WQ0006245_Regional Office Historical File Pre 2018 (7)

- _ - - -- -
i
ROY COOPER
Governor
j MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Director
■
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
RECEIPT # 7018 0360 0002 2099 0881
Mr. Andy Smith, Operations Manager
City of Statesville
P.O. Box 1111
State-svi4I4e NNorth-Earolina--28f68T
Dear Mr. Smith:
FILE
NORTH CAROLINA
Environmental Quality
April 30, 2019
Subject: NOTICE OF DEFICIENCY
NOD-2019-PC-0105
City of Statesville
Permit WQ0006245 Sta—Lime Distribution Program
Iredell County
The Mooresville Regional Office (MRO) has received and reviewed the 2018 Annual Report
(AR) for the above permit.
The Annual Report is not in compliance with the permit. The review of the Annual Report
revealed continued reporting deficiencies that have been identified in reviews of previously
submitted Annual Reports.
Condition III.3(4), requires that the wastewater effluent be sampled for the following parameters:
• Plant Available Nitrogen (PAN, by calculation)
• Sodium Absorption Ration (SAR, by calculation)
These parameters continue to be inconsistently reported by the contract laboratory. The contract
laboratory submitted PAN and SAR calculation correctly for May 22, 2018, in work order
number 8050101-1. This should be used as a template for how PAN and SAR calculations
should be presented in future Annual Reports.
North Carolina Department of Environmental Quality 1 Division of Water Resources
Mooresville Regional Office 1610 East Center ,Avenue. Suite 301 1 Mooresville, North Carolina 28115
11

NORTH CAROLINA
•
ANN.. UAL
'.�: •� } ,fie =r� t�
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r

RECEIVEDINCDL-NRi'G��4R
CITY of APR ® 8 2019
NORTH CAROLINA PJ^ROS
MOORESVILLE REGIONAL OFFICE
FEB 1 5 2Qi9
Table of Contents perMii ing unit
permitting �n
I: Third Creek. onofil (WQ0004040.)
20 City of Statesville Land Application (WQ001454
3e Alkaline Stabilization ( WQ0006245 �
PO Box 1111 • Statesville, NC 28687 • ci.statesville.nc.us

CPT' of W1
NORTH CAROLINA
January 30, 2019 RECEDNMF()IDW
FEB 15 2019
Non-Discharg^
Attention: Troy Doby QeR1llttinCl Jni?
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636 .
RE: Annual Reports for 2018
Third Creek Monofil (WQ0004040)������
FEB 1 5 2019
D"Vl� SECTION
n�4T10N PROCESSING UNIT
Dear Mr. Hardee:
Enclosed, you will find a copy of the required forms and lab data for the Third Creek Monad¢.
Permit#:WQ0004040. This monofil is currently closed and not being used for bio-solids disposal.
: _This permit was compliant for the year.
Shouldyou.require more information, or if further action is required, please contact me at 704- 878-3438.
Sincerely,
Ken Ga. oway
W WTP Supervisor, Fourth Creek W WTP
PO Box 1111 e Statesville, NC 28687 • ci.statesville.nc.us

GENERAL INFORMATION
BIOSOLIDS REPORT
CALENDER YEAR 2018
THIRD CREEK MONOFILL
PERMIT NO. WQ0004040
FACILITY NAME: Third Creek WWTP-NPDES NCO020591
LOCATION: 444 Third Creek Road
MAILING ADDRESS: P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Water Resources
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Scott Austin
Plant Supervisor
P. O. Box I I I I
Statesville,.NC 28687-1111
[phone]
RESIDUALS ORC Ken Galloway
Residuals Supervisor
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
APPLICATION: Surface disposal unit.
This unit was not used for biosolids
disposal in 2018, and has completed
closure activities. The permit is
maintained for well sampling and
reporting.

Management Practices Description
Third Creek WWTP Sludge Monofill (Surface Disposal Unit)
NPDES No. NC0020591
40 CFR 503.24
Non -Discharge Permit WQ0004040
THREATENED OR ENDANGERED SPECIES: No known threatened or endangered species
occupy or frequent the disposal site.
BASE FLOOD FLOW RESTRICTION: The site is located above the flood plain.
LOCATION OF GEOLOGICAL STABLE AREA: Soil consists of tight red clay on high ground
and the site has had no history of movement or shifting due to saturation with rainwater or
seismic conditions. No known faults exist in the area.
WETLANDS LOCATION: Not a wetland location.
RUNOFF COLLECTION: Trenches are constructed as to prevent disposed material from exiting
as a part of any runoff. Berming and swales are constructed to contain erosion. Finished trenches
are domed with clean earth to allow shedding of water out and away from filled trenches. A
"green belt" is maintained and encouraged to grow around the entire area.
LEACHATE COLLECTION: As a liner is not used, leachate collection is not required.
METHANE GAS MEASUREMENTS: Periodic checks of air with electronic air monitors reveal
that methane is not escaping the surface disposal area.
CROP PROHIBITION: Crops are not grown on the site.
GRAZING PROHIBITION: Grazing is not permitted on the site.
PUBLIC ACCESS RESTRICTED: Chain link fencing encloses the site property. NO
TRESPASSING signs are posted.
AQUIFER CONTAMINATION: Monitoring well samples for this calendar year show no danger
of aquifer contamination.
No disposal activities occurred in 2018.

CLASS A ,., ,,XAL DISTRIBUTION AND MARKETING/ SVRFA,DISPOSAL CERTIFICATION:ANDISUMMARY=FO�u.x
WQ PERMIT #: 4040 FACILITY NAME: Third Creek WWTP Monofill
PHONE: [phone] COUNTY: Iredell OPERATOR: Ken Galloway
FACILITY TYPE (please check one): 21 Surface Disposal (complete Part'A (Source(s) and "Residual In" Volume only) and Part C)
IA Distribution and Marketing (complete Parts A,-B, and C).
Was the facility in operation during the past calendar vear? Yes 11 No 21 ---► If No skip parts A, B, C and certifv form below
Part A*:
Part B*:
Month
Sources(s) s) ( include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
NO RESIDUALS
DISPOSED
OF IN
PERMITTED
UNIT IN 2018
August
September
October
November
December
Total from FORM DMSDF (sup)
Totals:
Annual (d tons):
0
0
0
....................
0
Amendments used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: 0 No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results. are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAN...ING-SUMMARYTOR1Vi
Please note that your permit may contain additional parameters to be analyzed: The parameters can -be- reported -.in.FORM RSSF_- B.
WQ Permit Number: WQ0004040 Laboratory: 1)
Facility Name: Third Creek WWTP Monofill 2)-
Residual Source WQ # or NCO020591 3)
NPDES #: 4)
WWTP Name: 5)
Residual Analvsis Data
Prism Labs'.
Parameter
(mg/kg)
Ceiling
Cone.
Limit
Sample or Composite Date
Percent Solids (%)
NA
Arsenic
75
Cadmium
85
Copper
4,300
Chromium
NA
Lead
840
Mercury
57
Molybdenum
75
Nickel
420
No
Residuah
disposed
of in
permitted
Selenium
100
unit
2018
Zinc
7,500
Total Phosphorus
NA
TKN
NA
Ammonia -Nitrogen
NA
Nitrate and Nitrite
NA
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for Wilting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
Z--12-fl
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Third Creek WWTP Monofill WQ Permit Number: WQ0004040
WWTP Name: Third Creek WWTP
NPDES Number: NCO020591
Monitoring Period: From 1/1/2018 To 12/31/2018
Pathosen Reduction (40 CFR 503.32) _ Please indicate level achieved and alternative performed:
Class A:
Alternative 1 C(
Alternative 2 [.j
Alternative [�
.-F-Alternative
4� L`i
Alternative 5 ll
Alternative 6 D
...........
...................
If applicable to alternative performed Cross A
only) indicate "Process to Further
Reduce Pat!i etts
Compost 13
Heat D!yjng 0
Heat Treatment 0
Thermo hilic D
Bet Ray ElY
Gamma R CI
Ray
Pasteurization
B:
'vAlternative
Alternate e 1 ❑
l 0Class
If applicable to alternative performed (Class B
only) indicate "Process to Sigpificantly
Reduce Pathogens":
Lime Stabilization ®
Air DryingO
I Composting Q
jAerobic Digestion GI
Digestion estion CI
g
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
um er of
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
ni ue
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
No
Residuals
disposed
of in
permitted
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
unit
@
2018
:Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.] (VS reduction) [1
Alt. 2 (40-day bench) (I
Alt. 3 (30-day bench) ®
Alt. 4 (Spec. 02 uptake) 13
Alt. 5 (14-Day Aerobic) D
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) D
Alt. 8 (Drying - Unstable) CI
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) [I'
No vector attraction reduction alternatives were performed [l
CERTIFICATION STATEMENT (please check the appropriate statement)
D "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector .:.
attraction reduction requirement in 40 CFR 503.33 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vect6f
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you 'Check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
6 n 6�10 f(o 11/0 1/ -
Preparer Name and Title type or print)
Signature of Preparer*
Land Applier Name and Title (if applicable)(type or print)
z -le-ff
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 503 (12/2006)

CITY of N
NORTH CAROLINA
4th CREEK& .3rd CR-F5K NfKkTP SLUDGE NARRATIVE
Ken Calloway
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester and dewatered
using a belt press. After dewatering, the residuals are transferred to the StaLime lime stabilization
process area where the biosolids are set aside for contract land application away from the plant site.
The contractor is Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids;
disposal is the StaLime process and that permit # is_WQ0006245.
PO Box 1111 •. Statesville, NC 28687 ° ci.statesville.nc.us ®_

CSCITY of VOW
NORTH CAROLINA
January 30, 2019
Attention: Troy Doby
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Report for 2018
City of Statesville Land Application (WQ0014543)
Dear Mr. Doby:
REC RITD',NOPOIDWRI
FEB 15 2D1
lion-Discharga,
P&I-Mittin,g Unit
FEB
P,� Div; S��;iION
R 4TION PROCE'SSINC UNfT
Enclosed, you will find a copy of the required fonns and lab data for the City of Statesville Land
,k,pplication,_permit #WQ0014543. This land application program has never been utilized. However, the
City of Statesville wishes to keep this permit active in case of an emergency.
This permit was compliant, for the year.
Should yopyr quire more information, or if further action is required, please contact me at 704- 878-3438.
Sincerely;;
Ken Galloway
WWTP Supervisor, Fourth Creek WWTP
PO Box 1111 • Statesville, NC 28687 ° ci.statesville.nc.us

GENERAL INFORMATION
LAND APPLICATION
CALENDAR YEAR 2018
Permit No. WQ0014543
FACILITY NAME: Fourth Creek WWTP-NPDES NCO031836
Third Creek WWTP- NPDES NCO020591
LOCATION: 693 Bell Farm Rd.
444 Third Creek Rd.
MAILING ADDRESS: P. O. Box 1111
Statesville, NC 28687-1111
[phone] `
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Dept. of Water Resources
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Ken Galloway
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Ken Galloway
P. O. Box I I I I
Statesville, NC 28687-1111
[phone]
APPLICATION: Land Application
No Residuals land applied in 2018.

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014543 County:
Facility Name (as shown on permit):
Iredell
Year: 2018
Fourth Creek WWTP
Land Application Operator: Ken Galloway Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes 0 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summa
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
704-878-3438
Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty.;grlhw, that the above information is, to the best of my knowledge and belief, true, "accurate,
and complete. I am aware'that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittee Name and Title (type or print)
Signature of Permittee Date
Signature of Prepare Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

CITY of
NORTH CAROLINA
4ftf CREEK & .?rah CREM MWPSLUDGE MARRATWE
Ken Galloway
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester and dewatered
using a belt press. After dewatering, the residuals are transferred to the StaLime lime stabilization
process area where the biosolids are set aside for contract land application away from the plant site.
The contractor is Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids
disposal is the StaLime process and that permit # is WQ0006245.
a
PO Box 1111 • Statesville, NC 28687 ci.statesville,nc.us

CITY of
NORTH CAROLINA
January 30, 2019
Attention: Troy Doby
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh; North Carolina 27699-1636
RE: Annual Report for 2018
Alkaline Stabilization.(WQ0006245)
rEB � 5 2oi9
� urn
;�&606
FEB 15 2019
Non -Discharge,
Permi'-nir;g Unit
Dear Mr. Doby:
Enclosed, you will find a copy of the required forms and lab data for the Alkaline Stabilization
program. Permit;# WQ0006245.
This permit was compliant for the year.
Should.you require mare information, or if further action is required, please contact me at 704- 878-3438.
Sincerely, .
Ks 5qaloway
WWTP Supervisor, Fourth Creek WWTP
PO Box 1111 • Statesville, NC 28687 ° ci,statesville.nc:us

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization
WWTP Name: Fourth Creek WWTP
Monitoring Period:
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
WQ0006245
NCO031836
From 1/1/2018 To
WQ Permit Number:
NPDES Number:
12/31 /2018
Class A:
Alt. A- (time/temp) D
Alt 13 (Ally Treatment)
Alt. C (Prier Testing)
:::::::::::::
::
AIt.D (i�lo Prior Test) C
Process to Further tltei• Reduce Paths eng Cl
....................
If applicable to alterative pet�'ornned (Class Ei
only indicate "Process to Further Reduce Patho ens":
Compost El
Heat 2!ittg Ej
Heat Treatment 11
Therirlo hilic C
............ .
....................
Beta RayC�
Gamma R.a (�
lr'ci5teiill�iltif5ll,i
`.i< ....................... . ..
Class B:
Alt: (1) Fecal Density: LJ
. Alt; (2) Process to Sipifcantly Reduce Pathogens 6
If applicable to alternativeperformed
(Class B
onI ) indicate "Process to Significantly Reduce Patho ens":
Lime Stabilization C7
AirD 'ng Cl
Composting 0
jAerobic Digestion Cl
robic Digestion Cl
Anaet g
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
ni ue
MinimumGeo.
Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<0.3
<0.3
mpn/g
60 days
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
`Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) E-j
Alt. 2 (40-day bench) 0
Alt. 3 (30-day bench) [j
Alt. 4 (Spec. 02 uptake) Cl
Alt. 5 (14-Day Aerobic) CT,
Alt. 6 (Alk. Stabilization d
Alt 7 (Drying - Stable) Cl
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Cl
Alt. 10 (Incorporation) []
No vector attraction reduction alternatives were performed Ci
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
cr l/Oc✓v��
Preparer Name and Aitle (type or print)
Signature of Prepar
Land Applier Name and Title (if applicable)(type or print)
-f—lZ—/q
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

City Of Statesville Alkaline Stabilization Record For
Process To Further'Reduce Pathogens (PFRP)
BIN # BACk G-Afeq
Setup Date: I- l a_ 18
Removal From Bin Date: I - is- 16
Date
Time
pH >12.0 For 7.2 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
I- i d-18
3 pM
Initial,pH: 0.-Gd
►-1�- rB
?0 ° 3 Prn
1- 13- IS
95 ° 03: ooM
R4 LJ
Corrected pH: 0. 84
I-i6-1g
I �m
. �
Final pH: 1 a, dA/
�LGJ_
Corrected pH: /d: 8�
Has 12 Hour Ternp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? N
BIB # covFR
Setup Date: I-
Removal From Bin Date: /-oil-./S
Date
Time
pH >12.0 For 72 Hrs:
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: la. IN
2- ig
9012:`/`/P/✓1
1-23-IS
830n 0W3`/
!?LlJ
Corrected pHs 13.01
1-a5-1S
1:117 pfn
Final pH: 1d , '7 /
Corrected pH: la.ITd
Has 12 Hour Ternp Criteria
Beenn Met? Y N
Has 72 *Hour. pH Criteria Been Met? ® N
BIN # J as Q
Setup Date:. A- 7- I S
Removal From Bin Date: ;i- la- 18
Date
Time
'pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH: U. 9`7
2-1- IS
65 ° @ 3: os Pfn
a-0-18
?.3° 6 o5
•
Rat W
Corrected pH: 12, 8y
2 : 13 PM
Final pH: 42.57
R kw
Corrected. pH: U. 71 - -
Has 12 Hour Ternp Criteria Been Met? Y N
-(YT
Has 7.2 Hour pH Criteria Been Met? N
BIN #,? ,g P; Je
Setup Date: a- 8- 18
Removal From Bin Date: a-161 •- IS
Date
I Time
pH >12:0 For.72 Hrs.
TEMP. >52 Deg. C -For 12 Hrs.
Operator
,a- 8- 18
1000
Initial pH: /,a,, 73
a- 8- is
d- 12- 1 g
V 8;,10
RA,w
Corrected pH: 11.9 1.
-1d- 18
2;13
Final pH: /a , 51
RAW
Corrected pH: Ia.65
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIB! #34 f ; e-
Setup Date: d- 4- 18
Removaf.From Bin Date: a-13- 18
Date
""Time
pH ?12.® For 72 VirS.
TEIMP.'>52Deg.0 For 12 Hrs.
Operator
a_9- 18
iU: 30
Initial pH: Id. 9 4
a-4- 18
9006 /o:iio
�- 1,�_ !8
71° 08:19
RtIJ
Corrected pH: IA.51d
Final pH: 1.2, Q 4.
Corrected pH: 12, 6 3
Has 12 Hour Tem*p Criteria Been Met? ® N
Has .7-2 Hour .p . Qiteria Been Mgt? ®: N

'City Of Statesville Alkaline Stabilization Record For
Process To Further*Reduce Pathogens (PFRP)
BIN ## C„4R. Pa 9
Setup Date: 3- as -16,
Removal From Bin Date: 3 - 24.. i-Y
Date
Time
pH >12.0 For 7.2 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator
3-,21- Is
04; y3'
Initial pH: /;L-.1'7
-aa-1S
90°Cam' 11: 08
3-,23-18'
750e 017.10
R4 iJ
Corrected pH: /2.117
Final pH: 12.59
Correctedl: 11,17S
Has 12 Hour Temp Criteria Been Met? Y N
Has 7 .2 Hour pH Criteria Been Met? f Y N
BIN ##Caamcq
Setup Date: 3--43--18
Removal From Bin Date: 3- a7-19
Date
Time
pH >12.0 For 72 Hrs:
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-.23-I8
A
to: ydM
Initial PH: /,4 , 73
3 -a3'-1 S
9006 11;01
3- aw- i s
9y0 II:aa
Row
Corrected pH: la,g3
3-ai-18
/o: SE
Final pH: is , SO
Corrected pH: /,?,70
Has 12 Hour Temp Criteria
Been Met? N
Has 72 *Hour.pH Criteria Been Met? Y N
BIN ## aPAD OF
Setup Date:.4-a 7- / S
Removal From Bin Date: 4- 30 -1 S
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
4-a7-i8
09�56
Initial pH: 1.2. 6 8
90°� 1/:a0
SG°@ 11'30
14L
Corrected pH: /a, $91
'#-30-18
11; 30
Final pHk Id. 65
hk
Corrected.pH: /a. S3 . -
Has 12 Hour Temp Criteria Been Met? Y N
Has 7.2 Hour pH Criteria Been Met? �Y- . N
BIN## or PAo
Setup Date: 5- R- I g
Removal From Bin Date, 5 II - I g
Date
Time
pH >12:0 For. 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5-8. IS'
I �'O8
Initial pH: 1j.•55
S-Sr-/8
QO°@ Ia:08
5-4-18
65" 0�7.'00
RA bi
Corrected pH:12.75
5-it-le
0 $: Ya
final pH: f.7.55
R� lJ
Corrected pH: /a . /Q
Has 12 Hour Temp Criteria Been Met? N
Has 72 Dour pH Criteria Been Met? Y N
BIN # e cN i C R
Setup Date: 5 - q - 18
Removal .From Bin Date: 5% 1 q I
Date
..Time
pH >12.0 F®r 72 Hrs.
Fok 11 Hrs:...
Operator
5-4-18
ii:pp
initial pH: 1),5d
SS° 11: 15
0 O 30
R41,A)
CorpectedpH: Q,70
S_ I q -18
10WOO
Final pH: 42. Yff .
R W
Corrected pH: Id. �5
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour .PH. Criteria Been Met? N

-;_...'_ _ �xs:r•�.. _e=F.r�"�'.✓._ .�G':-•._..... �, a. t..»r :��.s.3.. ..�5"..,i'�.-r E -'L<. .;t .,...h� i.a-.�_ _._t's.. ���_:�? .�75'� — - _ �.. . _ '3"•
'City of Statesville Alkaline Stabilization Record For.
Process To Further -Reduce Pathogens (PFRP)
BIN## -
Setup Date: $- 3o -18
Removal From Bin Date: 9- 4/-18
Date I
Time
pH >12.0 For 7.2 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
�-3o-18
$Corrected
D9111 0
Initial pH: /a.-93
q0°� 09: 10
F,2°�" 08': 10
R�iJ
pH: id. 83
9- �1- 18
0 8: 3 0
Final pH: lot, 50
Corrected pH: /c2.
Has 12 Hour Temp Criteria Been Met? v N
Has. 72 Hour pH Criteria Been Met? N
BIN #
Setup Date: /0-15-18
Removal From Bin Date: i0 -
Date
Time
pH >12.0 For 72 HrS..
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-15-IS
11:00
Initial pH: /a, 50o�
°� 0°@ II.,IS .
8`7 e07�y5
RxW
Corrected pHs /;t . 7-0
to -IS -IS
1�:30
Final pH: 1;A . S,q
Corrected pH: l,k,73
Has 12 Hour Temp Criteria
Been Met? I�
Has 72'Hour.pH Criteria Been Met?
BIN #
Setup Date: /0 -17 - / 8
Removal From Bin Date: /0
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
/0-14-18
09.'3O
Initial pH: /).90
i0-17-i8
90°C.-Y, 09: S I
io-19-1B
SS°@ 08:145
R��J
Corrected pH: /a, 80
i0-,2a-18
1p:I5
Final pH /,2, el
RZ
Corrected.pH:0,7 .
Has 12 Hour Ternp Criteria Been diet? 1( �
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date: /0 -18- / 8
Removal From Bin Date; / 0-
Date
time
pH >12:0 For' 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
/0-18-18
1�:yy
Initial pH: 12. 51
10- i 8- 19
qa,@ laccly
1 o - i q -1 B
87° to:06
RAW
Corrected pH- 1,2,71.
l 0-aa-18
l a: 4 9
Final pH: 1.7, 6 ,2
R W
Corrected pH: / d. 8l
Has 12 Hour ;hemp Criteria Been Met? v' N
Has 72 Hour pH Criteria Been Met? Y N
BIB! # qJ,7
Setup Date: is-a26 /,0
Removal.From Bin Date: 11-3I- I �
®ate
Time
pH >12.0 For 72 Hr' .
ttMP.'>52Deg. C For 12 Hrs:._
Operator
7
09:55
Initial pH: iJ . 6�-
900@ 09:00
$00(909: 30
RkW
Corrected pH: %d, br.2
08,`00
Final pH: /) .53.
Icorretted pH: id170
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hourpki, Criteria Been et? Y N

,7.,y ""-.., -9'.-x -. ^za: p_ .p-•�?- .a, it ,� *. Yr r' ?,,.." x' 4.xti'+t.,.5.' �`se_ ..s ++�ac .: it?, w t
':
City Of Statesville Alkaline Stabilization Record For.
Process To Further'Reduce Pathogens (PFRP)
BIN # 3 4 5
Setup Date: 1 d-a 7- I $
Removal From Bin Date: ld-31- Va
Date
Time
pH >12.0 For 72 I-Irs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
1 a- 27-18
11100
Initial,pH: /�7. 66
Ia-a 7- 18
SD° @ 11:1 a
la-ag- �g
65 °@ C81 /5
191 � ..
Corrected pH: 1:7. 8,3
1a-31-1.$
08/00 lCorrected
Final pH: 42,53
I
PAW
pH: /A 7 0
Has 12 Hour Temp Criteria Been Met? Y N
Ha-s 72 Hour pl-s Criteria Been Met?
BIN # Ie 7
Setup Date: id -a,--
Removal From Bin Date:
Date I
Time
pH >12.0 For 72 Hrs:
TEMP. >52 Deg. C For 12 Hrs.
Operator
ra-d8-l$
09l43
Initial pH: id.7a
Id-a8= It
90° @ 11,15.
1a2-31- if
80°@ 08,'Oo
%���
Corrected pHs i.1.9a
1A-31-1$
10: 30
Final pH: Id. 50
Corrected pH: 1a,17
Has 12 dour Temp Criteria
Been Met? Y N
Has 72'Hour.pH Criteria Been Met? Y N
BIN #
Setup Date:.
Removal From Bin Date:
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected.pH: -
Has 12 Hour Temp Criteria Been Met? 'Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date;
Date
time
pH >12:0 For .72 Hrs.
TEMP. >52 Deg.,C -For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIM #
Setup Date:
Removal.From Bin Date:
Date
..Time
p@,1 >12.® For 72 Hrs.
' -ttMP. >52 Deg.'C Foe 12 Hrs: "
Operator
Initial pH:
Corrected pH:
Final pFl:
Corrected pH:
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hoag .p Criteria Been Met? Y N

P �:,IRISM
in-,
YLABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime (60 Day/7 Fecal)
Lab Submittal Date: 01/16/2018
Prism Work Order: 8010226
Case Narrative
01/26/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample,
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced_ methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR=[Na]/SQRT {([Ca]+[Mg])/2}
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
[ 70/23 ] / SQRT { ([ 1300/20.04] + [ 0.03/12.15]) / 2 }
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
5Atic- p . 5 �J
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 18

Data Qualifiers Key Reference:
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
DM Sample diluted and RL increased due to the matrix.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18

PRISM
b" �LABORATOPIES, INC
Full -Service Analytical &
Environmental Solutions
Sample Receipt Summary
01 /26/2018
Prism Work Order: 8010226
CSample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
le Fecal #1
8010226-01
Solid
01/16/18
01/16/18
StaLime Fecal #2
8010226-02
Solid
01/16/18
01/16/18
StaLime Fecal #3
8010226-03
Solid
01/16/18
01/16/18
StaLime Fecal #4
8010226-04
Solid
01/16/18
01/16/18
StaLime Fecal #5
8010226-05
Solid
01/16/18
01/16/18
StaLime Fecal #6
8010226-06
Solid
01/16/18
01/16/18
StaLime Fecal #7
8010226-07
Solid
01/16/18
01/16/18
StaLime
8010226-08
Solid
01/16/18
01/16/18
Samples were received in good condition at 2.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 3 of 18

Laboratory Report
Ism
/� I EuviService al Solutions
01/26/2018
' V' Environmental Solutions
��LABORATORIES INC.
Citv_nf Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: StaLime Fecal #1
A/ idy Smith Prism Sample ID: 8010226-01
P ,_ _ -_Ix 1111 Prism Work Order: 8010226
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 67.3 % by 0.100 0.100 1 `SM2540 G 1/26/18 11:38 BJC P8A0406
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 1/16/18 14:07 EGC P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 18

- IsFull -Service Analytical&
Environmental Solutions
RIESINa
City_ of Statesville, NC
A idy Smith
F' Ix 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01 /26/2018
Client Sample ID: StaLime Fecal #2
Prism Sample ID: 8010226-02
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 71.7
% by
0.100
0.100 1
'SM2540 G 1/19/18 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 1/16118 14:07 EGC
P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18

P� 'n\//�1 Full -Service Analytical &
R_ I S 1 Y , Environmental Solutions
�� 'LA.ORATORIES, INC.
Laboratory Report
01 /26/2018
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: StaLime Fecal #3
idy Smith Prism Sample ID: 8010226-03
F lx 1111 Prism Work Order: 8010226
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 65.8 % by 0.100 0.100 1 'SM2540 G 1119118 12:00 BJC P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 1/16/18 14:07 EGC P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 Of 18

ISFull-Service Analytical s
Environmental Solutions
_ �Z'. LABORATORIES, INC.
City of Statesville, NC
/ ndy Smith
F ")X 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01 /26/2018
i
Client Sample ID: StaLime Fecal #4
Prism Sample ID: 8010226-04
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 65.9
% by
0.100
0.100 1
*SIV12540 G 1/19/18 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 1/16/18 14:07 EGC
P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 18

Laboratory Report
Full -Service Analytical &
'._ FR I S M I Environmental Solutions
01/26/2018
,r'L BORATORIE^.a INa
City -of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: StaLime Fecal #5
f' l idy Smith
Prism Sample ID: 8010226-05
F` >x 1111
Prism Work Order: 8010226
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 68.2
% by
0.100 0.100
1 `SM2540 G 1119/18 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 1116118 14:07 EGC
P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 Of 18

Laboratory Report
�� I Full -Service Analytical &
Environmental Solutions 01/26/2018
L r'L BORATORIE$ INC
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: StaLime Fecal #6
P ndy Smith Prism Sample ID: 8010226-06
F )x 1111 Prism Work Order: 8010226
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
% Solids 69.8 % by 0.100 0.100 1 *SM2540 G 1119/18 12:00 BJC PBA0288
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 1/16/18 14:07 EGC P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 9 of 18

I FullService Analytical &
Environmental Solutions
—=v'LASORATORIES. INC.
Laboratory Report
01 /26/2018
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: StaLime Fecal #7
lndy Smith
Prism Sample ID: 8010226-07
'Ox 1111
Prism Work Order: 8010226
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
67.8 % by
0.100 0.100
1 `SM2540 G 1/19/18 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 1/16/18 14:07 EGC
P8A0222
J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 18

�P� l I Full -Service Analytical
`-` Environmental Solutions
X:-_LABORATORIES, ING
Laboratory Report
01/26/2018
City of Statesville, NC
J ndy Smith
F )x 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Client Sample ID: StaLime
Prism Sample ID: 8010226-08
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit I Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1900
mg/kg dry
1100
230
10
*Calculation
1/22/18 10:49
CLB
[CALC]
% Solids
69.4
% by
0.100
0.100
1
*SM2540 G
1119118 12:00
BJC
P8A0288
Weight
Ammonia as N
180
mglkg dry
14
3.6
1
*SM4500-NH3 C
1118/18 14:00
BMS
P8A0246
Nitrate/Nitrite as N
29
mg/kg dry
7.2
0.79
1
*SM4500-NO3 F
1118/18 10:02
CLB
P8A0226
Phosphorus -Total
3600
mg/kg dry
72
10
20
*SM4500-P F
1/19/18 9:20
CLB
P8A0225
Total Kjeldahl Nitrogen
6000
mg/kg dry
3600
770
10
*351.2
1/22/18 10:49
CLB
P8A0239
Total Metals
Mercury
0.049
mg/kg dry
0.031
0.0030
1
*7471B
1/22118 17:12
JAB
P8A0298
SAR Soil Preparation
Complete
g
1
*2-78-054
1119/18 9:20
JAB
P8A0238
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
1/23/18 15:20
JAB
P8A0333
Weight
Arsenic
26 DM, J
mg/kg dry
35
4.3
100
6010D
1122/18 18:16
JAB
P8A0237
Sodium Absorption Ratio
0.53
[blank]
0.30
0.016
1
*2-78-054
1/26/18 16:51
JAB
P8A0256
Cadmium
BRLDM
mg/kg dry
35
0.95
100
6010D
1/22/18 18:16
JAB
P8A0237
Calcium
1300 BH
mg/L
10
1.0
100
*6010D
1/25118 16:51
JAB
P8A0256
C
47 DM, J
mg/kg dry
71
6.4
100
6010D
1/22118 18:16
JAB
P8A0237
L___
14 DM, J
mg/kg dry
35
6.6
100
6010D
1122118 18:16
JAB
PBA0237
Magnesium
BRL
mg/L
0.10
0.0086
1
*6010D
1123/18 12:26
JAB
P8A0256
Nickel
10 DM, J
mg/kg dry
71
2.5
100
6010D
1/22/18 18:16
JAB
P8A0237
Selenium
BRLDM
mg/kg dry
71
17
100
6010D
1/22/18 18:16
JAB
P8A0237
Sodium
630 DM, J
mg/kg dry
2100
69
100
6010D
1122/18 18:16
JAB
P8A0237
Sodium
70 BH
mg/L
50
1.8
100
*6010D
1123/18 12:18
JAB
P8A0256
Zinc
79 DM, J
mg/kg dry
350
13
100
6010D
1122/18 18:16
JAB
P8A0237
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 18

Level 11 QC Report
PIhz� Full -Service Analytical& 1/26/18
S 1 Y, Environmental Solutions
" 'LABORATORIES. INC.
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 8010226
Ai," dy Smith Time Submitted: 1/16/2018 12:55:OOPM
P. I K 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8AO237 - 3050B
Blank (P8A0237-131-1<1)
Prepared: 01/18/18 Analyzed: 01/23/18
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
0.0543
0.50
mg/kg wet
J
Lead
0.0866
0.25
mg/kg wet
J
Nickel
0.0737
0.50
mg/kg wet
J
Selenium
BRL
0.50
mg/kg wet
Sodium
1.41
15
mg/kg wet
J
Zinc
0.188
2.5
mg/kg wet
J
LCS (P8A0237-13S1)
Prepared: 01/18/18 Analyzed: 01/23/18
Arsenic
25.6
0.25
mg/kg wet
25.00 102 80-120
Cadmium
26.1
0.25
mg/kg wet
25.00 104 80-120
Copper
27.0
0.50
• mg/kg wet
25.00 108 80-120
Lead
26.0
0.25
mg/kg wet
25.00 104 80-120
Nickel
26.2
0.50
mg/kg wet
25.00 105 80-120
Selenium
24.4
0.50
mg/kg wet
25.00 98 80-120
$odium
283
15
mg/kg wet
250.0 113 80-120
24.7
2.5
mg/kg wet
25.00 99 80-120
Batch P8A0238 - SAR 2-78-054
Blank (P8A0238-BLK1)
Prepared: 01/18/18 Analyzed: 01/19/18
SAR Soil Preparation
Complete
g
Batch P8AO256 - 3010A
Blank (P8A0256-BLK1)
Prepared: 01/18/18 Analyzed: 01/23/18
Sodium Absorption Ratio
BRL
0.30
[blank]
Calcium
1.68
0.10
mg/L
BH
Magnesium
BRL
0.10
mg/L
Sodium
2.40
0.50
mg/L
BH
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 18

Full -Service Analytical Environmental
Environmental Solutions
LABORATORIES INC.
Level II QC Report
1 /26/18
City of Statesville, NC
A..". _ -dy Smith
P. X 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (60 Day/7 Fecal)
Prism Work Order: 80IQ226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBA0298 - 7471 B
Blank (P8A0298-BLK1) Prepared &Analyzed: 01/22/18
Mercury BRL 0.020 mg/kg wet
LCS (P8A0298-BSI) Prepared &Analyzed: 01/22/18
Mercury 0.462 0.020 mg/kg wet 0.4167 111 80-120
Batch P8A0333 - NO PREP
Duplicate (P8A0333-DUP1) Source: 8010226-08 Prepared: 01/18/18 Analyzed: 01/23/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 30 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 13 of 18

Level II QC Report
01VJPI n Full -Service Analytical 1/26/18
-' ' V' Environmental Solutions
! LABORATORIES INC.
City of Statesville, NC
A idy Smith
P x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (60 Day/7 Fecal)
Prism Work Order: 8010226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8A0225 - SM4500-PB5
Blank (P8A0225-BLK1) Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8A0225-BS1) Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total 95.6 2.5 mg/kg wet 100.0 96 90-110
Matrix Spike (P8A0225-MS1) Source: 8010226-08 Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total 3160 72 mg/kg dry 144.2 3590 NR 80-120 MC
Matrix Spike Dup (P8A0225-MSD1) Source: 8010226-08 Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total 3300 72 mg/kg dry 144.2 3590 NR 80-120 4 20 MC
Batch P8A0226 - NO PREP
Blank (P8A0226-BLK1) Prepared & Analyzed: 01/18/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P8A0226-BSI) Prepared &Analyzed: 01/18/18
Nitrate/Nitrite as N 48.3 5.0 mg/kg wet 50.00 97 80-120
Matrix Spike (P8A0226-MS1) Source: 8010226-08 Prepared &Analyzed: 01/18/18
I litrite as N 97.3 7.2 mg/kg dry 72.10 29.4 94 80-120
I Spike Dup (P8A0226-MSD1) Source: 8010226-08 Prepared &Analyzed: 01/18/18
Nitrate/Nitrite as N 97.8 7.2 mg/kg dry 72.10 29.4 95 80-120 0.5 20
Batch MOM - 351.2
Blank (P8A0239-BLK1) Prepared: 01/18/18 Analyzed: 01/22/18
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 18

A0-L Full -Service Analytical &
I S M Evironmental Solutions
•✓1A80RATORIES, ING
Level II QC Report
1 /26/18
City of Statesville, NC Project: Stal-ime (60 Day/7 Fecal)
At dy Smith
P., c 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 8010226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8A0239 - 351.2
LCS (P8A0239-BS1) Prepared: 01/18/18 Analyzed: 01/22/18
Total Kjeldahl Nitrogen 500 100 mg/kg wet 500.0 100 90-110
Batch P8AO246 - SM4500-NH3 B
Blank (P8A0246-BLK1) Prepared & Analyzed: 01/18/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8A0246-BSI) Prepared &Analyzed: 01/18/18
Ammonia as N 504 10 mg/kg wet 500.0 101 80-120
Batch P8A0406 - Solids, Dry Weight
Duplicate (P8A0406-DUPI) Source: 8010226-01 Prepared &Analyzed: 01/26/18
% Solids 67.5 0.100 % by Weight 67.3 0.3 20
This report should not be reproduced, except in its entirety, without'the written consent of Prism Laboratories, Inc.
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A==�17-,
Level II QC Report
-R I S M Full -Service Analytical s 1/26/18
Environmental Solutions ASOWOAIES INC.
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 8010226
Al dy Smith Time Submitted: 1/16/2018 12:55:OOPM
P. c 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8AO222 - NO PREP
Blank (P8A0222-BLK1) Prepared &Analyzed: 01/16/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 18

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
80 18
P8A0239
0.05 g
25 mL
01/18/18 10:00
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0246
1.01 g
50 mL
01/18/18 12:00
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0225
1 g
50 mL
01/18/18 7:08
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8010226-01
P8A0406
30 g
30 g
01/26/18 11:38
8010226-02
P8A0288
30 g
30 g
01/19/18 12:00
8010226-03
P8A0288
30 g
30 g
01/19/18 12:00
8010226-04
P8A0288
30 g
30 g
01/19/18 12:00
8010226-05
P8A0288
30 g
30 g
01/19/18 12:00
8010226-06
P8A0288
30 g
30 g
01/19/18 12:00
8010226-07
P8A0288
30 g
30 g
01/19/18 12:00
8010226-08
P8A0288
30 g
30 g
01/19/18 12:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
80 no'?n-08
P8A0256
50 mL
50 mL
01/19/18 9:20
8" -08
P8A0256
50 mL
50 mL
01/19/18 9:20
8:, . —`-08
P8A0256
50 mL
50 mL
01/19/18 9:20
8010226-08
P8A0256
50 mL
50 mL
01/19/18 9:20
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0237
2.04 g
50 mL
01/18/18 9:50
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0298
0.55 g
50 mL
01/22/18 10:55
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0238
250 g
250 g
01/18/18 9:20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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_rj
. . . . . ..
LABORATORIES, INC.
CHARM OF CUSUDDY RECORD
Full -Service Analytical &
Environmental Solutions FAGE_OF_Quoruli;-d a ENSURE PROPEPBOLt.IC,7G,
449 Springbrook Road ° Charlotte, NC 28217
Phone [phone] Fax: [phone]
Ciient Company Name: C n1& ®; JMR-Sya le
Report To/Contact Name: Aems&X 3-9 41
Reporting Address:
Project Nature:
Short Hold Analysis: (Yes) (MO) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL l li 111 11V)
provisions and/or QC Requirements
invoice To:
Address:
co
O
co
N
CM
cts
phone: 70- 9 70- VW Fax e ? (No): Feq- Y? - 9,999 Purchase Order No./Billing Reference
70 BE MLLED N BY CUMUSAM r( UNG PERSOMMEL
Entail Address: Requested Due Date © 1 Day ® 2 Days ❑ 3 Days ® 4 Days ® 5 Days
Certit'ication: HELAC DoD
FL MC
EDD `hype: PDF Excel Other "Working Days" ® 6-9 Days 13 Standard 10 days ® RushWork Must Be pproved
SC ®THER
N/A
Site Location Marne: A_ymr T h CR FC P. &w7p Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 41.5 Bas Fi roo Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS a, CONDITIONS REGARDING SERVICES
��(�®le lied Oro®llectu®BV: ��� NO
( p
BY PRISM LABORATORIES, INC. TO CLIENT)
—
TIME
TIME
MATRIX
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
°9
(PRISM
LAB
CLIENT
DATE
COLLECTED
(SOIL,
�� REMARKS
SAMPLE SCRIP7'ION
COLLECTED
MILITARY
WATER OR
"TYPE
NO.
SIDE
TIVES
� r�;
ID NO.
\\
HOURS
SLUDGE)
SEE BELOW
n2,�0
1
t.�
5Az
VYI .
c� Ge9
� I���M F. Ik� I +•1:. 4�ti�ul ,rt© µ�tl� u,.�.
� 12,10
Name) OIR� �iP/r✓�' o le Affiliation
Sampler's Si nature Sampled By (Print
Upon relinquishing, this Chain of Custody is your authorization for Prism to procee with the analyses as requested above. Any Changes must be
6nitialfized.
st�G�tnAted ' writing to th&aPristm Project Manager. (There will foe charges for slay c stages after analyses have been
Relpi i d (xgna e) Received By (lg iatuprp) o e Milit ear Additional Comments
Sits Arnuai Tnne
/
V
Relinquished By (Signature) Received By: (Si nature) D? e
Site Dep i (Ure Tlme
f s' r
Field Tech Fee
Relinquished By. (Signature) Recuived For Prism Laboratories By: Dat
Method of Shipment- OTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITI-I CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
,SAMPLES ARE NOT CCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
Eed -x ❑ UPS delivered ❑Prism Field Service ❑Other _
NPDES: us C OUNDWATER: DRINKING WASOLID WASTE: RCE2A: CERCLA LANDFILL OTHER:
SR: SO
U NC ® SC ®i : _ SC NC ® Sc ® NC 0 SC ® NC a SC ® NC [ ® NC ® SC I ® NC 0 SC ® NC L l SC
�-Te no snri�l�r2 -a vrr r r1nnrQ• a = .r,,. h— to = Plactir.• TI = TPflnn-Lined Car) VOA = Volatile Organics Analysis (Zero Head Space)

��PRISM
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 01/29/2018
Prism Work Order: 8010426
Case Narrative
02/06/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
SAR = [ 92/23.0 ] / SQRT { ( [1200/20.0] + [0.039/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 10

Data Qualifiers Key Reference:
A Recovery of Low-level ICV (73%) is less than the lower limit (80%). Result might have a slight low bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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n�
/7_�R-,
ISM
�' LABORATORIES, INC.
C"'',ample ID
Full -Service Analytical &
Environmental Solutions
Lab Sample ID Matrix
8010426-01 Solid
Samples were received in good condition at 3.6 degrees C unless otherwise noted.
Sample Receipt Summary
Date Sampled
01 /29/18
02/06/2018
Prism Work Order: 8010426
Date Received
01 /29/18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 10

/-`RF3 Full -Service Analytical &
Environmental Solutions
LABORATORIES INC.
Laboratory Report
02/06/2018
(:itv of Statesville, NC Project: StaLime Client Sample ID: StaLime
/ ndy Smith Prism Sample ID: 8010426-01
-)x 1111 Prism Work Order: 8010426
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/29/18 12:00
Time Submitted: 01/29/18 13:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1200
mg/kg dry
460
98
5
*Calculation
211118 9:42
CLB
[CALC]
Solids
82.6
% by
0.100
0.100
1
*SM2540 G
1130/18 14:00
JLR
P8A0474
Weight
Ammonia as N
110
mg/kg dry
12
2.9
1
*SM4500-NH3 C
1/31118 11:45
BMS
P8A0478
Nitrate/Nitrite as N
6.3
mg/kg dry
6.1
0.67
1
*SM4500-NO3 F
2/1/18 9:42
CLB
P81B0001
Phosphorus -Total
2200
mg/kg dry
61
8.7
20
*SM4500-P F
212/18 9:32
CLB
P8B0004
Total Kjeldahl Nitrogen
3900
mg/kg dry
1500
320
5
*351.2
1/31118 11:09
CLB
P8A0479
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
1/30/18 10:09
BMS
P8A0481
Total Metals
Mercury
0.17
mg/kg dry
0.024
0.0023
1
*7471B
212/18 12:56
JAB
P8B0039
SAR Soil Preparation
Complete
g
1
*2-78-054
2/1/18 10:00
JAB
P8130045
SAR Percent Moisture
67.2
% by
0.100
0.100
1
*2-78-054
2/2/18 11:10
PJF
PBB0050
Weight
Arsenic
4.5
mg/kg dry
3.0
0.36
10
*6010D
2/1/18 14:47
JAB
P8A0464
Absorption Ratio
0.71
[blank]
0.30
0.016
1
*2-78-054
212118 19:49
JAB
P8B0046
( n
BRL
mg/kg dry
3.0
0.080
10
*6010D
2/1/18 14:47
JAB
P8A0464
Calcium
1200
mg/L
1.0
0.10
10
*6010D
2/2/18 19:41
JAB
P8B0046
Copper
29
mg/kg dry
6.0
0.54
10
*6010D
211/18 14:47
JAB
P8A0464
Lead
7.3
mg/kg dry
3.0
0.55
10
*6010D
2/1/18 14:47
JAB
P8A0464
Magnesium
BRL
mg/L
0.10
0.0086
1
*6010D
2/2/18 19:49
JAB
P8B0046
Nickel
6.5
mg/kg dry
6.0
0.21
10
*6010D
2/9/18 14:47
JAB
P8A0464
Selenium
23 A
mg/kg dry
6.0
1.4
10
*6010D
2l1/18 14:47
JAB
P8A0464
Sodium
580
mg/kg dry
180
5.9
10
*6010D
2/1118 14:47
JAB
P8A0464
Sodium
92
mg/L
0.50
0.018
1
*6010D
212118 19:49
JAB
P8B0046
Zinc
68
mg/kg dry
30
1.1
10
*6010D
211/18 14:47
JAB
P8A0464
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 10

I V n A FWI-Service al Solutions
V � Environmental Solutions
,Axif
O 'LABORATORIE$ INC.
Level II QC Report
2/6/18
City of Statesville, NC Project: StaLime
Ai dy Smith
P. K 1111
Statesville, NC 28687
Total Metals - Quality Control
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8A0464 - 3050B
Blank (P8A0464-BLK1)
Prepared &Analyzed: 01/31/18
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mglkg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P8A0464-BS1)
Prepared &Analyzed: 01/31/18
Arsenic
12.2
0.25
mg/kg wet
12.50 97
80-120
Cadmium
12.4
0.25
mg/kg wet
12.50 100
80-120
Copper
13.3
0.50
mg/kg wet
12.50 107
80-120
Lead
12.6
0.25
mg/kg wet
12.50 101
80-120
Nickel
12.7
0.50
mg/kg wet
12.50 102
80-120
Selenium
11.9
0.50
mg/kg wet
12.50 95
80-120
Snrih Im
1280
15
mg/kg wet
1250 103
80-120
2
12.4
2.5
mg/kg wet
12.50 99
80-120
Batch P8B0039 - 7471 B
Blank (P8B0039-BLK1) Prepared &Analyzed: 02/02/18
Mercury BRL 0.020 mg/kg wet
LCS (P8B0039-BSI) Prepared &Analyzed: 02/02/18
Mercury 0.428 0.020 mg/kg wet 0.4167 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 10

0,;
I S n n Full -Service Analytical
' V' I Environmental Solutions
v 'LABORATORIES. ING.
Level II QC Report
2/6/18
City of Statesville, NC
Al'- dy Smith
P. t 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8B0045 - SAR 2-78-054
Blank (P8130045-BLK1) Prepared &Analyzed: 02/01/18
SAR Soil Preparation Complete g
Batch MOM - 3010A
Blank (P8130046-131-K1) Prepared &Analyzed: 02/02/18
Sodium Absorption Ratio BRL 0.30 [blank]
Calcium 0.194 0.10 mg/L BH
Magnesium BRL 0.10 mg/L
Sodium 1.74 , 0.50 mg/L BH
Batch P8130050 - NO PREP
Duplicate (P8130050-131UP1) Source: 8010426-01 Prepared &Analyzed: 02/02/18
SAR Percent Moisture 68.6 0.100 % by Weight 67.2 2 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 10

Level II QC Report
J� Ism
Full -Service Analytical & 2/6/18
Environmental Solutions
^--- `,I IR
City of Statesville, NC
A idy Smith
P. x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P8A0478 - SM4500-NH3 B
Blank (P8A0478-BLK1) Prepared &Analyzed: 01/31/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8A0478-BS1) Prepared &Analyzed: 01/31/18
Ammonia as N 484 10 mg/kg wet 500.0 97 80-120
Batch MOM - 351.2
Blank (P8A0479-BLK1) Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P8A0479-BS1) Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen 532 100 mg/kg wet 500.0 106 90-110
Matrix Spike (P8A0479-MS1) Source: 8010426-01 Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen 10700 1500 mg/kg dry 6055 3900 112 90-110 MI
Matrix Spike Dup (P8A0479-MSD1) Source: 8010426-01 Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen 11000 1500 mg/kg dry 6055 3900 117 90-110 3 20 MI
Batch P8B0001 - NO PREP
I P8B0001-BLK1
Naraie/Nitrite as N
BRL 5.0 mg/kg wet
& Analvzed: 02/01 /18
LCS (P8B0001-BS1) Prepared &Analyzed: 02/01/18
Nitrate/Nitrite as N 48.9 5.0 mg/kg wet 50.00 98 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 10

� li I S Full -Service Analytical Environmental Solutions
11 A00RATORIE$ INC.
Level II QC Report
2/6/18
City of Statesville, NC Project: StaLime Prism Work Order: 8010426
P Idy Smith Time Submitted: 1/29/2018 1:30:OOPM
F x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8B0001 - NO PREP
Matrix Spike (P8B0001-MS1) Source: 8010426-01 Prepared &Analyzed: 02/01/18
Nitrate/Nitrite as N 68.2 6.1 mg/kg dry 60.55 6.30 102 80-120
Matrix Spike Dup (P8B0001-MSD1) Source: 8010426-01 Prepared &Analyzed: 02/01/18
Nitrate/Nitrite as N 65.9 6.1 mg/kg dry 60.55 6.30 98 80-120 3 20
Batch P8B0004 - SM4500-PB5
Blank (P8B0004-BLK1) Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8B0004-BS1) Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total 96.3 2.5 mg/kg wet 100.0 96 90-110
Matrix Spike (P8B0004-MS1) Source: 8010426-01 Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total 2480 61 mg/kg dry 121.1 2150 269 80-120 MC
Matrix Spike Dup (P8B0004-MSD1) Source: 8010426-01 Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total 2560 61 mg/kg dry 121.1 2150 331 80-120 3 20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 10

/
Level II QC Report
P ISM
Full -Service Analytical &
2/6/18
.:-; '�P
Environmental Solutions
��— ��'✓'LABORATOR
City of Statesville, NC
Project:
StaLime
Prism Work Order: 8010426
A dy Smith
Time Submitted:
1/29/2018 1:30:OOPM
P c 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit
Units
Level Result %REC Limits
RPD Limit Notes
Batch P8A0481 - NO PREP
Blank (P8A0481-BLK1)
Prepared &Analyzed: 01/30/18
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample
Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8A0479
0.05 g
25 mL
01/30/18 9:40
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8A0478
1.03 g
50 mL
01/31/18 11:45
Prep Method: SM4500-PB5
I fiber
Batch
Initial
Final
Date/Time
£ s-01
P8B0004
1 g
50 mL
02/01/18 9:15
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8A0474
30 g
30 g
01/30/18 14:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8130046
50 mL
50 mL
02/02/18 11:00
8010426-01
P8B0046
50 mL
50 mL
02/02/18 11:00
8010426-01
P8130046
50 mL
50 mL
02/02/18 11:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8A0464
2.03 g
50 mL
01/31/18 9:00
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8130039
0.61 g
50 mL
02/02/18 9:33
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
DatelTime
>_6-01
P8130045
250 g
250 g
02/01/18 10:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 9 of 10

r �rv-�� *�} 1 �%n{'"Y. 4t7,� I ^. k. C ��l�yl'i.f S1Yl0_tN.i
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rd' 6„�,, s= „,r ''LABORA"CORIES, INC.
Project Name: ReLP.IVCCi ON Wt_7 IC:1 ?
449 Springbrook Road • Charlotte, NC 28217 short Hold Analysis: (Yes) (I I®) UST Project: (lies) (i!9®) PROPER PRESERVATIVES indicated?
Phone [phone] Fax: [phone]
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ATTACH any Project specific reporting (QC LEVEL I II Ill IV) Received WITHIN HOLDING TIMES?
CUSTODY SEAL. S.I11TAC;T?
Client Company Name: o O-P
provisions
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TEMP: Therm ID: } �/ `Observed:°C t Corr:__°C
Phone: m��� �r � .Faxs CGS (No):70g. PI B"S Purchase Order Ho./Billing Reference O BE MLLED lH BY CUENT/SAMPLMG PERSONNEL
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Site Location Physical Address: � U ��Q li
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COLLECTED
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Upon relinquishing, this Chain of Custody Is your authorization for
Prism to Proceed vuith the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will he charges for any chapoes after analyses have been initialized.
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A
R = ISM
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: Stal-ime
Lab Submittal Date: 02/12/2018
Prism Work Order: 8020215
Case Narrative
02/20/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT{([Cal +[Mg])/2}
sae, G-GS�
SAR = [ 84/23 ] / SQRT { ( [1100/20] + [0.022/12]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) t�- a_ "--
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 10

Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than IN the MB.
DM Sample diluted and RL increased due to the matrix.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 10

Sample Receipt Summary
02/20/2018
Al
jn I S Full -Service Analytical
r�''-� Environmental Solutions
/P--R, +LABORATORIES, INC.
C10-~l- Sample ID
e
Lab Sample ID Matrix Date Sampled
8020215-01 Solid 02/12/18
Samples were received at 21.3 degrees C. See case narrative for further information.
Prism Work Order: 8020215
Date Received
02/12/18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page T7771

A Laboratory Report
I s m Full -Service Analytical &
Environmental solutions 02/20/2018
LABORATORIES INC.
0-ifv nf Statesville, NC Project: StaLime Client Sample ID: StaLime
F ndy Smith Prism Sample ID: 8020215-01
F._. __)x 1111 Prism Work Order: 8020215
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/12/18 12:00
Time Submitted: 02/12/18 15:35
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1700
mg/kg dry
520
110
5
*Calculation
2119/18 9:20
CLB
[CALC]
% Solids
72.9
% by
0.100
0.100
1
*SM2540 G
2/13/18 15:11
BJC
P8130256
Weight
Ammonia as N
96
mg/kg dry
14
3.4
1
*SM4500-NH3 C
2/15/18 14:30
BMS
P8130325
Nitrate/Nitrite as N
21
mg/kg dry
6.9
0.75
1
*SM4500-NO3 F
2/16118 10:58
CLB
P8B0287
Phosphorus -Total
2300
mg/kg dry
69
9.9
20
*SM4500-P F
2114/18 11:53
CLB
P8B0248
Total Kjeldahl Nitrogen
5600
mg/kg dry
1700
370
5
*351.2
2/19/18 9:20
CLB
P8B0321
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
2/13/18 9:05
EGC
P880282
Total Metals
Mercury
0.13
mg/kg dry
0.028
0.0026
1
*7471B
2119/18 12:17
JAB
P8130339
SAR Soil Preparation
Complete
g
1
*2-78-054
2/19/18 9:00
JAB
P880279
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
2/19/18 8:00
JAB
P8130332
Weight
Arsenic
8.1 DM
mg/kg dry
3.4
0.41
10
*6010D
2116/18 16:41
JAB
P8130253
Absorption Ratio
0.68
[blank]
0.30
0.016
1
*2-78-054
2/16/18 18:35
JAB
P8130324
C n
BRLDM
mg/kg dry
3.4
0.091
10
*6010D
2/16/18 16:41
JAB
P8130253
Calcium
1100 B
mg/L
1.0
0.10
10
*6010D
2/16/18 18:26
JAB
P8B0324
Copper
37 DM
mg/kg dry
6.8
0.61
10
*6010D
2116118 16:41
JAB
P8130253
Lead
5.2 DM
mg/kg dry
3.4
0.63
10
*6010D
2/16/18 16:41
JAB
P8130253
Magnesium
BRL
mg/L
0.10
0.0086
1
*6010D
2/16/18 18:35
JAB
P8130324
Nickel
8.4 DM
mg/kg dry
6.8
0.24
10
*6010D
2/16/18 16:41
JAB
P8130253
Selenium
23 DM
mg/kg dry
6.8
1.6
10
*6010D
2/16118 16:41
JAB
PBB0253
Sodium
720 DM
mg/kg dry
200
6.7
10
*6010D
2116118 16:41
JAB
P8B0253
Sodium
84 B
mg/L
0.50
0.018
1
*6010D
2116/18 18:35
JAB
P8130324
Zinc
68 DM
mg/kg dry
34
1.2
10
*6010D
2/16/18 16:41
JAB
P8130253
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 10

Level II QC Report
J I Full -Service Analytical & 2/20/18
Environmental Solutions
✓LAEORAMRIES. ING
City of Statesville, NC
A idy Smith
P. K 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8B0253 - 3050B
Blank (P8130253-BLK1)
Prepared &Analyzed: 02/14/18
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P8130253-13SI)
Prepared &Analyzed: 02/14/18
Arsenic
12.7
0.25
mg/kg wet
12.50 101
80-120
Cadmium
12.9
0.25
mg/kg wet
12.50 103
80-120
Copper
13.5
0.50
mg/kg wet
12.50 108
80-120
Lead
13.1
0.25
mg/kg wet
12.50 105
80-120
Nickel
13.0
0.50
mg/kg wet
12.50 104
80-120
Selenium
12.3,
0.50
mg/kg wet
12.50 98
80-120
c��il Im
1320
15
mg/kg wet
1250 106
80-120
i
12.7
2.5
mg/kg wet
12.50 102
80-120
Batch P8B0279 - SAR 2-78-054
Blank (P8130279-13LK1) Prepared: 02/15/18 Analyzed: 02/19/18
SAR Soil Preparation Complete g
Batch P8B0324 - 3010A
Blank (P860324-BLK1)
Prepared & Analyzed: 02/16/18
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium
0.207 0.10 mg/L BH
Magnesium
BRL 0.10 mg/L
Sodium
1.05 0.50 . mg/L BH
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 10

J]1P-- I S Full -Service Analytical &
Environmental Solutions
V - -'✓ LABORATORIES, INC.
City of Statesville, NC Project: Stal-ime
Al dy Smith
P. c 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
2/20/18
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8BO332 - NO PREP
Duplicate (P8130332-DUP1) Source: 8020215-01 Prepared: 02/16/18 Analyzed: 02/19/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.2 200
Batch P8B0339 - 7471 B
Blank (P8130339-131-K1) Prepared &Analyzed: 02/19/18
Mercury BRL 0.020 mg/kg wet
LCS (P8B0339-BS1) Prepared &Analyzed: 02/19/18
Mercury 0.424 0.020 mg/kg wet 0.4167 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 6 of 10

Level II QC Report
A0;R Full -Service Analytical & 2/20/18
P�R I S M I Environmental Solutions
01
r''LABORATORIES, INC.
City of Statesville, NC
A Idy Smith
P, x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:00PM
Analyte
Reporting
Result Limit
Units
Spike Source %REC
Level Result %REC Limits RPD
RPD
Limit Notes
Batch P81B0248 - SM4500-PB5
Blank (P8B0248-BLK1)
Prepared &Analyzed: 02/14/18
Phosphorus -Total
LCS (P8B0248-BS1)
BRL 2.5
mg/kg wet
Prepared &Analyzed: 02/14/18
Phosphorus -Total
Matrix Spike (P8B0248-MS1)
95.2 2.5 mg/kg wet
Source: 8020215-01
100.0 95 90-110
Prepared &Analyzed: 02/14/18
Phosphorus -Total
Matrix Spike Dup (P8B0248-MSD1)
2190 69 mg/kg dry
Source: 8020215-01
137.1 2330 NR 80-120
Prepared &Analyzed: 02/14/18
MC
Phosphorus -Total
Batch P8B0287 - NO PREP
2470 69
mg/kg dry
137.1 2330 100 80-120 12
20
Blank (P8130287-BLK1)
Prepared: 02/15/18 Analyzed: 02/16/18
Nitrate/Nitrite as N
LCS (P8B0287-BS1)
BRL 5.0
mg/kg wet
Prepared: 02/15/18 Analyzed: 02/16/18
Nitrate/Nitrite as N
Matrix Spike (P8B0287-MS1)
47.6 5.0
Source: 8020215-01
mg/kg wet
50.00 95 80-120
Prepared: 02/15/18 Analyzed: 02/16/18
r litrite as N
1 Spike Dup (PBB0287-MSD1)
87.4 6.9
Source: 8020215-01
mg/kg dry
68.57 21.2 97 80-120
Prepared: 02/15/18 Analyzed: 02/16/18
Nitrate/Nitrite as N
Batch P8B0321 - 351.2
86.1 6.9
mg/kg dry
68.57 21.2 95 80-120 1
20
Blank (P8B0321-BLK1)
Prepared: 02/16/18 Analyzed: 02/19/18
Total Kjeldahl Nitrogen
BRL 25
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 10

/ s,l I S Full -Service Analytical &
Environmental Solutions
tsrLABORATORIE$ ING
Level II QC Report
2/20/18
City of Statesville, NC Project: StaLime
/ ndy Smith
F )x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:OOPM
Reporting Spike Source %aREC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBB0321 - 351.2
LCS (P8B0321-BS1) Prepared: 02/16/18 Analyzed: 02/19/18
Total Kjeldahl Nitrogen 513 100 mg/kg wet 500.0 103 90-110
Batch P8B0325 - SM4500-NH3 B
Blank(P8B0325-BLK1) Prepared &Analyzed: 02/15/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8B0325-BSI) Prepared &Analyzed: 02/15/18
Ammonia as N 456 10 mg/kg wet 500.0 91 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 Of 1

Level II QC Report
I n Full -Service Analytical 2/2l7/1$
- ' V' Environmental Solutions
�v�LA90RATORIES, INC.
City of Statesville, NC Project: StaLime Prism Work Order: 8020215
A idy Smith Time Submitted: 2/12/2018 3:35:OOPM
P. K 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8B0282 - NO PREP
Blank (P8B0282-BLK1) Prepared &Analyzed: 02/13/18
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
8020215-01 P860321 0.05 g 25 mL 02/16/18 10:15
Prep Method: SM4500-NH3 B
Lab Number Batch Initial Final Date/Time
8020215-01 P8130325 1 g 50 mL 02/15/18 14:30
Prep Method: SM4500-PB5
I ' -" nber Batch Initial Final Date/Time
F i-01 PBB0248 1 g 50 mL 02/14/18 6:30
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
8020215-01 P8B0256 30 g 30 g 02/13/18 15:11
Prep Method: 3010A
Lab Number Batch Initial Final Date/Time
8020215-01
P8B0324
50 mL
50 mL
02/16/18 9:00
8020215-01
P8B0324
50 mL
50 mL
02/16/18 9:00
8020215-01
P8130324
50 mL
50 mL
02/16/18 9:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8020215-01
P8B0253
2.02 g
50 mL
02/14/18 8:25
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8020215-01
P8B0339
0.59 g
50 mL
02/19/18 9:10
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
15-01
P8B0279
250 g
250 g
02/15/18 8:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 9 Of 10

CUSUDDY RECORD
Full-Service Analytical &
Solutions EAOE_
11 S M I
CD
YES NO: N/A r
®� �aa�o� c �® ��ssa rec �R®�tsR Buie urs�: INTAr a upon asnval r. `� - o
Environmental — , mples
r„ `'111
Clyed t0N WCT ICD
T
A"'l. �..,„,,,,, I.,na., n> LABORATORIES, INC. �r��@�$ Name:
449 Springbrook Road • Charlotte, INC 28217 l?R4t'LR PRLSCRV/'T'UCS 117cilcatr d?;:: '" N
Short Hold Analysis: (Yes) (Nod US � Project: (Yes) (NO)
IULDING TIMES?
Phone 704/529-G364 Fax: [phone]
0° fI *Please
�
ATTACFI any project specific6'ep®6rirtg (QC LE!/EL I BI Ill IV)cefved VVITWIN I - CZ
AC � a
F SEALS IN 1:1JT i ?
Client Company Name: C a 12 � U provislions and/or QC RequirementsGJSTOD _ _
Report To/Contact Name: ��ree�s9 ��e�� — IrnV®iC@To° Vbik:LESrecdVN/�Jl HCAD�F'F\CC?
f'Ri7Pl P �CiNTAiNGR , u ed?
Reporting Address: Address: TEMP' Thilm IDnb elvccl ` °C! Gorr A°C
�.._� _
Phone:702- 6 d 6° 3"13Fax es (1e9�): d�S�° ° "� Purchase Order No./Billing Reference TO BE FOLLED OVA BY CLIENT /SAM FLING PERSONNEL
Email Address: Requested Due Date ® 1 Day 132 Days ® 3 Days ® 4 Days © 5 Days CertfflcaUon° N1P-LAC D©D FL MC
EDD Type: PDFEaGGI Other "Working Days" ® 6-9 Days ® Standard 10 days p Rush pork Must Be
9 Y Y Pre -Approved SC O T HER MIA
�J
Site Location Name: °�� � caTr it Samples received after 14:00 will be processed next business day.
l ( Turnaround time is based on business days, excluding weekends and holidays. rIdatev Chlorinated: YES— NO_
Site Location Physical Address: b� Y 11)A FArPon � - REGARDING SERVICES
.
(SEE REVERSE FOR TERMS & CONDITIONS
S�r�i®le Iced ��®®r1®Ol��tl®t�: v��_ NO_
RENDERED BY PRISM LABORATORIES, INC. To CLIENT)
TIME MAT RIX
CLIENT DATE COLLECTED (SOIL,
SAMPLE CONTAINER ANALYSIS REQUESTED PRISM
PRESERVA- l�c� REMARKS LAB
� �i�
TIi/ES ID N®.
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
"TYPE N® SIZE
HOURS SLUDGE)
SEE BELOW
al
C¢a
SA A.
UaY 6
°�OaO
T
LT�
�' Sampled By (Print Name) /t 9 �' d�'� �� Affiliation
Sampler'sSignature��
Upon relinquishing, thus Chain of Custody is your author5zation for
Prism to proceed with the analyses as requested] above. Any changes must We
submitted In t'VPlting to the Prism Project Manager. There will PO@ CI➢aPgO ny Changes after analyses have been initialized.
Reli (shed By: (Sign re)Recel
�) g
d (Si alum} Date litary/ rs Additional Comments: Situ /arrival I line
/� E p ��"1 _
,4" € 51?e Departure Time
Relin shed By: (Signature) Re eived
By: (Signature) D e
I�m- I
. -
ll Field7ech Fee:: -.
'A Date
iva--
Relinquished By: (Signature) Recee Far p ism Laboratories By: Vi��l_ t - -- — - r -m ----
-
I nv' 4 .•�
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT I �H C STORY SEALS FOR TRANSPORTATION TO TEIE, LABORATORY. COC Group No. --
SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. l �p_$ 7 ,.y`^i) O
--nd-delivered Service ❑ Other ` �
El Fed Ex ID UPS Prism Field
NP®ES: t GROUNDWATER: DRINKING WATER:S®LIID UIIASTE: RCR CEpCLA LANDFILL I OTHER:
®NC®SC: L. 1-1SC®NC ©SC ONC ©SC
®NC ®SC 0N( ®NC ©SC ®NC ®SC I ®NC ®SC
R n
TI --r 1I".n_1 i-I f'o11 \/f ),q= XMIR111A LIME:1111L:5 HI ItIIVDIL 1LCIU 1ICO P-)

NC Certification No.402 Case Narrative
0PI S M I Full -Service Analytical & NC Drinking water cert No. 37735 04/04/2018
f"'� Environmental Solutions SC Certification No. 99012
�:rLABORAI UMIES, INC.
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 03/26/2018
Statesville, NC 28687 Prism Work Order: 8030410
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR = [ Na ] / SQRT { ( [Ca] + [Mg] ) / 2 }
SAR = [ 175/23 ] /SQRT { ([2810/201 + [1.2/12.21) / 2 } 5A Yz-
1Y_1Z11101111110071i
Intrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 17

X
i
Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration > RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1Ox the MB.
BL MB greater than one half of the RL, but the sample concentrations are less than the RL.
DM Sample diluted and RL increased due to the matrix.
BRL Below Reporting Limit)
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 Of 17

A
J�79 R I S Fult-Service Analytical &
.- Environmental Solutions
�:"LARORAT0RIE4 ING
Sample Receipt Summary
04/04/2018
Prism Work Order: 8030410
C"--` Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
ie (and Fecal 1)
8030410-01
Solid
03/26/18
03/26/18
Fecal #2
8030410-02
Solid
03/26/18
03/26/18
Fecal #3
8030410-03
Solid
03/26/18
03/26/18
Fecal #4
8030410-04
Solid
03/26/18
03/26/18
Fecal #5
8030410-05
Solid
03/26/18
03/26/18
Fecal #6
8030410-06
Solid
'03/26/18
03/26/18
Fecal #7
8030410-07
Solid
03/26/18
03/26/18
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 17

APR I S M EnvFull-Service Analytical &
ironmental Solutions
Q LABORATORIE% INC.
Laboratory Report
04/04/2018
C;*- -11 Statesville, NC
P idy Smith
F- -max 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: StaLime (and Fecal 1)
Prism Sample ID: 8030410-01
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1700
mg/kg dry
510
110
5
*Calculation
4/2/18 14:40
CLB
[CALC]
Solids
74.6
% by
0.100
0.100
1
*SM2540 G
3/28/18 15:00
BJC
P8130021
Weight
Ammonia as N
1900
mg/kg dry
13
3.3
1
*SM4500-NH3 C
4/2/18 14:40
BMS
138D0030
Nitrate/Nitrite as N
BRL
mg/kg dry
6.7
0.74
1
*SM4500-NO3 F
3/29/18 10:29
CLB
P8C0465
Phosphorus -Total
2800
mg/kg dry
67
9.7
20
*SM4500-P F
3/29/18 7:07
CLB
P8C0413
Total Kjeldahl Nitrogen
4300
mg/kg dry
1700
360
5
*351.2
4/2/18 7:44
CLB
P8C0484
Microbiological Parameters
Fecal Coliforms
Total Metals
BRL
MPN/g dry
0.3
1
*SM9221 E
3/27/18 9:48
BMS
P8C0486
Mercury
0.030
mg/kg dry
0.026
0.0025
1
*7471B
3/28/18 14:19
JAB
P8C0466
SAR Soil Preparation
Complete
g
1
*2-78-054
4/4/18 10:11
MMR
P8C0473
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
4/2/18 9:52
MMR
P8D0007
Weight
Arsenic
BRLDM
mg/kg dry
6.7
0.41
10
*6010D
3129118 16:43
JAB
P8C0462
Absorption Ratio
0.91
[blank]
0.30
0.016
1
*2-78-054
3/29/18 16:06
JAB
P8C0491
( n
BRLDM
mg/kg dry
3.3
0.089
10
*6010D
3/29/18 16:43
JAB
P8C0462
Calcium, SAR
2800 B
mg/L
1.0
0.10
10
*6010D
3/29/18 16:06
JAB
P8C0491
Copper
33
mg/kg dry
6.7
0.60
10
*6010D
3/29118 16:43
JAB'
P8C0462
Lead
3.6
mg/kg dry
3.3
0.62
10
*6010D
3/29/18 16:43
JAB
P8C0462
Magnesium, SAR
1.2
mg/L
1.0
0.086
10
*6010D
3/29/18 16:06
JAB
P8C0491
Nickel
6.9
mg/kg dry
6.7
0.24
10
*6010D
3/29/18 16:43
JAB
P8C0462
Potassium
2300
mg/kg dry
170
6.0
10
*6010D
3/29/18 16:43
JAB
P8C0462
Selenium
13
mg/kg dry
6.7
1.6
10
*6010D
3/29/18 16:43
JAB
P8C0462
Sodium
610
mg/kg dry
200
6.5
10
*6010D
3129/18 16:43
JAB
P8C0462
Sodium, SAR
180 B
mg/L
5.0
0.18
10
*6010D
3/29/18 16:06
JAB
P8C0491
Zinc
59
mg/kg dry
33
1.2
10
*6010D
3/29/18 16:43
JAB
P8C0462
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 17

Laboratory Report
Full -Service Analytical &
P}R I � � Environmental Solutions
/
04/04/2018
•.' LABORATORIES, ING
Citv of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Fecal #2
P idy Smith
60Day 7 Fecal)
Prism Sample ID: 8030410-02
F Ix 1111
Prism Work Order: 8030410
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 68.3
% by
0.100 0.100
1 *SM2540 G 3/28118 15:00 BJC
PBD0021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 3/27/18 9:48 BMS
P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 17

PR I S M Full -Service Analytical &
OiiATOPIES ING
t Environmental Solutions
�LAB
City_ of Statesville, NC
/ ndy Smith
F )x 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
04/04/2018
Client Sample ID: Fecal #3
Prism Sample ID: 8030410-03
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 71.7
% by
0.100
0.100 1 *SM2540 G 3/28118 15:00 BJC
P8D0021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 3/27/18 9:48 BMS
P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 17

O I S n n Full -Service Analytical 8
r� ' V' I Environmental Solutions
'\✓LABORATORIES INO
Laboratory Report
04/04/2018
Citv of Statesville, NC
,ridy Smith
F >x 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #4
Prism Sample ID: 8030410-04
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datef-l-ime
ID
General Chemistry Parameters
% Solids 75.3
% by
0.100
0.100 1
*SM2540 G 3/28/18 15:00 BJC
P8130021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 3/27/18 9:48 BMS
P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 17

Laboratory Report
R I S AP Full -Service Analytical R
04/04/2018
Environmental Solutions
�`.-�L BORATORIE$ ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #5
F ndy Smith 60Day 7 Fecal) Prism Sample ID: 8030410-05
F )x 1111 Prism Work Order: 8030410
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date[Time ID
General Chemistry Parameters
% Solids 73.9 % by 0.100 0.100 1 'SM2540 G 3128118 15:00 BJC PBD0021
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 3/27/18 9:48 BMS P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 17

R I V' M n Full -Service Analytical &
' Environmental Solutions
LABORATOHIE$ ING
Citv of Statesville, NC
P tidy Smith
F )x 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
04/04/2018
Client Sample ID: Fecal #6
Prism Sample. ID: 8030410-06
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Daterrime
ID
General Chemistry Parameters
% Solids 72.9
% by
0.100
0.100 1
*SM2540 G 3/28118 15:00 BJC
PBD0021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 3/27118 9:48 BMS
P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 17

a-, moo,
J� I s Full Service Analytical &
Environmental Solutions
. LABORATORIES, INC.
Laboratory Report
04/04/2018
Citv of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #7
/ ndy Smith 60Day 7 Fecal) Prism Sample ID: 8030410-07
F )x 1111 Prism Work Order: 8030410
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
% Solids 75.3 % by 0.100 0.100 1 `SM2540 G 3/28118 15:00 BJC P8130021
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 3/27/18 9:48 BMS P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 10 of 17

/•� 2 I S n I Full -Service Analytical &
'v' Environmental Solutions
�MLABORATORIES INC.
Level II QC Report
4/4/18
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8030410
A idy Smith 7 Fecal) Time Submitted: 3/26/2018 3:00:OOPM
P. x 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
I
Batch P8C0462 - 3050B
Blank (P8C0462-BLK1)
Prepared: 03/28/18 Analyzed: 03/29/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
BH
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
2.85
2.5
mg/kg wet
BH
LCS (P8C0462-BS1)
Prepared: 03/28/18 Analyzed: 03/29/18
Arsenic
13.2
0.50
mg/kg wet
12.50 105 80-120
Cadmium
13.5
0.25
mg/kg wet
12.50 108 80-120
Copper
14.2
0.50
mg/kg wet
12.50 114 80-120
Lead
13.6
0.25
mg/kg wet
12.50 109 80-120
Nickel
13.7
0.50
mg/kg wet
12.50 109 80-120
Pr,ta�gi lm
1420
12
mg/kg wet
1250 114 80-120
n
12.0
0.50
mg/kg wet
12.50 96 80-120
1430
15
mg/kg wet
1250 115 80-120
Zinc
13.5
2.5
mg/kg wet
12.50 108 80-120
Batch P8C0466 - 7471 B
Blank (P8C0466-BLK1) - Prepared &Analyzed: 03/28/18
Mercury BRL 0.020 mg/kg wet
LCS (P8C0466-BS1) Prepared &Analyzed: 03/28/18
Mercury 0.438 0.020 mg/kg wet 0.4167 105 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 17

J®r�R ISM Full -Service Analytical &
Environmental Solutions
1•%'E AOOR TCRIE$ INC.
Level II QC Report
4/4/18
City of Statesville, NC
Al dy Smith
P. K 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8030410
Time Submitted: 3/26/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8CO473 - SAR 2-78-054
Blank (P8C0473-BLK1) Prepared: 03/28/18 Analyzed: 04/04/18
SAR Soil Preparation Complete g
Batch P8C0491 - 3010A
Blank (P8C0491-BLK1)
Prepared & Analyzed: 03/29/18
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium, SAR
0.386 0.10 mg/L BH
Magnesium, SAR
BRL 0.10 mg/L BL
Sodium, SAR
2.59 0.50 mg/L A
Batch P8D0007 - NO PREP
Duplicate (P8D0007-DUP1) Source: 8030410-01 Prepared &Analyzed: 04/02/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.4 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 17

WSM
ORATORIES' INC.
Full -Service Analytical &
Environmental Solutions
Level II QC Report
4/4/18
City of Statesville, NC
A; ' idy Smith
P, x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality,Control
Analyte
Batch P8CO413 - SM4500-PB5
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8030410
7 Fecal) Time Submitted: 3/26/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8C0413-BLK1) Prepared: 03/28/18 Analyzed: 03/29/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8C0413-BS1) Prepared: 03/28/18 Analyzed: 03/29/18
Phosphorus -Total 96.0 2.5 mg/kg wet 100.0 96 90-110
Batch P8CO465 - NO PREP
Blank(P8C0465-BLK1) Prepared: 03/28/18 Analyzed: 03/29/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P8C0465-BSI) Prepared: 03/28/18 Analyzed: 03/29/18
Nitrate/Nitrite as N 49.8 5.0 mg/kg wet 50.00 100 80-120
Batch P8C0484 - 351.2
Blank (P8C0484-BLK1) Prepared: 03/29/18 Analyzed: 04/02/18
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P8C0484-BS1) Prepared: 03/29/18 Analyzed: 04/02/18
TntaLKieldahl Nitrogen 548 100 mg/kg wet 500.0 110 90-110
I Spike (P8C0484-MS2) Source: 8030410-01 Prepared: 03/29/18 Analyzed: 04/02/18
)o[al ryeldahl Nitrogen 11400 1700 mg/kg dry 6703 4290 106 90-110
Batch P8DO030 - SM4500-NH3 B
Blank (P8D0030-BLK1) Prepared & Analyzed: 04/02/18
Ammonia as N BRL 10 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 77-7-1
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 17

R I � %� Environmental
Analytical
' V' Environmental Solutions
�,✓LABORATORIES, INC.
Level II QC Report
4/4/18
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8030410
A. idy Smith 7 Fecal) Time Submitted: 3/26/2018 3:00:OOPM
P. x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8DO030 - SM4500-NH3 B
LCS (P8D0030-BSI) Prepared &Analyzed: 04/02/18
Ammonia as N 512 10 mg/kg wet 500.0 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 17

Level II QC Report
I S Full -Service Analytical 4/4/18
Environmental Solutions
LAOORATORIES, INC.
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 8030410
A dy Smith 7 Fecal) Time Submitted: 3/26/2018 3:00:00PM
P., K 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8C0486 - NO PREP
Blank (P8C0486-BLKI) Prepared &Analyzed: 03/27/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 17

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
80'' )1
P8C0484
0.05 g
25 mL
03/29/18 10:10
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8D0030
1.01 g
50 mL
04/02/18 14:02
C
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0413
1 g
50 mL
03/28/18 10:00
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8D0021
30 g
30 g
03/28/18 15:00
8030410-02
P8D0021
30 g
30 g
03/28/18 15:00
8030410-03
P8D0021
30 g
30 g
03/28/18 15:00
8030410-04
P8130021
30 g
30 g
03/28/18 15:00
8030410-05
P8D0021
30 g
30 g
03/28/18 15:00
8030410-06
P8D0021
30 g
30 g
03/28/18 15:00
8030410-07
P8D0021
30 g
30 g
03/28/18 15:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0491
50 mL
50 mL
03/29/18 2:30
gngnn+n-01
P8C0491
50 mL
50 mL
03/29/18 2:30
I -. thod:3050B
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
PBC0462
2.01 g
50 mL
03/28/18 8:45
8030410-01
P8C0462
2.01 g
50 mL
03/28/18 8:45
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0466
0.61 g
50 mL
03/28/18 11:20
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0473
250 g
250 g
03/28/18 14:14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 17

VlY WAN O CUSTODYRECORD
�" Full -Service Analytical &
J,�PI Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
.Y.",RSM
�.-. 1111
`LABOR.arORIES, INC.
Project Name:
449 Springbrook Road • Charlotte, NC 28217 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Phone [phone] • Fax: [phone]
�, , � n �.�A I E$y,� f p�, *Please ATTACH any project specific reporting (QC LEVEL 1 II Ill IV)
Client Company Name: �r n'P' - ' d provisions and/or QC Requirements
Report To/Contact Name: A N o1y' S i;4-Ji Invoice To:
Reporting Address: Address:
YES NO NIA r\
Samples INTACT upon arrival? T
Received ON WET ICE?
PROPER PRESERVATIVES indicated? r
Received WITHIN HOLDING TIMES? N
CUSTODY SEALS INTACT?
VOLATILES redd WIOUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: ThermlD:ltUi-? Observed:
_L7 .°C/Corr 2 I°C�
Phone:70+ 17N93t Fax es (No): 7®°l• $7 f- Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
EDD Type: PDF Excel Other "Working Days" U 6-9 Days ❑ Standard 10 days ❑ P sh Nor Mdust Be SC OTHER
N/A
//�
Site Location Name: Fod4R44 Ct?1TCY Samples received, after14:00 will be processed next bOsiness'day.
Site Location Physical Address: � Eltf FAR+'ri l5 Turnaround time is basad on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO_
SERVICES
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING
sample Iced upon Collection: YES_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) 1� p
NO
TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- !� f f f. \1y -, " i REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE TIMES (► ! f �;�'r r'
NO. SIZE 1{ f r
:S:
ID NO.
HOURS SLUDGE) EE BELOW 411,''
�I�/'L 'Cyi
3-a`-i8
d�• !
[
14A as20�
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i_�e�wf,ek
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41 to
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7 F
CA
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SA
PL66
i
.44
I
I
Name) T I R J K Affiliation
Sampler's Signature Sampled By (Print
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed With-th analyses as requested above. Any changes must be1.1
L.
°
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin ed:By: (Signal ) / Racelvatl y (£'gnaturel� � Date r�illloyrh{ours Additional Comments:
Site Arrival Time:
Departure Time:
a Gt/ _
Rel' bed By: (Signature) -/ 136nived By: (Signature) / D�te r
Site
/ Rexive.d For Ptism Lnlmrntorle .By:
Relingtii ed�y: ( lgnatura) // /� /vo
1 6 �
rD t
Field Tech Fee:
Mileage:
f 0E Group No:
-WITH
Macho 1pmeN: OTE:iSLL SAMPt3='COOLERS.�1•IOULD BE TAPED SI1UT CUSTODY SEALS FO�t TRANSPORTATION T. THE LABORATORY,
F
SAMPLES ARE NOT-A'CCEP7ED AND, VERIFIED AGAINST COC UNTIL RECEIVED AT TjFiE LABORATORY. n ► J *�
r/I(
l►�//{
❑ titer r (/1j
�
❑ Fed Ex ❑ UPS 1-delivered I$ Prism Field Service
NPDES: U: DRINKING WATER: SOLID WASTE: RCRP CERCLA LANDFILL OTHER:
❑NC❑SCI ❑.._ _SC ❑NC ❑SC I ❑❑NC ❑SC ONC ❑SC 10ENC aNC ❑SC oNC ❑SC oNC ❑SC
IGnROUNDWATER:
n- r_in— P = Plagtic: I L = Zenon -Linea uav vvra — vulau1w viya1u r.­�y­ r'1%pl(31N1A1

A.'
PE! ISM
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No.402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11/2019
Environmental Solutions SC Certification No. 99012
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 05/07/2018
Prism Work Order: 8050101
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the first revised report dated 01/29/19. The SAR comment has been added
below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
__ _ : = [ 120/23.0 ] / SQRT { ( [1500/20.0] + [0.085/12.21) / 2 }
SA ►-s 0 40,5
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
1z:::: ��_ 61"C' -
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 20

A,
NC Certification No. 402 Case Narrative
/A;
M Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11/2019
Environmental Solutions SC Certification No. 99012
7�.7LLABORATORIE$ INC.
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 05/07/2018
Statesville, NC 28687 Prism Work Order: 8050101
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the first revised report dated 01/29/19. The SAR comment has been added
below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
_...: _ [ 120/23.0 ] / SQRT { ( [1500/20.0] + [0.085/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
001
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 20

Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration >1/2 RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
DM Sample diluted and RL increased due to the matrix.
M Matrix spike outside of the control limits:'
BRL Below Reporting Limit
MDL Method Detection Limit
I Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDLwith values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 2 of 20

Analytical &
Full-S�r] I Environmental
-�'" 1=nvironmental Solutions
sm I
LABORATORIES INC.
Sample Receipt Summary
02/11/2019
Prism Work Order: 8050101
r";-nt Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
_ime (and Fecal 1)
8050101-01
Solid
05/07/18 13:05 05/07/18 15:00
Fecal #2
8050101-02
Solid
05/07/18 13:05 05/07/18 15:00
Fecal #3
8050101-03
Solid
05/07/18 13:05 05/07/18 15:00
Fecal #4
8050101-04
Solid
05/07/18 13:05 05/07/18 15:00
Fecal #5
8050101-05
Solid
05/07/18 13:05 05/07/18 15:00
Fecal #6
8050101-06
Solid
05/07/18 13:05 05/07/18 15:00
Fecal #7
8050101-07
Solid
05/07/18 13:05 05/07/18 15:00
Samples were received in good condition at 2.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 20

Full -Service Analytical &
-�P R I S M Environmental Solutions
Laboratory Report
02/11 /2019
City of Statesville, NC
is Andy Smith
Box 1111
Statesville, NC 28687
Client Sample ID: StaLime (and Fecal 1)
Prism Sample ID: 8050101-01
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst
Limit Factor Date/Time
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Batch
ID
General Chemistry Parameters
Plant Available Nitrogen
2000
mg/kg dry
470
100
5
*Calculation
6110118 8:58
CLB
[CALC]
% Solids
81.5
% by
0.100
0.100
1
*SM2540 G
5/10118 14:50
TJY
P8E0251
Weight
Ammonia as N
2500
mg/kg dry
12
3.1
1
*SM4500-NH3 C
5/8/18 14:08
BMS
P8E0162
Nitrate/Nitrite as N
11
mg/kg dry
6.1
1.7
1
*SM4500-NO3 F
5/9/18 9:11
CLB
P8E0174
Phosphorus -Total
3200
mg/kg dry
61
8.8
20
*SM4500-P F
518/18 10:31
CLB
P8E0084
Total Kjeldahl Nitrogen
4800
mg/kg dry
1500
330
5
*351.2
5110118 8:58
CLB
P8E0178
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
5/8/18 9:39
BMS
P8E0184
Total Metals
Mercury
0.24
mg/kg dry
0.025
0.0023
1
*747113
5/11118 15:02
JAB
P8E0248
SAR Soil Preparation
Complete
g
1
*2-78-054
5/9/18 10:25
MMR
P8E0152
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
5/10/18 10:50
MMR
P8E0218
Weight
Arsenic
BRLDM
mg/kg dry
6.1
0.37
10
*6010D
5/9/18 21:46
JAB
P8E0182
_ m Absorption Ratio
0.88
[blank]
0.30
0.016
1
*2-78-054
6111/18 14:49
JAB
P8E0188
iium
BRLDM
mg/kg dry
3.1
0.082
10
*6010D
5/9/18 21:46
JAB
P8E0182
Calcium, SAR
1500
mg1L
10
1.0
100
*6010D
5111/18 14:40
JAB
P8E0188
Copper
170 DM
mg/kg dry
6.1
0.55
10
*601013
5/9118 17:42
JAB
P8E0182
Lead
5.1 DM
mg/kg dry
3.1
0.57
10
*6010D
519118 21:46
JAB
P8E0182
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
5/11/18 14:49
JAB
P8E0188
Nickel
10 DM
mg/kg dry
6.1
0.22
10
*6010D
5/9/18 21:46
JAB
P8E0182
Potassium
2500 DM
mg/kg dry
150
5.5
10
*6010D
5111/18 15:31
JAB
P8E0182
Selenium
BRLDM
mg/kg dry
6.1
1.5
10
*6010D
5/9/18 17:42
JAB
P8E0182
Sodium
3800 DM
mg/kg dry
180
6.0
10
*6010D
5/9/18 17:42
JAB
P8E0182
Sodium, SAR
120 B
mg/L
5.0
0.18
10
*601013
6/9118 17:42
JAB
P8E0188
Zinc
76 DM
mg/kg dry
31
1.1
10
*6010D
519/18 21:46
JAB
P8E0182
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 20

PI Full-ServiceService Analytical/A, Environmental Solutionss�--S.��LABORATORIES INC,SM
City of Statesville, NC
Andy Smith
.._. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #2
Prism Sample ID: 8050101-02
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 91.2 % by 0.100 0.100 1 *SM2540 G 5/10/18 14:50 TJY P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2
1 *SM9221 E 5/8/18 9:39 BMS P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-300/529-6364 - Fax: [phone] Page 5 of 20

R I n Full -Service Analytical &
rJ ' V' Environmental Solutions
��-'LABORATORIES, ING
Laboratory Report
02111 /2019
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Fecal #3
: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 8050101-03
.._. Box 1111
Prism Work Order: 8050101
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/07/18 13:05
0
Time Submitted: 05/07/18 15:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
89.6 % by
0.100 0.100
1 'SM2540 G 5/10/18 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 `SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 20

�/- R ISM
S � %� FulliService Analytical &
/l<' J � V � Environmental Solutions
5—l7—QRATCAIE$ Ma
Laboratory Report
02/11 /2019
City of Statesville, NC
I: Andy Smith
.__.Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #4
Prism Sample ID: 8050101-04
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 89.1
% by
0.100
0.100 1
*SM2540 G 6/10118 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 20

I %� Fun -Service Analytical &
' b' Environmental Solutions
T� ,'LABORATORIESINC.
City of Statesville, NC
: Andy Smith
.. _ . Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #5
Prism Sample ID: 8050101-05
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 88.1
% by
0.100
0.100 1
*SM2540 G 6/10118 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
*SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 20

A., IFull-Service Analytical &
—Environmental Solutions
ABORATORIES, INC.
City of Statesville, NC
Andy Smith
�. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #6
Prism Sample ID: 8050101-06
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatefTime ID
General Chemistry Parameters
% Solids 72.2 % by 0.100 0.100 1 'SM2540 G 5/10/18 14:50 TJY P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 `SM9221 E 5/8/18 9:39 BMS P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 20

Laboratory Report Is FullService Analytical &
AP'�--,R
environmental Solutions 02/11/2019
LARORATORIES, INO
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #7
n: Andy Smith 60Day 7 Fecal) Prism Sample ID: 8050101-07
). Box 1111 Prism Work Order: 8050101
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 85.9 % by 0.100 0.100 1 *SM2540 G 6/10/18 14:50 TJY P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 5/8/18 9:39 BMS P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 20

Full -Service Analytical
Environmental Solutions
�'i
LABORATORIES,
ING.
Level II QC Report
2111/19
City of Statesville, NC
Andy Smith
3ox 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 8050101
7 Fecal) Time Submitted: 5/7/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8EO152 - SAR 2-78-054
Blank (P8E0152-BLK1) Prepared: 05/08/18 Analyzed: 05/09/18
SAR Soil Preparation Complete g
Batch P8EO182 - 3050B
Blank (P8E0182-BLK1)
Prepared &Analyzed: 05/09/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
BH
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P8E0182-BS1)
Prepared &Analyzed: 05/09/18
Arsenic
12.2
0.50
mg/kg wet
12.50 98
80-120
ium
12.5
0.25
mg/kg wet
12.50 100
80-120
;r
13.1
0.50
mg/kg wet
12.50 105
80-120
Leao
12.4
0.25
mg/kg wet
12.50 99
80-120
Nickel
12.6
0.50
mg/kg wet
12.50 100
80-120
Potassium
1310
12
mg/kg wet
1250 105
80-120
Selenium
11.6
0.50
mg/kg wet
12.50 93
80-120
Sodium
1230
15
mg/kg wet
1250 98
80-120
Zinc
12.4
2.5
mg/kg wet
12.50 99
80-120
Matrix Spike (P8E0182-MS1)
Source: 8050101-01
Prepared &Analyzed: 05/09/18
Arsenic
20.7
6.1
mg/kg dry
15.35 4.93 103
75-125
Cadmium
15.2
3.1
mg/kg dry
15.34 0.476 96
75-125
Copper
59.5
6.1
mg/kg dry
15.35 166 NR
75-125
M
Lead
20.2
3.1
mg/kg dry
15.35 5.12 99
75-125.
Nickel
25.3
6.1
mg/kg dry
15.35 10.4 97
75-125
Potassium
4240
150
mg/kg dry
1534 2500 113
75-125
Selenium
24.4
6.1
mg/kg dry
15.34 BRL 159
75-125
M
Sodium
2600
180
mg/kg dry
1534 3780 NR
75-125
M
Zinc
89.1
31
mg/kg dry
15.35 75.8 87
75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 20

Full -service Analytical &
PR I S Environmental Solutions
•l __Y_1-L4B0RAT0RIES, INC.
Level Il QC Report
2/11/19
City of Statesville, NC Project: StaLime (Qtrly, Biweekly, 60Day Prism Work Order: 8050101
Andy Smith 7 Fecal) Time Submitted: 5/7/2018 3:00:OOPM
3ox 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8EO182 - 3050B
Matrix Spike Dup (P8E0182-MSD1)
Source: 8050101-01
Prepared &Analyzed: 05/09/18
Arsenic
21.2
6.1
mg/kg dry
15.35 4.93 106
75-125
3
20
Cadmium
15.5
3.1
mg/kg dry
15.34 0.476 98
75-125
1
20
Copper
59.9
6.1
mg/kg dry
15.35 166 NR
75-125
0.7
20
M
Lead
20.4
3.1
mg/kg dry
15.35 5.12 100
75-125
0.8
20
Nickel
25.6
6.1
mg/kg dry
15.35 10.4 99
75-125
1
20
Potassium
3900
150
mg/kg dry
1534 2500 91
75-125
8
20
Selenium
24.2
6.1
mg/kg dry
15.34 BRL 158
75-125
0.8
20
M
Sodium
2660
180
mg/kg dry
1534 3780 NR
75-125
2
20
M
Zinc
90.0
31
mg/kg dry
15.35 75.8 92
75-125
1
20
Batch P8EO188 - 301 OA
Blank (P8E0188-BLK1)
Prepared &Analyzed: 05/09/18
Calcium, SAR
BRL
0.10
mg/L
BH
Magnesium, SAR
BRL
0.10
mg/L
Sodium, SAR
4.05
0.50
mg/L
A
" h P8E0218 - NO PREP
icate (P8E0218-DUP1)
Source: 8050101-01
Prepared &Analyzed: 05/10/18
SAR Percent Moisture
Complete
0.100
% by Weight
Complete
3
200
Batch P8EO248 - 7471 B
Blank (P8E0248-BLK1)
Prepared &Analyzed: 05/11/18
Mercury
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 20

I S Full -Service Analytical &
/'J-111
Environmental Solutions
✓ 1210 ATORIES, INC.
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8050101
Time Submitted: 5/7/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8EO248 - 7471B
LCS (P8E0248-BS1) Prepared &Analyzed: 05/11/18
Mercury 0.397 0.020 mg/kg wet 0.4167 95 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 20

i
Rt, ISM
��'✓ LABORATORIES, INC.
Full -Service Analytical &
Environmental Solutions
Level li QC Report
2111/19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8E0084 - SM4500-PB5
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8050101
7 Fecal) Time Submitted: 5/7/2018 3:00:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8E0084-BLK1) Prepared &Analyzed: 05/08/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8E0084-BS1) Prepared &Analyzed: 05/08/18
Phosphorus -Total 103 2.5 mg/kg wet 100.0 103 90-110
Batch P8E0162 - SM4500-NH3 B
Blank (P8E0162-BLK1) Prepared: 05/07/18 Analyzed: 05/08/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8E0162-BS1) Prepared: 05/07/18 Analyzed: 05/08/18
Ammonia as N 482 10 mg/kg wet 500.0 96 80-120
Batch P8E0174 - NO PREP
Blank (P8E0174-BLK1) Prepared &Analyzed: 05/09/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P8E0174-13SI) Prepared &Analyzed: 05/09/18
Nitrate/Nitrite as N 51.3 5.0 mg/kg wet 50.00 103 80-120
xSpike (P8E0174-MS1) Source: 8050101-01 Prepared &Analyzed: 05/09/18
Nitrate/Nitrite as N 74.4 6.1 mg/kg dry 61.37 11.4 103 80-120
Matrix Spike Dup (P8E0174-MSD1) Source: 8050101-01 Prepared &Analyzed: 05/09/18
Nitrate/Nitrite as N 71.9 6.1 mg/kg dry 61.37 11.4 99 80-120 3 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 14 of 20

Level II QC Report
I Full -Service Analytical & 2/11/19
f - Environmental Solutions
.�' -tea'✓LABORATORIES, ING
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8EO178 - 351.2
Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 8050101
7 Fecal)- Time Submitted: 5/7/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8E0178-BLK1) Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P8E0178-BS1) Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen 469 100 mg/kg wet 500.0 94 90-110
Matrix Spike (P8E0178-MS1) Source: 8050101-01 Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen 10600 1500 mg/kg dry 6137 4790 95 90-110
Matrix Spike Dup (P8E0178-MSD1) Source: 8050101-01 Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen 11600 1500 mg/kg dry 6137 4790 111 90-110 9 20 M
Batch P8E0251 - Solids Dry Weight
Duplicate (P8E0251-DUP4) Source: 8050101-01 Prepared &Analyzed: 05/10/18
% Solids 80.8 0.100 % by Weight 81.5 0.8 20
I
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 15 of 20

Level II QC Report
Full -Service Analytical & 2/11/19
Ah I S 1 tl , Environmental Solutions
�ORATORIES ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8050101
Andy Smith 7 Fecal) Time Submitted: 5/7/2018 3:00:OOPM
Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8EO184 - NO PREP
Blank (PBE0184-BLK1) Prepared & Analyzed: 05/08/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 16 of 20

Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
D1-01 P8E0178 0.05 g 25 mL 05/09/18 9:35
Prep Method: SM4500-NH3 B
Lab Number Batch Initial Final Date/Time
8050101-01 P8E0162 1 g 50 mL 05/08/18 9:00
Prep Method: SM4500-PBS
Lab Number Batch Initial Final Date/Time
8050101-01 P8E0084
Prep Method: Solids, Dry Weight
Lab Number Batch
1 g
Initial
50 mL
Final
05/08/18 6:15
Date/Time
8050101-01
P8E0251
30 g
30 g
05/10/18 14:50
8050101-02
P8E0251
30 g
30 g
05/10/18 14:50
8050101-03
P8E0251
30 g
30 g
05/10/18 14:50
8050101-04
P8E0251
30 g
30 g
05/10/18 14:50
8050101-05
P8E0251
30 g
30 g
05/10/18 14:50
8050101-06
P8E0251
30 g
30 g
05/10/18 14:50
8050101-07
P8E0251
30 g
30 g
05/10/18 14:50
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
101,101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
0uw101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0182
2 g
50 mL
05/09/18 8:20
8050101-01
P8E0182
2 g
50 mL
05/09/18 8:20
8050101-01
P8E0182
2 g
50 mL
05/09/18 8:20
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0248
0.6 g
50 mL
05/11/18 12:00
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0152
250 g
250 g
05/08/18 10:25
J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 17 of 20

-CHAEN OF CUSTODY RECORD
�� ` Full -Service Analytical &
r• S M I Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
x r— —.,.
ORATORIES. INC,
449 Springbrook Road • Chaflotte, NC 28217 Project Name:
Phone [phone] • Fanx: 7041525-0409 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
C a i S 1q 1 F.5 V JJS *Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Client Company Nance: r o Y- provisions and/or QC Requirements
Report To/Contact Name: A a RY Sm, A - invoice To:
Reporting Address: Address:
YES NO N/A CD
N
Samples INTACT upon arrival? —
0
Received ON WET ICE? _G cp
PROPER PRESERVATIVES indicated? �' T
Received WITHIRHOLDING TIMES?
CUSTODY SEALS INTACT? cd
VOLATILES reed W/OUT HEADSPACE? _
PROPER CONTAINERS used?
TEMP: Therm IQ i_l Observed: •• &'G°rco
Phone:704f- 979. 3qj $ FaX4E3) (No): VON- 819- At SS purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC Do® FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ P h Work Mdust Be
SC OTHER NIA
Site Location Name: Foua.°ih r~aeE�'k Samples received after 14:00 will be processed next business day.
t�- np
Site Location Physical Address' -9 _R 'Sd/ FAyw9 RJQ- Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YE NO_
TIME
MATRIX
SAMPLE CONTAINER
PRESERVA-
ANALYSIS
r f
REQUESTED
RISM
FLAB
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
(SOIL,
WATER OR
TIMES
; j•' \y ; f` % REMARKS
U� r'�' l i
ID NO.
*TYPE I
NO.
SIZE
HOURS
SLUDGE)
SEE BELOW I
S > A ` L'of 4f
3: 7— J
/3.
S
P
I
A�
I
03
cQ
6� ��� ���W 1
Pb
I NA
s
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IN
I
I
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H:
P&SIAJ,
07
Se
PA •
ZAP
SA
I
1
I m I
oe
e.
Sampler's Signature Sampled By (Print Name) IRV gemk Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
°
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relingk�ished 6y;,(S;goal ), Rece et1 By:'(S,Ignnturol Date
Military/Hours Additional Comments: Site Arrival Time:
Rot' hed By: (Slgna ed y: (Signature) ! Date
Site Departure Time:
Relinq sh By (Signa[ur Received For Prism lnhofatar �'6 : JJ `Date
Field Tech Fee:
00
15 Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION T THE LABORATORY. COG Group No.
SAMPLES ARE NOTA EPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT TH LABORATORY.
�O s®
n j
I v I
Q Fed Ex ❑ UPS ❑ n Hand -delivered m Field Service El Other
NPDES: U GR U DWATER: DRINKING WATER: SOLID WASTE: If RCRP • CERCLA LANDFILL
OTHER:
°
❑NC❑SC ❑ ]SC ❑ C ❑SC ❑NC ❑SC ❑NC ❑SC I ❑NC El NC ❑SC ❑NC El SC
❑NC ❑SC
❑ 0 ❑ . ❑ ❑ I ❑ ❑ ❑
0

_
Main Office:
Full Saivica Analytical and
449 Springbrook Road
P.O. Box 240543
'PRISM;Environmental Solutions
Charlotte, NC 28224 0543
Phone: [phone]
1/800/529-6364
Fax: [phone]
www.prismiabs.com
Plant Available Nitrogen
Sample Numberl 8050101-01 1 Sample Narne Stal-ime
Mineralization
Rate
TKN
NH3
NOX
me/L
MAIL
Mq/L
0.3
4791
2522
11.3
PAN Surface
2,000 mglkg
Calculated By:
MR(TKN-NH3)+ 0.5(NH3)+NOX = PAN mg/kg
77-7-1
Page 19 of 20

Main Office:
449 Springbrook Road
i Full Sarviro Analytical and P.O. Box 240543
', I
.,• I Environi�onYal Solutions Charlotte, NC 28224-0543
Phone: [phone]
11800/529-6364
Fax: [phone]
www.prismlabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Number8050101-01 1 Sample Name Sta-Lime
Na: Sodium (mg/L) Equivalent weight: 23
Ca: Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg1L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam /L . Cam /L MgLrn /L
123 T--1-4-80-7 0.085
Na ME'
Ca ME
Nlq_(ME),
5.35
1 74
1 0.01
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.88 (From mg/L entered above)
Calculated By:
Page 20 of 20

I
"J/P''sm
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 05/22/2018
Prism Work Order: 8050384
Case Narrative
02/11 /2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the first revised report dated 01/29/19. The SAR comment has been added
below.
Analysis note for SAR: 5A�, d
SAR = [ Na ] / SQRT { ( [Ca] + [Mg] ) / 2 }
= [ 100/23.0 ] / SQRT { ( [1500/20.01 + [0.089/12.2] ) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 13

Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration >1/2 RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
mmq Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13

,P R ISFull-Service Analytical &
.'' Environmental Solutions
��' LABORATORIES, INC.
Sample Receipt Summary
02/11 /2019
Prism Work Order: 8050384
Client Sample ID
Jrne
Lab Sample ID Matrix
8050384-01 Solid
Samples were received in good condition at 2.4 degrees C unless otherwise noted.
Date/Time Sampled
05/22/18 12:06
Date/Time Received
05/22/18 13:26
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13

/dPRISM Full -Service Analytical &
Environmental Solutions
- JLg...RIE$ING
Laboratory Report
02/11 /2019
City of Statesville, NC
Project: StaLime
Client Sample ID:
StaLime
Andy Smith
Prism Sample ID: 8050384-01
_ _ _ _ Box 1111
Prism Work Order:
8050384
Statesville, NC 28687
Sample
Matrix: Solid
Time
Collected: 05/22/18 12:06
Time
Submitted: 05/22/18 13:26
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
2100
mglkg dry
460
98
5
*Calculation
6/6/18 8:01
CLB
[CALC]
% Solids
83.7
% by
0.100
0.100
1
*SM2540 G
5/25/18 15:55
TJY
P8E0562
Weight
Ammonia as N
1700
mglkg dry
12
3.0
1
*SM4500-NH3 C
5/24/18 14:30
BMS
P8E0518
Nitrate/Nitrite as N
BRL
mg/kg dry
6.0
1.6
1
*SM4500-NO3 F 5/25/18 8:20
CLB
P8E0497
Phosphorus -Total
3000
mglkg dry
60
8.6
20
*SM4500-P F
5124118 8:31
CLB
P8E0432
Total Kjeldahl Nitrogen
5800
mglkg dry
1500
320
5
*351.2
616118 8:01
CLB
PSE0557
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
5123/18 9:23
BMS
P8E0517
Total Metals
Mercury
0.17
mglkg dry
0.024
0.0023
1
*747113
5/30118 14:22
JAB
P8E0575
SAR Soil Preparation
Complete
g
1
*2-78-054
5/25/18 14:25
MMR
P8E0482
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
5/25/18 14:25
MMR
P8E0537
Weight
Arsenic
BRL
mg/kg dry
5.9
0.36
10
*6010D
6/5/18 13:20
JAB
P8E0492
1-fi--m Absorption Ratio
0.71
[blank]
0.30
0.016
1
*2-78-054
5125118 4:50
PJF
P8E0502
ium
BRL
mg/kg dry
3.0
0.080
10
*6010D
6/5118 13:20
JAB
P8E0492
Calcium, SAR
1500 B
mg/L
1.0
0.10
10
*6010D
5125118 4:50
PJF
P8E0502
Copper
34 BH
mg/kg dry
5.9
0.54
10
*6010D
615/18 13:20
JAB
P8E0492
Lead
4.1
mg/kg dry
3.0
0.55
10
*6010D
5129118 14:07
JAB
P8E0492
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
5/25118 4:58
PJF
P8E0502
Nickel
8.6
mg/kg dry
5.9
0.21
10
*6010D
5129118 14:07
JAB
P8E0492
Potassium
2100
mg/kg dry
150
5.4
10
*60101)
615/18 13:20
JAB
P8E0492
Selenium
18
mg/kg dry
5.9
1.4
10
*6010D
5129/18 14:07
JAB
P8E0492
Sodium
590 BH
mg/kg dry
180
5.8
10
*6010D
5/29/18 14:07
JAB
P8E0492
Sodium, SAR
100 B
mg/L
5.0
0.18
10
*6010D
5/25/18 4:50
PJF
P8E0502
Zinc
61
mglkg dry
30
1.1
10
*6010D
6/5/18 13:20
JAB
P8E0492
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 13

Full -Service Analytical & ism
? � Environmental Solutions
-1Vv'L SQ0 T0RIES INC.
Level II QC Report
2/11 /19
City of Statesville, NC
, Andy Smith
IBox 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8E0482 - SAR 2-78-054
Project: StaLime
Reporting
Result Limit Units
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P8E0482-BLK1)
Prepared: 05/23/18 Analyzed: 05/25/18
SAR Soil Preparation
Complete
g
Batch P8E0492 - 3050B
Blank (P8E0492-BLK1)
Prepared: 05/24/18 Analyzed: 05/25/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
0.601
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P8E0492-BSI)
Prepared: 05/24/18 Analyzed: 05/25/18
Arsenic
12.2
0.50
mg/kg wet
12.50 97 80-120
Cadmium
12.4
0.25
mglkg wet
12.50 99 80-120
°r
13.7
0.50
mg/kg wet
12.50 110 80-120
____
12.5
0.25
mg/kg wet
12.50 100 80-120
Nickel
12.6
0.50
mg/kg wet
12.50 101 80-120
Potassium
1270
12
mg/kg wet
1250 102 80-120
Selenium
11.5
0.50
mg/kg wet
12.50 92 80-120
Sodium
1230
15
mg/kg wet
1250 98 80-120
Zinc
12.4
2.5
mg/kg wet
12.50 99 80-120
Matrix Spike (P8E0492-MS1)
Source: 8050384-01
Prepared: 05/24/18 Analyzed: 05/29/18
Arsenic
19.9
6.0
mg/kg dry
14.94 3.89 107 75-125
Cadmium
15.5
3.0
mg/kg dry
14.94 0.272 102 75-125
Copper
48.7
6.0
mg/kg dry
14.94 33.9 99 75-125
Lead
19.6
3.0
mg/kg dry
14.94 4.15 103 75-125
Nickel
23.3
6.0
mg/kg dry
14.94 8.63 98 75-125
Potassium
3750
150
mg/kg dry
1494 2150 107 75-125
Selenium
32.2
6.0
mg/kg dry
14.93 18.5 92 75-125
Sodium
2100
180
mg/kg dry
1494 592 101 75-125
Zinc
73.0
30
mg/kg dry
14.94 61.1 80 75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 13

Level II QC Report
R Full -Service Analytical & 2/11/19
�l Environmental Solutions
--�'��LI 20R TORIES. INC
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Reporting
Analyte Result Limit Units
Batch P8E0492 - 3050B
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P8E0492-MSD1)
Source: 8050384-01
Prepared: 05/24/18 Analyzed: 05/29/18
Arsenic
21.3
6.0
mg/kg dry
14.94
3.89
116
75-125
7
20
Cadmium
15.4
3.0
mg/kg dry
14.94
0.272
101
75-125
0.2
20
Copper
50.2
6.0
mg/kg dry
14.94
33.9
109
75-125
3
20
Lead
19.2
3.0
mg/kg dry
14.94
4.15
101
75-125
2
20
Nickel
23.5
6.0
mg/kg dry
14.94
8.63
99
75-125
0.6
20
Potassium
3820
150
mg/kg dry
1494
2150
112
75-125
2
20
Selenium
34.7
6.0
mg/kg dry
14.93
18.5
109
75-125
7
20
Sodium
2130
180
mg/kg dry
1494
592
103
75-125
2
20
Zinc
75.2
30
mg/kg dry
14.94
61.1
94
75-125
3
20
Batch P8EO502 - 3010A
Blank (P8E0502-BLK1)
Prepared: 05/24/18 Analyzed: 05/25/18
Sodium Absorption Ratio
BRL
0.30
[blank]
Calcium, SAR
1.00
0.10
mg/L
BH
Magnesium, SAR
BRL
0.10
mg/L
A
Sodium, SAR
3.43
0.50
mg/L
BH
h P8EO537 - NO PREP
Duplicate (P8E0537-DUP1)
Source: 8050384-01
Prepared &Analyzed: 05/25/18
SAR Percent Moisture
Complete
0.100
% by Weight Complete 0.7 200
Batch P8EO575 - 7471B
Blank (P8E0575-BLK1)
Prepared &Analyzed: 05/30/18
Mercury
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] - Page 6 Of 13

/ Full -Service Analytical &
�P, Y , Environmental Solutions
✓�LAOOR TOHIES, INC.
Level II QC Report
2/11 /19
City of Statesville, NC Project: StaLime
Andy Smith
'Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8E0575 - 7471 B
LCS (1P8E0575-BS1) Prepared &Analyzed: 05/30/18
Mercury 0.387 0.020 mg/kg wet 0.4167 93 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 13

Full -Service Analytical &
Environmental Solutions
1�'7 B RATORIE8, INC
Level II QC Report
2/11 /19
City of Statesville, NC Project: StaLime
Andy Smith
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8E0432 - SM4500-PB5
Reporting
Result Limit Units
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P8E0432-BLK1)
Prepared: 05/23/18 Analyzed: 05/24/18
Phosphorus -Total
BRL 2.5
mg/kg wet
LCS (P8E0432-BS1)
Prepared: 05/23/18 Analyzed: 05/24/18
Phosphorus -Total
103 2.5
mg/kg wet
100.0 103 90-110
Batch P8E0497 - NO PREP
Blank (P8E0497-BLK1)
Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N
BRL 5.0
mg/kg wet
LCS (P8E0497-BS1)
Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N
51.0 5.0
mg/kg wet
50.00 102 80-120
Matrix Spike (P8E0497-MS1)
Source: 8050384-01
Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N
65.6 6.0
mg/kg dry
59.75 2.81 105 80-120
Matrix Spike Dup (P8E0497-MSD1)
Source: 8050384-01
Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N
62.8 6.0
mg/kg dry
59.75 2.81 100 80-120 4 20
Batch P8E0518 - SM4500-NH3 B
k (P8E0518-BLK1) Prepared &Analyzed: 05/24/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8E0518-BS1) Prepared &Analyzed: 05/24/18
Ammonia as N 487 10 mg/kg wet 500.0 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 13

J,.
I Full -Service Analytical &
Environmental Solutions
Qr'iLA O0 T0FIE5. ING
Level II QC Report
2/11 /19
City of Statesville, NC Project: StaLime
Andy Smith
3ox 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8E0557 - 351.2
Blank (P8E0557-BLK1)
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
BRL 25 mg/kg wet
LCS (P8E0557-BS1)
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
537 100 mg/kg wet
500.0 107 90-110
Matrix Spike (P8E0557-MS1)
Source: 8050384-01
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
11400 1500 mglkg dry
5975 5840 92 90-110
Matrix Spike Dup (P8E0557-MSD1)
Source: 8050384-01
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
10700 1500 mglkg dry
5975 5840 81 90-110 6 20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 13

/�,-ZR
IFull-Service Analytical&
Environmental Solutions
Z"i`L BORATORIES, INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
2/11 /19
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8E0517 - NO PREP
Blank (P8E0517-BLK1)
Prepared &Analyzed: 05/23/18
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0557
0.05 g
25 mL
05/29/18 10:30
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0518
1 g
50 mL
05/24/18 14:30
Prep Method: SM4500-13135
-` ?lumber
Batch
Initial
Final
Date/Time
384-01
P8E0432
1 g
50 mL
05/23/18 10:45
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0562
30 g
30 g
05/25/18 15:55
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0502
50 mL
50 mL
05/24/18 14:15
8050384-01
P8E0502
50 mL
50 mL
05/24/18 14:15
8050384-01
P8E0502
50 mL
50 mL
05/24/18 14:15
Prep Method: 3050B
Lab Number
Batch
Initial
Final
DatelTime
8050384-01
P8E0492
2.01 g
50 mL
05/24/18 8:20
8050384-01
P8E0492
2.01 g
50 mL
05/24/18 8:20
8050384-01
P8E0492
2.01 g
50 mL
05/24/18 8:20
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0575
0.6 g
50 mL
05/30/18 9:45
Prep Method: SAR 2-78-054
Number
Batch
Initial
Final
Date/Time
8050384-01 P8E0482 250 g 250 g 05/23/18 13:55
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 13

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Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be PR1_ ONLY
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Main Office:
449 Springbrook Road
f' Full Service Analytical and P.O. Box 240543
R I S M Environmental Solutions Charlotte, NC 28224-0543
Phone: [phone]
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Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Numberl 8050384-01 Sample Namel Stal-ime
Na: Sodium (mg/L) Equivalent weight: 23
Ca : Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam /L Cam /L M m /L
100 1500 1 0.089
Na (ME)
Ca ME
Mg_ ME
4.35
1 75
1 0.01
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.71 (From mg/L entered above)
Calculated By: ,f `6U(
V �.
Page 12 of 13

�' � IS I� /( I Fuq aI aoI t and
_ f_� �/ � Envlro!i�uunlal SolufIon o
Plant Available Nitrogen
Main Office:
449 Springbrook Road
P.O. Box 240543
Charlotte, NC 28224.0543
Phone: [phone]
11800/529.6364
Fax: [phone]
www,prlsmlabs.com
Sample Numberl 8050384-01 1 Sample Name Stal-ime
Mineralization
Rate TKN NH3 NOX
ma/L M /L M- /L.
0.3 5800 1700 2.8
PAN Surface
---2,083 1 mg/kg
Calculated By: I�,�
MR(TKN-NH3)+ 0.5(NH3)+NOX = PAN mg/kg
Page 13 of 13

NC Certification No. 402
Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11 /2019
/A/P� I S MEnvironmental Solutions SC Certification No. 99012
ABORATORIES, INC.
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 09/10/2018
Statesville, NC 28687 Prism Work Order: 8090114
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised laboratory report dated 01/29/19. The SAR comment has been
added below.
Analysis note for SAR:
SAR = [ Na ] / SQRT { ( [Ca] + [Mg] ) / 2 )
= [ 130/23.0 ] / SQRT { ( [16000/20.01 + [0/12.2] ) / 2 )
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Fecal Coliform test failed Quality Control and were cancelled by the laboratory.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 12

Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than IN the MB.
D RPD value outside of the control limits.
M Matrix spike outside of the control limits.
Mc
Sample concentration too high for recovery evaluation.
PS
Post Spike recovery is outside of the control limits.
BRL
Below Reporting Limit
MDL
Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 12

Sample Receipt Summary
AY Full -Service Analytical &
I Environmental Solutions 02/11/2019
SMI
�✓ LABORATORIES, INC.
Prism Work Order: 8090114
c';ant Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
_time (and Fecal 1) 8090114-01 Solid 09/10/18 8:25 09/10/18 13:15
Samples were received in good condition at 2.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 12

r'
.� Full -Service Analytical &
e�ism Environmental Solutions P
-1",77 SORATORIES, ING
Laboratory Report
02/11 /2019
City of Statesville, NC
Andy Smith
r.v. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: StaLime (and Fecal 1)
Prism Sample ID: 8090114-01
Prism Work Order: 8090114
Time Collected: 09/10/18 08:25
Time Submitted: 09/10/18 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1900
mg/kg dry
400
86
5
*Calculation 9/17/18
8:34
CLB
[CALC]
% Solids
95.1
% by
0.100
0.100
1
*SM2540 G 9/14118
9:45
TJY
P810191
Weight
Ammonia as N
4100
mg/kg dry
10
2.6
1
*SM4500-NH3 C 9/14/18
16:00
BMS
P810196
Nitrate/Nitrite as N
0
mg/kg dry
5.3
1.4
1
*SM4500-NO3 F 9114118
9:33
CLB
P810183
Phosphorus -Total
2r00
mg/kg dry
53
12
20
*SM4500-P F 9113/18
7:23
CLB
P810138
Total Kjeldahl Nitrogen
3460
mg/kg dry
1300
280
5
*351.2 9/17118
8:34
CLB
P810167
(j
Total Metals
f
Mercury
0.13
mg/kg dry
0.021
0.0020
1
*7471B
9/12118 11:21
MMR
P810134
SAR Soil Preparation
Complete
g
1
*2-78-054
9/12/18 13:00
MMR
P810133
SAR Percent Moisture
59.7
% by
0.100
0.100
1
*2-78-054
9113118 13:15
MMR
P810175
Weight
Arsenic
6.5
mg/kg dry
0.53
0.032
1
*6010D
9/12118 14:47
JAB
P810136
Sodium Absorption Ratio
BRL
[blank]
2.0
0.016
1
*2-78-054
9/12118 15:54
JAB
P810146
Cadmium
BRL
mg/kg dry
0.26
0.0070
1
*601 OD
9/12/18 14:47
JAB
P810136
-'-'-Im, SAR
16000 B
mg/L
10
1.0
100
*6010D
9/12118 15:46
JAB
P810146
ar
35
mg/kg dry
0.53
0.048
1
*6010D
9112118 14:47
JAB
P810136
Lead
3.6
mg/kg dry
0.26
0.049
1
*6010D
9112/18 14:47
JAB
P810136
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
9/12/18 15:54
JAB
P810146
Nickel
6.1
mg/kg dry
0.53
0.019
1
*6010D
9112118 14:47
JAB
P810136
Potassium
1600
mg/kg dry
13
0.47
1
*6010D
9112118 14:47
JAB
13810136
Selenium
BRL,,
mg/kg dry
0.53
0.12
1
*601 OD
9/12/18 14:47
JAB
P810136
Sodium
460
mg/kg dry
16
0.52
1
*6010D
9/12118 14:47
JAB
P810136
Sodium, SAR
130 B
mg/L
0.50
0.018
1
*6010D
9112118 16:54
JAB
P810146
Zinc
34
mg/kg dry
2.6
0.094
1
*6010D
9/12/18 14:47
JAB
P810136
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 12

I SM Full -Service Analytical
Environmental Solutions
A I BORATORIE$ INC.
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8090114
Time Submitted: 9/10/2018 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P810133 - SAR 2-78-054
Blank (P810133-BLK1) Prepared: 09/11/18 Analyzed: 09/12/18
SAR Soil Preparation Complete g
Batch P810134 - 7471 B
Blank (P810134-BLK1) Prepared &Analyzed: 09/12/18
Mercury BRL 0.020 mg/kg wet
LCS (P810134-BS1) Prepared &Analyzed: 09/12/18
Mercury 0.489 0.020 mg/kg wet 0.4167 117 80-120
Batch P810136 - 3050B
Blank (P810136-BLK1)
Prepared &Analyzed: 09/12/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
iium
BRL
12
mg/kg wet
um
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P810136-BSI)
Prepared &Analyzed: 09/12/18
Arsenic
12.2
0.50
mg/kg wet
12.50 98
80-120
Cadmium
12.4
0.25
mg/kg wet
12.50 99
80-120
Copper
12.9
0.50
mg/kg wet
12.50 103
80-120
Lead
12.3
0.25
mg/kg wet
12.50 99
80-120
Nickel
12.5
0.50
mg/kg wet
12.50 100
80-120
Potassium
1250
12
mg/kg wet
1250 100
80-120
Selenium
12.1
0.50
mg/kg wet
12.50 97
80-120
Sodium
1250
15
mg/kg wet
1250 100
80-120
Zinc
11.9
2.5
mg/kg wet
12.50 95
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 12

0�1 Level II QC Report
I`- Full -Service Analytical 2/11 /19
JEnvironmental Solutions
1, LABORATORIES INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P810136 - 3050B
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8090114
7 Fecal) Time Submitted: 9/10/2018 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike (P810136-MS1)
Source: 8090114-01
Prepared &Analyzed: 09/12/18
Arsenic
19.6
0.53
mg/kg dry
13.15
6.47
100
75-125
Cadmium
9.78
0.26
mg/kg dry
13.14
0.211
73
75-125
M
Copper
47.3
0.53
mg/kg dry
13.15
35.1
93
75-125
Lead
13.6
0.26
mg/kg dry
13.15
3.59
76
75-125
Nickel
15.9
0.53
mg/kg dry
13.15
6.13
75
75-125
Potassium
3040
13
mg/kg dry
1314
1640
107
75-125
Selenium
14.5
0.53
mg/kg dry
13.14
0.332
108
75-125
Sodium
1770
16
mg/kg dry
1314
456
100
75-125
Zinc
45.1
2.6
mg/kg dry
13.15
33.8
86
75-125
Matrix Spike Dup (P810136-MSD1)
Source: 8090114-01
Prepared
&Analyzed:
09/12/18
Arsenic
19.5
0.53
mg/kg dry
13.15
6.47
99
75-125
0.5
20
Cadmium
9.82
0.26
mg/kg dry
13.14
0.211
73
75-125
0.4
20
M
Copper
46.6
0.53
mg/kg dry
13.15
35.1
87
75-125
2
20
Lead
13.3
0.26
mg/kg dry
13.15
3.59
74
75-125
2
20
M
Nickel
16.0
0.53
mg/kg dry
13.15
6.13
75
75-125
0.3
20
Potassium
3010
13
mg/kg dry
1314
1640
104
75-125
1
20
um
15.1
0.53
mg/kg dry
13.14
0.332
112
75-125
4
20
m
1740
16
mg/kg dry
1314
456
98
75-125
2
20
Zinc
45.3
2.6
mg/kg dry
13.15
33.8
88
75-125
0.5
20
Post Spike (P810136-PSI)
Source: 8090114-01
Prepared
&Analyzed:
09/12/18
Arsenic
0.773
mg/L
0.5001
0.246
105
80-120
Cadmium
0.387
mg/L
0.5000
0.00804
76
80-120
PS
Copper
1.88
mg/L
0.5001
1.34
109
80-120
Lead
0.532
mg/L
0.5001
0.137
79
80-120
PS
Nickel
0.624
mg/L
0.5001
0.233
78
80-120
PS
Potassium
117
mg/L
50.00
62.5
110
80-120
Selenium
0.592
mg/L
0.4999
0.0126
116
80-120
Sodium
69.4
mg/L
50.00
17.3
104
80-120
Zinc
1.79
mg/L
0.5001
1.28
102
80-120
I`
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 12

M n Environmental
Analytical
V' ' "J' Environmental Solutions
--�•%LABORATORIES, ING
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P810146 - 3010A
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
2/11/19
Prism Work Order: 8090114
Time Submitted: 9/10/2018 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P810146-BLK1) Prepared &Analyzed: 09/12/18
Sodium Absorption Ratio BRL 2.0 [blank]
Calcium, SAR 0.730 0.10 mg/L BH
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 2.18 0.50 mg/L BH
Batch P810175 - NO PREP
Duplicate (P810175-DUP1) Source: 8090114-01 Prepared: 09/12/18 Analyzed: 09/13/18
SAR Percent Moisture 57.1 0.100 % by Weight 59.7 4 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 12

fy .
1kis
e .✓VLABORATORIES. INC.
Full -Service Analytical &
Environmental Solutions
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P810138 - SM4500-PB5
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8090114
7 Fecal) Time Submitted: 9/10/2018 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P810138-BLK1) Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P810138-BSI) Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total 98.1 2.5 mg/kg wet 100.0 98 90-110
Matrix Spike (P810138-MS1) Source: 8090114-01 Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total 2460 53 mg/kg dry 105.1 2320 127 80-120 MC
Matrix Spike Dup (P810138-MSD1) Source: 8090114-01 Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total 2420 53 mg/kg dry 105.1 2320 94 80-120 1 20
Batch P810167 - 351.2
Blank (P810167-BLK1)
Prepared: 09/13/18 Analyzed: 09/17/18
Total Kjeldahl Nitrogen
LCS (P810167-BS1)
BRL 25
mg/kg wet
Prepared: 09/13/18 Analyzed: 09/17/18
Total Kjeldahl Nitrogen
Matrix Spike (P810167-MS1)
126 25 mg/kg wet
Source: 8090114-01
125.0 101 90-110
Prepared: 09/13/18 Analyzed: 09/17/18
Geldahl Nitrogen
mamx Spike Dup (P810167-MSD1)
8310 1300 mg/kg dry
Source: 8090114-01
5257 3380 94 90-110
Prepared: 09/13/18 Analyzed: 09/17/18
Total Kjeldahl Nitrogen
Batch P810183 - NO PREP
4760 1300
mg/kg dry
5257 3380 26 90-110 54 20 D, M
Blank (P810183-BLK1)
Prepared & Analyzed: 09/14/18
Nitrate/Nitrite as N
BRL 5.0
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 12

/'P
® IFull-Service Analytical�Environmental Solutionss �✓f BOR MRIE$ INC
Level II QC Report
2/11 /19
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8090114
Andy Smith 7 Fecal) Time Submitted: 9/10/2018 1:15:OOPM
3ox 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P810183 - NO PREP
LCS (P810183-BSI) Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N 49.4 5.0 mg/kg wet 50.00 99 80-120
Matrix Spike (P810183-MS1) Source: 8090114-01 Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N 170 5.3 mg/kg dry 52.57 108 119 80-120
Matrix Spike Dup (P810183-MSD1) Source: 8090114-01 Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N 168 5.3 mg/kg dry 52.57 108 114 80-120 2 20
Batch P810196 - SM4500-NH3 B
Blank (P810196-BLK1) Prepared: 09/13/18 Analyzed: 09/14/18
Ammonia as N BRL 10 mg/kg wet
LCS (P810196-BS1) Prepared: 09/13/18 Analyzed: 09/14/18
Ammonia as N 498 10 mg/kg wet 500.0 100 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 12

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
14-01
P810167
0.05 g
25 mL
09/13/18 10:00
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810196
1.01 g
50 mL
09/13/18 10:55
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810138
1 g
50 mL
09/12/18 9:43
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
13810191
30 g
30 g
09/14/18 9:45
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810146
50 mL
50 mL
09/12/18 13:00
8090114-01
P810146
50 mL
50 mL
09/12/18 13:00
8090114-01
P810146
50 mL
50 mL
09/12/18 13:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810136
2 g
50 mL
09/12/18 8:05
Vethod: 7471 B
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810134
0.61 g
50 mL
09/12/18 8:45
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810133
250 g
250 g
09/11/18 13:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 12

"'M
..LABORATORIES, ING
CHAIN. OF CUS700Y RECORD
Full -Service Analytical &
Environmental Solutions PAGE_ OF _ QUOTE # TO ENSU DPER BILLING:
449 Springbrook Road • Charlotte, NC 28217
Phone 704152M364 Fax: [phone]
Client Company Name: C;4y air VAIESY3:/E'
Report To/Contact Name kc,4 01aljoen Ay
Reporting Address: d
Project Name,
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
1 NO N/A
Samples INTACT upon arrival?
Received ON WET ICE? LG .
PROPER PRESERVATIVES indicated?�
Received WITHIN HOLDING TIMES? C/
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE? w
PROPER GOIgTAlNERS'uatd?
TEMP: Therm IDj_ [=l.Observed: 'Z '' °C! Corr: °C
Phone:70T 678' -343$ -Faxa (No):701/- 878 f6 S� purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
SC OTHER N/A
Site Location Name: Fomalh CR EE k Samples received after 14:00 will be processed next business day.
_
Site Location Physical Address: 41�'8E1(` FA1?n) Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS S CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO_
p p
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED, 1j
PRISM
CLIENT
%. ,;, REMARKS
/
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
"TYPE
NO.
SIZE
TIMES
�� f dry
ID NO.
HOURS
SLUDGE)
SEE BELOW
SfA�dC:eaa�
4^1®-It
M=25
nn
I
N
n2
�
CA
40 DAV7 e
03
I�
C
SA R
bl
1 I
7i
I
I
I
� de Affiliation
Sampler's Signature Sampled By (Print Name) J
Upon relinquishing, this hairs of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager., There will be chargesfQr any changes after analyses have been initialized.
nature) 0�ele- MllitaryMours Additional Comments: Site Arrival Time:
Re shed By. (Signature) 1 ®
%O� O
� / �
Rallnyc yi hed By: (Signamro) ure) ate Site Departure Time:
4,�adBy,'
Field Tech Fee:
lulshed By: (Signature) Lehamlories By: Date
%/� / J. %.� Mileage:
t 7�/j/✓fiL
CDidqJSlfipmant NOTE: SAMPLE COOLERS SHOULD BE TAPED -SHUT- CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No,
1 SA S ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
Ex o ❑ Handilelivered Prism Field Service ❑ Other
UST: G OUNDtNATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
C ❑SC❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑s( ❑NC ❑SCI ®NC ❑SCI LlNC ❑SC••❑
L
❑ ❑,se
rw�eevre rv�o rnn�c. A — A.. kti r — rl.,.,. ('— r_'1 ­ o — Dhoti.-• 71 - T 11 -1 in —I ( `nn 11f)A - Vnlatila Ornanice Annlv.,is (Zero Head Snacel

Main Office:
449 Springbrook Road
Full Servlee Analytical and P.O. BOX 240543
fr Environn;ental Solutions Charlotte, NC 28224-0543
Phone: [phone]
9 /800/529-6364
Fax: [phone]
www.prism[abs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Number8090114-01 1 Sample Name Sta-Lime
Na: Sodium (mg/L) Equivalent weight: 23
Ca: Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam /L Caf m 1L _ Mg(mg/L)
126 1 16300 1 0
Na (ME)
I Ca ME
Mg (ME)
5.48
815.000
1 0.0
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = < 2 (From mg/L entered above) 5pJ-
Calculated By:
c
0'0 '
Page 12 of 12

i . Case Narrative
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11 /2019
P I S M Environmental Solutions SC Certification No. 99012
J�`'v7LLABORATORIES, INC.
City of Statesville, NC Project: StaLime (60 Day/7 Fecal)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 09/11/2018
Statesville, NC 28687 Prism Work Order: 8090131
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised aboratory report dated 01/29.19 The SAR comment has been
removed. There was not an SAR request on this work order.
Please call if you have any questions relating to this analytical report.
pectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 11

A,Ji_4771ll I S 1 V 1
ABORATORMSB INC.
Full -service Analytical&
Environmental Solutions
Sample Receipt Summary
02/11/2019
Prism Work Order: 8090131
"';-nt Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
. __al #1
8090131-01
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #2
8090131-02
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #3
8090131-03
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #4
80901.31-04
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #5
8090131-05
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #6
8090131-06
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #7
8090131-07
Solid
09/11/18 12:00 09/11/18 14:35
Samples were received at 23.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone]
Page 2 of 11

,f
/Ppi �//�' Full -Service Analytical &
:.i�R ISM
S, Y , Environmental Solutions
i �SORATORIES, INC.
Citv of Statesville, NC
Andy Smith
. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #1
Prism Sample ID: 8090131-01
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 82.5
% by
0.100
0.100 1 *SM2540 G 9114/18 9:45 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 *SM9221 E 9/12118 10:39 BMS
P810172
I
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 11

r.,
t Full -Service Analytical &
�P R I S Environmental Solutions
-�� rL 50RATORIM INC
City of Statesville, NC
Andy Smith
.._.Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #2
Prism Sample ID: 8090131-02
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 99.5
% by
0.100
0.100 1
*SM2540 G 9114118 9:45 TJY
P8I0191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
"SM9221 E 9/12/18 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 11

A
��_ ISM I EnviService Analytical s
:' Environmental Solutions
�v L OR TORIEa ING
City of Statesville, NC
: Andy Smith
.._. Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #3
Prism Sample ID: 8090131-03
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 95.2
% by
0.100
0.100 1
"SM2540 G 9/14118 9:45 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
`SM9221 E 9/12/18 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 11

R i Full -Service Analytical s
Environmental Solutions
ABORATORIES ING
City of Statesville, NC
Andy Smith
Box 1111
Statesville. NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
0
Client Sample ID: Fecal #4
Prism Sample ID: 8090131-04
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
% Solids 95.1
% by
0.100
0.100 1 `SM2540 G 9114118 9:45 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 9/12118 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 11

zPRa Full -Service Analytical &
Environmental Solutions
Ism
_'K LW ORATORIES, ING
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #5
Prism Sample ID: 8090131-05
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
% Solids 94.8
% by
0.100
0.100 1
`SM2540 G 9/14/18 9:45 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 9/12/18 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 11

I � %� Full -Service Analytical
' V' Environmental Solutions
� L4BOMTORIE$ INC.
City of Statesville, NC
Andy Smith
_ _ Box 1111
'Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11/2019
Client Sample ID: Fecal #6
Prism Sample ID: 8090131-06
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 94.9
% by
0.100
0.100 1
`SM2540 G 9/14/18 9:45 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 9/12118 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 11

I ASM Full -Service Analytical s
f' r, Environmental Solutions
A�BORATORIES, IN.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #7
Prism Sample ID: 8090131-07
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 93.3 % by 0.100 0.100 1 *SM2540 G 9/14/18 9:45 TJY P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 9/12/18 10:39 BMS P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone]
Page 9 of 11

Jp I S Full -Service Analytical &
Environmental Solutions
0, ✓ I 50.TCRIES. INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime (60 Day/7 Fecal)
Level II QC Report
2/11/19
Prism Work Order: 8090131
Time Submitted: 9/11/2018 2:35:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P810172 - NO PREP
Blank (P810172-BLK1) Prepared &Analyzed: 09/12/18
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
8090131-01
P810191
8090131-02
P810191
8090131-03
P810191
8090131-04
P810191
8090131-05
P810191
8090131-06
P810191
8090131-07
P810191
Initial Final DatelTime
30
g 30 g
09/14/18
9:45
30
g 30 g
09/14/18
9:45
30
g 30 g
09/14/18
9:45
30
g 30 g
09/14/18
9:45
30
g 30 g
09/14/18
9:45
30
g 30 g
09/14/18
9:45
30
g 30 g
09/14/18
9:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 11

01P_
Full -Service Analytical &
1 Environmental Solutions
'F f -- 'I'7L4BORATORIE$ INC.
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] - Fax: [phone]
Client Company Name: C:¢v o-P Sql4a5y:1 C
Report To/Contact Name: krw GA 11010wy
Reporting Address: f
�.r v . �,s 4 �";"I Irbil �`: �,' �� �,}, d�I ��� t1` �.�;!.. �-• .r� �C�i'(J
PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
'Please ATTACH any project specific reporting (CSC LEVEL 1 II III IV)
provisions and/or OC Requirements
Invoice To:
Address:
Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID: 19--T - Observe
YES NO NI/i r
I v-
-s- — a>
�a-
d: " C Corr:
Phone:70H- 87 S- 3Y3 T Fax es (No):70sl- 6'7 f- rL55 purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DoD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ P e h Work Must Be SC OTHER N/A
Site Location Name: Foe,e r-`ti CRE ek n Samples received after 14:00 will be processed next business day.
Site Location Physical Address' 6 4 3 BE Q j F re, N. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES_ NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIMES
ANALYSIS REQUESTED
% ,� / '
REMARKS
�Q' i / �,tr� J ` �
`
fI fJ /
PRISM
LAB
ID NO.
*TYPE
SEE BELOW
I NO.
SIZE
S4A -�
M% as a 03
I®Z.. 7 FED
d )
A s
I
0 Z.
63
03
i
J
I
Sampler's Signature l.!/�
Sampled By (Print Name)�/�aC f+'
l Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be rkarges for any changes after analyses have been initialized.
R'li�ished By: (Sl lure) ) Recely e :i(slgnn � Mil rylHours Additional Comments:
o C//
Site Arrival Time:
Site Departure Time:
Rali � s y_ )
Rbadived By: (Signature)
I
Date
Field Tech Fee:
Reli(tLpWhed By: (,signature)-�i
Receitired Far Priam L o�t�R ,s sy�
Date
) - ] 1" �
1 q 3S
Mileage:
Method olShlpment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH. CUSTODY SEALS FFOR TRANSPORTATION-YO THE LABORATORY.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVE D �T THE LABORATORY.
❑ Fed Ex ❑ UPS O Hand -delivered Wism Field Service ❑`Olhaf
CCC Group No.
(/ 0 o
xU
DRINKING
SOLID
LANDFILL❑
❑ NC ❑ S( �,U
❑ SC
I o C 0 SCTER:
NC❑ SCATER.
I
❑❑ NC ❑ SCE
I
❑❑ N(
:I
O NC ❑ SC
I El NC SC
El NC ❑ SIC
❑
U
Ll

NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11/2019
RismEnvironmental Solutions SC Certification No. 99012
Z/===R
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl)
Ken Galloway
P.O. Box 1111 Lab Submittal Date: 10/22/2018
Statesville, NC 28687 Prism Work Order: 8100388
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised laboratory report datedl/29/19. The SAR comment has been
added below.
Analysis note for SAR:
SAR =[Na]/SQRT{([Ca]+[Mg])/2}
.R=[120/23.0]/SQRT{([1200/20.0]+[0/12.2])/2}
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 18

Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
BHL MB greater than one half of the RL, but sample concentrations are either less than the RL or greater than 1 Ox the
MB.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
D Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18

J� I S Full -Service Analytical &
environmental Solutions
' L_ABORATORIES, INC.
Sample Receipt Summary
02/11/2019
Prism Work Order: 8100388
r'i-it Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
-ime (and Fecal 1)
8100388-01
Solid
10/22/18 11:25 10/22/18 12:30
Fecal #2
8100388-02
Solid
10/22/18 11:25 10/22/18 12:30
Fecal #3
8100388-03
Solid
10/22/18 11:25 10/22/18 12:30
Fecal #4
8100388-04
Solid
10/22/18 11:25 10/22/18 12:30
Fecal #5
8100388-05
Solid
10/22/18 11:25 10/22/18 12:30
Fecal #6
8100388-06
Solid
10/22/18 11:25 10/22/18 12:30
Fecal #7
8100388-07
Solid
10/22/18 11:25 10/22/18 12:30
Samples were received in good condition at 1.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 3 of 18

Laboratory Report
� _ R I S Environmental
Analytical 8
` Environmental Solutions 02/11/2019
^1 LABORATORIES.ING
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Client Sample ID: StaLime (and Fecal 1)
,i: Ken Galloway Prism Sample ID: 8100388-01
r-.J. Box 1111 Prism Work Order: 8100388
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
PlantAvailable Nitrogen
BRL
mg/kg dry
1100
330
5
*Calculation
10/29/18 9:15
CLB
[CALC]
Solids
66.6
% by
0.100
0.100
1
*SM2540 G
10/25/18 14:00
TJY
P8J0554
Weight
Ammonia as N
380
mg/kg dry
15
3.7
1
*SM4500-NH3 C
10/25/18 15:32
BMS
P8J0519
Nitrate/Nitrite as N
25
mg/kg dry
7.5
2.1
1
*SM4500-NO3 F
10/29/18 9:15
CLB
P8J0524
Phosphorus -Total
3200
mg/kg dry
75
17
20
*SM4500-P F
10/26/18 8:39
CLB
P8J0495
Total Kjeldahl Nitrogen
BRL
mg/kg dry
3800
1100
5
*351.2
10/24/18 8:08
CLB
P8J0419
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
10/22/18 13:25
BMS
P8J0422
Total Metals
Mercury
0.11
mg/kg dry
0.030
0.0028
1
*7471B
10/24/18 15:25
MMR
P8J0448
SAR Soil Preparation
Complete
g
1
*2-78-054
10/25/18 14:15
MMR
P8J0504
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
10/26/18 14:30
MMR
P8J0542
Weight
Arsenic
BRL
mg/kg dry
7.5
0.46
10
*6010D
10/29/18 22:52
JAB
P8J0453
" um Absorption Ratio
1.0
[blank]
0.80
0.016
1
*2-78-054
10/29/18 23:08
JAB
P8J0498
nium
BRL
mg/kg dry
3.7
0.10
10
*6010D
10/29/18 22:52
JAB
P8J0453
Calcium, SAR
1200 B
mg/L
1.0
0.10
10
*6010D
10/29/18 23:08
JAB
P8J0498
Copper
42
mg/kg dry
7.5
0.68
10
*6010D
10/29/18 22:52
JAB
P8J0453
Lead
BRL
mg/kg dry
3.7
0.69
10
*6010D
10/29/18 23:08
JAB
P8J0453
Magnesium, SAR
BRL
mg/L
1.0
0.086
10
*6010D
10/29/18 23:08
JAB
P8J0498
Nickel
11
mg/kg dry
7.5
0.27
10
*6010D
10/29/18 22:52
JAB
P8J0453
Potassium
2100
mg/kg dry
190
6.7
10
*6010D
10/29/18 22:52
JAB
P8J0453
Selenium
BRL
mg/kg dry
7.5
1.8
10
*6010D
10/29/18 22:52
JAB
P8J0453
Sodium
4500
mg/kg dry
220
7.3
10
*6010D
10/29/18 23:08
JAB
P8J0453
Sodium, SAR
120 B
mg/L
5.0
0.18
10
*6010D
10/29/18 23:08
JAB
P8J0498
Zinc
79
mg/kg dry
37
1.3
10
*6010D
10/29/18 22:52
JAB
P8J0453
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 18

Ab
Laboratory Report
P R IS� %jFull-Service Analytical 02/11/2019
' V' Evironmental Solutionss"- I.......ORIES ING
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Client Sample ID: Fecal #2
n: Ken Galloway Prism Sample ID: 8100388-02
_ -). Box 1111 Prism Work Order: 8100388
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 70.8 % by 0.100 0.100 1 'SM2540 G 10/25/18 14:00 TJY P8J0554
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3 1 'SM9221 E 10/22/18 13:25 BMS P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 18

Laboratory Report
Full-Service Anal tical&02/11/2019
RISMI Environmental Slutions
/'�'�Z—K
L BORATORIE$ ING
City of Statesville, NC
Project: Stal-ime Orly, & BiWeeklyl)
Client Sample ID: Fecal #3
Ken Galloway
Prism Sample ID: 8100388-03
Box 1111
Prism Work Order: 8100388
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 70.3
% by
0.100 0.100
1 "SM2540 G 10/25/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 18

�, R I V Full -Service Analytical &
Environmental Solutions
�:V ABORA CRIES, INC.
Laboratory Report
02/11 /2019
City of Statesville, NC
Project: StaLime (Qtrly, & BiWeeklyl)
Client Sample ID: Fecal #4
tn: Ken Galloway
Prism Sample ID: 8100388-04
D. Box 1111
Prism Work Order: 8100388
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
73.0 % by
0.100 0.100
1 *SM2540 G 10/26/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 *SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 18

I Full -Service Analytical &
JP R Environmental Solutions
LABORATORIES INC.
Laboratory Report
02/11/2019
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl)
Client Sample ID: Fecal #5
Ken Galloway
Prism Sample ID: 8100388-05
_ _ Box 1111
Prism Work Order: 8100388
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 70.3 % by 0.100 0.100 1 *SM2540 G 10/26118 14:00 TJY P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 *SM9221 E 10/22/18 13:25 BMS P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 18

fl r]I I S � %� Full -Service Analytical
� V � Environmental Solutions
'✓ LABORATORIES, ING
Laboratory Report
02/11 /2019
City of Statesville, NC
Ken Galloway
--Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Client Sample ID: Fecal #6
Prism Sample ID: 8100388-06
Prism Work Order: 8100388
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 72.3
% by
0.100
0.100 1
*SM2540 G 10/25/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 18

Full -Service Analytical &
o_j'R I S Environmental Solutions
, '�VIBOHATOFIE$ INC
Laboratory Report
02/11/2019
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl)
Client Sample ID: Fecal #7
In: Ken Galloway
Prism Sample ID: 8100388-07
D. Box 1111
Prism Work Order: 8100388
Statesville, NC 28687 Sample Matrix: Solid
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date[Time ID
General Chemistry Parameters
% Solids 68.9 % by, 0.100 0.100 1 *SM2540 G 10/25/18 14:00 TJY P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 *SM9221 E 10/22/18 13:25 BMS P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 18

1P'1�
I `-Full-Service Analytical &
Rn'Environmental Solutions
_] JLASON TONIES, INC.
Level 11 QC Report
2/11 /19
City of Statesville, NC
is Ken Galloway
1. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8J0448 - 7471 B
Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8J0448-BLK1) Prepared &Analyzed: 10/24/18
Mercury BRL 0.020 mg/kg wet
LCS (P8J0448-BS1) Prepared &Analyzed: 10/24/18
Mercury 0.417 0.020 mg/kg wet 0.4167 100 80-120
Batch P8J0453 - 3050B
Blank(P8J0453-BLK1)
Prepared: 10/24/18 Analyzed: 10/26/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
3 (P8J0453-BSI)
Prepared: 10/24/18 Analyzed: 10/26/18
'Dnic
11.7
0.50
mg/kg wet
12.50 93 80-120
Cadmium
12.3
0.25
mg/kg wet
12.50 99 80-120
Copper
12.5
0.50
mg/kg wet
12.50 100 80-120
Lead
12.4
0.25
mg/kg wet
12.50 99 80-120
Nickel
12.3
0.50
mg/kg wet
12.50 98 80-120
Potassium
1290
12
mg/kg wet
1250 103 80-120
Selenium
11.1
0.50
mg/kg wet
12.50 89 80-120
Sodium
1310
15
mg/kg wet
1250 105 80-120
Zinc
11.7
2.5
mg/kg wet
12.50 94 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 18

j
Level II QC Report
P+ Full -Service Analytical &
A
2/11/19
Environmental Solutions
-�'�'v�LABORATOFIES, ING
City of Statesville, NC
Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 8100388
Ken Galloway
Time Submitted: 10/22/2018
12:30:00PM
Sox 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result Limit Units
Level Result %REC Limits RPD
Limit Notes
Batch P8J0498 - 3010A
Blank (P8J0498-BLK1)
Prepared: 10/25/18 Analyzed: 10/29/18
Calcium, SAR
0.605 0.10 mg/L
BH
Magnesium, SAR
BRL 0.10 mg/L
BHL
Sodium, SAR
5.05 0.50 mg/L
BH
Batch P8J0504 - SAR 2-78-054
Blank (P8J0504-BLK1)
Prepared: 10/24/18 Analyzed: 10/25/18
SAR Soil Preparation
Complete g
Batch P8J0542 - NO PREP
Duplicate (P8J0542-DUP1)
Source: 8100388-01
Prepared &Analyzed: 10/26/18
SAR Percent Moisture
Complete 0.100 % by Weight Complete 0.6
200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 12 of 18

o110)R9SMEnviService Analytical &
Environmental Solutions
���+'v' 00R TOHIES, INC.
City of Statesville, NC
is Ken Galloway
). Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8J0419 - 351.2
Project: StaLime (Qtrly, & BiWeeklyl)
Level II QC Report
2/11 /19
Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8J0419-BLK1) Prepared: 10/23/18 Analyzed: 10/24/18
Total Kjeldahl Nitrogen BRL 50 mg/kg wet
LCS (P8J0419-BS1) Prepared: 10/23/18 Analyzed: 10/24/18
Total Kjeldahl Nitrogen 124 50 mg/kg wet 125.0 99 90-110
Batch P8J0495 - SM4500-PB5
Blank (P8J0495-BLK1)
Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total
LCS (P8J0495-BS1)
BRL 2.5
mg/kg wet
Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total
Matrix Spike (P8J0495-MS1)
106 2.5 mg/kg wet
Source: 8100388-01
100.0 106 90-110
Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total
Matrix Spike Dup (P8J0495-MSD1)
3370 75 mg/kg dry
Source: 8100388-01
150.2 3230 88 80-120
Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total
Batch P8J0519 - SM4500-NH3 B
3460 75
mg/kg dry
150.2 3230 154 80-120 3 20 MC
,nk (P8J0519-BLK1)
Prepared &Analyzed: 10/25/18
Ammonia as N
LCS (P8J0519-BS1)
BRL 10
mg/kg wet
Prepared &Analyzed: 10/25/18
Ammonia as N
515 10
mg/kg wet
500.0 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 13 of 18

n
J I S Full Service Analytical &
Environmental Solutions
� -2r LABORATORIES. ING
Level II QC Report
2/11/19
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl)
is Ken Galloway
. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8JO519 - SM4500-NH3 B
Matrix Spike (P8J0519-MS1) Source: 8100388-01 Prepared & Analyzed: 10/25/18
Ammonia as N 1100 15 mg/kg dry 750.9 383 95 80-120
Batch P8JO524 - NO PREP
Blank (P8J0524-BLK1) Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (PBJ0524-BS1) Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N 48.7 5.0 mg/kg wet 50.00 97 80-120
Matrix Spike (P8J0524-MS1) Source: 8100388-01 Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N 96.3 7.5 mg/kg dry 75.09 24.6 95 80-120
Matrix Spike Dup (P8J0524-MSD1) Source: 8100388-01 Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N 97.3 7.5 mg/kg dry 75.09 24.6 97 80-120 1 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 18

Full -Service Analytical &
R i S Environmental Solutions
L�^�BORATOFIES. LNG
City of Statesville, NC
Ken Galloway
3ox 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime (Qtrly, & BiWeeklyl)
Level II QC Report
2/11 /19
Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8J0422 - NO PREP
Blank (P8J0422-BLK1) Prepared &Analyzed: 10/22/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 18

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
)388-01
P8J0419
0.05 g
25 mL
10/23/18 11:25
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0519
1.01 g
50 mL
10/25/18 8:55
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0495
1 g
50 mL
10/25/18 10:30
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0554
30 g
30 g
10/25/18 14:00
8100388-02
P8J0554
30 g
30 g
10/25/18 14:00
8100388-03
P8J0554
30 g
30 g
10/25/18 14:00
8100388-04
P8J0554
30 g
30 g
10/25/18 14:00
8100388-05
P8J0554
30 g
30 g
10/25/18 14:00
8100388-06
P8J0554
30 g
30 g
10/25/18 14:00
8100388-07
P8J0554
30 g
30 g
10/25/18 14:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0498
50 mL
50 mL
10/25/18 14:10
A+n0388-01
P8J0498
50 mL
50 mL
10/25/18 14:10
.._p Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0453
2.01 g
50 mL
10/24/18 8:50
8100388-01
P8J0453
2.01 g
50 mL
10/24/18 8:50
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0448
0.61 g
50 mL
10/24/18 10:05
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0504
250 g
250 g
10/24/18 14:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 16 of 18

r'
r
LABORATORIES, [NC
CHAIN OF CIJF"'r0®Y RECORD
Full -Service Analytical &
Environmental Solutions PAGE_ OF _ QUOTE # TO ENSI TOPER BILLING:
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax: [phone]
Client Company Name: C•-Q-v a+ SSA -AUy.11E
Report To/Contact Name: Kc j r"I 11 w av
Reporting Address:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
NO NIA
Samples INTACT upon arrival?
Received ON WET ICE?�
PROPER PRESERVATIVES indicated?_
Received WITHIN HOLDING TIMES.,
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPAC
PROPER CONTAINERS used? F
TEMP_ Therm II]' � Qbserved:�°C /,CerrL�-C
Phone: 70Y- 875- 3" a Fax es (No): 9'0Y- lt79'• 8L55 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD
FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rushh Work Mdust BePre-Approve
Site Location Name: Fou r i P C iR e fFk Samples received after 14:00 will be processed next business day.
SC OTHER
NIA
Site Location Physical Address: 993 6-11 FA.?,,, 'R i . Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO —
(SEETERMS & CONDITIONS NNnSERVICES
ED BY ISM LABORATORIES, INC. TO CLIENT)
R RENDERED PRISM
Sample Iced Upon Collection: YES
NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
LITA
MATRIX
(SOIL,
WATER OR
SAMPLE CONTAINER
PRESERVA-
TIMES
ANALYSIS REQUESTED
/ f `�j / %f / REMARKS
f
PRISM
LAB
*TYPE
{
HI
OURS
SLUDGE)
NO.
f SIZE
�{�� �jt! /J
ID NO.
SEE ELOW
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Sampler's Signature o_tt _ Sampled By (Print Name) y /• Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceediwith the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charge a y'cha ges after analyses have been initialized.
Relinl&hed By (Slgnntum) Recciva By; (S° ature} Date - Mlltery7Ftours Additional Comments:
Site Arrival Time:
O �
L L �lS
Rel' ished By: (Signature) R etvedBy: (Signetu D e
Site Departure Time:
qui-,had'8y; (Sig ure) RBc lved FnrPfiSm 6a crier B : 1 Date
/DIiZ/ la % 7-J l�
Field Tech Fee:
I
Mileage:
(0 d of Sh - ent: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR WNSPORTATION TO rHE LABORATORY. COC Group No.
AND CDC UNTIL RECEIVED AT THE LABORATORY.
J y Opp �J
F Field ServiceRIFIE❑DOARECEIVEDAINST
d Ex ❑•LIPS ❑ Hand-delered P smPTED
)ES: UST: GFWLINDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
0- C❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC I ❑NC ❑SC ❑NC❑SC ❑NC ❑SCI❑NC ❑SCI ❑NC ❑SC
❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑
NTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic: TL = Teflon -Lined Can VOA = Volatile Organics Analvsis (Zero Head Space)

Main Office:
449 Springbrook Road
f Full Service Analytical and P.O. Box 240543
PH
I Environmental Solutions Charlotte, NC 28224-0543
INN- Phone: [phone]
1/800/529-6364
Fax: [phone]
www.prismiabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Numberl 8100388-01 1 SampleNamel StaLime Fecal 1
Na: Sodium (mg/L) Equivalent weight: 23
Ca: Calcium (mg/L) Equivalent weight: 20
Mg: Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Na nl9/L). Cam /L M (m /L
120.0 1190.0 -0.2
Na PAE
Ca PJEJ
Nlg WE)
5.22
1 50.50
1 -0.01
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 1.0 (From mg/L entered above)
Calculated By: 1�00 ' - r �/; �.• , , z� _ - _
Page 18 of 18

r- NC Certification No.402 Case Narrative
P1 Full -Service Analytical & NC Drinking Water Cert No. 37735 11 /02/2018
I S 1 V 1 Environmental Solutions SC Certification No. 99012
LAB WORIES, INC.
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP Short List
Ken Galloway
P.O. Box 1111 Lab Submittal Date: 10/17/2018
Statesville, NC 28687 Prism Work Order: 8100342
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
TCLP Herbicide analysis was subcontracted to GCAL. Laboratory report is attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
n LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
--- Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 21

.� �p p
�I R I `- SnviService Analytical s
--� —' J Environmental Solutions
e=-=a'ZL ORATORIES. [No
Sample Receipt Summary
11 /02/2018
Prism Work Order: 8100342
Cl---* Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
)ek Sludge
8100342-01
Solid
10/17/18 8:45
10/17/18 16:15
3rd Creek Sludge
8100342-02
Solid
10/17/18 9:00
10/17/18 16:15
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 21

)..
Laboratory Report
Full -Service &
al Solutions
' V' Environmental SoWtions
J j Ism
11/02/2018
BORATOFIES, INC.
C'ih, nf Statesville, NC
Project: 3rd and 4th Creek Sludge
Client Sample ID: 4th Creek Sludge
en Galloway
TCLP Short List
Prism Sample ID: 8100342-01
F._. __)x 1111
Prism Work Order: 8100342
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/17/18 08:45
Time Submitted: 10/17/18 16:15
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateMme ID
TCLP Extraction by EPA 1311
TCLP Extraction Complete
N/A
1 *1311 10/23/18 8:40 MMR P8J0412
TCLP Organochlorine Pesticides by GC/ECD
gamma-BHC BRL
mg/L
0.00050 0.000065
1 *8081B 10/26/18 19:00 ZRC P8J0478
Surrogate
Recovery Control Limits
Decachlorobiphenyl
113 % 13-186
Tetrachloro-m-xylene
77 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2-Methylphenol BRL
mg/L
0.050 0.0018
1 *8270D 10/25/18 17:24 JMV P8J0443
3/4-Methyl phenol BRL
mg/L
0.050 0.0015
1 *8270D 10/25/18 17:24 JMV P8J0443
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
95 % 43-140
2-Fluorobiphenyl
88 % 44-119
2-Fluorophenol
55 % 19-119
Nitrobenzene-d5
84 % 44-120
Phenol-d5
37 % 11-52
Terphenyl-d14
91 % 50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 3 of 21

_en R ISM Full -Service Analytical
��I' Environmental Solutions
� LABORATORIES. ING
Laboratory Report
11 /02/2018
City of Statesville, NC
/ en Galloway
F )x 1111
Statesville, NC 28687
Project: 3rd and 4th Creek Sludge
TCLP Short List
Sample Matrix: Solid
Client Sample ID: 3rd Creek Sludge
Prism Sample ID: 8100342-02
Prism Work Order: 8100342
Time Collected: 10/17/18 09:00
Time Submitted: 10/17/18 16:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
TCLP Extraction by EPA 1311
TCLP Extraction Complete N/A 1 *1311 10/23/18 8:40 MMR P8J0412
TCLP Organochlorine Pesticides by GC/ECD
gamma-BHC BRL mg/L 0.00050 0.000065 1 *8081 B 10/26/18 19:12 ZRC P8J0478
Surrogate
Recovery Control Limits
Decachlorobiphenyl 124 % 13-186
Tetrachloro-m-xylene 88 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2-Methylphenol BRL mg/L 0.050 0.0018 1 *8270D 10/25/18 17:47 JMV P8J0443
314-Methyl phenol BRL mg/L 0.050 0.0015 1 *8270D 10/25/18 17:47 JMV P8J0443
Surrogate Recovery Control Limits
2,4,6-Tribromophenol
85 %
43-140
2-Fluorobiphenyl
85 %
44-119
2-Fluorophenol
56 %
19-119
Nitrobenzene-d5
81 %
44-120
Phenol-d5
37 %
11-52
Terphenyl-d14
85 %
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 21

Level II QC Report
/7-�-RISM Full -Service Analytical 11/2l18
Environmental Solutionss:=-LABORATORIES. 1 NG
City of Statesville, NC
Al n Galloway
P. ( 1111
Statesville, NC 28687
Project: 3rd and 4th Creek Sludge TCLP
Short List
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P8J0443 - 3510C MS
Prism Work Order: 8100342
Time Submitted: 10/17/2018 4:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (PBJ0443-BLK1)
Prepared: 10/24/18 Analyzed: 10/25/18
2,4,5-Trichlorophenol
BRL
0.25
mg/L
2,4,6-Trichlorophenol
BRL
0.10
mg/L
2,4-Dinitrotoluene
BRL
0.012
mg/L
2-Methylphenol
BRL
0.050
mg/L
3/4-Methylphenol
BRL
0.050
mg/L
Hexachlorobenzene
BRL
0.010
mg/L
Hexachlorobutadiene
BRL
0.050
mg/L
Hexachloroethane
BRL
0.050
mg/L
Nitrobenzene
BRL
0.050
mg/L
Pentachlorophenol
BRL
0.25
mg/L
Pyridine
BRL
0.25
mg/L
Surrogate: 2,4,6-Tribromophenol
0.0804
mg/L
0.1000
80
43-140
Surrogate:2-Fluorobiphenyl
0.0420
mg/L
0.05000
84
44-119
Surrogate:2-Fluorophenol
0.0549
mg/L
0.1000
55
19-119
Surrogate: Nitrobenzene-d5
0.0405
mg/L
0.05000
81
44-120
Surrogate: Phenol-d5
0.0366
mg/L
0.1000
37
11-52
`e: Terphenyl-d14
0.0448
mg/L
0.05000
90
50-134
L 13J0443-BS1)
Prepared: 10/24/18 Analyzed: 10/25/18
2,4,5-Trichlorophenol
0.0435
0.25
mg/L
0.05000
87
53-123
2,4,6-Trichlorophenol
0.0426
0.10
mg/L
0.05000
85
50-125
2,4-Dinitrotoluene
0.0451
0.012
mg/L
0.05000
90
57-128
2-Methylphenol
0.0368
0.050
mg/L
0.05000
74
30-117
3/4-Methyl phenol
0.0304
0.050
mg/L
0.05000
61
29-110
Hexachlorobenzene
0.0422
0.010
mg/L
0.05000
84
53-125
Hexachlorobutadiene
0.0283
0.050
mg/L
0.05000
57
22-124
Hexachloroethane
0.0268
0.050
mg/L
0.05000
54
21-115
Nitrobenzene
0.0375
0.050
mg/L
0.05000
75
45-121
Pentachlorophenol
0.0386
0.25
mg/L
0.05000
77
35-138
Pyridine
0.0219
0.25
mg/L
0.05000
44
10-53
Surrogate: 2,4,6-Tribromophenol
0.0841
mg/L
0.1000
84
43-140
Surrogate:2-Fluorobiphenyl
0.0403
mg/L
0.05000
61
44-119
Surrogate:2-Fluorophenol
0.0515
mg/L
0.1000
51
19-119
Surrogate: Nitrobenzene-d5
0.0350
mg/L
0.05000
70
44-120
Surrogate: Phenol-d5
0.0348
mg/L
0.1000
35
11-52
Surrogate: Terphenyl-d14
0.0433
mg/L
0.05000
87
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 21

Full-
�1 _'_l I `- Environmental
Analytical &
r J Environmental Solutions
`� (L480 RATORIE� ING
Level II QC Report
11/2/18
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP Prism Work Order: 8100342
A n Galloway Short List Time Submitted: 10/17/2018 4:15:OOPM
P. K 1111
Statesville, NC 28687
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8J0443 - 3510C MS
LCS Dup (P8J0443-BSD1)
Prepared: 10/24/18 Analyzed: 10/25/18
2,4,5-Trichlorophenol
0.0435
0.25
mg/L
0.05000
87
53-123
0.02
20
2,4,6-Trichlorophenol
0.0445
0.10
mg/L
0.05000
89
50-125
4
20
2,4-Dinitrotoluene
0.0456
0.012
mg/L
0.05000
91
57-128
1
20
2-Methylphenol
0.0389
0.050
mg/L
0.05000
78
30-117
6
20
3/4-Methylphenol
0.0328
0.050
mg/L
0.05000
66
29-110
7
20
Hexachlorobenzene
0.0428
0.010
mg/L
0.05000
86
53-125
1
20
Hexachlorobutadiene
0.0306
0.050
mg/L
0.05000
61
22-124
8
20
Hexachloroethane
0.0299
0.050
mg/L
0.05000
60
21-115
11
20
Nitrobenzene
0.0386
0.050
mg/L
0.05000
77
45-121
3
20
Pentachlorophenol
0.0425
0.25
mg/L
0.05000
85
35-138
10
20
Pyridine
0.0224
0.25
mg/L
0.05000
45
10-53
2
20
Surrogate: 2,4,6-Tribromophenol
0.0869
mg/L
0.1000
87
43-140
Surrogate:2-Fluorobiphenyl
0.0427
mg/L
0.05000
85
44-119
Surrogate:2-Fluorophenol
0.0564
mg/L
0.1000
56
19-119
Surrogate: Nitrobenzene-d5
0.0368
mg/L
0.05000
74
44-120
Surrogate: Phenol-d5
0.0358
mg/L
0.1000
36
11-52
'e: Terphenyl-d14
0.0431
mg/L
0.05000
86
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 21

0��,i
RiS Full -Service Analytical &
I Environmental Solutions
1 A50R TORIES, INC.
Level II QC Report
11/2/18
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP Prism Work Order: 8100342
Ai. n Galloway Short List Time Submitted: 10/17/2018 4:15:00PM
P. c 1111
Statesville, NC 28687
TCLP Organochlorine Pesticides by GC/ECD - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8J0478 - 3510C GC
Blank (P8J0478-BLK1)
Prepared: 10/25/18 Analyzed: 10/26/18
Chlordane
BRL
0.0025
mg/L
Dieldrin
BRL
0.00050
mg/L
Endrin
BRL
0.00050
mg/L
gamma-BHC
BRL
0.00050
mg/L
Heptachlor
BRL
0.00050
mg/L
Heptachlor Epoxide
BRL
0.00050
mg/L
Methoxychlor
BRL
0.00050
mg/L
Toxaphene
BRL
0.025
mg/L
Surrogate: Decachlorobiphenyl
0.00127
mg/L
0.001000
127
13-186
Surrogate: Tetrachloro-m-xylene
0.000837
mg/L
0.001000
84
40-134
LCS (P8J0478-BS1)
Prepared: 10/25/18 Analyzed: 10/26/18
Dieldrin
0.000828
0.00050
mg/L
0.001000
83
69-130
Endrin
0.000892
0.00050
mg/L
0.001000
89
69-144
gamma-BHC
0.000895
0.00050
mg/L
0.001000
89
66-129
Heptachlor
0.000863
0.00050
mg/L
0.001000
86
61-136
I-lantnrhlor Epoxide
0.000836
0.00050
mg/L
0.001000
84
69-131
P chlor
0.000865
0.00050
mg/L
0.001000
87
70-157
_ `e: Decachlorobiphenyl
0.00121
mg/L
0.001000
121
13-186
Surrogate: Tetrachloro-m-xylene
0.000801
mg/L
0.001000
80
40-134
LCS (P8J0478-BS2)
Prepared: 10/25/18 Analyzed: 10/26/18
Chlordane
0.00717
0,0025
mg/L
0.01000
72
50-150
Surrogate: Decachlorobiphenyl
0.000672
mg/L
0.001000
67
13-186
Surrogate: Tetrachloro-m-xylene
0.000728
mg/L
0.001000
73
40-134
LCS (P8J0478-BS3)
Prepared: 10/25/18 Analyzed: 10/26/18
Toxaphene
0.0106
0.025
mg/L
0.01000
106
50-150
Surrogate: Decachlorobiphenyl
0.000797
mg/L
0.001000
80
13-186
Surrogate: Tetrachloro-m-xylene
0.000854
mg/L
0.001000
85
40-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 21

�'' C'pa //�Y
JP�F I �/' Full -Service Analytical s
Environmental Solutions
LABORATORIES. JNQ.
Level II QC Report
11 /2/18
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP
At n Galloway Short List
P., c 1111
Statesville, NC 28687
TCLP Organochlorine Pesticides by GC/ECD - Quality Control
Reporting
Analyte Result Limit Units
Batch P8J0478 - 3510C GC
Prism Work Order: 8100342
Time Submitted: 10/17/2018 4:15:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P8J0478-BSD1)
Prepared: 10/25/18 Analyzed: 10/26/18
Dieldrin
0.000864
0.00050
mg/L
0.001000
86
69-130
4
20
Endrin
0.000940
0.00050
mg/L
0.001000
94
69-144
5
20
gamma-BHC
0.000928
0.00050
mg/L
0.001000
93
66-129
4
20
Heptachlor
0.000899
0.00050
mg/L
0.001000
90
61-136
4
20
Heptachlor Epoxide
0.000862
0.00050
mg/L
0.001000
86
69-131
3
20
Methoxychlor
0.000959
0.00050
mg/L
0.001000
96
70-157
10
20
Surrogate: Decachlorobiphenyl
0.000937
mg/L
0.001000
94
13-186
Surrogate: Tetrachloro-m-xylene
0.000838
mg/L
0.001000
84
40-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 8 of 21

Level II QC Report
I S
Full -Service Analytical
11/2/18
JI��
Environmental Solutions
All�
AV' I ASORATORIES, INC.
City of Statesville, NC
Project: 3rd and 4th Creek Sludge TCLP Prism Work Order: 8100342
Al n Galloway
Short List
Time Submitted: 10/17/2018 4:15:00PM
P. K 1111
Statesville, NC 28687
TCLP Extraction by EPA
1311 - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result
Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8J0412 -1311
Blank (P8J0412-BLK1)
Prepared: 10/22/18 Analyzed: 10/23/18
TCLP Extraction
Complete
N/A
Sample Extraction Data
Prep Method: 1311
Lab Number
Batch Initial
Final Date/Time
8100342-01
P8J0412 100 g
2000 mL 10/22/18 15:50
8100342-02
P8J0412 100 g
2000 mL 10/22/18 15:50
Prep Method: 3510C GC
Lab Number
Batch Initial
Final Date/Time
8100342-01
P8J0478 200 mL
10 mL 10/25/18 9:00
8100342-02
P8J0478 200 mL
10 mL 10/25/18 12:45
F thod: 3510C MS
Lau niulnber
Batch Initial
Final Date/Time
8100342-01
P8J0443 200 mL
1 mL 10/24/18 9:10
8100342-02
P8J0443 200 mL
1 mL 10/24/18 9:10
Subcontracted Analyses
The following analyses
were subcontracted to Gulf Coast
Analytical Labs, Inc.
Lab Number
Analysis
8100342-01
Herbicides TCLP (Sub)
8100342-02
Herbicides TCLP (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 21

if CHAIN OF CUSTODY OD RECORD
/r Full -Service Analytical &
M + Environmental Solutions PAGE-_ of _ QUOTE # TO EN ROPER BILLING:
LABORATORIES, INC.
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax: [phone]
Client Company Name: _
Report To/Contact Name:
Reporting Address:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID: LILT_ y Observed:
NO NIA
r
-L
i
ram'
°C / Corr:°
Phone: Fax (Yes) (No):
Email Address:
EDD Type: PDF Excel Other
Site Location Name:Samples
Purchase Order No./Billing Reference
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Pre-ApprovedhWoust Be M
received after 14,00 will be processed next business day.
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC DOD FL NC
SC OTHER NIA
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Water Chlorinated: YES_ NO_
Sample Iced Upon Collection: YES NO_
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIMES
ANALYSIS REQUESTED
L
~S M 1 REMARKS
{f t` / " 5°
f,r v� /� Get+/ �/
/
PRISM
LAB
ID NO.
•TYpE
SEE BELOW
NO.
SIZE
VA Ca,-Ek Slm)g c
W-/7-le
0 T: qs
S
G
MOVE
f
J
Tc i P r«
61
I
3JCarJ S!u
Q0E
✓
J
67,-
I
I
I
Sampler's SignatureZM_! L'Jtrr�✓.c
Sampled B Print Name � ,, !!
p y ) q( LJ vr, cI Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any, changes must be
in writing to the Prism Project Manager, There will be charge"o any changes after analyses have been initialized.IdRelin
/lsubmitted
(shed ey; (Sigmiture)
He9eived 8y: (5i nature) Date, ildaryHours Additional Comments: 7Arrival
R_^II shr:d 0y:,(Signaturel
Raoaivad.Py: (SiflRature) Date
i
lulshcd i (� ure)-Received For Priem Labomtones !. Da[e% � Field Tech Fee:
Sv `//i`�'�J �/ tt �/ - Mileage:
CQ d of ShiFina �OTE: ALL,S MPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANS oRTATION TO -THE LABO ORY. COG Group No,
(D SA 3akES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LAB RATORY, Ul
C) I E3,_,Q.0P d-dnllvorod VF5,sm Field Service ❑ Othar0 ed
ES: UST GO NDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
1 C❑SC El NC El SIC ONC ❑SC ANC El 0❑NC ❑SC ❑❑NC❑SC ❑❑NC ❑SC ❑SC ❑SC
°
'
NTAINER TYPE CODES: A = AmhPr (= Char
ONC
LlNC
r,= Alags P = Plagti,- TI v Thfi -I i—i cam., vnA = v I�ril- nr ­ ;: A. I. i� 17— ue-a 0--- e1

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
RobbiJones
PROJECTID
8100342
LABORATORY REPORT NUMBER
218101921
DATE
10/31 /2018
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashlev B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 218101921 Pa e 1 of 11
Page 11 of 21

LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL LABORATORIES, LLC
ANALYTICAL RESULTS
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70820
Report Date 10/31/2018
GIIcai xenon ziaiopiI9ezi
Project 8100342
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
'All
,.
17025`` !
Feu
WD FLAP
Lab Report#:218101921 Page 2 o
Page 12 of 21

1% ILL Report#: 218101921
040 GC Project ID: 8100342 Report Date: 10/31/2018
.u:.�4'fqul Ln�9Rs.I:ONLRa. Ct,c.
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAUs Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed In the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
GCAL Report 218101921
Lab Report#: 218101921
Page 13 of 21

Report#: 218101921
Project ID: 8100342
Certifications
Report Date: 10/31/2018
Certification
Certification Number
DOD ELAP
L16-398-R5
Alabama
01955
Arkansas
18-062-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 218101921 Pa e 4 of
Page 14 of 21

i
Report#: 218101921
Projec -ID: 8100342--"— _ " Report Date: "10y3172018"
Case Narrative
Client: Access Analytical Report: 218101921
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
0
Lab Report#: 218101921
Page 15 of 21

C(3
Report#: 218101921
ANALI II:SI .APfJIf4rnHIEl.ILLC Project ID: 8100342 Report Date: 10/31/2018
Sample Summary
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
21810192101 4th Creek Sludge Solid 10/17/2018 08:45 10%1'9/2018 09:35
21810192102 3rd Creek Sludge Solid 10/17/2018 09:00 10/19/2018 09:35
Lab Report#: 218101921 Page 6 of 11
Page 16 of 21

�'ii4
Report#: 218101921Enip„_, �F�ur:,•,n��r� i Project ID: 8100342"- "" RepoitDate: 107317201S
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Lab Report#: 218101921
Page 17 of 21

,, Report#: 218101921
uic� nn:7mdes. l.�c Project ID: 8100342 Report Date: 10/31/2018
Sample Results
Collect Date
10/17/2018 08:45
GCAL ID
2181.0192101
4th Creek Sludge
Receive Date
10119/2018 09:35
- ,
Matrix
Solid ,
EPA 1311/8151A
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
10/24/2018 11:00 646481 EPA 1311/8151A 1 10/30/2018 16:55 MFS 646954
CAS#
Parameter
Result DL
LOQ
Reg Limit
Units
94-75-7
2,4'-D
0.001000 0.00100
0.00500
10
mg/L
93-72-1
2,4,5-TP (Silvex)
0.001000 0.00100
0.00500
1
mg/L
CAS#
Surrogate
Conc. Spiked Conc. Rec
Units
% Recovery
Rec Limits
19719-28-9
DCAA
0.02 .00737
mg/L
37
18 - 136
Collect Date
10/17/2018 09:00
GCAL ID
21810192102
3rd Creek Sludge
Receive Date
10/19/2018 09:35
Matrix
Solid
EPA 1311/8151A
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
10/24/2018 11:00 646481 EPA 1311/8151A 1 10/30/2018 17:35 MFS 646954
CAS#
Parameter
Result DL
LOQ
Reg Limit
Units
94-75-7
2,4'-D
0.001000 0.00100
0.00500
10
mg/L
93-72-1
2,4,5-TP (Silvex)
0.00100U 0.00100
0.00500
1
mg/L
CAS#
Surrogate
Conc. Spiked Conc. Rec
Units
% Recovery
Rec Limits
19719-28-9
DCAA
0.02 .0133
mg/L
67
18 -136
Lab Report#: 218101921 Page 8 of 11
Page 18 of 21

Report#:
P?o)eet ID:
GC Semi-Volatiles QC Summary
218101921
8100342
ReporfDate: 10/31/2018 -
Analytical Batch
Client ID'
MB646481 .
LCS64a,481
LCSt]645481-
646664.
GCALID
1861130
1861131''.;
1861.132:. .
Prop Batch .,-
Sample Type
MB
L`CS
LCSD
646,481
Przp D6(6-
10124/2018 11 00 '
10/24120"18, 1�1:00
i0/24/201811 00
.,
Prop Method
Analysls 64e
10126120/8 2'2:41,
10)25/20113 23 61'"
10/2612018 23:22
-Matrix
Water
EPA 131118161A
Units
Result
mg/L
DL
Spike
Added
Result
°
.Control.
Limits%R
. -Spike
� .Added
Result
%R
RPD
RPD
Limit
2,4'-D
94-75-7
0.001000
0.00100
0.00099
0.00075
75
45 - 152
0.00099
0.00079
80
5
30
2,4,5-TP (Stivex)
93-72-1
b40100U
0.00100
0.00100
0.00074
74
51 -134
0.00100
0.00076
75
1
30
Surrogate
DCAA
19719-28-9
.00112
56
.002
.00127
64
18 -136
.002
.0013
65
NA
NA
Lab Report#: 218101921 1320a 9 of 11
Page 19 of 21

T
!M 17VII-Service Analytical
Environmental Solutions
r, 4A
J,f)'r— r-2-cf SUBCONTRACT ORDER
Cellificilidw ftl.AC 1-j5ACE
34 Prism Lhboeatorles, Inc. NC
IlAr)-l"NI -5qQQ 8100342 W/A
SENDINC. URMNToRy.-
RECEIVING LABORATORY:
Prism Laboratories, Inc;
Gulf Coast Analytical'Labs, Ift.
R. O. Box 240543
10781 Coursey 9 Nd
Charlotte, NC 2.822410543
Baton Rouge, LA 70816
Phone: [phone]
Phone:[phone]
Fax, 704-525-0409
rax: (22-5) 767-5717
PrRjMMpnQw' .90WA7J' s
L9b, 7'�?ryiE�
Ann[ -Due ipy, )9.111110nts I I
--- -Ssm , ._ . . _ -(
08:45
14crb cl -(sub) e
'i-0 S2Adl--, 09
��-rqp'lelo '81004
2,4-*4 and 2,4,3 I*('
6
:}
flerbicidez'TC0 (sub)'
2.4-D nnd:2,4,5 T T4
L
.k
Ij
Rth:eivid 139
Lbic
ACidd ri�'V
MjU
R,cle.-Oid 11v
Dow.
ltcvcived ByDaly
(MIC
Receircti By'
Dntc
Page I (i
I
I Page 20 of 21 1

SAMPLE RECEIVING CHECKLIST tl12I1 8WI�NIIIV
SAMPLE DELIVERY, GROUR:218101921
t =
YES
NO
:CHC-C}dlSTm r
Client PM AM
Transport Method
Samples received with proper thermal preservation?
0
❑
4565 -Access Analytical
FEDDC
— — -- - -— —
RadioactiNity is <1600 cpm? If no, record cpm value in notes section.
❑v
❑
Profile Number
Feceived Dj
COC relinquished and complete (including sam lelDs, collect times, and sampler)?
q P ( 9 P�—❑
d
❑
80251
Savage, Tiffany R
—• —•-
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
I 0
v❑
❑
❑
Line Items)
Receive Date(s)
4 - Solid
10/19/18—
PreservatNe added to any containers?
I ❑
❑,r
If received, was headspace for VOC water containers < 6mm?
®
❑
Samples collected in containers prodded by GCAL?
i ❑FRI
COOLERS
DISCREPANCIES".'-) : `'=,"';-�'` ;:':,':' °' . ;
-LAB'PRESERVATIONS
Airbill Thermometer ID: E29
Temp °C
Wne
Wne
7735-1386-5980
1.5
NOTES
fevision 1.6
Page 1 of 1
Lab Report*: 218101921 Page 11 of 11

- NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 09/26/2018
PR Environmental Solutions SC Certification No. 99012
_, LABORATORIES, INC.
City of Statesville, NC Project: Sludge (Hazardous Testing)
Andy Smith Project No.: 3rd Creek/4th Creek/Stal-ime
P.O. Box 1111 Lab Submittal Date: 09/10/2018
Statesville, NC 28687 Prism Work Order: 8090113
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Reactivity and flashpoint analyses were subcontracted to Gulf Coast Analytical Labs. Laboratory report is
attached.
TCLP 8151 analyses were subcontracted to Analytical Environmental Services. Laboratory report is
attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash For Robbi A. Jones
VP Laboratory Services
A Pass
D RPD value outside of the control limits.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364-Fax:[phone] Page 1 of 30

rAPiJ 7 R I S tl 1 Full -Service Analytical
' 4 Environmental Solutions
- XLARORATORIEs INC.
0-11 4 Sample ID
ie
4th Creek
3rd Creek
Sample Receipt Summary
09/26/2018
Prism Work Order: 8090113
Lab Sample ID Matrix Date/Time Sampled Date/Time Received
8090113-01
Solid
09/10/18
8:20
09/10/18
13:15
8090113-02
Solid
09/10/18
8:03
09/10/18
13:15
8090113-03
Solid
09/10/18
8:15
09/10/18
13:15
Samples were received in good condition at 2.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 30

Full Service Analytical & Laboratory Report
A'"J*IUILABOFIATORIES
'/(I 09/26/2018
' b'Environmental Solutions
INr
Citv of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: StaLime
r ndy Smith Prism Sample ID: 8090113-01
1 ox 1111 Project No.: 3rd Creek/4th Creek/Stal-ime Prism Work Order: 8090113
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/10/18 08:20
Time Submitted: 09/10/18 13:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DatelTime
ID
General Chemistry Parameters
% Solids
95.3
% by
0.100
0.100
1
*SM2540 G
9/12118 15:40
SLS
P810152
Weight
Corrosivity-pH
13
pH Units
1
*9045D
9/14118 16:09
CBP
P810221
Ignitability
BRLA
mm/sec
0.10
1
*1030
9/20/18 13:14
BMS
P810286
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
9/13/18 7:20
MMR
P810153
TCLP Extraction
Complete
N/A
1
*1311 ZHE
9/21/18 15:10
KDM
P810314
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
*7470A
9/13/18 14:04
MMR
P810159
Arsenic
BRL
mg/L
0.10
0.016
1
*601OD
9113/18 17:53
JAB
P810157
Barium
BRL
mg/L
5.0
0.0040
1
*601OD
9/13/18 17:53
JAB
P810157
Cadmium
BRL
mg/L
0.025
0.00075
1
*6010D
9113/18 17:53
JAB
P810157
Chromium
BRL
mg/L
0.25
0.0018
1
*6010D
9/13/18 17:53
JAB
P810157
Lead
BRL
mg/L
0.050
0.0040
1
*6010D
9113/18 17:53
JAB
P810157
Selenium
BRL
mg/L
0.10
0.028
1
*6010D
9/13/18 17:53
JAB
P810157
BRL
mg/L
0.25
0.0020
1
*6010D
9l13/18 17:53
JAB
P810157
Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00086
1
*8081 B
9/20/18 17:08
JMC
P810235
Dieldrin
BRL
mg/L
0.00050
0.000070
1
*8081B
9/20/18 17:08
JMC
P810235
Endrin
BRL
mg/L
0.00050
0.000075
1
*8081B
9/20/18 17:08
JMC
P810235
gamma-BHC
BRL
mg/L
0.00050
0.000065
1
*8081B
9/20/18 17:08
JMC
P810235
Heptachlor
BRL
mg/L
0.00050
0.000085
1
*8081 B
9120/18 17:08
JMC
P810235
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000065
1
*8081 B
9/20/18 17:08
JMC
P810235
Methoxychlor
BRL
mg/L
0.00050
0.00020
1
*8081B
9120/18 17:08
JMC
P810235
Toxaphene
BRL
mg/L
0.025
0.00037
1
*8081B
9/20/18 17:08
JMC
P810235
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
81
%
13-186
Tetrachloro-m-xylene
59
%
40-134
TCLP Semivolatile Organic Compounds
by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
*8270D
9117/18 17:41
JMV
P810203
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
*8270D
9/17/18 17:41
JMV
P810203
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
*8270D
9/17/18 17:41
JMV
P810203
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
*8270D
9/17/18 17:41
JMV
P810203
3/4-Methyl phenol
BRL
mg/L
0.050
0.0015
1
*8270D
9/17/18 17:41
JMV
P810203
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
*8270D
9/17/18 17:41
JMV
P810203
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
*8270D
9117/18 17:41
JMV
P810203
Hexachloroethane
BRL
mg/L
0.050
0.0017
1
*8270D
9/17/18 17:41
JMV
P810203
mzene
BRL
mg/L
0.050
0.0026
1
*8270D
9/17/18 17:41
JMV
P810203
hlorophenol
BRL
mg/L
0.25
0.0012
1
*8270D
9/17/18 17:41
JMV
P810203
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 3 of 30

' IFull -Service Analytical &
Environmental Solutions
LABORATORIES ING
City of Statesville, NC
F idy Smith
F )x 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Project No.: 3rd Creek/4th Creek/StaLime
Sample Matrix: Solid
Laboratory Report
09/26/2018
Client Sample ID: StaLime
Prism Sample ID: 8090113-01
Prism Work Order: 8090113
Time Collected: 09/10/18 08:20
Time Submitted: 09/10/18 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pyridine BRL mg/L 0.25 0.0010 1 *8270D 9/17/18 17:41 JMV P810203
Surrogate Recovery Control Limits
2,4,6-Tribromophenol
77 %
43-140
2-Fluorobiphenyl
88 %
44-119
2-Fluorophenol
37 %
19-119
Nitrobenzene-d5
84 %
44-120
Phenol-d5
28 %
11-52
Terphenyl-d14
93 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.00083
1
*8260B
9/22/18
2:50
KDM
P810322
1,2-Dichlorcethane
BRL
mg/L
0.025 0.00066
1
*8260B
9122/18
2:50
KDM
P810322
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.00050
1
*8260B
9/22/18
2:50
KDM
P810322
Benzene
BRL
mg/L
0.025 0.00048
1
*8260B
9/22/18
2:50
KDM
P810322
Carbon Tetrachloride
BRL
mg/L
0.025 0.0011
1
*8260B
9/22/18
2:50
KDM
P810322
Chlorobenzene
BRL
mg/L
5.0 0.00062
1
*8260B
9/22/18
2:50
KDM
P810322
Chloroform
BRL
mg/L
0.30 0.00076
1
*8260B
9/22/18
2:50
KDM
P810322
A thyl Ketone (2-Butanone)
BRL
mg/L
10 0.0024
1
*8260B
9/22/18
2:50
KDM
P810322
l )roethylene
BRL
mg/L
0.035 0.00098
1
*8260B
9/22/18
2:50
KDM
P810322
Trichloroethylene
BRL
mg/L
0.025 0.00078
1
*8260B
9/22118
2:50
KDM
P810322
Vinyl chloride
BRL
mg/L
0.020 0.00097
1
*8260B
9/22/18
2:50
KDM
P810322
Surrogate Recovery Control Limits
4-Bromofluorobenzene 99 % 80-124
Dibromofluoromethane 77 % 75-129
Toluene-d8 100 % 77-123
a
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 30

J®® I S Full -Service Analytical &
Environmental Solutions
"-ON TOFIES, [Na
Laboratory Report
09/26/2018
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID:
4th Creek
/ ndy Smith
Prism
Sample ID: 8090113-02
1 3x 1111
Project No.:
3rd Creek/4th Creek/StaLime
Prism
Work Order: 8090113
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/10/18 08:03
Time Submitted: 09/10/18
13:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
15.2
% by
0.100
0.100
1
*SM2540 G
9112118 15:40
SLS
P810152
Weight
Corrosivity-pH
8.8
pH Units
1
*9045D
9114118 16:09
CBP
P810221
Ignitability
BRLA
mm/sec
0.,10
1
*1030
9/20/18 13:14
BMS
P810286
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
9/13/18 7:20
MMR
P810153
TCLP Extraction
Complete
N/A
1
*1311 ZHE
9/21/18 15:10
KDM
P810314
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
*7470A
9113/18 14:15
MMR
P810159
Arsenic
BRL
mg/L
0.10
0.016
1
*6010D
9/13/18 18:16
JAB
P810157
Barium
BRL
mg/L
5.0
0.0040
1
*6010D
9/13/18 18:16
JAB
P810157
Cadmium
BRL
mg/L
0.025
0.00075
1
*6010D
9/13/18 18:16
JAB
P810157
Chromium
BRL
mg/L
0.25
0.0018
1
*6010D
9/13/18 18:16
JAB
P810157
Lead
BRL
mg/L
0.050
0.0040
1
*6010D
9/13/18 18:16
JAB
P810157
Selenium
BRL
mg/L
0.10
0.028
1
*6010D
9/13/18 18:16
JAB
P810157
BRL
mg/L
0.25
0.0020
1
*6010D
9/13/18 18:16
JAB
P810157
__. Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00086
1
*8081B
9/20/18 17:20
JMC
P810235
Dieldrin
BRL
mg/L
0.00050
0.000070
1
*8081 B
9120/18 17:20
JMC
P810235
Endrin
BRL
mg/L
0.00050
0.000075
1
*8081B
9/20/18 17:20
JMC
P810235
gamma-BHC
BRL
mg/L
0.00050
0.000065
1
*8081B
9/20118 17:20
JMC
P810235
Heptachlor
BRL
mg/L
0.00050
0.000085
1
*8081 B
9/20/18 17:20
JMC
P810235
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000065
1
*8081 B
9/20/18 17:20
JMC
P810235
Methoxychlor
BRL
mg/L
0.00050
0.00020
1
*8081 B
9/20/18 17:20
JMC
P810235
Toxaphene
BRL
mg/L
0.025
0.00037
1
*8081 B
9/20/18 17:20
JMC
P810235
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
78 %
13-186
Tetrachloro-m-xylene
58 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
*8270D
9/17/18 18:04
JMV
P810203
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
*8270D
9/17/18 18:04
JMV
P810203
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
*8270D
9/17/18 18:04
JMV
P810203
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
*8270D
9/17/18 18:04
JMV
P810203
3/4-Methylphenol
3.8
mg/L
0.50
0.015
10
*8270D
9/18/18 10:14
JMV
P810203
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
*8270D
9/17/18 18:04
JMV
P810203
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
*8270D
9/17/18 18:04
JMV
P810203
Hexachloroethane
BRL
mg/L
0.050
0.0017
1
*8270D
9/17/18 18:04
JMV
P810203
nzene
BRL
mg/L
0.050
0.0026
1
*8270D
9117/18 18:04
JMV
P810203
:hlorophenol
BRL
mg/L
0.25
0.0012
1
*8270D
9/17/18 18:04
JMV
P810203
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 30

I�
SM
7 I Full -Service Analytical &
Environmental Solutions
._- LABORATORIES. ING
Laboratory Report
09/26/2018
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: 4th Creek
f ndy Smith
Prism Sample ID: 8090113-02
F 3x 1111
Project No.: 3rd Creek/4th Creek/Stal-ime
Prism Work Order: 8090113
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/10/18 08:03
Time Submitted: 09/10/18 13:15
Parameter
Result Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Pyridine
BRL mg/L 0.25 0.0010
1 *8270D 9/17/18 18:04 JMV P810203
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
76 %
43-140
2-Fluorobiphenyl
82 %
44-119
2-Fluorophenol
45 %
19-119
Nitrobenzene-d5
79 %
44-120
Phenol-d5
33 %
11-52
Terphenyl-d14
88 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.00083
1
*8260B
9/22/18
3:16
KDM
P810322
1,2-Dichloroethane
BRL
mg/L
0.025 0.00066
1
*8260B
9/22/18
3:16
KDM
P810322
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.00050
1
*8260B
9/22/18
3:16
KDM
P810322
Benzene
BRL
mg/L
0.025 0.00048
1
*8260B
9/22/18
3:16
KDM
P810322
Carbon Tetrachloride
BRL
mg/L
0.025 0.0011
1
*8260B
9/22/18
3:16
KDM
P810322
Chlorobenzene
BRL
mg/L
5.0 0.00062
1
*8260B
9/22/18
3:16
KDM
P810322
Chloroform
BRL
mg/L
0.30 0.00076
1
*8260B
9122/18
3:16
KDM
P810322
P !thyl Ketone (2-Butanone)
BRL
mg/L
10 0.0024
1
*8260B
9/22/18
3:16
KDM
P810322
1 :)roethylene
BRL
mg/L
0.035 0.00098
1
*8260B
9/22/18
3:16
KDM
P810322
Trichloroethylene
BRL
mg/L
0.025 0.00078
1
*8260B
9/22/18
3:16
KDM
P810322
Vinyl chloride
BRL
mg/L
0.020 0.00097
1
*8260B
9/22/18
3:16
KDM
P810322
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
99 %
75-129
Toluene-d8
100 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 30

P'R_ M Laboratory Report
Full -Service Analytical &
J Environmental Solutions 09/26/2018
�i LABORATORIES$ INC.
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: 3rd Creek
andy Smith Prism Sample ID: 8090113-03
3ox 1111 Project No.: 3rd Creek/4th Creek/StaLime Prism Work Order: 8090113
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/10/18 08:15
Time Submitted: 09/10/18 13:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
17.1
% by
0.100
0.100
1
*SM2540 G
9/14/18 9:45
TJY
P810191
Weight
Corrosivity-pH
6.7
pH Units
1
*9045D
9114/18 16:09
CBP
P810221
Ignitability
BRLA
mm/sec
0.10
1
*1030
9/20/18 13:14
BMS
P810286
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
9/13/18 7:20
MMR
P8I0153
TCLP Extraction
Complete
N/A
1
*1311 ZHE
9/21/18 15:10
KDM
P810314
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
*7470A
9/13/18 14:19
MMR
P810159
Arsenic
BRL
mg/L
0.10
0.016
1
*601OD
9/13/18 18:25
JAB
P810157
Barium
BRL
mg/L
5.0
0.0040
1
*6010D
9/13/18 18:25
JAB
P810157
Cadmium
BRL
mg/L
0.025
0.00075
1
*6010D
9/13/18 18:25
JAB
P810157
Chromium
BRL
mg/L
0.25
0.0018
1
*6010D
9/13/18 18:25
JAB
P810157
Lead
BRL
mg/L
0.050
0.0040
1
*6010D
9/13/18 18:25
JAB
P810157
Selenium
BRL
mg/L
0.10
0.028
1
*6010D
9/13/18 18:25
JAB
P810157
BRL
mg/L
0.25
0.0020
1
*6010D
9/13/18 18:25
JAB
P810157
Drganochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00086
1
*8081 B
9/20/18 17:32
JMC
P810235
Dieldrin
BRL
mg/L
0.00050
0.000070
1
*8081 B
9/20/18 17:32
JMC
P810235
Endrin
BRL
mg/L
0.00050
0.000075
1
*8081 B
9120/18 17:32
JMC
P810235
gamma-BHC
BRL
mg/L
0.00050
0.000065
1
*8081 B
9/20/18 17:32
JMC
P810235
Heptachlor
BRL
mg/L
0.00050
0.000085
1
*8081B
9/20/18 17:32
JMC
P810235
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000065
1
*8081 B
9/20/18 17:32
JMC
P810235
Methoxychlor
BRL
mg/L
0.00050
0.00020
1
*8081 B
9/20/18 17:32
JMC
P810235
Toxaphene
BRL
mg/L
0.025
0.00037
1
*8081B
9/20118 17:32
JMC
P810235
Surrogate
Recovery
Control Limits '
Decachlorobiphenyl 84 % 13-186
Tetrachloro-m-xylene 74 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
*8270D
9/17/18 18:26
JMV
P810203
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
*8270D
9/17/18 18:26
JMV
P810203
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
*8270D
9/17/18 18:26
JMV
P810203
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
*8270D
9/17/18 18:26
JMV
P810203
3/4-Methylphenol
BRL
mg/L
0.050
0.0015
1
*8270D
9117/18 18:26
JMV
P810203
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
*8270D
9/17/18 18:26
JMV
P810203
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
*8270D
9/17/18 18:26
JMV
P810203
Hexachloroethane
BRL
mg/L
0.050
0.0017
1
*8270D
9/17/18 18:26
JMV
P810203
r"' ' lzene
BRL
mg/L
0.050
0.0026
1
*8270D
9/17/18 18:26
JMV
P810203
I lorophenol
BRL
mg/L
0.25
0.0012
1
*8270D
9/17/18 18:26
JMV
P810203
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 30
11

�®I Full -Service Analytical &
`'i SM I Environmental Solutions
, LABORATORIES INC
City of Statesville, NC
\ndy Smith
lox 1111
Statesville, NC 28687
Laboratory Report
09/26/2018
Project: Sludge (Hazardous Testing) Client Sample ID: 3rd Creek
Prism Sample ID: 8090113-03
Project No.: 3rd Creek/4th Creek/stal-ime Prism Work Order: 8090113
Sample Matrix: Solid Time Collected: 09/10/18 08:15
Time Submitted: 09/10/18 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pyridine BRL mg/L 0.25 0.0010 1 '8270D 9117/18 18:26 JMV P810203
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
101 %
43-140
2-Fluorobiphenyl
99 %
44-119
2-Fluorophenol
65 %
19-119
Nitrobenzene-d5
93 %
44-120
Phenol-d5
41 %
11-52
Terphenyl-d14
96 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.00083
1
'8260B
9/22/18
3:42
KDM
P810322
1,2-Dichloroethane
BRL
mg/L
0.025 0.00066
1
'8260B
9/22/18
3:42
KDM
P810322
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.00050
1
`8260B
9/22/18
3:42
KDM
P810322
Benzene
BRL
mg/L
0.025 0.00048
1
'8260B
9/22/18
3:42
KDM
P810322
Carbon Tetrachloride
BRL
mg/L
0.025 0.0011
1
'8260B
9122/18
3:42
KDM
P810322
Chlorobenzene
BRL
mg/L
5.0 0.00062
1
'8260B
9/22/18
3:42
KDM
P810322
Chloroform
BRL
mg/L
0.30 0.00076
1
'8260B
9/22/18
3:42
KDM
P810322
P" ' Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0024
1
'8260B
9/22/18
3:42
KDM
P810322
croethylene
BRL
mg/L
0.035 0.00098
1
'8260B
9122/18
3:42
KDM
P810322
Trichloroethylene
BRL
mg/L
0.025 0.00078
1
'8260B
9/22/18
3:42
KDM
P810322
Vinyl chloride
BRL
mg/L
0.020 0.00097
1
"8260B
9122/18
3:42
KDM
P810322
Surrogate
Recovery Control Limits
4-Bromofluorobenzene 100 % 80-124
Dibromofluoromethane 100 % 75-129
Toluene-d8 98 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 30

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
80 )1
P810152
30
g
30 g
09/12/18 15:40
80.,., � .--J2
P810152
30
g
30 g
09/12/18 15:40
8090113-03
P810191
30
g
30 g
09/14/18 9:45
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810153
100
g
2000 mL
09/12/18 14:25
8090113-01
P810314
12.5
g
250 mL
09/20/18 16:30
8090113-02
P810153
100
g
2000 mL
09/12/18 14:25
8090113-02
P810314
12.5
g
250 mL
09/20/18 16:30
8090113-03
P810314
12.5
g
250 mL
09/20/18 16:30
8090113-03
P810153
100
g
2000 mL
09/12/18 14:25
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810157
10
mL
50 mL
09/13/18 10:10
8090113-02
P810157
10
mL
50 mL
09/13/18 10:10
8090113-03
P810157
10
mL
50 mL
09/13/18 10:10
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810159
20
mL
30 mL
09/13/18 10:00
8090113-02
P810159
20
mL
30 mL
09/13/18 10:00
8090113-03
P810159
20
mL
30 mL
09/13/18 10:00
F thod: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810235
200
mL
10 mL
09/18/18 9:30
8090113-02
P810235
200
mL
10 mL
09/18/18 9:30
8090113-03
P810235
200 inL
10 mL
09/18/18 13:16
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810203
200
mL
1 mL
09/17/18 9:06
8090113-02
P810203
200
mL
1 mL
09/17/18 9:06
8090113-02
P810203
200
mL
1 mL
09/17/18 9:06
8090113-03
P810203
200
mL
1 mL
09/17/18 9:06
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810322
1
mL
10 mL
09/21/18 15:57
8090113-02
P810322
1
mL
10 mL
09/21/18 15:57
8090113-03
P810322
1
mL
10 mL
09/21/18 15:57
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 30

Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab Number
Analysis
M Herbicides TCLP (Sub)
W Herbicides TCLP (Sub)
8090113-03 Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number
Analysis
8090113-01
Reactivity, Cyanide (Sub)
8090113-01
Reactivity, Sulfide (Sub)
8090113-02
Reactivity, Cyanide (Sub)
8090113-02
Reactivity, Sulfide (Sub)
8090113-03
Reactivity, Cyanide (Sub)
8090113-03
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 30

�l
` 'RSM Full -Service Analytical &
I Environmental Solutions
A"-�`': LABORATORIES INC.
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] • Fax: [phone]r-0409 BB
Client Company Name: C: � y n-P S4a-�•£SVr / 1C
Report To/Contact Name: Ke.j bra 116 W A if
Reporting Address: i
PAGE OF QUOTE til TO ENSURE PROPER BILLING:
Project Name:✓y`{-
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
a -
-
YE^, NO
NIA ce)
Samples INTACT upon arrival?
-
i o
Received ON WET ICE?
r
PROPER PRESERVATIVES indicated?
1
'-
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
v
VOLATILES reed W/OUT HEADSPACE?
t/
PROPER CONTAINERS used?
TEMP: Therm IM Y 5 _° % Observed: • ?. °C / Carr:
°C
Phone:70- 878' V13T Fax es (No):7o+978- 86$5 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DoD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ RushWork Must Be
SC OTHER NIA
Ir�ouR�rbr f
Site Location Name: C ZC ti k Samples received after 14:00 will be processed next business day.
Site Location Physical Address: 6113 Le In &&V, Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES
BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
p p —
TIME
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
f
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
` REMARKS
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
`TYPE
NO.
SIZE
TIVES
%
ID NO.
HOURS
SLUDGE)
SEE BELOW
r' f
Si•ak&7
9- to- is
I
Imo'`
�O1 a� � G/ TCJP
01
1
RE.4
k, Y
r� "
,queck e S A
o3
rC IL
P 9
G
®j�
S em
a 1/0d'
s
�.
-
0.3
rn,
f
I
I 2V lJ�� Affiliation
Sampler's Signature fi' Sampled By (Print Name) /Z r C
Upon relinquishing, this Chain of Custody is your authorization for Prism -to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges -for ny changes after analyses have been initialized. y�
Rellnquishe By: (Signalu IRecely By: (Sign lure) D)arte % /Miilbry/Hours Additional Comments: Site Arrival Time:
/��>0� / �C3 y
Relin ' had By- (Signalure) P cTMed ey;. ,nature). Date Site Departure Time:
Rellrnlulshe ": (Sign turn)) ! Recuiva or P DateLabor cries By: Date Field Tech Fee:
J 3''�
� ��� ��j•^'/��� � •,
.�.�-,/%� Mileage:
d of Shl ent: NOTE: ALL SAMPLE COOLERS SHOULDBETAPED, SHUT VaM CUSTOD-Y.SEALS FOR TRANSPORTATIONTOTHE LABORATORY. COG Group -No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY.O
�11
PL03F,'d
Ex ❑ UPS i-dellvered Prlsm Field Service O Other
NPDES: UI GR UNDWATER: DRINKING WATER: SOLID WASTE: RCRI CERCLA LANDFILL OTHER:
El NC ❑ SC D.... J SC ❑ NC ❑ SC ❑ NC ❑ SC NC ❑ SC EI NC 0❑ NC El SC ❑❑ NC E3 SC ❑❑ NC El SC
❑ n ❑ ❑ - Ll
*n��arn �nr�e rnnc n�nCa. A - A-k-. h - r`I..... !`- !_'Inoo D - DI—N- TI - T f,nn_I innti Cnn \/r)A = \/nlatila Omnninq Angly-qlq I7P_rn HPRrI SnACP_i

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Terri W. Cole
PROJECTID
8090113
LABORATORY REPORT NUMBER
1809871
DATE
September 21, 2018
Primary Data Review By Secondary Data Review By
Chris Pafford
Project Manager, AES
PLEASE NOTE:
Ashley Amick
Project Manager, Access Analytical
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDI-IEC certified laboratory # 98016, NCDENR certified lab Al 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- AIIIA-LAP,LLC Laboratory ID:100671 for Industrial flygiene samples (Organics, Metals, PCNI Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page
Page 12 of 30

l' ^ 1 S lEnvironmental
Service Analytical s��'�"� ; J Solutions
1+' LSECDX;0NE`12:�
SUBCONTRACT ORDER
roa98 w
64 ff-�C `/!f //8'
Certification: NELAC_ USACC
Prism Laboratories, Inc. 14cC Z S'C_ Other
8090113 N/A
SENDING LABORATORY: RECEIVING LAP,ORATORY:
Prism Laboratories, Inc. Analytical Environmental Services, Inc.
P. O. Box 240543 3080 Presidential Parkway
Charlotte, NC 28224-0543 Atlanta, GA 30340
Phone: [phone] Phone :[phone]
Fax: [phone] Fax: NA
Project Manager: Robbi A. Jones
Analysis Due Expires Laboratory ID Comments
Simple 1D:8090113-01 Solid SamplSd:09/10/1808.20
Herbicides TCLP (Sub)
09/17/18 08:20
Containers Supplied.•
Sample 1D: 8090113-02
Solid
Sampled :09/10/18 08:03
Herbicides TCLP (Sub)
09/17/18 03:03
Containers Supplied:
Som09/I0/13 08:13
r
Sample ID: 3090113-03
Solid
pled:
Herbicides TCLP (Sub)
09/17/18 08:15
Containers Supplied
Released 0y D:dc Received 13y Dnle
Pa,e I of I
Page `
Page 13 of 30

Analytical Environmental Services, Inc
Date: 20-Sep-18
Client:
Prism Laboratories
Client Sample ID:
Sta Lime
Lab Order
1809871
Tag Number:
8090113-01
Project Name:
8090113
Collection Date:
9/10/2018 8:20:00 AM
Lab ID:
1809871-OOIA
Matrix:
Solid
Analyses Result Qua[ MDL Reporting Units BateblD DF Date Analyzed Analyst
Limit
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 79.5
Qualifiers: IValue exceeds maximum contaminant level
BRL Not Detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
D Analyte detected in ilia associated melhod blank
(SW3510C)
0.030 0.20 tng/L 267209 1 09/18/201817:05 UH
0.051 0.20 fng/L 267209 1 09/18/201817:05 UH
0 50.4-133 %REC 267209 1 09118/201817:05 UH
E Estimated value above quamimfion range
S Spike Recovery outside lints due to malix
Graaler Ilion Result value
1 Estimated value detected below Reporting Limit
< Less Ilion Result value
Page `
Page 14 of 30

Analytical Environmental Services, Inc
Date: 20-Sep-18
Client:
Prism Laboratories
Client Sample ID:
4th Creek
Lab Order
1809871
Tag Number:
8090113-02
Project Name:
8090113
Collection Date:
9/10/2018 8:03:00 AM
Lab ID:
1809871-002A
Matrix:
Solid
Analyses
Result
Qual MDL
ReportingUnits
Limit
BatchID
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
mg/L 267209
1 09/18/2018 17:26 UH
2,4-D
BRL
0.051
0.20
tng/L 267209
1 09/18/2018 17:26 UH
Surr: DCAA
80.9
0
50.4-133
%REC 267209
1 09/18/2018 17:26 UH
QunliGers: • Value exceeds maximum contaminant level E Estimated value above quamitation range
BRL Non Detected al MDL S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded > Greater than Result value
N Analyte not NELAC certified J Estimated value detected below Reporting Limit
B Analyle detected in the associated method blank - Lrs than Re,uli Nalw
Page I -'-
Page 15 of 30

Analytical Environmental Services, Inc
Date: 20-Sep-18
Client:
Prism Laboratories
Client Sample ID:
3rd Creek
Lab Order
1809871
Tag Number:
8090113-03
Project Name:
8090113
Collection Date:
9/10/2018 8:15:00AM
Lab ID:
1809871-003A
Matrix:
Solid
Analyses
Result
Qua] MDL
Reporting
Limit
Units BatchID
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
inElL 267209
1 09/18/2018 17:46 UH
2,4-D
BRL
0.051
0.20
mr)L 267209
1 09/18/201817:46 UH
Surr: DCAA
84
0
50.4-133
%REC 267209
1 09/18/2018 17:46 UH
Qunliriers: • Value exceeds maximum contaminant level
BRL Not Dctecicd ul MDL
H Holding times for preparation or analysis exceeded
N Analyte not NE -LAC cenified
B Analyie detected in the associated method blank
E Estimated value above quamitalion range
S Spike Recovery outside limits duc to matrix
> Greater than Result value
J Estimated value detected below Reporting Limit
Less than Result value
Page r, G-
IPage 16 of 30

f
1,tt_,-I•It:A.1. - Clear - _ - ,. ve as
DES IFIQVIRMOMIZ AT.
SrRvtcrs, ixc. SAMPLE/COOLER RECEIPT CHECKLIST
1. Client Name: Access Analytical, Inc. AES Work Order Number: 1809871
2. Carrier: FedEx ❑d UPS ❑ USPS❑ Client❑ Courier❑ Othei
Yes No N/A Details Comments
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13. Cooler 1 Temperature 0.6 °C Cooler 2 Temperature
14. Cooler 5 Temperature °C Cooler 6 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27. Comments:
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). ED 9/12/18
checked at Sample Receipt. Yes No N/A Details Comments
Shipping container/cooler received in good condition?
a
damaged ❑ leaking ❑ other❑
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
Temperature blanks present?
•
Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for
temperature recordings.]
®
®
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (COC) present?
a
Chain of Custody signed, dated, and timed when relinquished and received?
•
Relinquished: Signed/dated
Sampler name and/or signature on COC?
a
Were all samples received within holding time?
o
TAT marked on the COC?
a
If no TAT indicated, proceeded with standard TAT per Terms & Conditions. U
°C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 7 Temperature 0C Cooler 8 Temperature 0C
I certify that I have completed sections 1-15 (dated initials).
Yes No N/A Details Comments
MH 9/12/18
Were sample containers intact upon receipt?
o
Custody seals present on sample containers?
•
Custody seals intact on sample containers?
o
Do sample container labels match the COC?
Q
®
O
incomplete info ❑ illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
e
all of the samples listed on the COC received?
O
samples received but not listed on COC ElWere
samples listed on COC not received ❑
Was the sample collection date/time noted?
o
Did we receive sufficient sample volume for indicated analyses?
o
Were samples received in appropriate containers?
•
Were VOA samples received without headspace (< 1/4" bubble)?
Were trip blanks submitted?
Ilisted on COC ❑ not listed on COC ❑
28. Have containers needing chemical preservation been checked? I U {U 1 o
29. Containers meet preservation guidelines? 1 •
W 30. Was pH adjusted at Sample Receipt? 0 0 1•
LQ
m ' Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
v _ I certify that I have completed sections 28-30 (dated initials).
Checklist 6.9.17 Rev 2
ca Locked
ED 9/12/18
o Page 6 of 7

Analytical Environmental Services, Inc
Client: Prism Laboratories
Project Name: 8090113
Workorder. 1809871
Date: 20-Sep-18
ANALYTICAL QC SUMMARY REPORT
BatchID: 267209
Sample ID: MB-267209
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: NIBLK
TestCode: HERBICIDES,TCLP SW1311/8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8473938
Analyte
Result RPT Limit SPK value SPK Ref Val
%RFC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 0.3556 0 0.5000 71.1 50.4 133
Sample iD: MB-267209-2
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: MBLK
TestCode: HERBICIDES,TCLP SW1311/8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8476476
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
2.4-D BRL 0.20
Surr: DCAA 0.4079 0 0.5000 81.6 50.4 133
Sample ID: LCS-267209
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: LCS
TestCode: HERBICIDES,TCLP SWI311/8151A
BatchlD:267209
Analysis Date: 09/18/2018
Seq No: 8473939
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4302
0.20
0.5000
86.0
49.1
119
2,4-D
0.4451
0.20
0.5000
89.0
50.9
129
Surr: DCAA
0.4377
0
0.5000
87.5
50.4
133
Sample TD: 1809998-001BMS
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: NIS
TestCode: HERBICIDES,TCLP SW1311/8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8473941
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qua]
2,4,5-TP (Silvex)
0.4443
0.20
0.5000
88.9
48.2
125
2,4-D
0.4892
0.20
0.5000
97.8
44.5
138
Surr: DCAA
0.4283
0
0.5000
85.7
50.4
133
F1
U Qualirrers: I Greater lhon Result value
(D
BRL Below reporting limit
-� J Estimated value detected below Reporting Limit
00
0 Rpt Lim Reporting Limit
W
O
< Less than Result value
E Estimated (value above quantilation range)
N Analyle not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding limes for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 7 of 7

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
8090113
LABORATORY REPORT NUMBER
218091310
DATE
09/18/2018
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amidlr
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 218091310 Page 1 of 12
Page 19 of 30

ANALYTfC„L LABORATORIES, LLC
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
a �3 tvl 1' .; i • I i . 1._ .s .'i. a.. _J� L �,_ t T
PERFORMED BY
GCAL, LLC
7979 Innovation Park Dr.
Baton Rouge, LA 70820
Report Date 09/18/2018
GCPL ReportII 218091310
��III l� luO lsl��lull
Project 8090113
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
kr"t 4
7025 I .�PJLA
r qi
Testing
Don EIAP
Lab Report#: 218091310 Page 2 of 12
Page 20 of 30

Report#: 218091310
Project ID: 8090113
Laboratory Endorsement
Report Date: 09/18/2018
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed In accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
NO Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLO Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD —see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution Is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
GCAL Report 218091310
Lab Report#: 218091310 Page 3 of 12
Page 21 of 30

Report#: 218091310
Project ID: 8090113
Certifications
Report Date: 09/18/2018
Certification
Certification Number
DOD ELAP
L14-243
Alabama
01955
Arkansas
12-060-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
USDA Soil Permit
P330-10-00117
Lab Report#: 218091310 Page 4 of 12
Page 22 of 30

Report#: 218091310
ko
Project ID: 8090113
Case Narrative
Client: Access Analytical Report: 218091310
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Report Date: 09/18/2018
Lab Report#: 218091310 Page 5 of 12
Page 23 of 30

GCAL ID Client ID
21809131001 StaLime
21809131002 4th Creek
21809131003 3rd Creek
Report#: 218091310
Project ID: 8090113
Sample Summary
Matrix
Collect Date/Time
Solid
09/10/2018 08:20
Solid
09/10/2018 08:03
Solid
09/10/2018 08:15
Report Date: 09/18/2018
Receive Date/Time
09/13/2018 09:40
09/13/2018 09:40
09/13/2018 09:40
Lab ReporW 218091310
Page 6 of 12
Page 24 of 30

Report#: 218091310
0;`!,� .,:��r`- . Project ID: 8090113 Report Date: 09/18/2018
Summary of Compounds Detected
4th Creek Collect Date 09/10/2018 08:03 GCAL ID 21809131002
Receive Date 09/13/2018 09:40 Matrix Solid
EPA 9034
CAS#
18496-25.811
Parameter
Reactivity Sulfide
Result DL LOQ Units
425 250 250 mglkg
Lab Report#: 218091310
Page 25 of 30

of�
Report#: 218091310
Project ID: 8090113
Sample Results
Report Date: 09/18/2018
StaLime Collect Date 09/10/2018 08:20 GCAL ID 21809131001
Receive Date 09/13/2018 09:40 Matrix Solid
Ef
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643869 EPA 7.3.3.2 (1997) 1 09/17/2018 12:49 TMT 644001
CAS# Parameter Result DL LOQ Units
57-12-5R Reactivity Cyanide 25OU 250 250 mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643870 EPA 7.3.4.2 (1997) 1 09/17/2018 15:40 JRB 643979
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result DL LOQ
250U 250 250
4th Creek Collect Date 09/10/2018 08:03 GCAL ID 21809131002
Receive Date 09/13/2018 09:40 Matrix Solid
9012B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643869 EPA 7.3.3.2 (1997) 1 09/17/2018 12:51 TMT 644001
CAS# Parameter
57-12-5R Reactivity Cyanide
EPA 9034
Result
DL
LOQ
Units
250U
250
260
mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643870 EPA 7.3.4.2 (1997) 1 09/17/2018 15:40 JRB 643979
CAN
Parameter
Result
DL
LOQ
Units
18496-25-8R
Reactivity Sulfide
425
250
250
mglkg
Lab Report#:218091310
Page 8 of 12
Page 26 of 30

£ Report#: 2180913100
T��
. ��,,.,{�,,�,,�„�„_„�,, _�. Project ID: 8090113 Report Date: 09/18/2018
Sample Results
Collect Date 09/10/2018 08:15 GCAL ID 21809131003
3rd Creek Receive Date 09/13/2018 09:40 Matrix Solid
Ef
)12B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643869 EPA 7.3.3.2 (1997) 1 09/17/2018 12:53 TMT 644001
CAS# Parameter Result DL LOQ Units
57-12-5R Reactivity Cyanide 250U 250 250 mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643870 EPA 7.3.4.2 (1997) 1 09/17/2018 15:40 JRB 643979
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result
DL
LOQ
Units
250U
250
250
mg/kg
Lab Report#: 218091310

Report#: 218091310
Project ID: 8090113
General Chemistry QC Summary
Report Date: 09/18/2018
Analytical Batch Client ID
M8643870
LCS643870
643979 GCALID
1848779
1848780
Prep Batch Sample Type
MB
LCS
643870 Prep Date
09/14/2018 12:31
09/14/2018 12:31
Prep Method Analysis Date
09/17/2018 15:40
09/17/2018 15:40
EPA 7.3.4.2 (19971 Matrix
Solid
Solid
EPA 9034
Units
mg/kg
Spike
IResult
%R
Control
Result
DL
Added
Limits%R
Reactivity Sulfide 18496-25-8R
250U
250
1000
1282
128
47 - 135
Analytical Batch Client ID
MB643869
LCS643869
644001 GCALID
1848776
1848777
Prep Batch Sample Type
MB
LCS
643869 Prep Date
09/14/2018 12:31
09/14/2018 12:31
Prep Method Analysis Date
09/17/201812:33
09/17/2018 12:35
EPA 7.3.3.2 (1997) Matrix
Solid
Solid
EPA 9012B
Units
mg/kg
Spike
sult
%R
Control
Result
DL
Added
pi239
Limits%R
Reactivity Cyanide 57-12-5R
ND
250
250
10
1 - 25
Lab Report#: 218091310 Page 10 of 12
Page 28 of 30

r
v
tp
0
0
N
r
Envir orvlCeswen Analytical s
I l 1 Enviro:�rtental5alutions
SrNDiNG uknonxroiz ':
Prism Laboratories, Inc.
P. 0, Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
Fax: [phone]
Project Manager: Robbi A. Jones
doe' n4 lm 4565 Access Analytical
SDG: 2180310
t/ Ph1 AEC'
. ----------
SUBCONTRACT ORDER
Certification: ELAC_ USACE _
Prism Laboratories, Inc. NC SC Other
8090113 N/A
RyerIVINC 1.21nORNFORY:
Gulf Coast Analytical Labs, Inc.
10781 Coursey Blvd
Baton Rouge, LA 70816
Phone ,[phone]
Fax: [phone]
Annlysis Due Expires Laboratory 1D Comments
Sample ID:8090113-01 Solid Sampled:09/1011808:20
Reactivity, Sulfide (Sub) 09/17/18 08:20
Reactivity, Cyanide (Sub) 09/24/18 08:20
Containers supplied:
SntapleID. 8090113-OZ Solid Sanipled:09110/1808:03 '�_=_`.•_i'' ttiYi '%
Reactivity, Sulfidc (Sub)
09117/18 08:03
Re;ictivily, Cynnide (Sub)
09/24/18 08:03
Containers Supplied:
Sample 1D: 8090113-03 Solid
snmplcd:09/10/18 08:15
1:
Reactivity, Cyanide (Sub)
09/24/18 0& 15
Reactivity, Sullde (Sub)
09117/18 08:15
Coruainers ,Supplied:
-77 (�l 9
r
I �leas4tl tit}'
( �
U:ue
Received Ilv
/
Mile
✓`
R�Ica:;.d f3y
O uc
Rccci IDaw
Released D?'
1)utr
RcCcivctl 13),
Dale
Released liy
D'Itc
Received By
Dale
Page I of I
Page 29 of 30

Q�(SC{gL SAMPLE RECEIVING CHECKLIST _ IIuBl�HIA'3II�07
SAMPLE DELIVERY GROUP
218091310
CHECKLIST
YES
NO
Client PM AEC
Transport Method
Samples received with proper thermal preservation?
0
❑
4565 - Access Analytical
F®DC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
0
0
❑
❑
Profile Nimber
Received Ey
80251
Savage, Tiffany R
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
®
®
❑
❑
Line Item(s)
Receive Date(s)
2 - Solid
09/13/18
-
Preservative added to any containers?
❑
❑N
If received, was headspace for VOC water containers < 6mm?
®
❑
Samples collected in containers provided by GCAL?
❑
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer la E29
Temp °C
Pbne
Nbne
i731-9086-6869
2.0
NOTES
FRsvision 1.6 Page 1 of 1
Lab Report#: 218091310 Page 12 of 12

�VMICROBAC`
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K810048
City of Statesville Project Name: Sta-lime/Sludge Sample - 4th Creek
WWTP
Mr Ken Galloway Project / PO Number: N/A
Post Office Box 1111 Received: 09/05/2018
Statesville, NC 28687-1111 Reported: 09/18/2018
Analytical Testing Parameters
Client Sample ID: Sludge
Sample Matrix: Sludge Collected By: Galloway
Lab Sample ID: K810048-01 Collection Date: 09/05/2018 12:00
Analyses Subcontracted to: Microbac Laboratories, Inc. - Baltimore
Wet Chemistry Result RL Units Note Prepared Analyzed Analyst
Method: SM 2540 G-11
% Solids 87.30 0.05 % by Weight 09/11/18 1551 09/12/18 1216 RDM
Microbiology Result RL Units Note Prepared Analyzed Analyst
Method: EPA 1682
Salmonella <0.030 0.030 MPN/4g dry 09/06/18 1720 09/07/18 1909 EMS
D Dns
RL: Reporting Limit
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to ,
applicable accreditation standard unless otherwise noted.�
9 data and information on this, and other accompanying documents, represents Jeanne Overstreet
ly l l e sanalyzed. This report is incomplete unless a// ages indicated
Client Relationship Specialist, Environmental
thefootnote are present and an authorized signature is included
Reported: 09/18/2018 09:27
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 2

IM
Microbac-Fayetteville SHOj'
'LDS ACCEPTED MONDAY-THURSDAYUNTIL 1600 *KPfnn48*
{ Q G 2592 Hope Mills Rd.
CHAIN OF CUSTODY RECI
Fayetteville, NC 28306
Number II��I�IIIII1�>►«��«��„��I�I�illf�l��l�l
Instructions on back
Lab Report Address Invoice Address
Turnaround Time TO BE COMPLETED 8 Y M
Client Name: City of Statesville 4th Creek Client Name: 0i4/ of Statesville
outlne (5 to 7 business days) Temp. Upon Receipt (-C)
Address: 693 Bell Farm Road Address. 693 Bell Farm Road
[ j RUSH' (notify lab) Holding Time
City, State, Tip: Statesville, NC 28625 City, State, Zip: Statesville, NC 28625
(needed by) Samples Received on Ice? Yes No NIA
Contact: Ken Galloway Contact: Ken Galloway
Report Type Custody Seals Intact? Yes No N/A
Telephone No.: 704-878-3438 Telephone No.: 704-678-3438
Results Only [ j Level 1 [ ] Level 2 (] Leve13 [ I Level 4 [ ] EDD
Send Report via: (} Mail (] Fax ll-mail kaaltoway@gtatesvi_llenc.net Send Invoice via: [ j Mail [ j Fax -mail kpallowayi�statesyinenc.net
+
,
Project:
ILocation:
Sampled by
PO No.: Compliance Monitoring? ( ]Yes [ ] No [ I Agency/Program
(PRINT): Ken Gall!
av Sampler Signature,
Sampler Phone No.: 704-878.343a
. Matrix Types: Soil/Solid (S),
ludge, Oil, Wipe, Drinking Water (DW), Groundwater (GW), Surface Water (SW), Waste Water (W W), Other (specify)
Preservative Types: (1) HNO3, (2)
2SO4, (3) HCl. (4) NaOH, (5) Zinc Acetate, (6) Methanol, (7) Sodium Bisulfate, (8) Sodium Thiosulrate, (9) Hexane, (U) Unpreserved
DCnl 1=Zrt=n AA1AI VCIC
Lab I
Client Sample ID
Date
ollected
Time
Collected
No. of
Containers
Matrix
or B
Comp
Preservative
type " o
� �z
Additional Notes
1
4th Creek Sta-Lime
/5/2018
1 1200
1
S
Grab
A
I�
I
�
I
I
i
I
I
i
i
4
I
1 I
Possibte Hazard Identificatio []
[I Non -Hazardous [] Radioactive
DatelTi me
uished By (signature) DateMme
Relinquished By (signature) Daterl-ime
Sam [] Dispose as appropriate [] Return [I Archive
Received By (signature) Date/Time
Received By (signature) Date/Time
Received By (signature) DatelTime
77-77-1
Page 2 of 2

Jr`1
NC Certification No. 402
Case Narrative
PM I S M Full -Service Analytical & NC Drinking Water Cert No. 37735 04/24/2017
Environmental Solutions SC Certification No. 99012
i BORATORIE$ Ma
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 04/10/2017
Prism Work Order: 7040188
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR=[Na]/SQRT(([Ca]+[Mg])/2},
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating_to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
—f� ?�_ a- -
Reviewed By Robbi A. Jones
President/Project Manager
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference -
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 15

�_ I S n n I Full -Service Analytical Solutions
'-�� - ' V' EnvironmentalFull-Service
Atical&
LABORATORIES —
Sample Receipt Summary
04/24/2017
Prism Work Order: 7040188
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
StaLime (and Fecal 1)
7040188-01
Solid
04/10/17
04/10/17
Fecal #2
7040188-02
Solid
04/10/17
04/10/17
Fecal #3
7040188-03
Solid
04/10/17
04/10/17
Fecal #4
7040188-04
Solid
04/10/17
04/10/17
Fecal #5
7040188-05
Solid
04/10/17
04/10/17
Fecal #6
7040188-06
Solid
04/10/17
04/10/17
Fecal #7
7040188-07
Solid
04/10/17
04/10/17
Samples were received in good condition at 5.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 15

Laboratory Report_
® I S � %� Full -Service Analytical &
' V' Environmental Solutions 04/24/2017
'7BORA ORIEB, INO.
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: StaLime (and Fecal 1)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 7040188-01
P.O. Box 1111 Prism Work Order: 7040188
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1700
mg/kg dry
490
110
5
*Calculation 4118/17 6:53
CLB
[CALC]
% Solids
78.2
% by
0.100
0.100
1
*SM2540 G 4/12/17 16:07
JLB
137D0208
Weight
Nitrate/Nitrite as N
35
mg/kg dry
6.4
0.70
1
*SM4500-NO3 F 4/17/17 10:12
CLB
' 137D0233'-
Phosphorus-Total
290
mg/kg dry
64
9.2
20
*SM4500-P F 4/19/17 7:54
CLB
P7D02ti8
Total Kjeldahl Nitrogen
5500
mg/kg dry
1600
340
5
*351.2 4118/17 6:53
CLB
P7D0152
Ammonia as N
110
mg/kg dry
32
10
5
*SM4500-NH3 G 4/17117 6:56
CLB
P7130197
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 4/11/17 9:15
BMS
P7D0168
Total Metals
Mercury
0.11
mg/kg dry
0.027
0.0015
1
*7471B
SAR Soil Preparation
Complete
g
1
*2-78-054
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
Weight
Arsenic
5.3
mg/kg dry
3.2
0.39
10
*6010D
Sodium Absorption Ratio
0.43
[blank]
0.30
0.016
1
*2-78-054
Cadmium
BRL
mg/kg dry
3.2
0.085
10
*601 OD
Calcium
1400
mg/L
20
2.0
200
*601013
Copper
38
mg/kg dry
6.4
0.68
10
*6010D
Lead
3.2
mg/kg dry
3.2
0.59
10
*6010D
Magnesium
BRL
mg/L
1.0
0.086
10
*6010D
Nickel
6.4
mg/kg dry
6.4
0.23
10
*6010D
Potassium
1700
mg/kg dry
160
5.7
10
*6010D
Selenium
BRL
mg/kg dry
6.4
1.5
10
*6010D
Sodium
490
mg/kg dry
190
6.2
10
*6010D
Sodium
59 BH
mg/L
5.0
0.18
10
*6010D
Zinc
66
mg/kg dry
32
1.1
10
*6010D
4/17117 11:42
JAB
P71010230
4/13/17 9:40
JAB
P7D0179_
4/17/17 10:25
JAB
P7D0246
4117/17 20:06
bgm
P7D0203
4/20117 19:56
bgm
K..D0209
4/17/17 20:06
bgm
P7D0203
4/20117 19:56
bgm
P7D0209
4/17/17 20:06
bgm
P7D11203
4/17117 20:06
bgm
P7D020v
4/17/17 21:17
bgm
P7D020Q
4/17/17 20:06
bgm
P7DOY03
4117/17 20:06
bgm
P7D0203
4/17/17 20:06
bgm
P7D0203
4/17/17 20:06
bgm
P7D0203
4/17/17 21:17
bgm
P7, 40209
4/22117 0:19
bgm
P7D0203,
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 15

Laboratory Report
—� A Full -Service Analytical'&
s R ISM I Environmental Solutions 04/24/2017
1..LABORATORIE$ INC
City of Statesville, NC Project: Stal-ime (Qtrly, Biweekly, Client Sample ID: Fecal #2
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 7040188-02
P.O. Box 1111 Prism Work Order: 7040188
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch .
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids - 74.3
% by
0.100
0.100 1
*SM2540 G 4/12/17 16:07 JLB
P7D0208
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 4/11/17 9:15 BMS
P7D0168
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 15

P R I S n n Full -Service al Solutions
' V' Environmental Solutions
LAeORATORIE$ ING.
Laboratory Rep®ft_ _..
04/24/2017
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #3
Attn: Andy Smith
6013lay 7 Fecal)
Prism Sample ID: 7040188-03
P.O. Box 1111
Prism Work Order: 7040188
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor DateTme ID
General Chemistry Parameters
% Solids
78.2 % by
0.100 0.100
1 *SM2540 G 4112117 16:07 JLB P7D0208
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 *SM9221 E 4/11/17 9:15 BMS P7D0168'
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 15

�] n n Full -Service Analytical
rR I S '
'v' Environmental Solutions
UIaOPATOPIE$ ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
04/24/2017
Client Sample ID: Fecal #4
Prism Sample ID: 7040188-04
Prism Work Order: 7040188
Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids 74.0
% by
0.100
0.100 1 *SM2540 G 4/12/17 16:07 JLB
P7D0208
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 4111117 9:15 BMS
137D0168
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 15

�] ®I S n Full -Service al Solutions
s
r R ' V' Environmental Solutions
��' LABORATORIES, -
Laboratory ,R�epp
04/24/2017.1,.-
City of Statesville, NC
Project: Stal-ime (Qtrly, Biweekly,
Client Sample ID: Fecal #5
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 7040188-05
P.O. Box 1111
Prism Work Order: 7040188
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
71.0 % by
0.100 0.100
1 `SM2540 G 4112/17 16:07
JLB P71D0208
Weight
Microbiological Parameters
-
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 4/11/17 9:15
BMS ' ' PA)0168--
_5 i7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 15

LJI_ Full -Service Analytical
R I S M
Environmental Solutions
� "' � LABORATORIES ING
Laboratory Report
04/24/2017
City of Statesville, NC
Project: Stal-ime (Qtrly, Biweekly,
Client Sample ID: Fecal #6
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 7040188-06
P.O. Box 1111
Prism Work Order: 7040188
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
81.1 % by
0.100 0.100
1 *SM2540 G 4/12/17 16:07 JLB
P7D0208
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 *SM9221 E 4/11/17 9:15 BMS
P7D0168
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529.6364 - Fax: [phone] Page 8 of 15

Labor ®
R �-
6`v=
�'
y ,n n Full -Service Analytical & �] I
environmental Solutions
_
' • -
04/24/2017
IABORATORIE$ ING
City of Statesville, NC
Project: Stal-ime (Qtrly, Biweekly,
Client Sample ID: Fecal #7
Attn: Andy Smith
60Day 7 Fecal)
Prism Sample ID: 7040188-07
P.O. Box 1111
Prism Work Order: 7040188
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/10/17 11:15
Time Submitted: 04/10/17 13:05
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
Solids
74.2 % by
0.100 0.100
1 'SM2540 G 4/12/17 16:07 JLB
P7D0208
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E ' 4/11/17 9i16 ' BMS'
P7l]01fi8'
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 15

.P Level II QC Report
1?1R I C I� /I FnService Analytical 4/24/17
V ��/� Environmental Solutions
' �LABORATORIE$ ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 7040188
Attn: Andy Smith 7 Fecal) Time Submitted: 4/10/2017 1:05:00PM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P7D0179 - SAR 2-78-054
Blank (P7D0179-BLK1)
Prepared: 04/12/17 Analyzed: 04/13/17
SAR Soil Preparation
Complete
g
Batch 137D0203 - 3050B
Blank (137D0203-BLK1)
Prepared: 04/13/17 Analyzed: 04/14/17
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P7D0203-BSI)
Prepared: 04/13/17 Analyzed: 04/14/17
Arsenic
22.4
0.25
mg/kg wet
25.00 90 80-120
Cadmium
21.7
0.25
mg/kg wet
25.00 87 80-120
Copper
25.1
0.50
mg/kg wet
25.00 100 80-120
Lead
21.9
0.25
mg/kg wet
25.00 88 80-120
Nickel
22.5
0.50
mg/kg wet
25.00 90 80-120
Potassium
482
12
mg/kg wet
500.0 96 80-120
Selenium
21.7
0.50
mg/kg wet
25.00 87 80-120
Sodium
499
15
mg/kg wet
500.0 100 80-120
Zinc
22.6
2.5
mg/kg wet
25.00 90 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-3001529-6364 - Fax: [phone] Page 10 of 15

PI S n n Fun -Service Analytical
_ ' V' I Environmental Solutions
L BORNTORIM ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P7DO209 - 3010A
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II .QC .Report° - ;
4/24117
Prism Work Order: 7040188
Time Submitted: 4/10/2017 1:05:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P7D0209-BLK1)
Prepared: 04/13/17 Analyzed: 04/17/17
Sodium Absorption Ratio
BRL
3.0
[blank]
Calcium
BRL
1.0
mg/L
ti='
Magnesium
BRL
1.0
mg/L
Sodium
BRL
5.0
mg/L
BH
Batch P7130230 - 7471 B
Blank (P7DO230-BLK1)
Prepared &Analyzed: 04/17/17
Mercury
BRL
0.020
mg/kg wet
LCS (P71DO230-13W)
Prepared &Analyzed: 04/17/17
Mercury
0.396
0.020
mg/kg wet
0.4167 95 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 15

Level II QC Report
I n Full -Service Analytical 8 4/24/17
'v' Environmental Solutions
LABORATORIES, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P7D0152 - 351.2
Project: StaLime (Qtrly, Biweekly, 60Day Prism Work Order: 7040188
7 Fecal) Time Submitted: 4/10/2017 1:05:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P7D0152-BLK1) Prepared: 04/11/17 Analyzed: 04/18/17
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P7D0152-BS1) Prepared: 04/11/17 Analyzed: 04/18/17
Total Kjeldahl Nitrogen 478 100 mg/kg wet 500.0 96 90-110
Batch P7DO197 - NO PREP
Blank (P7D0197-BLK1) Prepared: 04/13/17 Analyzed: 04/17/17
Ammonia as N BRL 5.0 mg/kg wet
LCS (P7D0197-BSI) Prepared: 04/13/17 Analyzed: 04/17/17
Ammonia as N 123 5.0 mg/kg wet 125.0 98 80-120
Matrix Spike (P7D0197-MS1) Source: 7040188-01 Prepared: 04/43/17 Analyzed: 04/17/17
Ammonia as N 249 32 mg/kg dry 159.9 106 90 80-120
Matrix Spike Dup (P7D0197-MSD1) Source: 7040188-01 Prepared: 04/13/17 Analyzed: 04/17/17
Ammonia as N 253 32 mglkg dry 159.9 106 92 80-120 1 20
Batch P7130233 - NO
Blank (P7D0233-BLK1) Prepared & Analyzed: 04/17/17
Nitrate/Nitrite as N BRL 5.0 mglkg wet
LCS (P7D0233-BS1) Prepared &Analyzed: 04/17/17
Nitrate/Nitrite as N 47.0 5.0 mg/kg wet 50.00 94 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 15�

>' Level II;C2C .ReRo,rt "u
}PRISIi�I
Full -Service Analytical& ''" 4/24117•"•-'`
Environmental Solutions
' LAaeNATeflIES INF
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 7040188
Attn: Andy Smith 7 Fecal) Time Submitted: 4/10/2017 1:05:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P7DO233 - NO PREP
Matrix Spike (P7D0233-MS1)
Source: 7040188-01
Prepared & Analyzed: 04/17/17
Nitrate/Nitrite as N
89.6 6.4 mg/kg dry
63.95 34.6 86 80-120
Matrix Spike Dup (P7D0233-MSD1)
Source: 7040188-01
Prepared & Analyzed: 04/17/17
Nitrate/Nitrite as N
89.5 6.4 mg/kg dry
63.95 34.6 86 80-120 0.07 20
Batch P7DO263 - SM4500-PB5
Blank (P7DO263-BLKI)
Prepared: 04/18/17 Analyzed: 04/19/17
Phosphorus -Total
BRL 2.5 mg/kg wet
LCS (P7DO263-BSI)
Prepared: 04/18/17 Analyzed: 04/19/17
Phosphorus -Total
96.4 2.5 mg/kg wet
100.0 96 90-110
Matrix Spike (P7D0263-MS1)
Source: 7040188-01
Prepared: 04/18/17 Analyzed: 04/19/17
Phosphorus -Total
92.1 3.2 mg/kg dry
127.9 294 NR 80-120 MI
Matrix Spike Dup (P7D0263-MSD1)
Source: 7040188-01
Prepared: 04/18/17 Analyzed: 04/19/17
Phosphorus -Total
92.7 3.2 mg/kg dry
127.9 294 NR 80-120 0.7 20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 15

'
Level II QC Report
n I S n
Full -Service Analytical
&
4/24/17
r. J IV'
Environmental Solutions
':, LAaO-RIER, ING
City of Statesville, NC
Project: StaLime (Qtrly, Biweekly, 60Day Prism Work Order: 7040188
Attn: Andy Smith
7 Fecal)
Time Submitted: 4/10/2017 1:05:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit Units
Level Result %REC Limits RPD Limit Notes
Batch P7DO168 - NO PREP
Blank (P7DO168-BLK1)
Prepared & Analyzed: 04/11/17
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0152
0.05 g
25 mL
04/11/17 10:55
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0263
1 g
50 mL
04/18/17 10:20
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0208
30 g
30 g
04/12/17 16:07
7040188-02
P7D0208
30 g
30 g
04/12/17 16:07
7040188-03
P7D0208
30 g
30 g
04/12/17 16:07
7040188-04
P7D0208
30 g
30 g
04/12/17 16:07
7040188-05
P7D0208
30 g
30 g
04/12/17 16:07
7040188-06
P7D0208
30 g
30 g
04/12/17 16:07
7040188-07
P7D0208
30 g
30 g
04/12/17 16:07
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0209
50 mL
50 mL
04/13/17 11:00
7040188-01
P7D0209
50 mL
50 mL
04/13/17 11:00
7040188-01
P7D0209
50 mL
50 mL
04/13/17 11:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0203
2.01 g
50 mL
04/13/17 8:35
7040188-01
P7D0203
2.01 g
50 mL
04/13/17 8:35
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0230
0.56 g
50 mL
04/17/17 9:05
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Daterrime
7040188-01
P7D0179
250 g
250 g
04/12/17 9:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 15

Full -Service Analytical Y
A Environmental Solutions
._. . ... I_AEOR.ATORIES. INC.
449 Sprinrgbrook Road • Charlotte, NC 28217
T'hone 704/529-6364 Fax: [phone]
Client Company Nance: y 9 tat:S b t�61 G
Report To/Contact Nance:_
Reporting Address:
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PAGE_ OF _ QUOTE # TO ENSURE PROPER SELLING.
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*Please ATTACH any project specific reporting (QC LEVEL 111 III IV)
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SLUDGE)
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