WQ0006245_Regional Office Historical File Pre 2018 (6)

41
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RECEIVED
WATER OUAtJTYSECiION
14 January 2002 R 2 1
Non-Dlmm ga p ro
NCDENR-Non Discharge Permitting Unit
Attn: Theresa Nartea
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: Additional Information for Permit Number WQ0006245
Dear Miss Nartea:
Attached is the information you requested for the above referenced Permit. If we can
provide any further information, please feel free to contact me at 704-878-3438.
Sincerely,
k
rry W. Byerly
ssistant Director
Water Resources

�Ct
SOC PRIORITY PROJECT: Yes_No_X
If Yes, SOC No.
To: Permits and Engineering Unit
Water Quality Section
Attention: Theresa Nartea
February 22, 2002
NON -DISCHARGE STAFF REPORT AND RECOMMENDATION
Mooresville # 01-119
County: Iredell
Permit No.WQ0006245
Renewal
PART I - GENERAL INFORMATION
1. Facility and address: City of Statesville
P.O. Box 1111
Statesville, NC 28687
2. Date of site visit: N/A
3. .Report prepared by: Dee Browder
4. Person(s) contacted and tel. number: N/A
5. Directions to site(s): From the intersection of I-77 north and NC Hwy 70 travel east on
NC Hwy 70 to Bell Farm Road. Turn left and travel north on Bell Farm Road to Forth
Creek WWTP (entrance on right side of road).
6. Size (land permitted for application): N/A
7. Topography (relationship to 100-year flood plain included): N/A
S. Buffer conflicts with location of nearest dwelling and water supply well: Yes _No X
9. Watershed stream basin information for land application sites: N/A
Page 1

PART II - DESCRIPTION OF WASTES AND TREATMENT WORDS
a. Residuals volume: 4000 dry tons per year
b. Types and quantities of wastewater: 100% domestic 0% Industrial
C. Volume of class A residual storage: There is approximately 2 acres of paved
uncovered storage next to the covered bay area. The covered cement pad area has
four bays with push walls on three sides. Finished Class A product has 2
designated bays and is stored in the uncovered storage area. De -watered sludge
from the 3`a & 4 h Creek plants is stored in designated bays. The entire storage
area has stormwater collection. The water is returned to the head of the plant.
d. Estimated days of storage: 90 days
2. Wastewater treatment facilities
a. Current permitted capacity of the facility: 6 mgd
b. Average daily flow of the facility: 2.8 mgd
C. Description of existing wastewater treatment facilities: N/A
d. Description of proposed wastewater treatment facilities: N/A
3. Residuals handling and utilization/disposal scheme: Class B aerobically digested residuals
(solids) are processed into a Class A residual using the N-Viro process of lime stabilization.
The City of Statesville holds a Class A permit (WQ0006245) for the distribution of lime
stabilized sludge produced at the Fourth Creek WWTP. Sludge from Third and Fourth Creek
are lime stabilized at the Fourth Creek WWTP.
PART III - OTHER PERTINENT INFORMATION
1. Special monitoring requests: n/a
2. Important SOC, JOC or Compliance Schedule dates: n/a
3. Other special items: n/a
Page 2

PART IV - EVALUATION AND RECOMMENDATIONS
This Office recommends that the permit be renewed.
Signature of Report Preparer
Water% uality Regional Supervisor
Date
Page 3

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality /
I
2 '
Michael F. Easley, Governor
William G. Ross; Jr., Secretary
Gregory J. Thorpe, Ph.D., Acting Directo
January 29, 2002
u 1_ u_ 1.9X 1 ju_
TO: Mooresville Regional Office -Water Quality
1 � •
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
rn n T
11{{�^^��� ate'+. �t- r_?.,y'E.�)i��,"': fi;•n..`'t,r.;
(ul6�lbl'°��C',y�; Yf12;'�a ��yr��4.!';e�•!✓�Yia
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FEB 0 4 2002
FROM: Theresa Nartea, Soil Scientist-ItDPIJ
4 t
:~ M1
RE: WQ0006245-City of Statesville-DRS permit renewal
Additional information response to Central Office letter dated December 19, 2001. For your
review. Thank you.
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] Fax [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/10% post -consumer paper

lieparLmenL vi jc nvtrunmenL, ned1LL1 d11u 1-44LUL-di l%CJVU1 %-CJ
Division of Environmental 'Management
Non -Discharge Pernut Application Form
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
DISTRIBUTION OF RESIDUAL SOLIDS
This application is intended for facilities which are to be regulated under 40 CFR Part 503
I. GENERAL INFORMATION:
1. Applicant's name (please specify the name of the municipality, corporation, individual, etc.):
City od Statesville
y 2. Print owners or signing official's name and title (the person who is legally responsible for the facility and its compliance):
John Marshall, Mayor
3. Mailing address
City:
P. Q. BOX 1111
Statesville, NC
Telephone Number: ( 704 )
S tate:
8783438
Zip: 28687
4. Application Date: October 2001
5. Fee Submitted: S 325.00 [The permit processing fee should be as specified in 15A NCAC 2H .0205(c)(5).]
6. Specify how these residuals will be distributed: sold or given away in bags or other containers; lawn (bulk);
x_ home garden (bulk); X_ other,
farm land
7. If the alternative for residual disposal consists of "surface disposal" as defined under 40 CFR Part 503, please complete the
application titled "SURFACE DISPOSAL OF RESIDUAL SOLIDS. Please identify if there is any storage of residuals in
a surface impoundment or disposal thru landfilling. Explain:
8. Is the residual process facility also the generator? X Yes; No
9. Latitude: 80 ° 47' 20" Longitude: 350 46' 22" of residual process facility
10. Specify whether the process facility is owned by: federal; private; state; X local government;
11. County where facility is located: Iredell
II. PERMIT INFORMATION:
1. Application No. (will be completed by DEM):
2. Specify whether project is: new; X renewal*; modification
* For renewals, complete all sections included in the application. Engineering Signature and Seal not required for
renewals or if there is not any construction involved with the subject project
3. If this application is being submitted as a result of a renewal or modification to an existing permit, list the existing permit
number , WQ0006245 and its issue date March 5, 1997
FORM: DRS 06/94
Page 1 of 8
KFECEIVED
WATER QUALITYSECII®N
JA 4 2
No1i-Discharge Parrang

9 •�
1. t 1

III. FACILITY INFORMATION (attach additional pages for additional sources of residuals): City of Stat
ville WTP
1. Name of facility where residuals are generated or prepared: 4th. Creek WWTP — 3rd Creek WWTP
2. Facility permit number: NCO031836 ; facility permit holder: City of Statesville
3. Specify whether facility in Section III.1 is owned by
4. Specify facility design flow: 6MGD
5
Type of residual storage
Volume of residual storage:
federal; private;
mgd; facility average daily flow:
aerobic digester
1.5 MG
state; X local government;
2.8 MOD mgd;
Length of residuals storage at facility: 45 days (the Division requires a minimum 30 days storage in units that
are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.);
000
Estimated volume of residuals: 4,(dry tons/yr.);
If the residual process facility is not the same as the generator, please specify delivery frequency and quantity of residual to
be processed: NA
6. Facility contact (person familiar with residuals preparation): Andy Smith -
7. Facility contact's telephone number: ( 704 ) 878-3439
8. Location of treatment facility: 693 Bell Farm Rd.State; N. c — Iredell_ County
9. Mailing address: P • 0. Box 1111 Statesville, NC 28687
10. Specify the source of the residuals: _y_ treatment of domestic wastewater, treatment of industrial wastewater;
X other (explain). Alum sludge from Water Treatment Plant
Attach an explanation of either the treatment process, manufacturing process, or how the waste is generated. Provide full
and complete details of the entire process.
11. Does the facility which generates the residuals have an approved pretreatment program? X Yes; No.
This includes facilities which are classified as a "Class I" facility (any publicly owned treatment works required, under 4C
CFR 403.8, to have an approved pretreatment program or any facility treating domestic sewage that is classified as "Class
I" by the appropriate federal or State authority)
IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals):
1. Information for Hazardous Waste (RCRA) Determination. The information requested on the limitations specified below
pertain only to those residuals that are generated from a municipal wastewater treatment facility with industrial contributior
or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources.
a. Are any of the residuals covered by this application listed in 40 CFR 261.31-261.33?
list the number(s):
Yes; X No. If Yes
b. Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? Yes; X No
Attach laboratory results for the Toxicity Characteristic Leaching Procedure Analyses, Reactivity, Ignitability, an(
Corrosivity for each residual.
RECENED
01 ERR OUALITY SECTION
FORM: DRS 06/94 Page 2 of 8 Noll-DI8clmpoPenW

Note: If the following constituent levels (as determined by the Toxicity Characteristic Leaching Procedure Analyses) are
exceeded in the residuals or if the pH of the residual is not within the range listed below, the residual is by
definition a Hazardous waste. Chemical analyses must be made to Minimum Detection Levels.
RPM
PPM
Arsenic
5.0
Barium
100.0
Benzene
0.5
Cadmium
1.0
Carbon tetrachloride
0.5
Chlordane
0.03
Chlorobenzene
100.0
Chloroform
6.0
Chromium
5.0
o-Cresol
200.0
m-Cresol
200.0
p-Cresol
200.0
Cresol
200.0
2,4-D
10.0
1,4-Dichlorobenzene
7.5
1,2-Dichloroethane
0.5
1,1-Dichloroethylene
0.7
2,4-Dinitrotoluene
0.13
Fndrin
0.02
Heptachlor (and its hydroxide)
0.008
Hexachlorobenzene
0.13
Hexachloro-1,3-butadiene
0.5
Hexachloroethane
3.0
Lead
5.0
Lindane
0.4
Mercury
0.2
Methoxychlor
10.0
Methyl ethyl ketone
200.0
Nitrobenzene
2.0
Pentachlorophenol
100.0
Pyridine
5.0
Selenium
1.0
Silver
5.0
Tetrachloroethylene
0.7
Toxapbene
0.5
Trichloroethylene
0.5
2,4,5-Trichlorophenol
400.0
2,4.6-Tricblorophenol
2.0
2,4,5-TP (Silvex)
1.0
Vinyl chloride
0.2
pH (2:1 vol./wt.): >2.0 s.u. - <12.5 s.u.
NOTE: IF ANY OF THE RESIDUALS MEET THE DEFLNITIONS OF A HAZARDOUS WASTE,
AS NOTED IN EITHER "A" OR "B" ABOVE, A PERMIT CANNOT BE ISSUED FOR
THAT MATERIAL AND IT SHOULD NOT BE INCLUDED AS PART OF THIS
APPLICATION.
2. For each residual, please attach a complete chemical analysis of the material. This analysis must be comprehensive enough
to completely characterize the residual and must be based upon a review of the process that generates the material. If the
facility that will generate the residual is not yet in operation, the characterization must be based on similar existing
facilities and projection based on the type of facility:. The analysis must include a minimum of the following parameters
and any other known and suspected contaminants that are tributary to the system.
Arsenic
Molybdenum
Cadmium
Nickel
Chromium *- NA
Selenium
Copper
Zinc
Lead
Aluminum
Mercury
Ammonia -Nitrogen
Calcium
Phosphorus
Magnesium
Potassium
Nitrate -Nitrite Nitrogen
Sodium
% Total Solids
TKN
pH
Plant Available Nitrogen
(by calculation)
FORM: DRS 06/94 Page 3 0l 6

a
3
4
5
Wastewater residuals can not be sold or given away if the concentration of any -wdutant in the residuals exceeds the ceiling
concentrations specified in the table below. Specify the pollutant concentration of these residuals (attach lab analysis).
Provide, all applicable pilot studies and any bench scale tests performed on each residual source and the results, including
the approximate fertilizer equivalent.
Wastewater residuals can't be sold or given away in bags or other containers for application to the land unless one of the
following options is satisfied.
Specify either A or B. Please be advised, if the residuals are to be sold or given away in bulk for application tc
lawn or home garden then Option A is the only option.
A . The pollutant concentration of the residuals must be less than Pollutant Monthly Average Concentration!
listed in the table below.
Pollutant
Monthly Average Concentrations
Dry Weight Basis (mJka)
Pollutant uoncentrauon
Dry Weight Basis (mgfkg)
Arsenic
41
_7
Cadmium'
39
.1
Chromium
1200
NA
Co er
1500
Lead
300
97
17
0.18
Mercury
Nickel
420
16
Selenium
36
Zinc
2800
1 75
B . The product of the concentration of each pollutant in the residual and the annual whole residual appti.catic
rue fc,r u e residual shot not cause the Annual Pollutant Loading Rate to be exceeded.
In order for the Annual Whole Residual Application Rate (AWRAR) to be calculated the Annual Polluta
Loading Rate (APLR) is divided by the pollutant concentradon (PC) times 0.001 (a conversion factor)
follows:
AWR.AR = APLR
PC * 0.001
FORM: DRS 06/94 Page 4 of 8

NA
Pollutant
Pollutant
Concentration
Dry Weight Basis
(m 1;/kg)
Annual Pollutant
Loading Rates
(APLR)
k Jhectare
Annual Whole Residual
Application Razz
(AWRAR)
kg/hectare
Arsenic
2.0
Cadmium
1.9
Chromium
150
Copper
75
Lead
15
Mercury
0.85
Nickel
21
Selenium
5.0
. Zinc
140
The AWRAR for the residual is the lowest AWRAR calculated. This is the maximum rate at which the
subject residual can be applied (to convert kg/hectare to lbs/acre multiply by 0.8924). Please specify
kg/hectare or lbs/acre:
AWRAR =
V . PATHOGEN AND VECTOR ATTRACTION REDUCTION INFORMATION (attach additional pages for
additional sources of residuals):
1. In order for the residuals to be Class A, in accordance with the pathogen requirements in 40 CFR 503.32(a), either Part a or
Part b and one of the options in Part c must be completed (please submit all lab analysis, test results and calculations):
X a. A Fecal coliform density less than 1000 Most Probable Number per gram of total dry solids, or
b. A SalMonella sp. density less than 3 Most Probable Number per 4 grams of total dry solids.
2 c. In addition to Part a or Part b being met, one of the following alternatives must also be completed. Please
specify 1, 2, 3, 4, 5a, 5b, 5c, 5d, 5e, 5f, 5g or 6 below being met:
1. time/temperature - an increased residuals temperature should be maintained for a prescribed period of time, in
accordance with the following guidelines. The results (D) shall be the amount of time, in days, that the residuals
shall remain at the given temperature:
11L , all
Notes
Total Solids
Temperature (t)
Minimum Time
E4uation
No heating of small
> or = 7%
> or = 500 C
> or = 20 minutes
D = 131.700.000
particles by warmed
100.14 t
gases or immiscible
-liquid.
> or = 7%
> or = 500 C
> or = 15 seconds
D =131.7 DMQ
Small particles heated by
100.14 f
warmed gases or
immiscible liquid,
< 7%
> or = 501) C
> or = i5 seconds
D = 111.700, 0
to
100.14 t
< 30 minutes
< 7%
> or = 500 C
>or = 30 minutes
D = 50,070,000
100.14 t
FORM: DRS 06194 Page 5 of 8

alkaline treatment - the pH of the residuals is raised to greater than 12 for at least 72 hours. During this time, the
temperature of the residuals shouio be gigs c, titan 5'0 C for at last 12 hours. In addition, after the 72 hour
period, the residuals are to be air dried to at least 50% total solids.
prior testing for Enteric VirusNiable. He minth Ova - the residuals are analyzed for the presence of enteric viruses
(Plaque -forming units) [pfu] and viable helminth ova. If the residuals are analyzed before the pathogen reduction
process and found to have densities of enteric virus <1 pfu/4 grams of total solids and viable behninth ova <1/4g
total solids, the residuals are Class A with respect to enteric virus and viable helminth ova until the next
monitoring episode. If the residuals are analyzed before the pathogen reduction process and found to have densities
of enteric virus > or = 1 pfu/4 g total solids or viable helminth ova > or = 1/4 g total solids, and tested again after
processing and found to meet the enteric virus and viable helminth ova levels listed under "4" below, then the
processed residuals will be Class A with respect to enteric viruses and viable helminth ova when the operating
parameters for the pathogen reduction process are monitored and shown to be consistent with the values or ranges
of values documented.
4. no prior testing for Enteric VirusNiable HeIr inch_ Ova - if the residuals are not analyzed before pathogen reduction
processing for enteric viruses and viable helminth ova, the density of enteric viruses must be less than 1 pfu/4 g of
total dry solids and the density of viable helminth ova must be less than 1/4 g of total dry solids, or the residuals
must be treated by a "Process to Further Reduce Pathogens" or a "Process to Further Reduce Pathogens" equivalent
process.
5. The "Processes to Further Reduce Pathogens" (PFRP) are described as follows:
a. Composting - using either the within -vessel or static aerated pile composting methods, the temperature of the
residuals are raised to 550 C or higher for three days. Using the windrow composting method, the residuals are
raised to 550 C or higher for fifteen days. During the high temperature period, there will be a minimum of five
turnings of the windrow.
b. Heat Drvin2 - residuals are dried by direct or indirect contact with hot gases to reduce the moisture content of
the residuals to look or lower. Either the temperature of the gas in contact with the residuals exceeds 800 C or
the wet bulb temperature of the gas in contact with the residuals, when the residuals leave the dryer, exceeds
800 C.
c. Heat Treatment - liquid residuals are heated to a,temperature of 1800 C or higher for thirty minutes.
d Thermophilic Aerobic Digestion stion - liquid residuals are agitated with air or oxygen to maintain aerobic conditions
at residence times of ten days at temperatures of 550 C to 600 C.
e. Beta Rav Irradiation - residuals are irradiated with beta rays from an accelerator at dosages of at least 1.0
megarad at room temperature (ca. 200 Q.
f. Gamma Rav Irradiation - residuals are irradiated with gamma rays from certain isotopes such as 60Co and
137Ce, at dosages of at least 1.0 megarad at room temperature (ca. 200 Q.
g. Pasteurization - the temperature of the residuals is maintained at 700 C or higher for at least thirty minutes.
6. The residuals shall be treated in a process that is equivalent to a "Processes to Further Reduce Pathogens" (PFRP),
as determined by the permitting authority based on evaluations of the recommendations provided by the Pathogen
Equivalency Committee.
2. When residuals are to be sold or given away, one of the following vector attraction reduction requirements (a, b, c, d, e, f,
g, or h) described below must be met.
F Specify the letter of the vector attraction reduction requirement that has been met (submit lab results, test results and
calculations). Any variation of the below must be described in full detail and attached.
a. Aerobic or Anaerobic Digestion -The mass of volatile solids are reduced by at least 38f,7o. Volatile solids reduction is
measured between the residuals, prior to stabilization, and the residuals ready for use or disposal. This criterion should
be readily met by properly designed and operated anaerobic digestors, but not as readily met by aerobic digestors.
Treatment facilities with aerobic digestors may need to meet the vector attraction reduction requirement through 19c or
19d.
FORM: DRS 06/94 Page 6 of 8

b A� ,_f,hi.� n�•,'ctinn - If �Soc volatile solid; reduction cannot be achieved. vector atsaction reduction c;.. l.�
demonstrated by further digesting a portion tit the previously digested residuals u1 a cc)encn s.,:aie unit iur an adu._.indi
40 days at 300 C to 37° C. If, at the end of the 40 days, the volatile solids are reduced by less than 171/c, sector
attraction reduction is achieved.
c. Aerobic Digestion - If 38% volatile solids reduction cannot be achieved, vector attraction reduction can be demonstrated
by further digesting a portion of the previously digested residuals that have a solids content of 2% or less in a bench
scale unit for an additional 30 days at 201 C. If, at the end of the 30 days, the volatile solids are reduced by less than
15%, vector attraction reduction is achieved.
d. Aerobic Di eg suon - The specific oxygen uptake rate (SOUR) shall be'equal to or less than 1.5 milligrams of oxygen
per hour per gram of total dry solids at 20° C.
e. Aerobic Processes - The temperature of the residuals for at least 14 days shall be greater than 40° C. During this tithe,
the average temperature shall be greater than 450 C.
f. Alkaline Stabilization - The pH of the residuals is raised to 12 or higher by alkali addition and, without the addition of
more alkali, remains at 12 or higher for 2 hours and then at 11.5 or higher for an additional 22 hours.
g. J?Uin'(stabilized solids) - The total solids of residuals that do not contain unstabilized solids, and which are generated
in a primary wastewater treatment process, shall be equal to or greater than 75%. Blending with other materials is not
allowed to achieve the total solids percentage.
h. 2[yin (unstabilized soLds) - The total solids of residuals that contains unstabilized solids, and which are generated in s
primary wastewater treatment process, shall be equal to or greater than 90%. Blending with other materials u no
allowed to achieve the total solids percentage.
VI. GENERAL INFORMATION:
1. Please provide a brief narrative concerning materials handling, including the following:
a. How will the materials will be handled and transported from where the residuals were produced to where it will be
treated?
b. Where will the residuals be stored until processed?
c. How will leachate collection be handled?
d- What will be the duration of treatment?
e. Where will the final product be stored?
f. How long will the final product be stored before being distributed?
g. How will the final product be distributed (packaging)?
2. Please - attach a marketability statement detailing destinations and approximate amounts of the final product to b
distributed.
3. Please provide either a label which shall be affixed to the bagged processed residual or an information sheet which shall b�
provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, thi
following information:
* sta lime
info a. The name and address of the person who prepared the residual that is sold or given away in a bag or other container for
sheet application to the land.
b. A statement that application of the residual to the land is prohibited except in accordance with the instructions on the
label or information sheet.
c. A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
d A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or storr-j
e. Information on all applicable buffers including a 10 foot buffer between application site and any public or private wate
supply source (including wells) and any stream, lake, river, or natural drainage way.
f. The Annual Whole Residual Application Rate (AWRAR) for the residual that does not cause any of the annual
pollutant loading rates to be exceeded (if necessary).
FORM: DRS 06!94 Page 7 of 8

Cite:
Telephone Number: c
Professional Engineer's Certification:
State:
I. . attest that this application for
Zip:
has been reviewed by me and is accurate and complete to the best of my kznowledge. I further attest that to the best of my lmowled,
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submits
package may have been developed by otber professionals, inclusion of these materials under my signature and seal signifies that I ha
reviewed this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
I _John Marshal
attest that this application for
Dist i r ion of Residual Solid - Class A Permit No WQ0006245
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that if all required pans of th
application are not completed and that if all required supporting information and attachments are not included, this application packa;
will be returned io
me as "gicomplete.
Si � Signature g
mar( (Ll'l�, Date✓ /
THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTL'NG LNFORMATION AND
MATERIALS, SHOULD BE SENT TO THE FOLLOWLNI G ADDRESS:
FORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
PERMITS AND ENGINEERING UNIT
POST OFFICE BOX 29535
RALEIGH, NORTH CAROLINA 27626-0535
TELEPHONE NUMBER:
(9I9) 733-5083
FORM: DRS 06'04 Pate 8cif c

DATA FOR REACTNITY,
CORROSIVITY, AND
IGNITABILITY

..pan-U7-Ut Ue:51P
P-02
Lab Report
pRS
u., LAHORA7Qp1EM
r,,,t ;..•,� �y annrym�at .t r•,,,;.rx,r+erlal :;�:bd,,:,,.:
119/02
Page 1 of 2
City of Statesville
Customer Project ID: Sta-L-ime
Attn; Mr. Andy Smith
Customer Sample ID: STA1UMF-
P O. Box 1111
Prism Samote ID: AC3b128
Statesville, NC 28687
Loqtn Group: 6054H1
Sample Collection Date/Time: 112102
13:50
Lab Submittal Date/Time: 112/02.
15:45
The following analytical results have been obtained
for the indicated sample which
was submitted
to this laboratory
-
TEST
NARAMETER
TEST
RESULT
REPORTING METHOD
UNITS
ME
•
LIMIT REF_REN_ tic
57ARTED
STARTED
ANALYST
MOLYBDENUM• TOTAL
4.a
mg/kg 1.0 601p
_
CALCULATIONS BASED ON DRY WT.
62
117i0213:45
MSC
% DRY WT. 0.01 SM 2540 G
1,4/02 14:00
JMV
FECAL COLIFORM. SOLID SM9221E
Less than
colonies/gram 4 0
CYANIDE. REACTIVITY
SM _2_t )_
112/02 17.00
TAR
Less than
pllm 2.0 SW-840 9413
!J8.02 15:00
CVM
SULFIDE, REACTIVITY
Less than
ppm 10 S'1V•846 4030
!:8%02 16 00
(;vM
REACTIVITY
Passed
ICNITIBILITY OF SOLIDS
SW-846 Ch. 7 3
1J9J02 10,50
JAS
Passed
PAS&FAIL SW846-1030
117102 17:40
EHT
METALS DIGESTION .METHOD 3050
Completed
SW846.3050
114102 14AS
LC2
ARSENIC, TOTAL
11
mg/kg 1.0 S'INB46.6010B
1a7;0:13:45
MSC
CADMIUM. TOTAL
Less than
mg/kg 1.0 SV1846-6010B
V7.'02 13.45
MSC
COPPER. TOTAL
87
mgfkJ 20 SW846-60109
VW021145
M$(
LEAD. TOTAL
41
mg/kg 1.0 SW846-601CfR
117/02 13:45
MSC
NICKEL. TOTAL
17
mq!kg 1.0 SWe46.60110B
117102 13:45
MSC
ZINC. TOTAL
86
mg/kg 10 SW846.60,,OB
1/7,0213:45
MSC
SELENIUM. TOTAL
19
mg/kg 0.20 SW846-60105
1;7,02 13:45
MSC
MERCURY DIGESTION
Completed
SW846-7471
10,102 08'30
LC2
MERCURY. TOTAL
0,55
mg/kg 0-03 5W846.7471
11710214:02
TAR
CORROSIVITY AS PH
12.3
UH Units SW646-9n40190451/7i02
09:12
SMG
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL CariLcatlon No. E87519
I i•> •:�yll',:;�nH.k I.:,.u! L't) ,,,, ':;���ALc n,nl� ll,. V( _. '71 ..
4.
.. t' I.F."C::2tl -,7,4 A, I,— •l;ti: i_..j, It t,

�..... ... ._. v c c Z? i r—
Lab Report
P.03
1 /9/02
City of Statesville
Attn: Mr. Andy Smith
P.O. Box 1111
Statesville, NC 28687
PRISM
r+
LA80RATCWIE& INC.
FWt 1w•w•. a 0.nlryl+Cl1
5 Cnvu�:mm�nt0l SU�.IHws
Page 2 of 2
Customer Project 11):
Sta-Lime
Customer Sample ID:
STA4.IME
Prism Sample ID:
AC30128
Login Group:
6054H1
Sample Collection Date/Time:
1/2/02 13:50
Lab Submittal Date/Time:
1/2/02 15:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD gATEITIME
PARAMETER RESULT UNITS LIMIT REFEREINCE 57ARTED ANALYST
Sarnote Comments:
HG COMMENT: MS and MSD failed due to matrix interference. High sample value Caused poor recovery.
(MS=59%. MSD= absorbance was greater than highest standard).
4��
Angela D. Overcash, V.P. Laboratory Services
NC Cortiflcation No 402 - SC Certification No. 99012 - NC Drinking Water Cort. No. 37735 - FL Certification No. E87519
44051T,::rl t.n.•i•! IL:.tcl > I•l + I'— '4I -i.' & C I:..rirlh'. \i _.i:}•I fl;i.;

Sample Progress Report
Prism Laboratories _
User: Munroe, Whitney
Date: 01-07-2002 Time: 16:12:17
Sample ID: AC30128
Status: Analyses incomplete
Old Login Group #: 6054H1
Customer Reference: 7232-1
Customer Code: STATESVI
Customer Sample I. DO: STA-LIME
Project: Sta-Lime
Ponumber
Clientprojmgc Andy Smith
Matrix:
Date collected: 01/02/02 13:50:
Date submitted: 01/02/02 15:46
Due date: 01/02/02 2359
Specification checking: on
Phone Number: (704)87B-34381rax(704)878-8655
Login .Group Number. 6054M 1
Satescode: 600
Prismpmmgr: WMM
Workorderno*
Ane"is Y+d
Result
MDL
Unit
Rh Origin
Due Dale
Stwted
Ended
AM
SAMPLE PICK-UP FEE
Completed
manual
O1/02102
6110dM 17:23
01104J02
17:23
KEW
METALS DIGESTION METHOD 3050
Completed
manual
olAW2
0B/04102 14:45
01/04/02
01107M2
13:45
12:02
LC2
MSC
ARSENIC, TOTAL
11 .
1.D
mg/kg
manual
01105/02
C{ /07102 13:45
CADMIUM. TOTAL
Less than
1.0
mg/kg
Manual
01/05J02
0107102 13:45
01/07/02
12:02
MSC
COPPER. TOTAL
87
2.0
mg/ka
manual
01/05M2
gl/07102 13:45
01107/02
12:02
MSC
LEAD, TOTAL
41
1.0
mg/kg
manual
01/05/02
107102 13:45
01107102
12:02
MSC
MERCURY DIGESTION
Completed
manual
01/vwuw
07RZ 09:30
01407/02
11.40
LC2
MERCURY. TOTAL
0.56
0.03
11-09
manual
01/05102
1107102 14:02
01/07/02
14:41
TAR
NICKEL TOTAL
17
1.0
Mpg
manual
01A)$W
107102 13:45
01/07/02
12:02
MSC
ZINC, TOTAL
86
1.0
mg/kg
manual
01/05102
13:45
01/07i0Z
12:02
MSC
SELENIUM, TOTAL
19
0.20
mglkg
manual
01/05102
107102 13:45
01/07M2
12:02
MSC
MOLYBDENUM.TOTAL
4.8
1.0
MgAg
manual
OIAW02
1107tO2
J07102 13:45
01107/02
12:02
MSC
FECAL COLIFORM, S000 SL 9221E
Less than
4
coloniesWam
manual
01/02/02
IMM 17:00
011D3102
16:06
TAR
CORROSWrY AS PH
12.3
pH Unite
manual
01/03102
107102 09:12
01/07102
10:11
SMG
IGNITIBILITY OF SOLIDS
—
CYANIDE, REACTIVITY
—
SULFIDE. REACTIVITY
—
REACTIVtTY
CALCULATIONS BASED ON DRY WT
62
0.01
% DRY WT.
manual
D7104/02
01/04/02 14:00
OIJ07102
09.34
JMV
Sample comments:
HG COMMENT: MS and MSD failed due to matrix interference. High
aampte value caused
poor recovery. (MS=59%. MSD= absorbance was greater than highest standard)
End of progress report on sample: AC30128

RESIDUALS
ANALYSIS

—.V-4101
PATHOGEN/VECTOR ATTRACTION REDUCTION
CERTIFICATION STATEMENT
Pertaining to The Fourth Creek
Alkaline Stabilization Facility
I certify, under penalty of law, that the pathogen
requirements in 503.32 (a)(4) and vector attraction reduction
requirements in 503.33 (b)(6) have been met.
503.32 (a)(4): Pathogen Reduction
Stating the pH of the sewage sludge that is used or disposed
shall be raised to above 12 and shall remain above 12 for 72
hours. By adding fine alkaline materials and through exothermic
elevated the temperature to 52 Degrees Celsius for twelve hours
or longer during the period that the pH of the sewage sludge
is above 12. The sewage sludge has been air dried to achieve
a percent solids in the sludge greater than 50 percent.
503.33 (b)(6): Vector Attraction Reduction
The pH of sewage sludge has been raised to 12 or higher by alkali
addition and, without the addition of more alkali, has remained
at 12 or higher for two hours and then at 11.5 or higher for
an additional 22 hours.
This determination has been made under my direction and
supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the
information used to determine that these requirements have been
met. I am aware that there are significant
certification includingthe penalties for false
possibility of fine and imprisonment.
Signed
Title l `
Date ��

,Lab. Report
1 /12/01
City of Statesville
Attn: Ms. Judy Wilcox
P.O. Box 1111
Statesville, NC 28687
1 ;
Full Service Analytical & Environmental Solutions
Page 1 of 2
Customer Project ID: Sta-Lime
Customer Sample ID:
STALIME
Prism Sample ID:
AB93896
Loqin Group:
WM112G1
Sample Collection Date/Time:
1/9/01 10:15
Lab Submittal Date/Time:
119/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
METALS DIGESTION METHOD 3050
Completed
3050
1/10/01 08:30
PRF
AMMONIA DISTILLATION
Completed
4500-NH38
1/10101 16:25
KAP
AMMONIA AS N _
380
mg/kg
9.0
4500-NH3E
1/10/01 19:00
KAP
ARSENIC, TOTAL
11
mg/kg
1.0
6010
11/10/01 23:32
MSP
CADMIUM, TOTAL
1.1
mg/kg
1.0
6010
11/10/01 23:32
MSP
COPPER, TOTAL-
52
mg/kg
2.0
6010
11/10/01 23:32
MSP
LEAD, TOTAL
60
mg/kg
1.0
6010
11/10/01 23:32
MSP
NICKEL, TOTAL ,
16
mg/kg
1.0
6010
11/10/01 23:32
MSP
ZINC, TOTAL .
56
mg/kg
1.0
6010
11/10/01 23:32
MSP
SELENIUM, TOTAL
16
ring/kg
2.0
6010
11/10/01 23:32
MSP
MOLYBDENUM, TOTAL
5.1
mg/kg
1.0
6010
11/10/01 23:32
MSP
CALCIUM, TOTAL
250000
mg/kg
10000
6010
1/11101 16:30
MSP
MAGNESIUM, TOTAL
8400
mg/kg
100
6010
1/11101 16:30
MSP
SODIUM, TOTAL
1500
mg/kg
100
6010
1/11101 16:30
MSP
POTASSIUM, TOTAL
22000
mg/kg
100
6010
1111/01 16:30
MSP
ALUMINUM, TOTAL
13000
mg/kg
100
6010
1/11101 16:30
MSP
MERCURY DIGESTION
Completed
7471
1/11/01 11:30
PRF
MERCURY, TOTAL '
0.32
mg/kg
0.03
7471
1112101 13:06
PRF
NITRATE.
Less than
mg/kg
1.5
EPA 300
1110/01 15:22
TAR
NITRITE
2.5
mg/kg
1.0
EPA 300
1/10/01 15:22
TAR
TOTAL PHOSPHORUS
34
mg/kg
0.67
EPA 365.2
1/10/01 12:40
MBS
PLANT AVAILABLE NITROGEN
3.9
lb PAN/ton
0.05
NC Dept. Ag.
1/12/01
TAR
TOTAL RESIDUE
67
%
0.01
SM 2540 B
1/10/01 16:10
JLW
CALCULATIONS BASED ON DRY WT.
67
% DRY WT.
0.01
SM 2540 G
1/10101 16:10
JLW
TOTAL PHOSPHORUS DIGESTION
Completed
SM 4500-P B
1/10/01 09:05
MBS
TOTAL KJELDAHL NITROGEN
6300
mg/kg
110
SM4500-NH3 E
1110101 13:55
MBS
TKN DIGESTION
Completed
SM4500-NorgB
1110/01 06:35
MBS
pH
12
pH Units
SW 846 9045A
1110/01 09:00
SMG
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road P.O. Box 240543 � Charlotte, NC 28224-0543

.. Lab Report
1/12/01
City of Statesville
Attn: Ms. Judy Wilcox
P.O. Box 1111
Statesville, NC 28687
--• 1061
Customer Project ID:
Customer Sample ID:
Prism Sample ID:
Loqin Group:
'Sample Collection Date/Time:
Lab Submittal Date/Time:
4 [L
.•�_:�= W,'"�;�4i����-fie
Full Service Analytical 8 Environmental Solutions
Page 2 of 2
Sta-Lime
STALIME
AB93896
WM112G1
1/9/01 10:15
1 /9/01 14:40
The following analytical result$ have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
NOTE: pH was analyzed out of the established EPA holding time.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road P.O. Box 240543 � Charlotte, NC 28224-0543

;Lab Report
VAN 12 2001 __."Ap'
Full Service Analytical & Environmental Solutions
1/11/01 Page 1 of 7
City of Statesville Customer:Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample 1D: STALIME 1
P.O. Box 1111 Prism Sample ID: AB93887
Statesville, NC 28687 Login Group: WM112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The following analytical results. have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTFn enlel V�
CALCULATIONS BASED ON DRY WT. 69 % DRY WT. 0.01 SM 2540 G 1110101 11:30 JMV
FECAL COLIFORM, SOLID Less than colonies/gram 3.0 SM 9221 E 1/9/01 15:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ,. P.O. Box 240543 � Charlotte, NC 28224-0543

Lab Report
M
Full Service Analytical S Environmental solutions
1/11/01 Page 2 of 7
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 2
P.O. Box 1111 Prism Sample ID: AB93888
Statesville, NC 28687 Login Group: WM112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The following analytical results, have been obtained for the indicated sample which was submitted to this laboratory
I to I
PARAMETER
TEST
REPORTING
METHOD
DATE/TIME
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
70
% DRY WT.
0.01
SM 2540 G
1110/01 11:30 JMV
FECAL COLIFORM, SOLID
Less than
colonies/gram
3.0
SM 9221 E
1/9/01 15:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - INC Drinking Water Cert. No. 37735 - FL Certification No. ,E87519
449 Springbrook Road h, P.O. Box 240543 � Charlotte, NC 2821-4-0543

Lab Report
1/11/01
City of Statesville
Attn: Ms. Judy Wilcox
P.O. Box 1111
Statesville, NC 28687
AQ
Full Service Analytical 8 Environmental Solutions
Page 3 of 7
Customer Project ID:
Sta-Lime
Customer Sample ID:
STALIME 3
Prism Sample ID:
AB93889
Login Group:
WM112G7A
Sample Collection Date/Time:
1/9/01 10:15
Lab Submittal Date/Time:
1/9/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST
PARAMETER RESULT
CALCULATIONS BASED ON DRY WT. 67
FECAL COLIFORM, SOLID Less than
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
REPORTING
METHOD
DATEITIME
UNITS
LIMIT
REFERENCE
STARTED ANALYST
% DRY WT.
0.01
SM 2540 G
1/10/01 11:30 JMV
colonies/gram
3.0
SM 9221 E
1/9/01 16:00 MLD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 � Charlotte, NC 281-4-0543

. Lab Report
----w—n
iR
Full Service Analytical 8, Environmental Solutions
1/11/01 Page 4 of 7
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 4
P.O. Box 1111 Prism Sample ID: AB93890
Statesville, NC 28687 Login Group: WM112G7A .
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
'"0' TEST
PARAMETER RESULT
CALCULATIONS BASED ON DRY WT. 69
FECAL COLIFORM, SOLID Less than
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
REPORTING METHOD DATE/TIME
UNITS LIMIT REFERENCE STARTED ANALYST
% DRY WT. 0.01 SM 2540 G 1/10101 11:30 JMV
colonies/gram 3.0 SM 9221 E 1/9/01 16:00 MLD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ,&� P.O. Box 240543 � Charlotte, NC 28224-0543

- . Lab Report
- - Y � Plo-ar a� W�•
q m 11TY stcroN
,I -4
•:M Y � -r
Full Service Analytical 6 Environmental Solutions
1 /11 /01 w®n aschSlg® Pemdttirg
Page 5 of 7
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 5
P.O. Box 1111 Prism Sample ID: AB93891
Statesville, NC 28687 . Login Group: WM112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
REPORTING
METHOD
DATE/TIME
UNITS LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
69
% DRY WT. 0.01
SM 2540 G
FECAL COLIFORM, SOLID
Less than
1/10/01 11:30 JMV
colonies/gram 3.0
SM 9221 E
119/01 16:10 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road a P.O. Box 240543 e Charlotte, NC 28224-0543
Phone: 704/;79_AIA.1 - -r n c_,._ . -- --- - -- ----

Lab Report
Full Service Analytical & Environmental Solutions
1/11/01
Page 6 of 7
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 6
P.O. Box 1111
Prism Sample ID: AB93892
Statesville, NC 28687
Login Group: WM112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The following analytical results,have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED
ANALYST
CALCULATIONS BASED ON DRY WT.
64 % DRY WT. 0.01 SM 2540 G 1/10/01 11:30 JMV
FECAL COLIFORM, SOLID
Less than colonies/gram 3.0 SM 9221 E 119/01 16:10 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 � Charlotte, NC 282-74-0543

Lab Report
Full Service Analytical & Environmental Solutions
1/11/01 Page 7 of 7
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 7
P.O. Box 1111 Prism Sample ID: AB93893
Statesville, NC 28687 Login Group: WM112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED AMAI va-
CALCULATIONS BASED ON DRY WT. 68
FECAL COLIFORM, SOLID Less than
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
% DRY WT.
colonies/gram
0.01 SM 2540 G 1/10101 11:30 JMV
3.0 SM 9221 E 1/9/01 16:15 MLD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road P.O. Box 2.10543 � Charlotte, NC 28224-0543
P{.....,..-n.v/cart c", -r_.. .. - ---- -

� p�
RECEIVED
w
ATFR l AUTYSM70N
JAI 2 J 'U'
AlmOscharge Pemnlft
PATHOGEN/VECTOR ATTRACTION REDUCTION
CERTIFICATION STATEMENT
Pertaining to The Fourth Creek
Alkaline Stabilization Facility
I certify, under penalty of law, that the pathogen
requirements in 503.32 (a)(4) and vector attraction reduction
requirements in 503.33 (b)(6) have been met.
503.32 (a)(4): Pathogen Reduction
Stating the pH of the sewage sludge that is used or disposed
shall be raised to above 12 and shall remain above 12 for 72
hours. By adding fine alkaline materials and through exothermic
elevated the temperature to 52 Degrees Celsius for twelve hours
or longer during the period that the pH of the sewage sludge
is above 12. The sewage sludge has been air dried to achieve
a percent solids in the sludge greater than 50 percent.
503.33 (b)(6): Vector Attraction Reduction
The pH of sewage sludge has been raised to 12 or higher by alkali
addition and, without the addition of more alkali, has remained
at 12 or higher for two hours and then at 11.5 or higher for
an additional 22 hours.
This determination has been made under my direction and
supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the
information used to determine that these requirements have been
met. I am aware that there are significant penalties for false
certification including the possibility of fine and imprisonment.
Signed Cl�
(,J
Title
Date % 2,10 1

Lab Report
kh'.
.
f ls�.
Full Service Analytical & Environmental Solutions
4/10/01 Page 1 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 1
P.O. Box 1111 Prism Sample ID: AC03090
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2/01 11:40
Lab Submittal Date/Time: 4/2/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
I EST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
67
% DRY WT.
0.01
SM 2540 G
4/3101 22:00 JLW
FECAL COLIFORM, SOLID
Less than
colonies/gram
3.0
SM 9221 E
4/2/01 15:30 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road a P.O. Box 240543 — Charlotte, NC 282-74-0543

Lab Report J
Full service Analytical S Environmental solutions
4/10/01 Page 2 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 2
P.O. Box 1111 Prism Sample ID: AC03091
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 412101 11:40
Lab Submittal Date/Time: 4/2/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
I t"i I
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
57
% DRY WT.
0.01
SM 2540 G
4/3101 22:00 JLW
FECAL COLIFORM, SOLID
Less than
colonies/gram
4.0
SM 9221 E
4/2101 15:30 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road P.O. Box 240543 � Charlotte, NC 282-74-0543

Lab Report - -_-_
.�wsH.�Y�PM�Liwluwy�"?I19:1i^v
Full Service Analytical & Environmental Solutions
4/10/01 Page 3 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 3
P.O. Box 1111 Prism Sample ID: AC03092
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2/01 11:40
Lab Submittal Date/Time: 412/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
' CJ'
PARAMETER
TEST
REPORTING
METHOD
DATE/TIME
RESULT
UNITS
LIMIT
REFERENCE
STARTED
CALCULATIONS BASED ON DRY WT.
52
% DRY WT.
0.01
SM 2540 G
4/3/01 22:00
FECAL COLIFORM, SOLID
Less than
colonies/gram
4.0
SM 9221 E
4/2/01 15:30
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
ANALYST
JLW
MLD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road , P.O. Box 240543 —Charlotte, NC 28224-0543

Lab Report
Full Service Analytical & Environmental Solutions
4/10/01
Page 4 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 4
P.O. Box 1111
Prism Sample ID: AC03093
Statesville, NC 28687
Login Group: WM45G8
Sample Collection Date/Time: 4/2/01
11:40
Lab Submittal Date/Time: 4/2/01
13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED
ANALYST
CALCULATIONS BASED ON DRY WT.
63 % DRY WT. 0.01 SM 2540 G
413101 22:00 JLW
FECAL COLIFORM, SOLID
Less than colonies/gram 3.0 SM 9221 E
4/2/01 15:10 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road — P.O. Box 240543 � Charlotte, NC 28224-0543

Lab Report ,._.,�...:..�
ISM -
=i "uBORATORIE`
Full Service Analytical 8 Environmental Solutions
4/10/01
Page 5 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 5
P.O. Box 1111
Prism Sample ID: AC03094
Statesville, NC 28687
Login Group: WM45G8
Sample Collection Date/Time: 4/2/01
11:40
Lab Submittal Date/Time: 4/2/01
13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
59 % DRY WT. 0.01 SM 2540 G
4/3101 22:00 JLbv
FECAL COLIFORM, SOLID
Less than colonies/gram 3.0 SM 9221 E
4/2101 15:10 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road , P.O. Box 240543 � Charlotte, NC 28224-0543

Lab Report
Full Service Analytical & Environmental Solutions
4/10/01
Page 6 of 9
City of Statesville
Customer Project 1D: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 6
P.O. Box 1111
Prism Sample ID: AC03095
Statesville, NC 28687
Login Group: WM45G8
Sample Collection Date/Time: 4/2/01
11:40
Lab Submittal Date/Time: 4/2/01
13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT
DATE/TIME
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
60 % DRY WT. 0.01 SM 2540 G
413101 22:00 JLW
FECAL COLIFORM, SOLID
Less than colonies/gram 3.0 SM 9221 E
4/2/01 15:10 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road . P.O. Box 240543 — Charlotte, NC 28224-0543

Lei Report
,.:
t ISM
:
Full Service Analytical & Environmental Solutions
4110/01 Page 7 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 7
P.O. Box 1111 Prism Sample ID: AC03096
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2101 11:40
Lab Submittal Date/Time: 4/2/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
CALCULATIONS BASED ON DRY WT
FECAL COLIFORM, SOLID
Sample Comments:
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE ;TARTP:n
62 % DRY WT. 0.01 SM 2540 G
Less than colonies/gram 3.0 SM 9221 E
Angela D. Overcash, V.P. Laboratory Services
4/3/0122:00 JLW
4/2/0115:30 MLD
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 5pringbrook Road — P.O. Box 240543 � Charlotte, NC 28224-0543

Lab Report
Full Service Analytical & Environmental Soludons
4/10/01 Page 8 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME
P.O. Box 1111 Prism Sample ID: AC03097
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2101 11:40
Lab Submittal Date/Time: 4/2/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD DATE/TIME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
AMMONIA AS N
250
mg/kg
90
4500-NH3E
419101 17:15
KAP
MOLYBDENUM, TOTAL
2.7
mg/kg
1.0
6010
4/4/01 20:53
PRF
NITRATE
Less than
mg/kg
16
EPA 300
413/01 04:38
TAR
NITRITE
28
mg/kg
20
EPA 300
4/3/01 04:38
TAR
TOTAL KJELDAHL NITROGEN IN SOIL
2200
mg/kg
5.0
EPA 351.1
4/6101 21:17
LNE
TOTAL PHOSPHORUS
21
mg/kg
4.0
EPA 365.2
4/4/01 12:15
MBS
PLANT AVAILABLE NITROGEN
1.5
lb PAN/ton
0.05
NC Dept. Ag.
4/10/01 18:15
TAR
CALCULATIONS BASED ON DRY WT.
62
% DRY WT.
0.01
SM 2540 G
4/3/01 22:00
JLW
TOTAL PHOSPHORUS DIGESTION
Completed
SM 4500-P B
4/4101 09:05
MBS
AMMONIA DISTILLATION
Completed
SM4500-NH3B
4/9/01 16:00
KAP
TKN DIGESTION
Completed
SM4500-NorgB
414/01 07:55
NABS
pH
12•5
pH Units
SW 846 9045A
4/3/01 10:42
SMG
METALS DIGESTION METHOD 3050
Completed
SW846-3050
4/3/01 13:30
LC2
ARSENIC, TOTAL
8.0
mg/kg
1.0
SW846-6010B
4/4/01 20:53
PRF
CADMIUM, TOTAL
1.8
mg/kg
1.0
SW846-6010B
4/4/01 20:53
PRF
COPPER, TOTAL
40
mg/kg
2.0
SW846-6010B
4/4/01 20:53
PRF
ALUMINUM, TOTAL
350
mg/kg
4.0
SW846-6010B
415101 21:05
PRF
LEAD, TOTAL
95
mg/kg
1.0
SW846-6010B
4/4/01 20:53
PRF
NICKEL, TOTAL
18
mg/kg
1.0
SW846-6010B
4/4/01 20:53
PRF
ZINC, TOTAL
56
mg/kg
1.0
SW846-6010B
414/01 20:53
PRF
SELENIUM, TOTAL
28
mg/kg
0.20
SW846-6010B
4/4/01 20:53
PRF
CALCIUM, TOTAL
6900
mg/kg
1000
SW846-6010B
4/5101 21:05
PRF
MAGNESIUM, TOTAL
250
mg/kg
100
SW846-6010B
415101 21:05
PRF
SODIUM, TOTAL
53
mg/kg
1.00
SW846-6010B
4/5/01 21:10
PRF
POTASSIUM, TOTAL
440
mg/kg
100
SW846-60106
415/01 21:05
PRF
MERCURY DIGESTION
Completed
SW846-7471
4/5/01 11:50
LC2
MERCURY, TOTAL
0.05
mg/kg
0.03
SW846-7471
4/5/01 19:44
PRF
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 . Charlotte, NC 28224-0543

Lab Report
Full Service Analytical & Environmental Solutions
4110/01 Page 9 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME
P.O. Box 1111 Prism Sample ID: AC03097
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2/01 11:40
Lab Submittal Date/Time: 4/2/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATEMME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
NOTE: pH was analyzed out of the established EPA holding time.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 — Charlotte, NC 28224-0543

WATER uAttTYsgcnoN
NMp1sc9 P80WtU,,
PATHOGEN/VECTOR ATTRACTION REDUCTION
CERTIFICATION STATEMENT
Pertaining to The Fourth Creek
Alkaline Stabilization Facility
I certify, under penalty of law, that the pathogen
requirements in 503.32 (a)(4) and vector attraction reduction
requirements in 503.33 (b)(6) have been met.
503.32 (a)(4): Pathogen Reduction
Stating the pH of the sewage sludge that is used or disposed
shall be raised to above 12 and shall remain above 12 for 72
hours. By adding fine alkaline materials and through exothermic
elevated the temperature to 52 Degrees Celsius for twelve hours
or longer during the period that the pH of the sewage sludge
is above 12. The sewage sludge has been air dried to achieve
a percent solids in the sludge greater than 50 percent.
503.33 (b)(6): Vector Attraction Reduction
The pH of sewage sludge has been raised to 12 or higher by alkali
addition and, without the addition of more alkali, has remained
at 12 or higher for two hours and then at 11.5 or higher for
an additional 22 hours.
This determination has been made under my direction and
supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the
information used to determine that these requirements have been
met. I am aware that there are significant penalties for false
certification including the possibility of fine and imprisonment.
c
Signed W
TitlER I n
Date ( � IQ F
� I

t 1'._

Lab Report
JUL 1 9 20M
>J
Fug service Anayacw S Envir� SokMO s
7/18/01
Page 1 of 10
City of Statesville Customer Project ID: Sta-Lime 7/9101
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 1
P.O. Box 1111 Prism Sample ID: AC12326
Statesville, NC 28687 Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST
PARAMETER RESULT
CALCULATIONS BASED ON DRY WT. 75
FECAL COLIFORM, SOLID SM9221 E Less than
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
REPORTING
METHOD
DATE/TIME
UNITS
LIMIT
REFERENCE
STARTED ANALYST
% DRY WT.
0.01
SM 2540 G
7/9/01 17:00 ,1Lw
colonies/gram
3
SM 9221 E
7/9/01 16:20 TAR
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road & P.O. Box 240543 &. Charlotte, NC 28224-0543
Phone: [phone] � Toll Free Number 1-Rn015?o-fue - r— -7nAIC— ,,.,,,.

Lab Report
7/18/01
City of Statesville
Attn: Ms. Judy Wilcox
P.O. Box 1111
Statesville, NO 28687
- .1-Z
Full Service Analytical 3 Ernrircrwymu SW V,,s
Page 2 of 10
Customer Project ID:
Sta-Lime 719/01
Customer Sample ID:
STA LIME 2
Prism Sample ID:
AC12327
Login Group:
18761-19
Sample Collection Date/Time:
7/9/01 10:57
Lab Submittal Date/Time:
7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
PARAMETER
RESULT
CALCULATIONS BASED ON DRY WT.
75
FECAL COLIFORM, SOLID SM9221E
Less than
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
REPORTING METHOD DATE/TIME
UNITS LIMIT REFERENCE STARTED ANALYST
% DRY WT. 0.01 SM 2540 G 7/9101 17:00 JLW
colonies/gram 3 SM 9221 E 7/9/01 16:25 TAR
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road & P.O. Box 240543 �& Charlotte, NC 28224-0543
Phone: [phone] AL Tnll P—w.,., v-- i_annic,o cep. ,-___ -.--

Lab Report
Fus Service A-Vdcal 3 Emmot wdal Sauft s
7/18/01 Page 3 of 10
City of Statesville Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 3
P.O. Box 1111 Prism Sample ID: AC12328
Statesville, NC 28687 Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9101 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
REPORTING
UNITS LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
75
% DRY WT. 0.01
SM 2540 G
719/01 17:00 JLW
FECAL COLIFORM, SOLID SM9221E
Less than
coloniEs/gram 3
SM 9221 E
7/9/01 16:30 TAR
Sample Comments:
4��
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road .&, P.O. Box 240543 a, Charlotte, NC 28224-0543

7118101 Page 5 of 10
City of Statesville Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 5
P.O. Box 1111 Prism Sample ID: AC12330
Statesville, NC 28687 Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS BASED ON DRY WT. 65 % DRY WT. 0.01 SM 2540 G 719/01 17:00 JLW
FECAL COLI FORM, SOLID SM9221E Less than colonies/gram 4 SM 9221 E 7/9/01 16:40 TAR
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 &. Charlotte, NC 28224-0543
Phone: [phone] � Toll Free Number. 1-800/529-6364 � Fax: [phone]

Lab Report
a
:E •a
Full Service Maytleal 3 Envimnmental Solutions
7/18/01 Page 4 of 10
City of Statesville 'Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 4
P.O. Box 1111 Prism Sample ID: AC12329
Statesville, NC 28687 Login Group: 1876H9
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATEMME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
75
% DRY WT.
0.01
SM 2540 G
719/01 17:00 JLW
FECAL COLI FORM, SOLID SM9221E
Less than
colonies/gram
3
SM 9221 E
719/01 16:35 TAR
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road &� P.O. Box 240543 � Charlotte, NC 28224-0543
Phone: [phone] ,&. Toll Free Number: 1-800/529-6364 .A, Fax: [phone]

7/18/01 Page 5 of 10
City of Statesville Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 5
P.O. Box 1111 Prism Sample ID: AC12330
Statesville, NC 28687 Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
65
% DRY WT.
0.01
SM 2540 G
7/9/01 17:00 JLW
FECAL COLIFORM, SOLID SM9221E
Less than
colonies/gram
4
SM 9221 E
7/9/01 16:40 TAR
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Celt. No. 37735 - FL Certification No. E87519
449 Springbrook Road a. P.O. Box 240543 & Charlotte, NC 28224-0543
Phone: [phone] � Toll Free Number. 1-800/529-6364 A� Fam 704/525-0409

Lab .Report
--
Ain
:.� — N
Full service Ana"cal & Enviyonmeeta, Sokldwm
7/18/01 Page 6 of 10
City of Statesville Customer Project ID: Sta-Lime 7/9101
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 6
P.O. Box 1111 Prism Sample ID: AC12331
Statesville,.NC 28687 Login Group: 1876H9
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATEMME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
63
% DRY WT.
0.01
SM 2540 G
7/9/01 17:00 JLW
FECAL COLIFORM, SOLID SM9221E
3
colonies/gram
3
SM 9221 E
7/9/01 16:45 TAR
Sample Comments:
Angela D. Overcash, V.P. Laboratory Service's
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road .&, P.O. Box 240543 AL Charlotte, NC 28224-0543
Phone: [phone] & Toll Free Number. 1-800/529-6364 &. Fax: [phone]

Lab Report
"-1;
FuA Service Malytkal 6 Err horaroertW SohrUOM
7/18/01
Page 7 of 10
City of Statesville
Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox
Customer Sample ID: STA LIME 7
P.O. Box 1111
Prism Sample ID: AC12332
Statesville, -NC 28687
Login Group: 1876H9
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted
to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD DATEMME
RESULT UNITS LIMIT
REFERENCE STARTED ANALYST
CALCULATIONS BASED ON DRY WT..
66 % DRY WT. 0.01 SM 2540 G 7/9/01 17:00
FECAL COLIFORM, SOLID SM9221E
JLW
Less than colonies/gram 4 SM 9221 E
7/9/01 16:50 TAR
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 � Charlotte, NC 28224-0543
Phone: [phone] AL Toll Free Number: 1-800/529-6364 AL Fax: [phone]

Lab ,ReportA � ,
W-Mm'',
FuH Service Analytical 3 EnNrornnentW Sok rKm
7/18/01
Page 8 of 10
City of Statesville
Customer Project ID: Sta-Lime
7/9/01
Attn: Ms. Judy Wilcox
Customer Sample ID: STA LIME
P.O. Box 1111
Prism Sample ID: AC12333
Statesville,.NC 28687
Login Group: 1876H9
Sample Collection Date/Time: 7/9/01
10:57
Lab Submittal Date/Time: 7/9/01
14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED
ANALYST
SALMONELLA
Less than MPN/4g 1.3 503 SLUDGE
7/9/01 16:00 TAR
CALCULATIONS BASED ON DRY WT.
61 % DRY WT. 0.01 SM 2540 G
7/11/01 16:30 JLW
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 = NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 ,ft Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number. 1-800/529-6364 &. Fax: [phone]

Lao Report
7/18/01
City of Statesville
Attn: Ms. Judy Wilcox
P.O. Box 1111
Statesville, NC 28687
Full Service Analytical & Environmental Sdutlom
Page 9 of 10
Customer Project ID: Sta-Lime 7/9/01
Customer Sample ID: STA LIME
Prism Sample ID: AC12334
Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 .10:57
Lab Submittal Date/Time: 7/9/01 14:4.5
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED
ANALYST
AMMONIA AS N
420
mg/kg
79
4500-NH3E
7/11/01 14:15
MBS
MOLYBDENUM, TOTAL
3.6
mg/kg
1.0
6010
NITRATE
7117/01 11:47
MSC
Less than
mg/kg
16
EPA 300
7111/01 12:24
TAR
NITRITE
Less than
mg/kg
16
EPA 300
7/11/01 12:24
TAR
TOTAL KJELDAHL NITROGEN IN SOIL
6600
mg/kg
0.5
EPA
TOTAL PHOSPHORUS
351.1
7/11/01 17:11
EHT
52
mg/kg
10
EPA 365.2
7/10/01 13:35
MBS
PLANT AVAILABLE NITROGEN
4.1
lb PAN/ton
0.05
NC Dept. Ag.
7/16/01 13:56
CALCULATIONS BASED ON DRY WT.
63
JAS
% DRY WT.
0.01
SM 2540 G
719/01 17:00
JLW
TOTAL PHOSPHORUS DIGESTION
Completed
SM 4500-P B
7/10/01 10:20
MBS
AMMONIA DISTILLATION
Completed
TKN DIGESTION
SM4500-NH3B
7/11/01 12:05
MBS
Completed
SM4500-Norg6
7/10/01 07:20
MBS
METALS DIGESTION METHOD 3050
Completed
SWB46-3050
7/10/0112:45
LC2
ARSENIC, TOTAL
12
rng/kg
1.0
SWB46-6010B
7/17/01 11:47
MSC
CADMIUM, TOTAL
Less than
m g/kg
1.0
SW846-6010B
7/17/01 11:47
MSC
COPPER, TOTAL
68
mg/kg
2.0
SW846-601013
7117101 11:47
MSC
ALUMINUM, TOTAL
16000
mg/kg
100
SW846-6010B
7/17/01 12:01
MSC
LEAD, TOTAL
29
mg/kg
1.0
SW846-6010B
7/17/01 11:47
MSC
NICKEL, TOTAL
15
mg/kg
1.0
SW846-6010B
7/17101 11:47
.
MSC
ZINC, TOTAL
69
mg/kg
1.0
SW846-6010B
7/17/0111:47
MSC
SELENIUM, TOTAL
23
mg/kg
2.0
SW846-6010B
7/17/01 11:47
MSC
CALCIUM, TOTAL
320000
mg/kg
10000
SW846-6010B
7/17101 12:25
MSC
MAGNESIUM, TOTAL
12000
mg/kg
100
SW846-60108
7/17101 12:01
MSC
SODIUM. TOTAL
1500
mg/kg
20
SW846-6010B
7/17/01 11:57
MSC
POTASSIUM, TOTAL
16000
mg/kg
100
SW846-60108
7/1710112:01
MSC
MERCURY DIGESTION
Completed
MERCURY, TOTAL
SW846-7471
7/12101 12:30
LC2
0.04
mg/kg
0.03
SW846-7471
7/13/01 13:12
PRF
pH
12.0
pH Units
SW846-9045C
7/10/01 14:35
SMG
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road � P.O. Box 240543 ,&� Charlotte, NC 28224-0543
Phone: [phone] ah, Toll Free Number. 1-800/529-6364 � Fax: [phone]

Lan meport
7/18/01
Page 10 of 10
City of Statesville
Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox
Customer Sample ID: STA LIME
P.O. Box 1111
Prism Sample ID: AC12334
Statesville,.NC 28687
Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD DATEMME
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
NOTE: pH was analyzed out of the established EPA holding time
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ,.& P.O. Box 240543 -& Charlotte, NC 28224-u543
Phone: [phone] &� Toll Free Number: 1-800/529-6364 A� Fam 704/525-0409

I certify,
requirements in
requirements in
RECEIVED
WEROUAt ITYSEG770N
PATHOGEN/VECTOR AT « MAIWHIMWTION
CERTIFICATION STATEMENT
Pertaining to The Fourth Creek
Alkaline Stabilization Facility
under penalty of law, that the pathogen
503.32 (a)(4) and vector attraction reduction
503.33 (b)(6) have been met.
503.32 (a)(4): Pathogen Reduction
Stating the pH of the sewage sludge that is used or disposed
shall be raised to above 12 and shall remain above 12 for 72
hours. By adding fine alkaline materials and through exothermic
elevated the temperature to 52 Degrees Celsius for twelve hours
or longer during the period that the pH of the sewage sludge
is above 12. The sewage sludge has been air dried to achieve
a percent solids in the sludge greater than 50 percent.
503.33 (b)(6): Vector Attraction Reduction
The pH of sewage sludge has been raised to 12 or higher by alkali
addition and, without the addition of more alkali, has remained
at 12 or higher for two hours and then at 11.5 or higher for
an additional 22 hours.
This determination has been made under my direction and
supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the
information used to determine that these requirements have been
met. I am aware that there are significant penalties for false
certification including the possibility of fine and imprisonment.
Signed LS
Title
Date %d - i' 0

I certify,
requirements in
requirements in
-- -Z
PATHOGEN/VECTOR ATTRACTION REDUCTION
CERTIFICATION STATEMENT
Pertaining to The Fourth Creek
Alkaline Stabilization Facility
under penalty of law, that the pathogen
503.32 (a)(4) and vector attraction reduction
503.33 (b)(6) have been met.
503.32 (a)(4): Pathogen Reduction
Stating the pH of the sewage sludge that is used or disposed
shall be raised to above 12 and shall remain above 12 for 72
hours. By adding fine alkaline materials and through exothermic
elevated the temperature to 52 Degrees Celsius for twelve hours
or longer during the period that the pH of the sewage sludge
is above 12. The sewage sludge has been air dried to achieve
a percent solids in the sludge greater than 50 percent.
503.33 (b)(6): .Vector Attraction Reduction
The pH of sewage sludge has been raised to 12 or higher by alkali
addition and, without the addition of more alkali, has remained
at 12 or higher for two hours and then at 11.5 or higher for
an additional 22 hours.
This determination has been made under my direction and
supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the
information used to determine that these requirements have been
met. I am aware that there are significant penalties for false
certification including the possibility of fine and imprisonment.
Signed L
LA
Title
Date / 2-9- 0

Lab Report
C 12 20 S S2 mc I N
Full Service Analytical & ErMronmental Solutions
10/11/01 Page 1 of.9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith Customer Sample ID: STA-LIME
P.O. Box 1111 Prism Sample ID: AC21938
Statesville, NC 28687 Login Group: WM05H8
Sample Collection Date/Time: 10/2/01 11:00
Lab Submittal Date/Time: 10/2/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
AMMONIA AS N
190
mg/kg
3.4
4500-NH3E
10/10/01 15:35
MBS
MOLYBDENUM, TOTAL
3.8
mg/kg
1.0
6010
10/5101 13:07
MSC
NITRATE
Less than
mg/kg
6.8
EPA 300
10/9101 00:56
TAR
NITRITE
6.8
mg/kg
6.8
EPA 300
10/9/01 00:56
TAR
TOTAL KJELDAHL NITROGEN IN SOIL
79000
mg/kg
51000
EPA 351.2
10/4/01 20:29
EHT
TOTAL PHOSPHORUS
19
mg/kg
3.0
EPA 365.2
10/3101 13:45
MBS
PLANT AVAILABLE NITROGEN
47.5
lb PAN/ton
0.05
NC Dept. Ag.
10/10/01 15:30
TAR
TOTAL RESIDUE
750000
%
500
SM 2540 B
10/4101 19:00
EHT
CALCULATIONS BASED ON DRY WT.
74
% DRY WT.
0.01
SM 2540 G
10/3/01 17:30
JLW
TOTAL PHOSPHORUS DIGESTION
Completed
SM 4500-P B
10/3/01 08:25
MBS
AMMONIA DISTILLATION
Completed
SM4500-NH3B
10/10/01 14:10
MBS
TKN DIGESTION
Completed
SM4500-NorgB
10/3/01 08:00
MBS
METALS DIGESTION METHOD 3050
Completed
SW846-3050
1013/01 11:30
LC2
ARSENIC, TOTAL
10
mg/kg
1.0
SW846-6010B
10/5101 13:07
MSC
CADMIUM, TOTAL
1.4
mg/kg
1.0
SW646-6010B
10/5101 13:07
MSC
COPPER, TOTAL
53
mg/kg
2.0
SW846-6010B
1015/01 13:07
MSC
LEAD, TOTAL
73
mg/kg
1.0
SW846-6010B
10/5101 13:07
MSC
NICKEL, TOTAL
13
mg/kg
1.0
SW846-6010B
10/5/01 13:07
MSC
ZINC, TOTAL
52
mg/kg
1.0
SW846-6010B
1015101 13:07
MSC
SELENIUM, TOTAL
39
mg/kg
2.0
SW846-6010B
10/5/01 13:07
MSC
SODIUM, TOTAL
1300
mg/kg
20
SW846-6010B
10/5/01 13:30
MSC
POTASSIUM, TOTAL
22000
mg/kg
1000
SW846-60108
10/5/01 13:26
MSC
MERCURY DIGESTION
Completed
SW846-7471
10/5/01 11:00
LC2
MERCURY, TOTAL
0.29
mg/kg
0.02
SW846-7471
10/5/01 17:27
TAR
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report f
- M
Full Service Analytical & Envcprff�ffll Sc6lio g
10/11/01 Page 2 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith Customer Sample ID: STA-LIME
P.O. Box 1111 Prism Sample ID: AC21938
Statesville, NC 28687 Login Group: WM051-18
Sample Collection Date/Time: 10/2/01 11:00
Lab Submittal Date/Time: 10/2/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report.
Fu0 Service Anwyr W 6 E-mnmeniw Sd ff*,.
10/11/01
Page 3 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIMEi
P.O. Box 1111
Prism Sample ID: AC21939
Statesville, NC 28687
Login Group: WM051-18
Sample Collection Date/Time: 10/2/01
11:00
Lab Submittal Date/Time: 10/2/01
14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED AN1AI VQT
CALCULATIONS BASED ON DRY WT. 64 % DRY WT. 0.01 SM 2540 G 1013/01 17:30 JLW
FECAL COLIFORM, SOLID SM9221 E Less than colonies/gram 4.0 SM 9221 E 10/2101 15:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report
ON -
Fug Service An*ucw 3 ErtvironmenW Soklwm
10/11/01
Page 4 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIME2
P.O. Box 1111
Prism Sample ID: AC21940
Statesville, NC 28687
Login Group: WM05H8
Sample Collection Date/Time: 10/2/01
11:00
Lab Submittal Date/Time: 10/2/01
14:40
The following analytical results have been obtained for the indicated sample which was submitted
to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATEMME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
68
% DRY WT.
0.01
SM 2540 G
10/3/01 17:30
JLW
FECAL COLIFORM, SOLID SM9221E
Less than
colonies/gram
4.0
SM 9221 E
1012101 15:45
MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report
srµ
Full Service Analyt}cal 3 FrvkonmenW Sohifion,
10/11/01
Page 5 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIME3
P.O. Box 1111
Prism Sample ID: AC21941
Statesville, NC 28687
Login Group: WM051-18
Sample Collection Date/Time: 10/2/01
11:00
Lab Submittal Date/Time: 10/2/01
14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD
DATE/TIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
80 % DRY WT. 0.01 SM 2540 G
10/3/01 17:30 JLW
FECAL COLIFORM, SOLID SM9221 E
Less than colonies/gram 3.0 SM 9221 E
1012101 15:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification, No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report
ti
FuA Service Anaytical 3 Envkonmental gpkypp,,
10/11/01
Page 5 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIME3
P.O. Box 1111
Prism Sample ID: AC21941
Statesville, NC 28687
Login Group: WM05H8
Sample Collection Date/Time: 10/2/01 11:00
Lab Submittal Date/Time: 10/2101 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD DATE(rIME
PARAMETER
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
80 % DRY WT. 0.01 SM 2540 G 1013101 17:30 JLW
FECAL COLIFORM, SOLID SM9221 E
Less than colonies/gram 3.0 SM 9221 E 1012/01 15:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report _-
• � j....,�._ ".may
FuB Service An*Ucw 3 EnVkornnWM Solutions
10/11/01
Page 6 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIME4
P.O. Box 1111
Prism Sample ID: AC21942
Statesville, NC 28687
Login Group: WM05H8
Sample Collection Date/Time: 10/2/01
11:00
Lab Submittal Date/Time: 10/2/01
14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATEITIME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
78 % DRY WT. 0.01 SM 2540 G
10/3/01 17:30 JLW
FECAL COLIFORM, SOLID SM9221E
Less than colonies/gram 3.0 SM 9221 E
10/2/01 16:30 MLD
Sample Comments:
4��
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report -�
FuU SMICG AnW YWal 3 Errii wmw fal Solt,,
10/11/01 Page 7 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith Customer Sample ID: STA-LIME5
P.O. Box 1111 Prism Sample ID: AC21943
Statesville, NC 28687 Login Group: WMO51­18
Sample Collection Date/Time: 10/2/01 11:00
Lab Submittal Date/Time: 10/2/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
80
% DRY WT.
0.01
SM 2540 G
10/3101 17:30 JLW
FECAL COLIFORM, SOLID SM9221 E
Less than
colonies/gram
3.0
SM 9221 E
1012/01 16:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report
R�
Full Service Analyt 3 Envlr nmen}al Solutions
10/11/01 Page 8 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith Customer Sample ID: STA-LIME6
P.O. Box 1111 Prism Sample ID: AC21944
Statesville, NC 28687 Login Group: WM05H8
Sample Collection Date/Time: 10/2/01 11:00
Lab Submittal Date/Time: 10/2/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
I is l
TEST
REPORTING
METHOD
DATE/TIME
—PARAMETER'
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
68
% DRY WT.
' 0.01
SM 2540 G
10/3/01 17:30 JLW
FECAL COLIFORM, SOLID SM9221E
Less than
colonies/gram
3.0
SM 9221 E
10/2/01 16:45 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

Lab Report
VAN,��1 Full Service Analytical s E � Sokdjom
2 1-5
10/11 /01
NoI}Dlacharg® Pam
.no
Page 9 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIME?
P.O. Box 1111
Prism Sample ID: AC21945
Statesville, NC 28687
Login Group: WM05H8
Sample Collection Date/Time: 10/2/01
11:00
Lab Submittal Date/Time: 10/2/01
14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
73 % DRY WT. 0.01 SM 2540 G
10/3101 17:30 JLW
FECAL COLIFORM, SOLID SM9221E
Less than colonies/gram 3.0 SM 9221 E
10/2/01 16:55 MLD
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519

MPN
DATA

._,a n- 07 - 02 1 5 : 26
P_02
i S.
t3oRATORIE_S, INC.
Full Service Anaryaral & Envuonrnental Solufions
City of Statesville
Attn: Mr, Andy Smith
PO Box 1 111
Statesville, NC 28687
Dear Mr. Smith,
RECEIVED
WATER QUALITY MOTION
.0 —
NOBi��I�GG�!!�� P�mti
.January 7, 2( 02
Main Office:
449 Springbrook Road
P.O.'Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
1 /800/529-6364
Fax: [phone]
[e-mail]
This letter is in reference to your request for a change in the reporting units for fecal
coliform. Prism can only report MPNs as "colonies/gram" because of our reps rting system. This
unit of measure can also be interpreted as "most probable number per gram c , total dry solids. I
hope this does not inconvenience you in your quarterly reports, as we have re,ised and are
sending new ones to you. If you need any further assistance, please give me a call.
Sinc rely,
Whitney Mut roe
Project Mani Eger

. .,; �..�
,,., •L, ,. � .,.°

Lab Report
Todays Date: January 7, 2002
City of Statesville
Attn: Andy Smith
P.O. Box 1111
Statesville. NC 28687
K
PRISM
LASOgAL[ORIE9, INC.
Full Scivk ❑ AmAyl,c:,l
ft �uvnunurtsunl ±UIUI;U�•;
REVISED LABORATORY REPORT
Client Project ID: StaLime
Client Sample ID: StaLime
Prism Sample ID: AB93887-93; AC03090-6
AC12326-32; AC21939-45
Prism Login Group: WM112G7A; WM45G8:
1876Hg; WM051-18
The attached laboratol y report is a revision and supersedes our original laboratory report dated
January 11, 2001 April 10, 2001
July 18, 2001 October 11, 2001
It you have questions, )lease call us.
Angela D. Overcash, �.P_ Laboratory Services
Prepared by: Cara Rusmisell
F-%commonlrevlab.xls
Created 3/16/00 Revised 3130100
I I.1 Ko.v A. 1'0- &,,. 24:'-, d h.,,!, ,,, \C• 24224-(I'.:I:1
li I(- 70•ii-7?9-0o4 & T„11 rry N n,tii•( I r0i1:5",+-h{A•1L Vo>7114;;;';-041r,

Lab Report
I�.
PRISM
LABORATORIES, INC.
fiI
Lull r; Analytical
d tnwionine,ttal bOIUl.On6
117/02
Page 1 of 7
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 1
P.O. Box 1111
Prism Sample ID: AB93887
Statesville, NC 28687
Login Group: Wfd1112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time: 1/9101 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD DATE(rIME
PARAMETER
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS BASED Ol, DRY WT.
68 °!" DRY WT. 0,01 SM 2540 G 1/10101 11:30 JMV
FECAL COLIFORM, SOLID
Less than coloniesigram 3.0 SM 9221 E 111r01 15:45 MLD
Sample Comments:
NOTE: Fecal conform is reported in colonies/gram. This can also be interpreted as "most probable number
per grant of total dry s, Aids".
NOTE: This report is. I revision and supersedes our original laboratory report dated 1/11/01.
Angela D. Overcash, 1 .P. Laboratory Services
NC Certification No. 402 SC Cortitication No. 99012 • NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
1'1`J til�tin�;Lntt�h Rtmd A I'() I1,, )#(,; � (711, ItIII , :'�(' �!i?;�Q 11;41
19� RtC 'UJ; i'�N.l�.SI�'I � :JII t t:c \umhrr: 7-tilNl'.i�u-(i;3nQ � t'it� i1)i: ti_''1-(1.1117
F, 0 - .4

Lab Report
117/02
}gay.
PRISM
LABORATORIES, &C.
[t[ t--•
I I,II ;ir!n,:,� A:781y h�:ii
ii t,lvil (111r11P,�IRi S:,luil(1115
Page 2 of 7
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 2
P.O. Box 1111
Prism Sample ID: AB93888
Login Group: WM112G7A
Statesville, NC 286a7
Sample Collection Date/Time: 119/01 10:15
Lab Submittal Date/Time: 1/9/01 14:40
The folio -wing analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD UATEMME
PARAMETER
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS BASED ON DRY WT. 70 % DRY WT. 0.01 SM 2540 (33 1/10/111 11:30 JMV
FECAL COLIFORM. SOLID Lass than colonies/gram 30 S1V1 9221 F 119101 15:45 MILD
Sample Comments:
NOTE: Fecal cc111form is roported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s Aids".
NOTE. This report is. I revision and supersedes our original laboratory report dated 1/11/01.
Angela D, Overcash, \ P. Laboratory Services
NO Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cort, No, 37735 - FL Certification No. EU7519
441, `,L)rmgl,ioo I:n.1,i & 11C1 13,- :LJrI t A6 (Jio -loue NC' tr-'' 4.0) i 1
'• !n: 'Q� • ��'+-[i 1r,1 � IJIi I'r Cc I\unrhrr� I-4i 1;1; ;r;�l.(,1h4 ® I�;r� 711�i't l'�-t bl(hl

Lab Report
Nr.
PRLSM
Lw9pRA7pglES, INC.
hill .`:hfV".? AlIVyh[al
& tilw01lflatllal Solullon5
117/02
Page 3 of 7
City of Statesville
Customer Project ID: Sta-lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 3
P.O. Box 1111
Prism Sample 10: AB93889
Statesville, NC 28687
Login Group: WM112G7A
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date/Time' 1/9/01 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTIN(3 METHOD DATEfTIME
PARAMETER
RESULT UNITS LIMIT REFEkENCE STARTED ANALYST
CALCULATIONS GASED OP DRY WT.
67 % DRY WT. 0.01 SM 25A0 r; 1/10101 11 30 JMV
FECAL COLIFORM, SOLID
Less than colonieslgram 3.0 SM 9221 E '119101 16.00 MLD
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s )Iids".
NOTE: This report is I revision and supersedes our original laboratory report dated 1/11/01.
Angela D. Over -cash, \ .P. Laboratory Services
INC Certification No 402 - SC Certification No. 99012 - NC Drinking Waco► Cert. No. 37735 - FL Certification No. E87519
I.1'l tihrrr�� l'nKJ. Ro,id 0 I'() li i ?40 54°• A C'har:.>nr, N(. .'.8224 0
- Tull rrry Nimi rl 900 52'L-01e1 A I -'t. 7(11; i' , 040,)
Cn - A

Lab Report
PRISM
LA®OWATOPIES, INC.
-•ti,l1a
=wi S"v �7 Analytical 3 Environmcm4 Sottgwn;
117/02
Page 4 of 7
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID.- STALIME B
P.O. Box 1111
Prism Sample ID: AB93890
Statesville, NC 28687
Login Group: WM112G7A
Sample Collection DatelTime: 1 /9101 10:15
Lab Submittal Date/Time: 1 /9/01 14 40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD DATE/TIME
PARAMETER
RESULT UNITS LIMIT REFERENCE 51ARTED ANALYST
CALCULATIONS BASED OD DRY WT. 69 "/o DRY WT. 0.01 SM 2540 G 1r10/01 11:30 JP.".v
FECAL COLIFORNI, SOLID Less than colonioslgram 3.0 SM g221 E UP101 1CN:00 MLD
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s aids".
NOTE: This report is 1 revision and supersedes our original laboratory report dated 1111101.
Angela D. Overcash, 1 P. Laboratory Services
NC Certification No 402 - SC Certification No. 99012 - INC Drinking Water Cert. No. 37739 - FL Certllication No. E87519
'I1` 1,pinhbrook road 0 ll.t,l. It,-?4054,', Ak s,harlotty. Vt 2812'1•If;,11
1'I� tlu•:';•11-0j �?t)-l��r;d �'it�ll Pnrc I\umhrl". 1-411(t; j'�I•h;(�; � I�at:'ll�{r ti,{',.IFlil'i

Lab Report
PRISM
't
a
cy I.A80RATOMES.INC.
ruu Se"ncc Analvuwl is Envi+or+mcnyl ;ntutl.I
117102
Page 5 of 7
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 5
P.O. Box 1111
Prism Sample ID: AB93891
Login Group: WM112G7A
Statesville, NC 28687
Sample Collection Date/Time: 1/9/01 10:15
Lab Submittal Date(Time- 1/9101 14:40
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD DATElTIME
PARAMETER
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS RASEr) (In DRY WT.
G9 % DRY WT 0.01 SM 2540 G 1/10/01 11:30 .1MV
FECAL COLIFORM_ SOLO
Less than Colonieslgram 3.0 SM 9221 E liljiot 16:10 MLu
Sample Comments:
NOTE: Fecal coliform Is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s )lids".
NOTE: This report is I revision and supersedes our original laboratory report dated 1/11101
Angela D. Ovorcash. V.P. Laboratory Services
NC Cortlbcatlon No. 402 SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certlticatlon No. E87519
H',) 5Vtmgbrook Road & PO Iim 2•I11.311 Aki.harlt !tc \l
1'I +nc: 704/ "I-6:' Id AL lull t`:cc .Numbt•r' 1-KINIr SL'1-!::I(ri A h'at-iu1:,2 , t14t1•,

Lab Report
PRISM
LABORATORIES, INC.
fVfl GCrvi1':- Aniriyti;;, 1 f. r'r;vir,:nrnr:nl;rl $nlirrinrr:
1/7102
Page 6 of 7
City of Statesville
Customer Proloct 10: Sta-Lime
Attn. Ms. Judy Wilcox
Customer Sample ID: STALIME 6
P.O. Box 1111
Prism Sample ID: AB93892
Statesville, NC 28687
Login Group: WM112G7A
Sample Collection Date/Time: 1/9101
10:15
Lab Submittal Date/Time: 119/01
14A0
The following analytical results have been obtained
for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING METHOD
DATE/TIME
PARAMETER
RESULT
UNITS LIMIT REFERENCE
SIAHTEU ANALYST
CALCULATIONS BASED OP DRY WT.
64
% DRY WT. 0.01 SM 2540 G
1110/01 11:30 JMV
FECAL COLIFORM. SOLID
Less than
colonies/gram 1.0 SM 9221 E
1 /91W 18:10 MLO
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram, This can also be interpreted as "most probable number
per gram of total dry s Yids".
NOTE: This report is I revision and supersedes our original laboratory report dated 1/11101.
Angela D. Overcash. 1 P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
Il nno. (F1; .,xr-636.4 - Tell rrrr: Number SIIfI. 5'(14)3i4 A F:A: %04. ti'1-fbll:4

Lab Report
PRISM
`• ylh'"... �4,,,, LABORATORIES, INC.
AnalyG(.ad R bwomnmemal SoWuona
1/7102
Page 7 of 7
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 7
P.O. Box 1111
Prism Sample ID: A593893
Login Group: WM112G7A
Statesville, NC 28687
Sample Collection Date/Time: 1/9101
10:1 S
Lab Submittal Date/Time: 119101
14:40
The following analytical results have been obtained for the indicated sample which was submitted
to this laboratory
TEST
TEST REPORTING METHOD
DATEITIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED OP DRY WT.
68 DRY WT. 0.01 SM 2540 G
1110101 11:30 JMV
FECAL COLIFORM, SQI.tU
Less than cotenies/gram 3.0 SM 9221 E
'119,01 16:15 MLD
Sample Comments:
NOTE: Fecal conform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s )lids".
NOTE: This report is 1 revision and supersedes our original laboratory report dated 1/11101
Angela D. Overcash. V.P. Laboratory Services
NC Certification No. 402 • SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No 287519
4•II �prutl;lvvuh Ru, d � i'(1. Iil�s ? I(I;r13 � Lhariullc. NC _i?_4-115•ia
IT me: 7011;52Q 6164 �& Toll rn- Numbir. 1 1400i;;29 63M O 1-,iv

Lab Report
PRISM
F"II $rrYici• An;dylu:, { n ruvirUnrnenl;d ^wdnli...
1/7/02 Page 1 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn. Ms. Judy Wilcox Customer Sample ID: STALIME 1
P.O. Box 1111 Prism Sample ID: AC03090
Statesville, NC 28687 Login Group: WM45GB
Sample Collection Date/Time-. 4/2/01 11.-40
Lab Sunmlttal Date/Time, 412/01 13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
I)ATErrlME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED Or DRY WT.
67
% DRY WT.
0.01
SM 2540 G
4/3/01 22.00 JLW
FECAL COLIFORM. SOLID
Less than
colonies/gram
3.0
SM 9221 E
412/01 15:30 MILD
Sample Commonts:
NOTE: Fecal coliform is reported in colonies/gram.
This can also
be interpreted as "most
probable number
per gram of total dry s Aids".
NOTE: This report is I revision and supersedes our original laboratory report dated 4110/01
Angela D. Overcash• 1'.P. Laboratory Services
NC Cortlficatlon No. 402 SC Certification No 99012 - NC Drinking Water Cert, No, 37735 - FL Certificat-ion No. E87519
43H tipnn�hrnnw 1t(-d A ttU. Liu\ 240541 A, Chorlotty N( 1+ 02141i.O
7(14: 5N 6364 A, Trill FrNr .Vuroh7r. 1-13011529 (13e4'A F;:x::04 i.12)-0II')
0T e-1 -

Lab Report
r
PRISM
LA®ORATOp188, INC.
run Sehwi.Anatyldet & tunonmantal Solutions
1 /7/02
Page 2 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 2
P.O. Box 1111
Prism Sample ID: A003091
Statesville, NC 28687
Login Group: WM45G8
Sample Collection Date/Time: 412101
11:40
Lab Submittal DatelTime: 4/2101
13:15
The following analytical results have been obtained for the indicated sample which was submitted
to this laboratory
TEST
TEST REPORTING METHOD
DATEITIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED Ob DRY WT.
57 % DRY WT. 0.01 SM 2540 G
4/3/01 22:00 JLW
FECAL CULIFORM, SOl10
Lass than coloniesigram 4.0 SM 922 t C.
4!2/Ot %SiK MLD
Sample Commcnts:
NOTE: Fecal coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s Aids". ,
NOTE: This report is I revision and supersedes our original laboratory report dated 4/10101
.
Angela D. Overcash. V.P. Laboratory Services
NC Cortlficatton No. 402 SC C,a:i,;icauun Nu 99012 - NC Drinking Water Cert, No. 37735 - FL Certification No. E87519
a�`. 51ntn} hn :k 4ved 0 PO tint, 2 it1S;'t p ( harlojj%�• 1'(- '�8214 0;41
I'1 .a:e[ 114i i2t1-f:.ih•I S Ii1il Fnvo Nuntln•r 7-h 111/^."t-e;iti•IA )•,i\: 704/;);_l141?11
L L o

Lab Report
fi.
PRISM
LABORATORIES. INC.
3
r n Scw,rc AuaiyNcal
a E11W611d1B0I91 SOWIIons
1/7102
Page 3 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 3
P.O. Box 1111
Prism Sample ID: AC03092
Login Group: WM45G8
Statesville, NC 28687
Sample Collection Date/Time: 412101
11:40
Lab Submittal Date(Time: 4/2101
13:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD
DATE/TIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
52 % DRY WT. 0.01 SM 2540 ti
4/3/01 12:00 JLW
FECAL COLIFORM. SOLID
Loss than roionios/gram 4.0 SM 9221 E
4/2!01 15,30 MILD
Sample Comments:
NOTE: fecal coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s Aids".
NOTE: This report is I revision and supersedes our original laboratory report dated 4/10101.
Angela D. Overcash, N P. Laboratory Services
NC Certification No. 402 • SC Ccritication No. 99012 - INC Drinking Wator Cori, No. 37736 - FL Certification No. E87 519
440 Springbrook Rood ♦ 11C1 Hox 24i1;41 Ak (harlove, Ni
VI- mv: 04i 521) 1i164 Ak'Ia+1'. I-rrr Numhpr; 1 ht?p/ 5?`> o.364 & Fax 109

Lab Report
PR.ISM
ai.
r
LABORATORIES, INC.
uil Sf.iW­ A•lelycica! d Enwonmoltal !;,Aprons
1/7/02 Page 4 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME 4
P.O. Box 1 111 Prism Sample ID: AC03093
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4001 11.40
Lab Submittal Date/Time: 4/2/01 13:15
The following analytical -esults have been obtained for the Indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATEMME
PARAMETER
RESULT
UNITS LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY wT,
63
% DRY WT. 0.01
SM 2540 G
411/01 22:00 JLw
FECAL COLIFORMI, SOLID
Less than
colonies/gram 3.0
SM 922I E
4r2101 15-t(D MLO
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram. This can also be interpreted as "most
probable number
per gram of total dry s, )lids".
NOTE. This report is - I revision and supersedes our original laboratory report dated 4110101
Angela D. Overcash, V.P. Laboratory Services
�"C C2rt; cation ?40. "07 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification Fvo. E87519
4414 tihrinphnhok hood A I'.(_). Bvx 1an>4'� (ii,(rl.�ilr. \(: 2K24 (1543
PI',.nc 7(14/�2q 1064 A 1041 Frei• Number l•r ilU %.7'_ 1 6�(� O 1dz 7O•li i'.i-(LIC)

Lab Report RECENE®
WATER OUALI Y sEcn®m c4 PRISM
I y LA90R=RtEs, If'IC.
0*uil Sn—t;: Anidylgt jd A r.wi.n...... +l &LIL(lonl,
117102
Page 5 of 9
City of Statesville
Customer project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 5
P.O. Box 1111
Priam Sample ID: AC03094
Statesville, NC 28687
Login Group: WM45G8
Sample Collection Date/Time, 4/2/01
11:40
Lab Submittal Date/Time: 4/2101
13:15
The following analytical results have been obtained for the indicated sample which was submilted to this laboratory
TEST
TEST REPORTING METHOD
DATE1TIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS UASED O1� DRY WT.
59 % DRY WT, 0.01 SM 2540 G
4/3/0'1 22:00 JLW
FECAL COUFORM. SOLID
Less than coloniesigram 3.0 SM 9221 F
4/2/01 15:10 MLD
Samplo Comments:
NOTE: Fecal Coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s )lids".
NOTE: This report is I revision and supersedes our original laboratory report dated 4110/01.
Angela C. Overcash. \ P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 • NC Drinking Water Cert. No. 37735 - FL Cr:rtification No. E87519
I I,, LI;f'n • nn•,l 11 1' cl �& I'O Hox '- Hl i 13iii
i'I .rlr ;11q:=9'Lb-it:iGi �, dull I`rcc Nulnhr•r: I-NUn: i ��Id.in1 Fax. 7t14i midi;u4

Lab Report
t._
PRISM
.� LABORAT01111ei, INC.
It
r,,a L;-v.-: Artatyaaal & hnvntonmental SOutiong
1/7102
Page 6 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 6
P.O. Box 1111
Prism Sample ID: AC03095
Login Group: WM45G8
Statesville, NC 28687
Sample Collection DatelTime: 4/2101
11 A0
Lab Submittal Date/Time: 4/2101
13:15
The following analytical esults have been obtained for the indicated sample which was submitted
to this laboratory
TEST
TEST REPORTING METHOD
VATEITIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT..
60 % DRY WT. 0.01 SM 2540 G
413101 22:00 JLW
FECAL COLIEORM, SOLID
Less than colonies/gram 3.0 SM 9221 F
412101 15:10 MLD
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s, )lids".
NOTE: This report is; I revision and supersedes our original laboratory report dated 4110101
Angela D. Overcash, \ P. Laboratory Services
NC Certification No. 402 • SC Certification No. 99012 • NO urink&oU :vater Cen, No. 37735 - FL Certlf r-Mion No. E87519
�44 ;l.nn} 4irthrk Npdk1 L 111). Box 240543 & ('I,mloilr, NC2y224i3 1
I'l miv: 704/529-634,1 AL 101 FPgc Number: I-fi1RlJ'y_t'i_(i 441 AL Faer'U1; 525 04114

Lab Report
PRISM
' LA6pRATORlEB, INC
Ilf 'Y
=i .II ,r, rvx:c Analytir.:d R f-nvuunnnndAl ;ihlutlML:
117102
Page 7 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Ms. Judy Wilcox
Customer Sample ID: STALIME 7
P.O. Box 1 111
Prism Sample ID: AC03096
Statesville, NC 28587
Login Group: WM45G8
Sample Collection Date/Time: 4/2101
11:40
Lab Submittal Date/Time: 4/2/01
13.15
The following analytical 'esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPOHTING METHOD
DATE/TIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
62 % DRY WT. 0.01 SM 2540 G
413/01 22:00 JLW
FECAL COLIFORM. SOLID
Less than colonies/gram 3.0 SM 0221 E
4/2/01 15:30 MILD
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry sAids".
NOTE: This report is; I revision and supersedes our original laboratory report dated 4110101.
Angela D, Overcasts, V.P. Laboratory Services
llcativn No. 432 - SC Certification No. 59012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
CIT - J
4•0 Shrinf;bri K,k Rood �& P.O. Ifnz L•Lli 1'i (-harlouw \X
VI )fw ii14/.S_'"�-rr:Nil 1,11 tier Nrumbrl: 1 svul: ,7�1-7iih$ I .rz 7(i4: ��?1_il•Ilf f

Lab Report
�: PRISM�ASORATOR169, INC.
a1 � u.
fall Serw-? Analyllcal & Enwonmsnlal .So4nior.;:
1/7/02 Page 8 of 9
City of Statesville Customer Project ID: StaLime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME
P.O. Box 1111 Prism Sample ID: AC03097
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2/01 11:40
Lab Submittal Date/Time: 412/01 13:15
The following analytical -esults have been obtained for the indicated sample which was submllted to this laboratory
TEST
TEST
REPORTING
METHOD
DATEITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
AMMONIA AS N
260
mg/kg
90
4500-NH;12
419/01 17:15
KAP
M0LY90ENUM, TOTAL
2.7
mg/kg
1.0
6010
4e4101 20:53
PRF
NITRATE
Less than
mg/kg
16
EPA 300
4/3101 04:38
TAR
NITRITE
28
mg/kg
20
EPA 300
4/3/01 04-.36
TAR
TOTAL KJELDAHt, NITROCI N IN SOIL
2200
mg/kg
5.0
EPA 351 2
4/6/01 21:17
LNE
TOTAL PHOSPHORUS
21
mg/kg
4.0
EPA 365.2
414101 12:15
MBS
PLANT AVAILABLE NITROG =N
1.5
lb PANlton
0.05
NC Dept. Ag.
4110101 18A S
TAR
CALCULATIONS BASED ON DRY WT.
62
No DRY WT,
0.01
SM 2540 G
4/3101 22:00
JLW
TOTAL PHOSPHORUS DIGI STION
Completed
SM 4500-P D
04/01 00:05
MBS
AMMONIA DISTILLATION
Completed
SM4500-NH35
4/9101 16:00
KAP
TKN DIGESTION
Completed
SM4500-Nor9A
4/4101 07:55
MBS
METALS DIGESTION METH )D 3050
Completed
SW846-3050
413101 13:30
LC2
ARSENIC, TOTAL
8.0
my/ky
1.0
SW846-6u1LiG
4/4101 20:53
PRF
CADMIUM, TOTAL
1.8
mg/kg
1.0
SIN846.60105
414/01 20:53
PRF
COPPER. TOTAL
40
mg/kg
2.0
SW846.6010B
4/4i01 20:53
PRF
ALUMINUM. TOTAL
350
mg/kg
4.0
8W845-6it10H
415101 21;05
PRF
LEAD, TOTAL
95
mg/kg
1.0
SW846.60106
4/4/01 20-53
PRF
NICKEL. TOTAL_
18
mg/kg
1.0
SW846-60100
4/4101 20:53
PRF
ZINC. TOTAL
56
mg/ky
1.0
SW846-60105
4/4/01 20:53
PRF
SELENIUM, TOTAL
28
mg/kg
0.20
SW646.60108
414/01 20,53
F°RF
CALCIUM. TOTAL
6000
mg/kg
1000
SW846"-6010H
4/5/01 21:05
PRF
MAGNESIUM, TOTAI,
250
mg/kg
100
SW846.60108
415/01 21.05
PRF
SODIUM, TOTAL
53
mg/kg
1.00
SW846-60108
4/5101 21:10
PRF
POTASSIUM. TOTAL
A40
mgtKQ
100
SVd84o-Si ii>F3
115i0 i 21.05
PRF
MERCURY DIGESTION
Completed
5W846-7471
415101 11:50
LC2
MERCURY, TOTAL
0.05
nlg/kg
0.03
SW846-7471
4/5101 19:44
PRF
PH
12.5
pH Units
SW846.9C45C
413/01 10:42
SMG
NC Certification No. 402 - SC Cortification No. 99012 - NC Drinking Water Cert. No. 3* 735 - FL Certification No E87519
+W ',print 0mol, Ia .,.1 & t'l! 13, 2d1l) i 3 t.li.u; ttc. Nc- =n" i-iil i 3
6,364 A lull Frrr t is 1
N% m � •
l t14i-

Lab Report
i Plusim
LABOAA70PmEB, INC,
J;
ruu :��,nu;c °nil�yl�cdl s Emironmenim solulrJn3
1/7/02 Page 9 of 9
City of Statesville Customer Project ID: Ste -Lime
Attn: Ms. Judy Wilcox Customer Sample ID: STALIME
P.O. Box 1111 Prism Sample ID: AC03097
Statesville, NC 28687 Login Group: WM45G8
Sample Collection Date/Time: 4/2/01 1140
Lab Submittal Date/Time: 4/2i01 13:15
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE1rJ1WE
PARAMETER RESULT UNIY.q LIMIT REFERENCE STARTED ANALYST
Sample Comments:
NOTE. pH was analy-, ed out of the established EPA holding time.
Angela D. Overcash, b.P. Laboratory Services
NC Certification No 402 - SC Ccrtlticatlon No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
4.49 ",I',in}t-rook R,mo ® PO. (4px 24Q441 t.11,11!ott;•. Nt ?S'224-054S
+'hi ic: i(J1; �2<t (iiii4 li it frcr ,29 0(i-1 a
191-d

Lab Report
RECEVED.
WATER 01JALITYSECTION
AiN 2 j `,I,-''
T
ftism
LARCRATORMS. INC.
a1
DUI ,A-NWi- Au Slylie.: l
R Grvin:nmm n:d $uh�lk;m,:
1/7/02 Page 1 of 11
City of Statesville Customer Project ID: Sta-Lime 719/01
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME 1
P.O. Box 1 1 11 Prism Sample ID: AC123260
Statesville, NC 28687 Login Group: 18761-19
Sample Collection Dale/Time. 7/9/01 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical 'esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TE$T
PARAMETSk
RESULT
CALCULATIONS BASED ON DRY WT.
75
FECAL COLIFORM. SOLID : MI)221 E
Less than
REPORTING
METHOD
DATE/TIME
UNITS
LIMIT
REFERENCE
STARTED
% DRY WT,
0.01
SM 2540 G
719rb1 1 T:ou
rolonlvstgram
3
Ski 9221 C
71!)101 1e:20
ANALYST
JLW
TAR
NC Certific@hon No. 402 - SC Cert,iication No. 99012 - NC Dr;nk:ng Watar Cert. No. 37735 - FL Cortlfication No. E87519
i47'�hringtrunl: I(/�,iiJ S P.17. Iklt ">•(.•;:+,j �, �.'l�;ttttltic, \(?Zt??7 115,:1
f'lu (w. 7041'52'JI-6364 �& 7;ilf r,Vk: NUM11— I d(4)i ^1N-hits i rilx :OS; i7� (yl; r
G T - -4

Lab Deport
Plusm
LASORATOR)E9, I►IC.
it; mot.
F!m �Crvµ'CAraiyucal a EnvironiTionfal sautinn
1/7/02
Page 2 of 11
City of Statesville
Customer Project ID: Sta-Lime 7001
Attn: Ms, Judy Wilcox
Customer Sample ID: STA LIME 1
P.O. Box 1111
Prism Sample ID: AC12326
Statesville, NC 28687
Login Group: 1876H9
Sample Collection Date/Time: 719/01 10:57
Lab Submittal Date/Time: 719101 14.45
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD DATErrIME
PARAMETER
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
NOTE: Fecal.coliform is
reported in colonies/gram. This Can also be interpreted as "most probable number
per gram of total dry so riids".
NOTE. This report is; i
revision and supersedes our original laboratory report dated 7118101.
Angela D. Overcash. V P. Laboratory Services
NC tCertificalicn No. 402 . SC Certification No 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
44 ,I`,.ngL•r(,ot itr,aki A I .l ). ook 240�41 AL
I'iu tc: iU i r `2V 6'(ie A i,rii mice Numia`r I

Lab Repot
PRIS1Vi
i1 LAaOBATOWS, iWC.
rnn scwic.•
Ar 1y1w d c rnviriwnuiernul S01utiv ,:
1/7/02
Page 3 of 11
City of Statesville
Customer Project ID:
Sta-Lime 719101
Attn: Ms. Judy Wilcox
Customer Sample ID:
STA LIME 2
P.O. Box 1111
Prism Sample ID:
AC12327
Statesville, NC 28687
Login Group:
18761-19
Sample Collection Date/Time:
7/9101
10:57
Lab Submittal DatelTime;
719/01
14-45
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
UATEiii iME
PARAMETER
RESULT
UNITS LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY 1NT.
75
% DRY WT, 0.01
SM 2540 11
719/01 17!00 JLW
FECAL COLIFORM, S01-1U : M9221E
Less than
colonies!gram 3
SM 9221 E
7!9101 1£t25 TAR
Sample Comments:
NOTE; Fecal conform is reported in colonies/gram.
This can also be interpreted as "most probable number
per gram of total dry so Ilids11.
NOTE: This report is : i revision and supersedes our original laboratory report dated 7118101.
Angela D. Overcash, VP. Laboratory Services
NC Certification No. 402 - SC CertiLcatior) No. 99012 - NC Drinking Wator Cert No 37735 - FL Cert,ficaoc, No E87519
Yav i{,rn,ct+•p,.i. i{��,!:! .a It, N„_ i.;�'±I't a (I,ss;rt•. "L � __ _,
AL Tull hrv� .VuinfK r: ! tii)O/j�9.(,:(,.i i Fdn 703rj=',-(1•II1t`
Z Z d 7 T = C2 T 7/l- / /1-11D1-

Lab Report PRISE
LABORATORIES, INC.
�tit Servica An llyttCdl 8'enoironmamai SDiOtlOtfS
1/7102
Page 4 of 11
City of Statesville
Customer Project ID:
Sta-Lime 7/9101
Attn: Ms. Judy Wilcox
Customer Sample ID:
STA LIME 3
P.O. Box 1111
Prism Sample ID:
AC12328
Statesville, NC 28687
Login Group:
1876H9
Sample Collection Date/Time:
7/9/01 10-57
Lab Submittal Date/Time:
7/9/01 14.45
The following analytical -esults have been obtained for the Indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD uATETIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS BASED ON DRY WT. 75 % DRY WT. 0.01 SM 2540 G 719101 17:00 JLW
FECAL COLIF0KM, ',;0UI14 M9221 E Less than colonies/gram 3 Sul 9221 F. 71S,01 I&M TAR
Sample Comments:
NOTE: Fecal caliform Is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry si ilids'.
NOTE: This report is ; I revision and supersedes our original laboratory report dated 7/18101.
Angela D. Overcash, \v.P, Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
f'hl n< 'tGIiS?9-5j(i4 lilll F-oov Nu-nln•r: 1-.400'5294i to AL 1•'.lx 704/:-Q6,-q•1I"-

Lab Report
-� PRISM
LABONATOMES, M_
"•,III h2IW:
A-Mlyfical k Solwmni
117/02
Page 5 of 11
City of Statesville
Customer Project le:
Sta•Lime 7/9101
Alin. Ms. Judy Wilcox
Customer Sample ID:
STA LIME d
P-O. t30x 1111
Prism Sample ID:
AC12329
Statesville, NC 26687
Login Group:
18761-19
Sample Collection Date/Time:
7/9/01
10:57
Lab Submittal Date/Time:
7/9/01
14:45
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE sTARTED ANALYST
CALCULATIONS BASED ON DRY WT. 75 % DRY WT. 0.01 SM 2540 Ci 7/9101 17:00 JLW
FECAL COLIFORM, SOLID t M9221E Less Man colonies/gram 3 SM 9221 [ 7r9l01 16:35 TAR
Sample Comments:
NOTE: Fecal colifor111 is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry s1-lids".
NOTE: This report is ; revision and supersedes our original laboratory report dated 7/18/01
Angela D. Overcash, V .P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC unnking Water Cen. No. 37735 - FL Certification Na. E8751g
4,19 Sprinhhmi)k lNtiiKl A P.t'). 240;4^ f.h,l.iliiuc.
19a r,c: 7114r::JU-t fi4 a -loll Frcc Number: I •;�(1(l;'�_>9-f(it 1ALfan "U4(i'_::I-f)4n•
Ez�d 7T:4:1T 7n—/n-Uer'

Lab Report
PRISM
.
LAROPAYp/1rE8, INC.
;li
,
Environmental Sclulions
117102
Page 6 of 11
City of Statesville
Customer Project ID:
Sta-Lime 7/9101
Attn. Ms. Judy Wilcox
Customer Sample ID:
STA LIME 5
P.O. Box 1111
Prism Sample ID:
AC12330
Statesville, NC 28687
Login Group:
1876H9
Sample Collection Date/Time:
7/9/01
10:57
Lab Submittal Date/Time:
7/9/01
14:45
The following analytical -esults have been obtained for the indicated sample which was submitted to This laboratory
TEST
PARAMETER
TEST REPORTING
RESULT
METHOD
DATE/TIME
UNITS LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS ©ABED ON 0KY WT.
65 n /a DRY WT. 0.01
SM 2540 G
719101 17:00 JLW
FECAL COLIFORM, SOLID c M9221E
Less than Cutanieslgrarn 4
SM 9221 E
OU101 1514G TAR
Sample Comments:
NOTE, Fecal coliform is reported in Colonies/gram. This can also be interpreted as "mosl
probable number
per gram of total dry $t Aids",
NOTE: This report is i i revision and supersedes our original laboratory report dated 7/18/01
Angela D. Overcash, v.P. Laboratory Services
NC COrtiflCation ^:o 402 - SC Cortificat,un No. 99012 - NO Drinking Water Cart. No. 377:95 - FL Certific:atlon No. E87519
x,m,i rA r i 1 It,
li,i(FrveNulflhi'r: I2i;q!/S'ltii! I Fnx.7(?4'�)�.IU1(YI
bZ"d

Lab Report
PRISM
rl LA®OpATOMES, INC,
DWI &erwt.v A,lAlyhriil R r:,v«,Hu"cn,pl $c'It,Mors
1/7/02
Page 7 of 11
City of Statesville
Customer Project ID: Sta-Lime 7/9101
Attn: Ms. Judy Wilcox
Customer Sample ID: STA LIME 6
P.O. Box 1111
Prism Sample ID: AC12331
Statesville, NC 28687
Login Group: 18761-19
Sample Collection DatelTime: 719/01
10:57
Lab Submittal Date/Time: 719101
14.45
The following analytical °esulis have been obtained for the indicated sample which was submitted
to this laboratory
TEST
PARAMETER
TEST REPORTING METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED
ANALYST
CALCULATIONS BASED ON DRY WT.
63 % DRY WT. 0.01 SM 7540 G
719101 17:00 JLW
FECAL COLIFORM, SOLID ; M9221E
3 colonies/gram 3 SM 9221 [
71W(11 16:45 TAR
Sample Comments:
NOTE: Fecal coliforrn is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry st dids".
NOTE: This report is i revision and supersedes our original laboratory report dated 7/18/01-
1-7
Angela D. Overcash, V P. Laboratory Services
NC Certlk2flon :No, 402 • SC Certification No. 99012 - NO ur;nking Water Cert. No. 3773.5 - FL Certification No. E87519
441I Spru1g,brYx,k hp;kt O t'.t ). I{VR 3dll:i•i i LIl;victtu', INC 7+!14-0:, }:1
('f,ra �,:: 704/�2'1-hlfr{ a'Inll Fi,,. Nwrnher' (- i17ii Spy h364 J I -a, 7W J i'S-Q409
5Z -d —_

Lab Report
PRISM
°#S tweoaaToruee, rHc.
F,dr SrrvwC- AOaYtc&i 6 tnv)rOnrnenIhI SAIutiUnr:
1/7/02 Page 8 of 11
City of Statesville
Customer Project ID:
Sta-Lime 7/9101
Attn.- Ms. Judy Wilcox
Customer Sample ID:
STA LIME 7
P.O. Box 1111
Prism Sample ID:
AC12332
Statesville, NC 28B87
Login (3roup:
18761-19
Sample Collection Date/Time:
719101 10:57
Lab Submittal Date/Time,
7i9/01 14:45
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
REPORTING
MET-HOr)
DATEMME
RESULT UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
66 % DRY WT.
0.01
SM 2540 (1
7/9101 1%:00 JLW
FECAL COLIFORM. SOLID M9221E
Less than Colonies/gram
4
SM 9221 E
719101 tG:50 TAR
Sample Comments.
NOTE: Fecal coliform is reported in colonies/gram, This can also be interpreted as "most
probable number
per gram of total dry s(-lids".
NOTE: This report is t revision and supersedes our original laboratory report dated 7118101.
Angela D. Overcash, V P. Laboratory Services
NC Certification No. 402 - SC Certification No. gW.12 - `i= ^z,rG'-Na:er Cert. No. 37735 - FL Certification No. E87519
(d4r ti nrrti�ri, }, F Rnad T Ilk), Ism . rU;g3 (Ir,iciuttr N(' 2t 224-05.i-(
.. 1';«rc. 7(;$/,r,�u(„h„ Tnli F,t'c ti'u mh,r• l Slp7/124-h'c64 A Pax- 704/52l-t1 i(N
9Z-d r

Lab Report
A PRISM
LAOQRATGRIM tke
Pull Sotvire Anaylical es Enwronmenial Sotusone
1/7102
Page 9 of 11
City of Statesville
Customer Project ID: Sta-Lime 719/01
Attn: Ms. Judy Wilcox
Customer Sample ID- STA LIME
P.O. Box 1111
Prlsm Sample ID: AC12333
Statesville, NC 28687
Login Group: 18761-19
Sample Collection Date/Time: 7/9/01 10:57
Let) Submittal Date(Time: 7/9/01 14:45
The following analytical 'esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD UATEITIME
PARAMETER
RESULT UNITS LIMIT REFERENCE STARTED ANALYST
SALMONELLA Lass than
CALCULATIONS BASED OK DRY WT, 61
Sample Comments:
Angela D. Overcash, \ .P. Laboratory Services
MPN/4g
13
503 SLUDGE
7/SIIGI 16:00
TAR
%DRY WT.
0.01
SM 75401.3.
71ti101 16:30
1LW
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert. No.. 37735 - FL Certification No. E87519
#44 tih1'Inj'hrP1 6. Itu,!I A v(.). Ht-N 240-+F; �1 �Il.ii it ttc n t 'k
Hit no: Tull fnx Nwnl><e: I-h(Hlyi:9.6364 A F,m 701, 25 ;14o,
LZ'd c-T -ar

Lab Report PRISM
LADDRATO ea. ale.
hull S;f-lvu;v A,.Aylii;:d R Cirvimm�icu6il S,ihue)ns
117/02 Page 10 of 11
City of Statesville Customer Project ID: Sta-Lime 719/01
Attn. Ms. Judy Wilcox Customer Sample ID: STA LIME
P.O. Box 1 1 1 1 Prism Sample ID: AC12334
Statesville, NC 28687 Login Group: 18761­19
Sample Collection Date/Time- 7/9101 10:57
Lab Submittal Date/Time: 7/9/01 14:45
The following analytical •esults have been obtained for the indicated sample Which waS submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
S`lARTEn
ANALYST
AMMONIA AS N
420
mg/kg
79
4500-NH3E
7/11101 14:15
MBS
MOLYBDENUM. TOTAL
3.6
mg/kg
1.0
6010
7/17/01 11:47
MSC
NITRATE
Less than
mglkg
16
EPA 300
1111/01 12:24
TAR
NITRITE
Less than
mgAg
16
EPA 300
7111/01 12:24
TAR
TOTAL KJELDAHL NITROGI N IN SOIL
6600
mg/ky
05
EPA 351-2
7/11/01 17:11
EHT
TOTAL PHOSPHORUS
52
mg/kg
10
EPA 365.2
7110101 13:35
MBS
PLANT AVAILABLE NITROG =N
41
Ib PANlion
0.05
NC Dept. Ag.
7116101 13:56
JAS
CALCULATIONS BASED ON DRY WT.
63
% DRY WT.
0.01
SM 2540 0
//9101 17 00
Jt.W
TOTAL PHOSPHORUS DIGS STION
Completed
SM 4500-P H
711ot01 10:20
MBS
AMMONIA DISTILLATION
Completed
SM4500-NH3B
r711/01 12:05
MBS
TKN DIGESTION
Completed
SM4500 Nory8
7/10/01 07:20
MBS
METALS DIGESTION METHOD 3050
Completed
SW846-3050
7110101 12:45
LC2
ARSENIC, TOTAL
12
mglkg
1.0
SW846-6C106
7!17101 11:47
MSG
CADMIUM. TOTAL
Less than
mg/kg
1.0
SW846.60108
7!1 7/01 11:47
MSC
COPPER, TOTAL
68
mglkg
2.0
5W846-6010B
/! 17/01 11:d7
MSC
ALUMINUM, TOTAL
16000
mglkg
100
SW846-6010B
7117i01 12:01
MSC
LEAD.TOTAL
29
mg/kg
t,o
SW646-6C106
7117101 11.47
MSC
NICKEL, TOTAL
15
mglkg
1.0
SW846-60102
7117101 11:47
MSC
ZINC, TOTAL
69
mg/kg
1.0
SW846-60100
7117/0111A7
MSC
SELENIUM, TOTAL
23
mg/kg
2.0
SW846-GDIOB
7/17/01 11:47
MSC
CALCIUM, TOTAL
320000
mg/kg
10000
SW846-60to6
7117101 12:25
MSC
MAGNESIUM. TOTAL
12000
mg/kg
100
SW846-601oH
7117/01 12:01
MSC
SODIUM, TOTAL
1500
mglkg
20
SW846-60108
It17;01 11:57
MSC
POTASSIUM, TOTAL
15000
mg/kg
100
S'.':846-60108
%: 17 01 12:01
MSC
MERCURY DIGESTION
Completed
SW846-7471
7112101 12:30
LC2
MERCURY, TOTAL
0.04
mg/kg
0.03
SW846-7471
7/13101 1312
PRF
PH
12.0
pH Units
SW846-9045C
7/10i0I 14-35
SMG
NC Certification No. 402 - SC CerO!Calmn No. 990 12 - INC Drn,<<ng ;,rater ;ert No, 37735 - FL Certification No. E87519
44a Sprnyb(owl, Roil) ® (,.CI Eua 24t1,;,1 A::horinttd, %C 2h224-;I,z I i
I'tt, Ili•. i0ai7ti�r".{-h:+t�a T,41 I;n'C Nt; idwr. I•xx.'{)! _9.6,1,; Ah, I•,1,; ii)yi•�_,-f)iU

Lab Report t:a PRISM
J- LABORATORIE6, INC.
Full tier.:: Avaly!i1:al R C-i....Snhnwmz
1 /7/02 Page 11 of 11
City of Statesville Customer Project ID: Sta-Lime 7/9/01
Attn: Ms. Judy Wilcox Customer Sample ID: STA LIME
P.O. Box 1111 Prism Sample ID: AC12334
Statesville, NC 28687 Login Group: 1876H9
Sample Collection Date/Time: 7/9101 10:57
Lab Submittal Dateffime: 7/9101 14:45
The following analytical esuits have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATEMME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED
Sample Comments:
NOTE: pH was analy, ed out of the established EPA holding time.
Angela D. Overcash, 1, .P. Laboratory Services
ANALYST
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
y4`?tilnn!�iruuk !tna,1 A PO Nix 2-10,_-Q A+"!
Tiff Froe Nunibcr: 1-M M1/a2y 614i4 ® F,i\.
6Z"d +,T=oT :7n-in-uvrr

Lab Report
PRISM
LASOA&TOftS, ttiC.
II
Pull SerV Cr A!1AlyI%'t! A Ctwtfuf nx'ntill Sclutions
1/7f02 Page 1 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smi111 Customer Sample ID: STA-LIME
P.O. Box 1111 Prism Sample ID: AC21938
Statesville, NC 28687 Login Group: WM05HB
Sample Collection Date/Time: 1012/01 11:00
Lab Submittal Date/Time: 1012101 14-40
The following analyticaf •esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
AMMONIA AS N
MOLYBD6NuM,TOTAL
NITRATE
NITRITE
TOTAL KJELDAHL NITROQE N IN SOIL
TOTAL PHOSPHORUS
PLANT AVAILAGLE NITROG :N
TOTAL RESIDUE
CALCULATIONS BASED ON DRY WT.
TOTAL PHOSPHORUS DICE 3TION
AMMONIA DISTILLATION
TKN DIGESTION
METALS DIGESTION METH( D 3050
ARSENIC. TOTAL
CADMIUM, TOTAL
COPPER.TOTAL
LEAD,TOTAL
NICKEL. TOTAL
ZINC. TOTAL
SELENIUM, TOTAL
SODIUM, TOTAL
POTASSIUM. TOTAL
MERCURY DIGESTION
MERCURY, TOTAL
TEST REPORTIN(; METHOD
RESULT UNITS LIMIT REFERENCE
DATE/TIME
STARTED ANALYST
190
4500-NH3E
10/10/0115:35
3.8
6010
10/5101 13:07
Less than
EPA 300
1019101 00•56
6.8
EPA 300
1019/01 00:56
79000
EPA 351.2
10/4/01 20 29
19
EPA 365.2
1013101 13:45
47.5
NC Dopt. Ay.
10/10/01 15.3o
750000
Ski 2540 8
1014101 19 00
74 ,
SM 2540 G
1013/01 17:30
Completed
SM 4500-P B
10/3/01 08:25
Completed
SM4500-NH38
10/ 10101 14:10
Completed
SM4500-Norg8
1013/01 08:00
Completed
S W 846-3050
1013i01 11-30
10
SW846-6010D
1015r0113:07
1.4
SW846-601013
1015101 13:07
53
6W846-60108
10/5/01 13:07
73
SW846-60 109
1015/01 13:07
13
SW846.6010G
101si0113,07
52
SW846-6010B
10/510113:07
39
SW846-6010f3
10/5/01 13 07
1300
S W 846.601013
1015/01 13:30
22000
SW 846-60108
1 015i01 13-26
ComN(Qled
SW846-747 t
1015101 71-00
029
SW846-7471
10/5/01 17-27
mg/kg
mg/kg
mg/kg
mg/kg
my/kg
mgtkg
Ib PAN/ton
°!A DRY WT,
mglky
mg/kg
mg/kg
mgikg
mg/kg
mg/kg
mg/kg
mg/kg
rngs4tg
my/kg
3.4
1.0
fi.8
6.8
51GOD
3.0
0.05
500
0.01
1.0
1.0
20
1.0
}.0
1.0
2.0
20
1000
0.02
MEIS
Msc
TAR
TAR
EHT
MBS
TAR
EHT
JLW
MBS
MEiS
MBS
LC2
MSC
MSC
MSC
MSC
Msc
MSC
MSC
MSC
MSG
LC2
TAR
NC Certification No. 402 - ;C Ciartificalion No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certlt+ral,r`n Nh PA7519
11`) ilirin}.l,i n0F\ j7,-,1 2_4t;`4-
- t-hen c. /li4/axJ fi.t(,•i AL Tcl(f Fivc Numl`t`r: I M;H)i:i_y i�l(r1 IL f:.i)(- 71)J=2�-R1f:u

Lab Report PRISM
LANORAWRIES, WC.
III
Arcdylical tl ;Fnvimnmental Solullon6
1/7/02
Page 2 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID: STA-LIME
P.O. Box 1111
Prism Semple ID: AC21938
Statesville, NC 28667
Login Group: WM05HB
Sample Collection Date/Time: 10/2101
11.00
Lab Submittal Date/Time: 10/2101
14.40
The following analytical
-esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST REPORTING METHOD
pATE/TIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTEO ANALYST
Sample Comments:
Angela D Overcash. V P. Laboratory Services
NC CortlfiCatien No 402 - C Certification NO. 9y012 - NC uriltking Water Cert. No- 37735 - FL Certification No. E87519
119 }F,ru�t`t' in i. Q,41,j Ak I'.(Y h— 2.u?14 c 4L I_l .,,!,nlciI-
� yi
!'lu;.rt•.:;ll;$�4•A:lGi L► T,;ii Pil'u NUnihp,'. 1 M%1!/'i7V 611rI G f':U:'iil=UJ�S if411'I
I d br:PT 2n-in-uer

Lab Report
PRISM
ueor+ATOEt", wc.
�NI Suet".,.. AoAlyw;il N Eilvlrmmyrn4d :,nLrlinnv;
1/7/02 Page 3 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr Andy Smith Customer Sample ID: STA-LIME1
P.O. Box 1111 Prism Sample ID: AC21939
Statesville, NC 28687 Login Group: WM051-18
Sample Collection Date/Time: 1012101 11:00
Lab Submittal Date/Time: 10/2/01 14:40
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
CALCULATIONS BASED ON DRY WT. 64 % DRY WT. 0.01 5M 2540 G 1013101 17:30 JLW
FECAL COLIFORM, SOLID : M9221E Less than colonieslgram 4.0 SM 9221 E t012101 15AS MLD
Sample Comments:
NOTE: Fecal col iform is reported in colonies/gram. This can also be interpreted as "most probable number
per gram of total dry st Aids".
NOTE: This report is; revision and supersedes our original laboratory report dated 10111/01.
Angela D. Overeash, V P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 • NC Dnnkinq Water Cert. No. 37735 - F_ Certification No. Ea7519
14", ;trrn y;i7r.,rd: Ro.m A 1,) tfnr ' 0541 A
I'llrr a :(4i S�r�_;,3i i l 'iiifl F'ccc :\uml?i c ! !qU:' 29 ti ;(i-i A ,71)4
ZG d

Lab Report
PRISM
' � LAlOrIASOp1E5, 1MC.
I}1
Full .`;eni..c Malylir.:d R fuvirunnrt,nr�J K}I�giptl,
1 /7/02
Page 4 of 9
City of Statesville
Customer Project ID: Sta-Lime
Attn Mr. Andy Smith
Customer Sample ID: STA•LIME2
P.O. Box 1111
Prism Sample ID: AC21940
Login Group: WM05H8
Statesville, NC 28687
Sample Collection Date/Tirne: 10/2/01
11:00
Lab Submittal Date/Time: 10/2/01
14:40
The following analytical 'esulls have been obtained for the indicated sample which was submitted
to this laboratory
TEST
TEST REPORTING METHOD
DATErrIME
PARAMETER
RESULT UNITS LIMIT REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON nRY WT.
68 % DRY WT. 0.01 SM 2540 G
10/3101 17:30 JLW
FECAL COLIFORM, SOLID : M9221E
Less than coloniesfgram 4.0 SM 9221 E
1012}01 1&4S MLD
Sample Comments:
NOTE: Fecal cofiform is reported in colonies/gram. This can also be interpreted as "most provable number
per gram of total dry solids",
NOTE: This report Is ; revision and supersedes our original laboratory report dated 10111101.
Angela D. Overcash, V P. Laboratory Services
NC Certification No. 41,12 • SC Ce. Ufication No. 99012 - NC Drinking Water Cort. No. 37735 - FL Certification No. E87519
a1•i �hr�n••irr�„•k !�iaa! e I'.(1 a �ytr� t;
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RECEWED
Lab Report VMTER QUALITY SEC11ON
FJX,3 2 ''U ' .' PRISM
.
LABORATORIES, INC.
woolp9���p
- hallo POM It tihZbii:ie AnaIyGCB K t+lwrunnlEnt51 SJIUBo i l
117102 Page 5 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith Customer Sample ID: STA-LIME3
P.O. Box 1111 Prism Sample ID: AC21941
Statesville, NC 28687 Login Group: WMO5H8
Sample Collection Date/Time: 10/2101 11:00
Lab Submittal Date/Time: 1012101 14.40
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
L3ATE�1IMF_
PARAMETER.
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED (Ih DRY WT,
80
% DRY WT.
0.01
SM 2540 Q
1013101 17:30 JLW
FECAL COLIFOHM. Sk)LID < M9221 E
Less than
cotonif.-Clgram
3 ❑
SM 9221 F.
1012101 15:45 MLD
Sample Comments:
NOTE' Fecal coliforlil is reported in colonies/gram. This Can also be interpreted as "most probable number
per gram of total dry s(,lidS".
NOTE; This report is. i revision and supersedes our original laboratory report dated 10/11 /01.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Wator Cert. No. 37735 - FL Certification No E8751g
447 5 >+K,+ i ri, �. I�ilir, .'�i• _5_'_ i-II ,;j
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b£ d

Lab Report
1 /7102
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PRISM
ri+tl ti:rvK;c On, IY1ic;J
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Page 6 of 9
City of Statesville Customer Project ID: Sta-Lime
Attn: Mr. Andy Smith Customer Sample ID: STA-LIME4
P.O. Box 1111 Prism Sample ID: AC21942
Statesville, NC 28687 Login Group: WMO5H8
Sample Collection Date/Time: 10/2101 11:00
Lab Submittal bate/Time: 10/2101 14:40
The following analytical esults have been obtained For the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON ❑RY WT.
78
% DRY WT.
0.01
SM 2540 G
1013101 17:30 JLW
FECAL COLIFORM, SOLID' M9221 E
Less than
colonies/gram
3.0
SM 9221 1_
1012J01 16:30 MILD
Sample Comments:
NOTE: Fecal coliform is reported in colonies/gram.
This can also
be interpreted
as "most probable number
per gram of total dry s1 Aids".
NOTE: This report is , I revision and supersedes our original laboratory report dated 10/11101.
Angela 0, Overcash, % .P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certd,cation No. E87519
119Spruigbrook Noad AL RO. Box 741.1 ;43 A, l h irlotte. NC 29224-11 i I i
Vh, no. 7(1:1;:i2y ti;Ni4 Bill I rcc Number: 1•i;00i529.6.4,11 AkF,,,. 7114; ;= , 0-101,
9£-d 9I=91 ZO—LO—URC`

Lab Report
PRISM
u11110RATORIES. INC.
:ta
I
%,uu `le,Ylce!
A118"Cat 5 trnrtrontnentai 9ottmona
1/7/02
Page 9 of 9
City of Statesville
Customer Project ID:
Sta-Lime
Attn: Mr. Andy Smith
Customer Sample ID:
STA-LIME?
P 0. Box 1111
Prism Sample ID:
AC21945
Statesville, NC 28687
Login Group:
W M05H8
Sample Collection Date/Time.
10/2/01
11:00
Lab Submittal Date/Time:
10/2/01
14:40
The following analytical -esults have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT UNITS
LIMIT
REFERENCE
STARTED ANALYST
CALCULATIONS BASED ON DRY WT.
73 % DRY WT.
0.01
SM 2540 <;
10/3101 17.30 JLW
FECAL COLIFORM, SOLID S M9221 E
Less than colonies/dram
3.0
SM 9221 E
1012/41 15155 MLD
Sample Comments:
NOTE: Fecal coliforiTI is reported in colonies/gram. This can also
be interpreted
as "most probable number
per gram of total dry s( lids".
NOTE: This report is, revision and supersedes our original laboratory report dated 10/11101.
Angela D. Overcash, V P. Laboratory Services
NC Certification No 402 - 3C Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
Ro.1,1 i [i0 ISn, _40:i 4t ,t\ t_j.l„ttc, \tr 'ti?_.i•O;yZ
I'Itn is 704/.594,3h4l L Ittll Frt't• Nu,7tt-e- 'I-�(HI' :�q_h:li.1 1it t•i /52; 0-;n,t
19E-d -- QT:PT ;70-LO-L(QC'

NARRATIVE

City of Statesville
Fourth Creek WWrP
January7. 2002
Theresa Nartea, Sal Scientist
Non- Permitting Unit
1617 Mail Service Center
Raleigh NC 27699-1617
Subject: Permit No. WQ0006245
City of Statesville
Distribution of Residual Solids Class A
Additional Information Request
Iredell County
Dear Theresa:
I have gathered the information that you requested concerning the materials handling. The following is
a brief narrative of Application Item VI. 1. a-g.
A. Residuals from the 3m Creek facility are produced from a belt press. It is loaded onto a dump truck
and then transported to the a Creek WWTP. At this point it will be dumped into covered hoppers
and sent through the N-Viro process or dumped on a % acre concrete pad. This sludge will then be
used for contracted land application.
The residuals from the water plant are produced through a large plate and frame press. It is then
transported to the 0 Creek VVVVTP and dumped into a hopper to be sent through the N-Viro
process. This sludge does not go to any land application.
The 4"' Creek residuals are pumped from the aerobic digester to the belt thickener via pumps and
underground piping. It is then sent through the plate and frame press and dumped into its
designated hopper for the N-Viro process or to be sent down to the pad for the land application
program.
B. The residuals at 3`d Creek and 4t' Creek will be held in an aerobic digester until the next phase. The
water plant has holding cells that the plate and frame press pull from.
C. The a Creek facility has drains at various points of the N-Viro system and they feed into the
headwork's of the VVVTP. The pad itself has berms and walls surrounding it to keep any wash off
from escaping.
D. The duration of treatment can be from 7 to 10 days depending on what facility the residuals is
coming from, the weather conditions and other unforeseen problems.
E. The N-V ro process at the 4t' Creek facility has % acre concrete pad where the final processes take
place such as mixing and aerating the product to get to the final product, which is Sta-Lime.
F. The final product will be stored on average for about 2 weeks.

• Page 2
January 7, 20002
G. After all of the lab results have come in and are within the permit limits we give it to farmers and
private haulers. Per there discretion, they apply as needed. The e Creek WWTP loads the Sta-
Lime by using a large rubber tire loader.
If you need more information, please contact me at 704-878-3438.
Sincere y,
(
Andy Smith
Residuals Supervisor
CC: Joe Hudson
Jerry Byeriy

VECTOR ATTRACTION
REDUCTION
[�71111:1

(CITY OF STATESVILILE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # -f REMOVE FROM BIN 01- - 01
DATE 0 l - o y - 01
Final % Solids 7W, )
TIME/
DATE
I pH
> 12.0 / 3 DAYS
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INITIAL pHor
- - 1
CORRECTED H /
30
INITIAL H j , 3
CORRECTED off 1

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # a REMOVE FROM
BIN
DATE J /O % j
Final % Solids
TIME/
pH
TEMPI C
152DEG.
SAMPLER
DATE
> 12.0 / 3 DAYS
/12HRS.
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0/'/0-o CORRECTED
H J .7
3 il'i INITIAL H Ja? ed
CORRECTED H 7
1�_61 CORRECTED RH /

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # .3
REMOVE FROM
BIN 0 I -ra 1
DATE /A 0 9-01
Final % Solids 79. I
TIME/
pH
TEMP° C
SAMPLER
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> 12.0 / 3 DAYS
52DEG. /12HRS.
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// A „'
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+
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--
WL
CORRECTED pH IQ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # Ll . REMOVE FROM BIN a/- ly-o!
DATE cal ` /! - 1 Final % Solids �'1,3
TIME/
DATE
I pH
> 12.0 / 3 DAYS
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52DEG./12HRS.
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/,2`
/- /•5-001 f8ORRECTED pH
�,

RECEIVE®
WER QUALITYSEG110N
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #
REMOVE FROM
BIN l -%9-01
DATE__ I -/6-pI
Final % Solids 6/ 9 a
TIME/
pH
TEMP° C
152DEG.
SAMPLER
DATE
> 12.0 / 3 DAYS
/12HRS.
INITIAL
-0.39
_INITIAL
pH THicKNER 4/r
$ °
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Corrected H
3: 16 rr,
11-1tr-01—CORRECTED
INITIAL 5,7
pH /a, 7
INITIAL PH
a
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Z5 Awe INITIAL RH 1Z,
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11:3314 M INITIAL PH 4d,36
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INITL L H %W. 0
70 ° '
RCkJ
/ - w- a 1 CORRECTED PH /d .7
oZ2

R
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #_
REMOVE FROM
BIN 61-a5- 01
DATE 0/-d - 0 j
Final % Solids
G
TIME/
DATE
pH
TEMP° C
152DEG.
SAMPLER
> 12.0 / 3 DAYS
/12HRS.
INITIAL
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INITIAL pH /-1, 70
00
�� w
CORRECTED pH J- 90
INITIAL pH 14,(�
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63 '
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CORRECTED pH Id .7
'04 ry
3.3 P,' INITIAL pH 12,6
� Y
/-3 -01 CORRECTED pH

(CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN ## REMOVE FROM BIN
DATE / /,2I Final % Solids '
TIME/
DATE
PH
TEMPO C
152DEG.
SAMPLER
> 12.0 / 3 DAYS
/12HRS.
INITIAL
2. 0? M
n8i
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0 4- 2 b- o l
Corrected pH /3
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8 � ®
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3: 30PM
9, 135
INITIAL H Ia,
'70
I - a9 - o I
CORRECTED pH /�, ��

ICITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 7 REMOVE FROM BIN 0 /-4Z-0 J
DATE_ 0 /-07.3 -©/ Final % Solids k3 t?
TIME/
DATE
PH
TEMP° C
152DEG.
SAMPLER
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/12HRS.
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n--
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CORRECTED pH / _ q
9.30A M
o. i6 5
INITIAL pH /a?, 4e
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/-.�4-01
CORRECTED pH

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
'PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # S' REMOVE FROM BIN I --t7-o1
DATE / --? `/ -O
Final % Solids. f77 3
TIME/
DATE
I pH
TEMP° C
SAMPLER
> 12.0 / 3 DAYS
52DEG. /12HRS.
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6
2 6- o
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0
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CORRECTED pH-,JA
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'CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # c? REMOVE FROM BINya -Ood -0 J
DATE O l -30 - 0) Final % Solids
TIME/
PH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
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INITIAL H
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on I INITIAL pH -R,
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a 0 / ICORRECTED DH > > CZ C;

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # Vi REMOVE FROM BIN d
DATE 1 1 O Final % Solids
TIME/
DATE
pH
> 12.01 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
r—
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a
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a
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INITIAL pH jjqi
g o o
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CORRECTED pH ,6J
INITIAL pH
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CORRECTED pH 1 Z 3

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # _ REMOVE FROM BIN , p
DATE__ Final % Solids 7E. q
TIME/ pH TEMP° C SAMPLER
DATE > 12.0 / 3 DAYS 152DEG. /12HRS. INITIAL
c 55
INITIAL H Tr ricKrvER
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INITIAL p H / ,
7Q
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ICORRECTED
pH 1.2.79

ICITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN Z
DATE 2 I Z j t� , Final % Solids Z3-
TIME/ I pH
DATE > 12.0 / 3 DAYS
P� INITIAL H THICKNER ,
Corrected PH „ .3
INITIAL pH 12.5
c� CORRECTED H ! 71 ,
INITIAL pH
CORRECTED pH -:?
INITIAL PH r `J
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{ ' ' M INITIAL pH
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INITIAL H IZ;70
CORRECTED pH
INITIAL PH
a S-� CORRECTED pH
TEMP" C
52DEG. /12HRS.
. o -
�4
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S
SAMPLER
INITIAL
I

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN
DATE2Rj Final % Solids _ (r
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
us
a
b
INITIAL p H THICKNER
10
5-1 n
Corrected pH ,
la /D Pm
INITIAL pH la. 61
d- 16-01
CORRECTED H 13 .3
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INITIAL PH %
7�
CORRECTED pH a, G 3
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CORRECTED pH -.5
INITIAL pH %
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-a,/
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- Z
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2-4-01
CORRECTED H '
4f"
INITIAL pH ; ,'(, ,
6 70
D1
CORRECTED pH !Z •,q7

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN
REMOVE FROM
BIN a b
DATE_ �2�1y f
Final % Solids .5J7,3
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
-.5l
INITIAL H' THicKNER �,
D
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Corrected pH
l9? , 30
INITIAL pH / a •
a- a -0
CORRECTED PH 13, 3 9
9` :
INITIAL H ,).5 7
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rim INITIAL pH 1,97.60
-a Ol CORRECTED pH
0 PrA INITIAL pH
YU
-a-0 CORRECTED, pH i Q..,
SOS~ INITIAL pH
2 `zS =o / CORRECTED H 12
+� INITIAL H
�?
a �(� CORRECTED pH �3 3

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # i
REMOVE FROM
BIN 0 1
DATE 3 -- 1- 0 1
Final % Solids
t/, 0, J
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.01 3 DAYS
52DEG. /12HRS.
INITIAL
INITIAL oH THICKNER
Corrected EH
INITIALpH 1 d, y 0
3 - I - 0 ►
CORRECTED pH % , 5 (F
INITIAL pH I a - b
-)- 01 CORRECTED pH
6.04 INITIAL pH /W-
I CORRECTED pH
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3-Z-o CORRECTED. PH /a, S-D
i M'D f --4 INITIAL pH
CORRECTED pH ` t %' i4
INITIAL pH l '' 14
f c
�� I CORRECTED EH l .
'

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
4!
BIN # REMOVE FROM BIN 3 - 1-0 I
DATE - -- 0 / Final % Solids 97,0
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
INITIAL DH THICKNER
Corrected pH
6/?m
INITIAL pH
3 - - 0)
CORRECTED PH
Cl - ; �f M
INITIAL pH 2- 57
,
-D I
CORRECTED pH
:3 ado
INITIAL H Z9. 61
CORRECTED pH
+ , r s-b
INITIAL pH f 2 ,
3 - Z -d
CORRECTED pH (2 , 5 `7
INITIALpH �� =/
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,
CORRECTED H � , �;
I'M
INITIALpH
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CORRECTED pH

IU I Y VF 5TATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #_ REMOVE FROM BIN
DATE Final % Solids ,
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
INITIAL pH THICKNER
Ouj
1 o
Corrected pH
I o 15 A M
INITIAL pH
3- i5- i o
CORRECTED pH /3, 7
INITIAL pHj�—
�'-c? l
CORRECTED pH
INITIAL 2H �d.5"
730
%il GU
3-16-el
CORRECTED pH
INITIAL pH f a
o
CORRECTED pH ,
INITIAL pH
3
CORRECTED pH /9,
G� h
INITIAL pH
a
r r
-fI
CORRECTED pH

CITY OF STATESVILLE
ALKALINE STAEII_17®TION PPnrEcc D=e%nom
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
IBIN
#
REMOVE FROM
BIN J/?�p
DATE3 //�k y
Final % Solids 5
TIME/
pH
TEMP° C
152DEG.
SAMPLER
DATE
> 12.01 3 DAYS
/12HRS.
INITIAL
- .. iq Z
b
© �O 0
INITIAL PH THICKNER t'a , 3
L
3 at
Corrected RH (� ,
•'36 Aoi
INITIAL DH
3 - Y -o 1
CORRECTED EH
-6VAM
INITIAL pH o2• (
p
- H -G l CORRECTED pH
'S o INITIAL pH I Z. S S^
- 0 CORRECTED H 12.
Ani INITIAL pH / , I L7
goo
R4 W
3- jS- o j CORRECTED pH 6
O INITIAL pH
CORRECTED eH �
tP, M INITIAL pH--
/ G CORRECTED vH la ,/ L

RECEIVED
TEF? OUALITY SECTION
JhN 2 ..j '
CITY OF STATESVILLE
Newt! edtog
A I WA I INN Q'rA PF1 17A Tvn1ht nn^^r-e%t .,.-�...
--• — ••.•• ••� •• • �.�,...�r� i iv� ` I1V<sCJJ il�l.lJSiU
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #— REMOVE FROM
BIN 2
DATE
Final % Solids ,
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
-0,®4
INITIAL pH THICKNERn/-, 77
02°
73
Corrected pH d , 68
3 'd o P
INITIAL pH /W
3-/I-ol
CORRECTED PH
INITIAL H 1 �. (D
7S Cd
3 - / -v
CORRECTED pH a, o
3 `o°
INITIAL pH %t
F3
CORRECTED RH
© `b0
INITIAL pH
Le
3L2aol
CORRECTED pH
a,A�S
:2 /7"
INITIAL pH %7, Y3
9;00
- -�o-o
CORRECTED pH !a?,70
7,'y5q
INITIAL pH 14. 3 7
Na e RCW
- l�o
CORRECTED PH la,Sy
m •5y
G a
3-a6- o l
/-Z b

CITY OF STATESVILLE
BI K61 IAIP CTAMII I7AT1nU v0nr%ce0 ccnnpn
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # '7 REMOVE FROM BIN 3 - a a -o 1
DATE 3 - ! 4 -o l Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
3 o P,-)
INITIAL pH THICKNER 6. %
o2 J,
3 -1 4 -o !
Corrected H �,
3�do P,,1
INITIAL pH
00
�LL
3-1 4 -
CORRECTED pH 1a, 7
INITIAL pH
CORRECTED pH
ac �S
INITIAL p IN, r�Lc1
3 -aa -ej
CORRECTED pH Z Q
rU �, -
9
INITIAL pH
0
a0
CORRECTED pH
Pro
o. t6.
INITIAL pH SV
Z�S4 °
;� L' i
3-,,2g-qj
CORRECTED PH /a, 7/
INITIAL pH 34
7 $ °
Ric W
3- a 1- o 1
CORRECTED pH U. d
5 : d,5 P�
/Z 5-3
/d , 61-1
Z-Q o RJ,"./ 0. 10s

CITY OF STATESVIL
Al 1/A/ fair e'—A ►l If r�r+
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
SIN # _ REMOVE FROM BIN
DATE_ 3 /O a /p Final % Solids -9 7,
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
— - t) I
INITIAL oH THICKNER
D
z.= 3o
Corrected pH - g
Prr
INITIAL pH 1W. q6
go"
CORRECTED pH /?, 6 '
INITIALpH a. 7
9L3�
j wL
CORRECTED pH , (,
-2',eZgzh
INITIAL pH
/7j Cj
- 3
CORRECTED gH
.1:
INITIAL pH M. S-3
60 °
lilt in}
3--�3- ol
CORRECTED RH d,70
INITIAL pH lq�. (�
3-
CORRECTED pH ,g
INITIAL pH
CORRECTED H
? rvi
3-ab-01
/a . -
/-�, i

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN 6
DATE_. � Final % Solids �. 6
TIME/
DATE
pH
TEMP° C
152DEG.
SAMPLER
> 12.0 / 3 DAYS
/12HRS.
INITIAL
2 O
INITIAL PH THICKNER (9 .'?
b
3
Corrected PH
o,s?l
5 3AM
INITIAL H N �
.�a °
f� W
CORRECTED PH i3,q3
I
INITIAL H
CORRECTED H 13 : o
Cti.4�
w
3��
INITIAL H /o�• !i
�D°
���
3 `a7
el
CORRECTED PH J3, 1
102: 31 i�..n
o, iso
INITIALpH U.
75
W
-� - ° /
CORRECTED PH /W. �3
o.235
5 pm
I INITIAL OH 1A 1�0
700
3 dt8--d
CORRECTED PH /,f, 17�'
!,::o�4cORRECTED
c,i3 j
NITIAL H I.�,y
70 °
ReCLJ-a
PH 14,,K3

!CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # c REMOVE FROM BIN 3 3
DATE f 73, / Final % Solids�—
TIME/
DATE
pH
> 12.0/ 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
to
`i3(.9
INITIAL PH THICKNER ( ,
C7
)!
a O
Corrected pH ,
.0, [fro
INITIAL pH
k5 Q
3- a8- Q 1
CORRECTED pH /a, 13
/Z
INITIAL DH 12,53
40
�¢
z -
CORRECTED pH IZ.71
//%
INITIAL pH .?,y
—3-.27-ol
CORRECTED pH
�'m
INITIAL H ,'-) 3
'7�'°
R,, W
- 0-df
CORRECTED H /
/
INITIALpH 1a l g l
0
- -D
CORRECTED pH .3
INITIAL pH I L. 6 c)
(a q
80
-
CORRECTED H )Z. �

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #_ REMOVE FROM BIN
DATE 1 t Final % Solids 3,
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
-- 34
INITIAL PH THICKNER
0
is
ail
3 o
Corrected H (, ,
5 Pm
Q, f iro
INITIAL pH -49 ea
3 -d,r- o f
CORRECTED pH /3, O a
2l9M
INITIAL pH
,3
CORRECTED pH
l/: S✓�Ar�
INITIAL pH I.1lle
05 °
3 -a9-0 /
CORRECTED pH /d.
/a pM
INITIAL pH I ;?, K)
77 c
/?4 W
3-30-01
CORRECTED pH la,d
f
02 i! M
INITIAL H 1,9,11
t
3 - 1
CORRECTED pH ,
10 yD
INITIAL pH
>) o
CORRECTED pH /Z, 7r7

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM
BIN '� 6
DATE_ %�� �p 1
Final % Solids-(? 3
TIME/ pH
TEMP° C
SAMPLER
DATE > 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
6 % 10 INITIAL PH THICKNER %
) 3 b
W
3 2cl k) f Corrected EH ,
1
INITIAL pH U. -5
CORRECTED H /� 7o
oo JINITIAL DH
0
3• a g or CORRECTED pH /,T . -76
3'a® 'y' INITIAL pH O .o
A
�CcJ
3 - 3 o -el CORRECTED pH ,
/ d p n INITIAL DH
3-30-01 1CORRECTED pH /a, 6y
INITIAL pH
-4I CORRECTED pH �•
` O INITIAL PH Z,
a
CORRECTED EH , 7

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # y REMOVE FROM BIN 3-.� 9-o a
DATE 2.a - 1 Final % Solids 70, 3
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
3 o
INITIAL pH THICKNER-
c,
�o�' r..
Corrected EH G,
5.'d5P�
o. I4.5
INITIAL H 1-24-5
900
lZL tN
3 - 2 6- o I
CORRECTED PH I-, Y-5
r�,�
INITIAL pH
CORRECTED PH /a, 'z.3
3:
INITIAL pH /.3, 63
- 7jo
CORRECTED pH
/d 3/ ►'M
0,I"
INITIAL pH 12. 5-S
3 -a ? -a i
CORRECTED pH
a,15 0
INITIAL pH U.% 3
750
�� W
I
CORRECTED pH A?, ,?
11,'ySAr�l
INITIAL pH ` , ��
7 5�'
CORRECTED H I , p

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #_ REMOVE FROM BIN
DATE__ .3�p t
Final % Solids 4 � - �-)
TIME/
I pH
TEMP° C
152DEG.
SAMPLER
DATE
> 12.0 / 3 DAYS
/12HRS.
INITIAL
INITIAL H THICKNER
l
l)
3
Corrected H ,tea
y 31 I'
INITIAL H 53
- / 3 - o
CORRECTED ell
INITIALpH a, b .7�
a
-► 'D
CORRECTED H �.
: oo 4
INITIAL pH
. I -d
CORRECTED H z ,
// : 39 Am
-1 INITIAL pH /.?, 43
°
R� CA)
3- 1y - o I
CORRECTED pH 14,91
A2&' I-IA/7I
INITIAL 12H /a. 7 �
3-)5-01
CORRECTED pH
1 INITIAL H
3
CORRECTED pH 1 , q 5

ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN �Ztjp 1,6
DATE d /13 )Q ! Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
INITIAL H THicKNER
0
3 c) 1
Corrected rpH Le
fm
INITIAL H
3 - 3 - a1
CORRECTED pH
M
INITIAL pH! o <6_1
v v
�- -0 }
CORRECTED pH F
;00.
INITIAL PH
-
CORRECTED H 2.-D \
3 6A�I
INITIAL pH /Al, 6/_3
9��
RL
3- q-0
CORRECTED. pH /.?, /
/0- /.5A"'7
INITIAL H
3 - I - o
CORRECTED pH /d ,gS
y
lNITL H
r� 0
> i
CORRECTED pH / a ,
rf
'"

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # / REMOVE FROM B1N j/ /6Q
DATE h p Final % Solids 7
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
qU Am
.-.. ' al
INITIAL DH THICKNER ,9
D
ul
lit lot
I Corrected pH
INITIAL H /W. A 5
- /-o
CORRECTED pH /,�, `/3
—1 s n FrA
IINITIALnH /c2•, 7
V
- 1- 01
ICORRECTED H ` .
44b
INITIAL DH
14 - I - eyN
CORRECTED pH
!r,.
INITIAL PH
o
CORRECTED pH
INITIAL pH
- -0 I
CORRECTED pH / ` . SD
. P
H
INITIAL H
°
� -i I
CORRECTED off

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # _�REMOVE FROM BIN '/- /L/- O /
DATE Final % Solids 9,
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMPO C
152DEG. /12HRS.
SAMPLER
INITIAL
""/d A.17
IINITIALDH THICKNER 6. 9 y
]
J
Corrected pH 4. 73
5y«i
INITIAL DH /Z � Y
afQ °
R4t�j
CORRECTED pH /,�7. y4/
t 0Cih
INITIAL pH • 1� fl
�,
-t� J
CORRECTED pH ,
INITIAL H
-/IL0
CORRECTED pH 12.E S
•
INITIAL pH ,Aq
,411
CORRECTED PH z ,')
90
I INITIAL pH
goo
-1
1 CORRECTED H ,
INITIAL H a a7
S
' `i
I CORRECTED pH !{ ,

U TY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 3 REMOVE FROM BIN 41-1 Q-o 1
DATE_ Y�O / Final % Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
38 Pm
INITIAL H THiCKNER �. 7 rJ
/ rJ
o
Corrected pH b/, 5A
+ o,1"
330 pm
INITIAL pH 1d.69
R.4W
- /4- 01
CORRECTED pH
T
INITIAL PH
c
CORRECTED pH a
A
INITIAL pH °13
.900
�f
CORRECTED pH
�►�
J INITIAL H l . Y 1
%' °
y - / 7 -
CORRECTED pH / 4
3. 5�o P►�
40,150
INITIAL PH 10 . J'S
750
0 !n/
CORRECTED pH ,�, 7o
' ?M
INITIAL pH /�, �d
rl0
R),
- - o
CORRECTED PH 1,Q

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS
TO FURTHER REDUCE PATHOGENS PFRP
BIN #
REMOVE FROM
BIN
DATE y-
/7-o j
Final % Solids 9
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG.112HRS.
INITIAL
—0, a'7
I %`/'
INITIAL pH THICKNER , 5q
/0/
y- i 7- 01
Corrected H 6, 3-�
a
to.150
pfn
INITIAL PH /Z 53
ti -11---a ►
CORRECTED pH /,?, 6 le
-�6 P
INITIAL DH 22,47
- / - D '
CORRECTED pH
INITIAL DH 5 -2-
c�
-1 a -v
CORRECTED pH , In
3 % Yd PSI
INITIAL PH /W. �5
'] 3
Al Z11)
CORRECTED H /W.
P
o. .0yc
INITIAL pH /.�, S J
R
I
CORRECTED pH Id, 6
? % 4'5A M
INITIAL H / `/j
7,� °
Lt - �� - 1
,
CORRECTEu H %�, d
v

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #�_ REMOVE FROM BIN _ y--Z3-D
DATE �'-d - / Final % Solids 7,3
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
7
INITIAL pH THICKNER
'q- d o- v
Corrected pH g, d 9
-L/ pin
INITIAL pH / 6 I
't
CORRECTED H 13 . Q
INITIAL pH
a e • o
CORRECTED pH
J''gh+
INITIAL pH
CORRECTED RH 5
"---P1—i614CORRECTED
ITIAL H o�
2H
S,' fS4zn
INITIAL pH
-� -�
CORRECTED pH
-�-Z- eY /
INITIAL pH
O
.23 ;
CIORRECTcu pH Z, --.'

CEWED
WATER BUAUTYSEC-10N
TJAIN 2 J D,'9,
ICITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # r-
REMOVE FROM BIN _� -- a d - 0 /
DATE_ Final % Solids , y
TIME/
I PH
TEMP° C
152DEG.
SAMPLER
DATE
> 12.0 / 3 DAYS
/12HRS.
INITIAL
'1 pf-1
INITIAL PH THICMER�,J
%
Corrected pH
;3 9 Pm
'1-/9-01
INITIAL H %.7, �9
g� D
ICORRECTED pH )3,14Qcr
' 0,
INITIAL pH
19 r,1
CORRECTED pH
7% `Y5.4rn
INITIAL PH Y5
%`
�1
RA"
Yr � 1 o - O /
CORRECTED RH 1g.,10
INITIAL DH 9
7
- =Z&--ol
ICORRECTED RH ,;?, CQ
5.
INITIAL pH 14,66
-, f 9
CORRECTED pH l' ,
INITIAL H J
L-2t -p/
I'. ORRCEC T ED off I.J. AX I
I
v

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #
REMOVE FROM
BIN 6-3- 01
DATE 5- 30 - 01
Final % Solids
TIME/
PH
TEMP° C
SAMPLER
DATE
> 12.01 3 DAYS
52DEG. /12HRS.
INITIAL
/0 , .�0 Am
INITIAL PH THICKNER b R 7 /
�Q
��
S-3 0- e 1
Corrected H 6.a8
+ o• l Yo
: 00 AM
INITIAL pH
5-3o-oi
CORRECTED pH /,?, /
+. 156
d
INITIAL H Ja,
rs2L40j CORRECTED PH )a, Lf
-f W 1Y a
o
Am INITIAL pH Ja, ;k
$
CORRECTED pH A,
+oo5a
?n7 INITIAL pH
3-3) -o I CORRECTED pH
�o.i5a
Prf1 INITIAL PH
CORRECTED pH J j A
INITIAL pH
`ate CORRECTED pH o

UTY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #_ REMOVE FROM BIN _L/-.Z6•�%
DATE LI - a 3 -O) Final % Solids -59, 41
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
-o..1q
3 %0 .2 Pry
I N ITIAL p H THICKNER
Y- 3--0
Corrected pH `. J
INITIAL PH /a�• J�8'
700
Li -A - of
CORRECTED pH
441
t�
'i T, 0 ID m
INITIAL PH a ,
} ;t b-)
CORRECTED pH !` `1Qp
INITIAL H
CORRECTED pH
a.11-5
INITIAL pH
- d - o
CORRECTED pH /d.
INITIAL PH/,� 3 IV
750
,� L
`� - • 8
CORRECTED pH
l5 �.-r�
INITIAL H U. 3
4- a 9- 0
CORRECTED pH

(-
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #�_ REMOVE FROM BIN ti-a9-0 1
DATE Li� -0 j Final % Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
o. A 7
11:30 Ann
INITIAL pH THiCKNER d•.S�
��
R4LA)
`!-A5 - 01
Corrected pH &.3o?
pin
0.0135
INITIAL PH
70 d
R1 w
y-A3-0
CORRECTED pH/ .
INITIAL pH j a , 81744
5'
CORRECTED pH 12, 2-
�m
INITIAL pH
'] 3
-YaV o I
CORRECTED pH
-.13PIV
INITIALpH f,W, yZ
17o
Rz
A- {- a
CORRECTED pH Id, D
0,�6
INITIAL pH
'7,5
n
K1, w
4! -.kl_ o I
CORRECTED pH
' Z !-1
lN1T!AL pu t?, 3 �
CORRECTED pH

rr
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN 30-01
DATE L%- a 7 - 01 Final % Solids 7 0, d
TIME/
DATE
- pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
7: at 4 An?
INITIAL pH THICKNER .Y
��
Rj. w
"1-47.0I
lCorrected pH
4, 165
3-5 Pm
INITIAL pH M. qq��a
n
RLW
y-,49-01
CORRECTED pH ),1,5
1 ©';90pm
INITIALpH /;?.31
'?
-
CORRECTED pH 7
INITIAL pH 191/
.960
- g-d
CORRECTED pH ,
m
INITIAL pH JZ 0
_2$-o I
CORRECTED pH jZ
'
INITIAL pH /2, 3
760�r
CORRECTED pH 12, `-
.3 pm
INITIAL pH
�1- 30 - o 1
CORRECTED H / .

U r Y OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # c
REMOVE FROM 131N S-.S- G
DATEJ-•,R - 01 Final % Solids 6/1. 6
DATE
> 12.0 P 3 DAYS
152DEG.Po C
/12HRS.
SAMPLER
INITIAL
30 A�
INITIAI PH THICKNER (, . 7 1
J 7 0
�(
3-�- a
Corrected H y7
�i 3 0 �!'1
INITIAL H / a
D
S-- l
CORRECTED H 13
Ob A,4,1
INITIAL PH % a, 1
(�S o
5-3-01
CORRECTEDPH
M
INITIAL 10H a , 5
I
I CORRECTED H
LJ
,` 15 A++�
INITIAL PH
GJ
CORRECTED PH
INITIAL PH
s'-(1--el
CORRECTED H
�
INITIAL H g
0
- -0 1
CORRECTED OH /� ,

RECEBVED
WM QUALITYSE00N
IJAM 2 JJ "U =r
Wan•Dischrarp PorfWtUng
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #
REMOVE FROM
BIN 5-11-01
DATE 5-
$ - Qj
Final %Solids �S
TIME/
pH
TEMP° C
152DEG.
SAMPLER
DATE
> 12.0 / 3 DAYS
/12HRS.
INITIAL
bo
INITIAL DH THICKNER
5 - 8 - 01
Corrected pH
c
+-1'? (
INITIAL H ,3-�
c
5 - b' - 0 1
CORRECTED H
4-• I T /
G
00
INITIAL H R
ga
- I
CORRECTEDpH 9
t 5 oo 16
Y ► 17 Prl
IMTIAL pH Id, q
FO
S- 9 - D I
ICORRECTED pHj-,-:59
t 0.1(,5
3 "713 ?In
INITIAL pH i'a�, y0
�f Q O
f /o —o 1
CORRECTED pH %d, 57
1!: 3 o AIV
t 0. /L3
INITIAL pH / ,, 3
S 0
R4 W
0
CORRECTED pH./.�p
3 0n
INITIAL pH ; - • 37
,
/ a-D 1
CORRECTED nH ` - 5

(CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # q REMOVE FROM BIN 5- JA - O j
DATE_ 5- 9-01 Final % Solids
TIME/
DATE
PH
TEMP° C
152DEG.
SAMPLER
> 12.0 / 3 DAYS
/12HRS.
INITIAL
INITIAL JDH THicKNER
Corrected pH
Y�7P�
t o. r95
INITIAL H Jol.y
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5-9-01
lCORRECTED pH /.2, L 9
M
INITIAL pH
r
47
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CORRECTED H 7 Z
INITIAL pH
—1 0 --O I
CORRECTED PH /W, 7
/l 304m
7-0, i,to
INITIAL p H /• . 5�2
R4 W
5- / t- o
CORRECTED pH / , 7 6
INITIAL pH
i-L� 0I
_CORRECTED off 1.

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM
BIN
DATE 0/
Final % Solids
TIME/ pH
TEMP° C
SAMPLER
DATE > 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
INITIAL pH THICKNER
LLo
6-1 -01 Icorrected pH
-¢'•ab4
o
r • , = o INITIAL pH
CORRECTED pH
m INITIAL PH
- / r—o I CORRECTEDpH )
INITIAL pH 2„ 07
7
A
- CORRECTED pH i .Z.
+,Iqa /Q,o�I
O PAI INITIAL PH
- l S - O CORRECTED pH
to, tyo
AL H /e�. 1 3
8. 30 A m IN&REC
$50
le�tt�
CTED pH /
INITIAL H

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # b REMOVE FROM BIN b"- 9- d 1
DATE Final %Solids
TIME/
DATE
pH
I > 12.0 / 3 DAYS
TEMP° C
152DEG. /12HRS.
SAMPLER
INITIAL
d,L5
1
INITIAL PH -MICKNER 6. 7/
5-3J-0/ Corrected pH 4,56
t0, rq5
,Q- 0 Pn-1
INITIAL H U. 3
04
� J,
S- i - o i
CORRECTED pH
k..
INITIAL pH
3
CORRECTED pH / 7 ,
INITIAL H a .4
a
Ca 1 (�
CORRECTED H J � �
1:30Pn'1
INITIAL H %7. ,�
S A O
R•� LtJ
- a /
CORRECTED' pH /3,3 7
Gi 1pj
INITIAL pH
go
�r
-p-0 I
CORRECTED H
f •qo
`
INITIAL pH ) , A16
CORRECTED off 12 . -�D

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # .7 REMOVE FROM BIN 6-q-dl
DATE_--O Final % Solids Cp 4
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
2- /d An9
INITIAL pH THICKNER 6. 71
IV
9411
Corrected pH
INITIAL DH % ,33
7
R44J
CORRECTED pH
+ . i 71
tD
INITIAL pH f , 4
Z
r U
CORRECTED pH
0 m
INITIAL pH `aZ.*a
.290
127 GJ
-A-61
CORRECTED pH l
(,'v f N1
INITIALpH = 31
2�5 C)
Iry
CORRECTED pH 'Q
,�.lSo r
INITIAL pH 1 Z-
7
3
CORRECTED H I Z.
�0
INITIAL pH / ,
- - �1 CORRECTED pH ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN
REMOVE FROM
BIN 4-1y-01
DATE 6 - /1-D I
Final % Solids
7y. y
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
- o.oq
q' 95AM
INITIAL pH THICKNER7.51
,?a °
z w
6- U- d!
Corrected H 7. 6
w0.135
3% O Pry
INITIAL DH /a. 5Y
7 Q°
Rt w
6.11 - 01
CORRECTED pH
INITIAL pH
�-7 0
CORRECTED pH
-�
02 Ob INITIAL nH 1p�r �Q
/
-70
-/ - CORRECTED H .
33 Pm INITIAL pH U. VY
75 a
R4
CORRECTED pH 14.51
40,t35
'2 Pm INITIAL PH �07. 3q
700
R4 W
CORRECTED H/,�, ;Wj'
4
INITIAL PH
c CORRECTED pH a ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
M1114 iF HEMOVE FROM BIN 6-/1-01
DATE Final % Solids If, r
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
9: 3o
- o. oq
INITIAL PH THICKNER
®
Rk w
6-13 •o►
Corrected pH 7,,r
3/ 0
f d.►3s
INITIAL PH 1W, 7.1
700
R4 Lul
6-13-01
CORRECTED pH /,RJ/6
INITIALpH
7 D�
< <
CORRECTED pH
42'I`'1
INITIAL pH o2� �5
Q
6
- d
CORRECTED pH
ry7
0.)(95
INITIAL pH
00
�3
�-1 `�-b ►
CORRECTED H / ►
d. pm
INITIAL pH 4. 3 1'
®°
IQ� w
L. I.S. o l
CORRECTED pH 1.1.5.6
INITIAL pH
is
CORRECTED pH ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # Ll REMOVE FROM BIN 4-/b'-o i
DATE � -15 -d 1 Final % Solids
TIME/
DATE
P
I
152DEG.oC
SAMPLER
> 12.0 3 DAYS
/12HRS.
INITIAL
�
-0.06
55 fn
INITIAL THICKNER % $�
lCorrecteVp—H7.
�,3p
94W
6 -1 - 0 /
54
Pen
INITIAL pH % tyb'
°
R4 W
CORRECTED pH /a. 6
S- v0,p>
INITIAL H
w L
CORRECTED pH
=2?0 4,u
INITIAL H
- -
CORRECTED H
]4 . /y%
INITIAL pH ,
CORRECTED pH
.ILU
% `OS -Ark
INITIAL pH / .Z , q Ll
/7
CORRECTED DH 2,s
9 % 30 Aril
to, ISO
INITIAL H /�
S- / � - a 1
CORRECTED

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 5 REMOVE FROM BIN _6-49-0j
DATE d ,t0. 0/ Final % Solids 7
TIME/
I pH
TEMP° C
152DEG.
SAMPLER
DATE
> 12.0 / 3 DAYS
/12HRS.
INITIAL
-o. o6
4W -'4/ Jar-/
INITIAL PH THICKNER 7-all
6.Zo-a
Corrected H ?.SS
o.l�5t
0? : 30 PM
INITIAL H
6-4/-01 ICORRECTED
PH
'7
INITIAL pH a
m
o CORRECTED PH ? ,
1- 6 s
% O0 INITIAL PH
b
CORRECTED PH /a ,
o,IL�
� ''� INITIAL H /a,�.
'%9Q
'a-l_ 01 CORRECTED PH
a.i",z
Q
� • rc. INITIAL pH /
�
CORRECTED PH IQ.-
INITIAL OH
dL:T
W
CORRECTED pH ) ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # I REMOVE FROM BIN
DATE Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
152DEG. /12HRS.
SAMPLER
INITIAL
q4az
INITIAL H THICKNER
0 0
Corrected PH ,
-"V5,f 1
6 -AS-o 1
INITIAL
CORRECTED PH /W. g
754
W
t00 .�
INITIAL H >d•85
g®°
- -
CORRECTED PH /3.6a
6-A4-ol
-to.ISO
INITIAL PH
CORRECTED PH
/ C
a
INITIAL H '-
CORRECTED H
We
INITIAL Htz/
CORRECTED PH - 6
;30 pm
INITIAL H
6- ��d1
CORRECTED PH �,

'CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # d
REMOVE FROM
BIN 7 /-• 0 /
DATE
Final % Solids
TIME/
DATE
pH
TEMP" C
SAMPLER
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
-0.06
/0,'d0 A177
INITIALpH
THICKNER 7I, ` -5
230
LW
-.td -0 f
Corrected
PH i
7A*1
+o,��o
INITIAL pH
/o?. `%0
�}
-td•a
CORRECTED
PH
%5 P�
INITIAL pH
7-0 -C)l
CORRECTED
EH' /
73,130 fM
!NITIAL PH-.
I CORRECTED
PH /a?, 6
-f, t�Ca
a
e
INITIAL PH'
,
CORRECTED
PH
�= cS
INITIAL PH
�Z3
��-
7'I-M
CORRECTED
H I2, 1f
4•'?`F
d
m
INITIAL H
j a
" — G i
ICORRECTED
pH % 1<4 f 1I
c

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 7
REMOVE FROM
BIN
DATE -
�C1 J
Final % Solids
TIME/
pH
TEMP° C
DATE
> 12.0 /,3 DAYS
152DEG. /12HRS.
.3%3o c I"m
INITIAL PH
THICKNER a 3
' - 4 - a
Corrected
EH 7,,Qo
,:,w , 39
3'33 91 rn
INITIAL H
/o?. 'i r
CORRECTED PH /
f.ixQ
U
SAMPLER
INITIAL
L
INITIAL Prl
a
CORRECTED
pH ! o
:3-t3
INITIAL DH
a
Q-
CORRECTED
EH / , a
INITIAL pH..
j.
CORRECTED
PH ,�
`3SR
1-U
.l i
INITIAL H
CORRECTED
p H 1 z.
�C M
4 - ),sg
INITIAL off
/� , la
? -2"- 0 1
CORRECTED
pH ) , '7 1 �,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 60 REMOVE FROM BIN 7-5- ® t
DATE___ Z 5- O Final % Solids
TIME/ pH TEMP° C SAMPLER
DATE > 12.0 / 3 DAYS 52DEG. /12HRS. INITIAL
0
JaD
INITIAL pH THICKNER 6 ,;? 4j
7 ®5 -0 /
Corrected pH
,
0.145¢
3 :3) Pff 7 IINITIALpH
'1- 5 -O j I
CORRECTED pH
r
INITIAL pH j
0 1 CORRECTED H , a
�
-f0.JS0
"if _0
-- INITIAL H . ��r ��
r5 °
7- 6-01& CORRECTED pH /J, 6,3
.a PA INITIAL
a
H .'/ �2 • a 9c
` 1 CORRECTED pH r
INITIAL H /
-29 0
rJ- 9-d J CORRECTED H
-t-
AINITIAL H
YQ 0'
C
R
)w
Lw

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # y REMOVE FROM BIN 7- 9- 0 j
DATE_ %- 6- d/ Final % Solids
TIME/ pH TEMP° C SAMPLER
DATE > 12.0 / 3 DAYS 152DEG. /12HRS. INITIAL
% 9 A r1 INITIAL pH THICKNER 7. 30
-o/
Corrected H y4
t o, t4s
INITIAL pH
7-d- O1
CORRECTED pH /
5,p h-
INITIAL pH /,;? ,
`7- G 1 -1
CORRECTEDpH ;? .'7 v
3 •�--
INITIAL pH. g'
-7- `? r b !
CORRECTED pH 7
l; �M
INITIAL pF,
- -v
CORRECTED pH / ,
5
INH
- , a 1
CORRECTED pH,
9'30Ar")
INITIAL pH /4,.5e
7-10-0/
CORRECTED H /.?,7S
0
r•
q �-r
9 S0
�4 4o
.eo o

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN REMOVE FROM BIN 7-13 - 0 I
DATE 7 - /d - 0 / Final % Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
- v.0z
9 : 50 A ►•Y1
INITIAL vH THICKNER % / 6'
R.3
1,j
7-10-01
Corrected pH 7, l a
M
INITIAL pH :Zt 5^7
q^v
7 - l d - 01
CORRECTED H `
6D,4"•z
INITIAL PH /z,�b
�,Z °'
/1
CORRECTED pH i2 b
�.165
3 : e4 3 h,j
INITIAL DH /
800
7- //- o /
CORRECTED pH / 6
�.p
10 Y
INITIAL pH.' �02�6
C7
,,. -
CORRECTED pH �
to, ia5
4)"S 41'l
INITIAL PH
a
7-la-o ?
CORRECTED pH /,, 75
o, l -is
INITIAL H
'l - /i-o 1 JCORRECTEDpH
/�,�

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 3 REMOVE FROM BIN 7-15-0I
DATE 7` Id -o Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
/ 1" 3O
,-0,o6 ,e�
INITIAL H THICKNER b, Ll t
a,3
l�
7-/oZ-0 1
Corrected pH
SAM
to.rq.5
INITIAL H JW.• --5
O G
7- / -�Z - o j
CORRECTED EH /d . 75
3S ,-
INITIAL pH
o
0
CORRECTED PH (Q 0
INITIAL T
-dl
CORRECTED pH
INITIAL pH '®�
J�L�„/
- 1 -J
CORRECTED pH
i • - ) FM
INITIAL pH j �,- 01
9 °
(S
-/ 1
CORRECTED pH o2�
11 0Ob
INITIAL pH
CORRECTED pH 12.,Sn

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # e? REMOVE FROM BIN _7-/9-o l
DAT
Final % Solids
SAMPLER
TIME/
pH
TEMP° C
152DEG.
DATE
> 12.0 / 3 DAYS
/12HRS.
INITIAL
- o, o.6
8: 30 Ark
INITIAL PH THICKNER6.37
a 3 J
-/& -a/
Corrected PH d, 3
0. ! 95+
30 Pfn
INITIAL H d..SO
90°
7- l & -d
CORRECTED
.)jct
` b P
INITIAL H a
g;
CORRECTED PH a
INITIAL PH f ,
0
CORRECTED pH a,
Cv
a
INITIAL PH
�
CORRECTED pH a
4
INITIAL PH
CORRECTED PH
LA
INITIAL PH
1
CORRECTED PH j a. i, x I,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # �_ REMOVE FROM BIN a3 0
DATE `1 i i 0 ; Final %Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.01 3 DAYS
52DEG. /12HRS.
INITIAL
r,
INITIAL pH THICKNER
r
Corrected PH
INITIAL pH
0
pf
CORRECTED pH jaJ2U
. 6
INITIAL pH
r
CORRECTED pH ' ,
�.
INITIAL H .
U a
r
- -0 1
CORRECTED PH I
%3Sa cti
INITIAL pH'- la ,
CORRECTED pH / ,
7 1d0 A�
o, r so
INITIAL H 0, :53'
°
'� �
R4 W
7-A3-oj
CORRECTED pH /a, 73
INITIAL
-�LL)
?-a'5oJl
CORRECTED pH 1a,jq

(CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 6
DATE 7'a
REMOVE FROM
- 4 j
BIN
Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
152DEG. /12HRS.
SAMPLER
INITIAL
5 : 0 O
7-d 5-a 1
INITIAL H THICKNER
Corrected pH
c
(f ;Do AM
'i-as-o/
0"""
INITIAL pH /R,,4,7
1 CORRECTED pH Ja,
INITIAL H , (, 2
- a5 - o
CORRECTED pH 3
INITIAL p
cv
CORRECTED pH )Z
Y%30
7-a2 �O J
fINITIAL H '
CORRECTED p H
INITIAL PH
CORRECTED PH
INITIAL pH
CORRECTED PH

(CITY OF STA I ESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN
DATE Final % Solids_
TIME/ pH TEMP° C
DATE > 12.0 / 3 DAYS 152DEG. /12HRS
INITIAL pH THICKNER 23
7 -d 7 -o l Corrected H
INITIAL PH
CORRECTED
H
7 - ?,7-
INITIAL PH
/, ,3 -7
CORRECTED
H
7- 8' 6
INITIAL H
1q1, flJc
3
CORRECTED
PH 4g,A.
INITIAL H 33
'a-�( -J I
CORRECTED
H -L
INITIAL DH
, d
7 z -
CORRECTED
INITL4L H
/� �o�
CORRECTED
H�,
-7o
SAMPLER
INITIAL
Pow
Ri'vi
�o
•
w
4

(CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # '
DATE 7 - d j�— O /
REMOVE FROM BIN
TIME/
pH .
DATE
> 12.0 / 3 DAYS
30 INITIAL H --R ". I
7-d15-0 J
Corrected_pH
�, S
') ; 30 I'm
INITIAL pH
7-AG-O)
CORRECTED
PH
M i'-36
INITIAL JDH
-e)t
CORRECTED
H ,
#X/
INITIAL H
'a
CORRECTED
pH ,
' a
O.Sobs INITIAL H '
CORRECTED
pH
3
INITIAL pH
,
�� 4%
CORRECTED
H
ol "^
INITIAL H
�{(
�
CORRECTED p
;1 a
f
;3e
7` �`' � �
ice• � z�
Final % Solids
TEMP° C SAMPLER
52DEG. /12HRS. INITIAL
8-50 ' Rz,"/
3 w
y 0 . . I f4w
�l ll
6?`
Ks°
w

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # y REMOVE FROM BIN
DATE 8-% - O / Final % Solids d
TIME/
DATE
I pH
> 12.0 / 3 DAYS
TEMP° C
152DEG. /12HRS.
SAMPLER
INITIAL
-a, o�
INITIAL H THICKNER
Corrected pH ,5'; o
3 m
+- 0 f esa
INITIAL H M63
CORRECTED H H-
01L",30
+C), 180
INITIAL H
°
�
b-a-Ol
CORRECTED H
-7 f'1
INITIAL H 01 ` 5 7
C�
-®
CORRECTED pH j
Ib Am
INITIAL H '
g-
CORRECTED pH j a , '�l
INITIAL pH
g O�
t
CORRECTED p H �, 7
J
INITIAL pH
3 `� 1
CORRECTED AH .'7

ICITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN * R . REMOVE FROM BIN J- 5- a 1
DATE S-a- 0 j Final % Solids 0/4 %
DATE PH TEMP° C SAMPLER
12.0 / 3 DAYS 152DEG. /12HRS. INITIAL
e,49
8- I d A M INITIAL H S/A '^ d
8 - A -01
TFIICKNER i
Corrected pH _r p
�o,/�
a 3v Pf*
INITIAL H Q
0i
CORRECTED
.� • LU
INITIAL pH
�`r?1
CORRECTED pH j
INITIAL pH r�
,K-
CORRECTED H .
r
+-�
INITIAL H ' . 70
�s- ' - a
CORRECTED , H o
INITIAL pH
-el
CORRECTED pH 3
INITIAL H
CORRECTED
KA U1
q0 °
is °
rnly
[ j

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 3 REMOVE FROM BIN 8-IO - 0/
DATE_ 8 - `% - p / Final % Solids
DATE
> 12.0 % 3 DAYS .
152DEG.PoC
/12HRS.
SAMPLER
INITIAL
PM
INITIAL H THICKNER
Corrected pH
. f
INIT'AL�H
g5
8 - 7- o
CORRECTED H 1 ,
t Gt�
INITIAL H o� 6
-J 1 CORRECTED H 6
M INITIAL H
°
+
-U CORRECTED H -
INITIAL PH' %a. 4 q
qQ ,4
R4
- CORRECTED H / , 6 y
3 p INITIAL H
CIO
�� W
- O / CORRECTED pH
gAn1 INITIAL pH
� ! CORRECTED pH 7 j
11

W ER QUALITY,81500N
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # �_ REMOVE FROM
BIN
DATE_ 5-13 -O J
Final % Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
INITIAL pH THICKNER
�3-0Corrected pH
? %y5 AM INITIAL PH
8-13 -d 1 CORRECTED H /•,
'/ "/74., INITIAL pH
-1 q-O I CORRECTED pH l fa
• �S� INITIAL pH
Y-/ o CORRECTED pH
o, 1d0 a
INITIAL pH
I CORRECTED pH / , '7.3
%gym INITIAL pH /.-? .53
g� -a CORRECTED pH ,
INITIAL pH �/ .
m
f-17-el CORRECTED EH

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # -0 REMOVE FROM BIN F-1y-01
DATE S -15 - 01
TIME/
DATE
pH
> 12.0 / 3 DAYS
AM
INITIAL EDH TtHiCKNER
Y- /3- d
Corrected pH
6.3.E A rn
INITIAL pH 1 Q
5-16-o I
CORRECTED pH 7
INITIAL phl /o , go
1 CORRECTED pH
;- INITIAL H �.��
- - a CORRECTED H d
' INITIAL H �a���9
- 56Y CORRECTED H 3
INITIAL H lR? �%
8-i 7 -o CORRECTED H /a
0,135 ,t
INITIAL H ia.7.6
CORRECTED r)H /-7. z? 6
Final % Solids 77,
TEMP° C SAMPLER
52DEG. /12HRS. INITIAL
° 1 E
)4 [�

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # a? REMOVE FROM BIN 2�-a3-01
DATE 8-,?d r a 1 Final % Solids 10
TIME/ pH TEMP° C SAMPLER
DATE > 12.01 3 DAYS 52DEG. /12HRS. INITIAL
-o.a3
0
/ d ,4,-n
INITIAL pH THICKNER /, 0 0
8'- o - o
Corrected pH 7, 0 5
% % 0AIn
0.195+
INITIAL pH &1 1_3
Q
.0
0
CORRECTED pH
z5' rn
INITIAL pH
,Er-,;zo-of
CORRECTEDpH
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INITIAL H fa��
t�S 7°
/%Z LO
f
CORRECTED pH 102 t
a
INITIAL H"'
0
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CORRECTED pH c
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INITIAL pH /)°
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CORRECTED pH
.��
o, lYo �-
INITIAL off
6
Rz
-o2a --0
CORRECTED pH / 3 , O Q

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # LI
REMOVE FROM
BIN _F-d
DATE _-�a
-o /
Final % Solids 77.
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
152DEG. /12HRS.
SAMPLER
INITIAL
INITIAL H-HICKNER , o '
G
94
Corrected pH 9, --
INITIAL H
CORRECTED H/
10
INITIAL H z,
o
b �1.-
CORRECTED H
-- 12.9s
T—�
b5
INITIAL pH
�•-ol
CORRECTED pH j2,. 8,I
3!�T)
0,145 a .
INITIAL H ` %�,
0 Li
3-O
CORRECTED H Z,
-
INITIAL
- —o
CORRECTED pH ,7,.
INITIAL H
CORRECTED pH .71-1?

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN 9-7-4 1
DATE_ - y -0 j Final % Solids 7 q, L/
TIME/ pH TEMP° C SAMPLER
DATE > 12.0 / 3 DAYS 52DEG. /12HRS. INITIAL
A
°
INITIAL pH TNicKNER 7. d,7
3
1 lCorrected
pH
a plr�
INITIAL H 3, /�
�? - 11/ - o /
CORRECTED pH 13, 7
INITIAL joH
gn
- 1 CORRECTED pH
mINITIAL H
9019
I
- -U
CORRECTED pH
-
3 Pr>j
-M. l Yo _,
INITIAL pH
f
CORRECTED pH
f o, /b-o
INITIAL H
a
2-7-ol
1CORRECTED p H 1.2, 9
/1,
� • IYo
INITIAL H / ", `4
-1 d -aI
CORRECTED DH 17. nU

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 7
REMOVE FROM
BIN q - 0 -0 1
DATE 4- `7-41
-�z
Final % Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
q A rrm
INITIAL PH THICKNER 7. 41
3'
Rl W
9 - 7 - 01
Corrected pH
INITIAL PH j .:?,
PILAI-
-7-a
CORRECTED- H ,
INITIAL pH
c
inll�
-'9Q/ CORRECTED pH D
11 INITIAL H o?-%S
95 °
- -v CORRECTED H
b INITIAL PH'
_ - a CORRECTED pH a,
INITIAL H ' a ,& 2
$ 9 a
/71 OJ
-01 CORRECTED pH
l 1 N !T!A L H / ,� . � g
�a
�L-
- --o CORRECTED pH /-? ,5

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN REMOVE FROM BIN 9-30-0 /
DATE q-A %-a J Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
12M
INITIAL pH THICKNER 756
` a /?L
Corrected PH 7,Y/
`f0 P
INITIAL pH /
/ �wi
CORRECTED pH �?, SS
' S ni
INITIAL H L� "D 0�
$ `7
6�-Q8--tt
CORRECTED pH .� d
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INITIAL pH 141 ( 1
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CORRECTED pH a, 72
a2 : nO ►'-)
INITIAL pH.'
f -b I
CORRECTED H ,
—�►
INITIAL pH
/ �1
cY 3 -D
CORRECTED pH
a
INITIAL pH Y 7
J L
���- o
CORRECTED pH

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM
BIN
DATE
Final % Solids?, y
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 ! 3 DAYS
52DEG. /12HRS.
INITIAL
oC /,SPm INITIAL PH THICKNER%5�
Jaw
Corrected pH 7,10
o, /8o a-
a�% 3 O P INITIAL p
4-a,'-o 1 CORRECTED pH
�;U M INITIAL H 0 ,' 3
� jv
-a) -D ► CORRECTED pH /.Oq,
00 RM INITIALpH to? • , . ~
."! b �
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/A INITIAL H '/,?,
goo
1-4 4-0CORRECTED pH
a Pt-� JINITIAL pH 75"
0 6
- a 7 - o I CORRECTED pH / .
INITIAL pH �a, 7 3
L
CCRRECTED I-f (j

CITY -OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 3 REMOVE FROM BIN 10-9-01
DATE %D - 3 - 4) Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
% 30 Pryi
0,30—
INITIAL pH THiCKNER1, 0 0
1:)r
124
/0-3 -ol
Corrected pH �, 70
11 Ann
0.105
INITIAL pH c/.
��
/�.�
to-3-01
CORRECTED pH
71`00
INITIAL pH fQ•
'93 J
- 1
CORRECTED PH ,
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INITIAL PH
-d�
CORRECTED pH
INITIAL H '
R
0 — LI- 0
CORRECTED pH
INITIALpH I -v0
_7
J w 4—
,lo-ell,ol
CORRECTED pH
` 70A m
INITIAL off la-77
— —C ICORRECTED
pH A.195

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM
BIN _/0 - S-d
DATE
Final % Solids
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
-o,a7
._Wso
/
INITIAL pH THICKNER b / J
W
to - - o
Corrected H 5',. fl
O.IYof
Am
INITIAL pH
10-,5-01
CORRECTED H f ,
4'6-Z>5 p hjINITIAL
pH J.
3
O 's o
CORRECTED pH ,
rdV Xxi
INITIAL p H A-? • %o�
l� `el,l0O
CORRECTED EH ,
INITIAL pH
0-
CORRECTED H o?
15 pm
INITIAL DH
CORRECTED pH a , -Br
V 6,L)y
INITIAL pH
/'D ` 7-d /
CORRECTED ^H

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # - REMOVE FROM
BIN _l0 -/l-0
DATE
Final % Solids
,
TIME/ pH
TEMP° C
152DEG.
SAMPLER
DATE > 12.0 / 3 DAYS
/12HRS.
INITIAL
1d%410 Plt7 INITIAL pH T-nCKNERb,
50
8
la-*-01 Corrected pH 4�,
0,1q�+
3: ]5 Pi,? INITIAL PH I-3 7
9O °
/0-9-01 CORRECTED H
S INITIALpH g
LO
6-9- of CORRECTED ,-?,
-pH
INITIAL DH
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v INITIAL H '
1 o
/ CORRECTED pH /
r
c,22 j9M INITIAL pH
- 0-) CORRECTED H
4 �SOAir1 INITIAL uH 0, 560
0 -/ -n I CORRECTED pH / , 7 ,ir

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # _�� _ REMOVE FROM B1N 10 -13-01
DATE /0 — - J Final % Solids G7 n
TIME/
DATE
pH
> 12.01 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
10,41y)
0•30- - 9
INITIAL pH THICKNER6. d
/5
�
/ O -/ D - /
Corrected pH
3'0 Ad"T
o, /f'df
INITIAL H
/ - -
CORRECTED pH / 3
:U0 PtN
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CORRECTEDPH L,
c0 8M
INITIALPH
90
a - -0/
CORRECTED pH jZqp
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INITIAL Fi
`76c'
5[a
b- -o
CORRECTED H
15 Am
INITIAL pH .Jr�
85
An w
o -r;t -&I
CORRECTED pH .
to%Am
t
INITIAL off /
g0�
A
-/ -o
CORRECTED pH

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #�_ REMOVE FROM BIN /D,l?- O /
DATE /0-/d -01 Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
INITIAL pH THICKNER
Corrected pH
`7 D �
INITIAL H
O^
CORRECTED pH
r:
INITIAL pH �O�' Iq
7 -Y 10
/D- -,41
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INITIAL DH '
/ d
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' 30
INITIAL pH
$ v
CORRECTED pH .W• 7
G 5 0
INITIAL pH
so
o
CORRECTED pH j�,�

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # -REMOVE FROM BIN
DATE Final %Solids
TIME/
I pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
INITIAL pH THICKNER SA
0
' Corrected_pH
, ©, )TF
INITIAL pH
' M CORRECTED pH ,
INITIAL H 93
- 01 CORRECTED pH 3,
U o A M INITIAL pH a- f l
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pH C,
i CORRECTED pH
s
INITIAL H a
S' lQiyl CORRECTED pH
�0 INITIAL H
J 1-0 I 1 CORRECTED cH :F
�1

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # _ REMOVE FROM BIN _ /p- Af
DATE jp -.� 8-[�� Final % Solids_
TIME/
pH
TEMP° C
SAMPLER
DATE
> 12.0 / 3 DAYS
52DEG. /12HRS.
INITIAL
A,Y1`
��pp
d ya3r
INITIAL pH THICKNER
% D
Corrected H / 1,
3.'3a PM .
�' 315
a
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lee
0-
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INITIAL pH
o
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a�cu,
INITIAL pH
CORRECTED pH 73
INITIAL pH j
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c,,
INITIAL pH d��
L
-moo-o
CORRECTED pH ,?
INITIAL pH ,? ' 1
900
-,-�D-J
CORRECTED pH /

OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 3 REMOVE FROM BIN ) 0 -a7-0I
DATE_ 10 -a Ll - 0 i Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
e/' 3 :5A M
/ 0 -d V- 61
—0,2,l
INITIAL pH THICKNER b• aZ
Corrected pH
r LR4
LA)
7 P r.,7
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/ v0 o
G D
/a-aV-0!
CORRECTED pH /3,O
An?
INITIAL DH l,? , fl 7
1000
Cr D
i0-d5-01
CORRECTED pH 13,07
/ A rn
o , 150
INITIAL p
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CORRECTED pH
INITIAL pH /,;? .
7 �
75 z-o L
o -zs-o
CORRECTED RH -2 , �$
,3.15 •'�'c
INITIAL pH ! 1. &
l c
%%1 Gt1
/d -9�-6
CORRECTED pH , -f
g i �Jr-
INITIAL pH ZR,S
�-
J -a ^o
CORRECTED pH

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # C�Z REMOVE F - FROM BIN 10�a� Q If
DATE 10 Z Z `0 1 Final % Solids 7�, %
TIME/
DATE
PH
> 12.0 / 3 DAYS
TEMPOIC
152DEG. /12HRS.
SAMPLER
INITIAL
9 ; 3a /t fri
INITIAL pH THiCKNER �, S'
)� -
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Corrected pH bl$
01i
00`�•
. 2+0
INITIAL H AR, 37
ICC �+
-OI
CORRECTED H
3° -#
INITIAL pH
919
AD --73-iV
CORRECTED pH
M
INITIAL pH J
0
- 3 I
CORRECTED pH 1 on
OU
INITIALpH
a
0 - 4 -U 1
CORRECTED pH ,
%,'U
INITIAL H o2� 'a
I
CORRECTED H l 7
I((-)
INITIAL H o?
Z `� I
CORRECTED off Y ,

RECENED
WATER OURLITY sECT10N
Non-1019charg®PaffhIdI ►g
CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #_ REMOVE FROM BIN /0 A Q
DATE10� l /-0 Final % Solids U,
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
0,30
/0 AM
INITIAL pH THICKNER b , 5;�
J-5 �
Rt Li
Corrected pH W, 42
INITIAL pH �;? .53
0
J W L
-10-A4-ol
CORRECTED pH ia.
INITIAL pH _5
d -97-6,(
CORRECTED pH
/G
INITIAL pH 0,
070
,
-1-1-0 I
CORRECTED pH l
D,Prn
INITIAL PH /,W, `'6.p-
� 5�
-"
CORRECTED pH a. 7
- Id Am
INITIAL pH �q
o$-
CORRECTED pH
5,55P
IMTIAL H
0
v -,-, ^-d i 1CORRECTED
pH 7�

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # ,5 REMOVE FROM BIN /I-a-01
Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
61 A n'%
- 0, au
INITIAL H THicKNER % 0 J!'
7 °
Ao.(
1,0-.30-ol
Corrected pH 6,
?� PM
INITIAL PH g r
9510
to -0_ I
CORRECTED pH 0/
a"ou Rm
INITIAL H azo
�v
!u ' „p / 'CORRECTED
pH , 0 v
01fM
INITIAL DH
10 - -o
CORRECTED pH }
t, D M
INITIAL DH 0?, iq
. 10(9
- -U 1
CORRECTED pH t 7
.3 Pm
+0,19y
INITIAL H / ,
330
RZWz 6:
CORRECTED pH / , q
1 l l A M
t0, IS-0
INITIAL pH
//-a?- 0 1 ICORRECTED
pH! Q-3

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 6 REMOVE FROM BIN //- y-y/
DATE //- /-y / Final % Solids 77,
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
3 m
d,Iv-
INITIAL PH THICKNER&,SZ
19'
LA)
- -
Corrected RH /. 3P
-3 Pd?'1
Fo.l�S
INITIAL PH , 8 3
Q c
R� l/1) %� G
-/-a
CORRECTED pH
INITIAL pH a,4?
O
�f�
��vL,
CORRECTED pH
INITIAL pH .a �f 0
0
W
CORRECTED pH ,
a" (0cL
INITIAL pH 1A,65
0
d
v w L
111- 3 - o
CORRECTED pH
T�
INITIAL pH a
1
Li
CORRECTED pH
H �,Lf-7
9-
E11',-�jfplINITIAL
-0 / ICORRECTED
pH ,-2.97

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 7 REMOVE FROM BIN
DATE //-A -O / Final % Solids 71, 7
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
INITIAL pH -rHiCKNER %, 5
% °
pktj
//- -0 1
Corrected pH G,
INITIAL PH.7
CORRECTED pH
►-+1
INITIAL pH / -72
1-3 - o
CORRECTED pH
r� �^
INITIAL H %�`�r
�j�-�
A
6-
CORRECTED H 1p.
Prn
INITIAL pH
V-3-of
CORRECTED pH 1 .9, Ce
:15.4
INITIAL PH' /,�, 5 �
Z 3 0
/'y1 GtI
- 4 -el
CORRECTED p H
o2:c5 0-F d
INITIAL p H J • y 6L-
'
i (- Y -b/ ICORRECTED
pH /,7,66

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN 1 /-e-c) J
DATE //- 5-0f Final % Solids J3 3
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
Z AIV,
i INITIAL PH Tt ICKNEE
RL w
a-5-e)l
Corrected pH
INITIAL PH
L,
7'50-p:-.
CORRECTED pH
-( -61
INITIALpH /d, �?
` 7 °
/'?Z4)
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-'6130h
INITIAL pH
- ` 1
CORRECTED pH/c2,-77
'2' M
INITIALpH o?j C%
°
-
CORRECTED pH ,
INITIAL H f P,
:J90
11--7-01
CORRECTED pH
INITIAL H - 9
a
1- - 0 1
CORRECTED pH ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # a REMOVE FROM BIN / /- - d 1
DATE Final % Solids
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
yov p6�1
INITIAL pH icx�vE
11_
L..1
Corrected H
1-s-b
INITIAL p
7 ;.SO P:ti
CORRECTED pH
INITIAL PH
CORRECTED pH
9t ,3D M
INITIAL pH • %
10D °
L -0
CORRECTED pH
tM
INITIAL pH go 67
c
,
i ` 1
CORRECTED pH
3
INITIAL pH a• /
- -0
CORRECTED pH j
' JINITIAL
H
1- -0
CORRECTED pH / , 6

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD >
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 3 - REMOVE FROM BIN 11-1 l - o
DATE ___/ Final % Solids f' , a
TIME/
DATE
pH
> 12.0 / 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
Ah-t
INITIAL pH THICKNER
I�C Gil
Corrected pH
INITIAL PH -3;
i r- 4c-o r
CORRECTED pH ,v
7� Din
INITIAL pH /7.
6�
rl-
CORRECTED pH .;?,S
INITIAL pH (o
9a
11-1-oi
CORRECTED pH ,
;30?h
INITIAL pH / P-
1) -! 0 -0 1
CORRECTED pH
`% ' .5 G P
INITIAL pH "? . 7 �
�"` � ��
J C,J �-
- t o -o
CORRECTED pH , g
3%1-5',m
INITIAL pH
1- ! 1 -21
ICORRECTED p H a�`"

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN REMOVE FROM BIN
DATE %/ -9 -O / Final % Solids t/1 fJ
TIME/
DATE
pH
> 12.01 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
INITIAL pH THIcKNER
Corrected pH
INITIAL pH a 3 Ce
9�
` J w L-
1(- -o
CORRECTED H .<11,
INITIAL pH fc).
z�''I4i
11-lo-61
CORRECTED EH ,
/ Q'
INITIAL pH J 02, 6 0
1-1-D
CORRECTED pH Du
'2 �50-p�
INITIAL pH <Q 9
a�
Lj L
CORRECTED RH
INITIAL PH
1 -
CORRECTED pH
.5Q Ff'L
INITIAL H
- // - o
CORRECTED pH ,

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN /(-l-6-Q 1
DATE ll- /a -o Final % Solids .s-
TIME/
DATE
pH
> 12.01 3 DAYS
TEMP° C
152DEG. 112HRS.
SAMPLER
INITIAL
1 a a.-i oc ►,t
0,3Q -
INITIAL PH THICKNER Z,
Q
21-4A- d 1
Corrected pH 6, O Q
Pr?
•o.rYat
INITIAL pH
o
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//-id, --o
CORRECTED pH1W, 7
�; Od
INITIAL pH
`t✓ d
LcJ
CORRECTED pH
3� /�•� ►�
INITIAL pH
1�7 Al
CORRECTED pH 77/-77
a Ar77
INITIAL pH
Q
-0
CORRECTED pH
INITIAL pH 3
!-/ -0 /
CORRECTED pH �
f:00 N1
INITIAL pH I a,
f'
/l-1 -01
CORRECTED pH

CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # 1 REMOVE FROM BIN ! 1-17- 01
DATE P-1 y -y 1 Final % Solids ?3. O
TIME/
DATE
pH
> 12.01 3 DAYS
TEMP° C
52DEG. /12HRS.
SAMPLER
INITIAL
0 : q 5 Am
-o,tZ,
INITIAL pH THICKNER 5*1 ?9
1, uj
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CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN # REMOVE FROM BIN //- 4 -0 )
DATE // - l-0 I Final % Solids
TIME/
DATE
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CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
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CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
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CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
B1N # REMOVE FROM BIN //-30 - O/
DATE //4 d'-D / Final % Solids
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ALKALINE STABILIZATION PROCESS RECORD
PROCESS TO FURTHER REDUCE PATHOGENS PFRP
BIN #�_ REMOVE FROM BIN 1A4-o j
DATE /Q - Final % Solids
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CITY OF STATESVILLE
ALKALINE STABILIZATION PROCESS RECORD
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STA-LIME
INFORMATION
SHEET

.i
STA-LIME
PRODUCT INFORMATION AND USE GUIDE
itiIANUFACTURED BY THE CITY OF STATESVILLE
POST OFFICE BOX 1 1 1 1
STATESVILLE. NORTH CAROLINA 28687-111
AT THE
FOURTH CREEK WASTEIvVATER TREATMENT FACILITY
LOCATED ON BELL FARM ROAD IN IREDELL COUNTY
The City of Statesville manufactures Sta-Lime from dewatered municipal wastewater
sludge, cement kiln dust, and quicklime. These ingredients are blended together in a
stabilization process to produce a material valuable to the agricultural community as a soil
liming agent and minor macronucrient source. Sta-Lime meets the Environmental Protection
Agency's Part 503 sludge regulations, which apply co all municipal wastewater treatment
facilities and regulate production and quality of biosolids.
Sta-Lime is not sludge - it is a stabilized sludge product. Pathogenic bacteria are
destroyed by combining these three products in an EPA approved process so this valuable
product can be safely recycled on land. This process meecs the EPA 503 regulations for
Pathogen reduction through Alternative 2 and vector attraction reduction through Option 6.
The primary use of Sta-Lime is as an agricultural liming material. It reacts in the soil
root zone to adjust soil pH, improve soil productivity, and help provide optimum crop
production. The- additional nutrients .supplied may also help to reduce fertilizer costs for
Phosphorus and Potassium. Users of this product should review the following information on
Sta-Lime's lime value, nutrient content, application methods, and rates of application in order
to receive the maximum benefit from this valuable product.
STA-LI.1IE ALKALIYE LEMI G :MATERIAL DATA
Avera,2e Densicy:
Solids Concenc:
Mgr cu��ura� Limz Equivaiency
CaCo, Concenc:
Calcium Concenc:
Magnesium Concenc:
65 ^c_.7C,S foot
8 0 c
85 c
76.5 c
367 pounds per con
10 pounds per ton

STA-LINTE
PRODUCT ENFORMATION AND USE GUIDE
Page 2
STA-LDIE NIAJOR NUTREENT CONTENT
Plant Available Nitrogen
Phosphorus:
Potassium:
2.0 pounds per ton
6.5 pounds per ton
30.0 pounds per ton
APPLICATION RATE FOR STA-LLN E
The ratio of application for agricultural lime versus Sta-Lime is 1 : 1.5, meaning that
for every ton of agricultural lime normally applied, one and one-half tons of Sta-Lime should
be applied. For example, if a recent soil report recommends that 2 tons per acre of
agricultural Iime should be applied to a particular corn field, then 3 tons per acre of Sta-Lime
should be applied (2 X 1.5 = 3). Sta-Lime should be applied in the same manner as any
other agricultural soil amendment, such as fertilizer or agricultural lime, using the same
methods and procedures as one would for any farming operation which practices sound
environmental techniques, including the following:
• Application of Sta-Lime is prohibited except in accordance with instructions on this sheet.
• Maintain a 10' buffer between ,any Sta-Lime application site and any public or private
water supply source (including wells) and any stream, lake, or river.
• Do not apply Sta-Lime to any site that is flooded, frozen, or snow-covered.
• Provide adequate procedures to prevent surface runoff from carrying any Sta-Lime into
any surface waters.
• Take necessary steps to prevent wind erosion and surface runoff from carrying Sta-Lime
onto adjacent property or into any surface waters.
We look forward to continuing to provide you with this very beneficial product and
hope that you are pleased with its quality. We invite your comments or questions by writing
10 the above address, or by calling [phone].

Time Day.
so-
Class A Exceptional Quality Product
Loading Record
Date 19,W- Weather
Receiver's Name Address
City County State
Instructions for the use of this material and information as to its contents have been
provided to the receiving person.
Information provided here is correct and accurate to the best of my Imowledge.
Aclmowl ed. and Received by
(sign) Loaded by
e-

0,4 ce of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
Jack King
City of Statesville - Fourth Creek
P.O. Box 1111
Statesville, NC 28687-11
Dear Jack King,
February 2,1998
D E ...N= R
i
Subject: Annual Monitoring and Reporting Requirements
Distribution and Marketing or Surface Disposal
Permit Number: WQ0006245
City of Statesville - Fourth Creek
Iredell County
The purpose of this letter is a reminder that the monitoring reports required by the
subject permit must be submitted as an Annual Report for calendar year 1997 by no later than
March 1, 1998. The report must be submitted (in triplicate) to the following address:
DENR/DWQ/Water Quality Section
Non -Discharge Compliance Unit
P.O. Box 29535
Raleigh, N.C. 27626-0535
Due to limitations in storage space, please submit the reports in bound form rather than
in notebook form. Permittees are subject to civil penalty for failing to submit the Annual Report
as required by their permit.
Enclosed are the summary and certification sheets that must be used for your annual
report. Please complete these sheets and if necessary make copies of the blank forms if extras are
needed. The forms have not changed since last year, so you may use those you already have on
hand.
You will note that the forms include information required by EPA as outlined in 40 CFR
Part 503. Since the requirements of 40 CFR Part 503 are self implementing, they are legally .
binding and enforceable Federal requirements for all persons subject to the requirements of 40
CFR Part 503, even if these requirements are not currently contained in the state permit. The
annual reports for the EPA must be received by EPA at the following address on or before
Febuary 19,1998.
Melinda Green
Clean Water Act Enforcement Section
Water Programs Enforcement Branch
Water Management Division
U.S.EPA Region 4
61 Forsyth Street, S.W.
Atlanta, Ga. 30303-3104
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

Annual Monitoring and Reporting Requirements
WQ0006245
Page 2
If there is a need for any information or clarification on the State reporting requirements,
please do not hesitate to contact Kevin Barnett of our staff at 919-733-5083 extension 529. For
further information on the Federal requirements, you should call Vince Miller of the
Environmental Protection Agency at 404-562-9345.
Sincerely,
t, Dennis R. Ramsey
Assistant Chief for Non Discharge
Cc: Vince Miller, EPA Region IV
Mooresville Regional Supervisor
Compliance / Enforcement File
Central Files

:a
�,,.1A U 'tics �'., •:sJ'1�,.4,i'�
State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. Jack King, City Manager
City of Statesville
P.O. Box 1111
Statesville, NC 28687
Dear Mr. King:
Ar7,
1991
• RE�;uttAl. ©�icE
MAWRmom
[DEH N F=1
March 5, 1997
Subject: Permit No. WQ0006245
City of Statesville
Distribution of Class A Wastewater Residuals
Iredell County
In accordance with your application received on December 30, 1996, we are forwarding herewith
Permit No. WQ0006245, dated March 5, 1997, to the City of Statesville for the continued operation of a
wastewater residuals facility for the distribution of Class A residuals.
As requested in the City of Statesville's letter dated January 23, 1997 the Division has evaluated
the request for reduction of monitoring for the pathogen requirements and the pollutant concentrations.
The data shows that no violations have been found over the last two years and therefore the monitoring
frequency has been reduced to quarterly as requested.
This permit shall be effective from the date of issuance until February 28, 2002, shall void Permit
No. WQ0006245 issued June 6, 1994, and shall be subject to the conditions and limitations as specified
therein. Please pay particular attention to the monitoring and reporting requirements contained in this.
permit. Failure to establish an adequate system for collecting and maintaining the required operational
information will result in future compliance problems.
If any parts, requirements, or limitations contained in this permit are unacceptable, you have the
right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of
this permit. This request must be in the form of a written petition, conforming to Chapter 150B of North
Carolina General Statutes, and. filed with the Office of Administrative Hearings, P.O. Drawer 27447,
Raleigh, NC 27611-7447. Unless such demands are made this permit shall be final and binding.
If you need additional information concerning this matter, please contact Mr. Randy Kepler at
[phone] extension 544.
Sincerely,
xolo a2_ /,
A. Preston Howard, Jr., P.E.
cc: Iredell County Health Department
Mooresville Regional Office, Water Quality Section
w,-ater-Sectienw
Bob Cheek, Groundwater Section, Central Office
Training and Certification Unit, no change in rating
Facilities Assessment Unit
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX (919) .733-0719
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
RALEIGH
PERMIT FOR THE DISTRIBUTION OF CLASS A RESIDUALS
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
The City of Statesville
Iredell County
FOR THE
continued operation of a wastewater residuals facility for the distribution of Class A residuals consisting of
dewatered sludge from the Fourth Creek WWTP being transported by a conveyor belt from the Fourth
Creek filter press facilities to a 53 foot long covered, cleated feeder conveyor; two, 25 cubic yard sludge
storage hoppers (for dewatered Third Creek WWTP sludge and the Water Plant alum sludge) with bottom
screw conveyors to convey sludge from hopper to flanged connections above the 53 foot cleated, feeder
conveyor; a 25 foot long, 12 inch diameter twin screw sludge mixer; two, 12 foot diameter by 23 foot
straight wall (60 ton capacity) leg supported silos with variable speed volumetric feeders and a common
transfer screw conveyor to convey lime and/or kiln dust to the sludge mixer; a covered, cleated side wall
conveyor from the end of the sludge mixer to the truck loading station; appropriate nonleaking transport
truck(s) or approved equivalent to convey lime/kiln dust mixed sludge; protected pulse bins (where truck
loaded sludge will be dumped and allowed to heat for pathogen reduction); a 150 foot by 300 foot curbed
sludge curing asphalt slab for treated sludge mix to be put in windrows, allowed to continue to heat, and
then to dry including periodic turning with stormwater swale and drain system draining back to the
wastewater treatment facilities (walled and roofed pulse bins along the up slope 300 foot side of sludge
curing slab); all necessary measuring devices to ensure that each truck load of mixed sludge reaches a pH
of 12 for 2 hours and the temperature in the heated sludge is maintained at a minimum of 70 degrees C for
a minimum of 30 minutes and/or for measuring to ensure that all of the subject sludges meet the
requirements listed in Condition I.7; and all associated controls, support structures, piping, and
appurtenances for the distribution of approximately 3,900 dry tons per year of residuals from the sources
listed in Condition 112, to serve the City of Statesville, with no discharge of wastes to the surface waters,
pursuant to the application received on December 30, 1996, and in conformity with the project plan,
specifications, and other supporting data subsequently filed and approved by the Department of
Environment, Health and Natural Resources and considered a part of this permit.
This permit shall be effective from the date of issuance until February 28, 2002, shall void Permit
No. WQ0006245 issued June 6, 1994, and shall be subject to the following specified conditions and
limitations:
I. PERFORMANCE STANDARDS
1. The distribution of Class A residuals program shall be effectively maintained and operated
as a non -discharge system to prevent the discharge of any wastes resulting from the
operation of this program.

2. This permit shall become voidable in the event of failure of the residuals program to
adequately protect the assigned water quality standards of the surface waters and
groundwaters.
3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages
to surface or groundwaters resulting from the operation of this program.
4. In the event that the residuals program is not operated satisfactorily, including the creation
of nuisance conditions, the Permittee shall take any immediate corrective actions as may be
required by the Division.
5. Diversion or bypassing of the untreated residuals or leachate from the residual treatment
facilities is prohibited.
6. All leachate must be reused as a wetting agent for the processing of residuals or routed to
the head of the treatment plant.
7. When wastewater residuals are sold or given away, one of the Class A pathogen
requirements in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements
in 40 CFR Part 503.33 must be met. Additionally, an evaluation must be performed which
demonstrates the residuals ability to comply with this requirement. Upon request, a copy
of this evaluation must be submitted to the Assistant Chief, Technical Support Branch,
Division of Water Quality, Post Office Box 29535, Raleigh, NC 27626-0535.
In addition to the above, the Division has approved the following stabilization criteria for
the City of Statesville:
a. Lime/kiln dust mixed sludge reached a pH of 12 for 2 hours and the temperature in
the heated sludge is maintained at a minimum of 70' C for a minimum of 30 minutes.
b. N-Viro Soil Process
Alternative 1 Fine alkaline materials are uniformly mixed by mechanical mixing into
dewatered sludge to raise the pH to greater than 12 for seven days. The
dewatered sludge cake is then air dried (while pH remains above 12 for
at least seven days) through intermittent turning of windrows at least 30
days and until the solids levels reach and maintain a minimum of 65%
solids. A solids concentration of at least 60% is achieved before the pH
drops below 12. Mean temperature of the air surrounding the pile must
be above 50 C (41 o F) for the first seven days.
Alternative 2 Fine alkaline materials are uniformly mixed by mechanical mixing into
dewatered sludge to raise the pH to greater than 12 for at least 72 hours.
The sludge cake is then heated, while the pH exceeds 12, using
exothermic reactions or other thermal processes to achieve temperatures
of at least 520 C (126 F) throughout the sludge for at least 12 hours.
The stabilized sludge is then air dried (while the pH remains above 12
for at least three days) to at least 50% solids.
8. No residuals which tests, or is classified, as a hazardous or toxic waste under 40 CFR Part
261 shall be land applied or distributed and marketed.
H. OPERATION AND MAINTENANCE REQUIREMENTS
1. The residuals treatment facilities shall be properly maintained and operated at all times.
F?

i
2. No residuals other than the following are hereby approved for distribution in accordance
with this permit:
Permit Volume
Source
County
Number (Dry Tons/Year)
Fourth Creek WWTP
Iredell
NC0031836
Third Creek WWTP
Iredell
NC0020591 3,900*
Statesville Water Plant
Iredell
* A maximum of 3,900 dry tons per year of combined wastewater and alum residuals
3. All residuals shall be adequately stored to prevent leachate runoff until treated. The
finished product may be placed on a concrete pad, placed under shelter or covered until
such time as it is distributed to the buyer. The City of Statesville may also use the defunct
drying beds to store the finished product with all leachate routed to the wastewater
treatment facility. If an alternate storage site is to be used, approval must be obtained from
the Division of Water Quality.
4. No other residuals other than those specified under Condition II 2 above may be
distributed. The Permittee shall request and obtain a permit amendment from the Division
of Water Quality for each additional residual source prior to acceptance of that residual.
5. For a Class A residual to be sold or given away in bags or other container for application to
the land, the following must be satisfied:
The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Monthly
Average Concentrations (Dry Weight Basis) must be maintained:
Ceiling Monthly Average
Concentrations Concentrations
Parameters mg/kg m &g
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
6. Upon classification of the facility by the Certification Commission, the Permittee shall
employ a certified residuals operator to be in responsible charge (ORC) of the residuals
program. The operator must hold a certificate of the type classification assigned to the
residuals program by the Certification Commission. The Permittee must also employ a
certified back-up operator of the appropriate type to comply with the conditions of Title
15A NCAC 8A, .0202.
7. Adequate provisions shall be taken to prevent wind erosion and surface runoff from
conveying pollutants from the residuals treatment area onto the adjacent property or into
any surface waters.

8. A label shall be affixed to the bag or other container in which residuals that are sold or
given away for application to the land, or an information sheet shall be provided to the
person who receives the residuals sold or given away in an other container for application
to the land. The label or information sheet shall contain the following information:
a. The name and address of the person who prepared the residuals that is sold or given
away in a bag or other container for application to the land.
b. A statement .that application of the residuals to the land is prohibited except in
accordance with the instructions on the label or information sheet.
c. Information on all applicable buffers including a 10 foot buffer between application site
and any public or private water supply source (including wells) and any stream, lake,
or river.
d. Residuals shall not be applied to any site that is flooded; frozen or snow-covered.
e Adequate procedures shall be provided to prevent surface runoff from carrying any
disposed or stored residuals into any surface waters.
MONITORING AND REPORTING REQUIREMENTS
Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue
analyses) deemed necessary by the Division of Water Quality to insure protection of the
environment will be established and an acceptable sampling and reporting schedule shall be
followed.
2. Proper records shall be maintained by the Permittee tracking all residual activities. These
records shall include, but are not necessarily limited to the following information:
a. source, volume and analysis of each residuals
b. name of residuals' recipient, volume received, and intended use
3. A residual analysis shall be conducted quarterly from the date of permit issuance by the
Permittee. The results of all analysis shall be maintained on file by the Permittee for a
minimum of five years. The residuals analysis shall include the following parameters:
Arsenic Molybdenum
Cadmium Nickel
Copper Selenium
Lead Zinc
Mercury
Aluminum
pH
Ammonia -Nitrogen
Phosphorus
Calcium
Plant Available Nitrogen (by calculation)
Magnesium
Potassium
Nitrate -Nitrite Nitrogen
Sodium
% Total Solids
TKN
After the residuals have been monitored for two years at the above frequency, the Permittee
may submit a request to the Division for a permit modification for the reduction of the
frequency of monitoring for pollutant concentrations and for the pathogen density
requirements, but in no case shall the frequency of monitoring be less than once per year
when residuals are sold or given away.
In

0.
4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the
Permittee annually. The TCLP analysis shall include the following parameters (please note
the regulatory level in mg/L in parentheses):
Arsenic (5.0)
Benzene (0.5)
Carbon tetrachloride (0.5)
Chlorobenzene (100.0)
Chromium (5.0)
m-Cresol (200.0)
Cresol (200.0)
1,4-Dichlorobenzene (7.5)
1,1-Dichloroethylene (0.7)
Endrin (0.02)
I4exachlorobenzene (0.13)
Hexachloroethane (3.0)
Lindane (0.4).
Methoxychlor (10.0)
Nitrobenzene (2.0)
Pyridine (5.0)
Silver (5.0)
Toxaphene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,5-TP (Silvex) (1.0)
Barium (100.0)
Cadmium (1.0)
Chlordane (0.03)
Chloroform (6.0)
o-Cresol (200.0)
p-Cresol (200.0)
2,4-D (10.0)
1,2-Dichloroethane (0.5)
2,4-Dinitrotoluene (0.13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Lead (5.0)
Mercury (0.2)
Methyl ethyl ketone (200.0)
Pentachlorophenol (100.0)
Selenium (1.0) .
Tetrachloroethylene (0.7)
Trichloroethylene (0.5)
2,4,6-Trichlorophenol (2.0)
Vinyl chloride (0.2)
5. All residuals included in this permit must be monitored quarterly, from the date of permit
issuance, for compliance with condition 19 of this permit. Data to verify stabilization of
the residuals must be maintained by the Permittee. The required data is specific to the
stabilization process utilized, but should be sufficient to clearly demonstrate compliance
with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction
reduction requirements in 40 CFR Part 503.33. In addition, the EPA certification
statements concerning compliance with pathogen requirements, vector attraction reduction
requirements and management practices must be completed quarterly by the proper
authority or authorities if more than one is involved, either the person who generates the
residuals or the person who prepares the residuals to be sold or given away.
After the residuals have been monitored for two years at the above frequency, the Permittee
may request a permit modification for the reduction of the frequency of monitoring for
pollutant concentrations and for the pathogen density requirements, but in no case shall the
frequency of monitoring be less than once per year when residuals are sold or given away.
6. Three copies of all required monitoring and reporting requirements as specified in
conditions III 1, II12,11I 3, III 4, and 1115 shall be submitted annually on or before March
1 of the following year to the following address:
NC Division of Water Quality
Water Quality Section
Facility Assessment Unit
PO Box 29535
Raleigh, NC 27626-0535
5

7. Noncompliance Notification:
The Permittee shall report by telephone to the Mooresville Regional Office, telephone
number 704-663-1699, as soon as possible, but in no case more than 24 hours or on the
next working day following the occurrence or first knowledge of the occurrence of any of
the following:
a. Any occurrence with the distribution program which results in the land application of
significant amounts of wastes which are abnormal in quantity or characteristic.
b . Any failure of the distribution program resulting in a release of material to receiving
waters.
c. Any time that self -monitoring information indicates that the facility has gone out of
compliance with the conditions and limitations of this permit or the parameters on
which the system was designed.
d. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
e. Any spillage or discharge from a vehicle or piping system during transportation of
residuals.
Persons reporting such occurrences by telephone shall also file a written report in letter
form within five (5) days following first knowledge of the occurrence. This report must
outline the actions taken or proposed to be taken to ensure that the problem does not recur.
I V . GROUNDWATER REQUIREMENTS
1. Any groundwater quality monitoring, as deemed necessary by the Division, shall be
provided.
V . INSPECTIONS
The Permittee or his designee shall inspect the residuals storage, transport, and treatment
facilities to prevent malfunctions and deterioration, operator errors and discharges which
may cause or lead to the release of wastes to the environment, a threat to human health, or a
nuisance. The Permittee shall maintain an inspection log or summary including at least the
date and time of inspection, observations made, and any maintenance, repairs, or corrective
actions taken by the Permittee. This log of inspections shall be maintained by the Permittee
for a period of five years from the date of the inspection and shall be made available to the
Division of Water Quality or other permitting authority, upon request.
2. Any duly authorized officer, employee, or representative of the Division of Water Quality
may, upon presentation of credentials, enter and inspect any property, premises or place on
or related to the treatment site or facility at any reasonable time for the purpose of
determining compliance with this permit; may inspect or copy any records that must be kept
under the terms and conditions of this permit; and may obtain samples of groundwater,
surface water, or leachate.
X

V I . GENERAL CONDITIONS
1. This permit shall become voidable unless the distribution activities are carried out in
accordance with the conditions of this permit, the supporting materials, and in the manner
approved by this Division.
2. This permit is effective only with respect to the nature and volume of residuals described in
the application and other supporting data.
3. This permit is not automatically transferable. In the event that there is a desire for the
facilities to change ownership or a name change of the Permittee, a formal permit request
must be submitted to the Division of Water Quality accompanied by an application fee,
documentation from the parties involved, and other supporting materials as may be
appropriate. The approval of this request will be considered on its merits and may or may
not be approved.
4. Failure to abide by the conditions and limitations contained in this permit may subject the
Permittee to an enforcement action by the Division of Water Quality in accordance with
North Carolina General Statute 143-215.6(a) to 143-215.6(c).
5. The annual administering and compliance fee must be paid by the Permittee within thirty
(30) days after being billed by the Division. Failure to pay the fee accordingly may cause
the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205
(c)(4)•
6. The issuance of this permit does not preclude the Permittee from complying with any and
all statutes, rules, regulations, or ordinances which may be imposed by other government
agencies (local, state, and federal) which have jurisdiction.
7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its
extension. Upon receipt of the request, the Commission will review the adequacy of the
facilities described therein, and if warranted, will extend the permit for such period of time
and under such conditions and limitations as it may deem appropriate.
8. This permit may be modified, or revoked and reissued to incorporate any conditions,
limitations and monitoring requirements the Division of Water Quality deems necessary in
order to adequately protect the environment and public health.
Permit issued this the Fifth day of March, 1997
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
Preston Howard, Jr., P.A., Director
Division of Water Quality
By Authority of the Environmental Management Commission
Permit Number WQ0006245
7

Mate of North Carolina
Department of Environment,
Health and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
AW
f IN
Mr. Jack King, City Manager
City of Statesville
P.O. Box 1111
Statesville, NC 28687
Dear Mr. King:
03 V1%
1
C) E f--1 N F=1
March 5, 1997
Subject: Permit No. WQ0006245
City of Statesville
Distribution of Class A Wastewater Residuals
Iredell County
In accordance with your application received on December 30, 1996, we are forwarding herewith
Permit No. WQ0006245, dated March 5, 1997, to the City of Statesville for the continued operation of a
wastewater residuals facility for the distribution of Class A residuals.
As requested in the City of Statesville's letter dated January 23, 1997 the Division has evaluated
the request for reduction of monitoring for the pathogen requirements and the pollutant concentrations.
The data shows that no violations have been found over the last two years and therefore the monitoring
frequency has been reduced to quarterly as requested.
This permit shall be effective from the date of issuance until February 28, 2002, shall void Permit
No. WQ0006245 issued June 6, 1994, and shall be subject to the conditions and limitations as specified
therein. Please pay particular attention to the monitoring and reporting requirements contained in this
permit. Failure to establish an adequate system for collecting and maintaining the required operational
information will result in future compliance problems.
If any parts, requirements, or limitations contained in this permit are unacceptable, you have the
right to request an adjudicatory hearing upon written request within thirty (30) days following receipt. of
this permit. This request must be in the form of a written petition, conforming to Chapter 150B of North
Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447,
Raleigh, NC 27611-7447. Unless such demands are made this permit shall be final and binding.
If you need additional information concerning this matter, please contact Mr. Randy Kepler at
[phone] extension 544.
Sincerely,
x�o ate -- /,--
A. Preston Howard, Jr., P.E.
cc: Iredell County Health Department
aM-o gion e • uah, �ctivn
Mooresville Regional Office, Groundwater. Section
Bob Cheek, Groundwater Section, Central Office
Training and Certification Unit, no change in rating
Facilities Assessment Unit
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
RALEIGH
PERMIT FOR THE DISTRIBUTION OF CLASS A RESIDUALS
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
The City of Statesville
Iredell County
FOR THE
continued operation of a wastewater residuals facility for the distribution of Class A residuals consisting of
dewatered sludge from the Fourth Creek WWTP being transported by a conveyor.belt from the Fourth
Creek filter press facilities to a 53 foot long covered, cleated feeder conveyor; two, 25 cubic yard sludge
storage hoppers (for dewatered Third Creek WWTP sludge and the Water Plant alum sludge) with bottom
screw conveyors to convey sludge from hopper to flanged connections above the 53 foot cleated, feeder
conveyor; a 25 foot long, 12 inch diameter twin screw sludge mixer; two, 12 foot diameter by 23 foot
straight wall (60 ton capacity) leg supported silos with variable speed volumetric feeders and a common
transfer screw conveyor to convey lime and/or kiln dust to the sludge mixer; a covered, cleated side wall
conveyor from the end of the sludge mixer to the truck loading station; appropriate nonleaking transport
truck(s) or approved equivalent to convey lime/kiln dust mixed sludge; protected pulse bins (where truck
loaded sludge will be dumped and allowed to heat for pathogen reduction); a 150 foot by 300 foot curbed
sludge curing asphalt slab for treated sludge mix to be put in windrows, allowed to continue to heat, and
then to dry including periodic turning with stormwater swale and drain system draining back to the
wastewater treatment facilities (walled and roofed pulse bins along the up slope 300 foot side of sludge
curing slab); all necessary measuring devices to ensure that each truck load of mixed sludge reaches a pH
of 12 for 2 hours and the temperature in the heated sludge is maintained at a minimum of 70 degrees C for
a minimum of 30 minutes and/or for measuring to ensure that all of the subject sludges meet the
requirements listed in Condition I.7; and all associated controls, support structures, piping, and
appurtenances for the distribution of approximately 3,900 dry tons per year of residuals from the sources
listed in Condition R 2, to serve the City of Statesville, with no discharge of wastes to the surface waters,
pursuant to the application received on December 30, 1996, and in conformity with the project plan,
specifications, and other supporting data subsequently filed and approved by the Department of
Environment, Health and Natural Resources and considered a part of this permit.
This permit shall be effective from the date of issuance until February 28, 2002, shall void Permit
No. WQ0006245 issued June 6, 1994, and shall be subject to the following specified conditions and
limitations:
I. PERFORMANCE STANDARDS
1. The distribution of Class A residuals program shall be effectively maintained and operated
as a non -discharge system to prevent the discharge of any wastes resulting from the
operation of this program.
- ---1

2. This permit shall become voidable in the event of failure of the residuals program to
adequately protect the assigned water quality standards of the surface waters and
groundwaters.
3. The issuance of this permit shall not relieve the Permittee of the responsibility for damages
to surface or groundwaters resulting from the operation of this program.
4. In the event that the residuals program is not operated satisfactorily, including the creation
of nuisance conditions, the Permittee shall take any immediate corrective actions as may be
required by the Division.
5. Diversion or bypassing of the untreated residuals or leachate from the residual treatment
facilities is prohibited.
6. All leachate must be reused as a wetting agent for the processing of residuals or routed to
the head of the treatment plant.
7. When wastewater residuals are sold or given away, one of the Class A pathogen
requirements in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements
in 40 CFR Part 503.33 must be met. Additionally, an evaluation must be performed which
demonstrates the residuals ability to comply with this requirement. Upon request, a copy
of this evaluation must be submitted to the Assistant Chief, Technical Support Branch,
Division of Water Quality, Post Office Box 29535, Raleigh, NC 27626-0535.
In addition to the above, the Division has approved the following stabilization criteria for
the City of Statesville:
a. Lime/kiln dust mixed sludge reached a pH of 12 for 2 hours and the temperature in
the heated sludge is maintained at a minimum of 70' C for a minimum of 30 minutes.
b. N-Viro Soil Process
Alternative 1 Fine alkaline materials are uniformly mixed by mechanical mixing into
dewatered sludge to raise the pH to greater than 12 for seven days. The
dewatered sludge cake is then air dried (while pH remains above 12 for
at least seven days) through intermittent turning of windrows at least 30
days and until the solids levels reach and maintain a minimum of 65%
solids. A solids concentration of at least 60% is achieved before the pH
drops below 12. Mean temperature of the air surrounding the pile must
be above 5° C (41 OF) for the first seven days.
Alternative 2 Fine alkaline materials are uniformly mixed by mechanical mixing into
dewatered sludge to raise the pH to greater than 12 for at least 72 hours.
The sludge cake is then heated, while the pH exceeds 12, -using
exothermic reactions or other thermal processes to achieve temperatures
of at least 520 C (126 F) throughout the sludge for at least 12 hours.
The stabilized sludge is then air dried (while the pH remains above 12
for at least three days) to at least 50% solids.
8. No residuals which tests, or is classified, as a hazardous or toxic waste under 40 CFR Part
261 shall be land applied or distributed and marketed.
H. OPERATION AND MAINTENANCE REQUIREMENTS
The residuals treatment facilities shall be properly maintained and operated at all times.
2

2. No residuals other than the following are hereby approved for distribution in accordance
with this permit:
Permit Volume
Source County Number Mry Tons/Year)
Fourth Creek WWTP Iredell NC0031836
Third Creek WWTP Iredell NC0020591 3,900*
Statesville Water Plant Iredell
A maximum of 3,900 dry tons per year of combined wastewater and alum residuals
3. All residuals shall be adequately stored to prevent leachate runoff until treated. The
finished product may be placed on a concrete pad, placed under shelter or covered until
such time as it is distributed to the buyer. The City of Statesville may also use the defunct
drying beds to store the finished product with all leachate routed to the wastewater
treatment facility. If an alternate storage site is to be used, approval must be obtained from.
the Division of Water Quality.
4. No other residuals other than those specified under Condition II 2 above may be
distributed. The Permittee shall request and obtain a permit amendment from the Division
of Water Quality for each additional residual source prior to acceptance of that residual.
5. For a Class A residual to be sold or given away in bags or other container for application to
the land, the following must be satisfied:
The Ceiling . Concentrations (Dry Weight Basis) and the Pollutant Monthly
Average Concentrations (Dry Weight Basis) must be maintained:
Ceiling Monthly Average
Concentrations Concentrations
Parameters mg1a mg/kg
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
6. Upon classification of the facility by the Certification Commission, the Permittee shall
employ a certified residuals operator to be in responsible charge (ORC) of the residuals
program. The operator must hold a certificate of the type classification assigned to the
residuals program by the Certification Commission. The Permittee must also employ a
certified back-up operator of the appropriate type to comply with the conditions of Title
15A NCAC 8A, .0202.
7. Adequate provisions shall be taken to prevent wind erosion and surface runoff from
conveying pollutants from the residuals treatment area onto the adjacent property or into
any surface waters.
3

8. A label shall be affixed to the bag or other container in which residuals that are sold or
given away for application to the land, or an information sheet shall be provided to the
person who receives the residuals sold or given away in an other container for application
to the land. The label or information sheet shall contain the following information:
a. The name and address of the person who prepared the residuals that is sold or given
away in a bag or other container for application to the land. .
b. A statement that application of the residuals to the land is prohibited except in
accordance with the instructions on the label or information sheet.
c. Information on all applicable buffers including a 10 foot buffer between application site
and any public or private water supply source (including wells) and any stream, lake,
or river.
d . Residuals shall not be applied to any site that is flooded, frozen or snow-covered.
e Adequate procedures shall be provided to prevent surface runoff from carrying any
disposed or stored residuals into any surface waters.
MONITORING AND REPORTING REQUIREMENTS
Any monitoring (including groundwater, surface water, residuals, soil, or plant tissue
analyses) deemed necessary by the Division of Water Quality to insure protection of the
environment will be established and an acceptable sampling and reporting schedule shall be
followed.
2. Proper records shall be maintained by the Permittee tracking all residual activities. These
records shall include, but are not necessarily limited to the following information:
a. source, volume and analysis of each residuals
b . name of residuals' recipient, volume received, and intended use
3 . A residual analysis shall be conducted quarterly from the date of permit issuance by the
Permittee. The results of all analysis shall be maintained on file by the Permittee for a
minimum of five years. The residuals analysis shall include the following parameters:
Arsenic Molybdenum
Cadmium Nickel
Copper Selenium
Lead Zinc
Mercury
Aluminum
pH
Ammonia -Nitrogen
Phosphorus
Calcium
Plant Available Nitrogen (by calculation)
Magnesium
Potassium
Nitrate -Nitrite Nitrogen
Sodium
% Total Solids
TKN
After the residuals have been monitored for two years at the above frequency, the Permittee
may submit a request to the Division for a perriiit modification for the-Teduction of the
frequency of monitoring for pollutant concentrations and for the pathogen density
requirements, but in no case shall the frequency of monitoring be less than once per year
when residuals are sold or given away.
M

4. A Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the
Permittee annually. The TCLP analysis shall include the following parameters (please note
the regulatory level in mg/L in parentheses):
Arsenic (5.0)
Benzene (0.5)
Carbon tetrachloride (0.5)
Chlorobenzene (100.0)
Chromium (5.0)
m-Cresol (200.0)
Cresol (200.0)
1,4-Dichlorobenzene (7.5)
1,1-Dichloroethylene (0.7)
Endrin (0.02)
Hexachlorobenzene (0.13)
Hexachloroethane (3.0)
Lindane (0.4)
Methoxychlor (10.0)
Nitrobenzene (2.0)
Pyridine (5.0)
Silver (5.0)
Toxaphene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,5-TP (Silvex) (1.0)
Barium (100.0)
Cadmium (1.0)
Chlordane (0.03)
Chloroform (6.0)
o-Cresol (200.0)
p-Cresol (200.0)
2,4-D (10.0)
1,2-Dichloroethane (0.5)
2,4-Dinitrotoluene (0.13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Lead (5.0)
Mercury (0.2)
Methyl ethyl ketone (200.0)
Pentachlorophenol (100.0)
Selenium (1.0)
Tetrachloroethylene (0.7) .
Trichloroethylene (0.5)
2,4,6-Trichlorophenol (2.0)
Vinyl chloride (0.2)
5. All residuals included in this permit must be monitored quarterly, from the date of permit
issuance, for compliance with condition 19 of this permit. Data to verify stabilization of
the residuals must be maintained by the Permittee. The required data is specific to the
stabilization process utilized, but should be sufficient to clearly demonstrate compliance
with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction
reduction requirements in 40 CFR Part 503.33. In addition, the EPA certification
statements concerning compliance with pathogen requirements, vector attraction reduction
requirements and management practices must be completed quarterly by the proper
authority or authorities if more than one is involved, either the person who generates the
residuals or the person who prepares the residuals to be sold or given away.
After the residuals have been monitored for two years at the above frequency, the Permittee
may request a permit modification for the reduction of the frequency of monitoring for
pollutant concentrations and for the pathogen density requirements, but in no case shall the
frequency of monitoring be less than once per year when residuals are sold or given away.
6. Three copies of all required monitoring and reporting requirements as specified in
conditions III 1, III 2, III 3, III 4, and III 5 shall be submitted annually on or before March
1 of the following year to the following address:
NC Division of Water Quality
Water Quality Section
Facility Assessment Unit
PO Box 29535
Raleigh, NC 27626-0535
5

7. Noncompliance Notification:
The Permittee shall report by telephone to the Mooresville Regional Office, telephone
number 704-663-1699, as soon as possible, but in no case more than 24 hours or on the
next working day following the occurrence or first knowledge of the occurrence of any of
the following:
a. Any occurrence with the distribution program which results in the land application of
significant amounts of wastes which are abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to receiving
waters.
c. Any time thatself-monitoring information indicates that the facility has gone out of
compliance with the conditions and limitations of this permit or the parameters on
which the system was designed.
d . Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
e. Any spillage or discharge from a vehicle or piping system during transportation of
residuals.
Persons reporting such occurrences by telephone shall also file a written report in letter
form within five (5) days following first knowledge of the occurrence. This report must
outline the actions taken or proposed to be taken to ensure that the problem does not recur.
I V . GROUNDWATER REQUIREMENTS
Any groundwater quality monitoring, as deemed necessary by the Division, shall be
provided.
V . _ INSPECTIONS
The Permittee or his designee shall inspect the residuals storage, transport, and treatment
facilities to prevent malfunctions anddeterioration, operator errors and discharges which
may cause or lead to the release of wastes to the environment, a threat to human health, or a
nuisance. The Permittee shall maintain an inspection log or summary including at least the
date and time of inspection, observations made, and any maintenance, repairs, or corrective
actions taken by the Permittee. This log of inspections shall be maintained by the Permittee
for a period of five years from the date of the inspection and shall be made available to the
Division of Water Quality or other permitting authority, upon request.
2. Any duly authorized officer, employee, or representative of the Division of Water Quality
may, upon presentation of credentials, enter and inspect any property, premises or place on
or related to the treatment site or facility at any reasonable time for the purpose of
determining compliance with this permit; may inspect or copy any records that must be kept
under the terms and conditions of this permit; and may obtain samples of groundwater,
surface water, or leachate.
Al

V I. GENERAL CONDITIONS
1. This permit shall become voidable unless the distribution activities are carried out in
accordance with the conditions of this permit, the supporting materials, and in the manner
approved by this Division.
2. This permit is effective only with respect to the nature and volume of residuals described in
the application and other supporting data..
3. This permit is not automatically transferable. In the event that there is a desire for the
facilities to change ownership or a name change of the Permittee, a formal permit request
must be submitted to the Division of Water Quality accompanied by an application fee,
documentation from the parties involved, and other supporting materials as may be
appropriate. The approval of this request will be considered on its merits and may or may
not be approved.
4. Failure to abide by the conditions and limitations contained in this permit may subject the
Permittee to an enforcement action by the Division of Water Quality in accordance with
North Carolina General Statute 143-215.6(a) to 143-215.6(c).
5 The annual administering and compliance fee must be paid by the Permittee within thirty
(30) days after being billed by the Division. Failure to pay the fee accordingly may cause
the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205
(c)(4).
6. The issuance of this permit does not preclude the Permittee from complying with any and
all statutes, rules, regulations, or ordinances which may be imposed by other government
agencies (local, state, and federal) which have jurisdiction.
7. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its
extension. Upon receipt of the request, the Commission will review the adequacy of the
facilities described therein, and if warranted, will extend the permit for such period of time
and under such conditions and limitations as it may deem appropriate.
8. This permit may be modified, or revoked and reissued to incorporate any conditions,
limitations. and monitoring requirements the Division of Water Quality deems necessary in
order to adequately protect the environment and public health.
Permit issued this the Fifth day of March, 1997
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
) W-lo aa/— - ..
-
. Preston Howard, Jr., P.A., Director
Division of Water Quality
By Authority of the Environmental Management Commission
Permit Number WQ0006245
7

State of North Carolina
it Department of Environment,
Health and Natural Resources 1 • •
Mooresville Regional Office
James B. Hunt, Jr., Governor ®E H N FZ
Jonathan B. Howes, Secretary
DIVISION OF WATER QUALITY
March 6, 1997
Mr. Jack King, City Manager
City of Statesville
Post Office Box 1111
Statesville, North Carolina 28687
Subject: Permit No. WQ0006245
City of Statesville
Distribution of Class A
Wastewater Residuals
Iredell County, NC
Dear Mr. King:
Our records show that Permit No. WQ0006245 was issued on
March 5, 1997 for the distribution of Class A wastewater
residuals generated by your wastewater treatment facility. The
purpose of this letter is to advise you of the importance of the
Permit and the liabilities in the event of failure to comply
with the terms and conditions of the Permit. If you have not
already done so, it is requested that you and other appropriate
employees thoroughly read the Permit.
The Permit sets forth specific performance standards,
operation and maintenance requirements, monitoring requirements,
including annual reporting and groundwater monitoring activities
to be performed by the Permittee, plus general conditions
applicable to non -discharge permits. Failure to comply with the
terms and conditions of the Permit subjects the Permittee to
enforcement action pursuant to Section 143-215.6 of the North
Carolina General Statutes. A civil penalty of up to $10,000 per
violation may be assessed for such violations.
Please note that the subject Permit expires on February 28,
2002. Part VI, No. 7 of the Permit requires that a renewal
request be submitted at least six (6) months prior to
expiration. Also the Permit is non -transferable until such time
that the Permittee has requested a name change to the new.
Permittee.
919 North Main Street, 4C FAX [phone]
Mooresville, North Carolina 28115 An Equal Opportunity/Affirmative Action Employer
Voice 704-663-1699 50% recycled/10% post -consumer paper

0
Mr. Jack King
March 6, 1997
Page Two
As mentioned previously, the purpose of this letter is to
advise you of the importance of your Permit. Please read the
Permit and contact this Office at 704/663-1699 in Mooresville if
you have any questions or need clarification. We look forward
to providing any assistance.
Sincerely,
2 D. Rex Gleason, P. E.
Water Quality Regional Supervisor

MEMO
TO:
From:
DATE: -?/I '?/cl .?
SUBJECT:
If, STATE o
North Carolina Department of Environment,
Health, and Natural Resources eo printed on Recycled Paper

f I i
•t U4,
a les We
V. ' 4Tox-�Natrouille, Nort4 Qrolina 28687
March 11, 1997
Mr. D. Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional Office
919 North Main Street
Mooresville, NC 28115
Re: Follow Up to Report of Non -Compliance
Distribution of Class A Residuals Permit
Permit No. WQ0006245
Iredell County
Dear Mr. Gleason:
y
NATI �DUIPES
MAR 1 1997
MVlSIqP11 a ' lL 'mi;itr
l-VOWESILV P{%IU-10 t OK
As a follow up to our February 28, 1997 report of non-compliance, we have
completed the TCLP analysis for our Class A material. Please find enclosed a copy of the
results.
Should you require any additional information, please contact me at 878-3438.
Sincerely,
eh",
Renee Parkman, Asst. Director
Water/Wastewater Treatment
RP/sg
Enclosure

lab, Report
Fi'oi m : NC Cert i f i r.,af i nn Nn A_017
SC Certification No. 99012
NC Drinking Water Cart. No. 37735
FL Certification No. E87519
March 10, 1997
To; City of Statesville
Attn: Me. Carol Rogers
P.O. Box lilt
Statesville, HC 28687
Full Servlce Analytical & Environmental SOlutionS
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample T�D, AA64547 Customer Code: STATESVI
Login Group *: 2255C1 Customer Reference: 7232-1
Phone Humber: [phone]/Fax[phone]
Customer Sample I.D*: STALIME
Sample collection date: 02/28/97 Time: 15:00
Lab submittal date: 03/03/97 Time: 08:30
Received by: SMV Validated by: ADO
Parameter: TCLP EXTRACTION (VOLATILES ONLY)
Method reference: 1311 Unit;
Result: Completed MDL or sensitivity:
Date started; 03/05/97 Date finished: 03/06/97
Time started: 14:00 Analyst: DRR
Parameter: METALS DIGESTION
Method reference: EPA 3010
Result: Completed
Date started: 03/06/97
Time started: 10:45
Parame-ter : PREP. METHOD- 3510
Method reference: 3510
Result: Completed
Date started: 03/06/97
Time started: 10:45
Unit:
MDL or sensitivity:
Date finished: 03/06/97
Analyst; JAM
Unit.-
MDL or sensitivity:
Data finished: 03/06/97
Analyst: DRR
Parameter: PREP. METHOD 3510 WITH EXCHANGE
Method reference; 3510 Unit:
Result: Completed MDL or sensitivity:
Date started: 03/05/97 Date finished: 03/07/97
Time started: 20:00 Analyst:
Parameter: PREP. METHOD 3510 WITH EXCHANGE
Method reference: 3510 Unit:
Result: Completed
Date ota.rted : 03/05/97
Time started:
MDL or sensitivity:
Date fl-niched: 02/05/97
Analyst: SA
449 9pringbrook Road &. PA. Box 240543 A, Charlotte, NC 28224-0543
Phone, 704/529.6364 A. Toil Free Number; 1-800/529-6364 ,L. Fax. [phone]

4ab Report
City of Statesville
Page: 2
March 10, 1997
Sample I. D. AA64547 (continued)
Full Service Analytical & Environmental Solutions
Parameter: ARSENIC, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time started: 09:00
Parameter: SELENIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started:03/0'7/97
Time started: 09:00
Parameter: CADMIUM, LEACHABLE
Method reference: Selo
Result: Leas. than
Date started: 03/07/97
Time started: 09:00
Parameter: CHROMIUM, LEACHABLE
Method reference; 6010
Renault: Less than
Date started: 03/07/97
Time started; 09:00
Parameter: LEAD, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time started: 09:00
Parameter: SILVER, LEACHABLE
Method reference; 6010
Result: Less than
Date started: 03/07/137
Time started: 09:00
Parameter: MERCURY, LEACHABLE
[[a4• he�ri r•o�arorno • 7d71
Result: Less than
Date started; 03/04/97
Time started: 14:00
Parameter: BARIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started; 03/07/97
Time started: 09:00
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/07/97
Analyst: DHJ
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/07/97
Analyst: DRJ
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/07/97
Analyst: DHJ
Unit; mg/L
MDL or sensitivity: 0.50
Date finished: 03/07/97
Analyst: DHJ
Unit: mg/L
MILL or sensitivity: 0.30
Date finished: 03/07/97
Analyst: DHJ
Unit; mg/L
MDL or sensitivity., 0.50
Date finished: 03/07/97
Analyst: DH-7
11n4t.
MDL or sensitivity. 0.102
Date finished: 03/04/97
Analyst: LAS
Unit: mg/L
MDL or sensitivity: 10.00
Date finished: 03/07/97
Analyst: DHJ
Parameter: TCLP VOLATILES BY 8240
Method reference: SW846--8240 Unit: mg/L
Result: see below.
Date started: 03/06/97 Date finished: 03/06/97
Time started: 14:58 Analyst: HP
449 Springbrook Road P.O. BOX 240543 & Charlotte, NC 28224-0543

Lab, Report
City of Statesville Sample I. D. AA64547 (oontinued)
Page: 3
a I 3hh a,:
March 10, 1997
Full Service Analytical & Environmental Solutions
Parameter: TCLP SEMI-VOLATILES BY 8270
Method reference: 8270 Unit: mg/L
Result: see below
Date started: 03/06/97 Date finished: 03/06/97
Time aterted:`17:40 Analyst: MP
Parameter; TCLP PESTICIDES
Method reference:
Result: see below
Date startedt 03/07/97
Time started: 08:23
Parameter: TCLP HERBICIDES
Method reference;
Result: see below
Date started; 03/07/97
Time started:
Parameter: MERCURY DIGESTION
Method reference: 7471
Resultt Completed
Date started: 03/04/97
Time started: 09:45
Parameters TCLP EXTRACTION
Method reference: 1311
Results Completed
Date started: 03/03/97
Time startedi 16:00
Data for TCLP VOLATILES BY 8240 mg/L:
Component dame
BENZENE
CARBON TETRACHLORIDE
CHLOROSENZENE
CHLOROFORM
1,4-DICHLOROBENZENE
1,2-DICHLOROETHANE
1, 1-DICHLOROETHENE-
METHYL ETHYL KETONE
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE -
Unit; mg/L
?ate finished: 03/07/97
Analyst: HWC
Unit: mg/L
Date f i.nished : 03/07/97.
Analyst: SA
Unit:
MDL or sensitivity:
Date finished; 03/04/97
Analyst: LAS
Units
MDL or sensitivity:
Date finished: 03/04/97
Analyst: DHJ
Result
Not detected
Not detected
Not detected
Not detected
Not .detected
Not detected
Not detected
Not detected
Not detracted
Not detected
Not detected
Data for TCLP SEMI-VOLATILES BY 8270 mg/L:
Component MDL
0.01
0.01
0.01
0.01
0,014
0.01
0.01
0.04
0.012
0.01
0.02
Component Name Result Component MDL
CRES0LS ,' Not detected 0.050
1,4-DICHLOROBENZENE Not detected 0.050
2,4-DINITROTOLUENE' Not detected 0,012
HEXACHLOROBENZENE Not detected 0.010
449 Springbrook Road A. P.O. Box 240543 & Charlotte, NC 28224-0543
Phone; 704/529-6364 ,& Toll Free Number: 1-800/529-6364 ..►. Fax: [phone]M

Lab Report
City of Statesville Sampler I.D. AAE4547 (continued)
Page: 4
March 10, 1997
F20 Service Analytical & Environmentai $ojuti0ns
flats f'n,r TM ATTI Cc my o'77M ',.���
Component Name
HEXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
PYRIDINE
2, 4, 5- TRI CHLOROPHENOL
2, 4, 6-TRICHLOROPHENOL
Data for TCLP PESTICIDES :n>g/L:
Component Name
CHLORDANE
ENDRIN
HEPTACHLOR
HEPTACHLOR EPDXIDE
LINDANE
METHOXYCHLOR
TOXAPHENE
Data for TCLP HERBICIDES mg/L:
Component Name
2t 4-D
SILVEX
Sample commentat
Result
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Result
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Result
Not detected
Not detected
TCLP herbicides subcontracted to XC certified lab # 387.
Component WDL
0.050
0.050
0.050
0.25
0.25
0.25
0.10
Component XDL
0.015
0.010
0.005
0.005
0.2
1.0
0.25
Component NDL
5.0
0.5
If there are any questions regarding this data, please call.
Angela D. Overcash
Laboratory Director
449 Springbrook Road & P.O, Box 240543 w Charlotte, NC 28224-0543 -
Phone: [phone] a. Toll Free Number: 1-600/529-6364 � Fax: [phone]Q

CMAIM OF CUSTODY RECORD •
PACE to Sampft 10ACT upon an*Wl, YES !JD NdR
4 449 SprIngbiroolk ROad-AktharbIle. NC 282117
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State of North Carolina
Department of Environment,
Health and Natural Resources
Mooresville Regional Office
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
DIVISION OF WATER QUALITY
March 13, 1997
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. Jack King, City Manager
City of Statesville
Fourth Creek Monofill
P.O. Box 1111
Statesville, NC 28687-1111
Subject: Notice of Violation
Permit Condition, Part III (4)
Distribution of Class A Residuals
Permit No. WQ0006245
Iredell County
Dear Mr. King:
The City of Statesville was issued Permit No. WQ0006245, effective June 6, 1994, to
distribute Class A residuals. Part III, Condition 4 of the Permit requires that "a toxicity
characteristics leaching procedure (TCLP) analysis shall be conducted by the Permittee
annually". The City's Annual Report, received March 5, 1997, indicated that no such procedure
was filed, which is a violation of the above permit condition and North Carolina General Statute
(NCGS) 143-215.1. The City also indicated in a letter from Ms. Renee Parkman dated February
28, 1997, that the City is in the processes of conducting a TCLP analysis and will forward the
results as soon as they are available.
It is requested that a written response be submitted to the attention of Mr. D. Rex
Gleason, Water Quality Regional Supervisor, by no later than March 26, 1997. Also, North
Carolina General Statute (NCGS) 143-215.6A provides for a civil penalty assessment of not
more than ten thousand dollars ($10,000.00) per violation per day against any person who
919 North Main Street,
Mooresville, North Carolina 28115
Voice 704-663-1699
1
FAX [phone]
An Equal Opportunity/Affirmative Action Employer
50% recycled/10% post -consumer paper

d SENDER:
1
v ■Complete items 1 and/or 2 for additional services.
w ■Complete items 3, 4a, and 4b.
I also Wish to receive the
following services (for an
Y Print your name and address on the reverse of this form so that we can return this card to you. extra fee):
> ■Attach this form to the front of the mailpiece, or on the back if space does not
permit. 1. ❑ Addressee's Address
am ■Write°Return Receipt Requested' on the mailpiece below the article number.
■The Return Receipt will show to whom the article was delivered and the date 2 ❑Restricted Delivery
c delivered.
O
Consult postmaster for fee.
0 3. Article Addressed to:
4a. Article Number
v MR JACK KING, CITY MANAGER
P 431 483 315
`n
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FOURTH CREEK
4b. Service Type
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5. Received By: (Print Name)
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6. Signature:-( ddressee or Agent)
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Mr. Jack King
March 13, 1997
page 2
violates or fails to act in accordance with the terms, conditions, or requirements of any permit
issued pursuant to NCGS 143-215.1. Should a decision be made to pursue enforcement, you will
be advised in separate correspondence.
If you have questions, please do not hesitate to contact Mr. Todd St. John, Mr. Rex
Gleason (Water Quality Regional Supervisor), or me at 704/663-1699.
Sincerely,
B. Keith Overcash, P.E.
Regional Supervisor
cc: Mr. Bob Sledge, DWQ

r3
1,76 /+ff
GENERAL INFORMATION
SLUDGE STABILIZATION REPORT
CALENDAR YEAR 1996
.N.C. DT''i: of
rrATUk—SAL I:LSGU2C!rS
MAR 5 1 7�
DIVISION Gf
FACILITY NAME: Fourth Creek WWTP-NPDES NC0031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P. O. Box 1111
Statesville, NC 28687-1111
704-878-3438
RESPONSIBLE OFFICIAL:
L. F. "Joe" Hudson, Jr., Director
Water/Wastewater Treatment
P. O. Box 1111
Statesville, NC 28687-1111
704-878-343 8
FACILITY OPERATOR:
Harold Anderson
Plant Manager
P. O. Box 1111
Statesville, NC 28687-1111
7
APPLICATION: 04-878-343 8
Class A Exceptional Quality product. Test data and
summary of operations attached.
R E D
AR, 33 1997
EACILMES ASSE SNIENT UNIT

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
FACILITY NAME FcAAC, A L
_ �J- ciZtk�PERMIT #
FACILITY TYPE (please check one): COUNTY
�] Surface Disposal (complete Part A (Source(s) and "Residual IN" Volume only) and Part C) y
Q Distribution and Marketing (complete Parts A, B, and C)
WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? �/ YES
NO. If NO, skip Parts A, B, and C and certify form below.
Part A`
Sources(s) VPart Bk
Volume (dry tons)
Month (include NPDES 11 it applicable) Admendment/ Recipient Information
nulkin Agent INName(s) Volume Intended use(s)
9 9 ��ReskdUallN Product January dry tons
February
March
April
May
June
July
August
September
October
November
December
Totals: Annual (dry t
Admendment(s) used:
Bulking Agent(s) used:
If more space is required than given, please use the comment space provided below or attach additional sheet(s).] Check box if additional sheet(s) are attached.
Comments:
Part C
-----------------------------------------------------------------------------
Facility was compliant during calendar year 1996 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Environmental Management _ YES _�/_NO. If NO, please provide a written desription why the facility was not compliant.
1. All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached.
2. All operations and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Environmental Management.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT
THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR KNOWING VIOLATIONS."
- /
SIGNATURE OF PERMITTEE DATE------^� 4-mot
------------- ---
SIGNATURE OF'PREPARER' DATE
(if different from Permittee) 'Preparer is defined in 40 CFR Part 503.9(r)

Cott
. (�. fax 1111 • 3tatesuille, Nartll Carolina 20687
February 28, 1997
Mr. D. Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional Office
919 North Main St.
Mooresville, NC 28115
Re: Report of Non -Compliance
Distribution of Class A Residuals Permit
Permit No. WQ0006245
Iredell County
Dear Mr. Gleason:
As I reported to Mr. Todd St. John on February 28, 1997, we were non -compliant with
the referenced permit for 1996. The permit requires that an annual TCLP analysis be conducted
on the Class A material. We failed to perform this analysis for 1996.
We are currently in the process of having a TCLP run on our Class A product and will
forward the results to you as soon as they are available. We have taken measure in house to
prevent any further compliance problems.
Should you require any additional information, please contact me at 878-3438.
Sincerely,
Renee Parkman, Asst. Director
Water/Wastewater Treatment

FOURTH CREEK ALKALINE STABILIZATION FACILITY
Stalime Class A Exceptional Quality Product
Table 1 - Annual Production Distributions Report
Dry Metric Tons
1996
Month Biosolids Alkaline Product Product
1996 Feed Feed Total Distributed
January
271.67
379.59
651.26 529.0
February
66.59
178.94
245.54 241.4
March
264.84
3 74
582.93 1939.1
147.92 2841.8
April
29.72
118.2
MaY
228.7
355.37
584.07 925.3
June
5
E44.
130.45
195.68 1387.4
July
2
89.64
134.46 139.42
August
126.675
239.11
365.79 714.4
September
431.30
289.16
720.46 435.4
October
285.06
194.16
479.22 685.8
282.5 539.6
November
168.72
113.78
December
179.3 8
18 8.62
368 110.0
Annual Totals
2162.7
r�2651.02
4757.83 1�7 1743.4
Biosolids Source - Fourth Creek NCO031836 and Water Plant alum sludge

FOURTH CREEK ALKALINE STABILIZATION FACILITY
Table 2 - SUNEWARY OF PRODUCT RECIPIENTS
CALENDAR YEAR 1996
APPROXIMATE
DRY METRIC
MONTH DELIVERED TO: TONS
January Brawley-Swicegood-Wike 529.0
February Brawley-McNeely-Gray-P.Bell 241.4
March Brawley-Arrington-B.Bell-R.Bell
Dull-James-Kurfee-McNeely-
Pad Removal Project-Wike-Williams 1939.1
April Brawley-Wike-Swicegood-Southern
States Co -op -Pad Removal Project-
Moore-McNeely-Warren-Keyes-
Johnson-James-Iredell Milk-Gray-
Fesperman-Doby-Clayton Farms 2841.8
May Brawley-Arrington-Carrington-Colpetzer-
Fesperman-Iredell Milk -Letter -Maness -
McNeely 925.3
June Brawley-Jack Wooten Trucking -McNeely -
McClain Bros. Farm-Doby-Carrigan 1387.4
July Brawley-Sigmon-Maness-McClain Bros.
Farm-Millsaps 1394.2
August Brawley-Weston-Parker-Maness-Doby 714.4
September Brawley-Royster Clark-Ag-Liquids-
Weston 435.4
October Brawley-Benfield Sanitation-R. Bell -
Arrington 685.8
November Brawley-Southern States Co -Op 539.6
December Neal -Southern States Co -Op 110.0

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additionalclparametersl this form to tohe os be aingv an �iatoryit---y-
-- -uyunuu ro De summarized on Ihis form.
Permit Number /,�)nnnn r:,•�rlr-
Facility Name
NPDES #
or WO A (residual only lacllillos)
WWTP Name
Laboratory
Residual Analysis Data
Dale Sampled (grab) or /
Date Com osited / 14 C _� _
Percent Solids F
/ 1g= 0- _y
-i� c
(SIGNATURE OF PREPARER).---- —1DATE
"I certify, under penalty of law, flint this document was prepared under my direction or suporvislon In accordance will, a system
designed to assure Il,at qualified personnel properly gathered and evaluated the Informalion submitted. I am aware that Ilere are
significant penalllos for submitting raise Information, including lho possibility of fines and Imprisonment for knowing violations.•'
,
DEM FORM SSF (10194)

i r'
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name Fuial�zac 57414tu ZATr a, e;t;�Permit Number f.J
WWTP Name r`ou irik Gt., k -
NPDES # N C O o 3183 r;
Monitoring Period: From l / i /_cLj, To Ia. 4.71 /_21
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed
Class A
Alternative 1 Alternative 2 ✓ Alternative 3
Alternative 4 Alternative 5 Altemative 6
Class B
Alternative 1 Alternative 2 Alternative 3.
If applicable to alternative performed (class B only) indicate "Process to Significantly Reduce Pathogens":
Aerobic Digestion _ Air Drying — Anaerobic Digestion _ Composting P g _Lime Stabilization
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Fecal Coliform
bacteria (in
lieu of fecal
Allowable Level
in Sludge
2x106 MPN
per gram of total
solids or 2 x 106
CFU per gram
Minimum I Geo. Mean I Maximum Units
1000 MPN
per gram of
total solid
(dry weight) < 2
3 MPN per 4
grams total
solid (dry
5,65 1 ) g,
Number of Frequency of I Sample Analytical
Exceedences Analysis Type Technique
MFIJ
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed
Opt 1
P Option 2 Option 3 Option 4 Option 5
Option 6 t/ Option 7
P Option 8 Option 9 Option 10
No vector attraction reduction options were performed
5 nm
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note If you check
this statement attach an explanation why you have not met one or both of the requirements.)
`This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
miv�ln�ru,v
Preparer Name and Title (type or print)
`Signature of Preparer Date
Land Applier Name and Title (if 'applicable) (type or print)
Signature of Land Applier (if applicable) Date
DEM FORM RF (10/94)

DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box 1111
Statesville, North Carolina 28687
Received 1-26-96
Reported 2-20-96
Work Order # 02-0126
SAMPLE ID: Sta-Lime
SAMPLE #
02-0126-1
02-0126-1
02-0126-2
02-0126-2
02-0126-3
02-0126-3
02-0126-4
02-0126-4
02-0126-5
02-0126-5
02-0126-6
02-0126-6
02-0126-7
02-0126-7
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
PARAMETER
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
pH
TKN
T. Phos.
NH3-N
Nitrate/Nitrite
Cadmium
Lead
Copper
Page 1 of 2
RESULTS DRY WEIGHT
<2.75 MPN/g
72.6 %
<3.50 MPN/g
66.6 %
<2.96 MPN/g
67.5 %
<2.82 MPNg
70.9 %
<2.91 MPN/g
68.7 %
<3.03 MPN/g
65.9 %
<3.09 MPN/g
64.7 %
12.0 .
2820 PPM
53.3 PPM
51.4 PPM
<1.0 PPM
<.002 PPM
<.002 PPM
3.50 PPM
P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697

SAMPLE #
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
02-0126-1
PARAMETER
Chromium
Zinc
Mercury
Molybdenum
Nickel
Arsenic
Calcium
Potassium
Aluminum
Selenium
Magnesium
Sodium
Barium
% Solids(comp)
Respectfully Submitted,
Dena Myers
NC Cert. # 440
Page 2 of 2
RESULTS DRY WEIGHT
0.702 PPM
<.077 PPM
0.14 PPM
3.90 PPM
4.25 PPM
11.4 PPM
153000 PPM
12600 PPM
10100 PPM
<1.0 PPM
4090 PPM
1710 PPM
126 PPM
64.9 %

SPECIALIZED ASSAYS, INC.
2960 Foster Crei-
ehton Dr.
P.O. Box 40566
Nashville, TN 37204-0566
Phone [phone]
STATESVILLE ANALYTICAL 6445)
ATT: DENA MYERS
122 COURT STREET
STATESVILLE, NC 29677
;ample ID: 02-C)126-1
F',-oJett:
Project Name: STATESVILLE ANALYTICAL
Sampler: DENA MYERS
-ate reY-tif i cation: 3e7
ANInk L-Ne_T' I CALL_ FREF}ORT
Lab Number : 96-AO(-)624e
Date Collected:
Time Collected:
Date Received; 2/ 6/96
Time Received: 10:00
Sample Type: Soil
---
Report
--
Quan
Dil
-
-
---------
Analyte
Result
Units
-------
Limit
------
Limit
------
Factor
------
Date
--------
Time
-----
�y
Analyst
----------
Method
d
--------
Aluginum_
10100
mg/kg
1.0
1.0
110
2/ 9/96
13:47
R.Street
6010A
Arsenic
11.4
ag/kg
1.0
11.0
1.0
2/ 9/%
13:47
R.Street
6010A
Barium
126.
ag/kg
1.0
1.0
1.0
2/ 9/96
13:47
R.Street
6010A
Calciu6
153000
MG/kg
1.0
1.0
1.0
2/ 9/96
13:47
R.Street
6010A
Magnesium
4090
mg/kg
1.0
1.0
1.0
2/ 9/96
13:47
R.Street
6010A
Mercury
0.14
mg/kg
0.10
0.10
1.0
2/ 8/96
13:53
B.Hamilton
7471
Molybdenua
3.9
mg/kg
1.0
1.0
1.0
2/ 9/96
13:47
R.Street
6010A
Potassium
12600
mg/kg
110
1.0
1.0
2/ 7/96
13:47
R.Street
6010A
Selenium
ND
mg/kg
1.0
1.0
1.0
2/ 9/96
13:47
R.Street
6010A
Sodius
1710
mq/kg
1.0
1.0
1.0
2/ 9/96
13:47
R.Street
6010A
Nitrite-N
ND
mg/kg
1.0
0.1
10.0
2/12/96
14:01
K.Witte
9056
Nitrate-N
ND
®g/kg
1.0
0.1
10.0
2112/96
14:00
K.Witte
9056
Kjeldahl Nitrogen
2820
fig/kg
1.0
1.00
1.0
2/ 8/96
12:33
K.Witte
351.4
ND = Not detected at the report limit.
'eport Appi-owed By:
Theodore J. DUello, Ph.D.
Michael H. Dunn, M.S.
Danny B. Hale, M.S.
Report Date: 2/12/96
COPY 1

Client:
Address: ✓. . J, t i !' �'
Contact Person: Phone #
PO # Requisitioned by:
Customer Lab ID X Sam led Preservative
Sample ID # Time Date Matrix
ir1 I
Preservative Codes:
1. HNO3
2. HCI
3. NaOH
4. H2SO4
5. Other chemical
6. Chemicals in containers, lab.
7. Chemicals in containers, client
8. Chemicals added upon receipt
9. Received chilled
ib.- Samples delivered as soon as pulled
11. Samples chilled upon receipt
12' Other
FAX #
(Time Date)
Parameters requested foranalysis
Relinquished by: Time/Date
Received by: Time/Date
Relinquished by: Time/Date
Received in lab: �% Time/Date i
r
Lab Comments:
STATES VILLE ANALYTICAL
122 Court Street • P.O. Box 228
Statesville. NC 28687
f704) 872-4697
Chain of
Custody Record
Arrival Date
�• PH Analyzed
Sampled by:
Transported via: ; -t"
Holding times met:
Compliance work:
Non-compliance work:
0

DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box 1111
Statesville, NC 28687
ATTN: Renee Parkman
Received 3-14-96
Reported 3-16-96
Work Order # 03-0314
SAMPLE ID: Sta-Lime D 1-7
SAMPLE # PARAMETER
03-0314-1D
Fecal Coliform
03-0314-1D
% Solids
03-0314-2D
Fecal Coliform
03-0314-2D
% Solids
03-0314-3D
Fecal Coliform
03-0314-3D
% Solids
03-0314-4D
Fecal Coliform
03-0314-4D
% Solids
03-0314-5D
Fecal Coliform
03-0314-5D
% Solids
03-0314-6D
Fecal Coliform
03-0314-6D
% Solids
03-0314-7D
Fecal Coliform
03-0314-71)
% Solids
Page 1 of 3
AS RECEIVED
<2.0 MPN/g
13.0 MPN/g
8.0 MPN/g
13.0 MPN/g
<2.0 MPN/g
<2.0 MPN/g
<2.0 MPN/g
8
DRY ` TIGHT
<3.0 MPN/g
66.4 %
16.9 MPN/g
77.1 %
11.8 MPN/g
67.7 %
18.4 MPN/g
70.5 %
< 2.82 NiPN/g
70.7 %
<2.73 M[PN/g
73.0 %
<2.98 MPN/g
67.2 %
P.O. Box 228 • Statesville, North Carolina 28687 • 704/872J46�

Page 2 of 3
Sample ID: Sta-Lime E 1-7
SAMPLE #
PARAMETER
AS RECEIVED
DRY WEIGHT
03-0314-1E
Fecal Coliform
<2.0 MPN/g
<2.95 MPN/g
03-0314-1E
% Solids
67 7 %
03-0314-2E
Fecal Coliform
<2.0 MPN/g
<2,93 MPN/g
03-0314-2E
% Solids
68.3 %
03-0314-3E
Fecal Coliform
<2.0 MPN/g
<2,93 MPN/g
03-0314-3E
% Solids
68 2
03-0314-4E
Fecal Coliform
<2.0 MPN/g
<3.0 MPN/g
03-0314-4E
% Solids
64.9 %
03-0314-5E
Fecal Coliform
<2.0 MpN/g
<3.03 MPN/g
03-0314-5E
% Solids
65.8 %
03-0314-6E
Fecal Coliform
<2.0 MPN/g
<3.03 MPN/g
03-0314-6E
% Solids
66.1 %
03-0314-7E
Fecal Coliform
<2.0 MPN/g
<2,95 MPN/g
03-0314-7E
% Solids
67 7 %
SAMPLE ID: Sta-Lime F 1-7
SAMPLE #
PARAMETER
AE RECEIVED
DRY WEIGHT
03-0314-1F
Fecal Coliform
<2.0 MPN/g
<2,84 MPN/g
03-0314-1F
% Solids
70.5 %
03-0314-2F
Fecal Coliform
<2,0 MpN/g
<2,82 MPN/g
03-0314-2F
% Solids
70 9 %
03-0314-3F
Fecal Coliform
<2.0 MPN/g
<3.05 MPN/g
03-0314-3F
% Solids
65.6 %
03-0314-4F
Fecal Coliform
<2.0 MPN/g
<3.20 MPN/g
03-0314-4F
% Solids
62.5 %
03-0314-5F
Fecal Coliform
<2.0 MPN/g
<3.02 MPN/g
03-0314-5F
% Solids
66.3 %
03-0314-6F
Fecal Coliform
<2.0 MPN/g
<3.00 MPN/g
03-0314-617
% Solids
66.7 %
03-0314-7F
Fecal Coliform
<2.0 MPN/g
<3,13 MPN/g
03-0314-7F
% Solids
63.8 %

Page 3 of 3
SAMPLE ID: Sta-Lime G 1-7
SAMPLE #
PARAMETER
AS RECEIVED
03-0314-G1
Fecal Coliform
13,0 MPN/g
03-0314-G1
% Solids
03-0314-G2
Fecal Coliform
<2.0 MPN/g
03-0314-G2
% Solids
03-0314-G3
Fecal Coliform
<2.0 MPN/g
03-0314-G3
% Solids
03-0314-G4
Fecal Coliform
<2.0 WN/g
03-0314-G4
% Solids
03-0314-G5
Fecal Coliform
<2.0 MPN/g
03-0314-G5
% Solids
03-0314-G6
Fecal Coliform
<2.0 MPN/g
03-0314-G6
% Solids
03-0314-G7
Fecal Coliform
<2,0 MPNr/g
03-0314-G7
% Solids
Note: Dry weight is expressed as MPN per gram of total solids.
Respectfuully Submitted,
Dena Myers
NC Cert. # 440
NC DW Cert. # 37755
SC Cert. # 99010
RESULTS
19.2 MPN/g
67.8 %
<2.81 MPN/g
71.3 %
<2.91 MPN/g
68.7 %
<2.77 MPN/g
72.3 %
<2.92 MPN/g
68.6 %
<2.79 MPN/g
71.7 %
<2.81 MPN/g
71.1 %

- )
Address: /
Contact Person:
Pp #
Customer Lab ID #
'Sam le ID # n
t� J
V '
J
t J
z 0 o
-Preservative codes:
1.. ' HNO3
2. HCl
3. NaOH
4. H2SO4
5: Other chemical
6. Chemicals In containers, lab.
7. Chemicals in containers, client
8'"Chemicals added upon receipt
9. Received chilled
10. Samples delivered as soon as pulled
11. - Samples chilled upon receipt
Other
_ X gen -S -'r> I
am led Preservak,
ne Date
? S-r :?)dz-A/ I ! :)
STATES VILLE ANALYTICAL
122 CourtStreet • P.O. .228 1
Statesville, NC 286
b !3 7p. ) 87. �
Phone #
O ffFAX # b1. Ii
Chain
Requisitioned by: (Time Date) Custody ReCOI'd'"'
D,atel
Matrix Parameters requested foranalysis Arrival Date:li
c7
Anal zed'
— J .15
71
Relinquished by: TiG
me/Date Sampled by
Received by: Time/Date 1 D 5 3 - /MM
Transported via:
Relinquished by: Time/Date
Holding times met: Vie
r=.
Race i/1 . ✓-i.. .. .•_..,,:;�..�,�,�
ived in lab:
Time/Date
Compliance work: =i
F
Non-compliance work: =;
Lab Comments: q-
.._ _r•u�r,er._ .

DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box I 1 1 I
Statesville, North Carolina 28687
Received 3-14-96
Reported 4-20-96
Work Order # 03-0314
SAMPLE ID: Sta-Lime
SAMPLE #
PARAMETER
AS RECEIVED
DRY WEIGHT
03-0314-1
H
03-0314-1
TKN
1540 PPM
12.4
2171 PPM
03-0314-1
T. Phosphorus
1331 PPM
1877 PPM
03-0314-1
NH3-N
140 PPM
197.4 PPM
03-0314-1
NO3/NO2
12.7 PPM
17.9 PPM
03-0314-1
Cadmium
0.722 PPM
1.02 PPM
03-0314-1
03-0314-1
Lead
Copper
3.05 PPM
4.30 PPM
03-0314-1
Chromium
1.91 PPM
3.10 PPM
2.69 PPM
03-0314-1
Zinc
20.9 PPM
4.37 PPM
29.5 PPM
03-0314-1
Mercury
0.27 PPM
0.381 PPM
03-0314-1
Molybdenum
2.80 PPM
3.95 PPM
03-0314-1
03-0314-1
Nickel
0.675 PPM
0.95 PPM
03-0314-1
Arsenic
Calcium
4.1 PPM
5.78 PPM
03-0314-1
Potassium
172,000PPM
7910 PPM
242,520 PPM
03-0314-1
Aluminum
10,200 PPM
111153 PPM
14,382
03-0314-1PPM
03-0314-1
Selenium
<1.0 PPM
<1.41 PPM
03-0314-1
Magnesium
Sodium
5720 PPM
8065 PPM
03-0314-1
Barium
1310 PPM
1847 PPM
03-0314-1
% Solids (Comp.)
112 PPM
158 PPM
o
70.9 /o
Respectfully Submitted,
Dena Myers
NC Cert. # 440
P.O. Box 228 • Statesville, North Carolina 28687 0 704/872i46°

Client: �.
1�------------- --- ----- --
Address: n
Contact Person:Phone #FAX< . �c loneRequisitioned by: ( Dato)
CustomerSampled Preservati e
Sam le ID arno Date tutatrix Parameters requested for analysis
3 -Q 3 / o L/ �LI�1'1 (fin 1
_L_1 o G,
rya
1 L(
�-10 3 -03/4 �U),, Ij.
Preservative Codes:
1. HNO3
2. HCl
I NaOH
4. HZSO4
5. Other chemical
6. Chemicals in containers, lab.
7. Chemicals in containers, client
8. Chemicals added upon receipt
9. Received chilled
-a0. Samples delivered as soon as pulled
11. Samples chilled upon receipt
-12. Other
STATESVILLE ANALYTICAL
122 COull Stmct • P.O. Box 228
Statesvillc, NC 28687
[phone]
Chain of
Custody Record
i
!tlu
Date
Anal zed
( JJR
U C�(D
Relinquished by: ,< <_ .: �-, _�
i 0'—
Time/Date 3h,
Sampled byr G"
Received by:
Time/Date 1 ' D 5
Transported via:
Relinquished by:
Time/Date
I/
Holding times met:
Received in lab:,,
Time/Date j I T�� j7'1-/y
�
mpliance work:
Non-compliance work:
Lab Comments:

.SPAEC:IALI'LED ASSAYS INC;
29M Foster Creighton Dr.
P. O. Box 40.566
Nalhville. TN 3721D14)566
Phone [phone]•0177
ANAI_._Y7' I CAL FZEPpRT.
CAENA
'
-
.. _ � tom?: Y 1 * 1 _ � T y i2;� . �•?
����
.
.'(:/
_ _ -
eeatlt.
ur,iis
Liai+
7
:aia-----------------------------------w ;d aa:'
-------
-
-i-.-i0-:-i-t-
-�-1;-n-
--: -�-o-
-
----------_t_ ti
:-�-.-.;••7-eC�
CA olmes ^A 4004
3araua
p12.
ltglYq
R
GNolies a04 4L`i3
egitg
1.0
2.0
i
3'?.'
. y�
:5:_8
5
es t ,
C.Ho1lt=5�10�Y 440ti
1"anes"Ja
5720
to /� q
;.0
1.+;
2
3i2?:9b
1s:�s
C Holses
x
ag;'
9 '�9
1.0
I.0
1
V22-2
1 :c9
_
%.HoIaes b414A';4000
u.t+nun
0.10
0.0
3/2':0
ie::5
;47ikg/kg
re'.940
_
sg/ig
1.0
1.0
Or1
L N0o!:'9e79,0
'43e:en'u
a k
,.te,s .6b00+1
So:7i
ag,;g
1.00
2.0
3ic':7b
:5=
c 60 O44'000080000
`
i
M
sg;kg
1.0
1.0
1
%E
3 'c.9.:
C.. o,
Q40
-3!kq
q
I.0
0.1
:1
3;=br'96
Iy:?9
iC.+li:te+ 90�b ' '244
;e:._:I !litrogen
1340
ag;kg
1.0
`1
90�a t i'Q.b3 .
1.00
3:25 93
1�;1 B
K. .ticto a 351:4..'.`2455

Page Iof2
DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box 1111
Statesville, North Carolina 28687 - -
Received 5-9-96
Reported 6-10-96
Work Order 9 06-0509
SAMPLE ID: Sta-Lime
SAMPLE #
PARANMTER
AS RECEIVED
DRY WEIGHT
06-0509-1
06-0509-2
Fecal Coliform
% Solids
<2 %IPN/gm
<2.61 MpN/gm
06-0509-2
06-0509-2
Fecal Coliform
<? N/gm
76.6 %
<2'89 WN/gm
% Solids
06-0509-3
06-0509-3
Fecal Coliform
<2 NPN/gm
69.1
<2.64 MPN/gm
Solids
06-0509-4
06-0509-4
Fecal Coliform
< 2N/gm
75.7
<2'87 MPN/gm
06-0509-5
% Solids
Fecal Coliform
< 2 MPN/gm
69.6 %
<2.53
06-0509-5
%Solids
MPN/gm
06-0509-6
06-0509-6
Fecal Coliform
< i
2 MPIT/gm
78.9 %
<2.60 MPN/gm
06-0509-7
% Solids
Fecal Coliform
< gm
MpN/
<.
06-0509-7
Solids
a
262
2 3 MPN/gm
06-0509-1
pH
76.0
06-0509-1
06-0509-1
TKN
2290 PPM
11.8
3066 PPM
.
06-0509-1
T. Phosphorus
NH3-N
460 PPM
616 PPM
06-0509-1
NO3/NO2
11.2 PPM
67.5 PPM
15.0 PPM
90.4 PPM
P.O. Box 228 • Statesville, North Carolina 28687 • 704/872i4697

1 1'
Page 2 of 2
SAMPLE #
PARAMETER
AS RECEIVED
DRY WEIGHT
06-0509-1
06-0509-1
Cadmium
<0.001 PPM
<0.0013 PPM
06-0509-1
Lead
Copper
0.063 PPM
0.084 PPM
06-0509-1
Chromium
3.74 PPM
0.153 PPM
5.01 PPM
06-0509-1
Zinc
1.19 PPM
0.205 PPM
06-0509-1
Mercury
0.21 PPM =
1.59 PPM
0.281 Pl?M
06-0509-1
06-0509-1
Molybdenum
2.4 PPM
3.21 PPM
06-0509-1
Nickel
Arsenic
0.740 PPM
0.991 PPM
06-0509-1
Calcium
6.6 PPM
180000 PPM
8.84 PPM
06-0509-1
Potassium
8710 PPM
240966 PPM
06-0509-1
Aluminum
11600 PPM
11660 PPM
15529 PPM
06-0509-1
06-0509-1
Selenium
Magnesium
<1•0 PPM
<1.34 PPM
06-0509-1
Sodium
5520 PPM
7389 PPM
06-0509-1
.
Barium
1370 PPM
1834 PPM
06-0509-1
Solids (Comp.)
151 PPM
02 PPM
74 7 %
SAMPLE: ID 3rd Creek Viability
06-0509-2
06-0509-2
Cadmium
Lead
<0.001 PPM
<0.0013 PPM
06=0509-2
Copper
0.233 PPM
0.303 PPM
06-0509-2
Chromium
7.25 PPM
0.240 PPM
9.44 PPM
06-0509-2
Zinc
1.3 PPM
0.313 PPM
06-0509-2
Nickel
2.55 PPM
1.69 PPM
3 32 PPM
06-0509-2
06-0509-2
Molybdenum
3.4 PPM
4,43 PPM
06-0509-2
Selenium
Arsenic
<1.0 PPM
<1.30 PPM
06-0509-2
0
/o Solids
8.1 PPM
10.6 PPM
76 8 %
Respectfully Submitted,
;\C,
Dena Myers
NC Cert. # 440

Client:
Address: . 0 r X l l
Contact Personas ��r t-
PO #
Customer Lab ID # am I
Sample ID # Time
�D �o
3 3
//S
to J �c:J
7 �a
d
I
Preservative Codes•
1. HNO3
2. HCl
I NaOH
4. H2SO4 .
5. Other chemical
6. Chemicals in containers, lab.
7. Chemicals in containers, client
8. Chemicals added upon receipt
9. Received chilled
` 10. Samples delivered as soon as pulled
-11. Samples chilled upon receipt
12. Other
28(-9-7— ////
Phone # � '� g — 3 3 FAX #
Requisitioned by: (Time Date)
Preservative :d Matrix Parameters requested for analysis
cl-
Relinquished by: �/ Time/Date '
s
STATESVILLE ANALYTICAL
1 1(122 Court Street • P.O. Box 228
Statezvdic, NC 28687
704) 872-4697
Chain of
Custody Record
T Arrival Date
Sampled by:
Received by: Time/Date
Transported via:
Relinquished by: Time/Date
Holding times met:
Received in lab:
J I%e Time/Date h.) compliance work:
Lab Comments:
Non-compliance work:

Page 1 of 2
DATA REPORT
City of Statesville
Fourth Creek MVTP
Post Office Box 111 1
Statesville, NC 28687
ATTN: Steve Lambert
Received 7-10-96
Reported 8-9-96
Work Order # 0 1 -0710
SAMPLE LD: Sta-Lime
SAMPLE # P ARAiVMTER DRY WEIGHT
01-0710-1
Fecal Coliform
01-0710-1
%Solids
_ 0 P�T/o
01-0710-2
Fecal Coliform
66.4 /o
01-0710-2
% Solids
<2 0 MPNLg
01-0710-3
Fecal Coliform
64.1 %
O 1-0710-3
0
Solids -
<2.0 MPN/g
01-0710-4
Fecal Coliform
66.3 %
01-0710-4
% Solids
<2 0 NIPN/g
01-0710-5
Fecal Coliform
66.4
01-07I0-5
% Solids
<2 0 MPN/a
01-0710-6
Fecal Coliform
66.3 °i°
01-0710-6
% Solids
<2.0 MPNLg
01-0710-7
Fecal Coliform
66.2
01-0710-7
% Solids
<2 0 MPN/1Z
o
64.4 /o
P.O. Box 228 • Statesville, North Carolina 2RRR7 . 70Aia'70in9Zo7

SAMPLE #
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
01-0710-1
Page 2 of 2
PARAN4ETER
pH
T.Kjeldahl Nitrogen
Ammonia as N
Nitrate/Nitrite
T.Phosphorus
Cadmium
Lead
Copper
Chromium
Zinc
Mercury
Molvbdenum
Nickel
Arsenic
Calcium
Potassium
Aluminum
Selenium
Magnesium
Sodium
Barium
% Solids
Respectfuully Submitted,
j --Omc& '
Dena Mvers
NC Cert. # 440
NC DW Cert. # 37755
SC Cert. # 99010
DRY WEIGHT
11.8
2840 ma/Ka
124.8 ma/Ka
18.2 mg/Kg
3920 mg/Kg
0.045 mg/Kg
0.62 mg/Kg
18.1 mg/Kg
0.98 mg/Ka
3.34 mg/Kg
0.52 mg/Kg
3.7 mg/Ka
0.238 mg/Kg
8.6 mg/K.a
242,000 ma/Ka
13,100 nia/Kg1
15,800 ma/Ka
<1.44 mg/Kg
7070 mg/Ka
2080 mg/Kg
180 mg/Kg
67.3 %

Client:
Address:
—
SI'ATESVILLF ANALYTICAL
122 Court Suter • P.O. Box 228
Statesville, NC 28687
Contact Person:
S, / /
/,
[phone]
PO #
„
Phone #
FAX #
Chain of
Customer
Requisitioned by:
(Time
Date)
Custody Record
Sam le ID #
Lab ID # ID 1e
Time Date
Preservative -9 Matrix
Parameters requested for analysis
Arrival
Date
P Anal zed
Al
S
G/--
lV-4s IJ
J)vi IVA _
Preservative Codes,
1. HNO3
2. HCI
I NaOH
4. HZSO4
S. Other chemical
6. Chemicals in containers, lab.
7.' Chemicals in containers, client
8.. Chemicals added upon receipt
9. • Received chilled
10. Samples delivered as soon as pulled
'11. Samples chilled upon receipt
s12. Other
W-
Relinquished
Abftt Sampled P bY:.
Received by: Time/Date � l� -�6 /��//,�,w
—T` Transported via: kan
Relinquished by:C I
Time/Date
Holding times met:
Received in lab: �J Time/Date 7 " t d Cj (o � � �� 0
Compliance work:
Lab Comments:
Non-compliance work:

DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box 11 11
Statesville, NC 28687
ATTN: Renee Parkman
Received 9/18/96
Reported 10/1/96
Work Order # 11-0911
SAMPLE ID: Sta-Lime
SAMPLE #
11-0918-1
11-0918-1
11-0918-2
11-0918-2
11-0918-3
11-0918-3
11-0918-4
11-0918-4
11-0918-5
11-0918-5
1 1-0918-6
11-0918-6
11-0918-7
11-0918-7
PARAMETER
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Fecal Coliform
% Solids
Page 1 of 2
DRY WEIGHT
<2.85 MPN/g
70.2 %
< 1.24 MPN/g
61.7 %
<2.87 MPN/g
69.6 %
<2.67 WN/a
74.8 %
<3.1 I MPN/g
63.8 %
<2.92 MPN/sz
68.4 %
<2.86 MPN/g
70.0 %
P.O. Box 228 • Statesville, North Carolina 28687 • 70.1/872/4697

SAMPLE #
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
I1-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
11-0918-1
Page 2 of 2
PARAMETER
pH
T.Kjeldahl Nitrogen
Ammonia as N
Nitrate/Nitrite
T.Phosphorus
Cadmium
Lead
Copper
Chromium
Zinc
Mercury
Molybdenum
Nickel
Arsenic
Calcium
Potassium
Aluminum
Selenium
Magnesium
Sodium
Barium
% Solids
Respectfuully Submitted,
-N.na Mvers
NC Cert. # 440
NC DW Cert. # 37755
SC Cert. # 99010
DRY WEIGHT
11.4
3635 mg/Kg
4.91 mg/Kg
<1.46 mg/Kg
10 1. 2 mg/Kg
0.034 mg/Kg
0.235 mg/Kg
9.77 mg/Kg
2.28 mg/Kg
1.28 mg/Kg
0.628 mg/Kg
8.76 mg/Kg
3.33 mg/Kg
10.4 mg/Kcr
20,002 mg/Kg
24,090 mg/Kg
18,250 mg/Kg
<1.40 mg/Kg
6161 mg/Kg
3241 mg/Kg
172 mg/Kg
68.4 %

Client:
i
Address:
Contact Person: ' Phone #
-3� 3
PO # Requisitioned by:
Customer Lab ID # Sam led Preservative
Sample ID # Time Date -0 9 Matnx
Preservative Codes;
1. HNO3
2. HCl
3. NaOH
4. H2SO4
5. Other chemical
6. Chemicals in containers, lab.
7. Chemicals in containers, client
8. Chemicals added upon receipt
9. Received chilled
10. Samples delivered as soon as pulled
11. Samples chilled upon receipt
12. Other
Y FAX #
(Time Date)
Parameters requested for analysis
�&Mw
StATESVILLE ANALYTICAL
122 Court Street • P.O. Box 228
Statesville, NC 28687
[phone]
Chain of
Custody Record
Arrival Data
J. P Analyzed
Tl 1 ' j ('f
Relinquished by: Time/Date Sampled
Received by: Time/Date'
Transported via:
Relinquished by: v
Time/Date Holding times met:
Received in lab: J , Time/Date
I Compliance work:
Lab Comments:
Non-compliance work:
llj'^JI ° I -

SPECIALIZED.' ASSAYS -ENVIRONMENTAL 4NALYT I CAL 'REPORT' -
2960* Fo ' st ' e' r * 'Crei.g.ht6n Diive
Nashvill-6-,' Tennebsee .37204'
Original report -and a copy of . the cha-in of custody will follow by mail:
S , TATESVILLE ANALYTICAL 6445
ATT:. DENA�- MYERS
122 COURT STREET'
STATESVILLE.- NC 28677
Sample -ID:.11-0918--i
Project:
Project Name:
Sampler:
State' Certification: -,87
Lab Number: 96-A061-293
Date Collected:
� Time Col-le-cted: - --
Date Received: 9/20/96
Time Received: 8:30
Sample Type: Solid
Report
Quan
Dil
Anal te
------------------------
-----------
!""its
-------
Limit
------
Limit
------
Factor
Date
--------
Tine
1 s t
----------
r.1euho3 Bat"h
-------- -----
A 1 um 4 1 lum
m6
i.0
9 Z
5 cl;
S - Sturm
6 0 i
7625
Ar�)eliic
mg/hg
0
1. C)
19-6
y5 9
S . S t unn
6010A
7625
zig
1. C.
,26/96
9:59
S - S t LUM
6010;!
76,25
..0
9 2 ("S 9 6
0:59
S. Sturm
6 0 1 OA
7,25
9/2 6 91 6
9 5 9
s
6 0 1 0A
1;
Ak:xcury
0. 43
mg/kg
0.10
0.10
9124196
1A, 36
S. Sturm
7471
746-2
1 1; Aden tm
6.o
mglkg
1.
1.0
i
9./26/96
9:59
S . S r urm
6010.41
7625
Potassium
165CO
mg/,kg
0.
1.0
1
9/26,19C,
c,,: 59
3 . S t1u, ma
6010-A
7625
Seleliitw
UD
U. :16
0.06
1
9/26/96
9:59
S.StuL.,Q
6010 A
7625
Soii
_220
9.6
1.0
1
9/26/96
9: 5 '1
S. S turm
6010A
7625
Nitrit6-N
ND
mg/kg
1.0
0.1
1
9/28/96
14:47
D. Hoover-
9056
8776
Nifrate7k
ND
.
1.0
0.1
1
9/28/96
14:38
D. Hoove-,
9056
7 9,!, 1
4Cjeld.ihl Nitrogen
�490
m g/kg
1.0
1.0
9/27/96
18:50
D. Hoover
8693
.-ND '=.Not detected at the: report .. -Iiait.
Repor-t:­Approved By:
Report Date: 9/30/96
Theodore J. Ph-.D.
e.Dunn,,
Michal H. DM.S..
Danny B. Hal6,-M.s.
-7-

Page I of 2
DATA REPORT
City of Statesville
Fourth Creek WWTP
Post Office Box I l 1 I
Statesville, \C 28687
Attn: Renee Parkman
Received 10/7/96
Reported 10/ 16/96
Work Order -4 03-1007
S:kVIPLE ID: Sta-Lime
SAMPLE PAR2-\;VIETER
03-1007-1
Fecal Coliform
03-1007-1
% Solids
03-1007-2
Fecal Coliform
03-1007-2
% Solids
03-1007-3
Fecal Coliform
03-1007-3
% Solids
03-1007-4
Fecal Coliform
03-1007-4
% Solids
03-1007-5
Fecal Coliform
03-1007-5
% Solids
03-1007-6
Fecal Coliform
03-1007-6
% Solids
03-1007-7
Fecal Coliform
03-1007-7
°-o Solids
03-1007-1
pH
03-1007-1
% Solids
03-1007-1
Barium
03- l 007-1
Cadmium
03-1007- l
:arsenic
RESULTS
<3 NIPNN/gr
70.1 %
<3 NiP'_v/cr
75.0 %
<3 VIPN/a
72.8 %
<3 �IPN/Q .
68.6 ° o
<3 LIPN/,cr
67.1 %
<3
68.0 %
< 3 %IPN/a
6 6. 1 °/o
11.6
70.0 %
137
0.435 m,>>/KiT
8.29 ni`,/K�V
P.O. Box 228 • Statesville, North Carolina 28687 9 70•L'8 7 2/469

Page 2 of 2
03-1007-1
Nickel
03-1007-1
Chromium
18.4 mg/Kg
03-1007- I
Molvbdenum
47.8 mg,•'Kg
03-1007-1
Magnesium
6.58 mg/K2
03-1007-1
Sodium
5405 mgiT{g
03-1007-1
Nitrate & Nitrite
3089 mg/Kc,
03-1007-1
Zinc
2.29 mg/Kg
03-1007-1
Copper
142 mg/Kg
03-1007-1
Lead
62.9 mg/Ko,
03-1007-1
03-1007-1
Total Kjeldahl Nitrogen
8.72 mg/Kg
4705 mg/Ka
03-1007-1
Ammonia as Nitrogen
Selenium
1344 m o
03-1007-1
Total Phosphorus
<1..39 mg/Kg
03-1007-1
Mercury
rY
2I5 mg/Ka
g
03-1007-1
Potassium
<0.143 mg/Kg
03-1007-1
Aluminum
28,457 mg/Kg
17.017 mg/Kg
Respectfully Submitted,
Dena Myers
NC Cert. 9 440

Client:
Address:
r,/�• x
LCu:ntact Person:
erLab ID # Sam led
ID # Time Date
'. 7
Preservative de
1. HNO3
2. HCl
I NaOH
4. H2SO4
S. Other chemical
6. Chemicals in containers, lab.
7. Chemicals in containers, client
8. Chemicals added upon receipt
9. Received chilled
10. Samples delivered as soon as pulled
,11. Samples chilled upon receipt
12. Other
Phone # gjft 3y �h
Requisitioned by:
Preser7valve Matrix
STATESVILLE ANALYTICAL
122 CourtSweet • P.O. Box 228
Statesville, NC 28687
[phone]
FAX # Chain of
(Time Date) Custody Record
Parameters requested for analysis
Arrival Daps
P Analyzed
11
At, n ,
7-1' //, k- t
I,+« l:, .
Relinquished by:
10 Time/Date /) 7 //
Sampled by:
Received by:
Transported via:
Relinquished by:Z.
Time/Date ,`," j'
Holding times met:
Received in lab:
Time/Date it-, 'i i r, /;' /; ; , Compliance work:
Lab Comments:
Non-compliance work:

LiAa report
'r From: NC Certification No, 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Ms. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
` c
Full Service Analytical & Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA60087 Customer Code: STATESVI
Login Group #: 9471B8 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: METALS 1
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D
Result: Less than
Date started: 12/03/96
Time started: 14:15
Parameter: TOTAL RESIDUE
Method reference: SM 2540 B
Result: 72
Date started: 12/03/96
Time started: 16:35
Parameter: pH
Method reference: SW 846 9045A
Result: 13.0 units
Date started: 12/03/96
Time started: 09:50
Parameter: METALS DIGESTION METHOD
Method reference: 3050
Result: Completed
Date started: 12/03/96
Time started: 10:45
Parameter: BARIUM, TOTAL
Method reference: 6010
Result: 58 mg/kg
Date started: 12/04/96
Time started: 10:30
Unit: colonies/gram
MDL or sensitivity: 100
Date finished: 12/04/96
Analyst: WMM
MDL or sensitivity:
Date finished: 12/03/96
Analyst: EJS
MDL or sensitivity:
Date finished: 12/03/96
Analyst: WMM
3050
Unit:
MDL or sensitivity:
Date finished: 12/03/96
Analyst: LAS
MDL or sensitivity: 10.0
Date finished: 12/04/96
Analyst: LAM
449 Springbrook Road & P.O. Box 240543 ,a, Charlotte, NC 28224-0543
Phone: [phone] A. Toll Free Number: 1-800/529-6364 � Fax: [phone]
- — - - - - — ------ — — -

LclL'� rseFJvri %�
'c City of Statesville Sample I. D. AA60087 ( cauritinuad
Page: 2
December 5, 1996
Full Service Analytical & Environmental Solutions
Parameter: CALCIUM, TOTAL
Method reference: 6010
Result: 240000 mg/kg
Date started: 12/05/96
Time started: 08:00
Parameter: CADMIUM, TOTAL
Method reference: 6010
Result: Less than
Date started: 12/04/96
Time started: 10:30
Parameter: ARSENIC, TOTAL
Method reference: 6010
Result: 11 mg/kg
Date started: 12/04/96
Time started: 10:30
Parameter: NICKEL, TOTAL
Method reference: 6010
Result: Less than
Date started: 12/04/96
Time started: 10:30
Parameter: CHROMIUM, TOTAL
Method reference: 6010
Result: 12 mg/kg
Date started: 12/04/96
Time started: 10:30
Parameter: MOLYBDENUM, TOTAL
Method reference:
Result: Less than
Date started: 12/04/96
Time started: 10:30
Parameter: MAGNESIUM, TOTAL
Method reference: 6010
Result: 4000 mg/kg
Date started: 12/05/96
Time started: 08:00
Parameter: SODIUM, TOTAL
Method reference: 6010
Result: 1300 mg/kg
Date started: 12/05/96
Time started: 08:00
MDL or sensitivity: 10.0
Date finished: 12/05/96
Analyst: DHJ
Unit: mg/kg
MDL or sensitivity: 2.0
Date finished: 12/04/96
Analyst: LAM
MDL or sensitivity: 0.2
Date finished: 12/04/96
Analyst: LAM
Unit: mg/kg
MDL or sensitivity: 10.0
Date finished: 12/04/96
Analyst: LAM
MDL or sensitivity: 10.00
Date finished: 12/04/96
Analyst: LAM
Unit: mg/kg
MDL or sensitivity: 0.05
Date finished: 12/04/96
Analyst: LAM
MDL or sensitivity: 2.0
Date finished: 12/05/96
Analyst: DHJ
MDL or sensitivity: 1.00
Date finished: 12/05/96
Analyst: DHJ
Parameter-: NITRATE AND NITRITE
Method reference: SM4500-NO3 E.
Result: 5.6 mg/kg MDL or sensitivity:
Date started: 12/03/96 Date finished: 12/03/96
Time started: 16:22 Analyst: CEM
449 Springbrook Road A, P.O. Box 240543 A, Charlotte, NC 28224-0543
— _ Phone- 704/529-6364 AL Toll Free Number: 1-800/529-6364 & Fax: [phone]

data„report -,
City of Stataevillia Samplia 1, 0, AA600437 lr,ontirluedi
Page: 3
December 5, 1996 tl
Full Service Analytical & Environmental Solutions
Parameter: ZINC, TOTAL
Method reference: 6010
Result: 45 mg/kg
Date started: 12/04/96
Time started: 10:30
Parameter: COPPER, TOTAL
Method reference: 6010
Result: 69 mg/kg
Date started: 12/04/96
Time started: 10:30
Parameter: LEAD, TOTAL
Method reference: 6010
Result: 21 mg/kg
Date started: 12/04/96
Time started: 10:30
MDL or sensitivity: 2.0
Date finished: 12/04/96
Analyst: LAM
MDL or sensitivity: 2.0
Date finished: 12/04/96
Analyst: LAM
MDL or sensitivity: 2.50
Date finished: 12/04/96
Analyst: LAM
Parameter: TOTAL KJELDAHL NITROGEN
Method reference: SM4500-NH3 E
Result: 2000 mg/kg MDL or sensitivity: 15
Date started: 12/05/96 Date finished: 12/05/96
Time started: 07:30 Analyst: WMM
Parameter: TKN DIGESTION
Method reference: SM4500-NorgB
Result: Completed
Date started: 12/04/96
Time started: 12:45
Parameter: AMMONIA AS N
Method reference: 4500-NH3E
Result: 270 mg/kg
Date started: 12/03/96
Time started: 16:48
Parameter: AMMONIA DISTILLATION
Method reference: 4500-NH3B
Result: Completed
Date started: 12/03/96
Time started: 15:50
Parameter: SELENIUM, TOTAL
Method reference: 6010
Result: 8.0 mg/kg
Date started: 12/04/96
Time started: 10:30
Unit:
MDL or sensitivity:
Date finished: 12/04/96
Analyst: WMM
MDL or sensitivity: 2.5
Date finished:-12/03/96
Analyst: PAG
Unit:
MDL or sensitivity:
Date finished: 12/03/96
Analyst: PAG
MDL or sensitivity: 0.20
Date finished: 12/04/96
Analyst: LAM
Parameter: MERCURY, TOTAL
Method reference: 7471
Result: 0.10 mg/kg MDL or sensitivity: 0.02
Date started: 12/03/96 Date finished: 12/03/96
Time started: 11:00 Analyst: LAS
449 Springbrook Road &, P.O. Box 240543 A6. Charlotte, NC 28224-0543
Phone: [phone] & Toll Free Number: 1-800/529-6364 � Fax: [phone]

LaIJ rieport
t" City of Statesville Sample I. D. AAGO087 (continued) "4"
Page: 4
December 5, 1996
Full Service Analytical & Environmental Solutions
Parameter: MERCURY DIGESTION
Method reference: 7471
Result: Completed
Date started: 12/02/96
Time started: 16:00
Parameter: POTASSIUM, TOTAL,/
Method reference: 6010
Result: 14000 mg/kg
Date started: 12/05/96
Time started: 08:00
Parameter: ALUMINUM, TOTAL
Method reference: 6010
Result: 12000 mg/kg
Date started: 12/05/96
Time started: 08:00
Parameter: TOTAL PHOSPHORUS
Method reference: EPA 365.2
Result: 230 mg/kg
Date started: 12/04/96
Time started: 18:02
Unit:
MDL or sensitivity:
Date finished: 12/02/96
Analyst: DHJ
MDL or sensitivity: 1.0
Date finished: 12/05/96
Analyst: DHJ
MDL or sensitivity: 0.04
Date finished: 12/05/96
Analyst: DHJ
MDL or sensitivity: 0.50
Date finished: 12/04/96
Analyst: CEM
Parameter: TOTAL PHOSPHORUS DIGESTION
Method reference: EPA 365.2 Unit:
Result: Completed . MDL or sensitivity:
Date started: 12/04/96 Date finished: 12/04/96
Time started: 15:25 Analyst: CEM
Parameter: CALCULATIONS.BASED ON DRY WEIGHT
Method reference:
Result: 72 % DRY WT. MDL or sensitivity:
Date started: 12/03/96 Date finished: 12/03/96
Time started: 16:35 Analyst: EJS
If there are any questions
regardin this data,
Angela D. Overcash
Laboratory Director
please call.
449 Springbrook Road ,& P.O. Box 240543 AL Charlotte, NC 28224-0543
Phone: [phone] � Toll Free Number: 1-800/529-6364 ,& Fax: [phone]

, Lai Hep®rt
From: NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Ms. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
et }
Full Service Analytical & Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA60088 Customer Code: STATESVI
Login Group #: 9471B8 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: FECAL 2
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D
Result: Less than
Date started: 12/02/96
Time started: 14:20
If there are any questions regardin
Unit: colonies/gram
MDL or sensitivity: 100
Date finished: 12/03/96
Analyst: WMM
this data, please call.
Angela D. OVercash
Laboratory Director
449 Springbrook Road &. P.O. Box 240543 & Charlotte. NC 28224-0543
Phone: [phone] � Toll Free Number: 1-800/529-6364 &. Fax: [phone]

L.cau riepori
�~ '' From: NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Me. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
Full Service Analytical 3 Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA60089 Customer Code: STATESVI
Login Group #: 947198 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: FECAL 3
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D Unit: colonies/gram
Result: Less than MDL or sensitivity: 100
Date started: 12/02/96 Date finished: 12/03/96
Time started: 14:20 Analyst: WMM
If there are any questions
regarding his data,
Angela D. Overcash
Laboratory Director
please call.
449 Springbrook Road ,& P.O. Box 240543 & Charlotte, NC 28224-0543
—Phone: [phone] &. Toll Free Number: 1-800/529-6364 ,& Fax: [phone]

• Lap. Report
From: NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Ms. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
Full Service Analytical & Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA60090 Customer Code: STATESVI
Login Group #: 9471B8 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: FECAL 4
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D Unit: colonies/gram
Result: Less than MDL or sensitivity: 100
Date started: 12/02/96 Date finished: 12/03/96
Time started: 14:20 Analyst: WMM
If there are any questions regardingAhis dat4, please call.
Angela D. Overcash
Laboratory Director
449 Springbrook Road & P.O. Box 240543 &, Charlo[[e, NC 28224-0543
Phone: 7O4/529-6364 &. Toll Free Number: 1-800/529-6364 &. Fax: [phone]

ray rseport
1r =From: NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Ms. Carol Rogers
P.O., Box 1111
Statesville, NC 28687
Full Service Analytical d Environmental Solutions
The following analytical results have been obtained for tha
indicated sample which was submitted to this laboratory:
Sample I.D. AA00091 Customer Code: STATESVI
Login Group #: 9471B8 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: FECAL 5
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15.
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D Unit: colonies/gram
Result: Less than MDL or sensitivity: 100
Date started: 12/02/96 Date finished: 12/03/96
Time started: 14:20 Analyst: WMM
If there are any questions
regarding is da a,
Angela D. Overcash
Laboratory Director
please call.
449 Springbrook Road &, P.O. Box 240543 Charlotte, NC 28224-0543
Phone:[phone] ,& Toll Free Number: 1-800/529-6364 & Fax: [phone]

Last? Report
From: NC Cer tificatio, No, 402
SC Certification No..99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996.
To: City of Statesville
Attn: Ms. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
rrc.
Full Service Analytical & Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA60092 Customer Code: STATESVI
Login Group #: 947168 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: FECAL 6
Sample collection date: 12/02/96 Time: 08:30
Lab -submittal date: 12/02/96
Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D
Result: Less than Unit: colonies/gram
Date started: 12/02/96 MDL or sensitivity: 100
Time started: 14:30 Date finished: 12/03/96
Analyst: WMM
If there are any questions regardin this ata, please call.
An ela D. Overcash
Laboratory Director
449 Springbrook Road &. P.O. Box 240543 &, Charlotte. NC 28224-0543
Phone: [phone] .& Toll Free Number: 1-800/574_FZAe - r.,-.

Laf,_ Report
From: NC Certification No. 40.2
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Me. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
Full Service Analytical & Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA6OO93 Customer Code: STATESVI
Login Group: 9471B8 Customer Reference; 7232-1
Phone Number: [phone]/Fax(7O4)878-8655
Customer Sample I.D#: FECAL 7
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D Unit: colonies/gram
Result: Less than MDL or sensitivity: 100
Date started: 12/02/96 Date finished: 12/03/96
Time started: 14:30 Analyst: WMM
If there are any questions
regarding this data,
Ange a D. Overcash
Laboratory Director
please call.
449 Springbrook Road .,h, P.O. Box 240543 AL Charlotte, NC 28224-0543
Phone: [phone] -& Toll Free Number: 1-800/529-6364 &. Fax: [phone]

;fit. Report
From: NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
FL Certification No. E87519
December 5, 1996
To: City of Statesville
Attn: Ms. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
, A�l
Full Service Analytical'& Environmental Solutions
The following analytical results have been obtained for the
indicated sample which was submitted to this laboratory:
Sample I.D. AA00094 Customer Code: STATESVI
Login Group #: 9471B8 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I.D#: FECAL 8
Sample collection date: 12/02/96 Time: 08:30
Lab submittal date: 12/02/96 Time: 14:15
Received by: CP Validated by: SMM
Parameter: FECAL COLIFORM, SOLID
Method reference: SM 9222 D
Result: Less than Unit: colonies/gram
Date started: 12/02/96 MDL or sensitivity: 100
Time started- 14:30 Date finished: 12/03/96
Analyst: WMM
If there are any questions
regarding this data,
Ange a D. Overcash
Laboratory Director
please call.
449 Springbrook Road — P.O. Box 240543 ,& Charlotte, NC 28224-0543
Phone: [phone] ,& Toll Free Number: I-800/529-6364 — FnY• 70ei.7c_nenn

t r•"-
Full Service Analytical 8 Environmental Solutions
Statement of Data Qualification
for Duplicate Samples
on Analyses Performed by Prism Laboratories, Inc.
Main Office:
449 Springbrook Road
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
Client: City of Statesville
Fax: [phone]
Laboratory Group ID No.: 9471B8
The following analyses have been qualified for the reason(s) cited.
Sample No.: AA60087
Matrix: Solid
Explanation:
Parameter(s): Mercury
The relative percent difference (RPD) for the duplicate sample analyses is outside our established QA/QC
acceptance limits. The RPD value is an indicator of the reproducibility of a test in a particular sample
matrix. All other quality assurance/quality control data associated with the analytical batch were within
acceptable QA/QC limits. Collectively, the QA/QC data indicates the analytical test is in control. The
poor reproducibility for the recovery of the noted analyte(s) in the duplicate sample may have been due to
a matrix effect.
Duplicated Sample Dup. 1 Value
AA60087 0.103 mh/ke
Comments:
Dup. 2 Value JH��820%46
��Accept. Range
0.043 mg/kg 35%
If you have any questions concerning this data qualification report, please contact me at [phone]
or [phone].
Data Reviewed By:
Date: 12/5/96
This Statement of Qualification is included as pout of tite final analytical report for the abo%-e referenced sample(s) and must
be retained as part of that permanent record.

_. ISM
TATORIES, INC.
Full Service Analylical & Environmental Solt.1tions
Client cas S4A
Report To
Address P, o, Box I1 f 1 f
Bill To
5 A e l /V .7 8!8
P.O.#Billing Reference
Phone 74_Y-�7, - 3114
Project Name
CLIENTTIME
SAMPLE DESCRIPTION
LLE CTfD._
�ILITARY
IX SAMPLE CONTAINER
,(SOIL,
COLLECTED
.
WATER OR *TYPE
LDATS-
OURS
SLUDGE) SEE BELOW NO. SIZE
FecAl 3
_
-- << CAI_-- --- y---
-
-------- ------
._tGcA.L ... _
fcCy
Samplers Signature
I
PRESERVA-
TIVES
e...__._, .._ . ... V n . .. e
CHAIN OF C!/STODY RECORD
449 Springbrook Road , Charlotte, NC 2r�1',,
P.O. I3ox 240543 , Charlotte, NC 28224-0-�4.,
Phone: [phone] &. Fax: [phone],1
Lab Location Requested
for Certified Analysis NC — SC _ Other
Water Chlorinated Yes— No _ NA_
Sample Iced Upon Collection Yes — No _
Requested Due Date 3 - l/s ,
ANALYSES REQUESTED
SUB LAB PRISM
W
L REMARKS CERT. LAB
ID NO ID NO.
----- - -- - __ - - - - --- -- --- Lam. ; •�
,n
Additional Comments:
(111110
NPDES: NC Usr: NC - GROUNDWATER: NC
SC — SC - SC DRINKING WATER: NC SOLID WASTE: NC
OTHER OTHER SC OTHER: NC
OTHER OTHER SC SC
'CONTAINER TYPE CODES: A='Amber C =Clear G =Glass P =Plastic; TL =Teflon -Lined C OTHER OTHER
Cap VOA = Volatile Organics Analysis (Zero Head Space) FINAL REPORT COPY

of
•
V. 8.;
March 19, 1997
Mr. D. Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional Office
919 North Main Street
Mooresville, NC 28115
Re: Notice of Violation 3/13/97
Distribution of Class A Residuals
Permit No. WQ0006245
Iredell County
Dear Mr. Gleason:
1997
We are in receipt of the Notice of Violation for the referenced permit and offer the
following response.
On February 28, 1997, we discovered that we were noncompliant with permit
condition Part III (4) which requires that a TCLP analysis be conducted on our Class A
material. We immediately reported the noncompliance to Mr. Todd St. John of your
office and followed up on this conversation with a Report of Noncompliance dated
February 28, 1997. We have since completed a TCLP analysis on the Class A material
and have forwarded the results to your office via letter dated March 11, 1997. In addition,
we have taken measures in house to prevent any further compliance problems. Copies of
all correspondence are enclosed for your files.
Should you require any additional information please contact me at 878-3438.
Sincerely,
� ?, a, LWZL'-
Renee Parkman, Asst. Director
Water/Wastewater Treatment
Enclosure

�VvA_
Cat of
. 0. RIax 1111 ttttesuille, artll &ralina 20687
February 28, 1997
Mr. D. Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional GiFice
919 North Main St.
Mooresville, NC 28115
Re: Report of Non -Compliance
Distribution of Class A Residuals Permit
Permit No. WQ0006245
Iredell County
Dear Mr. Gleason:
As I reported to Mr. Todd St. John on February 28, 1997, we were non -compliant with
the referenced permit for 1996. The permit requires that an annual TCLP analysis be conducted
on the Class A material. We failed to perform this analysis for 1996.
We are currently in the process of having a TCLP run on our Class A product and will
forward the results to you as soon as they are available. We have taken measuresin house to
prevent any further compliance problems.
Should you require any additional information, please contact me at 878-3438.
Sincerely,
Renee Parkman, Asst. Director
Water/Wastewater Treatment

Cat of
tatestuffir
. M. i5ox 1111 • ttatesuille, Xvrtll &rnitna 28687
March 11, 1997
Mr. D. Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional Office
919 North Main Street
Mooresville, NC 28115
Re: Follow Up to Report of Non -Compliance
Distribution of Class A Residuals Permit
Permit No. WQ0006245
Iredell County
Dear Mr. Gleason:
As a follow up to our February 28, 1997 report of non-compliance, we have
completed the TCLP analysis for our Class A material. Please find enclosed a copy of the.
results.
Should you require any additional'information, please contact me at 878-3438.
Sincerely,
�C,, P44�-
Renee Parkman, Asst. Director
Water/Wastewater Treatment
RP/sg
Enclosure

m_do rteport
Fiom: NC Cert.ifir-Afinn v, a_rr7
SC Certification Ho. 99012
NC Drinking Water Cart. No. 37735
FL Certification No. E87519
March 10, 1997
To: City of Statesville
Attn: Me. Carol Rogers
P.O. Box 1111
Statesville, NC 28687
AA
Full SMIC-4 analytical S Environmental Solution;
The following analytical results have been obtained for the
indicated Sample Which was submitted to this laboratory;
Sample T.D. AA64547 Customer Code: STATESVI
Login Group #: 2255C1 Customer Reference: 7232-1
Phone Number: [phone]/Fax[phone]
Customer Sample I. D#F: STALIME
Sample collection date: 02/28/97 Time; 15:00
Lab submittal date: 03/03/97 Time: 08:30
Received by: SMV Validated by; ADO
Parameter: TCLP EXTRACTION (VOLATILES ONLY)
Method reference: 1311 Unit:
Result: Completed MDL or sensitivity
Date started: 03/05/97 Date finished: 03/06/97
Time started: 14:00 Analyst: DRR
Parameter: METALS DIGESTION
Method reference: EPA 3010
Result: Completed
Date started: 03/06/97,
Time started: 10:45
Parameter: PREP. METHOD 3510
Method reference: 3510
Result: Completed
Date started: 03/06/97
Time started: 10:45
Unit:
MDL or sensitivity:
Date finished: 03/06/97
Analyst: JAM
Unit:
MDL or sensitivity:
Date finished: 03/06/97
Analyst: DRR
Parameter: PREP. METHOD 3510 WITH EXCHANGE
Method reference: 3510 Unit:
Result: Completed MDL or sensitivity:
Date started: 03/05/97 Date finished: 03/07/97
Time started: 20:00 Analyst:
Parameter: PREP. METHOD 35,10 WITH EXCHANGE
Method reference: 3510 Unit:
Result: Completed MDL or sensitivity:
Date startedi 03/05/97 Date finished: 03/05/97
Time started: Analyst: SA
449 9pringbrook Road &. P.O. Box 240543 & Charlotte, NC 28224-0543
__ Phone: 704i529-6364 — Toll Free Number. 8eh0;529-6364 .& Fax: 704;515_n4r)Q

Lab Report
= o 7. lj-
City of Statesville
Page: 2
March 10, 1997
Sample I.D. AA64547 (continued)
Full Service Analytical d Enwronmentai Solutions
Parameter: ARSENIC, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time Started: 09100
Parameter: SELENIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time started: 09:00
Parameter: CADMIUM, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time started: 09:00
Parameter: CHROMIUM, LEACHABLE
Method reference: E,010
Result: Less than
Date started: 03/07/97
Time started; 09:00
Parameter: LEAD, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time started: 09:00
Parameter: SILVER, LEACHABLE
Method reference: 6010
Result: Less than
Date started: 03/07/97
Time started: 09:00
Parameter: MERCURY, LEACHABLE
No+E+nri rcfero_nno. 7d71
Result: Lees than
Date started; 03/04/97
Time started; 14;00
Parameter: BARIUM, LEACHABLE
Method reference: 6010
Result: Less, than
Date started: 03/07/97
Time started: 09:00
Unit: mg/L
MDL of sensitivity: 0.50
Date finished: 03/07/97
Analyst: DHJ
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/07/97
Analyst: DHJ
Unit: mg/L
MDL or sensitivity: 0.10
Date finished: 03/07/97
Analyst: DHJ
Unit: mg/L
MDL or sensitivity: 0.50
Date finished: 03/07/97
Analyst: DHJ
Unit; mg/L
MDL or sensitivity: 0.30
Date finished: 03/07/97
Analyst: DHJ
Unit: mg/L.
MDL or sensitivity: 0.50
Date finished: 03/07/97
Analyst: DHJ
f In 4 4t . mrr/i
MDL or sensitivity: 0.02
Date finished: 03/04/97
Analyst: LAS
Unit: mg/L
MDL or sensitivity: 10.00
Date finished: 03/07/97
Analyst: DHJ
Parameter: TCLP VOLATILES BY 8240
Method reference: SW846-8240 Unit: mg/L
Result: Bee below
Date Started: 03/06/97 Date finished: 03/06/97
Time started: 14:58 Analyst: HP
449 Springbrook Road. P.O. BOX 240543 ,& Charlotte, NC 28224-0543

Lan Report
City of Stateaville
Page: 3
March 10, 1997
s
Sample I. D. AA64547 ( cant i nued
Felt Service Anetytical 6 Environmental soluaons
Parameter: TCLP SEMI-VOLATILES
Method reference: 8270
Result: see below
Date started: 03/06/97
Time started: 17:40
Parameter: TCLP PESTICIDES
Method reference:
Result: see below
Date started: 03/07/97
Time started: 08:23
Parameter: TCLP HERBICIDES
Method reference:
Result: see below
Date started: 03/07/97
Time started:
Parameter: MERCURY DIGESTION
Method reference: 7471
Result: Completed
Date started: 03/04/97
Time started: 09:45
Parameter; TCLP EXTRACTION
Method reference: 1311
Result: Completed
Date started: 03/03/97
Time started: 16:00
BY 8270
Unit: mg/L
Data for TCLP VOLATILES BY 8240 mg/L:
Component Have
BENZENE
CARBON TETRACHLORIDE
CHLOROBENZENE
CHLOROFORM
1,4-DICHLOROBENZENE
1,2-DICHLOROETHANE
1,1-DICHLOROETHENE-
METHYL ETHYL KETONE
TETRACHLOROETHENE
TRICHLOROETHENE
VINYL CHLORIDE
Date finished: 03/06/97'
Analyst: MP
Unit: mg/L
Date finished: 03/07/97
Analyst: HWC
Unit: mg/L.
Date finished: 03/07/97
Analyst: SA
Unit:
MDL or sensitivity:
Date finished: 03/04/97
Analyst: LAS
Unit:
MDL or sensitivity:
Date finished: 03/04/97
Analyst: DHJ
Result
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not; detected
Not detected
Data for TCLP SEMI-VOLATILES BY 8270 mg/L:
Component HDL
0.01
0.01
0.01
0.01
0.014
0.01
0.01
0.04
0,012
0.01
0.02
Component Name Result Component XDL
CRESOLIS Not detected 0.050
1,4-DICHLOROBENZENE Not detected 0.050
2, 4-DINITROTOLUENE Not detected 0.012
HEXACHLOROBENZENE Not detected 0.010
449 Springbrook Road A. P.O. Box 240543 & Charlotte. NC 28224-0543
Phone: [phone] ,& Toll Free NumhPr- t -A,- - r,v.

Laa Heport
City of Statesville Sample I.D. AA64547 (continued)
Page: 4
March 10, 1997
Oa3ta -Pnr Try p Q=WT_Vn1 ATTLZIC nv a-),yfh i
V;• j V ♦ Continued J �
Component Name
HEXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
PYRIDINE
2, 4, 5- TRI CHLOROPHENOL
2, 4, 6-TRICHLOROPHENOL
Data for TCLP PESTICIDES mg/1„
Component Name
CHLORDANE
ENDRIN
HEPTACHLOR
HEPTACHLOR EPDXIDE
LINDANE
METHOXYCHLOR
TOXAPHENE
Data for TCLP HERBICIDES mg/L:
Component Name
2, 4-D
SILVEX
Sample comments:
Result
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Result
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Not detected
Result
Not detected
Not detected
TCLP herbicides subcontracted to NC certified.lab # 387.
Full SOMCO Malylical d Environmental Solutions
Component XDL
0.050
0.050
0.050
0.25
0.25
0.25
0.10
Component MDL
0.015
0.010
0.005
0.005
0.2
1.0
0.25
Component NDL
5.0
0.5
If there are any questions regarding this data, please call.
Angela D. Overcash
Laboratory Director
449 Springbrook Road & P 0, Box 240543 w Charlotte. NC 28224-0543
Phone: [phone] A6 Toll Frec Number !.- r— -

CKAIN OF CU"My RECORD
PAOE _ CIO YES fxD M^
449 SpringhTook FloMf .� CharkVtc, NC Sernples IN1ACTupon „�ws
17 _
P-0- Box 240 543 ` Charlotte. NC 28224-0543 PROPOR PFFSERVAV1YIE5 Ji,dfpbrT!
Phone: 704l529-6364 ,& Fax: 704152S--0409
� WITNII+NOiDltf(J TJI�s� a
COMUDY SEAW MJTAG77 _ s
Full Service Analylical b Environmental SOIU11Oot VOLATJLEsacalYlUUTJtFJfDSJ'/ 7
UPI�jYalAAbess . - --- AEiO►TTTQI�pYs _-..�.—_._._- ._._ ---- -"
Name— _-"-- Paquasbd _- - _ P1hs Fax_ - - - --- - - ... - -- -- SC - O1W . - _ KA -
R.O.Vas6vRrfnnw. Adi+ea _._._._ .- _ --. •- -- _ WAIorChbrinsGetl Yes No NA
Pr�jKtN.mr ----- SDes Dale.--.-.- .___------_-..__.-.-- - pJat*dUponcoleetion Yp
- - Sim ...4b
`- - (SEE REYMSE81DEFOR RUSH 9wMINIM JN0 FJ9E) GMUD WOES 07HER ----
TIME MATJAIx S RMr4E C10NTlkI11E/1 r C1 '- ANALYSE3 REMESTa
tl1ERT DALE CIJ!_lEC1Et) '�(
SAN►LE DE?SCU n101! {TM • - PRNMN i S11s
�-. COLLElrTEA ATfU�#RY IAtA:TEROA 'TYPE ��/ � � LA! PPllt
IMOURS f SLLOGE) SEE BEtDP! MA_ an TJYFS f r`V '% �� l w-ftF fis CpT Lli
Z.
�c Jl.
LL
LTSn,arlar's signature- _-s/1�-15mmp�d BJr OWYtI Atame) S
auliatJon . _G1 Q
., ar- QS nr,ef J R.o.u�.d JlJt l&�� Dry. - - - • -
J
r++ws addOvnal Co+ostatlfcs
C. %iAcr
GkiL.�
-4 UDorillAnaBr. - —•---- -
r
�S HC UST: r+c
GROUNDWATEP MC _ ORINKMiG WATER: Me_ —_ .._ _ 5dUD V1rASlE: NC ..,- -
sc sC
OTHER SC . SC.. __ - - OTlEIR
OTHER orr"Em . 8C _ .._ .. OC -
Cj11fE1i.- , O7FER..._-•- OTHEH _ - :OQMYAINEA TYPE COLYESr Il = Art•J,[K C = CXesr G = C3J�sa R � Plastic: �L � TAMcx�•Ll�aci (`An Mf1+1 = Uw.�wtti.,,a,,., a...,�..►,..T.-_ .,__ � ..----• _

of
#tat Avon U itte
V. 0. i9ax 1111 • 3takouille. North &ralina 28687
February 28, 1997
Mr. D. Rex Gleason, P.E.
Water Quality Supervisor
Mooresville Regional Office
919 North Main St.
Mooresville, NC 28115
Re: Report of Non -Compliance
Distribution of Class A Residuals Permit
Permit No. WQ0006245
Iredell County
Dear Mr. Gleason:
N C DEFT. OF
ENV1R01 : EY=T, HEArA
VIVUE er E1,4111 I,_
As I reported to Mr. Todd St. John on February 28, 1997, we were non -compliant with
the referenced permit for 1996. The permit requires that an annual TCLP analysis be conducted
on the Class A material. We failed to perform this analysis for 1996.
We are currently in the process of having a TCLP run on our Class A product and will
forward the results to you as soon as they are available. We have taken measure in house to
prevent any further compliance problems.
Should you require any additional information, please contact me at $78-3438.
Sincerely,
Renee Parkman, Asst. Director
Water/Wastewater Treatment

y e�f
4'
outtle
P. @. Max 1111 • -1,145tateouille, Nort4 Tarnlina 28677
May 30, 1989
Jesse W.-Wells
Division of Environmental Management
P. 0. Box 950
Mooresville, NC 28115-0950
ater/Wastewater Oretttment Plants
704-878-3438
OF NAr
coaffS�NIT3VIDE�: �
C7 a J
I17" F t
Subject: Resample of Permit #13849 - Well #1 & #2
Third Creek WWTP
Dear Mr. Wells:
Please find enclosed the results of two of our four wells,
resampled on 5-17-89, at our Third Creek WWTP, NC0020591 for
the below listed non -compliant parameters:
Well Parameter Violation Resample
1 T. Coliform = 6300/100 1/100
2 NO3-N = 13.4 mg/1 5.4 mg/1
Our Fourth Creek WWTP Lab, #181, ran the onsight measurements,
including pH. Our Water Plant Lab, #37-620, analyzed the T.
Coliform test.
Please find attached the GW-59 forms. The Nitrate as Nitrogen
was performed by Bold Laboratories in Charlotte, NC. We are
pleased that these results show that we are back into compliance.
We believe large amounts of rainfall over the past few months
following a long period of drought is responsible for these elevated
values. Please note also the number one well is the control well
and is upstream from the landfill. The second well is also in the
general area of the first. Wells are located in a pasture used for
periodic grazing of livestock (cows). This, along with the mentioned
wet conditions following a drought could account for these wells
showing a permit violation. Please note wells 3 and 4 are located
beside the landfill and did not show a violation. We do not believe
this situation is an actual violation, but a result of groundwater
activity. However, we understand the conditions of the permit and
realize these wells will have to be closely monitored.

Environmental Mgmt. Div.
Groundwater Section
May 30, 1989
Page 2
Please direct any questions and correspondence on this
matter to Joe Hudson, Director of Water and Wastewater Treatment,
[phone]:.
Sincerely,
Peter T. Connet
City Manager
Enclosure
cc: Dennis Crowson
Brenda J. Smith

COMPLIANCE MONITORING Division Groundwater Environmental
P.O. Sox 27687
REPORT FORM Raleigh, N.C. 27611
For additional forms please write or call: [phone]
Facility Name Third Creek WWTP Landfill County Iredell
Address US 70E Permit Number: 13849 (Resample )
Statesville, NC 28677 Non -Discharge
Well Location Downgradient NPDES NC0020591
Well Identification Number 42 Well Depth 38 Ft. Water Use
Well Diameter 2" Sample (Screened) Interval Ft. To Ft. Injection Well
Depth to Water Level 34' ft. below measuring point. Cbefore sampling) Well Construction
Measuring point is 2' feet above land surface Other
Gallons of water pumped/bailed before sampling 6
Field Analysis: pH 6.9 Specific Conductance uMhos Temp. o C Odor Appearance
Date Sample Collected 5-17-89 Date Lab Sample Analyzed
Laboratory Name 4t-h Creek WWTP Lab Certification No. _ #f 1 Al
COD mg/I NO as N mg/I Ni - Nickel mg/1
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
Dissolved Solids: Total
mg/I
pH (when analyzed)
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
2
NO 3 as N 5 _4
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
Cu - Copper _
Fe - Iron
Pb - Lead mg/I
Zn - Zinc mg/I
Pesticides/Herbicides (Specify Compounds)
mg/I Other (Specify)
mg/I
mg/I
Hg - Mercury mg/I
K - Potassium mg/I
Mg - Magnesium mg/I
Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese mg/I
TKN as N mg/I Na - Sodium mg/I
CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
SIGNATURE OF PERMITTEE (OR AUTHORIZED AGENT't) DATE
GW-59 Revised 6/88
Note:
ug/I
ug/I
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Values should reflect total concentrations
Eback forinstructions.
it blue and green copies only to address above.

COMPLIANCE MONITORING
REPORT FORM
Division of Environmental Management
Groundwater Section
P.O. Box 27687 1
Raleigh, M.C. 27611
For additional forms please write or call: [phone]
Facility Name Third Creek WWTP Landfill
Address US 70E
Statesville, NC 28677
Well Location Upgradien
Well Identification Number #1 Well Depth 6P Ft.
Well Diameter 2" Sample (Screened) Interval Ft. To Ft.
Depth to Water Level 51' ft. below measuring point. (before sampling)
County TrPrlpl1
Permit Number: 13849 (Resample)
Non -Discharge
NPDES—NCO02ngcal
Water Use
Injection Well _
Well Construction
Measuring point is 2' feet above land surface Other
Gallons of water pumped/bailed before sampling 19 gals
Field Analysis: pH 7.0 Specific Conductance uMhos Temp. o C Odor Appearance
Date Sample Collected 5-17-89 Date Lab Sample Analyzed
Laboratory Name 4th Creek WWTP Lab *(T.Co1if.-W.P1t.LabL Certification No. E181 *(W P1 _T,ab 37-620_)
COD mg/I NO2 as N mg/I Ni - Nickel mg/I
* Coliform: MF Fecal 41 /100ml NO3 as N mg/I Pb - Lead mg/I =
Coliform: MF Total
Dissolved Solids: Total
pH (when analyzed)
TOC
Chloride
Arsenic
Grease and Oils
Hardness: Total
Phenol
Sulfate
Specific Conductance
/100ml
_ mg/I
_ units
_ mg/I
- mg/I
_ mg/I
_ mg/I
_ mg/I
_mg/I
- mg/I
uMhos
Phosphorus: -Total as P
Al - Aluminum
Ba - Barium
Ca - Calcium _
Cd - Cadmium
mg/I Zn - Zinc mg/I
mg/I Pesticides/Herbicides (Specify Compounds)
mg/I
mg/I
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
Total Ammonia(NH3 t NH 4) mg/I Mn - Manganese_
TKN as N mg/I Na - Sodium
CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
SIGNATURE OF PERMITTEE (OR AUTHORIZED AGENT*)
GW-59 Revised 6/88
DATE
mg/I
mg/I
mg/I
Other (Specify)
Note:
ug/I
ug/I
ug/l
ug/I
ug/I
ug/I
ug/I
ug/I
ug/I
Values should reflect total concentrations
See back for instructions.
# 'Submit blue and green copies only to address above.

Bold Research Labs
4 Incorporated
ANALYTICAL TESTING & CONSULTING SERVICES
P.O. BOX 31486 • CHARLOTTE, NC 26231 . TELEPHONE [phone] • FAX: [phone]
LAB SAMPLE NO.(s): 14 7B 1
0i3KILil
RECEIVED FROM:
NAME: DENNIS G. CROWSON
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLE(s) of WATER
MARKED: A:3RD CREEK WELL #2
A
SAMPLE/TEST NO. 1
DATE OF REPORT: 0 5/ 2 5/ 8 9
DATE RECEIVED: 0 5 / 17 / 8 9
CUSTOMER NO.: 6084
TELEPHONE NO.: 704-878-3438
U3
A
A: B 1 B: C: D:
ANALYSIS UNITS
H
TOTAL RESIDUE
m /L
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L
BOD
m /L
COD
m /L
AMMONIA AS N
m /L
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE ASP
m /L
CHLORIDE AS Cl-
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL
m /L
METALS UNITS
ARSENIC
(mg/L)
SELENIUM
(mg/L)
CADMIUM
(mg/L)
CHROMIUM
(mg/L)
COPPER
(mg/L)
, .W °✓ mil ��
LEAD
(mg/L)
''• (��1
NICKEL
(mg/L)
ZINC
(mg/L)
i.x. �i
7
MERCURY
(mg/L)�;'
APPROVED BY: L • o • Jeffrey K. O'Ham, Manager 303 MEACHAM ST. 9 CHARLOTTE, NC 28203

N- C. DEPT. Or, NATURAL
rraSWjo RCS UJ1'CEc Az%ID
Q.'®i311@/TgJl''TY L-I' /ELF. PMENT
E ildR 2 4 1992
DIVISION GF Ef191flONhIENTA1 11ANAGEI1EIIT
State of North Carolina 4160RESVGIeE REG1911% OFFIGI
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor
William W. Cobey, Jr., Secretary
March 18, 1992
Mr. Jack King, City Manager
City of Statesville
Post Office Box 1111
Statesville, North Carolina 28677
George T. Everett, Ph.D
Director
Subject: Permit No.WQ0006245
Sludge Stabilization Facility
Fourth Creek Wastewater Treatment Plant
Wastewater Treatment Facility
Iredell County
Dear Mr. King:
In accordance with your application received December 5, 1991 we are forwarding herewith Permit
No. WQ0006245 dated March 18, 1992 to City of Statesville for the construction and operation of the
subject facilities.
This permit shall be effective from the date of issuance until February 28, 1997 and shall be subject
to the conditions and limitations as specified therein. Please pay particular attention to the monitoring
requirements in this permit. Failure to establish an adequate system for collecting and maintaining the
required operational information will result in future compliance problems.
If any parts,'requirements, or limitations contained in this permit are unacceptable to you, you have
the right to request an adjudicatory hearing upon written request within 30 days following receipt of this
permit. This request must be in the form of a written petition, conforming to Chapter 150B of North
Carolina General Statutes, and filed with the Office of Administrative Hearings, P.O. Drawer 27447,
Raleigh, NC 27611-7447. Unless such demands are made this permit shall be final and binding.
Regional Offices
Asheville Fayetteville Mooresville Raleigh Washington Wilmington Winston-Salem
704/251-6208 919/486-1541 704/663-1699 919/733-2314 919/946-6481 919/395-3900 919/896-7007
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

City of Statesville
WQ0006245
Page Two
One set of approved plans and specifications is being forwarded to you. If you need additional
information concerning this matter, please contact Mr. John Seymour at 919/ 733-5083.
cc: Iredell County Health Department
Mooresville Regional Office, Water Quality
Training and Certification Unit
Facilities Assessment Unit
(90: or illsve e Region_a-Office,-Groundwater_ .
Groundwater, Jack Floyd_
- -
George T. Eve I Ytt
2

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
RALEIGH
COMPOST PERMIT
In accordance with the provisions of Article 21 of Chapter 143' General Statutes of North Carolina ,
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
City of Statesville
Iredell County
FOR THE
construction and operation of a wastewater treatment plant sludge stabilization facility for the stabilization
of process dewatered sludges from Fourth Creek WWTP Third Creek WWTP, and alum sludge from
Statesville's water plant to meet PFRP requirements via pH and temperature conditions, consisting of
Fourth Creek dewatered sludge transported by an existing conveyor belt from the existing Fourth Creek
filter press facilities to a new 53 foot long covered cleated feeder conveyor, two 25 cubic yard sludge
storage hoppers (for dewatered Third Creek and alum sludges transported in) with bottom screw
conveyors to convey sludge from hopper to flanged connections above the 53 foot cleated feeder
conveyor, 25 foot long 12 inch diameter twin screw sludge mixer, two 12 foot diameter by 23 foot straight
wall (60 ton capacity) leg supported silos with variable speed volumetric feeders and a common transfer
screw conveyor to convey lime and/or kiln dust to the sludge mixer, a covered cleated side wall conveyor
from the end of the sludge mixer to the truck lading station, an appropriate nonleaking transport truck(s) or
approved equivalent to convey lime/ kiln dust mixed sludge, protected pulse bins (where truck loaded
sludge will be dumped and allowed to heat for pathogen reduction), a 150 foot by 300 foot curbed sludge
curing asphalt slab for treated sludge mix to be put in wind rows and allowed to continue to heat and then
to dry including periodic turning with stormwater swale and drain system draining back to the wastewater
treatment facilities (walled and roofed pulse bins along the up slope 300 foot side of sludge curing slab),
all necessary measuring devices to ensure that each truck load of mixed sludge reaches a pH of 12 for 2
hours and the temperature in the heated sludge is maintained at a minimum of 70 degrees C for a minimum
of 30 minutes, and all associated controls, support structures, piping, and appurtenances for the sludge
sources listed in Condition II 3. with no discharge of wastes to the surface waters, pursuant to the
application received December 5, 1991 and in conformity with the project plan, specifications, and other
supporting data subsequently filed and approved by the Department of Environment, Health and Natural
Resources and considered a part of this permit.
This permit shall be effective from the date of issuance until February 28, 1997 and shall be subject
to the following specified conditions and limitations:

U : ►" DIL3 Kiel 1 : , 1
1 • Upon completion of construction and prior to operation of this permitted facility, a
certification must be received from a professional engineer certifying that the permitted
facility has been installed in accordance with this permit, the approved
specifications. Mail the Certification to the Permits and EngineeriUna, plans O. Box
29535, Raleigh, NC 27626-0535.
2.
The Mooresville Regional Office, phone no. 704/ 663-1699 shall be notified at least forty-
eight (48) hours in advance of operation of the installed facilities so that an in -place
inspection can be made. Such notification to the regional supervisor shall be made during
the normal office hours from 8:00 a.m. until 5:00 p.m. on Monday. through Friday,
excluding State Holidays.
3. This permit shall become voidable in the event of failure of the sludge stabilization facility
to adequately protect the assigned water quality standards of the surface _waters and
groundwaters and meet sludge PFRP standards.
4• The sludge stabilization program shall be effectively maintained and operated as a non -
discharge system to prevent discharge of any wastes resulting from the operation of this
program.
5 • The issuance of this permit shall not relieve the Permittee of the responsibility for damages
to surface or groundwaters resulting from the operation of this facility.
6. In the event that the sludge stabilization program is not operated satisfactorily, including the
creation of nuisance conditions, the Permittee shall take such immediate corrective action as
may be required by this Department, including the construction of additional or replacement
wastewater treatment or disposal facilities.
7. Diversion or bypassing of the untreated sludge or compost drainage wastewater from the
stabilization facilities is prohibited.
8. Stabilized sludge that meets PFRP standards should not be used in areas of intense public
use (schools, playgrounds, etc.). Sludges that do not meet PFRP standards should only be
disposed of in accordance with.State regulations and permitted authority.
II. OPERATION AND AINTENANr'E RE00R MENTS
1 • The facilities and disposal sites shall be properly maintained and operated at all times.
2. The sludge composting operation must be conducted under the supervision of the certified
wastewater treatment plant operator required by the Certification Commission for operation
of the Fourth Creek Wastewater Treatment Plant, NPDES Permit No. N00031836.
2

13. No sludges other than the following are hereby approved for composting in accordance
with this permit:
source Permit
aunty Number
Fourth Creek WWTP Iredell NC0031836
Third Creek WWTP Iredell NC0020591
Statesville Water Plant Iredell
4. All stabilized and unstabilized sludges shall be stored at the appropriate Fourth Creek
Wastewater Treatment Plant facilities until such time as it is disposed of. If an alternate
storage site is to be used, approval must be obtained from the Division of Environmental
Management.
5i No stabilized sludge shall be disposed of or marketed that does not meet the criteria for the
Process to Further Reduce Pathogens (PFRP), which for this facility a lime/ kiln dust
mixed sludge reaches a pH of 12 for 2 hours and the temperature in the heated sludge is
maintained at a minimum of 70 degrees C for a minimum of 30 minutes. The use of any
other stabilizing method shall require a permit amendment prior to the distribution of any
such compost.
6. Any sludge which does not meet PFRP criteria can only be disposed of as per a specific
disposal permit.
-- - ��'� -.tea i�17 �/U��7►�A]
1 • Any monitoring (including groundwater, surface water, sludge, soil, or plant tissue
analyses) deemed necessary by the Division of Environmental Management to insure
protection of the environment will be established and an acceptable sampling and reporting
schedule shall be followed
2. The City of Statesville shall maintain records including, but not limited to the following:
a. volume, source, and analysis of dewatered sludge
b. date, time, pH and duration after mixing, duration and temperature during
heating, on a per batch basis
c. name and location of PFRP sludge disposal site or recipient, volume applied or
received, and intended use
An annual summary report (three copies) of the records required above shall be submitted
on or before March 1 of the following year by City of Statesville to the following address:
NC Division of Environmental Management
Water Quality Section
Facility Assessment Unit
PO Box 29535
Raleigh, NC 27626-0535
3

3. The City of Statesville shall present to each recipient of stabilized sludge written
information that clearly states that stabilized sludge cannot be used on areas where root or
leaf crops for direct human consumption are to be grown within one (1) year of the last
application of sludge to the site. The City of Statesville shall also include written
recommendations to the compost recipients for satisfactory uses of compost material such
as horticulture, silvicultural, other agricultural uses not specifically'prohibited, etc.
4'. Noncompliance Notification:.
The Permittee shall report by telephone to the Mooresville Regional Office, telephone no.
704/ 663-1699, as soon as possible, but in no case more than 24 hours or on the next
working day following the occurrence or first knowledge of the occurrence of any of the
following:
a. Any occurrence with the sludge program which results in the stabilizing of
significant amounts of wastes which are abnormal in quantity or characteristic.
b. Any failure of the sludge program resulting. in a discharge of wastes to receiving
waters.
C. Any time that self -monitoring information indicates that the facility has gone out of
compliance with the conditions and limitations of this permit or the parameters on
which the system was designed.
d. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate sludge treatment.
e. Any leakage or spillage that occurs during the transfer or transport of the sludge
material.
Persons reporting such occurrences by telephone shall also file a written report in letter
form within 15 days following first knowledge of the occurrence. This report must outline
the actions taken or proposed to be taken to ensure that the problem does not recur.
IV. GROUNDWATER REQUIREMENTS
1. Any groundwater quality monitoring as deemed necessary by the Division of
Environmental Management shall be provided.
1. The Permittee or his designee shall inspect the sludge storage, transport, and composting
facilities to prevent malfunctions and deterioration, operator errors and discharges which
may cause or lead to the release of wastes to the environment, a threat to human health, or a
nuisance. The Permittee shall keep an inspection log or summary including at least the date
and time of inspection, observations made, and any maintenance, repairs, or corrective
actions taken by the Permittee. This log of inspections shall be maintained by the Permittee
for a period of three years from the date of the inspection and shall be made available upon
request by the Division of Environmental Management or other permitting authority.
4

2. Any duly authorized officer, employee, or representative of the Division of Environmental
Management may, upon presentation of credentials, enter and inspect any property,
premises or place on or related to the composting facility and facility at any reasonable time
for the purpose of determining compliance with this permit; may inspect or copy any
records that must be kept under the terms and conditions of this permit; or may obtain
samples of groundwater, surface water, or leachate.
► 1; IN I) 1►
1. This permit shall become voidable unless the land application activities are carried out in
accordance with the conditions of this permit and in the manner approved by this Division.
2. This permit is effective only with respect to the nature and volume of wastes described in
the application and other supporting data.
3. This permit is not transferable. In the event there is a desire for the facilities to change
ownership or a name change of the Permittee, a formal permit request must be submitted to
the Division of Environmental Management accompanied by an application fee,
documentation from the parties involved, and other supporting materials as may be
appropriate. The approval of this request will be considered on its merits and may or may
not be approved
4. Failure to abide by the conditions and limitations contained in this permit may subject the
Permittee to an enforcement action by the Division of Environmental Management in
accordance with North Carolina General Statute 143-215.6.
5. The annual administering and compliance fee must be paid by the Permittee within thirty
(30) days after being billed by the Division. Failure to pay the fee accordingly may cause
the Division to initiate action to revoke this permit as specified by 15 NCAC 2H .0205
(c)(4).
6. The issuance of this permit does not preclude the Permittee from complying with any and
all statutes, rules, regulations, or ordinances which may be imposed by other government
agencies (local, state, and federal) which have jurisdiction.
7. A set of approved documents for the subject project must be retained by the applicant for
the life of the project.
8. The Permittee, at least six (6) months prior to the expiration of this permit, shall request its
extension. Upon receipt of the request, the Commission will review the adequacy of the
facilities described therein, and if warranted, will extend the permit for such period of time
and under such conditions and limitations as it may deem appropriate.
5

9. This permit may be modified or reissued to incorporate any conditions, limitations and
monitoring requirements the Division of Environmental Management deems necessary in
order to adequately protect the environment and public health.
Permit issued this the 18th day of March 1992
� LINA ENVIRONMENTAL MANAGEMENT COMMI lSSION
George Everett, ' ec r
Division of En o en ana ement
By Authority of a Enviro a tal Management Commission
Permit No. WQ0006245
Rl

Permit No. WQ0006245
March 18,1992
Engineer's Certification
as a duly registered Professional Engineer in the State of North
Carolina, having been authorized to observe (periodically, weekly, full time) the construction of the
project, for the
- Project Name 9 Location
Permittee hereby state that, to the best of my abilities, due care and diligence was used in the observation
of the construction such that the construction was observed to be built within substantial compliance and
intent of the approved plans and specifications.
Signature
Date
Registration No.
7

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4•tatjees-
t lie
August 24, 1989
Environmental Management Divison
Groundwater Section
P. 0. Box 27687
Raleigh, NC 27611-7687
RE: WWTP Landfill Wells Analyses
Permit #13849
Dear Sirs:
11fater/Wastewater 01reatment Vlants
784-878-3438
Please find enclosed the results of three (3) of our four (4)
landfill wells, sampled July 17, 1989, at our Third Creek WWTP,
NC0020591. Due to the failure of the screen in Well #2, we were unable
to sample this well. Construction for a new well is now underway.
Our Fourth Creek WWTP Lab, #181, ran the onsite measurements,
including pH. All other parameters were contracted out to Bold Research
Lab in Charlotte.
After reviewing the results from the above sampling, we found
all three wells were in non-compliance for Total Coliform, Total
Dissolved solids and TOC. Therefore, we resampled on August 22, 1989.
Our Fourth Creek WWTP Lab ran the T. Dissolved Solids and pH. Our
Water Plant Lab, #37-620 analyzed the T. Coliform test. The TOC's were
performed by Bold Research Lab. We are pleased that these results show
that we are in compliance on these parameters, (results enclosed).
We believe that our high values were due to sampling procedure
error. Upon discussion with Mr. Jesse Wells of the Mooresville office,
we decided to purge our wells one day, and take samples the next.
This new procedure improved the quality and clarity of our samples.

August 24, 1989
WWTP Landfill Wells Analyses
Permit #13849
Page 2
Please find attached the GW-59 forms for the results of all
parameters for both sampling events.
Sincerely,
L. F. "Joe" Hudson, Director
Water/Wastewater Treatment
LFH/sg
Enclosures

L ab 81) Bold Rec4arcl�
ANALYTICAL TEST, a CONSULTING SERVICES
P.O. BOX 31486 -CHARLOTTE, NC 2f ­ TELEPHON...* [phone] -FAX: [phone]
LAB SAMPLE NO-(S): 405B1-3
P.O. NO.:
RECEIVED FROM:
NAME:
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLE(s) of WATER
MARKED: A: 3RD CRREK WELL #1
C:3RD CREEK WELL #4
SAMPLE/TEST NO. 1
DATE OF REPORT: 0 8/10/8 9
DATE RECEIVED: 07/17/89
CUSTOMER NO.: 6084
TELEPHONE NO.: 704-878-3438
v
T-8
B: 3RD CREEK WELL 0000
D:
A:B1 B: B2 C: B3 D:
ANALYSIS UNITS
pH
TOTAL RESIDUE
(m
TOTAL VOLATILE RESIDUE
(mg/L'
TOTAL NONFILT. RESIDUE
(mg/L)
TOTAL DISSOLVED RESIDUE
(mg/L)'
/128
6TE2F
7936
BOD
(mg/L)
COD
(mg/L)
AMMONIA AS N
(mg/L)
<
< I
<
TOTAL KJELDAHL NITROGEN
(mg/L)
NITRATE AS N
(mg/L)1.9s-
TOTAL PHOSPHATE ASP
(mg/L)
CHLORIDE AS Cl-
(mg/L)
9.9
8.9
5.
OIL & GREASE
(mg/L)
CYANIDE TOTAL,
TOTAM
c/1uUmL
T.N.T.C.—
T.N.T.C.
T.N.T.C.
METALS UNITS
ARSENIC
(mg/L)
SELENIUM
(mg/Li
CADMIUM i�vll','.-' A�, -f,,
(mg/L) <0.02
<0.02
<10.02
CHROMIUM
(mg/L;
COPPER
(mg,
LEAD :4
(mc �__l
NICKEL
(mg/L)
ZINC
(mg/L)
.02
.03
.05
MERCURY
(mg/L)
APPROVED BY: Jeffrey K. O'Ham, Manager
303 MEACHAM ST. e CHARLOTTE, NC 28203

[mold 4-- S-- `��RI�IGP,ROOK RD. o o n
Incorporated
P (Z! 8
CHARLOTTE N. C.
ANALYTICAL TESTING & CONSULTING SERVICES NEW PHONE 2823I
NO.: p04} 521.4I83
P.O. BOX 31486 • CHARLOTTE, NC 28231 • TELEPHONE [phone] • FAX: [phone] FAX [phone]
LAB SAMPLE NO.(S): 405B1-3
P.O. NO.:
RECEIVED FROM:
NAME:
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLE(s) of: WATER
MARKED: A:3RD CREEK WELL #1
C:3RD CREEK WELL #4
SAMPLE/TEST NO. , A: „
DATE OF REPORT: 0 8 / 18 / 8 9
DATE RECEIVED: 0 7 / 17 / 8 9
CUSTOMER NO.: 6084 -
TELEPHONE NO.: 704-878-3438
t�,�'\.
01
B' 3RD CREEK WELL
D:
B C', In.
ANALYSIS UNITS
H
L-
TOTAL RESIDUE
m /L
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L
BOD
m /L
COD
m /L
AMMONIA AS N
m /L
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE ASP
CHLORIDE AS Cl-
m /L
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL
m /L
TOTAL
METALS UNITS
ARSENIC
(mg/L)
SELENIUM
(mg/L)
/,` :'�
"_••j
CADMIUM
(mg/L)
CHROMIUM
Im9/Lj
COPPER
(mg/L)
LEAD
(mg/L)
NICKEL
(mg/L);j'
ZINC
(mg/L)
vV�,
MERCURY
(mg/L)
0J
APPROVED BY: "�� Jeffrey K. O'Ham, Manager 303 MEACHAM ST. • CHARLOTTE, NC 28203

Bold Research Labs
Incorporated
ANALYTICAL TESTING & CONSULTING SERVICES
P.O. BOX 31486 • CHARLOTTE, NC 28231 . TELEPHONE [phone] . FAX: [phone]
LAB SAMPLE N0.(S): 5 6 5B 1-3
P.O. NO.:
RECEIVED FROM:
NAME: CAROL WAUGH
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLES) of: WATER
MARKED: A:3RD CREEK #1
C:3RD CREEK #4
SAMPLE/TEST NO. 1
DATE OF REPORT: 0 8/ 2 2/ 8 9
DATE RECEIVED: 08/22/89
CUSTOMER NO.: 6084
TELEPHONE NO.: 704-878-3438
t
IZVil
B: 3RD CREEK #3
D: GftV
A:R _ 1 B:R _ 9 C:R _ R D:
ANALYSIS UNITS
H
TOTAL RESIDUE
m /L
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L
_
BOD
m /L
COD
m /L
AMMONIA AS N
m /L .
_
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE AS P
m /L
CHLORIDE AS Cl-
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL '
m /L
TOTAL ORGANIC CARBON
MG/L
2
3
4
METALS UNITS
ARSENIC
SELENIUM
(mg/L)
CADMIUM
(mg/L)
Sit
CHROMIUM
(mg/L)
c
�k
COPPER
(mg/L)
LEAD
(mg/L)
C.
%
NICKEL
(mg/L)
ZINC
(mg/L)
V.
MERCURY
(mg/L)
j-
z
_
yof
APPROVED BY: Jeffrey K. O'Ham, Manager 303 MEACHAM ST. • CHARLOTTE, NC 28203

Bold Labs
Incorporated
ANALYTICAL TESTING & CONSULTING SERVICES
P.O. BOX 31486 • CHARLOTTE, NC 28231 . TELEPHONE [phone] . FAX: [phone]
LAB SAMPLE NO.(S): 565B1-3
P.O. NO.:
RECEIVED FROM:
NAME: CAROL WAUGH
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLES) of: WATER
MARKED: A:3RD CREEK #1
C:3RD CREEK #4
SAMPLE/TEST NO. j
DATE OF REPORT: 0 8/ 2 2/ 8 9
DATE RECEIVED: 0 8/ 2 2/ 8 9
CUSTOMER NO.: 6084
TELEPHONE NO.: 704-878-3438
B: 3RD CREEK
D:
AB-1 BR-7 CRR3�LC���° D.
ANALYSIS UNITS
H
TOTAL RESIDUE
m /L
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L
_
BOD
m /L
COD
m /L
AMMONIA AS N
m /L
_
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m lL
TOTAL PHOSPHATE AS P
m /L
CHLORIDE AS Cl-
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL
m /L
TOTAL ORGANIC CARBON
MG/L
2
3
4
METALS UNITS
ARSENIC
(mg/L)
SELENIUM
(mg/L)
, }.;
: ;
CADMIUM
(mg/L)
CHROMIUM
(mg/L)
c
:.
COPPER
(mg/L)
> ;,. ` r'
,
LEAD
(mg/L)
NICKEL
(mg/L)
ZINC
(mg/L)
V.
MERCURY
(mg/L)
APPROVED BY: Z Jeffrey K. O'Ham, Manager 303 MEACHAM ST. 9 CHARLOTTE, NO 28203

Laos
ANALYTICAL TESTig(j d CONSULTING SERVICES
P.O. BOX 31486 • CHARLOTTE, NC 26,1) : TELEPHONF [phone] . FAX: [phone]
LAB SAMPLE NO.(s): 4 0 5 B 1— 3
P.O. NO.:
RECEIVED FROM:
NAME:
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLE(s) of: WATER
MARKED: A:3RD CRREK WELL #1
C:3RD CREEK WELL #4
SAMPLE/TEST NO. 1
DATE OF REPORT: 0 8 / 10 / 8 9
DATE RECEIVED:
0 7 / 17 / 8 9
CUSTOMER NO.:
6084
TELEPHONE NO.:
704-878-3438
B: 3RD CREEK
WEL(LRC#i
D:
A: B 1 B: B 2 C: B 3 D:
ANALYSIS UNITS
H
TOTAL RESIDUE
mc....
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L)
-93
BOD
m /L
COD
m /L
AMMONIA AS N
m /L
1
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE ASP
m /L
CHLORIDE AS Cl-
m !L
OIL & GREASE
m /L
CYANIDE TOTAL
m /L
0
c
:N.
T.N.T.C.
METALS UNITS
ARSENIC .�%-. i ;i . ; `
(mg/L)
SELENIUM
(mg/L;
CADMIUM
(mg/L) < . 0 2
<0 .0 2
<0.0 2
CHROMIUM l.- 6J'., .;,^^,
(mg/L)
COPPER {° '` r, `� `�
(mg;— —
LEAD
NICKEL 'i
(m91L) .
ZINC -"
(mg/L)
.02
.03
.05
MERCURY ``? :%
(mg/L)
f
APPROVED BY: Jeffrey K. O'Ham, Manager
303 MEACHAM ST. • CHARLOTTE, INC 28203

ld ReseaLabe
4 SP121t`lGP,ROOK RD. (Z►P; 2821:
IncorporatedP O. COX 31486�—
CHA"RLOTTE, N, C. 28231
ANALYTICAL TESTING & CONSULTING SERVICES MEW PHONE NO.: ppq? 5214183
P.O. BOX 31486 • CHARLOTTE, NC 28231 . TELEPHONE [phone] • FAX: [phone] �7041 525 p-009
LAB SAMPLE NO.(s): 4 05 B 1-3 DATE OF REPORT: 0 8 / 18 / 8 9
P.O. NO.: DATE RECEIVED:
07/17/89
RECEIVED FROM: CUSTOMER NO.:
6084
NAME: TELEPHONE NO.:
ORG. CITY OF STATESVILLE/FOURTH CRK 704-878-3438_y.-
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE
NC 28677
SAMPLE(s) of WATER
irla,9yT�r'6
�
MARKED: A: B:
°
3RD CREEK WELL #1 3RD CREEK W�.L 1;r#F3)''j'',
C:3RD CREEK WELL #4 D:
SAMPLE/TEST NO. , A' — _ A. _ (I. n.
ANALYSIS UNITS
H
TOTAL RESIDUE
m /L
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L
BOD
m /L
COD
m /L
AMMONIA AS N
m /L
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE ASP
m /L
CHLORIDE AS Cl-
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL
m /L
TO
METALS UNITS
�..
�•.r"J'~
ARSENIC
SELENIUMff"
(mg
(mg/L)
CADMIUM
CHROMIUM
COPPER
LEAD
NICKEL
(mg/L)
(mg/L)
(mg
(mg/L)
(mg/L)
qJ
_
ZINC
(mg/L)
J`°
MERCURY
(mg/L)
_ . •—�
n i i
r
APPROVED BY: ► Jeffrey K. O'Ham, Manager 303 MEACHAM ST. e CHARLOTTE, NC 28203

W Research Labs
Incorporated
ANALYTICAL TESTING 8 CONSULTING SERVICES
P.O. BOX 31486 o CHARLOTTE, NC 28231 • TELEPHONE [phone] . FAX: [phone]
LAB SAMPLE NO.(S): 565B1-3
P.O. NO.:
RECEIVED FROM:
NAME: CAROL WAUGH
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLES) of:- WATER
MARKED: A:3RD CREEK #1
C:3RD CREEK #4
SAMPLE/TEST NO. j
DATE OF REPORT: 0 8/ 2 2/ 8 9
DATE RECEIVED: 08/22/89
CUSTOMER NO.: 6084
TELEPHONE NO.: 704-878-3438
B: 3RD CREEK #3
D:
AB-1 B:B-2 C:B-3 D:
ANALYSIS UNITS
-
H
;, 1 - Ix;11.,
TOTAL RESIDUE
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
-
TOTAL DISSOLVED RESIDUE
m /L
BOD
m /L
a� rn34�
COD
m /L
AMMONIA AS N
m /L
_
—
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE ASP
m /L
CHLORIDE AS Cl-
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL
m /L
TOTAL ORGANIC CARBON
MG/L
2
3
4
METALS UNITS
ARSENIC
(mg/L)
SELENIUM
(mg/L)
, h'
..i',�
CADMIUM
(mg/L)
CHROMIUM
(mg/L)
COPPER
(mg/L)
LEAD
(mg/L)
NICKEL
(mg/L)
ZINC
(mg/L)
MERCURY
(mg/L)
APPROVED BY: X Jeffrey K O'Ham, Manager 303 MEACHAM ST. • CHARLOTTE, NC 28203

uom iiesearmll Laos
I; ,;:c„ porated J
ANALYTICAL TESTJg0 d CONSULTING SERVICES
P.O. BOX 31486 • CHARLOTTE, NC 26z 1) ; TELEPHONe [phone] . FAX: [phone]
LAB SAMPLE NO-N: 405B1-3
P.O. NO.:
RECEIVED FROM:
NAME:
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLE(s) of: WATER
MARKED: A:3RD CRREK WELL #1
C:3RD.CREEK WELL #4
SAMPLE/TEST NO. 1
DATE OF REPORT: 0 8 / 10 / 8 9
DATE RECEIVED: 0 7 / 17 / 8 9
CUSTOMER NO.: 6084
TELEPHONE NO.: 704—�878-341138
B: 3RD CREEK WE #•34w��, t,tit 5.
D:
A: B 1 B: B 2 C: B 3 D:
ANALYSIS UNITS
H
TOTAL RESIDUE
..
TOTAL VOLATILE RESIDUE
im
TOTAL NONFILT. RESIDUE
LTOTAL
DISSOLVED RESIDUE
L)
BOD
m /L
COD
m /L
AMMONIA AS N
(_mg/L)<
< 1
TOTAL KJELDAHL NITROGEN .
m /L
NITRATE AS N
m !L
TOTAL PHOSPHATE ASP
m /L
CHLORIDE AS Cl-
m !L
OIL & GREASE
m /L
CYANIDE TOTAL
m /L
c OmL
T.C.
METALS UNITS
ARSENIC
(mg/L)_
SELENIUM
(mg/L.'.
CADMIUM , ;•,Y'
(mg/L)
. 0 2
0. 0 2
< 0. 0 2
CHROMIUM /,- 6�' ,' ; �, `'
(mg/L)�
COPPER {° '�; �. , , r,;� -�j
(mg/ _
LEAD
(ME; _I
NICKEL �.' y�,,%:,'r• ° f .
(mg/L)
ZINC :'r
(mg/L)
.02
.03
.05
MERCURY `; . . • , %
(mg/L)
APPROVED BY: — Jeffrey K. O'Ham, Manager
303 MEACHAM ST. • CHARLOTTE, NC 28203

Bold Research La�bs,
`1' S'IZI�iGP,ROOK RD. �Z1P: zg2j;
Incorporated p O BMX 31 6-_
CHAPLp7TE, N, C
ANALYTICAL TESTING & CONSULTING SERVICES NEW PNONE NO,; 28231
fAX [phone]-Nog 274�3
P.O. BOX 31486 •CHARLOTTE, NC 28231 •TELEPHONE [phone] . FAX: [phone]
LAB SAMPLE NO.(s): 405B1-3
P.O. NO.:
RECEIVED FROM:
NAME:
ORG. CITY OF STATESVILLE/FOURTH CRK
ADD: U.S. 70 EAST OFF BELL ROAD
P.O. BOX 1111
STATESVILLE NC 28677
SAMPLE(s)of WATER
MARKED: A:3RD CREEK WELL #1
C:3RD CREEK WELL #4
SAMPLE/TEST NO. ,
DATE OF REPORT. 0 8 / 18 / 8 9
DATE RECEIVED: 0 7 / 17 / 8 9
CUSTOMER NO.: 6084 -
TELEPHONE NO.: 704-878-3438
B' 3RD CREEK WEaV1f�s�°° �
A-- A. (I•
i
D-
-
ANALYSIS UNITS
H
TOTAL RESIDUE
m /L
TOTAL VOLATILE RESIDUE
m /L
TOTAL NONFILT. RESIDUE
m /L
TOTAL DISSOLVED RESIDUE
m /L
BOD
m /L
COD
m /L
AMMONIA AS N
m /L
TOTAL KJELDAHL NITROGEN
m /L
NITRATE AS N
m /L
TOTAL PHOSPHATE ASP
m /L
CHLORIDE AS Cl-
m /L
OIL & GREASE
m /L
CYANIDE, TOTAL
m /L
TOT
METALS UNITS
ARSENIC
SELENIUM (mg/L)
{ 1' ..i
.,
CADMIUM
m
( g/L )
�f
_
CHROMIUM
(mg/L)
I� ....
COPPER
(mg/L)
LEAD
(mg/L)
NICKEL
(mg/L)
�,
ZINC
(mg/L)
MERCURY
(mg/L)
n i
APPROVED BY: I Jeffrey K. O'Ham, Manager 303 MEACHAM ST. • CHARLOTTE, NC 28203

A I
.a.
i N 4Ji
1
I� N Taraftna 28677
May 1.8 , 1989
Mr. Jesse Wells
Div. of Environments:': Management
P . 0. Bo:: 950
Mooresville, NC 281.15-0950
RE. Notice of Violation Response
Permit No. 13849
Dear Mr. Wells:
Water/Wastemater Greatment 111ants
784-878-3438
^"T• OF 19A
RESOURCE? Al,T_,
COMMUNITY -�IITE
MAY 2
OFFICE"
DIVISIN OF EPPUF,': P T.--1 i.: T-G"!i71J
hi:l0;~ESVIi�E F.E�I?fU�E QrFII;I:
This let-Cer is in response to the Notice of Violation
received from your office May 1.2, 1989.
As instructed, we have resampled the appropriate wells and
will submit the results to your office as soon as we receive
them. We believe a possible explanation may be due to some
difficulties experienced with the sampling equipment during
this sampling event.
If you have any questions, please call me at [phone].
Sincerely,
G. ) "Joe" Hudson, Director
Water/Wastewater Treatment
cc: D. Crowson
H. Anderson
S. Lambert

State of North Carolina
Department of Natural Resources and Community Development
Mooresville Regional Office
James G. Martin, Governor Albert F. Hilton, Regional Manager
William W. Cobey, Jr., Secretary
DIVISION OF ENVIRONMENTAL MANAGEMENT
May 12, 1989
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. Peter T. Connet, City Manager
City of Statesville
Post Office Box 1111
Statesville, North Carolina 28677
Subject: Notice of Violation
15 NCAC 2L Classification and Water
Quality Standards Applicable to the
Gr-oundwaters
City.bf Statesville
Third Creek WWTP
Permit No. 13849
Iredell County, N. C.
Dear Mr. Connet:
Chapter 143, North Carolina General Statutes, authorizes and
directs the Environmental Management Commission of the
Department of Natural Resources and Community Development to
protect and preserve the water and air resources of the State.
The Division of Environmental Management has the delegated
authority to enforce adopted pollution control rules.
Based upon a review of your groundwater compliance
monitoring data submitted on May 1, 1989 as a requirement of
Permit No. 13849, the Division has reason to believe that the
permitted activities have resulted in noncompliance with 15 NCAC
2L Classifications and Water Quality Standards Applicable to the
Groundwater. Condition No. 9 of your permit states:
"The issuance of this permit shall not relieve the Permittee
of the responsibility for damages to surface or groundwaters
resulting from the operation of this facility."
Specific violations of 15 NCAC 2L were as follows:
919 North Main Street, P.O. Box 950, Mooresville, N.C. 28115-0950 • Telephone [phone]
An Equal Opportunity Affirmative Action Employer

2L Standard
1. Monitoring Well No. 1 -
Total Coliform - 6300/100 ml Total Coliform - 1/100 ml
2. Monitoring Well No. 2 -
"NO"3 as N - 13.4 mg/l Nitrate: (as N) - 10 mg/l
It is requested a written response be submitted to this
Office by no later than fifteen (15) days after receipt of this
Notice explaining reasons for the noncompliance.
In the interim, the City of Statesville must perform the
following:
Resample the two monitoring wells for the parameters noted
in noncompliance.
This information.must be submitted within thirty (30) days
after receipt of this letter.
If continued groundwater.quality.standard violations are
verified the City of Statesville must undertake to define the
horizontal and vertical extent of the contamination and propose
corrective action.
Failure to respond within the time specified and to
voluntarily achieve compliance may result in the recommendation
of enforcement action, including the issuance of a special order
against you under the authority of General Statute 143-215.2;
and/or revocation of your permit.
Your response and/or questions should be first directed to
Jesse W. Wells, Hydrogeologic Technician, if unavailable then to
Eric J. Klingel, Regional Hydrogeologic Supervisor of the
Mooresville Regional Office at [phone].
Sincerely,
Brenda J. Smit , . G.
Regional Supervisor
cc: Office of Legal Affairs
Bob Cheek
D. Rex Gleason
JWW:sju