WQ0006245_Regional Office Historical File Pre 2018 (10)

A FILE.
A
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory Donald van der Vaart
Governor Secretary
May 5, 2015
Mr. Andy Smith, Fourth Creek WWTP Supervisor
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Subject: Acknowledgement of Receipt of the 2014 Annual Report
City of Statesville N-Viro Processing Facility and Sta-Lime
Distribution Program - Permit No.: W00006245
Distribution of Residuals (503)
Iredell County
Dear Mr. Smith:
The Mooresville Regional Office (MRO) received and reviewed the 2014 Annual Report for the
above permit. The report reflects distribution was conducted from January through December
2014. Data submitted appears to reflect compliance with the permit requirements through 10-09-
2014; however, the alkaline stabilization records submitted are incomplete after this date. Please
submit the remaining alkaline stabilization records through December 315t, 2014 to me at
the email address below.
I may be reached by phone at [phone] or email (maria.schutte(cDmcdenr.gov) should you
have questions. _
Sincerely, $$
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
CC: Mr. L.F. Hudson, Director of Water Resources, Town of Statesville (email)
Ed Hardee, LAU Compliance, CO -Raleigh (email)
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28115
Phone: [phone] Fax: [phone] Customer Service:1-877-623-6748
Internet: www.ncdenr,gov
An Equal Opportunity i Affirmative Action Employer — Made in part by recycled paper

V. (P.'Bnx 1111 ® Statestlille, Nort4 &rolina 28687
February 12, 2015
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Reports for 2014
Alkaline Stabilization (WQ0006245)
Dear Mr. Hardee:
Dlvisior't a3F ✓f, _ 'w —r?!.AL1TY
MAR 2 2015
MGOET.... n 'l
Enclosed, you will find 1 original and 2 copies of the required forms and lab data for the Alkaline
Stabilization program. Permit # WQ0006245.
This'permit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
Sii er
I
i
Andy Si ith
WWTP Supervisor, Fourth Creek WWTP

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2014 REC-EVED
PERMIT NO. WQ0006245 Dwss9cr1 o - kAiA E ER QUALITY
MAR 2 2015
FACILITY NAME: Fourth Creek WWTP NPDES NC00M36
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box I 1 l l
Statesville, NC 28687-1 1 11
[phone]
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
RESIDUALS ORC:
L.F. "Joe"' Hudson Jr., Director
Water Resources
P.O. Box 1111.
Statesville, NC 28687-4111
[phone]
Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data avid Summary Operatiimis
Attached

FACILITY NAME:
CLASS A ANNUAL. DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Fourth Creek Alkaline Stabilization
Iredell OPERATOR: Ray Wyrick
Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) PEA, ;_.! ;-D
DP°JF onFti t SF t 1rt I ��ti:'1+
J±r� Distribution and Marketing (complete. Parts A, B, and C)
War thu far•ility in A eratinn AlTrino the pact ralPnrlar vPar9 VP-4 PI No i ..1 —fi If No skin parts A. B. C and certify form below
WQ PERMIT #: WQ0006245
PHONE: [phone]
COUNTY:
FACILITY TYPE (please check one):
Part A':
Part B*: IVIM A
Month
Sources(s) (include NPDES # if
Volume (dry tons)
Recipient Information r_; ;
Amendment/
Bulking AAgentapplicable)
Residual In
Product Out
Name(s)
Z`
Volume (dry tons)
`,-'`- 3v' ` s r- ° nzrz -,lt
Intended use(s�
January
4th Creek WWTP
4
60
64
Various Fanners
65
Farmland
February
NPDES# N0003.1836
5
90
95
Various Fanners
227
Personal & Faml
March
4th Creek WWTP
11
101
112
Various Fanners
1.53
Farmland
April
NPDES# NC0031836
16
140
156
Various Fatmers
406
Farmland
Mav
4th Creek W)AITP
?0
175
195
Various Farmers
67
Turf
,tune
NPDES# NCO031836
0
0
0
Various Fariners
1.19
FarinfGarden.
July
4th Creek WWTP
4
65
69
Various Farmers
113
Fannland
August
NPDES# N000318 36
4
70
74
Various Farmers
0
Farmland
September
4th Creek WWTP
8
90
98
Various Farmers
124
Landscaping
October
NPDES# NCO031816
23
350
373
Various Farmers
92
Farmland
November
4th Creek WWTP
3
65
68
Various Falrmers
211
Farmland
December
NPDES# NCO031836
10
120
130
Various Fanners
79
Farnlavd
Total from FORM DMSDF (sup)
0
0
0
0
Totals:
Annual (dry tons):
108
1326
1434
1656
Amendment(s) used:
Bulking Agent(s) used: Lime Kiln Dust
If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C::
total Number of Form DMSDF (Stipp)1
Facility was compliant during the past calendar year with all conditions of the land application permit F Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: s. l No 0 If No, Explain in Narritive
1. All numitoring was done in accordance with the pernut and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or. in the case of a deviation. prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and impril4nnioit for knowing v!�lations."
SiLmature. of Permittee. Date
%; �`Preparer is defined in 40 CFR Part 503.9(0 and 15A NCAC. 2T .1102 (26)
r
Signature f Preparer" Date
(if differ nt from Petinittee)
015
M; 4 t
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORNI RSSF - 13
WQ Permit Number: WQ0006245
Facility Name:
Residual Source WQ # or
NPDES #:
W WTP Name:
�?nririn�l ®s��lvcic ��e4a
Fourth Creek WWTP
NPDES # NCO031836
Laboratory: 1) Prism Labs
2)
3)
4) Flr 711 IF-n
S) DIViSIQI`d QUALITY
i,r1AR 2 2015
Parameter
Cone.
Limit
Sample or Composite Date
1/13/14
5/5/14
7/14/14
12/15/14
r� 00R,FE=
_V:i'_LE (.-i
0f\lAL el=
Percent Solids (%)
NA
70.80%
83%0
56%
67%
Arsenic
75
5.2
5
6.5
<0.053
Cadmium.
85
<0.0033
<0.0029
<0.042
0.57
Copper
4.300
29
23
310
26
Cluroini um
NA
N/A
N/A
N/A
N/A
Lead
840
8.2
6.2
1.00
12
Mercury
57
0.17
0.24
0.38
0.18
Molybdenum
75
N/A
N/A
N/A
N/A
Nickel
420
11.()
89
630
10
Selenium
100
<0.084
2.1
<1.1
<0.090
Zinc
7,500
57
41
66
4.5
Total Phosphorus
NA
2,000
2,200
3,100
2,100
TKN
NA
3.300
2,200
5,200
3,600
Ammonia -Nitrogen
NA
47
14
150
92
Nitrate and Nitrite
NA
8.3
34
54
11
I=or surface disposal facilities the ceiling concentration linuts listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
4ase that qualified p rsonne.l properly gathered. and evaluated the information submitted. I am aware ghat there are significant
, f r sub ><tti�i alse information, including the possibility of fines and imprisonment for knowing violations."
�)f Preparer Date
tD
710E
°Preparer is defined in 40 CFR Part 503.9(r) and 1.5A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization WQ Permit Number: WQ0006245
WWTP Name: Fourth Creek WWTP
Monitoring Period: From 1/1/2014
NPDES Number: NCO031836
To 12/31 /2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time; temp) r` .
Alt B (Alk Treatment) _�
Alt. C (Prior Testing)
A1t.D (No Prior Test)
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A onh) indicate "Process to Further Reduce Pathogens":
Compost '
Heat Di-yitic, :.
Heat Treatment
Thennophilic _-_
Beta Ray
Gamma Ray =
Pasteurization �`
.
Class P:
jAlt. (1) Fecal Density i ..
Alt. (2) Process to Sigmificantly Reduce Pathogens iL_
rea�JlieJie o alaeiiti�C1r_i__ e' Class n VIi-•. • ld1CatC T_ jt CSl iirltgl i1 filc [._l.lt-n ilLC nitiV�ll lll 1\ i eiis".
Lime Stabilization -,1
Air Drying "
Composting : '
Aerobic Digestion
Anaerobic Digestion 0
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
umer of
Excee-
dences
Frequency
of Analysis
Sample
Type
Ana ytica
Tech-
ni h-
gue
Minimutr
an ean
Me
Maximun
Units
Fecal Coliform
2 x 10 to the
6th power
per ;ram of
total solids
MPN
<0.2
<1
mpn/g
60 days
grab
sm9221e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 NIPN per 4 grams
total solid (dry
weight)
<0.076
n7pll/4g
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) 1
Alt. 2 (40-day bench) -..i.
Alt.. 3 (30-day bench) .. !
Alt_ 4 (Spec. O, uptake) E-1
Alt. 5 (14-Day Aerobic) !x
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable)
Alt_ 8 (Drying - Unstable) ....
Alt. 9 (Injection)
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the'appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
tha the pathogen and vector attraction reduction requirements have been met. I am aware that there are
siUNIficant penalties for false certification including fine and imprisonment."
and Tit)e (Vpe or print)
Land Applier Name and Title (if applicable)(type or print)
iignature(of Preparers` Date Signature of Land Applier (if applicable) Date
'Preparer is delined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26)
DENR FORM PVRF 02T (12/2006)

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFPP)
BIN # R
Setup Date: /-a7-14
Removal From Bin Date: /-30-1y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Q
Initial PH: j,2 5 3
07
Corrected PH:U,7.3
y,
Final PH: / i. C
L Ij
Corrected PH:
Has 72 Hour & PH Criteria Been Met? O�) N
BIN # L
Setup Date: ;-dj i4
Removal From Bin Date: 3-3'-144
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1'ri`(�
Initial PH: ?Iwl ES'
Corrected PH: 1,W, 5 7
_
Final PH: /,�, 7 ./
Corrected PH: Ia.17 -7
Has 72 Hour & PH Criteria Been Met? OYN
BIN #1: LY
Setup Date:
Removal From Bin Date: 5
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
2 ") !`(
t ( ti �fl
Initial PH:
Corrected PH: 13. !
3 lt(
�.
( f „7
Final PH: r
Corrected PH: t 3, f
Has 72 Hour & PH Criteria Been Met? Y N 3 - )1i-W
BIN #
Setup Date: 3 -10 - /L-(
Removal From Bin Date:
_ Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
j ',r(;`l ' (`1
i �? ire
Initial PH: ; ;�, je
(y
,
1\
�
Corrected PH: ..3, 1
3.•. y.t �/
6 y� e�
Final PH:
Corrected PH: 1 j
Has 72 Hour & PH Criteria Been Met? Y N
BIN # �j-
Setup Date:
Removal From Bin Date: 3 ;� 7-/ 4
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3 l �1
1 3 S r',
7
initial Pn: ? ,
`� a
v
Corrected PH: II . `3 (
' iLi
-� n
P °'
Final PH: l,j , 97
q o
Corrected PH: 13 : {
Has 72 Hour & PH Criteria Been Met? N

Cite Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # i
Setup Date: 3 5 • i`I
Removal From Bin Date:3 -J 3'-/q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 0,7
q o
R�
Corrected PH: /�sf'I
Final PH: 1) , 7 `j
Corrected PH:
Has 72 Hour & PH Criteria Been Yet? N
BIN #
Setup Date: `I - 7- 14
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1� . %e
'i
Corrected PH: Q . 4.
Final PH: M. 35
��,
�� VV
Corrected PH: 13.
Has 72 Hour & PH Criteria Been Met? N
BIN #
Setup Date: Lf - 1y - I14
Removal From Bin Date: 11 •- I `•I •- 1 �i
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
A
Initial PH: 1,4,
Corrected PH: /�. � a�
qS-
Final PH: 112.ly
C 0
Corrected PH: J �, i
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:., ig
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Cj 0
Corrected PH: 1,2,1
Final PH: /,j, �
Corrected PH:
Has 72 Hour & PH Criteria Been Met? fjY N
BIM #
Setup Date: e-1-,)$- I'r
Removal From Bin Date: 5"--
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1•°30 P,q
Initial PH: /,,, 5'.3
�f
Corrected PH: 13.
1y
�S ���
Final PH: /J.1?d
30
Corrected PH: / 3.1
Has 72 Hour & PH Criteria Been Met? i( N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date:
Removal From Bin Date: 3-- / -/q
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
e!
1/: 3; ;
Initial PH:
�
Corrected PH:
A
Final PH: /,� , Lf.3
.�
Corrected PH: 1,2,e
Has 72 Hour & PH Criteria Been Met? CO N
BIN #
Setup Date: 4-30- 1 y
Removal From Bin Date:.- 3 •� y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
y-�a Jul
A'�i�Pr�
Initial PH:
Corrected PH: Q,C3
"J 4 1 y
7 ' y''"'
Final PH: 1,�. 5,:3
Corrected PH: 0,7 3
Has 72 Hour & PH Criteria Been Met? Us N
BIN #/
Setup Date: J - / - 1 y
Removal From Bin Date: 5,
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
s i.l-/`✓
l P,j
Initial PH: 1 ,2,5 6
o
R4 uv
Corrected PH: 1 1,17 S
Final PH: /a. G
J.
D
Rk�
Corrected PH: /,2. �
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 3
Setup Date: `i .. r3 •_ l4i
Removal From Bin Date: 5 •- &- J y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
S-13 1 `i
1 �.��
Initial PH: ! $
Corrected PH: T
a
Final PH: 1a2.7b'
, s�
�
Corrected PH: Jd A
Has 72 Hour & PH Criteria Been filet? Y N
BIN # q
Setup Date:.j- J,j -JLj
Removal From Bin Date: 5-- 1'7-1y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
9 b °
A,4V,l
Correcteu PY:
S J9-ly
A'"n
Final PH: /a , R
o
Corrected PH: 13,0
Has 72 Hour & PH Criteria Been Met? UY N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFPP)
BIN # s
Setup Date: S. /5'_ jai
Removal From Bin Date: .- /,A'- /y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5 s� I
to qd,�
Initial PH:
Corrected PH: f 3,
Final PH: J, . q y
�
Corrected PH:
Has 72 Hour & PH Criteria Been Met? 1( N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
'PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
initial pun:
Corrected PH;
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been stet? Y N

City Of Statesvi lie Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFPP)
BIN # 3
Setup Date: (- /,�- It/
Removal From Bin Date: �-11-/y
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 12. 7q
7
Corrected PH: Jvl q7
'I A
Final PH: J,a. T r7
Gy
Corrected PH: 13,
Has 72 Hour & PH Criteria Been Met? UY N
BIN # q
Setup Date: 1-I%-141
Removal From Bin Date: �-do-14
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: dd.7 1
Yo
Corrected PH:
^�4
d 6
Final PH: / �, �' p
R1, VV
Corrected PH: jj, 9 ,l
Has 72 Hour & PH Criteria Been Diet?, CY) N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: 7-/4-14
Removal From Bin Date: `7- 11- lq
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs. I
Operator
-B5 /W
rlr�
Initial PH: /,R.-Y$
o
(30,
����
Corrected PH: /,7,
®.t
Final PH: 1W.59
0.�
�J��V
Corrected PH: ®�,%'�
Has 72 Hour & PH Criteria Been Met? (Y) N
BIN # �
Setup Date: L
p �- I I 1 �
Removal From Bin Date: lit- I Lf
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
• !I / �/
f (' `' T
Initial PH: /a.52
n �
7
R� Gil
Corrected PH: id, 7
f; 3`7 ('°*�
Final PH:
IJ
2� w
Corrected PH: 14, S.-I
Has 72 Hour & PH Criteria Been Met? Y N
BIN # r7
Setup Date: S- i,i - i y
Removal From Bin Date: $-
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
.,y
1�;59P^i
Initial PH: /�.�C7
70o
RjcAJ
Corrected PH: 0. $?
1 ' 33 P
Final PH: . tE1: ,7 ..
<<
d'� �w
Corrected PH: I�.`�
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: e-,25-- iy''
Removal From Bin Date: - T- I
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
!�
Initial PH: 1). ,j `1
vV
Corrected PH: Id, 7
Final PH: f ),1-7
£.
Corrected PH: 1
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
. PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
.. _
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesviiie Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: ?-to - Iti
Removal From Bin D ; :-
®
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For
Aerator
lien
Initial PH: !, S
�`J
�[ vv'
Corrected PH:i,?,73
-ta I5
j`l'!.�•,'�
Final PH: (-�, e.a
�2j� �`•
Corrected PH:/j, J'_)
Has 72 Hour & PH Criteria Been Met? N
BIN # Y
Setup Date: q-11- 14
Removal From Bin Date: L? -d S -jq
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:I,;Z, E3
6,� o
AU Vv
Corrected PH: /,7 .7a
�" 17 OL®
Final PH:
13
�� w
[Corrected PH:
Has 72 Hour & PH Criteria Been Met? N
BIN
Setup Date: I- 1 ! q
Removal From Bin Date: 1- 4- 14
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Q
^
Initial PH: !�, `7
7 �
�'�
Corrected PH:1.,?, 35"
_ d a! y
➢` `iS Piyl
Final PH: j j JT5
Corrected PH: E 3. J
Has 72 Hour & PH Criteria Been Met? ':jY) N
BIN #
Setup Date: I - ff, III
Removal From Bin Date: 9 -- :a -1 i
Date
Time
I PH >12.0 For 72 Hrs.
TEMP. >52 Deg.'C For 12 Hrs.
Operator
I '3-1 y
0 3
Initial PH:U, 517
��
k'� t l
Corrected PH: ? .'�']
A
Final PH: %j, E'
Corrected PH: /,) J...j
e
Has 72 Hour & PH Criteria Been Met? YN
BIN #
Setup Date: t?- 3;7- /q
Removal From Bin Date: Jr}-3, jq
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�- j�--/�/
d•1 /'11
initial PH: 1), 7- j
r3
r
Corrected PH:
A
„"
Final PH: 11,
Corrected PH: 13_
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (P .FRP)
BIN # 3
Setup Date: / 0 - t - l y
Removal From Bin Date: 10 -
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3'�'"
Initial PH: t_),
J `J
,� �u
Corrected PH: I Z
da ' `l' iq
r'm
Final PH: jj. q0
Corrected PH: /3, p
Has 72 Hour & PH Criteria Been diet? � N
BIN ## '-/
Setup Date: /0 -1 3-• I y
Removal From Bin Date: /0 - / `%- dq
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
fd -r3 I6l
I 3�t P�
Initial PH: /a. 5q
o
. --�
_Corrected-P-H j:�q'-7- -�-
Final PH:
_
f
Corrected PH:
-_---_H.as_7.2_H_o-ur..&-PH-Criteria been diet? Y N
BIN ##
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria BeenMet? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been filet? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PPH:Corrected
PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been filet? Y N

lt`� Ci t.ate5llille �?.l;kaline..S$ss i i%a$IC n..i.,cor. � UC
Process: To Further B>? Cat.3C athog.ens: (PrRP). .
BIN :# 3
Setup Date::
Removal- From Bin Da e:
Date
Time.
PH >12.0 For.72 'Hrs.
TE MP. >5'2 Deb. C r c•r =? - =: :- _-ator
/-
�4l
30 :.
Initial PH. 7(D
o
Corrected PH:
1
I/ 3j)I lM
Final PH:..': .
0
Corrected PH:
Has 72 Hour c PH Cnt eria: Been •Met? Y N
BIN # 7 .
Setup Date:
Removal'Fro.m Sin Date:
S~
Date
Time
PH >12.0 For.72 Hrs:
TEMP. >52 deg: C For 12 l:;�. 5��rator
Initial PH:. f
G o 74
l (�
Corrected PH:
I
Final PH: j` :ZiO:
{ L 4:J
Corrected PH:
:Has: 72 Hour & PH Criteria Been Met?: Y N
B1N # 1:
Setup,Date:
RemoVal From. -Bin Date:
Date
. Time`
PH >12.0 For 72 Hrs.::
TEMP. >52 De : C For 12 -rs. ., pera orl
I r�'
ip Do�M
Initial PH: 3
4
Corrected PH:: ( ,
oP,r^
Final PH;
_
q
Corrected PH:1J:3::
�. .
Has 72 Hour.& PH..Criteria Been Met?. Y: N
BIN.
'Setup Date:
Removal From Bin ate: ,
Date
Time PH >12.0 For 7.2; Hrs.
q TEMP. >52 Dea. C.For 12 S. --
-
Initi.a:f PH:
'Co -r=coed PH:
:':Final PH.:
CerrFec PH:
Has 72 H:our &:PH Criteria
Been Met. Y N..
BIN: :
Da:4::.
hemo.ai From Sin C�cte: ..
Date
Time H >12.D.For 7Z Hrs.
-CMP :»2 Deg: C F:
Has 72: Hour &=.PH Criteria
Been Met. Y N

NC Certification No.402
SC Certification No. 9909012 Case Narrative
P I
Full -Service Analytical & NC Drinking Water Cert No. 37735 01/20/2014
S M Environmental Solutions VA Certification No. 460211
�DoD ELAP: L-A-B Accredited Certificate No. L2307 '.,�....,.....__._.. , ". LABORATORIES, INC.
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 01/13/2014
Statesville, NC 28687 Prism Work Order: 4010154
This data package contains the analytical results fur the project identified above and indudes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Samples were received on wet ice at a temperature 9.2 degrees C; however, samples were collected and
submitted to the laboratory within one hour of sample collection time.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 1471

f�Full -Service Analytical
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Tom-'..... IARORPTORIES ING
Sample Receipt Summary
01 /20/2014
Prism Work Order: 4010154
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Sta'Lime
4010154-01
Solid
01/13/14
01/13/14
Sta-Lime (Fecal #2)
4010154-02
Solid
01/13/14
01/13/14
Sta-Lime (Fecal #3)
4010154-03
Solid
01/13/14
01/13/14
Sta-Lime (Fecal #4)
4010154-04
Solid
01/13/14
01/13/14
Sta-Lime (Fecal #5)
4010154-05
Solid
01/13/14
01/13/14
Sta-Lime (Fecal #6)
4010154-06
Soiid
ui/ 13114
01/13/14
Sta-Lime (Fecal #7)
4010154-07
Solid
01/13/14
01/13/14
Samples were received at 9.2 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 14

/ ^ , I FWLService Analytical
r- Environmental Solutions
,f=.. .^.. LA 00PAT 1--
Laboratory Report
01 /20/2014
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Sta-Lime
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4010154-01
P.O. Box 1111
Prism Work Order: 4010154
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Plant Availabie Nitrogen
720
mg/kg
160
13
2 *Calculation 1/20114 9:52
CLB
lICALCI
Solids
70.8
% by
0.100
0.100
1 *SM2540 G 1/15/14 16:02
JAB
P4A0199
Weight
Nitrate/Nitrite as N
8.3
mg/kg dry
7.1
0.78
1 *SM4500-NO3 F 1/16/14 12:52
CLB
P4A0208
Phosphorus -Total
2000
mg/kg dry
71
10
20 *SM4500-P F 1117/14 10:08
JAB
P4A0162
Total Kjeldahl Nitrogen
3300
mg/kg dry
710
59
2 *351.2 1120/14 9:52
CLB
P4A0259
Ammonia as N
47
mg/kg
5.0
0.48
1 *SM4500-NH3 G 1114/14 10:37
CLB
P4A0140
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 1/13/14 13:08
MES
P4A0156
Total Metals
Mercury
0.17
mg/kg dry
0.028
0.0094
1 *7471B 1117/14 16:19
MEH
P4A0221
Arsenic
5.2
mg/kg dry
0.35
0.051
1 *6010C 1115/14 0:34
BGM
P4A0151
Cadmium
BRL
mg/kg dry
0.35
0.0033
1 *6010C 1/15/14 0:34
BGM
P4A0151
Copper
29
mg/kg dry
0.69
0.0087
1 *6010C 1/15/14 0:34
BGM
P4A0151
Lead
8.2
mg/kg dry
0.35
0.041
1 *6010C 1/15/14 0:34
BGM
P4A0151
Nickel
110
mg/kg dry
1.4
0.011
1 *6010C 1115/14 0:34
BGM
P4A0151
Potassium
4700
mg/kg dry
350
22
20 *6010C 1/17/14 17:36
BGM
P4A0151
Selenium
BRL
mg/kg dry
0.69
0.084
1 *6010C 1/15/14 0:34
BGM
P4A0151
Sodium
590
mg/kg dry
17
0.16
1 *6010C 1115/14 0:34
BGM
P4A0151
Zinc
57
mg/kg dry
3.5
0.024
1 *6010C 1115/14 0:34
BGM
P4A0151
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 0f 4

.l, Full -Service Analytical 8
M I Environmental Solutions
LABORA —Es —
Laboratory Report
01 /20/2014
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Sta-Lime (Fecal #2)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4010154-02
P.O. Box 1111 Prism Work Order: 4010154
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
o Soiids 65.5 % by 6.166 0.100 1 °SM2540 6 1115114 16:02 JAB P4AG,i99
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 1/1.3114 13:08 MES P4A0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone],409 Page 4 of 14

Laboratory Report
PRISM Full -Service Analytical 01/20/2014
Environmental Solutionss
0' "B ATORIES ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Sta-Lime (Fecal #3)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4010154-03
P.O. Box 1111 Prism Work Order: 4010154
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
..oII..� .... by.I vvv V.1VV i `S,02540G i/i5/i4 16:02 .iAE; +A0. 9,
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 `SM9221 E 1/13/14 13:08 MES P4A0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 Of 14

Laboratory Report
R I S � ,yl Full -Service Analytical 3
1 �' Environmental Solutions 01I20/2014
__.. LABORATORIES ING
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, . Client Sample ID: Sta-Lime (Fecal #4)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4010154-04
P.O. Box 1111 Prism Work Order: 4010154
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
^/ Solids 69.3 by 10(! 0..00 . 5-42540 .., ,1 5,14 16:02
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 1/13/14 13:08 MES P4A0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 14

Laboratory Report
Full -PRISM I Service Analytical &
environmental Solutions
01/20/2014
...„_...,...,... . LABORATORIES INC.
City of Statesville, NC
Project: Sta Lime (Qtrly, BiWeekly,
Client Sample ID: Sta-Lime (Fecal #5)
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4010154-05
P.O. Box 1111
Prism Work Order: 4010154
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter Result
Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids 68.2
% by n_100 n_100
1 •SM25e0 r_ 1!15/14 15•02 iea P4A0199
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry 0.3
1 SM9221 E 1/13114 13:08 MES P4A0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 14

Laboratory Report
J/P R I S Full -Service Analytical 8
Environmental Solutions 01/20/2014
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Sta-Lime (Fecal #6)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4010154-06
P.O. Box 1111 Prism Work Order: 4010154
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
,o ,v.i io by GAGO GAGG 1 'SIV12540 V Ui5%14 16:02 JAi3 -4A 01.
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 - 1 SM9221 E 1113/14 13:08 MES P4A0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 14

Laboratory Report
Full -Service Analytical &
Environmental Solutions
,..., ... LABORATORIES, INO
01/20/2014
City of Statesville, NC
Project: StaLime (Qtrly, Biweekly,
Client Sample ID: . Sta-Lime (Fecal #7)
Attn: Andy Smith'
60Day 7 Fecal)
Prism Sample ID: 4010154-07
P.O. Box 1111
Prism Work Order: 4010154
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/13/14 10:23
Time Submitted: 01/13/14 11:35
Parameter Result
Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids 75.1
"/ by
0.100 nano
1 *cpe2510 r_ 1/1c/1e le:02 jAS P4A0199
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 1/13114 13:08 MES P4A0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 14

P R I S„ ,y Full -Service Analytical 8
� ' � I Environmental Solutions
.. I-A-RATORIE$ INC.
Level II QC Report
1 /20/14
City of Statesville, NC
Project: Stal-ime (Qtrly, Biweekly, 60Day
Prism Work Order: 4010154
Attn: Andy Smith
7 Fecal)
Time Submitted: 1/13/2014 11:35:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result
%REC
Limits RPD Limit Notes
Batch 1P4A0151 - 3050B
Blank (P4A0151-BLK1)
Prepared & Analyzed: 01/14/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
13
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
13
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4AO151-BS1)
Prepared & Analyzed: 01/14/14
Arsenic
22.6
0.25
mg/kg wet
24.75
91
80-120
Cadmium
21.6
0.25
mg/kg wet
24.75
87
80-120
Copper
23.2
0.50
mg/kg wet
24.75
94
80-120
Lead
21.4
0.25
mg/kg wet
24.75
87
80-120
Nickel
22.0
0.99
mg/kg wet
24.75
89
80-120
Potassium
445
12
mg/kg wet
495.0
90
80-120
Selenium
22.5
0.50
mg/kg wet
24.75
91
80-120
Sodium
446
12
mg/kg wet
495.0
90
80-120
Zinc
22.1
2.5
mg/kg wet
24.75
89
80-120
Batch P4A0221 - 7471 B
Blank (P4A0221-BLK1) Prepared: 01/16/14 Analyzed: 01/17/14
Mercury BRL 0.021 mg/kg wet
LCS (P4A0221-BS1) Prepared: 01/16/14 Analyzed: 01/17/14
Mercury 0.489 0.020 mg/kg wet 0.4167 117 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 14

t I Full -Service Analytical &
Environmental Solutions
-..,,„ GApORATORIES. ING.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (Qtrly, Biweekly, 60Day
7 Fecal)
Level II QC Report
1 /20/14
Prism Work Order: 4010154
Time Submitted: 1/13/2014 11:35:OOAM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P4AO140 - NO PREP
Blank (P4A0140-BLKI)
Prepared & Analyzed: 01/14/14
Ammonia as N
BRL
5.0
mg/kg
LCS (P4AO140-BS1)
Prepared & Analyzed: 01/14/14
Ammonia as N
123
5.0
mg/kg
125.0 98 80-120
Batch P4AO162 - SM4500-PB5
Blank (P4A0162-BLK1)
Prepared: 01/14/14 Analyzed: 01/17/14
Phosphorus -Total
BRL
2.5
mg/kg wet
LCS (P4A0162-BS1)
Prepared: 01/14/14 Analyzed: 01/17/14
Phosphorus -Total
101
2.5
mg/kg wet
100.0 101 90-110
Batch P4AO199 - NO PREP
Blank (P4AO199-BLKI)
Prepared & Analyzed: 01/15/14
% Solids
100
0.100
% by Weight
Batch P4AO208 - NO PREP
Blank (P4A0208-BLK1)
Prepared & Analyzed: 01/16/14
Nitrate/Nitrite as N
BRL
5.0
mg/kg wet
LCS (M0208-113SI)
Prepared & Analyzed: 01/16/14
Nitrate/Nitrite as N
48.8
5.0
mg/kg wet
50.00 98 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 14

Full -Service Analytical &
Level UQCReport
1/20/14
City ofStatesville, NC Project: StaLkno(Qtrly.BNVooNy.0oDay Prism Work Order: 401O154
Attn: Andy Smith 7F000|) Time Submitted: 1/13/2O14 11:35:O08M
P.O. Box1111
Statesville, NC 28687
General Chemistry Parameters ' Quality Control
Reporting snm° Source %nEo Rpo
^" ** Result Limit unit" Level Result mnEo umm` mpo Limit Notes
Blank (p4pO259-aLKo_- __ __ _ _prepamu:ox,7'/14^na-1-yzeu:n1/zm_1_4__� _
Total qemomNitrogen a*L 25 momo°et
Lcs Prepared: 'V1/1T/14—Analyzed: 01/20/14��__
Total xjemamNitrogen mc mo momowm 500.0 102 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
*movn"ubro":Road - P ' 0. Bo"e40sm cx°n"x° woxozm-0sm

Level II QC Report
y
Full -Service Analytical &
1/20/14
-Fj Environmental Solutions
j" LA90RATORIES INC.
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 4010154
Attn: Andy Smith
7 Fecal)
Time Submitted: 1/13/2014 11:35:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result
Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4A0156 - NO PREP
Blank (P4A0156-BLK1)
Prepared & Analyzed: 01/13/14
Fecal Coliforms
BRL
0.2 IVPN1g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch
Initial
Final Daterrime
4010154-01 P4A0259
0.05 g
25 mL 01/17/14 12:45
Prep Method: SM4500-PS5
Lab Number Batch
Initial
Final Daterrime
4010154-01 P4A0162 1 g 50 mL 01/14/14 15:45
Prep Method: 3050E
Lab Number Batch Initial Final Daterrime
4010154-01
P4A0151
2.04 g
50 mL
01/14/14 11:15
4010154-01
P4A0151
2.04 g
50 mL
01/14/14.11:15
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
4010154-01
P4A0221
0.61 g
50 mL
01/16/14 14:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 Of 14

R
� f '; �fwr=ull-Se:vice. A.nalyticai &CHAIN F USTOY RECORD
n E`:>i Environmental Solutions M "� 6. I PAGIE _ OF QUOTE t1 TO ENSURE PROPER WILLING:
t.naona.Ton"rs. "roc.
449 Springbrof l( Road P.O. Cox 240543 ,, Gharloite, NC 28224-0543 Project Name:
Phone: [phone] Fax: 704/525-O409 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: C ;4 y S a r.• s ✓, `��' "Please ATTACH any project specific reporting (OC LEVEL I H Ill) M
— provisions and/or OC Requirements
Report To/Contact Name: A r v
Invoice To:
Reporting Address: R 01" 0Il tl tl Address:
NC
G`
! �'
YEy NO N/A
Samples INTACT --Ipon arrival? •
_-
Received ON WE-i ICE? Temp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
r
CUSTODY SEALS INTACT?
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
Phone: 12 `7- . J U - 44 3 1 Fax es (No): 10'S' �7 `� 6'CDZi, Purchase Order No./grilling Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC
EDD Type: PDF— Excel _Other Rush Work Must Be
"Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ Pre -Approved StI OTHER N/A
Site Location Name: Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 623 %3 rz11 FA r 1?. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO—
.dJ(` (SEE REVERSE FOR TERMS 4+ CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT —
ANALYSES REQUESTED
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE
CONTAINER
RRESERVA-
TIVES
�'"
�Kk' REMARKS
'TYPE
SEE BELOW
NO.
SIZE
.� -
_, ,
Tms-
- 4
/�
cl
,
i
14 r
----- /✓vim / _ __
IN
Sampler's Signature' zz ' Sampled By (Print Name) !/c + Affiliation P
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin'shed By: (Signature)
�) Receive By nature)^ -, Da /� -Military/Hours Additional Comments:
�f LLCG�vt?^ mil. fl L/G .P-2cCi>�� �j / 7 �C j
Reli s ed By: (Si?nature)/ J Received By: (Signature) Date
inquisFtetr By: (Signature) Received F61 Prism Laboratory B.yp Dale / 1
((D hod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT yTH CUSTODY SEALS FOR TRANSPORTA I I N TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINS -COC UNTIL RECEIVED AT THE LABORATORY.
O
ad Ex El UPS ElHand-deliveredrrism Field Service U Other~`
DES: UST: GROUNDWATER: DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
VC ❑ SC ❑ NC ❑ SC El NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC i ❑ NC ❑ SC
❑._. ❑—__ _ ❑_ ❑_ ❑ . ❑ ❑ I ❑
"CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
PRISM
LAB
ID NO.
6-
Site Arrival Time:. Site Departure Time:
Field Tech Fee:
Mileage:

NC Certification No. 402 ���� Narrative
Certification No. 99012
M � I Full -Service Analytical & NC Drinkinq Water Cert No. 37735 02/03/2014
� Environmental Solutions VA Certification No. 460211
taeonaroaies, INC.DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 01/27/2014
Statesville, NC 28687 Prism Work Order: 4010396
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash For Robbi A. Jones
VP Laboratory Services
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 6

PR I S Full Service Analytical Environmental Solutions
,,,. LAaOnATONIES ING
Sample Receipt Summary
02/03/2014
Prism Work Order: 4010396
Client Sample ID Lab Sample ID Matrix Date Sampled . Date Received
Sta-Lime
4010396-01 Solid 01/24/14 01/27/14
Samples were received in good condition at 3.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 6

Laboratory Report
Full -Service Analytical
&
I Environmental Solutions
,�-_,�.� _ ._-0-ORIES. INc.
02/03/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4010396-01
P.O. Box 1111
Prism Work Order: 4010396
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/24/14 12:08
Time Submitted: 01/27/14 13:35
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
70.E
% by
0.100
0.100
1 *SM2540 r__ 1129114 14:30
JAB
P4A0450
Weight
Total Metals
Mercury
0.14
mg/kg dry
6.030
0.010
1 *7471B 1/29/14 14:37
MEH
P4A0433
Arsenic
6.5
mglkg dry
0.35
0.051
1 *6010C 1130/14 22:06
BGM
P4A0429
Cadmium
BRL
mg/kg dry
0.35
0.0033
1 *6010C 1/31114 18:20
BGM
P4A0429
Copper
27
mg/kg dry
0.70
0.0088
1 *6010C 1/30114 22:06
BGM
P4A0429
Lead
6.4
mg/kg dry
0.35
0.041
1 *6010C 1/30114 22:06
BGM
P4A0429
Nickel
99
mg/kg dry
1.4
0.011
1 *6010C 1/30114 22:06
BGM
P4A0429
Selenium
BRL
mg/kg dry
0.70
0.085
1 *6010C 1/31/14 18:20
BGM
P4A0429
Zinc
44
mg/kg dry
3:5
0.024
1 *6010C 1/30114 22:06
BGM
P4A0429
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543-7-Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Of 6

j 1 P I S Full -Service Analytical 8
`� Environmental Solutions
LADOFATOFIEB, INC.
Level II QC Report
2/3/14
City of Statesville, NC Project: StaLime Prism Work Order: 4010396
Attn: Andy Smith Time Submitted: 1/27/2014 1:35:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4A0429 - 3050B
Blank (P4A0429-BLK1)
Prepared: 01/28/14 Analyzed: 01/30/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4A0429-BS1)
Prepared_ 01/28/14 Analyzed: 01/30/14
Arsenic
20.3
0.25
mg/kgmg/kg wet
25.13 81 80-120
Cadmium
22.2
0.25
mg/kg wet
25.13 88 80-120
Copper
22.2
0.50
mg/kg wet
25.13 89 80-120
Lead
20.1
0.25
mg/kg wet
25.13 80 80-120
Nickel
20.2
1.0
mg/kg wet
25.13 81 80-120
Selenium
21.5
0.50
mg/kg wet
25.13 86 80-120
Zinc
20.7
2.5
mg/kg wet
25.13 83 80-120
Batch P4A0433 - 7471 B
Blank (P4A0433-BLK1) Prepared: 01/28/14 Analyzed: 01/29/14
Mercury BRL 0.020 mg/kg wet
LCS (P4A0433-BS1) Prepared: 01/28/14 Analyzed: 01/29/14
Mercury 0.462 0.020 mg/kg wet 0.4167 111 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 6

r
ISFull-Service Analytical Environmental Solutions
IAAOPATOPIES, INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
2/3/14
Prism Work Order: 4010396
Time Submitted: 1/27/2014 1:35:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4AO450 - NO PREP
Blank (P4A0450-BLK1) Prepared & Analyzed: 01/29/14
% Solids 100 0.100 % by Weight
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
4010396-01
P4A0429
2.04 g
50 mL
01/28/14 10:00
4010396-01
P4A0429
2.04 g
50 mL
01/28/14 10:00
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date rime
4010396-01 P4A0433 0.57 g
50 mL 01/28/14 12:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001526-6364 - Fax: [phone] Page 5 Of 6

........... ...... .... .. - 7 .. ........ ..... .. ........... ... ........ .
P-HIIIANKM flT CRORTGBY RECORD ,0.1 M_
•
P
I M
Full -Service Analytical &
Solutions
NIA
(D
0
Environmenial
PAGE OF QUOTE 70 ENSURE PROPER MULLING:
Sai CTupon arrival?
Samples INTACT
CD
UNDURA70RIEs INC.
mnip
Received ON WET ICE? TL
x 240543 - Charloft,��, NC 28224-0543
449 Springbrook Road P,O. Bo,
Fax; 704/625-0409
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes)
PROPER PRESERVATIVES indicated?
(1)
Phone: [phone]
C 4V SYWe": He
*Please ATTACH any project specific reporting (QC LEVEL I II III I
Received WITHIN HOLDING TIMES?
eo�
a_
Client Company Name. 0-F 14
;4J, 3"'41,
provisions and/or QC Requirements
CUSTODY SEALS INTACT?
VOLATILES W/OUT HEADSPAC E?
Report To/Contact Name:
Invoice To:
rec'd
.
ReportinP. g Address: ox. PI j j
PROPER CONTAINERS used?
_ZL
/V(2
Address:
Phone: 7v q- 67' - � 599 Pax Ye (No):70LF1e-1Ti6S
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date 0 1 Day C] 2 Days 0 3 Days 0 4 Days (15 Days
Certification: NELAC—USACE—FL—
NC
EDD Type: PDF_ Excel —Other
Site Location Name: F;jr-I 411 i.oL4.TP
"Working Days" 0 6-9 Days El Standard 10 days Cl Rush Work Must Be
Pre -Approved
Samples received after 15:00 will be processed next business day.
Sc OTHER
N/A
Site Location Physical Address: 03 Se-0
kends d h liday I
Turnaround time is based on business days, excluding weekends an
Water Chlorinated: YES NO
45t,'Ila-
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERV CE
RENDERED BY PRISM LABORATORIES, INC. TO CLIEN1)
j;P L
Sample Iced Upon Collection: YES
NO
_1YIN
%
.
'k,"ANALYSES
REQUESTED
TIME
MATRIX
SAMPLE
CONTAINER
PRISM
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
(SOIL,
WATER OR
PRESERVA-
TIVES
REMARKS
LAB
ID NO.
*TYPE
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
A�_
C k
AW, 0
7%
It
e
.... ... ...
'T e�� ZZ Sampled By Zkr",..
Sampler's Signature Print Name)
Affiliation
Upon relinquishing, this Crr.in of Cu'stody is your authorization for Prism to proceed with the anal as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Reelinhed By: (Signature) Hece by: �,Signat rg
Date Military/Hours
Additional Comments: Site Arrival Tirne:
elf,
F�,Iin�h'�y. �(;,�nalu�,,�� RedeiveI!rBy: (Signature)
Dale
Site Departure Time:
Field Tech Fee:
Rei,nclishy: dB (�J ature) Receded For Pri Laboratories By:
Date
iMileage.
c�
4
E: L SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSP9,FITATION TO THE LABORATORY.
MWhod of SilipMebt: 0, E.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST 30C UNTIL VECEIVED AT THE LAB�,�ATORY.
Goc; Group No.'
0Fed Ex QUIPS Q Hand -delivered ZI Prism Field Service Q Other
NPDES: I UST: GROUNDWATER: DRINKINGWATER: SOLID WASTE: 1 RCRA: CERCLA LANDIOILL OTHER:
0 NC. NC :1 SC C SC
C) NC 0 SC� 0 NC C] SC -0 NC El SC SC Cl N Q 0 NC U SC. :],NC Q SC ONC OSC
"CONTAINER TYPE CODES: A = Amber C - Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 9402
90 Case Narrative
SC Certification No. 99012 Narrative
Full -Service Analytical & NC Drinkinq Water Cert No. 37735 02/07/2014
Environmental Solutions VA Certification No. 460211
"RI M 6 LABORATORIES, INC.DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 02/03/2014
Statesville, NC 28687 Prism Work Order: 4020025
MIS Uald JGIKCJC Contains the CllaIytical results rv.. ",ha project °,dent,fed above and i„n,dudes a C83e Narrative, S-le
..I.-.--
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 6

Full -Service Analytical &
I Environmental SolutionsL B-ATO ES. INC
Sample Receipt Summary
02/07/2014
Prism Work Order: 4020025
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
4020025-01 Solid 02/03/14 02/03/14
Samples were received in good condition at 1.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 6

Laboratory Report
�� Full -Service Analytical &
,// Environmental Solutions 02/07/2014
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4020025-01
P.O. Box 1111 Prism Work Order: 4020025
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/03/14 12:40
Time Submitted: 02/03/14 14:45
Parameter Result Units' Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
o�. Sc!;ds 71.7 1/ by 1 *SM2.5d0 G 2/5/14 15:10 JAB P4B0063
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 214/14 12:33 MES P4B0061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 6

f PRISM I Full -Service Analytical �s'
L Environmental Solutions
t.. 1__ LAOOA l—ES INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
2/7/14
Prism Work Order: 4020025
Time Submitted: 2/3/2014 2:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4B0063 - NO PREP
Blank (P4B0063-BLK1) - Prepared & Analyzed: 02/05/14
% Solids 100 0.100 /o by Weight
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 6

Ad Full -Service Analytical &
y�Jp P R ISM I Environmental Solutions
/�„':..,:: —OnATORIES. INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
2/7/14
Prism Work Order: 4020025
Time Submitted: 2/3/2014 2:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4B0061 - NO PREP
Blank (P4B0061-BLK1) Prepared & Analyzed: 02/04/14
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 6

.
P i" '� j Ftlil-Servlr:e Analytical A CHAPham
�., EnVivortmCntal Sciutions PAGE _ or
�44D®u E it V® ENSURE PROPER P,CLr..o CJPn:
..'...: LABORATORIeS, INC.
:9 Sprsngbrook Road ° P.0, Box 240543 - Chiriotte, NC 23224 0543 Project Name:
Phone: [phone] Far.: 704/525-0409 Short Gold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name. - %'� �+ o j'a45 P.,
+ "Please ATTACH any project specific reporting (QC LEVEL 111 Ili M
provisions and/or QC Requirements
To/Contact Name: �t+' S,�+, �''✓S
Invoice To:
Repotting Address: P ��. fox 61 4 Address:
J � /de
YES NO
N/A
Samples INTACT upon arrival? (+ 7
_�
_ O
Received ON WET ICE? Tem 2
p -i-,X—
-- --
CD
—
PROPER PRESERVATIVES indicated?
_l
a)
a
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
Phone: Jag-V 9-- :3LI3 `6 Fax es (No): 11i �' ��- b 6�;� Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC_
EDD Type: PDF_ Excel _Other Working Days" ❑ 6-9 Days ❑ Standard 10 days p Rush Work Must Be
e _ Pre -Approved SC OTHER N/A
Site Location Name: r'o +� �� c,,-.e k &L' °L _I_ — Samples received after 15:00 will be processed next business day.
Si?e Location Physical Address: Z VY 8 t' I fR4 Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO _
/ (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES SSam le Iced Upon Collection: YES NO
34114C.5yl ✓'Y <'_ C RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ID p TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE TIVES /' uS' ,.-' REMARKS ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE /. % .r�
Sampler's Signature Gi> eZ'2tt% Sampled By (Print Name) 11A L IP 1 4' k Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin ished By: (Signature) Receaved By: (Si Date Military/Hours
/E �vpa2•>TYlt'C �t• Gi•�ii.2-C i ' � 1 'it,?Fr�. .y: l�P!
Rel' ished By: (Signature) Received By: (Sicj' aMre) _ Date
Relin,�luished By: (Sig ture) Rec iv For Prism Lab , ries By: Date g,j;,,
1411 ` r
Methbd of Shipment: NOTE: A L SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SF, S FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACC TED AND VERIFIED AGAINST CO UNTIL RECEIy D AT THE LABORATORY. _
t! eI,C�C�LS
❑ Fed Ex ❑ UPS ❑ Hand -delivered El - Field Service ❑ Other
DRNN
W: SOLID WAS: R
❑ NC ❑ SC p INC ❑ SC I ❑❑ NC N❑ SCTEIi. ❑O NICKI❑ SC ATER ❑❑ NC ❑ SCTE— C2 NC 'p SC ❑] N C LO SC 0❑ NC LANDFILL❑SC 0 INC ❑ SC
❑ —❑ —
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Comments:
Site Arrival Time:
Site.Departure Time:
Field Tech Fee:
Mileage.-
--

NC Certification No. 9402
90 Case Narrative
e�w i� SC Certification No. 99012 �.o �!f
�' 11 , Full -Service Analytical & NC Drinkinq Water Cert No. 37735
11�51 Environmental Solutions VA Certification No. 460211 02/18/2014
7; LABORATORIES, inc. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 02/10/2014
Statesville, NC 28687 .Prism Work Order: 4020186
da,La c.,a c �v ntt"ain.�a the analyticui resu is for the pr v�en+f idonFi{ied ehnie wnrwl i„cl�des e (ve�c n����et:�: �, C�mple
a pa �,y.. �.�y.
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 Of 7

Full -Service Analytical &
R
Environmental Solutions
S
0.M
Sample Receipt Summary
02/18/2014
Prism Work Order: 4020186
Client Sample ID Lab Sample ID Matrix . Date Sampled Date Received
Sta-Lime
4020186-01 Solid 02/10/14 02/10/14
Samples were received in good condition at 1.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364- Fax: [phone] L Page 2 of 7

,,,""PRISM
Full -Service Analytical& Laboratory Report
PI S Environmental Solutions 02/18/2014
LAeOnATORIES INO. ,
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4020186-01
P.O. Box 1111 Prism Work Order: 4020186
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/10/14 10:35
Time Submitted: 02/10/14 14:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
^/_ Cnlirlc 77 7 % by n Ann n ann i *SM254n G 2!12!1n 12•15 ino P4B@204
._ .. Weight ......,. ,......, ....._..,.. � _.._... ._..., .,,.�
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 2111/14 9:30 MES P4130214
Total Metals
Mercury
0.14
mg/kg dry
0.028
0.0093
1
*7471B
2/17/14 15:47
MEH
P4130244
Arsenic
7.5
mg/kg dry '
0.35
0.051
1
*6010C
2114114 19:16
BGM
P4130220
Cadmium
BRL
mg/kg dry
0.35
0.0033
1
*6010C
2114/14 19:16
BGM
P4B0220
Copper
33
mg/kg dry
0.70
0:0088
1
*6010C
2/14/14 19:16
BGM
P4B0220
Lead
8.4
mg/kg dry
0.35
0.041
1
*6010C
2114114 19:16
BGM
P4B0220
Nickel
130
mglkg dry
1.4
0.011
1
*6010C
2114/14 19:16
BGM
P4130220
Selenium
BRL
mg/kg dry
0.70
0.085
1
*6010C
2/14/14 19:16
BGM
P460220
Zinc
51
mglkg dry
3.5
0.024
1
*6010C
2114114 19:16
BGM
P4B0220
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

/ P R 0 I Full -Service Analytical
l' Environmental Solutions
LABORATORIES -
City of Statesville, NC . Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
2/18114
Prism Work Order: 4020186
Time Submitted: 2/10/2014 2:00:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4B0220 - 3050B
Blank (P4B0220-BLK1)
Prepared & Analyzed: 02/14/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4B0220-BS1)
Prepared & Analyzed: 02/14/14
Arsenic
23.1
0.25
mg/kg wet
25.25 91
80-120
Cadmium
22.4
0.25
mg/kg wet
25.25 89
80-120
Copper
24.4
0.51
mg/kg wet
25.25 97
80-120
Lead
22.6
0.25
mg/kg wet
25.25 g0
80-120
Nickel
22.7
1.0
mg/kg wet
25.25 90
80-120
Selenium
22.1
0.51
mg/kg wet
25.25 88
80-120
Zinc
22.8
2.5
mg/kg wet
25.25 90
80-120
Batch P4B0244 - 7471 B
Blank (11341130244-BLK1) Prepared & Analyzed: 02/17/14
- - -- --- --- -- -- - - ----- ------
Mercury BRL 0.018 mg/kg wet
LCS (P4B0244-BS1) Prepared & Analyzed: 02/17/14
Mercury 0.422 0.019 mg/kg wet 0.3968 106 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of %

/PRISM
Full-Service Analytical &
Environmental Solutions
pO41A--a INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
2/18/14
Prism Work Order: 4020186
Time Submitted: 2/10/2014 2:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4BO204 - NO PREP
Blank (P4B0204-BLK1) Prepared & Analyzed_: 02/12/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 7

Full -Service. Analytical &
/ Environmental Solutions
- U. eORnTORM
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch P4BO214 - NO PREP
Project: StaLime
Level II QC Report
2/18/14
Prism Work Order: 4020186
Time Submitted: 2/10/2014 2:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P4B0214-BLK1) Prepare_ d & Analyzed: 02/11/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Daterrime
4020186-01 P4B0220 1.98 g 50 mL 02/14/14 9:50
Prep Method: 7471B
Lab Number Batch Initial Final Daterrime
4020186-01 P460244 0.6 g 50 mL 02/17/14 9:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 7

p ` n�kl' MI Ilfll-ueIVIC@.Ar&lyClCstli CHARM OF ` U I� ODY fifcala '
Environmenl.al Solutions PAGE _ GG _ 0007E t14® ENSURE PROPER BILLING:
. "'. LABORATORIES. INC.
:119 Slaringl)eooI< Road < P.O. Box 240543 , Charlotte, NC 28224-054 i Project Name:
Phom: 704/529-6364 " Fax: [phone] / [ 6 Short Hold Analysis: (Yes) (No) UST Project: (lies) (No)
Client Company Name: C + o�'It JOY z r.s't sr �a4� -Please ATTACH any project specific reporting (i�C LEVEL I II 111 11�
Report To/Contact Name: r E provisions and/or OC Requirements
rr,� . J r+J r r GI
Invoice To:
Reporting Address. P.O, BOX 11 l l Address:
S f ,r-trr--S rr, Il r IBC°
7-41/- "�8 3°l3�' 701-g9�-92"7°-
YES �
NO NIP, I
Samples INTACT upon arrival? t. ( _-e 0
Received ON WET ICE? Temp �__—....___ ____ ti
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT? _
VOLATILES rec'd VV/OUT HEADSPACE?
^_
PROPER CONTAINERS used?" _
-._......_..
Phone. o Fat, es (No).— u �'J Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC
EDD Type: PD F_ E1u-cel —Other _ "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushPre-Work
roved dust Be SC OTHER N/A
Site Location Name: T, u r^+ , C,—e <. - GV' rr V I P Samples received after 15:00 will be processed next business day.
Site Location Physical ,address: T3 i. c! I Fo -,, l?' , Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES — NO
I e (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
'r RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED
CLIENT DATE COLLECTED (SOIL, PRESERVA- fey,,/ PRISM
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TYPE TIVES j »� �cr ; REMARKS ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE %; YV� �' y;;
H
r<
PA
Sampler's Signature -'2.0
Sampled By (Print Name) K
Affiliation
Upon relinquishing, this- hain o ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
'
Reli uished By: (Sign Lure) )
�
Received By: (aignalur,"
r
Dare
Military/Hours
I
Rel' a ed By: (Signature)
Re erd d By: (Signature)
Dale
—7
C ,Iv/61 l 1 )
Relinquished By: (Sign u
Received For Prism La oratories By:
Date
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT'W ITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
COC Group N
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST_COC UNTIL RECEIVED AT THE LABORATORY.
-
n'
D Fed Ex El UPS ❑ Hand -delivered 6ism Field Service ❑ Other
li
NPDES: UST: 1 GROI�DWATER: DRINKING WATER: ! SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC :1 NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC
❑ ❑ ❑ __ ❑ ❑ ❑ I ❑ .._. _. .... --- ❑ ❑
'CONTAINER TYPE CODES: A = Amber C =Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
al Comments:
Y:1041'�^S�W41
Site Arrival Time:
Site Departure Time:
Field Tech Fee:
Mileage:

NC Certification No. 402 ��Se Narrative
Certification No. 99012
fF{ S M � Full -Service Analytical & NC Drinking Water Cert No. 37735 03/03/2014
p I Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
LABORATORIES, INC.
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111' Lab Submittal Date: 02/24/2014
Statesville, NC 28687 Prism Work Order: 4020418
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
r
Reviewed By Terri W. Cole For Robbi A. Jones
Project Manager
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.., .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 8

P ISM n Full -Service Analytical
'� _ I V I Environmental Solutionss
.F - � LAeORAT 1-1Na
Sample Receipt Summary
03/03/2014
Prism Work Order: 4020418
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 4020418-01 Solid 02/24/14 02/24/14
Samples were received in good condition at 1.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529.6364 - Fax: [phone] Page 2 of 8

r] I %� Service Analytical Envi
`! r I V 0 Environmental Solutions
",--_ LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
03/03/2014
Project: StaLime Client Sample ID: Sta-Lime
Prism Sample ID: 4020418-01
Prism Work Order: 4020418
Sample Matrix: Solid Time Collected: 02/24/14 00:00
Time Submitted: 02/24/14 16:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
66.1
% by
0.100
0.100
1
*SM2540 G
2/27114 15:30
MJO
P41305U4
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
2/25/14 12:15
MES
P4130476
Total Metals
Mercury
0.11
mg/kg dry
0.032
0.011
1
*7471B
2/28/14 13:04
MEH
P4130513
Arsenic
5.9
mg/kg dry
0.38
0.056
1
*6010C
2126114 18:40
BGM
P4B0449
Cadmium
BRL
mg/kg dry
0.38
0.0036
1
*6010C
2/26114 18:40
BGM
P4B0449
Copper
33
mg/kg dry
0.76
0.0096
1
*6010C
2/26/14 18:40
BGM
P4130449
Lead
8.4
mg/kg dry
0.38
0.045
1
*6010C
2/26/14 18:40
BGM
P4130449
Nickel
120
mglkg dry
1.5
0.012
1
*6010C
2/26/14 18:40
BGM
1`4130449
Selenium
BRL
mg/kg dry -
0.76
0.092
1
*6010C
2/26/14 18:40
BGM
P4130449
Zinc
56
mg/kg dry
3.8
0.026
1
*6010C
2126/14 18:40
BGM
P41B0449
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 8

Full -Service Analytical &
� P R I Environmental Solutions
/:. -"?�. LA-ATOnIEr, INC..
Level II QC Report
3/3114
City of Statesville, NC Project: Stal-ime Prism Work Order: 4020418
Attn: Andy Smith Time Submitted: 2/24/2014 4:15:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4B0449 - 3050B
Blank (P4B0449-BLK1)
Prepared & Analyzed: 02/26/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.49
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4B0449-BSI)
Prepared & Analyzed: 02/26/14
Arsenic
23.1
0.25
mg/kg wet
25.25 91
80-120
Cadmium
22.4
0.25
mg/kg wet
25.25 89
80-120
Copper
24.7
0.51
mg/kg wet
25.25 98
80-120
Lead
22.7
0.25
mg/kg wet
25.25 90
80-120
Nickel
22.8
1.0
mg/kg wet
25.25 90
80-120
Selenium
22.2
0.51
mg/kg wet
25.25 88
80-120
Zinc
22.8
2.5
mglkg wet
25.25 90
80-120
Matrix Spike (P4BO449-MS1)
Source: 4020418-01
Prepared & Analyzed_ 02/26/14
Arsenic
34.2
0.38
mg/kg dry
38.20 5.85 74
75-125
MI
Cadmium
19.1
0.38
mg/kg dry
38.20 BRL 50
75-125
MI
Copper
65.8
0.76
mglkg dry
38.20 33.2 85
75-125
Lead
29.3
0.38
mg/kg dry
38.20 8.38 55
75-125
MI
Nickel
138
1.5
mg/kg dry
38.20 116 57
75-125
MI
Selenium
24.4
0.76
mg/kg dry
38.20 BRL 64
75-125
MI
Zinc
82.7
3.8
mg/kg dry
38.20 56.2 70
75-125
MI
Matrix Spike Dup (P4B0449-MSD1)
Source: 4020418-01
Prepared & Analyzed: 02/26/14
Arsenic
35.0
0.38
mg/kg dry
38.40 5.85 76
75-125
2
20
Cadmium
19.4
0.38
mg/kg dry
38.40 BRL 51
75-125
2
20 MI
Copper
63.8
0.77
mg/kg dry
38.40 33.2 80
75-125
3
20
Lead
29.8
0.38
mg/kg dry
38.40 8.38 56
75-125
2
20 MI
Nickel
138
1.5
mg/kg dry
38.40 116 58
75-125
0.3
20 MI
Selenium
24.5
0.77
mg/kg dry
38.40 BRL 64
75-125
0.4
20 MI
Zinc
85.0
3.8
mglkg dry
38.40 56.2 75
75-125
3
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 8

Level II QC Report
d j`Full-Service Analytical
3/3/14
EPRISMnvironmental Solutions
Aj , ......_. LABORATORIES. ING
City of Statesville, NC Project: Stal-ime Prism Work Order: 4020418
Attn: Andy Smith Time Submitted: 2/24/2014 4:15:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source
%REC
RPD
Analyte
Result
Limit Units
Level Result %REC
Limits RPD
Limit Notes
Batch P4BO449 - 3050B
Post Spike (P4B0449-PS1)
Source: 4020418-01
Prepared & Analyzed: 02/26/14
Arsenic
0.901
mg/L
1.D00 0.154 75
80-120
MI
Cadmium
0.507
mg/L
1.000-0:0158 52
80-120
MI
Copper
1.63
mg/L
1.000 0.872 76
80-120
MI
Lead
0.772
mg/L
1.000 0.220 55
80-120
MI
Nickel
3.48
mg/L
1.000 3.06 42
80-120
MI
Selenium
0.644
mg1L
1.000-0.0863 73
80-120
MI
Zinc
2.10
mg/L
1.000 1.48 62
80-120
MI
Batch P4B0513 - 7471 B
Blank (P4BO513-BLK1)
Prepared & Analyzed: 02/28/14
Mercury
BRL
0.020 mg/kg wet
LCS (P4B0513-BS1)
Prepared & Analyzed: 02/28/14
Mercury
0.437
0.020 mg/kg wet
0.4167 105
80-120
Matrix Spike (P4B0513-MS1)
Source: 4020418-01
Prepared & Analyzed: 02/28/14
Mercury
0.729
0.030 mg/kg dry
0.6200 0.114 99
80-120
Matrix Spike Dup (P4B0513-MSD1)
Source: 4020418-01
Prepared & Analyzed_ 02/28/14,
Mercury
0.805
0.031 mg/kg dry
0.6410 0.114 108
80-120 10
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 8

I S M I Full -Service Analytical &
Environmental Solutions
w...,.,,._..k LABORATORIES INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
3/3/14
Prism Work Order: 4020418
Time Submitted: 2/24/2014 4:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4130504 - NO PREP
Blank (P4B0504-BLK1) Prepared & Analyzed: 02/27/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 8

{/ n M
Full-Service Analytical &
Environmental Solutions
—ORFTOR.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
3/3/14
Prism Work Order: 4020418
Time Submitted: 2/24/2014 4:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P460476 - NO PREP
Blank (P4B0476-BLK1) Prepared & Analyzed: 02/25/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Date/Time
4020418-01 P460449 1.99 g 50 mL 02/26/14 9:00
Prep Method: 7471E
Lab Number Batch Initial Final Daterrime
4020418-01 P4B0513 0.57 g 50 mL 02/28/14 10:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 8

(,{ t it
`FgEJ CUSTODY"�..'+'Ok;7 RECORD
}ry
�e� T -�YN °A�rsu��'I,�`
-
) � Q, yIJ=ull-,S ervice Analytical 3
� Pi
Lzi r�ElJ
•�, �1
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YES rJ0 IJ/4 v-
O
� Sf h Environn-if SoiLrtions
PANE - OL-- m�UD�BE y P® sNsr� $e PR®frOta Ban Laen�:
Samples INTACT upon arrival?
-- _ -- --
v,eoRATcniea INC.
e •
Received ON WET ICE? Temp /
e0
�I-;9 ��ri¢t-brook Raad ^ P.O. Box 24t1543 � C!3arlotse, NC `L822�d-O:i43
q
Project Nacre:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
� _ ?
PROPER PRESERVATIVES indicated.
a
- to
Phone: [phone] Fax: [phone]
Received WITHIN HOLDING TIMES?
`b
Name: I" J•old 04� t ,¢�=- t : ��e
*Please ATTACH any project specific reporting (CC LEVEL I Ill III no
CUSTODY SEALS INTACT?
------ .----- -
Client Company
Repork To/Contact Name: i ° ;�" J<%o ��
provisions and/or QC Requirements
VOLATILES rec'd W/OUT HEADSPACE?"
_-,_--
_—
Reporting Address: )D +� • - ,: 18 U I
1nVOICe To:
Address:
PROPER CONTAINERS use
c p ' p"fw ,'•iL
Faxe)-4- Phone: YPurchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days y 6 Days Certification: NELAC USAGE FL NC_
EDD Type: PDF_ Excel _Other _ .Working Days" Cl 6-9 Days ❑ Standard 10 days p Rush Wbrk Must Be
Pre -Approved SC OTHER N/A
Site Location Name: Fo a ,r-4 �"I C4. ce. do t P t'', i i Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 42 B,' !f "� 3 `'` ' �Ai.. � Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO _
(SEE REVERSE RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TERMS & CONDITIONS REGARDING
Sample Iced Upon COII2C$IOn: YES NO
�g,af�s6 —
T9fVfE MATRIX SAMPLE REQUESTED
SAMPLE CONTAINER PRISM
CLIENT DATE COLLECTED_ (SOIL, PRESERVA- LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR `TYPE TIVES c� :` Sys REMARKS ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE
iD
Sampler's Signature Sampled By (Print Name) Praa 1.,u I Affiliation
Upon relinquishing, this Chain of _ ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relino fished By: (Signature) Receiv. By: (Signature) Da e•1� Military/Hours Additional Comments:
Relin shed By: (Signature) Red i By: (Signatu e) Date
Received rism Labor t ri B Date
Reim is ed By: (Signature) �%' ��°� Y�
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT VJHTI,,i•CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COD Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST�.,•pC UNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand-delivered`Prism Field Ser✓ice ❑ Other
NPDES: ! UST: G - OUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC ❑SC' ❑NC ❑SC: [jNC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC! ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

P R
I Full -Service Analytical &
S M � Environmental Solutions
s _ LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 03/10/2014
Prism Work Order: 4030172
Case Narrative
03/21 /2014
Thic rintn nnrkana rnntainc the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Terri W. Cole For Robbi A. Jones
Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 13

Laboratory Report
fID Full -Service
I
Analytical &
Environmental
-ORATORIES INC.
Solutions
'
03/21/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: StaLime and Fecal
#1
Attn: Andy Smith
Prism Sample ID: 4030172-01
P.O. Box 1111
Prism Work Order: 4030172
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
io by
Weight
�.iu0
v.ivv
i �J WILD- G 3i i4/i4 15:00 jAB
F-4CC20v
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E ' 3111/14 10:37 MES
P4CO223
Total Metals
Mercury
0.14
mg/kg dry
0.032
0.011
1 *7471B 3/14114 14:26 MEH
P4CO262
Arsenic
1.1
mg/kg dry
0.39
0.057
1 *6010C 3/21/14 13:41 BGM
P4CO229
Cadmium
BRL
mg/kg dry
0.39
0.0037
1 *6010C 3/21114 13:41 BGM
P4CO229
Copper
28
mg/kg dry
0.77
0.0097
1 *6010C 3118/14 23:38 BGM
P4CO229
Lead
14
mg/kg dry
0.39
0.045
1 *6010C 3121114 13:41 BGM
P4CO229
Nickel
130
mg/kg dry
1.5
0.013
1 *6010C 3/20114 17:45 BGM
P4CO229
Selenium
BRL
mglkg dry
0.77
0.094
1 *6010C 3121/14 13:41 BGM
P4CO229
Zinc
58
mg/kg dry
3.9
0.026
1 *6010C 3121/14 13:41 BGM
P4CO229
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13

i' "PRISM
P R I S M Fullir o meo Analytical s
V � Environmental Solutions
:i-TI INC.
Laboratory Report
03/21 /2014
City of Statesville, NC Project: StaLime Client Sample ID: Fecal #2
Attn: Andy Smith Prism Sample ID: 4030172-02
P.O. Box 1111 Prism Work Order: 4030172
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
...--.....-s ..-.... .G ..� ai. �vv 1 ..rN,c.i4v v .i/141 lY I.'.Gv .iru N..........
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 3111/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 3

lr Full -Service Analytical &
,"'P R I ogQTOfl'E Environmental Solutions
Laboratory Report
03/21 /2014
City of Statesville, NC Project: Stal-ime Client Sample ID: Fecal #3
Attn: Andy Smith Prism Sample ID: 4030172-03
P.O. Box 1111 Prism Work Order: 4030172
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
re Y O. 100 O.1OO '1 SM254O U 3/14N4 '15:60 JAB P4CO266
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 SM9221 E 3/11/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

PR I S Full -Service Analytical Environmental Solutions
,..... .........IE$ ING.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
03/2112014
Project: Stal-ime Client Sample ID: Fecal #4
Prism Sample ID: 4030172-04
Prism Work Order: 4030172
Sample Matrix: Solid Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 'SM9221 E 3/11/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 13

, P R I S Full -Service Analytical Environmental Solutions
A-...+._.� -011ATOn1EG ING
(Laboratory Report
03/21 /2014
City of Statesville, NC Project: Stal-ime Client Sample ID: Fecal #5
Attn: Andy Smith Prism Sample ID: 4030172-05
P.O. Box 1111 Prism Work Order: 4030172
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
/o —11— vll.J /o Uy U.-luu U.'I UU 1 "'JIYILJ4U %3 3/14/'14 'IJ:UU JH tS --u
Weight
Microbiological Parameters -
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 3/11/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 13

Full -Service Analytical 8 Laboratory Report
..R'SM Environmental Solutions 03/21/2014
-1A80RATORIE$ NC.
City of Statesville, NC Project: Stal-ime Client Sample ID: Fecal #6
Attn: Andy Smith Prism Sample ID: 4030172-06
P.O. Box 1111 Prism Work Order: 4030172
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
ofSol
ids 66.1. of o4r0285
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 3/11/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 13

`P R I S Full -Service Analytical Environmental Solutions
AveonarMIEC INC.
Laboratory Report
03/21 /2014
City of Statesville, NC Project: StaLime Client Sample ID: Fecal #7
Attn: Andy Smith Prism Sample ID: 4030172-07
P.O. Box 1111 Prism Work Order: 4030172
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/10/14 11:10
Time Submitted: 03/10/14 12:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
7o JUauS 00a /o uy U.'luu U.'luu '1 "JIYILJ4U L� J/'14114 'IJ:Uu JAb rwa,uco0
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 3/11/14 10:37 MES P4CO223
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook. Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 13

^ M
Level II QC Report
Full -Service Analytical &3/21/14
Environmental Solutions
LAOORATOR
City of Statesville, NC Project: Stal-ime Prism Work Order: 4030172
Attn: Andy Smith Time Submitted: 3/10/2014 12:45:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4CO229 - 3050B
Blank (P4CO229-BLK1)
Prepared: 03/12/14 Analyzed: 03/21/14
Arsenic
BRL
0.26
mg/kg wet
Cadmium
BRL
0.26
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.26
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.6
mg/kg wet
LCS (P4CO229-BS1)
.-..._ _----- --_.._..,. ..—
-..-. ... --
—--...__.._.
_..-
Prepared: 03/12/14 Analyzed: 03/21/14
._ __. - ...... .... .
Arsenic
23.5
0.25
mg/kg wet
24.88 95 80-120
Cadmium
23.6
0.25
mg/kg wet
24.88 95 80-120
Copper
24.7
0.50
mg/kg wet
24.88 99 80-120
Lead
23.9
0.25
mg/kg wet
24.88 96 80-120
Nickel
21.9
1.0
mg/kg wet
24.88 88 80-120
Selenium
22.6
0.50
mg/kg wet
24.88 91 80-120
Zinc
23.5
2.5
mg/kg wet
24.88 95 80-120
Batch P4CO262 - 7471 B
Blank (P4CO262-BLK1)
Prepared: 03/13/14 Analyzed: 03/14/14
Mercury
BRL
0.018
mg/kg wet
LCS (P4CO262-BSI)
Prepared: 03/13/14 Analyzed: 03/14/14
Mercury
0.462
0.021
mg/kg wet
0.4310 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 13

PR i S Full -Service Analytical Environmental Solutions
:s-... LA 0-OFIM INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
3121 /14
Prism Work Order: 4030172
Time Submitted: 3/10/2014 12:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4CO286 - NO PREP
Blank (P4CO286-BLK1) Prepared & Analyzed: 03/14/14
% Solids 100 0.100 % by Weight
Duplicate (P4CO286-DUP1) Source: 4030172-04 Prepared & Analyzed: 03/14/14
% Solids 66.3 0.100 % b Wei ht 66.5 0.3 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 13

e' �p FullService Analytical
I �' Environmental Solutions
-OnnTORIEG. INC. -
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
3/21 /14
Prism Work Order: 4030172
Time Submitted: 3/10/2014 12:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4CO223 - NO PREP
Blank (P4CO223-BLK1) Prepared & Analyzed: 03/11/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Date/Time
4030172-01
P4CO229
1.97 g
50 mL
03/12114 10:30
4030172-01
P4CO229
1.97 g
50 mL
03/12/14 10:30
4030172-01
P4CO229
1.97 g
50 mL
03/12/14 10:30
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
4030172-01 P4CO262 0.57 g 50 mL 03/13/14 15:05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 12 of 13

�: ( itit?! l tal!-Servic> Analytical R,f" "'NL`°V�] OF GUSTOD� G?�C���u�
:.. .. fj ' ' g Envircnmen�al :'s 9IUtIO nS PAGE _ Or _ QUOTEN To EG`75aDRE PROPERBaa-P.aP-02�:
I_AEORATORIF.S, INC.
n ri >pr Isgbl uok Road A P.O. Box 240543 h Cnarlotte, NC 28224-0543 Project Name:
PI na; 704/ 29-€�364 Fax: [phone] Short Woad Analysis: (Yes) (No) UST Project: (Yes) IV)
Client Company Name: C )�';y o� �'Ea�a=a v;+�'c� *Please ATTACH any project specific reporting (QC LEVEL I Il lit l�
provisions and/or QC Requirements
Report To/Contact Name: ���v s� + Invoice To:
Reporting Address: 0,na I l it l
,� Address:
SGc s a. ,'A- /i c
Samples INTACT upon arrival?
Received ON WET ICE? Temp
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES iec'd WlOUT HEADSPACE?
PROPER CONTAINERS used?
YES
NO N/^,
`—
i
00
•
M
a�
Fax es (No): 70-V79" U55 TO BE FILLED IN BY CLIENT/SAMPLINGPERSONNELPurchase Order No./Billing Reference
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE EL NC
EDD Type: PDF_ Excel ^ _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
�Pre-Approved' SC OTHER N/A
Site Location Name: F,7, .� �,a' e (, L`S t Ka—�— Samples received after 15:00 will be processed next business day.
Site Location Physical Address: � y3 Bc l �a"�' �' Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
n� A (SEE REVERSE FOR.TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES _ NO
J 7'8- C.-J L•., A�L'.t» RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- ��;
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR `TYPE TiVES� ID NO.
REMARKS LAB
HOURS SLUDGE) SEE BELOW NO. SIZE
1�0.
7. v V
y.
Fit A�
- 1A ...
two
J C a '' � aZvi
Sampler's Signature e7+ e L-Cr+� �` �' Sampled By (Print Name) 1,
Sampler's Z,�/v r t` Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Fee vay: (Signs m Date Militai
Relinq,�ished By: (Signatured B
) � g� f
r3 J / � r.' l a • .✓ f . �/1 A''r� (.� "D ., ea ''� ..i:.' � 1 i '•
By:
Relinquished By: (Sig n) p R ceiv', or Pris aboratorles By: I v--am ( t
�� G7
iw 1, wu -o.I-ion,. 11-1..--- .•...... __..-_.-- l} t�
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC 7 TIL REC IVED AT THE LABORATORY.LJ
❑ Fed Ex U UPS ❑ Hand -delivered U Prism Field Service ❑ Other
NPDES: I UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: ! RCRA: CERCLA I LANDFILL I OTHER:
❑ NC U SC :INC ❑ SC ❑ NC ❑ SC ❑ NC U SC U NC :1 SC ❑ NC U SC ❑ NC ❑ SC ❑ NC ❑ SC I ❑ NC ❑ SC
"`CONTAINER TYPE CODES: A = Amber C Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:

1
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOAEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 03/24/2014
Prism Work Order: 4030430
i ,max 1 3! ;I i 1 iF'
03/28/2014
.a_ta package a..:_.. e._ a. s'....a u.. t.., sa..., � , :,, r...a-r;,,.a "vvVc ^"A :^^lud2S ^ C--�
i iria Bata paGnayc wiitalaaa L— aiaaaytit,ao acSUILo ava uac prujeut auvraaiaac� o — U1J o .p...,
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC_
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]i364 - Toll Free Number:1-800f529-6364 - Fax: [phone] Page 1 Of 7

Sample Receipt Summary
03/28/2014
Prism Work Order: 4030430
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 4030430-01 Solid 03/24/14 03/24/14
Samples were received at 24.9 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc-
449 Springbrooh Road - P-0- Box 240543 - Charlotte, MC 28224-0543 --------- I
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

Laboratory Report
N'
03/2812014
City of Statesville, NC
Project: StaUme
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4030430-01
P.O. Box 1111
Prism Work Order: 4030430
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 03/24/14 13:20
Time Submitted: 03/24/14 14:30
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
69-6
by
0-100
0.100
1 *SM2540 G 3126/14 16:36
JAB
P4C0613
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 31251114 12:21
MES
P4C0522
Total Metals
Mercury
0.19
mg/kg dry
0.028
0.0094
1 *7471B W26114 15:03
MEH
P4C0454
Arsenic
8.5
mg/kg dry
0.37
0.064
1 *6010C 3126114 14:26
BGM
P4C0462
Cadmium
BIRL
mglkg dry
0.37
0.0035
1 *6010C 3r26114 14:26
BGM
P4C0462
Copper
36
mg/kg dry
0.73
0.0092
1 *60111C 31265114 14-26
BGM
P4C6462
Lead
SA
mq1kq dry
627
❑.043
1 *6010C 3126114 14:26
BGM
P4C0462
Nickel
140
mg/kg dry
1.5
0.012
1 *6010C 3126/14 14:26
BG119
P4C0462
Selenium
4.6
mg/kg dry
0.73
0.089
1 *6010C 3126114 14:26
BGM
P4C0462
Zinc
56
mgfkg dry
3.7
0.025
1 *6010C 3126114 14:26
BGM
P4C0462
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number., 11-8001529-6364 - Fax: [phone] -Page

p FJ iiyncni
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level 11 QC Report
3/28114
Prism Work Order: 4030430
Time Submitted: 3/24/2014 2:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPID Limit Notes
Batch P4C-04164 - 7471 B
Blank (134C0464-BILIKI)
... . ...... — -----
Prepared: 03124114 Analyzed: 03125114
Mercury
BRL
0.018
mg/kg wet
LCS (P4C0454-BSI)
— ----------
Prepared: 03124/14 Analyzed: 03/25114
-----------------
Mercury
0.461
0.021
mg/kg wet
0.4386 105 80-120
Batch M0462 - 3050B
Blank (P4C0462-BLKI)
Prepared: 03/25114 Analyzed: 03126/14
Arsenic
BRL
0.25
rng/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.98
mg/kg wet
Selenium
BRL
0.49
mg/kgwet
Zinc
BRL
2.5
mg/kg wet
LCS (P4C0462-BSI)
Prepared: 03/25114 Analyzed: 03/26114
Arsenic
22.9
0.25
mg/kg; wet
25.25 91 80-120
Cadmium
22.8
0.25
mg/kg wet
25.25 90 80-120
Copper
25.4
0.51
mg/kg wet
25.25 101 80-120
Lead
23.1
0.25
mg/kg wet
25.25 92 80-120
Nickel
23.3
1.0
mg/kg wet
25.25 92 80-120
Selenium
22.7
051
mg/kg wet
25.25 90 80-120
Zinc
22.8
2.5
mg/kg wet
25.25 90 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - ToR Free Number: 1-8001529-6364 - Far: 7041525-0409

City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters -(duality Control
Level II QC Report
3128114
Prism Work Order: 4030430
Time Submitted: 3/24/2014 2:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
t3atch P4C0513 - NO PREP
Blank (P4C8513-BLKI) Prepared & Analyzed: 03/26/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P-O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364-Fax:[phone] Page 5 of 7

City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level 11 QC Report
3M/14
Prism Work Order: 4030430
Time Submitted: 3/24/2014 2:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4CO522 - NO PREP
Blank (P4CO522-BLKI)
Prepared & Analyzed: 03125/14
Fecal Coliforms
BRL
0.2 MPNIg vvet
Sample Extraction Data
Prep Method: 3450E
Lab Number
Batch
Initial
Final
Daternme
4030430-01
P4C0462
1.99 g
50 mL
03/25114 10:30
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
4030430-01
P4C0454
0.63 g
50 mL
03/24114 16:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, MC 28224-4543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax, 7041526-0409 Page 6 of 7

I, t
�t+p r uI!-S.'rvii:%;.iliiirai iv
l N Ja: F k [ Et!vi !trn;:r.tai Seluti!)ns
LAtlORAIORIES !, ,.,
-'E•lena i p4i5?S�-fi3f,•� .. rar: T 14r .�-L`�IOr
Client Company Name: cli?'
Deport, To/Contact N a,rne: s�.3� v Ji n e iA-,
Reporting Address: � �y, P)WX I I ( 3
Phone:70'1-'370-343,, Faq es (No):7o'i-s7g 5
Entail Address:
EDOs Types: PDF_E)tcei_C9ther
Site Location Name: F0ai tar^�.�.�3iyTP
Site Location Physical Address:
1
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TINIE I MATRIX
I COLLECTED (SOIL,
MILrFARY I WATER OR
HOURS SLUDGE)
to
i
CHAIN OF CUSTODYRECORD
PAGE_ OF _ OU07E # To ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111 Ill IV)
provisions anchor QC Requirements
1 i 'rn
Address:
i
o
I
/r/..
co
r.L I I �:I �✓r'1 I' it
I'/ram:
f —_. __...
._
....
.....
..et+: ll ••...ml X.
Purchase Order No./Billing Reference TO BE FILLED IN B t' CLIEiNTISAMPLIN G PERSONNEL
Requested Due Date is 'I Day ❑ 2 Days U 3 Days O 4 Days O 5 Days Certification: NELAC_, DOD FL NC
"VUorlting Days" 0 6-9 Days Q Standard 10 days ❑ Prp Must Be
eArrovdSC OTHER- N/64
Sat triples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding %,,,eekends and holidays. Water Chlorinated: YES_ � _
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_ iNO_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) -
SAMPLE CONTAINER
*TYPE NO .I SIZE
SEE BELOW ,
M
ANALYSIS REQUESTED i PRISM
PRESERVA REMARKS LAB
TIVES ID MO.
In-
r Sampled B Print Name ,'0, ✓ LC� `� r '(! Affiliation
/ J
Sampler's Signature
P Y ( s,r 1 i
rbri
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above, Any changes must.ba Ilw r rye �I + t 7Y� ,F,) ,_Gd I
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. Date Military/Hours Additional Comments: r' Arr+ rs,1 l i!IIeI
atuey' I
Relinc7�ished By: (Signature) Rec4i ed By, (sign.� : � 7 � ��� .
J+r•' :•,v'Y.iJ-,'G1.%i.c;•'L•bt."r� Date
Relin shed By: (Sign cute R c V_d 8y: {Signature) 1.
Rl✓ ci`: Date _ i
Received For Prism Laboratorieggg by:
Rtlin `Ished By: (Signolure7
Method or Shipment: NOTE: ALL SAMPLE COOLERS SH5ULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COO Group Ito.
SAMPLES ARE NOT,! ffEPTED AIJD VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. �
LI Fed Ex 0 UPS U Hand -delivered • ,Prism Field Service ❑ Other - + t
NPDES: UST: G tyNDWATE:R: 1 ORiP1ItING WATER: SOLI) tNASTE: I RCRA: CERCLA LANDFILL OTHER: 'S
t�NC�SCI ❑NC ®SC I ❑NC CJSC — CiNC ❑5C i ❑NC CSC i C�NCi�SCI f3iVC L3SC C1NC QSG CsNC OSC
Volatile Organics ) ( Space)
*CONTAINER TYPE CODES: A = Amber = Clear G= Glass P = Plastic; TL =Teflon -Lined Cap VOA ganics Analysis Zero Head S ace

NC Certification No. 402
R
SC Certification No. 99012 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735f a M Environmenia! Soiutio+ s VA Certification No. 460211 04/28/2014
LABORATORIES_ INC;. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 04/21/2014
Statesville, NC 28687 Prism Work Order: 4040411
This da-ta ,.r.agc cantainj the a!ytica! . ult3 for th ••i :dciii'�ic'i "vv Jc ••••d �••••lild $ " vuS �:urruii v'� C�.....L.
pc.„,.4y� .,..,, a„u,y.t..<., �.,�u �
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J. -
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone] Page 1 of 7

I S NA Full -mm,er- Fln aiytico' &
ptl I5i En��,ironmental Solutions
Sample Receipt Summary
04/28/2014
Prism Work Order 4040411
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stalime
4040411-01 Solid 04/21/14 04/21/14
Samples were received in good condition at 1.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1 -8001629-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
_
r-siBien.a,:,iolut, &
o Brvrcnmenial Solutions
04/28/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: Stalime
Attn: Andy Smith
Prism Sample ID: 4040411-01
P.O. Box 1111
Prism Work Order: 4040411
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/21/14 13:57
Time Submitted: 04/21/14 15:45
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
solids
eu.0
% by
0.100
0.100
1 "SM2540 G 4124114 15:00
JAB
0406612
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 4/22/14 13:05
MES
P4D0496
Total Metals
Mercury
0.24
mg/kg dry
0.029
0.0099
1 *7471B 4122M4 17:36
MEH
P4D0442
Arsenic
BRL
mg/kg dry
3.7
0.54
10 *6010C 4/25/14 19:54
BGM
P4D0485
Cadmium
BRL
mg/kg dry
3.7
0.036
10 *6010C 4/25114 19:54
BGM
P4D0485
Copper
41
mg1kq dry
7.4
0.094
10 *6010C 4125114 19.54
BGM
P41130485
Lead
19
mg/kg dry
3.7
0-"
10 *6010C 4/25114 19.64
BGM
P4D0485
Nickel
170
mglkg dry
15
0.12
10 *6010C 4/25114 19:54
BGM
P4D0485
Selenium
BRL
mg/kg dry
7.4
0.90
10 *6010C 4125/14 19:54
BGM
P4D0485
Zinc
71
mglkg dry
37
0.25
10 *6010C 4/26114 19:64
BGM
P4130485
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543'- Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: l-8001529-6364- Fax: [phone] Page 3 of 7

F!AI-^aerv[ce Analytical &
En--oin—tai Solu Ucr,s
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4D0442 - 7471B
Project: StaLime
Level II QC Report
4/28/14
Prism Work Order: 404.0411
Time Submitted: 4/21/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result % REC Limits RPD Limit Notes
Blank(P4DO442-BLKI) -_ --
- - -
---
Prepared:04/21/14 Analyzed_04/22/14 -_
Mercury
BRL
0.019
mgA<g wet
LCS (P4D0442-BSI)--.-.----_.. ------
--. -
--- - -
-Prepared:
04/21/14 Analyzed_04/22/14
Mercury
0.445
0.019
mg/kg wet
0.3906 114 80-120
Batch MUM - 3050B
Blank (P4D0485-BLK1)
Prepared: 04/24/14 Analyzed_04/25/1
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.49
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4D0485-BSI) -- --- ---
-- - -
- - - -
— - - - -Prepared:
04124/14 Analyzed: 04/25/14 - -- - ----- - ----- -
Arsenic
0.985
mg/L
1.000 99 . 80-120
Cadmium
0.982
mg/L
1.000 98 80-120
Copper
1.04
mg/L
1.000 104 80-120
Lead
0.964
mg/L
1.000 96 80-120
Nickel
0.966
mg/L
1.000 97 80-120
Selenium
0.995
mg/L
1.000 100 80-120
Zinc
0.969
mg/L
1.000 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spiingbrook Road - P-O- Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 4 of 7

P I S M Full -Service Analytical &
En':roninenzal Solutror,s
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level 11 QC Report
4/28/14
Prism Work Order: 4040411
Time Submitted: 4/21/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P4D0512-BLKI) Prepared & Analyzed: 04/24/14
% Solids 100 0.100 %byWeight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 5 of 7

I M I Full -Service- Flnalyiical &
Environmertal Sclutlr, ns
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch P4bO496 - NO PREP
Project: Stal-ime
Level 11 QC Report
4/28/14
Prism Work Order: 4040411
Time Submitted: 4/21/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P4DO496-BLK1) Prepared & Analyzed: 04/22/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
4040411-01
P41D0485
1.98 g
50 mL
04/24/14 9:55
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateTme
4040411-01
P4D0442
0.6 g
50 mL
04/21/14 14:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -'Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 6 of 7

' ". .. . _..._ -_.... ........ .. . ..._ .. ... ...-
... _-. -
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[� L } y `-'rivi; print:. ntai SOlUtirns PO.GE OF _ allOTE 0 TO ENSURE: PPOPER BILLING: _
7 O
au nk IL IT- I rl,on an Iv ai y� 0
t
' `r�^ '• WBGItI.'ONIl5, II Ic;.
_. . •... Project
Name:
' Received O I.1frl !--
a nl .it d? ✓_ m
PROF�. I'I ES i, / \J I'•./4 a
eS49 1riral r ok I end ° CPtasioYte, YdL: 8217
PSrGn= r04152'a-fi3C�3 C'cur: 704/h�5-s40S Short Hold Analysis: (Yes) (NO} UST Project: (Yes) (NO} i Recehrtl U!ITHI '1CJI DI IG IINIP S?' "._ N
*Please ATTACH any project specific reporting (QC LEVEL III III IV) I —
c
Ciient Company Name: � Y�(v '9 � ��� c a� f; provisions
and/or QC Requirements
Si�ALS INTACT?
.� �7o'rae_4'P"t
Report To/Contact Name: A • Ia ,A Invoice To:
; /<li fi(ILr. pI r JlT 4_;7 !�I D�Pnf E1
� /
I";Ut' ( I IIPJ \III iz� �i^'Reporting
..
p q Adalress:. 1.•�, 8 ¢ & V Address:
7Etni h:;ir, IL> Lr fc� c l cu _ L r r
Phone:70 1 ,' '7 8' _ 43 7 Fax (' es ,(No) 'j' :t /- `3 ' Y65 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL'
Ernait Address: Requested Due Date ❑ 1 Day 0 2 Days CU 3 Days 0 4 Days ❑ 5 Days
Certification: NELAC DOD I=L NC
ED,D Type: PDF_EXce! tither "Working
Days" s" ❑ 6-9 Days ❑ Standard 10 days C] Rush Work Must Be —
Y Pre -Approved SC OTHER lei/A
Site (Location Name: i + r 4 i, C }' Il` s t" u y Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NQ—
Site Location Physical Address: a�'l .3 � • t ( 'tea' va /s •� .
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
TO CLIENT)
Sample Iced Upon Collection: YES_ NO_
p
,, .�,, ¢'7� k•. D �,', �t� L'
RENDERED BY PRISM LABORATORIES, INC.
,
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED PRISM
v `r
LAB
CLIENT
SAMPLE DESCRIPTION
DATE COLLECTED
COLLECTED MILITARY
(SOIL,
WATER OR
SLUDGE)
PRT V� VA /
�/' g..
4��';,r / REMARK I
Zr / ID NO.
/�/ --
'TYPE
BELOW
r--�
NO. SIZE
♦ 1 --�
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Zd
„�` Name Affiliation
)
Sampler's Signature �t'a tz •` + Sampled By (Print
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the prism Project Manager. There will be cha'.ges far any changes a�_775e5
ve been initialized.
Receiv' By: (Signature) Date MilitarylHours AddIt10
Reiinqui�shad By: (Signatus-
Relin e v: (Signature} Received By: (Signature)
I ,„ ✓--
Relinquisi \ y: (Signature �� -1 II RecaFor Laboratories By: , _ F(� • \ I, <� '
Method (Shipment PIOTE: A .L SAMPLE COO RS SHOULD BE TAPED SHUT gH CU ODY SEALS FOR TRANSPORTATION TO THE LABOPATORY. COC Group NO.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST GUN L RECEIVED AT THE LABORATORY. - t
CI Fed E : ❑ UPS ❑ Hand -delivered ❑ Prism Field Service ❑ Other add' 9
NPDES: UST: GROUNDWATER: DRINKING WATER: I SOLID WASTE: i GiCRA: CBRCLA LANDFILL ; C3NCOTHER:
0NCCJSC C]NC QSC ®NC ®SC I CI NC ®SC 1, ®NC ®SC ; ®NCOSC ®NC 0SC ®NC L�SC ©NC OSC
C]❑ 0 ® --
"CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Comments:

NC Certification No. 402
SC Certification No. 99012 Case Narrative
PRIt Full -Service Analytical U NC Drinking Water Cert No. 37735
M ' Environmental Solutions VA Certification No. 460211 05/15/2014
LAEORA-T, eRIES, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 05/05/2014
Statesville, NC 28687 Prism Work Order: 4050093
This data package coniains the anaiyticai results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
t�_
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-800/629-6364 - Fax: [phone] Page 1 of 14

Sample Receipt Summary
1
FUII-Service A —lyrical a
N
F_nv ironmental Soltilirns
05/15/2014
.Prism Work Order: 4050093
Client Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
StaLime
4050093-01
Solid
05/05/14
05/05/14
Fecal #2
4050093-02
Solid
05/05/14
05/05/14
Fecal #3
4050093-03
Solid
05/05/14
05/05/14
Fecal #4
4050093-04
Solid
05/05/14
05/05/14
Fecal #5
C.
#'I
4050093-05
A/lG/1 Q0 nC
Solid
C`..I:A
05/05/14
!1 1/ /A A
05/05/14
/1c lnc/AA
cal
� G�.qr >rV
Fecal #7
YVJVVJJ-VV
4050093-07
JVIIU
Solid
VJlVJI IY
05/05/14
VJ/VJ/IY
05/05/14
Samples were received at 33.4 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 2 of 14

6 � �y, Full-Servic c• Analytical Y.
-�.�..'.,"+�' � � En•�iromm�ntal Solutions
(Laboratory Report
05/15/2014
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: StaLime
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4050093-01
P.O. Box 1111
Prism Work Order: 4050093
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Piani Avaiiabie Nitrogen
560
mgikg
160
13
2 *Calculation 5114/14 8:36
CLB
1CALC]
Solids
82.6
% by
0.100
0.100
1 *SM2540 G 517114 15:15
JAB
P4E0128
Weight
Nitrate/Nitrite as N
14
mglkg dry
6.1
0.67
1 *SM4500-NO3 F 517114 11.35
CLB
P4E0109
Phosphorus -Total
22a6
mg/kg dry
120
26
40 *SM4500-P F 5112114 925
CLB
P4E0171
Total Keldahl Nitrogen
2200
mg/kg dry
610
51
2 *351.2 5114114 8:36
CLB
P4E0217
Ammonia as N
34
mglkg
5.0
1.2
1 *SM4500-NH3 G 518114 10:31
CLB
P4E0134
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
02
1 *SM9221 E 516/14 10:35
MES
P4E0176
Total Metals
Mercury
0.24
mglkg dry
0.022
0.0075
1 *7471B 6/8114 13.58
MEH
P4E0141
Arsenic
5.0
mg/kg dry
0.30
0.044
1 *6010C 517114 17.41
BGM
P4E0112
Cadmium
BRL
mg/kg dry
0.30
0.0029
1 *601OC 5/7/14 17:41
BGM
P4E0112
Copper
23
mglkg dry
0.60
0.0076
1 *6010C 517114 17:41
BGM
P4E0112
Lead
6.2
mg/kg dry
0.30
0.035
1 *6010C 517114 17.41
BGM
P4E0112
Nickel
89
mg/kg dry
1.2
0.0097
1 *6010C 5/7/14 17:41
BGM
P4E0112
Potassium
5100
mglkg dry
300
19
20 *6010C 5113/14 2122
BGM
P4E0112
Selenium
2.1
mglkg dry
0.60
0.072
1 *6010C 577114 17.41
BGM
P4E0112
Sodium
610
mg/kg dry
15
0.14
1 *6010C 5l7/14 17.41
BGM
P4E0112
Zinc
41
mglkg dry
3.0
0.020
1 *6010C W7/14 17,41
BGM
P4E0112
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1 -80 01529-6364 - Fax: [phone] Page 3 of 14

pp `'ice Fidl-Service Analytical &
f1 I Fn--niemel s"Mions
Laboratory Report
05/15/2014
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, Client Sample ID: Fecal #2
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4050093-02
P.O. Box 1111 Prism Work Order: 4050093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
bonos Uu.v "/o ®y 0.100 0.100 1 "SM2540 G 517114 15:15 JAB 114Cu1 ca
Weight
Microbiological Parameters
Feral Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 516/14 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: [phone] Page 4 of 14

Full -Service Analylicw Laboratory
Report
P� � I Fnvironmanlal Snlulior.; 05/15/2014
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #3
Attn: Andy Smith 6ODay 7 Fecal) Prism Sample ID: 4050093-03
P.O. Box 1111 Prism Work Order: 4050093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Dateffime
ID
General Chemistry Parameters
Soiias 80.6
% by
0.100
0.100 1 "SM2540 G 517114 15:16 JAB
P4E0128
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 5/6/14 10:35 IVIES
P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 -Fax: [phone] Page rJ Of 14

roll-Sen;ice Analytical &
r_rroironmental Solutron=_
Laboratory Report
05115/2014
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, Client Sample ID: Fecal #4
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4050093-04
P.O. Box 1111 Prism Work Order: 4050093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
o ounu's a[.4 % by 0.100 0.100 1 `SM2540 G 5n114 15:16 JAB P4E0128
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 5/6114 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 14

Full-Senrice Analytical Zy
Environmental Sch.itions
Laboratory Report
05/15/2014
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #5
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4050093-05
P.O. Box 1111
Prism Work Order: 4050093
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
5oiids
86.4 1. by 0.100 0.190
1 "SM2540 G 577n4 15.15 JAB P4rui28
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.2
1 *SM9221 E 5/6/14 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 25224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 7 Of 14

1 I Full -Senile Analylical
Environmental Solution.=_
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/15/2014
Client Sample ID: Fecal #6
Prism Sample ID: 4050093-06
Prism Work Order: 4050093
Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids sci.0
% by
6.10o
0.100 1
*SE>M2540 G 5f7/14 15:15 JAB
P4Eo128
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 5/6/14 10:35 MES
P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NG 28224-0543
Phone: 704/52M364 - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 8 of 14�

Laboratory Report
Full -Service Analytical !i
_ , @� �$ Er.ironmantal So;ution' 05115/2014
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #7
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4050093-07
P.O. Box 1111 Prism Work Order: 4050093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/05/14 10:40
Time Submitted: 05/05/14 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
t c,rtt 5
-- --"-- w 1. e`+y UA 66 6.i66 i "SM2540 G 5F7114 15:15 JAB P4t0128
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 `SM9221 E 5/6/14 10:35 MES P4E0176
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road'- P.O. Box 240643 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 14

_,g ISp I Full -Service F;n 2lytir al &-"-hR dt crn,ironmFnial S�lutiCrs
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
5/15/14
Project: Stal-ime (Qtdy, BiWeekly, 6ODay Prism Work Order: 4050093
7 Fecal) , Time Submitted: 5/5/2014 3:00:OOPM
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P4EO112 - 3050B
Blank (P4E0112-BLK1)
Prepared & Analyzed: 05/07/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
13
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Sodium
BRL
13
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4E0112-113SI)—
Prepared & Analyzed: 05/07/14
Arsenic
24.6
0.25
mg/kg wet
25.25 97
80-120
Cadmium
24.4
0.25
mg/kg wet
25.25 97
80-120
Copper
25.8
0.51
mg/kg wet
25.25 102
80-120
Lead
24.2
0.25
mg/kg wet
25.25 96
80-120
Nickel
24.1.
1.0
mg/kg wet
25.25 96
80-120
Potassium
514
13
mg/kg wet
505.1 102
80-120
Selenium
24.8
0.51
mg/kg wet
25.25 98
80-120
Sodium
506
13
mg/kg wet
505.1 100
80-120
Zinc
24.1
2.5
mg/kg wet
25.25 96
80-120
Batch P4E0141 - 7471 B
Blank (134E0141-BLKI)
Prepared & Analyzed: 05/08/14
Mercury
BRL
0.020
mg/kg wet
LCS (P4E0141-BSI)
Prepared &Analyzed: 05/08/14
Mercury
0.421
0.020
mg/kg wet
0.4098 103
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001529-6364 -Fax: [phone] Page 10 of 14

P@ S S M I Full -Service Analyiical G
Enoironmeniai Solutions
Level II CSC Report
5/15/14
City of Statesville, NC Project: StaLime (Qtdy, Biweekly, 60Day Prism Work Order: 4050093
Attn: Andy Smith 7 Fecal) Time Submitted: 5/5/2014 3:00:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4EO109 - NO PREP
Blank (P4EO109-BLK1)
Prepared & Analyzed: 05/07/14
--- --- -
Nitrate/Nitrite as N
BRL
5.0 mg/kg wet
- - - --
LCS (P4EO109-BSI)
-- ---- -
- ---- -- - -
Prepared & Analyzed: 05/07/14
.._,._ . — - -----. ---
Nitrate/Nitdte as N
51.0
5.0 mglkg wet
---- - -- -- - --
50.00 102 80-120
Matrix Spike (P4E0109-MS1)
Source: 4050093-01
Prepared & Analyzed: 05/07/14
Nitrate/Nitrite as N
78.5
6.1 mg/kg dry
60.53 14.3 106 80-120
Matrix Spike Dup (P4EO109_MSD1)
-- ------------
Source_ 4050093-01
Prepared & Analyzed: 05/07/14
Nitrate/Nitrite as N
76.3
6.1 mg/kg dry
--.._ . _ _— ..------- ----- - - - - -- ------ _ --- ------
60.53 14.3 102 80-120 3 20
Batch P4EO128 - NO PREP
Blank (P4EO128-BLK1) -- - _
-- --- -
Prepared & Analyzed: 05/07/14
- --- - - --- -- - ---
% Solids
100
0.100 % by Weight
----- .------------ --
Duplicate (P4E0128-DUP2)
------ - ------------ -- -
..
Source: 4050093-07
Prepared & Analyzed: 05/07/14
% Solids
82.8
- -- _.._ _._.._..___ ---- - --..__... -- --- -- - --- ---
0.100 % by Weight 78.5 5 20
Batch P4EO134 - NO PREP
Blank (P4EO134-BLK1)
-- — -- - --- - --- — - - -
- - -- - - --
Prepared & Analyzed: 05/08/14
-- _ --- ----- - - - - - -- - - --
Ammonia as N
BRL
5.0 mg/kg
-- - --- -
LCS (P4EO134-BSI) _
Prepared & Analyzed: 05/08/14
Ammonia as N
128
5.0 mg/kg
125.0 102 M120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P_O_ Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 14

PC) P I Full -Service An
I) J Environmental solu'tior s
Level 11 QC Report
5/15/14
City of Statesville, NC Project: StaLime (Qtdy, BiWeekly, 60Day Prism Work Order: 4050093
Attn: Andy Smith 7 Fecal) Time Submitted: 51512014 3:00:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4EO134 - NO PREP
Matrix Spike (P4E0134-MS1)
Source: 4050093-01
Prepared & Analyzed: 05/08/14
Ammonia as N
210 5.0 mg/kg
125.0 34.5 140 80-120 M
Matrix Spike Dup (P4E0134-MSD1)
Source: 4050093-01
Prepared &Analyzed: 05108/14
Ammonia as N
209 5.0 mg/kg
125.0 34.5 139 80-120 0.5 20 M
Batch P41E0171 - SM4600-PBS
Blank(P4E0171-BLK1)
Prepared: 05/09114 Analyzed: 0-5/12/1.4--
Phosphorus-Total
BRL 2.5 mg/kg wet
---------
LCS (P4EO171-BS1)
Prepared: 05/09/14 Analyzed: 05/12/14
- ------ ---
Phosphorus -Total
102 2.5 mg/kg wet
100.0 102 90-1110
Batch P4EO217 - 351.2
Blank.(P4EO217-BLKI)
Prepared: 05/13/14 Analyzed: 05/14/14
Total Kjeldahl Nitrogen
BRL 25 mg/kg wet
LCS (P4EO217-BS1)
Prepared: 05/13/14 Analyzed: 05114/14
Total Kjeldahl Nitrogen
5040 1000 mg/kg wet
5000 101 90-110
Matrix Spike (P4E0217-MS1)
Source: 4050093-01
Prepared: 05/13/14 Analyzed: 05/14/14
Total Kjeldahl Nitrogen
9650 3000 mg/kg dry
— ----- ----- ---
6053 2190 123 90-110 MI
Matrix Spike Dup (P4E0217-MSDI)
Source: 4060093-01
Prepared: 05/13114 Analyzed: 05/14/14
Total Kjeldahl Nitrogen
8570 3000 mg/kg dry
----------- --- -- ----- - - - . ..... ­ . . . ........ ......
6053 2190 105 90-110 12 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbro6k Road'- P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page �120f 14

Level II QC Report
a ''�
f
Full -Service .4n�1tic21 S
Environmcr.;21 Solutions
5/15/14
City of Statesville, NC
Project: Stal-ime (Qtdy, BiWeekly,
60Day Prism Work Order: 4050093
Attn: Andy Smith
7 Fecal)
Time Submitted: 5/5/2014 3:00:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P4EO176 - NO PREP
Blank (P4E0176-BLK1)
Prepared & Analyzed: 05/06/14
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
DateTme
4050093-01
P4E0217
0.05 g
25 mL
05/13/14 10:00
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Daterrrme
4050093-01
P4E0171
1 g
50 mL
05/09/14 14:11
Prep Method: 3050E
Lab Number
Batch
Initial
Final
DateTme
4050093-01
P4E0112
2.03 g
50 mL
05/07/14 10:15
4050093-01
P4E0112
2.03 g
50 mL
05/07/14 10:15
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateTme
4050093-01
P4E0141
0.65 g
50 mL
05/08/14 9:55
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 13 of 14

CHAIN OF CUSTODY RECORD:
L "rf 4� dt Sq tg j ¢i7 u +d . cs� T r i
r �t )) � i 0�� k` 3'
z1.�
� ) I F
t
1
Fuli•Service. Ar a3vtical �:
PioE-t A:rr-95A ..�
I YES c 1,vy�.
,�
t 1 ti a m� tv
i
i vironment l Solutioins
PAGE OF GIRBO rE #'PO ENSURE PROPER BILLING:
)t I IN ' 1 upon arrr/..1'i
O
F1CS. INC.
Project Name:
1 Ijn� C ) J /ET ICE?
441S;sringbrookRoad , Charlotte, NC282,7
Phone [phone] : Fax: [phone]
r
,short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
� PROPER }tr.. � rfir it r]^ - --
N
�
00 �' d ����
Client Company Name:P� J zd °=�'s ;
Please ATTACH any project specific reporting (QC LEVEL I II III IV)
-
OUS LI YSC II`rTa,
CD
provisions and/or QC Requirements
I11]/OLJT DSPA
Report To/Contact Name:
Invoice To:
red P _?
Reporting Address:
Address:
I h' : rll II�LI S iscd _
i
� aY 5c•:d&tl� i4'c
7r-4IE ._...hereillsl.e --fiber -1:: �_�.._ /C r ..Z�Y`
i
Phone:70ji- 'P3 Faac� es {No):`ri�' - -'�G
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ® 3 Days O 4 Days ❑
5 Days
Certification: NELAC Do'O FL NC
EDD 'type: PDF_Excei Other "Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ RushWorMust Be
�� PP
Pats �d Ci^Ie'' h t 7 1 business day.
SC
OTHER N/A
Site Location Name: illuo
I? _ Samples received after 14:00 will be processed next
Site Location Physical Address: 693 B 1.1 � �"� rin . Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated:
YES_ No_
` o a a (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
fe. RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I
Sample Iced Upon an Collection: YES_ NO —
TIME
MATRIX
j SAMPLE CONTAINER
/
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLI-CTED
(SOIL,
PRESERVA-
TIVES
REMARKS LAB
'TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
HOURS
WATER OR
SLUDGE)
NO. SITE
i
j + ;
/ i'
ID NO.
j
SEEBELOW I
el - - -- -
e'y
�'•ti :a a "J
j �8'�)
--.__
i
ie4Y p, c.� All
e''
j— —.
I t': �_ S'� B ip _ d ,✓ ,'af1F7
.%'? C i_fx�_&.+'�
—
✓
$''fit d>„• arra �
-
'�
g
N
I �-• .- /l� � ,
_H� �,, .� 1: !-- --
1
i
J
,✓y� am r'' rr% •"2
o
Sampler's Signature ./f-a—ZIr "C',�.i��,e Sampled By (Print Name) v Z4,0/ i' JC Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
t` dam
submitted in writing to the Prism Project Manager. There will be charges for any change �fter analyses have been initialized.
I`
; �L ��{xrr����
Relinggjshed By: (Signature > ,i. Received By: (Si r'alture)� ,L;
y✓d,r>e, .
�,
Date MIIRaryiHours Additional Comments . it F I n\.aI ri1 I
7 ill . %d w>7 + :
I I j
Site, irnc;
Relingt' od By: (Signature) Receved By: (Signature)
Date
Pepal l..0 d.
p
Relin 1' e,+By: (Sigi a G ')J Received F� �m Laboratodesj.'
Date
�- 4=i! 1 f�Ch1,Fa
r
od o�Shipment• NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT�YKH k?USTODY SEALS FOR TRANSPORTATION TO HE LABORATORY.
11 SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINSL Oe�UNTIL RECEIVED AT THE LABORATORY,
COC Group No.
._...__.._...__.-__,_.....,_.__.,.....__._-.......,
r of
❑ Fod Ex ❑ UPS ❑ Hand -delivered Cl Prism Field Service ❑ Other
NPDES: UST: j GROUNDWATER: j DRINKING WATER: j SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
®NC❑SCi ©NC Im1SC',, Cl NC El SC � ❑NC ❑SC ®r!C ®SC ®NC�1SC L�NC CSC:®NC ❑SC ®NC 0SC
n n I n F1 ❑ ❑ ❑ 'r❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic: TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

402
NC Certification No.990 Case Narrative
SC Certification No. 99012 !Ft
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No. 460211 05/28/2014
P'R. I S, K"-V1
ABOA470niFs i;,c DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOIIEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 05/19/2014
Statesville, NC 28687 Prism Work Order: 4050464
This data package contains the anaiyticai results for the project identified above and includes a Case Niarrative, Sampie
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
)� L��- a- 01-
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with. a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 1 of 7

�"° Futl-Service Analytical
u S
I ee IN Environmental Solutions
Sample Receipt Summary
05/28/2014
Prism Work Order: 4050464
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime
4050464-01 Solid 05/19/14 05/19/14
Samples were received at 25.4 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P_O. Box 240543 -charlotte, ING 28224-0543
Phone: 704I529-6364 - Toll Free Number:1-800l529-6364 - Fax: [phone] Page 2 Of %

Laboratory Report
PR4e RitLSer•✓icc
6
BM
Annlylical &
/2812014
G � Envn"onmcntai
Solutions
05
City of Statesville, NC
Project: StaLime
Client Sample ID: StaLime
Attn: Andy Smith
Prism Sample ID: 4050464-01
P.O. Box 1111
Prism Work Order: 4050464
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/19/14 00:00
Time Submitted: 05/19/14 16:55
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
o 5oiios
78.6
! by
u.i0o
rJA50
i `SM2646 G Si23ii4 i5:32
iAB
P4EG.434
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 'SM9221 E 5/20/14 10:00
MES
P4E0456
Total Metals
Mercury
0.17
mg/kg dry
0.025
0.0084
1 *7471B 5122114 19:00
MEH
P4E0425
Arsenic
6.2
mglkg dry
0.32
0.047
1 •6010C 5123/14 16:16
BGM
P4E0446
Cadmium
BRL
mg/kg dry
0.32
0.0031
1 '6010C 5/23/14 16:16
BGM
P4E0446
Copper
31
mg/kg dry
0.65
0,0082
1 •6010C 5123M4 16:16
BGM
P4E0446
Lead
8-2
mg/kg dry
0-32
0.038
1 '6010C 5/23M4 16:16
BGM
P4E0446
Nickel
120
mglkg dry
1.3
0.011
1 •6010C 5/23114 16:16
BGM
P4E0446
Selenium
3.1
mglkg dry
0.65
0.078
1 `6010C 5123114 16:16
BGM
P4E0446
Zinc
66
mg/kg dry
3.2
0.022
1 '6010C 5123114 16:16
BGM
P4E0446
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 0f 7

v J J I Full-Sc�vice Analytical &
iUf Environmen;ai SotuLens
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
5/28114
Prism Work Order: 4050464
Time Submitted: 5/19/2014 4:55:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch NE0425 - 7471 B
Blank(P4E0425-BLK1) - - - -- -- _--- Prepared:05/21/14 Analyzed_ 05/22/14_-
Mercury BRL 0.019 mg/kg wet
LCS (P4E0425-BS1) - Prepared_ 05/21/14 Analyzed: 05/22/14
Mercury 0.485 0.021 mglkg wet 0.4386 111 80-120
Batch NE0446 - 3050B
Blank (P4E0446-BLK1)
Arsenic -- ----
Cadmium
Copper
Lead
Nickel
Selenium
Zinc
LCS (P4EO446-BS1)
Arsenic
Cadmium
Copper
Lead
Nickel
Selenium
Zinc
Prepared: 05/22/14 Analyzed: 05/23/14
BRL
0.24
mg/kg wet
BRL
0.24
mg/kg wet
BRL
0.49
mg/kg wet
BRL
0.24
mg/kg wet
BRL
0.98
mg/kg wet
BRL
0.49
mg/kg wet
BRL
2.4
mg/kg wet
---- - - - --
---------
- --
Prepared: 05/22/14 Analyzed: 05/23/14
-------------------
24.1
0.25
mg/kg wet
25.00
96
80-120
24.0
0.25
mg/kg wet
25.00
96
80-120
25.2
0.50
mg/kg wet
25.00
101
80-120
24.0
0.25
mglkg wet
25.00
96
80-120
23.8
1.0
mg/kg wet
25.00
95
80-120
23.8
0.50
mg/kg wet
25.00
95
80-120
23.9
2.5
mg/kg wet
25.00
96
80-120
BH
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 249543 - Chadolfe, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 4 of 7

��+��5,+, � � �. FuII-Service Analyiicat &
P 1 Y ,�-�� I �i�vironrncnial Sciuiin ns
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
5/28114
Prism Work Order: 4050464
Time Submitted: 5/19/2014 4:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4EO494 - NO PREP
Blank (P4EO494-BLKI) --__ -
- - - Prepared & Analyzed: 05/23/14
% Solids
100 0.100 % by Weight
Blank (P4EO494-BLK2)
- - --- -- -- -- - _
Prepared & Analyzed: 05/23/14
- --- - - - - - - - - --- -- --_--- ------ - - ---- - - -
% Solids
100 0.100 % by Weight
Blank (P4EO494-BLK3)
--- ----- —---------------
Prepared & Analyzed: 05/23/14
---- --- _._ _ .. - -----
% Solids
100 0.100 % by Weight
Blank (P4EO494-BLK4)
Prepared & Analyzed: 05/23/14
% Solids
100 0.100 % b Wei ht
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P-O. Box 240543 _ Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 5 of 7

PR p S � I Fun -Service ic: i4
tUl ¢ Environmcnial al SOi Solutir. ns
.,. .. IJ.L+GriM1l V fiiLS. III �.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch NE0456 - NO PREP
Blank (P4E0456-BLK1)
Fecal Col'rforms
Prep Method: 3050B
Lab Number Batch
Project: Stal-ime
Level 11 QC Report
5/28/14
Prism Work Order: 4050464
Time Submitted: 5/19/2014 4:55:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Prepared & Analyzed: 05/20/14
-------------------------- -----
BRL 0.2 MPN/g wet
Sample Extraction Data
Initial Final DateFrime
4050464-01 P4E0446 1.96 g 50 mL 05/22/14 10:45
Prep Method: 7471B
Lab Number Batch Initial Final Date/Time
4050464-01 P4E0425 0.61 g 50 mL 05/21/14 13:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 -Fax: [phone] Page 6 of 7

�r�;I�nEw�t Irby gp�p t�gy ropy F�c�g� P�y�r�{ RECORD fp�p�ga
C YS Udm51 OF C'`US70i Y RECO 1LSD
t � 60.� i�} yx�;� .f+�� i?.7� T �S 9 'Vr :? K�' �i •ISM �. 1L� fl �.
I� e NO,,,FS��', ��.,, pp�b � �-•�.F �a �� ��i�."�����
uil-Set-vice Analytical &
�nvironn.enlal Solutions P___ OF QUOTE 1) TO ENSURE PROPER BILLIHO:
r E.,S t O ill
p
G —t-
rrtrq I IN 1:',i T upon arrwai'? /--
_ .-"'-:-' L LOIiFIIORIFi II�G. -
Project Name:
/
I'
RKcal,.d Dt;,Ft! T Imo_
449 Springbrook Roar! - Charlotte, NC 2G217
Phone [phone]/b . Fax: 04,625 Oat.: Short bold Analysis: (Yes) (No) UST Project: (Yes) (NO)
-i'OPLR FF,1=.:L i`JPTiI f S [I li aic:o7 � �_
- — --- ---
CA
�
�+ y *Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Company Name: ao Y 3 ; ` •,
eceiv:=c: L`dI i l tll'! NOLDIPf` "fIr,1E ?. _✓'_ ____ _._..__-
a.
Client provisions and/or QC Requirements
�.. SEALS INTACT?
K
Report To/Contact Name: 't ;i �u'n "� iz Invoice To:
V(A.,Al'ti_LS_t rec. vdii IJT IEADSPf�C;E r:
I
Reporting Address: _ °� 6�'�x d' d 3 Address:
n::,H! F? i:1P•.Ti;l
P r :AItNER =
i. .: - .,_ �;-�• 5a ,-" - `,/�
..
i
Phone:70 - F1,YY ��° Fax(12es (No): 21• o1S 5
Purchase Order No./Billing Reference
PERSONNEL,
TO BE FILLED IN BY CLIENT/SAMPLING ONNEL,
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification:
NELAC I3®ID FL NC
EDID Type: PDC Excel Other "Working Days" L1 6-9 Days ❑ Standard 10 days ❑ Wust Be
Pre-ApprovedSC
OTHER NIA
T—
Site Location Name: f6, Y'4p3 �. ,, je Lotz; TP Samples received after 14:00 will be processed next business day.
Site Location Physical Address:.' d Sell/ r ;•A-o Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
`a (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
eve' RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO —
DATE
TIME MATRIX
COLLECTED ! SOIL,
(
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRESERVA- j/ �� % i
PRISM
CLIENT
_. _
i ti ` k
i` REMARKS
LAB
SAMPLE DESCRIPTION COLLECTED
MILITARY WATER OR
*TYPE
NO. SIZE
TIVES / `L i / %
/ �� i
j" /
{D NO.
HOURS SLUDGE)
SEE BELOW
/i ,i G"
- ----
53
C'
I
I
i
z
Sampler's S1gnature0,,X - Sampled By (Print Name) v.",(, Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must betof�
)iKy��i 1�t �U,at',
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized..t,ij�t.1?<.�5-",1�;5,
Relin hed B (Signat") -,, Recei d B (Signature) Date Milltary/Hours
x(s ") rY
✓mil
Additional Comments: SiteArrivd-fl.we: I '
K v tl B SI naturd Date
Rehnp ied By: (Sin ire) �' r y: ( g
Srtc C`eperlure 1 imo: ;
Rel " u" hed By: (Sig arure) Ra�eiae Fo.Prism lab. ",orles By: Date
_
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No,
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEI .AD AT THE LABORATORY. A /, ,
❑ Fed Ex ❑ UPS ❑ Hand -delivered ,-Prism Field SeR'ice ❑ Other
NPDES: US'I: j G6 IUNDWATER: I DRINKING WATER: SOLID WASTE: i RCRA: CERCLA I LANDFILL OTHER:
❑ NC ❑ SCI ❑ NC ❑ SC ❑NC ❑ SC O NC ❑ SC ❑ NC ❑ SC ! ❑ NC ❑ SC! ❑ NC © SC ❑ NC ❑ SC ❑ NC ❑ SC
❑ i❑ ❑ O ❑ 1❑ ❑ ❑ ❑
*CONTAINER TYPE CODES: A = Amber C Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. Case Narrative
SC Certification No. 990 99012
Full -Service Analytical ° NC Drinking Water Cert No. 37735
06/11/2014
Environmental Sohffion5 VA Certification No.460211
uooauTORIE . iNC. DoD FLAP: L-A-B Accredited Certificate No. L2307
ISOIIEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 06/02/2014
Statesville, NC 28687 Prism Work Order: 4060041
This its data package contains the arralyticai Pesuiis for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Diluted due to interference from high Calcium concentration.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road P.O. Box 240W - Charlotte, NC 28224-0543'
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax_ 7041525-0409
Page 1 of 8

PRISMFLl1-Service Analytical &
Environmental Soluii.-ns
Sample Receipt Summary
06/1 1/2014
Prism Work Order: 4060041
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta Lime 4060041-01 Solid 06/02/14 06/02/14
Samples were received in good condition at 1.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 SpHridbrook Road - P.O. Box 240643 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001629-6364 - Fax: [phone] Page 2 of 8

Laboratory Report
F5B—"at S Fnvirunmr-ntal
Solutions
06/11/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta Lime
Attn: Andy Smith
Prism Sample ID: 4060041-01
P.O. Box 1111
Prism Work Order: 4060041
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/02/14 10:15
Time Submitted: 06/02/14 15:40
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
;_ ��••��
•+G.
y
v:iu6
ii.lvu
1 "SM264ii G 6;4V14 'i6:35
.iAG
r•,rvvoo
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1 *SM9221 E 6/3/14 10:05
MES
P41`0080
Total Metals
Mercury
0.14
mglkg dry
0.022
0.0073
1 *747113 6/4114 14:09
MEH
P411`0067
Arsenic
3-2 A
mglkg dry
2.9
0.42
10 *6010C 619114 13:05
BGM
P4F0033
Cadmium
BRLA
mglkg dry
2.9
0.027
10 *6010C 6/9114 13:05
BGM
04F0033
Copper
36 A
mglkg dry
5.7
0.072
10 *6010C 619114 13:06
BGM
P4F0033
Lead
25 A
mglkg dry
2.9
0.33
10 *6010C 619114 13:06
BGM
P4170033
Nickel
160 A
mglkg dry
11
0.093.
10 *6010C 619114 13.05
BGM
P411`0033
Selenium
BRLA
mglkg dry
5.7
0.69
10 *6010C 6/9/14 13:05
BGM
P4F0033
Zinc
58 A
mg/kg dry
29
0.20
10 *6010C 619114 13:05
BGM
P411`0033
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number:1-8001529-6364 -Fax: [phone] Page 3 Of 8

MM 1I FWI-Service t3iAnalytical &
{°nvirOnm9nSOl aliens
Level II QC Report
6/11114
City of Statesville, NC
Project: Stal-ime
Prism Work Order: 4060041
Attn: Andy Smith
Time Submitted: 6/2/2014
3:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike
Source
°/REC
RPD
Analyte
Result
Limit
Units
Level
Result
%REC
Limits
RPD
Limit Notes
Batch P41F0033 - 3050B
Blank (P4F0033-BLK1)
Prepared & Analyzed: 06/03/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS(P4F0033-BS1)--- - ----
- ---
- - - --
--- ---
Prepared
& Analyzed: 06/03114
------------
-- -
Arsenic
24.0
0.25
mg/kg wet
25.38
95
80-120
Cadmium
24.0
0.25
mg/kg wet
25.38
94
80-120
Copper
24.7
0.51
mg/kg wet
25.38
97
80-120
Lead
23.4
0.25
mg/kg wet
25.38
92
80-120
Nickel
23.7
1.0
mg/kg wet
25.38
93
80-120
Selenium
23.9
0.51
mg/kg wet
25.38
94
80-120
Zinc
23.7
2.5
mg/kg wet
25.38
93
80-120
Matrix Spike (P4F0033_MS1) -
Source 40 60041-01
Prepared:
06/03/14 Analyzed_ 06/09/14
Arsenic
30.5
2.9
mg/kg dry
29.26
3.20
93
75-125
Cadmium
24.9
2.9
mg/kg dry
29.26
0.125
85
75-125
Copper
62.7
5.9
mg/kg dry
29.26
35.2
94
75-125
Lead
49.7
2.9
mg/kg dry
29.26
25.3
84
75-125
Nickel
187
12
mg/kg dry
29.26
162
85
75-125
Selenium
18.9
5.9
mg/kg dry
29.26
BRL
64
75-125
MI
Zinc
86.8
29
mg/kg dry
29.26
57.8
99
75-125
Matrix Spike Dup (P4F0033-MSD1)
- Source:
4060041-01_
Prepared: 06/03/14 Analyzed_ 06/09/14
Arsenic
29.1
2.9
mg/kg dry
29.41
3.20
88
75-125
5
20
Cadmium
24.5
2.9
mg/kg dry
29.41
0.125
83
75-125
2
20
Copper
62.3
5.9
mg/kg dry
29.41
35.2
92
75-125
0.7
20
Lead
48.4
2.9
mg/kg dry
29.41
25.3
79
75-125
3
20
Nickel
185
12
mg/kg dry
29.41
162
77
75-125
1
20
Selenium
20.3
5.9
mg/kg dry
29.41
BRL
69
75-125
7
20 MI
Zinc
99.5
29
mg/kg dry
29.41
57.8
142
75-125
14
20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Full -Service al Solutions
s
imm RS
ti FnvironmenF�l Solulions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4F0033 - 3050B
Project: StaLime
Level II CSC Report
6/11/14
Prism Work Order: 4060041
Time Submitted: 6/2/2014 3:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Post Spike (P4F0033-PS1)
Source: 4060041-01
Prepared & Analyzed: 06/03/14
Arsenic
0.926
mg/L
1.000 0.112 81
80-120
MI
Cadmium
0.538
mg/L
1.000 0.00439 53
80-120
MI
Copper
1.60
mg/L
1.000 1.23 37
80-120
MI
Lead
1.03
mg/L
1.000 0.887 14
M120
MI
Nickel
3.81
mg/L
1.000 5.69 NR
80-120
MI
Selenium
0.874
mg/L
1.000 -0.264 114
80-120
MI
Zinc
2.29
mg/L
1.000 2.02 26
80-120
MI
Batch PV0067 - 7471 B
Blank (P4F0067-BLK1)
Prepared & Analyzed: 06/04/14
Mercury
BRL
0.020 mg/kg wet
LCS (P4F0067-BS1)
Prepared & Analyzed: 06/04/14
Mercury
0.413
0.019 mgikg wet
0.3906 106
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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y S gy I Full -Service Analytical &
a,e a. x fFf� �� Envi:onrncr.iaf Solutigns
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
6/11/14
Prism Work Order: 4060041
Time Submitted: 6/2/2014 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PV0083 - NO PREP
Blank (P4FD083-BLK1) Prepared & Analyzed: 06/04/14
-- - - -- — - ---- -- --- - - - ---- ----- ---- -- - --- . — ....... - - - —
% Solids 100 0.100 % by Weight
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Level II QC Report
1 � I Full -Service Analytical6/11/14
g L-'nviron menial Solutirns
City of Statesville, NC Project: Stal-ime Prism Work Order: 4060041
Attn: Andy Smith Time Submitted: 6/2/2014 3:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41F0080 - NO PREP
Blank (P4F0080-BLK1)
Prepared & Analyzed: 06/03/14
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial
Final Daterrime
4060041-01
P41=0033
2.03 g
50 mL 06/03/14 9:15
Prep Method: 7471B
Lab Number
Batch
Initial
Final DateTme
4060041-01
P41`0067
0.64 g
50 mL 06/04/14 10:10
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CHAIN F CUSTODY RECORD �� w0,11.fityIWk, m;�i�� � n�� �`�`1111.
�� yf
L`_ai`"1'��li'u'1,.,. '.ut9 t 4�'."ss"2 s K t+v
F ii ". iI I Full -Service Analytical & YES dC
�� �'� r Lnvironmenlcd Solutions PA3E_ tDF _ �fY®TE dk TO ENSURE PROPER BILLING: _ � —.._ _-___ _
ao
S n+.. p! s h r"'T cq . n riv " O
' ... .t , AMMArurucSINC.Receives OM 9JET ICI + .... ✓ _ ..- 00 l
Project Name:
49 SpringLronk Roan/ Charlotte, NC 2R21 i F(,Yr R, 1 F + >; FV4TI✓Ct� in.(i tech / _ .. �
Phone 704152ts-v364 Fax: 04,'525-04,09 Short Hold Analysis: (Yes) (No) US7 Project: (Yes) (NO) - (D r
*Please ATTACH any project specific reporting (QC LEVEL 1 Il III IV) c i', +'I Dill Nc DIr.IG TIN.- '- _ / ..___ —_. m
Client Company Name: C AX o` 5 �.tl�.s �. GLISTr�DYSt:1iL71�,TACT? r' 11 I
�—�1 g ¢�1 �pfi provisions and/or QC Requirements
Re ort To/Contact Name: F7ol4 Jra.4b I VOLATILE: raCUVV/JUTHEADi AGE?
p Invoice To•
Reporting Address: N 0 I'3.>t 919 jut C f a�Tnll L F used?
Address:
ail iLIiP ilrinitC°'✓t.._._L)bS Wren�� Cwr,ufi._f'�l(.___i
Phone. %�'f-b"78-.3'r.3' Fax es (No): 7J'y . 7Y- S'd S5 purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC_-DoD FL, NC
EDD Type: FD€=_Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Wpork Mlust Be
Q y ," SC OTHER N/A
Site Location Name: Fo �.. d'� °� �r'�-�-� T P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: �! :�.. f3r':1d i ar , u21C • Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO
r`� J (SEE REVERSE FOR TERMS CONDITIONS REGARDING SERVICES Sam le Iced Upon Collection: YES_ NO
-� Ca-t' {.`. S u• %J C. %W��: RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) h
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM
i / COLLECTED {SOIL, PRESERVA- REMARKS 1
CLIENT DATE i a r i / ' i'
T1VES /° i�i% LABSAMPLE DESCRIPTION COLLECTED I IUIILITAf2Y WATER OR *TYPE i ID NO.
NO. SIZE , ° i`/° HOURS --
SLUDGE) SEE BELOW
5�'a .d ',.�G 6 • a 1�1 I lit ➢,� �� 14a:4 S i:).5, I rr` �i s iBi" L:, e-Jdlg r S�;:w - a;
.`J C a °°e:�irr� j 6 'ot'i`7' �ti % ✓�:+2 I -` _ � t',` �—
`.ram
Sampler's Signature +I'Q Sampled By (Print Name) Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prised to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
l Receive By: (Signal r ) Date
ti
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC/ IL RECEIVED AT THE LABORATORY.
/U
❑ Fed Ex ❑ UPS ❑ Hand -delivered '� nsm Field Service ❑ Other
NPDES: US7: I GRNDllilATER: DRINKING WATER: j SOLID WASTE: I RCRA: I CERCLA LANDFILL OTHER:
❑ NC ❑ SCI Q NC ❑ SC j ❑ NC ❑ SC ❑ NC ® SC ❑ NC ❑ SC i ® NC ID SC: ❑ NC 13 SC ❑ NC ❑ SC ❑ NC ❑ SC
❑ I❑ I❑ __—' ❑ ❑ �❑ ❑ ❑ 1❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
��yaRE{ERS'FtF
ER S &;�6 MP..ITION..

NC Certification No. 402 SC Certification No. 99012 Case ase Narrative
iA� Full -Service Anal foal NC Drinking Water Cert No. 37735
y 06/23/2014
P
Environmental Solutions VA Certification No. 460211
yon,.mn,e, inc DoD FLAP: L-A-B Accredited Certificate No. L2307
ISOIIEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 06/16/2014
Statesville, NC 28687 Prism Work Order: 4060328
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
61- ?P111-
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Se-
E—rAnlytcalI Enwrnmeniidl s
Solutions
Sample Receipt Summary
06/23/2014
Prism Work Order: 4060328
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime
4060328-01 Solid 06/16/14 06/16/14
Samples were received at 29.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 2 of 8

Laboratory Report
+}�S—vicc Analytical 8 06/23/2014
Il
- I SJ '+� §1 environntenial Sql utions
City of Statesville, NC
Project: StaLime Client Sample ID: StaLime
Attn: Andy Smith
Prism Sample ID: 4060328-01
P.O. Box 1111
Prism Work Order: 4060328
Statesville, NC 28687
Sample Matrix: Solid Time Collected: 06/16/14 11:33
Time Submitted: 06/16/14 1525
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 69.0
% by
0.100
0.100 1
*SM2640 G 6/18114 16:46 MJO
P4F0334
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 6/17/14 11:25 JHB
P4F0340
Total Metals
Mercury
0.14
mg/kg dry
0.029
0.0098
1
*7471B
6117114 16:48
MEH
P411`0299
Arsenic
4.1
mglkg dry
3.6
0.62
10
*6010C
6119114 16:40
BGM
P4F0303
Cadmium
BRL
mglkg dry
3.6
0.034
10
*6010C
6119/14 16:40
BGM
P4F0303
Copper
35
mg/kg dry
7.1
0.090
10
*6010C
6/19114 16:40
BGM
P4F0303
Lead
14
mg/kg dry
3.6
0.42
10
*6010C
6/19M4 16:40
BGM
P4F0303
Nickel
200
mglkg dry
14
0.12
10
*6010C
6119114 16:40
BGM
P4F0303
Selenium
BRL
mglkg dry
7.1
0.86
10
*6010C
6119/14 16:40
BGM
P4F0303
Zinc
68
mglkg dry
36
0.24
10
*6010C
6/19114 16:40
BGM
PV0303
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 of 8

Level II QC Report
& Fuji -Service ! nzrytfcai 6123/14
�"` �'-'� I CnvironniE•ntai ;;r�i«iign5
City of Statesville, NC Project: StaLime Prism Work Order: 4060328
Attn: Andy Smith Time Submitted: 6/16/2014 3:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P4FO299 - 7471B
Blank (P4F0299-BLK1)
Prepared & Analyzed: 06/17/14
Mercury
BRL
0.021
mg/kg wet
LCS (P4F0299-BS1)
Prepared & Analyzed: 06/17/14
Mercury
0.354
0.020
mg/kg wet
0.4167 85
80-120
Matrix Spike (P4F0299-MS1)
Source: 4060328-01
Prepared & Analyzed: 06/17/14
Mercury
0.680
0.031
mg/kg dry
0.6470 0.143 83
80-120
Matrix Spike Dup (P4F0299-MSD1)
Source: 4060328-01
Prepared & Analyzed: 06/17/14
Mercury
0.657
0.031
mg/kg dry
0.6356 0.143 81
80-120 3 20
Batch P4FO303 - 3050B
Blank (134F0303-BLK1)
-- - ------- -- ---- - - ----- -----
_ - --- -- --- - -
-- - ------
Prepared & Analyzed: 06/17/14
- -- -- -----.._.-..---- --- ---
- ---- - - -- -- - - - -- -
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mglkg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mgikg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4F0303-BSI)
Prepared & Analyzed: 06/17/14
Arsenic
22.4
0.25
mglkg wet
25.13 89
80-120
Cadmium
22.2
0.25
mg/kg wet
25.13 89
80-120
Copper
23.9
0.50
mglkg wet
25.13 95
80-120
Lead
22.2
0.25
mg/kg wet
25.13 88
80-120
Nickel
22.2
1.0
mglkg wet
25.13 88
80-120
Selenium
22.3
0.50
mgikg wet
25.13 89
80-120
Zinc
22.6
2.5
mgikg wet
25.13 90
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-8001629-6364 - Fax: [phone] Page 4 of 8

e I S I Fuli-$ervicc Analytical
+....n. Environmental Solutions
Level II QC Report
6/23/14
City of Statesville, NC Project: Stal-ime Prism Work Order: 4060328
Attn: Andy Smith Time Submitted: 6/16/2014 3:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41F0303 - 3050B
Matrix Spike (P4F0303-MS1)
--- ----
Source: 4060328-01
-- -
Prepared: 06/17/14 Analyzed: 06/19/14
Arsenic
-
38.9
-- ---------
3.7
mg/kg dry
-- -
36.78
----
4.08
-
95
---------
75-125
--------
---- --
-
Cadmium
31.6
3.7
mg/kg dry
36.78
0.110
86
75-125
Copper
67.8
7.4
mg/kg dry
36.78
34.7
90
75-125
Lead
46.4
3.7
mg/kg dry
36.78
14.5
87
75-125
Nickel
236
15
mg/kg dry
36.78
197
107
75-125
Selenium
28.6
7.4
mg/kg dry
36.78
BRL
78
75-125
Zinc
99.8
37
mg/kg dry
36.78
67.9
87
75-125
Matrix Spike Dup (P4F0303-MSD1)
----- - - -..... -- ..-
Source:
--
4060328-01
------ -- ---------
Prepared: 06/17/14 Analyzed: 06/19/14
--._... ---- -
Arsenic
36.2
3.5
mg/kg dry
35.35
4.08
-----.--------._...
91
75-125
7
20
Cadmium
29.7
3.5
mg/kg dry
35.35
0.110
84
75-125
6
20
Copper
66.6
7.1
mg/kg dry
35.35
34.7
90
75-125
2
20
Lead
43.7
3.5
mg/kg dry
35.35
14.5
83
75-125
6
20
Nickel
213
14
mg/kg dry
35.35
197
46
75-125
10
20
MC
Selenium
23.4
7.1
mg/kg dry
35.35
BRL
66
75-125
20
20
MI
Zinc
103
35
mg/kg dry
35.35
67.9
100
75-125
3
20
Post Spike (P4F0303-PSI)
Source:
4060328-01
Prepared: 06/17114 Analyzed: 06/18/14
Arsenic
0.834
mg/L
1.000
0.115
72
80-120
MI
Cadmium
0.492
mg/L
1.000
0.00310
49
80-120
MI
Copper
1.42
mg/L
1.000
0.977
44
80-120
MI
Lead
0.715
mg/L
1.000
0.407
31
80-120
MI
Nickel
3.75
mg/L
1.000
5.53
NR
80-120
MC
Selenium
0.773
mg/L
1.000
-0.191
96
80-120
Zinc
2.18
mg/L
1.000
1.91
27
80-120
MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
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tzl Sol
I] I FUII-Service Analytical &
PRIS14Yt 5R Environ menution<
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch PV0334 - NO PREP
Blank (P4FO334-BLKI)
% Solids
Level II QC Report
6/23/14
Prism Work Order: 4060328
Time Submitted: 6/16/2014 3:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Prepared & Analyzed: 06/18/14
99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 8

d S I Full-Ser n al S.1 ti 8
4;� Fnviconmr-n ial Sol:.itir. ns
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
6/23/14
Prism Work Order: 4060328
Time Submitted: 6/16/2014 3:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41FO340 - NO PREP
Blank (P4FO340-BLK9) Prepared & Analyzed: 06/17/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Date/Time
4060328-01 P41`0303 2.04 g 50 mL 06/17/14 10:10
Prep Method: 7471E
Lab Number Batch Initial Final Date/Time
4060328-01 P41`0299 0.6 g 50 mL 06/17114 13:56
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RECORD
CHAIN OF CUSTODY
1�
earl
I S'ery ce Analytical C
Puti-
EnVlfOnm('ntal JO{LI il01'1S
PAGE_ OF 4lP+DT@ # TO EINSORE PROPER BALLING:
I
�amLl� IrI �
YE yC' I•.,',
✓�
co
�
0
a�. I
1A..11,11MES. INC.
_
I} h(JC IT BffIV91
Pecal� l u(I vLE f !r �,
_
ti
00
449 Springbrook Road Cimflotte, NC" 28217
Project Name
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
4 F r'top r�Cn
Phone [phone]A Fax.: [phone]
�4%"( H&E,
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
1: 'Rene \cu.J"TrII(t tiQLP(NG l"Iiv1L ?
___._ .._ _ _ '_
`
C
Client Company Name: 9 7' 'Syi
provisions and/or QC Requirements
CUSTODY OD SEALS INTACT?
Report To/Contact Name: h � �� .�,, : � �a
Invoice 70:
Val i II_G4+ rc c, r1r;OtiT i ,;DSPAc'?
_ ____
T
Reporting Address: Pal, go.'i 1111
i c.:.:r•!''P,II! �e
ivc
Address:
TL:JviP: rherll, l J: , i- at; arded:
_�_> �. , ;U.
Phone:iio l- US'- 343S' Fax es (No):;ld i°' ���"- �'�'+ � Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day © 2 Days 0 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC IDoi7
FL NC
EDD Type: PDF_Excel_Other "Working Days" O 6-9 Days ❑ Standard 10 days ❑ P Pre -Approved provMust Be SC OTHER
N/A
Site Location Name: F-.,4 +4j� C. ee. k Samples received after 14:00 will be processed next business day.
Site Location Physical Address: e9i° Bail rs•^ Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO
—
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample iced Upon Collection: YES_ NO
✓V a RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) _ p p NO —
ANALYSIS MATRIX SAMPLE CONTAINER i ANALYSIS REQUESTED
COLLECTED (SOIL, PRT VA i ' i /
/
PRISM
LAB
CLIENT DATE n / fit` ++ REMARKS
i
VE /!
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR "TYPE v / i%
NO. SIZE
ID NO.
14OURS SLUDGE) SEE BELOW
—
-!_1/
l ! &:3 i
�"
P
NAS a0 3 1
�y
��1
her, C e
k
_ a 1
i
CS
Fib
I
� C
I
I
i
,
I
�2 LG` ' Affiliation
Sampler's Signature Ji'a �i2!- �z'-�: Sampled By (Print Name) PFcz s' C _
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must bev`av1ge
submitted in writing to the Prism Project Manalger. There will be charges for any changes after analyses have been initialized.
Re ed B (Signature) 0 to Military/Hours
Relin shed By: (S gnalure) v Y ( 9 ) Additional Comments:
+ Si r
o .�fle Arrival iinle: 7
Re e d B Si nature Date
d B(Slgnalu.'e) Y� ( 9
Relinsl y:
.i rite Del.art:.;re rirnr;:
!__�
._._�...v_,..-._._,..__._....._. .._.... V
Ic( Te i .
Reli quis etl By: (Sign- ture) Received fgr Prism Lab rato as By: Date
^e. �— —
�l^
--- �
Method of Shipment: NOTE: ALL SAMPLE COOLER-S SHOULD BE TAPED SHUT WIi7H'CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Gaup No,
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST C C UNTIL RECEIVED AT THE LABORATORY. Tr 2 �(•j
......._.......,_»...e........_._-.,_...�.:,_......__,...._...,�.
V J
❑ Fed Ex ❑ UPS ❑ Hand-deliveredrism Field Service ❑ Other
NPDES: UST: GR UNDWVATEIR: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
r'
LINC❑SC El NC ®SCI ❑RC ❑SC El ❑SC I ®NC ❑SC Oa NCC9SC ®NC QSC ®NC El SC ]NC ❑SC
n n `
*CONTAINER TYPE CODES: A = Amber G = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (/-ero rleaD Space)

NC Certification No.Haase Narrative
SC Certification No. 990 99012 Aoo !i9
Full -Service Analytical & NC Drinking Water Cert No. 37735
f� L M Environmental Solutions VA Certification No. 460211 07/10/2014
LAnor,ATOR iEs. uic. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 06/30/2014
Statesville, NC 28687 Prism Work Order: 4070017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
1: � �L �_ I � C, - ( �
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting.Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 14

i Full -Service Analytical
i En vironmental Sokrticii
Sample Receipt Summary
07/10/2014
Prism Work Order: 4070017
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Sta-Lime
4070017-01
Solid
06/30/14
06/30/14
Sta-Lime
4070017-02
Solid
06/30/14
06/30/14
Sta-Lime
4070017-03
Solid
06/30/14
06/30/14
Sta-Lime
4070017-04
Solid
06/30/14
06/30/14
Sta-Lime
4070017-05
Solid
06/30/14
06/30/14
Sta-Lime
4070017-06
Solid
06/30/14
06/30/14
Sta-Lime
4070017-07
Solid
06/30/14
06/30/14
Samples were received at 30.6 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.Q. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 2 of 14

Laboratory Report
FR I S �� r i Elks ry Analytical &
¢ � � ,� I i Environmental Solutions 07/10/2014
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-01
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
-- ----- ---
— — --
Solids 96-3
/ by
0.100
0.100 1
*St612540 G 7/2114 14:30 JAB
P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/100
1
1
*SM9221 E 7/1/14 13:19 JHB
P4G0052
mL
Total Metals
Mercury
0.38
mg/kg dry
0.021
0.0035
1
*7471B
718/14 15:47
MEH
P4G0088
Arsenic
1.3
mg/kg dry
0.78
0.11
3
*6010C
7/10/14 12:02
MEH
P4G0051
Cadmium
BRL
mg/kg dry
0.78
0.0074
3
*6010C
7/10/14 12:02
MEH
P4G0051
Copper
38
mglkg dry
1.6
0.020
3
*6010C
7/10114 12:92
MEH
P4130051
Lead
10
mg/kg dry
0.78
0.091
3
*6010C
7110114 12:02
MEH
P4G0051
Nickel
110
mglkg dry
3.1
0.025
3
*6010C
7110114 12:02
MEH
P4G0051
Selenium
BRL
mg/kg dry
1.6
0.19
3
*6010C
7/10/14 12:02
MEH
P4G0051
Zinc
82
mg/kg dry
7.8
0.053
3
*6010C
7110114 12:02
MEH
P4G0051
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: 704152"409 Page 3 of 14

FUlI-Service Analytical Jx
Eniiro n:rent:�l Sold iicns
Laboratory Report
07/10/2014
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-02
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 86.9 % by DA00 0.100 1 "SM2540 G 712114 14:30 JAB P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/100 1 1 'SM9221 E 7/1114 13:19 JHB P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P_O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 14

I Laboratory Report
P R S
Full -Service Analytical &
Enrvironniental Solutions 07/10/2014
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-03
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 92.3
% by
0.100
0.100 1
`SM2540 G 7/2114 14:30 JAB
P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/100
1
1
'SM9221 E 7/1114 13:19 JHB
P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 14

Fu II p R I p� I ll-Seniice Analytical &
(�® '� �' n Er�vironm�m al Solulr�n=_
Laboratory Report
07/10/2014
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4070017-04
P.O. Box 1111 Prism Work Order: 4070017
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 90.2 % by 0.100 0.100 1 `SM2640 G 7/2/14 14:30 JAB P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/100 1 1 "SM9221 E 7/1/14 13:19 JHB P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O_ Box 240543 - charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number 1-800/629-6364 - Fax: [phone] Page 6 of 14

Laboratory Report
Ir illl-.c. r:l'VIC3
Analyti—I E
c� Erc ironmental
Soluliors
07/10/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4070017-05
P.O. Box 1111
Prism Work Order: 4070017
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
%Solids
88.3 % by
0.100
0.100 1 "SM2640 G 7/2H4 14:30 JAB P4G0043
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/100
1
1 'SM9221 E 711/14 13:19 JHB P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P-O- Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 14

P I S p�, pp I Full -Service Analytical s
5� � Ercaironmantal Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Sample Matrix: Solid
Laboratory Report
07/10/2014
Client Sample ID: Sta-Lime
Prism Sample ID: 4070017-06
Prism Work Order: 4070017
Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 92.9 % by 0.100 0.100 1 `SM2540 G 712114 14:30 JAB P4G0043
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN1100 1 1 "SM9221 E 7/1114 13:19 JHB P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 14

Laboratory Report
Full -Service
Analytical &
_ _ 99Environmantal
I S M i
Solutions
07/10/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4070017-07
P.O. Box 1111
Prism Work Order: 4070017
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/30/14 14:34
Time Submitted: 06/30/14 16:40
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
87.6 % by
0.100
0.100 1 *SM2640 G 712/14 14:30 JAB
P4G0043
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/100
1
1 *SM9221 E 711114 13:19 JHB
P4G0052
mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 14

y' j Fulliron-vice : nalyticml s
� .✓' I Y�' Environmental Soltilirn
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4G0051 - 30Sma
Project: StaLime
Level II QC Report
7/10/14
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P4G0051-BLK1)
Prepared: 07/03/14 Analyzed: 07/08/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4G0051-BS1)
-- - ----- - --- - -
--- ---- - -
- -- - ---- -
- -- --
Prepared: 07/03/14 Analyzed: 07/08/14
-- ------
Arsenic
23.5
0.25
mg/kg wet
25.00 94 80-120
Cadmium
23.8
0.25
mg/kg wet
25.00 95 80-120
Copper
24.5
0.50
mg/kg wet
25.00 98 80-120
Lead
23.1
0.25
mg/kg wet
25.00 92 M120
Nickel
23.5
1.0
mg/kg wet
25.00 94 80-120
Selenium
23.7
0.50
mg/kg wet
25.00 95 80-120
Zinc
24.0
2.5
mg/kg wet
25.00 96 80-120
Duplicate (P4G0051-DUP1)
-- --------- - -- -- -- - -- --
Source: 4070017-01
- - --- --- -- --------- ---- -
Prepared: 07/03/14 Analyzed: 07/10/14
--- _----
Arsenic
1.41
0.78
mg/kg dry
1.34
5
200
Cadmium
0.236
0.78
mg/kg dry
0.193
20
200
Copper
40.8
1.6
mg/kg dry
38.3
6
200
Lead
10.3
0.78
mg/kg dry
10.1
2
200
Nickel
105
3.1
mg/kg dry
108
3
200
Selenium
BRL
1.6
mg/kg dry
BRL
200
Zinc
90.8
7.8
mg/kg dry
81.8
10
200
Matrix Spike (P4G0051-MS1)
Source: 4070017-01
Prepared: 07/03/14 Analyzed: 07/10/14
Arsenic
25.2
0.79
mg/kg dry
26.23 1.34 91 75-125
Cadmium
19.7
0.79
mg/kg dry
26.23 0.193 74 75-125
Copper
60.8
1.6
mg/kg dry
26.23 38.3 86 75-125
Lead
28.9
0.79
mg/kg dry
2623 10.1 72 75-125
Nickel
123
3.1
mg/kg dry
26.23 108 55 75-125
Selenium
16.1
1.6
mg/kg dry
26-23 BRL 61 75-125
Zinc
102
7.9
mg/kg dry
26.23 81.8 77 75-125
BH
MI
MI
MI
MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-8001629-6364- Fax: [phone] Page 10 of 14

P p_1 1 pt I Full -Service al S.I lio s
I t � Environmcr„al Solutions
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
7/10/14
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4G0088 - 7471 B
Blank (P4GO088-BLK1) _ Prepared: 07/07/14 Analyzed: 07/08/14
Mercury BRL 0.021 mg/kgwet
LCS (P4GO088-BSI) — - Prepared: 07/07/14 Analyzed_07/08114
Mercury 0.479 0.020 mg/kg wet 0.4167 115 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-800/529-6364 - Fax: [phone] Page 11 of 14

Fui[-Se—ice Analytical &
pf--"�"Iflsm Icnvi:onrnrnial Solutions
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level ll QC Report
7/10/14
Prism Work Order: 4070017
Time Submitted: 6/3012014 4:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPID Limit Notes
Batch MG0043 - NO PREP
Blank (P4G0043-BLKI) Prepared & Analyzed: 07/02114
% Solids 99.8 0.100 %byWeight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 14

"@ -y I ,� Y � � I Full -Service Analytical &
SKSK-�" o".y>', EEF iWW! 6R Environmer•ial SoWUors
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
7/10/14
Prism Work Order: 4070017
Time Submitted: 6/30/2014 4:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P400062 - NO PREP
Blank (P4G0052-BLK1) Prepared & Analyzed: 07/01/14
Fecal Col'dorms BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final DateTme
4070017-01 P4G0051 2.02 g 50 mL 07/03/14 8:45
Prep Method: 7471B
Lab Number Batch Initial Final DatelTime
4070017-01 P4G0088
0.59 g 50 mL 07/07/14 11:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-8001529-6364 - Fax: [phone] Page 13 of 14

m; _.. f� I Full -Service: PAnalytical &
r Is
� I Environmental
nvironmeal Solutions
e�
.-� •v ,.,,,.? -.Z:'• I.AHOHATORIES, INC.
449 Sprhtgbrook Road ° Charlotte, 1,1t: 28217
Phone [phone] Fax: 70,14525-0403 yd
Client Company Name:
Report To/Contact Name A n S ,r
Reporting Address: P. 0. 21 j —
O i 1 91,s its l"I
s r � � � �� - M,w. r , ,•.y ^t �, � � .,, � ,, �� bra ¢!�y
PAGE_ OF — QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 11 I11 IV)
provisions and/or QC Requirements
Imrnire Tn'
Address:
an.pl�-,:� ir; IF,.C' f utis�p 2rsivell'i
i i cei� �l UI f'C� iCE?,
f-RCPER PRESET NA,- IIVES u[n(;,,ate
occived WITHIN HOLDING 111VIE ?
VOOVFILES rec'd 0.10UT HEA(.'1SPACE?
,(Ipfl t ol'lT41CIFFps .ia
rru 0_ t i 9 C bsc.rv., d:
??n'S','; i eii`ff.'i`ifi'E,nygrA36'4.�40+3 tYkS
Nr
.
O
!
_ -
4{
Phone: 7J q-°a Fax ((es No):'�dl�' '� j`� Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel Other "Working
Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be pproved SC OTHER
N/A
Site Location Name: E.)u r'-_ j, Samples received after 14:00 will be processed next business day.
�qj B I Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO_
Site Location Physical Address: e
d
-e3ar+. t'S 6'✓ �9 C� Air
. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Ort Sample Iced t.I Collection: YES N®
ant RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p Ig NO —
TIME MATRIX
CLIENT DATE COLLECTED (SOIL,
ANALYSIS REQUESTED
SAMPLE CONTAINER i / / PRISM
PRE
A ( / / y��� / / REMARKS i LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
VE3 g
'TYPE NO. SIZE �'i�g� / s /l
ID NO.
HOURS SLUDGE)
SEE BELOW
�'a'- ✓� � t'>'��f�'� Ili:. .
IVA � !� S I �°J ��
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Sampler's Signature /1 1rc ��.✓� �r_ Sampled By (Print Name) lax LP�y9�'8 Cie Affiliation
a '
Upon relinquishing, this Chain Of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
ash"xs��"4 tiro �^ T� Y
submitted in writing to the Prism Project Manager. There will be c
es for any changes after analyses have been initialized'
f"
Helin ished By: (Signature O . - Recei a By: (Signature) Date Military/Hour Additional Comments:
_
'
I
Site Arrival riiiie.:
J_._...;
Rele / a By: (Signature) u Re a(Signature)
Date
Site G p Irtt.li Ln`ir3:, W
Relin wished By: (Sign Received
For Pri m Laborator' V By: Date
of Shipment: NOTE: ALL SAMPLE C OLERS SHOU LD BE TAPED SHUT WITH Cj15,/BODY SEALS FOR TRANSPORTATION TO THE LABORATORY. CDC Gro�Sp No.
M�Fad
•--••-^--•^•- •�^ —--.,•,_�--..•�.
SAMPLES ARE NOT EPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
'i.
❑Ex L7 UPS ❑ Hand -delivered Pr m Field Service D Other
NPDES: I UST: GRQ DINATER: DRINKINGWATER: SOLIDWASTE: j RCRA: CERCLA LANDFILL OTHER:
❑❑NC ❑SC
_
0
w o o ~s
❑NC❑SC [INC ❑SC I U C ❑SC I ®NC C] SC
®NC C] SC i ❑❑NC❑SCi ®NC ❑SC ®NC ❑SCI
111111
*CONTAINER TYPE CODES: A = Amber C :: Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile OrganiCS Analysis (/-ero rleaa bpace)

NC Certification No.9402
90 Case Narrative
SC Certification No. 99012
R0 1 Fuli-Service Analytical & NC Drinking Water Cert No. 37735 07/24/2014
' A Environmental Solutions VA Certification No. 460211
;;.eo: kio ies. in DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Quarterly Parameters)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/14/2014
Statesville, NC 28687 Prism Work Order: 4070262
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Blank Spike recovery is greater than the control limit due to carryover. Results should be considered an estimate
with high bias.
Aa Method Blank is greater than the reporting limit due to carryover. Results should be considered an estimate with
high bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative. Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 10

y Sample Receipt Summary
PRISM
''``��
I S ��6 � I F_n'di �nmenial So ; ins 07/24/2014
Prism Work Order: 4070262
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime
4070262-01 Solid 07/14/14 07/14/14
Samples were received in good condition at 2.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 10

.. nuoenaouies. . Seie &
Laboratory Report
cnvironmcntalSolulions 07/24/2014� M_IFu-
we
City of Statesville, NC Project: StaLime (Quarterly Client Sample ID: StaLime
Attn: Andy Smith Parameters) Prism Sample ID: 4070262-01
P.O. Box 1111 Prism Work Order: 4070262
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/14/14 12:40
Time Submitted: 07/14/14 15:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
910
mg/kg
160
13
2
*Calculation
7/23114 8:01
CLB
1CALC]
Solids
65.6
% by
0.100
0.100
1
*SM2640 G
7116114 15:10
JAB
P4G0235
Weight
Nitrate/Nitrite as N
54
mg/kg dry
9.0
0.99
1
*SM4500-NO3 F
7122114 9:13
CLB
P4G0346
Phosphorus -Total
3100
mg/kg dry
90
19
20
*SM4500-P F
7122114 13,44
JAB
P41G0299
Total Kjeldahl Nitrogen
6200
mglkg dry
900
76
2
*351.2
7123114 8:01
CLB
P4G0361
Ammonia as N
150
mglkg dry
9.0
2.2
1
*SM4500-NH3 G 7/21114 9:31
CLB
P460257
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.4
1
*SM9221 E
7/15/14 12:33
JHB
P4G0285
Total Metals
Mercury
0.38
mg/kg dry
0.037
0.0060
1
*7471B
7118114 11:45
BGM
P4G0268
Arsenic
6.5
mg/kg dry
4.4
0.64
10
*6010C
7118114 1:46
BGM
P4G0273
Cadmium
BRL
mg/kg dry
4.4
0.042
10
*6010C
7/18/14 1:46
BGM
P4G0273
Copper
310
mglkg dry
8.8
0.11
10
*6010C
7118114 1:46
BGM
P4G0273
Lead
100
mg/kg dry
4A
0.51
10
*6010C
7MB114 1:46
BGM
P4G0273
Nickel
630
mg/kg dry
18
0.14
10
*6010C
7118114 1:46
BGM
P4G0273
Potassium
4200
mg/kg dry
220
14
10
*6010C
7/18/14 18:56
BGM
P4G0273
Selenium
BRL
mg/kg dry
8.8
1.1
10
*6010C
7118/14 1:46
BGM
P4G0273
Sodium
570
mglkg dry
220
2.0
10
*6010C
7118114 18:56
BGM
P4G0273
Zinc
66
mg/kg dry
44
0.30
10
*6010C
7MB114 18:56
BGM
P4G0273
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 of 10

...-PRISM I Full -Service :n2ly tical &
E m�ironmen.al Sohrticns
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control ,
Analyte
Project: StaLime (Quarterly Parameters)
Level II QC Report
7/24/14
Prism Work Order: 4070262
Time Submitted: 7/14/2014 3:45:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4C-0268 - 7471 R
Blank (P4G0268-BLKI)
Prepared: 07/17/14 Analyzed: 07/18/14
Mercury
BRL
0.020
mg/kg wet
LCS (P4G0268-BSI)
Prepared: 07/17/14 Analyzed: 07/18/14
Mercury
0.471
0.020
mg/kg wet
0.4167 113 80-120
Batch P4GO273 - 3050B
Blank (P4GO273-BLK1)
Prepared & Analyzed: 07/17/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
9.96
2.5
mg/kg wet
Aa
LCS (P4G0273-BSI)-
-
Prepared &Analyzed: 07/17/14
Arsenic
24.2
0.25
mg/kg wet
25.00 97 W120
Cadmium
24.2
0.25
mg/kg wet
25.00 97 80-120
Copper
26.1
0.50
mg/kg wet
25.00 104 80-120
Lead
24.0
0.25
mg/kg wet
25.00 96 80-120
Nickel
24.1
1.0
mg/kg wet
25.00 96 80-120
Potassium
495
12
mg/kg wet
500.0 99 80-120
Selenium
24.5
0.50
mg/kg wet
25.00 98 80-120
Sodium
450
12
mg/kg wet
500.0 90 80-120
Zinc
33.7
2.5
mg/kg wet
25.00 135 80-120 A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone:[phone] -Toll Free Number:1-8001529-6364 - Fax: [phone] Page 4 of 10

�y I �� � I Full -Sera n al Soy tia &
u"" yf7 �' Environmentzl So:utiors
Level II QC Report
7/24/14
City of Statesville, NC Project: Stal-ime (Quarterly Parameters) Prism Work Order: 4070262
Attn: Andy Smith Time Submitted: 7/14/2014 3:45:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P4GO235 - NO PREP
Blank (P4GO235-BLK7)
Prepared & Analyzed: 07/15/14
% Solids
99.9
0.100 % by Weight
Batch P41130257 - NO PREP
Blank (P4GO257-BLKI)
Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N
BRL
5.0 mg/kg wet
LCS (P4G0257-BS1)
Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N
124
5.0 mg/kg wet
125.0 100 80-120
Matrix Spike (P4GO257-MSI)
Source: 4070262-01
Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N
302
9.0 mg/kg dry
224.8 146 70 80-120 MI
Matrix Spike Dup (P4GO257-MSD1)
Source: 4070262-01
Prepared: 07/17/14 Analyzed: 07/21/14
Ammonia as N
297
9.0 mg/kg dry
224.8 146 68 80-120 1 20 MI
Batch P4GO299.- SM4500-PB5
Blank (P4GO299-BLK7)
Prepared: 07/18/14 Analyzed: 07/22/14
Phosphorus -Total
BRL
2.5 mg/kg wet
LCS (P4GO299-BSI)
Prepared: 07/18/14 Analyzed: 07/22/14
Phosphorus -Total
109
2.5 .mg/kg wet
100.0 109 90-110
Matrix Spike (P4GO299-MS1)
-- -- — - -- -- — --
Source: 4070262-01
_.- — ---- —
Prepared: 07/18/14 Analyzed: 07/22/14
-- - - -
Phosphorus -Total
3600
--
90 mg/kg dry
------------- — -- ---
179.9 3110 272 80-120 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 5 of 10

I Full -Service Analytical &
PRISMEnrnen.ai Solutions
Level 11 QC Report
7/24114
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 4070262
Attn: Andy Smith Time Submitted: 7/14/2014 3:45:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit units Level Result %REC Limits RPD Limit Notes
Batch P4GO-299 - SM4500-PB5
Matrix Spike Dup (P4G0299-MSDI) Source: 4070262-01 Prepared: 07/18/14 Analyzed: 07/22114
Phosphorus -Total 3530 90 mg/kg dry 179.9 3110 230 80-120 2 20 MC
Batch P4GO346 - NO PREP
Blank (P4G0346-BLK1)
Prepared & Analyzed: 07122/14
Nitrate/Nitrite as N
BRL 5.0
mg/kg wet
LCS JPIG_"36-BSjj
Prepared &Analyzed: 07/22114
Nitrate/Nitrite as N
49.2 5.0
mg/kg wet
50.00 98 80-120
Matrix Spike (P4G0346-MS1)
Source: 4070262-01
Prepared & Analyzed: 07/22/14
Nitrate/Nitrite as N
145 9.0
mg/kg dry
89.93 537 101 80-120
Matrix Spike Dup (P4G0346-MSDI)
Source: 4070262-01
Prepared & Analyzed: 07/22114
Nitrate/Nibite as N
146 9.0
mg/kg dry
89.93 517 103 80-120
Batch P4GO361 - 351.2
Blank (P4GO361-BLKI).
Prepared: 07/22/14 Analyzed: 07/23/14
Total Kjeldahl Nitrogen
BRL 25
mg/kg wet
LCS (P4G0361-BSI)
Prepared: 07122/14 Analyzed: 07123/14
Total Kjeldahl Nitrogen
508 100
mg/kg wet
500.0 102 90-110
Matrix Spike (P4G0361-MSI)
-------
Source: 4070262-01
---
Prepared: 07/22/14 Analyzed: 07/23/14
Total Kjeldahl Nitrogen
14600 2200
mg/kg dry
8993 5180 105 90-110
0.7 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 10

Se-i
g I FUII ronmee l;�iAnalytical %
q. e Fhvirormenlal Saicns
Level 11 QC Deport
7/24/14
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 4070262
Attn: Andy Smith Time Submitted: 7/14/2014 3:45:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4GO361 - 351.2
Matrix Spike Dup (P4G0361-MSD1) Source: 4070262-01 Prepared: 07/22/14 Analyzed: 07/23/14
Total Kjeldahl Nitrogen 12600 2200 mg/kg dry 8993 5180 82 90-110 15 20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 7 of 10

Level II QC Report
PMJ
q� t �t� I Full -Service Analytical & 7124114
x Environmental SOIUticns
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 4070262
Attn: Andy Smith Time Submitted: 7/14/2014 3:45:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4GO285 - NO PREP
Blank (P4GO285-BLK1) Prepared & Analyzed: 07/15/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final DateTme
4070262-01 P4G0361 0.05 g 25 mL 07/22/14 10:30
Prep Method: SM4500-PB5
Lab Number Batch Initial Final Daterrime
4070262-01 P4G0299 1 g 50 mL 07/18/14 14:38
Prep Method: 3050E
Lab Number Batch Initial Final Date/Time
4070262-01 P4G0273 2.05 g 50 mL 07/17/14 15:26
4070262 01 P4G0273 2.05 g 50 mL 07/17/14 15:26
Prep Method: 7471B
Lab Number Batch Initial Final Date/rime
4070262-01 P4G0268 0.59 g 50 mL 07/17/14 10:21
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 0f 10

CHAIN OF CUSTODY `dffl' F9 �:L
TTM lit 1.z,�'n`t Yi^Y A ,�A' ed r'
^'+ 4 'p i1j.'t1 TA'1uGY 15,
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Full -Service Analytical &
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PAGE OF QUOTE a To ENSURE PROPER BILLING-
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Project Name:
R@tir iv d, ON, +vr ICE' _
rn
449 Springhrook Roiid - Charlotte, N C 282-i r'
7041 �.
Short Hold Analysis: (Yes) (No) UST Project: (Yes)
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Phone [phone]i!. • Far: -0409
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"Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV}
I � v ri t n rHlti IiL L[l I Ir nrArS? � _ _
r al IM ;A c
c»
Client Company Name: o�
provisions and/or QC Requirements
CU IJI s:
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Report To/Contact Name: A n Ry � do i �1 l-',
Invoice To:
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Reporting Address: P 'Ved d
Address:
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TEMP: lit rn u j 1 ll t?bsened. ( ,lr
Ph,one:7011- M-313 "7 Fax Yes (No): !70-V-r3r1S- 34,55 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date �:] 1 Day O 2 Days ❑ 3 Days ❑ 4 Days Q 5 Days Certification: NELAC DoD FL NC
EDD Type: PDF_Excel Other "Working Days" 0 6-9 Days ❑ Standard 10 days Fj Rush
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—� SG OTHER N/A
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Site Location Name- F, : T'U "b � � � � `` t° �' r P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: Off 94'• d Far;;1? Turnaround time is based on business days, excluding weekends and holidays, Water Chlorinated: YES_ NO-
�,p y (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YEor's NO -
G3 3t1 RENDERED BY PRISM LABORATORIES, INC, TO CLIENT) p p -
ANALYSIS
TIIViE MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
/ / PRISM
CLIENT DATE COLLI=CTED, SOIL, PRESERVA- % "ea / /�
( — TIVES ' �:" e�, j / i REMARKS LAS
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR ; TYPE ID NO,
HOURS SLUDGE) ! SEE BELOW NO. SIZE�i0
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Sampler's Signature /T a ^ '' Sampled By (Print Name) , 4"1 o s0/, Affiliation
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Upon relinquishing, this Chain of Custodyis our authorization for Prism to roceed with the analyses as requested above. Any changes must be
' y p Y q g ! �` „
�A'D letma4!:kt3,,+'irk+,}t_i
submitted in writing to the Prism Project Manager. There will be charg for aqy anges after analyses have been initialized. E ".;
Roll i^hod ey, (Signa vra) �. Recai d 8 •(;Signature to Mi a� !fours Additional Comments I S Ito \ v i f
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41
Method of Shipment: NO : ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH GUSTO SEALS FOR TRANSPORTATION TO THE LABORATORY. OC ur up W. ----•-----• -• ••-----•••-----•--------••--!
• ,s MALES ARE N,�T AgCEPTED AND VERIFIED AGAINST CDC UNTIL EIVED AT THE LABORATORY.
J�
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❑ FedOHond-delivered ' J Prism Field Service 0 Other
6`dPDES: I UST: G 07UNDWATEF2: I DRINKING WATER- SOLID WASTE: I RCRA; I CERCLA LANDFILL ;OTHER:
�
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1 r, n F1 r9 ® Q
*CONTAINER TYPE TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

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Project Name:
Short {3ole� Analysis: (Yes) (Gtie7) ii`�T PYOjeCT: (Yes) ({',O)
PROF�Et? t'RE S!-t11/ATlV�� u'rc'Ic ttzd%
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*Please ATTACH any project specific reporting (QC LEVEL1 11 H11 M
Re@� v d WITHIN HO(:DING'THAES?
GU�1 F,Lti
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Client Company Narne:
provisioris and/or CIC Requirements
t')DY SI INTACT.'r
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invoice To;
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-
CONTAINERS u ed'? ;
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Reporting Address:OROPER
Address;
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Phone: Fax (Yes) (No):. Purchase Order No./Billing Reference
Email (Yes) (No) Email eQ ddre:ss Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
EpDD Type: P(OP— Excel _Other "Wortcing Days" a 6-9 Days ❑ Standard 10 days ❑ Rush Work Must B
Pre -Approved
Site Location Narne: Samples received after 15:00 will be processed next business day,
Turnaround time is based on business days, excluding weekends and holiday
Site Location Physical Address:
(SEE REVERSE FOR TERMS L+ CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC, TO CLIEN1y
CLIENT I DATE
SAMPLE DESCRIPTION COLLECTED
TIMEi Mr Rix SAMPLE CONTAINER
COLLECTED (SOIL, PRESERV.A-
MILITARY i WATER OR "TYPE TIVES
HCURS SLUDGE) SEE BELOWNO. SIZE
i
I
Sampler's Signature �l `—' �g% �w��( ---i Sampled By (Print Name) _
Upon relinquishing, this Chain of Custody is hour authorizations for Prism to prod
submitted in writing to the Prism Project Manager. There will be charges for am c
R,IJJquished By: (Sigualure✓)Received By: (Signatu )'
Relic q ished By: (Signature) Received By: (SignatLPr
L0
O
TO SWILLED IN BY CLIENT/SAI` FLING PERSONNEL
O ifilcStion: NELAO USAGE FL NO_
e
SC; OTHER N/A
QValter Ch!.Irinated: YES_ NO_
Samoa lced Upon Collection: YES NO
ANALYSES REOLIESTED
pRlSPA
REMARKS
LAB
ICE NO.
Affiliation
as requested above. Any changes must lie
:s have been initialized. e
11
VU �, all IPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC U1dT C RECEIVED AT THE LABORATORY. I
//{ ll
❑ Fcd E>:'•-••@"UPS ❑ Hand -delivered ❑ Prism Field Sort ice ❑ Other ✓ ,
NPDES: i LIST: GROUNDMIATER: ' OPINKBNGVIJATIER: SOLID WASTE: I RC:RA: 1 GERCLA I_nwimDPiLL OTHER:
❑ , I ❑ NC ❑ 5C IVC a SCI LJ SC
❑ NC SC NC ❑ SCSC � �1C CSC n NCSCNC FJ SCONC ❑
*C NTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
0
Additional Comments;

NC Certification No. 402 ��9'r�$6��
SC Certification No. 99012 Case N
. r Fuii-Service Analytical & NC Drinking Water Cert No. 37735
08/11/2014
L nvironmental Solutions VA Certification No.460211
E
�t.rs->naTo.,ie... rlc- DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/30/2014
Statesville, NC 28687 Prism Work Order: 4070590
This data package cunicaiii5 the analytical Icauiw Ivl ulc PrvjcCi iucnuucu cwvvc and nn..lucw u ..a.ze Na.—a.. amp!..
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0543 71
Phone: [phone] - Toil Free Number:1-8001529-6364 - Fax: [phone] Page 1 of 7

FRg Full-Scrvicn Flnalyticzil F.
q Environmental Solutio rls
Sample Receipt Summary
08111 /2014
Prism Work Order: 4070590
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime 4070590-01 Solid 07/30/14 07/30/14
Samples were received in good condition at 5.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrbok'Road- P_O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
Full -Service
P.nalytical 8.
PRISMElmroomentai
solutions
08/11/2014
City of Statesville, NC
Project: StaLime
Client Sample ID: StaLime
Attn: Andy Smith
Prism Sample ID: 4070590-01
P.O. Box 1111
Prism Work Order: 4070590
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
o Sbiius
i"o.o
in by
0.90u
u.-iuv
'i `SiM2540G iiiii'i4'i4AS
jAE
P-11.1".
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 7/31/14 13:12
JHB
P4H0023
Total Metals
Mercury
0.15
mgikg dry
0.029
0.0048
1 *747113 8/6114 13:07
MEH
• P4H0071
Arsenic
1.6
mglkg dry
1.0
0.16
3 "6010C 815114 19:28
BGM
P4H0011
Cadmium
BRL
mg/kg dry
1.0
0.0097
3 *6010C 8/5/14 19:28
BGM
P41-10011
Copper
31
mg/kg dry
2.0
0.026
3 *6010C 815N4 19:28
BGM
P4H0011
Lead
15
mglkg dry
1.0
0-12
3 *6010C 815114 19:28
BGM
P4H0011
Nickel
82
mg/kg dry
4.1
0.033
3 *6010C 8/5114 19:28
BGM
P4H0011
Selenium
BRL
mg/kg dry
2.0
0.25
3 *6010C 815114 19:28
BGM
P4H0011
Zinc
74
mg/kg dry
10
0.669
3 *6016C 815114 19:28
BGM
P4H0011
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 "Springbrook`Road - P-0. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3 of 7

Level II CSC Report
Rrt!-Service Analytical &
8/11/14
I S Envi-.nn'-,ntai Solutions
City of Statesville, NC Project: Stal-ime Prism Work Order: 4070590
Attn: Andy Smith Time Submitted: 7/30/2014 5:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4H0011 - 3050B
Blank (P4H0011-BLKI)
Prepared: 08/01/14 Analyzed: 08/05/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
025
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
2.96
2.5
mg/kg wet
BH
LCS (P41-10011-BSI)
—
-- --- -
Prepared: 08/01/14 Analyzed: 08/05/14
- - --- — --------
Arsenic
21.6
0.26
mg/kg wet
25.51 85 80-120
Cadmium
21.7
0.26
mg/kg wet
25.51 85 80-120
Copper
24.5
0.51
mg/kg wet
25.51 96 80-120
Lead
21.6
0.26
mg/kg wet
25.51 85 80-120
Nickel
22.0
1.0
mg/kg wet
25-51 86 80-120
Selenium
21.6
0.51
mg/kg wet
25.51 85 80-120
Zinc
23.9
2.6
mg/kg wet
25.51 94 80-120
Batch P4H0071 - 7471B
Blank (P41-110071-BLK1) Prepared: 08/05/14 Analyzed: 08/06/14
Mercury BRL 0.020 mg/kg wet
LCS (P41.10071-BSI) Prepared: 08/05/14 Analyzed: 08/06/14
-- — ------ __ ----- ---- --
Mercury 0.400 0.019 mg/kg wet 0.3906 102 M120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springlirook Road - P.O: Box 240543 _ Charloffe, NC 28224-0543-
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: 704I525-0409 Page 4 of 7

P`{, Fuli-Ser•✓ice .Analytical 3
e p i I°nvironmeni2i SOIWIOns
City of Statesville, NC Project: StaUme
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Deport
8/11114
Prism Work Order. 4070590
Time Submitted: 7/30/2014 5:10:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4FI0019 - NO PREP
Blank (P4110019-BLK1) Prepared & Analyzed: 08/01/14
% Solids 100 0.100 % by Weight
Duplicate (P4M0019_DUP'I) _ Source 4070590_01 Prepared &Analyzed_ 08/01/14
% Solids 68.0 0.100 % by Weight 73.6 8 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, -Inc.
449 Springbrook'Road P.O. Box 240543 - Charlotte, NC 28224-0543 -
Phone: [phone] - Toil Free Number: 1-800/529-6364 - Fax: [phone] {�BCJe J Of 7

Full -Service Analytical R
P R I S M Solutin,
7
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality. Control
Analyte
Project: StaLime
Level 11 QC Report
8/11114
Prism Work Order: 4070590
Time Submitted: 7/30/2014 5:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4HOO23 - NO PREP
Blank (P4H0023-BLK1)
Prepared & Analyzed: 07130/14
Fecal Coliforms
BRL
0.2 MPN1g wet
Sample Extraction Data
Prop Method: 3050E
Lab Number Batch
Initial
Final Date/Time
4070590-01 P41-1001 1
2.01 g
50 mL 08/01/14 9:30
Prep Method: 7471B
Lab Number Batch
Initial
Final Date/Time
4070590-01 P41-10071 0.56 9 50 mL 08105/14 10:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc-
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: 704t529-6364 -Toll Free Number: 1-800/529-6364 -Fax: [phone] Page 6 of 7

Sampler's Signature /-i5eW, Sampled By (Print
Upon relinquishing, this Chain of Custody is y0Ur authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be chat,ges for . any changes after analyses have been Initialized.
'
`
Relinquished (Signature, IN,
-nt: :U 6HUT VV'ITH C DY SEALS FOR TRANSPORTATION TO THE LABORATORY. C5C Group No.
ff� 7 _ho 1'� 1.1 h i rnpm e . LI N 0 T E: I I I A I I �L. I I I I �E-RS; S H 0 IJ L D B E TA P F
AINSTCOCU IL RECEIVED AT THE LABORATORY.
SAMPLES ARE NOT �ACEPTED AND VERIFIED AG
'
13-Fed Ex 0 UPS CJ Han Prism Field Service 0 Oth( OTHER:
/| mruES: I °".: GROUNDWATER:'^ | ~'~~-'--'-- � SOLID -WASTE: — �RCFZA
CERCLA LANDFILL
ow000c|omo oaoowo 000 owo ouo L3mt Uen 0woC3ao |ow�-oac||oNc ono'
0_wo--oo_o
u c/ o ��-2-�_o_o__/o_io
°oomTxmsnTYPE CODES: �����~Clear G=n|aoo P ~P|asmc; TL~Teflon-Lined Cap VOA ~Volatile Organics Analysis (Zero Head Space)
Additional Comments:

NC Certification No.Case Narrative
SC Certification No. 990 99012
PRI Full -Service Analytical & NC Drinkinq Water Cert No. 37735 08/18/2014
Isr.' Environmental Solutions VA Certification No. 460211
'.?`. LABORATORIES, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: Sludge (Hazardous Testing)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/30/2014
Statesville, NC 28687 Prism Work Order: 4070591
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Reactivity analysis was subcontracted to GCAL. TCLP Herbicide analysis was subcontracted to AES.
Laboratory repors are attached.
Please call if you have, any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A ECV result is above range. Results are BDL. No further action taken.
Aa ECV results on secondary column are above range. Results are reported from primary column. No further action
taken.
D RPD value outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the,written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 32

Full -
/r'� P R I S Environmental
Analytical s
`/ Environmontel Solutions
LABORATORIES INC.
Sample Receipt Summary
08/18/2014
Prism Work Order: 4070591
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
StaLime
4070591-01
Solid
07/30/14
07/30/14
Third Creek Sludge
4070591-02
Solid
07/30/14
07/30/14
Fourth Creek Sludge
4070591-03
Solid
07/30/14
07/30/14
Samples were received in good condition at 5.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 32

R I I Full -Service Analytical s Laboratory Report
08/18/2014
Environmental Solutions
f sT:, LABORATORIES INC.
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: Stal-ime
Attn: Andy Smith Prism Sample ID: 4070591-01
P.O. Box 1111 Prism Work Order: 4070591
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
73.2
% by
0.100
0.100
1
*SM2540 G
8/5/14 11:40
JAB
P4H0072
Weight
Corrosivity-pH
12
pH Units
1
*9045D
8/1/14 13:15
MES
P4H0014
Ignitability
Pass
mm/sec
0.10
1
*1030
8/7/14 9:09
JAB
P41-10101
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/8/14 9:00
ANG
P4H0120
TCLP Extraction
Complete
N/A
1
*1311
8/12/14 9:30
MEH
P41-10174
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
*7470A
8/13/14 12:17
MEH
P4H0190
Arsenic
BRL
mg/L
0.050
0.0060
1
*6010C
8/14/14 16:55
BGM
P41-10192
Barium
BRL
mg/L
5.0
0.012
1
*6010C
8/14/14 16:55
BGM
P4H0192
Cadmium
BRL
mg/L
0.025
0.00022
1
*6010C
8/14/14 16:55
BGM
P4H0192
Chromium
BRL
mg/L
0.25
0.0019
1
*6010C
8/14/14 16:55
BGM
P41-10192
Lead
BRL
mg/L
0.050
0.0028
1
*6010C
8/14/14 16:55
BGM
P4H0192
Selenium
BRL
mg/L
0.10
0.018
1
*6010C
8/14/14 16:55
BGM
P41-10192
Silver
BRL
mg/L
0.25
0.0012
1
*6010C
8/14/14 16:55
BGM
P41-10192
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
*8081B
8/14114 1:50
JMV
P41-10214
Dieldrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/14/14 23:59
JMV
P41-10214
Endrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/14/14 23:59
JMV
P41-10214
gamma-BHC
BRL
ug/L
0.50
0.0049
1
*8081B
8/14/14 23:59
JMV
P41-10214
Heptachlor
BRL
ug/L
0.50
0.0077
1
*8081B
8/14/14 23:59
JMV
P4H0214
Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
8/14/14 23:59
JMV
P41-10214
Methoxychlor
BRLA
ug/L
0.50
0.0087
1
*8081B
8/14/14 23:59
JMV
P41-10214
Toxaphene
BRLAa
ug/L
25
0.15
1
*8081B
8/14/14 1:50
JMV
P41-10214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
79
%
13-186
Tetrachloro-m-xylene
61
%
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.012
1
*8270D
8/13/14 19:00
KC
P41-10170
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.012
1
*8270D
8/13/14 19:00
KC
P41-10170
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0048
1
*8270D
8/13/14 19:00
KC
P41-10170
2-Methylphenol
BRL
mg/L
0.050
0.012
1
*8270D
8/13114 19:00
KC
P4H0170
3/4-Methylphenol
BRL
mg/L
0.050
0.012
1
*8270D
8/13/14 19:00
KC
P41-10170
Hexachlorobenzene
BRL
mg/L
0.050
0.0070
1
*8270D
8/13/14 19:00
KC
P41-10170
Hexachlorobutadiene
BRL
mg/L
0.050
0.011
1
*8270D
8113/14 19:00
KC
P41-10170
Hexachloroethane
BRL
mg/L
0.050
0.0097
1
*8270D
8/13/14 19:00
KC
P41-10170
Nitrobenzene
BRL
mg/L
0.050
0.0098
1
*8270D
8113/14 19:00
KC
P41-10170
Pentachlorophenol
BRL
mg/L
0.25
0.0082
1
*8270D
8/13/14 19:00
KC
P41-10170
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 32

I� r Full -Service AnalyPRISMtical & Laboratory Report
Environmental Solutions 08/18/2014
+;-0-OFIES. INC.
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 4070591-01
P.O. Box 1111 Prism Work Order: 4070591
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pyridine
BRL
mg/L
0.25 0.016
1
*8270D 8113/14 19:00
KC
P41-10170
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
107 %
49-109
2-Fluorobiphenyl
67 %
55-96
2-Fluorophenol
51 %
27-74
Nitrobenzene-d5
82 %
53-99
Phenol-d5
31 %
11-52
Terphenyl-d14
100 %
42-133
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35 0.78
1
*8260B 8/8/14 14:37
VHL
P41­10172
1,2-Dichloroethane
BRL
ug/L
25 1.4
1
*8260B 8/8114 14:37
VHL
P41­10172
1,4-Dichlorobenzene
BRL
ug/L
380 0.68
1
*82606 8/8/14 14:37
VHL
P41­10172
Benzene
BRL
ug/L
25 0.72
1
*8260B 8/8/14 14:37
VHL
P41­10172
Carbon Tetrachloride
BRL
ug/L
25 1.2
1
*8260B 8/8/14 14:37
VHL
P41­10172
Chlorobenzene
BRL
ug/L
5000 0.61
1
*8260B 8/8/14 14:37
VHL
P41­10172
Chloroform
BRL
ug/L
300 0.89
1
*8260B 8/8114 14:37
VHL
P41­10172
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
10000 9.0
1
*82606 8/8/14 14:37
VHL
P41­10172
Tetra chlorcethylene
BRL
ug/L
35 0.69
1
*8260B 8/8/14 14:37
VHL
P41­10172
Trichloroethylene
BRL
ug/L
25 0.54
1
*8260B 818/14 14:37
VHL
P41-10172
Vinyl chloride
BRL
ug/L
20 1.6
1
*8260B 8/8/14 14:37
VHL
P41­10172
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene 109 % 80-124
Dibromofluoromethane 78 % 75-129
Toluene-d8 101 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-300/529-6364 - Fax: [phone] Page 4 of 32

Laboratory Report
Full -Service
Analytical &
j�/f�,fr./«.� Environmental Solutions
! -Aa(lll TOMEy INC.
08/18/2014
City of Statesville, NC
Project:
Sludge (Hazardous Testing)
Client
Sample ID:
Third Creek
Sludge
Attn: Andy Smith
Prism
Sample ID:
4070591-02
P.O. Box 1111
Prism
Work Order:
4070591
Statesville, NC 28687
Sample
Matrix: Solid
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
17.5
90 by
0.100
0.100
1
*S612540 G
0/5/14 11:40
JAB
P4H0072
Weight
Corrosivity-pH
7.4
pH Units
1
*9045D
8/1/14 13:15
MES
P4H0014
Ignitability
Pass
mm/sec
0.10
1
*1030
8/7/14 9:13
JAB
P41-10101
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/8/14 9:00
ANG
P41-10120
TCLP Extraction
Complete
N/A
1
*1311
8112/14 9:30
MEH
P41-10174
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
*7470A
8/13/14 12:20
MEH
P41-10190
Arsenic
BRL
mg/L
0.050
0.0060
1
*6010C
8/14/14 17:02
BGM
P41-10192
Barium
BRL
mg/L
5.0
0.012
1
*6010C
8/14/14 17:02
BGM
P41-10192
Cadmium
BRL
mg/L
0.025
0.00022
1
*6010C
8/14/14 17:02
BGM
P41-10192
Chromium
BRL
mg/L
0.25
0.0019
1
*6010C
8/14/14 17:02
BGM
P41-10192
Lead
BRL
mg/L
0.050
0.0028
1
*6010C
8/14/14 17:02
BGM
P41`10192
Selenium
BRL
mg/L
0.10
0.018
1
*6010C
8/14/14 17:02
BGM
P4H0192
Silver
BRL
mg/L
0.25
0.0012
1
*6010C
8/14/14 17:02
BGM
P41-10192
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
*8081B
8/14/14 2:33
JMV
P41-10214
Dieldrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/15114 0:42
JMV
P41-10214
Endrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/15/14 0:42
JMV
P41-10214
gamma-BHC
BRL
ug/L
0.50
0.0049
1
*8081B
8/15/14 0:42
JMV
P41-10214
Heptachlor
BRL
ug/L
0.50
0.0077
1
*8081B
8/15/14 0:42
JMV
P41-10214
Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
8/15/14 0:42
JMV
P41-10214
Methoxychlor
BRLA
ug/L
0.50
0.0087
1
*8081B
8/15/14 0:42
JMV
P41-10214
Toxaphene
BRLAa
ug/L
25
0.15
1
*8081B
8/14114 2:33
JMV
P4H0214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
98 %
13-186
Tetrachloro-m-xylene
82 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.012
1
*8270D
8/13/14 19:22
KC
P41-10170
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.012
1
*8270D
8/13114 19:22
KC
P41-10170
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0048
1
*8270D
8/13/14 19:22
KC
P41-10170
2-Methylphenol
BRL
mg/L
0.050
0.012
1
*8270D
8/13/14 19:22
KC
P41-10170
3/4-Methylphenol
BRL
mg/L
0.050
0.012
1
*8270D
8/13/14 19:22
KC
P41-10170
Hexachlorobenzene
BRL
mg/L
0.050
0.0070
1
*8270D
8113/14 19:22
KC
P41-10170
Hexachlorobutadiene
BRL
mg/L
0.050
0.011
1
*8270D
8/13114 19:22
KC
P41-10170
Hexachloroethane
BRL
mg/L
0.050
0.0097
1
*8270D
8/13/14 19:22
KC
P41-10170
Nitrobenzene
BRL
mg/L
0.050
0.0098
1
*8270D
8/13/14 19:22
KC
P41-10170
Pentachlorophenol
BRL
mg/L
0.25
0.0082
1
*8270D
8/13/14 19:22
KC
1`41-10170
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 32

r' P R 9 S Full -Service Analytical s
Environmental Solutions
w...,.. LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Parameter
Pyridine
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Result Units
BRL mg/L
TCLP Volatile Organic Compounds by GC/MS
1,1-D ichlo roethylene
1,2-Dichloroethane
1,4-Dichlorobenzene
Benzene
Carbon Tetrachloride
Chlorobenzene
Chloroform
Methyl Ethyl Ketone (2-Butanone)
Tetrachloroethylene
Trichloroethylene
Vinyl chloride
Report MDL
Limit
0.25 0.016
Surrogate
2,4,6-Tribromophenol
2-Fluorobiphenyl
2-F.luorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-dl4,
BRL
ug/L
35
0.78
BRL
ug/L
25
1.4
BRL
ug/L
380
0.68
BRL
ug/L
25
0.72
BRL
ug/L
25
1.2
BRL
ug/L
5000
0.61
BRL
ug/L
300
0.89
BRL
ug/L
10000
9.0
BRL
ug/L
35
0.69
BRL
ug/L
25
0.54
BRL
ug/L
20
1.6
Surrogate
Laboratory Report
08/18/2014
Client Sample ID: Third Creek Sludge
Prism Sample ID: 4070591-02
Prism Work Order: 4070591
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
lution Method Analysis
Analyst Batch
actor Date/Time
ID
1 '8270D 8/13114 19:22
KC P41­10170
Recovery
Control Limits
81 %
49-109
55 %
55-96
43 %
27-74
63 %
53-99
27 %
1152
81 %
42-133
1 '8260B
8/8/14 15:03
VHL
P4H0172
1 '8260B
8/8114 15:03
VHL
P4H0172
1 '8260B
818/14 15:03
VHL
P41­10172
1 "8260B
8/8/14 15:03
VHL
P41­10172
1 '8260B
8/8/14 15:03
VHL
P41­10172
1 '8260B
8/8/14 15:03
VHL
P41­10172
1 '8260B
8/8/14 15:03
VHL
P41­10172
1 '8260B
8/8/14 15:03
VHL
P4H0172
1 '8260B
818/14 15:03
VHL
P41­10172
1 '8260B
8/8/14 15:03
VHL
P41­10172
1 '8260B
8/8/14 15:03
VHL
P4H0172
Recovery
Control Limits
4-Bromofluorobenzene 111 % 80-124
Dibromofluoromethane 102 % 75-129
Toluene-d8 101 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism. Laboratories_ Inc. ..
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 01 32

P R I S y` ,A EFull - nvironmental
Analytical 8
"' �--"� I � � Environmental Solutions
-„ -ORATORIES, INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Laboratory Report
08/18/2014
Client Sample ID: Fourth Creek Sludge
Prism Sample ID: 4070591-03
Prism Work Order: 4070591
Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
15.2
% by
0.100
0.100
1
*SM2540 G
8/5114 11:40
JAB
P4H0072
Weight
Corrosivity-pH
5.1
pH Units
1
*9045D
8/1114 13:15
MES
P4H0014
Ignitability
Pass
mm/sec
0.10
1
*1030
8/7/14 9:16
JAB
P41-10101
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/8/14 9:00
ANG
P4H0120
TCLP Extraction
Complete
N/A
1
*1311
8/12/14 9:30
MEH
P4H0174
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000012
1
*7470A
8/13/14 12:25
MEH
P4H0190
Arsenic
BRL
mg/L
0.050
0.0060
1
*6010C
8/14114 17:09
BGM
P41-10192
Barium
BRL
mg/L
5.0
0.012
1
*6010C
8114/14 17:09
BGM
P4H0192
Cadmium
BRL
mg/L
0.025
0.00022
1
*6010C
8/14/14 17:09
BGM
P4H0192
Chromium
BRL
mg/L
0.25
0.0019
1
*6010C
8/14/14 17:09
BGM
P4H0192
Lead
BRL
mg/L
0.050
0.0028
1
*6010C
8/14/14 17:09
BGM
P4H0192
Selenium
BRL
mg/L
0.10
0.018
1
*6010C
8/14114 17:09
BGM
P4H0192
Silver
BRL
mg/L
0.25
0.0012
1
*6010C
8114114 17:09
BGM
P41-10192
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.16
1
*8081B
8/14/14 3:16
JMV
P41-10214
Dieldrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/15/14 1:25
JMV
P4H0214
Endrin
BRLA
ug/L
0.50
0.0046
1
*8081B
8/15114 1:25
JMV
P4H0214
gamma-BHC
BRL
ug/L
0.50
0.0049
1
*8081B
8115/14 1:25
JMV
P4H0214
Heptachlor
BRL
ug/L
0.50
0.0077
1
*8081B
8/15/14 1:25
JMV
P4H0214
Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
8/15/14 1:25
JMV
P41-10214
Methoxychlor
BRLA
ug/L
0.50
0.0087
1
*8081B
8/15/14 1:25
JMV
P41-10214
Toxaphene
BRLAa
ug/L
25
0.15
1
*8081B
8/14/14 3:16
JMV
P41-10214
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
93 %
13-186
Tetra chloro-m-xylene
75 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
2,4,6-Trichlorophenol
BRL
mg/L
2,4-Dinitrotoluene
BRL
mg/L
2-Methylphenol
�RL��
mg/L
enol
mg/L
Hexachlorobenzene
Hexac tomb benzene
BRI
BRL
Q---:
mg/L
Hexachlorobutadiene
BR
mg/L
Hexachloroethane
BRL
mg/L
Nitrobenzene
BRL
mg/L
Pentachlorophenol
BRL
mg/L
0.25
0.012
1
*8270D
8113/14
19:43
KC
P41-10170
0.10
0.012
1
*8270D
.8/13/14
19:43
KC
P4H0170
0.050
0.0048
1
*8270D
8/13/14
19:43
KC
P4H0170
0,050
0.012
1
*8270D
8/13/14
19:43
KC
P4H0170
0.050
0.012
1
*8270D
8/13/14
19:43
KC
P4H0170
0.050
0.0070
1
*8270D
8/13114
19:43
KC
P4H0170
0.050
0.011
1
*8270D
8113114
19:43
KC
P4H0170
0.050
0.0097
1
*8270D
8113/14
19:43
KC
P4H0170
0.050
0.0098
1
*8270D
8/13/14
19:43
KC
P4H0170
0.25
0.0082
1
*8270D
8/13114
19:43
KC
P4H0170
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 32 i

Laboratory Report
r•i Full -Service Analytical &
PRISM Environmental Solutions 08/18/2014
—CRATOMES, INC.
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample. ID: Fourth Creek Sludge
Attn: Andy Smith Prism Sample ID: 4070591-03
P.O. Box 1111 Prism Work Order: 4070591
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/30/14 15:04
Time Submitted: 07/30/14 17:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DaterTime ID
Pyridine BRL mg/L 0.25 0.016 1 '8270D 8/13/14 19:43 KC P41­10170
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
1,2-Dichloroethane
BRL
ug/L
1,4-Dichlorobenzene
BRL
ug/L
Benzene
BRL
ug/L
Carbon Tetrachloride
BRL
ug/L
Chlorobenzene
BRL
ug/L
Chloroform
BRL
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
Tetrachloroethylene
BRL
ug/L
Trichloroethylene
BRL
ug/L
Vinyl chloride
BRL
ug/L
2,4,6-Tribromophenol
99 %
49-109
2-Fluorobiphenyl
69 %
55-96
2-Fluorophenol
48 %
27-74
Nitrobenzene-d5
74 %
53-99
Phenol-d5
30 %
11-52
Terphenyl-d14
96 %
.42-133
35
0.78
1
'8260B
8/8/14 15:28
VHL
P41­10172
25
1.4
1
'8260B
8/8/14 15:28
VHL
P41­10172
380
0.68
1
'8260B
8/8/14 15:28
VHL
P41­10172
25
0.72
1
'8260B
8/8/14 15:28
VHL
P41­10172
25
1.2
1
'8260B
8/8/14 15:28
VHL
P41­10172
5000
0.61
1
'8260B
8/8114 15:28
VHL
P41­10172
300
0.89
1
'8260B
8/8/14 15:28
VHL
P41­10172
10000
9.0
1
"8260B
8/8/14 15:28
VHL
P41­10172
35
0.69
1
'8260B
8/8114 15:28
VHL
P41­10172
25
0.54
1
*82606
8/8/14 15:28
VHL
P41­10172
20
1.6
1
'8260B
8/8/14 15:28
VHL
P41­10172
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene 112 % 80-124
Dibromofluoromethane 108 % 75-129
Toluene-d8 104 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 32

Sample Extraction Data
Prep Method: 1311
Lab Number Batch Initial Final Daterrime
4070591-01
P41-10120
25
g
500 mL
08/07/14 15:35
4070591-01
P41-10174
1000
mL
1000 mL
08/11/14 16:30
4070591-02
P41-10174
1000
mL
1000 mL
08/11/14 16:30
4070591-02
P41-10120
25
g
500 mL
08/07/14 15:35
4070591-03
P41-10174
1000
mL
1000 mL
08/11/14 16:30
4070591-03
P41-10120
25
g
500 mL
08/07/14 15:35
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
4070591-01
P41-10192
10
mL
50 mL
O8/12/14 14:50
4070591-02
P41-10192
10
mL
50 mL
08/12/14 14:50
4070591-03
P41-10192
10
mL
50 mL
08/12/14 14:50
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
4070591-01
P41-10190
20
mL
30 mL
08/12/14 12:35
4070591-02
P41-10190
20
mL
30 mL
08/12/14 12:35
4070591-03
P41-10190
20
mL
30 mL
08/12/14 12:35
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Daterrime
4070591-01
P41-10214
200
mL
10 mL
08/13/14 13:00
4070591-01
P41-10214
200
mL
10 mL
08/13/14 13:00
4070591-02
P41-10214
200
mL
10 mL
O8/13/14 13:00
4070591-02
P41-10214
200
mL
10 mL
08/13/14 13:00
4070591-03
P41-10214
200
mL
10 mL
08/13/14 13:00
4070591-03
P41-10214
200
mL
10 mL
.08/13/14 13:00
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Daterrime
4070591-01
P41-10170
200 mL
1 mL
08/12/14 13:30
4070591-02
P41-10170
200 mL
1 mL
08/12/14 13:30
4070591-03
P41-10170
200 mL
1 mL
08/12/14 13:30
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Daterrime
4070591-01 P41-10172 1 mL 10 mL 08/08/14 8:50
4070591-02 P41-10172 1 mL 10 mL 08/08/14 8:50
4070591-03 P41-10172 1 mL 10 mL 08/08114 8:50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
I Page 9 of 32

Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab Number
Analysis
4070591-01
Herbicides TCLP (Sub)
4070591-02
Herbicides TCLP (Sub)
4070591-03
Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number Analysis
4070591-01
Reactivity. Cyanide (Sub)
4070591-01
Reactivity, Sulfide (Sub)
4070591-02
Reactivity. Cyanide (Sub)
4070591-02
Reactivity. Sulfide (Sub)
4070591-03
Reactivity. Cyanide (Sub)
4070591-03
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 32

_ .... _ . CHAIN
,fie
CHAIN OF CUSTODY RECORD N IIi1
M
.,) i=uli Sortitice Analytical £ YESNO � � Environmer.tai Solutions Pt1raE _ ®� _ 0UoTG t1 ro Ea95u�a PROPet1 rsit6o iHo: Samples 1Nl -ACT-upon arrival? s �� ---
Received ON WET ICE" Temp
4S r,„ i ,c°^ U Lo,(%7 t543 ^ charlotte,NC 232y4-0543 Project Name: PROPER PRESERVATIVES indicated^ —�— — --
Ir _,.. cni( t,�, r
'^;cr a: t ^;r F'9 b^c �A. lt,4la?5-G1rttCt1) Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No) Received WITHIN HOLDING TIMES? -- _---
�( ��� *Please ATTACH any project specific reporting (QC LEVEL 9 II IVI BF0 CUSTODY SEALS INTACT?
Client: Company Name: r � , b � � _ _
previsions and/or C4C Requil'ements VOLATILES rec'd IOUHEADSPACF_? __W.
Repor 1i To/Contact Nam : 4,J 4/ sew 5Invoice To: PROPER CONTAINERS used?
--- --- J
Reporting Address: A 0, ��� �d d -- --
d Address: ,
Phone: l0-rrS 99- 343? Eax es (N®): TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL.
Purchase Order No./Rill'ing Reference
Email (yes) (No) Ermail Address Requested Due Date ❑ 1 Day ❑ 2 Days L] 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAO USACE EL NO
E®D Type: PDP_ Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved SC_ OTl-IEP� N/A
Site Location Name: �1b4 rP%' 4I Samples received after 15:00 will be processed next business day.
:site floe a4ion Physical Address: � �r d� ®� �� � Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES 6\I®
� (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES _ NO
Jl RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX ANALYSES REQUESTED PRISM
SAMPLE CONTAINER h LAB
CLIENT DATE COLLECTED (SOIL, PRESERVA- °S� ��9 j. REMARKS ID NO.
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR `TYPE TiVES
% y�
HOURS SLUDGE) SEE BELOW N®' SIZE "s
�q,
sppy -- — ----
=�—
pp- i i nA
/ /� pup p) ��•'j ........:
-- ------ --- — — -- �_lie--f� c r��/�L---�—------------ — ---
Sampler's Signature .1 c ��'`� ��'
Sampled By ( rint Name) 4, f ' ric Afflllation
the as requested above. Any changes must
be
Chain of Cusor
Upon relinquishing, this -Custody is your
submitted in writing to the Prism Pro, Manager.
authorization f P is
There will be cha
to proceed with analyses
s for any changes after analyses have been Initialized. Date MilitarylHours Additional
Comments:
Fell fished By: (Sig a ure)
Received 'Signature)
ell
fished By: (Signature) � turej
Receiv, By: (Signature)
Date
1
Received For Pr)s}n Laboratorles B
_ ,•
Date
�•_ SG '(.,
is
nat
wished By: (Sig0s�),/
f
(a tl tY� __/ Al'[� /
(D
d of Shipment: OTC!ALL SAMPLE COOLERS SIiOULD BE TAPED SHUT W ITH CySTODY SEALS FOR TRAPISPORTATION TO THE LABORATORY. (.QC Group 0.,
—a SAMPLES ARE NOT AC • EPTED AND VERIFIED AGAINST -OC UPTIL'RECEIVED AT THE LABORATORY. .= 0 __2
i!
Ex ❑UPS ❑ Hand delivered cr Prism Field Service ❑Other
iES. UST: GIROUNDWATER: I ®KINKING WATER: SOLI® UUASTC: RCRA: OERCLA „' i:LAN®TILL OTHER:
❑SCl ❑NC ❑SC ❑NC ❑SC i ❑NC ❑SC ❑NC ]SC ❑NC ❑SCI ❑NC ❑SCI ❑NC ❑SCi pNC ❑SC
1❑----'❑ ------ G-- --�❑-- ----
�•n�iTAialtcrs TVPP CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

Plyti'3 Full -Service Ana
r;al &
a� ® M ` Environmental Solutions
LAeonATORiea inC.
449 Springbrook Road • Charlotte, NC 28217
Phane 7641629-6364 Fa/x�: 7©4d525-0409 r
ant Company Name:
port To/Contact Name: n
CHANN ,Qj{µ
�sP 5 CUSTODY
QUOTE
Project Name: UST Project: (Yes) (NO)
Short Hold Analysis: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Samples INTACT up, n arrival?
Receiver/ ON WET ICE?
PFtOPEr PRESET M'ITIVES inilicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACI
VOLATILES reed W40UT HEADSPACE?
PROPER CONTAING,;S Us3c;?
TEMP:, Therm ID: _Obseived:
YES NO NfA
IC I
porting Address: D-J / I Address' ------
$ �r� d'11 ire: G PERSONNEL
�� TO BE MILLED IN BY CLIENT/SAMPLIN
Fax ' Yes (No)'.410 i- Purchase Order No./Billing Reference -Do® FL_ NC
nail Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days O 4 Rush Work Must Be ays L3 5 DaysCertification; AlELAC nTHER N/A
"Working Days" ❑ 6-9 Days ❑ Standard 10 days O Pre -Approved SC
],D Type: PDF_Excel Other _ _ _
t;e Location Name: a u r b cry Z✓tv Samples received after 14:00 will be processed next business day.
Turnaround time is based op business days, excluding weekends and holidays. Water
mple Iced lUpon Collection: YES_ N®—
t:e Location Physical Address: 6. `J /3 e r Qrm (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
S a Sr'r C V RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ANALYSIS REQUESTED PRISM
TIME MATRIX SAMPLE CONTAINER PRESERVA- �� / / / / / // REMARKS ID B
O.
(SOIL, —
CLIENT DATE COLLECTED — WATER OR MILITARY
TYPETIVES
' NO. SIZE
SAMPLE DESCRIPTION COLLECTED HOURS SLUDGE) SEE BELOW I �1 T o-- �P
— _ a
TC e'er
Affiliation
Sampled By (Print Name) y es must be
Sampler's Signature
Upon relincyuishing, this Chain of Custody is your authorization for P ism to proceed with the analyses as requested above. An changes MilitarylHours Additional Comments
submitted in writing to the Prism Project Manager. There will b Re ea es for ey (s gnatur ny changes afte analyses have been. initialized.
Relin4lr}shed 8y: (Si9ni�ure).r e' / .1 y�
Hale
0
d.
-
N or Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY S r
SAMPLES ARE NOT A�7y'CEPTED AND VERIFIED AGAINST COC TIL RECEIVED AT THE LABORATORY.
"��/ CERCLA LANDFILL I OTHER:
N Ex Q UPS ❑ Hand -delivered S� Prism Field Service ❑Other
S: UST; GROUNDWATEP.: DRINKING WATER: SOLID WASTE. RCRA:
GI SC ❑NC Cl SC I ®NC CSC- I C3NCOSCI 0NC ❑SCI ONC QSCI ONC ❑SC
I
Site Arrival Time:
Slle DCpL rWW .' I II`H':
Field Tech Pee.:
Milceaga:
SE�RE�Yj:BSE,,dR'
,ERrin"sscgio4Tirp. s
QSCI ❑NC ❑SCI ©NC ❑—_--- Ell
VOA = Volatile Organics Analysis (Zero Head Space) y,
- _Q, _.� .' nec• a = 4mhar C =Clear G=Glass P =Plastic; TL =Teflon -Lined
Cap

ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Rabbi A. Jones
PROJECT ID
4070591
LABORATORY REPORT NUMBER
1409083
Primary Data Review By
rt
Chantelle Kanhai
Project Manager, AES
PLEASE NOTE:
DATE
August 08, 2014
Secondary Data Review By
Ashley Amick
Project Manager, Access Analytical
[e-mail]
- Unless otherwise noted, all analysis on this report ped'ormed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDIIEC certified laboratory # 98016, NCDENR certified lab # S62, GA certified lab # FL-ES7582,
NELAP certified laboratory # WiS2
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page i of 7
Page 13 of 32

!: `= Full -Service Analytical &
11 Environmental Solutions
.fS
RM
SUBCONTRACT ORDER
Certification: ELAC_ USACE
Prism Laboratories, Inc. NC . SC_ Other
4070591 NIA
SENDING LABORATORY: RECEIVING LABORATORY:
Prism Laboratories, Inc. Analylical Environmental Services, inc.
P. O. Box 240543 3785 Presidential Parkway�����
Charlotte, NC 28224-0543 Atlanta, GA 30340
Phone: [phone] Phone :[phone]
Fax: [phone],109 Fat: NA
Proiect Mauaocr. Robbi A. Jones
Analysis Due Expires LaU0rat0l',v ID Continents
Sample ID: 4070591-01 Solid Sauipled:07/30114 15:04
Herbicides TCLP (Sub) 08106114 15:04
Coirlairiers Supplied-
tvm
C'r C_
Sample ID. 4070591-02 Solid Sampled:07/30/1415:04
Herbicides TCLP (Sub)
Containers SuppliecL-
08/06/14 15:04
Nil
Sample ID:4070591-03 Solid Sampled:07/30/1415:04
Herbicides TCLP (Sub)
Containers Supplied:
08/06/14 15:04
7-31- I r
Released By Date Received Qy LS D;ite
Releaed
Date
Date.
Date
Detc
Page 2 of %
Page 14 of 32

Analytical Environmental Services, Inc
Date: 8-Aug-14
Client:
Prism Laboratories
Client Sample ID:
STALIME
Lab Order
1408083
Tan Number:
4070591-01
Project Name:
4070591
Collection Date:
7/30/2014 3:04:00 PM
Lab ID:
1408083-001A
D4atrix:
Solid
Analyses
Result Qual
114llL
ReportingrtinnUnits
Limit
BatchlD
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.039
0.20
mg/L 194388
1 08/06/2014 12:21 RF
2,4-D
BRL
0.042
0210
mg/L 194388
1 08/06/2014 12:21 RF
Surr: DCAA
79.2
0
40.3-135
%oREC 194388
1 08/06/2014 12:21 RF
QnAlifirrs: ° Vzlue exceads n':aximum wntaminant level E Estimated value Auv_ auantitatton rm;_e
BRL Nut DeteaeJ at MDL S Sp h R--y outside limis due in mavie
41 Holding times 1'or preparation or attal}'sis exceeded - Greater than Result ml-
N Aaalne nM NELAC eeuilied 1 Estimated vaitte detected below Reposing Limit
B Aualvte detected in the associa;rd method blank Lrss titan Resuh value
f age 3 of 7
Page 15 of 32

Analytical Environmental Services, Me
Date: 8-Aug-14
Client:
Prism Laboratories
Client Sample ID:
THIRD CREEK SLUDGE
Lab Order
1408083
Tag Number:
4070591-02
Project Name:
4070591
Collection Date:
7/30/2014 3:04:00 PM
Lab 1D:
1403083-002A
Matrix:
Solid
ReportingllL
Analyses
Result
Qual M
knits 13atcbID
DF Date Analyzed :InaIyst
Limit
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BP.1.
0.039
0.20
mg/L 194388
1 08/06/2014 12:52 RF
2,4-D
BRL
0.042
0.20
mg!L 194388
1 08106/201412:52 RF
SUIT: DCAA
99.4
0
40.3-135
D%REC 194388
1 08/06/2014 12:52 RF
Qualifiers: Value exceeds maximum contaminant leeel
BRI, Not Detected at NIDL
H Holding times for prtPmvlion or analysis exceeded
N A-1ve nm NtELAC cenified
B Anal) to dzte.tnd m the y=sueiste:i method idsnk
E Estimated value abve yuanlitatiun r:Lige
S SPike Recovery nulsidt limits due to tuatrix
Greater than Resnit value
J Estimated-Im dcinctcd betas•l:ep;ntim_ Lunn
Leis than Result value
Pace 4 of 7
Page 16 of 32

Analvtical ]Environmental Services, Yne
Date: 8-Aug-14
Client:
Prism Laboratories
Client Sample ID:
FOURTH CREEK SLUDGE
Lab Order
.1408093
Tag Number:
4070591-03
Project Name:
4070591
Collection Date:
7/30/2014 3:04:00 PM
Lab ID:
1408083-003A
Matrix:
Solid
Analyses Result Qual MDL ReportingL)nits BatcbID DF Date Analyzed Analyst
Limit
HERBICIDES,TCLP SW1311/81SIA
2,4,5-TP (Silvex) BRL
2,4-D RRL
Sunr: DCAA 89.3
Qunlifiers: VA,, excerds iaaximum contamilml level
AFL No, Delcaed m NIDL
H Bolding times for prep. ation of mtalysis exceeded
;! :1m:h is not NELAC ceni0ed
R :kn:dvie deleted in the assncmtcd ntnthed blank
(SW3510C)
0.039 0.20 mg/L 194388 1 08/06/2014 13:24 RF
0.042 020 mg/L 194388 1 08/06/201413:24 RF
0 40.3-135 °'REC 194388 1 08106/201413:24 RF
E E-stinaated value above quantization range
S Spike lt--, outside limits doe to matrix
Greater Than Result value.
J Estimaied valve deleted bd.w Reporting Limit
Less Ibmz Result value
Page 5 of 7
t Page 17 of 32

Analytical Environmental] Services, Inc.
Client —
Sample/Cooler Receipt Checklist
'\York Order Number.
Checklist completed by �� /
Sig�t� to Dare
Carrier name:✓ UFedEx _PS — Courier— Client— US \Mail — Other
Shipping container/cooler in good condition? Yes iVo —
Custody seals intact on shipping container/cooler? Yes — No
Custody seals intact on sample bottles? Yes _f No —
Container/Temp Blank temperature in compliance? (4°C±2)* Yes ✓ No —
Not Present _.
Not Present
Not Present ✓
Cooler #1 OA0 C Cooler #2 Cooler #3
1�
Cooler #> #
„Cooler#5
Chain of custody present?
Yes
No —
Chain of custody signed when relinquished and received?
Yes
No —
Chain of custody agrees with sample labels?
Yes
No
S-ptuples in proper container/bottle?
Yes
t,
No _
Simple containers intact?
Yes
1
No —
Sufficient sample volume for indicated test?
Yes
No _
All samples received within holding time? Yes _ _ No
Was TAT marked on the COC? Yes No t
Proceed with Standard TAT as per project histoq? Yes _ No _
Water- VOA vials have zero headspace? No VOA vials submitted Yes _
Cooler #6
Not Applicable
No
Water - pi -I acceptable upon receipt? Yes — No — Not Applicable
Adjusted? • Checked by
Sample Condition: Good T. Other(Explain) _
(For diffitsive samples or AIHA lead) Is a known blank included? Yes — No
See Case Narrative for resolution of the Non-Conforinauee.
S.,mples do not have to comply uQlc the gi en range for certain r craa:ctcrs.
�I1,(7ualit} AssurancelCilecklists Receipt Check Ii.ts\Saniple_Cooler_Receipt_CIleekfist
Pa
Page 18 of 32

Analytical Environmental Services, Inc Date: 8-Aug-14
Client: Prism Laboratories ANALYTICAL QC SUMMARY RE, PORT
1'rgjert Name: 4070591
Workorder: 1408083 BatchI.D: 194388
Sample ID: NIB-194388
Client ID:
Units: mg/L
Prep Date: 08/04/2014
Run No: 273052
SainpIcType: I19BLK
TestCode: AERBICIDES,TCLP SW1311/8151A
BatchID: 194388
Analysis Date: 08/05/201.4
SegNo: 5761873
Analvte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qua1
2.d.5-TP (Silvex) BPI, 0.20
2.4-1) BRL 0.20
Surr: DCAA 0.4440 0 0.5000 88.8 403 135
Sample 1D: 1,CS-194388
Client ID:
Units: mg/L
Prep Date: 08/04/2014
Run No: 273052
Sampldlype: LCS
TestCode: NERBICIDES,TCLP SW131118151A
BatehID:194388
Analysis Date: 08/05/2014
SegNo: 5762303
Analvte
Result RPT Limit SPK value SPK Ref Val
%REC. Low Limit
High Limit RPD Ref Val %R-PD
RPD Limit Qual
2.4.5-"1'1' (SiIvex)
03607
0.20
0.5000
72.1
55.2
125 -
2.4-D
0.3655
0.20
0.5000
73.1
49.8
128
Surr: DCAA
0.4938
0
0.5000
98.8
40.3
135
Sample ID: 1408039-001 AMS
Client ID: ,
Units: mg/L
Prep Date: 08/04/2014
Run No: 273052
SompleType: NIS
TestCode: 11ERB1CIDES,TCLP SW1311/8151A
BatchID: 194388
Analysis Date: 08/05/2014
Seq No: 5762305
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
Higli Limit RPD Ref Val %RPD
RPD Limit Qual
2.4.5-IT (Silvex)
0.4163
0.20
0.5000
83.3
54
143
0.4288
0.20
0.5000
85.8
45
142
Surr: DCAA
0.5156 .
0
0.5000
103
40.3
135
1
iv
(Q
Il nalifirrs:
- Greater thin Result value
<
Less than Result value B Anah•te detegod in the associated method blank
(D
E
Estimated (value a
cove quantilatinn range) H Holding limes for preparation or analysis exceededBRL
Bclow reporting limit
(9
1 Estimated value detected below Reposing Limit
N
Analyte not NELAC certified R RPD outside limits due to matrix
ORpt
Lin, Repmling Limit
S
Spike Recovery outside limits due to matrix
Page 7 of 7
Iw

ACCESS
- ANALYTICAL, INC.
ANALYTMAL REPORT
CLIENT
Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECT ID
4070591
LABORATORY REPORT NUMBER
214080120
DATE
08/05/2014
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979
Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP
certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of
GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243.
i of 13
Page 20 of 32

AIELAP CERTIFICATE NUMBER € 1955
DOD FLAP CERTII=iCATE NUMBER L13-190
PERFORMED BY
GCA lL, LLC .
7979 Innovation Park Dr.
Baton Rouge, LA 70320
Report Date 08/05/2014
CAL
G I�IIIIIIIIIIIIIReport
NI�IIIIIIIIII�i1fIIIIIIIIIGII
Deliver To Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
Attn Robbi Jones
Project 4070591
2of13
Page 21 of 32
I

Case Narrative
Client: Access Analytical Deport: 214080120
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the sample cross-reference page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
3 of 13
Page 22 of 32

Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the
Environmental Protection Agency or other recognized agencies. The samples and their corresponding
extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention
period the samples will be disposed in accordance with GCAL's Standard Operating Procedures_
Common Abbreviations Utilized in this Report
ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
00:00 Reported as a time equivalent to 12:00 AM
Reporting Flags Utilized in this Report
J Indicates the result is between the MDL and RDL
U Indicates the compound was analyzed for but not detected
B Indicates the analyte was detected in the associated Method Blank
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with
NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results
contained within this report relate only to the samples reported. The documented results are presented
within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as
a permanent record thereof. The results contained within this report are intended for the use of the client.
Any unauthorized use of the information contained in this report is prohibited.
certify that this data package is in compliance with the NELAC standard and terms and conditions of the
contract and Statement of Work both technically and for completeness, for other than the conditions in the
case narrative. Release of the data contained in this hardcopy data package and in the
computer -readable data submitted has been authorized by the Quality Assurance Manager or his/her
designee, as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the
DOD QSM as specified in the contract if applicable.
k�X`P A ­ 4 � A 1) LA
Authorized Signature
GCAL REPORT 214080120 �,2
THIS REPORT CONTAINS PAGES.
4of13
Page 23 of 32

Report Sample Summary
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
21408012001 STALIME
21408012002 THIRD CREEK SLUDGE
21408012003 FOURTH CREEK SLUDGE
GCAL Report 214080120
Solid 07/30/201415:04 08/01/201410:30
Solid 07/30/201415:04 08/01/201410:30
Solid 07/30/201415:04 08/01/201410:30
5of13
Page 24 of 32

Summary of Compounds Detected
There were no detects
GCAL Report 214080120
Gof13
Page 25 of K

i_
GCAL ID i Client ID
Matrix
Collect Date/Time
Receive_DafelTime
I'
21408012001 STALIME
Solid
071301201415:04
08/01/201410:30
EPA 7.3.3.2, Rev 3/9012B
I=
Prep Date Prep Batch
Prep Method
Dilution
Analyzed
By
Analytical Batch
08/04/2014 11:30 538041
EPA 7.3.3.2
1
08/05/2014 07:35
DJH
538276
CAS# Parameter
Result
RDL
MDL
Units
57-12-5R Reactivity Cyanide
250U
250
250
mg/kg
EPA 7.3.4.2, Rev. 3/9034
Prep Date Prep Batch
Prep Method
Dilution
Analyzed
By
Analytical Batch
_
08/04/2014 11:30 538042
EPA 7.3.4.2
1
08/05/2014 10:00
MDW
538287
CAS# Parameter
Result
RDL
MDL
Units
18496-25-8R Reactivity Sulfide
80U
80
80
mg/kg _
RESULTS REPORTED ON A WET WEIGHT
BASIS
GCAL Report 214080120
7of13
Page 26 of 32

Receive Date/Time
AL IDClient ID Matnx `
Collect Date/Time
F24080120�02THIRD CREEK SLUDGE, Solid
07/30/2014 15:04
08/01/2014 10:30
EPA 7.3.3.2, Rev 3/9012B
Date Prep Batch Prep Method
Dilution Analyzed
By Analytical Batch
rp
4/2014 11:30 538041 EPA 7.3.3.2
1 08/05/2014 08:00
DJH 538276
=
CAS# Parameter
Result RDL
MDL Units
57-12-5R Reactivity Cyanide
250U 250
250 mg/kg
PPA 7 '1 4 9 RPv_ 'IM34
[08/04
rep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
!2014 11:30 538042 EPA 7.3.4.2 1 08/05/2014 10:00 MDW 538287
CAS# Parameter Result RDL MDL Units
18496-25-8R Reactivity Sulfide 80U 80 80 mg/kg
RESULTS REPORTED ON A WET WEIGHT BASIS
GCAL Report 214080120
8of13
Page 27 of 32

GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
214080I2003 FOURTH CREEK SLUDGE . Solid 07/30/2014 15:04 08/01l2014 10:30
EF
.3.2, Rev 3/9012B
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
08/04/2014 11:30 538041 EPA 7.3.3.2 1 08/05/2014 08:01 DJH 538276
CAS# Parameter Result RDL MDL Units
57-12-5R Reactivity Cyanide 250U 250 250 mg/kg
EPA 7.3.4.2, Rev. 3/9034
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
08/04/2014 11:30 538042 EPA 7.3.4.2 1 08/05/2014 10:00 MDW 538287
CAS# Parameter
18496-25-8R Reactivity Sulfide
RESULTS REPORTED ON A WET WEIGHT BASIS
GCAL Report 214080120
Result
RDL
MDL
Units
801-1
80
80
mglkg
9of13
Page 28 of 32

General Chemistry Quality Control Summary
Analytical Batch 538276
Client ID
MB538041
LCS538041
Prep Batch 538041
GCAL ID
1344024
1344025
Prep Method EPA 7.3.3.2
Sample Type
Method Blank
LCS
Prep Date
08/04/2014 11:30
08/04/2014 11:30
Analytical Date
08/05/2014 07:26
08/05/2014 07:27
Matrix
Solid
Solid
Units mg/kg
Spike
Control
EPA 7.3.3.2, Rev 319012B
Result RDL
Added
Result
% R
Limits % R
57-12-5R Reactivity Cyanide
25OU 250
1 2501
34.5
14
1 - 25
Analytical Batch 538276
Client ID
BOX RBM250055, N48872
1343755DUP
Prep Batch 536041
GCAL ID
21407307301
1344026
Prep Method EPA 7.3.3.2
Sample Type
SAMPLE
DUP
Prep Date
08/0412014 11:30
08/04/2014 11:30
Analytical Date
08/05/2014 07:28
08/05/2014 07:29
Matrix
Solid
Solid
EPA 7.3.3.2, Rev 3/9012B
Units mg/kg
Result
RPD
Result RDL
RPD
Limit
57-12-5R Reactivity Cyanide
0.0 250
0.0
0
20
GCAL Report 21408012D

general Chemistry Quality Control Summary
Analytical Batch 538287
Client ID
MB538042
LCS538042
Prep Batch 538042
GCAL ID
1344027
1344028
Prep Method EPA 7.3.4.2
Sample Type
Method Blank
LCS
Prep Date
08/04/2014 11:30
08/04/2014 11:30
Analytical Date
OB/05/2014 10:00
08/05/2014 10:00
Matrix
Solid
Solid
EPA 7.3.4.2, Rev. 3/9034
units mg/kg
Spike
Result
Control
Result RDL
Added
% R
Limits % R
1849'6'2�5--d-FF Reactivity Sulfide
80U 80
1000
890
89
55 - 146
Analytical Batch 538287
Client ID
BOX RBM250055, N48872
1343755DUP
Prep Batch 538042
GCAL ID
21407307301
1344029
Prep Method EPA 7.3.4.2
Sample Type
SAMPLE
DUP
Prep.Date
08/04/2014 11:30
08/04/2014 11:30
Analytical Date
08/05/2014 10:00
08/05/2014 10:00
Matrix
Solid
Solid
EPA 7.3.4.2 Rev. 3/9034
Units mg/kg
Result
RPD
Result RDL
RPD
Limit
-18496-25.8R Reactivity Sulfide
0 BO
0
0
25
W GCAL Report 214080120
W
0
O
—n
W
N

M-`
SENDING LABORAWIM"
E EQjV HNG LA 1,0
111-ism Laboratories, Inc.
Gulf Co-asl Analytical Lab ,
Inc.
P. 0. Pox 24043
7979 GSRl AVCMIC
Charlotte, NC 28224-0543
Baton Rou.ge, LA 70820
Phone: [phone]
Phone :[phone]
Fax: [phone]
Fax: (225.) 767-5717
ProJect Nlanager: Robbi A. Jones
7 7C)
37 6
Analysis Due Expires Laboratory ID Comments
Sample ID: 4070591-01 solid Suulpled-07/30/14 1.5 .:.04
Reactivity, Sullide (Sub) 08106114 15:04
Reactivity, Cyanide (Sub,) 08/13114 15:04
Containers Supplied.-
.Saniple.ID: 4070591-02
Reactivity. Sulfide (Sub)
Reactivity, Cyanide (Sub)
contuh - lers slipplied.
Solid
Sampleil:07/30/1.4 1.5:04
08106/14 15:04
08/13114-15:Q4
C1 Sample JD: 4070591-03 Solid Sampled:07/30f14 15;04
Reactivity, Sull'ide (Sub) 08/06/14 15:04
Reactivity, Cyanide (Sub) 08113114 15:04
COHI(Ih7el-S SHI)PUed.-
client ID: 4565 - Access Analytical
SDG: 214030
Due Date: 08/08114120
�I�I ll�lll li l l�1� �111
Released 13N. Daic lZfi%!ed 13Y (--
GC'1A j
'. i
kcicascd By Daw Jecci%ed B% Date
Released 11% 111tv Received lic Dale
I Page 31 of 32 1

I
j
SAMPLE RECEIVING CHECKLIST I IiI I��I ��III�11►����11il►�lllll���ll�l
II��Ilfllffl�f 11�lo e o i z o ,.
tas't fER�'LaRC9CdP :F,3 $0`iQ0
CFIECKUST
YES
NOI
Transport Method
Were all samples received using proper thermal preservation?(
!v
,4cceAnalytical
FEDEX
When used, were all custody seals intact?
_ . .
Were all samples received in proper containers?
f>r0ri1V� NUrnber
Received By
Were all samples received using proper chemical preservation?
__ +—I
;r 5
Saucier, Charlotte M.
Was preservative added to any container at the lab?
Were all containers received in good condition?
— t —I
--
;1._iim li:cni(s)
Receive Date(s)
. .............. ...._...—.....-- ...... ..... .-. __ .. .....
Were all VOA vials received with no head space?
J
I'
Solid
08/01/14
Do all sample labels match the Chain of Custody?
—
Did the Chain of Custody list the sampling technician?
--I
Was the COC maintained i.e. all signatures, dates and time of receipt included?
LAB PRESERVATIONS
.:0 L E R S
DISCREPANCIES
O.irbM Thermometer ID: E24
Temp(°C)
None
None
�I
I

RRJ'r� P
m
i Full Service Analytical 4:
Environmental Solutions
- LAB0RAI CRIES. INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No- 99012
NC Drinking Water Cart No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 08/11/2014
Prism Work Order: 4080182
Case Narrative
08/20/2014
This da!a pa(Aage cont airis Llle al, alyllca! resulLs IVI t! iJrUJ@l;t IUCnIIfICd abUVC dIIU III ;I L.1UEs d \idJC IVdII dIIVU, OdI I I It:
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543'
Phone: [phone] - Toll Free Number: 1-8001529-6364- Fax: [phone] Page 1 Of 7

ISM I Fu "-Service Analytical ;i
Eiraironmenial Solutions
Sample Receipt Summary
08/20/2014
Prism Work Order: 4080182
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime
4080182-01 Solid 08/11/14 08/11/14
Samples were received at 23.5 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spfingbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 7

Analytical 3 Laboratory Report
I Full -Service
PRISM I Environmental Solutions 08/20/2014
City of Statesville, NC Project: StaLime Client Sample ID: StaLime
Attn: Andy Smith Prism Sample ID: 4080182-01
P.O. Box 1111 Prism Work Order: 4080182
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/11/14 14:05
Time Submitted: 08/11/14 17:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
solids 62.9 % by 0.100 0-100 1 *SM2540 G 8114114 15:20 MJO P41-10259
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 8/12/14 12:50 MES P41-10213
Total Metals
Mercury
0.34
mgtkg dry
0.034
0.0056
1
*7471B
8114114 12:14
BGM
1341-110206
Arsenic
1.1
mg/kg dry
0.41
0.069
1
*6010C
8/18114 23.23
BGM
P41-110204
Cadmium
BRL
mgikg dry
0.41
0.0039
1
*6010C
8118/14 23:23
BGM
P41-10204
Copper
38
mg/kg dry
0.81
0.010
1
*6010C
8/18M4 23.23
BGM
P41`110204
Lead
12
mglkg dry
0.41
0.048
1
*6010C
8/18114 23:23
BGM
P41`110204
Mickel
83
mg1kg dry
1.6
0.013
1
*6010C
8118114 23:23
BGM
P41-110204
Selenium
BRL
mg/kg dry
0.81
0.098
1
*6010C
8/18114 23:23
BGM
P41-10204
Zinc
78
mglkg dry
4.1
0-028
1
*6010C
8/18M4 23:23
BGM
P41-10204
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P-O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-8001529-6364- Fax: [phone] Page 3 of 7

Level II QC Report
PRISM �Full-Service crvice Anzlytical &
environmental Solulicns
8/20/14
City of Statesville, NC Project: Stal-ime Prism Work Order: 4080182
Attn: Andy Smith Time Submitted: 8/11/2014 5:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P4HO204 - 3050B
Blank (P4H0204-BLK1)
---- — — -- - ... --- --
-----.-....--------------------
------
Prepared: 08/13/14 Analyzed: 08/18/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kq wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50.
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4H0204-BSI)
Prepared: 08/13/14 Analyzed: 08/18/14
Arsenic
23.9
0.25
mg/kg wet
25.13 95 80-120
Cadmium
24.1
0.25
mg/kg wet
25.13 96 80-120
Copper
25.6
0.50
mg/kg wet
25.13 102 80-120
Lead
24.2
025
mg/kg wet
25.13 96 80-120
Nickel
23.8
1.0
mg/kg wet
25.13 95 80-120
Selenium
23.8
0.50
mg/kg wet
25.13 95 80-120
Zinc
23.9
2.5
mg/kg wet
25.13 95 80-120
Batch P4H0206 - 7471 B
Blank (P4HO206-BLKI) Prepared: 08/13/14 Analyzed: 08/14/14
Mercury BRL 0.020 mg/kg wet
LCS (P411-10206-113SI) Prepared: 08/13/14 Analyzed: 08/14/14
Mercury 0.451 0.020 mg/kg wet 0.4167 108 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road'- P.O. Box 240543 -- Chartotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 4 of 7

- 18 •, I Full -Service Analytical &
Environment2l Solurir, r,s
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
8/20/14
Prism Work Order: 4080182
Time Submitted: 8/11/2014 5:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41i0259 - NO PREP
Blank (P4H0259-BLK1) Prepared & Analyzed: 08/14/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - charlotte; NC'28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 5 of 7

I M I Enviion en Analytical s
�-""ai s Eiwiro�imenc Solutions
Level II QC Report
8/20/14
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Prism Work Order: 4080182
Time Submitted: 8/11/2014 5:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P4H0213-BLK7)
----------- - -- ------
---
_ _ ..
Prepared & Analyzed: 08/12/14
-- -- ----- _ --- --------- ----- - ---- _ - -- .. ._.-...---------
Fecal Coliforms
BRL
02 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number
Batch
Initial
Final DateMime
4080182-01
P41-10204
1.96 g
50 mL 08/13/14 9:40
Prep Method: 7471B
Lab Number
Batch
Initial
Final DateMme
4080182-01
P41-10206
0.56 g
50 mL 08/13/14 10:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charioffe, NC.28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 7

CHAIN F CUSTODY ODY RECORD +� 33 ill Ell iyy�-�-3{S�'-i. F 3�
�� �
„� r•
r
rr
=t11+-S2n1i^:a An all;t;Cal &
Envirom-nentel SOILltiOnS
PAGE- OF QUOTE # TO (ENSURE PROPER BILLING.
1C VIA N/,
111 f ai,rNal,' -
O
b^.aar-h)
I
_
Samples lAG utmn -- -- _
L. e RATORIES, INC
Project Name:
j Fi LLIVC tl ON,I V(l [(,'I-? _
I�
449 S I gbrc`ok Road Char1011' M 1,7,1 ,`
short Hold Analysis: (Yes) (No) USTPro ect: (Yes) (NO)
I I I"E Lr V�UI c Lc�? - ------
1
�
, :
huse
f a-.
*Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Rece;vc_! �:+I fl IIN H )LDI � = TIMES?
] TACT?
Client Company Name: �, � i' o'd�. ; Ak
provisions and/or QC Requirements
C:USTOI Y s�.!;L.
Report To/Contact Name: .� n
Invoice To:
v ?L.A IL e 1 �llUU' I iL yli5f';�,C:E't _ ✓
Reporting Address: P 0; BoJ.
Address:
i EM Lr erm 0i')!Ft
TFh�^ Therm +rm I� Observed: i,p �I 'U I ca Ii �2)
/1;u
Phone:7,)Y-Y79- 3`11:�i' Fax Yes (NO): 7v.V- $7!� - +ge>s
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoD FL NC
EDD Type: PDF Excel Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days �:j Rushh Work dust Be
SC OTHER N/A
Site Location Name: L &1$^ 4 h e r—_ s _
Samples received after 14:00 will be processed next business day.
Water Chlorinated: YES_ h10_
Site Location Physical Address: L�r.1 f� n-.
Turnaround time is based on business days, excluding weekends and holidays.
SERVICES
�,� YJ.�•:Y 6ofY T` aft✓
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
p -
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
/ / G ;
PRESERVA- °� r;!
i
PRISM
LAB
CLIENT
DATE
COLLECTED
(SOIL,
` ti /`
TIVES ?j/ i
o /` REMARKS
SAMPLE DESCRIPTION
COLLECTED
MILITJi,RY
HOURS
WATER OR
SLUDGE)
*TYPE
j SEE BELOW I
NO.
SIZE
j
zo
1D NO.
S-eJ Z 1.
Sampler's Signature c k� = �° r� Sampled By (Print Name)
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed
submitted in writing to the Prism Project Manager. There will be charges for any chat
ReI'nq fished 8y: (Signature) ,,� Re pfp; vied By: (Suture)
P1
f`T'+
i4
Affiliation
the analyses as requested above. Any changes must be
after analyses have been initialized.
I `1 Military/Hours Additional Comments:
)f� 7 F111,3-1-
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAIN9.T1dOC UNTIL RECEIVED AT THE LABORATORY.
0 Fed Ex ❑ UPS Cl Hand -delivered *,ism Field Seryce 0 Other
NPDES: i UST: 1 GROUNDWATER: DRINKING WATER: ) SOLID WASTE: RCRA:
; CERCLA
LANDFILL
OTHER:
❑ NC ❑ SCI ❑ NC ❑ SC I ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC; ❑ NC ❑ SC
I
I ❑ NC ❑ SC
❑ NC ❑ SC
❑ ;❑ I® ❑ ❑ ❑
i❑
❑..
❑
*CONTAINER TYPE CODES: A = Amber C == Clear G= Glass P = Plastic; TL = Teflon -Lined Cap
VOA = Volatile Organics
Analysis (Zero Head Space)

402
NC Certification No.990 Case Narrative
SC Certification No. 99012 0.r
j Full -Service Analytical & NC Drinking Water Cert No. 37735
09/04/2014
rF--'R I SS MR i
Environmental Solutions VA Certification No.460211
_r-suralonie;. INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 08/25/2014
Statesville, NC 28687 Prism Work Order: 4080489
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Rabbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greaterthan 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 14

p _9 R a I Full -Service
PRISMp �a 3�
P.nalyutio 5,
Laboratory Report
�" 6 ll En�ironmentai
Solutions,
09/04/2014
City of Statesville, NC
Project: StaLime (Qtrly, Biweekly,
Client Sample ID:
Sta-Lime
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID:
4080489-01
P.O. Box 1111
Prism Work Order: 4080489
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter
Result
Units
Report
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
64.2
% by
0.100
0.100
1 •SM2540 G
8127114 15:40
MJO
P4H0507
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 'SM9221 E
8126/14 10:44
JHB
P4H0489
Total Metals
Mercury
0.26
mg/kg dry
0.031
0.0051
1 •7471113
8129114 12:63
BGM
P4H0508
Arsenic
4.7
mglkg dry
0.40
0.058
1 •6010C
912114 20.51
BGM
P4H0471
Cadmium
BRL
mg/kg dry
0.40
0.0038
1 '6010C
9/2/14 20:51
BGM
P41-10471
Copper
20 BH mg/kg dry
0.79
0.010
1 "6010C
912114 20:61
BGM
P4H0471
Lead
5.9
mglkg dry
0-40
0.046
1 '6010C
912114 20:51
BGM
P4H0471
Nickel
70
mglkg dry
1.6
0.013
1 '6010C
912114 20:51
BGM
P4H0471
Selenium
BRL
mg/kg dry
0.79
0.096
1 '6010C
9/2/14 20:51
BGM
P4H0471
Zinc
39
mg/kg dry
4.0
0-027
1 `6010C
912114 20:51
BGM
P4H0471
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc-
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 14

Laboratory Report
Ij� � p I EmiService al Solwi l &
�"`� `+ En'.ironmentSl Solution. _ 09/04/2014
City of Statesville, NC Project: Stal-ime (Qtrly, Biweekly, Client Sample ID: Sta-Lime
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4080489-02
P.O. Box 1111 Prism Work Order: 4080489
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
ro 5oiios oe_b / by 0.100 0.100 1 "SM2540 G 8/27114 15.40 MJO P4H0507
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 8/26/14 10:44 JHB P4H0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 14�

M I Full-Servien Analytical S
F rraircnmer�tal Snlu lions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly;
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/0412014
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-03
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DatelTime
ID
General Chemistry Parameters
Solids 70.3
% by
0.100
0.100 1
'SM2540 G 8127114 15:40 MJO
N4Hubut
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPNlg dry
0.3
1
'SM9221 E 8/26114 10:44 JHB
P4H0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-8001529-6364 - Fax: [phone] Page 5 of 14

I ".+' I Full -Service Analytical a
Hnvironniental Solulion=_
Laboratory Report
09/04/2014
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, Client Sample ID: Sta-Lime
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4080489-04
P.O. Box 1111 Prism Work Order: 4080489
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datelrime ID
General Chemistry Parameters
Solids 64.7 % by 0.100 0.100 1 "SM2540 G 8127/14 15:40 MJO P4H0507
Weight
(Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 8126114 10:44 JHB P4H0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-800/529-6364 -Fax: [phone] Page 6 Of 1444�

c, - 1 Full -Service Analytical &
Cnvim,m'ental Solution_
Laboratorry Report
09104/2014
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Sta-Lime
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4080489-05
P.O. Box 1111 Prism Work Order: 4080489
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 70.2 % by 0.100 0.100 1 "SM2540 G 8127114 16:40 MJO P41-10507
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN/g dry 0.3 1 'SM9221 E 8/26/14 10:44 JHB P41-10489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364- Fax: [phone] Page 7 of 14

q �n-dironinenta Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/04/2014
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-06
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 66.4
% by
0.160
0.100 1
"SM2540 G 8127114 15:40 MJO
P4H0507
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 8/26114 10.44 JHB
P4H0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 8 Of 14

Full -Service Analytical &
P. � S M I Environment, Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/04/2014
Client Sample ID: Sta-Lime
Prism Sample ID: 4080489-07
Prism Work Order: 4080489
Time Collected: 08/25/14 10:50
Time Submitted: 08/25/14 15:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
°lo Solids 69.7
-/o by
0.100
0.100 1
"SM2640 G 3127114 15:40 MJO
P4i5557
Weight
Microbiological Parameters
Fecal Colifonns BRL
MPN/g dry
0.3
1
*SM9221 E 8/26/14 10:44 JHB
P4H0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number:1-8001529-6364 - Fax: [phone] Page 9 of 14

Level II QC Report
R a tr i Fun -Service Analytical 9/4/14 ,
cm�ir.ninental Sob.rticns
Nc
City of Statesville, NC Project: Stal-ime (Qtdy, BiWeekly, 6ODay Prism Work Order: 4080489
Attn: Andy Smith 7 Fecal) Time Submitted: 8/25/2014 3:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4HO471 - 3050B
Blank (P41-110471-BLK1)
-- -- - - --
-- - _ ,..
- ---- --
---
Prepared: 08/27/14 Analyzed: 09/02/14
- - -- - -- - - --- -- ----- - -- - -- -
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
025
mg/kg wet
Copper
BRL
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (9P4H0471-BS1)
— --- ---- - -- - - -
------- -- . -- .
-- —
------
Prepared: 08/27/14 Analyzed: 09/02/14
- - - - — --.
Arsenic
22.1
025
mg/kg wet
25.00 88 80-120
Cadmium
22.8
0.25
mg/kg wet
25.00 91 80-120
Copper
23,5
0.50
mg/kg wet
25.00 94 80-120
Lead
22.6
0.25
mg/kg wet
25.00 90 80-120
Nickel
21.8
1.0
mg/kg wet
25.00 87 80-120
Selenium
22.4
0.50
mg/kg wet
25.00 89 80-120
Zinc
22.8
2.5
mg/kg wet
25.00 91 80-120
Batch P4HO508 - 7471 B
Blank (P4H0508-BLK1I) Prepared: 08/28/14 Analyzed: 08/29/14
Mercury BRL 0.020 mg/kg wet
LCS (P4HO608-BS1) Prepared: 08/28/14 Analyzed: 08/29/14
Mercury 0.436 0.020 mg/kg wet 0.4167 105 M120
Matrix Spike (P4H0508-MS7) Source: 4080489-01 Prepared: 08/28/14 Analyzed: 08/29/14
----------
Mercury 0.826 0.031 mg/kg dry 0.6490 0.254 88 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 10 of 14

- I Ful-SovFlnxJ ud
Fnvironmenial Solutions ISM
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime (Qtdy, Biweekly, 6ODay
7 Fecal)
Level II QC Report
9/4/14
Prism Work Order: 4080489
Time Submitted: 8/25/2014 3:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4H0508 - 7471B
Matrix Spike Dup (P4H0508-MSD1) Source: 4080489-01 Prepared: 08/28/14 Analyzed: 08/29/14
Mercury 0.933 0.031 mg/kg dry 0.6490 0.254 105 80-120 12 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 246543 - Chariotte, NC 28224-0543
Phone: [phone] - Tall Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 14

- I SM I Fulvironmcretei-Service Ana1yti-1-a
. , EnJ Solutions
Level II QC Report
9/4/14
City of Statesville, NC Project: Stal-ime (Qtdy, BiWeekly, 60Day Prism Work Order: 4080489
Attn: Andy Smith 7 Fecal) Time Submitted: 8/25/2014 3:30:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4HO507 - NO PREP
Blank (M0507-BL6C1) Prepared & Analyzed: 08/27/14
-
-- - ----. - - --- -- ---- - --- - - - -
% Solids 100 0.100 % by Weig ht
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 14

Full -Service Analytical t'
biro iron mr_ntrl Sol uiions
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, 60Day
Attn: Andy Smith 7 Fecal)
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
914/14
Prism Work Order: 4080489
Time Submitted: 8/25/2014 3:30:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4H0489 - NO PREP
Blank (P41-110489-BLK1) Prepared & Analyzed: 08/26/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number
Batch
Initial
Final
DatefTime
4080489-01
P41-10471
1.97 g
50 mL
08/27/14 9:05
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateTme
4080489-01
P41-10508
0.6 g
50 mL
08/28/14 9:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P-O_ Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 13 of 14

ME on
F. `, s'... �S il� f'�r Q _...i J%' r,.. a'l.~..1¢17
S +, YES NO _:. NIA
iqi �i 1=uii-Ser�•ice P,nalytical �. - .. ��4 SoutiPAGE_oEQ4JOTl #To ENSURE PROPER BYLL�NG: Saml es lh1TAt f upon otrlval — —_--
O
LAf50rtHTGrIES, INC, tie( iv d bN JI T I:,F�
. .......,,4:� :3'rrlr�LjvYOG� %�iU2J �7:Q7!Ctt?, NC �p21-% Project Name: - —`'
9 Prtr )PL F P tt SEP\/ATIVFo mdi aced r-
i�i(aiie +'i?41 28-G3f4 F,),c 7041112.5-0409 Short Hold Analysis: (Yes) (No) UST Project: {Yes) (No) frrFl ie( V`Irll Hm I i(JLUINL TIMES:
;Please ATTACH any project specific reporting (QC LEVEL 1 it III IV)
Client Company Name: t o' I>'C.�`b'✓� pCD
rovisions and/or QC Requirements'i : _ _-_IL
Report To/Contact Name s:.a ��sav, a'�1 VO.0PE F, N d Utr/011l iICAI�SI 4rl_1 __ _��
Invoice To: � {�I-t,f�CRCc�NiNNCRSu cr -
Reporting Address: ��' b n j Address: _
TEMP Th•�rm ID.t c-J _::Utvsat--cJ: `aS�.0 rote its= 7Cf
Phone:I �' " a'SS< Fax es '(No): J 'mod purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days L! 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC-
EQD Type: PDF Excel ®therms "Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ Rush
esWork Be
Pre -Approved
SC OTI6ER NIA
Site Location Name: F17 f' ' °" u-: l; '`.it r !i )� Samples received after 14:00 will be processed next business day.
`�., ic`= A Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YEAS_ NO_
Site Location Physical Address:
U 3 F`I' M -g`' (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample iced Upon Collection: YES_ NO
ANALYSIS REQUESTED PRISM
TIME I MATRIX SAMPLE CONTAINER Nr j
CLIENT DATE COLLECTED (SOIL, PRESERVA• �� 1' e��%; �i i% REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MIL.lTARY WATER OR i *TYPE 1 NO, SIZE TIVES j l�4 .� t j ID NO,
HOURS SLUDGE) SEE BELOW I ! % ! �Z— i % — -
--
e� . v �� IN�.
I I I I I rw
I P.
4
I
z , Sampled B Print Name Wax 21 j;,r�_ Affiliation
Sampler's Signature ,�!.,i;� �� � �.a"..�� I P Y ( )
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be. arges for any changes after analyses have been initialized.
Relln wished By: (Signature y .� Re i ed By: (Sigptur) Date h9illtt
Jt:
imemuw or angnnen,. i 1 1. — ,..,.,. ..-'-"- - .---- - - - -
SAMPLES ARE N0TjjC CEPTED AND VERIFIED AGAINST CO3,1ATIL RECEIVED AT THE LABORATORY. 3
❑ Fed Ex ❑ UPS ❑Hand -delivered 5' Prlsm Field FervicP ❑ Other'
Nt'DES: UST: G t d DWATER: ! DRINKING WATER: I SOLI® WASTE: I RCRA: I CERCLA LANDFILL OTHER.
®NCOSC QNC OSC' ZINC - SC ®NC ❑SC ❑NC G]SC i aNCOSCI OONC ®SC C�NC CSC; ❑NC LlSC
0-1 0 I Q------- 1 p 10—. 1® I® —
"CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
� 'SEE`RE �RSE�ORk'

NC Certification No. 402
f SC Certification No. 99012 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No: 37735
¢I 09/19/2014
a � � � Environmental Solutions VA Certification No.460211
- ABOnATOPIEs INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 09/08/2014
Statesville, NC 28687 Prism Work Order: 4090114
This data package contains the analytical- results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone] Page 1 of 7

PRISM€t �i Sample Receipt Summary
ti 4 I g� Bp j Full -Service Analytical S
4� � i Environmeniel Solu tins 09/1 .9!2014,
Prism Work Order: 4090114
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 4090114-01 Solid 09/08/14 09/08/14
Samples were received at 21.9 degrees C. See case narrative for further information. -
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc-
449 Springbrook Road - P.O. Box 240643 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 7

K_ p p_� fl l I Full-S—icc A-Mylical
.3
Laboratory Report
llN"� 19i�"ak !P %Sr En ironmenl.al Soiutions
09/1912014
City of Statesville, NC
Project: Stal-ime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4090114-01
P.O. Box 1111
Prism Work Order: 4090114
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/08/14 10:15
Time Submitted: 09/08/14 12:25
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
73.2
% uy
0.100
0.100
1 "SM2540 G 9/10/14 15:05
JAB
P419165
Weight
Microbiological Parameters
Feral Coliforms-
BRL
MPN/g dry
0.3
1 'SM9221 E 919/14 9:20
JHB
P410134
Total Metals
Mercury
0.18
mg/kg dry
0.029
0.0047
1 "7471B 9M7/14 15.30
BGM
P410167
Arsenic
3.9
mg/kg dry
0.34
0.050
1 •6010C 9113114 0:26
BGM
P410146
Cadmium
BRL
mg/kg dry
0.34
0.0033
1 '6010C 9/13114 0:26
BGM
P410146
Copper
17
mg/kg dry
0.69
0.0086
1 *6010C 9M3114 0.26
BGM
P410146
Lead
5.8
mglkg dry
0.34
0.040
1 '6010C 9M3114 0:26
BGM
P410146
Nickel
63
mg/kg dry
1.4
0.011
1 •6010C 9H3114 0.26
BGM
P410146
Selenium
BRL
mg/kg dry
0.69
0.083
1 '6010C 9113/14 0:26
BGM
P410146
Zinc
28
mglkg dry
3.4
0.023
1 *6010C 9/13M4 0:26
BGM
P410146
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 7

rI M I Full -Service Analytical &
" fi Fmironm2nlci Solutions
Level II QC Report
9/19/14
City of Statesville, NC Project: Stal-ime Prism Work Order: 4090114
Attn: Andy Smith Time Submitted: 9/8/2014 12:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410146 - 3050B
Blank (P410146-BLK1)
Prepared: 09/10/14 Analyzed: 09/12/14
Arsenic
BRL
0.25
mglkg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P410146_BSI) — _ -
Prepared: 09/10/14 Analyzed_ 09/12/14
Arsenic
22.2
0.25
mglkg wet
25.00 89 80-120
Cadmium
22.4
0.25
mg/kg wet
25.00 90 80-120
Copper
23.5
0.50
mg/kg wet
25.00 94 80-1120
Lead
22.2
0.25
mg/kg wet
25.00 89 80-120
Nickel
22.0
1.0
mg1kg wet
25.00 88 80-120
Selenium
22.0
0.50
mg/kg wet
25.00 88 80-120
Zinc
22.8
2.5
mg/kg wet
25.00 91 M120
Batch P410167 - 7471 B
Blank (P410167-BLK1) Prepared & Analyzed: 09/17/14
Mercury BRL 0.020 mg/kg wet
LCS (P410167-BSI) Prepared & Analyzed: 09/17/14
Mercury 0.469 0.020 mg/kg wet 0.4167 112 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotfe, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 & 7

Fall -Service Analytical &
g 1 I Environmental Solutions
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II CSC Report
9/19/14
Prism Work Order: 4090114
Time Submitted: 9/8/2014 12:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410165 - Solids, Dry sleight
Blank (P410165-BLK1) Prepared & Analyzed: 09/10/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 -Fax: 704162"409 Page 5 of 7

Full -Service Anaiyticel 8
Environmental Solutions
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
9/19/14
Prism Work Order: 4090114
Time Submitted: 9/8/2014 12:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4101134 - NO PREP
Blank (P410134-BLK1) Prepared & Analyzed: 09/09/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Datefrime
4090114-01 P410165 30 g 30 g 09/10/14 15:05
Prep Method: 3050E
Lab Number Batch Initial Final Daterrime
4090114-01 P410146 1.99 g 50 mL 09/10/14 8:45
Prep Method: 7471B
Lab Number Batch Initial Final DatelTme
4090114-01 1`410167 0.57 g 50 mL 09/17/14 11:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 6 of 7

1-Ulf-Cieivic lyl-alytical c4
�1
55f�i I Envirotlme'ital
Si,{UttQ11S
... ..i 1.......
.:. LABORATORIES. INC.
4-40 pringimook Road - Charloti::, NC:
2s217
Phone [phone]•636A, Fat:: 7041525-:14019
a
Client Company Name: f r ' , '.r F�d
Report To/Contact Name is ;v "
Reporting Address: q . 9 `'y
PAGE_ OF _ QUOTE # TO (ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (II UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111 III IV)
provisions and/or QC Requirements
Invoice To:
Address:
YES 1VU
NiA 4-
Samples If,]TACT up.bn arrival %
_ ✓ ,_- .._
-_.__ O
Received QN yIJ i II. E'Y.
_
--
PP.'OPL(, PRESERVATWES .l idir-ated r
C US ODY SEALS 11vTAC:T9
-_— __--
VOLATILES td j JIIGt 'f I I[ tll 3PAC t "
-
PROPER ( OPI f4MNERS. USEC
_TLMP' ThCrrn lD:'_i (�` _ Observed:
gi y t l C r
Fax' YeS'] (No): r_',ry ;I • z•` ;,'t"• ?F ' r,"
..,.._ Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF_E)ccel_Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
SIC_ OTHER
NIA
q
Site Location Name: yf' n. z "T' T, S) + e r' "a:' •;" ' a Samples received after 14:00 will be processed next business day.
r. Turnaround time Is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
Yi>
Site Location Physical Address:daY„ r' `. r .i, art ' .� a % -' " (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES_
NO
;�'a t'''Cq,•�"""r;;;r;-,..,'g°(1a• 7�,d ('b RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
; / %
PRISM
CLIENT
DATE COLLECTED (SOIL,
PRESERVA-
.r j /' �'
/ REMARKS
LAB
"TYPE No. SIZE
SAMPLE DESCRIPTION
COLLECTED MILITARY WATER OR
T1VES
,yl•i'"•l / r!a / %"/
ID NO.
HOURS SLUDGE)
SEE BELOW
' •'�
*"-" r_ ' f
) .
I
_1
G�""
7's _ _,r.. LL
1 �.
- ----
' i'
---
t;t. .r` ,`,
_
_
"'�,� ,.•d'f.J'Pi'.n f,;,r
1.
i..,Ntp--4
�—
�••'•.
__
_ _ __
1—.—_
I
i
I
I
Sampler's Signature' as „ led By (Print Name) .•' ° :" P e Affiliation
Samp
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
``�
submitted in writing to the Prism Protect Manager. There will be charges for any changes after analyses have been initialized.
BiL�isrS�il�a .,
Relinquished y: , ignature.) ec iv By: Signature DaSe Military/Hours Additional Comments.
r
- Time:.
cR iv�ITn
P.ellnqu • ed By: (Signature) x� Received By: (Signature) Date
Sale i) harlUrm i'Ime
i Z-Z.
t l
FiUd h Fe,_,,
(X
Relin y: (Signetu a Received For, s Laboratori ; S,✓ Date /
1ec - - _ _ ____•f,-,
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CJJSTODY SEALS FOR TRANSPORTATION I THE LABORATORY. CDC Group No,
- - --
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COC��f I!IL RECEIVED AT THE LABORATORY.
v
1�t _'
V)
❑ Fed Ex El ❑ Hand -delivered Wfism Field Servie:e ❑ Other
TER. DRINKING WATER. SOLID WASTE: RALANDFILL
e
❑AC ❑ SC❑ ❑ SC❑NNC ❑ SC ❑NCOSC El NC ❑ SC ❑ NC ❑SC I ❑ NC ®SC
P
Ira n n 0 ❑ ❑ ❑ ❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No.
990 Haase Narrative
SC Certification No. 99012 boo Narrative
�--�Full-Service Analytical Lt NC Drinking Water Cert No. 37735
P it � NA
, Environmental Solutions VA Certification No. 460211 10/01/2014
L ABORATORIr INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOhEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: Stal-ime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 09/23/2014
Statesville, NC 28687 Prism Work Order: 4090361
Thic rin n nnrknna rnnfninc the gnnlvtiral rpciiltc fnrthp nrnipr-t iripntifipri ahnvp nnri inrJ"ripc n Cacti Nnrrativr Samnlp
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
)� t�- a- av--
RObbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364-Fax:[phone] Page 1 Of7

Full -Service Analytical S
g_ y 1 Envirorimenial Solutions
Sample Receipt Summary
10/01/2014
Prism Work Order: 4090361
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta Lime 4090361-01 Solid 09/22/14 09/23/14
Samples were received at 21.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook, Road - P.O. Box 240543 - Charlotte, NC,28224-Q543 ,
Phone_ 704/629-6364 - Toll Free Number:1-8001529-6364 - Fax: [phone] Page 2 Of 7

Hull -Service Aneiytica!
Envi;cnmcntal Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
10/0112014
Project: Stal-ime Client Sample ID: . Sta Lime
Prism Sample ID: 4090361-01
Prism Work Order: 4090361
Sample Matrix: Solid Time Collected: 09/22/14 11:00
Time Submitted: 09/23/14 10:05
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
77.6
1 by
0.100
0-100
1
*SM2540 G
9124/14 1s:00
Mj0
PM0379
Weight
(Microbiological Parameters
Fecal Coliforms
BRL
MPNlg dry
0.3
1
*SM9221 E
9/23/14 10:33
JHB
P410367
Total Metals
Mercury
0.13
mglkg dry
0.027
0.0045
1
*7471B
9126114 15:06
BGM
P410406
Arsenic
4.6
mglkg dry
0.32
0.046
1
*6010C
9129M4 16:07
BGM
P410413
Cadmium
BRL
mglkg dry
0.32
0.0030
1
*6010C
9/29114 16:07
BGM
P410413
Copper
27
mg/kg dry
0.63
0.0080
1
*6010C
9129114 16:07
BGM
P410413
Lead
5.3
mg/kg dry
0.32
0.037
1
*6010C
9129114 16:07
BGM
P410413
Nickel
84 BN
mg/kg dry
1.3
0.010
1
*6010C
9129114 16:07
BGM
P410413
Selenium
2-2
mglkg dry
0.63
0-077
1
*6010C
9129114 16:07
BGM
P410413
Zinc
41 BH
mg/kg dry
3.2
0.022
1
*6010C
9129114 16:07
BGM
P410413
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449.Springbrook Road - P.O_ Box 240543 -,Charlotte, NG 28224-0543,.
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone] Page 3 of 7

i Full -Service Analytical &
a S M 1 Environmental Solutions
Level II CSC Report
1011 /14
City of Statesville, NC Project: Stal-ime Prism Work Order: 4090361
Attn: Andy Smith Time Submitted: 9/23/2014 10:05:00AM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410406 - 7471 B
Blank (P410406-BLK1)
Prepared & Analyzed: 09/26/14
Mercury
BRL
0.020
mg/kg wet
LCS (P410406-BSI)
Prepared & Analyzed: 09/26/14
Mercury
0.471
0.020
mg/kg wet
0.4167 113 80-120
Batch P410413 - 3050B
Blank (P410413-BLK1) _ --
- - -----
-- -- --
-_- --
Prepared: 09/26/14 Analyzed: 09/29/14- - - - - _--
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
2.44
1.0
mg/kg wet
BH
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
BH
LCS (P410413-BSI)
-- - -- - - -- - - ----- ---
- - - - --- --- -
-------------
-------
Prepared: 09/26/14 Analyzed: 09/29/14
- -- - ----- - --------------- - ---- ----
Arsenic .
24.2
0.25
mg/kg wet
25.00 97 80-120
Cadmium
24.2
0.25
mg/kg wet
25.00 97 80-120
Copper
25.8
0.50
mg/kg wet
25.00 103 80-120
Lead
24.1
0.25
mg/kg wet
25.00 96 80-120
Nickel
24.3
1.0
mg/kg wet
25.00 97 80-120
Selenium
24.2
0.50
mg/kg wet
25.00 97 80-120
Zinc
25.5
2.5
mg/kg wet
25.00 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449. Springbrook Road - P.O. Box 240543 - Charlotte,. NC 23224-0543. ,
Phone: [phone] - Toll Free Number 1-8001529-6364 - Fax: [phone] Page 4 Of 7

{ g S I Full -Service Analytical s
�" �" Environmenia! Solutions
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
10/1/14
Prism Work Order: 4090361
Time Submitted: 9/23/2014 10:05:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410379 - Solids, Dry Weight
ESiank (P4i0379-uLKi) Prepared & Analyzed: U9/Z4/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
_ .449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2822470543.
Phone: [phone] - Toll Free Number 1-8001529-6364 - Fax: [phone] Page 5 Of 7

SMI Full-Se-i—s Analyiical &
RRIEnvi,owncnEal Sohutions
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
1011/14
Prism Work Order: 4090361
Time Submitted: 9/23/2014 10:05:00AM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P410367 - NO PREP
Blank (PM0367-BLKII) Prepared & Analyzed: 09/23/14
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry !Weight
Lab Number Batch
Initial
Final
Date/Time
4090361-01 P410379
30 g
30 g
09/24/14 15:00
Prep Method: 3050E
Lab Number Batch
Initial
Final
DateTme
4090361-01 P410413
2.03 g
50 mL
09/26/14 9:00
Prep Method: 7471B
Lab Number Batch
Initial
Final
Date/Time
4090361-01 P410406
0.57 g
50 mL
09/26/14 10:28
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O_ Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 7

"Illy RECORD��TO
CHANN
�
tY�'r_
ull-, n icr An>ly`:al
1 4� st • t7 I �•;7,1
t1 Cr:irOruTCnil SUR�Ifors PAGE OF tOPEBILLING:UOTE#TP
r
�I Sain iee. ITACf upon affixis p
-r, i
I AW.-R ,TORTES. INC.
-N_C
_ --
iC coit (-d 0J I i dFl ICE?. - ---
> „.
14' ;t rringbrook'ito<Ir1 , char:c,te, NC ;.92l Project Name: UST Project: (Yes) (NO)
> WS29-S3^o4 -ax: U rlsz5•u.;T,e Short Hold Analysis: (Yes) (NO)
� �
PROP R 13EPVAI 1)E8 Indicted' / a
f
/
hane
rHOLD!
�• ` *Please
Client Company Name: � i �e 04, ..$ a r',s" �'� lie
ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Requirements
zc F.I e VI r4111� HUJ tI I iC 71PrFJ _ d
.CLJ TtDY `;t '+I 5 ItiTA
provisions
and/or QC
Report To/Contact Nature: r •�i a :�+.I �Va
p --� Invoice
To:
Lvl �1TILi_S roc' WIOU I HE,,-\DSPACE,,_
OrtonU Address: P. a� : oa' �9 % d
Re=.
p Address:
LPROPER r C 0!!T (P1Cf us d
-ILMI / t Ub,eleed.,1� �'_-°( ICI rr u1(S °Cf
r
T, e•nl:lf3_��J
Phone:&IJ 7 R- 34 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL,
Email Address: Requested Due Date '> 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF E)ccel Other 'Working
Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Mdust Be
SC_ OTI TER N/A
Site Location Name: Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
Site !Location Physical Address:
(SEE REVERSE FOR TERMS E CONDITIONS REGARDING SERVICES
Sampie Iced Upon Collection: YES NO
p
BY PRISM LABORATORIES, INC. TO CLIENT)
—
TIME:
MATRIX
SAMPLE CONTAINER
I
PRESERVA-
ANALYSIS REQUESTED
ANALYSIS
/ / i /
�,
PRISM
LAB
CLIENT
DATE
COLLECTED
MILITARY
(S(?IL,
WATER OR
*TYPE
TIVES°
/ �� REMARKS
; % /
ID NO.
SAMPLE DESCRIPTION 1
COLLECTED
HOURS
SLUDGE)
SEE BELOW i NO. SIZE
.
Xel
i
v
N S�03 I i I :" vie- � l v
L P I ; C
0
`s I
Sampler's Signature �tl' �'��..7rCr� _ I Sampled By (Print Name) �+ y',t'IV i Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
I Comments:
/0-6
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST,6,,0t UNTIL RECEIVED AT THE LABORATORY. t j
❑ Fed Ex ❑ UPS ❑ Hand -delivered L ,rism Field Service ❑ Other t,.
NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: j RCRA: I CERCLA LANDFILL OTHER:
❑IVC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SCi El NC ❑SC ❑NC ❑SC, ❑NC 05C
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
SE��kE
ERMS 8°CQILD_I.Sl��

NC Certification No. 402 NItl��r�tlV�
SC Certification No. 99012 Case
n Full -Service Analytical & NC Drinking Water Cert No. 37735 10/14/2014
Environmental Solutions VA Certification No. 460211
goon>mnies rar. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOIIEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 10/07/2014
Statesville, NC 28687 Prism Work Order: 4100092
I - "Mato paCiiagc Cv^toi^� u c u��uly uC.c.l rco — for "'- project Id.-..ntofied 2b3.... ...^d 6,c.1t:de.. r.'.2.,­ N� +n CMmple
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road'- P.O. Box 240543 - Chadofle, NC 28224-0643
Phone: [phone] - Toll Free Number: 11-8001529-6364 -Fax: [phone] Page 1 of %

! Full-Seict0 &PRISM!
RIMEn vironmer;al S01utlns
Sample Receipt Summary
10/14/2014
Prism Work Order: 4100092
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 4100092-01 Solid 10/06/14 10/07/14
Samples were received at 19.9 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449.Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 -. -
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax_ 7041525-0409 Page 2 Of 7

Laboratory Report
Environmental Solutions 10/14/2014
PRISM 1
City of Statesville, NC
Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4100092-01
P.O. Box 1111
Prism Work Order: 4100092
Statesville, NC 28687
Sample Matrix: Solid Time Collected: 10/06/14 12:20
Time Submitted: 10/07/14 07:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
of se!ids
69.0
of LY
n inn
n 1nn
1
*c M2640 G
10!V14 17•05
MjO
P4J6104
Weight
Microbiological Parameters
Fecal Col -dorms
BRL
MPN/g dry
0.3
1
*SM9221 E
10/7114 11:52
JHB
P4J0161
Total Metals
Mercury
0.31
mg/kg dry
0-029
0-0049
1
*7471B
1018114 13:21
BGM
P4J0093
Arsenic
4.6
mglkg dry
0.37
0.064
1
*6010C
10/11/14 1:25
BGM
P4J0125
Cadmium
BRL
mglkg dry
0.37
0.0035
1
*6010C
10/11/14 1:25
BGM
P4J0125
Copper
16
mglkg dry
0.74
0.0093
1
*6010C
10/11/14 1:25
BGM
P4J0125
Lead
6.0
mglkg dry
0.37
0.043
1
*6010C
10111/14 1:25
BGM
P4J0125
Nickel
63
mglkg dry
1.5
0.012
1
*6010C
10/11/14 1:25
BGM
P4J0125
Selenium
BRL
mg/kg dry
0.74
0.089
1
*6010C
10/11114 1:25
BGM
P4J0125
Zinc
29
mglkg dry
3.7
0.025
1
*6010C
10/11/14 1:25
BGM
P4J0125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.Q. Box 240543 - Charlotte; NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 7

rr"t
d 4 I Cull -Service finuUal &
EnvironSoI
mental Sotui�ons
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box '1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
10/14/14
Prism Work Order: 4100092
Time Submitted: 10/7/2014 7:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4J0093 - 7471 B
Blank (P4J0093-BLK9) Prepared: 10/07/14 Analyzed: 10/08/14
Mercury BRL 0.020 mg/kg wet
LCS (P4J0093-BSI) Prepared: 10/07/14 Analyzed: 10/08/14
Mercury 0.441 0.020 mg/kg wet 0.4167 106 80-120
Batch P4J0125 - 3650B
Blank --(P4J0125-BLK1)
------------------------------------------------
Prepared: 10/09/14 Analyzed: 10/11/14
--------------------------- ------------------
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4JO125-BSI)
Prepared: 10/09/14 Analyzed: 10/11/14
Arsenic
25.0.
0.25
mg/kg wet
25.00 100 80-120
Cadmium
25.5
0.25
mg/kg wet
25.00 102 80-120
Copper
26.2
0.50
mg/kg wet
25.00 105 80-120
Lead
25.3
0.25
mg/kg wet
25.00 101 M120
Nickel
25.2
1.0
mg/kg wet
25.00 101 80-120
Selenium
25.3
0.50
mg/kg wet
25.00 101 80-120
Zinc
25.9
2.5
mg/kg wet
25.00 104 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543 ,
Phone: [phone] -Toll Free Number 1-8001529-6364 -Fax: [phone] Page 4 Of %

I'9 H 9 I Full -Service Analytical
Environmental Solutions
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
10/14/14
Prism Work Order: 4100092
Time Submitted: 10/7/2014 7:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4JO104 - Solids, Dry Weight
Blank (P4J0104-BLK1) Prepared & Analyzed: 10/07/14
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
.O. Box 240543 - Charlotte, NC 28224-0543 449 Springbrook Road - P
Phone: [phone] - Toll Free Number: 1-800/629-6364- Fax: [phone] Page 5 of 7

- Level 11 QC Report
RRR IFull-Servier aj sol i io s
Environmental Solutions
10/14/14
City of Statesville, NC
Project:
StaLime
Prism Work Order: 4100092
Attn: Andy Smith
Time Submitted: 10/7/2014 7:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P4J0161 - NO PREP
Blank (P4J0161-BLK1}
Prepared & Analyzed: 10/07/14
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
4100092-01 P4J0104
30 g
30 g
10/07/14 17:05
Prep Method: 3050E
Lab Number Batch
Initial
Final
DateTme
4100092-01 P4J0125
1.97 g
50 mL
10/09/14 8:00
Prep Method: 7471B
Lab Number Batch
Initial
Final
DateTme
4100092-01 P4J0093
0.59 g
50 mL
10/07/14 13:20
This report should not be reproduced, except in its entirety, Without the written consent of Prism Laboratories, Inc.
"- 449 Springbrook Road - P.O. Box240543 - Charlotte, NC 28224>0643`
Phone: [phone] -Toll Free Number: 1-8001529-6364 -Fax: [phone] Page 6 Of 7

t 6 Full -Service
j 5 (ht �r.1 ai t 7� Ij f U(,-SefV lC.a :':n afyi'ICoi &
Ezi Ironrrpnta( Snlilifons
L•'.zns M conies. INC
4-191?,Pringblook Road • i,';is:l< tliy tic �3217
Phcne 70415 9-fi'C.,rl. .. Fax: I'10 52S-i 40t)
Client Company Name: nf
Report To/Contact Name x't vi 1 o , r i �-s
Reporting Address: !' a,;.,
�� �' '�ry �"�+� tiy.-. ,�,a �A,� � ga� �1.Ff �s�- �� �, "�i-. `'•�� i � a1�
PAGE_ OF— QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
'Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
YEC NO. NIA
Semmes INTACT up on,srrival? _
Received CAN Y" r ICE? I ~
- - - _-= N
-- -- -- to
Received V'•ATI 11N I IOLDING TIPdIEu^ . X _.....
Il
C:USTO_'rf SEALS iN.':TACT % --- _'
OL. i l F u ret LI VIUOUT -1 ADSPACE? J I
PROPER I .h ICON MINERS used?
x
l -tvl l Therm In
Phone: ` e"I '"3 i 6- ' ei s purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL. -
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days 114 Days O 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF_Excel Other "Working Days" O 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
T— Pre -Approved
SC OTHER N/A.
t.
Site Location Name: ,,i r" J^ ;=• , ` ' c' +- = : - r a Samples received after 14:00 will be processed next business day.
Se> a, r ,} y Turnaround time is based on business days, excluding weekends and holidays.
Site Location Physical Address: a "�" i'
Water Chlorinated: YES_ NO _
(SEE REVERSE DING SERVICES
TERMS & ES
�1`
Sample Iced Upon Collection: YES_ NO
;r'3::!,•;rF , t';" a,• . j`•; ,.�' :'`'x'/�,' RENDERED BY PRRISM LABORATORIINC. TO CNS LIENT)
j TIME MATRIX
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
i
/ ` `• r / i PRISM
CLIENT
DATE COLLECTED (SOIL,
1 .,r/ % REMARKS LAB
/
SAMPLE DESCRIPTION
COLLECTED I MILITARY I WATER OR
"TYPE
NO.
SIZE
TIVES
y,1'
/ a.` / / i
i' / j' ID NO.
HOURS I SLUDGE
SEE BELOW
:-.,�4.:-L.i ,1� 'r'"F f"
1Y! -�-/ 7 I /✓( •r ui 1d
S.R
!}&
�;i . tri�
i I
'
I
I •
Sampler's Signature Sampled By (Print Name) A, r,? t• :+' 1 -. i' Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the✓analyses as requested above. Any changes must be ` v I•}' wV,
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.e�'txit.:
Relinquished By: (Signature) - RercNved By: 4Signatur �� Date Millta�lHours Additional Comments: sit/ 1rnyaL:Tinle -
RelingtU hed By. (Signature) „r 17ec6146 y: (Signature) Date pit" 11t oartUCC 1 WMt
....-...... ,...
-. 7'\ ` �1 •�' ' !i�'� f 7C!
,l IaIc.1 TBCtI Fee:,.
P.elinqub;h y: (Signatures :• Recce d For Prism 1� orat�ries By: Date
Method of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY EALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.----•----------"----------�
7
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COO UNTIL RE EIVED AT THE LABORATORY.
❑ Fed Ex ❑UPS ❑ Hand -delivered 14ftrn Field Service ❑ Other/'r
NPDES: I UST: G NDWATER:: DRINKING WATER: SOLID WASTE: RC A: CERCLA LANDFILL OTHER:
❑NC❑SC ❑NC OSC ❑i C El SC ❑NC ❑SC ❑NC El SC ❑NC❑SC ❑NC ❑SCi❑NC ❑SC ❑NC ❑SC
n rI n ❑ ❑ ❑ LI . ❑ ❑
"CONTAINER TYPE CODES: A = Amber C Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402
SC Certification No. 99012 Case Narrative
I
NC Drinking Water Cart No. 37735Full-Service Analyti.,ai & 10/27/2014
a M i Environmental Solutionc VA Certification No.460211
n3oanTories. INC,DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/I EC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 10/20/2014
Statesville, NC 28687 Prism Work Order: 4100396
ThisThis data package non+aino the anaL,tiro1 r J+c for .. ect identified ak—n and innL„Icc a C'acc I�larra+iva Camnlo
......... p..........y.. .....�....... ..... ... ... .....�...,,.........v......... the p.r".j........... �......., .....,... ... ..... ........ ... .L....
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
D RPD value outside of the control limits.
DM Sample diluted and RL increased due to the matrix.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results arereported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road .-P.O. Box 240643 -Charlotte,. NC 28224-0543,
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Pape Of 4

Laboratory Report
FuII-Service
Analytical 3
} a Ertv,wc ,enlal
. ... v,tnrrmnues'. ras
Solutions
1012712014
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Sta-Lime
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4100396-01
P.O. Box 1111
Prism Work Order: 4100396
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/20/14 10:40
Time Submitted: 10/20/14 14:50
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateTme
ID
General Chemistry Parameters
Solids
81.2 % by
n 4nn
n inn
a •cMgsan r. ennzwe 13:45 MjO
v&1naY1
Weight
Microbiological Parameters
Fecal Colifonns
BRL MPN/g dry
0.2
1 *SM9221 E 10/21/14 10:39 JHB
P4J0432
Total Metals
Mercury
0.10 mglkg dry
0.027
0.0044
1 *747113 10/24/14 17.16 BGM
P4J0391
Arsenic
4.8 DM mglkg dry
1.6
0.22
5 *6010C 10122/14 18:32 BGM
P4J0390
Cadmium
BRLDM mg/kg dry
1.6
0.22
5 *6010C 10/22/14 18:32 BGM
' P4J0390
Copper
20 DM mglkg dry
3.1
0.57
5 *6010C 10/22114 18.32 BGM
P4J0390
Lead
9.2 DM mglkg dry
1.6
0.24
5 *6010C 19/22/14 18:32 BGM
P4J0390
Nickel
100 DM mglkg dry
6.2
0.80
5 *6010C 10/22/14 18.32 BGM
P4J0390
Selenium
BRLDM mg/kg dry
3.1
0.37
5 *6010C 10/22/14 18:32 BGM
P4J0390
Zinc
32 DM mglkg dry
16
3.4
5 *6010C 10122/14 18.32 BGM
P4J0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449-Springbrook Road.-. P.O. Box,240543 - Charlotte, NC 28224-0.543_.; .. ,
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 3 of 14

Full-Sevice Analyticals
PRISMEnionmnal S.utions
Laboratory Report
10127/2014
City of Statesville, NC Project: Stal-ime (Qtrly, Biweekly, Client Sample ID: Fecal #2
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4100396-02
P.O. Box 1111 Prism Work Order: 4100396
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/20114 10:40
Time Submitted: 10/20/14 14:50'
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 83.8 % by 0.100 0.100 1 `SM2540 G 10/23114 13:45 MJO P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O-. Box 240543.- Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800152M364 - Fax: [phone] Page 4 Of 4

Laboratory Report
F U!I-Service
Analytical /s
_,
-PR�,3 wironmantal
c
Solutions
10/27/2014
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #3
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4100396-03
P.O. Box 1111
Prism Work Order: 4100396
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/20/14 10:40
Time Submitted: 10/20/14 14:50
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateMme ID
General Chemistry Parameters
Solids
73.6 % by 0.109 0.100
1 "SM2540 G 10/23/14 13:45 MJO 134J0422
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3
1 'SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte,.NC 28224-0543 „
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 14

PRISM7� p _ � " gj � I Fun1- nice An alylical &
�", �"'� � ¢ H 4�� IPid Environmental Snluiion=_
Laboratory Report
10/27/2014
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #4
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4100396-04
P.O. Box 1111 Prism Work Order: 4100396
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/20114 10:40
Time Submitted: 10/20/14 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
Solids 80.6 % by 0.100 0.100 1 •StlM2540 G 10/23/14 13:45 MJO P4J0422
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN/g dry 0.2 1 'SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543,.
Phone: [phone] - Toll Free Number. 1-800/529-6364 - Fax: [phone] Page 6 of 14

Full. Sen;ice Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
10/2712014
Client Sample ID: Fecal #5
Prism Sample ID: 4100396-05
Prism Work Order: 4100396
Time Collected: 10/20/14 10:40
Time Submitted: 10/20/14 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 84-6 % by 0-100 0-100 1 "SM2540 G 10/23/14 13-45 IiRJO P4J0422
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 10/21/14 10:39 JHB P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543 - --
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 14

Laboratory Report
ppp�aa � ,�s� m
FWI-Sl0 p� e�
An
En,k..ry
� Environ mental
ol.tinl
Solutions
10/27/2014
City of Statesville, NC
Project: StaLime (Qtrly, Biweekly,
Client Sample ID: Fecal #6
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4100396-06
P.O. Box 1111
Prism work Order: 4100396
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/20/14 10:40
Time Submitted: 10/20/14 14:50
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
73.0 % by
n.1nn n_1nn
1 •-gRA2tan r_ 1n/23114 12•45 Wain
P410422
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 10/21/14 10:39 JHB
P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road-- P.O. Box 240543 - Charlotte, NC-28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 14

-� �� roil -Service �.nalytical
I Sr Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
10/27/2014
Client Sample ID: Fecal #7
Prism Sample ID: 4100396-07
Prism Work Order: 4100396
Time Collected: 10/20/14 10:40
Time Submitted: 10/20/14 14:50
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
Solids
84.6 % by
n ann
n ann i *snc7c40 i- annzwa VI-Ar R5.1n
PdJ0977
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 *SM9221 E 10/21/14 10:39 JHB
P4J0432
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449'SipringbrookRoad - P.O. Box 240543 - Charlotte; NC28224-0543,- + . - ^ • -'
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 9 of 14

I M I ni!I-Service Anelytical &
l Environmental Solutions
Level II QC Report
10/27/14
City of Statesville, NC Project: StaLime (Qtdy, Biweekly, 6ODay Prism Work Order: 4100396
Attn: Andy Smith 7 Fecal) Time Submitted: 10/20/2014 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4J0390 - 3050B
Blank (1P4J0390-BLK1) -- ---
-
- - _
Prepared &Analyzed: ---- 14
-
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4J0390-113SI) _-
Prepared &Analyzed: 10/22/14
_
Arsenic
23.2
0.25
mg/kg wet
25.00 93
80-120
Cadmium
23.4
0.25
mg/kg wet
25.00 93
8D-120
Copper
24.4
0.50
mg/kg wet
25.00 98
80-120
Lead
23.2
0.25
mg/kg wet
25.00 93
80-120
Nickel
23.2
1.0
mg/kg wet
25.00 93
M120
Selenium
23.3
0.50
mg/kg wet
25.00 93
80-120
Zinc
23.3
2.5
mg/kg wet
25.00 93
80-120
Matrix Spike (P4J0390-MS1) _
- ---- - - -
_ Source:4100396-01
Prepared&Analyzed:l0/22/14__
Arsenic
21.6
0.31
mg/kg dry
30.94 4.75 54
75-125
Cadmium
12.6
0.31
mg/kg dry
30.94 BRL 41
75-125
Copper
32.4
0.62
mg/kg dry
30.94 20.3 39
75-125
Lead
18.8
0.31
mg/kg dry
30.94 9.23 31
75-125
Nickel
82.2
1.2
mg/kg dry
30.94 103 NR
75-125
Selenium
14.5
0.62
mg/kg dry
30.94 BRL 47
75-125
Zinc
42.1
3.1
mg/kg dry
30.94 32.2 32
75-125
Matrix Spike Dup (P4J0390=MSD1)
Source: 4100396-01_
Prepared &Analyzed: 10/22/14
Arsenic
27.7
0.31
mg/kg dry
31.26 4.75 73
75-125
25
20
Cadmium
16.4
0.31
mg/kg dry
31.26 BRL 53
75-125
26
20
Copper
44.3
0.63
mg/kg dry
31.26 20.3 77
75-125
31
20
Lead
23.1
0.31
mg/kg dry
31.26 9-23 44
75-125
21
20
Nickel
102
1.3
mg/kg dry
31.26 103 NR
75-125
22
20
Selenium
25.8
0.63
mg/kg dry
31.26 BRL 82
75-125
56
20
Zinc
59.9
3.1
mg/kg dry
31.26 32.2 89
75-125
35
20
MI
MI
MI
MI
MI
MI
MI
- -D, MI
D, MI
D, MI
D, MI
D, MI
D. MI
D, MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road P.O. Box 240543 - Charlotte, NC 28224-0543 .
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax_ 7041525-0409 Page 10 Of 14

I p� � I Envi Serviceal Solna s
✓? 144f2 � Environ menial Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime (Qidy, Biweekly, 60Day
7 Fecal)
Level II QC Report
10/27/14
Prism Work Order: 4100396
Time Submitted: 10/20/2014 2:50:OOPM
Reporting
Spike Source
%REC RPD
Analyte.
Result
Limit
Units
Level Result %REC
Limits RPD Limit
Notes
Batch MOM - 3050B
Post Spike (P4J0390-PS1)
Source: 4100396-01
Prepared &Analyzed: 10/22/14
Arsenic
0.928
mg/L
1.000 0.154 77
80-120
MI
Cadmium
0.556
mg/L
1.000 0.000791 56
80-120
MI
Copper
1.30
mg/L
1.000 0.658 64
80-120
MI
Lead
0.772
mg/L
1.000 0.300 47
80-120
MI
Nickel
2.85
mg/L
1.000 3.36 NR
80-120
MI
Selenium
0.672
mg/L
1.000-0.0609 67
80-120
MI
Zinc
1.58
mg/L
1.000 1.04 54
80-120
MI
Batch P4J0391 - 7471 B
Blank (P4J0391-BLK1)
Prepared & Analyzed: 1 D/24/14
Mercury
BRL
0.020
mg/kg wet
LCS (P4J0391-BS1)
- —------- --
--- -- -- - - -----------
-- ----
Prepared &Analyzed: 10/24/14
------- - --------...- --
---- ----- -
- --------.._.---
Mercury
0.428
0.020
mg/kg wet
0.4167 103
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 _ Charlotte, INC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 14

I Full-Servicc, Analykical &
PRISM ' Environmcintal Solutions
Level 11 QC Report
10127/14
City of Statesville, NC Project: StaLime (Qtdy, BiWeekly, 60Day Prism Work Order: 4100396
Attn: Andy Smith 7 Fecal) Time Submitted: 10/20/2014 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4J0422 - Solids, Dry Weight
Blank (P4J0422-BLKI) Prepared &Analyzed: 10/23/14
% Solids 99.9 0.100 %byWeight
This report should not be reproduced, except in its entirety, Wthout the written consent of Prism Laboratories, Inc.
449 Springbrook Roid - P:0. Box 240643 - Charlottei NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12=

Level II SC Report
PRISMFW6Sevice
8
Environmental Solufon=
10/27/14
City of Statesville, NC
Project: Stal-ime (Qtdy, Biweekly, 6ODay Prism Work Order: 4100396
Attn: Andy Smith
7 Fecal)
Time Submitted: 10/20/2014 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological. Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P4J0432 - NO PREP
Blank (P4J0432-BLl(1)
-- -- --- - .... -
-------------
. _...... - -
-- — — -- -- --
Prepared &Analyzed: 10/21/14
---- -- - - --- -- ---- ---------------
Fecal Coliforms
BRL
0.2 MPN/g wet
--
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
DateTme
4100396-01
P4J0422
30 g
30 g
10/23/14 13:45
4100396-02
P4J0422
30 g
30 g
10/23/14 13:45
4100396-03
P4J0422
30 'g
30 g
10/23/14 13:45
4100396-04
P4J0422
30 g
30 g
10/23/14 13:45
4100396-05
P4J0422
30 g
30 g
10/23/14 13:45
4100396-06
P4J0422
30 g
30 g
10/23/14 13:45
4100396-07
P4J0422
30 g
30 g
10/23/14 13:45
Prep Method: 3050B
Lab Number
Batch
Initial
Final
DateTme
4100396-01
P4J0390
1.98 g
50 mL
10/22/14 8:40
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
4100396-01
P4J0391
0.55 g
50 mL
10/24/14 9:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 =Charlotte; WC 2822410543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 13 of 14

I ��9 r�� 1116 All, I Full-Rervi:* r\na!vflca' .�
Enviro ln-1cnral Solutions
. t..,_". LAnONATORICS• INC.
449 SPringilrook Road > Charfo te, NC 2.1,217
r'horle fCiaU:i2::-6:if�`b i=ax: `r'6w'S:S.p:�1in Client Company Name: C;4•y 7T �J� c st"I,flc
Report To/Contact Name: ANg,r Sot I'-s �t
Reporting Address:tl
a.is4 ' h&. it`,✓!, •c. �5
PAGE OF _ QUOTE A TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
"Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
��. •`§�.A�r,.ra���L�4�'� •.�`�G:��3L"rkA.�LS`u'�'J'.*fd�2.'f$iY+..�35' ��.3•.''t..�yL"'J,, a�7�.`�'
Y7 4 NO .. NIA
Samples IPi-I-Ar f ui,orrarrn,.kI?
_-..
Received ON. f.J f NCO.?
PROPEL;
Q
Received VVITH'JN I ROLDING IMES?
__--- _ —ca
CUSTODY SG" La INTACT,?
\•'UL \TILEJ ,l;G.i Il:/ll!UI IiL'f-'.1.1:'+F?.l:•L-:"
i'R0PIJ. COh;Tr'\Ii tE.f<S used.`
- -
--
'I EIviP: The:rin ID:._
Phone:'d J y9- 9'7Y- 3'-l3,r Fax Yes (No): }l t7'if _r75'-�6 ;�' Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Ernall Address: Requested Due Date El1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoD FL NC
EDD Type: PDF Excel Other "Working Days' ❑ 6-9 Days ❑ Standard 10 days .❑ Rush Pre -Approved k Must Be
SC OTHER N/A
Site Location Name: ,tea L, r4 k Creek L0 C,t: TP Samples received after 14:00 will be processed next business day.
pp
Site Location Physical Address: 3 �C If �+^�� Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
/ (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES_ NO
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
! � ANALYSISC�EQUESTED
/ / /
I PRISM
CLIENT j
DATE
TIVES
i Q REMARKS
i / /
LAB
"TYPE
SAMPLE DESCRIPTION
I
COLLECTED
i
MILITARY
WATER OR
i
NO.
SIZE
q j' !
" �! i � ,/ j' / i
ID NO.
HOURS
SLUDGE)
SEE BELOW
!; %!
/
f4 SA1J31
Ta
1
(c
I
I
I
i
ZJ'
9 ,� zA:e Sam �i �l { l s o m
Sampler's Si nature �-[tea>raf-ram pled By (Print Name) cL n�rJ�a t/ 'd'iC � Affiliation
Upon relinquishing, this Chain of Custody is our authorization for Prism to proceed'with the anal ses as requested above. An changes must be
p q 9, � Y p Y q Y g
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. p��LrtC tta }
Relinqui$hed By: (Signature) f� Received By: (Signature) Date Military/Hours Additional Comments: E Site AllvalTime:
Relin 'had By: (Signature) jf Received By: (Signature) Date I�.F:Di:pc`Irfure
' Fisad Tech Rec2 ved For Prism Laboratories B Date
Rellnquls(lad 8y: (Signature ,f �r y''`,.--, r (• 7 3 I v�-�-•�-
:.. ,, ,,._I r : r
' � % s V :' i ' ✓�'" v'.' '�' IYIII 1F
,...4.1 ..:.1,�J +..0�4�,„f�':.,:,n_"'Q1e'�
) .r�,✓-i -d i� +�._ .
Method of 5hlpment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED,' CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No. 'i"
SAMPLES ARE NOT ACCEPTED AND VERIFIED AG 116E T CDC UNTIL RECEIVED AT THE LABORATORY.
❑ Other
❑ Fed Ex ❑ UPS ❑ Hand -delivered 6i`Prisnl Mold Service
NPDES: I UST: i GROUNDWATER: DRINKING WATER: SOLID WASTE: i RCRA: CERCLA LANDFILL !OTHER: '
ONCOSC ❑NC OSIC ONC OSC ❑NC OSC ONC ❑SC ONCOSC ONC ❑SC ONC OSCi [INC CSC
n n i n ❑ ❑ a n ® I©
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402 ���� Narrative
SC Certification No. 99012
t Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutions VA Certification No. 460211 11/12/2014
R 1
aooFc. or, es, uac. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISOlIEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 11/03/2014
Statesville, NC 28687 Prism Work Order: 4110026
TL:_ J-.1.. .. ..1..�.... .. ..+..ie.e. +r,.... .,i„+�,..,i ,.i+� v„�+tio ., o�+ �.ian+�5o�1 ahnve and inrinr�ac a ('ace Narrative ;ArnnIR
1 Ills data package contains he analytical resin-- for he project ide identified ....._.e --l._ in _.-.___ _ .._..
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Rabbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole For Robbi A. Jones
Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 1 of 7

PRISMi FrneAnalytical &
Ennviroonmen, tal Solutions
Sample Receipt Summary
11 /12/2014
Prism Work Order: 4110026
Client Sample ID Lab Sample ID (Matrix Date Sampled Date Received
Sta-Lime 4110026-01 Solid 11/03/14 11/03/14
Samples were received in. good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
- 449 Springbrook.Road - P.O. Box 240543 - Charlotte, NC,28224-0543, .
Phone: [phone] -Toll Free Number: 1-8001529-6364 -Fax: [phone] Page 2 of 7

R Laboratory Report
q l jg i Full -Service Analy ticul 2
ftll � �' Environmental Solutions 11/12/2014
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 4110026-01
P.O. Box 1111 Prism Work Order: 4110026
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/03/14 15:05
Time Submitted: 11103/14 18:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
Bolick 72.0
% bV
0.100
0.100 1
*SM2540 G 11f7114 15:05 MJO
P4K0116
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 11/4/14 13:40 JHB
P41<0096
Total Metals
Mercury
0.11
mg/kg dry
0.026
0.0042
1
*7471B
1115114 17:43
BGM
P41<0011
Arsenic
3.0
mg/kg dry
1.8
0.26
5
*6010C
11f7114 23:26
BGM
P41<0075
Cadmium
BRL
mg/kg dry
1.8
0.25
5
*6010C
11l7/14 23:26
BGM
P41<0075
Copper
19
mg/kg dry
3.5
0.64
5
*6010C
1117114 23.26
BGM
P4K0075
Lead
8.3
mg/kg dry
1.8
0.27
5
*6010C
11r7114 23.26
BGM
P41(0075
Nickel
94
mg/kg dry
7.0
0-90
5
*6010C
1117M4 23.26
BGM
P4K0075
Selenium
BRL
mg/kgdry
3.5
0.42
5
*6010C.
11/11/14 1735
BGM
P4K0075
Zinc
39
mg/kg dry
18
3.9
5
*6010C
11f7114 23:26
BGM
P4K0075
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
-.-. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC12822.44543.. .
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Ot 7

Full -Service Analytical
Em,11.11mOWaf Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4KO01 1 - 7471 B
Project: Stal-ime
Reporting
Result Limit Units
Level 11 QC Report
11112/14
Prism Work Order: 4110026
Time Submitted: 11/3/2014 6:00:OOPM
Spike Source %REC RPID
Level Result %REC Limits RPD Limit Notes
Blank (P4K0011-BLK1) Prepared &Analyzed: 11 /05/14
Mercury BRL 0.020 mgA(g wet
LCS (P4K0011-BS1) Prepared &Analyzed: 11/05/14 ........
Mercury 0:439 0.020 mg/kg wet 0.4167 105 80-120
Batch P4100075 - 3050B
Blank (P4K0076-BLK1)
Prepared: 11/06114 Analyzed: 11/07/14
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mglkg wet
Copper.
BRL
0.50
mg1kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg1kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (1341<0075-13S11)
--------
------ ---
Prepared: 11/06/14 Analyzed: 11/07/14
----------- ----- - -------
Arsenic
23.6
0.25
mg/kg wet
25.00 95 80-120
Cadmium
24.0
0.25
mg/kg wet
25.00 96 80-120
Copper
24.8
0.50
mg/kg wet
25.00 99 80-120
Lead
23.7
0.25
mg/kg wet
25.00 95 80-120
Nickel
23.9
1.0
mgJkg wet
25.00 95 80-120
Selenium
23.3
0.50
mgJkg wet
2500 93 80-120
Zinc
24.0
2.5
mg/kg wet
25.00 96 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook,Road -,P.O- Box 240643 Charlotte, -NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

I FUI­A.Analytical &
PRISM Environ­nzal Sokqions
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level 11 QC Report
11/12/14
Prism Work Order: 4110026
Time Submitted: 11/3/2014 6:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4K01 16 - Solids, My Weight
Blank (P4K01 I 5-BILK11) Prepared & Anaiyzed: i i Wii 4
% Solids 99.9 0.100 %byWeight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spr.ingbro.ok Road: P.O- Box 240543. -,Charl offe,- NG. 28224.41543,
Phone: [phone] -Toll Free Number: 1-80DIS29-6364 -Fax: [phone] Page rJ Of 7

Level II QC Report
r � I Envr rviu: al Solijli 3 11/12/14
g EnviS—i— A iy jiar,s
City of Statesville, NC Project: StaLime Prism Work Order: 4110026
Attn: Andy Smith Time Submitted: 11/3/2014 6:00:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4100096 - NO PREP
Blank.(1341<0096-131-K1)
_
_ _-
Prepared&Analyzed:ll/04/14
Fecal Colifonns
BRL
0.2 MPN/g wet
Duplicate (P4K0096_DUP7)
- - Source: 4110026-01 - -Prepared
&Analyzed: 11/04/14
Fecal Coliforms
BRL
0.3 MPN/g dry
0.00 20
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab (dumber
Batch
Initial
Final
DateTme
4110026-01
P41<0116
30 g
30 g
11/07/14 15:05
Prep Method: 3050B
Lab Plumber
Batch
Initial
Final
DateTme
4110026-01
P41<0075
1.98 g
50 mL
11/06/14 8:20
4110026-01
P41<0075
1.98 g
50 mL
11106/14 8:20
Prep Method: 7471E
Lab Plumber
Batch
Initial
Final
bateTme
4110026-01
P41<0011
0.65 g
50 mL
11/05/14 9:05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook.Road- P.O. Box 240543-r Charlotte, NC.28224-0543:,-
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] PBCJE 6 Of 7

N !iOff._ },ic +t§�=oi,snarntinics i () F.tll•,.i=.iR.L? r-.Fi:; lgytlCal CHANN OF CUSTODY RECORD
u SRar reINikCT utaCunE zenval ? : L 1'`F/ x
I�O
f a Pniironnt t:tsi So!uticros sAo�_OF- QUOTE kT® ENSURE PROPEReiPLlNo: rnple C l n2tl OF1 NET
€9>g a I,)Flc si.ttoad t t� Lt t0i }7 ° C"ru!olier, tvC:::&224 0543 Project Name. PROPER PfiEo�RVATI%ES Indltated? _ [_ -.-_
Ea:: rf,aJb'5-0449 short l-Iogd Analysis: ores) (NO) UST Project: ('Yes) (NO){ecel�ed 1NITiiIN HOLDI.N�� T'I!�4ES n-
1 *Please ATTACH any project specific reporting (QC LEVEL 1 Ii 111 Illj CUSTC�U F SEALS INTA� I? l
Client Company Name: C + I V o P � tale:S v'r'l l d --- �
provisions and/or OO Requirements
VOLATILL-S rec d W(OUT I
liepol € To/ContactE9�rse: r� v 5>'! , Invoice To:
Reporting Address: 1 3��1 ►� PROPER CONTAINE R" used L -
�ra'cSz+ NC .Address:
Phone. "��'/' 8Z -3y3 Eax (Yes.(N9o):Purchase Order No./SiEling �teference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NdEL AC USACIE EL NO
WorEDD Type: PDE— Excel.—OtherO — "Working Days" ❑ 6-9 Days Standard 10 days 0 Rush Pre-Apppropro Must Beved SO_
OTHERhV/A
Site Location Nam.: ¢utt r-} �1 �'r ee,E LL'I�t � P Samples received after 16:00 will be processed next business day.
Site Location Physical Address;ess: �? 3c3V ru.l: "� �` Turnaround time is based on business days, excluding weekends and holidays. VVatel• Chlorinated: 'YES_ NO—
r (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample lC®Ci Upon COIIGC$IOrI: YES - NO
J t A•S ��' +iB PLC RENDERED BY PRISM LABORATORIES, INC. TO CLIEN1J
I I TIME MATRIX I SAMPLE CO{ {TAINER i ANALYSES REQUESTED PRISM
COLLECTED SOIL, PRESERVA- '
CLIENT DATE (' Q REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR °TYPE TIVES � ` � ID NO.
NO. SIZE ''f pv%;7u� i
HOUP SLUDGE)SEE EELOW CC ,
_ -
Upon relincgLhishiiig, this Chain of
stsbmltted In vvriUng to the Prism
v
is your authorization for Prism to I
rianaaer. There will be charges for
.Q S
Pb
Se
' r l C> Affiliation
Pith th analyses as requested above. Any changes must be
ges after analyses have been initialized.
Date [Military,
/- 1 Sff.r�.�� J-,
Relinquished By: (Signature) Received For Pdsm Laboratories Byr--
Method of Shlpmem NOTE: ALL SAMPL COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRA ORTATION TO THE LABORATORY. COC liroup No.
SAMPLES ARE NO C EPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT TRE-LABORATORY. I LA
D Fed Ex ❑ UPS ❑ Hand -delivered Prism Field Service ❑ Other
N PDES: I UST: GP U DWATER: DRINKING WATER: SOLID WASTE: I RCRA: CERCLA LANDFILL OTHER:
0 NC ❑ SCI ❑ NC ❑ SC ❑ NC SC I ❑ NC ❑ SC U NC ❑ SC ❑ NC ❑ SCI ZINC ❑ SC ❑ NC ❑ SC ®NC Cl SC
p _�❑ - - .. --� - - I 1:2 ❑ O a—... .._.
*CONTAINER TYKE CODES: A = Amber C ;:Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
`Site An ivl l'irne; ' '
;Srtc Departure Tirge j
'Field Tech. Feet
Mtlt �yE:

402
NC Certification No.990 Case Narrative
SC Certification No. 99012
Full -Service ar,aly*,ical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No.460211 11/25/2014
LA60RKIPRIE INC. DoD ELAP: L-A-BAccredited Certificate No. L2307
IS01IEC 17025: L-A-BAccredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 11/17/2014
Statesville, NC 28687 Prism Work Order: 4110343
This data Dackaae contains the analvtical results for the nrniPrt idant_ifiari a_ hnve and inrJi rips a f aca Narrative Samnle
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O- Box 240543 - Charlotte, NC 28224-0543... -.
Phone_ 7041529-6364 - Toll Free Number 1-8001529-6364 - Fax: [phone] Page 1 Of 7

I S ��� Full -Service nalytitio s
F_nvironmertal Sohrtirn
Sample Receipt Summary
11 /25/2014
Prism Work Order: 4110343
Client Sample ID Lab Sample ID . Matrix Date Sampled Date Received
Sta-Lime
4110343-01 Solid 11/17/14 11/17/14
Samples were received in good condition at 0.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
_..-449 Springbrook Road -. P.O.-Box 240543 - Charlotte, WC 28224-0643,- . .
Phone: [phone] - Toll Free (dumber: 1-800/529-6364 - Fax: [phone] Page 2 Of 7

R qq Puniro n
An ilytical &
Laboratory Report
Environmenen
tal 801utions
11/25/2014
City of Statesville, NC
Project: Stal-ime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 4110343-01
P.O. Box 1111
Prism Work Order: 4110343
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/17/14 10:17
Time Submitted: 11/17/14 12:48
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
Solids
73.7
IN, by
0.100
0.100
1 *SM2540 G 11/21/14 15:5n
M 10
-
P41(0399
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 11/18/14 9:50
MES
P41<0328
Total Metals
Mercury
0.14
mglkg dry
0.027
0.0045
1 *7471B 11/2OM4 12.43
BGM
P4K0327
Arsenic
4.4
mglkg dry
3.4
0.49
10 *6010C 11/22/14 3:38
BGM
P4K0343
Cadmium
BRL
mglkg dry
3.4
0.48
10 *6010C 11/22/14 3:38
BGM
P4KO343
Copper
30
mglkg dry
6.8
1.2
10 *6010C 11/22/14 3:38
BGM
P4KO343
Lead
12
mg/kg dry
3A
0.52
10 *6010C 11122/14 3:38
BGM
P4KO343
Nickel
170
mglkg dry
14
1.8
10 *6010C 11/22/14 3:38
BGM
P4KO343
Selenium
BRL
mglkg dry
6.8
0.82
10 *6010C 11/22/14 3:38
BGM
P4KO343
Zinc
60
mglkg dry
34
7.5
10 *6010C 11/22114 3.38
BGM
P4K0343
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road. RO. Box 240643 - Chariotte,.NC 28224-0543... _. ..
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 3 Of 7

� Full-SvicdPRISM Fmiromenal Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P4KO327 - 7471 B
Project: StaLime
Level II QC Report
11/25/14
Prism Work Order: 4110343
Time Submitted: 11/17/2014 12:48:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P4KO327-BLKI) - -_„ - - - - - Prepared: 11/19/14 Analyzed:.11/20114
Mercury BRL 0.020 mg/kg wet
LCS(P4KO327-BSI) ---_ Prepared: 11/19/14 Analyzed:11/20/14--- ----- - - -
Mercury 0.416 0.020 mg/kg wet 0.4167 100 80-120
Matrix Spike(P4KO327-MS1) Source:4110343-01 Prepared:11/19114 Analyzed: 11/20/14
- --------- _ ._ ---- --- ---- ----------- - ---- ---- ------------------------
Mercury 0.644 0.027 mg/kg dry 0.5654 0.140 89 80-120
Matrix Spike Dup (P4K0327-MSD1) Source: 4110343-01 Prepared: 11/19/14 Analyzed: 11/20/14
Mercury 0.632 0.027 mg/kg dry 0.5654 0.140 87 80-120 2 20
Batch MOM - 3050B
Blank (P4KO343-BLK1)
--------- --------------
-- - ---- -- -----
---- --
Prepared: 11/20/14 Analyzed: 11/22/14
------------------- ---- -----------------------
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P4KO343-BSI)
Prepared: 11/20/14 Analyzed: 11/22/14
Arsenic
27.9
0.25
mg/kg wet
25.00 111 80-120
Cadmium
27.5
0.25
mg/kg wet
25.00 110 80-120
Copper
28.3
0.50
mg/kg wet
25.00 113 80-120
Lead
27.1
0.25
mg/kg wet
25.00 109 80-120
Nickel
26.9
1.0
mg/kg wet
25.00 107 M120
Selenium
27.6
0.50
mg/kg wet
25.00 110 M120
Zinc
27.8
2.5
mg/kg wet
25.00 111 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
_-• 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC.28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 7

r—A I P Full -Service Analytical $
S M Environmental Solutions
I
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level 11 QC Report
11/25/14
Prism Work Order: 4110343
Time Submitted: 11/17/2014 12:48:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPID Limit Notes
Batch P4KO399 - Solids, Dry Weight
Blank (P4KO399-BLKI) Prepared &Anaiyzed: iw2iii4
--------------- . ..... .
% Solids 100 0.100 %byWeight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O: Box 240643 - Charlotte, -NC 28224-.0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of

I � f� I Fulf-Service Analytical &
F� Environmental Sotutlpns
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
11 /25/14
Prism Work Order: 4110343
Time Submitted: 11/17/2014 12:48:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P41<0328 - NO PREP
Blank (P4K03Z8-BLK7) Prepared &v,naiyzed: iiii8ii4
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
DateTme
4110343-01
P4K0399
30 g
30 g
11/21/14 16:50
Prep Method: 3060B
Lab Number
Batch
Initial
Final
Date/Time
4110343-01
P41<0343
1.99 g
50 mL
11/20/14 8:25
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DateTme
4110343-01 P41<0327 0.6 g 50 mL 11119/14 1230
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O..Box 240543 -.Charlotte,-NC.28224c0543 ,
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone] Page 6 Of 7

HANK OF CUSTODY RECORD
r -ull-
Ail!
!`,,­J�,! k` P" Jli N y FS N 0 N/A,
m e n tal Scd utio ns, n OF UOTE # TO EMSURS PROPER BILLING- 0
LALRO �ATORIEs_ INC.
Project Name-
.)�­,gtwoz,ii R,3ad P.O. Box '24064,1, ICI%ar�ottC, N1, 218224-0154$ CT
Phcln-?: 7�)415­6264 -ax: 7()4/5'_9.,,-0409 Short Hold Analysis: (Yes) (Flo) UST Project-. (Yes) (No)
'Please ATTACH any project specific reporting `QC LEVEL I Ill ➢III IV) IL
Gliank Company Name T(D D'Y S E A. S
provisions and/or OC Requirements
AT:J
rillepoil To/Cont-act l A',S, '311, L- - LES ACE �',
Invoice TO:
i!77
ing Address: Report Address: 'ROPE`) GOWA!NERS u ?
Phoneb'701-929"-_433 Fax Yes Purchase Order NodBilling Reference TO BE FILLED 16\1 BY CLI]EN'USAMFLING PERSONNEL
Ernafl (Yes) (No) Email Address Requested Due Date 0 1 Day 0 2 Days . Q 3 Days :14 Days 0 5 Days Certification: NELAC USAGE FL_ NC
ED D Type: PDF_ Excel —Othe "Working Days" ❑0 6-9 Days U Standard 10 days 0 Rush Work Must Be
Pre -Approved Sc OTHER _N/A
Site Location Name- F, , 4 A C, Samples received after 16:00 will be processed next business day.
Site Location Physical Address:�,�-73 Fqr, Turnaround line is based on business days, excluding weekends and holidays. Water Chlorinated: YES_
NO
vc (6FE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I - -
I RIN SAMPLE CONTAINER PRISM
CLIENT DATE COLLECTED, � M:TANALYSES REQUESTED
OIL, PRESERVA- LAB i *TYPE REMARKS
SAMPLE DESCRIPTION COLLE&ED MILITARY WATER OR ii TIVES ID NO.
Nob !SIZE
HOURS i SLUDGE) SEE BELOW
C)
0 S
Sampler's Signature
Upon relinquishing, this Chain of'Custody
submitted in writing to the Priisern Project
Reline} fished By: (Signature)
I I
Relh,46tshed By: (Signature)
is your aUth0riZati01`1 for Prism to proceed
Manager. There will be charges for any ch,,
Affiliation
analyses as requested above, Any changes must he
yr analyses have be.en initialized.
.7
Method of Shipment: - NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT VVITVI . GUSTf)DY SEALS FOR TRANSPORTATION TO THE LABORATORY.
COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO UNTIL ECEIVSD XF THE LABORATORY.
P
CU Fed Ex �CJUPS 0 Hand -delivered 0 Prism Field Service 0 Other
HPDES:
UST: 1 GROLINDWATFIR: 1 CRINKiNGWATER:
SOLIDWAs,rE:
I RCRA:
C ERGLA l LANDFILL 1 OTHER:
Q NC aSC
I 0 NC [_-J Sc :Jl\lC F—JSC 0 NC ij SC
-D NC Q SCt,
NC Ij sc
0NC 0 Sc 0 NC
�
.
0 SCONC OSC
FJ
1
1
D
'CONTAINER TYPE CODES: A=Amber C= Clear G=Glass P =Plastic; TL = Teflon -Lined Cap VOA =Volatile Organics Analysis (Zero Head Space
Additional Comments:
J
s

NC Certification No. 402
SC Certification No. 99012 Case Narrative
i Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutions VA Certification No. 460211 12(23/2014
oona orris ir�c. DoD ELAP: L-A-BAccredited Certificate No. L2307
ISO/I EC 17025: L-A-BAccredited Certificate No. L2307
City of Statesville, NC Project: StaLime (Qtdy, Biweekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 12/16/2014
Statesville, NC 28687 Prism Work Order: 4120290
This data Dackaoe contains the analytical results for the Droiect identified above and includes a Case Narrative. Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
..........,. , . 449.Springbrook Road -.P.O.. Box,240543 - Chartotte, ,WC,28224-0543, ,
Phone: 7D4/529-6364 - Toll Free Number. 1-800/529-6364 - Fax: 704/525-D409 page 1 Of 14

y y iEn,wo ivies Analytitio s
En�ai: onmenial golutinns
Sample Receipt Summary
12/23/2014
Prism Work Order: 4120290
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
StaLime
4120290-01
Solid
12/15/14
12/16/14
Fecal #2
4120290-02
Solid
12/15/14
12/16/14
Fecal #3
4120290-03
Solid
12/15/14
12/16/14
Fecal #4
4120290-04
Solid
12/15/14
12/16/14
Fecal #5
4120290-05
Solid
12/15/14
12/16/14
Fecal #6
4120290-06
Solid
12/15/14
12/16/14
Fecal #7
4120290-07
Solid
12/15/14
12/16/14
Samples were received in good condition at 2.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook. Road, P.O. Box 240643 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 2 of 14

Laboratory Report
Full -Service Hnalytical &
PRISM I Environmental solutions 12/23/2014
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: StaLime
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4120290-01
P.O. Box 1111 Prism Work Order: 4120290
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date<Tme
ID
General Chemistry Parameters
Plant AvailableNitrooen
750
malka
ten
43
9
*Catculatinn
1919911A 9.1A
MR
rCALCI
Solids
66.9
% by
0.100
0.100
1
*SM2540 G
12/18114 15:50
EGC
P4L0341
Weight
Nitrate/Nitrite as N
11
mg/kg dry
7.5
9.82
1
*SM4500-NO3 F
12/18/14 10:18
CLB
P411_0299
Phosphorus -Total
2100
mglkg dry
75
16
20
*SM4500-P F
12123/14 10:11
CLB
P4L0363
Total lCjeldahl Nitrogen
3600
mg/kg dry
750
63
2
*351.2
12/19114 8.50
CLB
P411_0329
Ammonia as N
92
mg/kg dry
7.5
1.8
1
*SM4500-NH3 G
12122/14 9:14
CLB
P41L0349
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
12/16/14 11:36
MES
P4L0378
Total Metals
Mercury
0.18
mglkg dry
0.029
0.0049
1
*7471B
12118114 11:53
MEH
P&0311
Arsenic
BRL
mg/kg dry
0.38
0.053
1
*6010C
12/19/14 23:34
BGM
P41_0330
Cadmium
0.57
mg/kg dry
0.38
0.063
1
*6010C
12119M4 23:34
BGM
P411_0330
Copper
26
mg/kg dry
0.76
0.14
1
*6010C
12/19/14 23:34
BGM
P411_0330
Lead
12
mg/kg dry
0.38
0.057
1
*6010C
12119/14 23:34
BGM
P4L0330
Nickel
10
mg/kg dry
1.5
0.19
1
*6010C
12/19114 23.34
BGM
P4L0330
Potassium
670
mg/kg dry
19
1.2
1
*6010C
12/19114 23.34
BGM
P4L0330
.Selenium
BRL
mg/kg dry
0.75
0.090
1
*6010C
12/19/14 23:34
BGM
P4L0330
Sodium
33
mg/kg dry
19
3.7
1
*6010C
12119/14 23:34
BGM
P4L0330
Zinc
45
mg/kg dry
3.8
0.83
1
*6010C
12/19/14 23.34
BGM
P41L0330
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449-Springbrook Road -P.O. Box 240543 - Charlotte, NC 28224-0543 --
Phone: [phone] - Toll Free Number. 1-8001529-6364 - Fax: [phone] Page 3 of 14

i En Service Analytical tt
PRISM Environmental Solution=
Laboratory Report
12/23/2014
City of Statesville, NC
Project: Stal-ime (Qtrly, Biweekly,
Client Sample ID: Fecal #2
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4120290-02
P.O. Box 1111
Prism work Order: 4120290
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateTme ID
General Chemistry Parameters
%Solids
70.2 %bv
0.100 ninn
1 "CBA95d0A 191 RI1d 49-An Pr--r PAL03d1
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 12/16/14 11:36 MES P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
' 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of � 4

�"'Il p E P � � �g I FWI-Service An o-fu lial s
�'-"'� a � fj En'dironaiental Solu 4ons
Laboratory Report
12/23/2014
City of Statesville, NC Project: Stal-ime (Qtrly, Biweekly, Client Sample ID: Fecal #3
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4120290-03
P.O. Box 1111 Prism Work Order: 4120290
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
Solids 68-7 % by n"1 nn n.1nn 1 •-SM2se0 C- 19119114 15•50 cgr Pal-n3di
Weight
Microbiological Parameters
Fecal Colifonns BRL MPN1g dry 0.3 1 'SM9221 E 12/16/14 11:36 MES P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
^` 449 Springbrook Road:: P.O. Box'240543 _ Charlotte, NC 28224-0543 - ,
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page rJ OfI4

PPRISMr� g� Laboratory Report
�'"�I NT F,j I En—.mvice,inalyiical&
i'� � Environmental Solutions 12/23/2014
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #4
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 4120290-04
P.O. Box 1111 Prism Work Order: 4120290
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids C_.7-7 % by n inn n ieo a SM25-1-1 0 `Gc o4Ln3e1
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 12/16/14 11:36 MES P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springhrook Road--- P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number 1-800/529-6364 - Fax: [phone] Page 6 O 14

Full - Service Analytical
Environmenal S,lutions
__ , -... �_.n�r...�-•nit; ��,,.
Laboratory Report
12/23/2014
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #5
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4120290-05
P.O. Box 1111
Prism Work Order: 4120290
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids
67.7 % by n 4nn n ann
-..-- -..__
i *e�i2ewn r n*t 03Al
.....�..-..... .�....•.-. .....,,. E.�., . --....—.
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3
1 *SM9221 E 12/16/14 11:36 MES P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbroafc Road - P.O. Box 244543 =Charlotte; NC'28224-0543 - "
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 14

�" PRISMII pig ,e�� I Full- nmee Analytical s
I� �`� Em:ironmental golution=_
Laboratory Report
12/23/2014
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Fecal #6
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 4120290-06
P.O. Box 1111
Prism Work Order: 4120290
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateMme ID
General Chemistry Parameters
Solids
66.3 % by 0100 n rnn
*SM2S4a r_ 12MV14 15.5n ECC oxi nael
Weight
Microbiological Parameters
Fecal Coliforrns
BRL MPNfg dry 0.3
1 'SM9221 E 12f16114 11:36 MES P4L0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
- 449�Springbrook Road -P.O. Box 240543 - Charlotte, NC 28224-0543'
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 'A

Ii�iI Fuq-Service Analytical &
PRISM
Environmental Solutionc_
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
12/23/2014
Client Sample ID: Fecal #7
Prism Sample ID: 4120290-07
Prism Work Order: 4120290
Time Collected: 12/15/14 11:45
Time Submitted: 12/16/14 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Solids 68.6 % by 0.100 0.100 1 •SM2540 G 12/18/14 15:50 EGC 113411-0341
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 "SM9221 E 12/16/14 11:36 MES P41-0378
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449-SpringbroolcRoad•- P:O. Box 240643 - Chariotte, NC 28224-0543
Phone_ 7041629-6364 -Toll Free Number 1-800/529-6364 - Fax:[phone] Page 9 of 14

I! e [{._ y ISM
I Full -Service Flnalytic it &
�-" � EmironmenEzl Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime (Qtdy, Biweekly, 6ODay
7 Fecal)
Level II QC Report
12/23/14
Prism Work Order: 4120290
Time Submitted: 12/16/2014 10:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4LO311 - 7471 B
Blank (P4L0311-BLKI)
Mercury BRL
LCS (P4L0311-BSI)
Mercury 0.439
Batch P4LO330 - 3060B
Blank (P41-0330-BLKI)
--------------------
Arsenic
BRL
Cadmium
BRL
Copper
BRL
Lead
BRL
Nickel
BRL
Potassium
BRL
Selenium
BRL
Sodium
BRL
Zinc
BRL
LCS (P4LO330-BS1)
Arsenic
22-2
Cadmium
22.7
Copper
23.2
Lead
22.3
Nickel
22.0
Potassium
432
Selenium
22.2
Sodium
459
Zinc
22.8
Prepared: 12/17/14 Analyzed: 12/18/14
0.020 mg/kg wet
Prepared: 12/17/14 Analyzed: 12/18/14
0.020 mg/kg wet 0.4167 105 80-120
------------------
Prepared: 12/18/14 Analyzed: 12/19/14
-------------------------------------
0.25
mg/kg wet
025
mg/kg wet
0.50
mg/kg wet
0.25
mg/kg wet
1.0
mg/kg wet
12
mg/kg wet
0.50
mg/kg wet
12
mg/kg wet
2.5
mg/kg wet
Prepared: 12/18/14 Analyzed: 12/19/14
0.25
mg/kg wet
25.00
89
80-120
0.25
mg/kg wet
25.00
91
80-120
0.50
mg/kg wet
25.00
93
80-120
0.25
mg/kg wet
25.00
89
80-120
1.0
mg/kg wet
25.00
88
80-120
12
mg/kg wet
500.0
86
80-120
0.50
mg/kg wet
25.00
89
80-120
12
mg/kg wet
500.0
92
80-120
2.5
mg/kg wet
25.00
91
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
.449 Springbrook Road— P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 14

Level II QC Report
MyI
u � Q I FWI-Service Analytical g
Env12J23/14
i ron—m-11 Sokftions
City of Statesville, NC Project: StaLime (Qtdy, BiWeekly, 60Day Prism Work Order: 4120290
Attn: Andy Smith 7 Fecal) Time Submitted: 12/16/2014 10:00:OOAM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P4LO299 - NO PREP
Blank (P4L0299-BLK1) Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P411-0299-BSI) Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N 49.6 5.0 mg/kg wet 50.00 99 80-120
Matrix Spike (P4L0299-MS7) Source: 4120290-01 Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N 75.4 7.5 mg/kg dry 74.74 10.6 87 80-120
Matrix Spike Dup (P4L0299-MSD1) Source: 4120290-01 Prepared: 12/17/14 Analyzed: 12/18/14
Nitrate/Nitrite as N 75.7 7.5 mg/kg dry 74.74 10.6 87 80-120 0.4 20
Batch P411-0329 - 351.2
Blank (P4L0329-BLK1) Prepared: 12/18/14 Analyzed: 12/19/14
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P41-0329-11331) Prepared: 12/18/14 Analyzed: 12/19/14
Total ICeldahl Nitrogen 492 100 mg/kg wet 500.0 98 90-110
Batch P411-0341 - Solids, Dry Weight
Blank (P4L0341-BLK1) Prepared & Analyzed: 12/18/14
% Solids 100 0.100 % by Weight
Batch P41L-0349 - NO PREP
Blank(P4L0349-BLKI)
Ammonia as N
Prepared &Analyzed: 12/22/14
- - - --- -- -------------------------------------------------- ---------------- - -
BRL 5.0 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
-,449 Springbrook.Road - P.O. Box 240543 -. Charlotte, NC 2822470543 -
Phone: [phone] - Toll Free Number: 1-8901529-6364 - Fax: [phone] Page 11 Of 4

B Y @.. S� I Full -Service Analytical &
�'�" Environmental Solutions
Level II QC Report
12/23/14
City of Statesville, NC Project: Stal-ime (Qtdy, Biweekly, 60Day Prism Work Order: 4120290
Attn: Andy Smith 7 Fecal) Time Submitted: 12/16/2014 10:00:OOAM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P411_0349 - No PREP
Lr;s (P4Lu349-BS1) Prepared &Analyzed: 12/22/14
Ammonia as N 126 5.0 mg/kg wet 125.0 101 80-120
Matrix Spike (P4L0349-MS1) — Source: 4120290-01 Prepared &Analyzed: 12/22/14
Ammonia as N 293 7.5 mg/kg dry 186.8 92.1 107 80-120
Matrix Spike Dup (P4LO349-MSD1) Source: 4120290-01 Prepared & Analyzed_ 12/22/14
Ammonia as N 292 7.5 mg/kg dry 186.8 92.1 107 80-120 0.1 20
Batch P411_0353 - S
Blank (P41-0353_BLK9)— Prepared: 12/22/14 Analyzed: 12/23/14
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P41_0353 _BSI) — Prepared: 12/19/14 Analyzed: 12/23/14
---------------...-------------- - - ---------------
Phosphorus-Total 102 2.5 mg/kg wet 100.0 102 90-110
Matrix Spike (P4L0353-MS1) Source: 4120290-01 Prepared: 12/19/14 Analyzed: 12/23/14
Phosphorus -Total 2450 75 mg/kg dry 149.5 2060 261 80-120
Matrix Spike Dup (P4LO353-MSD1) _ Source: 4120290-01 Prepared: 12/19/14 Analyzed: 12/23/14
-- -- — — -- ----- ---- -- - Prepared: 1--- 14 ---
Phosphorus-Total 2450 75 mg/kg dry 149.5 2060 257 80-120 0.2
20
MC
MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449, Springbrook Road - P-O. Box 240543 - Charlotte, NC'28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of-1-4-

Level II QC Deport
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I Full -Service Analytical &
Environmental Solutions
12/23/14
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City of Statesville, NC
Project: StaLime (Qtdy, Biweekly, 60Day Prism Work Order: 4120290
Attn: Andy Smith
7 Fecal)
Time Submitted:
12/16/2014 10:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit Units
Level Result %REC Limits
RPD Limit Notes
Batch P41_0378 - NO PREP
Blank (P4LO378-BLKi)
Prepared &Analyzed: i2ii6n4
Fecal Col"dorms
BRL
0.2 MPNIg wet
Sample Extraction
Data
Prep Method: 3512
Lab Number
Batch
Initial
Final
DateTme
4120290-01
P41_0329
0.05 g
25 mL
12/18/14 10:15
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
DateTme
4120290-01
P41-0353
1 g
50 mL
12/19/14 11:30
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
DateTme
4120290-01
P41_0341
30 g
30 g
12/18/14 15:50
4120290-02
P41_0341
30 g
30 g
12/18/14 15:50
4120290-03
P41_0341
30 g
30 g
12/18/14 15:50
4120290-04
P41_0341
30 g
30 g
12/18/14 15:50
4120290-05
P41_0341
30 g
30 g
12/18/14 15:50
4120290-06
P41_0341
30 g
30 g
12/18/14 15:50
4120290-07
P41_0341
30 g
30 g
12/18/14 15:50
Prep Method: 3050E
Lab Number
Batch
Initial
Final
DatelTme
4120290-01
P41-0330
1.99 g
50 mL
12/18/14 11:57
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
4120290-01
P41_0311
0.61 g
50 mL
12/17/14 11:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
-. ,;.449 Springbrook Road -P.O. Box 240543, Charlotte, NC 28224-0543 _-
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax:[phone] Page 13 Of 14

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CHAIN OF CUD, REGUND
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Or QUOTIE TO ENSURE PROPER BILLING:
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Flo vrc.n'Ias: 114c,
Project Name:
Cl)nlotle., lIC 2 224-LIS43
3c)(2405 .3 8 ST Project. (Yes) (No)
Short Hold Analysis: (Yes) (No) US
iTHi HOLD INGITi MES
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ATTACH any project specific reporting (00 LEVEL I It 101 IV)
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A yprovisions and/or QC Requirements Cheat Company Nam
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to w TP
Rush Work Must Be
Days" 0 6-9 Days EI.Standard 10 days (2 Pre -Approved
SC_ OTHER _N/A
Site Location Name: 11�114 li-, Samples received after 15:00 will be processed next business day.
6C11 FA Turnaround time is based on business days, excluding weekends and holidays.
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ID NO.
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HOURS
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SEE BELOW I,
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submitted in writing to the Prism project manager. There will be chftes for any changes aft
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Hand-deliverPrism Field SLM"
CJFQdEx UUPS Q n Other
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