WQ0006245_Regional Office Historical File Pre 2018 (9)

,f� ja ttf' CCt
ROY COOPER
Governor
- MICHAEL S. REGAN
Secretory
A S. JAY ZIMMERMAN
Water Resources Director
Environmental Quality
April 5, 2017
Mr. Andy Smith, Fourth Creek WWTP Supervisor
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Subject: Acknowledgement of Receipt of the 2016 Annual Report
City of Statesville N-Viro Processing and Sta Lime
Distribution Program - PermitWQ0006245
Distribution of Residuals (503)
Iredell County
Dear Mr. Smith:
The Mooresville Regional Office (MRO) has received and reviewed the 2016 Annual
Report(AR) for the above permit. The information submitted appears to meet permit
requirements.
For your convenience, The MRO has enclosed guidance documentation for the procedure on
how the Annual Reports are to be correctly assembled. The MRO is also requesting copies of
future reports be presented in a bound format for ease of review.
The information provided and supporting, documentation indicates the facility was not in
operation until April 2016 due to demolition of the old system and construction of the new
system. The report indicates 1,243 dry tons of Class A residual was distributed to various
famers.
As also noted for the 2015 AR, the contract laboratory is still not consistently supplying, the
Plant Available Nitrogen (PAN) or the Sodium Absorption Ration (SAR) calculations.. These
calculations are necessary in order to be able to verify the numbers generated. In future, please
have the contract laboratory submit these calculations as part of the analytical data.
State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1610 East Center -Avenue, Suite 3011 Mooresville, North Carolina 28115
704-663-1699

N1 I C)
February 15, 2017
Attention: Ed Hardee
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Reports for 2016
Alkaline Stabilization (WQ0006245)
I
RECEiVEDINCDENRIDWR
FEB 2 'J 2017
WQROS
MOORESVILLE REGIONAL OFFICE
rLB 2 2 2017
E%foimation roco—sGing Uilit
DIPVR section
Dear Mr. Hardee:
Enclosed, you will find I original and 2 copies of the required forms and lab data for the Alkaline
Stabilization program. Permit # WQ0006245.
This permit was compliant for the year.
Should you require more information, or:if further action is required, please- contact me at 704- 878-3438.
c
Ani
th
WWTP Supervisor, Fourth Creek WWTP

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2016
PERMIT NO. WQ0006245
FACILITY NAME: Fourth Creek WWTP NPDES NCO031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: L.F. "Joe" Hudson Jr., Director
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1 Ill
[phone]
RESIDUALS ORC: Andy Smith
Plant Supervisor
P.O. Box, 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization WQ Permit Number: WQ0006245
WWTP Name: Fourth Creek WWTP
NPDES Number: NCO031836
Monitoring Period: From 1/1/2016 To 12/31/2016
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
I Alt B (Alk Treatment) 21
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
amma Ra
G y
ati
n Pasteuz on ❑
Class B:
jAlt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
Num er ot
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
ni ue
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<0.3
1
mpn/g
.
60 days
grab
sm9221 e
CFU
`
IECEIV
:171�!CDENR
DWR
1000 mpn per gram
of total solid (dry
weight)
.
r E
? 7 Z 11,
WQROS
/
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
<0.031
mpn/4g
t
I'
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-daybench) ❑
Alt. 4 (Spec. Oz uptake)
R1
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
0
Alt 7 (Drying - Stable) ❑
1Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T A106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Pr ame and Title pe or print) // Land Applier Name and Title (if applicable)(type or print)
�CQ
Signat a of Preparer* hate Signature of Land Applier (if applicable) Date
*Preparer is defined in_40 'CFR Part 503.9(r) and 15A NCAC 2T'.1102 (26)
DENR FORM PVRF.02T (12/2006)

ANNUAL RESIDUAL SAMPLINGSUMMARY TORM..
Please note that your permit may contain additional parameters to be analyzed. The parameters canbe reported in FORM RSSF B - - .
WQ Permit Number: WQ0006245
Facility Name:
Residual Source WQ # or NPDES # NC0031836
NPDES #:
WWTP Name:
Residual Analvsis Data
Fourth Creek WWTP
Laboratory: 1)
2)
3)
4)
5)
Prism Labs
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
4/11/16
7/5/16
10/11/16
Percent Solids (%)
NA
*
64%
81 %
79%
Arsenic
75
*
0.48
7.4
<3.2
Cadmium
85
*
<0.39
<0.31
<3.2
Copper
4,300
*
2.9
26
43
Chromium
NA
*
N/A
N/A
N/A
Lead
840
*
1.7
11
3.2
Mercury
'57
*
0.14
0.16
<0.026
* -
No
sample
collected
Molybdenum
75
*
N/A
N/A
N/A
due to
constr.
of new
equip.
Nickel
420
*
23
230
7.2
Selenium
100
*
1.1
1.7
8.8
Zinc
7,500
*
7
37
44
Total Phosphorus
NA
*
1,800
1,400
2,400
TKN
NA
*
4,700
3,900
5,200
Ammonia -Nitrogen
NA
*
150
54
120
Nitrate and Nitrite
NA
*
8.5
<6.2
88
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to a u e that qualifiel personnel properly gathered and evaluated the information submitted. I am aware that there are significant
pe a i s for s, m1tY g false information, including the possibility of fines a7!/)7
nmentfor knowing violations."
Signa re of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

r
Initial pH: ,�j'J
Start Time/Date/Temp
i
PLt
Corrected pH: , b
/.
Final pH:
End Time/Date/Temp
Corrected pH:
Has 12 Hour Temp Criteria Been Met? lV
Has 72 Hour pH Criteria Been Met? N_
BIN #
Setup Date: -/(
Removal From Bin Date: S /2•/.1
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
/a O
Initial pH: 010
Start Time/Date/Temp
Corrected pH: / , j
Wop
Final pH'
End Time / Date / Temp
Corrected pH: Q
Has 12 Hour Temp Criteria Been toilet? Y N
Has 72 Hour pH Criteria Been Met? N
BIN.#o?
Setup Dater /0 /
Removal From Bin Date:°
Date
Time
pH >12':0' For 72-Hrs:
TEMP:->5Z Deg. C For 12 Hrs.'
Operator
./d,
Initial pH:
Start Time/Date/Temp
Corrected pH: 12,,bf
13 `t
j: ©D &
Final pH: ,Op
End Time/Date/Temp
0
Corrected pH: . /
Has_12 'Hour Temp Criteria Been Met? V N
.Has 72 Houk . H. Ciriteria Been:.t�let?
p

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: 5 -If -lb
Removal From Bin Date: 5-- * /
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Start Time / Date / Temp
p
L
Corrected pH: l •yp
•/ -/
l/.49h-
Final pH:
End Time/Date/Temp
lCorrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
BIN # . $
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: L2, /Q
Start Time/Date/Temp
.
Corrected pH: QG
- 9-1�
a
Final pH: /a ,
End Time/Date/Temp
Corrected pH:
Has 17 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
BIN # I
Setup Date: $- 1(5-
Removal From Bin Date: S%23-1L
Date
Time
pH >12.0 For 72 1-Irs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: f ,Off
Start Time/Date/Temp
rrected pH:nal
M
pH: I
End Time/Date/Temp
6 Gi 0
1
rrected pH:
Has 12 Hour Temp Criteria Been Met? N
F - ---- Has 72 Hour pH Criteria Been Met?- Y N
BIN # 'Z
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
f p
Initial pH: U,03
Start Time/Date/Temp
Corrected pH: /Q .
. j ,
o?,pb ,
Final pH: �; f
End Time / Date / Temp
�07
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
BIN,#.:... r, .-:,
Setup,.Date:-,:: :.
Removal, From Date:
Date
'Time
_ _pH_>1=2:0"�or'72 Hrs.""'"'
` TEMP. >52•Deg. C For 12 Hrs.-- '
-Operator,
J
Initial pH: )a,O
Start Time/Date/Temp
oCorrected
PLO
pH:
Final pH:
End Time/Date/Temp
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour -PH •.Criteeria,'Been,Met?•. •, ,i.;N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # Setup Date: ,,-20-/& Removal From Bin Date:
Date Time I pH >12.0 For 72 Hrs. TEMP. >52 Deg. C For 12 Hrs. Operator
Initial pH' Start Time/Date/Temp
Corrected pH: 3 77 d L
Final pH: End Time/Date/Temp e
Corrected pH: '70
Has 12 Hour Temp Criteria Been Met? N .
Has 72 Hour pH Criteria Been Met? N
BIN # . Setup Date: Removal From Bin Date:
Date Time pH >12.0 For 72 Hrs. TEMP. >52 Deg. C For 12 Hrs. Operator
Initial pH: /,SjY Start Time /Date /Temp
"1 l a.00Corrected pH: J ,7(� (� Us
Final pH: �. r�r7 End Time/Date/Temp
Corrected pH:
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
BIN # -1 Setup Date: y ;dq. Jk Removal From Bin Date:
Date Time pH >12.0 For 72 Hrs. TEMP. >52 Deg. C For 12 Hrs. Operator
Initial pH: ' Start Time/Date/Temp
apt l nWA,rrected pH:nal pH:End Time / Date / Temp
Irrected pH: 1340 l�✓
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH'Criteria Been Met? Y N
BIN # �' Setup Date: / /r/- Removal From Bin Date:
Date Time pH >12.0 For 72 Hrs. TEMP. >52 Deg. C For 12 Hrs. Operator
Initial pH: start rime/Date/Temp
Corrected pH:
Final pH' (p'S' End Time/Date/Temp ff �
J) - d _ I/. •1 ' Corrected pH: 1 J . Rq
Has 12 Hour Temp Criteria Been Met? Y N
Has 72-Hour pH Criteria Been Met? Y N
BiN'#.. 1-1
Setup Date:
Removal From Bin- Date:
Date
Time
OR>12'.0'For 72 Hrs:-
TEMP: >52 Deg. C For 12 Hrs.-
Operator.
Initial pH: b
Start Time/Date/Temp
Corrected pH:
Final pH: ,7g
End rime /Date /Temp
�S
Corrected pH:
Has 12 Hour Temp Criteria Been Met? Y N
Has 72- Hour-pKCrlteria Been MetT :._.._ Y .. N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 5
Setup Date: % - 6-4
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
ifCorrected
Initial pH arY9-
Start Time/Date/Temp
�
3
pH: JacS 1
o,
Final pH: 1a•!V &
End Time/Date/Temp
�`
Rud
Corrected'pH: J-2,
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? 60 N
BIN # _. `7
Setup Date:
Removal From Bin Date: Ja-
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3c,16%:
`is
Initial pH: a ,q r
start Time / Date / Temp
�s�
Corrected pH: a -(D
Final pH: Ja -! fk
End Time/Date/Temp
Ltd
Corrected pH: Z,
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? CY) N
BIN # a-
Setup Date: ,'- J,3.-4�
Removal From Bin Date:
Date
Time
pH >12.6 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
- A
Pgs-
Initial pH:
Start Time/Date/Temp
-A
Corrected pH: 9
Final pH: %�,s,�j
End Time
�L
p.
Corrected pH: , �
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pHf Criteria. Been Met? Y .-N
BIN # I
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
l)-I
'a
Initial pH' I ')—
Start Time/Date/Temp
LC)
Corrected pH: (J
-/(� / •
. .50
Final pH: �-
End Time/
71 �
Corrected pH:
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? N
BIN #>" ,... „
Setup Aate,:.,. , .-, , _..-. " .
Removal From Bin Date:
" Date'
-'TinT "'
`—`-PH-�12 OfOf'"72`HTs. --
TEMP:>52'Deg.'C'For12 Hrs. ''
`Operator'
Initial pH:
start Time/Date/Temp
Corrected pH:
Final pH:
End Time/Date/Temp
Corrected pH:
Has 12 Hour -Temp Criteria Been Met? Y N
Has 72 HourpRCriteria-Been -.Met-?,,Y N

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization WQ Permit Number: WQ0006245
WWTP Name: Fourth Creek WWTP NPDES Number: NCO031836
Monitoring Period: From 1 1/1/2015 To 12/31/2015
Pathoeen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (A1k Treatment) 0
Alt; C (Prior Testing)'❑
A1t.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative perfonned (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermo hilic ❑
............
::.:.:.:.:.:.:.:.:.:.:.
Beta Ray ❑
Gamma Ray ❑
Pasteurization
Class B:
jAlt. (1).Fecal Density p
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative
perfonned (Class B
only) indicate "Process to Sipificantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
I - Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion 13If
applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
ni ue
Minimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<0.2
1
mpn/g
60 days
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
<0.027
mpn/4g
Vector Attraction Reduction (15A NCAC
02T .1107) -Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑Alt.
4. (Spec. OZ uptake) 0
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9.(Injection) --- - ❑„
Alt. 10-(Incorporation)-. ❑
No vector: attraction.reduction alternatives were performed:. ❑
U K I Ir IUA I IVA J I A I L+ LVIV 1V I (please cnecK Tne appropriate Statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the . .
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system r
designed to ensure that qualified personnel properly gather and evaluate the information used to determine = -
.•that the pathogen and vector. attraction .reduction -requirements _havebeen meta Lam aware .that, there, ar_e-:....-.
Sig ficant penalties for false certification including fine and imprisonment." -
IlAk
Pr arl Name apd T' le (type or print) Land Applier Name and Title (if applicable)(type or print)
Sign re of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

City of Statesville
Mr. Andy Smith
Post Office Box 1111
Statesville NC, 28687-1111
�VIA'a
Fayetteville Division
Certificate of Analysis
Project: Sta-lime/Sludge Sample - 4th Creek W WTP
Sta-lime Sample, Grab
K6H0263-01
Date Reported: 08/27/16
Date Received: 08/08/16
Date Sampled: 08/08/16
Sampled By: Smith
Analyte
Result
Units
Analyzed Analyzed By
Method
Qualifier
Analyzed by: Microbac Laboratories, Inc. - Baltimore
% Solids
82.54
% by Weight
08/11/16 09:00 RLD
SM 2540 G-11
Salmonella
<0.031
MPN/4g dry
08/11/16 16:00 QLW
EPA 1682
QC Batch Run - (Microbac Laboratories, Inc. -Baltimore)
Analyte
Result
Units
Source
RPD
Limit
% Solids
24.39
% by Weight
16HO750
10.3
5
% Moisture
75.61
% by Weight
16HO750
3.11
5
Notes and Definitions
RI Sample Duplicate RPD was out of acceptance limits.
State Certifications:
NCDNR 911
NCDOH #37714
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. We invite your feedback on our level q(service to you. Please contact the Division Manager, Rob Dermer at 910-864-1920 tivith any
gn6timis. Yuri niay also' contact :I: Trevor Boyce, President at president a microbae.com � , , . , _. .. ,
Microbac Laboratories, Inc. Page 1 of 2
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 [phone] / 864-8774 fax
CHAIN OF CUSTODY RECORD
PAGE 1 OF 1
CLIENT NAME BADDRESS:
City of Statesville
693 Bell Farm Road
Stateville NC 28677
:•
Po# -
' 1.33432,
PROJECT I LOCATION:
4th Creek WWTP
W
0
m
0
#
TYPE
OF ANALYSIS
PRESERVATION (CODE)
o
a
Z
CL
2
E
CODE: A = None
B = HNO3 (pH<2) + <6°C
C = H2SO4 (P H<2 + <6°C
)
D = NaOH + <6°C
E = ZN Acetate + <6°C
F = HCI
G = Sodium Thio
CONTACT PERSON:
Mr. And Smith
PHONE:
704=878-3438
Sampled By:
Andy Smith
DATE METHOD OF SHIPMENT:
8/06 UPS Next Day Air
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
GRAB
r PH
FLOW
TEMP-C
CHLORINE
SULFIDE
Sta-Lime
8/8/16
12:00 Noon
X
1
A
VQ"
Relinquished by:
Date.
Time
Received by: (Signature)
Date
Time
AndySmith 1
08/08/16
12:15 P
Kt( ' l —I AL:-) Iitw"a
r4
Relinquished by:
Dates
Time
Received by: (Signature)
Date
Time
3
r
4
Relinquished by:
Date •
Time
Received y: (Signature)
Date
Time
g
6
pH Field : ph Field: water Levet;iFi
Temp Field 1: Temp Field 2: Water Level #2
Turnaround time: REGULAR
Comments or Special Hazards:
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH:
Page 2of2

NC Certification No. 402 Case Narrative
SC Certification No. 99012
I M
Full -Service Analytical 8� NC Drinking Water Cert No. 3773504/04/2016
Environmental Solutions VA Certification No. 460211
ABORATORIES, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/I EC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 03/28/2016
Prism Work Order: 6030461
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) t�_ A—.
?PV--
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
HT Sample received and analyzed outside of the hold time.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page Of 7

Sample Receipt Summary
3: I S n %� Full -Service Analytical 8
' V' environmental Solutions 04/04/2016
.y1ti,.._-y.�,-a..i.-.d'•LABOR-RIE$ING
Prism Work Order: 6030461
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime (A) 6030461-01 Solid 03/23/16 03/28/16
Samples were received at 26.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report'....
I I S n n Full -Service Analytical &
I V' Environmental Solutions 04/04/2016
LABORATORIES ING
City of Statesville, NC Project: StaLime Client Sample ID: StaLime (A)
Attn: Andy Smith Prism Sample ID: 6030461-01
P.O. Box 1111 Prism Work Order: 6030461
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/23/16 00:00
Time Submitted: 03/28/16 14:10
Parameter
Result Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids
57.6 % by
0.100
0.100 1
*SM2540 G 3/30/16 9:59 SLS
P6C0521
Weight
Microbiological Parameters
Fecal Coliforms
BRLHT MPN/g dry
0.3
1
*SM9221 E 3/28116 15:08 EGC
P6C0522
Total Metals
Mercury
0.14
mg/kg dry
0.034
0.0040
1
*7471B
3131/16 12:41
JAB
P6C0530
Arsenic
6.9
mg/kg dry
0.43
0.096
1
*6010D
3/31/16 3:11
bgm
P6C0504
Cadmium
0.46
mg/kg dry
0.43
0.0092
1
*6010D
3131116 3:11
bgm
P6C0504
Copper
53
mg/kg dry
0.87
0.15
1
*6010D
3/31116 3:11
bgm
P6C0504
Lead
8.0
mg/kg dry
0.43
0.046
1
*6010D
3/31/16 3:11
bgm
P6C0504
Nickel
140
mg/kg dry
0.87
0.081
1
*6010D
3/31/16 3:11
bgm
P6C0504
Selenium
1.6
mg/kg dry
0.87
0.063
1
*6010D
3/31116 3:11
bgm
P6C0504
Zinc
100
mg/kg dry
4.3
0.053
1
*6010D
3131/16 3:11
bgm
P6C0504
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Of 7

Level II, QC Report`""
Ism Full -Service Analytical & 4I4I16
Environmental Solutions
LABOR TORIGs INO
City of Statesville, NC Project: StaLime Prism Work Order: 6030461
Attn: Andy Smith Time Submitted: 3/28/2016 2:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6CO504 - 3050B
Blank (P6C0504-BLK1)
Prepared: 03/30/16 Analyzed: 03/31/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6C0504-BSI)
Prepared: 03/30/16 Analyzed: 03/31/16
Arsenic
24.4
0.25
mg/kg wet
25.00 97 80-120
Cadmium
23.4
0.25
mg/kg wet
25.00 94 80-120
Copper
26.3
0.50
mg/kg wet
25.00 105 80-120
Lead
23.6
0.25
mg/kg wet
25.00 95 80-120
Nickel
24.3
0.50
mg/kg wet
25.00 97 80-120
Selenium
24.3
0.50
mg/kg wet
25.00 97 80-120
Zinc
24.1
2.5
mg/kg wet
25.00 96 80-120
Batch P6CO530 - 7471 B
Blank (P6C0530-BLK1) Prepared &Analyzed: 03/31/16
Mercury BRL 0.020 mg/kg wet
LCS (P6C0530-BS1) Prepared &Analyzed: 03/31/16
Mercury 0.447 0.020 mg/kg wet 0.4167 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 7

I I n I Full Service Analytical &
'v' Environmental Solutions
LABORATORIES -
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
414/16
Prism Work Order: 6030461
Time Submitted: 3/28/2016 2:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6CO521 - Solids, Dry Weight
Blank (P6CO521-BLK1) Prepared & Analyzed: 03/30/16
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 7

Level 11 QC Report
n %�Full-Service Analytical &
I v' Environmental Solutions
F-Ei.
4/4/16
m.'?` LA9ORATORIEa INC.
City of Statesville, NC
Project:
StaLime
Prism Work Order: 6030461
Attn: Andy Smith
Time Submitted: 3/28/2016 2:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P6CO522 - NO PREP
Blank (P6CO522-BLK1)
Prepared & Analyzed: 03/28/16
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final'
Daterrime
6030461-01 P6C0521
30 g
30 g
03/30/16 9:59
Prep Method: 3050B
Lab Number Batch
Initial
Final
Daterrime
6030461-01 P6C0504
2 g
50 mL
03/30/16 8:55
Prep Method: 7471E
Lab Number Batch
Initial
Final
Daterrime
6030461-01 P6C0530
0.62 g
50 mL
03/31/16 9:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 7

Full -Service Analytical &
Environmental Solutions
u
LABORATOnirs, INC.
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] • Fax: [phone] yy
Client Company Name: Ca 1V or S4A�CSvs le_
Report To/Contact Name: 'A a S 1, Al
Reporting Address:
PAGIE OF - ®U®TE 9 To ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
"Please ATTACH any project specific reporting (QC LEVEL I.II III IV)
provisions andlor QC Requirements
Invoice To:
Address: -
YES
NO.. NIA
Q
Samples INTACT upon, amval? ✓
_, .
Received ON WET ICE?
PROPER PRESERVATIVES indicated? ✓
0)
N
Received WITHIN HOLDING TIMES _..--------D-
CUSTODY SEALS INTACT?
V,OLATII_ES rec'd W/OUi" HEADSPACE?
._
PROPER CONTAINERS used?:,'
TENtf': Therm ID:__ / to Obsarved: 7 °C! Corr: �2 �2 °C
Phone:[phone]' FaX Yes (No): 70''- &? CPurchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL`
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC Do®
FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush WorkeMust Be
ry0 OTHER
N/A
Site Location Name: Creek ��'p Samples received after 14:00 will be processed next business day.
-��
Site Location Physical Address: q 3 j P 7l1 rrt )� Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p
NO
NO -
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA-
REMARKS
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES
ID NO.
��:�t"
HOURS SLUDGE) SEE BELOW
As
c FQ
CQ
Pb
�/� il
Sampler's Signature /I' Sampled By (Print Name) a e91 Affiliation
GM
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
a
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
d B Si na a ate
Relin had By: (Signature)Re a eY�
%� l I 9 )
Military/Hours
� Additional Comments
sde An IvafTlme .:
Reaned By: n ure) i d By: (Signature) Date
Ste Deparlw e Timer
/GField
FeeRe
q is ed By: (Si lure) Received For n Lab od By: Date
Tech:
� 1-y lCp
� Yw
Mileage;,,
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH ODY SEALS FOR TRANSPORTATION TO THE LABORATORY C C Group No.
----- ------
SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST COC, IL RECEIVED AT THE LABORATORY.
d Ex ❑ UPS ❑ Hand delivered P sin Field Service ❑Other l�>u"tl
UST: G 0 DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
•�
❑NC ❑SC ❑ C ❑SC ❑NC ❑SC I ❑NC ❑SC ❑NC❑SCl ❑NC ❑SCI❑NC ❑SC ❑NC ❑SC
❑ ❑ ❑ ❑ ❑ ❑ ❑
ODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Gap vuA = volatile urganlCS Analysis (cero neaa opace)

NC Certification No. 402
M
SC Certification No. 99012
I Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No. 460211
AeoRATORIE3, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 03/28/2016
Prism Work Order: 6030460
Case Narrative
04/04/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
HT Sample received and analyzed outside of the hold time.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page] of 7

I n n Full -Service Analytical &
'v' I Environmental Solutions
%B-ORIES ING
Sample Receipt Summary .,.
04/04/2016
Prism Work Order: 6030460
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime 3
6030460-01 Solid 03/25/16 03/28/16
Samples were received at 26.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 7

S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 04/04/2016
\9ORATORIES ING
City of Statesville, NC
Project: StaLime
Client Sample ID: StaLime 3
Attn: Andy Smith
Prism Sample ID: 6030460-01
P.O. Box 1111
Prism Work Order: 6030460
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 03/25/16 00:00
Time Submitted: 03/28/16 14:10
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
71.6
% by
0.100
0.100
1 'SM2540 G 3/30/16 9:59
SLS
P6C0521
Weight
Microbiological Parameters
Fecal Coliforms
BRLHT MPN/g dry
0.3
1 'SM9221 E 3/28/16 15:08
EGC
P6C0522'
Total Metals.
Mercury
0.094
mg/kg dry
0.029
0.0035
1 *7471B 3/31/16 12:36
JAB
P6C0530
Arsenic
7.3
mg/kg dry
0.35
0.079
1 '6010D 3131/16 3:01
bgm
P6C0504
Cadmium
BRL
mg/kg dry
0.35
0.0075
1 '6010D 3/31/16 3:01
bgm
P6C0504
Copper
36
mg/kg dry
0.71
0.12
1 '6010D 3131/16 3:01
bgm
P6C0504
Lead
7.7
mg/kg dry
0.35
0.037
1 '6010D 3/31/16 3:01
bgm
P6C0504
Nickel
160
mg/kg dry
0.71
0.067
1 "6010D 3131/16 3:01
bgm
P6C0504
Selenium
1.4
mg/kg dry
0.71
0.051
1 '6010D 3/31116 3:01
bgm
136C0504
Zinc
70
mg/kg dry
3.5
0.043
1 '601013 3/31/16 3:01
bgm
P6C0504
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

�//�� Level 11 QC Repoi�""
.....:........
ISIVI :....
Full -Service Analytical & 4/4/16 r�
Environmental Solutions
%BOFATOFIE$ ING
City of Statesville, NC Project: Stal-ime Prism Work Order: 6030460
Attn: Andy Smith Time Submitted: 3/28/2016 2:10:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6C0504 - 3050B
Blank (P6C0504-BLK1)
Prepared: 03/30/16 Analyzed: 03/31/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6C0504-BSI)
Prepared: 03/30/16 Analyzed: 03/31/16
Arsenic
24.4
0.25
mg/kg wet
25.00 97 80-120
Cadmium
23.4
0.25
mg/kg wet
25.00 94 80-120
Copper
26.3
0.50
mg/kg wet
25.00 105 80-120
Lead
23.6
0.25
mg/kg wet
25.00 95 80-120
Nickel
24.3
0.50
mg/kg wet
25.00 97 80-120
Selenium
24.3
0.50
mg/kg wet
25.00 97 80-120
Zinc
24.1
2.5
mg/kg wet
25.00 96 80-120
Batch P6130530 - 7471 B
Blank (P6C0530-BLK1) Prepared &Analyzed: 03/31/16
Mercury BRL 0.020 mg/kg wet
L_CS (P6C0530-BS1) Prepared &Analyzed: 03/31/16,
Mercury 0.447 0.020 mg/kg wet 0.4167 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 7

IS M Full -Service Analytical Environmental Solutions
�'�LABORATORIES ING
City. of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report""
4/4/16`._..:.
Prism Work Order: 6030460
Time Submitted: 3/28/2016 2:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6CO521 - Solids, Dry Weight --
Blank (P6CO521-BLK1) Prepared & Analyzed: 03/30/16
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 Of 7

R ISM Fun
-Service
-Service Analytical
Environmental Solutions
,�.-w�'�w .-� LABOPATOPIES ING
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
4/4/16
Prism Work Order: 6030460
Time Submitted: 3/28/2016 2:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6CO522 - NO PREP
Blank (P6C0522-BLK1)
Prepared &Analyzed: 03/28/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final Daterrime
6030460-01 P6C0521
30 g
30 g 03/30/16 9:59
Prep Method: 3050E
Lab Number Batch
Initial
Final Date/rime
6030460-01 P6C0504 1.97 g 50 mL 03/30/16 8:55
Prep Method: 7471E
Lab Number Batch Initial Final Date/rime
6030460-01 P6C0530 0.57 g 50 mL 03131/16 9:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-6543
Phone: [phone] -Toll Free Number: 1-800/529-6364- Fax: [phone] Page 6 of 7

CHAIN OF CUSTODY RECORD
+SM PulliService Analytical &
.`..
NO NIA
YC�. ,. I --
e Environmental Solutions PAGE_ OF _ QUOTE # T® ENSURE PROPER BILLING:
..
Samples IN TACT upon arrival?
✓
f� _t
LABORATORIES, INC.
Project Name:
Received ON WET ICE?.
lv
449 Springbrook Road - Charlotte, NC 28217
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER PRESERVATIVES indicated? `
_
'` rn
c
Phone [phone] - Fax: [phone]
`Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
�%%y
Received WITHIN HOLDING TIMES.
Client Company Name: aT ���+ fib' '�r� provisions and/or QC Requirements
CUSTODY SEALS INTACT
HEADSPACE?
Ott To/Contact Name: v �.�� )t
Report -y Invoice To:
-VOLATILES reed W/OUT
Reporting Address:
P 9 Address:
PROPER CONTAINERS' used?
" TEMP: Therm ID: _i Observed; °C /Corr C
Phone: [phone]`1.3,3 Fax es (No): F73�-S 7S- �L3 � purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 pays ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
Must Be
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ P e Ap Work
SC OTHER
N/A
_ a LtiTL91
Site Location Name: F' . r-7 k Cre.c.A r Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 693 Be-!)i Fa r.n RA, Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES- NO
SERVICES
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING
Sample Iced Upon Collection: YES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p p
NO
- -
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- �\r
REMARKS
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE NO. SIZE TIVES �E. ��
ID NO!
HOURS SLUDGE) SEE BELOW
-3
3 uh
P
N sa 03
v /
° rn,x
A
C
►mob
Se
J
Zi4
Sampler's Signature / r Sampled By (Print Name) A ;, C Offillationpe-S,&IaL
012eiI
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relinquished By. (Signature) ec ived 8y: ( g nasl ture) D e
J
Military/Hours Additional Comments:
Site. Arrival Time:
.
Re inqu hed By. (Si ture) y: (Signature) Date
Site Departure Time:
Field Tech Fee:
Rern ished By: (Si re Received F rism L�t+O lofi s by: Dale
5 /vy—t� 5`Z� /(,+
�ci'1 C
Mileage:
r
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WI USTODY AL S FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST C UNTIL RECEIVED AT THE LABORATORY.
��
0
Fed Ex ❑ UPS ❑ Hand -delivered ' Pr m Field Service ❑ Other
S: UST: G DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:
SC ❑ NC ❑ SC I ❑ NC ❑ SC ❑O NC ❑ SC I NC ❑ SC I ❑❑ NC O SC I 0 NC ❑ SC O NC ❑ SC
O NC ❑ SC
n 0
'ODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (/-ero heao Space) ;> ; i,;r •;;

City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Quarterly Parameters)
Lab Submittal Date: 04/11/2016
Prism Work Order: 6040214
Case Narrative
04/25/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
' Vim• �_
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
�T
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 10

MFull-Service Analytical &
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iATORIES ING
Sample Receipt Summary
04/25/2016
Prism Work Order: 6040214
ID Lab Sample ID Matrix Date Sampled Date Received
Stal-ime 6040214-01 Solid 04/11/16 04/11/16
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Full -Service Analytical 8.
Environmental Solutions
v+c
JC
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
04/25/2016
Project: StaLime (Quarterly Client Sample ID: StaLime
Parameters) Prism Sample ID: 6040214-01
Prism Work Order: 6040214
Sample Matrix: Solid Time Collected: 04/11/16 14:30
Time Submitted: 04/11/16 16:20
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
Plant Available Nitrogen
910
mg/kg
160•
18
2
*Calculation
4/19/16 7:56
CLB
[CALC]
% Solids
63.7
% by
0.100
0.100
1
*SM2540 G
4/13/16 15:36
SLS
P6DO234
Weight
Nitrate/Nitrite as N
8.5
mg/kg dry
7.9
0.86
1
*SM4500-NO3 F
4/19/16 7:56
CLB
P6DO271
Phosphorus -Total
1800
mg/kg dry
79
37
20
*SM4500-P F
4/20/16 11:29
CLB
P61)0264
Total Kjeldahl Nitrogen
4700
mg/kg dry
790
89
2
*351.2
4/15116 8:51
CLB
P6DO203
Ammonia as N
150
mg/kg dry
16
6.1
2
*SM4500-NH3 G
4/14/16 8:34
CLB
P6DO236
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
4/12/16 9:41
EGC
P6DO213
Total Metals
Mercury
0.14
mg/kg dry
0.033
0.0018
1
*7471B
4/13/16 12:09
JAB
P6DO210
SAR Soil Preparation
0.0
g
1
*2-78-054
4/14/16 7:20
JAB
P6DO200
SAR Percent Moisture
54.2
% by
0.100
0.100
1
*2-78-054
4/14/16 11:45
JAB
P6DO249
Weight
Arsenic
0.48
mg/kg dry
0.39
0.048
1
*6010D
4115/16 21:32
bgm
P6DO208
Sodium Absorption Ratio
1.0
[blank]
0.30
0.016
1
*2-78-054
4/14116 22:47
bgm
P6DO244
Cadmium
BRL
mg/kg dry
0.39
0.011
1
*6010D
4/15/16 21:32
bgm
P6DO208
Calcium
2000
mg/L '
1.0
0.085
10
*6010D
4114/16 22:47
bgm
P6130244
Copper
2.9
mg/kg dry
0.79
0.071
1
*601013
4115/16 21:32
bgm
P6D0208
Lead
1.7
mg/kg dry
0.39
0.073
1
*6010D
4/15116 21:32
bgm
P61)0208
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
4/14/16 22:47
bgm
P6DO244
Nickel
23
mg/kg dry
0.79
0.028
1
*6010D
4/15/16 21:32
bgm
P6DO208
Potassium
750 BH
mg/kg dry
20
0.71
1
*6010D
4/15116 21:32
BGM
P6130208
Selenium
1.1
mg/kg dry
0.79
0.19
1
*601013
4/15/16 21:32
bgm
P6DO208
Sodium
160
mg/L
5.0
0.074
10
*6010D
4/14116 22:47
bgm
P6DO244
Sodium
970
mg/kg dry
24
0.77
1
*6010D
4/22116 17:49
BGM
P6DO208
Zinc
7.0
mg/kg dry
3.9
0.14
1
*6010D
4/15116 21:32
bgm
P6DO208
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OM
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 10

Level II'QC Report
I I n n I Full -Service Analytical & 4/25/19
V' Environmental Solutions
LABORATORIES -
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 6040214
Attn: Andy Smith Time Submitted: 4/11/2016 4:20:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6DO200 - SAR 2-78-054
Blank (P6D0200-BLKI)
Prepared: 04/13/16 Analyzed: 04/14/16
SAR Soil Preparation
0.00
g
Batch P6DO208 - 3050B
Blank (P61310208-1311-KI)
Prepared: 04/13/16 Analyzed: 04/15/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
BH
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
L_CS (P6D0208-BSI)
Prepared: 04/13/16 Analyzed: 04/15/16
Arsenic
23.1
0.25
mg/kg wet
25.00 93 80-120
Cadmium
23.5
0.25
mg/kg wet
25.00 94 80-120
Copper
24.7
0.50
mg/kg wet
25.00 99 80-120
Lead
23.5
0.25
mg/kg wet
25.00 94 80-120
Nickel
23.4
0.50
mg/kg wet
25.00 94 80-120
Potassium
498
12
mg/kg wet
500.0 100 80-120
Selenium
22.9
0.50
mg/kg wet
25.00 92 80-120
Sodium
524
15
mg/kg wet
500.0 105 80-120
Zinc
23.2
2.5
mg/kg wet
25.00 93 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 10

i n Full -Service Analytical &
' V' Environmental Solutions
LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Quarterly Parameters)
Level II QC Report
4/25/16
Prism Work Order: 6040214
Time Submitted: 4/11/2016 4:20:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6DO210 - 7471 B
Blank (P6D0210-BLK1)
Prepared & Analyzed: 04/13/16
Mercury
BRL
0.020
mg/kg wet
LCS (P6D0210-BS1)
Prepared & Analyzed: 04/13/16 _
Mercury
0.440
0.020
mg/kg wet
0.4167 106 80-120
Batch P6DO244 - 3010A
Blank (P6D0244-BLK1)
Prepared & Analyzed: 04/14/16
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
Batch P6DO249 - NO PREP
Blank (P6D0249-BLK1) Prepared & Analyzed: 04/14/16
SAR Percent Moisture BRL 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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I I A I Full -Service Analytical &
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l 00RATOFIM ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Annlvte
Project: StaLime (Quarterly Parameters)
Level II QC Report
4/25/16
Prism Work Order: 6040214
Time Submitted: 4/11/2016 4:20:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6DO203 - 351.2
Blank (P6D0203-BLK1) Prepared: 04/13/16 Analyzed: 04/15/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6DO203-BS1) Prepared: 04/13/16 Analyzed: 04/15/16 _
Total Kjeldahl Nitrogen 469 100 mg/kg wet 500.0 94 90-110
Batch P6130234 - Solids, Dry Weight
Blank (P6DO234-BLK1) Prepared & Analyzed: 04/13/16
% Solids 99.9 0.100 % by Weight
Batch P6130236 - NO PREP
Blank (P6D0236-BLK1) Prepared & Analyzed: 04/14/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6D0236-BS1) Prepared & Analyzed: 04/14/16
Ammonia as N 120 5.0 mg/kg wet 125.0 96 80-120
Batch 136DO264 - SM4500-PB5
Blank (P6130264-BLK1) Prepared: 04/15/16 Analyzed: 04/20/16 _
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P6D0264-BSI) Prepared: 04/15/16 Analyzed: 04/20/16
Phosphorus -Total 96.6 2.5 mg/kg wet 100.0 97 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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_% n e, Full -Service Analytical &
'v' Environmental Solutions
iATOR M Mc.
ille, NC
ith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (Quarterly Parameters)
Level II QC Report
4/25/16
Prism Work Order: 6040214
Time Submitted: 4/11/2016 4:20:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P61010271 - NO PREP
Blank (P6D0271-BLI(1) Prepared &Analyzed: 04/19/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6DO271-BSI) Prepared & Analyzed: 04/19/16
Nitrate/Nitrite as N 48.2 5.0 mg/kg wet 50.00 96 80-120
This report should not be, reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Level II QC Report—,
ViR I S M
Full -Service Analytical &
Environmental Solutions
" 4'/26/1$'' `"`
� LASO-RIES ING
City of Statesville, NC
Project: StaLime (Quarterly Parameters) Prism Work Order: 6040214 .
Attn: Andy Smith
Time Submitted: 4/11/2016 4:20:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters —Quality Control
Reporting Spike Source %REC RPD
Analyte
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6DO213 - NO PREP
Blank (P6D0213-BLK1)
Prepared & Analyzed: 04/13/16
Fecal Coliforms
BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab'Number
Batch
Initial
Final
Daterrime
6040214-01
P6D0203
0.05 g
25 mL
04/13/16 10:00
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Date/Time
6040214-01
P6D0264
1 g
50 mL
04/15/16 11:50
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
6040214-01
P6D0234
30 g
30 g
04/13/16 15:36
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
6040214-01
P6D0244
50 mL
50 mL
04/14/16 9:26
6040214-01
P6D0244
50 mL
50 mL
04/14/16 9:26
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
6040214-01
P6D0208
2 g
50 mL
04/13/16 8:04
6040214-01
P6D0208
2 g
50 mL
04/13/16 8:04
Prep Method: 7471 B
Lab Number
Batch
Initial
Final
Date/Time
6040214-01
P6D0210
0.58 g
50 mL
04/13/16 8:45
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
6040214-01
P6D0200
"`" 250 g ' "'
' 250'g
04/13/16 7:20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Page 8 of 10
Phone: [phone] -Toll Free Number: 1-800/529-6364 -Fax: [phone]

f SM Full -Service Analytical &
� Environmental Solutions
I'
IABORATORICS, INC.
449 Springbrook Road - Charlotte, NC 28217
'Phone [phone] • Fax:
7041525.0409
��� ait
Client Company Name: �`a,l°��b��C
Report To/Contact Name: A" - Dfl
Reporting Address:
CHAIN OF CUSTODY RECORD
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
'Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
YES% NO ,..NIA'" O
Samples INTACT upon arrivPI?"
Received ON WET ICE?
G7
'PROPER PRESERVATIVE ihdicated?_ ry
;ReceivedV�tITHIN FIOLDING.TIMES� M.
CUSTODY SEALS iNT4Cr?
VOLATII_ES rec d WIOUT HEADSPACC2'
PROPER CONTAINERS used?
TEMP: Therm ID. I� Observed ; C I Corif .°C
Phone:-70Y-s!?,` 3`l39 Fax' Yes (No):7 V-9 r- Sd 5-5 purchase Order No./Billing Reference TO BE FILLS® IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF_Excel _Other I "Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ Rush
re Apprrovedust Be Sc OTHER NIA
Site Location Name: ro w rj A C it e e.K A'' i i Samples received after 14:00 will be processed next business day. Water Chlorinated: YES NO
—
Site Location Physical Address: 73 i j j �'✓1c'T^ �a - Turnaround time is based on business days, excluding weekends and holidays.
y (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_ NO
t** C RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p --
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- �Y /A$`�� REMARKS LAB
FSAMPLEDESCRIPTION COLLECTED MILITARY WATER OR 'TYPE NO. SIZE TIVES +�( �C ID NO.
HOURS SLUDGE) SEE BELOW i
J A a✓n� 4i...d�'�� 1q'30
u
0
As.
c9 PA
P6 SA
N
S
Sampler's Signature CcJ Sampled By (Print Name) Ira �`+Ck' Affiliation eS`bS n1
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for an haages after analyses have been initialized.
Received By: (Signalur r Dale MiteryMours Additional Comments:
Relin YA
hed By: (Signature)
_1�.,11aB`
[hod o(Shipment: SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. TRANSPORTATION TO THE LABODRY. COC Group�� m
Fed Ex ❑ UPS ❑ Hand -delivered wprism Field Service ❑ Other
SC I LANDFILL
ESTER: (ATER: WASTE:
am
❑ NC ❑ SC ❑NC ❑SC❑NC ❑ SC❑NC ❑SC❑SC❑NC El SC ®NCO SC ❑ NC ❑ SCII❑ ❑ ❑ ❑ ❑
ftTYPECODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

r Full -Service Anat tica 8
sw
Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
INC;
Project Name:
449 one 70brook Road • Charlotte, 25 2809 Short Hold Analysis: Yes No UST Project: Yes NO
Phone [phone]-t'a364 Fax: [phone] y (Yes) ( ) j (Yes) ( )
�� /I �^����� ��Wt; *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Client Company Name: provisions and/or QC Requirements
Report To/Contact Name: Invoice To:
Reporting Address: Address:
Phone:10q- S ?y - %43 T Fax 8? '-`a'E 55 Purchase Order NoMilling Reference TO RE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days 113 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
re h work Must Be
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
SC OTHER
NIA
Site Location Name: e. e 00 %J7 P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 69-7 fie: I r A; 2 Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
SERVICES
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING
Sample Iced on Collection: YES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p P
NO —
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- \r / REMARKS
TIVES
LAB
ID NO.
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE �L �r
NO. SIZE 1
HOURS SLUDGE) SEE BELOW `Z
r`
AS
7�
C9
P�
Cif
i '
I�
S.A
1V :
lJ A
4./ �d'1 Sampled By Name) 1 aL LJ % tl G K Affiliation PC' SJ t3 A IS ofoeeaof
Sampler's Signature ,Z (Print
Upon relinquishing, this Chain of Custody is your authorization for Prism to p(:oceed with the analyses as requested above. Any changes must be
e
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin shed By: (Signature)
y % /� Received By: (SlgnalUre) -�� t, �afte Military/Hours Additional Comments:
Slte Arnv,l Timo.�
Reli shed By: (Signature) Received By: (Signature) Date
Site Departure Time
Fleld:l'ecI FeL
Relinquished By: (Signature) Received Forr Prism Laboratories By: Date ( '�
✓� l/�'vl/� �J �" ,,��p U� _��-;J
rTH
Mileage
Method of Shipment: NOTE: ALL SAMP CO LERS SHOULD BE TAPED SHUT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT A EPTED AND VERIFIED AGAIN S OC UNTIL RECEIVED AT THE LABORATORY.
I 1
❑ Fed Ex O UPS Cl Hand -delivered dsm Field Service ❑ Other
IPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: R%A: CERCLA LANDFILL OTHER:
❑SC ❑NC ❑SC ❑NC ❑SC I El NC ❑SC I ❑NC ❑SC I El NC El SC (INC ❑SCI ONC ❑SC
El
n ❑ ❑ ❑ -
IE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Linea trap vuA = volatue urganl(;s rnaryblb t/-cw naau �N... )

ism
ABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinkinq Water Cert No. 37735
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Qtrly, & BiWeeklyl)
Lab Submittal Date: 04/25/2016
Prism Work Order: 6040463
Case Narrative
05/09/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions. relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a-.
?rv--
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Sample might have been contaminated during pH adjustment.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Sample Receipt Summary
I S M 'v' n Full -Service Analytical
Environmental Solutions
05/09/2016
�LABOMTORIES ING
Prism Work Order: 6040463
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6040463-01 Solid 04/25/16 04/25/16
Samples were received at 24.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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I n n Full -Service Analytical &
' V' Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Laboratory Report
05/09/2016
Client Sample ID: Sta-Lime
Prism Sample ID: 6040463-01
Prism Work Order: 6040463
Time Collected: 04/25/16 11:20
Time Submitted: 04/25/16 12:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
980
mg/kg
760
86
10
*Calculation 5/3116 9:07
CLB
[CALC]
% Solids
69.7
% by
0.100
0.100
1
*SM2540 G 4/27/16 16:00
JLB
P6D0532
Weight
Nitrate/Nitrite as N
7.2
mg/kg dry
7.2
0.79
1
*SM4500-NO3 F 513/16 9:07
CLB
P6E0026
Phosphorus -Total
1300
mglkg dry
72
34
20
*SM4500-P F 4/29/16 6:29
CLB
P61)0452
Total Kjeldahl Nitrogen
4500
mg/kg dry
3600
410
10
*351.2 5/2/16 12:22
CLB
P6130528
Ammonia as N
170
mg/kg dry
7.2
2.8
1
*SM4500-NH3 G 512/16 8:49
CLB
P61)0485
Microbiological Parameters
Fecal Coliforms
34 A
MPN/g dry
0.3
1
*SM9221 E 4/25/16 13:02
EGC
P6D0476
Total Metals
Mercury
0.068
mg/kg dry
0.031
0.0017
1
*7471B
5/3/16 10:54
JAB
P6E0019
SAR Soil Preparation
Complete
g
1
*2-78-054
4/29/16 10:00
BGM
P6E0040
SAR Percent Moisture
70.9
% by
0.100
0.100
1
*2-78-054
4129/16 8:30
JAB
P6E0157
Weight
Arsenic
BRL
mg/kg dry
3.6
0.44
10
*6010D
5/6/16 12:59.
bgm
P6E0079
Sodium Absorption Ratio
0.64
[blank]
0.30
0.016
.1
*2-78-054
5/4116 1:10
BGM
P6E0039
Cadmium
BRL
mg/kg dry
3.6
0.097
10
*6010D
5/6/16 12:59
bgm
P6E0079
Calcium
1800 gH
mg/L
1.0
0.085
10
*60101)
5/4116 1:10
BGM
P6E0039
Copper
26
mg/kg dry
7.2
0.65
10
*6010D
5/6116 12:59
bgm
P6E0079
Lead
14
mg/kg dry
3.6
0.67
10
*6010D
5/6/16 12:59
bgm
P6E0079
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
5/4/16 1:10
BGM
P6E0039
Nickel
220
mg/kg dry
7.2
0.26
10
*6010D
5/6116 12:59
bgm
P6E0079
Potassium
5800
mg/kg dry
180
6.5
10
*6010D
5/6/16 12:59
bgm
P6E0079
Selenium
9.1
mg/kg dry
7.2
1.7
10
*6010D
5/6/16 12:59
bgm
P6E0079
Sodium
750
mg/kg dry
220
7.1
10
*6010D
5/6/16 12:59
bgm
P6E0079
Sodium
98
mg/L
5.0
0.074
10
*60101)
5/5/16 0:39
bgm
P6E0039
Zinc
55
mg/kg dry
36
1.3
10
*6010D
5/6116 12:59
bgm
P6E0079
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: 704/52"409
Page 3 of 9

I I n A Full -Service Analytical &
' V I I Environmental Solutions
LABORATORIES, INC.
Level 11 QC Report .
5/9/16 '
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 6040463
Attn: Andy Smith Time Submitted: 4/25/2016 12:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6EO019 - 7471 B
Blank (P6E0019-BLK1)
Prepared: 05/02/16 Analyzed: 05/03/16
Mercury
BRL
0.020
mg/kg wet
LCS (P6EO019-BSI)
Prepared: 05/02/16 Analyzed: 05/03/16
Mercury
0.430
0.020
mg/kg wet
0.4167 103 80-120
Batch P6EO039 - 3010A
Blank (P6E0039-BLK1)
Prepared: 04/29/16 Analyzed: 05/04/16
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
BH
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
Batch P6EO040 - SAR 2-78-054
Blank (P6E0040-BLK1)
Prepared &Analyzed: 04/29/16
SAR Soil Preparation
Complete
g
Batch P6E0079 - 3050B
Blank (P6E0079-BLK1)
Prepared: 05/05/16 Analyzed: 05/06/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 9

I I Full -Service Analytical &
Environmental Solutions
LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, & BiWeeklyl)
Level II QC Report
5/9/16
Prism Work Order: 6040463
Time Submitted: 4/25/2016 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6EO079 - 3050B
LCS (P6E0079-BS1)
Prepared: 05/05/16 Analyzed:
05/06/16
Arsenic
22.9
0.25
mg/kg wet
25.00
92
80-120
Cadmium
23.4
0.25
mg/kg wet
25.00
94
80-120
Copper
25.7
0.50
mg/kg wet
25.00
103
80-120
Lead
23.2
0.25
mglkg wet
25.00
93
80-120
Nickel
23.5
0.50
mg/kg wet
25.00
94
80-120
Potassium
469
12
mg/kg wet
500.0
94
80-120
Selenium
21.3
0.50
mg/kg wet
25.00
85
80-120
Sodium
476
15
mg/kg wet
500.0
95
80-120
Zinc
23.3
2.5
mg/kg wet
25.00
93
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 9

' n n Full -Service Analytical &
' V' Environmental Solutions
LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6D0452 - SM4500-PB5
Project: StaLime (Qtrly, & BiWeeklyl)
Level II QC Report-°`:-.
519/16 .. .
Prism Work Order: 6040463
Time Submitted: 4/25/2016 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P6D0452-BLK1) Prepared: 04/25/16 Analyzed: 04/29/16
Phosphorus -Total BRL 2.5 mgAg wet
LCS (P6D0452-BS1) Prepared: 04/25/16 Analyzed: 04/29/16
Phosphorus -Total 91.6 2.5 mg/kg wet 100.0 92 90-110
Batch P6130485 - NO PREP
Blank (P6DO485-BLK1) Prepared: 04/27/16 Analyzed: 05/02/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6DO485-BS1) Prepared: 04/27/16 Analyzed: 05/02/16
Ammonia as N 130 5.0 mg/kg wet 125.0 104 80-120
Matrix Spike (P6D0485-MS1) Source: 6040463-01 Prepared: 04/27/16 Analyzed: 05/02/16
Ammonia as N 319 7.2 mg/kg dry 179.4 167 85 80-120
Matrix Spike Dup (P6DO485-MSD1) Source: 6040463-01 Prepared: 04/27/16 Analyzed: 05/02/16
Ammonia as N 321 7.2 mg/kg dry 179.4 167 86 80-120 0.8 20
Batch P6D0528 - 351.2
Blank (P6D0528-BLK1) Prepared: 04/28/16 Analyzed: 05/02/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6DO528-BS1) _ Prepared: 04/28/16 Analyzed: 05/02/16
Total Kjeldahl Nitrogen 465 100 mg/kg wet 500.0 93 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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1 I n %� Full -Service Analytical &
' V 1 Environmental Solutions
LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime (Qtrly, & BiWeeklyl)
Level II QC Report
5/9/16
Prism Work Order: 6040463
Time Submitted: 4/25/2016 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6DO532 - Solids, Dry Weight
Blank (P6DO532-BLK1) Prepared & Analyzed: 04/28/16
% Solids 100 0.100 % by Weight
Duplicate (P6DO532-DUP3) Source: 6040463-01 Prepared &Analyzed: 04/28/16
% Solids 69.9 0.100 % by Weight 69.7 0.3 20
Batch P6EO026 - NO PREP
Blank (P6EO026-BLK1) Prepared & Analyzed: 05/03/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6E0026-BS1) Prepared &Analyzed: 05/03/16
Nitrate/Nitrite as N 49.4 5.0 mg/kg wet 50.00 99 80-120
Matrix Spike (P6E0026-MS1) Source: 6040463-01 Prepared &Analyzed: 05/03/16
Nitrate/Nitrite as N 74.3 7.2 mg/kg dry 71.77 7.25 93 80-120
Matrix Spike Dup (P6EO026-MSD1) Source: 6040463-01 Prepared & Analyzed: 05/03/16
Nitrate/Nitrite as N 71.7 7.2 mg/kg dry 71.77 7.25 90 80-120 4 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 7 of 9

I`- Full -Service Analytical &
JEnvironmental Solutions
-RATORIE$ INC.
City of Statesville, NC Project: Stal-ime (Qtrly, & BiWeeklyl)
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
5/9116
Prism Work Order: 6040463
Time Submitted: 4/25/2016 12:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6DO476 - NO PREP
Blank (P6DO476-BLK1) Prepared & Analyzed: 04/25/16
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Daterrime
6040463-01
P6D0528
0.05 g
25 mL
04/28/16 11:00
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
6040463-01
P6D0452
1 g
50 mL
04/25/16 11:38
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
6040463-01
P6D0532
30 g
30 g
04/27/16 16:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6040463-01
P6E0039
50 mL
50 mL
04/29/16 8:30
6040463-01
P6E0039
50 mL
50 mL
04/29/16 8:30
6040463-01
P6E0039
50 mL
50 mL
04/29/16 8:30
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
6040463-01
P6E0079
1.99 g
50 mL
05/05/16 7:45
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
6040463-01 P6E0019 0.55 g 50 mL 05/02/16 9:45
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Daterrime
6040463-01 P6E0040 . 250 g 250 g 04/28/16 8:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: '7,91L67ff-.3g33 Fax' es (No):701-379-is"d'5 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification, NELAC DOD
FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re h work dust Be SC ®f19EIP
N/A
Site Location Name: J o :d a^ Cr eel' UU W P Samples received after 14:00 will be processed next business day.
_7
Site Location Physical Address: Lip t A e^.YeTurnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO—
W
�r (SEE REVERSE FOR TERMS &CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES
•� �'."AC(.'.y_9,+i+YtlN, NC:. RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) am P P
NO
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
r
PRESERVA-
PRISM
CLIENT DATE COLLECTED (SOIL, �9 REMARKS
TIVES yi
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR "TYPE y�
NO. SIZE
ID NO.
HOURS SLUDGE) SEE BELOW
A
RA
S� 4
��
�'
C
SA
�,9 /.� Er Affiliation Pr.�s 2 u b1 i � e A k t
Sampler's Signature Cs.✓ Sampled By (Print Name) w c a .
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
o
submitted in writing to the Prism Project Manager. There will be harges for any changes after analyses have been initialized.
R inq Ailhed By: (Signalu,. Recei By: (Signature) Date _ Military/Hours Additional Comments:
�� r�
stleArrtval Ttme
77777777
R lin had By: (Sign /`' Rec v y: ( ignalurej ate
Slte Departure Time
:.
i - Ji�
Fleld loch Fee
R lirdl ed By: (Signatur Received FgrP ism LzTbr orie By: Date
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH/¢USTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO�NTIL RECEIVED AT THE LABORATORY.
❑ UPS ❑ Hand -delivered ` Pf'sm Field Service ❑ Other
Fed Ex
S: UST: GR U DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
C ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SCI ❑NC ❑SCI ❑NC ❑SCI El SC
oNC
171 ❑ ❑ ❑ 1 ❑ ❑ ❑
ES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

ism
ABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 05/03/2016
Prism Work Order: 6050014
Case Narrative
05/11 /2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V l..
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Rbbbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
D RPD value outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference .
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 9

I n A Full -Service Analytical &
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\eORATOPIM INC
Sample Receipt Summary
05/11 /2016
Prism Work Order: 6050014
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6050014-01 Solid 05/02/16 05/03/16
Samples were received at 20.2 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
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Laboratory Report
I n n I Full -Service Analytical 8
' V' Environmental Solutions 05/11/2016
City of Statesville, NC
Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 6050014-01
P.O. Box 1111
Prism Work Order: 6050014
Statesville, NC 28687
Sample Matrix: Solid Time Collected: 05/02/16 12:30
Time Submitted: 05/03/16 08:00
Parameter Result Units Report MDL Dilution Method Analysis . Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
910
mg/kg
380
44
5
'Calculation
5110116 8:06
CLB
[CALC]
% Solids
69.8
% by
0.100
0.100
1
'SM2540 G
513116 15:10
BJC
P6E0065
Weight
Nitrate/Nitrite as N
19
mg/kg dry
7.2
0.79
1
'SM4500-NO3 F
5/9116 9:23
CLB
P6E0148
Total Kjeldahl Nitrogen
4100 BH
mg/kg dry
1800
200
5
*351.2
5110116 8:06
CLB
P6E0156
Ammonia as N
270
mg/kg dry
7.2
2.8
1
'SM4500-NH3 G 5/6/16 9:58
CLB
P6E0126
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
5/3/16 10:06
EGC
P6E0062
Total Metals
Mercury
0.13
mg/kg dry
0.031
0.0017
1
'7471B
5/5/16 10:58
JAB
P6E0085
SAR Soil Preparation
Complete
g
1
'2-78-054
5/6/16 8:20
JAB
P6E0117
SAR Percent Moisture
55.5
% by
0.100
0.100
1
'2-78-054
516/16 14:31
JAB
P6E0120
Weight
Arsenic
7.2
mg/kg dry
0.36
0.043
1
•6010D
5/6116 13:07
bgm
P6E0079
Sodium Absorption Ratio
0.68
[blank]
0.30
0.016
1
`2-78-054
5/9/16 17:41
bgm
P6E0118
Cadmium
BRL
mg/kg dry
0.36
0.0095
1
'6010D
5/6/16 13:07
bgm
P6E0079
Calcium
2000
mg/L
5.0
0.42
50
'6010D
519/16 17:41
bgm
P6E0118
Copper
38
mg/kg dry
0.71
0.064
1
'6010D
5/6116 13:07
bgm
P6E0079
Lead
9.5
mg/kg dry
0.36
0.066
1
'6010D
5/6/16 13:07
bgm
P6E0079
Magnesium
BRL
mg/L
1.0
0.0070
10
'6010D
5/6/16 20:03
bgm
P6E0118
Nickel
170
mglkg dry
0.71
0.026
1
'6010D
516/16 13:07
bgm
P6E0079
Selenium
1.3
mg/kg dry
0.71
0.17
1
•6010D
5/6/16 13:07
bgm
P6E0079
Sodium _
110 BH
mg/L
5.0 "`
0.074
10
'6010D
5/6116 20:03
bgm
P6E0118
Zinc
52
mg/kg dry
3.6
0.13
1
`6010D
5/6/16 13:07
bgm
P6E0079
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Of .9

I I n n Fuli-Service Analytical &
' V' Environmental Solutions
-ORATORIES, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals : Quality Control
Analyte
Project: StaLime
Levd 1VQC Repot
5/11116' ...._
Prism Work Order: 6050014
Time Submitted: 5/3/2016 8:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - 3050B
Blank (P6EO079-BLK1)
Prepared: 05/05/16 Analyzed: 05/06/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6EO079-BS1)
Prepared: 05/05/16 Analyzed: 05/06/16
Arsenic
22.9
0.25
mg/kg wet
25.00 92 80-120
Cadmium
23.4
0.25
mg/kg wet
25.00 94 80-120
Copper
25.7
0.50
mg/kg wet
25.00 103 80-120
Lead
23.2
0.25
mg/kg wet
25.00 93 80-120
Nickel
23.5
0.50
mg/kg wet
25.00 94 80-120
Selenium
21.3
0.50
mg/kg wet
25.00 85 80-120
Zinc
23.3
2.5
mg/kg wet
25.00 93 80-120
Batch P6EO085 - 7
Blank (KE0085-BLK1) Prepared & Analyzed: 05/05/16
Mercury BRL 0.020 mg/kg wet
LCS (P6E0085-BS1) Prepared & Analyzed: 05/05/16 _
Mercury 0.499 0.020 mg/kg wet 0.4167 120 80-120
Batch P6EO117 - SAR 2-78-054
Blank (P6E0117-BLK1) _ Prepared: 05/05/16 Analyzed: 05/06/16
SAR Soil Preparation Complete g
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 9

Level II QC Report
I n %� Full -Service Analytical & 5/11116
v Environmental Solutions
1eORATORIES ING
City of Statesville, NC Project: StaLime Prism Work Order: 6050014
Attn: Andy Smith Time Submitted: 5/3/2016 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P6EO118 - 301OA
Blank (P6E0118-BLK1)
Prepared &Analyzed: 05/06/16
Sodium Absorption Ratio
BRL
3.0 [blank]
Calcium
BRL
1.0 mg/L
BH
Magnesium
BRL
1.0 mg/L
Sodium
BRL
5.0 mg/L
BH
Batch P6E0120 - NO PREP
Blank (P6E0120-BLK1)
Prepared & Analyzed: 05/06/16
SAR Percent Moisture
BRL
0.100 % by Weight
Duplicate (P6EO120-DUP1)
Source: 6050014-01
Prepared & Analyzed: 05/06/16
SAR Percent Moisture
54.7
0.100 % by Weight 55.5 1 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 Of 9

Full -Service Analytical &
EIBM I nvironmental Solutions
-ORATORIES. INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
5/11 /16
Prism Work Order: 6050014
Time Submitted: 5/3/2016 8:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P6EO065 - Solids Dry Weight
Blank (P6EO065-BLK1) Prepared & Analyzed: 05/03/16
% Solids 100 0.100 % by Weight
Duplicate (P6E0065-DUP1) Source: 6050014-01 Prepared & Analyzed: 05/03/16 _
% Solids 69.2 0.100 % by Weight 69.8 0.9 20
Batch P6EO126 - NO PREP
Blank (KE0126-BLK1) Prepared &Analyzed: 05/06/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6E0126-BS1) Prepared & Analyzed: 05/06/16
Ammonia as N 129 5.0 mg/kg wet 125.0 103 80-120
Matrix Spike (P6E0126-MS1) Source: 6050014-01 Prepared & Analyzed: 05/06/16
Ammonia as N 276 7.2 mg/kg dry 179.0 266 6 80-120 MI
Matrix Spike Dup (P6E0126-MSD1) Source: 6050014-01 Prepared & Analyzed: 05/06/16
Ammonia as N 269 7.2 mg/kg dry 179.0 266 2 80-120 3 20 MI
Batch P6EO148 - NO PREP
Blank (P6E0148-BLK1) Prepared & Analyzed: 05/09/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6E0148-BS1) Prepared &Analyzed: 05/09/16
Nitrate/Nitrite as N 48.6 5.0 mg/kg wet 50.00 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6 of 9

f n I Full -Service Analytical &
'v' Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Level If QC Report
5/11 /16
Prism Work Order: 6050014
Time Submitted: 5/3/2016 8`.00:OOAM
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit
Batch P6EO148 - NO PREP
Matrix Spike (P6E0148-MS1) Source: 6050014-01 Prepared & Analyzed: 05/09/16
Nitrate/Nitrite as N 88.0 7.2 mg/kg dry 71.58 19.0 96 80-120
Matrix Spike Dup (P6EO148-MSD1) Source: 6050014-01 Prepared & Analyzed: 05/09/16
Nitrate/Nitrite as N 87.9 7.2 mg/kg dry 71.58 19.0 96 80-120 0.08 20
Batch P6EO156 - 351.2
Notes
Blank (NE0156-BLK1) Prepared: 05/09/16 Analyzed: 05/10/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet BH
LCS (P6EO156-BSI) Prepared: 05/09/16 Analyzed: 05/10/16
Total Kjeldahl Nitrogen 514 100 mg/kg wet 500.0 103 90-110
Matrix Spike (P6E0156-MS1
Total Kjeldahl Nitrogen
Source:6050014-01 Prepared: 05/09/16 Analyzed: 05/10/16
9570 1800 mg/kg dry 7158 4120 76 90-110
MI
Matrix Spike Dup (P6EO156-MSD1) Source: 6050014-01 Prepared: 05/09/16 Analyzed: 05/10/16
Total Kjeldahl Nitrogen 12100 1800 mg/kg dry 7158 4120 111 90-110 23 20 D, MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 9

Level II QC Report
S n � I
' V'
�
Full -Service Analytical
Environmental Solutions
5/11 /16
f ,
LABOWORIM INa
City of Statesville, NC
Project: StaLime
Prism Work Order: 6050014
Attn: Andy Smith
Time Submitted: 5/3/2016 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P6E0062 - NO PREP
Blank (P6E0062-BLK1)
Prepared & Analyzed: 05/03/16
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample
Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Daterrime
6050014-01
PBE0156
0.05 g
25 mL
05/09/16 10:30
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
6050014-01
PBE0065
30 g
30 g
05/03/16 15:10
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6050014-01
P6E0118
50 mL
50 mL
05/06/16 8:20
6050014-01
P6E0118
50 mL
50 mL
05/06/16 8:20
6050014-01
P6E0118
50 mL
50 mL
05/06/16 8:20
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
6050014-01
P6E0079
2.01 g-
50 mL
05/05/16 7:45
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime
6050014-01
P6E0085
0.56 g
50 mL
05/05/16 8:05
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
6050014-01
P6E0117
250 g
250 g
05/05/16 7:20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-800/529-6364- Fax :[phone] Page 8 Of 9

C AIN OF CUSTODY RECORD
� � R,� � Full -Service, Analytical ".
Environmental Solution PAGE_ OF _ QUOTE 0 TO ENSURE PROPER BILLING:
nit
LABORATORIES, INC.
Project Name:
449 Springbrook Road - Charlotte, NC 282,17 (l Yes No UST Project:
` (Yes) ( NO)
Phone [phone] . Fax: [phone] y (Yes) ( )
Short Hold Analysis:
, *Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
Client Company Name: a ; O S "y �� - provisions and/or QC Requirements -
Report To/Contact Name: A r'a R y Son fh Invoice To:
Reporting Address: Address:
Phone:704' 619- 3`JI' Fax es (No): <��t - - ' purchase Order No.lBilling R_eferenco TO BE FELLED. IN;BY CLIEPIT/SAMPLItvCa. PERSONNEL _
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC .
re h Work dust Be
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
trC SC OTHER NIA
Site Location Name: o ti, 44 � 3a ' d P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: ` 4 d0 � e rr Turnaround time is based on business days, excluding weekends and holidays. Wafer Chlorinated: YES_ NO .
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES ANALYSIS REQUESTED Sample, Iced Upon Collection: YES_ NO_
y0iY �daf RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p . p .
TIME MATRIX SAMPLE CONTAINER PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA• �� REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES q, ID NO.
HOURS SLUDGE) SEE BELOW
�/a -_ �.t� �
�., m�' d �,
�� • ��`
�
�af1 •S a� +�
�{
�'g ��gg
Q' A
J
ie,0 df
ICU
v�O
A .
�6
N
Sampler's Signature
I Sampled By (Print Name) AK6"r
AfFiliation
-
Site Arrival Tlmo;
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the al6yses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Reli ed alu ReC d By: (Signs r� Date Military Hours Additional Comments:
Y (Sig l(
Slte DepaCture Tlme
Relinq hed By: (Si lure /� /
=- 'Y U [ ���
Relinquished By: (Signature)
f� d By: (Signatu
Re Ived For Prism Laboratories By:
Date
Date
/•, (,
I-teld Tech Fee
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
V�1011�Uv
m Fiold Rwrvira ❑Other
COC Group No.
iv
IDES: UST: G UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑SCI ❑NC ❑SC I ❑❑NC ❑SC ICNC ❑SC I ®NC ❑SC I ONC❑C SI El NC ❑SC El❑O❑C
NC SC NC S
YPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) i.,

A
INa
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402 Case Narrative
SC Certification No. 99012
Full -Service Analytical & NC Drinkinq Water Cert No. 37735
05/17/2016
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 05/09/2016
Prism Work Order: 6050164
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods..
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting lilimit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 16

Full -Service Analytical &
Environmental Solutions
Sample Receipt Summary
05/17/2016
Prism Work Order: 6050164
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Stal-ime
6050164-01
Solid
05/09/16
05/09/16
Fecal #1
6050164-02
Solid
05/09/16
05/09/16
Fecal #2
6050164-03
Solid
05/09/16
05/09/16
Fecal #3
6050164-04
Solid
05/09/16
05/09/16
Fecal #4
6050164-05
Solid
05/09/16
05/09/16
Fecal #5
6050164-06
Solid
05/09/16
05/09/16
Fecal #6
6050164-07
Solid
05/09/16
05/09/16
Fecal #7
6050164-08
Solid
05/09/16
05/09/16
Samples were received in good condition at 5.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 Of 16 71

I „ e, Full -Service Analytical &
v' Environmental Solutions
ABO-RIES ING
esville, NC
i m ith
P.O. Box 1111
Statesville. NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/17/2016
Client Sample ID: StaLime
Prism Sample ID: 6050164-01
Prism Work Order: 6050164
Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Plant Available Nitrogen
920
mg/kg
160
18
2
*Calculation
5/17/16 9:29
CLB
[CALC]
% Solids
77.6
% by
0.100
0.100
1
*SM2540 G
5112/16 10:41
BJC
P6E0252
Weight
Nitrate/Nitrite as N
12
mg/kg dry
6.4
0.71
1
*SM4500-NO3 F
5/16/16 9:34
CLB
P6E0283
Phosphorus -Total
1500
mg/kg dry
64
31
20
*SM4500-P F
SM1116 9:28
CLB
P6E0184
Total Kjeldahl Nitrogen
3800
mg/kg dry
640
73
2
*351.2
5/17/16 9:29
CLB
P6E0273
Ammonia as N
85
mglkg dry
6.4
2.5
1
*SM4500-NH3 G
5/12116 9:51
CLB
P6E0238
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
5110/16 10:22
EGC
P6E0224
Total Metals
Mercury
0.10
mg/kg dry
0.027
0.0015
1
*7471B
5110/16 12:41
JAB
P6E0189
SAR Soil Preparation
Complete
9
1
*2-78-054
5/12/16 8:40
JAB
P6E0221
SAR Percent Moisture
60.8
% by
0.100
0.100
1
*2-78-054
5112116 9:00
JAB
P6E0298
Weight
Arsenic
4.2
mg/kg dry
3.2
0.39
10
*6010D
5/13/16 21:49
BGM
P6E0192
Sodium Absorption Ratio
0.68
[blank]
0.30
0.016
1
*2-78-054
5113/16 22:13
BGM
P6E0251
Cadmium
BRL
mg/kg dry
3.2
0.086
10
*6010D
5113/16 21:49
BGM
P6E0192
Calcium
2000 BH, B
mg/L
5.0
0.42
50
*6010D
5/13/16 22:13
BGM
P6E0251
Copper
23
mg/kg dry
6.4
0.58
10
*601013
5/13/16 21:49
BGM
P6E0192
Lead
11
mg/kg dry
3.2
0.60
10
*6010D
5113/16 21:49
BGM
P6E0192
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
5112/16 21:46
bgm
P6E0251
Nickel
220
mg/kg dry
6.4
0.23
10
*6010D
5/13/16 21:49
BGM
P6E0192
Potassium
6300
mg/kg dry
160
5.8
10
*6010D
5113116 21:49
BGM
P6E0192
Selenium
9.6
mg/kg dry
6.4
1.5
10
*6010D
5/13/16 21:49
BGM
P6E0192
Sodium
110
mg/L
5.0
0.074
10
*6010D
5/12116 21:46
bgm
P6E0251
Sodium
810
mg/kg dry
190
6.3
10
*6010D
5/13/16 21:49
BGM
P6E0192
Zinc
47
mg/kg dry
32
1.2
10
*6010D
5/13/16 21:49
BGM
P6E0192
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 16

I`- n n Full -Service Analytical &
J' V I Environmental Solutions
%60P TOFIEa INC
Laboratory Report
05/17/2016
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Fecal #1
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 6050164-02
P.O. Box 1111
Prism Work Order: 6050164
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter '
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateMme ID
General Chemistry Parameters
% Solids
82.1 % by
0.100 0.100
1 *SM2540 G 5/12116 10:41 BJC P6E0252
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 *SM9221 E 5/10/16 10:22 EGC P6E0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 16

I n q FulliService Analytical &
' V' Envronmental Solutions
480RATORIE$ INC.
Laboratory Report
05/17/2016
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #2
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6050164-03
P.O. Box 1111 Prism Work Order: 6050164
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
% Solids 75.4 % by 0.100 0.100 1 'SM2540 G 5/12/16 10:41 BJC P6E0252
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/10/16 10:22 EGC P6E0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364.- Fax: [phone] Page 5 of 16

Laboratory Report'
I Fun -Service
Analytical
..
¢4,;t�� Environmental Solutionss
f m`ORATORIES INC.
05/17/2016
City of Statesville, NC i
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #3
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 6050164-04
P.O. Box 1111
Prism Work Order: 6050164
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateTme
ID
General Chemistry Parameters
% Solids
72.8 % by
0.100 0.100
1 'SM2540 G 5/12/16 10:41 BJC
P6E0252
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 5/10/16 10:22 EGC
P6E0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 16

PRISMLaboratory Report
Full -Service Analytical 8
Environmental Solutions 05/17/2016
LABORATORIE$ING
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #4
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6050164-05
P.O. Box 1111 Prism Work Order: 6050164
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 74.7 % by 0.100 0.100 1 'SM2540 G 5112/16 10:41 BJC P6E0252
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/10/16 10:22 EGC P6E0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 16

Laboratory Report
t I � � Full -Service Analytical s 05/� 7/2016
F.' r Environmental Solutions
-X _0RATORIEs ING, .
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #5
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6050164-06
P.O. Box 1111 Prism Work Order: 6050164
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 69.3 % by 0.100 0.100 1 "SM2540 G 5/12/16 10:41 BJC P6E0252
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/10/16 10:22 EGC P6E0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 16

Laboratory Report
i Full -Service Analytical
I l f S 1 V 1 Environmental Solutions
LABORATORIES ING
05/17/2016
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #6
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 6050164-07
P.O. Box 1111
Prism Work Order: 6050164
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
85.1 % by
0.100 0.100
1 'SM2540 G 5/12/16 10:41 BJC
P6E0252
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 'SM9221 E 5/10116 10:22 EGC
P6E0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 16

Full -Service Analytical 8
Environmental Solutions
Laboratory Report
05/17/2016
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #7
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 6050164-08
P.O. Box 1111
Prism Work Order: 6050164
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/09/16 12:30
Time Submitted: 05/09/16 13:50
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids
74.7 % by
0.100 0.100
1 `SM2540 G 5/12/16 10:41 BJC P6E0252
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 5/10/16 1022 EGC PBE0224
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 10 of 16

Level II QC Report
I I I� A Full -Service Analytical & 5/17/16
'v' Environmental Solutions
LA90RATORIE4ING '
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 6ODay Prism Work Order: 6050164
Attn: Andy Smith 7 Fecal) Time Submitted: 5/9/2016 1:50:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6E0189 - 7471 B
Blank (KE0189-BLK1)
Prepared &Analyzed: 05/10/16
Mercury
BRL
0.020
mg/kg wet
L_CS (P6E0189-BSI)
Prepared &Analyzed: 05/10/16
Mercury
0.430
0.020
mg/kg wet
0.4167 103
80.120
Batch P6EO192 - 3050B
Blank (P6E0192-BLK1)
Prepared &Analyzed: 05/10/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (HE0192-113SI)
Prepared &Analyzed: 05/10/16
Arsenic
25.1
0.25
mg/kg wet
25.00 100
80-120
Cadmium
24.6
0.25
mg/kg wet
25.00 98
80-120
Copper
26.8
0.50
mg/kg wet
25.00 107
80-120
Lead
24.6
0.25
mg/kg wet
25.00 98
80-120
Nickel
25.0
0.50
mg/kg wet
25.00 100
80-120
Potassium
531
12
mg/kg wet
500.0 106
80-120
Selenium
24.5
0.50
mg/kg wet
25.00 98
80-120
Sodium
519
15
mg/kg wet
500.0 104
80-120
Zinc
24.5
2.5
mg/kg wet
25.00 98
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 Of 16

I I Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P6EO221 - SAR 2-78-054
Level .11 QC' Report°-
" 5/17/16'
Project: StaLime (Qtrly, BiWeekly, 6ODay Prism Work Order: 6050164
7 Fecal) Time Submitted: 5/9/2016 1:50:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P6EO221-BLK1)
Prepared: 05/11/16 Analyzed: 05/12/16
SAR Soil Preparation
Complete
9
Batch P6EO251 - 301 OA
Blank (P6EO251-BLK1)
Prepared & Analyzed: 05/12/16
Sodium Absorption Ratio
BRL
3.0 [blank]
Calcium
2.03
1.0 mg/L BH
Magnesium
BRL
1.0 mg/L
Sodium
BRL
5.0 mg/L
Batch P6EO298 - NO PREP
Blank (P6EO298-BLK1)
Prepared & Analyzed: 05/12/16
SAR Percent Moisture
BRL
0.100 % by Weight
Duplicate (P6E0298-DUP1)
Source: 6050164-01 Prepared & Analyzed: 05/12/16
SAR Percent Moisture
59.8
0.100 % by Weight 60.8 2 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-8001529-6364 -Fax: [phone] Page 12 Of 16

I %I Fun -Service Analytical &
I V Environmental Solutions
ABOR-ONIM ING
Isville, NC
Smith
- -- 11
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Level II QC Report
5/17/16
Prism Work order: 6050164
Time Submitted: 5/9/2016 1:50:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Batch P6EO184 - SM4500-PB5
Blank (P6E0184-BLK1) Prepared: 05/10/16 Analyzed: 05/11/16
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P6E0184-BS1)
Phosphorus -Total
Prepared: 05/10/16 Analyzed: 05/11/16
107 2.5 mg/kg wet 100.0 107 90-110
Matrix Spike (P6E0184-MS1) Source: 6050164-01 Prepared: 05/10/16 Analyzed: 05/11/16
Phosphorus -Total 716 64 mg/kg dry 128.9 1550 NR 80-120 MC
Matrix Spike Dup (P6E0184-MSD1) Source: 6050164-01 Prepared: 05/10/16 Analyzed: 05/11/16
Phosphorus -Total 736 64 mg/kg dry 128.9 1550 NR 80-120 3 20 MC
Batch P6EO238 - NO PREP
Blank (P6E0238-BLK1) Prepared & Analyzed: 05/12/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6E0238-BS1) Prepared &Analyzed: 05/12/16
Ammonia as N 125 5.0 mg/kg wet 125.0 100 80-120
Matrix Spike (P6E0238-MS1) Source: 6050164-01 Prepared & Analyzed: 05/12/16
Ammonia as N 250 6.4 mg/kg dry 161.2 84.8 103 80-120
Matrix Spike Dup (P6E0238-MSD1) Source: 6050164-01 Prepared & Analyzed: 05/12/16
Ammonia as N 251 6.4 mg/kg dry 161.2 84.8 103 80-120 0.1 20
Batch P6EO252 - Solids, Dry Weight
Blank (P6E0252-BLK1) Prepared &Analyzed: 05/12/16
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 Of 16

Level II QC Report -
D I n Full -Service Analytical & 5I1"7J16`
` ' V' Environmental Solutions
LneOeATmm — -
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6EO252 - Solids. Dry Weiaht
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 6050164
Time Submitted: 5/9/2016 1:50:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Duplicate (P6E0252-DUP2) Source: 6050164-01 Prepared & Analyzed: 05/12/16
% Solids 78.7 0.100 % by Weight 77.6 1 20
Duplicate (P6E0252-DUP3) Source: 6050164-07 Prepared & Analyzed: 05/12/16
% Solids 86.9 0.100 % by Weight 85.1 2 20
Batch P6EO273 -
Blank (P6E0273-BLK1) Prepared: 05/13/16 Analyzed: 05/17/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6EO273-BS1) Prepared: 05/13/16 Analyzed: 05/17/16
Total Kjeldahl Nitrogen 478 100 mg/kg wet 500.0 96 90-110
Batch P6EO283 - NO PREP
Blank (1126E0283-BLK1) Prepared: 05/13/16 Analyzed: 05/16/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6EO283-BS1) Prepared: 05/13/16 Analyzed: 05/16/16
Nitrate/Nitrite as N 51.6 5.0 mg/kg wet 50.00 103 80-120
Matrix Spike (P6E0283-MS1) Source: 6050164-01 Prepared: 05/13/16 Analyzed: 05/16/16
Nitrate/Nitrite as N 74.1 6.4 mg/kg dry 64.47 12.3 96 80-120
Matrix Spike Dup (P6EO283-MSD1) Source: 6050164-01 Prepared: 05/13/16 Analyzed: 05/16/16
Nitrate/Nitrite as N 70.4 6.4 mg/kg dry 64.47 12.3 90 80-120 5 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 16

F.'.."�--.'RRISM
Full-Service Analytical &
Environmental Solutions
yi-�'LA60flATOFIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
5/17/16
Prism Work Order: 6050164
Time Submitted: 5/9/2016 1:50:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6EO224 - NO PREP
Blank (P6EO224-BLK1) Prepared &Analyzed: 05/10/16
Fecal Coliforms BRL 0.2 MPN/g wet
Prep Method: 351.2
Lab Number
Batch
6050164-01
P6E0273
Prep Method. SM4500-PB5
Lab Number
Batch
6050164-01
P6E0184
Prep Method: Solids, Dry Weight
Lab Number
Batch
6050164-01
P6E0252
6050164-02
P6E0252
6050164-03
P6E0252
6050164-04
P6E0252
6050164-05
P6E0252
6050164-06
P6E0252
6050164-07
P6E0252
6050164-08
P6E0252
Prep Method: 3010A
Lab Number
Batch
Sample Extraction Data
Initial
Final
Daterrime
0.05 g
25 mL
05/13/16 11:30
Initial
Final
Date/rime
1 g
50 mL
05/10/16 8:59
Initial Final Daterrime
30
g 30 g
05/11/16 15:15
30
g 30 g
05/11/16 15:15
30
g 30 g
05/11/16 15:15
30
g 30 g
05/11/16 15:15
30
g 30 g
05/11/16 15:15
30
g 30 g
05/11/16 15:15
30
g 30 g
05/11/16 15:15
.30
g 30. g
05/11/16 15:15
Initial Final Daterrime
6050164-01
P6E0251
50 mL
50 mL
05/12/16 9:00
6050164-01
P6E0251
50 mL
50 mL
05/12/16 9:00
6050164-01
P6E0251
50 mL
50 mL
05/12/16 9:00
Prep Method:3050B
Lab Number
Batch
Initial
Final
Daterrime
6050164-01
P6E0192
2 g
50 mL
05/10/16 9:30
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
6050164-01
P6E0189
0.57 g
50 mL
05/10/16 9:57
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/rime
6050164-01
P6E0221
250 g
250 g
05/11/16 8:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 Of 16

..................................._.......................................
CHAIN OF CUSTODY RECORD
....... ...........,.,. �.. �. �,.....,...�..�,..
..�
y
R IFull-Service Analytical
`� Environmental Solutions
OF ®DOTE # TO ENSURE PROPER BILLING:
YES .. NO
,.�
IVIA.-
.
PAGE_ _
Samples INTACT upon arnvah
O
„' T,.; , 'fa', i. oonnronIes, I
Project Name:
Received OI1,I WET ICE'7
t0
I49 Springbrook Road •Charlotte, NC 28217
Phone [phone] Fax: [phone]
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER I?RESERVATI�-77
ES Illdicaled�
Received WITHIN HOLDING TIMES
i
a�
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
-
a
Client Company Name: i di'� c:) l' �1 Ilvi `>e, k-f '
provisions and/or OC Requirements
CUSTODY SEALS iNTAC T�
Report To/Contact Nam
Invoice TO:
UOLAfILES recd W(OUT 1-IEADSPACE?
PROPER CONTAINE RS used
Reporting Address:
Address:
TEMP l he�rrl ID j �l I Observed:
Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF_Excel_Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Pre-ApprovWork Must Be
SC OTHER N/A
Site Location Name:
Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
Site Location Physical Address:
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_ NO
am p p
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED
(SOIL, PRESERVA-
cy REMARKS
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY
WATER OR *TYPE TIVES
NO. SIZE
ID NO.
HOURS
���
SLUDGE) SEE BELOW
5-q-14
M-3®
�.�� ®�
a
As
PAN
a
0 DAY 7
Cw
A
oy
Z14
j o
Sampler's Signature Zr6L t
l
Sampled By (Print Name) ?a ' r / C Affiliation 1 e S r K
1 • IN 1%WV
e"A-k
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
Relin 'hed By: (Signature)
Received By: (Signature) Date //•
Military/Hours Additional Comments: 5ite Arnval Time
'
Rel' hed By: (Signature)
Recei ed By: (Signature) Date
Site Departure Time:
:Field Tech Fee
Relinquished By: (Si nature)
By: Date
Received For Pri ab277�
&9 1
�`
! 3 S C'
./
Mileage
Method of Shipment: NOTE: ALL SAMPLE COO RS SHOULD BE TAPED SHUT WITH C ODY SEAL FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT AC PTED AND VERIFIED AGAINSTCOCU IL RECEIVED AT THE LAB ORATORY.
v J
❑ Fed Ex El UPS ❑ Hand -delivered rism Field Service ❑ Other v
REVERSE
DES: UST: GR NDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: TERMS'_
•*
❑ SC ❑ NC ❑ SC I NC ❑ SC I
NC ❑ SC NC ❑ SC O NC ❑ SC O NC ❑ SC O NC ❑ SCI O NC ❑ SC
n O a
El
CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

ism
.ABORATORIE$ INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 05/16/2016
Prism Work Order: 6050334
Case Narrative
05/25/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V L.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories,. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364- Fax: [phone] Page Of9

I Full -Service Analytical &
Environmental Solutions
ABOMTOflIE$ ING.
Sample Receipt Summary
05/25/2016
Prism Work Order: 6050334
lie ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6050334-01 Solid 05/16/16 05/16/16
Samples were received at 25.4 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 9

f Full -Service Analytical &
Environmental Solutions
ABOFATOPIE& -
:sville, NC
,yttn. Mlluy Omith
P.O. Box 1111
Statesville. NC 28687
Laboratory Report
05/25/2016
Project: Stal-ime Client Sample ID: Sta-Lime
Prism Sample ID: 6050334-01
Prism Work Order: 6050334
Sample Matrix: Solid Time Collected: 05/16/16 10:11
Time Submitted: 05/16/16 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1000
mg/kg
160
18
2
*Calculation
5123/16 9:20
CLB
[CALC]
% Solids
66.8
% by
0.100
0.100
1
*SM2540 G
5/19116 10:07
JLB
P6E0413
Weight
Nitrate/Nitrite as N
22
mg/kg dry
7.5
0.82
1
*SM4500-NO3 F 5/23/16 9:20
CLB
P6E0443
Total Kjeldahl Nitrogen
4700
mg/kg dry
750
85
2
*351.2
5/20116 7:46
CLB
P6E0391
Ammonia as N
550 a
mg/kg dry
7.5
2.9
1
*SM4500-NH3 G 5/18/16 8:07
CLB
P6E0352
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
5/17/16 10:10
BMS
P6E0368
Total Metals
Mercury
0.070
mg/kg dry
0.028
0.0015
1
*7471B
5123116 11:44
JAB
P6E0451
SAR Soil Preparation
Complete
g
1
*2-78-054
5119/16 8:00
JAB
P6E0365
SAR Percent Moisture
56.0
% by
0.100
0.100
1
*2-78-054
5/19/16 8:30
JAB
P6E0398
Weight
Arsenic
4.6
mg/kg dry
3.7
0.45
10
*6010D
5123/16 19:50
bgm
P6E0356
Sodium Absorption Ratio
0.46
[blank]
0.30
0.016
1
*2-78-054
5123/16 20:27
bgm
P6E0397
Cadmium
BRL
mg/kg dry
3.7
0.099
10
*6010D
5/23116 19:50
bgm
P6E0356
Calcium
2500 BH
mg/L
1.0
0.085
10
*60101)
5123/16 20:27
bgm
P6E0397
Copper
31
mg/kg dry
7.4
0.67
10
*6010D
5123/16 19:50
bgm
P6E0356
Lead
11
mg/kg dry
3.7
0.69
10
*6010D
5/23116 19:50
bgm
P6E0356
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
5/23/16 20:27
bgm
P6E0397
Nickel
200
mg/kg dry
7.4
0.27
10
*601011)
5123116 19:50
bgm
P6E0356
Selenium
12
mg/kg dry
7.4
1.8
10
*6010D
5/23/16 19:50
bgm
P6E0356
Sodium
84
mg/L
5.0
0.074
10
*60101)
5/23/16 20:27
bgm
P6E0397
Zinc
63
mg/kg dry
37
1.3
10
*60101)
5/23/16 19:50
bgm
P6E0356
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. _
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone]. Page 3 Of 9

ism.BORATORIES INc.
sville, NC
mith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
Total Metals - Quality Control
Analyte
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
5/25/16
Prism Work Order: 6050334
Time Submitted: 5/16/2016 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P6EO356 - 3050B
Blank (P6E0356-BLK1)
Prepared: 05/18/16 Analyzed: 05/19/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6E0356-BS1)
Prepared: 05/18/16 Analyzed: 05/19/16
Arsenic
24.5
0.25
mg/kg wet
25.00 98 80-120
Cadmium
24.7
0.25
mg/kg wet
25.00 99 80-120
Copper
26.1
0.50
mg/kg wet
25.00 105 80-120
Lead
24.3
0.25
mg/kg wet
25.00 97 80-120
Nickel
24.5
0.50
mg/kg wet
25.00 98 80-120
Selenium
24.5
0.50
mg/kg wet
25.00 98 80-120
Zinc
24.7
2.5
mg/kg wet
25.00 99 80-120
Batch P6EO365 - SAR 2-78-054
Blank (P6EO365-BLK1) Prepared: 05/18/16 Analyzed: 05/19/16
SAR Soil Preparation Complete g
Batch P6E0397 - 3010A
Blank (P6E0397-BLK1) Prepared: 05/19/16 Analyzed: 05/23/16
Sodium Absorption Ratio BRL 3.0 [blank]
Calcium BRL 1.0 mg/L BH
Magnesium BRL 1.0 mg/L
Sodium BRL 5.0 mg/L
This report should not be. reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 9

t I %� Full -Service Analytical &
' V Environmental Solutions
LABORATORIES I -
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Level II QC Report
5/25/16
Prism Work Order: 6050334
Time Submitted: 5/16/2016 4:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6EO398 - NO PREP
Blank (P6EO398-BLK1) Prepared &Analyzed: 05/19/16
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (P6EO398-DUP1) Source: 6050334-01 Prepared & Analyzed: 05/19/16
SAR Percent Moisture 59.5 0.100 % by Weight 56.0 6 200
Batch P6EO451 - 7471 B
Blank (P6EO451-BLK1) Prepared & Analyzed: 05/23/16
Mercury BRL 0.020 mg/kg wet
LCS (P6E0451-BS1) Prepared &Analyzed: 05/23/16
Mercury 0.432 0.020 mg/kg wet 0.4167 104 80-120
This report should not be reproduced, except in its entirety, without the -written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 Of 9

Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Level II QC,Report
. 5/25/16
Prism Work Order: 6050334
Time Submitted: 5/16/2016 4:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6EO352 - NO PREP
Blank (P6EO352-BLK1)
Prepared & Analyzed: 05/18/16
Ammonia as N
5.55 5.0. mg/kg wet
BH
LCS (P6E0352-BS1)
Prepared & Analyzed: 05/18/16
Ammonia as N
125 5.0 mg/kg wet
125.0 100 80-120
B
Matrix Spike (P6EO352-MS1)
Source: 6050334-01
Prepared &Analyzed: 05/18/16
Ammonia as N
785 15 mg/kg dry
187.2 550 125 80-120
MI, B.
Matrix Spike Dup (P6EO352-MSD1)
Source: 6050334-01
Prepared & Analyzed: 05/18/16
Ammonia as N
755 15 mg/kg dry
187.2 550 109 80-120 4
20 B
Batch P6EO391 - 351.2
Blank (P6E0391-BLK1)
Prepared: 05/19/16 Analyzed: 05/20/16
Total Kjeldahl Nitrogen
BRL 25 mg/kg wet
LCS (P6EO391-BS1)
Prepared: 05/19/16 Analyzed: 05/20/16
Total Kjeldahl Nitrogen
486 100 mg/kg wet
500.0 97 90-110
Matrix Spike (PSE0391-MS1)
Source: 6050334-01
Prepared: 05/19/16 Analyzed: 05/20/16
Total Kjeldahl Nitrogen
10900 1900 mg/kg dry
7488 4720 83 90-110 MI
Matrix Spike Dup (P6E0391-MSD1)
Source: 6050334-01
Prepared: 05/19/16 Analyzed: 05/20/16
Total Kjeldahl Nitrogen
11400 1900 mg/kg dry
7488 4720 89 90-110 4 20 MI
Batch P6EO413 - Solids Dry Weight
Blank (P6EO413-BLK1) Prepared: 05/18/16 Analyzed: 05/19/16
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6 of 9

Level II QC Report
t I S n %� Full -Service Analytical & 5/25/16
'v' Environmental solutions
L0.BC-RIEs INC.
City of Statesville, NC Project: StaLime . Prism Work Order: 6050334
Attn: Andy Smith Time Submitted: 5/16/2016 4:00:00PM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6E0443 - NO PREP
Blank (P6E0443-BLK1) Prepared & Analyzed: 05/23/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6E0443-BS1) Prepared &Analyzed: 05/23/16
Nitrate/Nitrite as N 48.8 5.0 mg/kg wet 50.00 98 80-120
Matrix Spike (P6E0443-MS1) Source: 6050334-01 Prepared & Analyzed: 05/23/16
Nitrate/Nitrite as N 80.9 7.5 mg/kg dry 74.88 22.2 78 80-120 MI
Matrix Spike Dup (P6E0443-MSD1) Source: 6050334-01 Prepared & Analyzed: 05/23/16
Nitrate/Nitrite as N 78.5 7.5 mg/kg dry 74.88 22.2 75 80-120 3 20 MI
This report should, not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 9

I Full -Service Analytical &
Environmental Solutions
.ORATORIES -
3ville, NC
mith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II,QC Report"
5/25/16...:..:
Prism Work Order: 6050334
Time Submitted: 5/16/2016 4:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6E0368 - NO PREP
Blank (P6EO368-BLK1)
Prepared &Analyzed: 05/17/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
6050334-01
P6E0391
0.05 g
25 mL
05/19/16 9:00
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
6050334-01
P6E0413
30 g
30 g
05/18/16 16:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
DateTme
6050334-01
P6E0397
50 mL
50 mL
05/19/16 9:09
6050334-01
P6E0397
50 mL
50 mL
05/19/16 9:09
Prep Method: 3050E
Lab Number
Batch
Initial
Final
DateMme
6050334-01 P6E0356 2.02 g 50 mL 05/18/16 8:20
Prep Method: 7471 B
Lab Number Batch Initial Final Daterrime
6050334-01 P6E0451 0.65 g 50 mL 05/23/16 9:25
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Date/Time
6050334-01 P6E0365 250 g 250 g 05/18/16 8:00
This report should not be.reproduced,.except in itsentirety,.withoutthe written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 9

•;1r_
Full -Service Analytical £e
gs
Environmental Solutions
iv f
'''LAP.ORATORIES,INC.
�.:iY�N.
449 Springbrook Road " Charlotte, NC 28217
Phone [phone]
• Far.: 704/525-0409
Client Company Name:
Report To/Contact Name:
A,,.,Y lr 5. ,4h
Reporting Address:
14& Pik OF CUSTODY RECORD
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111 III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone: 7°)4- 97-f- 313Y Fax' es (No):70- 97S'- Rt`S Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF_Ex_cel_Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
SC OTHER N/A
ti t d a
�-
Site Location Name: Four r� /9 C <^C-e C L3.� p Samples received after 14:00 will be processed next business day.
`�
Site Location Physical Address: 1 ``3 Be I /'a.ra, s j?2 a Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
J ,tea (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
p p
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
(SOIL,
WATER OR
PRESERVA-
TIVES
vy
vg REMARKS
LAS
*TYPE
HOURS
SLUDGE)
NO.
SIZE
��
®. g�
ID NO.
SEE BELOW
"C 1•
p o
^f'!d F mrw�'
-r3 i' ��
i(� G�
J
��� v°i
CR
�d
AA
5 A
r
Se
Sampler's Signature ,�., Cd✓ -2r� Sampled By (Print Name) /1� d i G Affiliation
Upon relinquishing, this hain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
ReJlin }wished By: (Signature) -DaRe�eiyedlte Military/Hours Additional Comments: SlteArrival Tlme r
SReli♦etnar� ure) Date Site Departure Time
tu_
Field Tech Fee'
R ILL i ed y: (Signal Received Fpr;}}Prism Laabb/orrralodes By: Date
_•
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY.
U 03
❑ Fed Ex ❑ UPS ❑ Hand -delivered Pr m Field Service O Other (J 1J
PDES: UST: GIB DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: RR 5
❑SC ❑NC ❑SC ❑!NC ❑SC El NC El SC El NC El SC ❑NC❑SC ❑NC EAEl NC ❑SC El NC El SC
I
E CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics.Analysis (Zero Head Space)

ism
ABORATORIES INO.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinkinq Water Cert No. 37735
Environmental Solutions VA Certification No.460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 05/23/2016
Prism Work Order: 6050461
Case Narrative
06/02/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) t�_ A—
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 9

I n n Full -Service Analytical &
' V' Environmental Solutions
AH-ORIM INC.
Sample Receipt Summary
06/02/2016
Prism Work Order: 6050461
)le ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6050461-01 Solid 05/23/16 05/23/16
Samples were received in good condition at 1.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 9

n I Full -Service Analytical &
/' Environmental Solutions
,aa
IC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
06/02/2016
Project: StaLime Client Sample ID: Sta-Lime
Prism Sample ID: 6050461-01
Prism Work Order: 6050461
Sample Matrix: Solid Time Collected: 05/23/16 13:22
Time Submitted: 05/23/16 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time - ID
General Chemistry Parameters
Plant Available Nitrogen
460
mg/kg
380
44
5
*Calculation 5/31/16 9:23
CLB
[CALC]
Solids
70.9
% by
0.100
0.100
1
*SM2540 G 5/25116 11:50
BJC
P6E0552
Weight
Nitrate/Nitrite as N
18
mg/kg dry
7.0
0.78
1
*SM4500-NO3 F 5127/16 8:15
CLB
P6E0565
Phosphorus -Total
2700
mg/kg dry
70
34
20
*SM4500-P F 5/31/16 6:57
CLB
P6E0567
Total Kjeldahl Nitrogen
2000
mg/kg dry
1800
200
5
*351.2 5/31116 9:23
CLB
P6E0551
Ammonia as N
78
mg/kg dry
7.0
2.7
1
*SM4500-NH3 G 6126/16 7:30
CLB
P6E0517
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 5/24/16 11:00
BMS
P6E0521
Total Metals
Mercury
0.23
mg/kg dry
0.028
0.0016
1
*7471B
5/27/16 13:15
JAB
P6E0570
SAR Soil Preparation
Complete
g
1
*2-78-054
5/24/16 8:40
JAB
P6E0553
SAR Percent Moisture
57.2
% by
0.100
0.100
1
*2-78-054
5126/16 10:15
JAB
P6F0017
Weight
Arsenic
4.0
mglkg dry
3.5
0.42
10
*6010D
5126/16 21:24
bgm
P6E0545
Sodium Absorption Ratio
0.51
[blank]
0.30
0.016
1
*2-78-054
5/26116 19:35
bgm
P6E0555
Cadmium
BRL
mg/kg dry
3.5
0.093
10
*6010D
5/26/16 21:24
bgm
P6E0545
Calcium
1400 gH, B
mg/L
1.0
0.085
10
*6010D
5126/16 21:24
bgm
P6E0555
Copper
35 BH
mg/kg dry
6.9
0.62
10
*6010D
5/26/16 21:24
bgm
P6E0545
Lead
12
mg/kg dry
3.5
0.64
10
*6010D
5/26/16 21:24
bgm
P6E0545
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
5/26/16 19:35
bgm
P6E0555
Nickel
210
mg/kg dry
6.9
0.25
10
*601013
5/26116 21:24
bgm
P6E0545
Potassium
6500 gH
mg/kg dry
170
6.2
10
*6010D
5/26116 21:24
bgm
P6E0545
Selenium
9.4
mg/kg dry
6.9
1.6
10
*6010D
5/26/16 21:24
bgm
P6E0545
Sodium
68
mg/L
5.0
0.074
10
*6010D
5126116 19:35
bgm
P6E0555
Sodium
860 BH
mg/kg dry
210
6.8
10
*6010D
5126/16 21:24
bgm
P6E0545
Zinc
60
mg/kg dry
35
1.2
10
*60101)
5126/16 21:24
bgm
P6E0545
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc..
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Of 9

ism
ARORATORICs I -
Full -Service Analytical &
Environmental Solutions
Level II QC Report"
6/2/16 `
:sville, NC Project: StaLime Prism Work Order: 6050461
Attn: Hnay Smith Time Submitted: 5/23/2016 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Ratch PRF0545 - 3050B
Blank (P6E0545-BLK1)
Prepared & Analyzed: 05/26/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
31.7
12
mg/kg wet
BH
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P6EO545-BS1)
Prepared & Analyzed: 05/26/16
Arsenic
24.6
0.25
mg/kg wet
25.00 99
80-120
Cadmium
24.7
0.25
mg/kg wet
25.00 99
80-120
Copper
26.7
0.50
mg/kg wet
25.00 107
80-120
Lead
24.7
0.25
mg/kg wet
25.00 99
80-120
Nickel
24.8
0.50
mg/kg wet
25.00 99
80-120
Potassium
529
12
mg/kg wet
500.0 106
80-120
Selenium
24.1
0.50
mg/kg wet
25.00 97
80-120
Sodium
530
15
mg/kg wet
500.0 106
80-120
Zinc
25.0
2.5
mg/kg wet
25.00 100
80-120
Batch P6E0553 - SAR 2-78-054
Blank (P6E0553-BLK1)
Prepared & Analyzed: 05/25/16
SAR Soil Preparation
Complete
g
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 4 Of 9

[ I n I Full -Service Analytical &
' V' Environmental Solutions
LABORATORIES ING.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P6EO555 - 3010A
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
6/2/16
Prism Work Order: 6050461
Time Submitted: 5/23/2016 2:50:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P6E0555-BLK1)
Prepared & Analyzed: 05/26/16
Sodium Absorption Ratio
BRL 3.0 [blank]
Calcium
2.32 1.0 mg/L BH
Magnesium
BRL 1.0 mg/L
Sodium
BRL 5.0 mg/L
Batch P6EO570 - 7471 B
Blank (P6E0570-BLK1) Prepared &Analyzed: 05/27/16
Mercury BRL 0.020 mg/kg wet
LCS (P6E0570-BS1) Prepared &Analyzed: 05/27/16
Mercury 0.470 0.020 mg/kg wet 0.4167 113 80-120
Batch P6F0017 - NO PREP
Blank (P6F0017-BLK1) Prepared & Analyzed: 05/26/16
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (P6F0017-DUP1) Source: 6050461-01 Prepared & Analyzed: 05/26/16
SAR Percent Moisture 57.3 0.100 % by Weight 57.2 0.2 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone : [phone] -Toll Free Number: 1-800/529.6364- Fax: [phone] Page 5 Of 9

I n I Full -Service Analytical &
I v' Environmental Solutions
ABORATCRIES INC.
esville, NC
—.,-r imith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Level II QC Report:
6/2116 ,
Project:. StaLime Prism Work Order: 6050461
Time Submitted: 5/23/2016 2:50:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6EO517 - NO PREP
Blank (P6EO517-BLK1) Prepared: 05/25/16 Analyzed: 05/26/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6E0517-BS1) Prepared: 05/25/16 Analyzed: 05/26/16
Ammonia as N 121 5.0 mg/kg wet 125.0 97 80-120
Matrix Spike (P6E0517-MS1) Source: 6050461-01 Prepared: 05/25/16 Analyzed: 05/26/16
Ammonia as N 254 7.0 mg/kg.dry 176.2 78.4 100 80-120
Matrix Spike Dup (P6EO517-MSD1) Source: 6050461-01 Prepared: 05/25/16 Analyzed: 05/26/16
Ammonia as N 253 7.0 mg/kg dry 176.2 78.4 99 80-120 0.4 20
Batch P6EO551 - 351.2
Blank (P6EO551-BLK1)
Prepared: 05/26/16 Analyzed: 05/31/16
Total Kjeldahl Nitrogen
LCS (P6E0551-BS1)
BRL 25 mg/kg wet
Prepared: 05/26/16 Analyzed: 05/31/16
Total Kjeldahl Nitrogen
Matrix Spike (P6E0551-MS1)
470 100 mg/kg wet
Source: 6050461-01
500.0 94 90-110
Prepared: 05/26/16 Analyzed: 05/31/16
Total Kjeldahl Nitrogen
Matrix Spike Dup (P6E0551-MSD1)
3740 1800 mg/kg dry
Source: 6050461-01
7049 2040 24 90-110 MI
Prepared: 05/26/16 Analyzed: 05/31/16
Total Kjeldahl Nitrogen
Batch P6EO552 - Solids Dry Weight
3540 1800 mg/kg dry
7049 2040 21 90-110 6 20 MI
Blank.(P6EO552-BLK1)
Prepared &Analyzed: 05/26/16
Solids
100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 9

�SIVI
ABORATORIES ING
sville, NC
imith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
General Chemistry Parameters - Quality Control
Project: StaLime
Level II QC Report
6/2/16
Prism Work Order: 6050461
Time Submitted: 5/23/2016 2:50:OOPM
Reporting Spike Source
Analyte Result Limit Units Level Result %REC
%REC RPD
Limits RPD Limit
Batch P6EO565 - NO PREP
Blank (P6E0565-BLK1) Prepared &Analyzed: 05/27/16
Nitrate/Nitrite as N BRL 5.0 .mglkg wet
LCS (P6E0565-BS1) Prepared & Analyzed: 05/27/16
Nitrate/Nitrite as N 48.6 5.0 mg/kg wet 50.00 97 80-120
Matrix Spike (P6E0565-MS1) Source: 6050461-01_ Prepared & Analyzed: 05/27/16
Nitrate/Nitrite as N 79.1 7.0 mg/kg dry 70.49 18.0 87 80-120
Batch P6EO567 - SM4500-PB5
Blank (P6E0567-BLK1) Prepared: 05/26/16 Analyzed: 05/31/16
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P6E0567-BS1) Prepared: 05/26/16 Analyzed: 05/31/16
Phosphorus -Total 102 2.5 mg/kg wet 100.0 102 90-110
Notes
Matrix Spike (P6E0567-MS1) Source: 6050461-01 Prepared: 05/26/16 Analyzed: 05/31/16
Phosphorus -Total 2780 70 mg/kg dry 141.0 2750 26 80-120 MC
Matrix Spike Du_p (P6E0567-MSD1) Source: 6050461-01 Prepared: 05/26/16 Analyzed: 05/31/16
Phosphorus -Total 2770 70 mg/kg dry 141.0 2750 19 80-120 0.4 20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 9

F*395=7��UPR
Full-Service Analytical &
I S M
Environmental Solutions
UIBo-RIE6 INC
.City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
6/2116
Prism Work Order: 6050461
Time Submitted: 5/23/2016 2:50:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit . Notes
Batch P6EO521 - NO PREP
Blank (P6E0521-BLK1) Prepared & Analyzed: 05/24/16
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Datei-rime
6050461-01
P6E0551
0.05 g
25 mL
05/26/16 11:00
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
6050461-01
P6E0567
1 g
50 mL
05/26/16 15:47
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
6050461-01
P6E0552
30 g
30 g
05/25/16 11:50
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daternme
6050461-01
P6E0555
50 mL
50 mL
05/26/16 10:15
6050461-01
P6E0555
50 mL
50 mL
05/26/16 10:15
6050461-01
P6E0555 .-
50 mL
50 mL
05/26/16 10:15 -
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
6050461-01
P6E0545
2.04 g
50 mL
05/26/16 8:55
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/rime
6050461-01
P6E0570
0.6 g
50 mL
05/27/16 8:40
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/rime
6050461-01
P6E0553
250 g
250 g
05/24/16 8:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page 8 of 9

CHAIM43F CUSTODY RECORD'
AM NIG
Full -,service Analytical 4
YES' S
NO N/A.
M
PH
.-
�
I Environmental Solution:4
PAGE_ GF _ CIEDOTE #'r0 EWS4IRE PROPER BILLING:
Samples INTACT uponarrival?
�
`0
O
�+ 'LABOnATOaies, INC.
Project Name:
Received ON \VET ICE?
449 Springbrook Road • Charlotte, NC 23217
Phone [phone] - Fax: [phone]
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER PRESERVATIVES inci cacedv
_ _ _
-'—:
p
Company Name: C 11
34,des'e ld
Please ATTACH any project specific reporting (OC LEVEL 1 II III IV)
RerelvedWITHIN"HOLDINGTIMLS7
CUSIODY:SEALS INTACT?
-
d
Client
o�
provisions and/or OC Requirements
_ .
Report To/Contact Name:
A n y S n r'
Invoice To:
VOLATILES rec'd W/OUT HEAD.SPACG? .
Reporting Address:
Address:
PROPER iCONIAINEI'S used,
%i — r _-
--^.
V-6. I -ate
Phone:70 -979— 4 3 -9 Fax es (No): 7,1q-57S— ?d6S Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
— I� Pre -Approved SC OTHER N/A
Site Location Name: 6`, +" f p"D C e k Low Tp Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 493 Be-il I711. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO —
(SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) am p p
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
CLIENT DATE COLLECTED (SOIL, PRESERVA- a �d7 PRISM
IS
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TYPE TIVES ^� �;� REMARKS ID NO.
HOURS SLUDGE) SEE BELOW N0. SIZEw
�+L
�ivr9s'�9b
y
d;�
rAy�K��A�
(��l
V'
CT
SA
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C �d
�9
0
a
¢
Sampler's Signature Lc�c rice
/
Sampled By (Print Name) .A' (✓j i",re:
Affiliation
•
•
Site Arrival Time.
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relinq hetl By: (Signature) .`yt� Receive By: (Signature) Dat Military/Hours Additional Comments:
Site DepartureTime
Relin ed By: (Signature)
Received By: (Signature)
Date
Field Tech Tee
Relinquished B , 99ignature)
A/
Received For Pri a ora/ t s By,
Date
h
Method of Shipment: NOTE: ALL SAMPLE COO ERS SHOULD BE TAPED SHUT WITH CUST • DY SEALS'FOR TRANSPORTATION TO THE LABORATORY.
SAMPLES ARE NOT AC EPTED AND VERIFIED AGAINST COC UNT RECEIVED AT THE LABORATORY.
O Fed Ex ❑UPS OBand-delivered rism Field Service ❑ Other
COC Group No.
L) L, )
S: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCT I, CERCLA LANDFILL OI hIER:
❑SCI ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC I ®NC ❑SC 0NC❑SCi ❑❑NC ❑SC ❑❑NC ❑SC ❑❑NC ❑SC
hElEl❑
—WR TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

smiBORATORIES
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No.Case Narrative
SC Certification No. 990 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735
06/08/2016
Environmental Solutions VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 05/31/2016
Prism Work Order: 6060007
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the.reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be,reproduced, except in its entirety, without the written consent of Prism. Laboratories,_ Inc.,_ _
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-800/529-6364- Fax: [phone] Page 1 of

Full -Service Analytical & Sample Receipt Summary
Environmental Solutions 06/08/2016
ING
Prism Work Order: 6060007
Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6060007-01 Solid 05/31/16 05/31/16
Samples were received at 13.8 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 9

I n n Full -Service Analytical &
'v' I Environmental Solutions
ABORATOME$ING
:sville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
06/08/2016
Project: StaLime Client Sample ID: Sta-Lime
Prism Sample ID: 6060007-01
Prism Work Order: 6060007
Sample Matrix: Solid Time Collected: 05/31/16 13:35
Time Submitted: 05/31/16 15:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Dateffime
ID
General Chemistry Parameters
Plant Available Nitrogen
3900
mg/kg
380
44
5
*Calculation
6/6/16 9:25
CLB
[CALC]
Solids
92.1
% by
0.100
0.100
1
*SM2540 G .
6/2/16 15:49
JLR
P61`0067
Weight
Nitrate/Nitrite as N
27
mg/kg dry
5.4
0.60
1
*SM4500-NO3 F
612/16 7:57
CDE
P6F0034
Phosphorus -Total
1700
mg/kg dry
54
26
20
*SM4500-P F
6/7/16 9:03
CDE
P6F0118
Total Kjeldahl Nitrogen
14000
mg/kg dry
1400
150
5
*351.2
6/3116 10:21
CLB
P6F0047
Ammonia as N
38
mg/kg dry
11
4.2
2
*SM4500-NH3 G
6/6/16 9:26
CLB
P6F0088
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
6/1/16 9:32
BMS
P6F0044
Total Metals
Mercury
0.058
mg/kg dry
0.020
0.0011
1
*7471B
6/6116 14:47
JAB
P6F0100
SAR Soil Preparation
Complete
g
1
*2-78-054
6/3/16 8:00
JAB
P6F0071
SAR Percent Moisture
62.5
% by
0.100
0.100
1
*2-78-054
6/3116 11:15
JAB
P6F0073
Weight
Arsenic
4.2
mg/kg dry
2.8
0.34
10
*6010D
6/3/16 13:38
bgm
P6F0039
Sodium Absorption Ratio
0.31
[blank]
0.30
0.016
1
*2-78-054
6/6/16 19:22
bgm
P00072
Cadmium
BRL
mg/kg dry
2.8
0.074
10
*6010D
6/3/16 13:38
bgm
P6F0039
Calcium
1100
mg/L
20
1.7
200
*6010D
6/6116 19:22
bgm
P6F0072
Copper
26
mg/kg dry
5.6
0.60
10
*6010D
6/3/16 13:38
bgm
P6F0039
Lead
12
mg/kg dry
2.8
0.51
10
*6010D
6/3116 13:38
bgm
P6F0039
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
6/3/16 15:20
bgm
P6F0072
Nickel
190
mg/kg dry
5.5
0.20
10
*6010D
6/3116 13:38
bgm
P6F0039
Potassium
6500
mg/kg dry
140
5.0
10
*6010D
6/3/16 13:38
bgm
P6170039
Selenium
7.8
mg/kg dry
5.5
1.3
10
*6010D
6/3116 13:38
bgm
P6170039
Sodium
37
mg/L
6.0
0.074
10
*60101)
613/16 15:20
bgm
P6F0072
Sodium
650
mg/kg dry
170
5.4
10
*6010D
6/3116 13:38
bgm
P6F0039
Zinc
49 BH
mg/kg dry
28
0.99
10
*6010D
6/3/16 13:38
bgm
P6F0039
.This report should not bereproduced, except in its entirety, without the written
consent of Prism Laboratories, Inc.. ,.,.
449 Springbrook Road - P.O. Box.240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:
1-800/529-6364 -
Fax: 704/52"409
Page
3 Of 9

I Full -Service Analytical &
Environmental Solutions
ABORA IE$ ING
wille, NC
/lttll. r+nuy Jmith
P.O. Box 1111
Statesville, NC 28687
Total Metals -,Quality Control
Project: Stal-ime
Level II QC Report
618/16
Prism Work Order: 6060007
Time Submitted: 5/31/2016 3:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6F0039 - 3050B
Blank (P6F0039-BLK1)
Prepared: 06/02/16 Analyzed: 06/03/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
BH
LCS (P6F0039-BSI)
Prepared: 06/02/16 Analyzed: 06/03/16
Arsenic
24.3
0.25
mg/kg wet
25.00 97 80-120
Cadmium
25.0
0.25
mg/kg wet
25.00 100 80-120
Copper
25.6
0.50
mg/kg wet
25.00 102 80-120
Lead
25.0
0.25
mg/kg wet
25.00 100 80-120
Nickel
24.8
0.50
mg/kg wet
25.00 99 80-120
Potassium
523
12
mg/kg wet
500.0 105 80-120
Selenium
23.9
0.50
mg/kg wet
25.00 95 80-120
Sodium
490
15
mg/kg wet
500.0 98 80-120
Zinc
25.3
2.5
mg/kg wet
25.00 101 80-120
Batch P6F0071 - SAR 2-78-054
Blank (P6F0071-BLK1) Prepared: 06/02/16 Analyzed: 06/03/16
SAR Soil Preparation Complete g
This report should not be reproduced, except in its entirety,, without the written consent of.Prism Laboratories,_Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: l-8001529-6364- Fax: [phone] Page 4 of 9

I Full -Service Analytical &
Environmental Solutions
ABORATORIES INC.
.sville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Level II QC Report
6/8/16
Prism Work Order: 6060007
Time Submitted: 5/31/2016 3:10:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6F0072 - 3010A
Blank (P6F0072-BLK1)
Prepared & Analyzed: 06/03/16
Sodium Absorption Ratio
BRL
3.0 [blank]
Calcium
BRL
1.0 mg/L
Magnesium
BRL
1.0 mg/L
Sodium
BRL
5.0 mg/L
Batch P6F0073 - NO PREP
Blank (1P6F0073-B1LK1)
Prepared & Analyzed: 06/03/16
SAR Percent Moisture
BRL
0.100 % by Weight
Duplicate (P6F0073-DUP1)
Source: 6060007-01 Prepared &Analyzed: 06/03/16
SAR Percent Moisture
65.3
0.100 % by Weight 62.5 4 200
Batch P6F0100 - 7471 B
Blank (P6F0100-BLK1)
Prepared & Analyzed: 06/06/16
Mercury
BRL
0.020 mg/kg wet
LCS (P6F0100-BS1.)
Prepared &Analyzed: 06/06/16
Mercury
0.433
0.020 mg/kg wet 0.4167 104 80-120
This report should not be reproduced,. except in its_entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 5 of 9

' sm I Full -Service Analytical &
Environmental Solutions
ABORATCRIES INC.
:sville, NC
rlurl. rvIuy smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime
Reporting
Analyte Result Limit Units
Level II QC Report
6/8/16
Prism Work Order: 6060007
Time Submitted: 5/31/2016 3:10:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P6170034 - NO PREP
Blank (1361F0034-BLKII) Prepared & Analyzed: 06/02/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6F0034-BS1) Prepared &Analyzed: 06/02/16
Nitrate/Nitrite as N 48.2 5.0 mg/kg wet 50.00 96 80-120
Matrix Spike (P6F0034-MS1) Source: 6060007-01 Prepared & Analyzed: 06/02/16
Nitrate/Nitrite as N 73.4 5.4 mg/kg dry 54.28 26.8 86 80-120
Matrix Spike Dup (P6F0034-MSD1) Source: 6060007-01 Prepared & Analyzed: 06/02/16
Nitrate/Nitrite as N 72.9 5.4 mg/kg dry 54.28 26.8 85 80-120 0.7 20
Batch P6F0047 - 351.2
Blank (P6F0047-BLK1) Prepared: 06/01/16 Analyzed: 06/03/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6F0047-BSI) Prepared: 06/01/16 Analyzed: 06/03/16
Total Kjeldahl Nitrogen 461 100 mg/kg wet 500.0 92 90-110
Batch P61F0088 - NO PREP
Blank (1361F0088-BLK1) Prepared & Analyzed: 06/06/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6F0088-BS1) Prepared &Analyzed: 06/06/16
Ammonia as N 126 5.0 mg/kg wet 125.0 101 80-120
This reportshould not be reproduced, except in its entirety, without, the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 9

ism
ABORATORIM 1-
:sville, NC
rrun. rtnuy omit"
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
General Chemistry Parameters - Quality Control
Project: Stal-ime
Level II QC Report
6/8/16
Prism Work Order: 6060007
Time Submitted: 5/31/2016 3:10:OOPM
Analyte
Reporting
Result Limit Units
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit Notes
Batch P6F0088 - NO PREP
Matrix Spike (P6F0088-MS1)
Source: 6060007-01
Prepared & Analyzed: 06/06/16
Ammonia as N
Matrix Spike Dup (P6F0088-MSD1)
169 11 mg/kg dry
Source: 6060007-01
135.7 38.0 97.
Prepared & Analyzed: 06/06/16
80-120
Ammonia as N
171 11 mg/kg dry
135.7 38.0 98
80-120 0.9 20
Batch P6FO118 - SM4500-PB5
Blank (P6F0118-BLK1) Prepared: 06/06/16 Analyzed: 06/07/16
Phosphorus -Total BRL 2.5 mg/kg wet
LC_S (P6FO118-BS1) Prepared: 06/06/16 Analyzed: 06/07/16
Phosphorus -Total 105 2.5 mg/kg wet 100.0 105 90-110
Matrix Spike (P6F0118-MS1) Source: 6060007-01 Prepared: 06/06/16 Analyzed: 06/07/16
Phosphorus -Total 1990 54 mg/kg dry 108.6 1710 252 80-120 me
Matrix Spike Dup_ (P6F0118-MSD1) Source: 6060007-01 Prepared: 06/06/16 Analyzed: 06/07/16
Phosphorus -Total 2040 54 mg/kg dry 108.6 1710 301 80-120 3 20 MC
This report should not be reproduced, except in its entirety, without the,written consent of Prism,Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 9

I`- n q I Full -Service Analytical &
J' V' Environmental Solutions
ABOR-ORIES ING
:sville, NC
Attn: Hnay Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
6/8/16
Prism Work Order: 6060007
Time Submitted: 5/31/2016 3:10:OOPM
Reporting Spike Source %REC - RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6F0044 - NO PREP
Blank (P6170044-BLK1)
Prepared & Analyzed: 06/01/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
DateTme
6060007-01
P6F0047
0.05 g
25 mL
06/01/16 11:00
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Date/rime
6060007-01
P6F0118
1 g
50 mL
06/06/16 12:20
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/rime
6060007-01
P6F0067
30 g
30 g
06/02/16 15:49
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/rime
6060007-01
P6F0072
50 mL
50 mL
06/03/16 11:26
6060007-01
P6F0072
50 mL
50 mL
06/03/16 11:26
6060007-01
P6F0072
50 mL
50 mL
06/03/16 11:26
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/rime
6060007-01
P6F0039
1.97 g
50 mL
06/02/16 8:35
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/rime
6060007-01
P6F0100
0.65 g
50 mL
06/06/16 10:50
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Datelrime
6060007-01
P6F0071
250 g
250 g
06/02/16 8:00
This. report should not, be reproduced, except in its entirety, without,the written consent of. Prism Laboratories,; Inc.,,.,, ,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/5.29-6364 - Fax: [phone] Page 8 Of 9

Full -Service Analytical
4�
Environmental Solutions
PP
LABORATORIES, RJC.
449 Springbrook Road ^ Charlotte, NC 28217
Phone [phone] ^ Fax: [phone]
Client Company Name: ��r 5�a�.s►'°d�
Report To/Contact Name: AaXly S,-n,A -
Reporting Address:
Phone:`70q-'3i3 3tiV
Fa>+ Yes (No):r 0q-Tly-US purchase Order No.lBilling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days Cl 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel
re h work Must Be
Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
SC OTHER N/A
Site Location Name: F u
�+
All Ci eak 10 : TP Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
Site Location Physical Address:
61 id farr," i� �
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES_ NO —
r 'Ale
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
PRTIVESESERVA
ANALYSIS
REQUESTED
�� REMARKS
PRISM
LAB
CLIENT
[SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
(SOIL,
WATER OR
��?0�/
ID NO.
*TYPE
Mo.
O
SIZE
HOURS
SLUDGE)
SEE BELOW
31.-louse 15-36-eg 18:35 1 S I P
Sampler's Signature
Upon relinquishing, this Chain of Custod
submitted in writing to the Prism Project
Sampled By (Print Name)
is your authorization for Prim to proceed with the a
a ger. There will be charge or any changes after
F Received By: 'gnature) 1
,SA
Affiliation
as requested above, Any changes must be
shave been initialized.
j� IISIA0
Memou Or anlpmel R: 1-1 M........,r. — � ------- -- -- - --
SAMPLES ARE NOT ICCEPTED AND VERIFIED AGAINST COC y L RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑UPS ❑Hand delivered Prism Field Service ❑Other
LERTYPECODES:
❑ NC ❑ SC ®INC ROC ❑ SID I L3 NC 0 SCATER: I EINC ❑ SCE ❑ NBC ❑ SC O NC ❑ SC O C FILL ❑ SC I EI NC ❑ SC
❑ ❑ —
A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
01
SEE,REVERSE'FOR.
TERMS'8 CONDITIONS

A
INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402 Case Narrative
NC Drinking Water Cert No. 37735
Full -Service Analytical & SC Certification No. 99012 07/15/2016
Environmental Solutions FL NELAC Cert No. E87519
VA NELAC Cert No.-460211 _ _.....
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 07/06/2016
Prism Work Order: 6070061
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V l..
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Full -Service Analytical & Sample Receipt Summary
"
F'ikllopi
R I S M Environmental Solutions 07/15/2016
Prism Work Order: 6070061
Client Sample ID Lab Sample ID Matrix. Date Sampled Date Received
Stal-ime (and Fecal 1)
6070061-01
Solid
07/05/16
07/06/16
Fecal #2
6070061-02
Solid
07/05/16
07/06/16
Fecal #3
6070061-03
Solid
07/05/16
07/06/16
Fecal #4
6070061-04
Solid
07/05/16
07/06/16
Fecal #5
6070061-05
Solid
07/05/16
07/06/16
Fecal #6
6070061-06
Solid
07/05/16
07/06/16
Fecal #7
6070061-07
Solid
07/05/16
07/06/16 .
Samples were received at 19.7 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 0f 18

PR Laboratory Report
Full -Service Analytical &
�r ^;,`, Environmental Solutions 07/15/2016
2�.'-�..'��" IABORATOPIE$ ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: StaLime (and Fecal 1)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6070061-01
P.O. Box 1111 Prism Work Order: 6070061
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Dateffime
ID
General Chemistry Parameters
Plant Available Nitrogen
960
mg/kg
380
44
5
*Calculation
7/14/16 8:17
CDE
[CALC]
% Solids
80.6
% by
0.100
0.100
1
*SM2540 G
7/7116 16:30
BJC
P6G0126
Weight
Nitrate/Nitrite as N
BRL
mg/kg dry
6.2
0.68
1
*SM4500-NO3 F 7/8/16 8:26
CDE
P6G0112
Phosphorus -Total
1400
mg/kg dry
62
30
20
*SM4500-P F
7114/16 10:58
TP04
P6G0214
Total Kjeldahl Nitrogen
3900
mg/kg dry
1600
180
5
*351.2
7/14/16 8:17
CDE
P6G0161
Ammonia as N
54
mg/kg dry
6.2
2.4
1
*SM4500-NH3 G 7/12/16 8:14
CLB
P6G0153
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
7/6/16 12:14
BMS
P6G0098
Total Metals
Mercury
0.16
mg/kg dry
0.030
0.0017
1
*7471B
7/13/16 11:59
JAB
P6130197
SAR Soil Preparation
Complete
g
1
*2-78-054
7/8116 9:00
JAB
P6G0091
SAR Percent Moisture
55.3
% by
0.100
0.100
1
*2-78-054
7/12116 14:15
JAB
P6G0186
Weight
Arsenic
7.4
mg/kg dry
0.31
0.038
1
*6010D
717/16 17:24
bgm
P6G0085
Sodium Absorption Ratio
0.50
[blank]
0.30
0.016
1
*2-78-054
7/12/16 16:38
bgm
P6G0123
Cadmium
BRL
mg/kg dry
0.31
0.0084
1
*6010D
717/16 17:24
bgm
P6G0085
Calcium
2000
mg/L
1.0
0.085
10
*6010D
7112116 16:38
bgm
P6G0123
Copper
26
mg/kg dry
0.62
0.056
1
*6010D
717/16 17:24
bgm
P6G0085
Lead
11
mg/kg dry
0.31
0.058
1
*6010D
7/7116 17:24
bgm
P600085
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
7/12116 16:38
bgm
P6G0123
Nickel
230
mg/kg dry
6.2
0.22
10
*6010D
7112/16 17:05
bgm
P600085
Potassium
7300
mg/kg dry
160
5.6
10
*6010D
7/12/16 17:05
bgm
P6G0085
Selenium
1.7
mg/kg dry
0.62
0.15
1
*6010D
7/7/16 17:24
bgm
P6G0085
Sodium
82 eH
mg/L
5.0
0.074
10
*6010D
7/12/16 16:38
bgm
P6130123
Sodium
910
mg/kg dry
19
0.61
1
*6010D
717/16 17:24
bgm
P600085
Zinc
37
mglkg dry
3.1
0.11
1
*6010D
717/16 17:24
bgm
P6G0085
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: l-800/529-6364- Fax: [phone] Page 3 0f 18

I S Laboratory Report`
Full -Service Analytical &
Environmental Solutions 07/15/2016
'IBORATORIE$ ING '
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #2 .
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6070061-02
P.O. Box 1111 Prism Work Order: 6070061
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
Solids 82.2
% by
0.100
0.100 1
'SM2540 G 7/7/16 16:30 BJC
P6G0126
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 7/6/16 12:14 BMS
P6G0098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 18

I I n %� Full -Service Analytical &
' V' Environmental Solutions
LABORATORIES ING
Laboratory Report
07/15/2016
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #3
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6070061-03
P.O. Box 1111 Prism Work Order: 6070061
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 97.4 % by 0.100 0.100 1 *SM2540 G 717116 16:30 BJC P6G0126
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 7/6116 12:14 BMS P6G0098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18

I`- %� I Full -Service Analytical 8
J M Environmental Solutions
Laboratory Report
07/15/2016
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #4
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6070061-04
P.O. Box 1111 Prism Work Order: 6070061
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 97.5 % by 0.100 0.100 1 •SM2540 G 717/16 16:30 BJC P6130126
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 `SM9221 E 716/16 12:14 BMS P6G0098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. ..
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:.1-800/529-6364 - Fax: [phone] Page 6 of 18

I I n Full -Service Analytical &
' V' Environmental Solutions
-RATORIES, ING
Laboratory Report
07/15/2016
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #5
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 6070061-05
P.O. Box 1111
Prism Work Order: 6070061
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Daterrime ID
General Chemistry Parameters
Solids
74.7 % by
0.100 0.100
1 'SM2540 G 7/7/16 16:30 BJC P6G0126
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 7/6/16 12:14 BMS P6G0098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 18

3 I S„ n Full -Service Analytical
'v' Environmental Solutions
LABORATORIES ING
Laboratory Report
07/15/2016
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #6
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 6070061-06
P.O. Box 1111 Prism Work Order: 6070061
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datenme ID
General Chemistry Parameters
% Solids 75.1 % by 0.100 0.100 1 *SM2540 G 7/7/16 16:30 BJC P6G0126
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 7/6/16 12:14 BMS P6G0098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 18

I`- Full -Service Analytical &
J M Environmental Solutions
ANORATONIE; ING
Laboratory Report
07/15/2016
sville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #7
'mith 60Day 7 Fecal) Prism Sample ID: 6070061-07
11 Prism Work Order: 6070061
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/05/16 12:40
Time Submitted: 07/06/16 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 83.5 % by 0.100 0.100 1 'SM2540 G 717/16 16:30 BJC P6G0126
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 7/6116 12:14 BMS P6GO098
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 Of 18

t I Full -Service Analytical &
Environmental Solutions
IABORATAFI s—
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
7/15/16
Project: StaLime (Qtrly, Biweekly, 60Day Prism Work Order: 6070061
7 Fecal) Time Submitted: 7/6/2016 8:00:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6GO085 - 3050B
Blank (P6G0085-BLK1)
Prepared & Analyzed: 07/07/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6GO085-BS1)
Prepared & Analyzed: 07/07/16
Arsenic
25.1
0.25
mg/kg wet
25.00 100
80-120
Cadmium
25.3
0.25
mg/kg wet
25.00 101
80-120
Copper
25.9
0.50
mg/kg wet
25.00 104
80-120
Lead
25.0
0.25
mg/kg wet
25.00 100
80-120
Nickel
24.8
0.50
mg/kg wet
25.00 99
80-120
Potassium
510
12
mg/kg wet
500.0 102
80-120
Selenium
24.9
0.50
mg/kg wet
25.00 100
80-120
Sodium
512
15
mg/kg wet
500.0 102
80-120
Zinc
24.7
9 5
—/kn woo
95 nn 00
An ion
Batch P6GO091 - SAR 2-78-054
Blank (P6GO091-BLK1) Prepared: 07/07/16 Analyzed: 07/08/16
SAR Soil Preparation Complete g
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 18

Level II QC Report
I S n Full -Service Analytical 8 7/15/16
' V' Environmental Solutions
%eo-ORIea Ina .
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 6070061
Attn: Andy Smith 7 Fecal) Time Submitted: 7/6/2016 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6GO123 - 301 OA
Blank (P6G0123-BLK1) Prepared: 07/08/16 Analyzed: 07/12/16
Sodium Absorption Ratio BRL 3.0 [blank]
Calcium BRL 1.0 mg/L
Magnesium BRL 1.0 mg/L
Sodium BRL 5.0 mg/L BH
Batch P6GO186 - NO PREP
Duplicate (P6GO186-DUP1) Source: 6070061-01 Prepared: 07/08/16 Analyzed: 07/12/16
SAR Percent Moisture 54.1 0.100 % by Weight 55.3 2 200
Batch P6G0197 - 7471 B
Blank (P6G0197-BLK1) Prepared & Analyzed: 07/13/16
Mercury BRL 0.020 mg/kg wet
LCS (P6G0197-BS1) _ Prepared & Analyzed: 07/13/16
Mercury 0.412 0.020 mg/kg wet 0.4167 99 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/829-6364 - Fax: [phone] Page 11 of 18

Level II -QC Report
t I `- n �I Full -Service Analytical &
J' V' Environmental Solutions " 7/15/16
LABORATORIES. ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 6070061
Attn: Andy Smith 7 Fecal) Time Submitted: 7/6/2016 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6GO112 - NO PREP
Blank (P6G0112-BLK1) Prepared & Analyzed: 07/08/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6G0112-BSI) Prepared & Analyzed: 07/08/16
Nitrate/Nitrite as N 51.4 5.0 mg/kg wet 50.00 103 80-120
Matrix Spike (P6G0112-MS1) _ _ Source: 6070061-01 Prepared &Analyzed: 07/08/16
Nitrate/Nitrite as N 62.5 6.2 mg/kg dry 62.02 3.04 96 80-120
Matrix Spike Dup (P6G0112-MSD1) Source: 6070061-01 Prepared & Analyzed: 07/08/16
Nitrate/Nitrite as N 62.6 6.2 mg/kg dry 62.02 3.04 96 80-120 0.2 20
Batch P6GO126 - Solids, Dry Weight
Duplicate (P6G0126-DUP4) Source: 6070061-06 Prepared & Analyzed: 07/07/16
% Solids 76.0 0.100 % by Weight 75.1 1 20
Batch P6GO153 - NO PREP
Blank (P6G0153-BLK1) _ _ Prepared: 07/11/16 Analyzed: 07/12/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6GO153-BS1) Prepared: 07/11/16 Analyzed: 07/12/16
Ammonia as N 120 5.0 mg/kg wet 125.0 96 80-120
Matrix Spike (P6G0153-MS1) Source: 6070061-01 Prepared: 07/11/16 Analyzed: 07/12/16
Ammonia as N 190 6.2 mg/kg dry 155.0 54.3 88 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 18

Level II QC Report
I I S n n I Full - Analytical & 7/15/16
' V' Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 6070061
7 Fecal) Time Submitted: 7/6/2016 8:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6GO153 - NO PREP
Matrix Spike Dup (P6G0153-MSD1) Source: 6070061-01 Prepared: 07/11/16 Analyzed: 07/12/16
Ammonia as N 191 6.2 mg/kg dry 155.0 54.3 88 80-120 0.4 20
Batch P6130161 - 351.2
Blank (P6GO161-BLK1) Prepared: 07/11/16 Analyzed: 07/14/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6GO161-BSI) _ Prepared: 07/11/16 Analyzed: 07/14/16 _
Total Kjeldahl Nitrogen 513 100 mg/kg wet 500.0 103 90-110
Matrix Spike (P6G0161
Total Kjeldahl Nitrogen
Source:6070061-01 Prepared: 07/11/16 Analyzed: 07/14/16
9750 1600 mg/kg dry 6202 3920 94 90-110
Matrix Spike Dup (P6G0161-MSD1) Source: 6070061-01 Prepared: 07/11/16 Analyzed: 07/14/16
Total Kjeldahl Nitrogen 8910 1600 mg/kg dry 6202 3920 80 90-110 9 20 M
Batch P6GO214 - SM4500-PB5
Blank (P6G021j
Phosphorus -Total
BRL 2.5 mg/kg wet
Prepared & Analyzed: 07/14/16
LCS (P6GO214-BS1) Prepared &Analyzed: 07/14/16
Phosphorus -Total 93.4 2.5 mg/kg wet 100.0 93 90-110
Matrix Spike (P6GO214-MS1) Source: 6070061-01 Prepared & Analyzed: 07/14/16
Phosphorus -Total 1330 62 mg/kg dry 124.0 1410 NR 80-120 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 18

Lever II- QG Report
I I S I� �I Fun -Service Analytical 7/15/1 6
'v' Environmental Solutionss
LABORATORIES INC.
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 6070061
Attn: Andy Smith 7 Fecal) Time Submitted: 7/6/2016 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6GO214 - SM4500-PB5
Matrix Spike Dup (P6G0214-MSD1) Source: 6070061-01 Prepared & Analyzed: 07/14/16
Phosphorus -Total 1430 62 mg/kg dry 124.0 .1410 10 80-120 7 20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 18

I n n I Full -Service Analytical &
' V' Environmental Solutions
1.0 --- IM INC.
Level II QC Report
7/15/16
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 6070061
Attn: Andy Smith 7 Fecal) Time Submitted: 7/6/2016 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6G0098 - NO PREP
Blank (136G0098-131LK1) Prepared & Analyzed: 07/06/16
Fecal Coliforms BRL 0.2 MPN/g wet
Duplicate (P6G0098-DUP1) Source: 6070061-07 Prepared & Analyzed: 07/06/16
Fecal Coliforms BRL 0.2 MPN/g dry BRL 20
This report should not be reproduced, except in its entirety, without.the written consent of Prism Laboratories, Inc. „
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 15 of 18

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
6070061-01
P6G0161
0.05 g
25 mL
07/11/16 11:00
Prep Method: SM4500-13135
Lab Number
Batch
Initial
Final
Daterrime
6070061-01
P6G0214
1 g
50 mL
07/14/16 6:15
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
6070061-01
P6G0126
30 g
30 g
07/07/16 16:30
6070061-02
P6G0126
30 g
30 g
07/07/16 16:30
6070061-03
P6G0126
30 g
30 g
07/07/16 16:30
6070061-04
P6G0126
30 g
30 g
07/07/16 16:30
6070061-05
P6G0126
30 g
30 g
07/07/16 16:30
6070061-06
P6G0126
30 g
30 g
07/07/16 16:30
6070061-07
P6G0126
30 g
30 g
07/07/16 16:30
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/rime
6070061-01
P6G0123
50 mL
50 mL
07/08/16 9:00
6070061-01
P6G0123
50 mL
50 mL
07/08/16 9:00
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
6070061-01
P6G0085
1.99 g
50 mL
07/07/16 8:25
6070061-01
P6G0085
1.99 g
50 mL
07/07/16 8:25
Prep Method: 7471B
Lab Number
Batch
Initial
Final
DaterTime
6070061-01
P6G0197
0.49 g
50 mL
07/13/16 9:25
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
-Final
Date/Time r
6070061-01
P6G0091
250 g
250 g
07/07/16 7:25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-ToUFree Number: 1-800/529-6364- Fax: [phone] Page 16 of 18

I ' CHAIN OF CUSTODY RECORD
s,
%•
RISMFull-Service
Solutions
Environmental Solutions
—
YES NO ' N/A` r
al PAGE o� ®UOTE it Y® ENSURE PROPER BILLIPIG:
n „l,ra Samples INTACT upon arrival?
O
...., ,,, I.P.BORATORIE9, IIJC.
Project Name: Received ON WET ICE?
r
449 Springbrook Road •Charlotte, INC 28217
Phone [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) PROPER PRESERVATIVES indicate
7 :' N
q y y "Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV) Received WITHIN HOLDING TIMES
Client Company Name: a 9 °r �wt'Y fv: 0/lt
cu
provisions and/or QC Requirements CUSTODY SEALS INTACT?-;_,
S",Jry
d
Report To/Contact Name: .4,_� y,
Invoice To VOLATILESrecd-W/OUT'HEQDSPA
E? 4
Reporting Address: PROPER CONTAINERS usetl?
Address:
1i
>>J
TEMP; Therm ID; I 4 Obs
Phone:70`®- "79- .WFax r es (No): 7-V- s % 5 ` 4.`5
Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENVSA�PLING
PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DoD
FL NC
EDD Type: PDF Excel �a Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days C]RushWork Mdust Be SG OTHER
d'o 1 Site Location Name: rT I Cr e L,+y Llj -
I NIA
.1 Samples received after 14:00 will be processed next business day.
e•�Kyy
Site Location Physical Address: i DC:I! Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
/ (SEE REVEFSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YiS_
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
®_
PRISM
CLIENT
DATE
COLLECTED
MILITARY
(SOIL,
WATER
PRESERVA-
�� REMARKS
LAB
*TYPE
SAMPLE DESCRIPTION
COLLECTED
HOURS
OR
SLUDGE)
NO.
SIZE
TIVES
///
1
ID NO.
SEE BELOW
�y �� K /
A
�I
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a�
.SA
1
�'
Sampler's Signature
Sampled By (Print Name) r9l t a d G
Affiliation
Upon relinquishing, this Chain o .Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Site ArriGal Tlme :
Relinq lied By: (Signature.) p
,i8•",1 ;a
ived By: (Sign r)
,�
Date
Military/Hours
Additional Comments:
Tn!y : Si nature)
R d By: (Signatur
D to
I
Site Departure Tilrie
Field Tach Fee
Relinquished By: ( gnature)
RecJvad For Pris Lahor tones By:
.-Dgte
Mileage:;
--
Method of Shipment: -NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
COC Group No..,
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
C
Q[- j
C)
❑ Fed Ex ❑ UPS ❑ Hand -delivered ism Field Service 0 Other
,� 0 1
•'
DES:❑
:
I❑
ILL
1
OTHER:
SC ❑ NC ❑ SC
I ❑❑R C ❑ SCTER
CATER:
Ll NC
O NC ❑SCE
®NRC ❑ SC
O NC ❑ SC
NCOF❑ SC
O❑ NC ❑ SC
❑
O
�fl ,l i d ,f
3DES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

CHAIN OF CUSTODY RECORD
�
r Full -Service Analytical &
7/
R I S M I
t"
�-
yEg Np NIA.
_ 6D
n Environmental Solutions PAGEOF _ QUOTE # TO ENSURE PROPER BILLING:0
Samples INTACT upon'arrlval?o,
i.neoanTORies, INC.
Project Name:
Recetvetl ON WET ICES
i r
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] • Pax: 7041525-0409 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER PRESERVATIVES indicate
"— N
7 y� to
�� •�� *Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
Client Company Name: ` a �p�fifi
Receroed'WI.THIN HOLDING TIMES
{'�^cu
provisions and/or QC Requirements
CUSTODY'SEALS INTACT?: `
Report To/Contact Name: fi o� v Se+B.y6+9 Invoice To:
Reporting Address:
VOLATILESirecd W/OUT HEADSPA
E� ` r
Address:
PROPER CONTAINERS used?'
TEM Therm Ohs
rverl; ` 0G /Corr, °C
Phone:70-?7 J-;3'4.3 `�' Fax Yes (No):70q_Si1e_ $e,.5 Purchase Order NoMilling Reference TO
BE FILLED IN BY CLIENT/S
PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoJIMPLING
FL NC
EDD Type: PDF_Epxxcel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushWork Must Be pproved
r Site Location Name: ai.(d h C:- bo w r p
SC OTHER
1 NIA
.c:;;I77c' Samples received after 14:00 will be processed next business day.
Site Location Physical Address: ®e r/ ra a wr i Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO-
._. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample
Iced Upon Collection: Y�S_
_
NO_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-`,�j
ANALYSIS REQUESTED
PRISM
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
RE ARKS
LAB
*TYPE
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
���'
ID NO.
A
A
l
QuarIef,1 si
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C
. hs
A
PA
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Sampler's Signature 1
/6
Sampled By (Print Name) L ®'e �/f
Affiliation
Upon relinquishing, this Chain of6ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
°
I
Site Arnval;Tlme
Relin uished By: (Signature)(B/f%y
R ived By: (Signs a
Date
MilitarylHours
Additional Comments
Rely ad B': (Si re) r ^�• f �:R
By: (Signature
o
ate
Sie Depure Tlme
Field Tech-.Feo
Rel uished By: (Signal e)•
Rece[Kq5 For Prism Looratories By:
Date
n
,•�
Mileage
• r•. --- -
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY.
n 1
Fed Ex ❑ UPS ❑ Hand -delivered IF11sm Field Service ❑ Other
S, DRINKINGSO WATER: SOLID DFCIS ILL OHE
(❑ SC E. OHER:
SEE REVERSE Foil
C ❑ NO❑ SC C ❑ SO i ❑ NO ❑ ❑❑ NR(❑ SC ❑ NRCLAC El ONO C❑TNC ❑ S
CONDITIONS
,ES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

smiBORATORIES�
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
FL NELAC Cert No. E87519
VA NELAC Cert No. 460211
Project: StaLime
Lab Submittal Date: 08/02/2016
Prism Work Order: 6080024
Case Narrative
08/09/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Vim• �-
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
C�
BH MB greater than one half of the RL, but the sample concentrations are greater than 1Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page I of 6

Full -Service . Analytical & Sample Receipt Summary
IS M I -Eunvironmental Solutions 08/09/2016
AGO -DRIES INC.
Prism Work Order: 6080024
lie ID Lab Sample ID Matrix Date Sampled Date Received
,.)ta-LlMe 60800214-01 Solid UOM13 08/02/ 16I/1
Samples were received in good condition at 1.4 degrees C unless otherwise noted.
-This%report should not be. reproduced, except in,its-,entirety, without themritten consent.of Prism Laboratories,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of

I`- I Full -Service Analytical &
J Environmental Solutions
ABO-RIE$ INC.
:sville, NC
imith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
08/09/2016
Project: StaLime Client Sample ID: Sta-Lime
Prism Sample ID: 6080024-01
Prism Work Order: 6080024
Sample Matrix: Solid Time Collected: 08/01/16 13:40
Time Submitted: 08/02/16 08:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 96.2 % by 0.100 0.100 1 *SM2540 G 8/2/16 15:26 JLB P61­10057
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 8/2/16 10:50 BMS P6H0058
Total Metals
Mercury
0.12
mg/kg dry
0.021
0.0012
1
*7471B
8/3/16 12:38
JAB
P6H0053
Arsenic
4.4
mg/kg dry
1.3
0.16
5
*6010D
8/4116 18:11
bgm
P61`10052
Cadmium
BRL
mg/kg dry
1.3
0.036
5
*6010D
8/4116 18:11
bgm
P61­10052
Copper
24
mg/kg dry
2.7
0.24
5
*6010D
8/4/16 18:11
bgm
P6H0052
Lead
11 BH
mg/kg dry
1.3
0.25
5
*6010D
8/4/16 18:11
bgm
P6H0052
Nickel
140
mg/kg dry
2.7
0.096
5
*6010D
814116 18:11
bgm
P6H0052
Selenium
5.0
mg/kg dry
2.7
0.63
5
*6010D
814116 18:11
bgm
P6H0052
Zinc
53
mg/kg dry
13
0.49
5
*6010D
814/16 18:11
bgm
1361­10052
This report should not be're roduced, exce t irrits entiret
y; without the written consent of.Rrism-Laboratories;.nc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/62976364 - Fax: [phone] Page 3 Of 6

%{ Full -Service Analytical &
r I Environmental Solutions
INC.
Level II QC Report
8/9/16
JC Project: StaLime Prism Work Order: 6080024
Time Submitted: 8/2/2016 8:30:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P61HI0052 - 3050B
Blank (P6H0052-BLK1)
Prepared & Analyzed: 08/03/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
BH
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6H0052-BS1)
Prepared &Analyzed: 08/03/16
Arsenic
23.9
0.25
mg/kg wet
25.00 96
80-120
Cadmium
24.4
0.25
mg/kg wet
25.00 98
80-120
Copper
26.7
0.50
mg/kg wet
25.00 107
80-120
Lead
24.6
0.25
mg/kg wet
25.00 98
80-120
Nickel
24.5
0.50
mg/kg wet
25.00 98
80-120
Selenium
23.0
0.50
mg/kg wet
25.00 92
80-120
Zinc
24.1
2.5
mg/kg wet
25.00 96
80-120
Batch P6H0053 - 7471 B
Blank (P6H0053-BLKI)
Prepared & Analyzed: 08/03/16
Mercury
BRL
0.020
mg/kg wet
LCS (P6H0053-BSI)
Prepared & Analyzed: 08/03/16
Mercury
0.468
0.020
mg/kg wet
0.4167 112
80-120
^ This report should not be reproduced; except in its entirety] without,the written consent of Prism Laboratories, Inc;,.-
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 6

Full -Service Analytical &
Environmental Solutions
-0-CRIES ING.
;sville, NC Project: Stal-ime
>mith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
8/9/16
Prism Work Order: 6080024
Time Submitted: 8/2/2016 8:30:OOAM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P6H0058 - NO PREP
Blank (P6H0058-BLK1)
Prepared & Analyzed: 08/02/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/rime
6080024-01 P61-10057
30 g
30 g
08/02/16 15:26
Prep Method: 3050B
Lab Number Batch
Initial
Final
Daterrime
6080024-01 P61-10052
1.95 g
50 mL
08/03/16 8:15
Prep Method: 7471E
Lab Number Batch
Initial
Final
Date/Time
6080024-01 P61-10053
0.59 g
50 mL
08/03/16 9:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories; Inc:;. ,.....;r..:•. _: , .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page eJ Of 6

CF�A�I� OF CUSTODY RECORD
S
Full-Service Analytical d /
r,w x Environmental Solutions PAGE OF QUOTE # TO ENSURE PROPER BILLING:
1.A[30RXr0R1ES, INC.
449 Springbrook Road • Charlotte, NC 25217 Project Name:
Phone [phone] • Fax: [phone]g Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
/ *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Cllent Company Name: ld. t r'l provisions and/or QC Requirements
Report To/Contact Name- Invoice To:
Reporting Address: Address:
CD
Samples IIVTACT upon arrival?
O
Received ON WET ICE?
7777
P
tD
PROPER:PRFSEP,77
VATIVCS'ii4 ated� ;
_
Q
Received..V1111HIN'HOLDINC'fIMES? ,
M
CUSTODY SEAL S INT/`C
?
VOLATiLES rec d W/OUT HEADSPACC'?
PROPER CONTAINERS used?
' {
TCMP, 7fjerm IQ:� :,, Observed
Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
EDD Type: PDF_Excel _Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ pre h Work Must Bepproved SC OTHER
NIA
Site Location Name:
Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_
Site Location Physical Address:
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I
TIME
MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED
(SOIL, PRESERVA- REMARKS LAB
TIVES
SAMPLE DESCRIPTION COLLECTED MILITARY
WATER OR *TYPE NO. SIZE ��
ID NO.
HOUR��sS,
SLUDGE) SEE BELOW
gg
14
�'`�Yf
8�i
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Sampler's Signature r+F
Sampled By (Print Name) 411 e;1 Affiliation
Upon relinquishing, this Chain of ustody is your authorization for Prlsm to proceed with th analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin shed B�]ure ,� _ ,�y
y, ( g
Re ei d B Si nature ate Military/Hours
Y t g ,.../ Additional Comments:
site Arrival Tlme
Relin a By: (Signature)
7
l
Ra ived By: (Signature) - Date
oils Departure,Tiine
Field Tech Fee
Relin Ished By: (Sig t re)
Receive�.F,or�rism Laboratories By: 4D
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
n ce,3 ❑„ n I IPq n H—ri-riasvereri VO'Jism Field Service ❑ Other
SOLID
NPD&�ERTYPECODES:
❑ NC ❑ SC I O NC ❑ SCTER. I DNC DRINKING❑ SCATER— O INC ❑ SCE I O NBC ❑ SC I ❑❑ NC L❑ SC ❑❑ NC F❑ SC ❑❑INC ❑ SC
A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

ism
ABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
NC Drinking Water Cart No. 37735
SC Certification No. 99012
FL NELAC Cart No. E87519
VA NELAC Cart No. 460211
Project: StaLime
Lab Submittal Date: 08/15/2016
Prism Work Order: 6080272
Case Narrative
08/25/2016 .
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR = [ Na ] / SQRT { ( [Ca] + [Mg]) / 21
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V L..
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without.the written consent of Prism Laboratories, Inc. .
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 12

Data Qualifiers Key Reference:
A Analysis was repeated with a similar result.
Aa Analyte is found in the blank at a concentration >1/2 RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1Ox the MB.
D RPD value outside of the control limits.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other.results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 Of 12

"GSMSample .Receipt Summary
Full -Service Analytical 8
Environmental Solutions 08/25/2016
LABoR o"IM INC.
Prism Work Order: 6080272
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Stalime 1
6080272-01
Solid
08/15/16
08/15/16
Stalime 2
6080272-02
Solid
08/15/16
08/15/16
Samples were received in good condition at 4.0 degrees C unless otherwise noted.
This_report should not be reproduced, except.in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 12

MFull-Service Analytical &
Environmental Solutions
ATOPIES INC.
Ile, NC
th
P.O. Box 1111
Statesville, NC 28687
Laboratory Report'
08/25/2016
Project: StaLime Client Sample ID: Stalime 1
Prism Sample ID: 6080272-01
Prism Work Order: 6080272
Sample Matrix: Solid Time Collected: 08/15/16 11:15
Time Submitted: 08/15/16 15:40
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateTme
ID
General Chemistry Parameters
Plant Available Nitrogen
1100
mg/kg
81
9.5
1
*Calculation
8123116 9:41
CLB
[CALC]
% Solids
92.8
% by
0.100
0.100
1
*SM2540 G
8/18116 15:45
JLB
P61­10334
Weight
Nitrate/Nitrite as N
210
mglkg dry
5.4
0.59
1
*SM4500-NO3 F
8/23/16 7:09
CLB
1361-10375
Phosphorus -Total
19
mg/kg dry
2.7
1.3
1
*SM4500-P F
8/24/16 8:25
CLB
P61`10394
Total Kjeldahl Nitrogen
3300
mg/kg dry
270
31
1
*351.2
8/23/16 9:41
CLB
P61­110321
Ammonia as N
39
mglkg dry
5.4
2.1
1
*SM4500-NH3 G
8119116 8:41
CLB
P61­110290
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
8/16/16 11:06
EGC
P61­10299
Total Metals
Mercury
0.15
mg/kg dry
0.023
0.0012
1
*7471B
8118/16 11:56
JAB
P61­110317
SAR Soil Preparation
Complete
g
1
*2-78-054
8/18/16 8:30
JAB
P61­10289
SAR Percent Moisture
84.0
% by
0.100
0.100
1
*2-78-054
8/18/16 9:35
JAB
1361-110371
Weight
Arsenic
5.5
mg/kg dry
1.4
0.17
5
*6010D
8/22116 23:07
bgm
P61­110286
Sodium Absorption Ratio
BRL
[blank]
0.30
0.016
1
*2-78-054
8/18/16 14:53
PJF
P61­10318
Cadmium
BRL
mg/kg dry
1.4
0.036
5
*6010D
8122116 23:07
bgm
P61­10286
Calcium
1100 B
mg/L
1.0
0.085
10
*6010D
8/18/16 14:53
PJF
P61­10318
Copper
39
mg/kg dry
2.7
0.25
5
*6010D
8/22/16 23:07
bgm
P61­110286
Lead
2.5
mg/kg dry
1.4
0.25
5
*6010D
8/22/16 23:07
bgm
P61­10286
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
8118/16 14:53
PJF
P61­10318
Nickel
17
mg/kg dry
2.7
0.098
5
*6010D
8/22116 23:07
bgm
P6H0286
Potassium
2000
mg/kg dry
68
2.5
5
*6010D
8122/16 23:07
bgm
P61­110286
Selenium
2.9
mg/kg dry
2.7
0.65
5
*6010D
8/22/16 23:07
bgm
P61­110286
Sodium
27 B
mg/L
5.0
0.074
10
*6010D
8/18/16 14:53
PJF
P61­110318
Sodium
490
mg/kg dry
82
2.7
5
*6010D
8/22/16 23:07
bgm
P6H0286
Zinc
38
mg/kg dry
14
0.49
5
*6010D
8122/16 23:07
bgm
P61i0286
This report should not be reproduced, except in its entirety,,. without the written consent of Prism Laboratories Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 12

I I^ n I Full -Service Analytical 8
' V' Environmental Solutions
LA90RATORIES ING
Laboratory Report
08/25/2016
City of Statesville, NC Project: StaLime Client Sample ID: Stalime 2
Attn: Andy Smith Prism Sample ID: 6080272-02
P.O. Box 1111 Prism Work Order: 6080272
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/15/16 11:15
Time Submitted: 08/15/16 15:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Datelrime ID
General Chemistry Parameters
Plant Available Nitrogen
1100
mglkg
81
9.5
1
*Calculation
8/23/16 9:41
CLB
[CALC]
% Solids
69.3
% by
0.100
0.100
1
*SM2540 G
8/18/16 15:45
JLB
P6H0334
Weight
Nitrate/Nitrite as N
140
mg/kg dry
7.2
0.79
1
*SM4500-NO3 F
8/23/16 7:09
CLB
P6H0375
Phosphorus -Total
BRL
mg/kg dry
3.6
1.7
1
*SM4500-P F
8/24/16 10:26
CLB
P61­10394
Total Kjeldahl Nitrogen
5000
mg/kg dry
360
41
1
*351.2
8/23116 9:41
CLB
P6H0321
Ammonia as N
120
mg/kg dry
7.2
2.8
1
*SM4500-NH3 G
8119/16 8:41
CLB
P61­110290
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
8/16/16 11:06
EGC
P6H0299
Total Metals
Mercury
0.20
mg/kg dry
0.030
0.0016
1
*7471B
8118116 12:01
JAB
P6H0317
SAR Soil Preparation
Complete
g
1
*2-78-054
8118/16 8:30
JAB
P61­10289
SAR Percent Moisture
68.0
% by
0.100
0.100
1
*2-78-054
8118/16 9:35
JAB
P6H0371
Weight
Arsenic
6.0
mg/kg dry
1.8
0.22
5
*6010D
8/18116 17:22
bgm
P6H0286
Sodium Absorption Ratio
BRL
. [blank]
0.30
0.016
1
*2-78-054
8/18/16 15:01
PJF
P61-10318
Cadmium
BRL
mg/kg dry
1.8
0.048
5
*6010D
8/18/16 17:22
bgm
P6110286
Calcium
1500 B
mg/L
1.0
0.085
10
*6010D
8/18/16 15:01
PJF
P6H0318
Copper
56
mg/kg dry
3.6
0.33
5
*6010D
8/18/16 17:22
bgm
P61HI0286
Lead
3.6
mg/kg dry
1.8
0.34
5
*6010D
8/18/16 17:22
bgm
P6H0286
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
8/18/16 15:01
PJF
P6H0318
Nickel
12
mg/kg dry
3.6
0.13
5
*6010D
8/18/16 17:22
bgm
P6H0286
Potassium
1800
mg/kg dry
90
3.2
5
*6010D
8/18/16 17:22
bgm
P6H0286
Selenium
8.1
mg/kg dry
3.6
0.86
5
*6010D
8/18116 17:22
bgm
P6H0286
Sodium
40 B
mg/L
5.0
0.074
10
*6010D
8118/16 15:01
PJF
P6H0318
Sodium
Soo
mg/kg dry
110
3.5
5
*6010D
8/18116 17:22
bgm
P6H0286
Zinc
47
mg/kg dry
18
0.65
5
*6010D
8/18/16 17:22
bgm
P6H0286
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 23224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 12

'M
i
ORIEE. IRO
e, NC
1
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
Total Metals - Quality Control
. Project: Stal-ime
Reporting
Analyte Result Limit Units
Level II QC Report
8/25/16
Prism Work Order: 6080272
Time Submitted: 8/15/2016 3:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P6HO286 - 3050B
Blank (P6H0286-BLK_1)
Prepared: 08/17/16 Analyzed: 08/18/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6H0286-BS1)
Prepared: 08/17/16 Analyzed: 08/18/16
Arsenic
25.5
0.25
mg/kg wet
25.00 102 80-120
Cadmium
25.3
0.25
mg/kg wet
25.00 101 80-120
Copper
26.9
0.50
mg/kg wet
25.00 108 80-120
Lead
25.0
0.25
mg/kg wet
25.00 100 80-120
Nickel
25.2
0.50
mg/kg wet
25.00 101 80-120
Potassium
530
12
mg/kg wet
500.0 106 80-120
Selenium
25.1
0.50
mg/kg wet
25.00 100 80-120
Sodium
531
15
mg/kg wet
500.0 106 80-120
Zinc
25.0
2.5
mg/kg wet
25.00 100 80-120
Matrix Spike (P6HO286-MS1)
Source: 6080272-01
Prepared: 08/17/16 Analyzed: 08/18/16
Arsenic
40.0
0.27
mg/kg dry
27.09 5.46 127 75-125
MC
Cadmium
20.4
0.27
mg/kg dry
27.09 0.139 75 75-125
Copper
79.4
0.54
mg/kg dry
27.09 39.1 149 75-125
MC
Lead
22.4
0.27
mg/kg dry,
27.09 , 2.52 73 75-125
MC
Nickel
35.2
0.54
mg/kg dry
27.09 17.1 67 75-125
MC
Potassium
3710
14
mg/kg dry
541.7 1950 325 75-125
MC
Selenium
32.3
0.54
mg/kg dry
27.09 2.86 109 75-125
Sodium
1470
16
mg/kg dry
541.7 487 182 75-125
MC
Zinc
69.3
2.7
mg/kg dry
27.09 37.5 117 75-125
This report should not be reproduced, except in.its,entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 Of 2

I n n Full -Service Analytical &
'v,' Environmental Solutions
4e0RATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control .
Analyte
Project: Stal-ime
Level II QC Report
8/25/16
Prism Work Order: 6080272
Time Submitted: 8/15/2016 3:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6HO286 - 3050B
Matrix Spike Dup (P6HO286-MSD1)
Source: 6080272-01
Prepared:
08/17/16
Analyzed:
08/18/16
Arsenic
32.9
1.3
mg/kg dry
26.55
5.46
103
75-125
19
20
Cadmium
22.8
1.3
mg/kg dry
26.55
0.139
85
75-125
11
20
Copper
65.9
2.7
mg/kg dry
26.55
39.1
101
75-125
18
20
Lead
26.4
1.3
mg/kg dry
26.55
2.52
90
75-125
16
20
Nickel
45.7
2.7
mg/kg dry
26.55
17.1
108
75-125
26
20
D, MC
Potassium
3120
66
mg/kg dry
531.1
1950
221
75-125
17
20
MC
Selenium
31.8
2.7
mg/kg dry
26.55
2.86
109
75-125
2
20
Sodium
1150
80
mg/kg dry
531.1
487
125
75-125
25
20
D, MC
Zinc
78.1
13
mg/kg dry
26.55
37.5
153
75-125
12
20
MC
Batch P6110289 - SAR 2-78-054
Blank (P6H0289-BLK1) Prepared: 08/17/16 Analyzed: 08/18/16
SAR Soil Preparation Complete g
Batch 136140317 - 7471 B
Blank (P6HO317-BLK1) Prepared & Analyzed: 08/18/16
Mercury BRL 0.020 mg/kg wet
LCS (P61-110317-13SI) Prepared &Analyzed: 08/18/16
Mercury 0.442 0.020 mg/kg wet 0.4167 106 80-120
Batch 136140318 - 301 OA
Blank (P6H0318-BLK1)
Prepared & Analyzed: 08/18/16
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium _
0.190 0.10 mg/L BH
Magnesium
BRL 0.10 mg/L
Sodium
3.03 0.50 mg/L Aa
This report should not be reproduced, except in its, entirety,. without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 7 Of 12

t n n FuH-Service Analytical &
'v' Environmental Solutions
%80RATORI8 INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
8/25/16
Prism Work Order: 6080272
Time Submitted: 8/15/2016 3:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6HO371 - NO PREP .
Blank (P6H0371-BLK1) Prepared & Analyzed: 08/18/16
SAR Percent Moisture BRL 0.100 % by Weight
Duplicate (P6HO371-DUP1) Source: 6080272-01 Prepared & Analyzed: 08/18/16
SAR Percent Moisture 82.3 0.100 % by Weight 84.0 2 200
This report should not be,,reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.. .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 Of 12

A Full -Service Analytical &
I v' I Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6H0290 - NO PREP
Level II QC Report
8125/16
Project: Stal-ime Prism Work Order: 6080272
Time Submitted: 8/15/2016 3:40:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P6H0290-BLK1) Prepared: 08/17/16 Analyzed: 08/19/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6H0290-BS1) _ Prepared: 08/17/16 Analyzed: 08/19/16
Ammonia as N 122 5.0 mg/kg wet 125.0 98 80-120
Matrix Spike (P6H0290-MS1) Source: 6080272-02 Prepared: 08/17/16 Analyzed_ 08/19/16
Ammonia as N 316 7.2 mglkg dry 1.80.3 119 109 80-120
Matrix Spike Dup (P6H0290-MSD1) Source: 6080272-02 Prepared: 08/17/16 Analyzed: 08/19/16 _
Ammonia as N 316 7.2 mg/kg dry 180.3 119 109 80-120 0.07 20
Batch P61HI0321 - 351.2
Blank (P6H0321-BLK1) Prepared: 08/18/16 Analyzed: 08/23/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6H0321-BSI) Prepared: 08/18/16 Analyzed: 08/23/16
Total Kjeldahl Nitrogen 499 100 mglkg wet 500.0 100 90-110
Batch P61HI0334 - Solids Dry Weight
Duplicate (P6H0334-DUP4) Source: 6080272-01 Prepared: 08/17/16 Analyzed 08/18/16 —
% Solids 93.7 0.10.0 % by Weight 92.8 1 20
Batch P61HI0375 - NO PREP
Blank (P6H0375-B_LK1) Prepared: 08/22/16 Analyzed:
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
.This report should not be reproduced,.except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 9 of 12

I I n I Full -Service Analytical &
'v' Environmental Solutions
LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6HO375 - NO PREP
Project: StaLime
Reporting
Result Limit Units
Level II. QC Repprt
8/25116
Prism Work Order: 6080272
Time Submitted: 8/15/2016 3:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P6H0375-BS1) Prepared: 08/22/16 Analyzed: 08/23/16
Nitrate/Nitrite as N 48.5 5.0 mg/kg wet 50.00 97 80-120
Matrix Spike (P6H0375-MS1) Source: 6080272-01 Prepared: 08/22/16 Analyzed: 08/23/16
Nitrate/Nitrite as N 165 5.4 mg/kg dry 53.90 208 NR 80-120 MI
Matrix Spike Dup (P6H0375-MSD1) Source: 6080272-01 Prepared: 08/22/16 Analyzed: 08/23/16
Nitrate/Nitrite as N 157 . 5.4 mg/kg dry 53.90 208 NR 80-120 5 20 MI
Batch kH0394 - SM4500-PB5
Blank (P6H0394-BLK1) Prepared: 08/22/16 Analyzed: 08/24/16
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P6H0394-BS1) Prepared: 08/22/16 Analyzed: 08/24/16
Phosphorus -Total 105 2.5 mg/kg wet 100.0 105 90-110
Matrix Spike (P6H0394-MS1) Source: 6080272-01 Prepared: 08/22/16 Analyzed: 08/24/16
Phosphorus -Total 33.9 2.7 mg/kg dry 107.8 18.9 14 80-120 A. MI
Matrix Spike Dup (P6H0394-MSD1) Source: 6080272-01 Prepared: 08/22/16 Analyzed: 08/24/16
Phosphorus -Total 33.4 2.7 mg/kg dry 107.8 18.9 14 80-120 1 20 A. MI
This report should not.be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spring brook Road -P.O. Box 240543 -Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 12

Level II QC Report
I`- n n Full -Service Analytical & 8/25/16
J' V' Environmental Solutions
4BORATORIES INC.
City of Statesville, NC Project: StaLime Prism Work Order: 6080272
Attn: Andy Smith Time Submitted: 8/15/2016 3:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD
Limit Notes
Batch P6H0299 "NO PREP
Blank (P6H0299-BLK1)
Prepared & Analyzed: 08/16/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Daterrime
6080272-01
P61-10321
0.05 g
25 mL
08/18/16 10:00
6080272-02
P61-10321
0.05 g
25 mL
08/18/16 10:00
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Date/rime
6080272-01
P61-10394
1 g
50 mL
08/22/16 14:45
6080272-02
P61-10394
1 g
50 mL
08/22/16 14:45
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
6080272-01
P61-10334
30 g
30 g
08/17/16 14:39
6080272-02
P61-10334
30 g
30 g
08/17/16 14:39
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6080272-01
P61-10318
50 mL
50 mL
08/18/16 10:04
6080272-01
P61-10318
50 mL
50 mL
08/18/16 10:04
6080272-02
P61-10318
50 mL
50 mL
08/18/16 10:04
6080272-02
P61-10318
50 mL
50 mL
08/18/16 10:04
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Datelrime
6080272-01
P61-10286
1.98 g
50 mL
08/17/16 8:25
6080272-02
P61-10286
2 g
50 mL
08/17/16 8:25
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/rime
6080272-01
P61-10317
0.57 g
50 mL
08/18116 9:30
6080272-02
P61-10317
0.58 g
50 mL
08/18/16 9:30
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
6080272-01
P61-10289
250 g
250 g
08/17/16 9:08
6080272-02
P61-10289
250 g
250 g
08/17/16 9:08
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364
- Fax: [phone]
Page 11 of 12

CHAIN OF CUSTODY RECORD
Full -Service Analytical &
Environmental Solutions PAGE_ OF _ QUOTE It TO ENSURE PROPER BILLING:
l T i v.. �,�''� LABORATORIES, INC.
Project Name:
449 Springbrook Road • Charlotte, NC 28217 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Phone [phone] Fax: [phone]
o E , r _ , , *Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
Client Company Name: pro-
-
-
io
�ns and/or QC Requirements
Report To/Contact Name: %��y >eyr Invoice To:
Reporting Address: Address:
'�tkV
ti."'°" -:. � N
YES/, NO
N/A
Samples IIVTACT upon arrival?
_ O
Received ON WET ICE? E
cV
PROPER PRESERVATIVES indicated?
_
Received WITHIN HOLDING TIMES?
m
CUSTODY SEALS INTACT?
y n-
VOLATILES iec;'d W/OUT HE;-\USPf\CF
PROPER CONTAINERS used?
Therm Observed:
°C 1 Corr:
TEMP: IDT91
Phone:Fax esL (No): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
A pork dust Be gC OTHER NIA
Site Location Name: ��rr G"' li/' ��'r� �_��i//�% Samples received after 14:00 will be processed next business day.
Site Location Physical Address: i, �0 /°s' �//✓9,�} Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_
,,✓✓/—/'�' (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p p
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- / REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE TIVES ID NO.
HOURS SLUDGE) SEE BELOW NO, SIZE
/ f
/
21
Sampler's Signature
Sampled By (Print Name)
Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to, the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
B nature Dal Military/Hours
Relinquishe�l3y (Signal Race .._.- r•Si (s � Additional Comments: elfin
quishe'Yl"B�: (Signature) �,. Received By: (Signature) Date
SiteArn'�al TtTime:
�._,._.,�..,,.._��..._.�,.._
I Sire Departure 7irne.
Field Tech Fee;
Religqujshed By: (Signature)
Received For rism Laboratories By: _,,,.•-""`
Date �, I�.
r' i +�
IVlilcage:
' e od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WIT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY
SAMPLES ARE NOT JCEPTED AND VERIFIED AGAINST CM UNTIL RECEIVED AT THE LABORATORY.
G� n I Ivs ❑ Hand�tnlivared Prism Field Service ❑ Other
COC Group No.
(� (�'•� f
❑ NC ®SC [IOU GROUNDWATER: El NC DRINKINGWATER: C LI NC ❑LID SCE ❑ NRCA❑ SC El NC L❑ SC ❑ NC LANDFILL❑ SCI NC ❑ SC
❑ I ❑ —.--- ---- I ❑ ❑ ❑ ElO
&E CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

S Full -Service Analytical &
Environmental Solutions
30RATORIES. INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
FL NELAC Cert No. E87519
VA NELAC Cert No. 460211
Project: StaLime (60 Day/7 Fecal)
Lab Submittal Date: 08/29/2016
Prism Work Order: 6080503
Case Narrative
09/07/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR=[Na]/SQRT{([Ca]+[Mg])/2}
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a-. (Rrv--
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
- ' "This report should not be reprdducetl; ezcepfin"its' entirety; without the written consent of Prism laboratories; Inca
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 16

M Full -Service Analytical &
Environmental Solutions
RIM INC
Sample Receipt Summary
09/07/2016
Prism Work Order: 6080503
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
StaLime (and Fecal 1)
6080503-01
Solid
08/29/16
08/29/16
Fecal #2
6080503-02
Solid
08/29/16
08/29/16
Fecal #3
6080503-03
Solid
08/29/16
08/29/16
Fecal #4
6080503-04
Solid
08/29/16
08/29/16
Fecal #5
6080503-05
Solid
08/29/16
08/29/16
Fecal #6
6080503-06
Solid
08/29/16
08/29/16
Fecal #7
6080503-07
Solid
08/29/16
08/29/16
Samples were received in good condition at 4.5 degrees C unless otherwise noted.
" `This report should not be reproduced, -except in -its entirety; without the written consent of Prism Laboratories; Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 Of 16

R I S M Laboratory Report
I
Full-Service Analytical &
71; Environmental Solutions 09/07/2016
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: Stal-ime (and Fecal 1)
Attn: Andy Smith Prism Sample ID: 6080503-01
P.O. Box 1111 Prism Work Order: 6080503
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
Plant Available Nitrogen
1100
mg/kg
380
44
5
*Calculation
917/16 8:13
CLB
[CALC]
% Solids
62.4
% by
0.100
0.100
1
*SM2540 G
8/31/16 16:44
JLB
P610012
Weight
Nitrate/Nitrite as N
22
mg/kg dry
8.0
0.88
1
*SM4500-NO3 F
9/2/16 9:55
CLB
P610027
Phosphorus -Total
5800
mg/kg dry
80
38
20
*SM4500-P F
912/16 7:08
CLB
P610025
Total Kjeldahl Nitrogen
6900
mg/kg dry
2000
230
5
*351.2
9/6/16 9:08
CLB
P61-10538
Ammonia as N
170
mg/kg dry
8.0
3.1
1
*SM4500-NH3 G
917/16 8:13
CLB
P61-110513
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
8/30/16 10:00
BMS
P61­10536
Total Metals
Mercury
SAR Soil Preparation
SAR Percent Moisture
Arsenic
Sodium Absorption Ratio
Cadmium
Calcium
Copper
Lead
Magnesium
Nickel.
Selenium
Sodium
Zinc
0.25
Complete
76.0
BRL
0.51
BRL
2800
61
4.5
BRL
9.6
12
99
100
mg/kg dry
0.033
0.0018 1
g
1
% by
0.100
0.100 1
Weight
mg/kg dry
3.9
0.48 10
[blank]
0.30
0.016 1
mg/kg dry
3.9
0.11 10
mg/L
1.0
0.085 10
mg/kg dry
7.9
0.71 10
mg/kg dry
3.9
0.73 10
mg/L
1.0
0.0070 10
mg/kg dry
7.9
0.28 10
mg/kg dry
7.9
1.9 10
mg/L
5.0
0.074 10
mg/kg dry
39
1.4 10
*7471B
911/16 12:56
JAB
P61­110529
*2-78-054
9/1/16 7:20
JAB
P610011
*2-78-054
916/16 14:10
JAB
P610072
*6010D
9/2/16 2:52
bgm
P610005
*2-78-054
9/2116 0:26
bgm
P610013
*6010D
9/2/16 2:52
bgm
P610005
*6010D
9/2/16 0:26
bgm
P610013
*6010D
912116 2:52
bgm
P610005
*6010D
9/2/16 2:52
bgm
P610005
*6010D
9/2/16 0:26
bgm
P610013
*6010D
9/2/16 2:52
bgm
P610005
*6010D
9/2/16 2:52
bgm
P610005
*6010D
9/2116 0:26
bgm
P610013
*6010D
912/16 2:52
bgm
P610005
'This re ort'should not be'fe 'roduced,'exce f'in'its entirewithout_ p••• p p p ty, t a written consent°o Prism nc. • - - - -� -,.•3P.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1.800/629-6364 -Fax, 704/525-0409 Page 3 Of 16

Laboratory Report
=� I S FuService Analytical 8
Envivironmental Solutions 09/07/2016
mm w.•+.. I BORA QRIE$ INC.
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: Fecal #2
Attn: Andy Smith Prism Sample ID: 6080503-02
P.O. Box 1111 Prism Work Order: 6080503
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Solids 61.8 % by 0.100 0.100 1 `SM2540 G 8/31116 16:44 JLB P610012
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 'SM9221 E 8/30/16 10:00 BMS P61-10536
This "report should'not be reproduced;" except in its entirety,. without the written consent of Prism Laboratories, Inc:
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1.800/529-6364 - Fax: [phone] Page 4 Of 16

Full -Service Analytical 8 Laboratory Report
It Environmental Solutions 09/07/2016
rORIE$ INC.
le, NC Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #3
h Prism Sample ID: 6080503-03
P.O. Box 1111 Prism Work Order: 6080503
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 65.1 % by 0.100 0.100 1 *SM2540 G 8/31116 16:44 JLB P610012
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3 1 *SM9221 E 8/30/16 10:00 BMS P61­10536
- "'this -'report should not be reproduced;except in ds entirety; without the written cohs'erit of Prism Laboratories, Inc."
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 16

n Full -Service Analytical &
Environmental Solutions
)RIM ING
NC
i
F.U. box llll
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/07/2016
Client Sample ID: Fecal #4
Prism Sample ID: 6080503-04
Prism Work Order: 6080503
Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
% Solids 61.8
% by
0.100
0.100 1 'SM2540 G 8/31/16 16:44 JLB
P610012
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 8/30/16 10:00 BMS
P61­10536
ieport'should'hot'be'reproduced; except in- its -entirety,'without the writteh`consent of Prism -Laboratories, Inc. '�� ° -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 16

M I Full -se -ice Analytical &
Environmental Solutions
e, NC
h
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/07/2016
Client Sample ID: Fecal #5
Prism Sample ID: 6080503-05
Prism Work Order: 6080503
Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
% Solids 62.3 % by 0.100 0.100 1 *SM2540 G 8131116 16:44 JLB P610012
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 *SM9221 E 8/30116 10:00 BMS P61­10536
­Thi�-repbffshduld"not 6e"rb0r70_dubed-,`bzcdpt in'its'ehtitEity',Iwithoiit'the written -consent of Prism Laboratories; Inc.­-­
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 16

n n Full -Service Analytical &
'v I I Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
09/07/2016
Client Sample ID: Fecal #6
Prism Sample ID: 6080503-06
Prism Work Order: 6080503
Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Dateffime
ID
General Chemistry Parameters
Solids 61.0
% by
0.100
0.100 1
•SM2540 G 8131/16 16:44 JLB
P610012
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 8/30/16 10:00 BMS
P6H0536'
"This"re' , oPt'should notbere roduced,exce tin its entire - p p p ty;'withoutthe written consent of Prism Laboratories, Inc. ----­- • .�• • - -• . •- - - -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 Of 16

Laboratory Report
A Full -Service Analytical S
I Environmental Solutions 09/07/2016
ING
IC Project: StaLime (60 Day/7 Fecal) Client Sample ID: Fecal #7
Prism Sample ID: 6080503-07
1-.U. tsox I 1 1 1 Prism Work Order: 6080503
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/29/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
%Solids 62.5 % by 0.100 0.100 1 'SM2540 G 8/31/16 16:44 JLB P610012
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3 1 'SM9221 E 8130/16 10:00 BMS P61­10536
" This'rep''oif should not'be'reproduced;'except in its•entirety; without'the-written consent of Prism Laboratories, lnc:.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 Of 16

1 I Full -Service Analytical &
Environmental Solutions
IAeO..0A s.'NG
Level II QC Report
917/16
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 6080503
Attn: Andy Smith Time Submitted: 8/29/2016 3:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6HO529 - 7471 B
Blank (P6HO529-BLK_1_) _ Prepared & Analyzed: 09/01/16 _
Mercury BRL 0.020 mg/kg wet
LCS (P6H0529-BS1) Prepared & Analyzed: 09/01/16
Mercury 0.474 0.020 mg/kg wet 0.4167 114 80-120
Batch P610005 - 3050B
Blank (P610005-BLK1) _
_
Prepared: 09/01/16 Analyzed: 09/02/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P610005-BS1)
--------------------
-
Prepared: 09/01/16 Analyzed: 09/02/16
-------- -- -- -------
Arsenic
23.9
0.25
mg/kg wet
25.00 96 80-120
Cadmium
24.6
0.25
mg/kg wet
25.00 98 80-120
Copper
24.9
0.50
mg/kg wet
25.00 100 80-120
Lead
24.2
0.25
mg/kg wet
25.00 97 80-120
Nickel
23.9
0.50
mg/kg wet
25.00 96 80-120
Selenium
23.8
0.50
mg/kg wet
25.00 95 80-120
Zinc
23.5
2.5
mg/kg wet
25.00 94 80-120
Matrix Spike (P610005-MS1)
Source: 6080503-01
Prepared: 09/01/16 Analyzed: 09/02/16
Arsenic
42.6
3.9
mg/kg dry
39.09 2.27 103 75-125
Cadmium
36.2
3.9
mg/kg dry
39.09 0.441 92 75-125
Copper
106
7.8
mg/kg dry
39.09 61.2 114 75-125
Lead
40.9
3.9
mg/kg dry
39.09 4.46 93 75-125
Nickel
45.2
7.8
mg/kg dry
39.09 9.64 91 75-125
Selenium
49.4
7.8
mg/kg dry
39.09 11.6 97 75-125
Zinc
138
39
mg/kg dry
39.09 103 90 75-125
This'rep'ort should not be -reproduced; except in its -entirety, without.the written consent of Prism.Laboratories Inc .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529.6364 - Fax: [phone] Page 10 Of 6

p'�\,/q' _ Level II QC Report
I I S' V 1 Fuil-Service Analytical & 9/7/16
Environmental Solutions
U 80RATOHI INF
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 6080503
Attn: Andy Smith Time Submitted: 8/29/2016 3:10:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P610005 - 3050B
Matrix Spike Dup(P610005-MSD1)
Source: 6080503-01
Prepared: 09/01/16 Analyzed: 09/02/16
Arsenic
41.4
4.0
mg/kg dry
39.86
2.27
98
75-125
3
20
Cadmium
35.6
4.0
mg/kg dry
39.86
0.441
88
75-125
2
20
Copper
99.6
8.0
mg/kg dry
39.86
61.2
96
75-125
6
20
Lead
39.7
4.0
mg/kg dry
39.86
4.46
88
75-125
3
20
Nickel
44.1
8.0
mg/kg dry
39.86
9.64
86
75-125
3
20
Selenium
49.8
8.0
mg/kg dry
39.86
11.6
96
75-125
1
20
Zinc
137
40
mg/kg dry
39.86
103
87
75-125
0.3
20
Batch P610011 - SAR 2-78-054
Blank (P610011-BLK1) Prepared: 08/31/16 Analyzed: 09/01/16
SAR Soil Preparation Complete g
Batch P610013 - 3010A
Blank (P610013-BLK1)
Prepared: 09/01/16 Analyzed: 09/02/16
Sodium Absorption Ratio
BRL
3.0 [blank]
Calcium
BRL
1.0 mg/L BH
Magnesium
BRL
1.0 mg/L
Sodium
BRL
5.0 mg/L BH
Batch P610072 - NO PREP
Blank (P610072-BLK1)
Prepared: 09/01/16 Analyzed: 09/06/16
SAR Percent Moisture
BRL
0.100 % by Weight
This' report should not be reproduced; s xcept in' its entirety.'withoutlthe written consent of Prism Laboratories jnc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 16

Full -Service Analytical &
Environmental Solutions
Project: Stal-ime (60 Day/7 Fecal)
I— — I I I I
Statesville, NC 28687
Total Metals - Quality Control
Level 11 QC Report
9/7/16
Prism Work Order: 6080503
Time Submitted: 8/29/2016 3:10:00PIVI
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P610072 - NO PREP
Duplicate (P610072-DUPI) Source: 6080503-01 Prepared: 09/01/16 Analyzed: 0 9/06/16 — -----
SAR Percent Moisture 71.0 0.100 %byWeight 76.0 7 200
This'�6p'orfsKdbld'h6i'bi�!tepr6d6biid,'6kd6otih if§6rifirbty,-without the written consent of Prism Laboratories, -Inc.-- -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] .Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 12 Of 16

I I S^ A I Full -Service Analytical &
1 V' Environmental Solutions
ueoR RIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
P61`110513 - NO PREP
Project: StaLime (60 Day/7 Fecal)
Level 11 QC Report
917/16
Prism Work Order: 6080503
Time Submitted: 8/29/2016 3:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P6H0513-BLK1) Prepared: 09/06/16 Analyzed: 09/07/16
Ammonia as N BRL 5.0 mg/kg wet
LCS (P6H0513-BS1) Prepared: 09/06/16 Analyzed: 09/07/16
Ammonia as N
Batch P6HO538 - 351.2
120 5.0 mg/kg wet 125.0 96 80-120
Blank (P6H0538-BLK7) _ Prepared: 08/31/16 Analyzed: 09/06/16 _
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LC_S (P6H0538-BS1) Prepared: 08/31/16 Analyzed: 09/06/16
Total Kjeldahl Nitrogen 468 100 mg/kg wet 500.0 94 90-110
Matrix Spike (P6H0538-MS1) Source: 6080503-01 Prepared: 08/31/16 Analyzed: 09/06/16
Total Kjeldahl Nitrogen 14300 2000 mg/kg dry 8013 5930 105 90-110
Batch P610012 - Solids Dry Weight
Duplicate (P610012-DUP4) Source: 6080503-01 Prepared & Analyzed: 08/31/16
% Solids 62.8 0.100 % by Weight 62.4 0.6 20
Batch P610025 - SM4500-PB5
Blank (P610025-13LK1) _ Prepared & Analyzed: 09/02/16
Phosphorus -Total BRL 2.5 mg/kg wet
'This°repoit'sh'ouldhot be'reproduced;'except in its entirety;'wdtiout the written consent of Prism, Laboratories,, Inc. a- *• -- _- • • � - - °•=• - - - -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 16

3 1 S n n I Full -Service Analytical
' V' Environmental Solutions
s ueonnroaiEs we
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P610025 - SM4500-PBS
Project:'StaLime (60 Day/7 Fecal)
Level II QC Report
9/7/16
Prism Work Order: 6080503
Time Submitted: 8/29/2016 3:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P610025-BSI) Prepared & Analyzed: 09/02/16
Phosphorus -Total 104 2.5 mg/kg wet 100.0 104 90-110
Matrix Spike (P610025-MS1) Source: 6080503-01 Prepared &Analyzed: 09/02/16
Phosphorus -Total 5150 80 mg/kg dry 160.3 5770 NR 80-120 MC
Matrix Spike Dup (P610025-MSD1) Source: 6030503-01 Prepared & Analyzed: 09/02/16
Phosphorus -Total 5170 80 mg/kg dry 160.3 5770 NR 80-120 0.3 20 MC
Batch P610027 - NO PREP
Blank (P610027-BLK1
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
& Analyzed: 09/02/16
LCS (P610027-BSI) Prepared &Analyzed: 09/02/16
Nitrate/Nitrite as N 47.9 5.0 mg/kg wet 50.00 96 80-120
Matrix Spike (P610027-MS1) _ Source: 6080503-01 Prepared &Analyzed_09/02/16
Nitrate/Nitrite as N 96.1 8.0 mg/kg dry 80.13 22.0 93 80-120
Matrix Spike Dup (P610027-MSD1) Source: 6080503-01 Prepared & Analyzed: 09/02/16
Nitrate/Nitrite as N 94.9 8.0 mg/kg dry 80.13 22.0 91 80-120 1 20
This report Should 'not `be reproduced,^ exceptin'its entirety; without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: l-8001529-6364- Fax: [phone] Page 14of 16

F-Pethod:
Sample Extraction Data
351.2
Lab Number Batch
Initial Final Daterrime
6080503-01 P61­10538
0.05 g 25 mL 08/31/16 10:25
Prep Method: SM4500-PBS
Lab Number Batch
Initial Final Daterrime
6080503-01 P610025 1 g 50 mL 09/02/16 6:26
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/rime
6080503-01
P610012
30
g
30 g
08/31/16 16:44
6080503-02
P610012
30
g
30 g
08/31/16 16:44
6080503-03
P610012
30
g
30 g
08/31/16 16:44
6080503-04
P610012
30
g
30 g
08/31/16 16:44
6080503-05
P610012
30
g
30 g
08/31/16 16:44
6080503-06
P610012
30
g
30 g
08/31/16 16:44
6080503-07
P610012
30
g
30 g
08/31/16 16:44
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6080503-01
P610013
50
mL
50 mL
09/01/16 11:31
6080503-01
P610013
50
mL
50 mL
09/01/16 11:31
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/rime
6080503-01 P610005 2.03 g 50 mL 09/01/16 8:55
Prep Method: 7471B
Lab Number Batch Initial Final Date/rime
6080503-01 P61­10529 0.58 g 50 mL 09/01/16 9:30
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final - Daterrime
6080503-01 P610011 250 g 250 g 08/31/16 7:20
This'report'should not'be`reproduced' except in'its'entirety; without -the written consent of Prism Laboratories, Inc. -
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364.- Fax: [phone] Page 15 Of 6

CHAIN OF CU9700Y RECORD
,. :.
CID
Ism
Full-Service Analytical &
I Environmental Solutions
PAGE_ Dip _ QUVFE g To LtdSC9T_E prf ,31 ER IEILI.IIJG:
YEvO N/A
Samples INTACT upon arrival? _ _ - ___
r-
p
CD
` AnonaTomes. wc'
project Name:
Project: es NO
) ( )
Received ON WET ICE? — ..
PROPER PRESERVATIVES indicated?CD
449 Springbrook Road • Charlotte, NC 28217
2
Phone [phone] Fax: [phone]
UST
Short Hold Analysis: (Yes) (No) 1
'Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV)
Received WITI IIN'I HOLDING TIMES? --- j`
's
CY
,a
Client Company Name: O e � � j �� P�
provisions and/or QC Requirements
CUSTODY SEALS INTACT? _ -
VOLATILES reed WIOUT HEADSPACE?
d
p �t� o g,�
Report TO/Contact Name: reJl B
Invoice To:
eROPER CONTAq.� RS used?
Reporting Address:,.
Rep g
Address:
TEMP: Therm ID:-J._� Ob ervcd:°C! Gorr. r'
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Order No./Billing Reference
Phone:704-IMP- 4390 Fax C es (No):70-147911655purchase
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
RushBe
Certification: NELAC DOD FL. NC
EDD Type: PDF_Ex_cel_,Othe�re
( e^C.. Mfg&L
"Working Days" ❑ 6-9 Days ❑ Standard 1 C days ❑ re Apprrovedust
Samples received after 14:00 will be processed next business day.
SC OTHER N/A
Water Chlorinated: YES NO
Site Location Name
Turnaround time is based on business days, excluding weekends and holidays.
—
Site Location Physical Address: ��c �� Fit r r"a
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
CLIENT)
Sample Iced Upon Collection: YES_ NO
l
��+ACmS Ili d�� iJ
RENDERED BY PRISM LABORATORIES, INC. TO
SAMPLE CONTAINER
pRESERVA-
ANALYSIS /
REMARKS
PRISM
LAB
TIME
MATRIX
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
{SOIL,
WATER OR
•TYPE
NO.
SIZE
TIVES
rU�
(Lay
��
ID NO.
HOURS
SLUDGE)
SEE BELOW
^
IN
C� EL
i�b .III,
°S
silty r A rs ('
Ngo
r
S t;
Sampler's SignatureSampled By (Print Name)
Upon relinquishing, this Chain of Custody is your authorization for Pri m to proceed with the analyse
submitted in writing to the Prism Project Manager. There will be charg for any changes afterpn lys
Relin hed By: (Signature) Received 8y:.(Signature) ,, t
,­,
Relinq ed By: (signature) Received y: igneture
Relinquished By: (Signature) Received For Prism Lab�rato s By:
.71
,A I Affiliation
as requested above. Any changes must be
Is have been initialized.
�_�
SAO
otanipmem: nuia;tluu�.,,..��� _..----------- I
SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY.
r'
Ex ❑ UPS ❑ Hand -delivered Prism Field Service ❑ Other
S. SC . ❑ NC Ell SC ❑ NC ❑ SC El
DRINKING
I �KIN❑G WATER: I ❑ NC ❑ SCWATE I O❑ NRC ❑ SC I EENC L❑ SC Q NC A: CIRGA F❑ SC I LI INC ❑ SC
❑ I ❑ ❑ ❑—
PE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
:SEE.REVERSE FOR
TERMS & CONDITIONS

I M
Full -Service Analytical &
Environmental Solutions
ABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
NC Drinking Water Cart No. 37735
SC Certification No. 99012
Project: Sludge (Hazardous Testing)
Project No.: 4th Creek Stalime
Lab Submittal Date: 08/29/2016
Prism Work Order: 6080505
Case Narrative
09/15/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference'for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Reactivity analysis was subcontracted to GCAL. Herbicide analysis was subcontracted to AES.
Laboratory reports are attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
CCV CCV result is above the control limits. Analyte not detected in the sample. No further. action. taken...
D RPD value outside of the control limits.
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
-This report notbe•re roduced.,exce tin its p p P entirety; without the written consent of Prism Laboratories, Inc; r+ '•: • :• -•• -:�: • . .- •-- - .: - .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page Of 22

4 R I S M Sample Receipt Summary
Full -Service Analytical &
x F< Environmental Solutions 09/15/2016
''"LABORATORIES ING
Prism Work Order: 6080505
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime Hazardous Waste 6080505-01 Solid 08/26/16 08/29/16
Samples were received in good condition at 4.5 degrees C unless otherwise noted.
This report should not be re roduced; exce t in its'entire p p p ty, without-the•written consent of Prism' Laboratories, Inc: : •«- � -v= � _- -• --- •-
449 Springbrook Road- P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Pag@ 2 Of 22

Laboratory Report
'. Full -Service Analytical 8
ISM I Environmental Solutions 09/15/2016
---..e..3. LABOPATOHI --
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: Sta-Lime Hazardous Waste
Attn: Andy Smith Prism Sample ID: 6080505-01
P.O. Box 1111 Project NO.: 4th Creek Stalime Prism Work Order: 6080505
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/26/16 11:30
Time Submitted: 08/29/16 15:10
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
69.2
% by
0.100
0.100
1
*SM2540 G
9/1116 16:09
JLB
P610033
Weight
Corrosivity-pH
5.9
pH Units
1
`9045D
8/30/16 13:54
BMS
P6H0521
Ignitability
Pass
mm/sec
0.10
1
`1030
8130116 13:00
BMS
P61­10519
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
9/1/16 7:20
JAB
P61­10541
TCLP Extraction
Complete
N/A
1
*1311 ZHE
9/8/16 9:30
ANG
P610098
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
'7470A
912116 13:49
JAB
P610032
Arsenic
BRL
mg/L
0.050
0.0035
1
'6010D
9/2/16 0:02
bgm
P610010
Barium
BRL
mg/L
5.0
0.0035
1
'6010D
9/2/16 0:02
bgm
P610010
Cadmium
BRL
mg/L
0.025
0.00050
1
'6010D
9/2/16 0:02
bgm
P610010
Chromium
BRL
mg/L
0.25
0.0030
1
*6010D
9/2/16 0:02
bgm
P610010
Lead
0.69
mg/L
0.050
0.0065
1
'6010D
9/2116 0:02
bgm
P610010
Selenium
0.14
mg/L
0.10
0.016
1
'6010D
912/16 0:02
bgm
P610010
Silver
BRL
mg/L
0.25
0.0010
1
'6010D
9/2/16 0:02
bgm
P610010
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRLCCV
mg/L
0.0025
0.000094
1
*8081B
918/16 13:40
JMC
P610066
Dieldrin
BRLCCV
mg/L
0.00050
0.000022
1
*8081B
9/8/16 13:40
JMC
P610066
Endrin
BRLCCV
mg/L
0.00050
0.000020
1
*80818
9/8/16 13:40
JMC
P610066
gamma-BHC
BRL
mg/L
0.00050
0.000013
1
*8081B
918/16 13:40
JMC
P610066
- H'eptachlor
BRL
mg/L
0.00050--
0.000015
1
*8081B
9/8/16 13:40
JMC
P610066
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000018
1
'8081B
9/8/16 13:40
JMC
P610066
Methoxychlor
BRL
mg/L
0.00050
0.000033
1
*8081B
9/8/16 13:40
JMC
P610066
Toxaphene
BRL
mg/L
0.025
0.00032
1
'8081B
918/16 13:40
JMC
P610066
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
52
%
13-186
Tetrachloro-m-xylene
70
%
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
'8270D
918/16 15:53
JMV
P610057
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
'8270D
9/8116 15:53
JMV
P610057
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
'8270D
9/8/16 15:53
JMV
P610057
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
'8270D
9/8/16 15:53
JMV
P610057
3/4-Methylphenol
BRL
mg/L
0.050
0.0015
1
'8270D
9/8116 15:53
JMV
P610057
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
'8270D
9/8/16 15:53
JMV
P610057
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
'8270D
9/8/16 15:53
JMV
P610057
Hexachloroethane
BRL
mg/L
0.050
0.0017
1
'8270D
9/8/16 15:53
JMV
P610057
Nitrobenzene
BRL
mg/L
0.050
0.0026
1
'8270D
9/8/16 15:53
JMV
P610057
Pentachlorophenol
BRL
mg/L
0.25
0.0012
1
'8270D
9/8116 15:53
JMV
P610057
This report should not be reproduced, except in its entirety, without the written consent of Prism, Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 22

Full -Service Analytical &
Environmental Solutions
INC.
Laboratory Report
09/15/2016
1C Project: Sludge (Hazardous Testing) Client Sample ID: Sta-Lime Hazardous waste
Prism Sample ID: 6080505-01
Project No.: 4th Creek Stalime Prism Work Order: 6080505
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/26/16 11:30
Time Submitted: 08/29/16 15:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pyridine
BRL
mg/L
0.25 0.0010
1
*8270D
9/8116 15:53
JMV
P610057
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
91 %
43-140
2-Fluorobiphenyl
79 %
44-119
2-Fluorophenol
47 %
19-119
Nitrobenzene-d5
74 %
44-120
Phenol-d5
35 %
11-52
Terphenyl-d14
75 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.000083
1
'8260B
919/16
6:03
CGP
P610118
1,2-Dichloroethane
BRL
mg/L
0.025 0.000066
1
'8260B
9/9/16
6:03
CGP
P610118
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.000050
1
'8260B
9/9/16
6:03
CGP
P610118
Benzene
BRL
mg/L
0.025 0.000048
1
'8260B
9/9/16
6:03
CGP
P610118
Carbon Tetrachloride
BRL
mg/L
0.025 0.00011
1
'8260B
9/9/16
6:03
CGP
P610118
Chlorobenzene
BRL
mg/L
5.0 0.000062
1
'8260B
919/16
6:03
CGP
P610118
Chloroform
BRL
mg/L
0.30 0.000076
1
'8260B
9/9/16
6:03
CGP
P610118
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.00024
1
`8260B
9/9/16
6:03
CGP
P610118
Tetrachloroethylene
BRL
mg/L
0.035 0.000098
1
'8260B
9/9/16
6:03
CGP
P610118
Trichloroethylene
BRL
mg/L
0.025 0.000078
1
'8260B
9/9/16
6:03
CGP
P610118
Vinyl chloride
BRL
mg/L
0.010 0.000097
1
'8260B
919/16
6:03
CGP
P610118
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
87 %
80-124
Dibromofluoromethane
68 %
75-129
SR
Toluene-d8
86 %
77-123
This report should not'be reproduced, except in its entirety, without the written consent of Prism Laboratories; Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] rage 4 Of 22

Sample Extraction Data
rep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/rime
6080505-01
P610033
30 g
30 g
09/01/16 16:09
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/rime
6080505-01
P610098
25 g
500 mL
09/07/16 16:15
6080505-01
P61­10541
100 g
2000 mL
O8131/16 14:20
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/rime
6080505-01
P610010
10 mL
50 mL
09/01/16 10:15
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
6080505-01
P610032
20 mL
30 mL
09/02/16 8:45
Prep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/rime
6080505-01
P610066
200 mL
10 mL
09/06/16 12:50
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Daterrime
6080505-01
P610057
200 mL
1 mL
09/06/16 9:40
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Daterrime
6080505-01
P610118
10 mL
10 mL
09/08/16 15:40
Subcontracted Analyses
--The following analyses were subcontracted to Analytical Environmental Services ,..Inc.
Lab Number
Analysis
6080505-01
Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast
Analytical Labs, Inc.
Lab Number
Analysis
6080505-01
Reactivity, Cyanide (Sub)
6080505-01
Reactivity, Sulfide (Sub)
This report should not be reproduced, *except in its entirety, without the written consent of Prism Laboratories; Inc: -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 0f 22

+f Full -Service Analytical U
RSM � Environmental Solutions
.,,,�L9BORATOPIES n4C.
449 Springbrook Road • Charlotte, NC 282.17
Phone [phone] Fax: [phone]
Client Company Name: `-tl'i Of9OA I 1129V- ill
Report To/Contact Name: /4 NY S.-n a 4 h
Reporting Address:
CHAIN OF CUSTODY RECORD
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
`Please ATTACH any project specific reporting (QC LEVEL 111 III M
provisions and/or QC Requirements
Invoice To:
Address:
Samples INT4CT.'upon arrival?
Received ON WET ICE? ,.
PROPER PRESERVATNCS: indidated?
Received WITHIN HOLDING,TiMES?
CUSTODY SEALS INTACT,?,
VOLATILES read W/OUT HEADSFACE? ,
PROPER CONTAINERS .0sed?,-
TEMP: Therm ID: Ili it L Observed:
°C 1 Corr;_�],_7 °C
Phone: 70Y-979*-'3g3,T Fax es (No):'101-`3'1`s'-946 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days El3 Days ❑ 4 Days El Days
Certification: NELAC DOD FL NC
EDD Type: PDF_Excel_Other _ "Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ Pre-Approvedust Be
v^ �'
f.rcc' dsi,.a.:`s
Sc OTHER NIA
Site Location Name: r •h I Samples received after 14:00 will be processed next business day.
Site Location Physical Address: �93 Bell 6cm R4 , Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
a 1 1 (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
ID NO.
HOURS
SLUDGE)
SEE BELOW
`
S "a - x� air!
p
8,21-16
II' 3 �
�
�'C
r P
[�
� C4 I"
'J
Co r
ZIA
;y
1
:-,yyCe�i1./p.
/
a ,_ .
n 14
i
t^
D
I
.- s A y
Sampler's Signature O� �t�°c z Sampled By (Print Name) ( 10d'I " Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to roceed with the analyses as requested above. Any changes must be ,
submitted in writing to the Prism Project Manager. There will be charges for ny changes after analyse have been initialized.
Relin uis ed By: (Signat re) d d a Received By: (Sign lure) Dale - Idilitarylfiours Additiorial Comments: _
q Site Arrival Tlme
GL
���, �d .✓lifr
Rell shed By: (Signature) Received By: (Signature) " Date Site Departure, Time:
wished B (Signature) Re i ed For P 'sm Laboratories B Date ci Field Tech��Fee:,,
D
D) d of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT wIT C STODY SEALS FOR TRANS ORTATION TO THE LABORATORY. COC Group No.
(a SAMPLES SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST Cne UNTIL RECEIVED AT THE LABORATORY. ..
CD _ ..
CA Ex O UPS ❑ Hand -delivered Prism Field Service ❑ Other C) �� i �s
DRINKSOLID WASTE: ILL OTHER: •�
s: UST. I❑ L❑
❑ NC ❑ SC ❑ NOCU ❑ SCTER: ❑ NC SCATER: ❑ NC ❑ SC I O❑ NC ❑ SC I ❑❑ NC SC ❑❑ NCF❑ SC ❑❑ NC ❑ SC
�
NLTAINER
❑ 1 ❑ 1 ❑ ❑ `'4'71`''li�)�?
TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

ACCESS
ANALYT[CAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
RobbiJones
PROJECTID
6080505
LABORATORY REPORT NUMBER
216083118
DATE
09/06/2016
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955 _
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#:216083118
Page I of 11
Page 7 of 22
t

NELAP CERTIFICATE NUMBER: 01955
DOD ELAP CERTIFICATE NUMBER: L14-243
uoigF� s, LLr
ANALYTICAL RESULTS
PERFORMED BY
GCAL, LLC
7979 Innovation Park Dr.
Baton Rouge, LA 70820
Report Date 09/06/2016
III�ILIIdIIIINIIIIIY6083118
Project 6080505
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
I S 0
16 17026
PJLA d,
Don EL"
Lab Reportt 216083118
I Page 8 of 22

Report#: 216083118
41%
epplYTlC4l LGHONAiORI-ci: Llr Project ID: 6080505
Laboratory Endorsement
Report Date: 09/06/2616
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
DL Diluted analysis — when appended to Client Sample ID
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
P RPD between primary and confirmation result is greater than 40
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
A/
Authorized Signature
GCAL Report 216083118
Lab Report#: 216083118
Page 9 of 22

Report#: 216083118
Project ID: 6080505
Certifications
Report Date: 09/06/2016
Certification
Certification Number
DOD ELAP
L14-243
Alabama
01955
Arkansas
12-060-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
USDA Soil Permit
P330-10-00117
Lab Report#:216083118
Page 10 of 22

a 4 5
7
Report#: 216083118
Project ID: 6080505 Report Date: 09/06/2016
Case Narrative
Client: Access Analytical Report: 216083118
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
c
Lab Report* 216083118
Page 11 of 22

AL
nonn7ORIFS. LLC
r_r_ei in Client ID
21608311801 STA-LIME
Report#: 216083118
Project ID: 6080505
Sample Summary
Matrix Collect Date/Time
Report Date: 09/06/2016
Receive Date/Time
Solid 08/26/2016 11:30 08/31/2016 09:58
Lab Report#: 216083118 Page 12 of 22

G&CwA&lire
AKALVTI-L LAPOPATIPIGS, LLC
Report#: 216083118
Project ID: 6080505
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Report Date: 09/06/2016
Lab Report#: 216.083118
Page 13 of 2=2

Report#: 216083118
Project ID: 6080505
Sample Results
Report Date: 09/06/2016
Collect Date .08/26/2016 11:30 GCAL ID 21608311801
STA-LIME:
Receive Date. 08/31M16 09:58 Matrix Solid
El
D12B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/01/2016 08:30 593777 EPA 7.3.3.2 1 09/02/2016 14:22 SMR 593889
CAS# Parameter Result DL LOQ Units
57-12-5R Reactivity Cyanide 250U 250 250 mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/01/2016 08:30 593778 EPA 7.3.4.2 1 09/06/2016 09:55 RYC 594012 1
CAS#
Parameter
Result
DL
LOQ
Units
18496-25-8R
Reactivity Sulfide
250U
250
250
mg/kg
Lab Report#: 216083118 Page 1 4 4 of 22

ECAL
,LYTICAL LAP.ORATORIPS. LLC
Report#: 216083118
Project ID: 6080505 Report Date: 09/06/2016
General Chemistry QC Summary
Analytical Batch Client ID
MB593778
LCS5.93778
594012. �GCAL ID.
1604326
1604327
Prep Batch Sample Type
MB.
LCS
593778 Prep Date
09/0.112016 08:30
09/01/2016 08:30
Prep Method Analysis Date
09/06/201.6 09:5.5.:..
09/0612016,09:5.5
EPA 7.3.4.2 Matrix
Solid
Solid
EPA 9034
Units
lm.gft'
Spike
.Added
I Res.ItI
%R
Control
Result
DL
L
Limits%R
Reactivity Sulfide 18496-25-8R
250U
250
1000
1098
110147-135
I
Analytical Batch Client ID.
FCAKE
.1604071DUP
594012 GCALID
*2160831 0901:�
.1604328
Prep Batch Sample Type
SAMPLE
DUP
593778 Prep.D.ate
09/01/201608:30,
.09101/2016 08:30
Prep Method Analysis Date._ ate,
09106/2016 09:55
09/06/2016 09:55
EPA 7.3.4.2 Matrix
Solid
Solid
EPX 9034
Units
mg./kg
Re, ;UIt
RI
RPD
Result
DL
Limit
Reactivity Sulfide 18496-25-8R
01
2501
01
0
1 25
Analytical Batch Client ID
MB593777
LCS593777
593889 GCAL lb
1604323
.1604324
PrepPatch Sample Type
MB—
LCS
593777 Prep Date
09f01/2016 08:30
09/01/2016 08:30
Prep Method Analysis Date
09102/2016.13:54
09/02/2016 13:57
EPA 7.3.3.2 matrix
Solid-.
Solid
EPA 9012B
Units
mg/kg
I
':. Spike
Result
%R
I
Control
I
Result
DL
Addedi.
..
Limits%R
Reactivity Cyanide 57-12-5R
250U
1 250,
2501
30.31121
1-25
Analytical Batch Client ID.
FCAKE -
1604071DUP
593889 GCAL 11)
.21608310901.
.1604325:,
Prep Batch r Sample Type
:SAMPLE
DUP
'09/01/2016
593777 Prep Date
09101/2016 08:30.
08:30
Prep Method Analysis Date
09/02/20.16.1.4:0.1.
091021201 6 14:03
EPA 7.3.3.2 Matrix
Solid
Solid
EPA 9012B
-Units
m g/kg
Result
RPD
RPD
F
Result
DL
Limit
Reactivity Cyanide I 57-12--5R
1 0.01
2501
_0.0
1 0
1 20
Lab ReporW 216083118
Page 15 of 22

0
rn
O
W
C.
Full -Service Analytical € $DG 216083118
Environmental Solutions
ABURATORIE, INC.
PM SAK
SUBCONTRACT ORD,7 n
Celtification:,NELAC_ USAC);—
Prism Laboratories, Inc. NC,/ SC Other
6680505 N/A — --
SENDING LABOR4T01 RECEWMG LA110R4'r012Y:
Prism Laboratories_. Inc. Gulf Coast Anal�Kical Labs, Inc.
P_ O. Box 240543 7979 Inwwvation Park Dtive
Charlotte, NC 28224-0543 Batott Rouge, LA 70820
Phone: [phone] Phone :[phone]
Fax:[phone] Fax: [phone]
Project Manager. Robbi A. Jones
Analysis Due Expires Laboratory ID Comments
Sample ID: 6080505-01 Solid Sarnpled:08/26/1611:30
Reactivity, Sulfide (Sub) 09/01/16 11:30
Reactivity, Cyanidc (Sub) 09/09/16 1100
Gmtainers Supplied:
/j" L'
itcleascd Ay Uate Received Ry Uara
Released By Date Received By Date
Page I of I
7777) a� J
Page 16 of 22

Checklist
SAMPLE RECEIVING CHECKLIST
"I
SAMPLE DELIVERY GROUP 2160331l8
CHECKLIST
YES
NO
NA�
Client PM SAK.
Transport Method
Samples received with proper thermal and chemical pres.erva.tion?.
I
4565 - Access Analytical
FEDEX
. .... ..... . .
Radioactivity is <1 600 cmp? If no, record cmp value In notes section.
.. . . .. .... . ........... ..
Custody seals present and intact?
-5� JIL
El Ji
0-
..........
COC relinquished and complete (including sample IDs, collect dates/times, and sampler name)?
. . ............ . . ..... .. ...... .......... .
Short holds or RUSH samples received?
El R
1:1
-
Profile Number
Received By
80251
Lofton, Katie E.
. .....
All containers received in good condition and within hold time?
... ................... ... --- ------- ------- . . .......... .....
All sample labels and containers received match the chain of custody?
Preservation checked at receipt? Exceptions: VOC,. coliform, TOC, Oil and Grease, DOC
El
. .. ....... .......
11
Line Item(s)
Receive Date(s)
37 - Soil- Formaldehyde/
08/31116
........ . ....
Preservative added to any containers?
El
Cyanide /sulfide/ FP/TOX1PAH
....... . .....
VOC water containers received with headspace < 6mm?
.. ..... ....... .
Received filtered sample volume for.dissolved analysis?
...........
Trip blank present in all rooters containing VOC waters?
❑
El
Evi
Samples collected in containers provided by G CA L ?
Ell
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer][): E26
Temp(*C)
None
None
7771 1694 0136
1.6
NOTES
Pagel of
Revision 1.5
CD
—4 Lab Report#: 216083118 Page 11 of 11
0
............... ...... ...... ..... .

3'F
Ck- A�7--. ACCE-S 5
ANAL`tTiC�E
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
6080505
LABORATORY REPORT NUMBER
1608P46
DATE
September 07, 2016
Primary Data Review By Secondary Data Review By
Ashley Amick
Chris Pafford Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this reportshould be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at $83.315.4243
Page 1 of 5. ,
Page 18 of 22

ISM
AMM..-ATOMEAM
s�t�� �so� ���ai16 �c)�N-
Full-Service Analytical
Environmental Solutions
SUBCONTRACT ORDER Certification: NELAC USACE
Prism Laboratories, Inc. NC 1,­" SC_ Other
6080505 NIA
SENDING LABORATORY: RECEIVING LABORATORY
Prism Laboratories, Inc. Analytical Environmental Services, Inc.
P. O. Box 240543 3080 Presidential Parkway kP
Charlotte, NC 28224-0543 Atlanta, GA 30340
Phone: [phone] Phone -.[phone]
Fax: [phone] Fax: NA
Project Manager: Robbi A. Jones
Analysis Due Expires Laboratory 10D Comments
Sample 111): 6080505-61 Solid Sampled:08/26/16 11:30
Herbicides TCLP (Sub)
Containers Supplied:
0.�_
By
09/02/16 11:30
Y Date
M0*1A' /Fa IEP) 3116 10121
Y A. 6—f Date.
Released By Date Received By Date
Released By Date Received By Date 0 311 f
gepMi 0 1
Lori" Page 19 of 22

Analytical Environmental Services, Inc
Date: 7-Sep-16
Client:
Prism Laboratories
Client Sample ID:
Sta-Lime
Lab Order
1608P46
Tag Number:
6080505-01
Project Name:
6080505
Collection Date:
8/26/2016 11:30:00 AM
Lab 1D:
1608P46-001A
Matrix:
Solid
Analyses Result Qual MDL Reporting Units BatchlD DF Date Analyzed Analyst
Limit
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 127
(SW3510C)
0.064 0.20 rng/L 228953 1 09/06/201616:29 AW
0.076 0.20 mg/L 228953 1 09/06/201616:29 AW
0 50.1-148 %REC 228953 1 09/06/201616:29 AW
Qualifiers: s Value exceeds maximum contaminant level E Estimated value above quantitalion range
BRL Not Detected at MDL S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded > Greater than Result value
N Analyte not NELAC certified J Estimated value detected below Reporting Limit
B Analyte detected in the associated method blank < Less than Result value
ae g 3of5
Page 20 of 22

Analytical Environmental Services, Inc.
Sample/Cooler Receipt Checklist
Client Pwum— NS/'r1 Work Order Number 1 6 02f Lf to
Checklist completed by Pa4-�- 140A OZ(k y o 1 I L'
Sign tore Date
Carrier name: FedEx UPS _ Courier— Client— US M1 ail _ Other
Shipping container/cooler in good condition? Yes No
Custody seals intact on shipping container/cooler? Yes ✓ No _
Custody seals intact on sample bottles? Yes _ No _
Container/Temp Blank temperature in compliance? (0°56'Q* Yes
Cooler #1 2--fat' Cooler #2 Cooler #3 Cooler #4
Chain of custody present? Yes I/
Chain of custody signed when relinquished and received? Yes
Chain of custody agrees with sample labels? Yes ✓
No _
Not Present
Not Present _
Not Present
CooIer#5 Cooler 46
No CDC,
NoV/
No
Samples in proper container/bottle? Yes 1/ No _
Sample containers intact? Yes No _
Sufficient sample volume for indicated test? Yes V_// No _
All samples received within holding time? Yes v No
Was TAT marked on the COC? Yes No ` /
Proceed with Standard TAT as per project history? Yes I - / No _
Water - VOA vials have zero headspace? No VOA vials submitted v Yes _
Water - pII acceptable upon receipt? Yes — No
Not Applicable _
No _
Not Applicable
Adjusted? Checked by
Sample Condition: Good/ Other(Explain)
(For diffusive samples or AIHA lead) Is a known blank included? Yes _ No
See Case Narrative for resolution of the Non -Conformance.
* Samples do not have to comply with the given range for certain parameters.
\\Aes server\1\Sample Receipt\My Documents\COCs and pH Adjustment Sheet\Sample_Cooler Recipt Checklist Revl_rtf
t g 4 of
,Fa a 5. -
l-
Page 21 _of 22

2,4,5-TP (Silvex)
2,4-D
Surr: DCAA
BRL 0.20
BRL 0.20
0.5474 0 0.5000 109 50.1 148
Sample ID: LCS-228953
Client ID:
Units: mg/L
Prep Date: 09/02/2016
Run Into: 324643
SampleType: LCS
TestCode: HERBICIDES, TCLP Sw1311/8151A
BatchID: 228953
Analysis Date: 09/06/2016
Seq No: 7025929
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Lunt
High Limit RPD Ref Val %RPD
RPD Limit Qual
;. 2,4,5-TP (Silvex)
0.4581
0.20
0.5000
91.6
52.5
126
2,4-D
0.5439
0.20
0.5000
109
50.5
132
Surr: DCAA
0.5931
0
0.5000
119
50.1
148
Sample ID: 160SQ17-001AMS
Client iD:
Units: mg/L
Prep Dater 09/02/2016
Run No: 324643
SampleType: MS
TestCode: HERBICIDES, TCLP SW1311/8151A
BatchID: 228953
Analysis Date: 09/06/2016
Seq No: 7025932
Analyte
Result RPT Limit SPK value SPK Ref Val
%RFC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qua]
2,4,5-TP (Silvex)
0.4793 0.20
0.5000 95.9 49.4 131
2,4-D
0.5805 0.20
0.5000 116 44.1 137
Surr: DCAA
0.6060 0
0.5000 121 50.1 148
.,
Qualifiers: >
Greater than Result value
< Less than Result value B Analyte detected in the associated method blank
(!]
(D
BRL
Below reporting limit
E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded
N
N
I
Estimated value detected below Reporting Limit
N Analyte'notNELAC certified R RPD outside limits due to matrix page 5 of 5
Rpt Lim
Reporting Limit
S Spike Recovery outside limits duo to matrix
N
N

%M
DRIES, INC.
JC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical R
Environmental Solutions
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 09/26/2016
Prism Work Order: 6090436
Case Narrative
10/04/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Qnless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
)��;? �- J�(_.
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page I Of 6

I`- Full -Service Analytical &
JEnvironmental Solutions
ient Sample ID
Sample Receipt Summary
10/04/2016
Prism Work Order: 6090436
Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6090436-01 Solid 09/26/16 09/26/16
Samples were received in good condition at 4.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449. Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-toll Free Number: 1-8001529-6364-Fax:[phone] Page 2 of 6

S Laboratory Report
Full -Service Analytical &
Environmental Solutions 10/04/2016
�BORATORIES ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 6090436-01
P.O. Box 1111 Prism Work Order: 6090436
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/26/16 15:10
Time Submitted: 09/26/16 17:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 93.0
% by
0.100
0.100 1
*SM2540 G 9/28116 16:53 JLB
P610487
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 9/27/16 12:09 BMS
P610466
Total Metals
Mercury
0.26
mg/kg dry
0.022
0.0012
1
*7471B
9128/16 13:02
JAB
P610461
Arsenic
BRL
mg/kg dry
2.6
0.32
10
'6010D
9/30/16 19:29
bgm
P610451
Cadmium
BRL
mg/kg dry
2.6
0.071
10
'6010D
9/30/16 19:29
bgm
P610451
Copper
47
mg/kg dry
5.3
0.48
10
'6010D
9/30116 19:29
bgm
P610451
Lead
3.2
mg/kg dry
2.6
0.49
10
"6010D
9/30116 19:29
bgm
P610451
Nickel
7.0
mg/kg dry
5.3
0.19
10
'6010D
9/30/16 19:29
bgm
P610451
Selenium
10
mg/kg dry
5.3
1.3
10
'6010D
9130/16 19:29
bgm
P610451
Zinc
60
mg/kg dry
26
0.94
10
'6010D
9130/16 19:29
bgm
P610451
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 6

Level it QC Report
n n Full -Service Analytical &
' V' Environmental Solutions 1 �/4/16
I
LABORATORIES ING '
JFity of Statesville, NC Project: Stal-ime Prism Work Order: 6090436
Attn: Andy Smith Time Submitted: 9/26/2016 5:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P610451 - 3050B
Blank (P610451-BLK1)
Prepared: 09/28/16 Analyzed: 09/29/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P610451-BS1) _
Prepared: 09/28/16 Analyzed: 09/29/16
Arsenic
23.3
0.25
mg/kg wet
25.00 93 80-120
Cadmium
23.2
0.25
mg/kg wet
25.00 93 80-120
Copper
24.1
0.50
mg/kg wet
25.00 96 80-120
Lead
22.7
0.25
mg/kg wet
25.00 91 80-120
Nickel
22.7
0.50
mg/kg wet
25.00 91 80-120
Selenium
23.0
0.50
mg/kg wet
25.00 92 80-120
Zinc
23.0
2.5
mg/kg wet
25.00 92 80-120
Batch P610461 - 7471 B
Blank (P610461-BLK1) Prepared & Analyzed: 09/28/16
Mercury -- --_ BRL 0.020 mg/kg wet -------__-----
LC_S (P610461-BSI) _ Prepared &Analyzed: 09/28/16
Mercury 0.450 0.020 mg/kg wet 0.4167 108 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone]
Page 4 of 6

Level II QC Report
I I Full -Service Analytical &
Environmental Solutions
-
10/4/16
ABORATORIES INC.
Ftesville,
NC
Project:
Stal-ime
Prism Work Order: 6090436
Attn: Andy Smith
Time Submitted: 9/26/2016 5:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P610466 - NO PREP
Blank (P610466-BLK1)
Prepared & Analyzed: 09/27/16
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample
Extraction
Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
6090436-01 P610487
30 g
30 g
09/28/16 16:53
Prep Method: 3050B
Lab Number Batch
Initial
Final
Daterrime
6090436-01 P610451
2.04 g
50 mL
09/28/16 8:50
Prep Method: 7471B
Lab Number Batch
Initial
Final
Daterrime
6090436-01 P610461
0.59 g
50 mL
09/28/16 10:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone]-Toll Free Number: 1-800/529-6364- Fax: [phone] Page 5 of 6

CHAIN OF CUSTODY RECORD
Full -Service Analytical &
OF QUOTE # TO ENSURE PROPER BELLING:
�YErS' NO N/A �p
b p
Environmental Solutions PAGE_ _
Samples INTACT upon arrival?
_
St",
INC. Project Name:
Received ON WET ICE?
_ c0
449 Springbrook Road • Charlotte, NC 28217 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PRPR OPER ESERVI�TIVES indicated>
_ _ � �
Phone [phone] Fax: [phone]
� *Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Received WITHIN HOLDING TIMES?
cUST 0DY SEALS INTAC 7'
ca
Client Company Name:C +'4 of provisions and/or OC Requirements
Report To/Contact Name: �2 '� Invoice To:
VOLATLLE.S iec d WIQUT HEEILSPACL==?
PROPER CONTAINERS used?
Reporting Address Address:
�(__°
TEMP. Therm ID ':T Observed
C r °
( Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTlSAMPLING PERSONNEL
Phone:'10. 1-$711-M? Fax Yes No) : 9f' i'7y-Yi55
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC Do®
FL NC
EDD Type: PDF_Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ F re-h Work Mdust Be
Sc ®TI 9ER
NSA
Site Location Name- -1 k w V-. 1 Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
-8e:
Site Location Physical Address: � 93 Od j=.ar d?= •
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES
p p
NO ---
Ed.+>!es e, /fe l�� RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM
PRESERVA- �/ LAB
CLIENT DATE COLLECTED (SOIL, ��� REMARKS
TIMES
ID NO.
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE v
NO. SIZE 11
HOURS SLUDGE) SEE BELOW
r s �
3� 1. e-eK&
n1
�s
C 1
C44
-
Ph
12
Sampler's Signature `�'1 a c• Gc1 'a Sampled By (Print Name) dam)' ,- 3 O Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
' s
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
t
Relirtpylshed By: (Signal e)� �/� Re �� By: (Sign e) Dale
Military/Hours Additional Comments:
.gyp
Site Arrival Time: .
.�
Relin shed By: (Sig re) Re ed By: (Signature) Date
Site Departure Time:
Field Tech Fee:
Reli e : (Signal Received For P%aborat 'es By Dat
( �/ 1 �----✓ — ['
% D
�Mil_e___age:
elhod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEAL OR TRANSPORTATION TO THE LABORATORY.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC L}N/7)YRECEIVED AT THE LABORATORY.
OC G up No.
D urs O Hams-ueuve, eu „ ... , �_,� ��, • �� - -..._.
&ZODES:
GR DWATER: DRINKING WATER: SOLIDWASTE: RCRA: CERCLA LANDFILL OTHER:,SC ❑ C ❑SC ANC ❑SC ®NC ❑SC I aNCOSCONC ❑SC ®NC ❑SC ONC OSC
A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

MI Full -Service Analytical &
Environmental Solutions
rORIEB. INC.
/ City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: StaLime (Qtrly, & BiWeeklyl)
Lab Submittal Date: 10/10/2016
Prism Work Order: 6100216
Case Narrative
10/25/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR=[Na]/SQRT(([Ca]+[Mg])/2}
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A The ending CCV failed low at 85%. The result is reported with a potential low bias.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
"This re ort�should'nof be're" roduced; except in its entire - p p p ty'Without the written consent of Prism- Laboratories ; Inc: �
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/ Jlq-LIIIIC
Full -Service Analytical &
VI I Environmental Solutions
S ING
Lab Sample ID
Sample Receipt Summary
10/25/2016
Prism Work Order: 6100216
Matrix Date Sampled Date Received
6100216-01 Solid 10/10/16 10/10/16
Samples were received at 25.2 degrees C. See case narrative for further information.
" This repo'it should not be reproduced, except in its entirety, without the written consent'of Prism Laboratories,] ric.`
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free N umber: 1-8001529-6364 - Fax: [phone] Page 2 of 9

I Full -Service Analytical &
J'v Environmental Solutions
LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
% P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Laboratory Report
10/25/2016
Client Sample ID: Sta-Lime
Prism Sample ID: 6100216-01
Prism Work Order: 6100216
Time Collected: 10/10/16 11:45
Time Submitted: 10/10/16 16:17
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Plant Available Nitrogen
1300
mg/kg
160
18
2
*Calculation 10/18/16 8:51
CLB
[CALC]
Solids
78.6
% by
0.100
0.100
1
*SM2540 G 10/11/16 16:25
JLB
P6J0201
Weight
Nitrate/Nitrite as N
88
mg/kg dry
6.4
0.70
1
*SM4500-NO3 F 10/14/16 9:44
CLB
P6J0232
Phosphorus -Total
2400
mg/kg dry
64
30
20
*SM4500-P F 10/20/16 6:34
CLB
P6J0303
Total Kjeldahl Nitrogen
5200
mg/kg dry
640
72
2
*351.2 10/18/16 8:51
CLB
P6J0219
Ammonia as N
120
mg/kg dry
6.4
2.5
1
*SM4500-NH3 G 10/17/16 10:18
CLB
P6J0270
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 10/11/16 11:08
EGC
P6J0207
Total Metals
Mercury
BRL
mg/kg dry
0.026
0.0014
1
*7471B
10/18/16 13:28 JAB
P6J0304
SAR Soil Preparation
Complete
9
1
*2-78-054
10/14/16 13:00
JAB
P6J0262
SAR Percent Moisture
74.2
% by
0.100
0.100
1
*2-78-054
10/19/16 16:11
JAB
P6J0342
Weight
Arsenic
BRL
mg/kg dry
3.2
0.39
10
*6010D
10/20/16 22:07
bgm
P6J0282
Sodium Absorption Ratio
BRL
[blank]
0.30
0.016
1
*2-78-054
10/17/16 18:23
bgm
P6J0263
Cadmium
BRL
mg/kg dry
3.2
0.086
10
*6010D
10/20/16 22:07
bgm
P6J0282
Calcium
1100
mg/L
1.0
0.085
10
*6010D
10/14/16 19:20
bgm
P6J0263
Copper
43
mg/kg dry
6.4
0.58
10
*601013
10/20/16 22:07
bgm
P6J0282
Lead
3.2
mg/kg dry
3.2
0.59
10
*6010D
10/20/16 22:07
bgm
P6J0282
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
10/14/16 19:20
bgm
P6J0263
Nickel
7.2
mg/kg dry
6.4
0.23
10
*6010D
10/20/16 22:07
bgm
P6J0282
Potassium
1500
mg/kg dry
160
5.8
10
*6010D
16120MG 22:07
bgm
P6J0282
Selenium
8.8
mg/kg dry
6.4
1.5
10
*60101)
10/20/16 22:07
bgm
P6J0282
Sodium
27
mg/L
5.0
0.18
10
*6010D
10/17/16 18:23
bgm
P6J0263
Sodium
470 A
mg/kg dry
190
6.3
10
*60101)
10/21/16 15:04
bgm
P6J0282
Zinc
44
mg/kg dry
32
1.1
10
*6010D
10/20/16 22:07
bgm
P6J0282
This, report should not be reproduced, except in Its entirety without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 9

i I Full -Service Analytical &
Environmental Solutions
LAaOFA o-ir, I -
Level II QC Report
10/25/16
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 6100216
Attn: Andy Smith Time Submitted: 10/10/2016 4:17:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6J0262 - SAR 2-78-054
Blank (P6J0262-BLK1)
Prepared: 10/13/16 Analyzed: 10/14/16
SAR Soil Preparation
Complete
9
Batch P6J0263 - 3010A
Blank (P6J0263-B_LK1)
Prepared: 10/14/16 Analyzed: 10/17/16
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
Batch P6J0282 - 3050B
Blank (P6J0282-BLK1)
Prepared: 10/17/16 Analyzed: 10/19/16
Arsenic
BRL
0.25
mg/kg wet
_
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LC_S (P6J0282-BSI)
Prepared: 10/17/16 Analyzed: 10/19/16
Arsenic
_
25.0
0.25
mg/kg wet
25.00 100 80-120
Cadmium
24.5
0.25
mg/kg wet
25.00 98 80-120
Copper
26.8
0.50
mg/kg wet
25.00 - 107 80-120
Lead
24.6
0.25
mg/kg wet
25.00 98 80-120
Nickel
24.8
0.50
mg/kg wet
25.00 99 80-120
Potassium
462
12
mg/kg wet
500.0 92 80-120
Selenium
24.8
0.50
mg/kg wet
25.00 99 80-120
Sodium
478
15
mg/kg wet
500.0 96 80-120
Zinc
24.6
2.5
mg/kg wet
25.00 98 80-120
-This report should not be -reproduced; except in its entirety, without the written consent.of.Prism-Laboratories,.Jnc...,.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 9

I n n Full -Service Analytical &
' V' Environmental Solutions
4BORATORIEB. INO
'pity of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, & BiWeeklyl)
Level II QC Report
10/25/16
Prism Work Order: 6100216
Time Submitted: 10/10/2016 4:17:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6J0304 - 7471 B
Blank (P6J0304-BLK1) Prepared & Analyzed: 10/18/16
Mercury BRL 0.020 mg/kg wet
LCS (P6J0304-BS1) Prepared & Analyzed: 10/18/16
Mercury 0.417 0.020 mg/kg wet 0.4167 100 80-120
Batch P6J0342 - NO PREP
Duplicate (P6J0342-DUP1) Source: 6100216-01 Prepared: 10/14/16 Analyzed: 10/19/16
SAR Percent Moisture 69.8 0.100 % by Weight 74.2 6 200
This repo not be,re , coducedexce tin its entire p p p ty,.without the:,wntten copppritofPrism Labor atories nc• , ,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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r Level II QC Report
I I n I Full -Service Analytical & 10/25/16
V' Environmental Solutions
I RATORIES INO.
nity of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (Qtrly, & BiWeeklyl)
Prism Work Order: 6100216
Time Submitted: 10/10/2016 4:17:OOPM
Analyte
Reporting
Result Limit Units
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P6JO201 - Solids Dry Weight
Duplicate (P6J0201-D_UPS)
Source: 6100216-01
Prepared & Analyzed: 10/11/16
% Solids
Batch P6JO219 - 351.2
80.5 0.100 % by Weight 78.6 2 20
Blank (P6J0219-BLK1)
Prepared: 10/13/16 Analyzed: 10/18/16 —
Total Kjeldahl Nitrogen
LCS (P6J0219-BSI)
BRL 25 mg/kg wet
Prepared: 10/13/16 Analyzed: 10/18/16
Total Kjeldahl Nitrogen
Batch P6JO232 - NO PREP
481 100 mg/kg wet
500.0 96 90-110
Blank (P6J0232-BLK1) Prepared & Analyzed: 10/14/16
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS P6J0232-BS1 Prepared & Analyzed: 10/14/16
Nitrate/Nitrite as N 47.2 5.0 mg/kg wet 50.00 94 80-120
Matrix Spike (P6J0232-MS1) _ _ Source: 6100216-01 Prepared & Analyzed: 10/14/16_
Nitrate/Nitrite as N 175 6.4 mg/kg dry 63.65 88.2 136 80-120 M
Matrix Spike Dup (P6J0232-MSD1) Source: 6100216-01 Prepared & Analyzed: 10/14/16
Nitrate/Nitrite as N 174 6.4 mg/kg dry 63.65 .88.2 136 80-120 0.3 20 M
Batch P6JO270 - NO P
Blank (P6JO270-BLK1) _ Prepared & Analyzed: 10/17/16
Ammonia as N BRL 5.0 mg/kg wet
This.report.should . not-bere roduced„exce t in its entire <,. p p ty,-wlthoutthe_wntten consent.of Prism Laboratories.,,lnc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 9

I S M I Full -Service Analytical &
Environmental Solutions
r,ity of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6JO270 -
Level II QC Report
10/25/16
Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 6100216
Time Submitted: 10/10/2016 4:17:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P6JO270-BS1) Prepared &Analyzed: 10/17/16
Ammonia as N 122 5.0 mg/kg wet 125.0 98. 80-120
Matrix Spike (P6JO270-MS1) Source: 6100216-01 Prepared & Analyzed: 10/17/16
Ammonia as N 344 6.4 mg/kg dry 159.1 122 140 80-120 MI
Matrix Spike Dup (P6J0270-MSD1)Source: 6100216-01_ Prepared & Analyzed: 10/17/16_
Ammonia as N 340 6.4 mg/kg dry 159.1 122 137 80-120 1 20 MI
Batch P6JO303 - SM4500-PB5
Blank (P6JO303-BLK1) Prepared: 10/18/16 Analyzed: 10/20/16
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P6JO303-BS1) Prepared: 10/18/16 Analyzed: 10/20/16
Phosphorus -Total 96.8 2.5 mg/kg wet 100.0 97 90-110
Matrix Spike (P6JO303-MS1) Source: 6100216-01 Prepared: 10/18/16 Analyzed: 10/20/16 __-
Phosphorus -Total 2840 64 mg/kg dry 127.3 2350 385 80-120 MC
Matrix Spike Dup (P6JO303-MSD1) Source: 6100216-01 Prepared: 10/18/16 Analyzed: 10/20/16
Phosphorus -Total 3030 64 mg/kg dry 127.3 2350 530 80-120 6 20 MC
This.re ort should not,be reproduced, roducedexcept in.its entire p p p ty,..without the wntten,consent of Prism.. a pratones,,, nc, , ., • , , ,.. , ,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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I Full -Service Analytical &
Environmental Solutions
Project: Stal-ime (Qtrly, & BiWeeklyl)
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
10/25/16
Prism Work Order: 6100216
Time Submitted: 10/10/2016 4:17:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6JO207 - NO PREP
Blank (P6JO207-BLK1) Prepared & Analyzed: 10/11/16
Fecal Coliforms BRL 0.2 MPN/g wet
Duplicate (P6J0207-DUP1) Source: 6100216-01 Prepared &Analyzed: 10/11/16
Fecal Coliforms BRL 0.3 MPN/g dry BRL
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/rime
20
6100216-01
P6J0219
0.05 g
25 mL
10/13/16 10:00
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/rime
6100216-01
P6J0303
1 g
50 mL
10/18/16 10:02
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
6100216-01
P6J0201
30 g
30 g
10/11/16 16:25
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6100216-01
P6J0263
50 mL
50 mL
10/14/16 13:30
6100216-01
P6J0263
50 mL
50 mL
10/14/16 13:30
6100216-01
P6J0263
50 mL
50 mL
10/14/16 13:30
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
6100216-01
P6J0282
1.99 g
50 mL
10/17/16 9:20
6100216-01
P6J0282
1.99 g
50 mL
10/17/16 9:20
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/rime
6100216-01
P6J0304
0.58 g
50 mL
10/18/16 9:07
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
6100216-01
P6J0262
250 g
250 g
10/13/16 13:00
I nis report snowa not De reproaucea, except In its entirety, wrtnuuL. we wnuen consent ui resin—auurerunes,• inc:.: -•
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 Of 9

Full-Set'vien Analytical
r8 F_nvironmental Solutions
to P
LAtlGHATORRIS1e S, INC.
449 Springbrook Road • Charlotte, NC 28217
Phone [phone]•6364 Fax: [phone]
Client Company Name: � , T; o L .r3 �A$ ;5V GO e
Report To/Contact Name: a� m a ,a SaI^i a '
Reporting Address:
CHAIN OF CUSTODY RECORD
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
"Please ATTACH any project specific reporting (QC LEVEL I II III IV)
provisions and/or QC Requirements
Address:
-
Y ::NO " NIA.:
M
Samples INTACT upon arrival?
0
O
Received ON WET ICE?
PROPER PRESERVATIVES Indicated?
Q
Received WITHIN'HOLDIIVG TIMES
_:. —
d
CUS I ODY SEALS INTACT?
VOLPTILES rec'd W/OUT HEADSPACE?
,PROPER CONTAINERS.used?
TEMP: ,Therm iD:_u 1 \\ Observed i * °C / Corr'.
Phone:704- 9` 7 9- 3936 Fax es (NO): r70'1.9 7,?- ?,e55purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF_EXCeI_Other "WorkingDays" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Y y Pre -Approved
SC OTHER NIA
p y'�
Site Location Name' �� SI /'/'`+�� ��l �� ° Samples received after 14:00 will be processed next business day.
Water Chlorinated: YES_ NO_
Physical Address: 1��' 9 d !F/a s` Turnaround time is based on business days, excluding weekends and holidays.
REGARDING SERVICES
Site Location (SEE REVERSE FOR TERMS & CONDITIONS
CLIENT)
Sample Iced Upon Collection: YES NO
P p —
•��• •� y;, d��+ j,Jc'_ RENDERED BY PRISM LABORATORIES, INC. TO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRTVESVA
r ��ti REMARKS
LAB
ID NO.
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
SLUDGE)
*TYPE
SEE BELOW
NO.
SIZE
it ��/
HOURS
�k
stet 7t`S�-S
�tx- /'a r>a
o£
+
CS
PA !�
SAP
,.
IN ..
C'.
trein
,d
d e./
rJ� Sampled By (Print Name) Ei r�' 1�lAffiliation
Sampler's Signature .7��"
Upon relinquishing, this Cain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
Project Manager. There will be charges for any changes after analyses have been initialized.
submitted in writing to the Prism
Relin shed By; (Slgnatur Received By. (Signature) Date Military/Hours Additional Comments: Site, Arrival Urner
�d f
7 ` Received 8y: (Signature) Date S1ta,Departure.Tme
Relies hed By: (Signature)
Field Tech. Fee:
eiv For Prism Laboratories, Pat `�.',
Relinquished 6 ;- Signature) _ —, J�
� � Mileage
Lam.----
Method of Shipment: NOTE: ALL SAMPLE CO99 ERS SHOULD BE TAPED SHUT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACyOEPTED AND VERIFIED AGAINS C UNTIL RECEIVED AT THE LABORATORY. n u r,')A" ^ ,
CERCLA LANDFILL I OTHER:
UST: GROUNDWATER: UKIry Klrvli VVHI Crc: avL-ru vvr» r IQ. rww+•
❑NC ❑SCI 0NC ❑SC I UNC ❑SC I ❑NC ❑SC ❑NC❑SC El NC ❑SC ❑NC ❑SC El NC ❑SC
❑ ❑ ❑ ❑- ❑
L_eE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime (60 Day/7 Fecal)
Lab Submittal Date: 10/24/2016
Prism Work Order: 6100461
Case Narrative
11 /02/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report. .
Respectfully,
PRISM LABORATORIES, INC.
DRAFT REPORT
DATA SUBJECT TO CHANGE
Data Qualifiers Key Reference:
Reviewed By DRAFT REPORT
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values, between MDL and
reporting limit indicated with a J.
„ . .This report should not be,reproduced, except in its entirety,,without the written consent of Prism Laboratories, Inc..
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 13

ie-ice Analytical &
onmental Solutions
Sample Receipt Summary
11 /02/2016
Prism Work Order: 6100461
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
StaLime (and Fecal 1)
6100461-01
Solid
10/24/16
10/24/16
Fecal #2
6100461-02
Solid
10/24/16
10/24/16
Fecal #3
6100461-03
Solid
10/24/16
10/24/16
Fecal #4
6100461-04
Solid
10/24/16
10/24/16
Fecal #5
6100461-05
Solid
10/24/16
10/24/16
Fecal #6
6100461-06
Solid
10/24/16
10/24/16
Fecal #7
6100461-07
Solid
10/24/16
.10/24/16
Samples were received at 27.5 degrees C. See case narrative for further information.
p written et of
, Prism Laboratories, Inc.
This report should,not,be,[eproduced,;except R�lts,entire_ty,, without the wri , _ , „ _.. _,__ ,.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-05,43
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page-2 of 13

Service Analytical &
ronmentaI Solutions .
' City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
11/02/2016
Client Sample ID: Stal-ime (and Fecal 1)
Prism Sample ID: 6100461-01
Prism Work Order: 6100461
Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
% Solids
94.2 .
% by
0.100
0.100 1
*SM2540 G
10126/16 16:40
JLB
P6J0497
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
10/25/16 9:30
BMS
P6J0449
Total Metals
Mercury
0.12
mg/kg dry
0.023
0.0013 1
*7471B
10/28/16 13:15
JAB
P6J0510
SAR Soil Preparation
Complete
g
1
*2-78-054
10/27/16 14:00
JAB
P6J0500
SAR Percent Moisture
Complete
% by
0.100
0.100 1
*2-78-054
11/1/16 16:00
JAB
P61<0031
Weight
Arsenic
5.3
mg/kg dry
0.26
0.032
1
*6010D
10/27/16 3:34
bgm
P6J0460
Sodium Absorption Ratio
0.38
[blank]
0.30
0.016
1
*2-78-054
10/28/16 17:34
bgm
P6J0501
Cadmium
BRL
mg/kg dry
0.26
0.0070
1
*6010D
10/27/16 3:34
bgm
P6J0460
Calcium
2200
mg/L
1.0
0.085
10
*6010D
10/27/16 20:50
bgm
P6J0501
Copper
50
mg/kg dry
0.52
0.047
1
*6010D
10/27116 3:34
bgm
P6J0460
Lead
2.3
mg/kg dry
0.26
0.048
1
*6010D
10/27/16 3:34
bgm
P6J0460
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
10/27/16 20:50
bgm
P6J0501
Nickel
5.3
mg/kg dry
0.52
0.019
1
*6010D
10/27/16 3:34
bgm
P6J0460
Selenium
BRL
mg/kg dry
0.52
0.12
1
*6010D
10/27/16 3:34
bgm
P6J0460
Sodium
65
mg/L
5.0
0.18
10
*601013
10/28/16 17:34
bgm
P6J0501
Zinc
44
mg/kg dry
2.6
0.093
1
*601013
10/27/16 .3:34
bgm
P6J0460
report;should not be reproduced,.except.in its entirety, without,the,written consent.of Prism• Laboratories,.Inc.,.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] : Page 3 Of 13

Service Analytical 8
ronmental Solutions
Laboratory Report
11 /02/2016
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: Fecal #2
Attn: Andy Smith Prism Sample ID: 6100461-02
P.O. Box 1111 Prism Work Order: 6100461
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 92.3 % by 0.100 0.100 1 *SM2540 G 10/26/16 16:40 JLB P6J0497
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 10/25/16 9:30 BMS P6J0449
......__This, report should not be.reproduced,,except in, its entirety., wlthout,the Written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 13

I -Service Analytical 8
iironmental Solutions
PI City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
11 /02/2016
Client Sample ID: Fecal #3
Prism Sample ID: 6100461-03
Prism Work Order: 6100461
Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
Solids 84.9
% by
0.100
0.100 1
`SM2540 G 10/26116 16:40 JLB
P6J0497
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 10/25/16 9:30 BMS
P6J0449
This re ort�should not be re roduced, except inits
•<-. p p p entirety; without -ta written consent of -Prism Laboratories; Inc.-.'.. -.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

'I -Service Analytical & Laboratory Report
vironmental Solutions 11/02/2016
Project: Stal ime (60 Day/7 Fecal) Client Sample ID: Fecal #4
Attn: Andy Smith Prism Sample ID: 6100461-04
P.O. Box 1111 Prism Work Order: 6100461
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 90.2 % by 0.100 0.100 1 'SM2540 G 10/26/16 16:40 JLB P6J0497
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 10/25/16 9:30 BMS P6J0449
This report should not be reproduced; except -in its entirety., -without the writtemconsent-of Prism Laboratories,, Ina w
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] . Page 6 Of 13

City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Parameter
I -Service Analytical 8
rlronmental Solutions
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Result Units Report
Limit
Laboratory Report
. 11 /02/2016
Client Sample ID: Fecal #5
Prism Sample ID: 6100461-05
Prism Work Order: 6100461
Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
MDL Dilution Method Analysis Analyst Batch
Factor Date/Time ID
General Chemistry Parameters
% Solids 89.3 % by 0.100 0.100 1 `SM2540 G 10/26/16 16:40 JLB P6J0497
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 10/25/16 9:30 BMS P6J0449
This report,should not be reproduced; except in•its entirety; withoubthe written consent of Prism Laboratories, Inc, .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page 7 Of 13

li-Service Analytical &
vironmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
11 /02/2016
Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #6
Prism Sample ID: 6100461-06
Prism Work Order: 6100461
Sample Matrix: Solid Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 94.2
% by
0.100
0.100 1
'SM2540 G 10/26M 6 16:40 JLB
P6J0497
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 10/25/16 9:30 BMS
P6J0449
This reportshould not be,reproduced, except in its entirety,,without the written. consent of Prism Laboratories,.Inc;-....: -„ _ ::.,.....•., .:-
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 8 Of 13

ill -Service Analytical &
tvironmental Solutions
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
11 /02/2016
Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #7
Prism Sample ID: 6100461-07
Prism Work Order: 6100461
Sample Matrix: Solid Time Collected: 10/24/16 10:20
Time Submitted: 10/24/16 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
% Solids 91.1 % by 0.100 0.100 1 *SM2540 G 10/26/16 16:40 JLB P6J0497
Weight
Microbiological. Parameters
Fecal Coliforms
BRL MPN/g dry 0.2 1 *SM9221 E 10/25/16 9:30 BMS P6J0449
-* �� -- •- - -:. uus repun-5nuulu not ue reproaucea, except in -as emlreryyWlmout ine wnnen.consent of F'rism: Laboratories, --Inc.-
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 Of $

I -Service Analytical &
iironmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime (60 Day/7 Fecal)
Level II QC Report
1112/16
Prism Work Order: 6100461
Time Submitted: 10/24/2016 3:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6JO460 - 3050B
Blank (P6JO460-BLK1)
Prepared: 10/26/16 Analyzed: 10/27/16_ - -
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mglkg wet
Zinc
BRL
2.5
mg/kg wet
LC_S (P6J0460-BS1) _
_ -
_ _
Prepared: 10/26/16 Analyzed: 10/27/16
Arsenic
24.3
0.25
mg/kg wet
25.00 97 80-120
Cadmium
24.1
0.25
mg/kg wet
25.00 97 80-120
Copper
25.7
0.50
mg/kg wet
25.00 103 80-120
Lead
24.2
0.25
mg/kg wet
25.00 97 80-120
Nickel
24.1
0.50
mg/kg wet
25.00 96 80-120
Selenium
23.6
0.50
mg/kg wet
25.00 95 80-120
Zinc
24.0
2.5
mg/kg wet
25.00 96 80-120
Batch P6JO500 - SAR 2-78-054
Blank (P_6J0_500-BL_K_1_) _ -
_
- -
Prepared: 10/26/16 Analyzed: 10/27/16-
SAR Soil Preparation
Complete
g
Batch P6JO501 - 3010A
Blank (P6J0501-BLK1)
- - Prepared: 10/27/16 Analyzed: 10/28/16
Sodium Absorption Ratio
BRL 3.0 [blank]
Calcium
BRL 1.0 mg/L
Magnesium
BRL 1.0 mg/L
Sodium
BRL 5.0 mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 13

I I n n I IF Analytical &
' V' Environmental Solutions
-ORATORIM INO
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P6JO510 - 7471 B
Project: Stal-ime (60 Day/7 Fecal)
Level II QC Repoli
11 /2/16
Prism Work Order: 6100461
Time Submitted: 10/24/2016 3:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P6J0510-BLK1) Prepared & Analyzed10/28/16
Mercury BRL 0.020 mg/kg wet
LCS (P6J0510-BS1) _ _ Prepared & Analyzed: 10/28/16
Mercury 0.396 0.020 mg/kg wet 0.4167 95 80-120
Batch P6KO031 - NO PREP
Blank (P6K0031-BLK1) Prepared: 10/27/16 Analyzed: 11/01/16
SAR Percent Moisture Complete 0.100 % by Weight
Duplicate (P6K0031-DUP1) _ Source: 6100461-01 Prepared: 10/27/16 Analyzed_ 11/01/16 _
SAR Percent Moisture Complete 0.100 % by Weight Complete 1 200
This report should,not,be reproduced, except in its entirety, without the,written,consent of Prism Laboratories, lnc,,
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 13

Level II QC Report
-Service Analytical & 11/2/16
ironmental Solutions
Project: StaLime (60 Day/7 Fecal) Prism Work Order: 6100461
Attn: Andy Smith Time Submitted: 10/24/2016 3:30:00PM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6J0449 - NO PREP
Blank (PU0449-BLK1) _ Prepared & Analyzed: 10/25/16
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
6100461-01
136J0497
30 g
30 g
10/26/16 16:40
6100461-02
P6J0497
30 g
30 g
10/26/16 16:40
6100461-03
P6J0497
30 g
30 g
10/26/16 16:40
6100461-04
P6J0497
30 g
30 g
10/26/16 16:40
6100461-05
P6J0497
30 g
30 g
10/26/16 16:40
6100461-06
P6J0497
30 g
30 g
10/26/16 16:40
6100461-07
P6J0497
30 g
30 g
10/26/16 16:40
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6100461-01
P6J0501
50 mL
50 mL
10/27116' 15:00
6100461-01
P6J0501
50 mL
50 mL
10/27/16 15:00
6100461-01
P6J0501
50 mL
50 mL
10/27/16 15:00
Prep Method: 3050B
Lab Number_
Batch
Initial
Final
Date/rime
6100461-01
P6J0460
2.04 g
50 mL
10/26/16 10:05
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime
6100461-01
P6J0510
0.56 g
50 mL
10/28/16 9:42
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
6100461-01
P6J0500
250 g
250 g
10/26/16 14:00
Subcontracted Analyses
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number
Analysis
6100461-01
Ammonia (Automated)
6100461-01
Nitrate + Nitrite (Automated - SM)
6100461-01
Phosphorus, Total (Automated)
6100461-01
TKN (Automated)
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Phone [phone] • Fax: [phone]
Client Company Name: c l
Report To/Contact Name: Q "r S., -4 in,
Reporting Address:
CHAIN OF CUSTODY RECORD
PAGE_ OF _ QUOTE 9 TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
1 n Tn
Address-
Saniples IN iAC I
Received ON d,1 1' K F'
PI':OPLh PRPSLRVATIVC-S Ind;csloc?
Received VVII HIN HOL-•iNG 11iv1L-S"'
ClISfODY SEN_ S INPV. f
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yE NO N.1A
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EDD Type: PDF_Ex_cel_Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re Approvedust Be SC OTHER NIA .
Site Location Name: Cs.'et� W, `^- /
Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 16 -24z—j 9 �•a"r, %�,k a Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO —
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES on Sample Iced U Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) P p -
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- �� REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE NO. SIZE TIVES C� L ID NO.
HOURS SLUDGE) [SEE BELOW �� v'�
1t Lip:
P
I
.pb
S
Samplers Signature i-f Ge%s*iur� I Sampled By (Print Name) `'AZ L'I1 ��%Ck I Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be arges for any changes after analyses have been initialized.
Relliiny�pd B
hed By: (Signature) /' Re eiv y: (Si re Date MilN
/530
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST NTIL RECEIVED AT THE LABORATORY. r
❑ UPS ❑ Hand -delivered dsnn Feld Service . ❑ Other , 11 _` `
CERCLA
i
❑ NC ❑ SC I ❑ NC ❑ SCTER: I DRINKING
NC lLI CATER: I SOLID NC ❑ SCE I O NC O SC I O NC ❑ SC O❑ NC LANDFILL❑ SC ❑❑ NC ❑ SC
❑ I ❑ I ❑
TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
C� -o DA, f e f„
Additional Comments:
of
0

:.PRISM
LABORATORIES, ING
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 11/07/2016
Prism Work Order: 6110152
Case Narrative
11/18/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR = [ Na ] / SQRT { ( [Ca] + [Mg] )12 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
7z:t4___ �C' - (_ �
Reviewed By Robbi A. Jones
President/Project Manager
A Calibration verification standard recoveries (87 and 88% R) are less than the lower control limit (90%). Sodium
result might have a slight low bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 9

Full -Service Analytical &
Environmental Solutions
ING
Sample Receipt Summary
11/18/2016
Prism Work Order: 6110152
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6110152-01 Solid 11/07/16 11/07/16
Samples were received at 19.2 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
440`Sprin'gb'ro-'-o'W-fi'o'a'dP'.'.-O-' Box-.240543 -Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: . [phone] Page 2 of

P I S M
Full -Service Analytical 8
I
R
s LA80HATORIES ING
Environmental Solutionsa
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
11/18/2016
Project: StaLime Client Sample ID: Sta-Lime
Prism Sample ID: 6110152-01
Prism Work Order: 6110152
Sample Matrix: Solid Time Collected: 11/07/16 10:30
Time Submitted: 11/07/16 17:30
Parameter. Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1200
mg/kg
380
44
5
*Calculation 11/17/16 9:15
CLB
[CALC]
% Solids
58.3
% by
0.100
0.100
1
*SM2540 G 11/11/16 15:17
JLB
P6K0316
Weight
Nitrate/Nitrite as N
77
mg/kg dry
8.6
0.94
1
*SM4500-NO3 F 11/17/16 9:15
CLB
P61(0369
Phosphorus -Total
3300
mg/kg dry
86
41
20
*SM4500-P F 11/16/16 9:11
CLB
P6K0352
Total K]eldahl Nitrogen
6400
mg/kg dry
2100
240
5
*351.2 11/15/16 8:46
CLB
P61<0257
Ammonia as N
270
mg/kg dry
8.6
3.3
1
*SM4500-NH3 G 11/14/16 12:20
CLB
P61(0268
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 11/8/16 10:21
EGC
P61<0206
Total Metals
Mercury
0.23
mg/kg dry
0.037
0.0021
1
*7471B
11/15/16 12:53
JAB
P61<0331
SAR Soil Preparation
Complete
g
1
*2-78-054
11/11/16 14:00
JAB
P61<0281
SAR Percent Moisture
67.8
% by
0.100
0.100
1
*2-78-054
11/17/16 14:50
JAB
P6K0455
Weight
Arsenic
7.9
mg/kg dry
0.42
0.051
1
*6010D
11/14/16 23:32
bgm
P61(0263
Sodium Absorption Ratio
0.37
[blank]
0.30
0.016
1
*2-78-054
11/15/16 1:18
bgm
P61(0282
Cadmium
BRL
mg/kg dry
0.42
0.011
1
*6010D
11/14/16 23:32
bgm
P61<0263
Calcium
1000 BH
mg/L
1.0
0.085
10
*6010D
11/15/16 1:18
bgm
P61(0282
Copper
69
mg/kg dry
0.84
0.076
1
*6010D
11/14/16 23:32
bgm
P61<0263
Lead
3.7
mg/kg dry
0.42
0.078
1
*6010D
11/14/16 23:32
bgm
P6K0263
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
11/15/16 1:18
bgm
P61<0282
Nickel
6.6
mg/kg dry
0.84
0.030
1
*6010D
11/14/16 23:32
bgm
1361<0263
Selenium
1.3
mg/kg dry
0.84
0.20
1
*6010D
11/14M6 23:32
bgm
P61(0263
Sodium
43 A
mg/L
5.0
0.18
10
*6010D
11/15/16 1:18
bgm
P61(0282
Zinc
98
mg/kg dry
4.2
0.15
1
*6010D
11/14/16 23:32
bgm
P61(0263
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
t, . 449 Springbrook"Road'='P.O Boz 240543'- Charlotte; NC`28224-0543 :
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: 704/52"409 Page 3 Of Q

Full -Service Analytical &
Environmental Solutions
\TORIE$ ING.
Level II QC Report
11/18/16
City of Statesville, NC Project: Stal-ime Prism Work Order: 6110152
Attn: Andy Smith Time Submitted: 11/7/2016 5:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6K0263 - 3050B
Blank (P6K0263-BLK1)
Prepared: 11/11/16 Analyzed: 11/14/16
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6K0263-BS1)
Prepared: 11/11/16 Analyzed: 11/14/16
Arsenic
24.2
0.25
mg/kg wet
25.00 97 80-120
Cadmium
23.9
0.25
mg/kg wet
25.00 96 80-120
Copper
26.4
0.50
mg/kg wet
25.00 106 80-120
Lead
24.1
0.25
mg/kg wet
25.00 96 80-120
Nickel
24.5
0.50
mg/kg wet
25.00 98 80-120
Selenium
23.1
0.50
mg/kg wet
25.00 92 80-120
Zinc
24.3
2.5
mg/kg wet
25.00 97 80-120
Batch P6K0281 - SAR 2-78-054
Blank (P6K0281-BLK1) _
Prepared: 11/10/16 Analyzed: 11/11/16
SAR Soil Preparation
Complete
g
Batch P6K0282 - 3010A
Blank (P6K0282-BLK1)
Prepared: 11/11/16 Analyzed: 11/15/16
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
BH
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449'Spiringbrok'R6ad =P.O. Box 240543 -Charlotte; NC'28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 Of 9

Full-Semice Analytical 8
Environmental Solutions
G^•r,�.�.'.. '...--�. LABOflATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
11/18/16
Prism Work Order: 6110152
Time Submitted: 11/7/2016 5:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6KO331 - 7471 B
Blank (P6K0331-BLK1) _ _ — Prepared & Analyzed: 11/15/16
Mercury BRL 0.020 mg/kg wet
LC_S_(P6KO331-BSI) Prepared & Analyzed: 11 /15/16
Mercury 0.440 0.020 mg/kg wet 0.4167 106 80-120
Batch P6KO455 - NO PREP
Duplicate (11361<0455-DUP7) Source: 6110152-01 Prepared: 11/11/16 Analyzed: 11/17/16
SAR Percent Moisture 39.0 0.100 % by Weight 67.8 54 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road'-P.O: Box 240543 - Charlotte; NC•28224=0543••
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MFull-Service Analytical &
J Environmental Solutions
TORTES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6K0257 - 351.2
Project: StaLime
Reporting
Result Limit Units
Level II QC -Report
11/18/16
Prism Work Order: 6110152
Time Submitted: 11/7/2016 5:30:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P6K0257-BLK1)
— ------
Prepared: 11/11/16 Analyzed: 11/15/16
Total Kjeldahl Nitrogen
LCS (P6K0257-BSI)
-- —BRL _-- - 25
mg/kg wet
-----------_" ---_-----_--------- - - - -- _---
Prepared: 11/11/16 Analyzed: 11/15/16
Total Kjeldahl Nitrogen
Matrix Spike (P6K0257-MS1)
489 100 mg/kg wet
Source: 6110152-01
500.0 98 90-110
Prepared: 11/11/16 Analyzed: 11/15/16
Total Kjeldahl Nitrogen
Matrix Spike Dup (P6K0257-MSD1)
15200 2100 mg/kg dry
Source: 6110152-01
8575 6430 102 90-110
Prepared: 11/11/16 Analyzed: 11/15/16
Total Kjeldahl Nitrogen
Batch P6K0268 - NO PREP
14400 2100
mg/kg dry
8575 6430 93 90-110 5 20
Blank (113611<0268-13LK1)
Prepared: 11/11/16 Analyzed: 11/14/16
Ammonia as N
LCS (P6K0268-SS1)
BRL 5.0
mg/kg wet
Prepared: 11/11/16 Analyzed: 11/14/16
Ammonia as N
127 5.0
mg/kg wet
125.0 101 80-120
Batch P6K0352 - SM4500-PB5
Blank (P6K0352-BLK1) Prepared: 11/15/16 Analyzed: 11/16/16
------------- - --- --- -
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P6K0352-BS1) _Prepared: 11/15/16 Analyzed: 11/16/16
Phosphorus -Total 94.8 2.5 mg/kg wet 100.0 95 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spring brook Road - P.O. Box 240543- Charlotte, NC28224-0543-"' r
Phone:[phone]-Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 Of 9

M I Full -Service Analytical &
Environmental Solutions
RIM lNa
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6KO352 - SM4500-PB5
Reporting
Result Limit Units
Level II QC Report
11 /18/16
Prism.Work Order: 6110152
Time Submitted: 11/7/2016 5:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P6K0352-MS1) Source: 6110152-01 Prepared: 11/15/16 Analyzed: 11/16/16
Phosphorus -Total 3940 86 mg/kg dry 171.5 3300 374 80-120 MC
Matrix Spike Duo (P6KO352-MSD1) _ _ Source: 6110152-01 Prepared: 11/15/16 Analyzed: 11/16/16
Phosphorus -Total 3970 86 mg/kg dry 171.5 3300 392 80-120 0.8 20 MC
Batch P6KO369 - NO PREP
Blank_ (P6K0369-BLK1)
Prepared: 11/16/16 Analyzed: 11/17/16
Nitrate/Nitrite as N
BRL 5.0 mglkg wet
LCS (P6K0369-BS1)
Prepared: 11/16/16 Analyzed: 11/17/16
Nitrate/Nitrite as N
49.3 5.0 mg/kg wet
50.00 99 80-120
Matrix Spike (P6K0369-MS1)
Source: 6110152-01
Prepared: 11/16/16 Analyzed: 11/17/16
Nitrate/Nitrite as N
163 8.6 mg/kg dry
85.75 76.8 100 80-120
Matrix Spike Dup (P6K0369-MSD1)
Source: 6110152-01
Prepared: 11/16/16 Analyzed: 11/17/16
Nitrate/Nitrite as N
163 8.6 mg/kg dry
85.75 76.8 100 80-120 0.05 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone]=Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 9

Full -Service Analytical &
MEnvironmental Solutions
O.WS. LNG
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
'1 t/18/16
Prism Work Order: 6110152
Time Submitted: 11/7/2016 5:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6KO206 - NO PREP
Blank (P6K0206-BLK1)
Prepared &Analyzed: 11/08/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Daterrime
6110152-01
P61<0257
0.05 g
25 mL
11/11/16 10:15
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
6110152-01
P6K0352
1 g
50 mL
11/15/16 11:45
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
6110152-01
P6K0316
30 g
30 g
11/11/16 15:17
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6110152-01
P61<0282
50 mL
50 mL
11/11/16 14:10
6110152-01
P6Ko282
50 mL
50 mL
11/11/16 14:10
6110152-01
P6K0282
50 mL
50 mL
11/11/16 14:10
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daternme
6110152-01
P6K0263
2.05 g
50 mL
11/11/16 8:45
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
6110152-01
P61<0331
0.55 g
50 mL
11/15/16 8:45
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
6110152-01
P61<0281
250 g
250 g
11/10/16 14:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 Of 9

s. CHAIN OF CUSTODY RECORD
IFull -Service Analytical S
S M Environmental Solutions PAGE_ OF _ QUOTE # 80 ENSURE PROPER BILLING: _
LABORATORIES, INC.
449 Springbrook Road - Charlotte, NC 28217 Project Name:
Phone [phone] • Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
• 1, ` "Please ATTACH any project specific reporting (QC LEVEL 111 III IV)
Client Company Name: _ m o ��A'C� S i-': � � provisions and/or QC Requirements
Report To/Contact Name: 50„% ba Invoice To:
Reporting Address: Address:
Samples INTACT upon.arirval?
Received ON WE"r ICE?
PROPER PRESERVATIVES indica,,ed?
Received kNITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSRACE?
PROPER CONTAINERS used?
TEMP: Therm ID:Al2-_I 11 Observed:
YES NO N/A 0)
0
O
CD
0)
1/ °C / Corr:
Phone: �0 �" ��y' 3w Fax es (No): TO A- 3 ��- 5'S purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC Do®
FL NC
EDD Type: PDF_Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re h Work rMust Be
SC OTHER
NIA
Site Location Name: F2.xn4h CRE•ric tfJi;L;T P Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 693 Be.11 rAx., RI Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
;
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sam le Iced tD on Collection: YES
p p
NO
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
REMARKS
PRISM
LAB
*TYPE
COLLECTED
MILITARY
WATER OR
TIVES
��
SAMPLE DESCRIPTION
NO.
SIZE
Oil`'
ID NO.
HOURS
SLUDGE)
SEE BELOW
��
4
ire 30
P
AO.3
�.�b�eekI'
—T
�-�
As
PAd
C9
CW
SAPab
S�
A
Sampler's Signature Gc% c Sampled By (Print Name) /I .r9 /1/ C Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must
be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
°
Relinqu hed By: (Signature) Aeed y: (Signal Date
}J•'/ /;/
Mili ry/Hours
$�Additional Comments:
.A
Site An ival TuneRef
hed By. (Si�alure) Recqi ed By., (Signature) Date
Site Departure Time;
�? /
U
Reli ishe y: (Signs re) Received For P i �J abglathrles y: Date
/�
Field Tech Fee:
Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITWCJJSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST C,91XJINTIL RECEIVED AT THE LABORATORY.
t
Fed Ex ❑ UPS El Hand -delivered 50sm Field Service ❑ Other
ES: UST: G UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL
OTHER:
❑ SCI El ❑ SC NC ❑ SC I ❑ NC ElSC ❑3 NC ❑ SC ❑1 NC ❑ SC ❑ NC El a NC ❑ SC
ONC ElSC
71 El ❑ 0
D
TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

SM
)RATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 11/21/2016
Prism Work Order: 6110436
Case Narrative
12/01 /2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR=[Na]/SQRT{([Ca]+[Mg])/2}
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated With a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Sample Receipt Summary
12/01 /2016
Prism Work Order: 6110436
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaUrrie 6110436-01 Solid 11/21/16 11/21/16
Samples were received in good condition at 4.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 9

Full -Service Analytical 8
Environmental Solutions
ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
12/01/2016
Project: StaLime Client Sample ID: StaLime
Prism Sample ID: 6110436-01
Prism Work Order: 6110436
Sample Matrix: Solid Time Collected: 11/21/16 11:15
Time Submitted: 11/21/16 12:30
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1300
mglkg
380
45
5
'Calculation
12/1/16 10:44
CLB
[CALC]
Solids
66.1
% by
0.100
0.100
1
`SM2540 G
11/28/16 16:07
JLR
P6K0628
Weight
Nitrate/Nitrite as N
78
mg/kg dry
7.6
0.83
1
'SM4500-NO3 F
11/30/16 9:34
CLB
P6K0617
Phosphorus -Total
3700
mg/kg dry
76
36
20
"SM4500-P F
11/23/16 9:17
CLB
P6K0548
Total Kjeldahl Nitrogen
6000
mg/kg dry
1900
210
5
*351.2
12/1/16 10:44
CLB
P6K0592
Ammonia as N
250
mg/kg dry
38
15
5
'SM4500-NH3 G
11/29/16 8:57
CLB
P61<0585
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
'SM9221 E
11/22/16 10:15
EGC
P61<0555
Total Metals
Mercury
0.29
mglkg dry
0.032
0.0018
1
*7471B
11/28/16 13:50
JAB
P6K0579
SAR Soil Preparation
Complete
g
1
'2-78-054
11/29/16 14:00
JAB
P61<0609
SAR Percent Moisture
86.0
% by
0.100
0.100
1
'2-78-054
12/1/16 11:00
JAB
P61-0013
Weight
Arsenic
BRL
mg/kg dry
3.8
0.46
.10
'6010D
11/28/16 20:35
bgm
P6K0574
Sodium Absorption Ratio
0.46
[blank]
0.30
0.016
1
'2-78-054
11/29/16 22:53
bgm
P6K0627
Cadmium
BRL
mg/kg dry
0.37
0.0099
1
'6010D
11/24/16 1:11
bgm
P61<0528
Calcium
1700
mg/L
1.0 .
0.085
10
'6010D
11/29/16 22:53
bgm
P61<0627
Copper
59
mg/kg dry
0.74
0.067
1
'6010D
11/24/16 1:11
bgm
P61(0528
Lead
3.5
mg/kg dry
0.37
0.069
1
'6010D
11/24/16 1:11
bgm
P61(0528
Magnesium
BRL
mg/L
1.0
0.0070
10
'6010D
11/29/16 22:53
bgm
P61<0627
Nickel
6.9
mg/kg dry
0.74
0.027
1
•6010D
11124/16 1:11
bgm
P61<0528
Selenium
13
mg/kg dry
7.4.
1.7
10
'6010D
11/28/16 17:07
bgm
P61(0528
Sodium
450
mg/kg dry
220
7.2
10
'6010D
11/28/16 17:07
bgm
P6K0528
Sodium
69
mg/L
5.0
0.18
10
'6010D
11/29/16 22:53
bgm
P611(0627
Zinc
91
mg/kg dry
37
1.3
10
`601013
11/28/16 17:07
bgm
P6K0528
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Full -Service Analytical &
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-s ING
Level 11 QC Report
1211/16
City of Statesville, NC Project: Stal-ime Prism Work Order: 6110436
Attn: Andy Smith Time Submitted: 11/21/2016 12:30:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6KO528 - 3050B
Blank (P6K0528-BLK1)
Prepared: 11/22/16 Analyzed_11/23/16
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6K0528-BSI)
Prepared: 11/22/16 Analyzed: 11/23/16
_
Cadmium
23.9
0.25
mg/kg wet
25.00 96
80-120
Copper
25.7
0.50
mg/kg wet
25.00 103
80-120
Lead
23.6
0.25
mg/kg wet
25.00 94
80-120
Nickel
24.0
0.50
mg/kg wet
25.00 96
80-120
Selenium
22.9
0.50
mg/kg wet
25.00 92
80-120
Sodium
459
15
mg/kg wet
500.0 92
80-120
Zinc
23.8
2.5
mg/kg wet
25.00 95
80-120
Batch P6KO574 - 3050B
Blank (P6K0574_BLK1)
Prepared &Analyzed_
—
Arsenic
BRL
0.25
rng/kg wet
LCS(P6K_0574-BS_1)
Prepared & Analyzed: 11/28/16
_ _
Arsenic
23.7
0.25
mg/kg wet
25.00 95
80-120
Batch P6KO579 - 7471 B
Blank (P6K0579-BLK1)
Prepared &Analyzed: 11/28/16
Mercury
BRL
0.020
mg/kg wet
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M I Full -Service Analytical &
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I'm INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
12/1/16
Prism Work Order: 6110436
Time Submitted: 11/21/2016 12:30:OOPM
. Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P61K0579 - 7471 B .
LCS (P6KO579-BSI)
Prepared & Analyzed: 11/28/16
Mercury
0.433
0.020
mg/kg wet
0.4167 104 80-120
Batch P61K0609 - SAR 2-78-054
Blank (P6KO609-BLK1)
-----
Prepared: 11/28/16 Analyzed: 11/29/16
------- —
SAR Soil Preparation
- ----
Complete
g
----- ---------------------
Batch P6KO627 - 3010A
Blank (P6KO627-BLK1)
Prepared & Analyzed: 11/29/16
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
Batch P6L0013 - NO PREP
Duplicate (P611-0013-DUP1) _--source: 6110436-01 Prepared: 11/29/16 Analyzed: 12101/_16
SAR Percent Moisture 85.0 0.100 % by Weight 86.0 1 200
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S ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
12/1/16
Prism Work Order: 6110436
Time Submitted: 11/21/2016 12:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P61<0548 - SM4500-PB5
Blank(P6K0548-BLK1)_ Prepared:11122/16 Analyzed:11/23/16_
Phosphorus -Total BRL 2.5 mg/kg wet
LC_S (P6KO548-B_S_1) - _ _ Prepared: 11/22/16 Analyzed: 11/23/16
Phosphorus -Total 94.5 2.5 mg/kg wet 100.0 94 90-110
Matrix Spike (P_6_K_0.54_8_-MS1) _ _ __ __ Source: 6110436-01 _Prepared: 11/22/16 Analyzed: 11/23/16 _
Phosphorus -Total 3610 76 mg/kg dry 151.2 3690 NR 80-120 MC
Matrix Spike Dup (P6KO548-MSD1) - Source: 6110436-01 Prepared: 11/22116-Analyzed_11/23/16
Phosphorus -Total 3530 76 mg/kg dry 151.2 3690 NR 80-120 2 20 MC
Batch P6K0585 - NO PREP
Blank (P6K0585-BLK1) _—_
_
Prepared: 11/28/16 Analyzed: 11/29/16 —
Ammonia as N
BRL 5.0
mg/kg wet
LCS (P6K0585-BS1)
_____Prepared:
11/28/16 Analyzed: 11/29/16 --------- -
Ammonia as N
122 5.0
mg/kg wet
125.0 97 80-120
Matrix Spike (P6KO585-MS1)
Source: 6110436_01 -
Prepared_ 11/28/16 Analyzed: 11/29116
Ammonia as N
443 38
mg/kg dry
189.0 249 103 80-120
Matrix S_pike_Dup (P6KO585_MSD1)
Source: 6110436-01 —Prepared:
11/28/16 Analyzed: 11/29/16
Ammonia as N
452 38
mg/kg dry
189.0 249. 108 80-120 2 20
Batch P6KO592 - 351.2
Blank P6KO592-BLK1
Prepared: 11/28/16 Analyzed: 12/01/16
Total Kjeldahl Nitrogen
BRL 25
mg/kg wet
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Full -Service Analytical &
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S INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Level II QC Report
12/1 /16
Prism Work Order: 6110436
Time Submitted: 11/21/2016 12:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6KO592 - 351.2
LCS (P6K0592-BS1)
Prepared: 11/28/16 Analyzed: 12/01/16
Total Kjeldahl Nitrogen
483 100 mglkg wet
500.0 97 90-110
Batch P6KO617 - NO PREP
Blank (P6KO617-BLK1)
Prepared: 11/29/16 Analyzed: 11/30/16
Nitrate/Nitrite as N
BRL 5.0 mglkg wet
LCS_(P6K0617-BS1)
Prepared: 11/29/16 Analyzed: 11/30/16
Nitrate/Nitrite as N
54.4 5.0 mg/kg wet
50.00 109 80-120
Matrix Spike (P6K0617-MS1)
Source: 6110436-01
Prepared: 11/29/16 Analyzed: 11/30/16
Nitrate/Nitrite as N
116 7.6 mg/kg dry
75.61 78.2 49 80-120 MI
Matrix Dup_(P6K0617-MSD1)
Source: 6110436-01
Prepared: 11/29/16 Analyzed11/30/16
-Spike
Nitrate/Nitrite as N
115 7.6 mg/kg dry
75.61 78.2 49 80-120 0.6 20 MI
Batch P6KO628 - Solids, Dry Weight
Duplicate (P6KO628-DUP1) _
Source: 6110436-01
Prepared & Analyzed: 11/28/16
% Solids
66.1 0.100 % by Weight 66.1 0 20
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City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level 11 QC Report
12/1/16
Prism Work Order: 6110436
Time Submitted: 11/21/2016 12:30:OOPM
Reporting Spike Source %REC
RPD
Analyte
Result
Limit Units Level Result %REC Limits RPD
Limit Notes
Batch P6KO555 - NO PREP
Blank (P6KO555-BLK1)
Prepared & Analyzed_ 11/22/16
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final Daterrime
6110436-01
P61<0592
0.05 g
25 mL 11/28/16 11:15
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final Daterrime
6110436-01
P61<0548
1 g
50 mL 11/22/16 16:35
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final Daterrime
6110436-01
P61<0628
30 g
30 g 11/28/16 16:07
Prep Method: 3010A
Lab Number
Batch
Initial
Final DateMme
6110436-01
P61<0627
50 mL
50 mL 11/29/16 14:00
6110436-01
P61<0627
50 mL
50 mL 11/29/16 14:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final Daterrime
6110436-01
PBK0574
1.99 g
50 mL 11/28/16 8:20
6110436-01
P61<0528
2.05 g
50 mL 11/22/16 9:40
6110436-01
P61<0528
2.05 g
50 mL 11/22/16 9:40
Prep Method: 7471B
Lab Number
Batch
Initial
Final Date/Time
6110436-01
P61<0579
0.56 g
50 mL 11/28/16 9:07
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final Daterrime
6110436-01
PBK0609
250 g
250 g 11/28/16 14:00
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Phone [phone] Fax: [phone] Received VVITHIN HOLDING TIMES? a.
e , C. 'Please ATTACH any project specific reporting (QC LEVEL I II III IV) � --- --
Client Company Name: �- ^ �%y ' ,-p -a A� �`� � provisions and/or QC Requirements CUSTODY SEALS 11V"rACT�
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Reporting Address: PROPER CONTAINERS used" _
p g Address: TEMP:_ "C henn iD: � � Ohserved. °C , orr. {._, ..�°C
( ) Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
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Site Location Physical Address: 6 `� �. �p �! , Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_,_ NO
Y (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_
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CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSIS REQUESTED
�$ REMARKS
d q,
_-
PRISM
LAB
ID NO.
*TYPE
SEE BELOW
NO
SIZE
d
r
v-d
—�---
i
µ� 6
O
,�
.SS A
u,
lam
Sampler's Signature OT� r
Sampled By (Print Name) R, GL)' %"%C �
Affiliation
Site Arrival lime ;
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
ate Military)Hours
Relin(Signature J� _..,.. Additional Comments:
�all��jjshed By: (Signature) Receiv By:
Y/l �` /"'� .�•�'x f �`�_ "ram/`i"� ��at4.1
Relin ed By: (Signature) G1 Received By: {Signature)
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SAMPLES ARE NOT CEPTED AND VERIFIED AGAINST C NTIL RECEIVED AT THE LABORATORY.
n Other
COC Group No.
f uy 12 p
ea tx u ur i u nand-d.li a eu �. nimn .c.�..G�.... -• •--••-•
ES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: ,
❑SCI ❑NC ❑SC I ®NC El SC I DNC ❑SC I ❑❑NC ❑SC 111NC❑SCI ElNC ❑SC ONC ❑SC ❑❑NC ❑SC
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Full -Service Analytical &
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Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 12/05/2016
Prism Work Order: 6120098
Case Narrative
12/14/2016
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR = [ Na j / SQRT { ([Ca) + [Mgj) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V l..
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
A Initial Calibration Verification standard recovery (111 %) is greater than the upper control limit (105%). Result might
have a high bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
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Sample Receipt Summary
12/14/2016
Prism Work Order: 6120098
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 6120098-01 Solid 12/05/16 12/05/16
Samples were received at 18.2 degrees C. See case narrative for further information.
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I`- I Full -Service Analytical &
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City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
12/14/2016
Project: StaLime Client Sample ID: Sta-Lime
Prism Sample ID: 6120098-01
Prism Work Order: 6120098
Sample Matrix: Solid Time Collected: 12/05/16 15:10
Time Submitted: 12/05/16 17:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Dateffime ID
General Chemistry Parameters
Plant Available Nitrogen
930
mg/kg
380
45
5
*Calculation 12/12/16 8:14
CLB
[CALC]
% Solids
70.5
% by
0.100
0.100
1
*SM2540 G 12/8/16 16:31
JLR
P6L0190
Weight
Nitrate/Nitrite as N
40
mg/kg dry
7.1
0.78
1
*SM4500-NO3 F 12/8/16 11:06
CLB
P61-0131
Total Kjeldahl Nitrogen
4200
mg/kg dry
1800
200
5
*351.2 12/12/16 8:14
CLB
P6L0116
Ammonia as N
100
mg/kg dry
35
14
5
*SM4500-NH3 G 12/7/16 9:04
CLB
P6L0096
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
12/6/16 11:13
BMS
P61-0120
Total Metals
Mercury
0.10
mg/kg dry
0.027
0.0015
1
*7471B
12/8/16 13:06
JAB
P6L0141
SAR Soil Preparation
Complete
g
1
*2-78-054
12/8/16 12:00
JAB
P61-0123
SAR Percent Moisture
81.7
% by
0.100
0.100
1
*2-78-054
12/8/16 13:00
JAB
P6L0182
Weight
Arsenic
6.0
mg/kg dry
3.6
0.44
10
*6010D
12/13/16 17:04
bgm
P6L0108
Sodium Absorption Ratio
0.41
[blank]
0.30
0.016
1
*2-78-054
12/13/16 17:38
bgm
P6L0154
Cadmium
BRL
mg/kg dry
3.6
0.096
10
*6010D
12/13/16 17:04
bgm
P61-0108
Calcium
1300 BH
mg/L
20
1.7
200
*6010D
12/13/16 17:46
bgm
P6L0154
Copper
50
mg/kg dry
7.2
0.65
10
*6010D
12/13/16 17:04
bgm
P6L0108
Lead
4.8
mg/kg dry
3.6
0.67
10
*6010D
12/13/16 17:04
bgm
P6L0108
Magnesium
BRL
mg/L
1.0
0.0070
10
*6010D
12/10/16 1:44
bgm
P61-0154
Nickel
9.2
mg/kg dry
7.2
0.26
10
*6010D
12/13/16 17:04
bgm
P6L0108
Selenium
13
mg/kg dry
7.2
1.7
10
*601OD
12/13/16 17:04
bgm
P6L0108
Sodium
54 A
mg/L
5.0
0.18
10
*6010D
12/10/16 1:44
bgm
P61L0154
Zinc
91
mg/kg dry
36
1.3
10
*6010D
12/13/16 17:04
bgm
P6L0108
This report should not be reproduced,.except in, its. entirety, without the written consent of Prism Laboratories, Inc.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
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�I I -Service Analytical &
ivironmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime
Level II QC Report
12/14/16
Prism Work Order: 6120098
Time Submitted: 12/5/2016 5:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 1361-0108 - 3050B
Blank (P6LO108-BLK1)
_
Prepared: 12/07/16 Analyzed: 12/13/16
Arsenic
BRL
0.25
__
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P6L0108-BS1) _
_
Prepared_ 12/07/16 Analyzed: 12/13/16
Arsenic
24.1
0.25
mg/kg wet
25.00 96 80-120
Cadmium
24.3
0.25
mg/kg wet
25.00 97 80-120
Copper
27.0
0.50
mg/kg wet
25.00 108 80-120
Lead
24.6
0.25
mg/kg wet
25.00 98 80-120
Nickel
24.9
0.50
mg/kg wet
25.00 100 80-120
Selenium
23.0
0.50
mg/kg wet
25.00 92 80-120
Zinc
25.1
2.5
mg/kg wet
25.00 101 80-120
Batch P61-0123 - SAR 2-78-054
Blank (1361-0123-BLK1) _
_
Prepared: 12/07/16 Analyzed: 12/08/16
SAR Soil Preparation
Complete
g
Batch P61-0141 - 7471 B
Blank (P61-0141-BLK1)
—
------
Prepared- & Analyzed: 12/08/16
Mercury
BRL
0.020
mg/kg wet
-------- ------ -------------- --- --- -- —
This report should not be reproduced, except in its,entirety, without the written consent of Prism Laboratories Inca
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax, 704/525-0409 Page 4 Of 9

lll-Service Analytical &
ivironmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Level II QC Report
12/14/16
Prism Work Order: 6120098
Time Submitted: 12/5/2016 5:55:OOPM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units Level Result %REC Limits RPD Limit Notes
Batch P61_0141 - 7471 B
LCS (P6LO141-BS1)
—
Prepared &Analyzed: 12/08/16
Mercury
0.399
0.020
mg/kg wet 0.4167 96 80-120 -- -- — --_ — --
Batch P6L0154 - 301 OA
Blank (P6LO154-BLK1) _
_
_ Prepared: 12/08/16 Analyzed: 12/13/16
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L BH
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
Batch P611_0182 - NO PREP
Duplicate (13611_0182-DUP1) _ _
Source: 6120098-01 __Prepared & Analyzed: 12/08/16
SAR Percent Moisture
84.3
0.100 % by Weight 81.7 3 200
This report should not be reproduced, except in its entirety, without,the written consent of Prism Laboratories,. Inc.- , -
449 Springbrook Road P.O. Box 240543 - Charlotte, NC 28224-0543
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t Full -Service Analytical &
I S M
Environmental Solutions
LA80RATORIES INO.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Reporting
Analyte Result Limit Units
Batch P61LO096 - NO PREP
Level II QC Report
12/14/16
Prism Work Order: 6120098
Time Submitted: 12/5/2016 5:55:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P6L0096-BLK1) Prepared: 12/06/16 Analyzed: 12/07/16
Ammonia as N BRL 5.0 mg/kg wet ----------- ------ -_- -
LCS (P6L0096-BS1) _- _ _ Prepared: 12/06/16 Analyzed: 12/07/16
Ammonia as N 126 5.0 mg/kg wet 125.0 101 80-120
Matrix Spike (P6L0096-MS1) Source: 6120098-01 Prepared: 12/06/16 Analyzed: 12/07/16
Ammonia as N 265 35 mg/kg dry 177.3 103 91 80-120
Matrix Spike Dup (P6L0096-MSD1) Source: 6120098-01 Prepared: 12/06/16 Analyzed: 12/07/16
_--------- —------------- ---------- - --- -- ---- ----------------_ .----
Ammonia as N 261 35 mg/kg dry 177.3 103 89 80-120 1 20
Batch P6L0116 - 351.2
Blank (P6L0116-BLK1)
Prepared: 12/07/16 Analyzed: 12/12/16
Total Kjeldahl Nitrogen
BRL 25
mg/kg wet
LCS (P6L0116-BS1)
Prepared: 12/07/16_An_alyzed: 12/12/16
Total Kjeldahl Nitrogen
492 100
mg/kg wet
500.0 98 90-110
Matrix Spike (P6L0116-MS1)
Source: 6120098-01
Prepared: 12/07/16 Analyzed: 12/12/16
Total Kjeldahl Nitrogen
11300 1800
mg/kg dry
7092 4200 100 90-110
Matrix Spike Dup (P6L0116-MSD1)
- Source: 6120098-01
Prepared: 12/07/16 Analyzed: 12/12/16
Total Kjeldahl Nitrogen
11800 1800
mg/kg dry
7092 4200 107 90-110 4 20
Batch P6L0131 - NO PREP
Blank (P6L0131-BLK1)
- _
Prepared & Analyzed: 12/08/16
Nitrate/Nitrite as N
BRL 5.0
mg/kg wet
This report should not be reproduced, except in,its entirety, without the written consent of Prism Laboratories, Inc.-
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II -Service Analytical &
vironmental Solutions
Level II QC Report
12/14/16
City of Statesville, NC Project: StaLime Prism Work Order: 6120098
Attn: Andy Smith Time Submitted: 12/5/2016 5:55:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P61_0131 - NO PREP
LCS (P61-0131-13SI) Prepared &Analyzed: 12/08/16
Nitrate/Nitrite as N 49.4 5.0 mg/kg wet 50.00 99 80-120
Batch P61_0190 - Solids, Dry Weight
Duplicate (P61-0190-DUP1) _ Source: 6120098-01 Prepared &Analyzed: 12/08/16
% Solids 79.8 0.100 % by Weight --- 70.5 --- --- — 12-- 20 —
This report should not be reproduced, except.in its entirety,,without the written consent.of Prism Laboratories, Inc:
449 Springbrook Road - P.O. Box 240543 -,Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364- Fax: [phone] Page 7 Of 9

ill -Service Analytical &
ivironmental Solutions
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
12/14/16
Prism Work Order:.6120098
Time Submitted: 12/5/2016 5:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P611-0120 - NO PREP
Blank (P6LO120-BLK1) Prepared & Analyzed: 12/06/16
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Daterrime
6120098-01 P61-0116
Prep Method: Solids, Dry Weight
Lab Number Batch
0.05
Initial
g
25 mL
Final
12/07/16 9:50
Daterrime
6120098-01
P61-0190
30
g
30 g
12/08/16 16:31
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
6120098-01
P61-0154
50
mL
50 mL
12/08/16 13:00
6120098-01
P61-0154
50
mL
50 mL
12/08/16 13:00
6120098-01
P61-0154
50
mL
50 mL
12/08/16 13:00
Prep Method:3050B
Lab Number
Batch
Initial
Final
Daterrime
6120098-01 P61-0108 1.98 g 50 mL 12/07/16 8:05
Prep Method: 7471B
Lab Number Batch Initial Final DateMme
6120098-01 P61L0141 0.62 g 50 mL 12/08/16 9:40
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Daterrime
6120098-01 P610123 250 g 250 g 12/07/16 12:00
This report should not be reproduced, except_in its entirety, without the written consent of Prism Laboratories, I,nc.,. .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 79

11111111114111110
CNANN OF CUSTODY RECORD
W a
ti
Full -Service Analytical &
Environmental
� -
YES I\O NIA
(M
Solutions
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
`LABORATORIES, INC.
Sarnples INTACiTU(JC r! lll!1�211? ..
✓_ _ .:
Q
449 Spsingtarook Road Charlotte, NC 28217
Project Name:
Receiveo-ON WET ICE?
k'
--
Phone [phone]
Fax: [phone]
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER PRESERVATIVES indue:ledTCD
Client Company Name: r•
�/'
d 5A e.sv:fld
*Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV)
Received WITHIN HOLDING TIM =S'
--
-- —-
Report To/Contact Name:
Aml% Jr'° -,.-BIZ
provisions and/or QC Requirements
CUSTODY SEALS iN rAc L`r
— --`
Invoice To:
VOLATILE rec'd W/OUT HEADSPACE"
Reporting Address:
Address:
PROP ER.CONTAINERS used.
:TEMP:;Therm ID: l%LT' 6 I Observed
/i'C /Corr: (J',2°C
'
Valuff IC. " a r"dA4rUZi4(I4V)C
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL '
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF,Excel _Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ P e h Work Must Be
Site Location Name: f�zr 4 J1i CreeA QV C:, aT1O
Scoved OTHER
N/A
Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 01 13 A•
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
..
NO_
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
CLIENT
DESCRIPTION
DATE
COLLECTED
(SOIL,
PRESERVA-
�� REMARKS
PRISM
SAMPLE
COLLECTED
MILITARY
WATER OR
•TYPE
TIVESLAB
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
ty ��
ID NO.
As
PA
14
CR
C ;
S°A
ph
Se
Sampler's Signature �'�.�e.�
d
�5
,.
..
Sampled By
(Print Name) A ✓' A' I I�' Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be chqrges
for any changes after analyses have been initialized.
Rellnq hed By: Signa ure) « Rec iv By: (Si o 6 Date
�� y f%
/i' C ✓� ✓ " /
Milita / ours
ry Additional Comments:
!—
C
Site Arrival Time: `
Reli sh By: (Signature) _ r% RbdeNed
By: (Signal re)~ Date
Site Departure Time,,
Relinq 's By:(Signature) Received For Pr' a bor 6 S B .: Date
FieldTech Fee
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WIT
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO
STODY SEA S FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
Ibl_ RECEIVED AT THE LABORATORY.
Iviileago:
�7
(� 00
Fed Ex Cl UPS ❑ Hand -delivered lirism Field Service ❑ Other
ES: UST: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
TOVNDWATER:
❑SC ❑NC ❑SC C El SC ❑NC ❑SC
I El NC ❑SC ❑NC❑SC ❑NC El SC El NC ❑SC ❑NC ❑SC
'
❑ ® ®
- ❑-- ❑ ❑ ❑ I
n
R TYPE CODES: A = Amber C = Clear G= Glass P = Plastic: TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

0
i, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime (60 Day/7 Fecal)
Lab Submittal Date: 12/20/2016
Prism Work Order: 6120365
Case Narrative
01 /02/2017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BL MB greater than one half of the RL, but the sample concentrations are less than the RL.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entircty,wifh'out the written conserif of Prism Laboratories; Inc:
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Full -Service Analytical 8
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Sample Receipt Summary
01 /02/2017
Prism Work Order: 6120365
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime (and Fecal 1)
6120365-01
Solid
12/20/16
12/20/16
Fecal #2
6120365-02
Solid
12/20/16
12/20/16
Fecal #3
6120365-03
Solid
12/20/16
12/20/16
Fecal #4
6120365-04
Solid
12/20/16
12/20/16
Fecal #5
6120365-05
Solid
12/20/16
12/20/16
Fecal #6
6120365-06
Solid
12/20/16
12/20/16
Fecal #7
6120365-07
Solid
12/20/16
12/20/16
Samples were received in good condition at 4.0 degrees C unless otherwise noted.
-This report should nofbe reproduced, except in its 'entirety; without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of:,5

Full -Service Analytical 8
Environmental Solutions
Laboratory Report
01 /02/2017
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: StaLime (and Fecal 1)
Attn: Andy Smith
Prism Sample ID: 6120365-01
P.O. Box 1111
Prism Work Order: 6120365
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1100
mg/kg
380
45
5 *Calculation 12/28/16 8:40
CLB
ICALC]
Solids
62.4
% by
0.100
0.100
1 *SM2540 G 12/21/16 16:13
JLB
P6L0378.
Weight
Nitrate/Nitrite as N
72
mg/kg dry
8.0
0.88
1 *SM4500-NO3 F 12122/16 10:11
CLB
P6L0367
Total Kjeldahl Nitrogen
5700
mg/kg dry
2000
230
5 *351.2 12/28/16 8:40
CLB
P6L0393
Ammonia as N
110
mg/kg dry
40
15
5 *SM4500-NH3 G 12127/16 9:29
CLB
P611-0386
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 12/20/16 14:18
BMS
P61-0358
Total Metals
Mercury
SAR Soil Preparation
SAR Percent Moisture
Arsenic
Sodium Absorption Ratio
Cadmium
Calcium
Calcium
Copper
Lead
Magnesium
Magnesium
Nickel
Selenium
Sodium
Sodium
BRL
Complete
60.8
6.0
0.56
0.52
1500
370000
45
4.8
2500
BRL
9.2
1.6
570
79
mg/kg dry
0.034
0.0019
1
9
1
by
0.100
0.100
1
Weight
mg/kg dry
2.4
0.21
10
[blank]
0.30
0.016
1
mg/kg dry
0.40
0.18
10
mg/L
5.0
0.42
50
mg/kg dry
320
91
200
mg/kg dry
0.80
0.16
10
mg/kg dry
0.40
0.16
10
mg/kg dry
8.0
1.5
10
mg/L
1.0
0.0070
10
mg/kg dry
0.40
0.13
10
mg/kg dry
1.6
0.16
10
mg/kg dry
160
46
10
mg/L
5.0
0.18
10
*7471 B
12/22/16 15:11
JAB
P6L0374
*2-78-054
12/28/16 9:05
JAB
P610410
*2-78-054
12/29/16 14:55
JAB
P61-0422
*6020B
12/22/16 17:48
gmart
P61-0376
*2-78-054
12/30/16 18:08
bgm
P611-0421
*6020B
12/22/16 17:48
gmart
P611-0376
*6010D
12/30/16 18:16
bgm
P6L0421
*6020B
12/28116 17:31
bgm
P6L0376
*6020B
12/22/16 17:48
gmart
P61-0376
*60208
12/22/16 17:48
gmart
P6L0376
*6020B
12/22116 17:48
gmart
P6L0376
*6010D
12/30/16 18:08
bgm
P61-0421
*6020B
12/22116 17:48
gmart
P611-0376
*6020B
12/22/16 17:48
gmart
P611-0376
*6020B
12/22/16 17:48
gmart
P6L0376
*6010D
12/29/16 2:59
bgm
P6L0421
-- - 'This report shouldnot be reproduced; except in its, entirety; without the written consent of Prism Laboratories,.lnc. ,
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Full -Service Analytical 8
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01 /02/2017
Client Sample ID: Fecal #2
Prism Sample ID: 6120365-02
Prism Work Order: 6120365
Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 58.7
% by
0.100
0.100 1
'SM2540 G 12/21/16 16:13 JLB
P61_0378
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 12/20/16 14:18 BMS
P61_0358
_. .
"its'entirety, without written consent of Prism Laboratories, Inc.
This report should not be reproduced, except
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01 /02/2017
Client Sample ID: Fecal #3
Prism Sample ID: 6120365-03
Prism Work Order: 6120365
Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 59.5
% by
0.100
0.100 1
`SM2540 G 12/21/16 16:13 JLB
P61-0378
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 12/20/16 14:18 BMS
P61-0358
This report should not be reproduced, except in its entirety,, without the written consent of I'nsm Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 Of 1 rJ

Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
01 /02/2017
Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #4
Prism Sample ID: 6120365-04
Prism Work Order: 6120365
Sample Matrix: Solid Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter
Result Units Report MDL Dilution Method
Analysis Analyst Batch
Limit Factor
Dateffime
ID
General Chemistry Parameters
Solids
60.2 % by 0.100 0.100 1 *SM2540 G
12/21/16 16:13
JLB 1361L0378
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3 1 *SM9221 E
12/20/16 14:18
BMS P6L0358
This report should not be reproduced, except in its entirety; without the written consent of Prism Laboratories, Inc. • :...
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 6 Of 15

P/AofR
Laboratory Report
I S M I Full -Service Analytical 8
01/02/2017
Environmental Solutions
- IABOPAT ES ING
City of Statesville, NC
Project: Stal-ime (60 Day/7 Fecal)
Client Sample ID: Fecal #5
Attn: Andy Smith
Prism Sample ID: 6120365-05
P.O. Box 1111
Prism Work Order: 6120365
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateTme
ID
General Chemistry Parameters
Solids 58.7
% by
0.100 0.100
1 'SM2540 G 12/21/16 16:13 JLB
P61_0378
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 12/20/16 14:18 BMS
P61_0358
This report should not be reproduced, except in Its entirety, without ttie written consent of Prism Laboratories, Inc:
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 15

Full -Service Analytical 8
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory .Report
01 /02/2017
Project: StaLime (60 Day/7 Fecal) Client Sample ID: Fecal #6
Prism Sample ID: 6120365-06
Prism Work Order: 6120365
Sample Matrix: Solid Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 59.3 % by 0.100 0.100 1 'SM2540 G 12/21/16 16:13 JLB P61_0378
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 12/20/16 14:18 BMS P61_0358
This report should not be"reproduced; except in ifs "entirety;'wlthout the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 15

Fun -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01 /02/2017
Client Sample ID: Fecal #7
Prism Sample ID: 6120365-07
Prism Work Order: 6120365
Time Collected: 12/20/16 11:50
Time Submitted: 12/20/16 13:15
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateRme
ID
General Chemistry Parameters
% Solids 62.4
% by
0.100
0.100 1
'SM2540 G 12121/16 16:13 JLB
P61-0378
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 12/20/16 14:18 BMS
P61-0358
This report should not be'rep�oduced,'ezce'pt in its entirety; with'outthe written consent of Prism Laboratories, Inc;,,
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of �J

Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime (60 Day/7 Fecal)
Level II QC Report
1 /2117
Prism Work Order: 6120365
Time Submitted: 12/20/2016 1:15:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6L0374 - 7471 B
Blank (P6L0374-BLK1) Prepared & Analyzed:. 12/22/16 —_
Mercury BRL 0.020 mg/kg wet
LCS (P6L0374-BS1)_ Prepared & Analyzed: 12/22/16
--------- -------------------------
Mercury 0.439 0.020 mg/kg wet 0.4167 105 80-120
Batch P6L0376 - 3050B
Blank_(P6L0376-BLK1)
Prepared &Analyzed: 12/22/16
Arsenic
BRL
1.5
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Calcium
BRL
10
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Magnesium
BRL
5.0
mg/kg wet
Nickel
BRL
0.25
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Sodium
BRL
100
mg/kg wet
LCS (P6L0376-BS1)
—
_
_
Prepared & Analyzed: 12/22/16
Arsenic
22.6
1.5
mg/kg wet
25.00 91
80-120
Cadmium
24.4
0.25
mg/kg wet
25.00 97
80-120
Calcium
475
10
mg/kg wet
500.0 95
80-120
Copper
23.5
0.50
mg/kg wet
25.00 94
80-120
Lead
24.4
0.25
mg/kg wet
25.00 97
80-120
Magnesium
486
5.0
mg/kg wet
500.0 97
80-120
Nickel
23.8
0.25
mg/kg wet
25.00 95
80-120
Selenium
22.1
1.0
mg/kg wet
25.00 88
80-120
Sodium
531
100
mg/kg wet
500.0 106
80-120
BH
ThisYepotYshould not be reproduced, except in its entirety,' without the written consent of Prism Laboratories; Inc:
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 15

Full -Service Analytical &
Environmental Solutions
Level II QC Report
1/2/17
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Prism Work Order: 6120365
Attn: Andy Smith Time Submitted: 12/20/2016 1:15:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6L0410 - SAR 2-78-054
Blank (P611-0410-BLK1)
_ —
Prepared: 12/27/16 Analyzed: 12/28/16
SAR Soil Preparation
Complete
g
Batch P6L0421 - 3010A
Blank (P6L0421-BLK1)
Prepared: 12/28/16 Analyzed: 12/29/16
Sodium Absorption Ratio
BRL
3.0 [blank]
Calcium
BRL
1.0 mg/L
Magnesium
1.57
1.0 mg/L BL
Sodium
BRL
5.0 mg/L
Batch P6L0422 - NO PREP
Blank (P611-0422-BLK1)
-- _ Prepared: 12/28/16 Analyzed: 12/29/16
SAR Percent Moisture
BRL
0.100 % by Weight
Duplicate (P611-0422-DU_P1)
Source_: 6120365-01 Prepared: 12/28/16_ Analyzed_ 12/29/16
SAR Percent Moisture
60.8
0.100 % by Weight 60.8 0 200
_ -..
This reportsFiouldnot 6e reproduced; except ih'its entirety;'withouf'th written consent of Prism Laboratories, Inc,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page l l Of 5

Full -Service Analytical &
Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P6LO367 - NO
Level II QC :Report-
1 /2/17,...
Project: StaLime (60 Day/7 Fecal) Prism Work Order: 6120365
Time Submitted: 12/20/2016 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P6L0367-BLK1) Prepared & Analyzed: 12/22116_
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P6LO367-BS1) Prepared & Analyzed: 12/22/16
Nitrate/Nitrite as N 49.6 5.0 mg/kg wet 50.00 99 80-120
Matrix Spike (P6LO367-MS1) Source: 6120365-01 Prepared & Analyzed: 12/22/16
Nitrate/Nitrite as N 104 8.0 mg/kg dry 80.09 71.7 41 80-120 MI
Matrix Spike Dup (P611-0367-MSD1) Source: 6120365-01 Prepared & Analyzed: 12/22/16
Nitrate/Nitrite as N 105 8.0 mg/kg dry 80.09 71.7 41 80-120 0.2 20 MI
Batch PK0378 - Solids Dry Weight
Duplicate (P6LO378-DUP3) Source: 6120365-07 Prepared & Analyzed: 12/21/16 _ __ _
% Solids 61.2 0.100 % by Weight 62.4 2 20
Batch P61LO386 - NO PREP
Blank (P6LO386_BLK1) _ Prepared & Analyzed_12127/16
Ammonia as N BRL 5.0 mg/kg wet
LC_S (P6LO386-BSI) Prepared &Analyzed_12/27/16
Ammonia as N 125 5.0 mg/kg wet 125.0 100 80-120
Matrix Spike (P6L0386-MS1) _ Source: 6120365-01 Prepared & Analyzed: 12/27/16
Ammonia as N 423 40 mg/kg dry 200.2 109 157 80-120 MI
This Feport'should not be reproduced; except in its entirety; withouYthe written consent of Prism Laboratories; Inc. •- •='.• ' -•-
449 S rin brook Road - P O Box 240543 - Charlotte NC 28224-0543
P 9
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 Of 15

Full -Service Analytical &
Environmental Solutions
Level II QC Report
1 /2/17
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Prism Work Order: 6120365
Attn: Andy Smith Time Submitted: 12/20/2016 1:15:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6LO386 - NO PREP
Matrix Spike Dup (P6L0386-MSD_1) _ Source: 6120365-01 Prepared & Analyzed: 12/27/16
Ammonia as N 426 40 mg/kg dry 200.2 109 158 80-120 0.6 20 MI
Batch P6LO393 - 351.2
Blank (P6L0393-BLK1) Prepared: 12/27/16 Analyzed: 12/28/16
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P6LO393-BS1) Prepared: 12/27/16 Analyzed: 12/28/16
Total Kjeldahl Nitrogen 480 100 mg/kg wet 500.0 96 90-110
Matrix Spike (P6LO393-MS1) Source: 6120365-01 Prepared: 12/27/16 Analyzed: 12/28/16 -------
Total Kjeldahl Nitrogen 6460 2000 mg/kg dry 8009 5670 10 90-110 MI
Matrix Spike Dup (P6L0393-MSD1) Source: 6120365-01 Prepared: 12/27/16 Analyzed: 12/28/16
Total Kjeldahl Nitrogen 6190 2000 mg/kg dry 8009 5670 6 90-110 4 20 MI
- - This`re 'ort should not be'ie 'rodticed, except in'its•entire p p p ty; without the written consent of Prism Laboratories; Inc. -.. •, ,;.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1.800/529-6364-'Fax: [phone] Page 13 Of 15

Full -Service Analytical &
Environmental Solutions
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime (60 Day/7 Fecal)
Level II QC Report
1 /2/17
Prism Work Order: 6120365
Time Submitted: 12/20/2016 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P6LO358 - NO PREP
Blank (P6L0358-BLK1) Prepared & Analyzed: 12/20/16
Fecal Coliforms BRL 0.2 MPN/g wet
Duplicate (P6L0358_DUP1) _ _ _ Source: 6120365-01 Prepared & Analyzed: 12/20/16
Fecal Coliforms BRL 0.3 MPN/g dry BRL 20
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
6120365-01
P61_0393
0.05
g
25 mL
12/27/16 10:35
Prep Method: Solids, Dry
Weight
Lab Number
Batch
Initial
Final
Date/Time
6120365-01
P61_0378
30
g
30 g
12/21/16 16:13
6120365-02
P61_0378
30
g
30 g
12/21/16 16:13
6120365-03
P61_0378
30
g
30 g
12/21/16 16:13
6120365-04
P61_0378
30
g
30 g
12/21/16 16:13
6120365-05
P61_0378
30
g
30 g
12/21/16 16:13
6120365-06
P61_0378
30
g
30 g
12/21/16 16:13
6120365-07
P61_0378
30
g
30 g
12/21/16 16:13
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Datemme
6120365-01
P61_0421
50
mL
50 mL
12/28/16 9:20
6120365-01
P61_0421
50
mL
50 mL
12/28/16 9:20
6120365-01
P61_0421
50
mL
50 mL
12/28/16 9:20
6120365-01
PBL0421
50
mL
50 mL
12/28/16 9:20
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Datefrime
6120365-01
P61_0376
2.01
g
50 mL
12/22/16 8:45
6120365-01
P61_0376
2.01
g
50 mL
12/22/16 8:45
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime "
6120365-01
P61_0374 0.57 g 50 mL 12/22/16 10:38
Prep Method: SAR 2-78-054
Lab Number
Batch Initial Final Datefrime
6120365-01
P61_0410 250 g 250 g 12/27/16 9:05
This repoit'should'not be reproduced;' except in its en5rety; without the written consent of Prism Laboratories, Inc:
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Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 15

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