WQ0006245_Regional Office Historical File Pre 2018 (2)

PO Box 1111 • 'Statesville, NC 28687 _• ci.statesville.nc.us�

f.
A9CEIVEMCDEPIROWR
CITY of
FEB 19 2020
QltTH-bAR6tINA, 1NQROS
MOORESVILLE REGIONAL QFFICE
January 23, 2020 _ itnL,L IV11/NCDEQ/DW •
Y .JAN 3 i 2020
Attention: TroyDob Non -Discharge
y Permitting Unit
NCDWR
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1636
RE: Annual Reports for 2019
Third Creek Monofil (WQ0004040)
Dear Mr. Hardee:
Enclosed, you will find a copy of the required forms and lab data for the Third Creek Monofil.
Permit # WQ0004040. This monofil is currently closed -and not_ being used.for bio-solids disposal.
This permit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 704- 878-3438.
Sincerely,
Ken a loway
WWTP Supervisor, Fourth Creek WWTP
PO Box 1111 Statesville, NC 28687 ci.statesville.nc.us ���

r-
GENERAL INFORMATION
BIOSOLIDS REPORT
CALENDER YEAR 2019
THIRD CREEK MONOFILL
PERMIT NO. WQ0004040
FACILITY NAME: Third Creek WWTP-NPDES NCO020591
LOCATION: 444 Third Creek Road
MAILING ADDRESS: P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Water Resources
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Scott Austin
Plant Supervisor
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC Ken Galloway
Residuals Supervisor
P. O. Box 1111
Statesville, NC 28687-1111
[phone]
APPLICATION: Surface disposal unit.
This unit was not used for biosolids
disposal in 2019, and has completed
closure activities. The permit is
maintained for well sampling and
reporting.

Management Practices Description
Third Creek WWTP Sludge Monofill (Surface Disposal Unit)
NPDES No. NCO020591
40 CFR 503.24
Non -Discharge Permit WQ0004040
THREATENED OR ENDANGERED SPECIES: No known threatened or endangered species
occupy or frequent the disposal site.
BASE FLOOD FLOW RESTRICTION: The site is located above the flood plain.
LOCATION OF GEOLOGICAL STABLE AREA: Soil consists of tight red clay on high ground
and the site has had no history of movement or shifting due to saturation with rainwater or
seismic conditions. No known faults exist in the area.
WETLANDS LOCATION: Not a wetland location.
RUNOFF COLLECTION: Trenches are constructed as to prevent disposed material from exiting
as a part of any runoff. Berming and swales are constructed to contain erosion. Finished trenches
are domed with clean earth to allow shedding of water out and away from filled trenches. A
"green belt" is maintained and encouraged to grow around the entire area.
LEACHATE COLLECTION: As a liner is not used, leachate collection is not required.
METHANE GAS MEASUREMENTS: Periodic checks of air with electronic air monitors reveal
that methane is not escaping the surface disposal area.
CROP PROHIBITION: Crops are not grown on the site.
GRAZING PROHIBITION: Grazing is not permitted on the site.
PUBLIC ACCESS RESTRICTED: Chain link fencing encloses the site property. NO
TRESPASSING signs are posted.
AQUIFER CONTAMINATION: Monitoring well samples for this calendar year show no danger
of aquifer contamination.
No disposal activities occurred in 2019.

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: 4040 FACILITY NAME:
PHONE:[phone] COUNTY:
FACILITY TYPE (please check one):
0
Third Creek WWTP Monofill
Iredell OPERATOR:. Ken Galloway
Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes E7 No 21 If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
NO RESIDUALS
DISPOSED
OF IN
PERMITTED
UNIT IN 2019
August
September
October
November
December
Total from FORM DMSDF (sup)
....................
Totals:
Annual (d tons):
0
0
0
0 ,
Amendments used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: 0 No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
l
Date Signature of Preparer*
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
/--z 3- ZO
Date `
nGniQ Gnann nwznr ra)i,)innnN

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0004040 _ Laboratory:
Facility Name: Third Creek WWTP Monofill
Residual Source WQ # or NCO020591
NPDES #:
WWTP Name:
Recidiinl Analvcic Data
1) Prism Labs
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
Percent Solids (%)
NA
Arsenic
75
Cadmium
85
Copper
4,300
Chromium
NA
Lead
840
Mercury
57
Molybdenum
75
Nickel
420
No
Residual.,
disposed.
of in
permitted
Selenium
100
unit
2019
Zinc
7,500
Total Phosphorus
NA
TKN
NA
Ammonia -Nitrogen
NA
Nitrate and Nitrite
NA
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitti alse information, including the possibility of fines and imprisonment for knowing violations."
Sianature of Pre`varer *
i-a3 Zo
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
IIFNR FnRM RSSF f1717(1[1Fil

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Third Creek WWTP Monofill
WQ Permit Number: WQ0004040
WWTP Name: Third Creek WWTP NPDES Number:
Monitoring Period: From 1 /1 /2019 To 12/31 /2019
athogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
NCO020591
Class A:
Altemative 1 CAI
Alternative 2 C!
Alternative 3 El
Alternative Q(
u Alterative 5 D
� Alternative 6 0
If applicable to alternative. erfonned C7assA
onl fnclfcate `iProcess to Farther
ReducePatho eas"c
Compost 01
Heat D _
Heat Treatment 0
TI]eirlt®. hilie (�
:.;::;:_:.>:.;:.:.:
Beta Ray 11
G1amfl'la Ray
Pa murization (
>
Class B:
Altemative 10-
Alternative 2: CI
: >:: ;» :::<
If applicable to alternative performt4 (C'Iass 10
onl y indicate "Process to Sf nificapdy
Reduce Pathogens":
Lime Stabilization ' C.1 Air 2ryirrg1l
Composting, D
'Aerobie digestion U
Anaerobic Digestion estion CI
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Anal y
Sample
Type
Analytical
Tech -
ni ue
Minimu
Geo. Mean
Maximumsis
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
No
Residuals
disposed
of in
permitted
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight) ,
unit
@
2019
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
CI
Alt. 2 (40-day bench)
C1
Alt. 3 (30-day bench) U
Alt. 4 (Spec. OZ uptake)
Ll
Alt. 5 (14-Day Aerobic)
[I
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) 0
Alt. 8 (Drying - Unstable)
Cl
Alt. 9 (Injection)
D
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed
D
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
Ej "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
4,2 k/tV/2L0 !&�ry�sar'
Preparer Name and Title (type or print
Land Applier Name and Title (if applicable)(type or print)
ig ure o reparer Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

CITY of. ..:
,- - � I�IOlt,TIi . Cd.ROLIl�ih
4th CREEK And CREEK'WWTP SLUL70E AWRAME
Ken Galloway..
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester and_dewatered
using•a belt press. After dewafering, the residuals are transferred to the StaLime lime stabilization .
process area where the biosolids are set aside for contract.land application away from the plant site.
The contractor is Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids
disposal is the StaLime process and that permit # is WQ0006245.
PO Box 1111 ® Statesville, NC 286.87 ci.statesville.nc.us

CITY ofq¢���
January 23, 2020
JAN ' 3 1 2020
!Non -Discharge
ermltiir Unit'. -
Attention: Troy Doby
NCD W R
Water Quality Non -Discharge Permitting Unit
1617 Mail Service Center'
Raleigh, North Carolina27699-1636 - -
RE: Annual Report for 2019
City of Statesville Land Application (WQ0014543)
Dear Mr. Doby:
Enclosed; you will find a copy of the required forms and lab data for the City.of Statesville Land
Application, permit #WQ0014543. This land application program has never been utilized. However, the
City of Statesville wishes to keep this permit active in case of an emergency.
This permit was compliant for the year.
Should you require more information, or if further action is required, please contact me at 7047 878-3438.
Sincerely,
K oway
WWTP Supervisor, Fourth Creek WWTP . .
PO Box 1111 t Statesville, NC 286.87 ci.statesville.nc.us

GENERAL INFORMATION
LAND APPLICATION
CALENDAR YEAR 2019
Permit No. WQ0014543
FACILITY NAME: Fourth Creek WWTP-NPDES NCO031836
Third Creek WWTP- NPDES NCO020591
LOCATION: 693 Bell Farm Rd.
444 Third Creek Rd.
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-11 l 1
[phone]
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Dept. of Water Resources
P.O.Box IIII
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Ken Galloway
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Ken Galloway
P.O.Box I I I I
Statesville, NC 28687-1111
[phone]
APPLICATION: Land Application
No Residuals land applied in 2019.

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014543 County:
Facility Name (as shown on permit):
Iredell
Year: 2019
Fourth Creek WWTP
Land Application Operator: Ken Galloway Phone: [phone]
ind application of residuals as allowed by the permit occurred during the past calendar year?
A Yes 21 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Is
Total number of application fields in thepermit:
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2019 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ® Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
.i) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates. in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
;rmittee Name and Titer (type or print)
17I
Signature of Permittee
2 ,,�- 20
Date Signature of Land Applier
Date
Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

CITY of Air
I$C31tT CAA3,Nti
46) CREE f i Ad CREED WWTP SLUDGE Wslam'.. .
Ken -Galloway -
Both WWTP's generate biosolids that are currently stabilized using an aerobic digester and dewatered
using -a belt press. After dewatering, the residuals are transferred to the StaLime lime stabilization
process area where the biosolids are set aside for contract. land application away from the plant site. The contractor is Synagro and they hold permit # WQ0016247 for this. The primary method of biosolids
disposal is the StaLime process and that permit # is WQ0006245.
PO Box 1111 Stot sAlle, NC 28687 • ci.statesville.nc.us

i
KQR,TH : 'CA3!OLINA

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2019
PERMIT NO. WQ0006245
FACILITY NAME: Fourth Creek WWTP NPDES NCO031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality. Product
Test Data and Summary Operations
Attached

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0006245 FACILITY NAME:
Fourth Creek Alkaline Stabilization
PHONE: [phone] COUNTY: Iredell OPERATOR: Ray Wyrick
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In Volume only) and Part C)
I Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes i--, 12 No 0 ---► If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/ Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
4th Creek WWTP
87.98
126.35
214.33
0
February
NPDES# NCO031836
163.21
213.81
377.02
0
March
4th Creek WWTP
0
0
0
Various Farmers
286.2
Farmland
April
NPDES# NCO031836
0
0
0
Various Farmers
13.6
Farm / Landscape
May
4th Creek WWTP
244.76
435.33
680.09
Various Farmers
90.1
Farmland
June
NPDES# NCO031836
0
0
0
Various Farmers
110.5
Farm / Landscape
July
4th Creek WWTP
0
0
0
Various Farmers
25.5
Farmland
August
NPDES# NCO031836
0
0
0
Various Farmers
10.2
Farmland
September
4th Creek WWTP
0
0
0
Various Farmers
341.7
Farm / Landscape
October
NPDES#NCO031836
0
0
0
Various Farmers
144.5
Landscaping
November
4th Creek WWTP
86.95
128.16
215.11
0
December
NPDES# NCO031836
0
0
0
Various Farmers
76.5
Farmland
Total from FORM DMSDF (sup)
0
0
0
0
....................
Totals:
Annual (dry tons):
582.9
903.65
1486.55
1098.8
Amendments used: I Bulkin A ent s used: Lime Kiln Dust
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C
Facility was compliant during the past calendar year with all conditions of the land application permit fl Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: fl No 0- If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. '
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee Date Si re of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMP11-DING SUMMARY FORM= .,.. .
Please note that your permit may contain additional parameters to be analyzed. The parameters can be rep orted_in FORM RSSF - B ;
WQ Permit Number: WQ0006245
Facility Name:
Residual Source WQ # or
Fourth Creek WWTP
NPDES #: NPDES-# NCO031836
WWTP Name:
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
Prism Labs
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
1/03/19
5/22/19
3rd
Quarter
11/25/19
Percent Solids (%)
NA-
71.40%
72%
N
66%
Arsenic
75
<7
4.2
O
13
Cadmium
85
<3.5
<0.70.
N
<0.75
Copper
4,300
33
300
E
54
Chromium
NA
N/A
N/A
N/A
Lead
840
8.5
<1.4
P
9
Mercury
57
0.06
<0.070
R
0.095
Molybdenum
75
N/A
N/A
O
N/A
Nickel
420
9.6
37
C
15
Selenium
100
7.9
12
E
27-
Zinc
7,500
49
<14
S
100
Total Phosphorus
NA
2,300
3,100
S
4,300
TKN
NN
<3500
5,000
E
4,000
Ammonia -Nitrogen
NA
300
210
D,
120
Nitrate and Nitrite
NA
<7
<7
9.3
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed.
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization
WWTP Name: Fourth Creek WWTP
WQ0006245
NCO031836
Monitoring Period: From 1/1/2019 ::. To . 12/31/2019
athogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
WQ Permit Number:
NPDES Number:
Class A: .:
Alta A (time/thin .) 11 :
Alt B: (Alk Treatment) Ri.
Alt. C: (Nor Tosliu ) l
AILD (No Pribr Test) Q
Process to Further Deduce Pathe ens 0
If applicable to alternative erformed C`last:
onW indicate "Process to )Further Reduce Path ens":
Compost 0
Ho in 13,
Meat Treatment C�l Tham2 hilic [
4,
::'::::.::: :
Beta Ray D'
Gamma Ray 0'
Pasteurization CT
Alt: 1) Feel Densi E
Alt, (2) Process to Si i�cantl RWtice-Patho ens 0
Class B:
If applicable to alternative.performed
(Class B
do indicate "Process to Sl lllcantM Reduce Pathv ens"r
Lime Stabilization G� _ Air in Q..
1 Coen ostin (
Aerobic Di estion D
Anaerobic Digestion s _
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Ex Number o
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical -
Tech -
ni ue
Minimu
Geo. Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<0.2
<0.3
mpn/g
Quarterly
grab
sm9221 e
cFU
1000 mpn per gram
of total solid (dry
weight)
salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
%nn+nr Attrantinn Radnrtinn !1 SA NCAC
02T _11671 - Please indicate alternative performed:
Alt.l (VS reduction) El:
Alt. 2 (40-day bench) [l
Alt. 3 (30-day bench) ED
I Alt. 4 (Spec. OZ uptake) RJ
Alt. 5 (14-Day Aerobic) [3,
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) C7
JAIL 8 (Drying - Unstable) l
Alt. 9 (Injection) [I
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name
Land Applier Name and Title (if applicable)(type or print)
96)
2 Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

'City Of Statesville Alkaline Stabilization Record For.
Process To Further, Reduce Pathogens (PFRP)
Bl N ## I
Setup Date: 1- a 1?- 1 q
Removal From Bin Date: 1-31- I q
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
i-le- 1q
09''30
InitialpH: 1,2,5q
1-dS-Iq
93°@ 3: a0
1-aq- iq
12°@07;o5
1?4ln)
Corrected pH: 1 ;2,7
I - 31-1.7
14 rn
FinalpH: 12.5 8
1-3 I -1 q
'7 3 ° @ It A m
�
Corrected pH: id, 7 a
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? ® N
BIN # a'
Setup Date: /-a q-3
Removal From Bin Date: a-1-19
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1-,Z9-19
►I� 0-0
Initial pH: 12, d 3
1- 2 4- 19
45°@ Il MlWe-09.,00
1- 3 0- 1 9
Corrected pH: 1.7. $3
x-1- 19
wqs,Final
'q
pH: 1.2 , d �l
I
II
Rk w
Corrected pH: 1.1, !? q
Has 12 Hour Temp Criteria
Been Met? OY N
Has 72'Hour.pH Criteria Been Met? Y N
BIN # 7 8
Setup Date:. 1-30 - I q
Removal From Bin Date: a- 19
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1-30-19
o9:3y
Initial pH: 1.7.59
1-3o-Iq
qI� @ 1a. 0@
31- 1q
Tis 071rJ 1
R4U)
Corrected pH: 1,2.,7 9
,� _ y• I q
q
10 r,-I
Final pH: 1,2 5 `I
d-`1-1 q A
68 °Ca 10 ; Is 'n
Corrected.pH: /,2, 9 3
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN # 5"
Setup Date: 1-31-19
Removal From Bin Date: 1-5- 1q
Date
Time
pH >12:0 For.72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1-31- 19
09.30
Initial pH: 1a. 61
1-31- 19
q0 e IV 36
1x- 1- +9
Ord @ OW59
RkW
Corrected pH: 1,2.7 g
d-�- 19
101'i %rn
final pH: ! a, 5
2 -v- j q
S3' & 10 15 m
Corrected pH: 1 � ,
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN # ul
Setup Date:
Removal .From Bin Date:
Date
Time
pH >12.01=or 72 HrS.
1tM*1P. >52 Deg. C F& 12 Hrs:
Operator
a _ 1-19
09: 3 0
InitialpH: 1d.51
2-1-19
0 0-12.p ),,
d-y-14
GO °' 0 7: 3
Rol W
Corrected pH: 12.71 -
A
final pH: Id , 50
R1,
Corrected pH: 1,2, 63
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour .p". Criteria Been Met? UY N

City of Statesville Alkaline Stabilization Record For.
Process To Further,Reduce Pathogens (PFRP)
BIN # `P ' 13
Setup Date: Z- is-1 q
Removal From Bin Date: I-
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
a- i 8-19
I®• `�' rn
Initial pH: lJ. 50
�}0� 11.11 A
Sq @ 0T.Y1
P4L.a
Corrected pH: /�,
a 1- 19
ll: 30"I
Final pH: 12- 93
_ l-
I Iq
T..5'& 09:40 I
•n� vi o T�
hvc^ro v ao
Rol W.
Corrected pH:
Has 12 Hour Temp Criteria Been Met.) Y N
Has. 72 Hour pH Criteria Been Met? Y N
BIN # /
Setup Date: 1- /9-1
Removal From Bin Date: g-
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
.t-1 q- 1 Q
ll:.l d-
Initial pH: 12. 51
A- rq-' I q
$0'Ca 11: �0 �,
a- lo- IQ
RR W
Corrected pH: 12,'75
12;5fl
I �.59�R-fix-19
7f&&10;15�,
[FRinrrectealpf-1:
ilpH: IZ,73
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 'Hour.pH Criteria Been Met? Y N
BIN # 34-S
Setup Date:.?-.t0-/ 9
Removal From Bin Date: ,Z-•?5-99
Date
Time
I pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
2-zo-11
// C7
Initial pH: /.?. 9 S
A- A l-1 9
90'CV 0V90
ISo E' 07: /5
RkW
lCorrected pH: /Q. 98
.2 -.2s--19
11' 5()
Final pH: /;44
A-55-19
'15a CO 07;15
JU LV
Corrected.pH: l a. 7 ri
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN # 1/ t (
ISetup Date: A-,?/- 19
Removal From Bin Date;
Date
Time
pH >12.0 For.72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
-,11-1 al
09' H p
Initial pH: 12. 51
0 * '! 0 • e
A- A I. I q
D906& 07:3 o
Rl,W
Corrected pH: 12.71
Z 25-11
/2%..5s
Final pH:
9�Y s�o ��,�
k9 u�'
Corrected pH: 1 $' �
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
BIN # 1 4' ,Z
Setup Date: I- a a-19
Removal .From Bin Date:
Date
Time
pH >12.0 For 72 Hrs'.
TEIYIP. >52Deg. C For 12 Hrs. `
Operator
14 P`'�
Initial pH: 1.7.S7
A-1i-19
1140 @ 101 A0
-�i-aq
76-'& j7:ap
A M/
Corrected pH: U.7%
Final pH: /,,1. 5 8
n4r,r°
Corrected pH: 1.7.73
Has 12 Hour Tern.p Criteria Been Met? Y N
Has 72 Hour :pH. Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further'Reduce Pathogens (PFRP)
BIN #
Setup Date: S - t- I q
Removal From Bin Date: •S 13- / q
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
S-0-19
4
Initial pH: /a. 6a
s- -19
Wg3A 9a
s 9-1q_
0`:17 96"
RA W
Corrected pH:1�.8�
S-13-09
i0:50A
Final pH: U. 5 8
10:J9 90
94La-
CorrectedpN:1,7:78
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Beer! met? Y N
BIN # 3 e5
Setup Date: S q- I q
Removal From Bin Date: 5-13-I9
Date
Time
pki >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5- 4- I q
11: 0'1 A
Initial pH: 1.1. 57
S 9- 14
900
to. I q
07, 30 90 °
RkW
Corrected pN: 12. 17 111A
5-13-i q
Final pH: J;7, eel
s' t 3 - q 9
1®:3` A -70
R/, W
Corrected pH: If. Sr/
Has 12 Hour Tennp Criteria
Been Met? Y N
Has 72 *Hour.pH Criteria Been Met? VN N
BIN # 7V#8
Setup Date:.5-10- 19
Removal From Bin Date: 5-1g- 19
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
S-lo- i 9
Il: 09 A
Initial pH: /a, 55
S- Is- I q
11: 10 A Qp°
5-11-19
oS,'00 61 q
.
R4 W
Corrected pH: /,7. 75
S-13•-19
111149014
Final pH: /J. 5.2
10 ::)j A -70 *
Corrected.pH: 1 a,'7a
Has 12 Hour Ternp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date: 5- i3-19
Removal From Bin Date: .S'-16- 19
Date
Time
pH >12:0 For.72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
s-i3-19
I®:3SA
Initial pH: f.7 S;j
5.-13- 1 q
Id:36A 10*
5- N- i 9
07:32 * 90 °
RRW
Corrected pH: 1.J.7.?
5 rE-I9
II NSA
Final pH: /,,7 , C.1
W
Corrected pH: /,7. Sa
Has 12 Hour Temp Criteria Been Met? N
Y N
Has 72 Hour pH Criteria Been Met? Vj
BIN # 3 � $
Setup Date: S- q_ #9
Removal .From Bin Date: 5-17
-1
Date
-Time
pH ?12.0 FOP 72 Hrs.
TEMP. >52"Deg. C Fot 11 Hrs: `
Operator
S-Iw-19
1i:o0A
Initial pH: J,2, Co
5-1 N-.r 9
HA goo
S- I�_ 1 j
o,?;do 65°
Corrected pi-11a,907.
5 /7-19
14:15 P
Final pH: /.Z.
4 7:15 900
Corrected pH: /d, 59
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 H®ur pH. Criteria Been Met? Y N

�y
City Of Statesville Alkaline Stabilization Record For.
Process To Further -Reduce Pathogens (PFRP)
Biel # 1-4
r
Setup pate:.- / 5'-1 q
Removal From Bin Date:., - 2 a -19
Date
Time I
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
P
Initial pH: 14, 5-7
W30 �0°
Y-1G- 1q ,
07:15 90°
RICw
Corrected pH: 1a.7q
"�0 - q
0 �' `�
Final pH: 1�• j�. q,
R4 w -
Corrected pH: 1 j , j 8
Has 12 Hour Ternp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? Y N
BIN## lea
Setup Date:., -16-1q
Removal From Bin Date: 6-as-.19
Date
Time
pH >12.0 For 72 Hrs..
TEMP. >52 Deg. C For 12 Hrs.
Operator
34d- V4
11A
Initial pH: l.?.5%
09.'3o 9T*
0 : r$ 10®
Corrected pH: 12.7d
S d0 -19
09: a 7
Final pH: 12. 43
�z 1✓
Corrected pH: 1;?.d3
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 'Hour.pH Criteria Been Met? Y N
BIN # VS
Setup Date:.S-111-0
Removal From Bin Date: 5w-.R0- 1 q
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
S-17- jq
10A
Initial pH: 1a.53
5-17-1 q
09: 15 95 a
5- Xo - ! q
0°1:50 90°
R1,w
orrected pH: U.73
3*-20 -19
®q. � g
nal pH: 1,1, q3
r
R L `,
orrected.pH: #j , (, 3
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN ##3 ,5—
Setup Date: S, ;t 0 -1 q
Removal From Bin Date; 5- A 3 , 1
Date
Time
pH >12.0 For.72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
5-a0-19
09: 3 0
Initial pH: 12.5 3
Og4l- 749
ij;ga 1?5 °
k4bV
Corrected pH: /�. 773.
Final pH: `,) ,y 9
W1
Corrected pH: C 7
Has 12 Hour Temp Criteria Been Met?
Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
-pH k2.0 For 72 Hrs.
TEMP. >52 Deg.
C For 12 Hrs...
Operator
initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Ternp Criteria Been Met? Y N
Has 72 Hoag pH. Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # ► o2
Setup Date: 11_14_ Iq
Removal From Bin Date: 11-22-i 9
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
I1•i4-19
ils 3t1'n
Initial pH: 1,2. 53
`Jo° to:43,n
`70' 07: 19
Rkw
Corrected pH: 1.7,6'7
11.22-19
11:4.0M
Final pH: I;Z.qd
Rl,w
Corrected pH: 1,2. 40
- Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? �Y) N
BIN # 3 4.5
Setup Date: ►l-ao- lq
Removal From Bin Date: II-j5.19
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
il-do'1�
11*03
Initial pH: /J. Sq
w a7- Iq
19'3 U.03� '
it-12 I- III
17° 07:d7
JUW
Corrected pH: U.70
i1-a5-19
n
11�30�
Final pH:
Raw
CorrectedpH:/�.ty/
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN # 7
-'' 8
Setup Date: .)1-.j1-1 q
Removal From Bin Date: 11- 4 `-) 9
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
i1•a1-19
a
IlY�sry,
Initial pH: ►j.5.3
11-a1- 1q
�� ° i1 as An
it-;ta-1q
0$; 10
P��
Corrected pH: Id• 641
.4
3BM
Final pH: id.`1 q
RJLW
Corrected pH: 12.55
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:.
Has 12 Hour Temp Criteria Been Met? Y N
Has 72 Hour pH Criteria Been Met? Y N

` NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 ism I Environmental Solutions SC Certification No. 99012 5/8/19 10:16
LABORATORIES, ING
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 01/03/2019
Prism Work Order: 9010010
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised laboratory report date / 11/19 AN Equation has
been added to Case Narrative.
Analysis note for SAR:
SAR =[Na]/SQRT(([Ca]+[Mg])/2)
3AR = [ 130/23.0 ] / SORT (([1300/20,0] * [0,025/12,2]) / 2 )
SAR = 1.0
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SORT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) +
Nitrate -Nitrite
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
PAN Equation = 0.3 * (1750 - 300) + 0.5 * (300) + 3.5
PAN = <1100 mg/kg
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 17

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
DM Sample diluted and RL increased due to the matrix.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364-Fax:[phone] Page 2 of 17

,.�
J 1 Full -Service Analytical &
�n
!� R I S I V I I Environmental Solutions
KZ"A Amnmra ING
Sample Receipt Summary
05/08/2019
Prism Work Order: 9010010
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
Stal-ime (and Fecal 1)
9010010-01
Solid
01/02/19 11:00 01/03/19 8:00
Fecal #2
9010010-02
Solid
01/02/19 11:00 01/03/19 8:00
Fecal #3
9010010-03
Solid
01/02/19 11:00 01/03/19 8:00
Fecal #4
9010010-04
Solid
01/02/19 11:00 01/03/19 8:00
Fecal #5
9010010-05
Solid
01/02/19 11:00 01/03/19 8:00
Fecal #6
9010010-06
Solid
01/02/19 11:00 01/03/19 8:00
Fecal #7
9010010-07
Solid
01/02/19 11:00 01/03/19 8:00
Samples were received at 22.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 17

Laboratory Report
F' Full -Service Analytical &
PP1.:l Is M I Environmental Solutions 05/08/2019
%UIHORATOeIE$ ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: StaLime (and Fecal 1)
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 9010010-01
P.O. Box 1111 Prism Work Order: 9010010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
Plant Available Nitrogen
BRL
mg/kg dry
1100
310
5
*Calculation
117/19 10:48
CLB
[CALC]
% Solids
71.4
% by
0.100
0.100
1
*SM2540 G
1/8119 14:30
TJY
P9A0141
Weight
Ammonia as N
300
mglkg dry
13
3.3
1
*SM4500-NH3 C
117119 10:48
BMS
P9A0089
Nitrate/Nitrite as N
BRL
mg/kg dry
7.0
1.9
1
*SM4500-NO3 F
1/3/19 11:17
CLB
P9A0038
Phosphorus -Total
2300
mg/kg dry
70
16
20
*SM4500-P F
1/7/19 9:33
CLB
P9A0057
Total Kieldahl Nitrogen
BRL
mg/kg dry
3500
1000
5
*351.2
1/4/19 9:01
CLB
P9A0037
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
1/3/19 9:00
BMS
P9A0065
Total Metals
Mercury
0.060
mg/kg dry
0.028
0.0027
1
*7471B
117/19 12:37
MMR
P9A0078
SAR Soil Preparation
Complete
g
1
*2-78-054
1/7/19 8:30
MMR
P9A0046
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
1/7/19 8:30
MMR
P9A0075
Weight
Arsenic
BRLDM
mg/kg dry
7.0
0.43
10
*6010D
117/19 16:37
JAB
P9A0055
odium Absorption Ratio
1.0
[blank]
0.30
0.016
1
*2-78-054
1/8/19 10:59
JAB
P9A0056
admium
BRLDM
mg/kg dry
3.5
0.094
10
*6010D
1/7/19 16:37
JAB
P9A0055
Calcium, SAR
.1300
mg/L
10
1.0
100
*6010D
114119 17:16
JAB
P9A0056
Copper
33
mg/kg dry
7.0
0.63
10
*6010D
117/19 16:37
JAB
P9A0055
Lead
8.5
mg/kg dry
3.6
0.65
10
*6010D
1/7119 16:37
JAB
P9A0055
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
1/4/19 17:24
JAB
P9A0056
Nickel
9.6
mg/kg dry
7.0
0.25
10
*6010D
1/7/19 16:37
JAB
P9A0055
Potassium
1900 BH
mg/kg dry
180
6.3
10
*6010D
117119 16:37
JAB
P9A0055
Selenium
7.9
mg/kg dry
7.0
1.7
10
*6010D
117/19 16:37
JAB
P9A0055
Sodium
1100
mg/kg dry
210
6.9
10
*6010D
1l7/19 16:37
JAB
P9A0055
Sodium, SAR
130 BH, B
mg/L
50
1.8
100
*6010D
1/8119 13:64
JAB
P9A0056
Zinc
49
mglkg dry
35
1.3
10
*6010D
117119 16:37
JAB
P9A0055
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 17

�9` r�R, Full -Service Analytical &
LJP R I S M Environmental Solutions
�7L. CB TONIEr, INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/08/2019
Client Sample ID: Fecal #2
Prism Sample ID: 9010010-02
Prism Work Order: 9010010
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 72.0
% by
0.100
0.100 1
*SM2540 G 1/8119 14:30 TJY
P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 113/19 9:00 BMS
P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
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Laboratory Report
Full -Service Analytical &
/�_41
I S Evironmental Solutions 05/08/2019
7LABOR MRIE$ ING
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #3
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 9010010-03
P.O. Box 1111 Prism Work Order: 9010010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 70.2
% by
0.100
0.100 1
*SM2540 G 118/19 14:30 TJY
P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 1/3/19 9:00 BMS
P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 17

' t Full-Service Analytical &
I S M Environmental Solutions
LABORATORIES ING
Laboratory Report
05/08/2019
Jty of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #4
, ttn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 9010010-04
P.O. Box 1111 Prism Work Order: 9010010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 72.0 % by 0.100 0.100 1 *SM2540 G 118119 14:30 TJY PSA0141
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 1/3119 9:00 BMS P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 17

Full -Service Analytical &
I S Environmental Solutions
?zoB ToRIES. iNo
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/08/2019
Client Sample ID: Fecal #5
Prism Sample ID: 9010010-05
Prism Work Order: 9010010
Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 80.5 % by 0.100 0.100 1 *SM2540 G 1/8119 14:30 TJY P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 1/3/19 9:00 BMS P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 17

Laboratory Report
,��pp�1 Full -Service Analytical &
r`_i1E�r1 _ill I S I� Environmental Solutions 05/08/2019
-`'-7�0RAT..IES. ING
,ity of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #6
^ttn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 9010010-06
P.O. Box 1111 Prism Work Order: 9010010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
Solids 71.7
% by
0.100
0.100 1 *SM2540 G 118119 14:30 TJY
P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 1/3/19 9:00 BMS
P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 9 of 17

NR:�,
11 Laboratory Report
Full -Service Analytical &
f ISM Environmental Solutions 05/08/2019
7LAeOR TORIES, INC.
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #7
Attn: Andy Smith 60Day 7 Fecal) Prism Sample ID: 9010010-07
P.O. Box 1111 Prism Work Order: 9010010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/02/19 11:00
Time Submitted: 01/03/19 08:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 72.5
% by
0.100
0.100 1
*SM2540 G 118119 14:30 TJY
P9A0141
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 1/3/19 9:00 BMS
P9A0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 17

Level II QC Report
&rit33
pp'\ /A'Full-Service Analytical& 5/8/19
I S, V I I Environmental Solutions
`�LABORATORlm INa.
Ity of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 9010010
tn: Andy Smith 7 Fecal) Time Submitted: 1/3/2019 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9AO046 - SAR 2-78-054
Blank (P9A0046-BLK1)
Prepared: 01/03/19 Analyzed: 01/07/19
SAR Soil Preparation
Complete
g
Batch P9AO055 - 3050B
Blank (P9A0055-BLK1)
Prepared &Analyzed: 01/04/19
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (HA0055-BSI)
Prepared &Analyzed: 01/04/19
Arsenic
11.6
0.50
mg/kg wet
12.50 93
80-120
admium
11.9
0.25
mg/kg wet
12.50 95
80-120
opper
12.1
0.50
mg/kg wet
12.50 97
80-120
Lead
11.8
0.25
mg/kg wet
12.50 94
80-120
Nickel
12.0
0.50
mg/kg wet
12.50 96
80-120
Potassium
1230
12
mg/kg wet
1250 98
80-120
Selenium
11.2
0.50
mg/kg wet
12.50 90
80-120
Sodium
1380
15
mg/kg wet
1250 110
80-120
Zinc
10.5
2.5
mg/kg wet
12.50 84
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 17

1 Full -Service Analytical &
&6'
I Environmental Solutions
-'% LABORATORIES ING
;ity of Statesville, NC
Utn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
5/8/19
Prism Work Order: 9010010
Time Submitted: 1/3/2019 8:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9A0056 - 3010A
Blank (P9A0056-BLK1) Prepared &Analyzed: 01/04/19
Calcium, SAR BRL 0.10 mg/L
Magnesium, SAR BRL 0.10 mg/L BH
Sodium, SAR 5.46 0.50 mg/L
Batch P9A0075 - NO PREP
Duplicate (HA0075-DUP1) Source: 9010010-01 Prepared: 01/04/19 Analyzed: 01/07/19
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.2 200
Batch P9A0078 - 7471B
Blank (P9A0078-BLK1) Prepared &Analyzed: 01/07/19
Mercury BRL 0.020 mg/kg wet
LCS (139A0078-13S1) Prepared &Analyzed: 01/07/19
Mercury 0.405 0.020 mg/kg wet 0.4167 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364- Fax: [phone] Page 12 of 17

Level II QC Report
ghiR_3
11�/IFull-Service Analytical& 5/8/19
� �/ I Environmental Solutions
��LABORATOHIE$ ma
;ity of Statesville, NC
�ttn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P9AO037 - 351.2
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 9010010
7 Fecal) Time Submitted: 1/3/2019 8:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9A0037-BLK1) Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen BRL 50 mg/kg wet
LCS (P9A0037-13S1) Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen 127 50 mg/kg wet 125.0 102 90-110
Matrix Spike (P9A0037-MS1) Source: 9010010-01 Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen 10400 3500 mg/kg dry 7001 3390 101 90-110
Matrix Spike Dup (P9A0037-MSD1) Source: 9010010-01 Prepared: 01/03/19 Analyzed: 01/04/19
Total Kjeldahl Nitrogen 10400 3500 mg/kg dry 7001 3390 101 90-110 0.03 20
Batch P9AO038 - NO PREP
Blank (P9A0038-BLK1) Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P9A0038-BS1) Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N 48.0 5.0 mg/kg wet 50.00 96 80-120
Matrix Spike (P9A0038-MS1) Source: 9010010-01 Prepared &Analyzed: 01/03/19
itrate/Nitrite as N 71.6 7.0 mg/kg dry 70.01 2.52 99 80-120
aviatrix Spike Dup (P9A0038-MSD1) Source: 9010010-01 Prepared &Analyzed: 01/03/19
Nitrate/Nitrite as N 70.8 7.0 mg/kg dry 70.01 2.52 98 80-120 1 20
Batch P9AO057 - SM4500-PB5
Blank (P9A0057-BLK1) Prepared &Analyzed: 01/07/19
Phosphorus -Total BRL 2.5 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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-71 Level II QC Report
a Full -Service Analytical & 5/8/19
I s M I Environmental Solutions
®�LAEOnATORIES ING
;ity of Statesville, NC
�ttn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P9AO057 - SM4500-PB5
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 9010010
Time Submitted: 1/3/2019 8:00:OOAM
%REC RPD
%REC Limits RPD Limit Notes
LCS (P9A0057-BS1) Prepared &Analyzed: 01/07/19
Phosphorus -Total 91.6 2.5 mg/kg wet 100.0 92 90-110
Matrix Spike (P9A0057-MS1) Source: 9010010-01 Prepared &Analyzed: 01/07/19
Phosphorus -Total 2940 70 mg/kg dry 140.0 2320 438 80-120 MC
Matrix Spike Dup (P9A0057-MSD1) Source: 9010010-01 Prepared &Analyzed: 01/07/19
Phosphorus -Total 2900 70 mg/kg dry 140.0 2320 411 80-120 1 20 MC
Batch P9AO089 - SM4500-NH3 B
Blank (P9A0089-B
Ammonia as N
BRL 10 mg/kg wet
Prepared &Analvzed: 01/07/19
LCS (P9A0089-BS1) Prepared &Analyzed: 01/07/19
Ammonia as N 498 10 mg/kg wet 500.0 100 80-120
Matrix Spike (P9A0089-MS1
Ammonia as N
Source: 9010010-01 Prepared &Analyzed: 01/07/19
761 14 mg/kg dry 686.4 303 67 80-120
Ratch P9AO141 - NO PREP
uplicate (P9A0141-DUP2) Source: 9010010-04 Prepared &Analyzed: 01/08/19
% Solids 72.0 0.100 % by Weight 72.0 0.1 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
M
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 17

Level II QC Report
J:P � I t
Full -Service Analytical &
Environmental Solutions
5/8/19
✓LABt7eATOfl1E8. ING
;ity of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
60Day Prism Work Order: 9010010
Ittn: Andy Smith
7 Fecal)
Time Submitted:
1/3/2019 8:00:OOAM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters
- Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit Units
Level Result %REC Limits
RPD Limit Notes
Batch P9A0065 - NO PREP
Blank (P9A0065-BLK1)
Prepared &Analyzed: 01/03/19
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0037
0.05 g
25 mL
01/03/19 9:50
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0089
1.06 g
50 mL
01/07/19 10:48
Prep Method: SM4500-PB5
ab Number
Batch
Initial
Final
Date/Time
)10010-01
P9A0057
1 g
50 mL
01/07/19 6:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
9010010-01
P9A0056
50 mL
50 mL
01/04/19 9:22
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0055
2 g
50 mL
01/04/19 7:50
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0078
0.6 g
50 mL
01/07/19 8:35
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
9010010-01
P9A0046
250 g
250 g
01/03/19 14:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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f` CHAIN OF ,= ,ODY RECORD
Ffl( ,w` Full -Service Analytical $
,: .lI S I Environmental Solutions PAGF of_ GUMIMsToENSURE PROPER BULM& -
��^ LA9ORATORIES, INQ
449 Springbrook Road • Charlotte, NC 28217 Project Name:
Phone [phone] • Fax: [phone] t P Short Hold Analysis: (Yes) (No) UST Project (Yes) (NO)
Client Company Name: C`4'f� 01r VAJES ✓17le *PleaseATTAQf any project specific reporting (QC LEVEL 19 ID IV).
provisions andfor QC Requirements
Report To/Contact Name: Kea OnwOLAW Invoice To:
Reporting Address:
- Address: - -- - - - - -- - -- -- - -
,',,ES NO N/A
Samples INTACT upon arrival?
Received ON WET ICE? - —� -
PROPER PRESERVATIVES Ind(caI6d _.
Received WITHIN HOLDING TIMES?- '-
CUSTODY SEALS INTACT?_
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS. used? - v'
TEMP: _Therm ID: Ooserve C 1 Co
Phone: 70y-878-3i -IT FaxQj0(No):70i1-S9Y Yd36 Purchase Order NoJBiflingReference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Dire Date o 1 Day O 2 Days 133 Days O 4 Days U 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other RushW-kMust9e
-warwny Days ❑ r s Days o stars 10 day$ ❑��
Site Location Name: For[ 4-A; CRzeEjc Samples received after 1*00 will be processed nerd business day.
SC OTHER - N/A
Site Location Physical Address:.o693 1&.1/ FiNa n !� Tumarourd time is based on tress dam, excluding finds and hordays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR NDITIONS REGAIMINGSERInCES
RENDERED I' IABoEM �TORU ,I NC i T)
Sample Iced Upon Collection: YES_ NO
CLIENT
DATE
TIME
COLLECT®
MATRIX
(SOIL,
SAMPLE COMiA1NER
PRESERVA_
AN.MYSIS REQUESTEM.
Mh'
PRISM
NO.
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATEROR
TIMES
/`�i . REMARKS
LAS
N0.
HOURS i
SLUDGE)�ti
SEE
S
P
41s�a3
Pa
.
Iwe-Al . res s
01
A5
SA
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61L
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(-
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T
S__-
— -'go
Din 7 FeC41
03
C.
A
05
T
N
0-7
_J
zN
Sampler's Signature Sampled By (Print Name). u' R r Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed witty the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be es for any changes after analyses have been Initialized.
PRISM USE
ONLY
Ral n 0d,8y (Signa
- - — —
ltlOnet Comments: Site Arrival Time:
1 8yr(SI '. B�.(Siyrrahre) Dam
A
Ill
- Site Departure Time:
I
nquished By: (Sig ture) Received, For " _ te
// Da)
r { �(
' Feld Tech Fee:
Q
II. _ _ _-- ill
'- 0-40 Mileage:
hod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BETAPED SHUFVaTHONTOTi ELABORAFOKY. Coo GF9W Na-
SAMPLESARENOTACCEPTEDANDVERFIEDAGAINSTCOCUNirL"hCC9y®AT'IIfELABORAiORY �f•�� {11 -
ad Ex DUPS OHand-delivered ReldSetvce _00&er- -- - -- -- -- ------ -----
DES: UST: G NDWATER:. DRINKING WATER_ SOLID WASTE:: RCRAk CERCLA LANDFILL OTHER:
'
C O SC ❑ NC ❑ SC I ' C ❑ SC I ❑❑ NC ❑ SC I NC I] SC El NC O Sc I NC ❑ SC I O❑ NC ❑ SC I OO NC O SCTERMS & CONDITIONS
❑O ❑O
❑ !
NTAINER TYPE CODES: A= Amber C = Clear G= Glass P = Plastic: TL=Tellon-Lined Cap VOA= Volatile Organics Analvsis (Zero Head SDace) ,.r.,..

Main Office:
".
/�
3 s I v I I
6:- �'-'L&GORATOPIM 1Nc
and
Full Service ll1I Solutions
Enviro�lrnGR1�_� Solutions
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P.O. Box , NC 43
Charlotte NC 28224-0543
28
Phone: [phone]
1/800/529-6364
Fax- 704/525-0409
www.prismlabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Numberl 9010010 1 Sample Name Sta-Lime
Na: Sodium (mg/L) Equivalent weight: 23
Ca : Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam /L Cam /L)- M m /L
128.0 1 1340.0 T 0.0
N, a (ME)
5.57
c_ a (ME)
(ME)
67.00
0 00
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent+ Mg Milli equivalent)]0.5 power
SAR = 1.0 (From mg/L entered above)
Calculated By:
Page 17 of 17

NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 5/8/19 10:14
f �1 I M I Environmental Solutions SC Certification No. 99012
LABORATORIES, ING
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 02/04/2019
Prism Work Order: 9020029
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the original laboratory report dated 2/13/19. PAN Equation has
been added to Case Narrative.
Analysis note for SAR:
SAR=[Na]/SQRT{([Cal +[Mg])/2)
!AR = [224/23.0] / SQRT { ( [1540/20.0] + [0/1121) / 2 )
SAR = 1.6
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) +
Nitrate —Nitrite
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
PAN Equation = 0.3 * (1900 — 240) + 0.5 * (240) + 9.6
PAN = <1200 mg/kg
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 10

Please call if you have any questions relating to this analytical report.
Respectfully,
-RISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
DM Sample diluted and RL increased due to the matrix.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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'.' Sample Receipt Summary
P ] Full -Service Analytical &
_!' S environmental Solutions 05/08/2019
dig ''ffUS0 ATORIGs INC.
Prism Work Order: 9020029
lient Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
StaLime (and Fecal 1) 9020029-01 Solid 02/04/19 11:37 02/04/19 13:26
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 10

Laboratory Report
��A �x Full -Service Analytical &
�R I S Environmental Solutions 05/08/2019
LABORATORIES, ING
:ity of Statesville, NC Project: StaLime Client Sample ID: StaLime (and Fecal 1)
Attn: Ken Galloway Prism Sample ID: 9020029-01
P.O. Box 1111 Prism Work Order: 9020029
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/04/19 11:37
Time Submitted: 02/04/19 13:26
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
BRL
mg/kg dry
1200
340
5
*Calculation 217/19 16:02
CLB
[CALCI
% Solids
65.4
% by
0.100
0.100
1
*SM2540 G 218119 9:20
KBS
P9B0100
Weight
Ammonia as N
240
mg/kg dry
15
3.7
1
*SM4500-NH3 C 2/7/19 16:02
BMS
P9130090
Nitrate/Nitrite as N
9.6
mglkg dry
7.6
2.1
1
*SM4500-NO3 F 217/19 10:38
CLB
P9130084
Phosphorus -Total
3400
mg/kg dry
76
17
20
*SM4500-P F 2/5/19 9:40
CLB
P9B0038
Total Kjeldahl Nitrogen
BRL
mg/kg dry
3800
1100
5
*351.2 2/6/19 10:52
CLB
P9130051
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 2/4/19 13:17
BMS
P9130061
Total Metals
Mercury
0.079
mg/kg dry
0.031
0.0029
1
*7471B
218/19 12:15
ICP
PSB0118
SAR Soil Preparation
Complete
g
1
*2-78-054
2/6/19 10:15
MMR
P9130047
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
2/7/19 10:15
MMR
P9130079
Weight
Arsenic
BRLpM
mg/kg dry
76
4.7
100
*6010D
2/11119 19:58
JAB
P9130072
idiumAbsorption Ratio
1.6
[blank]
0.30
0.016
1
*2-78-054
218119 9:31
JAB
P9130078
idmium
BRLpM
mg/kg dry
38
1.0
100
*6010D
2/11/19 19:58
JAB
P9130072
Calcium, SAR
1500 BH, B
mg/L
10
1.0
100
*6010D
2/8/19 9:31
JAB
PSB0078
Copper
BRLpM
mg/kg dry
76
6.9
100
*6010D
2/11/19 19:58
JAB
P9130072
Lead
BRLpM
mg/kg dry
38
7.1
100
*6010D
2/11/19 19:58
JAB
P9B0072
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
2/8/19 9:31
JAB
P960078
Nickel
BRLpM
mg/kg dry
76
2.8
100
*6010D
2/11119 19:58
JAB
P9130072
Potassium
3900 DM
mg/kg dry
1900
69
100
*6010D
2111/19 19:58
JAB
P980072
Selenium
BRLpM
mg/kg dry
76
18
100
*6010D
2/11/19 19:58
JAB
P9B0072
Sodium
BRLpM
mg/kg dry
2300
75
100
*6010D
2/11/19 19:58
JAB
P9130072
Sodium, SAR
220 BH, B
mg/L
50
1.8
100
*6010D
2/8119 9:31
JAB
P9130078
Zinc
BRLpM
mg/kg dry
380
14
100
*6010D
2111/19 19:58
JAB
P9130072
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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`X'
Level II QC Report
Full -Service Analytical &
5/8/19
I I Environmental Solutions
LABORATORIES ING
ty of Statesville, NC
Project:
StaLime
Prism Work Order: 9020029
- ,tn: Ken Galloway
Time Submitted: 2/4/2019 1:26:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike
Source %REC RPD
Analyte
Result
Limit
Units
Level
Result %REC Limits RPD Limit Notes
Batch P9B0047 - SAR 2-78-054
Blank (PSB0047-BLK1)
Prepared:
02/05/19 Analyzed: 02/06/19
SAR Soil Preparation Complete
g
Batch P9B0072 - 3050B
Blank (P9130072-BLKI)
Prepared:
02/06/19 Analyzed: 02/07/19
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P9B0072-13SI)
Prepared:
02/06/19 Analyzed: 02/07/19
Arsenic
11.7
0.50
mg/kg wet
12.50
94 80-120
idmium
11.7
0.25
mg/kg wet
12.50
94 80-120
)pper
12.0
0.50
mg/kg wet
12.50
96 80-120
Lead
11.8
0.25
mg/kg wet
12.50
94 80-120
Nickel
11.8
0.50
mg/kg wet
12.50
94 80-120
Potassium
1210
12
mg/kg wet
1250
97 80-120
Selenium
11.1
0.50
mg/kg wet
12.50
89 80-120
Sodium
1180
15
mg/kg wet
1250
95 80-120
Zinc
11.1
2.5
mg/kg wet
12.50
89 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 10

Full -Service Analytical &
I S Environmental Solutions
©LABORATORIES. ING
ty of Statesville, NC Project: StaLime
An: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
5/8/19
Prism Work Order: 9020029
Time Submitted: 2/4/2019 1:26:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9B0078 - 3010A
Blank (P9B0078-BLK1)
Prepared: 02/06/19 Analyzed: 02/08/19
Sodium Absorption Ratio
BRL
0.30
[blank]
Calcium, SAR
1.26
0.10
mg/L
BH
Magnesium, SAR
BRL
0.10
mg/L
Sodium, SAR
2.46
0.50
mg/L
BH
Batch P9B0079 - NO PREP
Duplicate (P9B0079-DUP1)
Source: 9020029-01
Prepared: 02/06/19 Analyzed: 02/07/19
SAR Percent Moisture
Complete
0.100
% by Weight Complete 8 200
Batch P9B0118 - 7471 B
Blank (P9B0118-BLK1)
Prepared &Analyzed: 02/08/19
Mercury
BRL
0.020
mg/kg wet
LCS (P9B0118-BS1)
Prepared &Analyzed: 02/08/19
Mercury
0.428
0.020
mg/kg wet
0.4167 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 10

Level II QC Report
�R� Full -Service Anal tical & 5/8/19
�IR I S Environmental Solutions
`�LAaORATORIES. ING
ty of Statesville, NC Project: StaLime Prism Work Order: 9020029
...tn: Ken Galloway Time Submitted: 2/4/2019 1:26:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Result
Reporting
Limit
Units
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P91B0038 - SM4500-PB5
Blank (P960038-BLKI)
Prepared &Analyzed: 02/05/19
Phosphorus -Total
LCS (P9B0038-BSI)
BRL
2.5
mg/kg wet
Prepared &Analyzed: 02/05/19
Phosphorus -Total
Batch P9130051 - 351.2
103
2.5
mg/kg wet
100.0 103 90-110
Blank (P9B0051-BLK1)
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
LCS (P9B0051-BS1)
BRL
50
mg/kg wet
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
Matrix Spike (P960051-MS1)
123 50 mg/kg wet
Source: 9020029-01
125.0 102 90-110
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
Matrix Spike Dup (P960051-MSD1)
11800 3800 mg/kg dry
Source: 9020029-01
7642 3710 106 90-110
Prepared: 02/05/19 Analyzed: 02/06/19
Total Kjeldahl Nitrogen
—atch P9B0084 - NO PREP
11300
3800
mg/kg dry
7642 3710 99 90-110 5 20
ank (P9B0084-BLK1)
Prepared &Analyzed: 02/07/19
Nitrate/Nitrite as N
LCS (P960084-13SI)
BRL
5.0
mg/kg wet
Prepared &Analyzed: 02/07/19
Nitrate/Nitrite as N
50.0
5.0
mg/kg wet
50.00 100 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: l-8001529-6364- Fax: [phone] Page 7 of 10

Full -Service Analytical &
'�b4nq'I Environmental Solutions
07A ORATORIES ING
Level II QC Report
5/8/19
ty of Statesville, NC Project: StaLime Prism Work Order: 9020029
...tn: Ken Galloway Time Submitted: 2/4/2019 1:26:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9B0084 - NO PREP
Matrix Spike (P9B0084-MS1)
Source: 9020029-01
Prepared &Analyzed: 02/07/19
Nitrate/Nitrite as N
Matrix Spike Dup (P9B0084-MSD1)
83.1 7.6 mg/kg dry
Source: 9020029-01
76.42 9.63 96
Prepared &Analyzed: 02/07/19
80-120
Nitrate/Nitrite as N
Batch P9B0090 - SM4500-NH3 B
84.6 7.6 mg/kg dry
76.42 9.63 98
80-120 2 20
Blank (P9B0090-BLK1)
Prepared &Analyzed: 02/07/19
Ammonia as N
LCS (P9B0090-BS1)
BRL 10 mg/kg wet
Prepared &Analyzed: 02/07/19
Ammonia as N
Matrix Spike (P960090-MS1)
524 10 mg/kg wet
Source: 9020029-01
500.0 105
Prepared &Analyzed: 02/07/19
80-120
Ammonia as N
Matrix Spike Dup (P9B0090-MSD1)
1020 15 mg/kg dry
Source: 9020029-01
764.2 237 103
Prepared &Analyzed: 02/07/19
80-120
Ammonia as N
1020 15 mg/kg dry
734.8 237 107
80-120 0.2 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 10

A Full -Service Analytical &
R I M I Environmental Solutions
�LABOPATOPIES. ING
`ty of Statesville, NC
__tn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
5/8/19
Prism Work Order: 9020029
Time Submitted: 2/4/2019 1:26:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %oREC Limits RPD Limit Notes
Batch P9B0061 - NO PREP
Blank (P9B0061-BLK1)
Prepared &Analyzed: 02/04/19
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction
Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
9020029-01
P9B0051
0.05 g
25 mL
02/05/19 10:50
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
9020029-01
P9B0090
1.03 g
50 mL
02/07/19 9:25
Prep Method: SM4500-PB5
b Number
Batch
Initial
Final
Date/Time
20029-01
P9B0038
1 g
50 mL
02/05/19 6:15
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9020029-01
P9130078
50 mL
50 mL
02/06/19 10:10
9020029-01
P9B0078
50 mL
50 mL
02/06/19 10:10
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
9020029-01
P9130072
2 g
50 mL
02/06/19 8:35
Prep Method: 7471B I
Lab Number
Batch
Initial
Final
DateMme
9020029-01
P980118
0.6 g
50 mL
02/08/19 9:05
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
9020029-01
P9B0047
250 g
250 g
02/05/19 10:15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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P
Full-Service Analytical A
R l S M I Environmental Solutions
"'"'LABORATORIES. INC
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax:[phone]
Client Company Name, C-_� a s¢a�i&St✓,
:Report TolContadt Name: Kew Ca fo
Reporting, Address:.
CHAIN Of CUSTODY RECORD
PAGE OF- QUOTE 970 ENSURE PROPER BiWNG:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL I H III Ill)
provisions and/or QC Requirements
Invoice To:
Address:
YES_ NO N/A
Samples INTACT upon arrival?
.. O
Received ON WETICE? - _ p
PROPER PRESERVATIVES indicated?
Received WITHIN.HOLDING TIMES?CZ
CUSTODY SEALSdNTACT?
VOLATILES reediW/OUT HEADSPACE? -
PROPER CONTAINERS used? _
TEMP: Therm ID:. Observed ' ; !4G L Gorr °C
Phone:704f• T77.543T FaxQYe l[No):70Y 171t• Y955 purchase Order NoJBilling Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date 1 Day
❑ Ll 2 Days O 3 Days O 4 Days v 6 Days
Certification: NELAC DoD FL NC
EDD Type: PDF_Excel_ Other "Working Days" 13 6-9 Days O Standard 10 days LlRush W0r k M tie
Site Location Name: F w h CR E k Samples received after 14:00 will y be processed next business da
SC OTHER NIA
,7
Site Location Physical Address' 144A �� 11 Fe,f, R Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE
rPI�RAES s� RENDERED BYRS LABORATORIES. INC. O REGARDING
Sample Iced Upon Collection: YES NO
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
COLLECTED
MILITARY
(SOIL,
WATER OR
PRESERVA.
(! / REMARKS
PRISM
B
'TYPE
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
`4
/��� //
ID O.
stA
y- l9
Io 3 7
I
A
'
Ica
P6
_
N
i
S
I
l
�% Q o PRE:SS• • N. FIRMLY -3• PI ffSl
oGR
Sampler's Signature /�/ Sampled By (Print Name) a Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the PrlswPro)ect Manager. There villl be charge any changes after analyses have been i ' ' LMd.
Re In ulshod By: ISipndture) Rcc -- .( gn. feua) ,� rl�ltlarylHouts.
-- Oa� � . � Additional Comments: 'Site Arrival Time:
Reli fished By: (Signature) Received By. (Slgna re) 0$tB Site Departure Time:
Reran - a d By:,(SlgnalUreJ' Received g' La rry: O� - Field Tech Fee:
Z !7 Mileage: --
_
eth of ship enC NOTE: ALL SAMPLE COOLERS SHOUW BE TAPED SHrIT VATH C Y4So 5/FORTRANSPORTATION TO THE LABORATORY. COG Gr¢2 . .
SAMPLESARENOTACCEPTEDANDVERIF.IEDAGAINSTCDCUNTILRECEi H�ATTHELABORATORY. O ' O�y
VVV w L
❑ Fed Ex O UPS O Hand -delivered ❑ Prism Feld Service O Other
NPDES: I UST: GROUNDWATER: DRINKING WATER: I SOLIDWASTE: RCRA: CERCLA LANDFILL OTHER: '
❑ NC ❑ S( JC ❑ SC I o NC ❑ SC I ❑o NC ❑ SC , Oo NC 0 Se o Nr' ^ eC Oo NC ❑ SC ONC O Sc U NC O SC
in
❑ I171
`CONTAINI 'PE CODES A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined C-. IA= Volatile Organics Analysis (Zero Head Space) wmIGINAL

-� NC Certification No. 402 Case Narrative
f �D 1 I S M I Full -Service Analytical & NC Drinking Water Cert No. 37735 5/31/19 13:15
Environmental Solutions SC Certification No. 99012
LABORATORIES, INC.
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville. NC 28687
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 05/22/2019
Prism Work Order: 9050402
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR W [ Na ] / SORT { ([Ca] * [Mg]) / 2 )
SAR = [150/23 ] / SORT { ( [2600/20] + [-0,034/12.2]) / 2 }
SAR = 0.79
.;oncentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) +
Nitrate —Nitrite
PAN = 0.3 * (5000 — 210) + 0.5 * (210) + 2.9
PAN = 1500 mg/kg
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 17

Please call if you have any questions relating to this analytical report.
Respectfully,
-RISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
Mc Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
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v
u a Full -Service Analytical &
F'R I S M I Environmental Solutions
�VV LA6oH ToN1E61NC
Sample Receipt Summary
05/31 /2019
Prism Work Order: 9050402
-lient Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
Stal-ime (and Fecal 1)
9050402-01
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #2
9050402-02
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #3
9050402-03
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #4
9050402-04
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #5
9050402-05
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #6
9050402-06
Solid
05/22/19
9:00
05/22/19 14:15
Fecal #7
9050402-07
Solid
05/22/19
9:00
05/22/19 14:15
Samples were received in good condition at 3.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 17

Fu11-Service Analytical &
�J I S M I Environmental Solutions
;�'A ORATORmr, ING
;ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/31 /2019
Client Sample ID: StaLime (and Fecal 1)
Prism Sample ID: 9050402-01
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1600
mg/kg dry
18
6.4
2
*Calculation 5/29/19 11:02
CLB
[CALC]
Solids
71.6
% by
0.100
0.100
1
*SM2540 G 5/28/19 9:05
KBS
P9E0457
Weight
Ammonia as N
210
mg/kg dry
14
3.5
1
*SM4500-NH3 C 5/23/19 15:04
BMS
P9E0427
Nitrate/Nitrite as N
BRL
mg/kg dry
7.0
1.9
1
*SM4500-NO3 F 5/24/19 8:42
CLB
P9E0441
Phosphorus -Total
3100
mg/kg dry
140
42
20
*SM4500-P F 5/30119 7:21
CLB
P9E0483
Total Kjeldahl Nitrogen
5000
mg/kg dry
28
13
2
*351.2 5129/19 11:02
CLB
P9E0475
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 5/22/19 14:45
BMS
P9E0433
Total Metals
Mercury
BRL
mg/kg dry
0.070
0.024
1
*7471B
5/29/19 10:54
MMR
P9E0477
SAR Soil Preparation
Complete
g
1
*2-78-054
5/24/19 10:30
JAB
P9E0426
SAR Percent Moisture
52.8
% by
0.100
0.100
1
*2-78-054
5128/19 9:15
MMR
P9E0464
Weight
Arsenic
4.2
mg/kg dry
1.4
0.18
1
*6010D
5/29119 17:57
JAB
P9E0438
Idium Absorption Ratio
0.79
[blank]
0.30
0.016
1
*2-78-054
5/30119 8:46
JAB
P9E0453
idmium
BRL
mg/kg dry
0.70
0.047
1
*6010D
5/29/19 17:57
JAB
P9E0438
Calcium, SAR
2600
mg/L
50
0.50
50
*6010D
5/30119 8:46
JAB
P9E0453
Copper
300
mg/kg dry
170
24
50
*6010D
5/29/19 17:49
JAB
P9E0438
Lead
BRL
mg/kg dry
1.4
0.23
1
*6010D
5/29119 17:57
JAB
P9E0438
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
5/30/19 8:46
JAB
P9E0453
Nickel
37
mg/kg dry
1.4
0.42
1
*6010D
5129/19 17:57
JAB
P9E0438
Potassium
27000
mg/kg dry
7000
730
50
*6010D
5129/19 17:49
JAB
P9E0438
Selenium
12
mg/kg dry
1.4
0.38
1
*6010D
5/29119 17:57
JAB
P9E0438
Sodium
4800
mg/kg dry
140
19
1
*6010D
5/29119 17:67
JAB
P9E0438
Sodium, SAR
150 B
mg/L
25
0.90
50
*6010D
5/30119 8:46
JAB
P9E0453
Zinc
BRL
mg/kg dry
14
2.0
1
*6010D
5/29/19 17:57
JAB
P9E0438
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 17

IP 'p\ /p' Full -Service Analytical &
iJP I S 1 V , Environmental Solutions
Laboratory Report
05/31 /2019
;ity of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #2
,1ttn: Ken Galloway
60Day 7 Fecal)
Prism Sample ID: 9050402-02
P.O. Box 1111
Prism Work Order: 9050402
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids
70.3 % by
0.100 0.100
1 *SM2540 G 5/28119 9:06 KBS P9E0457
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 *SM9221 E 5/22/19 14:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 17

&IiR
ISn n I EnviService Analytical s'v'.Environmental SolutionsV�LABOMTORIM INC
'ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Parameter
Result
Laboratory Report
05/31 /2019
Project: Stal-ime (Qtrly, BiWeekly, Client Sample ID: Fecal #3
60Day 7 Fecal) Prism Sample ID: 9050402-03
Prism Work Order: 9050402
Sample Matrix: Solid Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date[Time ID
General Chemistry Parameters
% Solids 68.2. % by 0.100 0.100 1 `SM2540 G 5/28/19 9:06 KBS P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 5/22/19 14:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 17

rl,\ Laboratory Report
ARRIS
n A Full -Service Analytical &
' V' Environmental Solutions 05/31/2019
��LA ONATOHIE%INC
;ity of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #4
Attn: Ken Galloway 60Day 7 Fecal) Prism Sample ID: 9050402-04
P.O. Box 1111 Prism Work Order: 9050402
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Solids 71.2 % by 0.100 0.100 1 *SM2540 G 6/28/19 9:05 KBS P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 5/22/19 14:45 BMS P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 17

_>, ,
Full -Service Analytical &
/&�.Qli
31
S M Environmental Solutions
I LABOR TORTE& -
'ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, Biweekly
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/31 /2019
Client Sample ID: Fecal #5
Prism Sample ID: 9050402-05
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 68.9
% by
0.100
0.100 1
*SM2540 G 5128/19 9:05 KBS
P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 5/22/19 14:45 BMS
P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 17

.',
Laboratory Report
R� Full -Service Analytical R
JPpCl
1 I SMEnvironmental Solutions
05/31/2019
�l
'--- V LABORATOR
amity of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #6
Attn: Ken Galloway
60Day 7 Fecal)
Prism Sample ID: 9050402-06
P.O. Box 1111
Prism Work Order: 9050402
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids 69.0
% by
0.100 0.100
1 *SM2540 G 6128/19 9:05 KBS
PSE0457
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 5/22/19 14:45 BMS
P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 17

&14*
A Full -Service Analytical R
*�-Y I SM I Environmental Solutions
v UIBQ-ORIES ING
;ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, Biweekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
05/31 /2019
Client Sample ID: Fecal #7
Prism Sample ID: 9050402-07
Prism Work Order: 9050402
Time Collected: 05/22/19 09:00
Time Submitted: 05/22/19 14:15
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 70.2
% by
0.100
0.100 1
'SM2540 G 5128/19 9:05 KBS
P9E0457
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 5/22/19 14:45 BMS
P9E0433
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 17

Full -Service Analytical &
Ap..._01@ff��UBOMTORIE$I Environmental Solutions
INC.
ity of Statesville, NC
,,ttn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P9EO426 - SAR 2-78-054
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
5/31 /19
Prism Work Order: 9050402
Time Submitted: 5/22/2019 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9E0426-BLK1)
Prepared: 05/23/19 Analyzed: 05/24/19
SAR Soil Preparation
Complete
g
Batch P9E0438 - 3050B
Blank (P9E0438-BLK1)
Prepared: 05/24/19 Analyzed: 05/28/19
Arsenic
BRL
1.0
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Copper
BRL
2.5
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
100
mg/kg wet
Selenium
BRL
1.0
mg/kg wet
Sodium
BRL
100
mg/kg wet
Zinc
BRL
10
mg/kg wet
LCS (P9E0438-BS1)
Prepared: 05/24/19 Analyzed: 05/28/19
Arsenic
12.1
1.0
mg/kg wet
12.50 97 80-120
edmium
12.1
0.50
mg/kg wet
12.50 97 80-120
upper
12.9
2.5
mg/kg wet
12.50 103 80-120
Lead
12.2
1.0
mg/kg wet
12.50 98 80-120
Nickel
12.2
1.0
mg/kg wet
12.50 98 80-120
Potassium
1220
100
mg/kg wet
1250 97 80-120
Selenium
11.7
1.0
mg/kg wet
12.50 93 80-120
Sodium
1230
100
mg/kg wet
1250 98 80-120
Zinc
12.0
10
mg/kg wet
12.50 96 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 17

�Full-Service Anal tical &
APRISM Environmental Solutions
_�ai - V LABORATORIES, INC
ity of Statesville, NC
, .ttn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P9EO453 - 3010A
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level 11 QC Report
5/31 /19
Prism Work Order: 9050402
Time Submitted: 5/22/2019 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9E0453-BLK1) Prepared: 05/24/19 Analyzed: 05/30/19
Calcium, SAR BRL 1.0 mg/L
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 2.00 0.50 mg/L BH
Batch P9E0464 - NO PREP
Duplicate (P9E0464-DUP1) Source: 9050402-01 Prepared: 05/24/19 Analyzed: 05/28/19
SAR Percent Moisture 53.1 0.100 % by Weight 52.8 0.6 200
Batch P9E0477 - 7471 B
Blank (P9E0477-BLK1) Prepared &Analyzed: 05/29/19
Mercury BRL 0.050 mg/kg wet
LCS (P9E0477-BS1) Prepared &Analyzed: 05/29/19
Mercury 0.411 0.050 mg/kg wet 0.4167 99 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 17

h'n'2 Full -Service Analytical &
hI S M Environmental Solutions
LABORATORIES INa
ity of Statesville, NC
An: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P9EO427 - SM4500-NH3 B
Level II QC Report
5/31/19
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 9050402
7 Fecal) Time Submitted: 5/22/2019 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9E0427-BLK1) Prepared &Analyzed: 05/23/19
Ammonia as N BRL 10 mg/kg wet
LCS (P9E0427-BSI) Prepared &Analyzed: 05/23/19
Ammonia as N 507 10 mg/kg wet 500.0 101 80-120
Matrix Spike (P9E0427-MS1) Source: 9050402-01 Prepared & Analyzed: 05/23/19
Ammonia as N 859 14 mg/kg dry 691.1 207 94 80-120
Matrix Spike Dup (P9E0427-MSD1) Source: 9050402-01 Prepared &Analyzed: 05/23/19
Ammonia as N 866 14 mg/kg dry 684.3 207 96 80-120 0.8 200
Batch P9EO441 - NO PREP
Blank (P9E0441-BLK1) Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P9E0441-BS1) Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N 49.0 5.0 mg/kg wet 50.00 98 80-120
Matrix Spike (P9E0441-MS1) Source: 9050402-01 Prepared &Analyzed: 05/24/19
itrate/Nitrite as N 73.0 7.0 mg/kg dry 69.80 5.79 96 80-120
Matrix Spike Dup (P9E0441-MSD1) Source: 9050402-01 Prepared &Analyzed: 05/24/19
Nitrate/Nitrite as N 72.0 7.0 mg/kg dry 69.80 5.79 95 80-120 1 20
Batch P9EO457 - Solids, Dry Weight
Duplicate (PSE0457-DUP2) Source: 9050402-06 Prepared: 05/24/19 Analyzed: 05/28/19
% Solids 69.5 0.100 % by Weight 69.0 0.6 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 17

R
//�'
r 1n'� Full -Service Analytical &
P I� I S 1 Y 7 Environmental Solutions
_'Z 6 ATORIM ING
Level II QC Report
5/31 /19
ity of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 9050402
Atn: Ken Galloway 7 Fecal) Time Submitted: 5/22/2019 2:15:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9E0475 - 351.2
Blank (P9E0475-BLKI)
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
BRL 1.0 mg/kg wet
LCS (P9E0475-BS1)
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
124 1.0 mg/kg wet
125.0 100 90-110
Matrix Spike (P9E0475-MS1)
Source: 9050402-01
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
10400 70 mg/kg dry
6980 4990 78 90-110
MI
Matrix Spike Dup (P9E0475-MSD1)
Source: 9050402-01
Prepared: 05/28/19 Analyzed: 05/29/19
Total Kjeldahl Nitrogen
11200 70 mg/kg dry
6980 4990 89 90-110 7 20
MI
Batch P9E0483 - SM4500-PB5
Blank (P9E0483-1BLK1)
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
BRL 5.0 mg/kg wet
LCS (P9E0483-BSI)
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
110 5.0 mglkg wet
100.0 110 90-110
Matrix Spike (P9E0483-MS1)
Source: 9050402-01
Prepared: 05/29/19 Analyzed: 05/30/19
hosphorus-Total
3030 140 mg/kg dry
139.6 3140 NR 80-120
MC
Matrix Spike Dup (P9E0483-MSD1)
Source: 9050402-01
Prepared: 05/29/19 Analyzed: 05/30/19
Phosphorus -Total
3050 140 mg/kg dry
139.6 3140 NR 80-120 0.5 20
MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 14 of 17

flP �R ISM Full -Service al Solutions
s
I �'-� Environmental Solutions
.'LA6o—T=ES ING
ity of Statesville, NC
.ttn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch P9EO433 - NO PREP
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
5/31 /19
Prism Work Order: 9050402
Time Submitted: 5/22/2019 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9E0433-BLK1) Prepared &Analyzed: 05/22/19
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 17

Sample Extraction Data
Prep Method: 351.2
lb Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0475
0.05 g
25 mL
05/28/19 11:02
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0427
1 g
50 mL
05/23/19 8:56
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0483
1 g
50 mL
05/29/19 10:00
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
DateMme
9050402-01
P9E0457
30 g
30 g
05/24/19 16:10
9050402-02
P9E0457
30 g
30 g
05/24/19 16:10
9050402-03
P9E0457
30 g
30 g
05/24/19 16:10
9050402-04
P9E0457
30 g
30 g
05/24/19 16:10
9050402-05
P9E0457
30 g
30 g
05/24/19 16:10
9050402-06
P9E0457
30 g
30 g
05/24/19 16:10
9050402-07
P9E0457
30 g
30 g
05/24/19 16:10
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0453
50 mL
50 mL
05/24/19 11:00
050402-01
P9E0453
50 mL
50 mL
05/24/19 11:00
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0438
2 g
50 mL
05/24/19 7:05
9050402-01
P9E0438
2 g
50 mL
05/24/19 7:05
Prep Method: 7471 B
Lab Number
Batch
Initial
Final
Date/Time
9050402-01
P9E0477
0.6 g
50 mL
05/29/19 9:00
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
DateMme
9050402-01
P9E0426
250 g
250 g
05/23/19 10:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 16 Of 17

f CHAIN OF CUSTODY RECORD
Full -Service Analytical &
I
I Environmental Solutions PAGE OF_ QUOTE STOENSURE PROPER BILLING;
.s L,�aRFroRtE,s, INa
449 Springbrook Road • Charlotte, NC 28217 Project Name:.
Phone [phone] • Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project (Yes) (NO)
n ��A' I1IE 'Please ATTACH any project specific reporting (QC LEVEL I f) III M
Client Company Name:.C•'�)/ •ot �EStrr provisions andlorQCRequirements
Report To/Contact Name: KEN CrA iIn asg Invoice To:
Reporting Address:.
Address:
YES , 0 N/ �
r
Samples INTACT upon arrival?
�_ -
Received ON WET ICE?
o
T
PROPER PRESERVATIVES indicated? .
Received WITHIN:HOLDING TIMES?
CUSTODY'SEALS.INTACT?
VOIATILES reed WIOUT HEADSPACE?
PROPER CONTAINERS used?
TEMP. berm ID:� Observed:
`'� ;/ Corr: - C
Nnone:/D7-8 /S-» oa Fax Yes (No):7uY^s _/ �-�6�J. Purchase Order NoMilling Reference
TO BE FILLED IN -BY CLIENTISAMPLING PERSONNEL
Email Address: _ Requested Due Date O 1 Day 0 2 Days (3 3 Days O 4 Days O 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF_Ex_clel Other "Working Days" 0 6-9 Days o standard 10 days I] �ppMust Be
Site Location Name: a u YZl h Ca -- Samples received after 14,00 w01 be processed next business day.
SC- OTHER NIA
Site Location Physical Address: d 93leff Fin 0?W= 1? .-. Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS 6 CONDITIONS REGARDING SERVICES
RENDERED BYPRISM LABORATORIES. INC. TOCLfEM)
Sample Iced Upon Collection: YES NO_
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
M
MATRIX
IL,
(SOILITARY
WATER OR
SAMPLECONTAINER
PRTWES A-
TIM ES
ANALYSISREQUESTED
�! % REMARKS
ti`
PRISM
B
*TYPE
_
HOURS
SLUDGE)
,SEE BELOW
NO.
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ID NO.
%,a,(; a
5-22-l9
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Sampler's Signature / �� Sampled By (Print Name) &irJA Affiliation
Upon relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be ONLY -
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
Relln IShad.By: (Signature), - R=cen 8y (Signa J Oata__ AN4tary/Hours
- � Additioria(Comments: site Amval Time:
[</ P S7
Ft, n o.. y:,(Sl nature) ; }� - RebsMFd By. (Signs—) Date t Site Departure Time:
Field Tech Fee:
Relfiq41shed By: (S' nature) Rey%JvcJH3rr Prism LaboTt x_ie; By: Date
� f
Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE -TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO TMro-LABORATORY -CDC Gmdp No.
SAMPLES ARE NO ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
O Fed Ex ❑ UPS ❑ Hand -delivered . m Field Service O Other q� J r�
NPDES: UST: GR DWATER: DRINKING WATER: SOLID,WASTE:-• RCRA: CERCLA LANDFILL OTHER: '
o NC ❑ SCI ❑ NC ❑ SC I o C ❑ SC I Q NC ❑ SC I ❑ NC ❑ SC I LING Ll C I o NC L) LING ❑ SCI oNC ❑ SC r
El ❑
'CONTAIN fPE CODES: A =Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined G )A= Volatile Organics Analysis (Zero Head Space) ­ 1IGINAL

.
NC Certification No. 402 Case Narrative
D. I .� Full -Service Analytical & NC Drinking Water Cert No. 37735 8/21 /19 13:44
D I SM Environmental Solutions SC Certification No. 99012
_ `/LABORATORIES, INC.
City of Statesville, NC Project: Sludge (Hazardous Testing)
Ken Galloway
P.O. Box 1111 Lab Submittal Date: 08/07/2019
Statesville, NC 28687 Prism Work Order: 9080093
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Herbicide analysis was subcontracted to AES. Reactivity analysis was subcontracted to GCAL.
Laboratory reports are attached.
Prism Summary of Detections does not include subcontracted data.
r"lease call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
A Negative, Pass
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 30

4.. ,
Sample Receipt Summary
it I S M
Full -Service Analytical &
I Environmental Solutions
08/21/2019
�LABOFiATORIE%ING
Prism Work Order: 9080093
Aient Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
4th Creek Sludge
9080093-01
Solid
08/07/19 9:55 08/07/19 16:00
3rd Creek Sludge
9080093-02
Solid
08/07/19 9:45 08/07/19 16:00
Sta-Lime
9080093-03
Solid
08/07/19 9:30 08/07/19 16:00
Samples were received in good condition at 5.2 degrees C unless otherwise noted
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 30

:,'� Laboratory Report
//I��1 a Full -Service Analytical &
%1!3::11.�► ISM Environmental Solutions 08/21/2019
��LAeORhTORES wa.
amity of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: 4th Creek Sludge
Attn: Ken Galloway Prism Sample ID: 9080093-01
P.O. Box 1111 Prism Work Order: 9080093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/07/19 09:55
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
14.7
% by
0.100
0.100
1
*SM2540 G
8/16/19 8:30
EDV
P9H0264
Weight
Corrosivity-pH
5.4
pH Units
1
*9045D
8/9119 13:40
BMS
P9H0161
Ignitability
BRLA
mm/sec
0.10
1
*1030
819/19 8:25
BMS
P91-10143
Temperature
22
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/13/19 7:30
TBL
P91-10174
TCLP Extraction
Complete
N/A
1
*1311
8/13/19 7:50
MMR
P91-10185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
*7470A
8/15/19 14:09
MMR
P91-10261
Arsenic
BRL
mg/L
0.10
0.030
1
*6010D
8/13/19 17:06
JAB
P91-10203
Barium
BRL
mg/L
5.0
0.010
1
*6010D
8/13/19 17:06
JAB
P91-10203
Cadmium
BRL
mg/L
0.025
0.0020
1
*6010D
8/13119 17:06
JAB
P91-10203
Chromium
BRL
mg/L
0.25
0.015
1
*6010D
8/13/19 17:06
JAB
P91-10203
lead
BRL
mg/L
0.050
0.020
1
*6010D
8/13/19 17:06
JAB
P91-10203
elenium
BRL
mg/L
0.15
0.063
1
*6010D
8/13/19 17:06
JAB
P91-10203
Silver
BRL
mg/L
0.25
0.0045
1
*6010D
8/13/19 17:06
JAB
P91-10203
TCLP Organochlorine Pesticides
by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
*8081B
8/14/19 16:49
ZRC
P91-10227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
*8081B
8/14/19 16:49
ZRC
P91-10227
Endrin
BRL
mg/L
0.00050
0.000068
1
*8081B
8/14/19 16:49
ZRC
P91-10227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
*8081B
8/14/19 16:49
ZRC
P91-10227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
*8081B
8/14/19 16:49
ZRC
P91-10227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
*8081B
8/14/19 16:49
ZRC
P91-10227
Methoxychlor
BRL
mg/L
0.00050
0.000090
1
*8081B
8/14/19 16:49
ZRC
P91-10227
Toxaphene
BRL
mg/L
0.025
0.0018
1
*8081B
8114119 16:49
ZRC
P91-10227
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
82
%
13-186
Tetrachloro-m-xylene
92
%
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
*8270E
8/13/19 18:07
JMV
P91-10193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
*8270E
8/13/19 18:07
JMV
P91-10193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*8270E
8/13/19 18:07
JMV
P9H0193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
*8270E
8/13/19 18:07
JMV
P91-10193
3/4-Methylphenol
BRL
mg/L
0.050
0.0025
1
*8270E
8113/19 18:07
JMV
P91-10193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
8/13/19 18:07
JMV
P91-10193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
*8270E
8/13/19 18:07
JMV
P91-10193
Hexachloroethane
BRL
mg/L
0.050
0.0037,
1
*8270E
8/13/19 18:07
JMV
P91-10193
litrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
8/13/19 18:07
JMV
P91-10193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 30

piFull-Service Analytical &
R I S 1 Y, I Environmental Solutions
LABORATORIES, ING
'ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Laboratory Report
08/21/2019
Client Sample ID: 4th Creek Sludge
Prism Sample ID: 9080093-01
Prism Work Order: 9080093
Time Collected: 08/07/19 09:55
Time Submitted: 08/07/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Pentachlorophenol BRL mg/L 0.25 0.011 1 *8270E 8113/19 18:07 JMV P91­10193
Pyridine BRL mg/L 0.25 0.0016 1 *8270E 8/13/19 18:07 JMV P91­10193
Surrogate Recovery Control Limits
2,4,6-Tdbromophenol
91 %
43-140
2-Fluorobiphenyl
97 %
44-119
2-Fluorophenol
65 %
19-119
Nitrobenzene-d5
90 %
44-120
Phenol-d5
42 %
11-52
Terphenyl-d14
98 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
*8260D
8/13/19 19:18
KDM
P91­10197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
*8260D
8/13/19 19:18
KDM
P91­10197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
*8260D
8/13/19 19:18
KDM
P91­10197
Benzene
BRL
mg/L
0.025 0.0034
1
*8260D
8/13119 19:18
KDM
P91­10197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
*8260D
8/13/19 19:18
KDM
P91­10197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
*8260D
8/13/19 19:18
KDM
P91­10197
hloroform
BRL
mg/L
0.30 0.0048
1
*8260D
8/13/19 19:18
KDM
P91­10197
ethyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
*8260D
8/13/19 19:18
KDM
P91­10197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
*8260D
8113119 19:18
KDM
P91­10197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
*8260D
8/13119 19:18
KDM
P91­10197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
*8260D
8/13/19 19:18
KDM
P91­10197
Surrogate Recovery Control Limits
4-Bromofluorobenzene 103 % 80-124
Dibromofluoromethane 107 % 75-129
Toluene-d8 94 % 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 30

Laboratory Report
Full -Service Analytical &
3 I S 1 d 1 Environmental Solutions 08/21/2019
A31=1
7U noTORIEg ING
amity of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: 3rd Creek Sludge
Attn: Ken Galloway Prism Sample ID: 9080093-02
P.O. Box 1111 Prism Work Order: 9080093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/07/19 09:45
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
18.6
% by
0.100
0.100 1
*SM2540 G
8/16119 8:30
EDV
P9H0264
Weight
Corrosivity-pH
4.4
pH Units
1
*9045D
8/9/19 13:40
BMS
P9H0161
Ignitability
BRLA
mm/sec
0.10
1
*1030
8/9/19 8:25
BMS
P91-10143
Temperature
22
pH Units
1
*9045D
8/9119 13:40
BMS
P9H0161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/13/19 7:30
TBL
P91-10174
TCLP Extraction
Complete
N/A
1
*1311
8/13/19 7.50
MMR
P91-10185
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000034
1
*7470A
8/15/19 13:57
MMR
P91-10261
Arsenic
BRL
mg/L
0.10
0.030
1
*6010D
8/13/19 17:13
JAB
P91-10203
Barium
BRL
mg/L
5.0
0.010
1
*6010D
8/13119 17:13
JAB
P91-10203
Cadmium
BRL
mg/L
0.025
0.0020
1
*6010D
8/13/19 17:13
JAB
P91-10203
Chromium
BRL
mg/L
0.25
0.015
1
*6010D
8/13/19 17:13
JAB
P91-10203
Lead
BRL
mg/L
0.050
0.020
1
*6010D
8/13/19 17:13
JAB
P91-10203
elenium
BRL
mg/L
0.15
0.063
1
*6010D
8113/19 17:13
JAB
P91-10203
oilver
BRL
mg/L
0.25
0.0045
1
*6010D
8/13/19 17:13
JAB
P91-10203
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00090
1
*8081B
8/14119 17:00
ZRC
P91-10227
Dieldrin
BRL
mg/L
0.00050
0.000068
1
*8081B
8/14/19 17:00
ZRC
P91-10227
Endrin
BRL
mg/L
0.00050
0.000068
1
*8081B
8114/19 17:00
ZRC
P91-10227
gamma-BHC
BRL
mg/L
0.00050
0.000030
1
*8081B
8/14119 17:00
ZRC
P91-10227
Heptachlor
BRL
mg/L
0.00050
0.000065
1
*8081B
8/14/19 17:00
ZRC
P91-10227
Heptachlor Epoxide
BRL
mg/L
0.00050
0.00011
1
*8081B
8/14/19 17:00
ZRC
P9H0227
Methoxychlor
BRL
mg/L
0.00050
0.000090
1
*8081B
8114/19 17:00
ZRC
P91-10227
Toxaphene
BRL
mg/L
0.025
0.0018
1
*808113
8/14/19 17:00
ZRC
P91-10227
Surrogate Recovery Control Limits
TCLP Semivolatile Organic Compounds by GC/MS
Decachlorobiphenyl
Tetrachloro-m-xylene
82 %
83 %
13-186
40-134
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
*8270E
8/13119 18:30
JMV
P91-10193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
*8270E
8/13119 18:30
JMV
P91-10193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*8270E
8/13/19 18:30
JMV
P91-10193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
*8270E
8/13/19 18:30
JMV
P91-10193
3/4-Methylphenol
BRL
mg/L
0.050
0.0025
1
*8270E
8/13/19 18:30
JMV
P91-10193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
8/13/19 18:30
JMV
P91-10193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
*8270E
8/13/19 18:30
JMV
P91-10193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
*8270E
8/13119 18:30
JMV
P9H0193
itrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
8/13119 18:30
JMV
P91-10193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 30

,R S M Laboratory Report
gh Full -Service Analytical 8
10�
Environmental Solutions 08l21l2019
L soR TOFIEs, INC.
'ity of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: 3rd Creek Sludge
Attn: Ken Galloway Prism Sample ID: 9080093-02
P.O. Box 1111 Prism Work Order: 9080093
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 08/07/19 09:45
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DaterFime
ID
Pentachlorophenol
BRL
mg/L
0.25 0.011
1
*8270E
8/13/19 18:30
JMV
P91-10193
Pyridine
BRL
mg/L
0.25 0.0016
1
*8270E
8/13/19 18:30
JMV
P91-10193
Surrogate
Recovery
Control Limits
2,4,6-Tdbromophenol
106 %
43-140
2-Fluorobiphenyl
106 %
44-119
2-Fluorophenol
72 %
19-119
Nitrobenzene-d5
94 %
44-120
Phenol-d5
46 %
11-52
Terphenyl-d14
98 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
*8260D
8/13/19 19:52
KDM
P9H0197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
*8260D
8/13/19 19:52
KDM
P9H0197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
*8260D
8/13119 19:52
KDM
P91-10197
Benzene
BRL
mg/L
0.025 0.0034
1
*8260D
8/13/19 19:52
KDM
P91-10197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
*8260D
8/13/19 19:52
KDM
P91-10197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
*8260D
8/13/19 19:52
KDM
P91-10197
hloroform
BRL
mg/L
0.30 0.0048
1
*8260D
8/13/19 19:52
KDM
P9H0197
ethyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
*8260D
8/13/19 19:52
KDM
P91-10197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
*8260D
8/13/19 19:52
KDM
P91-10197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
*8260D
8/13/19 19:52
KDM
P91-10197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
*8260D
8/13119 19:52
KDM
P91-10197
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
104 %
80-124
Dibromofluoromethane
104 %
75-129
Toluene-d8
95 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 30

Full -Service Analytical &
' ism Environmental Solutions
�--TOFIES. INC
3ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville. NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Laboratory Report
08/21 /2019
Client Sample ID: Sta-Lime
Prism Sample ID: 9080093-03
Prism Work Order: 9080093
Time Collected: 08/07/19 09:30
Time Submitted: 08/07/19 16:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date[Time
ID
General Chemistry Parameters
% Solids
76.6
% by
0.100
0.100 1
*SM2540 G
8/16/19 8:30
EDV
P91-10264
Weight
Corrosivity-pH
12
pH Units
1
*9045D
819119 13:40
BMS
P91­10161
Ignitability
BRLA
mm/sec
0.10
1
*1030
8/9/19 8:25
BMS
P9H0143
Temperature
22
pH Units
1
*9045D
8/9/19 13:40
BMS
P91­10161
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311 ZHE
8/13119 7:30
TBL
P91­10174
TCLP Extraction
Complete
N/A
1
*1311
8/13/19 7:50
MMR
P9H0185
TCLP Metals
Mercury
BRL
Arsenic
BRL
Barium
BRL
Cadmium
BRL
Chromium
BRL
Lead
BRL
=lenium
BRL
oilver
BRL
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
Dieldrin
BRL
Endrin
BRL
gamma-BHC
BRL
Heptachlor
BRL
Heptachlor Epoxide
BRL
Methoxychlor
BRL
Toxaphene
BRL
mg/L
0.010
0.000034 1
mg/L
0.10
0.030 1
mg/L
5.0
0.010 1
mg/L
0.025
0.0020 1
mg/L
0.25
0.015 1
mg/L
0.050
0.020 1
mg/L
0.15
0.063 1
mg/L
0.25
0.0045 1
mg/L
0.0025
0.00090 1
mg/L
0.00050
0.000068 1
mg/L
0.00050
0.000068 1
mg/L
0.00050
0.000030 1
mg/L
0.00050
0.000065 1
mg/L
0.00050
0.00011 1
mg/L
0.00050
0.000090 1
mg/L
0.025
0.0018 1
*7470A
8/15/19
14:12
MMR
P91­10261
*6010D
8113/19
17:21
JAB
P91­10203
*6010D
8/13/19
17:21
JAB
P91­10203
*6010D
8/13/19
17:21
JAB
P91­10203
*6010D
8/13/19
17:21
JAB
P9H0203
*6010D
8/13/19
17:21
JAB
P91­10203
*6010D
8/13/19
17:21
JAB
P91­10203
*6010D
8/13119
17:21
JAB
P91­10203
*8081B
8/14/19
17:12
ZRC
P91­10227
*8081B
8/14/19
17:12
ZRC
P9H0227
*8081B
8/14/19
17:12
ZRC
P9H0227
*8081B
8/14/19
17:12
ZRC
P91­10227
*8081B
8/14/19
17:12
ZRC
P91­10227
*8081B
8/14/19
17:12
ZRC
P9H0227
*8081B
8/14/19
17:12
ZRC
P91­10227
*8081B
8/14/19
17:12
ZRC
P9H0227
TCLP Semivolatile Organic Compounds by GC/MS
Surrogate
Decachlorobiphenyl
Tetrachloro-m-xylene
Recovery
75 %
97 %
Control Limits
13-186
40-134
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0036
1
*8270E
8/13/19 18:53
JMV
P91-10193
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0045
1
*8270E
8/13/19 18:53
JMV
P91­10193
2,4-Dinitrotoluene
BRL
mg/L
0.012
0.0042
1
*8270E
8/13/19 18:53
JMV
P91­10193
2-Methylphenol
BRL
mg/L
0.050
0.0024
1
*8270E
8/13/19 18:53
JMV
P91­10193
3/4-Methylphenol
BRL
mg/L
0.050
0.0025
1
*8270E
8/13/19 18:53
JMV
P91­10193
Hexachlorobenzene
BRL
mg/L
0.020
0.0039
1
*8270E
8/13/19 18:53
JMV
P9H0193
Hexachlorobutadiene
BRL
mg/L
0.050
0.0045
1
*8270E
8/13/19 18:53
JMV
P91­10193
Hexachloroethane
BRL
mg/L
0.050
0.0037
1
*8270E
8/13/19 18:53
JMV
P91­10193
itrobenzene
BRL
mg/L
0.050
0.0038
1
*8270E
8/13/19 18:53
JMV
P9H0193
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 30

Full -Service Analytical &
/h-�.- R I S M I Environmental Solutions
�7LABORATORiES ING
'ity of Statesville, NC
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Laboratory Report
08/21 /2019
Client Sample ID: Sta-Lime
Prism Sample ID: 9080093-03
Prism Work Order: 9080093
Time Collected: 08/07/19 09:30
Time Submitted: 08/07/19 16:00
Parameter
Result Units Report MDL Dilution
Method Analysis Analyst Batch
Limit Factor
Date/Time ID
Pentachlorophenol
BRL mg/L 0.25 0.011 1
*8270E 8113/19 18:53 JMV P91­10193
Pyridine
BRL mg/L 0.25 0.0016 1
*8270E 8/13/19 18:53 JMV P91­10193
Surrogate
Recovery Control Limits
2,4,6-Tribromophenol
114 %
43-140
2-Fluorobiphenyl
104 %
44-119
2-Fluorophenol
73 %
19-119
Nitrobenzene-d5
92 %
44-120
Phenol-d5
46 %
11-52
Terphenyl-d14
95 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.0035
1
*8260D
8/13/19 20:26
KDM
P9H0197
1,2-Dichloroethane
BRL
mg/L
0.025 0.0041
1
*8260D
8/13119 20:26
KDM
P91­10197
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.0042
1
*8260D
8/13/19 20:26
KDM
P9H0197
Benzene
BRL
mg/L
0.025 0.0034
1
*8260D
8/13/19 20:26
KDM
P91­10197
Carbon Tetrachloride
BRL
mg/L
0.025 0.0055
1
*8260D
8/13119 20:26
KDM
P91­10197
Chlorobenzene
BRL
mg/L
5.0 0.0034
1
*8260D
8/13119 20:26
KDM
P91­10197
hloroform
BRL
mg/L
0.30 0.0048
1
*8260D
8/13/19 20:26
KDM
P91­10197
ethyl Ethyl Ketone (2-Butanone)
BRL
mg/L
10 0.0078
1
*8260D
8/13/19 20:26
KDM
P91-10197
Tetrachloroethylene
BRL
mg/L
0.035 0.0031
1
*8260D
8/13/19 20:26
KDM
P91­10197
Trichloroethylene
BRL
mg/L
0.025 0.0046
1
*8260D
8/13/19 20:26
KDM
P91-10197
Vinyl chloride
BRL
mg/L
0.010 0.0041
1
*8260D
8/13/19 20:26
KDM
P91­10197
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101 %
80-124
Dibromofluoromethane
88 %
75-129
Toluene-d8
96 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 30

Sample Extraction Data
Prep Method: Solids, Dry Weight
ab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10264
30
g
30 g
08/15/19 15:05
9080093-02
P91-10264
30
g
30 g
08/15/19 15:05
9080093-03
P91-10264
30
g
30 g
08/15/19 15:05
Prep Method: 1311
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10185
100
g
2000 mL
08/12/19 15:45
9080093-01
P91-10174
12.5
g
250 mL
08/12/19 13:40
9080093-02
P91-10174
12.5
g
250 mL
08/12/19 13:40
9080093-02
P91-10185
100
g
2000 mL
08/12/19 15:45
9080093-03
P91-10185
100
g
2000 mL
08/12/19 15:45
9080093-03
P91-10174
12.5
g
250 mL
08/12/19 13:40
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10203
10
mL
50 mL
O8/13/19 10:43
9080093-02
P91-10203
10
mL
50 mL
08/13/19 10:43
9080093-03
P91-10203
10
mL
50 mL
08/13/19 10:43
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10261
20
mL
30 mL
08/15/19 10:30
9080093-02
P9H0261
20
mL
30 mL
08/15/19 10:30
9080093-03
P91-10261
20
mL
30 mL
08/15/19 10:30
rep Method: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10227
200
mL
10 mL
08/14/19 9:08
9080093-02
P91-10227
200
mL
10 mL
08/14/19 9:08
9080093-03
P91-10227
200
mL
10 mL
08/14/19 9:08
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10193
200
mL
1 mL
08/13/19 10:30
9080093-02
P91-10193
200
mL
1 mL
08/13/19 10:30
9080093-03
P9H0193
200
mL
1 mL
08/13/19 10:30
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9080093-01
P91-10197
1
mL
10 mL
08/13/19 8:19
9080093-02
P91-10197
1
mL
10 mL
08/13/19 8:19
9080093-03
P91-10197
1
mL
10 mL
08/13/19 8:19
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 30

Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
ib Number
Analysis
y080093-01 Herbicides TCLP (Sub)
9080093-02 Herbicides TCLP (Sub)
9080093-03 Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number Analysis
9080093-01
Reactivity, Cyanide (Sub)
9080093-01
Reactivity, Sulfide (Sub)
9080093-02
Reactivity, Cyanide (Sub)
9080093-02
Reactivity, Sulfide (Sub)
9080093-03
Reactivity, Cyanide (Sub)
9080093-03
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 30

Full-
R�J�i l �ISM
IEnviService AnalyticalsEnvironmental Solutions PAGE OF QUOTE STOENSURE PROPER BIWNG--
:w_ - 'I--UIBORATORIES INC. i Samples INTACT upon arrival?
449 Spring brook Road • Charlotte, NC 28217 Project Name: _ - Received ON WET ICE?
Phone [phone] - Fax: c7�04152e5-0409 d,9 Short Hold Analysis: (Yes) (No) UST Project (Yes) (NO) PROPER PRESERVATIVES indicated?.
Client:Com aLl Name:: c:-�'v o i- .]4, ��r'lftIle 'Please ATTACH any project specific reporting (QC LEVEL III Ill M Received WITHIN, HOLDING TIMES?
p y provisions andior QC Requirements CUSTODY SEALS" INTACT?
Report_TolContact.Name ��Cj� G�'r�owriu . Invoice To: VOLATILES rec'd W/OUT HEADSPACE?
Repoiting Address: Address: PROPER-CQNTAINESS used?,
TEMP: Therm IDS . / •. Observed:
oH.......•fA4_QhUs 7;A7r� r_-d�1ru__Mn•rl re-�ri rs�rr - _
YES N,
L
oC
Email Address:
Purchase Order NoJBifling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
EDD Type: PDF Excel_Other
Requested Due Date 01 Day 0 2 Days 133 Days a 4 Days. n 5 Days
Certification: NELAC DOD FL NC
r�
Site Location Name: o to r� 1. s^f �!
"Wbilking Days" Lt6-9Days 1] Standard 10 days ;DRush Work:Must Be
p
Pre-Aproved Samples received'after
SC OTHER N/A
Site Location Physical Address:.6 73 ila II foern
14.00 wig be processed nod business day..
I?J. Turnaround time is based anbusiness days, excludingyreeuerids.add holiaairs
Water Chlorinated: YES NO
(SEEREVH2SE:-ORTERh95 & CONoiTtON3 REG.I1Ri1tN6 SERVICr-S
'RENDERED BY PRISM MORATORIES,INC.TOCLIEIM
Sample Iced Upon Collection: YES NO_
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
MATRD(
(SOIL,
WATER OR
SAMPLE CONTAINER
PRESERyA-
TNES
ANALYSIS REQUESTED —
REMARKS
PRISM
LAB
HOURS
SLUDGE)
SEE BELOW
No-
SIZE
ID NO.
qf4 C cQsw_k sIA
84-19
09:63
'3ak CRE k S iw I.
8- 7- l9
09,"V 6
Telk
01,-
S+A-4,we_
S- 7- /9
09.3
S
G-
TC
P
e- i
S
Sampler's Signature %
Sampled By (Print Name)V Sidi
LtlVr')C� Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
(submitted in writing to the Prism Project Manager. There will be charges y changes after analyses have been initialized.
ONLY
Re1in4r hed,By: (Slgnntule)
�. r
RewIV 'y: (51 .ahua) D� A7 !Hours
Additional Comments: Site Arrival Time:
Rolin hod By:: (Signature)
tid .,(Sig c+ture) Dale Site Departure Time:
up o (S gnat i
/ Rarah�d Far Prism Lettliratoric^+B . Tech Fee:
Field
I�l� /�,`�
;00. J.
Mileage:
Ip F'Sf+IPMOM NDTE:ALLSAMPLECOOLERSSHOULDBETAPPDSHUTWITH CUSTODY SEALS FOR TUANZ PORTATIONTOTHE RATORY. COCGreupNo.
' SAMPLES ARE NOT ACCEPTED AND VFAIFIEDAGAINST COC UNTIL RECEIVEDATTH ORATORY.. /%� n
-
1 E , UPS ❑ ❑ Hand -delivered Prism Field Service U01hur Oo
ES: UST GROUNDWATER: I DRINKING WAFER: ! SOLID WASTL3:. RCRA: CERCLA LANDFILL: OTHER: SEE REVERSE
❑ SCI ❑ NC ❑ SC I ❑ NC ❑ Sc
FOR
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NC ❑ SC I NC ❑ SC j NC ❑ SC NC ❑ SC I ❑ NC ❑ SC) ❑ NC ❑ SC '
'
❑❑
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❑❑
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v10� r -abut, r L_= reuun-urea cap vow = volante organics Analysis (Zero Head Space)

P
ACCESS
ANALYTICAL, INC.
Primary Data Review By
Authorized Signature
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
9080093
LABORATORY REPORT NUMBER
219081317
DATE
08116/2019
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory # 01955
Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 219081317 Page 12 of 30

LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
,AN.ALY TI��►L 'RESU L,
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 08/16/2019
GCAL ReportY 21y90e13II17
Project 9080093
Deliver To Additional Recipients .
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
S pt
1702PJLA
Don EIAP
5
resun� - eoRARO'
Lab Report#: 219081317 Page 2 of 12
Page 13 of 30

Report#: 219081317
Project ID: 9080093 Report Date: 08/16/2019
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOCI Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD —see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,.
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
-fir -
/
Authorized Signature
GCAL Report 219081317
Lab Report#: 219081317 Pane I of 19
Page 14 of 30

0'% Report#: 219081317
Project ID: 9080093 Report Date: 08/16/2019
Certifications
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentuckv
95
Louisiana
01955
Marvland
01955
Massachusetts
01955
-Michigan
01955
01955
-Mississippi
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
-Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 219081317 Page 4 of 12
Page 15 of 30

Report#: 219081317
Project ID; 9080093
Case Narrative
Client: Access Analytical Report: 219081317
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Report Date: 08/16/2019
Lab Report#: 219081317
Page 16 of 30

Report#: 219081317
Project ID: 9080093
Sample Summary
Report Date: 08/16/2019
GCAL ID _
Client ID
Matrix
' Collect Date/Time
Receive Date/Time
21908131701
4th Creek Sludge
Solid
08/07/2019 09:55
08/13/2019 10:20
21908131702
3rd Creek Sludge
Solid
08/07/2019 09:45
08/13/2019 10:20
21908131703
Sta-Lime
Solid
08/07/2019 09:30
08/13/2019 10:20
Lab Report#: 219081317
Page 17 of 30

Report#: 219081317
y ProjectID: 9080093 Report Date: 08/16/2019
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Lab Report#: 219081317
Page 18 of 30

E Report#: 219081317
3 Project ID: 9080093 Report Date: 08/16/2019
Sample Results
Collect Date
08/07/2019 09:55
GCAL ID
21908131701
4th Creek Sludge
Receive Date
08/13/2019 10:20
Matrix
Solid
El
12B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 08116/201914:48 MOS 665678
CAS# Parameter
57-12-5R Reactivity Cyanide
EPA 9034
Result
DL
LOQ
Units
248U
248 -
248
mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665476 EPA 7.3.4.2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result
DL
LOQ
Units
248U
248
248
mg/kg
Collect Date 08/07/2019 09:45 GCAL ID 21908131702
3rd Creek Sludge Receive Date 08/13/201910:20 Matrix Solid
Ef
12B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 08/16/2019 14:50 MOS 665678
CAS#
Parameter
57-12-5R
Reactivity Cyanide
EPA 9034
Result DL LOQ Units
250U 250 250 mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665476 EPA 7.3.4.2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS#
Parameter
Result
DL
LOQ
Units
18496-25-8R
Reactivity Sulfide
25OU
250
250
mg/kg
Lab Report#: 219081317 Pace 8 of 12
Page 19 of 30

Report#: 219081317
Project ID: 9080093 Report Date: 08/16/2019
Sample Results
5ia-Lime Collect Date 08/07/2019 09:30 GCAL ID 21908131703
Receive Date 0811312019 10:20 Matrix Solid
A 9O12B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665475 EPA 7.3.3.2 (1997) 1 08/16/2019 14:53 MOS 665678
CAS#
57-12-5R
Parameter
Reactivity Cyanide
Result
DL
LOQ
Units
248U
248
248
mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
08/16/2019 08:00 665476 EPA 7.3.4.2 (1997) 1 08/16/2019 13:16 RYC 665676
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result DL LOQ Units
248U 248 248 mg/kg
Lab Report#: 219081317
Page 20 of 30

Report#: 219081317
Project ID: 9080093
General Chemistry QC Summary
Report Date: 08/16/2019
Analytical Batch Client ID
M8665476
LCS665476
665676 GCALID
1952122
1952123
Prep Batch Sample Type
MB
LCS
665476 Prep Date
08/16/2019 08:00
08/16/2019 08:00
Prep Method Analysis Date
08/16/2019 13:16
08/16/2019 13:16
EPA 7.3.4.2 (1997) Matrix
Solid
Solid _
EPA 9034
Units
mg/kg
Spike
Result
%R
I
Control
Result
DL
Added
Limits%R ii
Reactivity Sulfide 18496-25-8R
250U
1 2501
10001
1026
103
47 - 135
Analytical Batch Client ID
MB665475
LCS665475
665678 GCAL ID
1952119
1952120
Prep Batch Sample Type
MB
LCS
665475 Prep Date
08/16/2019 08:00
08/16/2019 08:00
Prep Method Analysis Date
08/16/2019 14:39
08/16/201914:41
EPA 7.3.3.2 (1997) Matrix
Solid
Solid
EPA 9012B
Units
mg/kg
Spike
Result
%R
Control
Result
DL
Added
Limits%R .
Reactivity Cyanide 57-12-5R
NDI
2501
250
29.4
12
1-25
Lab Report#: 219081317 Pa e 10 of 12
Page 21 of 30

Client ID: 4565 - Access Analytical
SDG: 219081317
PM: DLH
Analytical &
Solutions
SUBCONTRACTORDER
75
&:IullUg:v;c IF ,:SACE_-7Prism Laboratories, Inc.
"Iuh"
9080993
SKNI71ING. TAVIORATORY!
_M-VDC-, L;%ROR'%Td'Rvt
Prism Laboratories, Inc.
GUYCOOSI Analytical Labs, Tim.
R 0. Box 1-40543
107S I Coursev 131vd
Chirlouc, NC 23224-0543
Baton Rougc, LA 70S 16
Phonc'. 300-529-6364
Phonc:(2.25) 769-4900
Fa-.,: 704-525-0409
Fax: [phone]
Robbi A. Jones
Analysis Duo Expires Laboratory ID C.M—ws
Sample 11): 9080093-01 Solid S.-PIA: 09107119 09:55 �k
Rz-ih-hy, Sulfide (Sub) 0811 4"i 9 07:55
Reactivity, Cya.ldc (Sub) ORP- V) 9 09:55
5l.'wp S .71,
�Sample ID: 9080093-02 Solid S--Pl-d: OV07119 09:45 Crek
Rczcii,icy. Su? fide (Sub? OS AIO 09:43
Rcuclift, Cyanide (Sub) 011in- 1"19 09:43
C'uu..'-m S.'PIA.F.d..
S—fid, In; 9080093-03 I Solid S—Pl-d! 0310711) 09:10
R-ctivity, Sulfide (Sub) OSIHM 01:30
Rc;tcti icy, Cyanide (S',)b) OV-1 V 19 119:30
cmil'i— S;q"'Ucd, I
ri
f�-V 11
RO.'—I By
V
Ily Rmilzo B., 0:11,
IW-*cd ily Dare R--I Ry D.g�
0
I Page 1 of
I Page 22 of 30

11%
SAMPLE RECEIVING CHECKLIST
IIIIIII III IIII
II
III I
� IIIIIII
* 2 1 9 0
6 1
3 1
7
SAMPLE DELIVERY GROUP
219081317'
CHECKLIST
YES
NO.
Client PM CLH
Transport Method
Samples received with proper thermal preservation?
4565 - Access Analytical
FECDC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
®
0.
❑
❑
Profile Number
I�aceived Qj
80251
Savage, Tiffany R
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
®
®
❑
❑
Line ltem(s)
Receive Date(s)
2 - Solid
08/13/19
Preservative added to any containers?
El
R
If received, was headspace for VOC water containers < 6mm?
®
❑
Samples collected in containers provided by GCAL?
❑
n
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer ID: E4
Temp °C
None
None
TI59-6349-3542
0.2
NOTES
Revision 1.6
Fbge 1 of 1
Lab Report#: 219081317 Page 12 of 12

{, ACCF,S5
p ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
9080093
LABORATORY REPORT NUMBER
1908C31
DATE
August 19, 2019
Prirnary Data Review By Secondary Data Review By
J Ashley Amick
Chris Pafford
Project Manager, AES
PLEASE NOTE:
Project Manager, Access Analytical
aamick?,axs-inc.corn
Unless otherwise noted, all analysis on this report performed atAnalytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDHEC certified laboratory # 98016, NCDENR certified lab 9 562, GA certified lab 4 FL-E87582,
NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
- Local support services for this project are provided by Access Analytical; Inc. Access Analytical is a
representative ofAES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll tee at 883.315.4243
Pag Page 24 of 30

cc h -�e �•�S o � �o n 9 I { 2 � E� �-
t Sn Fulf Setvlce Analytical &
v Environmental Solutions
,y""� ��-. LA50:.ACDf•JE.^�IVC
SUBCONTRACT ORDER
Ccllirjcatioli:' ELAC_ USACE_
Prism Laboratories, Inc Nc >� SC Other I
9080093 NIA I
1
SF.NDINC LARORATORY;
:R•ECE'E41NG LATLn12AT6jL :
t` Prism Laboratories, Inc.
Analytical Environmental Seiviccs, Inc,
P. 0. Box 240543
30SO Presidential Parkway
Cbarlolrc, NC'_'3324-0543
Atlanta, GA 30340
Phone: [phone]
Phone :(770) 457-S177
rnx: 704-525-0409
Fax: NA
Project Manager. Rabbi A. Jones
Analysis Due
Expires
Laboratory 1D CD-c"Is
� �� V �•��
Samplc ID: 9080093-01 Solid
S—it,10; 08107/19 09:55
:' �
llclbicidcs TC'LP (Sub)
031,4119 09t55
Cnnhri:r<v:a Sap/rlicd,•"•
��
lu �, Le
C
llerbickks TCLP (Sub) WWI 09:45
Carrnincrs .Snppl ic•<!: �„ r
Sample 1D: 9080093-03 Solid Sampled: 08/07/19 09:311 - _ - • - ^ �i? r tl
HcLbicides TrLP(Sub) Well 9 09:3 0
C'nrrrniners Supp1•"w1:
17;nc
r /'f
Rcka.:d Bg Date Ruecivud B'. )') Es Dart•
I?cicaxd By Date n-:: rrcd Fsp f'j Dzt:
1(t cauJ B, Ga:c Rocci:ca r.;y I?�•:
Page 1 of
7-1
Pag Page 25 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
4th Creek Sludge
Lab Order
1908C31
Tag Number:
9080093-01
Project Name:
9080093
Collection Date:
8/7/2019 9:55:00 AM
Lab ID:
190801-001A
Matrix:
Solid
Analyses
Result
Qual MDL
Reporting
Limit
Units BatchID
DF Date Analyzed Analyst
HERBICIDES, TCLP SW131118151A,
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
mg/1- 283568
1 08/16/2019 14:32 HB
2,4-D
BRL
0.051
0.20
mg/L 283568
1 08116/201914:32 HB
Surr: DCAA
69.1
0
49.4-120
%REC 283568
1 08/16/2019 14:32 HB
Qualifiers: IValue exceeds maximum conmininanl level E Estimated wlue above quanUmuon range
BRL Not Detected at M. DL S Spike Recovery outside limns due to matrix
H Holding tunes for preparation or anal%sts exceeded > Grmter than Result talue
N Analyze not NELAC cemGed J Estimated talue detected below Reporting Limit
B Anahte detected in the associated method blank < Less than Result salue
Page Page 26 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
3rd Creek SLUDGE
Lab Order
190801
Tag Number:
9080093-02
Project Name:
9080093
Collection Date:
W12019 9:45:00 AM
Lab ID:
1908C31-002A
Matrix:
Solid
Analyses Result Qua[ MDL Reporting Units BatchID DF Date Analyzed Analyst
Limit
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL
2,4-D BRL
Surr: DCAA 65.6
Qualifiers: • Valuc exceeds maximum contaminant level
BRI. Not Detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analvte detected in the associai d method blank
(SW3510C)
0.030 0.20 mg/L 283568 1 08/16/201914:53 HB
0.051 0.20 mg/L 283568 :1 08/16/201914:53 HB
0 49.4-120 9/-REC 283568 1 08/16/201914:53 HB
E Estimated value above quami+ation range
S Spike Recovery outside limits due to matrix
Greater than Result value
J Estimated value detected below Reporting Limit
< Less torn Result value
Pag Page 27 of 30

Analytical Environmental Services, Inc
Date: 19-Aug-19
Client:
Prism Laboratories
Client Sample ID:
Sta-Lime
Lab Order
1908C31
Tag Number:
9080093-03
Project Name:
9080093
Collection Date:
gn12019 9:30:00 AM
Lab ID:
1908C31-003A
Matrix:
Solid
Analyses
Result
Qual MDL
ReportingLimit
Units
BatchlD
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
mF/L
283568
108/16/2019 15:14 HB
2,4-D
BRL
0.051
0.20
mg/L
283568
1 08116/201915:14 HB
Surr: DCAA
66.2
0
49.4-120
%REC
283568
1 08/16/2019 15:14 HB
Qualifiers: ° Value exceeds maximum conmminent level E Estimated valueabove quantitation range
BRL Not Detected at MDL S Spike Recovery outside limns due to matrix
H Holding times for preparation or analysis exceeded > Greater than Result value
N Analyte not NELAC cenifcd 1 Estimated value detected below Reporting Limit
B Analvte detected in the associated melhod blank < Less than Result value
Pag Page 28 of 30

ANALYTICAL
Evtrutonsrr:N r,u
:SAS SiiRviLLas.1'\C.
1. Client Name: Access Analytical, Inc.
2. Carrier: FedEx ❑o UPS ❑ USPS ❑ Client❑ Courier Othei _
3,
4.
5,
6.
7.
8.
9,
10.
11.
12,
SAMPLE/COOLER RECEIPT CHECKLIST
Yac N. N/A
Details
AES Work Order Number: 190801
- _'Clear .: . .vwlas'
Comments
Shipping container/cooler received in good condition?
a
damaged ❑ leaking ❑ other❑
Custody seals present on shipping container?
e
Custody seals intact on shipping container?
•
'Temperature blanks present?
o
Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for
temperature recordings,]
®
©
O
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (CDC) present?
- .®
Chain of Custody signed, dated, and timed when relinquished and received?
•
—
Sampler name and/or signature on CDC?
o
Were all samples received within holding time?
;•
TAT marked on the CDC?
If no TAT indicated, proceeded with standard TAT per Terms & Conditions.
13. Cooler 1 Temperature 0.7 °C Cooler 2 Temperature
14. Cooler 5 Temperature °C Cooler 6 Temperature
15. Comments.,
16,
17,
18.
19,
20.
21.
22.
23.
24,
25.
26,
°C Cooler 3 Temperature °C Cooler 4 Temperature °C
°C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials). MJ 8/13/19
Vps Nn N/A Details Comments
Were sample containers intact upon receipt?
o
Custody seals present on sample containers?
o.
Custody seals intact on sample containers?
0OF
Do sample container labels match the CDC?
0
®
®
incomplete info ❑ illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the CDC?
'v
Were all of the samples listed on the CDC received?
G)
Q
C)
samples received but not listed on CDC ❑
samples listed on CDC not received ❑
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
•.
'Were samples received in appropriate containers?
e :
Were VOA samples received without headspace (< 1/4" bubble)?
•
Were trip blanks submitted?
listed on CDC ❑ not listed on CDC ❑
27. Comments:
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). EW 8/13/19
checked at Sample Receipt. Yes No N/A Details Comments
28.1 Have containers needing chemical preservation been checked? * U o.
29, Containers meet preservation guidelines? •
r� 30; -Vas pH adjusted at Sample Receipt? •
m Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
(C) I certify that I have completed sections 28-30 (dated initials).
oChecklist 6.9.17 Rev 2 Locked_
EW 8/13/19
Page 6 of 7

Analytical Environmental Services, Inc
Client: Prism Laboratories
Project Name: 9080093
NVorlcorder: 190801
Date: 19-Aug-19
ANALYTICAL QC SUMMARY REPORT
BatchlD: 283568
Sample ID: N[B-283568
Client ID:
Units: mg/L
Prep Date: 08/15/2019
Run No: 405118
SampleType: MBLK
TeSLCode: IIERBICIDES,TCLP SW1311/8151A
BatchlD: 283568
Analysis Date: 08/16/2019
Seq No: 9101944
Analytc
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2.4,5-TP (Silvex) BRL 0.20
2.4-D BRL 0.20
Sun•: DCAA 0.3375 0 0.5000 67.5 49.4 120
Sample ID: LCS-283568
Client ID:
Units: mg/L
Prep Date: 08/15/2019
Run No: 405118
SampleType: LCS
TestCode: HERBICIDES,TCLP SW1311/8151A
BatchlD: 283568
Analysis Date: 08/16/2019
Seq No: 9101945
Analytc
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4.5-TP (Silvex)
0.3451
0.20
0.5000
69.0
49
120
2.4-D
0.3658
0.20
0.5000
73.2
50.9
120
Surr: DCAA
0.3548
0
0.5000
71.0
49.4
120
Sample ID: 1908C31-003AMS
Client ID:
Sta-Lime
Units: mg/L
Prep Date: 08/15/2019
Run No: 405118
SampleType: MS
TestCode:
HERBICIDES, TCLP SW1311/8151A
BatchID: 283568
Analysis Date: 08/16/2019
Seq No: 9101950
Analyte
Result
RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) 0.3637 0.20 0.5000
2,4-D 0,3913 0.20 0.5000
Surr: DCAA 0.3670 0 0.5000
n
W
iQ Qppllftceso - Greater than Resuh,slue
BRL Below rcporlmg hat❑
Cl)
O .I Eiinnited .clue detected below Reporting Lunn
O_
Rpl Luce Rcponmg Lunn
W
O
72.7 48.2 120
78.3 45 130
73.4 49.4 120
< Less than Result value B Acolyte detected in the associated method blank
E Estimated (value above guaniitation range) H Holding times for preparation or analysis exceeded
N Analytc not NELAC certified R RPD outside limits due to matrix
S Spike Recovery outside limits due to matrix
Page 7 of 7

NC Certification No. 402 Case Narrative
M1
m
Full-Service Analytical & NC Drinking Water Cert No. 37735 12/5/19 11:46
� IS I Environmental Solutions SC Certification No. 99012
v,®77LA60RATORIE$ INC.
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Project: StaLime
Lab Submittal Date: 11/25/2019
Prism Work Order: 9110421
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[NaI/SQRT{([Ca]*[Mg])/2}
SAR = [ 180/23 ] / SQRT { ( [2400/201 + [0.047/12.2]) / 2 }
SAR = 1.0
concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
PAN Equation = 0.3 * (TKN - Ammonia) + 0.5 * (Ammonia) +
Nitrate -Nitrite
PAN = 0.3 * (4000 - 120) + 0.5 * (120) + 9.3
PAN = 1200 mg/kg
Equation uses Mineralization Rate (MR) for Aerobically Digested
Solids (0.3)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 17

Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Terri W. Cole
Project Manager
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole
Project Manager
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 17

Sample Receipt Summary
Full -Service Analytical &
/�7UBORATORIEr,PI� I S MEvironmental Solutions 12/05/2019
(—
Prism Work Order: 9110421
,lient Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
Stal-ime (and Fecal 1)
9110421-01
Solid
11/25/19 11:45
11/25/19 12:40
2
9110421-02
Solid
11/25/19 11:45
11/25/19 12:40
3
9110421-03
Solid
11/25/19 11:45
11/25/19 12:40
4
9110421-04
Solid
11/25/19 11:45
11/25/19 12:40
5
9110421-05
Solid
11/25/19 11:45
11/25/19 12:40
6
9110421-06
Solid
11/25/19 11:45
11/25/19 12:40
7
9110421-07
Solid
11/25/19 11:45
11/25/19 12:40
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 17

Laboratory Report
n� Full -Service Analytical $
cJP I S 1 V 1 Environmental Solutions 12/05/2019
�LABORPTORIE$ ING
;ity of Statesville, NC Project: StaLime Client Sample ID: StaLime (and Fecal 1)
Attn: Ken Galloway Prism Sample ID: 9110421-01
P.O. Box 1111 Prism Work Order: 9110421
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Plant Available Nitrogen
1200
mg/kg dry
120
63
1
*Calculation 12/4119 9:05
CLB
[CALC]
% Solids
66.3
% by
0.100
0.100
1
*SM2540 G 11/27/19 9:08
EDV
P9K0490
Weight
Ammonia as N
120
mg/kg dry
15
3.7
1
*SM4500-NH3 C 11/27/19 14:00
BMS
P91<0504
Nitrate/Nitrite as N
9.3
mg/kg dry
7.5
2.1
1
*SM4500-NO3 F 12/2/19 10:32
CLB
P91-0009
Phosphorus -Total
4300
mg/kg dry
150
46
20
*SM4500-P F 12/3119 12:15
CLB
P91-0031
Total Kjeldahl Nitrogen
4000
mg/kg dry
380
200
1
*351.2 1214119 9:05
CLB
P91-0041
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 11/25/19 14:30
BMS
P9K0483
Total Metals
Mercury
0.095
mg/kg dry
0.075
0.026
1
*7471B
11/27/19 10:34
MMR
P9K0493
SAR Soil Preparation
Complete
g
1
*2-78-054
11/27/19 13:30
EDV
P9K0491
SAR Percent Moisture
51.5
% by
0.100
0.100
1
*2-78-054
12/2/19 8:10
EDV
P91<0510
Weight
Arsenic
13
mg/kg dry
1.5
0.20
1
*6010D
12/2119 20:13
JAB
P9K0494
)dium Absorption Ratio
1.0
[blank]
0.30
0.016
1
*2-78-054
1213119 8:50
JAB
P91<0508
admium
BRL
mg/kg dry
0.75
0.051
1
*6010D
12/2119 20:13
JAB
P9K0494
Calcium, SAR
2400
mg/L
200
2.0
200
*6010D
12/3/19 8:50
JAB
P91<0508
Copper
54
mg/kg dry
3.8
0.51
1
*6010D
12/2/19 20:13
JAB
P9K0494
Lead
9.0
mg/kg dry
1.5
0.25
1
*6010D
12/2119 20:13
JAB
P9K0494
Magnesium, SAR
BRL
mg/L
1.0
0.086
10
*6010D
12/3/19 8:50
JAB
P91<0508
Nickel
15
mg/kg dry
1.5
0.45
1
*6010D
12/2/19 20:13
JAB
P91<0494
Potassium
4600
mg/kg dry
150
16
1
*6010D
12/2/19 20:13
JAB
P91<0494
Selenium
27
mg/kg dry
1.5
0.41
1
*6010D
12/2/19 20:13
JAB
P9K0494
Sodium
1100
mg/kg dry
150
20
1
*6010D
12/2/19 20:13
JAB
PSK0494
Sodium, SAR
180 B
mg/L
5.0
0.18
10
*6010D
12/3119 8:50
JAB
P91<0508
Zinc
100
mg/kg dry
15
2.1
1
*6010D
12/2/19 20:13
JAB
P9K0494
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 17

Full -Service Analytical 8
I S Environmental Solutions
-7ABBRATORIE% INC
Laboratory Report
12/05/2019
;ity of Statesville, NC Project: StaLime Client Sample ID: 2
Attn: Ken Galloway Prism Sample ID: 9110421-02
P.O. Box 1111 Prism Work Order: 9110421
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
% Solids 65.3 % by 0.100 0.100 1 'SM2540 G 11/27/19 9:08 EDV P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 17

1h
Laboratory Report
� Full -Service Analytical &
�� ism Environmental Solutions
12/05/2019
Ad==-, RATOHIE$ ING
amity of Statesville, NC
Project: StaLime
Client Sample ID: 3
Attn: Ken Galloway
Prism Sample ID: 9110421-03
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateRme
ID
General Chemistry Parameters
% Solids 63.9
% by
0.100
0.100 1 *SM2540 G 11/27/19 9:08 EDV
P9K0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 11/25/19 14:30 BMS
P9K0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 -Fax: [phone] Page 6 of 17

Full -Service Analytical &
J� I S M Environmental Solutions
�LABOWT 'U .c.
;ity of Statesville, NC Project: StaLime
Attn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
12/0512019
Client Sample ID: 4
Prism Sample ID: 9110421-04
Prism Work Order: 9110421
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date[Time ID
General Chemistry Parameters
Solids 65.1 % by 0.100 0.100 1 *SM2540 G 11/27/19 9:08 EDV P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 17

Laboratory Report
Full -Service Analytical &
RR_ I S M I Environmental Solutions
12/05/2019
�✓ LABORATORIES. INC
;ity of Statesville, NC
Project: StaLime
Client Sample ID: 5
Attn: Ken Galloway
Prism Sample ID: 9110421-05
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateTme
ID
General Chemistry Parameters
% Solids 66.4
% by
0.100
0.100 1 *SM2540 G 11/27/19 9:08 EDV
P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 11/25/19 14:30 BMS
P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 17

i
Laboratory Report
Full -Service Analytical &
I S 1 V 1 Environmental Solutions
12105/2019
_II�R
�/ LABORATORIES, ING
;ity of Statesville, NC
Project: Stal-ime
Client Sample ID: 6
r,ttn: Ken Galloway
Prism Sample ID: 9110421-06
P.O. Box 1111
Prism Work Order: 9110421
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DateMme
ID
General Chemistry Parameters
% Solids 64.0
% by
0.100
0.100 1 *SM2540 G 11/27/19 9:08 EDV
P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 11/25/19 14:30 BMS
P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 17

I Full -Service Analytical &
'n\//�'
I S 1 �/ , I Environmental Solutions
LABORATORIES, INC
Laboratory Report
12/05/2019
amity of Statesville, NC Project: Stal-ime Client Sample ID: 7
Attn: Ken Galloway Prism Sample ID: 9110421-07
P.O. Box 1111 Prism Work Order: 9110421
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/25/19 11:45
Time Submitted: 11/25/19 12:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Solids 67.2 % by 0.100 0.100 1 *SM2540 G 11/27/19 9:08 EDV P91<0490
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/25/19 14:30 BMS P91<0483
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 17

I 7 Full -Service Analytical &
JP I S M I Environmental Solutions
/'UIBOR TOBIEB INC.
ty of Statesville, NC
r Ltn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P9K0491 - SAR 2-78-054
Blank (P9K0491-BLK1) Prepared: 11/26/19 Analyzed: 11/27/19
SAR Soil Preparation Complete g
Batch P9K0493 - 7471 B
Blank (P9K0493-BLK1) Prepared &Analyzed: 11/27/19
Mercury BRL 0.050 mg/kg wet
LCS (P9K0493-BSI) Prepared &Analyzed: 11/27/19
Mercury 0.421 0.050 mg/kg wet 0.4167 101 80-120
Batch P9KO494 - 3050B
Blank (P9K0494-BLK1)
Prepared: 11/27/19 Analyzed: 12/02/19
Arsenic
BRL
1.0
mg/kg wet
Cadmium
BRL
0.50
mg/kg wet
Copper
BRL
2.5
mg/kg wet
Lead
BRL
1.0
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
)tassium
BRL
100
mg/kg wet
;lenium
BRL
1.0
mg/kg wet
Sodium
BRL
100
mg/kg wet
Zinc
BRL
10
mg/kg wet
LCS (P9K0494-BS1)
Prepared: 11/27/19 Analyzed: 12/02/19
Arsenic
12.8
1.0
mg/kg wet
12.50
103
80-120
Cadmium
12.8
0.50
mg/kg wet
12.50
103
80-120
Copper
13.8
2.5
mg/kg wet
12.50
110
80-120
Lead
13.0
1.0
mg/kg wet
12.50
104
80-120
Nickel
13.1
1.0
mg/kg wet
12.50
105
80-120
Potassium
1200
100
mg/kg wet
1250
96
80-120
Selenium
12.2
1.0
mg/kg wet
12.50
98
80-120
Sodium
1210
100
mg/kg wet
1250
97
80-120
Zinc
12.7
10
mg/kg wet
12.50
102
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 11 of 17

I I Full -Service Analytical
r� Environmental Solutions
_7A o-T.n,ES.,Na
ity of Statesville, NC Project: StaLime
..ttn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91<0508 - 3010A
Blank (P9K0508-BLK1) Prepared: 11/27/19 Analyzed: 12/03/19
Calcium, SAR BRL 1.0 mg/L
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 1.73 0.50 mg/L BH
Batch P9KO510 - NO PREP
Duplicate (P9K0510-DUP1) Source: 9110421-01 Prepared: 11/27/19 Analyzed: 12/02/19
SAR Percent Moisture 51.0 0.100 % by Weight 51.5 1 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 17

Level II QC Report
PP> > Full -Service Analytical & 12/5/19
I S Environmental Solutions
®7LA -TORjm wa
ity of Statesville, NC
ttn: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Reporting
Analyte Result Limit Units
Batch P9KO490 - NO PREP
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Duplicate (P9K0490-DUP2) Source: 9110421-01 Prepared: 11/26/19 Analyzed: 11/27/19
% Solids 66.5 0.100 % by Weight 66.3 0.2 20
Batch P9K0504 - SM4500-NH3 B
Blank (P9K0504-BLK1) Prepared &Analyzed: 11/27/19
Ammonia as N BRL 10 mg/kg wet
LCS (P9K0504-BS1) Prepared &Analyzed: 11/27/19
Ammonia as N 454 10 mg/kg wet 500.0 91 80-120
Matrix Spike (P9K0504-MS1) Source: 9110421-01 Prepared &Analyzed: 11/27/19
Ammonia as N 791 14 mg/kg dry 724.7 121 92 80-120
Matrix Spike Dup (P9K0504-MSD1) Source: 9110421-01 Prepared &Analyzed: 11/27/19
Ammonia as N 816 14 mg/kg dry 724.7 121 96 80-120 3 200
Batch P91L0009 - NO PREP
Blank (P91-0009-BLK1) Prepared &Analyzed: 12/02/19
"trate/Nitrite as N BRL 5.0 mg/kg wet
CS (P91-0009-13S1) Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N 47.7 5.0 mg/kg wet 50.00 95 80-120
Matrix Spike (P9L0009-MS1) Source: 9110421-01 Prepared &Analyzed: 12/02/19
Nitrate/Nitrite as N 89.8 7.5 mg/kg dry 75.37 9.35 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 17

I ++II 'nn'\\ ///A�'' Full -Service Analytical &
JP R IsI V I Environmental Solutions
01;LAB0RAT0R1E% ING
ity of Statesville, NC
..ttn: Ken Galloway
P.O. Box 1111
Statesville. NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P9L0009 - NO PREP
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9L0009-MSD1) Source: 9110421-01 Prepared & Analyzed: 12/02/19
Nitrate/Nitrite as N 89.2 7.5 mg/kg dry 75.37 9.35 106 80-120 0.8 20
Batch P9L0031 - SM4500-PB5
Blank (P91-0031-BLK1) Prepared &Analyzed: 12/03/19
Phosphorus -Total BRL 5.0 mg/kg wet
LCS (P9L0031-BS1) Frepared &Analyzed: 12/U:3/1y
Phosphorus -Total 97.6 5.0 mg/kg wet 100.0 98 90-110
Matrix Spike (P91_0031-MS1) Source: 9110421-01 Prepared &Analyzed: 12/03/19
Phosphorus -Total 4790 150 mg/kg dry 150.7 4250 353 80-120 MC
Matrix Spike Dup (P9L0031-MSD1) Source: 9110421-01 Prepared &Analyzed: 12/03/19
Phosphorus -Total 4920 150 mg/kg dry 150.7 4250 445 80-120 3 20 MC
Batch P9L0041 - 351.2
Blank (P9L0041-BLK1) Prepared: 12/03/19 Analyzed: 12/04/19
—>tal Kjeldahl Nitrogen BRL 25 mg/kg wet
CS (P9L0041-BS1) Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen 123 25 mg/kg wet 125.0 99 90-110
Matrix Spike(P9L0041-MS1) Source:9110421-01 Prepared: 12/03/19 Analyzed:12/04119
Total Kjeldahl Nitrogen 6750 750 mg/kg dry 1884 3960 148 90-110 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 17

1 Full -Service Analytical &
R I S M I Environmental Solutions
'7­TORIEa ING
ity of Statesville, NC
..An: Ken Galloway
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P9L0041 - 351.2
Project: StaLime
Level II QC Report
12/5/19
Prism Work Order: 9110421
Time Submitted: 11/25/2019 12:40:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9L0041-MSD1) Source: 9110421-01 Prepared: 12/03/19 Analyzed: 12/04/19
Total Kjeldahl Nitrogen 6490 750 mg/kg dry 1884 3960 134 90-110 4 20 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone; 704/529-6364 -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 17

t
Level II QC Report
I_ I S M
Full -Service Analytical &
12/5/19
11
Environmental Solutions
7�A80RATORIE$ ING
ity of Statesville, NC
Project: StaLime
Prism Work Order: 9110421
ttn: Ken Galloway
Time Submitted:
11/25/2019 12:40:00PM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC
RPD
Analyte
Result
Limit
Units
Level Result %REC Limits
RPD Limit Notes
Batch P9K0483 - NO PREP
Blank (P9K0483-BLK1)
Prepared &Analyzed: 11/25/19
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample
Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91_0041
0.05 g
25 mL
12/03/19 10:15
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91<0504
1.01 g
50 mL
11/27/19 8:55
Prep Method: SM4500-PB5
lb Number
Batch
Initial
Final
Date/Time
110421-01
P91_0031
1 g
50 mL
12/03/19 6:15
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P9K0508
50 mL
50 mL
11/27/19 13:30
9110421-01
P91<0508
50 mL
50 mL
11/27/19 13:30
Prep Method: 3050E
Lab Number
Batch
Initial
Final
DateMme
9110421-01
P91<0494
2 g
50 mL
11/27/19 8:05
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91<0493
0.6 g
50 mL
11/27/19 8:14
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
9110421-01
P91<0491
250 g
250 g
11/26/19 13:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 16 of 17

CHI .OF CUSUDi Y �, COP
Fll-Service Analytical &
ED
smI Enuvironmental Solutions PAGE OF _ QUOTE 9 TO ENSURE PROPER BILLINCk.
�ti"�LM1BOftATORIE£y'ING
449 Springbrook Road • Charlotte, NC 28217 Project Name:
Phone [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Client Company Name: C 311 a . S' fi-� ESI%-! fC 'Please ATTACH any project specific reporting (QC LEVEL 111111 M
provisions andlor QC Requirements
Report..T01Conta'ct Name:. KeAr GA110wq _-
Invoice To:
Reporting, Address: -
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Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID: L� 'Observe
YES NO N/A r
—G r
'Cl
Phone: /01- s'/.u- 313s Fax es purchase Order NoJBiiling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
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Certification: NELAC DOD FL NC
EDD Type: PDF_lExcel Other
Site Location Name: '&4'1- C i
"Working Days" ❑-6-9 Days 11Standard 10 day . O Pr Approv MustBe
SC OTHER N/A
: R -7 u
Samples recelved after 14:00 will be processed next business day.
Site Location Physical Address:: -93'-;n If
Frir, ,n P%,k Tiimaround time is based.on business days, excluding weelliand6 and holidays.
Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. To CLIENT)
Sample Iced Upon Collection: YES NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
MATRDC
(SOIL,
WATER OR
SAMPLE CONTAINER
PRESERVA_
TIMES
ANALYSIS REQUESTED
/
>C� // l REMARKS
PRISM
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Sampler's Signature G .� .� f�4'
Sampled By (Print Name) ar r. to !c Affiliation
Upon relinquishing, this Chain of Custody Is your
authorization for Prism to proceed withtthe analyses as requested above_ Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for an .changes after analyses have been initialized
°
. Ralin ad 9Y.((Signature) ,b,
Recalvcd BY: (S:lfcrctna) - Date .'n5711aryiH6UGi' Additional Comments.- Site Arrival Time:
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Recaive1 y:'isignatv:ev+`- OaA Site Departure Time:
Rsltnquisha . _ ign luro);
Recery rPrismLabcratarfesil an Field Tech Fee:
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Mot, of-5 Ipme . OTE: ALL SAMPLE COOLERS 9R0 LD BETAPED SHUT WITH CUSTODY SEALS FOR•TRAPJSPPRTATION TO THE LABOF CRY, C G*p , a.
f SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LAt3g TORY. I �]
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C1 Fetl ❑ UPS 0 Hand -delivered O Prism Field Service
0 other L V
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NC
CERCLA LANDFILL OTHER
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*CONTANNEI E CODES: A = Amber C =-Clear G= Glass P = Plastic; TL = Teflon -Lined Cap = Volatile Organics Analysis (Zero Head Space)
umiGINAL