P5D0107
2.01 g
50 mL
04/09/15 8:30
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0150
0.59 g
50 mL
04/13/15 9:00
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
5040074-01
P5D0123
250 g
250 g
04/09/15 9:05
This report should
not be reproduced,
except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 15 of 18

Pull -Service Analytical &
y Environmental Solutions
R ISM
�''r r IASORATORI[S, INC.
449 Springbrook Road • Charlotte, NC 28297
Phone [phone] Fax: [phone]
Client Company Name:
Report To/Contact Name:
Reporting Address:
CHAIN OF CUSTODY RECORD
PAGE OF�) :.QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL I If III IV)
provisions and/or QC Requirements
Invoice To:
Address:
YES
NO , :.N/A i
0�0
Samples INTACT upon arrival?
o
Received ON WET ICE?
—f '"
✓_ '
CD
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
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PROPER CONTAINERS used?
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Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoD
FL NC
EDD Type: PDF_Excel_Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushWork dust Be
SC OTHER
N/A
Site Location Name:
Samples received after 14:00 will be processed next business day.
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
TIME
COLLECTED
MATRIX
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
\
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DATE
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Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
e
submitted in writing to the Prism Project Manager. There
will be rh rges for any changes after analyses have been initialized.
Relinquished By: (Signature)
Recely By: (Sign Date Military/Hours Additional Comments:
Site Arrival Time:
Relin w- ed By: (Sign r)
R d By: (Signs Date
Site Departure Time:
Relirrqu' ted By:"(Signa
Received ForPkn Laboraattpos y: Dat/q/
Field Tech Fee:
Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH STODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED
AGAINST COC, NTIL RECEIVED AT THE LABORATORY.
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ElFed Ex ❑ UPS ❑ Hand -delivered rism Field Service ❑ OtherJ'0 0,9 -
NPDES: UST: G OUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC
El SC ❑NC ❑SC ❑NC❑SC ❑NC El SC ❑NC ❑SC 1 ❑NC ❑SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

CHAIN F CUSTODY RECORD
IR ISM
EnviFull-ronmental
lSolutions
Analytical &
Environmental Solutions PAGE OF QUOTE # TO ENSURE PROPER BILLING:
LAeoRwoptirsjmc
•149 Springbrook Road - Charlotte, NC 28217 Project Name:
Phone [phone]C364 - Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
l� Ld" *Please ATTACH any project specific reporting (QC LEVEL 1 it III IV)
Client Company Name: —' " r.�tiLCs' provisions and/or QC Requirements
Report To/Contact Name: Invoice To:
Reporting Address: Address: _
�._..
YES ` NO
N/A _
00
Samples INTACT upon arrival'?
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Received ON WET ICE?,
PROPER PRESERVATIVES: indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACF?
__ __
✓,
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VOLATILES rec'd'W/OUT HF_ADSPACE?
PROPER CONTAINERS used?
l'EMP Therm ID: / T_�,�. Observed. ` 7- °C / Corg 1!`°C
Phone: Fax (Yes) (No): Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
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FL NC
EDD Type: PDF_Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
Sc OTHER
N/A
Site Location Name: Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
Site Location Physical Address:
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES
p p
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
-
TIME MATRIX SAMPLE CONTAINER Q
ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA-
'TYPE TIVES
�� / REMARKS
LAB
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NO. SIZE
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submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Refn shed By: (Signature) Ric 've By: (Signature) �( �. Date
Military/Hours Additional Comments:
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Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG L f#IL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered PPrism Field Service ❑ Other
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OF CUSTODY RECORD
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Full. -Service Analytical &
� Environmental Solutions
,
�. OF � OUOTE # TO ENSURE PROPER BILLING:
-_ �7'•-G YFy,S NO-
Samples INTACT upon arrival? '
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S INC.
PAGE
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Received ON WET ICES Temp (? ( y _
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449 SpI ingbrook goad • P.O. Box 240543 - Charlotte, NC 28224-0543
Pro Project Name:
9
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
PROPER PRESERVATIVES mdlcated? �
— tU
rn
Phonc:704/529-6364 Fax: [phone]
*Please ATTACH any project specific reporting (QC LEVEL 1 II lit 1V0
Rived WITHIN HOLDING TIMES?
Client Company Name: � Ii
provisions and/or QC Requirements
CUSTODY SEALS INTACT'?,
Report To/Contact Nam
Invoice To:
VOLATILE& rec d W/OUT HEADSPACE?
_
(Reporting Address:
Address:
PROPER. CONTAINERS used?.. —
Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL
NC_
EDD Type- PDF_ Excel _Other
"Working Days" ❑ 6-9 Days ❑Standard 10 days p Rush Work Must Be
Pre -Approved
SC OTHER N/A
Site Location Name:
Samples received after 15:00 will be processed next business day.
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES _ NO _
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSES REQUESTED
PRISM
LAB
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
MILITARY
WATER OR
*TYPE
TIVES
, /
/-�)� / / REMARKS
ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE r ZL / / .�+✓/ �'
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Sampler's Signature / . '' Sampled By (Print Name) �� �t�' d' C Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Recelv B Si not Dale Military/Hours
Relin ulshAed�.By: (ySglgny/a11Fy1re/) v� (s r f e\f Additional Comments:
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SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CrNTIL
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b O U -T4
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t�' sm Field Service O Other
DRINKNG
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❑ NCF❑ SC
p NC ❑ S�
O
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass
P = Plastic; TL = Teflon -Lined Cap VOA =Volatile Organics
Analysis (Zero Head Space)

�Full -Service Analytical &
"R M I Environmental Solutions
ORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 04/20/2015
Prism Work Order: 5040349
Case Narrative
04/28/2015
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods. `,
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BL MB greater than one half of the RL, but the sample concentrations are less than the-RL. -
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 Of 9

Sample Receipt Summary
®I I Fulli Serviceal Solutions
s
n Environmental Solutions 04/28/2015
-., LABORATORIES. INC.
Prism Work Order: 5040349
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime 5040349-01 Solid 04/20/15 04/20/15
Samples were received in good condition at 2.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 9

I Laboratory Report
Full -Service Analytical 8
Environmental Solutions 04/28/2015
' LABORATORIEs G
City of Statesville, NC Project: StaLime Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 5040349-01
P.O. Box 1111 Prism Work Order: 5040349
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/20/15 11:05
Time Submitted: 04/20/15 12:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
350
mg/kg
160
13
2
*Calculation
4127115 8:43
CLB
[CALC]
Solids
79.9
% by
0.100
0.100
1
*SM2540 G
4123115 16:25
MJO
P5D0367
Weight
Nitrate/Nitrite as N
11
mg/kg dry
6.3
0.69
1
*SM4500-NO3 F
4/23115 10:18
CLB
P5D0348
Phosphorus -Total
1600
mg/kg dry
63
16
20
*SM4500-P F
4122115 11:29
CLB
P5D0295
Total Kjeldahl Nitrogen
1400
mg/kg dry
630
53
2
*351.2
4127/15 8:43
CLB
P5D0365
Ammonia as N
110
mg/kg dry
6.3
1.4
1
*SM4500-NH3 G
4/24115 7:53
CLB
PSD0356
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
4/20/15 14:07
EGC
P5D0334
Total Metals
Mercury
0.074
mg/kg dry
0.025
0.0042
1
*7471B
4122/15 15:01
JAB
P5130317
SAR Soil Preparation
Complete
g
1
*2-78-054
4/22/15 7:40
JAB
P5D0340
Arsenic
4.6
mg/kg dry
3.2
0.45
10
*6010C
4/24115 22:53
BGM
P5D0322
Sodium Absorption Ratio
0.62
[blank]
0.30
0.016
1
*2-78-054
4/24115 21:03
BGM
P5D0359
Cadmium
BRL
mg/kg dry
3.2
0.45
10
*6010C
4124115 22:53
BGM
P5D0322
Calcium
1200
mg/L
1.0
0.085
10
*6010C
4/24/15 21:03
BGM
P5D0359
Copper
21 BH
mg/kg dry
6.3
1.2
10
*6010C
4/24/15 22:53
BGM
P5D0322
Lead
16
mg/kg dry
3.2
0.48
10
*6010C
4124/15 22:53
BGM
P5b0322
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010C
4/24/15 21:03
BGM
P5D0359
Nickel
160
mg/kg dry
13
1.6
10
*6010C
4/24/15 22:53
BGM
P5130322
Potassium
3900
mg/kg dry
160
10
10
*6010C
4/24/15 22:53
BGM
P5D0322
Selenium
BRL
mg/kg dry
6.3
0.76
10
*6010C
4/24/15 22:53
BGM
P5D0322
Sodium
560
mg/kg dry
160
31
10
*6010C
4124/15 22:53
BGM
P5D0322
Sodium
79
mg/L
5.0
0.074
10
*6010C
4/24/15 21:03
BGM
P5130359
Zinc
96
mg/kg dry
32
7.0
10
*6010C
4/24115 22:53
BGM
P5D0322
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 9

"R I S n n Full -Service Analytical &
v Environmental Solutions
"BORATORIE$INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
4/28/15
Prism Work Order: 5040349
Time Submitted: 4/20/2015 12:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5D0317.- 7471 B
Blank (P5D0317-BLK1) _ Prepared & Analyzed: 04/22/15
Mercury BRL 0,020 mg/kg wet
LCS (P5D0317-BSI) Prepared &Analyzed: 04/22/15
Mercury 0.389 0.020 mg/kg wet 0,4167 93 80-120
Batch P5130322 - 3050B
Blank (P5D0322-BLK1)
_
Prepared: 04/22/15 Analyzed: 04/24/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
0.995
0.50
mg/kg wet
BH, BL
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P5D0322-BS1)
_ _
Prepared: 04/22/15 Analyzed: 04/24/15
Arsenic
23.4
0.25
mg/kg wet
25.00 94 80-120
Cadmium
23.6
0.25
mg/kg wet
25.00 94 80-120
Copper
27.9
0.50
mg/kg wet
25.00 111 80-120
Lead
23.6
0.25
mg/kg wet
25.00 95 80-120
Nickel
23.6
1.0
mg/kg wet
25.00 94 80-120
Potassium
484
12
mg/kg wet
500.0 97 80-120
Selenium
22.8
0.50
mg/kg wet
25.00 91 80-120
Sodium
490
12
mg/kg wet
500.0 98 80-120
Zinc
25.0
2.5
mg/kg wet
25.00 100 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 9

.� Full -Service Analytical 8
ISM I
Environmental Solutions
.Sww.�. LABOflA 16fl INC.
City of Statesville, NC Project: StaLir-he
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
4/28/15
Prism Work Order: 5040349
Time Submitted: 4/20/2015 12:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5DO340 - SAR 2-78-054
Blank (P5D0340-BLK1) Prepared &Analyzed: 04/22/15
SAR Soil Preparation 0.00 g
Batch P5DO359 - 301 OA
Blank (P5D0359-BLK1)
Prepared: 04/23/15 Analyzed: 04/24/15
Sodium Absorption Ratio
BRL 3.0 [blank]
Calcium
BRL 1.0 mg/L
Magnesium
BRL 1.0 mg/L
Sodium
BRL 5.0 mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone:[phone]-Toll Free Number: 1-800/529-6364- Fax: [phone] Page 5 Of 9

R I S n %� Full -Service al Solutions
8
1 v' Environmental Solutions
."PRISM
LAOOflATORIE$ INO
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P5DO295 - SM4500-PB5
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
4/28/15
Prism Work Order: 5040349
Time Submitted: 4/20/2015 12:10:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P5D0295-BLK1) Prepared: 04/21/15 Analyzed: 04/22/15
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P5D0295-BS1) Prepared: 04/21/15 Analyzed: 04/22/15
Phosphorus -Total 104 2.5 mg/kg wet 100.0 104 90-110
Matrix Spike (P5D0295-MS1) Source: 5040349-01 Prepared: 04/21/15 Analyzed: 04/22/15
Phosphorus -Total 1870 63 mg/kg dry 125.2 1610 210 80-120 MC
Matrix Spike Dup (P5DO295-MSD1) Source: 5040349-01 Prepared: 04/21/15 Analyzed: 04/22/15
Phosphorus -Total 1830 63 mg/kg dry 125.2 1610 179 80-120 2 20 MC
Batch P5130348 - NO PREP
Blank (P5DO348-BLK1
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
& Analvzed: 04/23/15
LCS (P5DO348-BS1) Prepared & Analyzed: 04/23/15
Nitrate/Nitrite as N 49.2 5.0 mg/kg wet 50.00 98 80-120
Batch P5DO356 - NO PREP
Blank (P5D0356-BLK1) _ _ Prepared: 04/23/15 Analyzed: 04/24/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (P5D0356-BS1)_ Prepared: 04/23/15 Analyzed: 04/24/15
Ammonia as N 119 5.0 mg/kg wet 125.0 95 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 9

' S M Full -Service Analytical 8
Environmental Solutions
L 90RATORIEC INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P5130356.- NO PREP
Project: Stal-ime
Level II QC Report
4/28/15
Prism Work Order: 5040349
Time Submitted: 4/20/2015 12:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike (P5D0356-MS1) Source: 5040349-01 Prepared: 04/23/15 Analyzed: 04/24/15
Ammonia as N 250 13 mg/kg dry 156.4 110 89 80-120
Matrix Spike Dup (P5D0356-MSD1) Source: 5040349-01 Prepared: 04/23/15 Analyzed: 04/24/15
Ammonia as N 255 13 mg/kg dry 156.4 110 92 80-120 2 20
h P5D0365 - 351.2
Blank (P5D0365-BLK1) Prepared: 04/23/15 Analyzed: 04/27/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P5D0365-BS1) Prepared: 04/23/15 Analyzed: 04/27/15
Total Kjeldahl Nitrogen 485 100 mg/kg wet 500.0 97 90-110
Matrix Spike (P5D0365-MS1) Source: 5040349-01 Prepared: 04/23/15 Analyzed: 04/27/15
Total Kjeldahl Nitrogen 7680 1600 mg/kg dry 6258 1360 101 90-110
Matrix Spike Dup (P5DO365-MSD1) Source: 5040349-01 Prepared: 04/23/15 Analyzed: 04/27/15
Total Kjeldahl Nitrogen 7320 1600 mg/kg dry 6258 1360 95 90-110 5 20
Batch P5DO367 - Solids. Dry We
Blank (P5DO367-BLK1) Prepared &Analyzed: 04/23/15
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page

Level II QC Report
77��11 1� ®®®
PRIS„,p
Analyticals
4/28115
'v'
Environmental
Environmental Solutions
I.ABON RlE$ INC.
City of Statesville, NC
Project:
StaLime
Prism Work Order: 5040349
Attn: Andy Smith
Time Submitted: 4/20/2015 12:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P5DO334 - NO PREP
Blank (P5D0334-BLK1)
Prepared & Analyzed: 04/20/15
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample
Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/rime
5040349-01
P5D0365
0.05 g
25 mL
04/23/15 11:45
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
5040349-01
P5D0295
1 g
50 mL
04/21/15 11:42
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
5040349-01
P5D0367
30 g
30 g
04/23/15 16:25
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Datemme
5040349-01
P5D0359
50 mL
50 mL
04/23/15 12:00
5040349-01
P5D0359
50 mL
50 mL
04/23/15 12:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Daterrime
5040349-01
P51D0322
1.98 g
50 mL
04/22/15 9:20
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateTme
5040349-01
P5D0317
0.59 g
50 mL
04/22/15 8:55
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
5040349-01
P5D0340
250 g
250 g
04/22/15 7:40
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CHAIN OF CUSTODY RECORD
e
Full -Service Analytical &
rELI
YES NO
N/A'
rn
'A
Environmental Solutions
PAGE_ OF _ ¢SUOTE # TO ENSURE PROPER BILLING:
SarnpleS INTACT upon arrival?
�,.
o
>i12 a j . rra.: LABORATORIES. ova
Project Name:
Received ON WET ICE?
449 7brook Road •Charlotte, NC
Phone [phone] •Fax: [phone]
Short Hold Analysis: (Yes) (No) USTProject: (Yes) (NO)
PROPER PRESERVATIVES indicated?
IT
C+
r /0
S✓� �!(.'
* Please ATTACH any project specific reporting (QC LEVEL I II 111 IV)
Received WITHIN HOLDING TIMES?
r
M
�
Client Company Name: ti<�
ofiE�iE
provisions and/or QC Requirements
CUSTODY SEALS INTACT?
Report To/Contact Name:
A N ,3t i/ Skn - g h
Invoice To:
VOLATILE& rec'd VV/OUT HEADSPACE?
Reporting Address:
Address:
PROPER CONTAINERS used?
TEMP; Therm IO Observed
1 1 °C /Corr:-'
- °c
Phone:`70'd-dT1B- 3`%•3 Y Fax es (No):70- 37F- 3155 Purchase Order No./Billing Reference
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
EDD Type: PDF_Excel_Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Pre -Approved Work Must Be
Site Location Name: ra u r+k C%`C<' fK W LO I Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 46 93 13e,11 ra 1-m tZ Turnaround time is based on business days, excluding weekends and holidays.
J r f (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
i a`.'QG'S(✓/ �/ 4° RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC DOD FL NC
SC OTHER NIA
Water Chlorinated: YES_ NO_
Sample Iced Upon Collection: YES NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSIS REQUESTED
\ \5 REMARKS
r
/ try
PRISM
LAB
ID NO.
*TYPE
SEE BELOW
NO.
SIZE
As
PA
��—C�,��
P
�a�
Cod
C
SA
Fib
N
N o'
z�J
Sampler's Signature /t GC�
Sampled By (Print Name) Gi., r r t K
Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proc ed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges f n hanges after analyses have been initialized.
i0
Site Arrival Tune -
Relin fished By: (Signature) /
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Rec ' y: (Sign e)
�'��
Date
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Orel'' i j�
Military/Hours
1
Additional Comments:
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Relin hed By: (Signature)
Rec ved By: (SI ature)
I
Date
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elingyishetf'By: ( gnature) i .,-
Received For in Labors s B ''ram
D to
Mileage;
Method of Shipr}fent: NOTE: L SAMPLE COOLERS SHOULD BE TAPED SHUT WITH STODY SEALS FOR TRANSPOR Ar TO THE LABORATORY.
SAMPL S ARE NOT ACCEPTED AND VERIFIED AGAINST COX NTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered rism Field Service ❑ Other
COC Group No.
^
Ji
. ✓ q
NPDES: UST: GRODNUWAItK: UKINKING WAfEK: SC)LIU WASTE: RGKA: GEKGLA LANDFILL OINER:
❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402
SC Certification No. 99012 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735. 05/12/2015
e1 jReI S M 1. Environmental Solutions VA Certification No. 460211
®'LABORATORIES, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307 .
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 05/05/2015
Statesville, NC 28687 Prism Work Order: 5050050
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V L-
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
IH Internal standard response below the QC limit. Analyte reported with possible high bias.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
-This This report should not be reproduced, except in it entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704/52"409
Page 1:& 9

q�k
NMIFull -Service Analytical &
IRRISM I Environmental Solutions
�'S 'u TDIIJES6 INC
Sample Receipt Summary
05/12/2015
Prism Work Order: 5050050
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 5050050-01 Solid 05/04/15 05/05/15
Samples were received at 16.5 degrees C. See case narrative for further information.
report should not ­.bp repr9clucedf except, injts,enti�rety,, without the.written consent of Prism�Laboratories;Jnci
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Laboratory Report'
❑❑� �:� Full -Service Analyticaf8
I S M I
1mll Environmental Solutions
05/12/2015
�lABO{NTOnIES ING
'
City of Statesville, NC Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 5050050-01
P.O. Box 1111
Prism Work Order: 5050050
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 05/04/15 10:00
Time Submitted: 05/05/15 08:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Dateffime
ID
General Chemistry Parameters
Plant Available Nitrogen
BRL
mg/kg
780
68
20
*Calculation
5/11/15 12:29
CLB
[CALCI
% Solids
75.2
% by
0.100
0.100
1
*SM2540 G
516/15 15:46
ARC
P5E0115
Weight
Nitrate/Nitrite as N
11
mglkg dry
6.7
0.73
1
*SM4500-NO3 F 518115 9:45
CLB
PSE0164
Total Kjeldahl Nitrogen
3300
mglkg dry
3300
280
10
*351.2
SM1/15 12:29
CLB
OSE0132
Ammonia as N
420
mglkg dry
130
30
20
*SM4500-NH3 G 5/7MS 7:43
CLB
PSE0102
Microbiological Parameters
Fecal Colifomts
BRL
MPN/g dry
0.3
1
*SM9221E
5/5/15 9:41
EGC
P5EO105
Total Metals
Mercury
0.076
mglkg dry
0.028
0.0046
1
*7471B
5/7115 14:04
JAB
P5E0136
SAR Soil Preparation
Complete
g
1
*2-78-054
5/11/15 14:44
BGM
P5EO145
SAR Percent Moisture
62.6
% by
0.100
0.100
1
*2-78-054
5/8115 8:55
JAB
P5E0193
Weight
Arsenic
7.7 IH
mglkg dry
0.34
0.048
1
*6010C
5r7M5 18:24
BGM
PSE0125
Sodium Absorption Ratio
0.66
[blank]
0.30
0.016
1
*2-78-054
5/8115 21:08
BGM
PSE0167
Cadmium
0.45 IH
mglkg dry
0.34
0.048
1
*6010C
5/7/15 18:24
BGM
PSE0725
Calcium
1800
mg/L
1.0
0.085
10
*6010C
518/15 21:08
BGM
PSE0167
Copper
50 BH
mglkg dry
0.67
0.12
1
*601OC
517/15 18:24
BGM
'PSE0125
Lead
37 IH
mglkg dry
0.34
0.051
1
*601OC
517115 18:24
BGM
P5E0125
Magnesium
BRL
mg/L
1.0
0.0070
10
*601OC
5/8/15 21:08
BGM
P5EO167
Nickel
170 IH
mg/kg dry
1.3
0.17
1
*6010C
517115 18:24
BGM
PSE0125
Selenium
2.6 IH
mglkg dry
0.67
0.081
1
*6010C
5/7/15 18:24
BGM
PSE0125
Sodium
100
mg/L
5.0
0.074
10
*6010C
5/8115 21:08
BGM
P5E0167
Zinc
96 IH
mg/kg dry
3.4
0.74
1
*601OC
517115 18:24
BGM
PSE0125
p y t be,reproduced, except.in,tts, entirety, without,the written co{Isent of Prism.Labaratories
his re ortshould no
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
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"- Level II QC Repgrt---
IC I� /I Fulllronmee Analytical s-5112/T5
`J � �/ � Environmental Solutions
'�usonAroniea wa
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P5E0125 - 3050B
Project: StaLime
Prism Work Order: 5050050
Time Submitted: 5/5/2015 8:15:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P5E0125-BLK1)
Prepared & Analyzed: 05/07/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
1.60
0.50
mg/kg wet
B. BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P5E0125-13SI)
Prepared & Analyzed: 05/07/15
Arsenic
24.3
0.25
mg/kg wet
25.00 97
80-120
Cadmium
24.6
0.25
mg/kg wet
25.00 98
80-120
Copper
27.1
0.50
mg/kg wet
25.00 108
80-120
Lead
24.4
0.25
mg/kg wet
25.00 98
80-120
Nickel
24.8
1.0
mg/kg wet
25.00 99
80-120
Selenium
23.6
0.50
mg/kg wet
25.00 94
80-120
Zinc
24.8
2.5
mg/kg wet
25.00 99
80-120
P5E0136 - 7471 B
Blank (P5E0136-BLK1) Prepared & Analyzed: 05/07/15
Mercury BRL 0.020 mg/kg wet
LCS (P5E0136-BSI) Prepared & Analyzed: 05/07/15
Mercury 0.447 0.020 mg/kg wet 0.4167 107 80-120
Batch P5E0145 - SAR 2-78-054
Blank(P5E0145-BLK1) -Prepared: 05/07/15 Analyzed:05/11/15
SAR Soil Preparation Complete g
This, report should not be reproduced,. except in its entirety, without the. written consent of Prism Laboratories Inc.
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Level II QC Report
Full -Service Analytical &
NP a, ISM Environmental Solutions 5/12/15
Aid' IES, INC
City of Statesville, NC Project: StaLime Prism Work Order: 5050050
Attn: Andy Smith Time Submitted: 5/5/2015 8:15:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5E0167 - 301 OA
Blank (P5E0167-BLK1)
Prepared & Analyzed: 05/08/15
Sodium Absorption Ratio
BRL
3.0 [blank]
Calcium
BRL
1.0 mg/L
Magnesium
BRL
1.0 mg/L
Sodium
BRL
5.0 mg/L
Batch P5EO193 - NO PREP
Blank (P5E0193-BLK1)
Prepared & Analyzed: 05/08/15
SAR Percent Moisture
BRL
0.100 % by Weight
Duplicate (P5E0193-DUP1)
Source: 5050050-01 Prepared & Analyzed: 05/08/15
SAR Percent Moisture
60.6
0.100 % by Weight 62.6 3 200
This report,should not.be reproduced„except in its ,entirety„without the,.written consent of. Prism Laboratories,, Inc
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-ReportLevel 11 QC
�? Full -Service Analytical & - s
O a'E ISM I Environmental solutions
A& 5/12/15-
MML MRTEa wa
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 5050050
Time Submitted: 5/5/2015 8:15:00AM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5E0102 - NO PREP
Blank (P5E0102-BLK1) Prepared: 05/06/15 Analyzed: 05/07/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (P5E0102-BSI) Prepared:,05/06/15 Analyzed: 05/07/15
Ammonia as N 130 5.0 mg/kg wet 125.0 104 80-120
Matrix Spike (P5E0102-MS1) Source: 5050050-01 Prepared: 05/06/15 Analyzed: 05/07/15
Ammonia as N 426 130 mg/kg dry 166.3 420 3 80-120 MI
Matrix Spike Dup (P5E0102-MSD1) Source: 5060050-01 Prepared: 05/06/15 Analyzed: 05/07/15
Ammonia as N 431 130 mg/kg dry 166.3 420 6 80-120 1 20 MI
Batch P5E0115 - Solids, Dry Weight
Blank (P5E0115-BLK1) Prepared & Analyzed: 05/06/15
% Solids 100 0.100 % by Weight
Batch P5E0132 - 351.2
Blank (P5E0132-BLK1) Prepared: 05/07/15 Analyzed: 05/11/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P5E0132-BS1) Prepared: 05/07/15 Analyzed: 05/11/15
Total Kjeldahl Nitrogen 513 100 mg/kg wet 500.0 103 90-110
Matrix Spike (P5E0132-MS1) Source: 5050050-01 Prepared: 05/07/15 Analyzed: 05/11/15
Total Kjeldahl Nitrogen 11500 6700 mg/kg dry 6653 3300 123 90-110 MI
This reportshould not be reproduced, except in.its entirety, without the.written consent of.Prism,L boratories, Inc._ ,
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Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 P.ag e.: 6 ' of 9

asap:.. Full -Service Analytical &
PR' S M I Environmental Solutions
V'LAOORATORIF$ INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P5E0132 - 351.2
Reporting
Result Limit Units
Level II QC Report
5/12/15
Prism Work Order: 5050050
Time Submitted: 5/5/2015 8:15:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P5E0132-MSD1) Source: 5050050-01 Prepared: 05/07/15 Analyzed: 05/11/15
Total Kjeldahl Nitrogen 11700 6700 mg/kg dry 6653 3300 127 90-110 2 20 MI
Batch P5EO154 - NO PREP
Blank (P5E0154-BLK1) Prepared & Analyzed: 05/08/15
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P5EO154-BS1) Prepared & Analyzed: 05/08/15
Nitrate/Nitrite as N 51.0 5.0 mg/kg wet 50.00 102 80-120
This report should not be reproduced except in its entirety, without the written consent of Prism Laboratories Inc
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364- Fax: 704/52"409 Page 7 of 9

Full -Service Analytical &
AMR ISM I Environmental Solutions
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level•II•QG Report• ',
5/1-2/15—. '
Prism Work Order: 5050050
Time Submitted: 5/5/2015 8:15:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes .
Batch P5EO105 - NO PREP
Blank (P5E0105-BLK1) Prepared &Analyzed: 05/05/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2'
Lab Number Batch Initial Final Date/Time
5050050-01 P5E0132 0.05 g 25 mL 05/07/15 11:30
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final DateTme
5050050-01 P5E0115 30 g 30 g 05/06/15 15:46
Prep Method: 3010A
Lab Number
Batch
Initial
Final
DateTme
5050050-01
P5E0167
50 mL
50 mL
05/08/15 10:00
5050050-01
P5E0167
50 mL
50 mL
05/08/15 10:06
Prep Method: 3050B
Lab Number
Batch
Initial
Final
DateTme
5050050-01
P5E0125
1.98 g
50 mL
05/07/15 8:05
Prep Method: 7471E
Lab Number
Batch
Initial
Final
DateTme
5050050-01 P5E0136 0.57 g 50 mL 05/07/15 11:00
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final DateTme
5050050-01 P5E0145 250 g 250 g 05/07/15 13:49
t' This°report-shouldnot be:reprodueed; except in,its entirety, ..withoutthe'written consent of Prism Laboratories; inwi:ci' . v •cr
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Phone, 704/529-6364-Toll Free Number: 1-800/529.6364- Fax: [phone] PaggZ8 Of 9

•.•rr. •rrr;: rr:: •rrry •r::
CHAIN OF CUSTODY RECORD LAB USE ONLY
a,///��� Full -Service Analytical &
Y . I Environmental Solutions PAGE__ OF _ QUOTE 0 TO ENSURE PROPER BILLING:. �Sample�S•`INTACT,IipOA S[rlvai�• + ` ` r ^-'��I- r �' '�'
Is
/Ail JY4f"i'7�LABORATORIES. INC
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax: 7D4/525-0409
Client Company Name: e+ } o T 9Eo.4e 3 Y,TE
Report To/Contact Name: Anb SM; 1%
Reporting Address:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
'Please ATTACH any project specific reporting (QC LEVEL 1 II III M
provisions and/or QC Requirements
Invoice To:
Address:
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EDD Type: PDF_Excel _other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be SC OTHER
N/A
Site Location Name: F m r-,P h Creek W vo f P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 913 C)( FA,-,n Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
S 0.�CSY! IC (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES
NO
TIME MATRIX SAMPLE CONTAINER \ ANALYS14 REQUESTED
\\
PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- REMARKS AB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TNES (yjC
NO.
HOURS SLUDGE) SEE BELOW rC (�
3EAken C
S
P
NA Sdo3
II
`weeki
As
PAAf
SEa ��'•-�e
S
P
NQrr e-
d
Ca
SA
�b
N
N;
Sc
Sampler's Signature � Sampled By (Print Name) IA Lc3 ric Affiliation
Upon relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
PRISM USE ONLY
submitted In writing to the Prism Project Manager. There will be c arges for any changes after analyses have been Initialized.
9 I ishe By: (Sign ture A Re v By: SI t Dale I Lary ours Additional Comment
1c: b cl),
Sit rivaLT,r'ie'>'-:;�:;:;;;
A
Rece ed B SI nat re Date
Rell 'shed By: (SI lure) Y� t 9 )
, aA�
Relinq Is ed By: (Slg eturer Received For Pd La oratades By. Data
r
AtA
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CYSTCPY SWS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UfYESMED AT THE LABORATORY.
C
SZ ) C) 0iS,o
❑ Fed Ex ❑ UPS ❑ Handdenvered sm Field Servlce ❑ Olhet
NPDES: UST: GR NDWATER: DRINKING WATER: SOLID WASTE: RC RA: CERCLA LANDFILL OTHER:
'
ORN
❑NC❑SCI ❑NC ❑SCI❑❑ C ❑SC ElNC ❑SC ONC ❑SC Er ONC ❑SCI ONC ❑SC 13NC ❑SC
*CONTAINER TYPE CODES: A=Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA= Volatile Organics Analysis (Zero Head Space) ORIGINAL

NC Certification No. 402
`F SC Certification No. 99012 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 05/27/2015
PR�•ISM I Environmental Solutions VA Certification No. 460211
'O' LABORATORIES, INQ DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No: L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 05/18/2015
Statesville, NC 28687 Prism Work Order: 5050337
This data package contains the analytical results for the project identified.above and includes Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
• a_.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than-1 Oxthe MB:
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone]del Of 9

PORE
Full -Service Analytical &
AAAR ISM I Environmental Solutions
VL WMUORIM INc
Sample Receipt Summary
05/27/2015
Prism Work Order: 5050337
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 5050337-01 Solid 05/18/15 05/18/15
Samples were received at 24.8 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: "00/529-6364 - Fax: [phone] Page 2 of 9

�t Full -Service Analytical 8
R. I S M I Environmental Solutions
UBONIMMA ING
Laboratory Report
05/27/2015
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta=Lime
Attn: Andy Smith Prism Sample ID: 5050337-01
P.O. Box 1111 Prism Work Order: 5050337
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/18/15 12:30
Time Submitted: 05/18/1516:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
Plant Available Nitrogen
640
mg/kg
160
60
2
*Calculation 5/22115 7:41
CLB
[CALC]
% Solids
70.1
% by
0.100
0.100
1
*SM2540 G 6/21115 15:00
EGC
P5E0434
Weight
Nitrate/Nitrite as N
25
mg/kg dry
7.1
0.78
1
*SM4500-NO3 F 5/20115 12:32
CLB
P5E0367
Total Kjeldahl Nitrogen
2900
mg/kg dry
710
280
2
*351.2 5/22115 7:41
CLB
P5E0420
Ammonia as N
160
mg/kg dry
7.1
1.6
1
*SM4500-NH3 G 5/21115 7:58
CLB
PSE0402
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 5/19/15 10:05
EGC
P5E0399
Total Metals
Mercury
0.11
mg/kg dry
0.028
0.0018
1
*7471B
6/20116 12:30
JAB
PSE0368
SAR Soil Preparation
Complete
g
1
*2-78-054
5/20/15 7:50
JAB
135E0391
SAR Percent Moisture
59.1
% by
0.100
0.100
1
*2-78-054
5/21/15 9:00
JAB
PSE0410
Weight
Arsenic
6.9
mg/kg dry
0.35
0.050
1
*6010C
5/20H5 21:16
BGM
PSE0365
Sodium Absorption Ratio
0.53
[blank]
0.30
0.016
1
*2-78-054
5/26/15 19:05
BGM
P5E0412
Cadmium .
BRL
mg/kg dry
0.35
0.049
1
*6010C
5/20/15 21:16
BGM
P5E0365
Calcium
2700
mg/L
20
1.7
200
*6010C
5/26115 19:05
BGM
P5E0412
Copper
37
mg/kg dry
0.70
0.13
1
*6010C
5120115 21:16
BGM
P5E0365
Lead
17
mg/kg dry
0.35
0.053
1
*6010C
5120/15 21:16
BGM
PSE0365
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010C
5/22/15 16:17
BGM
P5E0412
Nickel
160
mg/kg dry
1.4
0.18
1
*6010C
5120116 21:16
BGM
PSE0365
Selenium
3.1
mg/kg dry
0.70
0.084
1
*6010C
5120115 21:16
BGM
PSE0365
Sodium
100
mg1L
5.01 "
0.074
10
*6010C
5122MS 16:17
BGM
PSE0412
Zinc
69
mg/kg dry
3.5
0.77
1
*6010C
5/20115 21:16
BGM
PSE0365
This report should not be reproduced,, except in its entirety, without.the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone]o9 Page 3. of 9

' Level II QC Report
-k-il 3
PRFull-Service Analytical & .,.
R I S M I Environmental Solutions 5/27/15
i7usorurowea iva
City of Statesville, NC Project: Stal-ime Prism Work Order: 5050337
Attn: Andy Smith Time Submitted: 5/18/2015 4:00:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source' %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5E0365 - 3050B
Blank (P5E0365-BLK1)
Prepared & Analyzed: 05/20/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P5E0365-BSI)
Prepared & Analyzed: 05/20/15
Arsenic
25.8
0.25
mg/kg wet
25.00 103
80-120
Cadmium
25.4
0.25
mg/kg wet
25.00 101
80-120
Copper
27.5
0.50
mg/kg wet
25.00 110
80-120
Lead
25.4
0.25
mg/kg wet
25.00 101
80-120
Nickel
25.5
1.0
mg/kg wet
25.00 102
80-120
Selenium
25.7
0.50
mg/kg wet
25.00 103
80-120
Zinc
26.3
2.5
mg/kg wet
25.00 105
80-120
Batch P5E0368 - 7471 B
Blank (P5E0368-BLK1) Prepared & Analyzed: 05/20/15
Mercury BRL 0.020 mg/kg wet
LCS (P5E0368-BSI) Prepared & Analyzed: 05/20/15
Mercury 0.447 0.020 mg/kg wet 0.4167 107 80-120
Batch P5E0391 - SAR 2-78-054
Blank (P5E0391-BLK1) Prepared &Analyzed: 05/20/15
SAR Soil Preparation Complete g
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
P hone: 7041529-63 64 - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4.of 9

��-t 7
Full -Service Analytical &
';;_, I S M I Environmental Solutions
U MTORIF2, INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P5E0410 - NO PREP
Project: Stal-im6
Reporting
Result Limit Units
Level II QC Report
5127/15
Prism Work Order: 5050337
Time Submitted: 5/18/2015 4:00:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P5E0410-BLK1)
Prepared & Analyzed: 05/21/15
SAR Percent Moisture
0.100
0.100 % by Weight BH
Duplicate (P5E0410-DUP1)
Source: 5050337-01 Prepared &Analyzed: 05/21/15
SAR Percent Moisture
56.0
0.100 % by Weight 59.1 5 200
Batch P5E0412 - 3010A
Blank (P5E0412-BLK1)
Prepared: 05/21/15 Analyzed: 05/22/15
Sodium Absorption Ratio
BRL
0.30 [blank]
Calcium
BRL
0.10 mg/L
Magnesium
BRL
0.10 mg/L
Sodium
BRL
0.50 mg/L BH
This report should not be reproduced, except in its entirety, without the.written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
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Level II. QG Report
t'+'�• Full -Service Analytical & ro
I S M I Environmental Solutions 5/27/15
�1"__ToR1ES, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 5050337
Time Submitted: 5/18/2015 4:00:OOPM
' Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5E0367 - NO PREP
Blank (P5E0367-BLK1) Prepared & Analyzed: 05/20/15
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P5E0367-BS1) Prepared & Analyzed: 05/20/15
Nitrate/Nitrite as N 51.6 5.0 mg/kg wet 50.00 103 80-120
Matrix Spike (P5E0367-MS7) Source: 5050337-01 Prepared & Analyzed: 05/20/15
Nitrate/Nitrite as N 101 7.1 mg/kg dry 71.29 25.2 107 80-120
-Matrix Spike Dup (P5E0367-MSD1) Source: 5050337-01 Prepared & Analyzed: 05/20/15
Nitrate/Nitrite as N 101 7.1 mg/kg dry 71.29 25.2 107 80-120 0 20
Batch P5EO402 - NO PREP
Blank (P5E0402-BLK1) Prepared & Analyzed: 05/21/15
Ammonia as N ' BRL 5.0 mg/kg wet
LCS (P5E0402-BS1) Prepared & Analyzed: 05/21/15
Ammonia as N 123 5.0 mg/kg wet 125.0 98 80-120
Matrix Spike (P5E0402-MS1) Source: 5050337-01 Prepared & Analyzed: 05/21/15
Ammonia as N 353 7.1 mg/kg dry 178.2 160 109 80-120
Matrix Spike Dup (P5E0402-MSD1) Source: 5050337-01 Prepared & Analyzed: 05/21/15
Ammonia as N 355 7.1 mg/kg dry 178.2 160 110 80-120 0.6 20
Batch P5EO420 - 351.2
Blank (P5E0420-BLK7) Prepared: 05/21/15 Analyzed: 05/22/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of. Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page .6 0f 9

a
Full -Service Analytical &
E, I S 1 Y 1 I Environmental Solutions
AAllIR
��SLABOMTOME$ Ma
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P5E0420 - 351.2
Project: StaLirtie
Reporting
Result Limit Units
Level ll QC Report
5/27/15
Prism Work Order: 5050337
Time Submitted: 5/18/2015 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P5E0420-BS1) Prepared: 05/21/15 Analyzed: 05/22/15
Total Kjeldahl Nitrogen 474 100 mg/kg wet 500.0 95 90-110
Matrix Spike (P5E0420-MS1) Source: 5050337-01 Prepared: 05/21/15 Analyzed: 05/22/15
Total Kjeldahl Nitrogen 10900 1800 mg/kg dry 7129 2870 112 90-110 MI
Matrix Spike Dup (P5E0420-MSD1) Source: 5050337-01 Prepared: 05/21/15 Analyzed: 05/22/15
Total Kjeldahl Nitrogen 10700 1800 mg/kg dry 7129 2870 110 90-110 1 20
Batch P5EO434 - Solids. Dry Weiaht
Blank (P5E0434-BLK1) Prepared & Analyzed: 05/21/15
% Solids 99.9 0.100 % by Weight
Duplicate (P5E0434-DUP1) Source: 5050337-01 Prepared & Analyzed: 05/21/15
% Solids 70.1 0.100 % by Weight 70.1 0.05 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: 704/52"409 Page 7 of 9

Level II.;QC Repalrt- -
�f p3R t� Full -Service Analytical & d
a l`R ISM I Environmental Solutions 5i27/15
_'V'UBOHATOMEA ING
City of Statesville, NC Project: StaLime Prism Work Order: 5050337
Attn: Andy Smith Time Submitted: 5/18/2015 4:00:OOPM
P.O. Box-1111
Statesville, NC 28687
Microbiological. Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5E0399 - NO PREP
Blank (P5E0399-BLK1) Prepared & Analyzed: 05/19/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
5050337-01
P5E0420
0.05 g
25 mL
05/21/15 1.1:40
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/rime
5050337-01
P5E0434
30 g
30 g
05/21/15 15:00
Prep Method: 3010A
Lab Number
Batch
Initial
. Final
DateMme
5050337-01
P5E0412
50 mL
50 mL
05/21/15 9:30
5050337-01
P5E0412
50 mL
50 mL
05/21/15 9:30
5050337-01
P5E0412
50 mL
50 mL
05/21/15 9:30
Prep Method: 3050B
Lab Number
Batch
Initial
Final
DateTme
5050337-01 -
P5E0365 -
2.04 g
50 mL
05/20/15 8:05
Prep Method: 7471E
Lab Number
Batch
Initial
Final
bate/Time
5050337-01
P5E0368
0.62 g
50 mL
05/20/15 9:18
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
DateTme
5050337-01
P5E0391
250 g
250 g
05/20/15 7:50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toil Free Number: 1-8001529-6364 - Fax: [phone] Page' $,Of 9

:: , '''Fir,•
•V r , �ii ir,_JJ_nJ.._uJ..J J....JJ.JJ_J__....,_uJJJ_J. __.JJJ_J_..... ___�JJJ✓.IJJirJJJJJJJJJ..uJJ... �J_r ••rr r ._... _.. �.��JJ.J...�.JJJ.....,.r.�. J. ., ., :
CHAIN OF CUSTODY RECORD
1`
Full-Service Analytical &
1W&
R
Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
ISM I
uYW1INC.
Prnierf Name•
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax: 704ff1525-0409
Client Company Name: C.� 41 e� StA�CS✓+l��
Report To/Contact Name: n v S+� +•%
Reporting Address:
Short Hold Analysis: (Yes) (No) UST Projact: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone: %0Y• 0IY 305' Fax es (No):78Y- g"_ 9653 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
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EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushMust Be oved
re h Work
Cf
SC OTHER
NIA -
Site Location Name: id,4rT� V_e W W-T Samples received after 14:00 will be processed next business day.
Site Location Physical _ reSS: L �3 B e �'_A rr.l Turnaround time Is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES
S L'S VI J / / C am RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) P P
NO
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRESERVA-
PRISM
CLIENT DATE COLLECTED (SOIL, rJ"' REMARKS LAB
WATER OR `TYPE TNES [•v/,X/
SAMPLE DESCRIPTION COLLECTED MILITARY
NO. SIZE ��
ID NO.
HOURS SLUDGE) SEE BELOW
J-eA �,�,�e
s
p .
INIA, SAO3
As
PAN
S �► ,+� '� e
S
P
�!d N e
CJ
CU
SA
Pb
u
sz
ZN
Sampler's Signature /T �1P' Sampled By (Print Name), !id W P' GrC Affiliation
Upon relinquishing, this Ciffialin of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
PRISM USE ONLY
submitted in writing to the Prism Project Manager. There will be c es for any changes after analyses have been Initialized.
_
etu Date
Rell Ished By: (Signa re Rec 've By: n r..,
_ ! � J / -�
ll to /Hours
M. ry
© Additional Comments:
.Site,AtTIxalTirtte
A.
R� hed By: (Sigry� ) Recbived By: (Signature) I Date
Site Departure Tlrrlp
Fieltl!:Teeh`Feeas::::
R Is ed By. (Signa Received For P m Labors es Date
( O O
�D
'Mdgage
Method of Shlpment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT VATHAUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY COC Gro p Igo.
SAMPLES ARE NOT EPTED AND VERIFIED AGAINST CO NTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑UPS ❑ HandEelivered rism Field Service ❑OtherNPDES:
LAND
RC: CERCLA
UST. �OUNDWAI
�❑ F❑
r
❑ NC ❑ SIC ❑ NC. ❑ SC I ❑❑ NC ❑ SIC I Ll NC ❑ CATER: ❑ NC ❑ SCE I SC I U NC ❑ SC I O C SC O NC ❑ SC
❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

NC Certification No. 402 Case Narrative
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cart No. 37735 P I S M I Environmental Solutions VA Certification No: 460211 06/23/2015
V11AEORaroRIES. ING, DoD ELAP: L-A-B Accredited Certificate No. L2307 -
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 06/15/2015
Statesville, NC 28687 Prism Work Order: 5060288
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody.: Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report. .
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
)��;? �- J�(_. (�
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated With a J.
Y This report should not be reproduced except in Its entiretX without the written consent of Pnsm Laboratones Inc
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page ' of 16

Sample Receipt Summary
Full -Service Analyticals
Environmental Solutions I
06/23/2015
' ueoruioMEAJUM
Prism Work Order: 5060288
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime (and Fecal 1)
5060286-01
Solid
06/15/15
06/15/15
Fecal #2
5060288-02
Solid
06/15/15
06/15/15
Fecal #3
5060288-03
Solid
06/15/15
06/15/15
Fecal #4
5060288-04
Solid
06/15/15
06/15/15
Fecal #5
5060288-05
Solid
06/15/15
06/15/15
Fecal #6
5060288-06
Solid
06/15/15
06/15/15
Fecal #7
5060288-07
Solid
06/15/15
06/15/15
Samples were received in good condition at 1.9 degrees C unless otherwise noted
y r. a-. This report.should not.be_reproduced; except in its entirety,-without.themritten consent•of PrisrrfLaboratodes, lnc..:<s ..
449 Springbrook Road P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number. 1.8001529-6364 -Fax: 704152"409 1 Page'Zo

0511
Laboratory Report
Fn-Service
Analytical
LPISNIR
up� I S M I Environmental Solutionss
06/23/2015'
®V LABOMTOHIE$ING
City of Statesville, NC
Project: StaLime
Client
Sample ID:
StaLime (and Fecal 1)
Attn: Andy Smith
Prism Sample ID: 5060288-01
P.O. Box 1111
Prism Work Order: 5060288
Statesville, NC 28687
Sample Matrix: Solid
Time
Collected: 06/15/15 14:27
Time
Submitted: 06/15/15 16:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateTme
ID
General Chemistry Parameters
Plant Available Nitrogen
1700
mglkg
160
60
2
*Calculation
6123115 8:56
CLB
[CALC]
% Solids
75.4
% by
0.100
0.100
1
*SM2640 G
6116115 12:09
ARC
P5F0273
Weight
Nitrate/Nitrite as N
24
mg/kg dry
6.6
0.73
1
*SM4500-NO3 F 6MB115 9.27
CLB
PSF0287
Phosphorus -Total
2000
mg/kg dry
66
17
20
*SM4500-P F
6M7/15 7:51
CLB
05F0263
Total Kjeldahl Nitrogen
7300
mglkg dry
660
260
2
*351.2
6122115 9:10
CLB
P5F0330
Ammonia as N
14
mg/k9 dry
6.6
1.5
1
*SM4500-NH3 G 6123115 8:56
CLB
PSF0383
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
6/16/15 9:57
EGC
P5F0313
Total Metals
Mercury
0.27
mg/kg dry
0.025
0.0016
1
*7471B
6118/15 11:27
JAB
P5F0322
SAR Soil Preparation
Complete
g
1
*2-78-054
6/18/15 9:00
JAB
P5F0299
SAR Percent Moisture
62.7
% by
0.100
0.100
1
*2-78-054
6/18115 10:00
JAB
P5F0362
Weight
Arsenic
4.1
mg/kg dry
0.33
0.047
1
*6010C
6117115 20:10
BGM
PSF0292
Sodium Absorption Ratio
0.86
[blank]
0.30
0.016
1
*2-78-064
6122/15 14:15
BGM
P5F0331
Cadmium
BRL
mg/kg dry
0.33
0.047
1
*6010C
6/17/15 20:10
BGM
P5F0292
Calcium
2000 B
mg/L
10
0.85
100
*6010C
6/22/15 14:15
BGM
P5F0331 .
Copper
26
mg/kg dry
0.66
0.12
1
*6010C
6117115 20:10
BGM
PSF0292
Lead
6.8
mg/kg dry
0.33
0.050
1
*6010C
6117/15 20:10
BGM
05F0292
Magnesium
BRL
mg/L
10
0.070
100
*6010C
6/22/15 14:15
BGM
P5F0331
Nickel
78
mglkg dry
1.3
0.17
1
*6010C
6/17115 20:10
BGM
PSF0292
Selenium
1.6
mglkg dry
0.66
0.079
1
*6010C
6/17/15 20:10
BGM
PSF0292
Sodium
140 B
mg/L
50
0.74
100
*6010C
6/22115 14:15
BGM
P5F0331
Sodium
660
mg/kg dry
16
3.2
1
*6010C
6/17115 20:10
BGM
PSF0292
Zinc
40
mg/kg dry
3.3
0.73
1
*6010C
6/17115 20:10
BGM
PSF0292
1
This•reporishouldnot,bwreproducedpexceptWits entirety; withoutthe writtemconsentof,Prism,,Laboratories,,tne., •�,-k...
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364- Fax: [phone] Page_3 of.,16

r
Full -Service Analytical &
Environmental Solutions .
�'LABOMTORIEq ING -
Laboratory Report-.-
• 06/23/2015' s
City of Statesville, NC Project: Stal-ime Client Sample ID: Fecal #2
Attn: Andy Smith Prism Sample ID: 5060288-02
P.O. Box 1111 Prism Work Order: 5060288
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/15/15 14:27
Time Submitted: 06/15/15 16:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme - ID
General Chemistry Parameters
% Solids 73.6 % by 0.100 0.100 1 'SM2540 G - 6/16H5.12:09 ARC P5F0273
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 6/16115 9:57 EGC P5F0313
=_-;This°reportshouldinohbe reproduced,-except•in:its. entirety; .without the,written consent, of Prism: Laboratories, lncr.. - ra-:.,•w; « t•,.-
.449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-800/529.6364- Fax: 704/52&0409 Page 4:gf• 6.

Laboratory Report
❑ n� Full -Service P Analytical 8 Environmental Solutions 06/23/2015
��U9URATOPoE$ ING
City of Statesville, NC
Project: StaLime
Client Sample ID: Fecal #3
Attn: Andy Smith
Prism Sample ID: 5060288-03
P.O. Box 1111
Prism Work Order: 5060288
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/15/15 14:27
Time Submitted: 06/15/15.16:05
Parameter
Result Units
Report.
MDL Dilution Method Analysis Analyst
i
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
81.8 % by
0.100
0.160 1 'SM2540 G 6/17/15 11:06 EGC
P5F0301
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 `SM9221 E 6/16/15 9:57 EGC
P5F0313
report=shouldinot•be reproduced..except in its-entiretyswithoutthe..written consentof
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number:1-8001529-6364 - Fax: [phone] Page. J Of:1.6

Laboratory-Report
t� i I `- n I Full -Service Analytical &
® S V' Environmental Solutions 06/2312015
A&I uV TOME4INQ -
City of Statesville, NC
Project: Stal-ime Client Sample ID: Fecal #4
Attn: Andy Smith
Prism.Sample ID: 5060288-04
P.O. Box 1111
Prism Work Order: 5060288
Statesville, NC 28687
Sample Matrix: Solid Time Collected: 06/15/15 14:27
Time Submitted: 06/15/15 16:05
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DatefTme
ID
General Chemistry Parameters
% Solids 75.7
% by
0.100
0.100 1
*SM2540 G 6117/15 11:06 EGC
PSF0301
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
•SM9221 E 6/16/15 9:57 EGC
P5F0313
;.,
r ::This ,eportshould notibe reproduced,;except in its' entirely,' without the writteh-consentof Prism Laboratories, inc, �, y
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Pap 6 Of 16

Laboratory Report`
ffii
Full-Service Analytical 8
R„y I S M I Environmental Solutions 06/2k015
ti' LA60MTORIE41NC
City of Statesville, NC Project: Stal-ime Client Sample ID: Fecal #5
Attn: Andy Smith Prism Sample ID: 5060288-05
P.O. Box 1111 Prism Work Order: 5060288
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/15/15 14:27
Time Submitted: 06/15/15 16:05
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst '
Batch
Limit
Factor
DateRme
ID
General Chemistry Parameters
% Solids 87.2
% by
0.100
0.100 1
'SM2540 G 6117115 11:06 EGC
PSF0301
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 6/16/15 9:57 EGC
06F0313
report should: not be;reproduced,.,except in,its,,eetirety,-wittlout,the..wfitten;cpnsent oftPrism Lab¢tatories„lnc .,,.M,
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 7 Of 16

�i �. I S n A I Fun -Service Analytical s
r gy M Full-SEnviroervice
Al SolutionsAnalytical
�M lA80MT0MrA INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory, Report t
O'6%23%20'i5"
Project:'Stal-ime Client Sample ID: Fecal #6
Prism Sample ID: 5060288-06
Prism Work Order: 5060288
Sample Matrix: Solid Time Collected: 06/15/1514:27
Time Submitted: 06/15/15 16:05
Parameter Result
Units
Report
Limit
MDL Dilution Method Analysis Analyst
Factor Datefrime
Batch
ID
General Chemistry Parameters
Solids 73.2
Microbiological Parameters
% by
Weight
0.100
0.100 1-'SM2540 G 6/17/15 11:06 EGC
P5F0301
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 6/16/15 9:57 EGC
135F0313
-= .' : • .This report should not=be reprodueed'-'excepti6its•entirety,:I.Imthoutthe' written consentof Prism Laboratories,dtic.-i+:� r n � ,:;::: .•rr�� ,
449 Springbrook Road - P.O. Box 24050 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1.8001529-6364 - Fax: [phone]

Full-ServIce Analytical & -
R'I S M I Environmental Solutions
Lit�a�" 'uaorutomm, we
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory. Report
06/23/2015
Client Sample ID: Fecal #7
Prism Sample ID: 5060288-07
Prism Work Order: 5060288
Time Collected: 06/15/15 14:27
Time Submitted: 06/15/15 16:05
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DatelTme,
ID
General Chemistry Parameters
% Solids 84.1
% by
0.100
0.100 1 .
'SM2540 G 6117115 11:06 EGC
P5F0301
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 6/16/15 9:57 EGC
P5F0313'
—This-report should,not-be,reproduced,=except in its ::entirety,vwithout-the:written consent of,Prism.:,Laboratories,Inc.,.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - TO Free Number: 1-8001529-6364 - Fax: 704f525-0409 Page. 9 pf 6

�r Full -Service Analytical &
R•' S'M I Environmental Solutions
�GBOIUTOXIF$ IN6
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Lev�IrvlhQC Report
"6/23/1'5. 4
Prism Work Order: 5060288
Time Submitted: 6/15/2015 4:05:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5F0292 - 3050E
Blank (P5F0292-BLKI)
Prepared &Analyzed: 06/17/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
. BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (PSF0292-BSI)
Prepared & Analyzed: 06/17/15
Arsenic
23.2
0.25
mg/kg wet
25.00 93
80-120
Cadmium
23.8
0.25
mg/kg wet
25.00 95
80-120
Copper
26.8
0.50
mg/kg wet
25.00 107
80-120
Lead
24.0
0.25
mg/kg wet
25.00 96
80-120
Nickel
23.9
1.0
mg/kg wet
25.00 96
80-120
Selenium
22.2
0.50
mg/kg wet
25.00 89
80-120
Sodium
537
12
mg/kg wet
500.0 107
80-120
Zinc
24.0
2.5
mg/kg wet
25.00 96
80-120
Batch P5F0299 - SAR 2-78-054
Blank (P5F0299-BLK1)
Prepared: 06/17/15 Analyzed: 06/18/15
SAR Soil Preparation
Complete
g
Batch PSF0322 - 7471 B
Blank (PSF0322-BLK1)
Prepared & Analyzed: 06/18/15
Mercury
BRL
0.020
mg/kg wet
&- This report•should not be reprodueed;'ezcept in its"entirety 'iithoutthewrittenlconsentoffPrism'`Laboratories,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Frio Number 1-800/529-6364 - Fax. [phone] _Qf )6

P R ISM
n I- Envi Service Analytical
A'v�' Environmental Solutions
®�LA90flIRORIE$ ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P5170322 - 7471 B
Level II QC Report
6/23/15
Project: Stal-ime Prism Work Order: 5060288
Time Submitted: 6/15/2015 4:05:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits _ RPD Limit Notes
LCS (P5F0322-BSI)
Prepared & Analyzed: 06/18/15
Mercury
0.440
0.020
mg/kg wet 0.4167 106 80-120
Batch P5F0331 - 3010A
Blank (P5F0331-BLK1)
Prepared: 06/18/15 Analyzed: 06/22/15
Sodium Absorption Ratio
BRL
0.30
[blank]
Calcium
0.106
0.10
mg/L BH
Magnesium
BRL
0.10
mg/L
Sodium
1.78
0.50
mg/L BH
Batch P5F0362 - NO PREP
Blank (P5F0362-BLK1) Prepared & Analyzed: 06/18/15
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (135F0362-DUP1) Source: 5060288-01 Prepared & Analyzed: 06/18/15
SAR Percent Moisture 52.0 0.100 % by Weight 52.7 1 200
-+ . •.... This report=should not be;reproduced,.a. xcept in, its,entirety,,without,the,written;ponsent-of;P.rismrLaboratories ,Inc;:
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number.1-800/529-6364 - Fax: [phone] Page 11 Ofi 6

Levet 11..QC ;Report ,
Full -Service Analytical 8
Environmental Solutions -
iftii��ueodronies, inc
City of Statesville, INC Project: Stal-ime Prism Work Order: 5060288
Attn: Andy Smith Time Submitted: 6/15/2015 4:05:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result ' %REC Limits RPD Limit Notes
Batch PSF0263 - SM4500-PBS
Blank (P5F0263-BLK1) Prepared: 06/16/15 Analyzed: 06/17/15
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P5F0263-BSI) Prepared: 06/16/15. Analyzed: 06/17/15
Phosphorus -Total 101 2.5 mg/kg wet 100.0 101 90-110
Batch 05F0273 - Solids Dry Weight
Blank (P5F0273-BLK1) Prepared &Analyzed: 06/16/15
% Solids 100 0.100 % by Weight
Batch P5F0287 - NO PREP
Blank (P5F0287-BLK1)
Prepared: 06/17/15 Analyzed: 06/18/15
Nitrate/Nitrite as N
LCS (P5F0287-BSI)
BRL 5.0 mg/kg wet
Prepared: 06/17/15 Analyzed: 06/18/15
Nitrate/Nitrite as N
Matrix Spike (P5F0287-MS1)
49.1 5.0 mg/kg wet
Source: 5060288-01
50.00 98 80-120
Prepared: 06/17/15 Analyzed: 06/18/15
Nitrate/Nitrite as N
Matrix Spike Dup (P5F0287-MSD1)
78.3 13 mg/kg dry
Source: 5060288-01 -Prepared:
66.32 23.7 82 80-120
06/17/15 Analyzed: 06/18/15
Nitrate/Nitrite as N
Batch P5170301 - Solids Dry Weight
78.8 13 mg/kg dry
66.32 23.7 83 80-120 0.7 20
Blank (P5F0301-BLKI)
Prepared & Analyzed: 06/17/15
% Solids
100 0.100 % by Weight
*. n This`report should not=be reproduced except.in its entirety; without;the:written.consent of.Prism,l-abpratolies,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number. 1-8001529-6364 - Fax: 704/52"409 P8g@ 2 Of f6 '

"
�� � I n A I Fun -Service Analytical 8
' V' Environmental Solutions
ILA't'3ue0RXT0R1ea 1n
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control -
Level II QC Report
6/23/15 --'
Prism Work Order: 5060288
Time Submitted: 6/15/2015 4:05:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit - Notes
Batch P5F0301 - Solids, Dry Weight
Duplicate (P5F0301-DUP2) Source: 5060288-03 Prepared & Analyzed: 06/17/15
% Solids 82.6 0.100 % by Weight 81.8 0.9 20
Batch P5F0330 - 351.2
Blank (P5F0330-BLK1) Prepared: 06/18/15 Analyzed: 06/22/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P5F0330-BSI) Prepared: 06/18/15 Analyzed: 06/22/15
Total Kjeldahl Nitrogen 485 100 mg/kg wet 500.0 97 90-110
Matrix Spike (P5F0330-MS1) Source: 5060289-01 Prepared: 06/18/15 Analyzed: 06/22/15
Total Kjeldahl Nitrogen 10300 1700 mg/kg dry 6632 7300 45 90-110 MI
Matrix Spike Dup (P5FO330-MSD1) Source: 5060288-01 Prepared: 06/18/15 Analyzed: 06/22/15
Total Kjeldahl Nitrogen 11500 1700 mg/kg dry 6632 7300 63 90-110 11 20 MI
Batch P5F0383 - NO PREP
Blank (P5F0383-BLKI) Prepared & Analyzed: 06/23/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (P5F0383-BS1) Prepared &Analyzed: 06/23/15
Ammonia as N .127 5.0 . mg/kg wet 125.0 101 80-120
Matrix Spike (P5F0383-MSI) Source: 5060288-01 Prepared & Analyzed: 06/23/15
Ammonia as N 152 13 mg/kg dry 165.8 13.5 83 80-120
This report should,not be;reproduced,.oxceptin its entirety .without.th, a wrifter) consent of,Prism=:L-aboratories Inc tt_..
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone:[phone] -Toll Free Number:1-8001529-6364 - Fax: [phone]

Level II QC
PR1SMI R6e/2p3o/ir5t
Fuli-Service Analytical
Environmental Solutions
(ABOegTOnIF$ IHG
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 5060288
Time Submitted: 6/15/2015 4:05:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5F0383 - NO PREP
Matrix Spike Dup (P5F0383-MSD1) Source: 5060288-01 Prepared & Analyzed: 06/23/15
Ammonia as N 156 13 mg/kg dry 165.8 13.5 86 80-120 3 20
-, ,, 4i.nisrepor[snpuiono[oe,reproauceo,excepi,in,.ns,enurery;.Wirnourrne:wrigen.consenLor:t'.riAm.Lanomories lnc
449 Springbrook. Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone]. F age 14:Of 16

IFull-service Analytical &
Rea � Environmental Solutions
'�ueonaioaiee, iNc .
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level 11 QC Report
- 6/23/15
Prism Work Order: 5060288
Time Submitted: 6/15/2015 4:05:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5F0313 - NO'PREP
Blank (P5F0313-BLK1) Prepared & Analyzed: 06/16/15
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Daterrime
5060288-01 P5F0330 0.05 g 25 mL 06/18/15 12:15
Prep Method: SM4500-PBS
Lab Number Batch Initial Final Daterrime
5060288-01
P5F0263
1
g 50 mL
06/16/15 11:00
Prep Method: Solids,
Dry Weight
Lab Number
Batch
Initial
Final
Datemme
5060288-01
P5F0273
30
g 30 g
06/16/15 12:09
5060288-02
P5F0273
30
g 30 g
06/16/15 12:09
5060288-03
P5F0301
30
g 30 g
06/17/15 11:06
5060288-04
P5F0301
30
g 30 g
06/17/15 11:06
5060288-05
P5F0301
30
g 30 g
06/17/15 11:06
5060288-06
135F0301
30
g 30 g
06/17/15 11:06
5060288-07
P5F0301
30
g 30 g
06/17/15 11:06
Prep Method: 3010A
Lab Number Batch Initial Final Datefrime
506028E-01 P5F0331 50 mL 50 mL 06/18/15 9:30
5060288-01 135F0331 50 mL 50 mL 06/18/15 9:30
Prep Method: 3050B
Lab Number Batch Initial Final Daternme
5060288-01 P5F0292 2.01 g 50 mL 06/17/15 9:53
Prep Method: 74718
Lab Number Batch Initial Final Datemme
5060288-01 P5F0322 0.64 g 50 mL 06/18/15 8:15
Prep Method: SAR 2-784154
Lab Number Batch Initial Final Daterfime
5060288-01 P5F0299 250 g 250 g 06/17/15 9:00
ihis,reportshould,hq-t,be reproduced,.excgpt,,in,its:entiiety withput the written consent of.,Prismlaboratories Inc
si
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page.1.5Of 6

CHAIN OF CUSTODY RECORD
sm
Full -Service Analytical &
Solutions
BILLING:
}+rtijs3%I^t:?;.�
-
Environmental
PAGE_ OF _ QUOTE q TO ENSURE PROPER
•
�
i La` �i INC.
1
Project Name: a+
,.
449 Springbrook Road • Charlotte, NC 28217
' ' • Phone [phone] Fax: [phone] ...
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
ii
',r,Client.CompanyName: C:iy
at s�a�esyI (e-
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
9",
�•��
''-.. Report To/Contact Name:
A.v y S rn i:t
provisionsandlorQCRequirements
Invoice To:
Reporting Address:
Address:
.a
Phone- 70Y-971-31U5' Fax es (No):7a7J1-87S—WS3 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Ruh Work Must BePre-pproved
SC OTHER
N/A
Site. Location Name: Fau I_LI Coed: t♦< LUW TP Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 03 1301 I -As-, , F? Turnaround time Is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
/ (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
U- cs"i'lle %NIC RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES
NO -
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM.
PRESERVA- ` P�
CLIENT DATE COLLECTED (SOIL, REMARKS - LAB
TNES
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE
ID NO.:
HOURS SLUDGE) SEE BELOW 4�C ��
Sta-1".4 e_
6s15-15
1 ��
�'
P
Na2sa03'
As
RAN
C2
A R
Pb
�S
Zia
Sampler's Signature Sampled By (Print Name) Affiliation
Upon. relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
PRISM USE, ONLY
`submitted -in writing to the Prism Project Manager. There will be charges for any ch nges after analyses have been initialized.
_
Relin he By: (Sign re Received slur ate
lltery/Hours Additional Comments:
..Site Arrival
Rellnq I ed By: (Signature) Receiv By: (Sign re Date
,Site: pepartutern:;:':
Feld-Tech Fep ` f
:Relin By: (Sign re) Received Fo Ism Leborat B Date
Method Shipment 'NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT STODY SEALS FOR TRANSPORTATION TO THE LABORATORY. C C G up No.
-
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO. �l1NTIL RECEIVED AT THE LABORATORY.
l/
❑ Fed Ex ❑ UPS ❑ Hand-dellvered Prism Field Service ❑ Other o
NPDES: UST: G NDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑ NC O SCI ❑ NIC ❑ SC ❑ NC ❑ SC I ❑ NC ❑ SG I ❑ NC ❑ SIC I a NC ❑ SC O NC ❑ SC I LI NC ❑ SC I L3 NC ❑ SC
❑ ❑ ❑ ❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL

NC Certification No. 402 Case Narrative
wt SC Certification No. 99012
®�4 I M
IFull-Service Analytical & NC Drinking Water Cart No. 37735 07/24/2015
Environmental Solutions VA Certification No. 460211
®�ueoAnToeIES IN4. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISONEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/13/2015
Statesville, NC 28687 Prism Work Order: 5070212
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Terri W. Cole For Robbi A. Jones
Project Manager
Data Qualifiers Key Reference:
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
DM Sample diluted and RL increased due to the matrix.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with.values between MDL and
reporting limit indicated with a J.
•;- ,<,-- This•reporf should. not-be.reproduced; except in,its entirety,;without the,written.consent of Prism ;Laboratories
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1 -800/629-6364 - Fax: 704152"409 Pagel..Of 2

&fAP�
p Full -Service Analytical 3
.". If1 �I S M I Environmental Solutions
Mueopwrosim wa
Sample Receipt Summary.,.
07/24/2015
Prism Work Order: 5070212
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 5070212-01 Solid 07/13/15 07/13/15
Samples were received in good condition at 4.6 degrees C unless otherwise noted.
,.:_.:,. :-........ Thisreportsheuldnot.be,reproduced,;except.in,itsanti[ety..vvitho_ut, the jvritten,consentofPrism Labpratories Inc -
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001529-6364 - Fax: [phone] Page.2,.Of•:12

3 1 Full -Service Analytical &
P R ISM I Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
07/24/2015
Project: Stal-ime (Qtrly, & BiWeeklyl) Client Sample ID: Sta-Lime
Prism Sample ID: 5070212-01
Prism Work Order: 5070212
Sample Matrix: Solid Time Collected: 07/13/15 13:50
Time Submitted: 07/13/15 15:35
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor '
DateTme
ID
General Chemistry Parameters
Plant Available Nitrogen
770
mglkg
160
60
2
*Calculation
7122115 14:37
CLB
[CALC]
% Solids
72.9
% by
0.100
0.100
1
"SM2540 G
7114/15 11:26
ARC
PSG0201
Weight
Nitrate/Nitrite as N
0.6
mg/kg dry
6.9
0.75
1
'SM4500-NO3 F
7116115 8:18
CLB
PSG0227
Phosphorus -Total
1800,
mg/kg dry
69
18
20
`SM4500-P F
7/15115 8:52
CLB
P5G0217
Total Kjeldahl Nitrogen
3400
mg/kg dry
690
270
2
*361.2
7117/16 7:39
CLB
P5G0230
Ammonia as N
61
mg/kg dry
6.9
1.5
1
"SM4500-NH3 G
7122115 14:37
CDL
P5G0366
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
7/14/15 9:40
EGC
P5G0258
Total Metals
Mercury
0.11
mg/kg dry
0.027
0.0018
1
'7471B
7116115 16:20
JAB
PSG0270
SAR Soil Preparation
Complete
g
1
'2-78-054
7/16/15 10:00
JAB
P5G0240
SAR Percent Moisture
50.1
% by
0.100
0.100
1
'2-78-054
7116115 8:00
JAB
P5G0324
Arsenic
8.1
Sodium Absorption Ratio
0.75
Cadmium
BRL
Calcium
3000
Copper
42
Lead
6.5
Magnesium
BRL
Nickel
140
Potassium
5200
Selenium
BRLDM
Sodium
150
Sodium
900
Zinc
70
Weight
mglkg dry
0.35
0.049
1
'6010C
7115115 17:49
BGM
PSG0221
[blank]
0.30
0.016
1
'2-78-054
7116115 16:06
BGM
PSG0273
mg/kg dry
0.35
0.049
1
*6010C
7/15/15 17:49
BGM
P5G0221
mg/L
1.0
0.085
10
•6010C
7116115 16.06
BGM
PSG0273
mg/kg dry
0.69
0.13
1
'6010C
7115115 17:49
BGM
136G0221
mg/kg dry
0.35
0.053
1
'6010C
7115/15 17:49
BGM
PSG0221
mg/L
1.0
0.0070
10
'6010C
7/16/15 16:06
BGM
P5G0273
mglkg dry
1.4
0.18
1
`6010C
7115115 17:49
BGM
PSG0221
mg/kg dry
170
11
10
'6010C
7/15115 16:51
BGM
P5G0221
mg/kg dry
6.9
0.83
10
'6010C
7/15/15 16:51
BGM
P5G0221
mg/L
5.0
0.074
10
•6010C
7116115 16:06
BGM
P5G0273
mg/kg dry
17
3.4
-1
`6010C
7118116 17:49
BGM
P5130221
mg/kg dry
3.5
0.76
1
•6010C
7115/15 17:49
BGM
PSG0221
<. _ _-•This.reportshould..not be. reproduced;,except- in its.entirety,..without the written -consent of.Prism Laboratories, lnc
.. ., ,.. .. rr
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 Of 12

MR.
Full -Service Analytical'&
I Si M Environmental Solutions
{AeO WORIE9, ING
City of Statesville, NC
Attn: Andy Smith,
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime (Qtrly, & BiWeeklyl)
Level II QC Report '
5'7/24/15 `t
Prism Work Order: 5070212
Time Submitted: 7/13/2015 3:35:OOPM
Reporting Spike Source%REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5G0221 - 3050B
Blank (P5G0221-BLK1)
Prepared & Analyzed: 07/15/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P5G0221-BS1)
Prepared & Analyzed: 07/15/15
Arsenic
24.1
0.25
mg/kg wet
25.00 96
80-120
Cadmium
24.3
0.25
mg/kg wet
25.00 97
80-120
Copper
26.0
0.50
mg/kg wet
25.00 104
80-120
Lead
24.1
0.25
mg/kg wet
25.00 96
80-120
Nickel
24.0
1.0
mg/kg wet
25.00 96
80-120
Potassium
511
12
mg/kg wet
500.0 102
80-120
Selenium
23.5
0.50
mg/kg wet
25.00 94
80-120
Sodium
534
12
mg/kg wet
500.0 107
80-120
Zinc
23.9
2.5
mg/kg wet
25.60 95
80-120
Matrix Spike (PSG0221-MS1)
Source: 5070212-01
Prepared & Analyzed: 07/15/15
Arsenic
50.7
0.35
mg/kg dry
34.99 8.12 122
75-125
Cadmium
27.0
0.35
mg/kg dry
34.99 0.215 77
75-125
Copper
86.6
0.70
mg/kg dry
34.99 41.7 128
75-125
MC
Lead
33.9
0.35
mg/kg dry
34.99 6.48 78
75-125
Nickel
184
1.4
mg/kg dry
34.99 138 131
75-125
MC
Potassium
6640
170
mg/kg dry
699.9 5210 205
75-125
MC
Selenium
BRL
7.0
mg/kg dry
34.99 BRL
75-125
MI
Sodium
2020
17
mg/kg dry
699.9 896 160
75-125
MC
Zinc
109
3.5
mg/kg dry
34.99 69.6 113
75-125
= • • --.-This report should,not be-reproduced;:except in.its,entiiety, without the.;writtemconsent;of Prism. Laboratories, Inc., .;,.:, , .,•,_., K, „ ,._ ;,
449 Springbrook Road r P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Tall Free Number: 1-8001529-6364 = Fax: 704/52"409 1 Page 4712

Level II QC Report
&Ih�.-Full-Service Analytical& 7/24/15
R ISM I Environmental Solutions -
LmofwomEs, mr.
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 5070212
Attn: Andy Smith Time Submitted: 7/13/2015 3:35:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PSG0221 - 3050B
Matrix Spike Dup (135130221-MSD1)
Source: 5070212-01
Prepared & Analyzed: 07/15/15
Arsenic
49.4
0.34
mg/kg dry
34.12 8.12 121
75-125
3 .
20
Cadmium
26.9
0.34
mg/kg dry
34.12 0.215 78
75-125
0.5
20
Copper
80.9
0.68
mg/kg dry
34.12 41.7 115
75-125
7
20
Lead
33.8
0.34
mg/kg dry
34.12 6.48 80
75-125
-0.3
20
Nickel
173
1.4
mg/kg dry
34.12 138 102
75-125
6
20
Potassium
6500
170
mg/kg dry
682.5 5210 189
75-125
2
20
MC
Selenium
BRL
6.8
mg/kg dry
34.12 BRL
75-125
20
MI
Sodium
1930
17
mg/kg dry
682.5 896 152
75-125
4
20
MC
Zinc
112
3.4
mg/kg dry
34.12 69.6 125
75-125
3
20
Post Spike (135130221-PS11)
Source: 5070212-01
Prepared & Analyzed: 07/15/15
Arsenic
1.39
mg/L
1.000 0.237 116
80-120
Cadmium
0.785
mg/L
1.000 0.00627 78
80-120
MI
Copper
2.23
mg/L
1.000 1.22 101
80-120
Lead
0.961
mg/L
1.000 0.189 77
80-120
MI
Nickel
4.66
mg/L
1.000 4.02 .64
80-120
MC
Potassium
165
mg/L
20.00 152 67
80-120
MC
Selenium
0.0288
mg/L
1.000 -1.06 3
80-120
MI
Sodium
50.9
mg/L
20.00 26.1 124
80-120
MC
Zinc
3.00
mg/L
1.000 2.03 97
80-120
Batch PSG0240 - SAR 2-78-054
Blank (P5G0240-BLK1)
Prepared: 07/15/15 Analyzed: 07/16/15
SAR Soil Preparation
Complete
g
the written consent of Prism Laboratories Inc _ . This..reportshould not.-be,reproduc� ,". ,except m its entirety without: „- .,;
449 Springbrook Road P.O. Box 246543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 11-800/529-6364 - Fax: [phone] Page.5

"52 k
PI Full -Service Analytical &
R'I S M I Environmental Solutions
'Ti,ieonnranieet u+e
City of Statesville, NC Project: Stal-ime (Qtrly, & BiWeeklyl)
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
• 1/24/1-5
Prism Work Order: 5070212
Time Submitted: 7/13/2015 3:35:00PM
Reporting Spike Source . %REC RPD
Analyte Result Limit Units Level Result%REC Limits RPD Limit Notes
Batch P5G0270 - 7471 B
Blank (P5G0270-BLKI) Prepared & Analyzed: 07/16/15
Mercury BRL 0.020 mg/kg wet
LCS (PSG0270-BSI) Prepared & Analyzed: 07/16/15
Mercury 0.452 0.020 mg/kg wet 0.4167 109 80-120
Batch P5G0273 - 3010A
Blank (P5G0273-BLK1)'
Prepared & Analyzed: 07/16/15
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium
BRL 0.10 mg/L
Magnesium
BRL 0.10 mg/L
Sodium
BRL 0.50 mg/L
Batch PSG0324 - NO PREP
Blank (P5G0324-BLKI) Prepared & Analyzed: 07/16/15
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (P5G0324-DUPI) Source: 5070212-01 Prepared & Analyzed: 07/16/15
SAR Percent Moisture 50.6 0.100 % by Weight 50.1 0.9 200
This repprtshould. not.,be,rppnajuced axcapt.in its,entireiy- without the written consent.ot PrismlL-aboratories Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 -Fax, 704152"409 Page .6'. 2

Level II QC Report
d Full -Service Analytical & 7/24/15
,[R I S M -I Environmental Solutions
�VILABOqATomea uW.
City of Statesville, NC Project: Stal-ime (Qtrly, & BiWeeklyl) Prism Work Order: 5070212
Attn: Andy Smith Time Submitted: 7/13/2015 3:35:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5G0201 - Solids, Dry Weight
Blank (P5G0201-BLK1) Prepared & Analyzed: 07/14/15
% Solids 100 0.100 - % by Weight
Batch P5130217 - SM4500-PB5
Blank (PSG0217-BLK1) Prepared & Analyzed: 07/15/15
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P5G0217-BS1) Prepared & Analyzed: 07/15/15
Phosphorus -Total 99.8 2.5 mg/kg wet 100.0 100 90-110
Matrix Spike (P5G0217-MS1) Source: 5070212-01 Prepared & Analyzed: 07/15/15
Phosphorus -Total 2330 69 mg/kg dry 137.2 1780 404 80-120 MC
Matrix Spike Dup (PSG0217-MSD1) Source: 5070212-01 Prepared & Analyzed: 07/15/15
Phosphorus -Total 2320 69 mg/kg dry 137.2 1780 396 80-120 0.5 20 MC
Batch P5G0227 - NO PREP
Blank (PSG0227-BLK1) Prepared & Analyzed: 07/16/15
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P5G0227-BS1) Prepared & Analyzed: 07/16/15
Nitrate/Nitrite as N 49.5 6.0 mg/kg wet 50.00 99 80-120
Matrix Spike (P5G0227-MSI) Source: 5070212-01 Prepared & Analyzed: 07/16/15
Nitrate/Nitrite as N 69.5 14 mg/kg dry 68.59 9.60 187 80-120
This report hould not be reproduced except in ds entirety vyithout the writken consent of Fnsm Laboratories Inc
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-800/529-6364 - Fax: [phone] Page 7: of.12

LI&"Ra
Full -Service Analytical &
[S M I Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters -Quality Control
Analyte
Batch P5G0227 - NO PREP
Level IF -QC- Report--- t
7/24/15
Project: StaLime (Qtrly, & BWeeklyl) Prism Work Order: 5070212
Time Submitted: 7/13/2015 3:35:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result. %REC Limits RPD Limit Notes..
Matrix Spike Dup (P5G0227-MSD1)
Source: 5070212-01
Prepared & Analyzed: 07/16/15
Nitrate/Nitrite as N
Batch P560230 - 351.2
69.4 14 mg/kg dry
68.59 9.60 87 - 80-120 0.2 20
Blank (P5G0230-BLKI)
Prepared: 07/15/15 Analyzed: 07/17/16
Total Kjeldahl Nitrogen
LCS (P5G0230-BS1)
BRL 25 mg/kg wet
Prepared: 07/15/15 Analyzed: 07/17/15
Total Kjeldahl Nitrogen
Matrix Spike (P5G0230-MS1)
488 100 mg/kg wet
Source: 5070212-01
500.0 98 90-110
Prepared: 07/15/15 Analyzed: 07/17/15
Total Kjeldahl Nitrogen
Matrix Spike Dup (P5G0230-MSD1)
12000 1700 mg/kg dry
Source: 5070212-01
6859 3440 125 90-110 MI
Prepared: 07/15/15 Analyzed: 07/17/15
Total Kjeldahl Nitrogen
11300 1700 mg/kg dry
6859 3440 114 90-110 6 20 MI
Batch P5G0366 - NO PREP
Blank (P5G0366-BLKI) Prepared: 07/21/15 Analyzed: 07/22/15
Ammonia as N BRL 5.0 mg/kg wet BH
LCS (P5G0366-BSI) Prepared: 07/21/15 Analyzed: 07/22/15
Ammonia as N 122 5.0 mg/kg wet 125.0 98 80-120
Matrix Spike (P5G0366-MS1) Source: 5070212-01 Prepared: 07/21/15 Analyzed: 07/22/15
Ammonia as N 243 6.9 mg/kg dry 171.5 60.9 106 80-120
This report should'nobbe reproduced,- ezcepbin its entirety; without4he written consent of:Prism Laberatories, lnc.
449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page $r:Of •l2

Level II QC Report
n
R
Full -Service Analytical &
I
7/24/15
r
I S
M
Environmental Solutions
®'�ueoruiogiEg ixc
-
City of Statesville, NC
Project: StaLime (Qtrly, & BiWeeklyl)
Prism Work Order: 5070212
Attn: Andy Smith
Time Submitted: 7/13/2015
3:35:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting
Spike
Source %REC
RPD
Analyte
Result Limit Units
Level
Result %REC Limits- RPD
Limit Notes
Batch MOM - NO PREP
Matrix Spike Dup (P5G0366-MSD1)
Source: 5070212-01
Prepared:
07/21/15 Analyzed: 07/22/15
Ammonia as N
243 6.9 mg/kg dry
171.5
60.9 106 80-120 0.03
20
This report should not:be reproduced,except in its entirety,, without, the,writtemcgnsent of, Prism Laboratories Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-800/529-6364 - Fax: [phone] Page.9 .of 12

Level II; QC Repertr••-
ep
a Full -Service Analytical8
PR I..S M I .Envlronmentai Solutions -
®�ua'.x,6MFgiWE
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 5070212
Attn: Andy Smith Time Submitted: 7/13/2015 3:35:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level , Result %REC Limits RPD Limit Notes
Batch P5G0258 - NO PREP
Blank (P5G0258-BLK1) Prepared & Analyzed: 07/14/15
Fecal Coliforms BRL 0.2 MPN/g wet
1
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
5070212-01
P5G0230
0.05 g
25 mL
07/15/15 12:15
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Date/Time
5070212-01
P5G0217
1 g
50 mL
07/15/15 6:20
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
5070212-01
P5130201
30 g
30 g
07/14/15 11:26
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
5070212-01
P5G0273
50 mL
50 mL
07/16/15 10:00
5070212-01
P5G0273
50 mL
50 mL
07/16/15 10:00
Prep Method: 3060B
Lab Number
Batch
Initial
Final
Daterrime
5070212-01
P5130221
1.98 g
50 mL
07/15/15 8:30
5070212-01
P5130221
1.98 g
50 mL
07/15/15 8:30
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
5070212-01
P5G0270
0.6 g
50 mL
07/16/15 10:40
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
5070212101
P5130240
250 g
250 1. .g
07/15/15 7:30
This :reportshould.not;be;reproduced,; except inits,entirety,.withoutthewritte ,consent of Pr ismLaboratories lec,,•,;_
rS
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543-
Phone:[phone]- Toll Free Number: 1-800/529-6364- Fax: [phone] Page.lQ:Of 2

CHAIN OF CUSTODY RECORD'� LAB USE ONLY
Full -Service Analytical & YES Na. N/A N°
SM Environmental Solutions PAGE_ OF- v QUOTE !/ TO ENSURE PROPER BILLING: - S8mp10 JNTA0. Upon arrlt "N r +" O
vim,'! Vrf kl;. a%7
,3.y`�LABORATORIES, INC. ftecelved 0NWFRT-.AQ-V
Project Name: r
449 Springbrook Road • Charlotte, NC 28217 'I?ROPER PRESERVATIVES lneijcail, _ _ 0)
Phone [phone] Fax: [phone] Short Hold Analysts: (Yes) (No) UST Project: (Yes) (NO)
�1 `Please ATTACH any project specific reporting (QC LEVEL I It III IV) Reesrvec}�lSI1THlN HOLDINGTIMES�,,;
Client -Company Name: C+ y OP W454E Wd l e provisions and/or QC Requirements CUSTt�DY;SEALS INTACT?
Report To/Contact Name: Ii /V S nr r Invoice To: VQLATit �S rec d +NCOUT kIEADSPACE?:
PRQPI~RrCQNTAINERSnsed?,
Reporting Address: Address: HEMP, Tn rtn lA il* 4D , Obse..rved
Phone:70`1- 87 Sr- 3131T Fax es (No):70- 870- Sd S5 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email, --Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DoD FL NC
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre Approved SC OTHER N/A
Site;Locatlon Name: our r't Creek Lt?�7 F Samples received after 14:00 will be processed next business day.
Site. Location Physical Address: 6 93 6// rA.im Turnaround time Is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection' YES_ NO
.S4a rs vrUe_ AIC RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p p --
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE
CONTAINER
PRESERVA-
TNES
ANALYSIS REQUESTED
�h REMARKS
lY�P,S �llP
PRISM
LAB
ID,NO.
'TYPE
SEE BELOW
NO.
SIZE
aasa03
As
QIVAI-
VA-51�
S
p
C9
Cu
(�T► _ I,,,Q �.I`'
13S)
Sampler's Signature r, a. i�j �l.'��z I Sampled By (Print
Upon relinquishing, this Chain of Custody is your authorization for Prism
submitted In writing to the Prism Project Manager. There will be charges
Affiliation
with the analyses as requested above. Any changes must be
nges after analyses have been Initialized.
Drat , � Mlltt:
J V0-
SAMPLES ARE NOT CEPTED AND VERIFIED AGAINST COC L RECEIVED AT THE LABORATORY. �� -7 d X t L
ed;Ex UPS O Hand delivered rlsm Fleld Service ❑ OtherOUNDWA_4
❑ NC ❑ SC ❑ NC ❑ SC ❑ C ❑ SCGFkTER: DRINKING
NC I O CATER: I ❑ NC ❑ SCSOLID E. I ❑ �❑ SC I ❑❑ NC ❑ SC I ❑ NC F❑ SC ILL I ❑❑ NC ❑ SC
❑ I ❑ I ❑ I ❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Comments:
SEE REVERSE FOR
TERMS & CONDITIONS
ORIGINAL

rf.
CHAIN OF CUSTODY RECORD
w,`♦w,Full-Service Analytical & ''}} �
Environmental Solutions PAGE_ OF_J/ QUOTE IF TO ENSURE PROPER BILLING
:.:'. ,
`� LABORATORIES INC
c Project Name:
449 Springbrook Road •Charlotte, NC 28217 Short Hold Analysis: es No UST Project: es NO
Phone [phone] Fax: [phone] y ) ( ) j ) ( )
C o SWES ✓��//1r. - 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
;6lent Company Name: provisions and/or QC Requirements
'.Report-To/Contact Name: /� I✓ y Sr> % h Invoice To:
Reporting Address: Address:
Phone:10 *7F-3Y3 Fax es (No): ��y-ff9�' Purchase Order NoJBilling Reference
Email. Ad dress: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
EEC T e' PDF_Excel Their 'Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
yp. , (: 9 Y y Pre -Approved
Site Location Name: A-ouR 1 --ec
— � Samples received after 14:00 will be processed next business day.
Site Location Physical Address' 1-3 E/.44,n Turnaround time is based on business days, excluding weekends and holidays.
r (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
S A4 EiVI hP. 1Vr RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED.
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
*TYPE
SEE BELOW
NO.
SIZE
S
/0
SSA- �,,Mc
3 /'
13.4
13.E s P
Sampler's Signature 6Deni4 a 1 _ Sampled By (Print Name)
Upon,relinquishing, this Chain of Custody is your authorization for Prism to proo
submitted In writing to the Prism Project Manager. There.will be charges for a
PRESERVA-
TIVES
E
A
`Q__ Fj' H_ It I, rvF'' I Affiliation
mr.1.
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNI
Certification: NELAC DOD FL NC
SC OTHER NIA
Water Chlorinated: YES_ NO_
Sample Iced Upon Collection: YES_ NO_
with the analyses as requested above. Any changes must be
iges after analyses have been Initialized.
ARE NOT ACCEPTED AND VERIFIED AGAINST C,KUNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS" Hand -delivered Wrism Field Service ❑
0-70�Z.
0NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SC ❑NC ❑SC ❑NC ❑SC 1 ❑NC ❑S
"CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
PRISM
REMARKS LAB
ID NO.
0
Additional Comments:
SEE REVERSE FOR
TERMS 8 CONDITIONS

Full -Service Analytical&
60D R I S M I Environmental Solutions
®�LABORATORIE9, INQ
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012 Case Narrative,
NC Drinking Water Cart No. 37735 08/11/2015
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-BAccredited Certificate No. L2307
Project: Stal-ime (60 Day/7 Fecal)
Lab Submittal Date: 08/04/2015
Prism Work Order: 5080020
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V L.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
t
Reviewed By Robbi A. Jones
President/Project Manager
A No recovery of spike. Matrix Interference is suspected.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample. concentrations are greater than 10x the MB.
DM Sample diluted and RL increased due to the matrix. .
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
xr<-,rtnThisreport should:notbereproduced ;.except;in.itsentirety,.withoutthe;written:consentof;P.rism;Laboratories,Inc.;:„.
.449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number 1-8001529-6.364-Fax: 704/52"409 <'Page.'1 'of.16

Sample Receipt Summary
Full-Service
Environmental Solutions 08/11/2015��uLqv
.. ..
Prism Work Order: 5080020
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Stal-ime (and Fecal 1)
5080020-01
Solid
08/03/15
08/04/15
Fecal #2
5080020-02
Solid
08/03/15
08/04/15
Fecal #3
5080020-03
Solid
08/03/15
08/04/15
Fecal #4
5080020-04
Solid
08/03/15
08/04/15
Fecal #5
5080020-05
Solid
08/03/15
08/04/15
Fecal #6
5080020-06
Solid
08/03/15
08/04/15
Fecal #7
5080020-07
Solid
08/03/15
08/04/.15
Samples were received at 24.7 degrees C. See case narrative for further information.
,,;* ,,n, ; ., .; , r _ This,report,sh,ould not be,reproduced ,except.n ts,entirety without the -mitten consentof Prism Labo[ataries Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-8001529-6364 - Fax: [phone] Rage:;2:. of =16.

a Full Service Analytical 8
P R I S M I Environmental Solutions
1�LA90MTONIE4ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime-(60 Day/7 Fecal)
Sample Matrix: Solid
i
Laborai`
Client Sample ID: StaLime (an(an\l-i
Prism Sample ID: 5080020-01
Prism Work Order: 5080020
Time Collected: 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter
Result
Units,
Report
MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Tme
ID
General Chemistry Parameters
Plant Available Nitrogen
510
mglkg
160
60
2
*Calculation BMI116 9:34
CLB
ICALC]
% Solids
94.8
% by
0.100
0.100
1
•SM2540 G 8/4/15 16:46
EGC
PSH0054
Weight
Nitrate/Nitrite as N
14
mg/kg dry
5.3
0.58
1
'SM4500-NO3'F 8/11/15 9:34
CLB
P5H0136
Total Kjeldahl Nitrogen
1700
mg/kg dry
530
210
2
•361.2 811115 9:12
CLB
PSH0085
Ammonia as N
13
mg/kg dry
6.3
1.2
1
'SM4500-NH3 G 8110115 9:27
CLB
PSH0073
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1. •SM9221 E 814/15 10:54 EGC P51­10067
Total Metals
Mercury
0.13
mg/kg dry
SAR Soil Preparation
Complete
g
SAR Percent Moisture
51.4
% by
Weight
Arsenic
5.8
mg/kg dry
Sodium Absorption Ratio
0.94
[blank]
Cadmium
BRL
mg/kg dry
Calcium
2500
mglL
Copper
23
mg/kg dry
Lead
12
mglkg dry
Magnesium
BRL
mg/L
Nickel
110
mglkg dry
Selenium
BRL
mg/kg dry
Sodium
170 B
mg/L
Zinc
51
mg/kg dry
0.021
0.0014
1
`7471B
81611511:12
JAB
PSH0077
1
'2-78-054
8/6/15 8:30
JAB
P51­10053
0.100
0.100
1
'2-78-054
816115 8:45
JAB
PSH0084
2.6
0.38
10
'6010C
81611517:17
MWW
PSH0076
0.30
0.016
1
'2-78-054
817/1518:59
MWW
PSH0078
2.6
0.37
10
'6010C
8/6/15 17:17
MWW
P5H0076
1.0
0.085
10
•6010C
817/15 18:59
MWW
PSH0078
5.3
0.96
10
•6010C
8/6/1517:17
MWW
PSH0076
2.6
0.40
10
•6010C
8/6115 17:17
MWW
PSH0076
1.0
0.0070
10
'6010C
8/7/15 18:59
MWW
P51­10078
11
1.4
10
'6010C
8/6115 17:17
MWW
061-10016
5.3
0.63
10
'6010C
8/6/15 17:17
MWW
P5H0076
5.0
0.074
10
'6010C
8/7/15 18:59
MWW
PSH0078
26
5.8
10
•6010C
8/6/15 17:17
MWW
PSH0076
t. ;This report=shouId;not be. reproduced, -except,in: its ientirety,y.Wlth out.the writte n cc ns ant. of Prism Laboratories; I no,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number.1-800/529-6364 - Fax: 704/52U409
Pa9@. 3 Of 6

Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report'
08/11/2015
Client Sample ID: Fecal #2
Prism Sample ID: 5080020-02
Prism Work Order: 5080020
Time Collected-, 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter Result
Units
Report
MDL Dilution
Method Aniilysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 95.6
% by
0.100
0.100 1
*SM2540 G 814115 16:45 EGC
P5H0064
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 8/4/15 10:54 EGC
inIts,-entirety, without;thaiwritten;consent-of,Odsm,Labor.atorie&ilnc,,.,,;-,u= �,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone]

r
FI'& � ^ n Fu11-Service Analytical&
a ISM V' Environmental Solutions
�✓ IABOMTOH1Eq INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC.28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report,
08/11 /2015
Client Sample ID: Fecal #3
Prism Sample ID: 5080020-03
Prism Work Order: 5080020
Time Collected: 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefl-ime
ID
General Chemistry Parameters
% Solids 93.7
% by
0.100
0.100 1
*SM2540 G 8/4115 16:45 EGC
P5H0064
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 8/4/15 10:54 EGC
P51­10067
'' :: = • Thisaeport should not be reproduced, exespt.in its entirety, without the:written,consent of P_rism:Laboratories, Inc._
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -.Toll Free Number: 1-800/629-6364 - Fax: 704/52"409 Page

Full -Service -Analytical &
A&MIN R I M I Environmental Solutions
�LA�bnATOME41N6
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report r
�i
0$/11/2015
Client Sample ID: Fecal #4
Prism Sample ID: 5080020-04
Prism Work Order: 5080020
Time Collected: 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateRme
ID
General Chemistry Parameters
% Solids 96.8
% by
0.100
0.100 1
•SM2540 G 8/4115 16:45 EGC
P5H0054 '
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 8/4/15 10:54 EGC
P5H0067
r
>,.This.report should not Nk reproduced; exceptin its,entirety „withqut the,written,co Aent of Prism,l,abpratories-
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-800/529-6364 - Fax: [phone] P,.agt?',6-of 1 6

GORE I S n M I Funironmen al lotion s
'v.' Environmental Solutions
`®"uaoruianeaiNa-
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
08/11 /2015
Client Sample ID: Fecal #5
Prism Sample ID: 5080020-05
Prism Work Order: 5080020
Time Collected: 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
% Solids 95.2
% by
0.100
0.100 1
'SM2540 G 8/4115 16:45 EGC
135110054
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 8/4/15 10:54 EGC
P51-10067
This•report'should.not be reproduced; except=n, its:entirety„without the•written;consentof.Prism; Laboratofies,;Jnc
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 26224-0543
Phone: [phone] -Toll Free Number. 1.800/529-6364 - Fax: 704/52M409 Page•'T-:Of'.� 6

Laboratory Report -,
Full -Service Analytical 8-
R I S'M I Environmental Solutions OS/11I2d1b .Y
�IAeOR�rOHIE4ING
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #6
Attn: Andy Smith Prism Sample ID: 5080020-06
P.O. Box 1111 Prism Work Order: 5080020
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateRme ID
General Chemistry Parameters
% Solids 95.8 % by 0.100 0.100 1 "SM2540 G 814116 16:45 EGC PSH0064
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 8/4/15 10:54" EGC • P5HOO67'
reportshould.not;be.teproduced„-except,in,ils;entjrsty,Nithautthe..wr!4e,n copsentof P.,rism-Laboratories,,,lnc ,,.
"9 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OM
Phone: [phone] - Toll Free Number: 1.8001529-6364 - Fax: 704152"409 Page.: B.Of � 6

r
®® Full -Service Analytical a
Environmental Solutions
�{w60MiOPIFB',xG.
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal)
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
08/11/2016
Client Sample ID: Fecal #7
Prism Sample ID: 5080020-07
Prism Work Order: 5080020
Time Collected: 08/03/15 13:00
Time Submitted: 08/04/15 08:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Dateffime
ID
General Chemistry Parameters
% Solids 94.9
% by
0.100
0.100 1
"SM2540 G 8I4/15 16:45 EGC
PSH0054
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 8/4/15 10:54 EGC
P51­10067
This ,repatshould not be-reproduced;,except in its -entirety; without the; written.consent.of Prism Laboratories;, Inc A. f,s r
449 Springbrook Road -P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-800/529-6364 - Fax: 704/52"409 Pa9e;;9,Of=� 6

Level ll: QC Report°-•,
FUFull -Service Analytical & - f
R I SM I Environmental Solutions
��LA00MTOflIE$ INQ
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Prism Work Order: 5080020
Attn: Andy Smith Time Submitted: 8/4/2015 8:30:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5H0053 - SAR 2-78-054
Blank (P51-10053-BLK1)
Prepared: 08/05/15 Analyzed: 08/06/15
SAR Soil Preparation
Complete
g
Batch P5H0076 - 3050B
Blank (P5H0076-BLK1)
Prepared & Analyzed: 08/06/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (1551-110076-13SI)
Prepared & Analyzed: 08/06/15
Arsenic
26.8
0.25
mg/kg wet
25.00 107
80-120
Cadmium
27.4
0.25
mg/kg wet
25.00 110
80-120
Copper
29.2
0.50
mg/kg wet
25.00 117
80-120
Lead
27.1
0.25
mg/kg wet
25.00 109
80-120
Nickel
27.3
1.0
mg/kg wet
25.00 109
80-120
Selenium
26.0
0.50
mg/kg wet
25.00 104
80-120
Zinc
27.0
2.5
mg/kg wet
25.00 108
80-120
Matrix Spike (P5H0076-MS1)
Source: 5080020-01
Prepared & Analyzed: 08/06/15
Arsenic
32.3
2.6
mg/kg dry
26.36 5.78 101
75-125
Cadmium
24.2
2.6
mg/kg dry
26.36 BRL 92
75-125
Copper
48.5
5.3
mg/kg dry
26.36 22.9 97
75-125
Lead
35.7
2.6
mg/kg dry
26.36 12.4 89.
75-125
Nickel
135
11
mg/kg dry
26.36 114 79
75-125
Selenium
BRL
5.3
mg/kg dry
26.36 BRL
75-125 A
Zinc
74.1
26
mg/kg dry
26.36 50.6 89
75-125
This report should not be. reproduced, except in its entirety,. without the written consent of Prism Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] eiIg'610O 6f 16

�s;
n; Full -Service Analytical &
P R I •S M I Environmental Solutions
��LABOH�T0RIEs ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P51­10076 - 3050B
Project: Stal-ime (60 Day/7 Fecal)
Level II QC Report
8/11/15 `
Prism Work Order: 5080020
Time Submitted: 8/4/2015 8:30:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P5H0076-MSD1)
Source: 5080020-01
Prepared & Analyzed: 08/06/15
Arsenic
34.4
2.6
mg/kg dry
26.36 5.78 10B
75-125
6
20
Cadmium
26.1
2.6
mg/kg dry
26.36 BRL 99
75-125
8
20
Copper
48.2
5.3
mg/kg dry
26.36 22.9 96
75-125
0.7
20
Lead
38.3
2.6
mg/kg dry
26.36 12.4 98
75-125
7
20
Nickel
131
11
mg/kg dry
26.36 114 64
75-125
3
20
Selenium
BRL
5.3
mg/kg dry
26.36 BRL
75-125
20 A
Zinc
74.2
26
mg/kg dry
26.36 50.6 90
75-125
0.2
20
Post Spike (P5H0076-PSI)
Source: 5080020-01
Prepared & Analyzed: 08/06/15
Arsenic
1.09
mg/L
1.000 0.219 87
80-120
Cadmium
0.939
mg/L
1.000 0.00824 93
80-120
Copper
1.14
mg/L
1.000 0.870 27
80-120
Lead
0.993
mg/L
1.000 0.469 52
80-120
Nickel
1.31
mg/L
1.000 4.34 NR
80-120
Selenium
0.950
mg/L
1.000 -1.11 95
80-120
Zinc
1.20
mg/L
1.000 1.92 NR
80-120
Batch PSH0077 - 7471 B
Blank (P5H0077-BLK1)
Prepared & Analyzed: 08/06/15
Mercury
BRL
0.020
mg/kg wet
LCS (P5H0077-BSI)
Prepared & Analyzed: 08/06/15
Mercury
0.441
0.020
mg/kg wet
0.4167 106
80-120
Matrix Spike (P5H0077-MS1)
Source: 5080020-01
Prepared &Analyzed: 08/06/15
Mercury
0.566
0.021
mg/kg dry
0.4468. 0.133 . 97
80-120
"This report' should not bd reproduced, -except -in- its, entirety,'without the'wriften consent of Prism Laboratories, Inc:,` .,r•; .' ..> r-
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1.800/529-6364 - Fax: [phone] Page 1 1 'Of � 6

Level II -QC, Report--,
�Fara r, Full -Service Analytical &
( I Environmental Solutions
®'i�uieorviroMEs. wa
City of Statesville; NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime (60 Day/7 Fecal)
Prism Work Order: 5080020
Time Submitted: 8/4/2015 8:30:OOAM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P5H0077 - 7471 B
Matrix Spike Dup (P5H0077-MSD1)
Source: 5080020-01
Prepared & Analyzed: 08/06/15
Mercury
0.547
- 0.021
mg/kg dry
0.4321 0.133 96 80-120 3 20
Batch P5H0078 - 3010A
Blank (P5H0078-BLK1)
Prepared: 08/06/15 Analyzed: 08/07/15
Sodium Absorption Ratio
BRL
0.30
[blank]
Calcium
BRL
0.10
mg/L
Magnesium
BRL
0.10
mg/L
Sodium
0.921
0.50
mg/L
Batch P5HOO84 - NO PREP
Blank (P5H0084-BLK1) Prepared & Analyzed: 08/06/15
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (P5H0084-DUP1) Source: 5080020-01 Prepared & Analyzed: 08/06/15
SAR Percent Moisture 53.4 0.100 % by Weight 51.4 4 200
--.This report should pot,be.re roduced, exce t in. its entirety, without the wrilten.consent of Pds Laboratories;;Inc: •,, .;, :,>r_,-;:•;,.::,; .-,.,: -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-800/529.6364 - Fax: [phone] Page U.bf IT 6

ra Full-ServiceAnalytical &
�p I M I Environmental Solutions
®�L�eOMTOME& 1n
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Level II QC Report
8/11/15
Project: Stal-ime (60 Day/7 Fecal) Prism Work Order: 5080020
Time Submitted: 8/4/2015 8:30:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5HOO54 - Solids, Dry Weight
Blank (P5H0054-BLK1) Prepared &Analyzed: 08/04/15
% Solids 99.9 0.100 % by Weight
Duplicate (P5H0054-DUP3) Source: 5080020-06 Prepared & Analyzed: 08/04/15
% Solids 95.7 0.100 % by Weight 95.8 0.1 20
Batch P5H0073 - NO PREP
Blank (PSH0073-BLK1) Prepared & Analyzed: 08/06/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (PSH0073-BSI) Prepared & Analyzed: 08/06/15
Ammonia as N 123 5.0 mglkg wet 1.25.0 99 80-120
Matrix Spike (P5H0073-MS1) Source: 5080020-01 Prepared: 08/06/15 Analyzed: 08/10/15
Ammonia as N 146 11 mglkg dry 131.8 13.3 101 80-120
Matrix Spike Dup (PSH0073-MSD1) Source: 5080020-01 Prepared: 08/06/15 Analyzed: 08/10/15
Ammonia as N 147 11 mg/kg dry 131.8 13.3 102 80-120 0.6 20
Batch P5H0085 - 351.2
Blank (P5H0085-BLK1) Prepared: 08/06/15 Analyzed: 08/07/15
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P5H0085-BSI) Prepared: 08/06/15 Analyzed: 08/07/15
Total Kjeldahl Nitrogen 541 100 mg/kg wet 500.0 108 90-110
This report should not be:reproduced, except in its entirety, without the written consent of Prism Laboratories,anc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 -Fax: [phone] Page ;13.of .16

p P ' n ,wa /A' Full -Service Analytical &
�I,S t Y , I Environmental Solutions
®ueori�romes �r+c
Level ,II QC Report
'8111115
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 5080020
Attn: Andy Smith Time Submitted: 8/4/2015 8:30:OOAM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit ' Units Level Result %REC Limits RPD Limit Notes
Batch P5H0085 - 351.2
Matrix Spike (P5H0085-MS1)
Source: 5080020-01
Prepared: 08/06/15 Analyzed: 08/07/15
Total Kjeldahl Nitrogen
Matrix Spike Dup (P5H0085-MSD1)
7680 1100 mg/kg dry
Source: 5080020-01
5272 1730 113, 90-110 MI
Prepared: 08/06/15 Analyzed: 08/07/15
Total Kjeldahl Nitrogen
Batch P51­110136 - NO PREP
7250 1100 mg/kg dry
5272 1730 105 90-110 6 20
Blank (1351-10136-BLK1)
Prepared &Analyzed: 08/11/15
Nitrate/Nitrite as N
LCS (P5H0136-BSI)
BRL 5.0 mg/kg wet
Prepared &Analyzed: 08/11/15
Nitrate/Nitrite as N
Matrix Spike (P5H0136-MS1)
51.3 5.0 mg/kg wet
Source: 5080020-01
50.00 103 80-120
Prepared & Analyzed: 08/11/15
Nitrate/Nitrite as N
Matrix Spike Dup (P5H0136-MSD1)
65.4 5.3 mg/kg dry
Source: 5080020-01
52.72 14.2 97 80-120
Prepared & Analyzed: 08/11/15
Nitrate/Nitrite as N
65.5 5.3 mg/kg dry
52.72 14.2 97 80-120 0.2 20
This report should not be reproduced, -except in its entirety, without. the written consent of Prism Laboratories, Inc.,, -
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: 704152M409 Page 14..Of 1.67

Level II QC Report
i
S,
ull-Service Analytical &
F
8/11 h 5"
MR R1
Y
, Environmental Solutions
®�ueoanioaEg uic -
City of Statesville, NC
Project: Stal-ime (60 Day/7 Fecal) Prism Work Order: 5080020
Attn: Andy Smith
Time Submitted: 8/4/2015 8:30:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RFD
Analyte
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5H0067 - NO PREP
Blank (PSH0067-BLK1)
Prepared & Analyzed: 08/04/15
Fecal Coliforms
BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch
Initial Final Date/rime
5080020-01
P51­10085
0.05 g
25 mL
08/06/15 12:15
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daternme
5080020-01
P51­10054
30 g
30 g
08/04/15 16:45
5080020-02
1351-10054
30 g
30 g
08/04/15 16:45
5080020-03
P51­10054
30 g
30 g
08/04/15 16:45
5080020-04
P5H0054
30 g
30 g
08/04/15 16:45
5080020-05
P51­10054
30 g
30 g
08/04/15 16:45
5080020-06
P51­10054
30 g
30 g
08/04/15 16:45
5080020-07
1351-10054
30 g
30 g
08/04/15 16:45
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daternme
5080020-01
P51­10078
50 mL
50 mL
08/06/15 8:45
5080020-01
P51­10078
50 mL
50 mL
08/06/15 8:45
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Datemme
5080020-01
1351­10076
2 g
50 mL
08/06/15 8:05
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/rime
5080020-01
1351-10077
0.6 g
50 mL
08/06/15 8:35
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
5080020-01
1351-10053
250 g
250 g
08/05/15 8:30
This report should not,be:reproduced,except in its entirety, without the written consent of Prism Laboratories, Inc. _
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16,6f 16 .'

ld
if
t,
CHAIN OF CUSTODY RECORD
',v.. ISM
I Full -Service Analytical&
............ ....... Environmental Solutions PAGE_ OF QUOTE # TO ENSURE PROPER BILLING:
. . . . . . . . . . . . . . .
LASORATORIES, INC,
Project Name:
449 Springbrook Road - Charlotte, NC 28217
Phone.[phone] - Fak:704/525-0409 Short Hold Analysis: (Yet) (No) UST Project: (Yes) (NO)
"Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
ClienCCbmpany Name: C,JX
fi/AkPh provisions and/or QC Requirements
Report-_'4Td/Contact Name: , Sr,, :
Invoice To:
Reporting!: Address: Address:
* '7 1
Fax TO BE FILLED IN BY CLIENT/SAMPLING PERSONN'
Ph � i dVw89ff-:7Y39' -V - 9 7 9-Ad5s
onp.Z-,- -- - - U Purchase Order No.[Bllllng Reference
Emaif-; dress: -
Requested Due Date U 1 Day 13 2 Days U 3 Days 0 4 Days 13 5 Days Certification: NELAC DOD FL NC
PDF Excel "Working Days" 13 6-9 Days E3 Standard 10 days C] Rush Work Must Be
EDD-JY,0 Other Pre -Approved SC OTHER N/A
Site , Location Narrie: rae �f CRerle tv to rp Samples received after 14:00 will be processed next business day.
SlteaoTurnaround time is based an business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_
tion Physical Address: 4.93 afit FAR#"
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES NO
VATIF.511"lle NC RENDERED By PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YESNO
MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
:?.IL60-tLIENT DATE COLLECTED (SOIL, PRESERVA- /S 1 REMARKS
COLLECTED MILITARY WATER OR *TYPE TIVI
D NLAB
IO.
SAMPESCRIPTION NO. SIZE V
HOURS SLUDGE) SEE BELOW
C
10 DAv 7 FECA)
C4
03
P1
PA
tJ
5
A
d 7
—
Sampler'sSignature leu sampled By (Print Name) 2xina Affiliation
-
Upon ielinqiLilshlng,.,this'Ghain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be PRISM USE
ONLY
submitted in. writlhg.to_,thePrism Project Manager. There will be charges for any changes after analyses have been initialized.
Relp l!hed,By::(SlgnatureL Kely y. (Sign Date mil"'HOu's Additional Comments:
in u
I /-TZ->
Z.3, :: �t _3_(_
�Rll ly
Date Site re -nrrip:
�Rel1nqW%WZy*.,(Sl a Received By: (Signature) Qepartu
Tech F ee:.,
ReffiqGrithedrBT (Sig re 3d� For Prism Laboratories By. Date On .
0 80v
Mileage:
Methcd,ofShipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT VffrH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY.
•
,0Fed Ei_--_,PUPS U.Hand-delivered rlsm Field Service U Other
DRINKING LANDFILL OTHER:
_UST. GROUNDWATER: INKING WATER. SOLID WASTE: RCRA: CERCLA
I
L] NC L3 Sc El IZI NC ❑ SC I NC U SC IEl013
1 0L3 NC El SC I C3EI NC 0 SC I ElElNC 0 SC NC ❑ SC 0U El NC SC
n 13 - U -❑ ❑ _❑ — —
*CONTAINER TYPE CODES: A=Amber C=Clear G=Glass P=Plastic; TL=Teflon-Lined Gap vuA=voiaiiieorganics t%naiysisteurunuuuopdL;tr)
ORIGINX;L -

/w ISM
'IE% ING.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
gA0,r WK
Project: Sludge (Hazardous Testing)
Lab Submittal Date: 12/21/2015
Prism Work Order: 5120373
Case Narrative
01/06/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for Ignitability:
This method is not required by the Federal regulations to determine if a waste
passes or fails the characteristic of ignitability according to the RCRA regulatory definition at 40
CFR 261.21. To clarify, the test results of this method cannot be used to directly classify a
waste as a D001 hazardous waste, nor can the results be used by themselves to definitively
classify a waste as non -hazardous.
Reactivity analysis subcontracted to GCAL TCLP Herbicide analysis subcontracted to AES . Laboratory
reports are attached.
Please call if you have any questions relating to this analytical report. .
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
.Data Qualifiers Key Reference:
A Sample was taken off rotator on 12/23/2015 @ 06:45.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone:-704/529-6364 -Toll Free Number: 1-8001529-6364 - Fax: [phone] P-age'•' 4if'.'22.

I S M I Full-ServiceAnalytical
Sample Receipt SummaryP uEnvironmental Solutions 01/06/2016 Prism Work Order: 5120373
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Fourth Creek Sludge 5120373-01 Solid 12/21/15 12/21/15
Samples were received at 16.2 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. B6x 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: 704152"409 1 Page.2;Of>22

~' Labo'
Full -Service Analytical & i
Environmental Solutions -
®'S�ueoa�To�ea
1
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID:
Attn: Andy Smith Prism Sample ID: 51203,,
P.O. Box 1111 Prism Work Order: 5120373-,
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/21/15 08:30`
Time Submitted: 12/21/15 16:10
Parameter Result Units Report MDL Dilution Method Analysis Anal
Limit Factor Date/Time
General Chemistry Parameters
Solids
17.2
% by 0.100
0.100 1
`SM2540 G
12/23/15 16:02
ARC
PSL0392
Weight
Ignitability
Pass
mm/sec 0.10
1
*1030
12/28/15 14:20
ARC
P51_0421
pH
6.9
pH Units
1
`9040C
12/23MS 12:37
EGC
P5L0389
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
12/23/15 6:45
JAB
P51_0378
TCLP Extraction
Complete
N/A
1
*1311 ZHE
12/29/15 8:30
ANG
P51_0419
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
'7470A
12/28/15 12:37 JAB
P51_0407
Arsenic
BRL
mg/L
0.050
0.0035
1
'6010C
12/28/15 14:40
BGM
P51_0381
Barium
BRL
mg/L
5.0
0.0035
1
'6010C
12/28/15 14:40
BGM
P51_0381
Cadmium
BRL
mg/L
0.025
0.00050
1
'6010C
12/28/15 14:40
BGM
P51_0381
Chromium
BRL
mg/L
0.25
0.0030
1
'6010C
12/28/15 14:40
BGM
P51_0381
Lead
BRL
mg/L
0.050
0.0065
1
'6010C
12/28/15 14:40
BGM
P51_0381
Selenium
BRL
mg/L
0.10
0.016
1
'6010C
12/28/15 14:40
BGM
P51_0381
Silver
BRL
mg/L
0.25
0.0010
1
'6010C
12/28/15 14:40
BGM
P51_0381
TCLP Organochlorine Pesticides by GC/ECD
A
Chlordane
BRL
ug/L
2.5
0.34
1
'8081B
12/30/15 11:58
JCa
P51_0461
Dieldrin
BRL
ug/L
0.50
0.022
1
'8081 B
12/30/15 11:58
JCa
P51_0461
Endrin
BRL
ug/L
0.50
0.020
1
'8081B
12/30/15 11:58
JCa
P51_0461
gamma-BHC
BRL
ug/L
0.50
0.013
1
'8081 B
12/30/15 11:58
JCa
P51_0461
Heptachlor
BRL
ug/L
0.50
0.015
1
'8081B
12/30/15 11:58
JCa
P51_0461
Heptachlor Epoxide
BRL
ug/L
0.50
0.018
1
'8081 B
12/30/15 11:58
JCa
P51_0461
Methoxychlor
BRL
ug/L
0.50
0.033
1
•8081B
12/30/15 11:58
JCa
P51_0461
Toxaphene
BRL
ug/L
25
0.16
1
'8081B
12/30/15 11:58
JCa
P51_0461
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
2,4,6-Trichlorophenol
BRL
2,4-Dinitrotoluene
BRL
2-Methylphenol
BRL
3/4-Methylphenol -
0.058
Hexachlorobenzene
BRL
Hexachlorobutadiene
BRL
Hexachloroethane
BRL
Nitrobenzene
BRL
Pentachlorophenol
BRL
Surrogate Recovery Control Limits
Decachlorobiphenyl 66 % 13-186
Tetrachloro-m-xylene 62 % 40-134
mg/L
0.25
0.0023
1
'8270D
12/29/15 19:26 JMV
P51_0451
mg/L
0.10
0.0026
1
'8270D
12/29/16 19:26 JMV
P51_0451
mg/L
0.050
0.0019
1
'8270D
12/29/15 19:26 JMV
P51_0451
mg/L
0.050
0.0021
1
'8270D
12/29/15 19:26 JMV
P51_0451
mg/L
0.050
0.0019
1
'8270D
12/29/15 19:26 JMV
PSL0451
mg/L
0.050
0.0019
1
'8270D
12/29/15 19:26 JMV
P51_0451
mg/L
0.050
0.0026
1
'8270D
12/29/15 19:26 JMV
P51_0451
mg/L
0.050
0.0025
1
'8270D
12/29/16 19:26 JMV
P51_0451
mg/L
0.050
0.0024
1
'8270D
12/29/15 19:26 JMV
P51_0451
mg/L
0.25
0.0025
1
'8270D
12/29/15 19:26 JMV
P51_0451
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 6f .22

LaboratoryRed„/oi�....i1
� rR FII-Service Analytical & • "
I S M
P ; Enuvironmental Solutions 01/06/2016 1
®�Iaet)wDRIFA INC.
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: Fourth Creek Sludge
Attn: Andy Smith Prism Sample ID: 5120373-01
P.O. Box 1111 Prism Work Order: 5120373
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/21/15 08:30
Time Submitted: 12/21/15 16:10
Parameter
Result
Units
Report MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateMme
ID
Pyridine
BRL
mg/L
0.25 0.0021
1
'8270D
12/29/15 19:26 JMV
P51_0451
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
62 %
43-140
2-Fluorobiphenyl
61 %
44-119
2-Fluorophenol
24 %
19-119
Nitrobenzene-d5
58 %
44-120
Phenol-d5
15 %
11-52
Terphenyl-d14
70 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35 0.83
1
'8260B
12/30/15 23:25
KDM
P51_0491
1,2-Dichloroethane
BRL
ug/L
25 0.66
1
'8260B
12/30/15 23:25
KDM
P51_0491
1,4-Dichlorobenzene
BRL
ug/L
380 0.50
1
'8260B
12/30/15 23:25
KDM
P51_0491
Benzene
BRL
ug/L
25 0.48
1
'8260B
12/30/15 23:25
KDM
P51_0491
Carbon Tetrachloride
BRL
ug/L
25 1.1
1
'8260B
12/30/15 23:25
KDM
P51_0491
Chlorobenzene
BRL
ug/L
5000 0.62
1
'8260B
12/30/15 23:25
KDM
P51_0491
Chloroform
BRL
ug/L
300 0.76
1
'8260B
12/30/15 23:25
KDM
1351-0491
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
10000 2.4
1
'8260B
12/30/15 23:25
KDM
P51_0491
Tetrachloroethylene
BRL
ug/L
35 0.98
1
'8260B
12/30/15 23:25
KDM
P51_0491
Trichloroethylene
BRL
ug/L
25 0.78
1
'8260B
12/30/15 23:25
KDM
P51_0491
Vinyl chloride
BRL
ug/L
20 0.97
1
'8260B
12/30/15 23:25
KDM
P51_0491
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
97 %
80-124
Dibromofluoromethane
98 %
75-129
Toluene-d8
96 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4�Of 22

Sample Extraction Data
Prep Method: Solids, Dry weight
Lab Number
Batch Initial
Final
Daterrime
5120373-01
P51_0392 30 g
30 g
12/23/15 16:02
Prep Method: 1311
Lab Number
Batch Initial
Final
Datemme
5120373-01
P51_0419 25 g
500 mL
12/28/15 14:15
5120373-01
P51_0378 100 g
2000 mL
12/22/15 14:10
Prep Method: 3010A
Lab Number
Batch Initial
Final
Date/rime
5120373-01
1351-0381 10 mL
50 mL
12/23/15 10:55
Prep Method: 7470A
Lab Number
Batch Initial
Final
Datefrime
5120373-01
P51_0407 20 mL
30 mL
12/28/15 8:30
Prep Method: 3510C GC
Lab Number
Batch Initial
Final
Daterrime
5120373-01
1351-0461 200 mL
10 mL
12/30/15 7:35
Prep Method: 3510C MS
Lab Number
Batch Initial
Final
Date/Time
5120373-01
P51_0451 200 mL
1 mL
12/29/15 11:30
Prep Method: 5030B
Lab Number
Batch Initial
Final
Daternme
5120373-01
P51_0491 1 mL
10 mL
12/30/15 8:20
Subcontracted Analyses
The following analyses were subcontracted to Analytical
Environmental Services,
Inc.
Lab Number
Analysis
5120373-01
Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast
Analytical Labs, Inc.
Lab Number
Analysis
5120373-01
Reactivity, Cyanide (Sub)
5120373-01
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 22

A" CHAIN OF CUSTODY RECORD
r :� SM - Full -Service Analytical &
Environmental Solutions PAGE-- OF _ QUOTE # TO ENSURE PROPER BILLINA: -
<
,as .rc .,t ma t7-,_„ LABORATORIES, INC. '
449 Springbrook Road • Charlotte, NC 28217 Project Name:
Phone [phone] - Fax: [phone] Short Hold Analysis: (Yes) (No) UST Pro!' (Yes) (NO)
Client Company Name: C;& of VA trs V< Me "Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Report To/Contact Name: AN y Sry,'%/� provisions and/or QC Requirements
Invoice To:
Reporting Address: Address:
YES NC1 N A ..
...Samples INTACT upon arri4a17
Received ON WET ICE? :
PROPER PRESERVATIVES mdicat4
:Received WITHIN.HOLDING TIMES?
CUSTODY SEALS INTACT'?
VOLATILES reed WIOUT HEADSPACE?
.PROPER CONTAINERS used?.
TEMP: Therm ID: 2t7— D .Obsei'Ved:iilky
°.C/Corr:.- ..'-'0
Phone '70y- X'IY- ri'f-3Y Fax es No): 7D7-XVY- FfZS5 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel; Other 'Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
Work Must Be Pre-pproved
f CREE 14w
SC OTHER NIA
Site Location Name: u4 P % Samples received after 14:00 will be processed next business day.
, y(�'
Site Location Physical Address: 61,3 id E/ FARM /Cdt , Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
1 (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
5 A ESQ, ile � RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES_ NO_
p p
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
���5
1 REMARKS
LAB
`TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
L
ID NO.
HOURS
SLUDGE)
SEE BELOW
.
&4h
coR
o 3;vi%1V
TC1,P AArz p a
0
Sl 4
ZV,
.A i'
EA
it�V+'
C
it
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P
Zell
ZJ
Sampler's Signature /ti' Sampled By (Print Name) ,f"A ti r^, c K Affiliation
Upon relinqulshing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be ONLY
submitted in writing to the Prism Project Manager. There will be -chsrges for any changes after analyses have been initialized.
Relln shed By: (Signature) Rec iv By: (Sig natur Date Milita ours
�%� r� !� , Additional Comments: 15fte`i4rriGal;Time;� -'
Reli Is d By: (Signature) Rece a By: (Signature
uls ed By: (Signatu Received For m Labora es B Date Field Tech Fee
�? /44 i
CO ; d of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BET, SHUT WfrH TODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Grow No. .
SAMPLES ARE NO AC EPTEO AND VERIFIED AGAINST CO L RECEIVED AT THE LABORATORY.CD
` �}
Hand
_ Ex ❑ UPS ❑ -delivered sm Field Service ❑ Other-
`. ES: UST: G O NDWATER: DRINKING VJATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: '
N ❑ SCI NC ❑ SC I O NC ❑ SC O❑ NC ❑ SC ❑❑ NC ❑ SC NC ❑ SC O❑ NC ❑ SC NC ❑ SC O❑ NC ❑ SC`' '
❑❑ ❑❑ I;
I
r�.
TAINER TYPE CODES. A Amber C Clear G Glass P Plastic, TL Teflon Lined Cap VOA -Volatile Organics Analysis (Zero Head Space) QF;ii u[NAL %�
::cxr.-cTra:W;m,,,:•-.r:rJ:r .—[:: r�J:ra.-- r :--r . 'r __ __'_- __ ' __ _— __ _ _ _ __ —'_'
. r . r . � .... r . • � ..... � .: r I.-i.rJJJJJIJ.....i �.r:.�. i �.r.r.r.:.r.�J.r.r..r,� r„ JJ.r.. _r. J...r.: � r,r.r,rJ... ..............!_ :lJJ:. .. r � ..•............:.r:.�..,,�.v�JJJ�.u.r.rif �rJJ. JJ:rJJ. JJ.r. ..'�J:{r:....lJ:ej;'

�� e-•�vL4.'4S�?i-''45i4o ''•;ti- �:�.: '4 � aw '�.; _ 'a} lm � _ _ ___ _ _ __ ktix.-.�3 .. e.� �;�%'u+3k.A4.�.t4-. �._v_ _'h'k_.. ,: ti•:�_'.3�.3A'4'L�^h:-�:s"aa?� -v3 .. �v::�i� � ti? Y ��3A:.:jyy\::'.is _ v�vs-3.�� t: v?�-�:ae�e-�::- -;a
i.
ACCESS
ANALYUCAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Angie Overcash
PROJECTID
5120373
LABORATORY REPORT NUMBER
215122415
DATE
01 /04/2016
Primary Data Revie Secondary Data Review By
SUM . Ashley B. Amick
Authorized Signature Project Manager, Access Analytical, Inc.
aam ick@accessanalytical inc. com
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01956,
NELAP certified laboratory # 01955
Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 216122415
Page 7 Af 22` ...
I.

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NELAP CERTIFICATE NUMBER: 01955
C Mu L w DOD FLAP CERTIFICATE NUMBER: L14=243
ANOTC`'tii Lager 7TORit LLC
ANALYTICAL RESULTS
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70M
Report Date 01/04/2016
IIGCAL Report2I�15122615
Project 5120373
Deliver To Additional Recipients
Angie Overcash NONE
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
L< *WM
IPJLA
ustsua
nan LMM
Lab Report#: 215122415
.< N46-,8.of=22

.-s�:<<:':'i�3i:tgs �: i':: se:-'ki• - t�... s4 �.-l�:•::39-::S:eS Aa.. <_c�4-tw> a. 25YY a q^1 :'+?e. `.'.' �s.A,ti1�Y 1�:
• - •. eS•itii..t... 9 %e
r
Report#: 215122415
�� nrccAOPAT— on�s5. rr Project ID: 5120373 Report Date: 01/04/2016
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period. the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
DL Diluted analysis — when appended to Client Sample ID
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or 1 Indicates the result Is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009-and terms and conditions -of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and In the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report Is in compliance with the DOD QSM as specified in the contract if
applicable.
Lab Report#: 215122416
Page 9 of 22

I
AO ANALYTICAL LAHOPA70RIM LLO
Report#: 215122415
Project ID: 5120373
Certifications
10/02/2015
Report Date: 01/04/2016
Certification
Certification Number
DOD ELAP
L14-243
Alabama
01955
Arizona
AZ0718
Arkansas
12-060-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia.
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
USDA Soil Permit
P330-10-00117
Lab Report#: 215122415 . Page 10 of 22

GCAL
=LL� .... MI.I. U.
Client: Access Analytical
Report#: 215122415
Project ID: 5120373
Case Narrative
Report: 215122415
Report Date: 01/04/2016
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found in the analyzed sample(s).
Lab Repodt 215122415
Page ;14-&72-2—

- o: 3. �--:' '^• sy^1`.,•.4 =S :;'�� - � 6 _ - _ ti.l1.49'..A '::'�'> `� 4'` "._�'� a
-� i-i,.:z:' 'a s 7=H.•�.. .�*: w afi-. rG ;�.:S.:�.i+:�w� 4=:'* ... .t_<'x.°.3`c x..-, v IN.
GCAL Report#: 215122415
�
ariAIvTicaL LneOPATO'" niEs: «� Project ID: 5120373
Report Date: 01/04/2016
Sample Summary
GCAL ID Client ID Matrix Collect DatelTime Receive DatelTime
21512241501 FOURTH CREEK SLUDGE Solid 12/21/2015 08:30 12/23/2015 11:08

FIN'.
Reoort#: 215122415
GCALProject ID: 5120373
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Report Date: 01/04/2016
Lab Report#: 215122415 -;Parel 17-672-2

__ __ _ _ _ ___
«.• -_tom._ _ _ _
�S6 a �i'". { t ". 2'S.. g -y, -
�'` a 1<� .. �1?-: ca�- a'6`-.�4 :43a_a 'n ••:1
>S..g.la-
- _ ��'-• �1i
- 1. �-�:._a. _Six`'F.Sk �i•_�}_____S
�Report#:
Gi��
215122415
Project ID: 5120373
Report Date: 01/04/2016
P
€�
ANALYTICAL LABORATORIES. LLC
5:
i
Sample Results
FOURTH. CREEK'..
Collect Date
12/?1/2015 08 30
GCAL ID
' 21512241501
:.:... ..
.SLUDGE ., .:,. .....
.. ,:. Receive Date92/2
3/20151.1ij:._g
Matrix:.
r Solid _ -
El
112B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
12/29/2016 09:00 575723 EPA 7.3.3.2 1 12/31/201517:30 RXJ 576014
CAS# Parameter
57-12-5R Reactivity Cyanide
EPA 9034
Result DL LOQ Units
25OU 250 250 mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By . Analytical Batch
12/26/2015 1000 575556 EPA 7.3.4.2 1 12/28/2015 06:44 WRR 575633
CAS# Parameter
18496-25-811 Reactivity Sulfide
Result DL LOQ Units I
25OU 250 250 mg/kg j
t
f

`� GC/AL
Ar ANALVTIC*AL LAbOPAIORIES. LLC
Report#: 215122415
Project ID: 5120373
General Chemistry QC Summary
Report Date: 01/04/2016
.PknaIytI0J1,.Bptch
l'en*f
C :ID
6'..
M957655 -
­
.57
LCS 56
.5 75
QCANIJ
1,5.237911523800
Prep Batch
S a rn p I djy';p';
M BLCS
1*"1'21'26/2'0�l"5�.-I.O..-.Ot:D�
Prep:Qafe
�1212612015.10:00.
Analysis,Date ysisD.ate
12128/20.15 06:44'
`
fMk61560'44
EPA 7:3.4.2:'
Solid
Solid
E?A,9034:'."'*
U nits
mg/kg
S*0
% R
: esult
%R
- Cont 1`1
FO
-':' 1 ..
11.1, : I
Result"
..�DLI
Added
5.
Lim'Its%R
Reactivity Sulfide
--TI8496-25-8R
I 25OU
2501
10001
1162
116
L 47 - 120
Afialytical Batch
ieht*ID
MB575723
576614
.1524329* , - :� z..
. i5 4 0
.Pre _Batch
•GQAE--,'Jb
A. arnp.q Typo,
I�
CS
57
Prep Daiii
3.2129/21J16 09.
-00
12/2912015 09:06: -
Prep.Mqthod..
AnaljWi: Date�
'I 2i$ 1 12b I 5� 1702'
1 �6 i)�O i 20:49
EPA,7.3.3.2
Matrl�
Solid
01
S I'd"
OA-.901. 2B.
..Unit.
S.
k
rpg**/ g
''
. Spike
Result
:,`:Result
�bt_
-'Add ed
./°R;;Control
its%R
[—Reactivity Cyanide
67-12-5R
25OU
1 2501
2501
31.61
131
1-25
Lab Report#: 215122415
Page 15` of 22

10
CT
Certification: AC USACE
Prism Laboratones, Inc.
R-2073
NC C.
S(t�tber
N/A
Svqbwd
---:RECEMNG.LAUOP.ATORY:.!
a I J. ab i, Inc.
SR )lutY
C.'fiarlotte. NC. =24-0543
tig
PbOheAOM.2M3364
e -5. 0
Fax: 704-525=0409
fax.[phone].
ProjeptWitmer. Robbi Ajoa,69.
Analysis Due
]Expires xpires eRj
Snmpie jp::M.2037M] solid
.,SRplR!cii;1,2nW5 o0v! I -
Xz6 Yity; Sulflldi: (Sub)
12128/.15 0830
12dactlklityj. Cyaglde (Sub)
'PI10446 08:30
'onla�nersSu lied:
PP
N R,
V.,
J
pd By.
Mp;
c vbd y ata
RelegsA;
&d By
D4
w
fltelvgsed By
.... .....
Date
R'ee
c-c" W--d B
N: Adledsa. B —`R' 641:13"
y . .. ...
Y,4 PaAp:� I
Pi4ge -16, of 22

Revision XA:
Page 11 of l I

A��lrYtfc, A , INC
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
5120373
LABORATORY REPORT NUMBER
1512L74
Primary Data Review By
Chantelle Kanhai
Project Manager, AES
DATE
December 31, 2015
Secondary Data Review By
Ashley Amick
Project Manager, Access Analytical
[e-mail]
i
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDIIEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this pcojecfare provided by Access Analytical, Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 1 of 5
Page 18 of 22

iKKKM,
z
_0
Environmental 6olullons
Full -Service Analytical &
t I ''I
l �VLUOPATORIEgINQ
SQL.
-4-,7,
A ES n
t 2-
0
SUBCONTRACT ORDER
Prism Laboratories, Inc. Certification ELAC_ USACE
NQ1Z SC— Other
5120373 NIA
SENDING LABORATORY: RECEIVING LABORATORY:
Prisin. Laboratories, Inc,. Analytical Environmental Services, Inc.
P. O. Box 240543 3080 Presidential Parkway
Charlotte, NC 28224-0543 Atlanta, GA. 30340
Phone: [phone] Phone:[phone]
Fax: [phone] Fax: NA
Project Manager., RobbikJones
Analysis'*' "Due Expires Lnbontory ID Comments
Sample ID: 5120373-01 Solid Sampled:12/21115 08:30
Herbicides TCLP (Sub)
Contaftiers Supplied.
I /.X) It )
12/28/15 09:30
BY
I
mulcusua 15Y uatu Mccelyca Dy uare
A
Released By Date Received By Date
Page 2of5
I'-.,-,-P6ge 19,b

ii:S',» -4 _ ti_n v`-=-•.•- }i^k; r-e k. �. .. .. 4}.=>t.. ni 1
__ ��"� �_-tit- �_��.-_•�_�.=�-� < �.,_�4�_,.:�-_,s � __a_1.-_._ . ��'�tr�;.�t� z:�ti'�`_-::�:�;_ti _. _ ��.�_����:�_�xzY=..1�.,_�_o d _���_� ��.--_vr._ev.�.z:3 ":. �b3 e��..�J.:4�------�'-�
i`t 3
i
�I
A T,.... Date: 31-Dec-15
Client:
Prism Laboratories
Client Sample ID-.
FOURTH CREEK SLUDGE
Lab Order
1512L74
Tag Number:
5120373-01
Project Name:
5120373
Collection Date:
12/21/2015 8:30:00AM
Lab ID:
15121,74-001A
Matrix:
Solid
Analyses
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex)
2,4-D
Surr: DCAA
Qualifiers: • Value exceeds maximum contaminant level
BRL NotDetected at MDL
H Holding times for preparation or analysis exceeded
N Analyte act NELAC certified
B Analyte detected in the associated method blank
ReportingUnits
Result
Qua[ MDL
BatchID
DF Date Analyzed Analyst
Limit
(SW3510C)
BRL
0.017
0.20
mg/L
217658
1 12/30/201514:34 AW
BRL
0.031
0.20
mg/L
217658
1 12/30/201514:34 AW
115
0
50.1-148
a/nREC
217658
1 12/30/201514:34 AW
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
> Greater than Result value
7 Estimated value detected below Reporting Limit
< Less than Result value
Page 3 of 5
Page 20 of 22

__`__ --t: +i: Y
--- <_
- _ ;,ems_ -•= - - :. s� -
.�-=tom zr"� ;_� �� •�, � � � `� . P?�<�� t;<..5��
Analytical Environinental Services, Inc.
Sample/Cooler Receipt Checldist
Client �G'G' ��� �Work Order Number Acs%d�T T
Checklist completed by
Signature Date
Carrier name: FedEx_� UPS_ Courier_ Client_ US Mail Other
Shipping container/cooler in good condition? Yes ` No _ Not Present _
Custody seals intact on shipping container/cooler? Yes — No — Not Present —
Custody seals intact on sample bottles? Yes — No — Not Present
Container/Temp Blank temperature in compliance? (0*561C)* Yes No
Cooler DG Cooler92 Cooler#3 Cooler#4 Cooler#5
Chain of custody present?
Yes
No
Chain of custody signed when relinquished and received?
/
Yes r-`
No _
Chain ofeustody agrees with sample labels?
Yes �!
No —
Samples in proper container/bottle?
Yes
No _
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test?
Yes
No
All samples received within holding time?
Yes _✓
No _
Was TAT marked on the COC?
Yes
No
_
_✓
Proceed with Standard TAT as per project history?
Yes
Ido
—
Water - VOA vials have zero headspace? No VOA vials submitted
Yes
Water - pH acceptable upon receipt?
Yes —
No —
Adjusted? Checked by
Sample Condition: Good Other(Explain)
(For diffusive samples or A1HA, lead) Is a known blank included? Yes
See Case Narrative for resolution of the Non -Conformance.
Cooler #6
Not Applicable —
No _
Not Applicable ✓
* Samples do not have to comply-tvitli the. given range for certain parameters.
Mes server111Sample Receipt\My DocumentsICOCs and pH Adjushnent Sheet\Sample Cooler Recipt Checklist Revl.rtf
Pane

Analytical Environmexital Services, Inc Date: 31-Dec-15 X.,
Client: Prism Laboratories
ANALYTICAL QC SUMMARY REPORT
Project Name: 5120373
Workorder: 1512L74 BatchID: 217658
Sample ID: MEB-217658 Client ID: Units: mg/L Prep Date: 12128/2015 Run No: 307340
SampleType: NIBLK TestCode: RFRBICIDES,TCLP SW13IU8151A BatchID: 217658 Analysis Date: 12/29/2015 Seq No: 6595102
Analyte Result RPT Limit SPK value SPK Ref Val '/oREC Low Limit High Limit RPD Ref Val I/oRPD RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
214-D BRL 0.20
Surr: DCAA 0.4739 0 0.5000 94.8 50.1 148
Sample ID: LCS-217658 Client ID: Units: mg/L Prep Date: 12/28/2015 Run No: 307340
SampleType: LCS TestCode: HER13ICEDES,TCLP SWI311/8151A BatchID: 217658 Analysis Date: 12/29/2015 Seq No: 6595103
Analyte Result RPT Limit SPK value SPK Ref Val 9/oREC Low Limit High Limit RPD Ref Val 0/.RPD RPD Limit Qua]
2,4,5-TP (Silvex) 0.4732 0.20 0.5000 94.6 52.5 126 "rt
2,4-D 0.4897 0.20 0.5000 97.9 50.5 132
IM
Surr: DCAA 0.5215 0 0.5000 104 50.1 148
Sample ID: 1512K04-001AMS Client ID: Units: mg/L Prep Date: 12/28/2015 Run No: 307340
SampleType: MS TestCode: BERBICI]DES,TCLP SW1311/8151A BatchlD: 217658 Analysis Date: 12/2912015 Seq No: 6595105
Analyte Result RPT Limit SPK value SPK Ref Val 0/oREC Low Limit Hhzh Limit RPD Ref Val VoRPD RPD Limit Oual
;g;y
2,4,5-TP (Silvex) 0.4935
0.20
0.5000 98.7
49.4
131
2,4-D 0.5145
0.20
0.5000 103
44.1
137
Surr: DCAA 0.6325
0
0.5000 127
50.1
148
Cc
Qualifiers; > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blnak
CD'
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
J Estimated value detected below Reporting Limit
N Analyte not NELAC certified
R RPD outside limits due to matrix
Page 5of5
0
h
RptLirn Repotting Limit
S Spike Recovery outside limits due to matrix
M?q�

P ISM
LABORATORIES ING
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 2868.7
NC Certification No. 402 Case Narrative
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735 01/06/2016
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
VI C-[<
Project: Sludge (Hazardous Testing)
Lab Submittal Date: 12/21/2015
Prism Work Order: 5120374
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for Ignitability:
This method is not required by the Federal regulations to determine if a waste
passes or fails the characteristic of ignitability according to the RCRA regulatory definition at 40
CFR 261.21. To clarify, the test results of this method cannot be used to directly classify a
waste as a D001 hazardous waste, nor can the results be used by themselves to definitively
classify a waste as non -hazardous.
Reactivity analysis subcontracted to GCAL TCLP Herbicide analysis subcontracted to AES . Laboratory
reports are attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC,.. -
• VL•
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Sample was taken off rotator on 12/23/2015 @ 06:45.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to, the reporting -limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
_..,•, .. ..;.., .. ,;;This.report,shouId,noF be rep rod uced,.except-in its-entirety;;withoutthe:written consent of Rdsm;Lab oratories, Anc
449 Springbrook Road -,P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page Of.22.

I,
41"N Sample Receipt Summary
k-11,
Full -Service Analytical&
I S M I Environmental Solutions 01/06/2016
®'ia'ueonnrosiE4 we
Prism Work Order: 5120374
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Third Creek Sludge 5120374-01 Solid 12/21/15 12/21/15
Samples were received at 16.2 degrees C. See case narrative for further information.
i,,,,,-;,,.,..�-,.,,;This.,reportshoulc<not be •reproducedi. except in its-entirety,vithout the written consent of Prism Laboratodesjnc.i
449 Springbrook Road - P.O. Box 240M - charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page 2 of 22

Laboratory Report
sA I Full -Service alSolueAnalytical 8
' V' Environmental Solutions 01/06/2016
�ueoiuromtti we .
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: Third Creek Sludge
Attn: Andy Smith Prism Sample ID: 5120374-01
P.O. Box 1111 Prism Work Order: 5120374
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/21/15 08:30
Time Submitted: 12/21/1516:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids
17.4
% by 0.100
0.100 1
*SM2540 G
12/23116 16:02 ARC
PSL0392
Weight
Ignitability
Pass
mm/sec 0.10
1
*1030
12/28/15 14:20 ARC
1351_0421
pH
6.3
pH Units
1
*9040C
12/23/15 12:37 EGC
PSL0389
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
12/23/15 6:45 JAB
P51_0378
TCLP Extraction
Complete
N/A
1
*1311 ZHE
12/29/15 8:30 ANG
P51_0419
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
*7470A
12/28/15 12:41
JAB
P51_0407
Arsenic
BRL
mg/L
0.050
0.0035
1
*6010C
12/28/15 14:48
BGM
P51_0381
Barium
BRL
mg/L
5.0
0.0035
1
*6010C
12/28/15 14:48
BGM
P51_0381
Cadmium
BRL
mg/L
0.025
0.00050
1
*6010C
12/28/15 14:48
BGM
P51_0381
Chromium
BRL
mg/L
0.25
0.0030
1
*6010C
12/28/15 14:48
BGM
1351-0381
Lead_
BRL
mg/L
0.050
0.0065
1
*6010C
12/28/15 14:48
BGM
P51_0381
Selenium
BRL
mg/L
0.10
0.016
1
*6010C
12/28/15 14:48
BGM
1351-0381
Silver
BRL
mg/L
0.25
0.0010
1
*6010C
12/28/15 14:48
BGM
P51_0381
TCLP Organochlorine Pesticides by GC/ECD
A
Chlordane
BRL
ug/L
2.5
0.34
1
*8081B
12/30/15 12:10 JCa
P51_0461
Dieldrin
BRL
ug/L
0.50
0.022
1
*8081B
12/30/15 12:10 JCa
P51_0461
Endrin
BRL
ug/L
0.50
0.020
1
*8081B
12/30/15 12:10 JCa
P51_0461
gamma-BHC
BRL
ug/L
0.50
0.013
1
*8081B
12/30/15 12:10 JCa
P51_0461
Heptachlor
BRL
ug/L
0.50 --
0.015
1
*8081B
12/30/15 12:10 JCa
1351_0461
Heptachlor Epoxide
BRL
ug/L
0.50
0.018
1
*8081B
12/30/15 12:10 JCa
P51_0461 -
Methoxychlor
BRL
ug/L
0.50
0.033
1
*8081 B
12/30/15 12:10 JCa
P51_0461
Toxaphene
BRL
ug/L
25
0.16
1
*8081B
12/30/15 12:10 JCa
P51_0461
Surrogate Recovery Control Limits
Decachlorobiphenyl 63 % 13-186
Tetrachloro-m-xylene 56 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0023
1
*8270D
12/29/15 19:47 JMV
P51_0451
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0026
1
*8270D
12/29/15 19:47 JMV
P51_0451
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0019
1
*8270D
12/29/15 19:47 JMV
P51_0451
2-Methylphenol
BRL
mg/L
0.050
0.0021
1
*8270D
12/29/15 19:47 JMV
1351_0451
3/4-Methylphenol
BRL
mg/L
0.050
0.0019
1
*8270D
12/29/15 19:47 JMV
P51_0451
Hexachlorobenzene
BRL
mg/L
0.050
0.0019
1
*8270D
12/29/16 19:47 JMV
1351_0451
Hexachlorobutadiene
BRL
mg/L
0.050
0.0026
1
*8270D
12/29/15 19:47 JMV
P51_0451
Hexachloroethane
BRL
mg/L
0.050
0.0025
1
*8270D
12/29/15 19:47 JMV
P5L0451
Nitrobenzene
BRL
mg/L
0.050
0.0024
1
*8270D
12/29/15 19:47 JMV
P51_0451
Pentachlorophenol
BRL
mg/L
0.25
0.0025
1
*8270D
12/29/15 19:47 JMV
P51_0451
This.report.should.not.be.reproduced,:except in its. entirety,.without.the written, consent, of Prism .Laboratories,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2822"M .
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page,.3 'Of22 .

Laboratory Report
�n I S M I Full -Service Analytical &
r Environmental Solutions 01/06/2016
kLAB0FW0..s ING
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: Third Creek Sludge
Attn: Andy Smith Prism Sample ID: 5120374-01
P.O. Box 1111 Prism Work Order: 5120374
Statesville, NC-28687 Sample Matrix: Solid Time Collected: 12/21/15 08:30
Time Submitted: 12/21/15 16:10
Parameter Result Units Report MDL Dilution Method Analysis 'Analyst Batch
Limit Factor DateMme ID
Pyridine BRL . mg/L 0.25 0.0021 1 '8270D 12/29/15 19:47 JMV P51-0451
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
69 %
43-140
2-Fluorobiphenyl
57 %
44-119
2-Fluorophenol
26 %
19-119
Nitrobenzene-d5
58 %
44-120
Phenol-d5
15 %
11-52
Terphenyl-d14
71 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35 0.83
1
'8260B
12/30/15 23:51
KDM
P51-0491
1,2-Dichloroethane
BRL
ug/L
25 0.66
1
'8260B
12/30/15 23:51
KDM
P51-0491
1,4-Dichlorobenzene
BRL
ug/L
380 0.50
1
'8260B
12/30/15 23:51
KDM
P51-0491
Benzene
BRL
ug/L
25 0.48
1
'8260B
12/30/15 23:51
KDM
PSL0491
Carbon Tetrachloride
BRL
ug/L
25 1.1
1
'8260B
12/30/15 23:51
KDM
P51-0491
Chlorobenzene
BRL
ug/L
5000 0.62
1
'8260B
12/30/15 23:51
KDM
P51-0491
Chloroform
BRL
ug/L
300 0.76
1
'8260B
12/30/15 23:51
KDM
P51-0491
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
10000 2.4
1
'8260B
12/30/15 23:51
KDM
P51-0491
Tetrachloroethylene
BRL
ug/L
35 0.98
1
'8260B
12/30/15 23:51
KDM
P51-0491
Trichloroethylene
BRL
ug/L
25 0.78
1
'8260B
12/30/15 23:51
KDM
P51-0491
Vinyl chloride
BRL
ug/L
20 0.97
1
'8260B
12/30/15 23:51
KDM
P51-0491
Surrogate .
Recovery Control Limits
4-Bromofluorobenzene 96 % 80-124
Dibromofluoromethane 101 % 75-129
Toluene-d8 97 % 77-123
"'- -�••' .-' ..�..�IIIID'IUPU1L'SIIUUIU'IIU1 UG;IC'II UUUUUU,.UAIUP\111'IIS-C11LI]UL/,_WIIIIUU-III WIIIIGI1-11-111 UI 1711D111 ldUUId1U11GJ;:I I IV..Z.-;�1:;�.. �.li,..v ..F;r. •�-.�� .�:..:%".i•
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone]- Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page 4 Of 22

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
5120374-01
P51_0392
30 g
30 g
12/23/15 16:02
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/rime
5120374-01
P51_0419
25 g
500 mL
12/28/15 14:15
5120374-01
P51-0378
100 g
2000 mL
12/22/15 14:10
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/rime
5120374-01
P51_0381
10 mL
50 mL
12/23/15 10:55
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
5120374-01
P51_0407
20 mL
30 mL
12/28/15 8:30
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Datel ime
5120374-01
P5L0461
200 mL
10 mL
12/30/15 7:35
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Daternme
5120374-01
P51_0451
200 mL
1 mL
12/29/15 11:30
Prep Method: 5030B
Lab Number
Batch .
Initial
Final
Date/rime
5120374-01
P51_0491
1 mL
10 mL
12/30/15 8:20
Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services,
Inc.
Lab Number
Analysis
5120374-01
Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast
Analytical Labs, Inc.
Lab Number
Analysis
5120374-01
Reactivity, Cyanide (Sub)
5120374-01
Reactivity, Sulfide (Sub)
...._-. ,a_ „-. •�: .:.!a1--1a.,aanvuw n..a.c,cV, vuua.o..,., cn P1in nn,c,Au,cq,.vAuwua uic. rruuc, I WI IQcuL UI f 11J111."..' WI .:..
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-0001529-0364 - Fax: [phone] Page.S Of 22

S ■ - ■
ABORATORIES$ INC,
Full -Service Analytical &
Environmental Solutions
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] - Fax: [phone]
Client Company Name: C-X d $���e�sc•�l��
Report To/Contact Name: An RT S,-, ih
Reporting Address:
CHAIN OF CUSTODY RECORD
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
:.;
YES>:,;>: ,NOa;:':::N/A
Samples INTACT upon arrival?'"
Received ON WE,T ICE
PROPER PRESERVATIVES' indicatie' d
Received WITHIN'HOLDING TWES7
CUSTODY SEALS INTACT?
VOLATILES reed WIOUT HEADSPACE?
PROPER CONTAINERS used?"
✓ "'
TEMP: Therm ID: ; dr a Observed: ITT °C1 Corr /U c
Phone: 7,9'f-u7S-j'/3$ Fax 1fe '(No):74y-$78-SCSS" purchase OrderNoJBilling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF_ExCel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ P sh Wor dust Be pprov
SC OTHER NIA
Site Location Name: F ur-E A C. e e k &J Lip T P Samples received after 14:00 will be processed next business day.
Water Chlorinated: YES_ NO
Site Location Physical Address: 03 Bell Farm 1�ek. Turnaround time isbased on business days, excluding weekends and holidays.
S/ (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
f a1 t'S� �IC NC RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Coliec 'on: YES_ NO
p p -
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS RE
VESTED n�
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
j REMARKS
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
ID NO.
HOURS
SLUDGE)
SEE
pp
A,`Rd CREr k
/BELOW
Su
T N
4A61
�
C
WA
A
C
TIC
M IEA%s
u
�1O,M
r
e
/
Y �
r/
Ti'/
TC1
s
•
TC1
��
4
Sampled By (Print Name) /?AX j t r, C k Affiliation
Sampler`s Signature .s L
Upon relinquishing, this Chain of -Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be PRISM USE ONLY
submitted In writing to the Prism Project Manager. There will be cbLarges for any changes after analyses have been initialized.
ours Comments
By: SgneturMilte ry Additional
VReI1ueBy'.(81,'gnature)Receive
Date atu Re d y:(Signature)
uature) Received For P' Labors B Date
` d of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH C DY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
o y SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC RECEIVED AT THE LABORATORY.
Ex', ❑ UPS O Hand -delivered d m Field Service O Other
UST: GR DWATER: DRINKING WATER: SOLID WASTE: RCRACERCLA LANDFILL j OTHER:
SC ❑NC ❑SC ❑ C ❑SC ❑NC ❑SC ❑NC ❑SC ❑NCOSC❑❑NC ❑SCONG ❑SCI [INC ❑SC
J—ES:
❑ ❑ ❑ ❑ ❑AINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGIE�)AL.
V'.
r,.
"
+.fJ�1!
.r„•�
�;., , , ,s�.��^:r-
•: r % s r %,•r•: ,�., .1f;S:%:..,! �: �:v::r
:ry?

�,., _
,^^�. ....._ '- � _•_ �i- ems'>-., 'sxi z ='tiw"� -^ti ti: es+ a _ .. .:.: ati� - v, z
:'aa>•,-c3:.x- ' `': t... to a. t_v a :� `z .ca x.'-.-- �.: ``. 's :� .S _ '_' -= v._•-�,- .. _`
-t1s;,z,__�:-.�----..ti: �i�a,,,��.-:=��. .:wi,•x_•kti ��-,�s<.'x�s�,._:.=2v-.n.-'.::=�7 . F�-1z�5.F._t_�`:iv�� �a�,=,.:n . �.� ems:-sa.�•_��ra<.3��;c-- :9 :_ :��.$•._.�-
ACCESS
ANALyriCAL,. INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Angie Overcash
PROJECTID
5120374
LABORATORY REPORT NUMBER
215122416
DATE
01/04/2016
Primary Data Review By Secondary Data Review By
Ashley B. Amick
Cu 's
nzed Signa ure Project Manager, Access Analytical, Inc.
[e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820. 1
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory #-01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 215122416 Page:7'of22

&.
_
NELAP CERTIFICATE NUMBER: 01955
DOD FLAP CERTIFICATE NUMBER: L14-243
kdA caeqt1L0JRATDAIESs Lac
ANALYTICAL RESULTS
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70M
Report Date 01/04/2016
GCAL0.epor121512�20,16
1111111111111111111111111111111111111111111111111111
Project 5120374
Deliver To Additional Recipients
Angie Overcash NONE
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
+ f
Testing
/y Y Z LAY
Lab Report#: 215122416 Page 8 of 22

>11010
ti d . �., � `ice;=�`'� =''` '�`-as=:ids =•� '�' Y �� =-
ir:t-a__.�,:�:=:ti
�_'� >':> R.
s
_.,.._
5- _ '� . _ -.-:a_• .�.:��ti. rim__=___ ti''] ..s:.i=i :..:
r� Report#: 215122416
�� AN�A`opAr� qp Project ID: 5120374
Laboratory Endorsement.
Report Date: 01/04/2016
Sample analysis was perfonned in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAUs Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified -reporting limit
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted .
FLD Indicates the analysis was performed in the Field
DL Detection Limit
DL Diluted analysis — when appended to Client Sample ID
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are Intended for.the use of the client. Any unauthorized use of the Information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
(4 Curtis Ekk
Authoriz d Signature
GCAL Report 215122416 .
Lab Report#: 215122416 Page B.;Of'22

- - - -_ - .S'-4.a „ S"c:'>.i+. :-. Ltti�^7'..'l-<a.... 3.t. 1 a..'a•.•f;. =.'.- -:.4 p
� { :��=::e�".,- s=S'':-'r' _„ .,; �,�..-� . :'� -�:^a .S,,Ts..� wr.c:a-=-;,.��hc �. ��'`+i .,, ''• °' �,e-3 3Cs:._z-�?:.: _�'a �.tius=s•":;^'�
_ .
Report#: 215122416
4 1% . 40 Gc/,AkL Project ID: 5120374 Report Date: 01/04/2016
At1ALVTI AL LASo"10RIM LLC
Certifications
10/02/2015
Certification
Certification Number
DOD ELAP
L14-243
Alabama
01955
Arizona
AZ0718
Arkansas
12-060-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
USDA Soil Permit
P330-10-00117
Lab Report#: 215122416 Page.10. of 22 . .

_-s_--,.
- _ i'+�k.L.-��%a��vg`'4T=v?s`;`S`.•'k:�:i - � .. � � _�� .. L h'':- [E'a h�a^4� -. '�i`l v__ ..]
ti
.,. .ii:.>:?<t-,__-`-;-oi.��� ..
�'t "s:.s �:4� ., � �l _•�,y
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- _
ti�S' ��'i�.'�+}k'-Zcy..._: ��ti _. 'S� .. x'<+.�a_:'�::e..=--'__..: _-ti-?'-�
i�tia-*a_ca_�'�.'1 ...__..,. r:`.'9
_ _ccs_-_`_____�•-__�...5--�...r
Report#: 215122416
_AI,��A�OPA— p�Es. ��E Project ID: 5120374 Report Date: 01/04/2016
Case Narrative
Client: Access Analytical Report: 215122416
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found in the analyzed sample(s).
Lab Report#: 215122416

.i%....v.4'�.'yk �'c.. _ n- l 4 _
� �i$�=s .s4e4 - ?`i�3s x�..'.'-'.l''.� - -�y`41vo
-- _ �v�:ti R'yc� -i--•>-•_3 � <; tc.'i '�"• _ _'ti �.� �i -_-....`�ti': -..n ....
>.4
I.
art�cn�OWO
r'li,-nf in
Report#: 215122416
Project ID: 5120374
Sample Summary
Matrix Collect Date/Time
21512241601 THIRD CREEK SLUDGE Solid 12/21/2015 08:30
Report Date: 01/04/2016
Receive DatelTime
12/23/2015 11:08
Lab Report#: 215122416 Page 12;Of 22

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y� .�iy�.•�
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av'ib9.�:.1'i':�:a-� .`✓'•..4i-_.-"`4.'.,:`i:'
�'_�i:A`:'R•
__ 4'+:> �.
Report#: 215122416
Oaf��� Project ID: 5120374 Report Date: 01/04/2016
ANALYTICAL LAOO"TOAISS. LLC
- Summary of Compounds Detected
No anayytes were detected for analyses performed by GCAL-
_ i
Lab Report#: 215122416 Page So 22 i

. - __.__"---_ '_-_-___-•____.•-___--_._-`-:�
- _ _ �^v.•�:.::�.:--.
1 Si�� _�A :st'3`-q.� .�.�._ _ - ��ti ..'.: tii::ti?l.?. >'+��?ti:�
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AIlA LV TItAI LA90F AlOpIES. lLc
Report#: 215122416
Project ID: 5120374
Report Date: 01/04/2016
[Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
12/29/2015 09:00 575723 EPA 7.3.3.2 1 12/311201517:32 RXJ 576014
CAS#
57-12-5R
I=PA Afl'I4
Parameter
Reactivity Cyanide
Result uI- "WIA �••••�
25OU 250 250 mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
12/26/2015 10:00 575556 EPA 7.3.4.2 1 12/28/2015 06:44 WRR 575633
CAS# Parameter
18496-25-8R Reactivity Sulfide
KeSUIt uL-
25OU 250 250 mg/kg
Lab Report#: 215122416
Page 14 of 22

_ : - aCF;k:2 'tipti?,: iz:�{�" �.ii':-:Y E'`=°"ai-.. �": <3 �::s•-`*'-_•. `s�'::�.n gw=.v - w••1.:_< e +.w. �>a=_�,: •'.1 's: Wit..•\:_---va �,,.'a..a�^_'�'�,.-.� �.•.��tib��:..n: w.w,*.:s _.�•_..,-� .. 7:-xv.Wti ti_�`__-`__
-ti's`-v?r::. `i4 �,'_.,. �:+; a �?�•"i->___ ( �,.... �'�.�3�. ��.•s: -s _.3 �'h: n�_.ti_-.. _.... •_. .___-�,g7_ti k�:r:_:�ix.',�.s3-. _Y_..�_ i _�i v
lv
Report#: 215122416 ISN
GC/�LAHM1LYTICAL LM1HOAATOP155; LLG Project ID: 5120374 Report Date: OVO4/2016
General Chemistry QC Summary
ID.
GCAL ID
:.. ....:..
MB575556.;;°...:; ...`:.
:, . ,,
1523799
. ...
.,:;;; :
,;...
::....:
57555Client 6
L:•.:C_S.
1 ;;;;:
.5238b0
575633;'.
P�ep.i3atch %:. ,.
<:.
: . Sple.:7ype
am
MB ': :.-.,;; ;
`::..`::.;
LCS
575556
:Prep Date
,12/26/201b 10 00
00._
44
Prep Method, ..
:. ' -Analysjs Date
12/28/2015 06 44
12%28/2015 06
EPA7.3.4.2>
_:::.,. ...•::: Matrix
Solid ....,;ta
Solid:.:._'
:,,;;
:.
:;, :c ......Units
:
mglkg
::=:;Spike.
=
Result
o -
/oR
.Control
o
:: EPA' 9034
,..
,,. ..
:. Result
DL
"Added
..
Limits /oR
Reactivity Sulfide
18496-25-81K
25OU
1
250
10001
1162
116
47 -120
Analytical.Batch
:.:.
:: ; • . Client.ID
RIi-MFU-7-WS.. ? . -
` ": '':'
16221
575633 ' `.....
,: - :
::;:, : t:: GCAL ID
21512221101„
, .:.-
Prep Batch
.;:
Sample.Typ�
SAMPLE
575556..; . `
Prep. Date
12/26/2015 �10 00
1212E
Prep Method- :
:Analysis Date.
12/28/2015 0..6:44;;..
; °. =
:IMJ
EPA 7.3.4.2
.;'; `4
: Matrix
`...
Solid =. ,
Solid
_': •
=.Units
Ipg/kg
:.....::::... ..
EPA 9034.
:...:. .::;_::
Result
` '.:':; DL
Reactivity Sulfide
18496-25-8R
1 01
250
Lab Report#: 215122416 ?,Pagg,:;'IFof

K--:i
-K,
0-C-41,
A- ;USACE
Prism habokatorles, Inc.
wcSC� Other
5120374
RJE�—
,SENDING LABogAT6fz'f:.
REC41V!4G .4440RATORY:
iism Laboratories, Inc.
' nc.
P b. j3ok .2405.43
RI A?eppe,:
Charlotte, 146'J8�244543
Phofict 800-529-6364
Ph 769-4966
Roc 704-525-0.409
Project Manager. RobbiA-4ones
Analysis Due
Expires
Labdi.Aoy ID C.0"04
8AFhple lbw 5120374-61 Solid
SamplAd:j' 6PA130
R6.actiiV'uq,„byah.fdd (Sub)
M104116 08:30
lonidimrs Supplkd:
'flit
a/Ws
Relea;ry
c V B.; ale
I I dj�
Released By
Y
-RW ... --d-B-
Tate
Received Poo
pa 6 t
y.
-.4.
-Q qo 4M CP
Page 16 6

4
Checklist
SAMPUEUKLE9. 910;�19C
SA CHECKLIST.
MPLFDELrVERY:GeOUP 2. 012?4 0
'.gAl<, Transport MethbO Vere:all samplbs-received-using,-p ffiermal:preservationT
.Client M .Toper
'4566-jssAnaWcal FWEk
Wher.f Lfsddwere all custody. seals infant?
were. all sampfes1rec6lvqdIn"proper
containers?
.Profile Nyrn]00
60435
kzq6qlmqd qy,
L&W.Aitle.E.
Were all wreceiv. using - proper chemical -
6d " "*
Was:presetvdtiv . a -addedito anyl container atthelab?
cb t 'd I good condition?.
n Ow§�TecOlvp , n
Wera+all 'VWwiter samples receivedv Rhodt'liead space?
Do allisampla laboW.match the Chain ofCustody?
-7
Did.the.,Chalnl.pf-Custody'lis:i'+fh6 sampling technician?'
Was -the COC mail . dates- andtimeof. reasi
LA!3..PAESER
'Thermornate.rJD:%,.F_25
Tqnip,( qj
Nbqe:
None
..7752 7990 4647
1._1
Revision 1.4
215122416
1�21274-
'YES .:..
NO "'NA
y.,
EI:
9 1
El
RI
El.
7
T
i
MX ,ji'
2,
Page 11 of 11

b`k'`-` �•``tiYtitiz...�}'T,.Y�:�- t..z`�'1i�i•:':� - t' 4'.: i'46 -- a..�4., ..�..� '..__. _�i•__-�-_\:_.�_..
�-'�:M1 �. �a :_ _.•_v^`';Sr':"`--`�e.'-4i�.-;,,�J.'\.3'o-„c» [e. �.a �'_�<i-`_�. aa4titi _ -'C_a _ � .:.Y:e=-'.'--`Z"�.i?i� �.:ti.'�.•..s'*..-r::.-. tea::=:�.v....__. _.� a'..•a -.
.4�._ :..:.r3 _. :s'•i�%g.�1_:rti\?.A-'_..,`4. ___ ___h' .. �.1�Y.-______i4vti .ti=..,.,�..'tii - zt.-_izv+ilia____- _`
NA
l'Ct ,:ICd
ANALYTICAL
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
5120374
LABORATORY REPORT NUMBER
1512L75
Primary Data Review By
Chantelle Kanhai
Project Manager, AES
DATE
December 31, 2015
Secondary Data Review By
Ashley Amick
Project Manager, Access Analytical
[e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed atAnalytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCD11EC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page..1 of.5.. -
Page 18. of 22

- - _- -
-�.
�:12i•- _- •�-�._� : _> S ��i` ti -': :.� +.`- av\... - S 1-.
he - E-_•....t �: = -:-� :. cam:. z-:�#.._. j
`.
e S,� e+a...'.�'1? L�
L::.-4.-'>.'i_ ti �t-.s :.
^?s..- _ __ _
F}:..'.v�.c-r..=__„_.1
4 -
Ee:S�_1:5�4,:i+'S
�.a
�; .t+
...�.ov _tit __+:... .._.,a -.
_ �:^.."S- �..__ �... r�.;i=•e5_%..-_4%
1.ti +�.- i-_�-`.tin:_.`.:
e:-.V '�.-_. _...--_
a.-_-}v."�>.3::. __..
-._.�..___ .. _�-,.i�w,,..:.____��a
_-_'t..0
Full -Service Analytical & �
Ism Environmental Solutions G
SUBCONTRACT ORDER
Certification:AC USACE
Prism Laboratories, III(!. NC t/ SC Other
5120374 N/A
SBNDING LABO%kTORY; RECEIVING LABORATO12Y:
Prism Laboratories, Inc. Analytical Environmental Services, Inc.
P. O. Box 240543 3080 Presidential Parkway
Charlotte, NC 28224-0543 Atlanta, GA 30340
Phone: [phone] Phone :[phone]
Fax: [phone] Fax: NA
Project Manager: Robbi A. Jones
Analysis_.. - Duo Cxpires Laboratory ID Conunents'
.. �'• . r4 .
Sample ID: 5120374-01 SolId Sampled:12/21/15 08:30 : ' n 3 ��
Herbicides TCLP (Sub) 12/28/15 08:30 V J {"
Containers Supplied:
0-A)-.
1)
Released By Da a
Received By j1 Gs Date
Released By Date
Received By Date
I
Released By Date
Received By Date
Page 19 of 22

e � �4 "sue S e� •_,_'�� v � S' - of v'-•' � "_ � �� -�._-�:5.`.�\ a� j .s,.�.:
_.... ������ `_• __+- •_ a �_.+..3i _ 1 __ v-�---- ___�� � �::�11�:14��1 ��`. .. - b....__-. .• •- .-4 vt v.,_._�c�i:i�4'4�:: �.a � c .�
Analvtical Environmental Services, Inc
Date: 31-Dec-15
Client:
Prism Laboratories
Client Sample ID:
THIRD CREEK SLUDGE
Lab Order
15121,75
Tag Number:
5120374-01
Project Name:
5120374
Collection Date:
12/21/2015 8:30:00 AM
Lab ID:
1512L75-001A
Matrix:
Solid
Analyses Result Qual MDL ReportingLimit Units BatchlD DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 93.9
(SW3510C)
0.017 0.20 mg/L 217658 1 12/30/201515:05 AW
0.031 0.20 mg/L 217658 1 12/30/201515:05 AW
0 50.1-148 %aREC 217658 1 12/30/201515:05 AW
• Qualifiers: •
Value exceeds maximum contaminant level
E Estimated value above quantitation range
BRL Not Detected at MDL
S Spike Recovery outside limits due to matrix
H.
Holding tunes for preparation or analysis exceeded
> Greater than Resultvalue
N
Analyte not NELAC certified
J Estimated value detected below Reporting Limit
B
Analyte detected in the associated method blank
< Less than Result value
.page _
3 of 5
Page 20. of 22.

:.a i_Z_R`':
- 6ti^}x m-:4�'s ! �.��... ''.4..;1_.-.Slt�i�� — <.sE _.t .•.i _. +" _" �.i e�:i-a_
n 2<.-•V•-'
,i-.4.. ,.�a'... :e:�.^.<: ``'•..`:. _�^ -`a''v:i=ixi-_ .�4• ._''6�_-St :.�._s_ `�..�',�,�- -_ _ -_ .<�'l_
�«. - . <t<. ..Rsi. - . 1 - - -<._. v c b ..St.�t: : .x 5....• ci�vti._<S._+v':'�_1'
..: :::'•:=i�•.� «_ _=:§�>.,...... c_. ti-�� _ A.-rw^+'S::c,�.....�c.:=:; r: :_-..� :; i>::v zi-=<__<,. _..<......ti— -_� _ ^_%::.vii_iti ti.',_•_ ; =•.a:� .a _ ______ __. ......- � _ _ _
............................................................
_
-1
Analytical Environmental Services, Inc.
Y
k
Sample/Cooler Receipt Checklist
i='
Client `G��T//���7���
Work Order Number
Checklist completed by
Signature Date
Carrier name: FedEx _t�'UPS _ Courier_ Client_ US Mail
Other
Shipping container/cooler in good condition? Yes
v No Not Present —
Custody seals intact on shipping container/cooler? Yes
Custody seals intact on sample bottles? Yes
No — Not -Present —
— No — Not Present
f �
-
Container/Temp Blank temperature in compliance? (0°561C)* Yes ^ No _
!
Cooler #1C7. 4�/-Cooler #2 Cooler 43 Cooler #4 CooIer#5 Cooler 96 i
Chain of custody present? Yes
t- No
Chain of custody signed when relinquished and received? Yes
&-Z No —
!'
Chain of custody agrees with sample labels? Yes
1
No — f
Samples in proper container/bottle? Yes
No —
Sample containers intact? Yes
No _
Sufficient sample volume for indicated test? Yes No _
All samples received within holding time? Yes _� No ^
Was TAT marked on the COC? Yes No _� !
Proceed with Standard TAT as per project history? Yes No ` Not Applicable_ s
Water- VOA vials have zero headspace? No VOA vials submitted � Yes _ NO — l
-
Water - pH acceptable upon receipt? Yes
l
t
No Not Applicable
Adjusted?
Sample Condition: Good=. Other(Explain)
(For diffusive samples or A1HA lead) Is a known blank included?
— —
T
F
Checked by j
Yes _ No —
i:
'
See Case Narrative for resolution of the Non -Conformance.
r
[}
E
�.
* Samples do not have to comply with the given range for certain parameters.
11Aes server%Sample ReceiptiMy DocumentslCOCs and pH Adjustment Sheet%ample Cooler Recipt Checklist Revl.rtf _
t'
Page 4 of 5 .,_,
Page 21 `of 22
`:

Analytical Environmental Services, Inc
Date: 31-Dec.15
Client: Prism Laboratories
ANALYTICAL QC SUMMARY REPORT
s??'
Project Name: 5120374
f"
Workorder: 1512L75,
BatchID: 217658
sample ID: MB-217658 Client ID:
Units: mg/L
Prep Date: 12/28/2015 Run No: 307340
r;
SampleType: MBLIC TestCode: HERBICIDES,TCLP SW13I1/8151A
BatchID:217658
Analysis Date: 12/29/2015 SegNo: 6595102
'„fr
'?Analyte Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RFD Ref Val %RPD RPD Limit Qual
l.
2;4,5-TP (Silv6x) BRL
0.20
-
24-D BRL
0.20
'Surr' DCAA 0.4739
'
0 0.5000
94.8 50.1
148
is fir •,
;
2,4-D
0.4897
0.20
0.5000 97.9 50.5
132
'Surf: DCAA
0.5215
0
0.5000 104 50.1
148��
Sample ID: 1512K04-OOlAMS
Client ID:
Units: mg/L
Prep Date: 12/28/2015 Run No: 307340
!;;d
SampleType' MS
TestCode• HERBICIDES, TCLP
SW1311I8151A BatchID: 217658
Analysis Date: 12/29/2015 Seq No: 6595105
Analyte
Result
RPT Limit
SPK value SPK Ref Val %REC Low Limit
High Limit RPD Ref Val %RPD RPD Limit Qual
2,4,5-TP (Silvex)
0.4935
0.20
0.5000 98.7 49.4
131
rdur s
2,4-13
0.5145
0.20
0.5000 103 44.1
137
Surr: DCAA
0.6325
0
0,5000 127 50.1
148
a
gg'l
*
yfK
> Greeter than Result value
< Less than Result value
B Analyte detected in the associated method blank
(c
CD
_Qualifiers:
BRL Below reporting limit
E Estimated (value above quayntitation range)
H Holding times for preparation or anal is exceeded
g P P Ys
s,•
N
toN
7 Estimated value detected below Reporting Limit
Analyte not NELAC cetvfied
R RPD outside limits dun to matrix
Page 5 of 5
;�'• r;
0 .
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix

N ISM
LAe0RA70RIE9, ING
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402 Case Narrative
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735 01/29/2016
Environmental Solutions VA Certification No. 460211
Dob ELAP: L-A-B Accredited Certificate No. L2307
ISO/I EC 17025: L-A-B Accredited Certificate No. L2307 `
Project: StaLime (Quarterly and Haz Waste Parameters)
Lab Submittal Date: 12/21/2015
Prism Work Order: 5120379 .
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the original laboratory report dated 1/14/16. Hazardous Waste
Parameters were added to the Sta-Lime Sample at the request of the client.
Reacitivy analysis subcontracted to GCAL. TCLP Herbicide analysis was subcontracted to AEL.
Laboratory reports are attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
;.s :..,. This,report should;not be,reproduced,. except ir; its entirety„y+dhout the written consent of Prism Laboratories Inc „
449 Springbrook Road.- P.O. Box 240M , Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page , Of 42

Data Qualifiers Key Reference:
A Analyzed outside of holding time as requested by the client.
B Analyte is found.in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
D RPD value outside of the control limits.
HT Sample received and analyzed outside of the hold time.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
,:.-This report -should not:be reproduced,,exceptin_its entirety,;without,the wrikten,consent;of Prism Labgratones_,Inc
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number..1-8001529-6364 -Fax: [phone] Page z.Of 42

Sample Receipt Summary
Full -Service Analytical &
11 P0 R I SM I Environmental Solutions 01/29/2016
, /All I.. Prism Work Order: 5120379
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 5120379-01 Solid 12/21/15 12/21/15
Samples were received at 16.2 degrees C. See case narrative for further information.
.—This-reporLshould not be � reproduced, except in, its entirety,-,without.the written consent of. Prism L oratories„ a, . Ck's Rq
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 42

I n n I Full -Service Analyt bons
�+ ' V' Environmental Solutions
®IARORAMRIfA INC
Laboratory Report_
01 /29/2016
City of Statesville, NC Project: StaLime (Quarterly and Haz Client Sample ID: Sta-Lime
Attn: Andy Smith Waste Parameters) Prism Sample ID: 5120379-01
P.O. Box 1111 Prism Work Order: 5120379
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/21/15 08:30
Time Submitted: 12/21/15 16:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor. DateTme ID
General Chemistry Parameters
Plant Available Nitrogen
430
mg/kg
160
60
2
'Calculation 114116 9:42
CLB
[CALC]
% Solids
95.0
% by
0.100
0.100
1
"SM2540 G 12/23/15 16:02
ARC
P5L0392
Weight
Ignitability
Pass
mm/sec
0.10
1
•1030 1/19/16 15:30
CDL
136A02156
Nitrate/Nitrite as N
11
mglkg dry
5.3
0.58
1
*SM4500-NO3 F 12/29115 11:45
CLB
PSL0435
pH
12 HT
pH Units
1
"9040C 1118116 16:47
EGC
P6A0251
Total Kjeldahl Nitrogen
1400
mglkg dry '
530
210
2
*351.2 114/16 9:42
CLB
PSL0410
Ammonia as N
52
mglkg dry
11
2.4
2
'SM4500-NH3 G 12128/15 10:37
CLB
PSL0394
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
•1311 ZHE
1/19/16 9:00
ANG
P6A0249
TCLP Extraction
Complete
N/A
1
*1311
1/20/16 7:00
JAB
P6A0264
TCLP Extraction
CompleteA
N/A
1
*1311
1/20/16 7:00
JAB
P6A0264
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
'7470A
1/20/16 13:47
JAB
P6A0281
Arsenic
BRL
mg/L
0.050
0.0035
1
'6010C
1/20/16 18:23
bgm
P6A0289
Barium
BRL
mg/L
5.0
0.0035
1
'6010C
1/20/16 18:23
bgm
P6A0289
Cadmium
BRL
mg/L
0.025
0.00050
1
'6010C
1/20/16 18:23
bgm
P6A0289
Chromium
BRL
mg/L
0.25
0.0030
1
'6010C
1/20/16 18:23
bgm
P6A0289
Lead
BRL
mg/L
0.050
0.0065
1
'6010C
1/20/16 18:23
bgm
P6A0289
Selenium
BRL
mg/L
0.10
0.016
1
•6010C
1/20/16 18:23
bgm
P6A0289
Silver
BRL
mg/L
0.25
0.0010
1
`6010C
1/20/16 18:23
bgm
P6A0289
TCLP•Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.34
1
*8081B
1/21116 13:18
JMC
P6A0262
Dieldrin
BRL
ug/L
0.50
0.022
1
'8081B
1/21/16 13:18
JMC
P6A0262
Endrin
BRL
ug/L
0.50
0.020
1
'8081B
1/21/16 13:18
JMC
P6A0262
gamma-BHC
BRL
ug/L
0.50
0.013
1
'8081B
1/21/16 13:18
JMC
P6A0262
Heptachlor
BRL
ug/L
0.50
0.015
1
'8081B
1/21/16 13:18
JMC
PGA0262
Heptachlor Epoxide
BRL
ug/L
0.50
0.018
1
'8081 B
1/21/16 13:18
JMC
P6A0262
Methoxychlor
BRL
ug/L
0.50
0.033
1
'8081B
1/21/16 13:18
JMC
P6A0262
Toxaphene
BRL
ug/L
25
0.16
1
'8081B
1/21/16 13:18
JMC
P6A0262
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
51 %
13-186
Tetrachloro-m-xylene
46 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Tdchlorophenol
BRL
mg/L
0.25
0.0023
1
"8270D
1/20/16 21:54
JMV
P6A0290
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0026
1
'8270D
1/20/16 21:54
JMV
P6A0290
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0019
1
'8270D
1/20/16 21:54
JMV
P6A0290
2-Methylphenol
BRL
mg/L
0.050
0.0021
1
'8270D
1/20/16 21:54
JMV
.- P6A0290
3/4-Methylphenol
BRL
mg/L
0.050
0.0019
1
'8270D
1/20/16 21:54
JMV
P6A0290
,,. ._.; This rgportshould;not,be;reproduced,;axcept,in;its;entirety„withputthe_wnttep.conserat,of,Prism Laboratopes Inc
449 Springbrook Road - P.O. Box.240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 42

4
4
Laboratory Report
IA
; Full -Service Analyi:ieal 8 - ,-
R I S M I Environmental Solutions 01/29/2016
�LABOMTOPIF$ CMG
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Quarterly and Haz
Waste Parameters)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 5120379-01
Prism Work Order: 5120379
Time Collected: 12/21/15 08:30
Time Submitted: 12/21/15 16:10
Parameter
Result
Units
Report MDL
Limit
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Hexachlorobenzene
BRL
mg/L
0.050 0.0019
1
*8270D
1/20/16 21:54
JMV
P6A0290
Hexachlorobutadiene
BRL
mg/L
0.050 0.0026
1
*8270D
1/20/16 21:54
JMV
P6A0290
Hexachloroethane
BRL
mg/L
0.050 0.0025
1
*8270D
1/20/16 21:54
JMV
P6A0290
Nitrobenzene
BRL
mg%L
0.050 0.0024
1
*8270D
1120/16 21:54
JMV.
P6A0290
Pentachlorophenol
BRL
mg/L
0.25 0.0025
1
*8270D
1/20116 21:54
-JMV
P6A02§0e'
Pyridine
BRL
mg/L
0.25 0.0021
1
*8270D
1/20/16 21:54
JMV
P6A0290
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
81 %
43-140
2-Fluorobiphenyl
71 %
44-119
2-Fluorophenol
40 %
19-119
Nitrobenzene-d5
68 %
44-120
Phenol-d5
30 %
11-52
Terphenyl-d14
80 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35
0.83
1
*8260B
1/19/16 16:02
KDM
P6A0275
1,2-Dichloroethane
BRL
ug/L
25
0.66
1
*8260B
1/19116 16:02
KDM
P6A0275
1,4-Dichlorobenzene
BRL
ug/L
380
0.50
1
*8260B
1/19/16 16:02
KDM
P13A0275
Benzene
BRL
ug/L
25
0.48
1
*8260B
1/19/16 16:02
. KDM
136A0275
Carbon Tetrachloride
BRL
ug/L
25
1.1
1
*8260B
1/19/16 16:02
KDM
P6A0275.
Chlorobenzene
BRL
ug/L
5000
0.62
1
*8260B
1/19116 16:02
KDM
NA0275
Chloroform
BRL
ug/L
300
0.76
1
*8260B
1/19/16 16:02
KDM
P6A6275
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
10000
2.4
1
*8260B
1/19116 16:02
KDM
P6A0275
Tetrachloroethylene
BRL
ug/L
35
0.98
1
*8260B
1/19/16 16:02
KDM
P6A0275
Trichloroethylene
BRL
ug/L
25
0.78
1
*8260B
1119/16 16:02
KDM
P6A0275
Vinyl chloride
BRL
ug/L
20
0.97
1
*8260B
1/19/16 16:02
KDM
P6A0275
Surrogate
Recovery
Control Limits
Total Metals
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8
91 %
77 %
94 %
80-124
75-129
77-123
Mercury
0.077
mglkg dry
0.023
0.0015
1
*7471B 12/29/15 11:38
JAB
P5L0438
SAR Soil Preparation
Complete
g
1
*2-78-054 12/28/15 7:30
JAB
1351-0408
SAR Percent Moisture
79.9
% by
0.100
0.100
1
*2-78-054 12/30M S 9:40
JAB
PSL0433
Weight
Arsenic
5.2
mglkg dry
0.27
0.060
1
*6010C 12/31/16 19:40
bgm
PSL0404
Sodium Absorption Ratio
0.56
[blank]
0.30
0.016
1
*2-78.054 1/12/16 13:57
bgm
PSLO430
Cadmium
0.28
mglkg dry
0.27
0.0057
1
*6010C 12/31/15 19:40
bgm
P5L0404
Calcium
990 B
mglL
.20
1.7
200
*6010C 1112116 13:57
bgm
P5LO430
Copper
24
mglkg dry
0.54
0.094
1
*6010C 12/31/15 19:40
bgm
P5LO404
Lead
29
mglkg dry
0.27
0.028
1
*6010C 12/31/15 19:40
bgm
P5L0404
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010C 12/31/15 20:27
bgm
P51-0430
This. re port, should not.,be, rep roduced,-,exceptin, its, entirety.,withgu#thewrittenconsent.of.Prismlabotatones,Inc
449 Springbrook Road.- P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704/52"409 . Pa9Q Jr O.f,42,

�f 4
�P�&rtt A' Full -Service Analytical S
t I S M I Environmental Solutions
UBOMTOPIES, 1N
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Quarterly and Haz
Waste Parameters)
Sample Matrix: Solid
Laboratory Report
01 /29/2016
Client Sample ID: Sta-Lime
Prism Sample ID: 5120379-01
Prism Work Order: 5120379
Time Collected: 12/21/15 08:30
Time Submitted: 12/21/15 16:10 .
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
DateRme
Batch
ID
Nickel
120
mg/kg dry
0.54
0.051
1
`6010C
12/31/15 19:40
bgm
PSL0404
Potassium
4500
mg/kg dry
130
13
10
'6010C
1111/16 23,27
bgm
PSL0404
Selenium
BRL
mg/kg dry
5.4
0.39
10
'6010C
1111/16 23:27
bgm
P51-0404
Sodium
520
mg/kg dry
16
0.47
1
"6010C
12/31/15 19:40
bgm
PSL0404
Sodium
64
mg/L
5.0
0.074
10
"6010C
12/31/15 20:27
bgm
PSL0430
Zinc
56
mg/kg dry
2.7
0.033
1
•6010C
12/31/15 19:40
bgm
PSL0404
I,nis,report>nouiu not,De:reproaucea„ except.m its.entirety, wmoui me wnnen consent or rnsm-t.aooratonesiinc: „ 5 *k• .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-8001529-6364-Fax:[phone] Page 6=0.f 42

Full -Service Analyal &
11PRISM I Environmental Soliftutlons
RIEA INC,
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Quarterly and Haz
Waste Parameters)
Sample Matrix: Solid
Laboratory Report
01129/201'6"-
Client Sample ID: Sta-Lime
Prism Sample ID: 5120379-01RE1
Prism Work Order: 5120379
Time Collected: 12/21/15 08:30
Time Submitted: 12/21/15 16:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/l-ime ID
General Chemistry Parameters
Phosphorus -Total 1500 mg/kg dry 53 14 20 *SM4500-P F 115/16 7:45 CLB P6A0021
Tlils:report,should, not be -reproduced, except in,jts enfiretyi withoutthe, written.consent of Pdsm,1aboratories,;.lnc.:i.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7'o'f 42

�� Full -Service Analytical
�R',S M I Environmental Solutions
Ad, , MIHa
Level II QC Report
1/29/16
City of Statesville, NC Project: StaLime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
TCLP Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6AO275 - 5030B
Blank (P6AO275-BLK1)
Prepared &Analyzed: 01/19/16
1,1-Dichloroethylene
BRL
35
ug/L
1,2-Dichloroethane
BRL
25
ug/L
1,4-Dichlorobenzene
BRL
380
ug/L
Benzene
BRL
25
ug/L
Carbon Tetrachloride
BRL
25
ug/L
Chlorobenzene
BRL
5000
ug/L
Chloroform
BRL
300
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
10000
ug/L
Tetrachloroethylene
BRL
35
ug/L
Trichloroethylene
BRL
25
ug/L
Vinyl chloride
BRL
20
ug/L
Surrogate:4-Bromofluorobenzene
45.6
ug/L
50.00
91
80-124
Surrogate: Dibromofluoromethane
49.6
ug/L
50.00
99
75-129
Surrogate: Toluene-d8
46.8
U91L
50.00
94
77-123
LCS (P6AO275-BSI)
Prepared & Analyzed: 01/19/16
1,1-Dichloroethylene
19.8
35
ug/L
20.00
99
70-154
1,2-Dichloroethane
20.1
25
ug/L
20.00
100
68-131
1,4-Dichlorobenzene
20.2
380
ug/L
20.00
101
75-126
Benzene
20.2
25
ug/L
20.00
101
77-128
Carbon Tetrachloride
19.8
25
ug/L
20.00
99
72-142
Chlorobenzene
20.0
5000
ug/L
20.00
100
78-119
Chloroform
19.6
300
ug/L
20.00
98
77-130
Methyl Ethyl Ketone-(2-Butanone)
17.9
10000
ug/L
20.00
90
71-134
Tetrachloroethylene
18.6
35
ug/L
20.00
93
80-129
Trichloroethylene
21.0
25
ug/L
20.00
105
77-133
Vinyl chloride
15.0
10
ug/L
20.00
75
57-141
Surrogate:4-Bromofluorobenzene
45.8
U91L
50.60
92
80-124
Surrogate: Dibromofluoromethane
49.4
ug/L
50.00
99
75-129
Surrogate: Toluene -dB
48.5
ug/L
50.00
97
77-123
This+report should not be reproduced, except in -its entirety;' without the :written consent of+Prism Laboratories, fnaa:..
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Pag,2.:S,of

I S M Full -Service Analytical &
h E Environmental Solutions
�MrA wa
Level II QC Report
1 /29/16
City of Statesville, NC Project: StaLime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
TCLP Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6AO275 - 5030B
LCS Dup (P6AO275-BSD1)
Prepared & Analyzed: 01/19/16
1,1-Dichloroethylene
18.8
35
ug/L
20.00
94
70-154
5
20
1,2-Dichloroethane
20.7
25
ug/L
20.00
103
68-131
3
20
1,4-Dichlorobenzene
20.0
380
ug/L
20.00
100
75-126
0.7
20
Benzene
19.7
25
ug/L
20.00
99
77-128
2
20
Carbon Tetrachloride
19.5
25
ug/L
20.00
97
72-142
2
20
Chlorobenzene
19.8
5000
ug/L
20.00
99
78-119
0.7
20'
Chloroform
19.6
300
ug/L
20.00
98
77-130
0.05
20
Methyl Ethyl Ketone (2-Butanone)
19.5
10000
ug/L
20.00
97
71-134
8
20
Tetrachloroethylene
18.1
35
ug/L
20.00
91
80-129
3
20
Trichloroethylene
20.6
25
ug/L
20.00
103
77-133
2
20
Vinyl chloride
15.1
10
ug/L
20.00
76
57-141
0.7
20
Surrogate:4-Bromofluorobenzene
44.5
ug/L
50.00
89
80-124
Surrogate: DibromoMoromethane
48.9
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
48.1
ug/L
50.00
96
77-123
This report should not be.reproduced,<except in its entirety; -without the written -consent of Prism Laboratories,alnc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:_ 1-8001529-6364 - Fax: 704/52"409 Page 9 of 42

�a�5 Full-Sarvice Analytical &
R'I.S , tr , I Environmental Solutions
AMQMXI 7't.i-room 1�
Level II QC Report
1/29116
City of Statesville, NC Project: Stal-ime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111 .
Statesville, NC 28687
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6AO290 - 351 OC MS
Blank (P6A0290-BLK1)
Prepared & Analyzed: 01/20/16
2,4,5-Trichlorophenol
BRL
0.25
mg/L
2,4,6-Trichlorophenol
BRL
0.10
mg1L
2,4-Dinitrotoluene
BRL
0.050
mg/L
2-Methylphenol
BRL
0.050
mg/L
3/4-Methylphenol
BRL
0.050
mg/L
Hexachlorobenzene
BRL
0.050
mg/L
Hexachlorobutadiene
BRL
0.050
mg/L
Hexachloroethane
BRL
0.050
mg/L
Nitrobenzene
BRL
0.050
mg/L
Pentachlorophenol
BRL
0.25
mg/L
Pyridine
BRL
0.25
mg/L
Surrogate: 2,4,6-Tribromonhenol
0,330
mg/L
0.5000
66
43-140
Surrogate:2-Fluorobinhenyl
0.159
mg/L
0.2500
64
44-119
Surrogate:2-Fluoroohenol
0.211
mg/L
0.5000
42
19-119
Surrogate: Nitrobenzene-d5
0.176
mg1L
0.2500
70.
44-120
Surrogate: Phenol-d5
0.132
mg1L
0.5000
26
11-52
Surrogate: Terohenyl-04
0.190
mg/L
0.2500
76
50-134
LCS (P6A0290-BS1)
Prepared &Analyzed: 01/20/16'
2,4,5-Trichlorophenol
0.164
0.25
mg/L
0.2500
66
53-123
2,4,6-Trichlorophenol
0.157
0.10
mg/L
0.2500
63
50-125
2,4-Dinitrotoluene
0.171
0.050
mg/L
0.2500
68
57-128
2-Methylphenol
0.130
0.050
mg/L
0.2500
52
30-117
3/4-Methylphenol
0.122
0.050
mg/L
0.2500
49
29-110
Hexachlorobenzene
0.165
0.050
mg/L
0.2500
66
53-125
Hexachlorobutadiene
0.149
0.050
mg/L
0.2500
60
22-124
Hexachloroethane
0.127
0.050
mg/L
0.2500
51
21-115
Nitrobenzene
0.173
0.050
mg/L
0.2500
69
45-121
Pentachlorophenol
0.150
0.25
mg/L
0.2500
60
35-138
Pyridine
0.0902
0.25
mg/L
0.2500
36
10-53
Surrogate: 2,4,6-Tribromonhenol
0.352
mg1L
0.5000
70
43-140
Surrogate:2-Fluorobinhenyl
0.180
mg1L
0.2500
72
44-119
Surrogate:2-Fluoroohenol
0.221
mg1L
0.5000
44
19-119
Surrogate: Nitrobenzene-d5
0.177
mg1L
0.2500
71
44-120
Surrogate: Phenol-d5
0.137
mg1L
0.5000
27
11-52
Surrogate: Terohenyl-d14
0.186
mg1L
0.2500
74
50-134
This report -should not be reproduced except in•its entirety, -,without the. written.consent.of Prism. Laboratories;dnc: -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page. 6f:42 ; '

�x Level II QC Report
�pR�SM p
, Full -Service Analytical'& 1/29/16
�� Environmental solutions
��i,�6o17�iroRTEA 1 +
City of Statesville, NC Project: Stal-ime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Spike Source
%REC
RPD
Analyte
Result
Limit
Units
Level Result
%REC
Limits
RPD
Limit Notes
Batch P6A0290 - 3510C MS
LCS Dup (P6A0290-BSD1)
Prepared &Analyzed: 01/20/16
2,4,5-Trichlorophenol
0.188
0.25
mg/L
0.2500
75
53-123
14
20
2,4,6-Trichlorophenol
0.176
0.10
mg/L
0.2500
70
50-125
11
20
2,4-Dinitrotoluene
0.194
0.050
mg/L
0.2500
78
57-128
13
20
2-Methylphenol
0.147
0.050
mg/L
0.2500
59
30-117
12
20
3/4-Methylphenol
0.139
0.050
mg/L
0.2500
55
29-110
13
20
Hexachlorobenzene
0.182
0.050
mg/L '
0.2500
73
53-125
10
20
Hexachlorobutadiene
0.167
0.050
mg/L
0.2500
67
22-124
11
20
Hexachloroethane
0.142
0.050
mg/L
0.2500
57
21-115
11
20
Nitrobenzene
0.191
0.050
mg/L
0.2500
77
45-121
10
20
Pentachlorophenol
0.176
0.25
mg/L
0.2500
70
35-138
16
20
Pyridine
0.111
0.25
mg/L
0.2500
44
10-53
21
20 D
Surrogate: 2,4,6-Tribromoohenol
0.379
mg/L
0.5000
76
43-140
Surrogate:2-F/uorobiohenyl
0.196
mg/L
0.2500
78
44-119
Surrogate:2-Fluoroohenol
0.235
mg/L
0.5000
47 .19-119
Surrogate: Nitrobenzene-d5•
0.200
mg2.
0.2500
80
44-120
Surrogate: Phenol-d5
0.149
mg2
0.5000
30
11-52
Surrogate: Terohenyl-04
0.198
mg2
0.2500
79
50-134
report should not be:reproduced;;except.in its entirety; without the = written consent of.Pdsm,Laboratories;anc.,t
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page i f of 4M

=:r Level 11 QC Report -.l
* a Full-Sarvioe Analytical 8 .-
A� q' I,S invironmentalSolutione 1/29/16"°"l'
�! LABOMTOPoEA ING
City of Statesville, NC Project: Stal-ime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
TCLP Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6AO262 - 351 OC GC
Blank (P6AO262-BLK1)
Prepared: 01/19/16 Analyzed: 01/21/16
Chlordane
BRL
2.5
ug/L
Dieldrin
BRL
0.50
ug/L
Endrin
BRL
0.50
ug/L
gamma-BHC
BRL
0.50
ug/L
Heptachlor
BRL
0.50
ug/L
Heptachlor Epoxide
BRL
0.50
ug/L
Methoxychlor
BRL
0.50
ug/L
Toxaphene
BRL
25
ug/L
Surrogate: Decachlorobinhenyl
3.22
ug/L
5.000 64 13-186
Surrogate: Tetrachloro-m-xylene
2.95
ug/L
5.000 59 40-134
LCS (P6A0262-BS1)
Prepared: 01/19/16 Analyzed: 01/21/16
Dieldrin
4.21
0.50
ug/L
5.000 84 69-130
Endrin
4.30
0.50
ug/L
5.000 86 69-144
gamma-BHC
4.07
0.50
ug/L
5.000 81 66-129
Heptachlor
4.10
0.50
ug/L
5.000 82 61-136
Heptachlor Epoxide
4.22
0.50
ug/L
5.000 84 69-131
Methoxychlor
4.03
0.50
ug/L
5.000 81 70-157
Surrogate: Decachlorobinhenyl
3.13
ug/L
5.000 63 13-186
Surrogate: Tetrachloro-m-xylene
3.01
u91L
5.000 60 40-134
LCS (P6AO262-BS2)
Prepared: 01/19/16 Analyzed: 01/21/16
Chlordane
46.7
2.5
ug/L
50.00 93 50-150
Surrogate: Decachlorobinhenyl
2.92
ug/L
5.000 58 13-186
Surrogate: Tetrachloro-m-xylene
2.69
ug/L
5.000 54 40-134
LCS (PM0262-13W)
Prepared: 01/19/16 Analyzed: 01/21/16
Toxaphene
57.1
25
ug/L
50.00 114 50-150
Surrogate: Decachlorobinhenyl
2.96
ug/L
5.000 59 13-186
Surrogate: Tetrachloro-m-xylene
2.68
ug2.
5.000 54 40-134
h T • < ., - This report.should.not be, reproduced; except in. itsentirety,,.without the.written consent of P.rism,Laboratores; Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page; 2 'Of 42.

,a ow\ Full -Service Analytical &
P R I S/w' `1 Y, I Environmental Solutions
®'8�ueoR,vonMEL n�c
City of Statesville, NC Project: StaLime (Quarterly and Haz
Attn: Andy Smith Waste Parameters)
P.O. Box 1111
Statesville, NC 28687
TCLP Organochlorine Pesticides by GC/ECD - Quality Control
Reporting
Analyte Result Limit Units
Level II QC Report
1 /29/16
Prism Work Order: 5120379
Time Submitted: 12/21/2015 4:10:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P6AO262 - 351 OC GC
LCS Dup (P6A0262-BSD1)
Prepared: 01/19/16 Analyzed: 01/21/16
Dieldrin
4.23
0.50
ug/L
5.000
85
69-130
0.6
20
Endrin
4.32
0.50
ug/L
5.000
86
69-144
0.6
20
gamma-BHC
4.08
0.50
ug/L
5.000
82
66-129
0.2
20
Heptachlor
4.01
0.50
ug/L
5.000
80
61-136
2
20
Heptachlor Epoxide
4.23
0.50
ug/L
5.000
85
69-131
0.3
20
Methoxychlor
4.15
0.50
ug/L
5,000
83
70-157
3
20
Surrogate: Decachlorobiohenyl
3.16
ug/L
5.000
63
13-186
Surrogate: Tetrachloro-m-xylene
2.78
ug/L
5.000
56
40-134
_,. , _ , ;.,::•- This report should,not be reproduced, except in its entirety; :without the written consent of Prism.Laboratories;--Inc. <- :w
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 .Of 42

e
Level II QC Report
gp, Full-ServiceAnalytical& ^*• `1/29/1�6„�,'
P R' S'M I Environmental Solutions
®V• LABOFATORIEl, in
City of Statesville, NC Project: StaLime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5L0404 - 3050B
Blank (P51-0404-BLK1)
Prepared: 12/28/15 Analyzed: 12/31/15
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
'BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P51-0404-121SI)
Prepared: 12/28/15 Analyzed: 12/31/15
Arsenic
24.1
0.25
mg/kg wet
25.00 96
80-120
Cadmium
24.5
0.25
mg/kg wet
25.00 98
80-120
Copper
25.7
0.50
mg/kg wet
25.00 103
80-120
Lead
24.3
0.25
mg/kg wet
25.00 97
80-120
Nickel
23.9
0.50
mg/kg wet
25.00 96
80-120
Potassium
476
12
mg/kg wet
500.0 95
80-120
Selenium
24.2
0.50
mg/kg wet
25.00 97
80-120
Sodium
488
15
mg/kg wet
500.0 98
80-120
Zinc
24.9
15
mg/kg wet
25.00 100
80-120
Batch MUM - SAR 2-78-054
Blank (P51-0408-BLKI)
Prepared & Analyzed: 12/28/15
SAR Soil Preparation
Complete
g
report shouldmot:be reproduced, except in:its entirety,. without the written•consent,of Prism, Laborptones,,lnc ,
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Level 11 QC Report
i1'i�usos�ro�ea Full -Service b
1/29/6,1A Environmental Solutions
�Nc
City of Statesville, NC Project: Stal-ime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 1351-0430 - 3010A
Blank (P5LO430-BLKI)
Prepared: 12/29/15 Analyzed: 12/31/15
Sodium Absorption Ratio
BRL
0.30 [blank]
Calcium
0.268
0.10 mg/L
BH
Magnesium
BRL
0.10 mg/L
Sodium
BRL
0.50 mg/L
BH
Batch P5L0433 - NO PREP
Blank (1351-0433-131-K1)
Prepared: 12/29/15 Analyzed: 12/30/15
SAR Percent Moisture
BRL
0.100 % by Weight
Duplicate (P51-0433-DUP1)
Source: 5120379-01
Prepared: 12/29/15 Analyzed: 12/30/15
SAR Percent Moisture
74.9
0.100 % by Weight 79.9 6 200
Batch P5LO438 - 7471 B
Blank (P5LO438-BLKI)
Prepared & Analyzed: 12/29/15
Mercury
BRL
0.020 mg/kg wet
LCS (P5LO438-BSI)
Prepared & Analyzed: 12/29/15
Mercury
0.432
0.020 mg/kg wet
0.4167 104 80-120
- This reporbshoutd not be-reproduced,,except-in its entirety;=without the.written:consent of Prism;Laboratories;;,lne
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: 704/52"409 P89@,i:� Jr 0} 42

V.
Ad
ni Full -Service Analytical &
Environmental Solutions
Aa�idiuioaeaixd .
Level II QC Report
1/2916
City of Statesville, NC Project: Stal-ime (Quarterly and Haz Prism Work Order, 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
TCLP Metals - Quality Control
Reporting Spike Source %REC RPD
Amalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6AO281 - 7476A
Blank (P6A0281-BLK1)
Prepared & Analyzed: 01/20/16
Mercury
BRL
0.010
mg/L
LCS (P6A0281-BSI)
Prepared & Analyzed: 01/20/16
Mercury
0.00954
0.010
mg/L
0.009375 102
80-120
Batch P6AO289 - 301 OA
Blank (P6A0289-BLK1)
Prepared & Analyzed: 01/20/16
Arsenic
BRL
0.050
mg/L
Barium
BRL
5.0
mg/L
Cadmium
BRL
0.025
mg/L
Chromium
BRL
0.25
mg/L
Lead
BRL
0.050
mg/L
Selenium
BRL
0.10
mg/L
Silver
BRL
0.25
mg/L
LCS (P6A0289-BSI)
Prepared & Analyzed: 01/20/16
Arsenic
1.33
0.050
mg/L
1.250 106
80-120
Barium
1.29
5.0
mg/L
1.250 103
80-120
Cadmium
1.28
0.025
mg/L
1.250 102
80-120
Chromium
1.29
0.25
mg/L
1.250 .104
80-120
Lead
1.25
0.050
mg/L
1.250 100
80-120
Selenium
1.34
0.10
mg/L
1.250 107
80-120
Silver
0.503
0.25
mg/L
0.5000 101
80-120
;•, This: report,shou4not-be_reproduced, except ,in,•its:entirety%without, the: Written, consent of .P.,rism;Laboratories;;lncJ
449 Springbrook Road - P.O. Box 240543'- Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number; 1-8001529-6364- Fax: [phone] P89e.-• C) Of,4 2 ,;;`

®i
.Full-Service
bsRISM I. EnvIronmentalSolutlon
®�LABOMTONIEm INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime (Quarterly and Haz
Waste Parameters)
Level II QC Report
1129/16
Prism Work Order: 5120379
Time Submitted: 12/21/2015 4:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PSL0392 - Solids, Dry Weight
Blank (PSL0392-BLK1) Prepared & Analyzed: 12/23/15
% Solids 160 0.100 "/a. by Weight
Batch P5L0394 - NO PREP
Blank (PSL0394-BLK1) Prepared & Analyzed: 12/28/15
Ammonia as N BRL 5.0 mg/kg wet
LCS (P5LO394-BSI) Prepared & Analyzed: 12/28/15
Ammonia as N 121 5.0 mg/kg wet 125.0 97 80-120
Matrix Spike (P5L0394-MS1) Source: 5120379-01 Prepared & Analyzed: 12/28/15
Ammonia as N 122 11 mg/kg dry 131.5 51.6 53 80-120 MI
Matrix Spike Dup (P5L0394-MSD1) Source: 5120379-01 Prepared & Analyzed: 12/28/15
Ammonia as N 124 11 mg/kg dry 131.5 51.6 55 80-120 2 20 MI
Batch P51_0410 - 351.2
Blank (PSL0410-BLK1) Prepared: 12/28/15 Analyzed: 01/04/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (PSL0410-BSI) Prepared: 12/28/15 Analyzed: 01/04/16
Total Kjeldahl Nitrogen 471 100 mg/kg wet 500.0 94 90-110
Matrix Spike (PSL0410-MSI) Source: 5120379-01 Prepared: 12/28/15 Analyzed: 01/04/16
Total Kjeldahl Nitrogen 7340 530 mg/kg dry 5260 1440 112 90-110 MI
This report"should riot be "reproduced; except iri`its entlrety'witho'u#`the"written"consent'of Prism"L'aboYatories; lric. --�-
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 282M-0543
Phone: [phone] -Toll Free Number:1-800/529-6364 -Fax: [phone] P0901 7.Of 42..

A
VZ
5' Full -Service Analytical 9.
P R I S M I Environmental Solutions
A'ueoluToritEs, ixc
Level II QC Report
City of Statesville, NC Project: StaLime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:0013M
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P51_0410 - 351.2
Matrix Spike Dup (PSL0410-MSD1)
Source: 5120379-01
Prepared: 12/28/15 Analyzed: 01/04/16
Total K)eldahl Nitrogen
Batch P5L0435 - NO PREP
5960 530 mg/kg dry
5260 1440 86
90-110 21 20 D, MI
Blank (P5L0435-BLK1)
Prepared & Analyzed: 12/29/15
Nitrate/Nitrite as N
LCS (PSL0435-BSI)
BRL 5.0 mg/kg wet
Prepared & Analyzed: 12/29/15
Nitrate/Nitrite as N
Matrix Spike (P5L0435-MS1)
48.2 5.0 mg/kg wet
Source: 5120379-01
50.00 96
Prepared & Analyzed: 12/29/15
80-120
Nitrate/Nitrite as N
Matrix Spike Dup (P5L0435-MSDI)
56.5 5.3 mg/kg dry
Source: 5120379-01
52.60 10.6 87
Prepared & Analyzed: 12/29/15
80-120
Nitrate/Nitrite as N
57.7 5.3 mg/kg dry
52.60 10.6 89
80-120 2 20
Batch P51_0442 - SM4500-PBS
Blank (P5L0442-BLK1) Prepared: 12/29/15 Analyzed: 12/30/15
Phosphorus -Total BRL 2.5 mg/kg wet
Batch P6A0021 - SM4500-PBS
Blank (P6A0021-BLK1) Prepared: 01/04/16 Analyzed: 01/05/16
Phosphorus -Total BRL 2.5 mg/kg wet
This. report•.should not be reproduced,.except in.its; entirety,..without the written consent of:: P.rism.Laboratories, Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page;18 0f-42

m
Level II QC Report
PI IS
�, I Full -Service Analytical & - 1
Environmental Solutions
Ad 1/29/16'
...... rmm
City of Statesville, NC Project: Stal-ime (Quarterly and Haz Prism Work Order: 5120379
Attn: Andy Smith Waste Parameters) Time Submitted: 12/21/2015 4:10:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6AO021 - SM4500-PB5
LCS (P6AO021-BS1) Prepared: 01/04/16 Analyzed: 01/05/16
Phosphorus -Total 100 2.5 mg/kg wet 100.0 100 90-110
Matrix Spike (P6A0021-MS1) Source: 5120379-01REI Prepared: 01/04/16 Analyzed: 01/05/16
Phosphorus -Total 1070 53 mg/kg dry 105.2 1450 NR 80-120 MC'
Matrix Spike Dup (P6AO021-MSDI) Source: 6120379-01RE1 Prepared: 01/04/16 Analyzed: 01/05/16
Phosphorus -Total 1130 53 mg/kg dry 105.2 1450 NR 80-120 5 20 MC
Batch P6AO251 - NO PREP
LCS (P6AO251-BSI) Prepared & Analyzed: 01/18/16
pH 6.80 pH Units 6.880 99 99-101
Duplicate (P6A0251-DUP1) Source: 5120379-01 Prepared & Analyzed: 01/18/16
pH 12.5 pH Units 12.5 0.2 10
This..report.shouldnot baseproduced,;except in its_entirety„without;the,.wriften,coosentotprism:Laboratodesranc ,
449 Springbrook Road - P.O. Box 24050 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1.800/529-6364 - Fax: [phone] Page'?19<0f 42'

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Datelrime
5120379-01
P51_0410
0.05 g
25 mL
12/28/15 11:30
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Date rime
5120379-01RE1
P6A0021
1 g
50 mL
01/04/16 11:30
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
DateTme
5120379-01
P51-0392
30 g
30 g
12/23/15 16:02
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/rime
5120379-01
P6A0264
100 g
2000 mL
01/19/16 14:10
5120379-01
P6A0249
25 g
500 mL
01/18/16 16:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/rime
5120379-01
PGA0289
10 mL
50 mL
01/20/16 11:45
Prep Method: 7470A
Lab Number
Batch
Initial
Final
DateTme
5120379-01
P6A0281
20 mL
30 mL
01/20/16 8:30
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/rime
5120379-01
P6A0262
200 mL
10 mL
01/20/16 9:00
Prep Method: 3610C MS
Lab Number
Batch
Initial
Final
DateTme
5120379-01
P6A0290
200 -
mL
1 mL
=' 01/20/16 9:30 '
Prep Method: 5030B
Lab Number
Batch
Initial
Final
DateTme
5120379-01
P6A0275
1
mL
10 mL
01/19/16 8:54
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/rime
5120379-01
1351-0430
50
mL
50 mL
12/29/15 8:37
5120379-01
P51_0430
50
mL
50 mL
12/29/15 8:37
5120379-01
P51_0430
50
mL
50 mL
12/29/15 8:37
Prep Method: 3050B
Lab Number
Batch
Initial
Final
DateTme
5120379-01
P51_0404
1.95
g
50 mL
12/28/15 7:45
5120379-01
1351_0404
1.95
g
50 mL
12/28/15 7:45
Prep Method: 7471B
Lab Number -
Batch
Initial
Final
Daterrime
,,, ,;Thisx portshould:not bexeproduced,;except imits,entirety;.-without the written consentof.Prism-Laboratories,. inc: ... ,,
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] P892.>20 Of 4Z

Sample Extraction Data
Prep Method: 7471E
Lab Number Batch Initial Final Datemme
5120379-01 P5L0438 0.55 g 50 mL 12/29/15 8:15
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Daterrime
5120379-01 P51_0408 250 g 250 g 12/28/15 7:30
Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab Number Analysis
5120379-01 Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number Analysis
5120379-01 Reactivity, Cyanide (Sub)
5120379-01 Reactivity, Sulfide (Sub)
This.report hould not be.reproduced,: except in,its.entirety,,without the written consent of Prism laboratories, Inc: �:,:..:.; ,,,•;,- ., •..;..,r:..-:.: r. -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page Z j Of 42-

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Full -Service Analytical &
rr I S M I Environmental Solutions PAGE OF QUON 9 TO ENSURE PROPER BILLING:
•ip„'�"•-57'�LABORATORIES, ING
•'ai 449 Springbrook Road ��arlotte, NC Project Name:
Phone [phone]Fax: [phone] Short Hold Analysis: sis: �IAe.sN) (LNof ) 1�UjS,
T P,r.ojec.t:
(Yes) ( NO
)
Client Company Name /—r *Please ATTACH any project specific reporting (QC LEVEL I If III IV)
provisions and/or QC Requirements
Report {To/Contact Name: Invoice To:
Reporting Address: Address:
Samples INTACT upon arrival?
. Received,ON WET ICE1'
PROPER PRESERVATIVES Indicated?
Received 1NITHIN.HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd VVIOUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID: '�>"� Observed:
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Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
U Sample Iced on Collection: YES NO
P P
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
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CLIENT
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COLLECTED
(SOIL,
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NO.
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SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIMES
ID -NO.,
HOURS
SLUDGE)
SEE BELOW
ITSSI
Ie
f
NCL
4
Ph o
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PA14
Tk
SA
Sampler's Signature Sampled By (Print Name) Affiliation -
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be .
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Relinquished By: (Signature) ReceN By. (Signature DateMilitary ours Additional Comments: S(tes4nl4ai�7iirie �,
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BY`od of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT VW ., U -TODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COO Group o.
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q
``
N r I t o 41,
f t9 ed Ex ❑ UPS ❑ Hand -delivered Field Service U Other
DES: UST: G UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
p COSC ❑NC ❑SC ❑ C ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SC ❑NC ❑SC El NC El SC [INC El SC13
`
'NTAINER TYPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
" .
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ORIGINAL
rPC,'•.h4n ____. ____-__— _ --____ ____ ___ ___ _.__._.__- - ______.._____.....-- ._.--.._ -_._-_______.__....._._.-..._�.__.-.-__.....�.........-.._._-�...�_..-�_.r-T�....-...-.-.......'....._r..-.-_r..r...,-.rv..,..+,......r...rr..%�..•,rr.......i.,,
r,
I

1-T-e-r
?' CHAIN OF CUSTODY RECORD
Full -Service Analytical &
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RISM s PAGE aOF QUOTE # TO ENSURE PROPER BILLING:
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Phone [phone] • Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Client Company Name: /� �' 'Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
p y 'V r'( provisions and/or QC Requirements
Report To/Contact Name: Invoice To:
Reporting Address: Address:
Samples INTACT upon arrival?
" .:ReaeiV6d-6N WET ICE?.:
':PR.OPER PRESERVATIVES indicated?
Received INITHIN`}90LDING Tij
INtES?'
''CUSTODY SEALS INTACT? '.-
VOLATILES reed W10UT HEAbSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID:'1/y%`0 Observed:
}' °C / Corr: I6- 2 °CI
Phone: Fax (Yes) (No): Purchase Order NoJBilling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL -
Email Address: Requested Due Date ❑ 1 Da ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days y y y y
Certification: NELAC DOD
FL NC
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pprovedust
Site Location Name: Samples received after 14:00 will be processed next business day.
SC OTHER
N/A
Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) 1
Sample Iced Upon Collection: YES
NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS
REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
\�s REMARKS
.
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVESletf-
jL
ID NO.HOURS
SLUDGE)
SEE BELOW
it,
C�
Cu
SA 047
Pjt
.
N
Nr
S• e
..
T leMi
Sampler's Signature Sampled By (Print Name) Affiliation
— -
Upon relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analysqfi as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relinquished By: (Signature). Recev, 6 y Signature Date
Military/Hours Additional Comments:
Sita.Artivaf:7im3: ; '
Rel nq By gnetu Re (Slgna a Date
Site [7e artur@ iirile:
1410
'
qulshed By. (Signature) ReceNed Fo sm Labo tod y: l" Date
� �� (,l�dl
((jGl7
Field Te'cfi Fe 3:
.
Gj
Nlilea9e(
fG od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITHCYSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Grop No.
0Yi SAMPLES.ARE NOT ACCEPTED AND VERIFIED AGAINST COC TIL RECEIVED AT THE LABORATORY,
Iv; is
W d Ex. 13 UPS ❑ Hand -delivered sm F1eld,Servlce ❑ Other
b, ES: ' UST: ROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:.
�.
C [] SCI NC ❑.SC I NC O SC :•� NC ❑ SC ❑❑ NC ❑ SC NC ❑ SC NC ❑ SC ❑❑ NC ❑ SC
NC ❑ SC'
N ❑❑
❑ a
' NTAINFR TVPF rnnF3s . A-= Amhor :-r:=.('laar P cPlactic• .TI -= Taflnn-i'inari r•'.an VC)A = Vnlatile Oroanim Analvsls (Zero Head Soace)

CHAIN OF CUSTODY RECORD LAB USE ONLY
gur7; 5 RISM
Full-Service Analytical & I YES' N0 N/A
Environmental Solutions PAGE OF QUOTE 8 TO ENSURE PROPER BILLING:
Samples INTACT_upon �rrival7
v{"v{Ju:V LABORATORIES, ING c L p
449 Springbrook Road • Charlotte, NC 28217
Project Name- �ITIv� 1'rr� &a (`k Received ON WET ICE!': ✓
Phone [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NOy r, PROPER PRESERVATIVES indicated?
� `Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
sReceived WITHIN HOLDING TIMES? _
Client Company Name: �["1�+ j(`e provisions and/or QC Requirements CUSTODY SEALS INTACT?
ReportTo/Contact Name: Invoice To. VOLATILES reed W/OUT HEADSPACE?
Reporting Address: Address: PROPER CONTAINERS used? '•;
TEMP: Therm Observed: 17_;r °C / Corr: &P • °C
Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL .
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days Cl 5 Days
Certification:
NELAC -DOD
FL NC
EDD Type: PDF_Excel_Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Poo must Be
SC OTHER
N/A
Site Location Name:
Samples received after 14:00 will be processed next business day.
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
y
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
'TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
ID NO.
HOURS
SLUDGE)
SEE BELOW
5 bc-e 's 1PJ'/1C9t,�
Co
ro
t�:
As
61
A. 3o yr, S
!uI S
1
/
Al leg
02(--lds
Pb
�r
Skied
OM
D(
TIC
P
S, -/,1 07
re�°
S�
1A
L' Ie
��
ILA
TO
P
e'
cal
S
U
rcA
P N
e r-L
j l
Sampler's Signature G":'
Sampled By (Print Name) . 4-7 0-fr1kc Affiliation
Upon rfelinquishing, this Chadn of Custody Is your authorization for Prism to proceed with the analyses a6 requested above. Any changes must be
,
submitted In writing to the Prism Project Manager. There will be chapRes for any changes after analyses have been initialized.
Rellnqush 9y Slgnaatu '
Rece' y: (Sgnature) ^ „ Dale Military/Hours
Addition al Comments:
SifeArri4 dime:: '
Relinquished ignature)
Re Signature) Da a
Sife DOarture:'fime:
.
`
quishe B . (Signature)
Received For ! LaboratorleRl,Date
Mileage:`: .'
sod of Sh pment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH 9JZTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COO Group No. 1
SAMPLES ARE NOT ACCEPTED AND VERIFIED
AGAINST COC TIL RECEIVED AT THE LABORATORY.
d Fx ❑ UPS ❑ Hand-delNered sm Field Service
❑ Other
"p DES: UST: G DWATER:
DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
C❑SC ❑NC ❑SC ❑ C ❑SC
❑NC ❑SC I ONC ❑SC I oNC❑SC ONC ❑SCI ONC ❑SCI ONC ❑SC
N ❑ ❑
❑
~% NTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
ORIGINAL �:

i:;- ._ a...e �.:,.�______�=�4<i:r:S:::.a.... .. s __ __S�}:ase.
-41
0
ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Angie Overcash
PROJECTID
5120379
LABORATORY REPORT NUMBER
216011906
DATE
01 /25/2016
Primary Data Rev' w By
Robyn Migues/Director Data Del
Authorized Signature
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 216011906 Page 1 of 11:
Pages of 42

.:�,,.,:e f ..
r_�•s_.�e=�_.—�.��.' - <oti.;,::3 _—_.=}�u_ii_�v�-.> �r.<<,-t<,'c _� _
zi'�tc:-���.._��'za4'-=:zti_tir� � -. h�:_?'-�._3+.a.3,.a.,-;:�..-�rraav..si'_tv_`:�__�ti�-�,:�>-sst'.��ti�_s7
_ __`: ���ns�rt= __ram-.r�:;�
MA
NELAP CERTIFICATE NUMBER:
01955
'
DOD FLAP CERTIFICATE NUMBER:
L14-243
isNk�.TE'YtC.d'L LAifi IVAfaRfErs: LLC
ANALYTICAL RESULTS
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70820
Report Date 01/25/2016
GCAL Report mo216I031906
11111111111111111111111111111111111111111111111111111
Project 5120379
Deliver To Additional Recipients
Angie Overcash NONE
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
1S.0
17025..
tl� OHS
DOD EIAP
Lab Report#: 216011906
Pa e2of11

>S_>�LL_gi�ini=::4:v;�e�44h:�:ti�.� ,. 3:T� ?.�•.i4s`a'e..G'`e=:'wi�4a'ei•=i.�'i :.
AH�CA�07W
Report#: 216011906
Project ID: 5120379
Laboratory Endorsement
Report Date: 01/25/2016
Sample analysis was performed in accordance with approved methodologies. provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCA12s Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit .
DL Diluted analysis — when appended to Client Sample ID
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or 1 Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Robyn MgueslDlredor Data Del
Authorized Signature
GCAL Report 216011906
Lab Report#: 216011906 Page 3 of 11
Page 27 of 42

- 4'e'. i� ti• � __ __ _ _ = - � ' _ e..4 - :mil-" _ •� - t. i � - _ - _. - _
;_'3,�.,..,�ti'>_z,>.>..,-___a?i::..:i.:z
Report#: 216011906
40 GCALANAL4 PCA'L LIUOp AfOB1E5; LhC Project ID: 5120379 Report Date: 01/25/2016
I
y
Certifications
10/02/2015
Certification
Certification Number
DOD ELAP
L14-243
Alabama
01955
Arkansas
12-060-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
USDA Soil Permit
P330-10-00117
Lab Report#: 216011906 Pa e 4 of 11
Page28 of.:42:

_ ___ ____ ___ ____ _SLS'6v •TS `:?ate: ti-;__ _ _ __ _____ _____ _:.��. p:>pq z_ _ _______ _ „ems:
a�{a:_se_2:s:� :.. �:''�--a?:re>4.�cesS._i Eici._.e_r. �. _k 6 �p_"x'.-ssr�stia..'n�to=_:z3�•s' ]Gx] .: §i-.:=:>..-_4tic�. _��4:ss'C-hti.}zb'�?::�� e. \��x �
�� Report#: 216011906
�
aNnirnenL [eeonaTo— Hies: i�c Project ID: 5120379
Case Narrative
Client: Access Analytical Report: 216011906
Report Date: 01/25/2016
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found in the analyzed sample(s).
Lab Report#:216011906 Pacte 5 of 11
'. Ps9e:,29 of:42

A's - - -
�.a9 - __ _
� - c< 3- :. n .. Y ..___ _ _anxc`-�d`e<ani�e:S::•.•.
�_+�� "'.i:�'-c-.a
��
Aa cA dPATo— Ries.ILc
Report#:
Project ID:
216011906
5120379
Report Date: 01/25/2016
FC
GCAL ID
21601190601
Sample Summary
Client ID Matrix Collect Date/Time
STA LIME Solid 12/21/2015 08:30
Receive Date/Time
01/19/2016 09:50
Lab Report#: 216011906 Paae 6 of 11
P�ageg30 of 42 :":

•'�Z.a_ � � :4"i-=:'.`-_ - �a 4S'=mac :Se'"e _-� �k �: yti?a4'`�>e.S':?�etie :`: a - `.'bY S. _ o> �- � 5".4cz6^e� _
Report#: 216011906
Al
AKALYfICAL LpbtiAATOPIES. LLC Project ID: 5120379 Report Date: 01/25/2016
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.

Report#: 216011906
Project ID: 5120379 Report Date: 01/25/2016
ANALYTICAL LAEORA70RIE5. LLd
ti
Sample Results
:36 91 q91 I PPQO 1
TA L I M
�
ve,
Rec Dat Q O e 01119120 9,50.-*.*. el. MatriX.. Solid,
EPA 9012B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
01/19/2016 10:15 577207 EPA 7.3.3.2 1 01/1912016 16:18 RXJ- 577292
CAS#
57-12-5R
EPA 9034
Parameter Result DL LOQ Units
Reactivity Cyanide 25OU 250 250 mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
01/19/2016 10:05 677208 EPA 7.3.4.2 1 01/19/2016 14:15 RXJ 577263
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result DL LOQ Units
25OU 250 250 mg/kg
Lab ReporlIP 216011906
Paqe8o 11
PfA

Report#: 216011906
AOTICAL LAUORATMF!�. LCc p roj ect ID: 5120379 Report Date: 01/25/2016
General Chemistry QC Summary
'Analytical Batch
MB57720 8
L'CS5T7,2;0. 8
G ALIb
3
"1536644
'.
SaTpIe`jype
�B
LbS
571268
Prep qie
,
61/161201610�
01119/20116,10:0
Prep Method
'EPA
�n lysis Date
1
01119/2016. 4;15
0119/ 5::.
7.3.4.2
M al ax,
S611d;*
solid
q
4
mg/kg g-Spi§
�-Rii[�R
*
;:.Control.: ntrp):EPk
j
Result
DL
Added]
Limits/oR
ORes
Reactivity Sulfide
I 18496-25-8R
1 250U
1 2501
10001
114611151
47-120 1
*
Batch'.:..���.
�",�,: :�-lletIDTR#20950
*`Ahaloical
.7
1530319DOPt.,-
977263
8
0401
Prep Batch
Sample
LE
.166645
DUP
677208..-.:--
PrepDate.
01/19/2016 1*0.:05,�`
fOl/1912016
Prep Method
Analysis YS
dJilW61614-16
.1*0-.05
oi/f9/201614:15
EPA7.3:4.2
matrix
Solid'
Solid
EP A 4
U(IltS
'Og/kg
.::
I Re
DLI
Limit
1Reactivity Sulfide
18496-26-8R
1 01
2501
01
0
1 25 1
Analytical BatcW�-
HQ ;Client
..
MB577207
. .
LCS5�7207
w- ;.;
57729��
GCAL ID.
.
1-530640�
Prep p BatchMB
LCS
577207:�-
Prep Date
01/1912016-10:15�.5.
01/1912016,10.
P Method:.-,t--,-*.
An'al�sis Date
01/19;201616:64
M
9/2016 4
EPA 7.3.3.2
:'h x
Mat
'Solid S 0
Solid
Units
Md'*
ft
:.Splkp
f :
Result
iControl.E
�ql2
—
Result-
DLA
LmitSXR
Reactivity Cyanide
57-12-5R
I 25OU
2501
2501
49.5.1201
1
Lab Report#. 216011906 Page 9 of 11
Page 53,&,42

c
'C
C
A. e SM Full -Service Analytical &
tnvironment6l Solutions
ABOMTORIMINC:
certi&Ation: NEL USACEL
Prism. xc�—, Sq-- Other.
5420379 N/A
SENDING LABORATORY.:: REcFrvwG*LAB0RATORY.,
Prism Labbratories, Inc.
:Wf C444*4§11) AP9.
P.:O- Box 240545 7979 G RI vemie-
Charlptle; NC 28224:-0543 70.820
Phonc: 300=529T(5364
Fax: [phone] Fiix.'(225) 767=5,717
.Project lvfan4gcrs Robbi A. Jones
Analysis Due gxpires LhIlDratpry-)P. Conunents
Sample.111): 5170370-DI Solid Sqru le i2j.;i1! s P866
kcactij.,nly, Sulfidd (S*ijb)
Rcac&ity, Cyanidc.($U 01/04/14,68:30
eoulainers Supplied: WJ.
of 1

I
Ai
Revision M o 2:
CD
Lab Report#: 216011906 Page 11 of 11
0

.___;_..,,.__k�-__x=:-.��:9 .. �..__.. z__ __z=�=:2,.cti�=:i:::=a .. sz _ _4.:.iii;.i4'eii•=:: :-�: _=.�3 .. F:____3�««2::�...:::t__�c�`_=:� _. se:.
s
% ii�l, f fEai ,. [N .
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
5120379
LABORATORY REPORT NUMBER
1601D19
Primary Data Review By
Chantelle Kanhai
Project Manager, AES
DATE
January 26, 2016
Secondary Data Review By
Ashley Airsick
Project Manager, Access Analytical
[e-mail]
i
c
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed atAnalytical Environmental Services Inc. (AES Inc
3080 Presidential Drive, Atlanta, GA30340.
- AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 1 of 7
P;,age.,36 of,42;'.

l� M
6S
Full -Service Analytical &
I S ' I Environmental Solutions
64 Im. ov vee�
17=c
�LAEOnAT0n1ES,�YR
/1,0100
SUBCONTRACT ORDER
j Certification: LAC_ USACE
Prism Laboratories, Inc. NC SC_ Other
5120379 N/A
SENDING LABORATORY: RECEIVING LABORATORY:
Prism Laboratories, Inc. Analytical Environmental Services, Inc.
P. O. Box 240543 3080 Presidential Parkway
Charlotte, NC 28224-0543 Atlanta, GA 30340
Phone: [phone] Plione :[phone]
Fax: [phone] Fax: NA
Project Manager: RobbiA. Jones
Analysis Due E>Ires Laboratory ID Comments
Sample ID: 5120379-01 Solid Satnp)eti:12/21/15 08:30 - ' • y, - jj
herbicides TCLP (Sub) 12/28/15 08:30
Containers Supplied:
eiised By Date Received By Date
Irl
Released By Date Received By Date
Released By Date Received By" Date
Page37 of=42

:................... .. .................................... ...
l..:z:��+,.�-� -.... � .. � _ < � <`;z '�-' s=? :�a.._7:�:� ..- E-_.s � '' __=3iti�ossg �a-�:''s'. _•
Analytical Environmental Services, Inc
' cy
li
Date: 26-Jan-16
E
Prism Laboratories
5120379 Case Narrative
1601D19
Herbicides Analysis by Method SW1311/8151A:
Sample 1601D19-001 was received and analyzed outside EPA/Method specified holding time of 14 days. Per instructions from
the client (Robbi Jones) on the Chain of Custody, we proceeded with analysis.
Page 3 of 7

Analytical Environmental Services, Inc
Date: 26-7an-16
Client:
Prism Laboratories
Client Sample ID:
StaLime
Lab Order
1601D19
Tag Number:
5120379-01
Project Name:
5120379
Collection Date:
12/21/2015 8:30:00 AM
Lab lD:
1601D19-001A
Matrix:
Solid
Analyses Result Reporting
y Qual MDL Limit Units BatchID DF DatcAnalyzed Analyst
HERBICIDES, TCLP SW-1311/8151A (SW3510C)
2,4,5-TP (Silvex) BRL H 0.017 0.20 mfi/L 218782 1 01/25/2016 15:36 AW
2,4-D BRL H 0.031 0.20 mg/L 218782 1 01/25/201615:36 AW
Surr: DCAA 87.2 H 0 50.1-148 %REC 218782 1 01/25/2016 15:36 AW
11
Qualifiers: • Value exceeds maximum contaminant level E Estimated value above quantitation range f -
BRL Not Detected at WL S Spike Recovery outside limits due to matrix Ei
H Holdingtimes for preparation or analysis exceeded > F'
P eP� YS Greater than Result value
N Analyte not NELAC certified 7 Estimated value detected below Reporting Limit
B Analyte detected in the associated method blank < Less than Result value i
_ Page 4 of T 'a
t�
Page: 39,771

-
_ ._t d
,.-.a .__ __-_t3-»�.ai.: .., z_. _Se�_::,_.2���_:-.aii =i ti7 .. �-:: �-�i_ _3_x.._-a�,.,..t`1-0 x•'.�,.
-
�< <vs;se i fc___._'-___
FQ-,
i
Analytical Environmental Services, Inc.
Sarnple/Cooler Receipt Checklist
Client '14eew ��✓ %� Work Order 1lrumber WD,
Checklist completed by
Signature U Date
/
Carrier name, FcdEx J UPS Courier Client US Mail Other
Shipping container/cooler in good condition? Yes ✓ No Not Present
Custody seals intact on shipping container/cooler? Yes _ No _ Not Present ✓
Custody seals intact on sample bottles? Yes ` / No _ Not Present
Container/Temp Blank temperature in compliance? (0°_<6°C)* Yes ✓ No _
Cooler #1 ' Cooler #2 Cooler #3 Cooler #4 Cooler#5 Cooler 96
Chain of custody present?
Yes f
No
Chain of custody signed when relinquished and received?
Yes V/`
No _
Chain of custody agrees with sample labels?
Yes
No
Samples In propercontainerlbottle?
Yes f/
No _
Sample containers intact?
Yes J
NO _
Sufficient sample volume for indicated test?
Yes
No
All samples received within holding time?
Yes —
No
_I /
Was TAT marked on the COC?
Yes
No "
Proceed with.Standard TAT as per project history?
Yes
No
Water - VOA vials have zero headspace? No VOA vials submitted ✓/
Yes
Water - pH acceptable up on receipt?
Yes _
No _
Adjusted?
Sample Condition, Good v1- Ofher(Explain)
(For diffusive samples or AIHA lead) Is a known blank included?
See Case Narrative for resolution of the Non -Conformance.
Checked by
Not Applicable
. 1\10
Not Applicable "
Yes — No %./
Samples do not have to comply with the given range for certain parameters.
\\Aes server\1\Sample Receiptlh4y Documents\COCs and pH Adjustment SlteeMample Cooler Recipt Checklist Revl.rtf
Page 5 of 7

Analytical Environmental Services, Inc Date: 26-Jan-16 rj
Client: Prism Laboratories
Project Name: 5120379 rDates Report l:
Lab Order: 1601 D19
ry
Lab Sample ID Client Sample ID Collection Date Matrix Test Name TCLP Date Prep Date Analysis Date ^
1601D19-001A StaLime 12/21/2015 8:30:OOAM Solid HERBICIDES, TCLP Leached 01120/2D16 1/22/2016 12:42:29PM 01/25/2016
n:
70
;•r,
�f
1:.
4u
M.
Ili
o; Page 6 of 7
i;.
r - rr.•,o•rrr • — . -rrrrrKrr

Analytical Environmental Services, Inc
Client:
Prism Laboratories
Project Name:
5120379
Workorder:
1601D19
Date: 26-Jan-16
ANALYTICAL QC SUMMARY REPORT
BatehID: 218782
Sample ID: MB-218782
Client ID:
Units: mg/L
Prep Date: O1122/2016
Run No: 308972
SampleType: MBLK
TestCode: HERBICIDES, TCLP SW131L8151A
BatchID: 218782
Analysis Date: O1/25/2016
Seq No: 6632273
Analyte
Result RPT Limit SPK value SPK Ref Val
n/oREC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL
2,4-D BRL
Sun: DCAA 0.3763
Aj
0.20
0.20
0 0.5000 75.3 50.1 148
Sample ID: LCS-218782
Client ID:
Units: mg/L
Prep Date: 01/2212016
Run No: 308972
SampleType: LCS
TestCode:
HER131CIDEs, TCLP
SW131118151A
BatchID: 218782
Analysis Date: 01/2512016
Seq No: 6632275
I+Y
f.
Analyte
Result
RPT Limit
SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val a/oRPD
RPD Limit Qual
'- 2,4,5-TP (Silvex)
0,3756
0.20
0.5000
75.1 52.5
126
E
2,4-D
0.4086
0.20
0.5000
81.7 50.5
132
Surr: DCAA
0.4416
0
0.5000
88.3 50.1
149
Sample ID: 1601D19-001AMS
Client ID:
StaLime
Units: mg/L
Prep Date: O1/2212016
Run No: 308972
SampleType: MS
TestCode:
HERBICIDES, TCLP
SW131118151A
BatchID: 218782
Analysis Date: O1/25/2016
Seq No: 6633320
r;
Analyte
Result
RPT Limit
SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val 0/,RPD
RPD Limit Qual
2,4,5-TP (Silvex) 0.4065
2,4-D 0.4080
Surr: DCAA 0.4292
0.20 0.5000
0.20 0.5000
0 0.5000
81.3 49.4 131
81.6 44.1 137
85.8 50.1 148
N z
Qualifiers: > Greater than Result value
< Less than Result value
B Analyte detected in the associated method blank _ 1
(O
fD -
BRL Below reporting limit
E Estimated (value above quantitation range)
H Holding times for preparation or analysis exceeded
NJ
Estimated value detected below Reporting Limit
N Analyte notNELAC certified
R RPD outside limits due to matrix page 7 of 7 i^
Rpt Lim Reporting Limit
S Spike Recovery outside limits due to matrix^
1
N
,

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0006245 Laboratory: 1) Prism Labs
Facility Name: Fourth Creek WWTP
Residual Source WQ # or NPDES # NCO031836
NPDES #:
WWTP Name:
Recidnal Annivcic Data
Parameter
(mg/kg)1/12/15
Ceiling
Conc.
Limit
Sample or Composite Date
4/6/15
8/3/15
12/21/15
t
Percent Solids (%)
NA
73.70%
69%
95%
95%
Arsenic
75
7.9
6.1
5.8
5.2
Cadmium
85
<0.34
<1.8
<2.6
0.28
Copper
4,300
30
32
23
24
Chromium
NA
N/A
N/A
N/A
N/A
Lead
840
14
15
12
29
Mercury
57
0.12
0.13
0.13
0.077
Molybdenum
75
N/A
N/A
N/A
N/A
Nickel
420
160
200
110
120
Selenium
100
<0.67
<3.6
' <5.3
<5.4
Zinc
7,500
62
71
51
56
Total Phosphorus
NA
2,300
2,000
*
1,500
* -
Lab did
not
sample
TKN
NA
2,300
3,300
1,700
1,400
Ammonia -Nitrogen.
NA
140
180
13
52
Nitrate and Nitrite
NA
13
10
14
11
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to •ass e t at qualified per onnel properly gathered and evaluated the information submitted. I am aware that there are significant
pen e f sub ' in�g a information, including the possibility of fines and ' prison ent for knowing violations."
(Y
Signature f Preparer * Date
5
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)