WQ0006245_Regional Office Historical File Pre 2018 (4)

Water Resources May 10, 2017
Environmental Quality
Mr. L.F. Hudson, Jr., Director of Water Resources
City of Statesville
P.O. Box 1111 .
Statesville, North Carolina 28687
Mr. Hudson,
F L
9
0- . OOPER
Governor
MICHAEL S. REGAN -
Secretary
S. JAY ZIMMERMAN
Director
Subject: 2017 Compliance Inspection Report
City of Statesville N-Viro Processing and
Sta—Lime Distribution Program
Permit WQ0006245
Distribution of Residuals (503)
Iredell County
On May 3rd, 2017, the Mooresville Regional Office (MRO) completed a Compliance Inspection for the above stated
facility. The inspection included a records review and the -'residuals processing and storage at the Fourth Creek.
WWTP. The MRO would like to thank Andy Smith for his time during the inspection
Log entries for the lime stabilization analyses'and cross referenced records for the pH meter calibration were well.
organized. The material storage area has been upgraded and there was no significant odor present during the
inspection visit. The residual material was also well organized on the storage pad area.
A review:of the laboratory analysis presented by Prism labs indicates the lab reporting of the Sodium Absorption
Ration (SAR) calculations, continues to :be inconsistently presented. The entire. calculation should be presented for
the laboratory analytical data and not the general formula.
Overall, the facility was found to be compliant with the permit.,
The report should be self-explanatory. However, should you have any questions, please feel free to contact me at
104-235-2198 or by email at [e-mail].
Sincerely,
• E ardld�o�.yeologis
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Enclosure: Inspection Report
CC: Mr. Andy Smith, Town of Statesville (email)
State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1610 East Center Avenue, Suite 30r I Mooresville,.North Carolina 28115
704-663-1699

0
Compliance Inspection Report
Permit: WQ0006245 Effective: 04/02/15 Expiration: 09/30/20 Owner: City of Statesville
SOC: Effective: Expiration: Facility: City of Statesville Sta-Lime Processing Facility .
County: Iredell 693 Bell Farm Rd
Region: Mooresville
Statesville NC 28687
Contact Person: Andy Smith Title: Phone: [phone]
Directions to Facility:
From the intersection of 1-77 North and NC Hwy. 70, travel east on NC Hwy. 70 to Bell Farm Road. Turn left and travel north on Bell
Farm Road to the Fourth Creek WWTP. The WWTP is on the right-hand side of the road.
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 05/03/2017 Entry Time 09:54AM
Primary Inspector: Edward Watson
Secondary Inspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Distribution of Residual Solids (503)
Facility Status: 0 Compliant ❑ Not Compliant
Question Areas:
Miscellaneous Questions Record Keeping
Pathogen and Vector Attraction Storage
(See attachment summary)
Exit Time: 11:30AM
Phone:
Inspection Type: Compliance Evaluation
0 Treatment
Page: 1

Permit: WQ0006245 Owner - Facility: City of Statesville
Inspection Date: 05103/2017 _ _ Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
On May 3rd, 2017, a compliance inspection was performed by staff of the Mooresville Regional Office(MRO.)
pH calibration and chemical storage are now being handled by the on site laboratory staff.
The storage area was clean and there was a significant reduction in odor from the previous year's inspection. Operators logs
were in good. order and up-to-date.
Laboratory analytical data should also present the Sodium Absorbtion Ratio (SAR) calculations.
Page: 2

.z'
4
Permit: WQ0006245 Owner -Facility: City of Statesville
Inspection Date: 05/03/2017 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Type Yes No NA NE
Land Application ❑
Distribution and Marketing
Record Keeping
Yes No NA NE
Is GW monitoring being conducted, if required?
❑ 0 ❑ ❑
Are GW samples from all MWs sampled for all required parameters?
❑ ❑ 0 ❑
Are there any GW quality violations?
❑ ❑ 0 ❑
Is GW-59A certification form completed for facility?
❑ ❑ N ❑
Is a copy of current permit on -site?
E ❑ ❑ ❑
Are current metals and nutrient analysis available?
N ❑ ❑ ❑
Are nutrient and metal loading calculating most limiting parameters?
E ❑ ❑ ❑
a. TCLP analysis?
N ❑ ❑ ❑
b. SSFA (Standard Soil Fertility Analysis)?
❑ ❑ ❑
Are PAN balances being maintained?
0 ❑ ❑ ❑
Are PAN balances within permit limits?
N ❑ ❑ ❑
Has land application equipment been calibrated?
❑ ❑ ❑
Are there pH records for alkaline stabilization?
E ❑ ❑ ❑
Are there pH records for the land application site?
❑ ❑ ❑
Are nutrient/crop removal practices in place?
❑ ❑ ❑ E
Do lab sheets support data reported on Residual Analysis Summary?
K ❑ ❑ ❑
Are hauling records available?
❑ ❑ ❑
Are hauling records maintained and up-to-date?
❑ ❑ ❑
# Has permittee been free of public complaints in last 12 months?
0 ❑ ❑ ❑
Has application occurred during Seasonal Restriction window?
❑ E ❑ ❑
Comment: Land Application questions for specific field are not applicable for this site.
Pathogen and Vector Attraction
Yes No NA NE
a. Fecal coliform SM 9221 E (Class A or B)
❑ ❑ E ❑
Class A, all test must be <1000 MPN/dry gram
❑
Geometric mean of 7 samples per monitoring period for class B<2.0*10E6 CFU/dry gram
❑
Fecal coliform SM 9222 D (Class B only)
❑ ❑ ❑ ❑
Geometric mean of 7 samples per monitoring period for class B<2.0'10E6 CFU/dry gram
❑
b. pH records for alkaline stabilization (Class A)
0 ❑ ❑ ❑
c. pH records for alkaline stabilization (Class B)
0 ❑ ❑ ❑
Temperature corrected
❑
d. Salmonella (Class A, all test must be < 3MPN/4 gram day)
E ❑ ❑ ❑
Page: 3

i
Permit: WQ0006245 Owner - Facility: City of Statesville
Inspection Date: 05/03/2017 Inspection Type: Compliance Evaluation Reason for Visit: Routine
e. Time/Temp on: i ❑ ❑ ❑
Digester (MCRT)
Compost ❑
Class A lime stabilization
f. Volatile Solids Calculations ❑ ❑ 0 ❑
g. Bench -top Aerobic/Anaerobic digestion results ❑ ❑ 0 ❑
Comment: PVAR is met through lime stabilization. Further pathogen reduction is achieved by density of
Fecal Coliform bacteria under 15A NCAC 02T A 16(b)(2)(B) the density of Salmonella So.
bacteria is less than three Most Probably Number (MPN) per four grams of total solids.
Treatment Yes No NA NE
Check all that apply
Aerobic Digestion
Anaerobic Digestion
❑
Alkaline Pasteurization (Class A)
Alkaline Stabilization (Class B)
❑
Compost
❑
Drying Beds
❑
Other
Comment: Time and .pH data was available for review and the records appear to be in order.
As noted in the AR comments, this facility did not process material until the beginning of April
due to construction work being performed at the plant in the beginning of the calendar year.
Page: 4

3
Water Resources
Environmental Quality
Mr. L.F. Hudson, Jr., Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Mr. Hudson,
May 10, 2017
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
S. JAY ZIMMERMAN
Director
Subject: 2017 Compliance Inspection Report
City of Statesville N-Viro Processing and
Sta—Lime Distribution Program
Permit WQ0006245
Distribution of Residuals (503)
Iredell County.
On May 3rd, 2017, the Mooresville Regional Office (MRO) completed a Compliance Inspection for the above stated
facility. The inspection included a records review and the residuals processing and storage at the Fourth Creek
WWTP. The MRO would like to thank Andy Smith for his time during the inspection.
Log entries for the lime stabilization analyses and cross referenced records for the pH meter calibration were well
organized. The material storage area has been upgraded and there was no significant odor present during the
inspection visit. The residual material was also well organized on the storage pad area.
A review of the laboratory analysis presented by Prism labs indicates the lab reporting of the Sodium Absorption
Ration (SAR) calculations, continues to be inconsistently presented. The entire calculation should be presented for
the laboratory analytical data and not the general formula.
Overall, the facility was found to be compliant with the permit.
The report should be self-explanatory. However, should you have any questions, please feel free to contact me at
704-235-2198 or by email at [e-mail].
Sincerely,
Edward Watson, Hydrogeologist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Enclosure: Inspection Report
CC: Mr. Andy Smith, Town of Statesville (email)
State of North Carolina l Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1610 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115
704-663-1699

ar�
w
Water Resources
Environmental Quality
Mr. L.F. Hudson, Jr., Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Mr. Hudson,
May 10, 2017
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
S. JAY ZIMMERMAN
Director
Subject: 2017 Compliance Inspection Report
City of Statesville N-Viro Processing and
Sta—Lime Distribution Program
Permit WQ0006245
Distribution of Residuals (503)
Iredell County
On May 3rd, 2017, the Mooresville Regional Office (MRO) completed a Compliance Inspection for the above stated
facility. The inspection included a records review and the residuals processing and storage at the Fourth Creek
WWTP. The MRO would like to thank Andy Smith for his time during the inspection.
Log entries for the lime stabilization analyses and cross referenced records for the pH meter calibration were well
organized. The material storage area has been upgraded and there was no significant odor present during the
inspection visit. The residual material was also well organized on the storage pad area.
A review of the laboratory analysis presented by Prism labs indicates the lab reporting of the Sodium Absorption
Ration (SAR) calculations, continues to be inconsistently presented. The entire calculation should be presented for
the laboratory analytical data and not the general formula.
Overall, the facility was found to be compliant with the permit.
The report should be self-explanatory. However, should you have any questions, please feel free to contact me at
704-235-2198 or by email at [e-mail].
Sincerely,
Edward Watson, Hydrogeologist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Enclosure: Inspection Report
CC: Mr. Andy Smith, Town of Statesville (email)
State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations
Mooresville Regional Office 1610 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115
704-663-1699

Compliance Inspection Report
Permit: WQ0006245 Effective: 04/02/15 Expiration: 09/30/20 Owner: City of Statesville
SOC: Effective: Expiration: Facility: City of Statesville Sta-Lime Processing Facility and E
County: Iredell 693 Bell Farm Rd
Region: Mooresville
• Statesville NC 28687
Contact Person: Andy Smith Title: Phone: [phone]
Directions to Facility: .
From the intersection of 1-77 North and NC Hwy. 70, travel east on NC Hwy. 70 to Bell Farm Road. Turn left and travel north on Bell
Farm Road to the Fourth Creek WWTP. The WWTP is on the right-hand side of the road.
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 05/03/2017 Entry Time: 09:54AM
Primary Inspector: Edward Watson
Secondary Inspector(s):
Reason for Inspection: Routine
Permit Inspection Type: Distribution of Residual Solids (503)
Facility Status: Compliant ❑ Not Compliant
Question Areas:
Miscellaneous Questions Record Keeping
Pathogen and Vector Attraction Storage
(See attachment summary)
Exit Time: 11:30AM
Phone:
Inspection Type: Compliance Evaluation
E Treatment
Page: 1

.L4
Permit: WQ0006245 Owner - Facility: City of Statesville
Inspection Date: 05/03/2017 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
On May 3rd, 2017, a compliance inspection was performed by staff of the Mooresville Regional Office(MRO.)
pH calibration and chemical storage are now being handled by the on site laboratory staff.
The storage area was clean and there was a significant reduction in odor from the previous year's inspection. Operators logs
were in good order and up-to-date.
Laboratory analytical data should also present the Sodium Absorbtion Ratio (SAR) calculations.
Page: 2

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permit WQ0006245 Owner - Facility: City of Statesville
Inspection Date: 05/03/2017 Inspection Type: Compliance Evaluation Reason for Visit: Routine
e. Time/Temp on: 0 ❑ ❑ ❑
Digester (MCRT)
Compost ❑
Class A lime stabilization
f. Volatile Solids Calculations ❑ ❑ M ❑
g. Bench -top Aerobic/Anaerobic digestion results ❑ ❑ 0 ❑
Comment: PVAR is met through lime stabilization Further pathogen reduction is achieved by density of
Fecal Coliform bacteria under 15A NCAC 02T .116(b)(2)(B) the density of Salmonella sp.
bacteria is less than three Most Probably Number (MPN) per four -grams of total solids.
Treatment
Yes No NA NE
Check all that apply
Aerobic Digestion
Anaerobic Digestion
❑
Alkaline Pasteurization (Class A)
Alkaline Stabilization (Class B)
❑
Compost
❑
Drying Beds
❑
Other
Comment: Time and pH data was available for review and the records appear to be in order.
As noted in the AR comments this facility did not process material until the beginning of April
due to construction work being performed at the plant in the beginning of the calendar year.
Page: 4

Compliance Inspection Report
Permit: WQ0006245 Effective: 04/02/15 Expiration: 09/30/20 Owner: City of Statesville
SOC: Effective: Expiration: Facility: City of Statesville Sta-Lime Processing Facility
County: Iredell 693 Bell Farm Rd
Region: Mooresville
Statesville NC 28687
Contact Person: Andy Smith Title: Phone: [phone]
Directions to Facility:
From the intersection of 1-77 North and NC Hwy. 70, travel east on NC Hwy. 70 to Bell Farm Road. Turn left and travel north on Bell
Farm Road to the Fourth Creek WWTP. The WWTP is on the right-hand side of the road.
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 06/20/2016 Entry Time 01:OOPM
Primary Inspector: Edward Watson
Secondary Inspector(s):
Maria Schutte
Reason for Inspection: Routine
Permit Inspection Type: Distribution of Residual Solids (503)
Facility Status: Compliant ❑ Not Compliant
Question Areas:
Exit Time: 02:30PM
Phone:
Inspection Type: Compliance Evaluation
Miscellaneous Questions Record Keeping Treatment
Sampling Pathogen and Vector Attraction Storage
Wells
(See attachment summary)
Page: 1

U
Permit: WQ0006245 Owner - Facility: City of Statesville
Inspection Date: 06/20/2016 Inspection Type : Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
The permit is for a Class A Lime stabilized product. Material from the digester tank clean -out needs to be sent to an
appropriate land fill for disposal due to the significant amount of debris present.
Page: 2

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Permit: WQ0006245 Owner - Facility: City of Statesville
Inspection Date: 06/20/2016 Inspection Type : Compliance Evaluation Reason for Visit: Routine
e. Time/Temp on: M ❑ ❑ ❑
Digester (MCRT) ❑
Compost ❑
,Class A lime stabilization
f. Volatile Solids Calculations ❑ ❑ OR
g. Bench -top Aerobic/Anaerobic digestion results ❑ ❑ ❑
Comment: PVAR met throuqh lime stabilization ( time &pH)
Treatment
Check all that apply
Yes No NA NE
Aerobic Digestion ❑
Anaerobic Digestion ❑
Alkaline Pasteurization (Class A)
Alkaline Stabilization (Class B) ❑
Compost ❑
Drying Beds ❑
Other
Comment: Time and pH logs appear to be up to date. Stock bottles for pH buffers need to have the date
opened and expiration date noted on the bolttle.
Samplinq Yes No NA NE
Describe sampling:
Sampling shopuld be in accordance with permitted sampling plan.
Is sampling adequate? ❑ ❑ ❑
Is sampling representative? ❑ ❑ ❑
Comment: Material from the digester tank clean -out contains a significant amount of debris. This material
is to be sent to the appropriate land fill and not mixed with material intended to be land applied.
Page: 4

North Carolina Department of Environmental Quality
Pat McCrory
Governor
October 13, 2015
Jerry Byerly
Fourth Creek WWTP
693 Bell Farm Road
Statesville, NC 28625
Re: Termination of Hazardous Waste Requirements
City of Statesville Third Creek Wastewater Treatment Plant
Disposal Trenches
EPA ID # NCR 000 001 602
Dear Mr. Byerly:
Donald R. van der Vaart
Secretary
This is to notify you that the draft termination of RCRA monitoring and post -closure care as required
in the Administrative Order on Consent Docket #94-191 for the City of Statesville Third Creek Wastewater
Treatment Plant Disposal Trenches has been approved. This termination is for the RCRA monitoring and
post -closure care only and does not relieve you of any requirements imposed by any other permits, rules,
regulations, or laws. Not does this termination relieve you of your duty to comply with the North Carolina
Hazardous Waste rules.
The public comment period for the Draft Decision ended on October 5, 2015. No comments were received,
therefore this decision will be effective on the issue date, October 13, 2015.
A copy of this letter will be forwarded to our Financial Unit. They will address details concerning your
financial assurance under a separate letter.
If you have any questions, please contact Larry Stanley at [phone] or Larry. Stanleyna,ncdenr.Roy or
Bud McCarty at 919-707-8202 or Bud.McCarty(a,ncdenr.gov .
Sincerely,
Julie Woosle Chi
Y=
Hazardous Waste Section
Division of Waste Management, NC DEQ
Enclosures
cc: John E. Johnston, US EPA, Region 4 Ron Smith
Heather Goldman
Retha Gaither
Joe Hudson
Jane Murray
Chonticha McDaniel
Jenny Lopp
Larry Pressley
Larry Stanley
Brenda Fugett
Bud McCarty
1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone]Intemet: WWW_NcDENR.Gov _. .. .
An Equal Opportunity l Affirmative Action Employer — Made in part by recycled paper

NOTICE OF FINAL RCItA DECISION
FACILITY NAME: City of Statesville Third Creek Wastewater Treatment Plant Disposal Trenches
EPA ID Number: NCD 000 001 602
Location: 444 Third Creek Road
Statesville, North Carolina 28625
Facility Operator: City of Statesville
Facility Owner: City of Statesville
After due consideration of the facts applicable to the above named facility as they appear in the
Administrative Record and the requirements and policies expressed in the Federal Resource
Conservation and Recovery Act (RCRA) and applicable state regulations (15A NCAC 13A), the
Department has determined that the RCRA requirement including required monitoring and post -closure
care should be terminated.
In accordance with 40 CFR 124.15 as adopted in 15A NCAC 13A .0105, this termination will become
effective on October 13, 2015. Since no comments were received during the public comment period and
no changes have been made to the decision, there are no appeal rights under 40 CFR 124.19 as adopted
in 15A NCAC 13A .0105.
The Administrative Record, with respect to this determination, is maintained at the Department's offices,
217 West Jones Street, Raleigh, North Carolina 27603, and is available for public inspection between
the hours of 9:00 a.m. and 4:00 p.m. Monday through Friday. For further information on this permit
action or file room appointments, contact the File Room at [phone].
10)13 1,15-
Ju e S. Costey Date
Hazardous Waste Section

Termination of Monitoring and Post -closure Care Requirements
Third Creek Wastewater Treatment Plant disposal trenches
EPA ID NCR000001602
444 Third Creek Road, Statesville, NC, .
On March 8, 1995 the Department of Environment, Health and Natural Resources acting through
the its Division of Solid Waste Management entered into an Administrative Order on Consent
("Order"), Docket #94-191, with the City of Statesville Third Creek Wastewater Treatment Plant
(EPA ID # NCR 000 001 602).
The Order was to require proper management of landfilled sludge that exceeded the regulatory
limits of cadmium.
A Closure certification was submitted on September 2, 1997 and closure with waste in place was
approved on June 22, 1998. The Post -closure care period began on the date that the closure was
approved.
A Post -closure plan was submitted on September 13, 1996 and was approved on February 27,
1997. The Post -closure plan required, among other things, a groundwater monitoring plan,
planned maintenance activities for the capped units, recordkeeping requirements, inspection
requirements and a deed notification requirement.
Based on multiple years of groundwater monitoring, the attached Environmental Indicator
documentation, identification of the trenches on a plat with Iredell County, Notice of Disposal of
Residual Soils on a deed with Iredell County and the fact that the trenches are also being
monitored per the Division of Water Resources Permit No WQ0004040 it has been determined
that the City of Statesville Third Creek Monofill has met the requirements for post -closure as
described in 40 CRF 265 as adopted in 15A NCAC 13A .0110. In addition it has been
determined that the closure of the units is sufficient to protect human health and the environment
and the post -closure care period can be shortened and may be terminated.
This action. will also be a detennination of RCRA Remedy Constructed, CA550, and Corrective
Action Process Terminated, Remedial Activities Complete, CA999RM.
Comments will be accepted concerning the action from August 21, 2015 through October 5,
2015. Comments can be submitted to:
Julie Woosley
Attn: Bud McCarty
N.C. Division of Waste Management
Hazardous Waste Section
MSC 1646
Raleigh, NC 27699-1646
Or email to bud.mccartyCPncdenr.gov .

In addition a Public Hearing will be held to accept comment concerning this action. The Public
Hearing will be on September 29, 2015 at the Statesville Main Library at 201 North Tradd St,
Statesville, North Carolina beginning at 1:00 pm.

I. SCHEDULES
I. No Iater than six months prior to the expiration of this permit, the Permittee shall request
renewal of this permit on official Division forms. Upon receipt of the request, the Division
will review the adequacy of the facilities described therein, and if warranted, will renew the
permit for such period of time and under such conditions and limitations as it may deem
appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be
submitted with the permit renewal application
2. No later than January 31, 2015, monitoring wells MW-5 and MW-6 shall be permanently
abandoned. A North Carolina Certified Well Contractor shall abandon the monitoring wells
according to the North Carolina Well Construction Standards (15A NCAC 02C .0113) and
local county rules. Please note that additional monitoring wells may be required if deemed
necessary by the Division to insure effectiveness .of groundwater monitoring network at the
site.
H. PERFORMANCE STANDARDS .
L The surface disposal unit shall be effectively maintained and operated as a non -discharge
system to prevent the discharge of any wastes resulting from the operation of the unit.
2. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to
surface waters or groundwater resulting from the operation of the surface disposal unit.
3. In the event that the surface disposal unit is not operated satisfactorily, including the creation
of nuisance conditions, the Permittee shall contact the Mooresville Regional Office, and take
any immediate corrective actions as may be required by the Division.
4. No residuals shall be approved for disposal in the surface disposal unit.
5. The compliance boundary for the surface disposal unit is specified by regulations in
15A NCAC 2L (i.e., Groundwater Classifications and Standards). The Compliance
Boundary for, surface disposal units individually permitted after December 31, 1983,
shall be is established at either (1) 250 feet from the surface disposal unit or (2) 50
feet within the property boundary, whichever is closest to the surface disposal unit.
An exceedance of Groundwater .Quality Standards at or beyond' the Compliance
Boundary is subject to immediate remediation action according to 15A NCAC 2L
.0106 (d)(2).
6. The review boundary shall be established around the surface disposal unit midway
between the Compliance Boundary and the perimeter of the surface disposal unit.
Any exceedance -of Groundwater Quality Standards at the Review Boundary shall
require action in accordance with 1.5A NCAC 2L .0106 (d)(1).
WQ0004040 Version 3.0 Shell Version 131016 Page 2 of 6

ATTACHMENT C — Groundwater Monitoring and I..imitations
City of Statesville
Monitoring wells: MW-2, MW-3, MW 4, MW-7, MNV-S, and MW-9
Permit Number: WQ0004040 Version: 3.0
GROUNDWATER CHARACTERISTICS
GROUNDWATER STANDARDS
MONITORING REQUIREMENTS
PCS Code
Parameter Description
Daily Maximum
Frequency Measurement
Sample TypeEFs
82546
Water level, distance from measuring point
feet
Annually
Calculated
00400 �spl
su
Annually
Grab70300
Soltd Tita] jssolvec 1801eaC
mg/I
Annually
Grab00680
Carbon, Tot Organic (TOC)
mg/l
Annually
Grab
01002
Arsenic, Total (as As)
ug/l
Annually
Grab
6
00620
Nitrogen, Nitrate Total (as N)
mg/1
Annually
Grab
6
01027
Cadmium, Total (as Cd)
ug/l
Annually
Grab
6
01034
Chromium, Total (as Cr)
ug/l
Annually
Grab
6
71900
Mercury, Total (as Hg)
ugh -
Annually
Grab
6
01067
Nickel, Total (as Ni)
ug/l
Annually
Grab
6
01051
Lead, Total (as Pb)
ug/l
Annually
Grab
6
01007
Barium, Total (as Ba)
ug/i
Annually
Grab
6
GWVOC
Volatile Compounds, (GW)
yes = 1, no = 0
Annually
Grab
4, 5, 6
01147
Selenium, Total (as Se)
ug/l
Annually
Grab
6
01077
Silver, Total (as Ag)
ug/1
Annually
Grab
6
Footnotes:
1. The measurement of water levels shall be made prior to purging the wells. The depth to water in each well shall be measured from the surveyed point on the top of the casing. The measurement
of pH shall be made after purging and prior to sampling for the remaining parameters.
2. The measuring points (top of well casing) of all monitoring wells shall be surveyed to provide the relative elevation of the measuring point for each monitoring well. The measuring points (top
ofcasing) of all monitoring wells shall be surveyed relative to a common datum,
3. If TOC concentrations greater than 10 mg/I are detected in any downgradient monitoring well, additional sampling and analysis must be conducted to identify the individual constituents
comprising this TOC concentration. If the TOC concentration as measured in the background monitor well exceeds 10 mg/1, this concentration will be taken to represent the naturally occurring
TOC concentration. Any exceedances of this naturally occurring TOC concentration in the downgradient wells shall be subject to -the additional sampling and analysis as described above
4. If any volatile organic compounds (VOC) are detected as a result of monitoring as provided in Attachment C, then the Mooresville Regional Office supervisor, telephone number [phone],
must be contacted immediately for further instructions regarding any additional follow-up analyses required.
Page 1 of 2

ATTACHMENT C — Groundwater Monitoring and Limitations
City of Statesville
Footnotes (continue)
Permit Number: WQ0004040 Version: 3.0
Volatile Organic Compounds (VOC) - Analyze by one of the following methods:
a. Standard Method 6230D, PQL at 0.5 µg/L or less
b. Standard Method 6210D, PQL at 0.5 µg/L or less
C. EPA Method 8021, Low Concentration, PQL at 0.5 µg/L or less
d. EPA Method 82.60, Low Concentration, PQL at 0.5 pg/L or less
e. Another method with prior approval by the Water Quality Permitting Section Chief
Any method used must meet the following qualifications:
a. A laboratory must be D WQ certified to run any method used.
b. The method used must, at a minimum, include all the constituents listed in Table Vill of Standard Method 6230D.
c. The method used must provide a PQL of 0.5 µg/L or less that must be supported by laboratory proficiency studies as required by the DWQ Laboratory Certification
detected above the MDL but below the PQL of 0.5 µg/L must be qualified (estimated) and reported.
6. Monitoring wells shall be reported consistent with the nomenclature and Iocation information provided in Figure 2 and this attachment.
Page 2 of 2
Unit. Any constituents

PUBLIC NOTICE
PUBLIC HEARING FOR:
TERMINATION of MONITORING REQUIREMENTS for the HAZARDOUS WASTE SECTION
For Third Creek Wastewater Treatment Plant, Statesville
This is to notify the public of the termination of the monitoring requirement and the termination of post -closure
care requirements by the North Carolina Division of Waste Management's Hazardous Waste Section for Third
Creek Wastewater Treatment Plant facility, located at 444 Third Creek Road, Statesville.
A public hearing will be held on Sept. 29 at 1:00 p.m. at the Statesville Main Library at 201 North Tradd St,
Statesville. All attendees will have the opportunity to present five (5) minute oral statements regarding the
termination of monitoring and post -closure care requirement for the Hazardous Waste Section and/or to submit
written comments and data.
In conjunction with the Notice of Public Hearing, written comments can also be sent during the public comment
period of Aug. 21, 2015 — Oct. 5, 2015 to the following address:
Julie Woosley
Attn: Bud McCarty
N.C. Division of Waste Management
Hazardous Waste Section
MSC 1646
Raleigh, NC 27699-1646
All data supporting this action is part of the administrative record and available for your review Monday through
Friday during office hours (9:00 a.m. to 4:00 p.m.). Copies of the draft termination and a fact sheet are available
at the Hazardous Waste Section offices, located at 217 West Jones Street in Raleigh. Call [phone] for an
appointment before arriving. The documents can also be found at:
htt-o://-oortal.nedenr.org/web/wm/hw/news/pnotice
Summary:
Based on multiple years of groundwater monitoring, the attached Environmental Indicator documentation,
identification of the trenches on a plat with Iredell County Notice of Disposal of Residual Soils on a deed with
Iredell County, and the fact that the trenches are also being monitored per the Division of Water Resources
)Permit No WQ0004040), it has been determined that the City of Statesville Third Creek Monofill has met the
requirements for post -closure as described in 40 CRF 265 as adopted in 15A NCAC 13A .0110. In addition, it
has been determined that the closure of the units is sufficient to protect human health and the enviromnent and the
post -closure care period can be shortened and may be terminated. This action will also be a determination of
RCRA Remedy Constructed, CA550, and Corrective Action Process Termina d, Remedial Activities Complete,
CA999RM.
All comments received during the public comment period or at the hearing will be considered in the decision
regarding this action. Comments received after the public comment period ends will not be considered. The
statutory authority for calling the hearing is G.S. 130A-294(f). Applicable State rules are found in the North
Carolina Hazardous Waste Management Rules 15A NCAC 13A .0105, .0109, and .0113. These rules adopt the
requirements of the Federal Resource Conservation and Recovery Act as amended by the Hazardous and Solid
Waste Amendments 747
Anyone desiring additional information may contact Bud McCarty at [phone] or
bud.mccg9y(a_,ncdenr.gov or at the address listed above.

Termination of Monitoring and Post -closure Care Requirements
Third Creek Wastewater Treatment Plant disposal trenches
EPA ID NCR000001602
444 Third Creek Road, Statesville, NC
On March 8, 1995 the Department of Environment, Health and Natural Resources acting through
the its Division of Solid Waste Management entered into an Administrative Order on Consent
("Order"), Docket #94-191, with the City of Statesville Third Creek Wastewater Treatment Plant
(EPA ID # NCR 000 001 602).
The Order was to require proper management of landfill6d sludge that exceeded the regulatory
limits of cadmium.
A Closure certification was submitted on September 2, 1997 and closure with waste in place was
approved on. June 22, 1998. The Post -closure. care period began on the date that the closure was
approved.
A Post -closure plan was submitted on September.13, 1996 and was approved on February 27,
1997. The Post -closure plan required, among other things, a groundwater. monitoring plan,
planned maintenance activities for the capped units, recordkeeping requirements, inspection
requirements and a deed notification requirement.
Based on multiple years of groundwater monitoring, the attached Environmental Indicator
documentation, identification of the trenches on a.plat with Iredell County, Notice of Disposal of
Residual Soils on a deed with Iredell County and the fact that the trenches are also being
monitored per the Division of Water Resources Permit No WQ0004040 it has been determined
that the City of Statesville Third Creek Monofill has met the requirements for post -closure as
described in 40 CRF 265 as adopted in 15A NCAC 13A .0110. In addition it has been
determined that the closure of the units is sufficient to protect human health and the environment
and the post -closure care period can be shortened and may be terminated.
This action will also be a determination of RCRA Remedy Constructed, CA550, and Corrective
Action Process Terminated, Remedial Activities Complete, CA999RM.
Comments will be accepted concerning the action from August 21, 2015 through October 5,
2015. Comments can be submitted to:
Julie Woosley .
Attn: Bud McCarty
N.C. Division of Waste Management
Hazardous Waste Section
MSC 1646
Raleigh, NC 27699-1646
Or email to bud.mccartyAncdenr.gov .

In addition a Public Hearing will be held to accept comment concerning this action. The Public
Hearing will be on September 29, 2015 at the Statesville Main Library at 201 North Tradd St,
Statesville, North Carolina beginning at 1:00 pm.

Imo,-' \ ;'
From: Phase 1 Subsurface Characterization,
Third Creek Monofill, City of
N `�� Statesville, May 5, 1995
1 Legen� .
,ale �,\ 0 Monitoring Well Locatlon
0 10INIO
Z
Author. Drawing Layers Date Title Ground Water Contour Map
dg 53021-1 025 3-28-95 (From May 2,1995 Data)
a a= ° T1 Job rVo� Revision Figure Scale Project - ThIrd Creek MonofIII Facllity
UMMUM 53(�k?1c�0 0 3 1' = 200' StateWile, North Carolina
A GREAT LAKI'S CUELOCAL CORYORAT(ON COA{P.'NY

It
WXA
NCDENR
North Carolina Department of Environment and Natural o
-; S.
Pat McCrorys A;In derVaart
Governor tary
June 12, 2015
Mr. L.F. Hudson, Jr., Director of Water Resources
City of Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Mr. Marshall Puryear, Manager (Electronic mail)
Synagro Central, LLC
284 Boger Road
Mocksville, NC 27028
Subject: Non -Discharge Permit Inspections
City ofta esyille
Distribution of Residuals — Permit No-:-WQ000
Land Application of Residuals — Permit No.: WQ0014543
Iredell County
and Synagro Western Regional
Land Application of Residuals — Permit No.:WQ0016247
Alexander County
Dear Mr. Hudson and Mr. Puryear:
The Mooresville Regional Office (MRO) conducted a compliance inspection on May 27th, 2015,
which included a land application event of Third Creek residuals under the SYNAGRO Permit; and,
a records review and the residuals processing and storage at the Fourth Creek WWTP. The MRO
would like to thank Eric Thompson (Synagro) and Andy Smith (Statesville) for their time during the
inspections.
Permit expiration dates are listed below for your convenience.
WQ0004040 Third Creek Monofill, expires 12/30/2018
The monofill units were not inspected at this time.
WQ0006245 Statesville Class A — Lime Stabilized. expires 09/30/2020
Log entries for the lime stabilization analyses and cross referenced records for the pH
meter calibration appeared well organized and improved since the previous inspection.
W00014543 Statesville Class B - Emergency Land Application, expires 02/28/2019
There is currently no activity under this permit.
WQ0016247 SYNAGRO Class B - Land Application, expires 02/28/2018
This permit is held by SYNAGRO, but they rely on Statesville to collect and analyze for all
required parameters including Pathogen and Vector Attraction Reduction (PVAR), which
Mooresville Regional Office
610 East Center Avenue, Suite 301, Mooresville, North Carolina 28155
Phone: [phone] / Fax: [phone] Customer Service 1-877-623-6748
Internet: www.ncdenr.gov
An Fnimi nnnnrfunifv \ Arfrmnfiva Anfinn FmnFnVP.r — MAdA in nnrf by rrrvrlad nanar

would also apply to Statesville's Class B permit #WQ0014543, were it being utilized for land
application.
Per conversation with Andy Smith, the City of Statesville has increased the residuals
"SOUR" testing to once/month to help address odor and vector concerns noted in a
previous inspection and to ensure VAR is met, particularly with the Third Creek residuals,
which typically have more odors than the Fourth Creek residuals. The once/month
sampling exceeds the permit requirement; therefore, the City of Statesville may reduce
sampling frequency back to once/quarter at their discretion.
The attached report should be self-explanatory; however, should you have questions please
contact me by phone [phone]) or email (maria.schutteCc)-ncdenr.gov).
Sincerely,
Maria Schutte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Attachment: Inspection Report June 2015
CC: Mr. Andy Smith, Town of Statesville (email)
Mr. Eric Thompson, SYNAGRO (email)

State of North Carolina
Department of Environment
and Natural Resources
Division of Water Resources
Pat McCrory; Governor
Donald van der Vaart, Secretary
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Statesville County: Iredell
Permit No.: W00006245 Class A Lime Issued: 04/02/2015 Expiration: 09/30/2020
Permit No.: W00014543 Class B emergency Issued: 09/17/2013 Expiration: 02/28/2019
Permit No.: W00016247 SYNAGRO Land Application Issued: 03/27/2009 Expiration: 02/28/2018
Permittee Contact: Andy Smith (4' Creek WWTP ORC) Telephone No.: 704-878-3438
LA ORC: Marshall R. PMear (SYNAGRO) LA #994465 Telephone No.: 434-738-8002
LA BUORC: Froncy M. Dail (SYNAGRO) LA #13197 Telephone No.: 910-443-7696
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other
Inspection Date(s): May 27, 2015
Inspection Summary: (additional comments may be included on attached pages)
This inspection included an active land application (LA), of Third Creek residuals at field NC-IR-20-03,
under the Synagro — WQ0016247 permit; and, a review of records and residuals storage at Statesville's
Fourth Creek WWTP, for both of their permits referenced above. The 4th creek plant was undergoing
construction for repairs at the lime processing and storage areas, at the time of this visit. Statesville
maintains separate bay areas for the "class A" residuals storage and distribution, and the 3rd creek and 4t'
creek "class B" residuals handled by SYNAGRO.
• Strong odors were noticed in the Class B residuals at the field LA site; however, vectors
(flies) were minimal. Statesville has increased sampling frequency for SOUR testing to
ensure VAR is met. The once/month testing is at the discretion of the City of Statesville and
may be reduced to the permit requirement of once/quarter at anytime.
• Please contact maria.schutte(i),ncdenr.gov with any corrections to the contact information
noted above.
Is a follow-up inspection necessary _yes X no
Inspector(s): Maria Schulte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: May 27th, 2015

Residuals Inspection
WQ0006245, WQ0014543 Statesville & WQ0016247 Synagro
pg. 2
Type of Residual
WQ00016247 and WQ0014543
X Land Application (class B)
Y-yes N-no NE -not evaluated
Record Keeping (class B)
WQ0006245
X Distribution and Marketing (class A)
NA -not applicable
Y Copy of current permit
Y 'Current metals and nutrient analysis
Y TCLP analysis
*Y SSFA (Standard Soil Fertility Analysis)
*Y Nutrient and metals loading calculations
*Y Hauling records
*Y Field loading records
*Y Field site maps and information
NE Records of lime purchased
Y Pathogen & Vector Attraction Reduction
Record Keeping (class A)
Y Copy of current permit
Y Current metals and nutrient analysis
Y TCLP analysis
NA SSFA (Standard Soil Fertility Analysis)
NA Nutrient and metals loading calculations
Y Hauling records
NA Field loading records
NA Field site maps and information
Y Records of lime purchased
Y Pathogen & Vector Attraction Reduction
* Comments: Most data was reviewed as part of 2014 Annual Report. The only field maps reviewed were
for the land application sites visited.
Pathogen & Vector Attraction Reduction Records
Fecal coliform
X SM 9221 E (Class A or B)
SM 9222 D (Class B only)
Salmonella (Class A, all tests must be < 3MPN / 4 grams dry)
Class A lime stabilization X
SOUR _X
pH records for lime stabilization (Class A or B) X
Comments: The records were well organized. It was noted that the pH time and temp logs for the Class A
product and cross referencingreferencitzg to the pH calibration logbook appeared complete and improved over last
year.
Treatment
X Aerobic digestion anaerobic digestion
X Alkaline Stabilization Lime other -describe:
Transport
Spill control plan in transport vehicle?-Y
Does transport vehicle appear to be maintained? YY
Storage The 4th Creek residuals storage was only viewedfrom a plant vehicle due to construction activity.
Number of days/weeks/months of storage: Approximately 3 months.
Describe storage: Cake residuals are stored at the 4ch creek WWTP. There is
A 3rd Creek Class B and 4rh Creek Class B residuals.
Odors present NE Vectors present NE

Residuals Inspection pg. 3
WQQ006245, WQ0014543 Statesville & WQ0016247 Synagro
Sampling
Describe Sampling: Sampling and analyses are handled by the City of Statesville.
Is sampling adequate? NE Is sampling representative? Y, if the O&M plan is followed
Field Sites (end use for class B biosolids): NC-IR-20-03. This portion of the inspection is the
responsibility ofSYNAGRO under their permit #W00016247
Y Permit on site during application Y Spill plan on site
Y Buffers adequate Y Cover crop specified in permit
N Documented exceedances of PAN limits Y Site condition adequate
N Signs of runoff / ponding (if no, improvements recommended)
Y Rain Gauge on site during application
Are there any limiting slopes on fields?
Y 10 % for surface application N 18% for subsurface application
Comments: There were odors but minimal vectors detected at the land application site. The odors are
highlighted in this report just to remind all permittees of the potential for complaints & nuisance conditions.
Ad'a1 cent fields had been flagged for application. Per conversation with Eric Thompson, the existing maps
were obsolete due to setback changes. The buffers he flagged appeared adequate at the time of this
inspection.
Monitoring wells) Y/N: N
If yes, location of well(s): These permits currently do not require groundwater monitoring
Odors/vectors
Describe any nuisance conditions and any corrective actions needed. There were odors and minimal
vectors present at the LA site. The Fourth Creek residuals storage area was only viewed via drive -by in a
plant truck due to construction activity.
Odors present Y
Vectors present minimal
Other noted conditions:

5 4U=
j NF1
CDET�IR
North Carolina Department of Environment and Natural Resources
Pat McCrory John E. Skvarla, III
Governor Secretary
August 13, 2014
Mr. L.F. Hudson, Jr., Director of Water Resources
City of. Statesville
P.O. Box 1111
Statesville, North Carolina 28687
Subject: Non -Discharge Permit Inspection and Acknowledgement
of Receipt of the 2013 Annual Report
Permit Nos. W00004040, WQ006254, WQ0014543 and
WQ0016247 (SYNAGRO)
City of Statesville, lredell County
Dear Mr. Hudson:
The Mooresville Regional Office (MRO) conducted a compliance inspection on June 231d, 2014,
which included a land application event, records review and residuals processing and storage at
the Third Creek and Fourth Creek WWTPs. The MRO would like to thank Andy Smith for his time
during the inspection.
Please note the expiration dates and potential compliance issues are listed under each permit
below. Time sensitive matters and issues of most concern are highlighted.
WQ0004040 Third Creek Monofill, expires 12/30/2018
The monofill units were not inspected at this time. This- permit is mentioned to acknowledge
the receipt of the 2013 Annual Report, which reflected there was no disposal of residuals in
the monofll.
W00006254 Class A — Lime Stabilized, expires 09/30/2015
• The permit renewal application is due 180 days prior to expiration, which. is
03/31/2015.
• Records for the pH meter calibration are Incomplete. Calibration dates should
match dates for the lime stabilization analyses. This was discussed with Andy
Smith for correction on future log entries.
WQ0014543 Class B - Emergency Land Application. expires 02/28/2019
There is currently no activity under -this permit.
WQ0016247 Class B-_SYNAGRO Land Application, expires 02/28/2018
This permit is held by SYNAGRO, but they rely on Statesville to collect and analyze for all
required parameters including Pathogen and Vector Attraction Reduction (PVAR). In
addition, the comments below would also apply to Statesville's Class B permit'
#WQ0014543, were it being utilized for land application.
• Odors and files were detected at both the -residuals storage area and the land
application sites. This is an indication that VAR is not being properly met.
Mooresville Regional Office, 610 East Center Avenue, Mooresville, North Carolina 28155
Phone: [phone] Internet: www.ncdenr.gov
An Equal Opportunity 1 AtFrmarnre Action Employer— Made in part by recycled paper

^-1
• The city of Statesville meets both their PVAR requirements once per quarter. To
maintain compliance with permit conditions, it is recommended that SYNAGRO,
schedule land application events to coincide as close as possible to the PVAR
results time frame, and that ONLY currently. stored and analyzed residuals be
land applied.
The attached report should be self-explanatory; however, should you have questions please
contact me by phone [phone]) or email (maria.schutte(ci)-ncdenr.nov).
Sincerely,
LV
Maria Schulte, Environmental Specialist
Mooresville Regional Office
Water Quality Regional Operations Section
Division of Water Resources, NCDENR
Attachment: Inspection Report June 2014
CC: Mr. Andy Smith, Town of Statesville (email)
Mr. Marshall Puryear, SYNAGRO (email)

i fr
State. of North Carolina
Department of Environment
and Natural Resources
Division of Water Resources
Pat McCrory, Governor.
.John E. Skvarla, III, Secretary
NCDENR
NON -DISCHARGE COMPLIANCE INSPECTION
GENERAL INFORMATION
City/Town/Owner: Statesville County: Iredell
Permit No.: WQ0006245 Class A Lime Issued: 10/20/2006 . Expiration: 09/30/2015
Permit No.: W00014543 Class B emergency Issued: 09/17/2013 Expiration: 02/28/2019
Permit No.: W00016247 SYNAGRO Land Application Issued: 03/27/2009 Expiration: 02/28/2018
Permittee Contact: Andy Smith (4" Creek WWTP ORC) Telephone No.; 704-878-3438
LA ORC: Marshall R. Puryear (SYNAGRO) LA #994465 Telephone No.: 434-738-8002
LA BUORC: Froacy M. Dail.(SYNAGRO) LA #13107 Telephone No.: 910-443-7696
Reason for Inspection
X ROUTINE COMPLAINT FOLLOW-UP OTHER
Type of inspection
Collection System Spray Irrigation X Sludge Other.
Inspection Date(s): . June 23, 2014
Inspection Summary: (additional comments may be included on attached paw
This inspection included the Third Creek WWTP, Fourth Creek WWTP, and covers all three City of
Statesville residuals permits: #WQ0006245 (Class A), WQ0014543 (Emergency LA - not used) and
WQ0016247 (Class B - Synagro LA). The third Creek Monofill, permit #WQ0004040, was not inspected
for this report. It is only mentioned hereto note the receipt and review of the 2013 Annual Report.
The 4th creek plant was the only plant actively processing sludge (dewatering), at the time of inspection,
and 4th creek is where all residuals are stored.- There are separate bay areas for the "class.A" residuals
storage and distribution, and the 3r6 creek and 4th creek "class B" residuals handled by SYNAGRO. Issues
to address to maintain compliance are noted here and in the cover letter.
• Strong odors and vectors were noticed in the Class B residuals storage areas and at the field
Land Application sites. More timely land application is recommended upon passing PVAR
parameters.
• The pH calibration log for the Alkaline Stabilization meter should have matching dates to
the pH time and temperature records.
Is a follow up inspection necessary _yes X no
Inspector(s): Maria Schulte - Environmental Specialist
Telephone No.: 704-663-1699 Fax No.: 704-663-6040
Date of Inspection: June 23`d, 2014

Residuals Inspection
WQ0006245, WQ0014543, WQ0016247 Statesville, Iredell County
Tvue of Residual
pg. 2
WQ0006247 and WQ0014543
WQ0006245 ,
X
Land Application (class B)
X
Distribution and Marketing (class A)
Y-yes N-no NE -not evaluated NA -not applicable
Record Keeping (class B)
Record Keeping (class A)
Y
Copy of current permit
Y
Copy of current permit
Y
Current metals and nutrient analysis
Y
Current metals and nutrient analysis
Y
TCLP analysis
Y
TCLP analysis
*Y
SSFA (Standard Soil Fertility Analysis)
NA
SSFA (Standard Soil Fertility Analysis)
*Y
. Nutrient and metals loading calculations
NA
Nutrient and metals loading calculations
*Y
Hauling records
Y
Hauling records
*Y
Field loading records
NA
Field loading records
*Y
Field site maps and information
NA
Field'site maps and information
NE
Records of lime purchased
Y
Records of lime purchased
Y
Pathogen & Vector Attraction Reduction
Y
Pathogen & Vector Attraction Reduction
* Comments: Most data was reviewed as part of 2013 Annual Report The only field maps reviewed were
for the land application sites visited
Pathogen & Vector Attraction Reductions Records
Fecal colifonn
X SM 9221 E (Class A or B)
SM 9222 D (Class. B only)
Salmonella (Class A, all tests must be. < 3MPN / 4 grams dry)
Class A lime stabilization X
SOUR _X
pH records for lime stabilization (Class A or B) X
Comments: It was noted that the pH, time and temp logs for the Class A product appeared complete which
was an improvement over last year; however, the logbook for the pH meter calibration was missing dates
that should have coincided with the Class A analytical dates. This was discussed with And Smith during the
inspection.
Treatment
X Aerobic digestion anaerobic digestion
X Alkaline Stabilization Lime other -describe:
Transport
Spill control plan in transport vehicle?—Y
Does transport vehicle appear to be maintained? A
Comments: A transport vehicle was followed from the 4rh creek WWTP to a land application site.

xwsiauais inspection
WQ0006245, WQ0014543, WQ0016247 Statesville, Iredell County
Storage
:i
Number of days/weeks/months of storage: Approximatelymonths
j Describe storage: Cake residuals are stored at the ath rrovlr wLrrTv
Odors present Y
Comments:
Sampling
Describe Sampling;
Vectors present Y
FA
Samplft and analyses are handled by the City of Statesville
Is sampling adequate? NE Is sampling representative? NE
Field Sites (end use for class B biosolids)
Y Permit on site during application Y Spill plan on site
Y Buffers adequate Y Cover crop specified in permit
N Documented exceedances of PAN limits Y Site condition adequate
N Signs of runoff / ponding (if no, improvements recommended)
NE Rain Gauge on site during application
Are there any limiting slopes on fields?
Y 10 % for surface application N 18% for subsurface application
pg. 3
Comments: There were odors and vectors detected at both land application sites visited Vectors were
mostly concentrated at the stag areas as this is where the odors were most sigaaifacant Odors and vectors
were not detected on portions of the fields where spreading had taken place as residuals were sip_nf scantly
less concentrated.
Monitoring well(s) Y/N: N
If yes, location of well(s): This permit currently does not require groundwater monitoring,
Odors/vectors
Describe any nuisance conditions and any corrective actions needed. There were odors and vectors
resent at the residuals storage and the LA sites. Improved communication and coordination o land
application events with PVAR sampling results is suggested as apossible solution to alleviate nuisance
conditions. Per conversation with And Smith there have been delays with recent LA due to scheduling
difficulties. '—
Odors present Y
Vectors present Y
Other noted conditions: Per request from the Central O ace in Raleigh future annual reports can still
be mailed in the same package but should be compiled separately so as not to cause confusion for those
unfamiliar with facility operations This will also reduce the risk of any of our reports being overlooked
and not properly received at the data processing
facility

Administration
Official Website of the City of Statesville, North Carolina
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Departments < Water Resources < Administration
Administration
Administrative Offices
Fourth Creek Wastewater Treatment Plant
693 Bell Farm Road
Statesville, NC 28625
Phone: [phone]
Fax:[phone]
Third Creek Wastewater Treatment Plant
444 Third Creek Road
Statesville, NC 28677
Phone:[phone]
Fax: [phone]
Water Treatment Plant
232 Pump Station Road
Statesville, NC 28677
Phone: [phone]
Fax: [phone]
Government i Departments I Calendar
Statesville provides continuous, 24-hour per day, water and sewer service. There is
always a certified operator on duty at each plant as required by the state. This
ensures that the city's water supply and the water returned to nearby streams are
of the best quality possible. Operators are certified through the N.C. Division of
Environmental Management.
Statesville actively promotes beneficial reuse of water and wastewater treatment
byproducts. Water and wastewater processes produce sludge as a byproduct of
treatment. Statesville dewaters the sludge and blends it with lime and a drying
agent to produce an alkaline stabilized product, called Sta-Lime. Sta-Lime is
distributed locally to farmers as a liming agent.
GO
Joe Hudson,
Director
704-878-3438
email Joe
Jerry Byerly,
Assistant Director
704-878-3438
email Jerry
Brandy Johnson,
Pretreatment
704-878-3438
email Brandy
Scott Austin, Third
Creek Wastewater
Treatment
704-872-9621
email Scott
Andy Smith, Fourth
Creek Wastewater
Treatment
704-878-3438
email Andy
Weston Johnson,
Water Treatment
704-878-3441
e-mail Weston.
Resident I visitor I Business I Government I Departments I Contact Us I Calendar I Forms & Documents I Site Map
Home
MAILINGADDRESS: PO BOX 1111, Statesville, NC 28687-1111 1 PHYSICAL ADDRESS: 301 S. Center Street
704.878.3583 PHONE [phone] FAX
SITE DESIGNED BY: Granite Sky Design I SITE PROGRAMMED BY: Customer Connect
http://www.ci.statesville.nc.usIDepartmentslWaterResourceslAdministration/tabid1243IDefault.aspx 1/8/2013

Nm
F -
MODE V R
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Charles Wakild, P.E.
Governor
Director
August 22, 2012
MR. L.F. HUDSON, JR., DIRECTOR OF WATER RESOURCES
CITY OF STATESVILLE
POST OFFICE BOX 1111
STATESVILLE, NC 28687
Subject: Rescission of Surface Disposal of Residuals Permit
Permit No. WQ0001759
Fourth Creek Wastewater Treatment Plant
Iredell County
Dear Mr. Hudson:
Dee Freeman
Secretary
f
[1Z"
BYJ .. ....................... .
Reference is made to your request for rescission of the subject Surface Disposal of Residuals Permit. Staff
from the Mooresville Regional Office has confirmed that permit conditions for post closure have been
met and this Permit is no longer required. Therefore, in accordance with your request, Pen -nit No.
WQ0001759 will be rescinded upon completion of the monitoring well abandonment requirements as
specified below:
4 . Monitoring wells MW-1, MW-2, and MW-3 shall be permanently abandoned. Within 30 days of
abandonment, a Well Abandonment Record (Fonn GW-30) listing this permit number -.and the
appropriate monitoring well identification number shall be completed for each well abandoned
and mailed to the Division of Water Quality, Aquifer Protection Section, 1636 Mail Service
Center, Raleigh, NC 27699-1636. A North Carolina Certified Well Contractor shall abandon the
monitoring wells according to the North Carolina Well Construction Standards (15A NCAC. 02C
.0113) and local county rules.
o Please submit a copy of this letter along with the Well Abandonment Record (Form GW-30).
If it would be helpful to discuss this matter further, please do not hesitate to contact Chonticha NICDaniel
at telephone [phone], or the Mooresville Regional Office, Aquifer Protection Section.
Sincerely,
Charles Wakild, P. E.
cc: Iredell County Health Department
Mooresville - Aquifer Protection Regional Supervisor
Permit File WQ0001759
AQUIFER PROTECTION SECTION
1636 Mail Service Center, Raleigh, North Carolina 27699-1636
Location: 512 N. Salisbury St., Raleigh, North Carolina 27604 One
Phone: [phone] FAX: [phone] N Ol th Car oliD.a
Internet: mm.ncwaterquality.orq E
An Equal Opportunity, AFrmative Action Employer

'aT` do's
i
I. WELL CONTRACTOR:
WELL, ABANDONMENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality.
WELL CONTRACTOR CERTIFICATION # 2579
DANNY SUMMERS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
city or Town State Zip Code
704 ) 872-7686
Area code Phone number
S. WELL DETAILS:
a.Total Depth 38.0 ft. Diameter: '2.0 in.
b. Water Level (Below Measuring Point): ft.
Measuring point is ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): _ ' N/A.., ft
b. Casing Removed: N/A ft.
7. DISINFECTION: NIA
2. WELL INFORMATION: (Amount of 65%75% calcium hypochlorite used)
SITE WELL ID # (if applicable) MW-1 8. SEALING MATERIAL:
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable useg Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery ❑ 'Injectiori ❑ Irrigation
❑ Other (risi use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGLE NAME
NEARESTTOWN: STATESVILLE
493 BELL FARM ROAD 28625
(Sireet/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code) ;
TOPOGRAPHC / IKin SETTING:
❑ Slope ❑, Valley V Flat ❑ Ridge❑ Other_
(Check appropriate setting)
LATITUDE 35 47 10-4400 •, DMS OR DD
LONGITUDE 80 47 51.1000^ DMS OR DD
Latitude/longitude source: 03PS LITopographic map
(location of well must be shown on a USGS topo map andattached to
this form ifnot using GPS)
Neat CemQat Sand Cement
Cement lb. Cement lb -
Water gal. Watergal.
Bentonite
Bentonite lb.
Type: V Slurry ❑ Pellets
Water gal,
Other
Type material PORTLAND BENTONITE SLURRY
Amnmt 6-25 GALLONS
in.
in.
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
VIA TREMIE PIP WITH PORTI AND B NTONITE SLURRY
10. WELL DIAGRAM : Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materials,sed
11. DATE WELL ABANDONED 10/12/12
I DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
4a. FACILITY - The name of the business where the well is located. Complete 4a;
(If a residential well, skip 4a; complete 4b,
THIS RETH A NRD HAS BEEN ILL D TIDED TO TH ELL OWNER. AND THAT A COPY OF
well owner Information only.)
FACILITY ID # (if applicable)
d
NAME OF FACILITY 4TH-CREEK WWTP
10/26/12
SIGMA F C ED WE C RACTOR
STREET ADDRESS 493 BELL FARM ROAD
. DATE
STATESVILLE NC 28625
City or Town State Zip Code
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an individual
4b. CONTACT PERSONIWELL OWNER:
w ersonall bandons his/her residential well
in accordance with 15A NCAC 2C .0113.)
NAME CITY OF STATESVILLE/4TH CREEK W WTP
DANNY SUMMERS
• PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 493 BELL FARM ROAD STATESVILLE, NC 28625
Sublrlti: a copy to the;owtlrr::and the original to Divtsoon o� UVater Qua.Pity - lntannation. Processing;...'
'16971Yiail
Service Center; Raleigh hl1C 27699 181T, Phone (919)
807-6300 Form GW-30
Rev. 5/10

„7 �r 65rArt•O `�
• �,d 9rw b.+n
Tt
WELT, AIBANDONMENTRECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
«v �^ WELL CONTRACTOR CERTIFICATION # 2579
1. WELL CONTRACTOR:
5. WELL DETAILS:
DANNY SUMMERS
a. Total Depth 36.0 ft: Diameter: 2.0 in.
Well Contractor (Individual) Name
b. Water Level (Below Measuring Point):. ft.
GEOLOGIC EXPLORATION, INC
Measuring point is ft. above land surface.
Well Contractor Company Name
176 COMMERCE BLVD
6. CASING: Length Diameter
Street Address
STATESVILLE
NC 28625 a_ Casing Depth (if known): NIA ft. in.
City or Town
State Zip Code b. Casing Removed: N/A ft. in.
704 1 872-7686
Area code Phone number
7. DISINFECTION: N/A
2. WELL INFORMATION:
(Amount of 65%75% calcium hypochlorite used)
SITE WELL ID # (if applicable) MW-2
8. SEALING MATERIAL:
STATE WELL PERMIT # (if applicable)
Neat Cement Sand Cement
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)' Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery ❑� Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGE NAME
NEARESTTOWN: STATESVILLE
493 BELL FARM ROAD 28625
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley 19Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 _° 47 ' 10.4400 ” DMS OR DD
LONGITUDE 80 47 51.1000° DMS OR DID
Latitude/longitude source: RfGPS 01-opographic map
(location of well must be shown on a USGS topo map andattached to
this form If not using GPS)
Cement lb.
Water gal.
Bentonite
Bentonite lb.
Type: It Slurry ❑ Pellets
Water ' gal.
Cement lb.
Water gal.
Other
Type material PORTLAND BENTONITE SLURRY
6.0 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
VIA TREMIE PIPE WITH PORT AND BENTONITE SLURRY
IRRY
10. WELL DIAGRAM : Draw a detailed sketch of theell on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materialsised
11. DATE WELL ABANDONED 10112/12
4a. FACILITY - The name of the business where the is
I DO HEREBY CERTIFY THAT THIS WELL VVW ABANDONED IN ACCORDANCE
WITH 15A NCAC 2C, WELL CONSTRUCTIO TANDARDS, AND THATA COPY OF
well located. Complete 4a ;
(If a residential well, skip 4a; complete 4b, well owner information only.)
THIS RE D HAS BEE7VIDED TO TH ELL OWNER.
!�
FACILITY ID # (if applicable)
-NAME OF.FACILITY. 4TH CREEK WWTP ..
10/26/12
: SIGNATURE OF CERTIFIED WELL CONTRACTOR DATE
STREETADDRESS 493 BELL FARM ROAD
STATESVILLE NC 28625
City or TOwn State Zip Code
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
(The private well owner must be an individual w4eLsonall3abandons his/her
4b.CONTACT PERSONNUELt OWNER:
residential well
in accordance with 15A NCAC 2C .0113.)
CITY
Y OF STATESVILLE/4TH CREEK WWTP
DANNY SUMMERS
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 493 BELL FARM ROAD STATESVILLE, NC 28625
Su.i eo ownei
m : tathe and the.'prig,inah.to.:"D1.VAsion of Water Q:ualp . - jn `
pY ty IrormatlamProcessing,
1617IVlailServrce Cutter "Raleigh., N.G276 ;1617,.Rho"ne:: (81.9j.807763.00.
>... .
Form GW 3
:.. 0
:..
.`..
Rev.5/10

SfAtfo",,
o,
WELL ABANDONM ENT RECORD
North Carolina Department of Environment and Natural Resources- Division of Water Quality
WELL CONTRACTOR CERTIFICATION # 2579
1. WELL CONTRACTOR:
DANNY SUMMERS
Well Contractor (Individual) Name
GEOLOGIC EXPLORATION, INC
Well Contractor Company Name
176 COMMERCE BLVD
Street Address
STATESVILLE NC 28625
City or Town State Zip Code
704 872-7686
Area code Phone number
2. WELL INFORMATION:
SITE WELL ID # (if applicable) MW-3
STATE WELL PERMIT # (if applicable)
COUNTY WELL PERMIT # (if applicable)
DWQ or OTHER PERMIT # (if applicable)
WELL USE (Check applicable use)' Monitoring ❑ Residential
❑ Municipal/Public ❑ Industrial/Commercial ❑ Agricultural
❑ Recovery ❑ Injection ❑ Irrigation
❑ Other (list use)
3. WELL LOCATION:
COUNTY IREDELL QUADRANGIE-NAME
NEARESTTOWN: STATESVILLE
493 BELL FARM ROAD 28625
(Street/Road Name, Number, Community, Subdivision, Lot No., Parcel, Zip Code)
TOPOGRAPHC / LAND SETTING:
❑ Slope ❑ Valley IZ Flat ❑ Ridge❑ Other
(Check appropriate setting)
LATITUDE 35 0 47 10.4400 " DMS OR DD
LONGITUDE 80 .47 51.1000'. DMS OR DD
Latitude/longitude source: E` PS Qfopographic map
(location of well must be shown On a USGS topo map andattached to
this form if not using GPS)
5. WELL DETAILS:
a.Total Depth 39.0 ft. Diameter: 2.0 in.
b. Water Level (Below Measuring Point): ft.
Measuring point is ft. above land surface.
6. CASING: Length Diameter
a. Casing Depth (if known): NIA ft: in.
b. Casing Removed: NIA ft. in.
7. DISINFECTION: NIA
(Amount of 651475% calcium hypochlorite used)
8. SEALING MATERIAL:
Neat Cement Sand Cement
Cement lb. Cement lb.
Water gat. Watergal.
Benton!te
Bentonite lb.
Type: if Slurry ❑ Pellets
Water gal.
Other
Type material PORTLAND BENTONITE SLURRY
6.5 GALLONS
9. EXPLAIN METHOD OF EMPLACEMENT OF MATERIAL:
VIA TREMIF PIPE WITH PORTLAND DENTONITE RI I IRRY
10. WELL DIAGRAM :Draw a detailed sketch of th¢ell'on the back of this
form showing total depth, depth and diameter of screens (if any) remaining
in the well, gravel interval, intervals of casing perforations, and depths and
types of fill materialsised
11. DATE WELL ABANDONED 10/12/12
1 DO HEREBY CERTIFY THAT THIS WELL WAS ABANDONED IN ACCORDANCE
4a. FACILITY - p
The name of the business where the well is located. Com Complete 4a r
WITH 15A NCAC 2C, WELL CONSTRUCTIOIJ STANDARDS, AND THAT COPY OF
: THIS R ORD HAS BEE l�VIDED TO T WELL OWNER.
(If a residential well, skip 4a; complete 4b, well owner information only.)
FACILITY ID # (if applicable)
10/26/12
NAME OF FACILITY 4TH CREEK WWT.P
: SIGNAM E OF C_ IED WELL CONTRACTOR DATE
STREET ADDRESS 493 BELL FARM ROAD
STATESVILLE NC 28625
SIGNATURE OF PRIVATE WELL OWNER ABANDONING THE WELL DATE
City or Town State
Zip Code
(Me private well owner must bean individual wPersonall bandons hislher residential well
4b. CONTACT PERSONNVELL OWNER:
in accordance with 15A NCAC 2C .0113•)
NAME CITY OF STATESVILLE/4TH CREEK WWTP
DANNY SUMMERS
PRINTED NAME OF PERSON ABANDONING THE WE LL
STREET ADDRESS 493 BELL FARM ROAD STATESVILLE, NC 28625
�tlbmEt a.copy ..to: fhe .ouvn'er. and. Elie• or gjrial. go .`Dia%isi.an ofUiFafer Quafif=:'Infotinaiion: Rr s i y
ece s ng,
... - :..... Form GW-30
r :1617'f�lail Service Center, Raleigh, NG 27&99 3617, PHdte �9:f9:).8D7�6300
Rev. 5/10

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_
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p 610 E Center Ave
Mooresville, NC 28115
Take E Park Ave, Triplett Rd and
Cornflower Rd to Bell Farm Rd in
Chambersburg
f 1. bead west on E Center Ave toward Cedar
St
_.
246 ft
r'
2.
Turn right onto E Statesville Ave
0.4 mi
3.
Turn right at the 3rd cross street onto N
Church St
0.3 mi
4.
Turn left at the 3rd cross street onto E
Park Ave
3.8 m i
41
5.
Turn left onto Triplett Rd
7.1 mi
41
6.
Turn left onto Cornflower Rd
1.7 mi
-
408�798Mili;GardenRdC1
cvY =:2a3ess Ile 4 693 Befl Farm Rd
444 3id Creek Rd
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5/26/2015

Page 2mf3
Imagery @uoo
1'0 7. Turn right onto Bethesda RU
_-- _ __--_---- - .0.8m|
41 8. Turn left onto US-70 VV
-__-__-_-__-_------------_03m|
1~ 0. Turn right atthe 1stcross street onto
Salisbury Hwy
U.2m|
41 10. Turn left onto Bell Farm Rd
��DestinaUonwiUbeontheright
-- --- -- - '--- ' - 1.9mi
���/��-�'«��� MillsGarden [��
-,=� ^ �= .°.U//� =�n ��� ,wu
Statesville, NO28025
15. Head northeast onMills Garden Rd
�
m toward Barry Oak Rd
----------...... -- ----------- 0.4mi
lb. Turn left onto Barry Oak Rd
---------'------ --------- 07mi
lT Turn |*ft onto US-64 VV
*1
-71
5/2M/20l5

18. Turn.left onto Bell Farm Rd
4.0 mi
19. Turn right onto Salisbury Hwy
0.2 mi
20. Turn right onto US-70 W
_. 1.4mi
2.1. Turn left onto State Rte 2354/3rd
Creek Rd
Yv'i'i be on he ri::)Yi.
1.3 nl l
10.0 mi / 16 min
0 444 3rd Creek Rd
Statesville, NC 28677
These directions are for planning purposes only. You may find that construction
projects, traffic, weather, or other events may cause conditions to differ from the
map results, and you should plan your route accordingly. You must obey all signs or
notices regarding your route.
Page 3
5/26/2015

610 E Center Ave, Mooresville, NC 28115-2548 to 693 Bell Farm Rd Directions - Map...
Page 1 of 2
YOUR TRIP TO:
693 Bell Farm Rd
29 MIN I 17.0 MI
Est. fuel cost: $1.72
Trip time based on traffic conditions as of 8:36 AM on October 3, 2017. Current Traffic: Moderate
.....................................................................................................
1,. Start out going west on E Center Ave toward Cedar
St.
--------Then0,05 miles------------------------------ -------------------- ----------------------- -----O.B5-total-miles,
2. Take the 1st right onto E Statesville Ave.
E Statesville Ave is just past Cedar St.
If you reach N Sycamore St you've gone a little too far.
-----Then.0.5l-miles------- --------------------------------------------------- -------- ------- 0.56-total-miles
3. Turn right onto N Main St/NC-152.
r* N Main St is just past N Church St.
If you are on W Statesville Ave and reach Gum St you've gone a
little too far.
...Then.0-.28.miles-------------------- -----------------------------------------0:83-total-miles
4. Take the 2nd left onto W Park Ave/NC-801. Continue
to follow NC-801.
NC-801 is just past Culp St.
If you are on N Main St and reach W Stewart Ave you've gone about
0.1 miles too far.
Then.3.71.miles-------------------------------------------------------- ------------- •----- ----4.54.total-miles
5. Turn left onto Triplett Rd.
Triplett Rd is 0.5 miles past Wallaces Grant Dr.
If you reach Dupree Ln you've gone about 0.1 miles too far.
-------- Then4.54m iles-----------------_----..-...-.---..--------------------------------------------9:A8-total-miles
6. Turn left onto Ostwalt Amity Rd.
Ostwalt Amity Rd is 0.7 miles past Mount Tabor Rd.
If you reach Dixieland Dr you've gone about 0.3 miles too far.
--------Then1:62 miles ---------------------------------------------- -------------- ---------------40:70-total-miles
7. Turn right onto Bethesda Rd.
r+ Bethesda Rd is 0.2 miles past Brawley Rd.
If you reach Wheatfield Dr you've gone about 0.5 miles too far.
........Thea.3:90.m iles...............................••---...-------•----.......-.......-.------.....14.60.total. miles
` 8. Turn left onto US-70 W.
- Then0:31.miles. -------------•
-
total-miles
9. Take the 1st right onto Salisbury Hwy.
If you are on Salisbury Hwy and reach Old Warren Dr you've gone
about 0.2 miles too far.
Then 0:21-miles---------------------_----- ------ ---------------- ------- - 45.12-total-miles
httns://www.maDauest.comldirections/list/1 /us/north-carolinalmooresvillel28115-2548161... 10/3/2017

610 E Center Ave, Mooresville, NC 28115-2548 to 693 Bell Farm Rd Directions - Map... Page 2 of 2
' 10. Take the 2nd left onto Bell Farm Rd.
Bell Farm Rd is 0.1 miles past Chapel Hill Ln.
If you reach William Land Ln you've gone about 0.1 miles too far.
---- .Then-4:6&mi1es------------ •------------------ --------------- .... 46.73- total- mi!es
11. Turn right onto Sandpiper Rd.
r+ Sandpiper Rd is just past Katie Ln.
If you reach Farmwood Dr you've gone about 0.5 miles too far.
------Then-0.28.miles---------------------------------------------------- -- ----- •--r---------------17-.-Q1-total-miles
12. 693 Bell Farm Rd, Statesville, NC 28625-8555, 693
BELL FARM RD.
Your destination is at the end of Sandpiper Rd.
------------- ----------------- -------- --------- ---------------- ------------------ ---- ------ ------------------------------ -
Use of directions and maps is subject to our Terms of Use. We don't guarantee accuracy, route conditions or usability. You assume all risk of use.
Book a hotel tonight and Car trouble mid -trip?
save with some great deals! MapQuest Roadside
(1-877-577-5766) Assistance is here:
(1-888-461-3625)
htttis://www.maDauest. comldirections/list/ 1 /us/north-carolinalmooresville/281 l 5-2548161... 10/3/2017

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2013
PERMIT NO. WQ0006245
FACILITY NAME: Fourth Creek WWTP NPDES NCO031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: L.F. "Joe" Hudson Jr., Director
Water Resources
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Andy Smith J
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Andy Smith
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

Catof
tit
V. M. ISOX III • i$tatfsuillr, Nart4 Tarulina Z8687
I } MAR 3 2014 i �
'February 18, 2014
i t
Iq
Attention: Ed Hardee ...
NCDENR
1617 Mail Service Center
Raleigh, North Carolina 27699-1601
RE: Annual Reports for 2013
Third Creek Monofil. (WQ0004040)
Land Application (WQ0014543)
Alkaline Stabilization (WQ0006245)-
Dear Mr. Hardee:
Enclosed, you will find 3 copies each of the annual reports as referenced above.
All of the above referenced permits were in compliance for the calendar year 2013.
Should you require more information, or if further action is required, please contact me at 704- 878-343.8.
4Si cer 1
A dy S ith
WWTP upervisor, Fourth Creek WWTP
M 014
��F�R�Ario�;PR.,C�„U
�C�SSINf; t1NIT
2-Z
Olf A`�5� T d !'

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND" SUMMARY. FORM
WQ PERMIT #: WQ00062450 FACILITY NAME: Fourth Creek Alkaline Stabilization
PHONE: [phone] COUNTY: Iredell OPERATOR: Ray Wyrick
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
0 Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes 0 No ❑ —0� If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume
(dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
4th Creek WWTP
16.02
114
130
Various Farmers
128
Farmland
February
NPDES# NCO031836
35.47
280
315.47
Various Farmers
102
Personal & Farm
March
4th Creek WWTP
19.5
101
120
Various Farmers
142.2
Farmland
April
NPDES# NCO031836
29.9
375
405
Various Farmers
325.8
Farmland
May
4th Creek WWTP
10.5
87.3
97.8
Various Farmers
79.2
Turf
June
NPDES# NCO031836
16.75
134.7
151.45
Various Farmers
18
Farm/Garden
July
4th Creek WWTP
4
53
57
Various Farmers
0
Farmland
August
NPDES# NCO031836
3
60
63
Various Farmers
67
Farmland
September
4th Creek WWTP
20.2
140.6
160.8
Various Farmers
101
Landscaping
October
NPDES# NCO031836
36.3
301
340
Various Farmers
282.6
Farmland
November
4th Creek WWTP
23
245
268
Various Farmers
282.6
Farmland
December
NPDES# NCO031836
4.6
70.1
75
Various Farmers
0
Farmland
Total from FORM DMSDF (sup)
0
0
0
0
....................
Totals:
Annual (dry tons):
219.24
1961.7
2183.52
1528.4
Amendments used: Bulking Agent(s) used: Lime Kiln Dust
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and impriWnment for knowing violations."
Signature of Pennittee Date
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature o Preparer**
(if differen from Permittee)
�a-I
Date
DFNR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0006245. Laboratory: 1)
Facility Name: Fourth Creek WWTP 2)
Residual Source WQ # or NPDES # NCO031836 3)
NPDES #: 4)
WWTP Name: 5)
Re-eddi nl Annlvcic Dntn
Prism Labs
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
1/08/13
4/09/13
7/01/13
10/8/13
Percent Solids (%)
NA
68.80%
82%
80%
72%
Arsenic
75
4.9
7
20
6.9
Cadmium
85
<0.37
<0.31
<3.1
<0.34
Copper
4,300
32
27
290
30
Chromium
NA
N/A
N/A
N/A
N/A
Lead
840
6.8
14
14
9
Mercury
57
0.14
0.1
0.21
0.16
Molybdenum
75
N/A
N/A
N/A
N/A
Nickel
420
90
72
1 180
91
Selenium
100
2.5
2.1
<6.1
<.69
Zinc
7,500
150
66
57
41
Total Phosphorus
NA
3,800
1,800
1,700
2,000
TKN
NA
5,200
2,100
4,200
1,900
Ammonia -Nitrogen
NA
110
36
57
90
Nitrate and Nitrite
NA
18
38
7.7
20
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to a sure that qualified `pers nnel properly gathered and evaluated the information submitted. I am aware that there are significant
pe Iti s for su mitting f e information, including the possibility of fines and imprisonment for knowing violations.�4
Signature bf Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nGnio rnann QecG

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Fourth Creek WWTP Alkaline Stabilization
WWTP Name: Fourth Creek WWTP
Monitoring Period: From
1/1/2013
WQ Permit Number:
NPDES Number:
To 12/31 /2013
WQ0006245
NCO031836
Pnthnaen Rer111ctinn (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) 21
FAIt. C (Prior Testing) ❑
...................
AID (No Prior Test) ElProcess
to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A
only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray El
a
Gamma Ray El
ation ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑ jAerobic
Digestion ❑
on ti
c Digestion
A naerob �D ❑
g
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Allowable Level Pathogen Density
Number of Frequency Sample na yhca
Excee- Tech -
Parameter in Sludge
in Minimu Geo. Mean Maximum Units
of Analysis Type
dences ni ue
2 x 10 to the
MPN
<0.2
<1.0
mpn/g
60 days
grab
sm9221 e
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
<mpn/4g
coliform)
weight)
It/ +A++.-nn+.nn IJnAvid-tlnn 111A IVI -AL. IIG 1 _ 1 111 / 1 - I-WHSC 111111Ca LC a1LC111d L1 VC L10I 1VI 11AU; .
Alt.I (VS reduction)
❑
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) ❑
JAIL 4 (Spec. OZ uptake)
(]
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
❑
CERTIFICATION S'I'AIEMEN7" (please cnecK the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
si ifi ant penalties for false certification including fine and imprisonment."
Pre re ame an Title`(ty or print) / Land Applier Name and Title (if applicable)(type or print)
Signature f Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
DENR FORM PVRF 02T (12/2006)

NC Certification No. 402 Case Narrative
Full-Service Analytical &
RISMEnvironmental Solutions
t�'LAaORATORIES, INC.
SC Certification No. 99012
NC Drinkin Water Cert No. 37735
g 01/16/2013
VA Certification No. 1287
DoD ELAP Certification No. L2307
City of Statesville, NC Project: StaLime (Quarterly Parameters)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 01/08/2013
Statesville, NC 28687 Prism Work Order: 3010130
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
E Estimated concentration above the calibration range
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 5

Sample Receipt Summary
�,OP—i",',
,R I S Full -Service Analytical &
Environmental solutions 01/16/2013
Vi"L BORATORIEa INO
Prism Work Order: 3010130
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3010130-01 Solid 01/08/13 01/08/13
Samples received in good condition at 14.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 5

,,:.',t. _�..,. Laboratory Report
LN Full -Service Analytical &
®��'�k I S Environmental Solutions 01/16/2013
"—�—OFATOFIM ING
City of Statesville, NC Project: StaLime (Quarterly Client Sample ID: Sta-Lime
Attn: Andy Smith Parameters) Prism Sample ID: 3010130-01
P.O. Box 1111 Prism Work Order: 3010130
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/08/13 13:21
Time Submitted: 01/08/13 15:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1100
mg/kg
760
63
10
*Calculation 1/15113 10:21
CLB
[CALC]
Solids
68.8
% by
0.100
0.100
1
*SM2540 G 1/9/13 15:45
JAB
P3A0146
Weight
Nitrate/Nitrite as N
18
mg/kg dry
7.3
0.80
1
*SM4500-NO3 F 1115/13 10:21
CLB
P3A0104
Phosphorus -Total
3800
mg/kg dry
73
18
20
*SM4500-P F 1/11113 11:08
CLB
P3A0176
Total Kjeldahl Nitrogen
5200
mg/kg dry
3600
300
10
*351.2 1/12113 10:56
CLB
P3A0215
Ammonia as N
110
mg/kg
5.0
1.4
1
*SM4500-NH3 H 1/14/13 11:42
CLB
P3A0223
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1
*SM9221 E 1/9/13 13:05
MSV
P3A0196
mL
Total Metals
Mercury
0.14
mg/kg dry
0.027
0.0036
1
*7471B
1/11113 9:39
MEH
P3A0168
Arsenic
4.9
mg/kg dry
0.37
0.083
1
*6010C
1/10/13 17:44
BGM
P3A0152
Cadmium
BRL
mg/kg dry
0.37
0.039
1
*6010C
1110113 17:44
BGM
P3A0152
Copper
32
mg/kg dry
3.7
0.72
5
*6010C
1115113 20:42
BGM
P3A0152
Lead
6.8
mg/kg dry
0.37
0.091
1
*6010C
1/10/13 17:44
BGM
P3A0152
Nickel
90
mg/kg dry
1.5
0.45
1
*6010C
1/10/13 17:44
BGM
P3A0152
Potassium
5500
mg/kg dry
92
12
5
*6010C
1/15/13 20:42
BGM
P3A0152
Selenium
2.5
mg/kg dry
0.73
0.15
1
*6010C
1110113 17:44
BGM
P3A0152
Sodium
530
mg/kg dry
18
2.3
1
*6010C
1/10113 17:44
BGM
P3A0152
Zinc
150
mg/kg dry
3.7
0.38
1
*6010C
1/10/13 17:44
BGM
P3A0152
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 0f 5

Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Daterrime
3010130-01
P3A0215
0.05 g
25 mL
01/11/13 7:30
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Daterrime
3010130-01
P3A0176
1 g
50 mL
01/11/13 8:54
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
3010130-01
P3A0152
1.98 g
50 mL
01/10/13 8:00
3010130-01
P3A0152
1.98 g
50 mL
01/10/13 8:00
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime
3010130-01
P3A0168
0.65 g
50 mL
01/10/13 14:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 5

_ CHAIN OFCUSTODY RECORD
a Full -Service Analytical &
Environmental Solutions PAGE _ OF _ QUOTE # TO ENSURE PROPER BILLING:
LABORATORIES, IPIG
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224.0543 Project Name:
Phone: [phone] • Fax: 704/52S=01�4d9 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: C r �-v op S 40, eS V M t• *Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV)
�b provisions and/or QC Requirements
AN Sr►+ Report To/Contact Name: 46
Reporting Address: R O. -'BOX 1111 Invoice Address: :
SV0k;$& 11e NC
Phon®:.70 9- 8�8- 3Y3`7 FaX (Yes) {No):'70`1-S78-S653 purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) {NO) Email Address Requested Due Date ❑ 1. Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC_
EDD Type: PDF_ Excel —Other "Working Days" ❑ 6-9 Days El Standard 10 days ❑ Rush Work Must Be
Site Location Name: Jok4k CrecA Lt WTIP Pre -Approved SC OTHER N/A
11 Samples received after 15:00 will be processed next business day. —
Site Location Physical Address:03 Be// FA Girl R , Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO
S,EQ�CSYlII C NC (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES U Sample Iced on Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) P P
TIME MATRIX SAMPLE.CONTAINER ANALYSES REQUESTED
CLIENT DATE COLLECTED (SOIL, PRESERVA-
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 'TYPE TIVES /
HOURS SLUDGE) SEE BELOW NO. SIZE z�
PRISM
REMARKS LAB
ID NO.
1-8- 13 13. E I $ P — — -- Nis Q3 ✓ —As
C
Lb— TS
Se ---- �-
z.J TK
Signature �r
iguishing, this hain of Custo
In writing to the Prism Proje(
By:(Sign re)
By: (Signature)
\ 0 -FYI C
IES:
o .Shlpr
Ex ❑Lco) -
� C ❑ SC
NTAINE
your authorization.for Prism to I
nager. There will be charges for
I Affiliation
as requested above. Any changes must be
* have been initialized.
/-6.13 1 ?0b
S 13Hendrdellvered_ . Prism Field Service ❑Other
UST . GRQbW4TER: DRINKING WATER:, SOLID WASTE:. RCRA: CERCLA LANDFILL OTHER:.: :; ,..
❑ NC El SO ❑ NC ❑ SC .., I ❑ NC ❑ SC ❑ NC ❑ SC p NC ❑ SC ❑ NC ❑ SC ❑ NC' ❑ SC ❑ NC`:"❑ SC
El
I TYPE -CODES-, . A;=Amber _C = Clear G = Glass , P _. Plastic; TL ='Teflon L lned Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments
•
aSite Arrival Tlme �'� .� , ��3
Stte Departur ,Time t :.
7dlileage t ' + �.
�tC" SEE REVERSE FdR�"r
04TERIVIS A"' ONDt_IfdNS?'&
ORIGINAL

`- RISM
IES, INQ
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical R
Environmental Solutions
NC Certification No. 402
SC Certification No, 99012
NC Drinking Water Cart No. 37735
VA Certification No. 1287
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 01/22/2013
Prism Work Order: 3010458
Case Narrative
01 /28/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
., A--.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 5

,"Ism I
'_RATOA[ES INC.
Full -Service Analytical & Sample Receipt Summary
Environmental Solutions 01/28/2013
Prism Work Order: 3010458
Client Sample ID . Lab Sample ID Matrix Date Sampled Date Received
Sta Lime 3010458-01 Solid 01/22/13 01/22/13
Samples received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 5

' Laboratory Report
I R ISM I Full -Service ce al Solutions
&
Environmental Solutions 01/28/2013
7 U &O0 TORIM ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta Lime
Attn: Andy Smith Prism Sample ID: 3010458-01
P.O. Box 1111 Prism Work Order: 3010458
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/22/13 09:05
Time Submitted: 01/22/13 11:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatelTime ID
General Chemistry Parameters
% Solids
65.4
% by
0.100
0.100
1
*SM2540 G
1122/13 15:30
JAB
P3A0403
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
1/22/13 15:30
MSV
P3A0446
Total Metals
Mercury
0.23
mg/kg dry
0.029
0.0038
1
*7471B
1/25113 13:04
MEH
P3A0452
Arsenic
6.4
mg/kg dry
0.39
0.089
1
*6010C '
1/23/13 16:50
BGM
P3A0409
Cadmium
BRL
mg/kg dry
0.39
0.050
1
*6010C
1/23/13 16:50
BGM
P3A0409
Copper
34
mg/kg dry
0.77
0.15
1
*6010C
1/23/13 16:50
BGM
P3A0409
Lead
8.9
mg/kg dry
0.39
0.052
1
*6010C
1123/13 16:50
BGM
P3A0409
Nickel
110
mg/kg dry
1.5
0.014
1
*6010C
1/23/13 16:50
BGM
P3A0409
Selenium
2.8
mg/kg dry
0.77
0.18
1
*6010C
1/23113 16:50
BGM
P3A0409
Zinc
67
mg/kg dry
3.9
0.52
1
*6010C
1123/13 16:50
BGM
P3A0409
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 5

Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Daterrime
3010458-01 P3A0409 1.98 g 50 mL 01/23/13 8:30
Prep Method: 7471B
Lab Number Batch Initial Final Daterrime
3010458-01 P3A0452 0.64 g 50 mL 01/24/13 12:50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 5

1-
�� Y���I � n � I Full -Service Analytical &
_, i:�!, '< ' V I Environmental Solutions
ANKIEUMVIASORATORIM INC.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone:[phone] - Fax:[phone]
Client Company Name :C:+v o-fn S4e.4e.sw-Me
Report To/Contact Name: 41,12v Sr+ti-lt
Reporting Address: Z. 0. Bay I I I l
Swdcsyi!IG
CHAIN OF CUSTODY RECORD
PAGE _ OF _ QUOTE q TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) . (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or OC Requirements
Invoice To:
Address: —
Phone:70y- 578- 3g38 Fax es (No):701- 978- T655 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date di Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC
EDD Type: PDF_ Excel _Other "Working Days" O 6-9 Days. 0 Standard 10 days ❑ Rush Pork Must Be
Pro -Approved
SC OTHER N/A
Foss -k Greek W O TP
Site Location Name: Samples received after 15;00 will be processed next business day.
Site Location Physical Address: 493 B e II FArrr P Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
S �4� 11 NC
Sample Iced Upon Collection: YES NO
CSV� a RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENTFDATECOLLECTED
TIME
MATRIX
(SOIL,
SAMPLE CONTAINER
�
PRESERVA-
ANALYSES REQUESTED
\ / \5
PRISM
LAB
*TYPE
MILITARY
WATER OR
TIVES
o- k� REMARKS
/
ID NO.
SAMPLE DESCRIPTIO
NO.
SIZE
HOURS
SLUDGE)
SEE BELOW
W,A_ ,
09;�5
S
P
_.-
I'�a
✓
Zfow
I'b
S rp
O bit � I Affiliation
Sampler's Signature Sampled By (Print Name) AY
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be I e
submitted in writing to the Prism Project Manager. There will b harges for any changes after analyses have been initialized.
Relin 's ed By: (Signature) Rece e i By: (Signal Date MilltarylHo s Additional Comments Site Arrival Time _.
0
Site Departure Time
Relin ' had By: (Signature) y: (Signature) Date r
r/ 3 60Fleld Tech Fce
'aboratories By: Date _ -
ell is ed By: (Sig at e) Re�ITID'
D_zP
elhod of Shipment: NOTE: ALL SAMPLE COOLERSSHOULD.BE TAPED SHUT WITLS RANSPO16 RTATION TO THE LABORATORY. COC Group No.
SAMPLESARENOT C EPTED AND VERIFIED AGAINST COCD A HE LABORATORY.
CD �,ch►� KSS
Fed Ex ❑ UPS 0 Hand -delivered Ism Field Service ❑ Other
PDES: UST: G UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL . ,
�OTHER:.
NO El SC El NO ❑ SC ❑ C ❑ SC I ❑ NO ❑ SC ❑ NO ❑ SC I ❑ NO ❑ SC ❑ NC ❑ SC I ❑ NC El SC ❑.NC' O SC
I
❑ ❑ ORIGINAL
_
rr — el— r- — rla— P — Plactin• TI = Taflnn-I inarf Can VOA = Volatile Organics Analvsis (Zero Head Space)

{
fR I S
1,1�1'ltl'�'LABORATORIE$ INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 1287
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 02/04/2013
Prism Work Order: 3020044
Case Narrative
02111 /2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a—.
?rv--
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
*. Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 5

ISM I Sample Receipt Summary
Full -Service Analytical &
i' Environmental Solutions 02/11/2013
'.OR TOnIES ING
Prism Work Order: 3020044
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3020044-01 Solid 02/04/13 02/04/13
Samples received in good condition at 4.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its.entirety, without.the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 Of 5

f00-I S Full -Service Analytical & Laboratory Report
Environmental Solutions 02/11/2013
M;IIABORATORIEal—
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3020044-01
P.O. Box 1111
Prism Work Order: 3020044
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/04/13 11:20
Time Submitted: 02/04/13 15:30
Parameter
Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids
64.5 % by 0.100
0.100 1 *SM2540 G 218/13 8:30 LTB P3130134
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/100 1 1 *SM9221 E 2/5/13 9:54 MSV P3130147
mL
Total Metals
Mercury
0.16
mg/kg dry
0.032
0.0043 1
Arsenic
17
mg/kg dry
1.9
0.44 5
Cadmium
BRL
mg/kg dry
1.9
0.25 5
Copper
44
mg/kg dry
3.8
0.75 5
Lead
16
mg/kg dry
1.9
0.26 5
Nickel
120
mg/kg dry
1.5
0.014 1
Selenium
BRL
mg/kg dry
3.8
0.87 5
Zinc
75
mg/kg dry
19
2.6 5
*7471B
217/13 13:39
MEH
P3B0123
*6010C
218/13 12:42
BGM
P3130097
*6010C
2/8/13 12:42
BGM
P3130097
*6010C
218/13 12:42
BGM
P3B0097
*6010C
2l8/13 12:42
BGM
P3B0097
*6010C
217/13 19:59
BGM
P3130097
*6010C
218/13 12:42
BGM
P3B0097
*6010C
218/13 12:42
BGM
P3B0097
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 5

Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Datefrime
3020044-01
1`380097
2.03 g
50 mL
02/06/13 8:10
3020044-01
P3130097
2.03 g
50 mL
02/06/13 8:10
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
3020044-01
P3B0123
0.58 g
50 mL
02/07/13 9:35
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 5

n � I S
� nIFull-Service Analytical &
' V' Environmental Solutions
RIES, INC.
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone:[phone] • Fax:[phone]
Client Company Name: C;�v oP
Report To/Contact Name: AHR y SM fl,
Reporting Address: P-O• _BOV I I I I
3Fa4esv;11a NC
CHAIN OF CUSTODY RECORD
PAGE OF QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invnine Tin!
Address:
Phone:'/09-8'7If- sy i'! Fax QigDs (No):'101- d ZY-1635 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days. ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL NO
EDD Type: PDF_ Excel_Other "„ Rush Work Must Be
Working Days ❑ 6-9 Days ❑Standard 10 days ❑
Site Location Name: Feu r 1 t, G` rc e k LJ la1 TP Pre -Approved
SC OTHER
N/A
Samples received after 15:00 will be processed next business day.
Site Location Physical Address:19 3 Bc 11 Far ,m 99.. Turnaround time Is based on business days, excluding weekends and holidays.
—
Water Chlorinated: YES_ NO—
S�acCSV IIC NC
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample le Iced Upon Collection: YES
P P
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
GP llP REMARKS
ID NO.
HOURS
SLUDGE)
SEE BELOW
SE>a- �(,.��
a-�I-,
!I. ao
S
P
Nads�2
✓
t3; W«i�J
TcsL
As
C1
Cu
R
N,°
Se
zN
o a
Sampler's Sigriature Sampled By (Print Name) �a r1 c Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
Relln fished By: (Signat _ n R
ved B : (Sfgnat Date Military/Hours Additional Comments
YSite'Arnval Tlme
Refi ed B : (S ature) ��CC '99YY� eRed By: (Signature) Date
Slle. Departure T(me s
/
1
tFleld Tech Fee
quished By: (Sign ) ecei or Prism Laborator es y: Date
'O
2< Y-13 ISM
aIleage
N Tod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT W
CUSTODY A OR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT CCEPTED AND VERIFIED AGAINST C?D UNTIL
RECEIVED AT THE LABORATORY.
Ul d Ex ❑ UPS ❑ Hand -delivered rism Field Service ❑ Other
ES: I UST: G UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
U' C ❑ SC El NC ❑ SC ElC ❑ SC ❑ NC ❑ SC
❑ NC El SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC Cl SC I ❑ NC ❑ SC
❑ ______ ❑ ___ ❑ .
❑ __ ❑ ❑ _ ❑ ❑
ORIGINAL
NTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL =Teflon -Lined. Cap VOA = Volatile Organics Analysis (Zero Head Space)

� 1S
a'-'`LABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 1287
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 02/11/2013
Prism Work Order: 3020260
Case Narrative
02/19/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager Reviewed By
Data Qualifiers Key Reference:
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
:..-W . . This: report should not. be,reproduced,.except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 11

N R I S
£'^��€ti-' IAfiORATOPIES ING
Full -Service Analytical &
environmental Solutions
Sample Receipt Summary
02/19/2013
Prism Work Order: 3020260
Client Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
Sta-Lime 1
3020260-01
Solid
02/11/13
02/11/13
Sta-Lime 2
3020260-02
Solid
02/11/13
02/11/13
Sta-Lime 3
3020260-03
Solid
02/11/13
02/11/13
Sta-Lime 4
3020260-04
Solid
02/11/13
02/11/13
Sta-Lime 5
3020260-05
Solid
02/11/13
02/11/13
Sta-Lime 6
3020260-06
Solid
02/11/13
02/11/13
Sta-Lime 7
3020260-07
Solid
02/11/13
02/11/13
Samples received in good condition at 1.5 degrees C unless otherwise noted
This report should not :be;reproduced, except,in its entirety, without the written,ponsent of Prism-Lab1.oratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 0f 11

t
;.
Laboratory Report
0 I S Full -Service Analytical
&
�' .Environmental
•� LABORATORIES ING
Solutions
02/19/2013
City of Statesville, NC
Project: StaLime
Client Sample ID:
Sta-Lime 1
Attn: Andy Smith
Prism Sample ID:
3020260-01
P.O. Box 1111
Prism Work Order: 3020260
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/11/13 11:15
Time Submitted: 02/11/13 13:40
Parameter
Result Units
Report
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
66.1
% by
0.100
0.100
1 *SM2540 G
2/12/13 16:15
JAB
P3B0240
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
2
1 *SM9221 E
2/12/13 10:35
MSV
P3BO244
Total Metals
Mercury
0.15
mg/kg dry
0.030
0.010
1 *7471B
2114/13 12:51
MEH
P3B0261
Arsenic
21
mg/kg dry
3.8
0.87
10 *6010C
2/18/13 14:02
BGM
P3B0254
Cadmium
BRL
mg/kg dry
3.8
0.50
10 *6010C
2/18/13 14:02
BGM
P3B0254
Copper
39
mg/kg dry
7.6
1.5
10 *6010C
2/18/13 14.02
BGM
P3B0254
Lead
18
mg/kg dry
3.8
0.51
10 *6010C
2/18/13 14:02
BGM
P3B0254
Nickel
200
mg/kg dry
15
0.14
10 *6010C
2/18/13 14:02
BGM
P3B0254
Selenium
BRL
mg/kg dry
7.6
1.7
10 *6010C
2118/13 14:02
BGM
P3BO254
Zinc
74
mg/kg dry
38
5.1
10 *6010C
2118113 14:02
BGM
P3B0254
This reportshould not.be.reproduced,.except.in its entirety, without the written consent of ,Prism Laboratories ,Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 11

1.
C. Full -Service Analytical &
Environmental Solutions
�=�^�•K LABORATORIES, INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
02/19/2013
Client Sample ID: Sta-Lime 2
Prism Sample ID: 3020260-02
Prism Work Order: 3020260
Time Collected: 02/11/13 11:15
Time Submitted: 02/11/13 13:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 69.6 % by 0.100 0.100 1 'SM2540 G 2/12/13 16:15 JAB P3130240
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 1 1 'SM9221 E 2/12/13 10:35 MSV P3130244
J
:.: .
- " This, report should not be reproduced;, except in its:entirety,-without the.wntten consent of Prism, a oratories,Inc..--.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 0f.11

Laboratory
Report
'
R ISM Full -Service Analytical 8
/jnvironmental Solutions
! ='" % r E
ISM
02/19/2013
� - � - LABONATOPIES ING
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime 3
Attn: Andy Smith
Prism Sample ID: 3020260-03
P.O. Box 1111
Prism Work Order: 3020260
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/11/13 11:15
Time Submitted: 02/11/13 13:40
Parameter Result Units Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 66.8
% by 0.100
0.100 1 `SM2540 G 2/12113 16:15 JAB
P3B0240
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry 1
1 'SM9221 E 2112/13 10:35 MSV
PjB0244
' This report`should not be reproduced;,except,in.its entirety, without the written, consent of Prism1aboratories, oc. , ...,,,,
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 Of

Laboratory, Report-
f�C'x Full -Service Analytical &
I S M
L Ilh.� Environmental Solutions
02/19/2013
.a`�.ae'�w. �' LABORATORIES INC.
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime 4
Attn: Andy Smith
Prism Sample ID: 3020260-04
P.O. Box 1111
Prism Work Order: 3020260
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/11/13 11:15
Time Submitted: 02/11/13 13:40
Parameter Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids 65.8
% by
0.100
0.100 1 'SM2540 G 2112/13 16:15 JAB
P3B0240
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
2
1 'SM9221 E 2/12/13 10:35 MSV
P3B0244
"This report'should not be reproduced,' except in itsrentirety, without themritten consent of:Prism Laboratories, Inc..
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 0f 11

s
Full -Service Analytical &
I S Environmental Solutions
".Fi�a S'FLABO-RIM INC.
Laboratory Report
02/19/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime 5
Attn: Andy Smith
Prism Sample ID: 3020260-05
P.O. Box 1111
Prism Work Order: 3020260
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/11/13 11:15
Time Submitted: 02/11/13 13:40
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date rime
ID
General Chemistry Parameters
% Solids
66.8 % by
0.100
0.100 1 'SM2540 G 2/12113 16:15 JAB
P3B0240
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
1
1 `SM9221 E 2112/13 10:35 MSV
P3B0244
This report should not be reproduced, except in its entirety„without the, written consent of, Prism Laporatories Inc
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of ,

S �,.Full-Service Analytical &
[
R ISM Environmental Solutions
�.'-f' LA60PATORIE$ INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111 J
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
02/19/2013
Client Sample ID: Sta-Lime 6
Prism Sample ID: 3020260-06
Prism Work Order: 3020260
Time Collected: 02/11/13 11:15
Time Submitted: 02/11/13 13:40
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 66.5
% by
0.100
0.100 1
'SM2540 G 2/12113 16:15 JAB
P3B0240
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
2
1
'SM9221 E 2/12/13 10:35 MSV
P3B0244
This report should`not'be reproduced, exceptin its entirety, without thewritten consent•of Prism Laboratories,, Inc.,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 11

LaboratoryReport
flblzn�`R, ISM | | c=iro"m"m"o"uu"=
02n912013
City ofStatesville, NC
Project: StaLkna
Client Sample ID: 8ta-Lime7
Attn: Andy Smith
Prism Sample ID: 3U2O2O.0-n7
PD.Box 1111
Prism Work Order: uuu000O
Statesville, NC2o0O7
Sample Matrix: Solid
Time Collected: QD11/1311:Ys
Time Submitted: O2/ 1/1313:40
'
Parameter Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
General Chemistry Parameters
% Solids ma
% by
0.100
0.100 1 *SM254o 2n2/1316:15 JAB
P3aO240
Weight
Microbiological Parameters
This report should �ot:b,renmuucedaxceptmits entirety, wimounxe~nno consent mrnmnLaovratones,m�,._,_,~~`~
*monri"obr"okRoad 'p.O.Box c^mm'Charlotte, mcxmu*-0s*
Phone: mwso-6o64'Toll Free Number: 1-8omxe9-n36*'Fax: r04sx5-o*o

Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Date/Time
3020260-01 P3B0254 1.99 g 50 mL 02/13/13 11:00
Prep Method:7471B
Lab Number Batch Initial Final Daterrime
3020260-01 P3B0261 0.6 g 50 mL 02/13/13 13:15
This report should*not be repro uce , except in its entirety, wnnout ine w ,. r: ,. ,;;-:.::,..:>.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 -,Fax: [phone] Page 10 of 11

Full -Service Analytical &
sa
IS I Environmental Solutions
M
LABORATORIES INQ
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone:[phone] - Fax:[phone]
Client Company Name: Cj'L o7P
Report To/Contact Name: Andy S- dhi
Reporting Address. P 0 B Ay III I
S40,4C.-S,.; j(e MC
CHAIN OF CUSTODY RECORD
PAGE _ OF _ QUOTE tt TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone: 7Oq-B'IE-3LI38 Fax es (No):70`I- 878- 455 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC ---"
EDD Type: PDF_ Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Pre h Work Must Be
SC OTHER N/A
F-
Site Location Name: Kra � C rc mk W W TP Samples received after 15:00 will be processed next business day.
`—
Site Location Physical Address: 693 Be -I( tmrm RX . Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES _ NO _
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
S-(o_*e I I
Sample Iced Upon Collection: YES NO
p
SV r e A/C RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
`TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
NO.
SIZE
TIVES
�GP ��
ID NO.
HOURS
SLUDGE)
SEE BELOW
90 Isa43
—
AS
C9
gob
C,
PL
H
Nr
i 563
Sampler's Signature Sampled By (Print Name) �� Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be o
Prism Project Manager. There will be charges for any changes after analyses have been initialized.
submitted in writing to the
Rece etl By: Slgnatur D Military/Hours Additional Comments:
ISlte ArrrvalTlme
�Rye'!�ished By:. SI nature) O
� /�
'LDa Slte Departure flm a
R ad�By.. Re rve By: (Signature)d
(Signature)
By(Sign e) ceived F-r Prism Laboratories By: Date
NMlleage
1-4
ly �...
od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WIT CUSTODY SEAL R TRANSPORTATION TO THE LABORATORY. COC Group No.
(D SAMPLES ARE NO CEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY.
fo
d Ex ❑ UPS O Hand -delivered dsm Field Service ❑ Other
ES: UST: GR DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: •,
1
❑SC ❑NC pSC ,❑N ❑SC ' ❑NC ❑SC I ❑NC ❑SC ONO ❑SC ❑NC ❑SCI ❑NC ❑SC ❑NC ❑SC
I
❑ ❑ ❑ ❑ — ❑ ❑ —_— ❑ ❑ ORIGINAL
__—
......� . T...,.- .,.,.,_�. A - A.. kk (r - r_ - r-f— P - Plactii" TI = Tifinn-Lined Car) VOA = Volatile Organics Analysis (Zero Head Space)
i

i r-A 1 Y 1
,1' IA80RATORIES, INa
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 1287
DoD ELAP Certification No. L2307
Project; StaLime
Lab Submittal Date: 02/25/2013
Prism Work Order: 3020562
Case Narrative
03/04/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
FEW!
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 5

Sample Receipt Summary
�j'g R I S M Full -Service Analytical &
V � Environmental Solutions 03/04/2013
- --OR TORIES, ING
Prism Work Order: 3020562
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3020562-01 Solid 02/25/13 02/25/13
Samples received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 5

9-Jos—M—Nc.
IFunService AnalyticalEnvironmental Solutionss
Laboratory Report
03/04/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3020562-01
P.O. Box 1111
Prism Work Order: 3020562
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 02/25/13 11:50
Time Submitted: 02/25/13 13:40
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
_
Solids
70.3
% by
0.100
0.100
1 *SM2540 G 2128/13 9:30
LTB
P360558
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1 *SM9221 E 2/26/13 11:48
MSV
P3C0011
mL
Total Metals
Mercury
0.10
mg/kg dry
0.030
0.010
1 *7471B 2128/13 11:55
MEH
P3B0556
Arsenic
17
mg/kg dry
0.36
0.082
1 *6010C 2/28/13 14:08
BGM
P380505
Cadmium
BRL
mg/kg dry
0.36
0.046
1 *6010C 2/28/13 14:08
BGM
P3B0505
Copper
30
mg/kg dry
0.71
0.14
1 *6010C 2/27/13 0:42
BGM
13360505
Lead
11
mg/kg dry
0.36
0.048
1 *6010C 2127/13 0:42
BGM
13360505
Nickel
130
mg/kg dry
1.4
0.013
1 *6010C 2/27/13 0:42
BGM
P3B0505
Selenium
1.9
mg/kg dry
0.71
0.16
1 *6010C 2/27113 0:42
BGM
P3B0505
Zinc
57
mg/kg dry
3.6
0.48
1 *6010C 2/28113 14:08
BGM
P3B0505
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 5

Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Date/Time
3020562-01 P3B0505 2 g 50 mL 02/26/13 8:15
3020562-01 P3B0505 2 g 50 mL 02/26/13 8:15
Prep Method: 7471B
Lab Number Batch Initial Final Date/rime
3020562-01 P3130556 0.57 g 50 mL . 02/27/13 14:00
This reportshould not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 5

(E � I I Full -Service Analytical
SMEnvironmental Solutions
LABORATORIES INQ
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phohe:7047629-6364 • Fam 704/525-0409
Client Company Name: C I4v of' SEa �esv 1lc
Report.To/Contact Name: A..04 3ra:41l
Reporting Address: _P 0. 13ox 11 I I
$Ea Ersyi !!c NC
Phone:70'{- 878- 313 8 Fax es (No):709- 878-8955
Email (Yes) (No) Email Address
EDD Type: PDF_ Ex_cel_Othei .
Site Location Name: i'o w 4 6 C, Me (C W W T P
Site Location Physical Address: 693 Belt F41.1 1?d ,
S4-�C.SVIWe NC
TIME MATRIX
CLIENT DATE COLLECTED (SOIL,
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
HOURS SLUDGE)
CHAIN OF CUSTODY RECORD
PAGE — OF _ QUOTE # TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
In"nina Tn•
Address:
Purchase Order No./Billing Reference 'TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Pre -Approved hWork Must Be SC OTHER N/A
Samples received after 15:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO —
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection' YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
LE CONTAINER
ANALYSES REQUESTED
SAMPPRISM
*TYPE NO. SIZE PRTIVES A- /�e,�/
A��/
/ / / REMARKS LAB
ID NO.
SEE BELOW
Spa,- ;•re a"R-d5=13 111:50 I S 1� I 1N.ds?03 %s� I S� Z
spa„ Z.,rrl a. I I I s I P I L I I 1 I C u-I ! I ---I !-- I
Sampler's Signature /rtcu�rrzenaC Gt/�-��I Sampled By (Print Na
Upon relinquishing, this Chain of Custody is your authorization for Prism to I
submitted in writing to the Prism Project Manager. There will be charges for
Relin shed By: (Signature) Rec d By: Sigr
I
z.
n /` o -
MondC 6)_ IC Affiliation
with the analyses as requested above. Any changes must be
nges after analyses have been initialized.
D e ryry r Military/Hours Additional Comments
jt
itgtilshed By: (Signature) ne, Ur 1-1
0
t L-ZSIZ (3ttJ
N hod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH C STODY SEALS I-OR-9RANSPORTAT11ON TO THE LABORATORY. _ COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COO UNTIL RECEIVED.AT THE.LABORATORY. '3 011 /
0 ed Ex . ❑ UPS ,0 Hand -delivered - . � - .rism.Field Service O.Other (�
KING
CERC
LANDFILL' I OTHER:
C ❑ SC ❑ NO ❑ SC I 0 NO ❑ SCTER: I D❑NO - C3 CATER: I SOLID NC ❑ SC E. ❑❑ NO ❑ SCI ❑❑ NC L❑ SC O NO 3 SC El NO ❑ SC
lj_*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
•
F � {
Site Arrival Tlme
' S�te�Departu�e Tlme
r
kField Tech Fee P ?xi7
tulilage ,
ipt J
ORIGINAL

c.ati r
ism
n' LABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cart No. 37735
VA Certification No. 1287
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 03/11/2013
Prism Work Order: 3030258
Case Narrative
03/18/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call -if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) �_ U/t
President/Project Manager
WOW ' 11!illl '_ p
r
Reviewed By
Data Qualifiers Key Reference:
BH. MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported. to.the.MDL.with.values.between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except,in, its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 5

�Inull-Service Analytical 8
I . � V E
io"i"r—,nvironmental Solutions
-`.'ALA —T—es ING
Sample Receipt Summary
03/18/2013
Prism Work Order: 3030258
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3030258-01 Solid 03/11/13 03/11/13
Samples received in good condition at 4.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 5

^
Laboratory Report
�n Full -Service Analytical
iP I I V Environmental
&
Solutions
03118/2013
r LABORATORIES INC.
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3030258-01
P.O. Box 1111
Prism Work Order: 3030258
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 03/11/13 11:25
Time Submitted: 03/11/13 15:25
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
63.5
% by
0.100
0.100
1 *SM2540 G 3/12/13 14:30
LTB
133CO218
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 3/12/13 11:00
MSV
P3CO238
Total Metals
Mercury
0.21
mg/kg dry
0.033
0.011
1 *74718 3/13/13 14:20
MEH
P3CO212
Arsenic
11
mg/kg dry
0.39
0.089
1 *6010C 3113113 19:33
BGM
P3C0195
Cadmium
BRL
mg/kg dry
0.39
0.050
1 *6010C 3/13/13 19:33
BGM
P3C0195
Copper
32
mg/kg dry
0.77
0.15
1 *6010C 3/13/13 19:33
BGM
PX0195
Lead
33
mg/kg dry
0.39
0.052
1 *6010C 3/13/13 19:33
BGM
PX0195
Nickel
92
mg/kg dry
1.5
0.014
1 *6010C 3/13/13 19:33
BGM
P3C0195
Selenium
1.6
mg/kg dry
0.77
0.18
1 *6010C 3/13/13 19:33
BGM
PX0195
Zinc
62
mg/kg dry
3.9
0.52
1 *6010C 3/13/13 19:33
BGM
P3C0195
This report should not be reproduced,_ except, in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 5

Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Daterrime
3030258-01 P3C0195 2.04 g 50 mL 03/12/13 8:20
Prep Method: 7471B
Lab Number Batch Initial Final Daterrime
3030258-01 PKk12
0.58 g 50 mL 03/12/13 13:00
This report should not be_reproduced,,except in its entirety,, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 5

Full -Service Analytical &
�; Y I M I Environmental Solutions
LAsoRATORIES. INQ
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone:[phone] • Fax:[phone]
Client Company Name: C J11 o'F
Report To/Contact Name: A ng v Sm , 46
Reporting Address: P O. 13ox I I I I
9444csv%l1e "a
bnu_ cn a_ ou -2 d
CHAIN OF CUSTODY RECORD
PAGE _ OF _ QUOTE p TO ENSURE PROPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
���� - — �aA LiCsjIt1VVJ. a
Email (Yes) (No) Email Address
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
EDD.Type: PDF_Excel
Requested Due Date ❑ 1 Day C)p 2 Days 3 Days ❑ 4 Days Q,5 Days
Certification: NELAC USACE
FL NC
_Other
Site Location Name' Fom r4A C r oak W W T P
"Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ PreSApprrovedust Be
'
Site Location Physical Address: 9a I / Fo �.,, 1�
Samples received after 15:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
SC OTHER
Water Chlorinated: YES_ NO
N/A
/99.3
SYa��rS✓��I1 a /� C
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection. YES
_ NO _
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
PRESERVA-
TIVES
e'�i e
REMARKS
TYPE
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
���
IDLAB
NO.
S4q-1,;M� _
3-I/-13
IIraS
S
P
_P�oLasA03
✓
�;-wee l
7
1
Spa-�/•tee
3-11-•13
W.2.6
oNe
As
CQ
Cu
P6
w
t;
S�
ZN
Sampler's Signature 44CLZ
Sampled By
(Print Name) a f"0_1 C GV P;nk Affiliation
Upon relinquishing, this Chain of Custody is your authorization for
Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Rellr. hed By: (Signature) Re ived By: (Signs D MilitaryMours Additional Comments:Site
ArrivalrTime
Rel' shed B Si natur
Y: ( 9 ) RecNAd
By: (Signature) Date
Slte peparture Time-:`;
' J
linq By: (Signature) Rec iv d F r Prism La t s By: Date
E(eltl Tech Fee
-O thod o Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WI CUS SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
(D ARENOT ACCEPTEDVERIFIED AGAINST COC UN CEIVED ATTHE LABORATORY.
C
Ex ❑ UPS ❑ Handd�`(/
rmF Field Service ❑O1`°ed
el'veed
"��f ✓
3�63r�Sz
DRINKING SOLID E. LANDFILL❑
DES❑"SCI L❑
NC NICKI❑ SCATER:
❑❑ NC ❑ SC I ❑❑ N ❑ SCTER:
NC ❑ SC I ❑ NC ❑ SC ❑ NC SC ❑ NC SC ❑ NC ❑ SC
I
❑ ❑ ❑ — ❑ ❑
NTAINER TYPE"CODES:. A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head SDace)
ORIGINAL

4. 'RISM
LABORATORIES INC.
City of Statesville, NC
Andy Smith .
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 03/25/2013
Prism Work Order: 3030527
Case Narrative
04/02/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Vl.•
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
?,-
D RPD value outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
= This report should not be -reproduced, except in its.entirety, without the written consent of Prism Laboratories, lnc. .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543
Phone: [phone] -Toll Free Number: 1.800/529-6364 - Fax: [phone] Page 1 of 7

Sample Receipt Summary
t7 , Full -Service Analytical & is environmental Solutions 04/02/2013
RIF$ING Prism Work Order: 3030527
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3030527-01 Solid 03/25/13 03/25/13
Samples received in good condition at 1.4 degrees C unless otherwise noted.
p p p tyoratoriesInc.
This -re ort-should not be reproduced, except its entire, .without the written. consent of Pnsm ab= . , , .
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
®L* Full -Service Analytical &
RAR I S M Environmental Solutions 04102/2013
t XLABOR IMES'.a
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3030527-01
P.O. Box 1111 Prism Work Order: 3030527
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/25/13 11:50
Time Submitted: 03/25/13 14:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids
Microbiological Parameters
55.4
% by
Weight
0.100
0.100
1
*SM2540 G
3/26113 14:30
LTB
P3C0516
Fecal Coliforms
BRL
MPN/g dry
0.4
1
*SM9221 E
3/26/13 11:15
MSV
P3C0532
Total Metals
Mercury
0.26
mg/kg dry
0.038
0.013
1
*7471B
3126/13 11:58
MEH
P3C0498
Arsenic
13
mg/kg dry
2.2
0.51
5
*6010C
412/13 1:50
BGM
P3D0002
Cadmium
BRL
mg/kg dry
2.2
0.29
5
*6010C
4/2/13 1:50
BGM
P3D0002
Copper
62
mg/kg dry
4.4
0.86
5
*6010C
4/2/13 1:50
BGM
P3D0002
Lead
100
mg/kg dry
2.2
0.29
5
*6010C
4/2/13 1:50
BGM
P3D0002
Nickel
150
mg/kg dry
8.8
0.078
5
*6010C
4/2/13 1:50
BGM
P3D0002
Selenium
BRL
mg/kg dry
4.4
1.0
5
*6010C
4/2/13 1:50
BGM
P3D0002
Zinc
160
mg/kg dry
22
3.0
5
*6010C
4/2/13 1:50
BGM
P3D0002
This report should not be reproduced, except in its -entirety, without the written consent of Prism. Laboratories, Inc.. _
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 7

/&-:VC Full -Service Analytical &
wllRISEnvlronmental Solutions
= 'LABORATORIES,-
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
4/2/13
Prism Work Order: 3030527
Time Submitted: 3/25/2013 2:20:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P3C0498 - 7471 B
Blank (P3C0498-BLK1) _ Prepared & Analyzed: 03/26/13
Mercury BRL 0.021 mg/kg wet
LCS (P3CO498-BSI) Prepared & Analyzed: 03/26/13
Mercury 0.459 0,021 mg/kg wet 0.4386 105 80-120
Matrix Spike (P3CO498-MS1) Source: 3030527-01 Prepared & Analyzed: 03/26/13
Mercury 0.732 0.036 mg/kg dry 0.7398 0.261 64 80-120 MI
Matrix Spike Dup (P3CO498-MSD1) Source: 3030527-01 Prepared & Analyzed: 03/26/13
Mercury 0.915 0.038 mg/kg dry 0.7917 0.261 83 80-120 22 20 D
Batch P3D0002 - 3050B
Blank (1P3D0002-BLK1)
Prepared: 04/01/13 Analyzed: 04/02/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3130002-13SI)
Prepared: 04/01/13 Analyzed: 04/02/13
Arsenic
25.1
0.25
mg/kg wet
25.38 99 80-120
Cadmium
24.5
0.25
mg/kg wet
25.38 97 80-120
Copper
26.2
0.51
mg/kg wet
25.38 103 80-120
Lead
24.8
0.25
mg/kg wet
25.38 98 80-120
Nickel
24.8
1.0
mg/kg wet
25.38 98 80-120
Selenium
24.9
0.51
mg/kg wet
25.38 •98 80-120
Zinc
24.7
2.5
mg/kg wet
25.38 97 80-120
-. -. This -report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 7

ISn Full -Service Analytical/tF I �' Environmental Solutions
Z Y LABORATORIES INO
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Level II QC .Report
4/2/13
Prism Work Order: 3030527
Time Submitted: 3/25/2013 2:20:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PX0516 - Default Prep Metals
Blank (P3C0516_-BLK1) Prepared & Analyzed: 03/26/13
% Solids 99.9 0.100 % by Weight
p Laboratories, Inc.
This re ort should not be reproduced, except in its entirety, without the written consent of Prism Lab
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 7

-
Level II QC Report
Full -Service Analytical
4/2/13
L ' ISM
Environmental Solutionss
rlA80RATOPIES, INC.
City of Statesville, NC
Project: StaLime Prism Work Order: 3030527
Attn: Andy Smith
Time Submitted: 3/25/2013 2:20:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3C0532 - NO PREP
Blank (P3C0532-BLK1)
Prepared & Analyzed: 03/26/13
Fecal Coliforms
BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Default Prep Metals
Lab Number Batch
Initial Final Date/Time
3030527-01
P3C0516
30 g
30 mL
03/26/13 14:30
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/rime
3030527-01
P3D0002
2.05 g
50 mL
04/01/13 9:45
3030527-01
P3D0002
2.05 g
50 mL
04/01/13 8:20
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/rime
3030527-01 P3C0498 0.57 g 50 mL 03/26/13 9:00
- ,-This report should not be reproduced, except in its entirety, without.the written consent of Prism Laboratories, Inc. -
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 7

I S M Full -Service Analytical &
r I Environmental Solutions
LABORATORIES. INC.
449 Springbrook Road • P.O. Box 240543 • Charlotte, NO 23224-0543
Phone:[phone] Fax:[phone]
Client Company Name: C A v aT 344- - s Lfrr/(e
Report To/Contact Name: /(n 9 tr Sm J-6
Reporting Address: - 3 oy I C I I
S�&4esv llc NC
CHAWN OF CUSTODY RECORD
PAGE _ OF _ QUOTE # TO ENSURE PROPER BOLLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV)
provisions and/or QC Requirements
I mrnicra Tn-
Address:
Phone: 70Y- fT78- 3q3 tf Pax es (No): 7U`l-t571f- YE45 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC
EDD Type: PDF_ Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rushh WorPre-ApprokMustBe
Site Location Name: four`I Cr ak Li?tx5 jP Samples received after 15:00 will be processed next business day.
SC_ OTHER N/A
p
Site Location Physical Address: 6q3 t�� I1 Fu r„ r ��dl , Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO
SEq�eSy.,/�C: MC (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
MATRIX
(SOIL,
WATER OR
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
~ / k i� i REMARKS
PRISM
LAB
'TYPE
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
� � /
ID NO.
�Z
3-d5--`3
/l: ��
S
r'
N�,�Sd03
✓..
--
B;-Weekiv T,,54
1
-
--
,,Ljo•
Sampler's Signature /-v Luc Sampled By (Print NameA coon of L� �C (: Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be -
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin fished By: (signature) - �+ Rec d By: (Signature) Dale ��. Military/Hours
; urs Additional Comments Slte Arrival Tlrne
Reli By; (Signature) R9s ' d By: (Signature) Date Slte Departure Tlmo
/5
linquis :Signature) Recel�r �r Pris L oratories By: Date '.
� ..%�
(p et od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY, COC Group No.
(D SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO Ny1L RECEIVED AT THE LABORATORY,
j �S3vZ
O Fed Ex QUIPSElHand-delivered ;prism Field Service ❑Other
j PDES:' I UST: GR UNDWATER: DRINKING WATER: I SOLID WASTE: RCRA: CERCLA I LANDFILL OTHER: ,
NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC USC ❑NC ❑SC ❑NC ❑SC) ❑NC ❑SCI ❑NC El SCEl
-I—VIV 1 HIIVCIS 1 y TM t,VLJCD: /A = Mir IUCI U = I'ledi to = uldbb r, = ndbuc, I = I ouvn-ui tau v F y4„y­

�F Full -Service Analytical &
.Jr RISM Environmental Solutions
LABORATORIES, ING
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cart No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime (Quarterly Parameters)
Lab Submittal Date: 04/09/2013
Prism Work Order: 3040260
Case Narrative
04/18/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
MC Sample concentration too high for recovery evaluation
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 16

Full -Service Analytical &
I S M Environmental Solutions
R
Sample Receipt Summary
04/18/2013
Prism Work Order: 3040260
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime #1
3040260-01
Solid
04/09/13
04/09/13
Sta-Lime #2
3040260-02
Solid
04/09/13
04/09/13
Sta-Lime #3
3040260-03
Solid
04/09/13
04/09/13
Sta-Lime #4
3040260-04
Solid
04/09/13
04/09/13
Sta-Lime #5
3040260-05
Solid
04/09/13
04/09/13
Sta-Lime #6
3040260-06
Solid
04/09/13
04/09/13
Sta-Lime #7
3040260-07
Solid
04/09/13
04/09/13
Samples received in good condition at 28.3 degrees C unless otherwise noted
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 16

t( Fun -Service Analytical &
OF R I Environmental Solutions
'- �.ONATO—r, INC
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: StaLime (Quarterly
Parameters)
Sample Matrix: Solid
Laboratory Report
04/18/2013
Client Sample ID: Sta-Lime #1
Prism Sample ID: 3040260-01
Prism Work Order: 3040260
Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DatelTime ID
General Chemistry Parameters
Plant Available Nitrogen
560
mg/kg
81
6.9
1
*Calculation 4/17/13 15:15
CDE
[CALCI
Solids
82.2
% by
0.100
0.100
1
*SM2540 G 4/11/13 15:29
LTB
P3D0267
Weight
Nitrate/Nitrite as N
38
mg/kg dry
6.1
0.67
1
*SM4500-NO3 F 4115/13 8:40
CLB
P3D0256
Phosphorus -Total
1800
mg/kg dry
61
8.8
20
*SM4500-P F 4/15/13 10:56
CLB
P3D0296
Total Kjeldahl Nitrogen
2100
mg/kg dry
300
25
1
*351.2 4117/13 15:15
CDE
P31010377
Ammonia as N
36
mg/kg
5.0
0.48
1
*SM4500-NH3 G 4/16/13 10:00
CLB
P3D0306
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E 4/10/13 10:00
MES
P3D0390
Total Metals
Mercury
0.10
mg/kg dry
0.026
0.0086
1
*7471B
4115/13 12:42
LTB
P3D0302
Arsenic
7.0
mglkg dry
0.31
0.071
1
*6010C
4/10/13 16:29
BGM
P3D0234
Cadmium
BRL
mg/kg dry
0.31
0.040
1
*6010C
4/10/13 16:29
BGM
P3D0234
Copper
27
mg/kg dry
0.61
0.12
1
*6010C
4110/13 16:29
BGM
P3D0234
Lead
14
mg/kg dry
. 0.31
0.041
1
*6010C
4110/13 16:29
BGM
P31010234
Nickel
72
mg/kg dry
1.2
0.011
1
*6010C
4/10/13 16:29
BGM
P3D0234
Potassium
4200
mg/kg dry
150
20
10
*6010C
4/11113 23:19
BGM
P3D0234
Selenium
2.1
mg/kg dry
0.61
0.14
1
*6010C
4110/13 16:29
BGM
P3D0234
Sodium
490
mg/kg dry
15
3.9
1
*6010C
4/10113 16:29
BGM
P3D0234
Zinc
66
mg/kg dry
31
4.2
10
*6010C
4111113 23:19
BGM
P3D0234
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 16

Arb
Laboratory 'Report
Full -Service Analytical &
f S Environmental Solutions 04/18/2013
,-�'7 WRATORIE$ING
City of Statesville, NC Project: StaLime (Quarterly Client Sample ID: Sta-Lime #2
Attn: Andy Smith Parameters) Prism Sample ID: 3040260-02
P.O. Box 1111 Prism Work Order: 3040260
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 76.0 % by 0.100 0.100 1 'SM2540 G 4111/13 15:29 LTB P31310267
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 'SM9221 E 4/10/13 10:00 MES P3D0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 16

!� RX'R ISM n Full -service Analytical
'v' Environmental Solutions
:�LABORATORIE$ ING
Laboratory Report
04/18/2013
City of Statesville, NC
Project: StaLime (Quarterly
Client Sample ID: Sta-Lime #3
Attn: Andy Smith
Parameters)
Prism Sample ID: 3040260-03
P.O. Box 1111
Prism Work Order: 3040260
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
% Solids
77.1 % by
0.100
0.100 1 'SM2540 G 4/11/13 15:29 LTB P31)0267
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 'SM9221 E 4/10/13 10:00 MES P3D0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 16

Laboratory Report
A
� C /� Euvill-Service al Solutions
8 04/18/2013
t,J � V � Environmental Solutions
1 E-TORIEb INC.
City of Statesville, NC Project: Stal-ime (Quarterly Client Sample ID: Sta-Lime #4
Attn: Andy Smith Parameters) Prism Sample ID: 3040260-04
P.O. Box 1111 Prism Work Order: 3040260
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter Result, Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 71.8 % by 0.100 0.100 1 'SM2540 G 4/11/13 15:29 LTB P31)0267
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 4/10113 10:00 MES P31)0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 16

AAI:9-�2t!'�J-ORATORIES.
A /A'Full-Service Analytical 8
IS, Y 1Environmental Solutions
ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
04118/2013
Project: StaLime (Quarterly Client Sample ID: Sta-Lime #5
Parameters) Prism Sample ID: 3040260-05
Prism Work Order: 3040260
Sample Matrix: Solid Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 75.2 % by 0.100 0.100 1 'SM2540 G 4111/13 15:29 LTB P3D0267
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 4110/13 10:00 MES P3D0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 Of 16

ff. omi
mFull-Service Analytical &
L,'u�I , Y , Environmental Solutions
-'�'`- �' LaBOPnTORiE$ iNG
Laboratory Report
04/18/2013
City of Statesville, NC
Project: StaLime (Quarterly
Client Sample ID: Sta-Lime #6
Attn: Andy Smith
Parameters)
Prism Sample ID: 3040260-06
P.O. Box 1111
Prism Work Order: 3040260
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter
"Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
74.2 % by
0.100
0.100 1 •SM2540 G 4/11/13 15:29 LTB
P3D0267
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 `SM9221 E 4/10/13 10:00 MES
P3D0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 16

L Full -Service Analytical &
44 I S Environmental Solutions
-�` �' LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Stal-ime (Quarterly
Parameters)
Sample Matrix: Solid
Laboratory Report
04/1812013
Client Sample ID: Sta-Lime #7
Prism Sample ID: 3040260-07
Prism Work Order: 3040260
Time Collected: 04/09/13 11:00
Time Submitted: 04/09/13 14:25
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datelrime
ID
General Chemistry Parameters
Solids 72.7
% by
0.100
0.100 1
'SM2540 G 4/11/13 15:29 LTB
P3D0267
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 4/10/13 10:00 MES
P3D0390
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 16

*' Level II QC Report
Full -Service Analytical &
I S M I Environmental Solutions 4/18/13
�..�,�?}LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3DO234 - 3050B
Project: Stal-ime (Quarterly Parameters) Prism Work Order: 3040260
Time Submitted: 4/9/2013 2:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P3DO234-BLK1_)
_Prepared
& Analyzed: 04/10/13
---------_-_-------
------_-_
Arsenic
BRL
0.24
mg/kg wet
Cadmium
BRL
0.24
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.24
mg/kg wet
Nickel
BRL
0.98
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.49
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.4
mg/kg wet
LCS (P3DO234-BS1)
Prepared & Analyzed: 04/10/13
Arsenic
25.1
0.25
mg/kg wet
25.25 100
80-120
Cadmium
24.7
0.25
mg/kg wet
25.25 98
80-120
Copper
26.1
0.51
mg/kg wet
25.25 103
80-120
Lead
24.5
0.25
mg/kg wet
25.25 97
80-120
Nickel
24.5
1.0
mg/kg wet
25.25 97
80-120
Potassium
498
13
mg/kg wet
505.1 99
80-120
Selenium
24.9
0.51
mg/kg wet
25.25 99
80-120
Sodium
513
13
mg/kg wet
505.1 102
80-120
Zinc
25.0
2.5
mg/kg wet
25.25 99
80-120
Matrix Spike (P3D0234-MS1)
Source: 3040260-01
Prepared & Analyzed: 04/10/13
Arsenic
28.9
0.30
mg/kg dry
29.82 7.01 73
75-125
MI
Cadmium
16.5
0.30
mg/kg dry
29.82 0.215 55
75-125
MI
Copper
47.6
0.60
mg/kg dry
29.82 26.8 70
75-125
MI
Lead
34.0
0.30
mg/kg dry
29.82 14.0 67
75-125
MI
Nickel
95.6
1.2
mg/kg dry
29.82 71.7 80
75-125
Potassium
2.98E10
15
mg/kg dry
596.3 4190 NR
75-125
MC
Selenium
25.0
0.60
mg/kg dry
29.82 2.06 77
75-125
Sodium
1020
15
mg/kg dry
596.3 486 90
75-125
Zinc
103
30
mg/kg dry
29.82 65.7 125
75-125
MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Level II QC Report
F
I Fun -Service Analytical 4I18/13
Environmental Solutions
�w'LABO-ORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
h P3DO234 - 3050B
Project: Stal-ime (Quarterly Parameters) Prism Work Order: 3040260
Time Submitted: 4/9/2013 2:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P3D0234-MSD1)_ _
Source: 3040260-01
Prepared & Analyzed: 04/10/13
Arsenic
29.9
0.31
mglkg dry
30.88
7.01
74
75-125
3
20
MI
Cadmium
17.3
0.31
mg/kg dry
30.88
0.215
55
75-125
5
20
MI
Copper
48.2
0.62
mg/kg dry
30.88
26.8
69
75-125
1
20
MI
Lead
35.5
0.31
mg/kg dry
30.88
14.0 .
70
75-125
4
20
MI
Nickel
97.5
1.2
mg/kg dry
30.88
71.7
84
75-125
2
20
Potassium
3.09E10
15
mg/kg dry
617.5
4190
NR
75-125
3
20
MC
Selenium
26.2
0.62
mg/kg dry
30.88
2.06
78
75-125
5
20
Sodium
1080
15
mg/kg dry
617.5
486
96
75-125
5
20
Zinc
103
31
mglkg dry
30.88
65.7
121
75-125
0.04
20
MI
Post Spike (P3D0234-PS1)
Source: 3040260-01
Prepared
& Analyzed: 04/10/13
Arsenic
1.01
mg/L
1.000
0.228
79
80-120
MI
Cadmium
0.534
mg/L
1.000
0.00701
53
80-120
MI
Copper
1.64
mg/L
1.000
0.871
77
80-120
MI
Lead
0.993
mg/L
1.000
0.456
54
80-120
MI
Nickel
2.84
mg/L
1.000
2.33
50
80-120
MI
Potassium
1.00E9
mg/L
20.00
136
NR
80-120
MC
Selenium
0.883
mg/L
1.000
0.0670
82
80-120
Sodium
32.6
mg/L
20.00
15.8
84
80-120
Zinc
2.32
mg/L
1.000
2.14
19
80-120
MI
Batch P3DO302 - 7471
Blank (P3D0302-BLK1) Prepared & Analyzed: 04/15/13
Mercury BRL 0.020 mg/kg wet
LCS (P3D0302-B_S1) Prepared & Analyzed: 04/15/13
Mercury 0.441 0.020 mglkg wet 0.4098 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Level II QC Report
r Full -Service Anal tical &
A,adt:_O�r 4/18/13 "
'R I Environmental Solutions
i^ LAOORATORIES. INa
City of Statesville, NC Project: Stal-ime (Quarterly Parameters) Prism Work Order: 3040260
Attn: Andy Smith Time Submitted: 4/9/2013 2:25:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3DO256 - NO PREP
Blank_(P3D0256-BLK1)
Prepared: 04/11/13 Analyzed: 04/15/13 _
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
LCS (P3D0256-BS1)
Prepared: 04/11/13 Analyzed: 04/15/13 _
Nitrate/Nitrite as N
49.9 5.0 mg/kg wet
50.00 100 80-120
Matrix Spike (P3D0256-MS1)
Source: 3040260-01
Prepared: 04/11/13 Analyzed: 04/15/13 _
Nitrate/Nitrite as N
88.7 6.1 mg/kg dry
60.83 38.0 83 80-120
Matrix Spike Dup (P3D0256-MSD1)
Source: 3040260-01
Prepared: 04/11/13 Analyzed: 04/15/13
Nitrate/Nitrite as N
88.9 6.1 mg/kg dry
60.83 38.0 84 80-120 0.3 20
Batch P3DO267 - Default Pren Metals
Blank (P3D0267-BLKI) Prepared & Analyzed: 04/11/13
% Solids 99.9 0.100 % by Weight
Duplicate (P3D0267-DUP3) Source: 3040260-07 Prepared & Analyzed: 04/11/13
% Solids 76.7 0.100 % by Weight 72.7 5 20
Batch P3DO296 - SM4500-PB5
Blank (P3D0296-BLK1) Prepared: 04/12/13 Analyzed: 04/15/13
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P3D0296-13SI) Prepared: 04/12/13 Analyzed: 04/15/13
Phosphorus -Total 102 2.5 mg/kg wet 100.0 102 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 0f 16

Full -Service Analytical &
1 S M I Environmental Solutions
LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P3DO296 - SM4500-PB5
Project: StaLime (Quarterly Parameters)
Level II QC Report
4/18/13
Prism Work Order: 3040260
Time Submitted: 4/9/2013 2:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike (P3DO296-MS1) Source: 30_4_0260_-01 Prepared: 04/12/13 Analyzed: 04/15/13
Phosphorus -Total 2060 61 mg/kg dry 121.7 1830 186 80-120 MC
Matrix Spike Dup (P3D0296-MSD1) Source: 3040260-01 Prepared: 04/12/13 Analyzed: 04/15/13
Phosphorus -Total 2070 61 mg/kg dry 121.7 1830 197 80-120 0.6 20 MC
Batch P3DO306 - NO PREP
Blank (P3D0306-BLK1) Prepared: 04/15/13 Analyzed: 04/16/13
Ammonia as N BRL 5.0 mg/kg
LCS (P3D0306-BSI) Prepared: 04/15/13 Analyzed: 04/16/13
Ammonia as N 122 5.0 mg/kg 125.0 98 80-120
Matrix Spike (P3D0306-MS1) Source: 3040260-01 Prepared: 04/15/13 Analyzed: 04/16/13
Ammonia as N 146 5.0 mg/kg 125.0 36.2 88 80-120
Matrix Spike Dup (P3D0306-MSD1) Source: 3040260-01 Prepared: 04/15/13 Analyzed: 04/16/13
Ammonia as N 150 5.0 mg/kg 125.0 36.2 91 80-120 3 20
Batch P3DO377 - 351.2
Blank (1133D0377-BLKI) Prepared: 04/12/13 Analyzed: 04/17/13
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P3D0377-BS1) Prepared: 04/12/13 Analyzed: 04/17/13
Total Kjeldahl Nitrogen 133 25 mg/kg wet 125.0 107 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 16

&�vP^�,�{ Full -Service Analytical &
�R I S M I Environmental Solutions
LARo-ORIES ING
Level II QC Report
4118113
City of Statesville, NC Project: Stal-ime (Quarterly Parameters) Prism Work Order: 3040260
Attn: Andy Smith Time Submitted: 4/9/2013 2:25:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3DO377 - 351.2
Matrix Spike (P3D0377-MS1) Source., 3040260-01 Prepared: 04/12/13 Analyzed: 04/17/13
Total Kjeldahl Nitrogen 9130 3000 mg/kg dry 6083 2100 116 90-110 MI
Matrix Spike Dup (P3DO377-MSD1) - Source: 3040260-01 Prepared: 04/12/13 Analyzed: 04/17/13
Total Kjeldahl Nitrogen 8560 3000 mg/kg dry 6083 2100 106 90-110 6 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 14 of 16

A��
,Level II QC ReportFull-Service Analytical & 4/18/13
IEnvironmental Solutions
LABORATOFIES INa
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 3040260
Attn: Andy Smith Time Submitted: 4/9/2013 2:25:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3DO390 - NO PREP
Blank (P3130390-BLK1)
Prepared & Analyzed: 04/10/13
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch
Initial
Final Date/Time
3040260-01 P31710377
0.05 g
25 mL 04/12/13 10:30
Prep Method: Default Prep Metals
Lab Number Batch
Initial
Final Daterrime
3040260-01
P3D0267
30 g
30
mL
04/11/13 15:29
3040260-02
P3D0267
30 g
30
mL
04/11/13 15:29
3040260-03
P3D0267
30 g
30
mL
04/11/13 15:29
3040260-04
P3D0267
30 g
30
mL
04/11/13 15:29
3040260-05
P31D0267
30 g
30
mL
04/11/13 15:29
3040260-06
P3D0267
30 g
30
mL
04/11/13 15:29
3040260-07
P3D0267
30 g
30
mL
04/11/13 15:29
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Date/rime
3040260-01
P3D0296
1 g
50
mL
04/12/13 12:38
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
3040260-01 P3D0234 1.98 g 50 mL 04/10/13 8:00
3040260-01 P3D0234 1.98 g 50 mL 04/10/13 8:00
Prep Method: 7471B
Lab Number Batch Initial Final Date/rime
3040260-01 P3D0302 0.57 g 50 mL 04/15/13 9:05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Full -Service Analytical & AI OF CUSTODY RECORD
S M {I I Environmental Solutions PACE _ OF _ QUOTE # TO iQU7,C,7
sER BALLING:
N " LP.eOFIA70RIEG, INC. 16, I 1 I-' r O449 Springbrook Road- P.O. Box 240543 • Charlotte, NC 28224.0543Project Name: W/�� t�I V
Phone: [phone] • Fax: [phone] gg Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: J 4Jy- *Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
�+ provisions and/or QC Requirements
Reporting Address:
Report To/Contact Name: � r�t=� ��'�.� 17
D O /tit
Invoice To:
®1 "V c Address:
Phone: 7�1 1' ?79- 3v'es .38 Fax (No):7.11- $ �'y- a 6Y5 purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes).(No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL NC
EDD Type: PDF— Excel p—Other 'Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re h Work Must Be pproved
' `► �r 1� bjt'`11TP
SC OTHER
—
N/A
c J Cc
Site Location Name: i Samples
received after 15:00 will be processed next business day.
if F. + rrP Turnaround time is based on business days, excluding weekends and holidays.
Site Location Physical Address: '139
Water Chlorinated: YES _ NO —
/
•`r
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES
NO -
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSES REQUESTED
, /
j / �a ��/. �i/
PRISM
LAB
MILITARY
WATER OR
TIVES
j
�/ �d`� �f/ REMARKS
'TYPE
SAMPLE DESCRIPTION
COLLECTED
NO.
SIZE
s
/�j 1�
ID NO.
HOURS
SLUDGE)
SEE BELOW
4�e
ez.
F15
d `
Sol
c�
Sampler's Signature �I �• ` � Sampled By (Print Name) ', ,4 r'"`� e 1 Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism taproceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be char foj any changW after analyses have been initialized.
o
Reli q 'shed By: (Signal ) e/ n r Rec
B re Date Military/Hours Additional Comments:
y: )
Site Arrival TimZZ
Slte Departure Tinte
Relin (shed By: (Signature) ecelve y: ( Ignature to
f ielcl;lech Fee,
� ishe �y: (Signal � Y�
Received For Pris Labor for Dal L ��
(D of Shlpmen ✓NOTE: ALL pAMP •CO 1RS SHOULD BE TAPED SHUT WIT C ODY FOR TRANSPORTATION TO THE LABORATORY. CO,Group No.
__��' SAMPLES RE TAG ED AND VERIFIED AGAINST COC UNTIL D AT THE LABORATORY. �
O7 70 V C,
O_ Ex ❑UPS ❑ Hand-dellver Prism Field Service ❑ Other
f
1 $: UST: GR NDWATER: DRINKING WATER: SOLID WASTE: RCRA: I CERCLA LANDFILL OTHER:
,
rn ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC
❑ NC ❑ SC ❑ NC ❑ SC` ❑ NC ❑ SC I ❑ NC ❑ SC I ❑ NC ❑ SC
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass H = Mastic; I L = I erlon-Linea uap V VH = vUlawe vlyal uca ry iaiyaw tLUl V I— H­,

S M
+.r�LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 04/22/2013
Prism Work Order: 3040566
Case Narrative
04/30/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) t�_ A—.
(0_rV__
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
7z:::: �' �_ 19, - - (_� �
Reviewed By Robbi A. Jones
President/Project Manager
Mi Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
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Sample Receipt Summary
is fi Full -Service Analytical &
RISM I Environmental Solutions 04/30/2013
-''-� - LABORATORIES I.C.
Prism Work Order: 3040566
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3040566-01 Solid 04/22/13 04/22/13
Samples received in good condition at 9.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Laboratory Report
�+P�F"• � Full Service Analytical &
R I S Environmental Solutions
04/30/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3040566-01
P.O. Box 1111
Prism Work Order: 3040566
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 04/22/13 13:20
Time Submitted: 04/22/13 14:25
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date(Time
ID
General Chemistry Parameters
Solids
69.5
% by
0.100
0.100
1 •SM2540 G 4/24113 13:30
ANG
P3D0502
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1 'SM9221 E 4/23/13 12:51
MES
P3D0534
mL
Total Metals
Mercury
0.16
mg/kg dry
0.028
0.0096
1 '7471B 4124/13 13:47
MEH
P3D0507
Arsenic
15
mg/kg dry
3.6
0.83
10 '6010C 4124/13 18:14
BGM
P3D0508
Cadmium
BRL
mg/kg dry
3.6
0.47
10 '6010C 4/24/13 18:14
BGM
P3D0508
Copper
25
mg/kg dry
7.3
1.4
10 '6010C 4/24/13 18:14
BGM
P3D0508
Lead
140
mg/kg dry
3.6
0.49
10 '6010C 4124/13 18:14
BGM
P3100508
Nickel
130
mg/kg dry
15
0.13
10 '6010C 4124113 18:14
BGM
P31)0508
Selenium
BRL
mg/kg dry
7.3
1.7
10 '6010C 4/24/13 18:14
BGM
P3D0508
Zinc
64
mg/kg dry
36
4.9
10 `6010C 4124113 18:14
BGM
P31210508
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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/or
r RFull-Service Analytical &
bnk' .;► IEnvironmental Solutions
-f`� * LABORATORIES I NG
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
4%30/13
Prism Work Order: 3040566
Time Submitted: 4/22/2013 2:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P3D0507 - 7471 B
Blank (P3130507-13_LK1)
_Prepared: 04/23/13 Analyzed: 04/24/13
Mercury
BRL 0.020 mg/kg wet
LCS (P3DO507-BS1)
Prepared: 04/23/13 Analyzed: 04/24/13
Mercury
0.423 0.020 mg/kg wet
0.4098 103 80-120
Matrix Spike (P3DO507-MS1)
Source: 3040566-01
Prepared: 04/23/13 Analyzed: 04/24/13
Mercury
0.858 0.031 mg/kg dry
0.6540 0.156 107 80-120
Matrix Spike Dup (P3D0507-MSD1)
Source: 3040566-01
Prepared: 04/23/13 Analyzed: 04/24/13 _
Mercury
0.892 0.030 mglkg dry
0.6202 0.156 119 80-120 4 20
Batch P3D0508 - 3050B
Blank (P3DO508-BLK1)
Prepared & Analyzed: 04/24/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (123130508-BS1)
Prepared & Analyzed: 04/24/13
Arsenic
22.7
0.25
mg/kg wet
25.25 90
80-120
Cadmium
22.7
0.25
mg/kg wet
25.25 90
80-120
Copper
24.5
0.51
mg/kg wet
25.25 97
80-120
Lead
22.8
0.25
mglkg wet
25.25 90
80-120
Nickel
22.6
1.0
mg/kg wet
25.25 90
80-120
Selenium
22.6
0.51
mg/kg wet
25.25 90
80-120
Zinc
22.7
2.5
mg/kg wet
25.25 90
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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A��J
C's Full -Service Analytical &
P R I S Environmental Solutions
'M' LABORATORIES INa
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3130508 - 3050B
Project: Stal-ime
Reporting
Result Limit Units
Level II QC Report
4/30/13
Prism Work Order: 3040566
Time Submitted: 4/22/2013 2:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P3D0508-MS1)
Source: 3040566-01
Prepared & Analyzed: 04/24/13
Arsenic
48.3
3.6
mg/kg dry
36.15 14.6 93
75-125
Cadmium
28.6
3.6
mg/kg dry
36.15 BRL 79
75-125
Copper
59.4
7.2
mg/kg dry
36.15 24.7 96
75-125
Lead
178
3.6
mg/kg dry
36.15 140 104
75-125
Nickel
170
14
mg/kg dry
36.15 133 103
75-125
Selenium
Complete
7.2
mg/kg dry
36.15 BRL 69
75-125
Zinc
99.4
36
mg/kg dry
36.15 64.0 98
75-125
Matrix Spike Dup (P3D0508-MSD1)
Source: 3040566-01
Prepared & Analyzed: 04/24/13
Arsenic
46.4
3.5
mg/kg dry
35.09 14.6 91
75-125
4
20
Cadmium
28.1
3.5
mg/kg dry
35.09 BRL 80
75-125
2
20
Copper
57.9
7.0
mg/kg dry
35.09 24.7 95
75-125
3
20
Lead
174
3.5
mg/kg dry
35.09 140 96
75-125
2
20
Nickel
166
14
mg/kg dry
35.09 133 95
75-125
2
20
Selenium
25.8
7.0
mg/kg dry
35.09 BRL 73
75-125
3
20 MI
Zinc
97.2
35
mg/kg dry
35.09 64.0 95
75-125
2
20
Post Spike (P3D0508-PS1)
Source: 3040566-01
Prepared & Analyzed: 04/24/13
Arsenic
1.28
mg/L
1.000 0.401 88
80-120
Cadmium
0.767
mg/L
1.000-0.0266 79
80-120
MI
Copper
1.51
mg/L
1.000 0.679 83
80-120
Lead
4.49
mg/L
1.000 3.85 64
80-120
MI
Nickel
4.27
mg/L
1.000 3.65 62
80-120
MI
Selenium
0.702
mg/L
1.000 -0.133 84
80-120
Zinc
2.53
mg/L
1.000 1.76 77
80-120
MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 8

Full Service Analytical &
j R I S Environmental Solutions
'•' LABORATOFIEa ING
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
4/30/13
Prism Work Order: 3040566
Time Submitted: 4/22/2013 2:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3DO502 - NO PREP
Blank (P3DO502-BLK1) Prepared: 04/23/13 Analyzed: 04/24/13
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 8

r.•
Full -Service Analytical &
' 51 I S M I Environmental Solutions
LABOfl TORIE51N0
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
4/30/13
Prism Work Order: 3040566
Time Submitted: 4/22/2013 2:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3130534 - NO PREP
Blank (P3DO534-BLK1) _ Prepared & Analyzed: 04/23/13
Fecal Coliforms BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial Final Daterrime
3040566-01
P3D0508
1.98 g 50 mL 04/24/13 9:00
Prep Method: 7471B
Lab Number
Batch
Initial Final Daternme
3040566-01
P31)0507
0.61 g 50 mL 04/23/13 14:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 8

C'NAIN OF CUSTODY RECORD
PRISM(,I
Full -Service Analytical &
1 Environmental Solutions
PAGE _ OF QUOTE # TO ENSURE PROPER BOLLING:
LABORATORIES. mc.
440 Springbrook Road ^ P.O. Box 240543 • Charlotte, NC 28224-0543
Project Name:
Phone: [phone] Fax: [phone]
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Name: C111V a 1P S( -e_5y
"Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Client Company
An�v J�:s9,�i�a
provisions and/or QC Requirements
Report To/Contact Name:
Invoice To:
Reporting Address: R d B0-Y d d r II
Valesyi l% 14G
Address:
1,fta-8%.4--40-4$ 7,)4-_F7e
Phone: Fax kLew (No):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE
FL
NC
EDD Type: PDF_ Excel _Other ,
Site Location Name: 6aa r 1� i Cee� W'CO IP
"Working Days" ❑ 6.9 Days ❑ Standard 10 days ❑ P esh pork Mdust Be
SC OTHER
N/A
Site Location Physical Address:493 &JI KOLO ri
3,� .
Samples received after 15:00 will be processed next business day,
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES _ NO _
S f�• a8 tl'�se I1� ;, C
3 I o
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES
p p
C
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
-NO
CLIENT
DATE
TIME
COLLECTED
MATRIX.
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSES REQUESTED
��LAB
PRISM
"TYPE
/01
/ REMARKS
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
NO.
SIZE
TIVES
/
Vk-� / j
ID NO.
HOURS
SLUDGE)
SEE BELOW
, ki
e
S4A4 MC-13
13'
S
NaAs4J.3
Sampler's Signature /r"at{ �t �f''Z Sampled By (Print Name) ��
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed
submitted in writing to the Prism Project Manager. There will be charges for aw cis
Rell ed By: (Sign re)�/� Receive p v sl�rfat�r�,F
0 ..
/ C I Affiliation
analyses as requested above. Any changes must be
al, analyses have been initialized.
Date Military/Hours Additional Comments:
In Ratur, _ /' ived Fqr Prism Laboratories By: I Date
r -- 13 �
1. Field tech -Fe
Mileage
fD
(C hod of hipme t: NOTE: L SAMPLE COOLERS SHOULD BE TAPED SHUT WIT CUS D SEAL -O RANSPORTATION TO THE LABORATORY. f OC G up No.
(D SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO UNTIL RECEIVED THE LABORATORY. . 3 4 q
00 ad Ex ElUPS ❑ Hand -delivered ❑ Prism Field Service ❑ Other
O - ^
DES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL I OTHER: ,
C ❑ SCI ❑O NC ❑ SC ❑❑ NC ❑ SC p0 NC p SC p❑ NC ❑ SC ❑p NC ❑ SC pp NC ❑ SC ❑p NC ❑ SC 1 pp NC ❑ SC i dF=;f:S`:`:i1'.i
"CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

r.
`ISM
LABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 05/06/2013
Prism Work Order: 3050111
Case Narrative
05/14/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
t�_ A_.
?rv--
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 8

`� Sample Receipt Summary
�r" Full -Service Analytical &
■L' i� I S environmental Solutions 05/14/2013
��^-�m "LABORATORIES ING
Prism Work Order: 3050111
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3050111-01 Solid 05/06/13 05/06/13
Samples received in good condition at 7.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 8

Laboratory Report
d C I Full -Service Analytical &
�;P R Environmental Solutions 05/14/2013
-GORATOFIE61Na
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3050111-01
P.O. Box 1111 Prism Work Order: 3050111
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/06/13 14:05
Time Submitted: 05/06/13 15:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
69.6
% by
0.100
0.100
1
*SM2540 G
517/13 12:45
ANG
P3E0118
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
517/13 10:04
MES
P3E0140
Total Metals
Mercury
0.12
mg/kg dry
0.030
0.010
1
*7471B
5/9/13 14:03
MEH
P3E0163
Arsenic
5.6
mg/kg dry
0.37
0.084
1
*6010C
5/10/13 0:20
BGM
P3E0135
Cadmium
BRL
mg/kg dry
0.37
0.048
1
*6010C
5/10/13 0:20
BGM
P3E0135
Copper
27
mg/kg dry
0.73
0.14
1
*6010C
5/10/13 0:20
BGM
P3E0135
Lead
15
mg/kg dry
0.36
0.049
1
*6010C
5/11113 4:46
BGM
P3E0177
Nickel
98
mg/kg dry
1.5
0.013
1
*6010C
5/10/13 0:20
BGM
133E0135
Selenium
2.6
mg/kg dry
0.73
0.17
1
*6010C
5/10113 0:20
BGM
P3E0135
Zinc
61
mg/kg dry
37
5.0
10
*6010C
5/10/13 0:11
BGM
P3E0135
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 8

f" Full -Service Analytical &
Environmental Solutions
�- "r y��'LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3EO135 - 3050B
Project: StaLime
Level II QC Report
5/14/13
Prism Work Order: 3050111
Time Submitted: 5/6/2013 3:05:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P3E0135-BLK1)
_ _
Prepared: 05/08/13 Analyzed: 05/09/13
Arsenic
BRL
0.25
mglkg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.50
mglkg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3E0135-BS1)
Prepared: 05/08/13 Analyzed: 05/09/13
Arsenic
24.1
0,25
mg/kg wet
25.13 96 80-120
Cadmium
23.2
0.25
mg/kg wet
25.13 92 80-120
Copper
25.1
0.50
mg/kg wet
25.13 100 80-120
Nickel
23.5
1.0
mg/kg wet
25.13 94 80-120
Selenium
23.8
0.50
mg/kg wet
25.13 95 80-120
Zinc
23.9
2.5
mg/kg wet
25.13 95 80-120
Batch P3EO163 - 7471 B
Blank (P3EO163-BLK1) Prepared & Analyzed: 05/09/13
Mercury BRL 0.018 mg/kg wet
LCS (P3EO163-BS1) Prepared & Analyzed: 05/09/13
Mercury 0.476 0.019 mg/kg wet 0.4032 118 80-120
Batch P3EO177 - 3050B
Blank (P3E0177-BLK1) Prepared: 05/10/13 Analyzed: 05/11/13
Arsenic
BRL
0.26
mg/kg wet
Cadmium
BRL
0.26
mg/kg wet
Copper
BRL
0.51
mglkg wet
Lead
BRL
0.26
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.6
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 8

r+
E^ 1 Full -Service Analytical &
1R I S Environmental Solutions
vT'�'l�LABO TORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3EO177 - 3050B
Project: StaLime
Level II QC Report
5/14/13
Prism Work Order: 3050111
Time Submitted: 5/6/2013 3:05:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P3E0177-BS1)
Prepared: 05/10/13 Analyzed: 05/11/13
Arsenic
22.5
0.25
mg/kg wet
25.13 90 80-120
Cadmium
22.0
0.25
mg/kg wet
25.13 88 80-120
Copper
24.5
0.50
mg/kg wet
25.13 97 80-120
Lead
22.0
0.25
mg/kg wet
25.13 87 80-120
Nickel
22.6
1.0
mg/kg wet
25.13 90 80-120
Selenium
22.2
0.50
mg/kg wet
25.13 89 80-120
Zinc
22.5
2.5
mg/kg wet
25.13 89 80-120
Post Spike (P3EO177-PS1)
Source: 3050111-01
Prepared: 05/10/13 Analyzed: 05/11/13
Arsenic
0.893
mg/L
1.000 0.155 74 80-120 MI
Cadmium
0.486
mg/L
1.000 0.00728 48 80-120 MI
Copper
1.44
mg/L
1.000 0.748 69 80-120 MI
Lead
0.899
mg/L
1.000 0.412 49 80-120 MI
Nickel
3.09
mg/L
1.000 2.68 41 80-120 MI
Selenium
0.628
mg/L
1.000 0.0713 56 80-120 MI
Zinc
2.56
mg/L
1.000 1.67 89 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 8

A
Full-Service Analytical &
� I S Environmental Solutions
:- LABORATORIES ING
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
5114/13
Prism Work Order: 3050111
Time Submitted: 5/6/2013 3:05:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3EO118 - NO PREP
Blank (PM0118-BLK1) _ Prepared & Analyzed: 05/07/13
--- --------------- -- -
°% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 8

lr, Level II QC Report
eZ PcA
i^. q Full -Service Analytical & 5/14/13
R I S Environmental Solutions
T LABORATORIES ING
City of Statesville, NC Project: StaLime Prism Work Order: 3050111
Attn: Andy Smith Time Submitted: 5/6/2013 3:05:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3EO140 - NO PREP
Blank (P3E0140-BLK1) Prepared & Analyzed: 05/07/13
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Date/Time
3050111-01
P3E0177
1.97 g
50 mL
05/10/13 8:25
3050111-01
P3E0135
1.96 g
50 mL
05/08/13 9:D0
3050111-01
P3E0135
1.96 g
50 mL
05/08/13 9:00
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
3050111-01 P3E0163 0.57 g 50 mL 05/09/13 9:05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 '
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 8

t. CMAIN OF CUSTODY RECORD
Full -Service Analytical &
ti Environmental Solutions PACE _ OF
QUOTEif TO ENSURE PROBER B�LLIN29:
✓ "_i .;r. "LA6ORATORIES, INC.
Pro
449 Spr ngbrook Road ^ P.O. Box 240543 > Charlotte, NC 28224-0543
ect Name.
Phone: [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) LIST Project: (Yes) (No)
�+ ` ; � *Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
Client Company Name:
provisions and/or QC Requirements
Report To/Contact Name: An��°py" ° �'�
- Invoice To:
Reporting Address: I�i�X it d I Address:
ITAINERS`used 7
Phone: Wit" Vf- 3439 Fax es (No):`�°3` -871" Si �� purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC
EDD Type: PDF— Excel —Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ p Rush Work Must Be
Pre -Approved SC OTHER N/A
Site Location Name: f 0" "Th c' eek 63&.�'rp Samples received after 15:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO
Site Location Physical Address: 49�vd) F�`^^ ° _
�e (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES — NO
J _
zxic l,,,' Il RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX ANALYSES REQUESTED PRISM
SAMPLE CONTAINER
CLIENT DATE COLLECTED (SOIL, PRESERUA- /�% / LAB
i d / / REMARKS
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES c/ � / / ID NO.
HOURS SLUDGE) SEE BELOW
9
0
Sampler's Signature G• Sampled By (Print Name) t { ✓ d Affiliation
Upon relinquishing, this Chain Or ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager There will be charges fc, n han_gess a7ftersanaalyses have been initialized Date I munai
'O
N
L] od of Shipm -NUrE: ALL MYLC vL,Lc �� �• •- • • - -
(D SAMPLE ENO ACCE ED AND VERIFIED AGAINST COC UNTIL CENED AT THE LABORATORY.
00
J�9c1
O ed Ex ❑ UPS ❑ Hand-dellvered Prism Field Service ❑ other
OLID
oc) IDES: C ❑ SO UST: ulluvif ❑ NC ❑ SC ❑ NC ❑ SCTER: DRINKING NC❑ SCATER: SO NC ❑SCE- ❑❑ NC ❑ SCi ❑❑ NC L❑ SC I - NC
NC LANDFILL❑ SC I ❑❑ NC ❑ SC
❑ —. — ❑ _. I ❑ ❑ - Lined Ca VOA Volatile Organics Analysis (Zero Head Space)
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL - Teflon p
Comments:

r=
S M
LABORATORIES, INO.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical R
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 05/20/2013
Prism Work Order: 3050538
Case Narrative
05/29/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) �_ A—.
?-rl-
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
D RPD value outside of the control limits.
DH Dilution for this sample/analyte was analyzed outside method recommended hold time.
DM Sample diluted due to the matrix.
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 8

Sample Receipt Summary
FE R I S fl n Fun -Service Analytical s 05/29/2013 Y ' �/' Environmental Solutions
�.' LABORATORIES ING
Prism Work Order: 3050538
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3050538-01 Solid 05/20/13 05/20/13
Samples received in good condition at 22.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 8

Laboratory Report
Full -Service Analytical &
t 7 f M Environmental Solutions 05/29/2013
li�aa1.."' �..�' �LABORATORIE$ ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3050538-01
P.O. Box 1111 Prism Work Order: 3050538
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/20/13 09:20
Time Submitted: 05/20/13 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids
81.1
% by
0.100
0.100
1
*SM2540 G
5/22113 14:32
CGP
P3E0445
Weight
Microbiological Parameters
Fecal Coliforms
BRLDH
MPN/g dry
0.2
1
*SM9221 E
5/21/13 13:05
MES
P3E0540
Total Metals
Mercury
0.27
mg/kg dry
0.023
0.0078
1
*74716
5/21/13 16:51
MEH
P3E0429
Arsenic
8.8 DM
mg/kg dry
3.0
0.70
10
*6010C
5/23/13 2:25
BGM
133E0425
Cadmium
BRLDM
mg/kg dry
3.0
0.40
10
*6010C
5/23/13 2:25
BGM
P3E0425
Copper
32 DM
mg/kg dry
6.1
1.2
10
*6010C
5/23/13 2:25
BGM
P3E0425
Lead
19 DM
mg/kg dry
3.0
0.41
10
*6010C
5/23/13 2:25
BGM
P3E0425
Nickel
160 DM
mg/kg dry
12
0.11
10
*6010C
5/23/13 2:25
BGM
P3E0425
Selenium
BRL
mg/kg dry
6.1
1.4
10
*6010C
5/23/13 2:25
BGM
P3E0425
Zinc
51 DM
mg/kg dry
30
4.1
10
*6010C
5123/13 2:25
BGM
133E0425
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 8

r.: Level II QC Report
C" Full -Service Analytical & 5/29/13
I S 1 Environmental Solutions
L" LA—TORIES, INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Reporting
Analyte Result Limit Units
Batch P3EO425 - 3050B
Prism Work Order: 3050538
Time Submitted: 5/20/2013 2:15:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P3EO425-BLK1)
Prepared: 05/21/13 Analyzed: 05/22/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
. BRL
2.5
mg/kg wet
LCS (P3EO425-BS1)
Prepared: 05/21/13 Analyzed: 05/22/13
Arsenic
23.6
0.25
mg/kg wet
25.25 94 80-120
Cadmium
23.3
0.25
mg/kg wet
25.25 92 80-120
Copper
26.0
0.51
mg/kg wet
25.25 103 80-120
Lead
23.0
0.25
mg/kg wet
25.25 91 80-120
Nickel
23.6
1.0
mg/kg wet
25.25 94 80-120
Selenium
22.4
0.51
mg/kg wet
25.25 89 80-120
Zinc
23.0
2.5
mg/kg wet
25.25 91 80-120'
Batch P3EO429 - 7471 B
Blank (P3E0429-BLK1) Prepared: 05/20/13 Analyzed: 05/21/13
Mercury BRL 0.020 mg/kg wet
LCS (P3E0429-BS1) Prepared: 05/20/13 Analyzed: 05/21/13
Mercury 0.418 0.019 mg/kg wet 0.4032 104 80-120
Matrix Spike (P3E0429-MS1) Source: 3050538-01 Prepared: 05/20/13 Analyzed: 05/21/13
Mercury 0.639 0.027 mg/kg dry 0.5605 0.268 66 80-120 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 8

A i Full -Service Analytical 8
�1R ISM Environmental Solutions
'rLA80RATORIES ING _
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
5/29/13
Prism Work Order: 3050538
Time Submitted: 5/20/2013 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3EO429 - 7471 B
Matrix Spike Dup (P3E0429-MSD1) Source: 3050538-01 Prepared: 05/20/13 Analyzed: 05/21/13
Mercury 0.937 0.026 mg/kg dry 0.5505 0.268 122 80-120 38 20 D. M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 777-1
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 8

A
- -
/-1E Full -Service Analytical &
®PA i s Environmental Solutions
�v LABORATOFIES ING
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
5/29/13
Prism Work Order: 3050538
Time Submitted: 5/20/2013 2:15:OOPM
Reporting Spike Source °/REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3EO445 - Default Prep
Blank (P3EO445-BLK1)
% Solids
_ Prepared:05/21/13 Analyzed:05/22/13
100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 8

r' Full -Service Analytical &
/O,R I S Environmental Solutions
LABORATORIES INO
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
5129/13
Prism Work Order: 3050538
Time Submitted: 5/20/2013 2:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3EO540 - NO PREP
Blank (P3E0540-B_LK1_)
Prepared & Analyzed: 05/21/13
Fecal Coliforms
BRL
0.2 MPN/g wet
_
Sample Extraction Data
Prep Method: Default Prep Metals
Lab Number Batch
Initial
Final
Daterrime
3050538-01 P3E0445
30 g
30 mL
05/21/13 16:13
Prep Method: 3050B
Lab Number Batch
Initial
Final
Daterrime
3050538-01 P3E0425
2.03 g
50 mL
05/21/13 8:50
Prep Method: 7471B
Lab Number Batch
Initial
Final
Daterrime
3050538-01 P3E0429
0.64 g
50 mL
05/20/13 17:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
M 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 8

CHAIN OF CUSTODY RECORD
S M Full -Service Analytical R
Environmental Solutions PAGE _ OF _ QUOTE A TO ENSURE PROPER BILLING;
.. .. .+._. ...., ._,..nORATORIES, INC.
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224.0543 Project Name:
Phone: [phone] Fax: [phone] // Short Bold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: E-,r4'u J 9 14-e ""lit= *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Report To/Contact Name: rl S era r`i �I provisions and/or QC Requirements
Invoice To:
Reporting Address: P.O ox 0aIj Address:
S-64esS, 0)a I�iC
4 a
Phone:'U7- �/S'- 34-51 Fax es (No):12 (- D 7 N'0620 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL
NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re h Work dust Be.
Name: F r4h C d e bL':r T'P be business day.
SC OTHER N/A
Site Location -k Samples received after 15:00 will processed next
Location Physical Address: 9 93'Bell Far15 ^ Turnaround time is based on business days, excluding weekends and holidays.
Farm
Water Chlorinated: YES_ NO
Site
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
lg p
C'J I'✓�/� I'r
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
� O /
ANALYSES REQUESTED
/ ,C
PRISM
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
*TYPE
NO.
SIZE
TIVES
,
// ,i REMARKS
ID NO.
HOURS
SLUDGE)
SEE BELOW
FWA
Sampler's Signature �= e
Upon relinquishing, this Chain o Cus
submitted in writing to the Prism Proj
Reliulshed By: (S gnat e) /
�I �tl/� Cl2ZC
S I P
Sampled By (Print Name)
Is your authorization for Prism to proc
7anacler. There will be-qharges for any
9
J4r I i'_. Affiliation
the analyses as requested above. Any changes must be
after analyses have been initialized.
By:
Date
5 `Lc •t7 1 1E/r
(D SAMPLES ARE NOTIA, EPTED AND VERIFIED AGAINST COC U(�VIIL RECEIVED AT THEKABORATORY.
OD ] i y j L,
O adEx O UPS O Hand -delivered ' ,rism Field Service ❑ Other
cc DES: UST: GRQU DWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:.
C ❑ SC' ❑ NC ❑ SC ❑ iVC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC El NC ❑ SC ❑ NC ❑ SC . ❑ NC ❑ SC ❑ NC ❑ SC
❑— ❑ ❑ .. ❑ ... ❑ ❑ ❑. ❑ -
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
Site ArrvaLTnie :-
Situ.; De _ arture T)me::
p
Fleld Tecl F.ee
Mileage.:
0.J �SEE�REYERSESFOR't
tTiERMSG&gCONDIT,IONS�„,

Pcf.',, ISM
LABORATORIES, INa
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 06/03/2013
Prism Work Order: 3060010
Case Narrative
06/10/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
_ 449 Springbiook Road P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 13

Apdd&vmffn�L
Full-Service Analytical 8
R I M I Environmental Solutions
GO URIM ING ,
Sample Receipt Summary
06/10/2013
Prism Work Order: 3060010
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Sta-Lime #1
3060010-01
Solid
06/03/13
06/03/13
Sta-Lime #2
3060010-02
Solid
06/03/13
06/03/13
Sta-Lime #3
3060010-03
Solid
06/03/13
06/03/13
Sta-Lime #4
3060010-04
Solid
06/03/13
06/03/13
Sta-Lime #5
3060010-05
Solid
06/03/13
06/03/13
Sta-Lime #6
3060010-06
Solid
06/03/13
06/03/13
Sta-Lime #7
3060010-07
Solid
06/03/13
06/03/13
Samples received in good condition at 29.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13

Laboratory Report
r3 Full Service
I
Analytical
� Environmental Solutions
s
06/10/2013
��LA60RATORIES ING
�
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime #1
Attn: Andy Smith
Prism Sample ID: 3060010-01
P.O. Box 1111
Prism Work Order: 3060010
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Daterrime
ID
General Chemistry Parameters
% Solids
72.3
% by
0.100
0.100
1 *SM2540 G 6/4113 14:10
ANG
P3F0048
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 6/4/13 9:26
MES
P3F0070
Total Metals
Mercury
0.22
mg/kg dry
0.029
0.0098
1 *7471B 6/6/13 13:09
MEH
P3F0062
Arsenic
11
mg/kg dry
0.35
0.079
1 *6010C 615113 19:08
BGM
P31=0057
Cadmium
BRL
mg/kg dry
0.35
0.045
1 *6010C 615/13 19:08
BGM
P3F0057
Copper
29
mg/kg dry
0.69
0.14
1 *6010C 6/5/13 19:08
BGM
P31=0057
Lead
12
mg/kg dry
0.35
0.046
1 *6010C 6/5113 19:08
BGM
P31=0057
Nickel
99
mg/kg dry
1.4
0.012
1 *6010C 6/5/13 19:08
BGM
P3F0057
Selenium
BRL
mg/kg dry
0.69
0.16
1 *6010C 6/5/13 19:08
BGM
P3F0057
Zinc
44
mglkg dry
3.5
0.47
1 *6010C 615/13 19:08
BGM
P3170057
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13

1.
Laboratory Report
r Full -Service Analytical 8
I S M I
1� Environmental Solutions
06/10/2013
'^ - '�7 LASOAATORI E$ ING
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime #2
Attn: Andy Smith
Prism Sample ID: 3060010-02
P.O. Box 1111
Prism Work Order: 3060010
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter Result" Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 70.6
% by
0.100
0.100 1 'SM2540 G 6/4/13 14:10 ANG
P3F0048
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 'SM9221 E 6/4/13 9:26 MES
P3F0070
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 O 13

Full -Service Analytical &
Laboratory Report
�
i I S Environmental Solutions 06/10/2013
111150R TORTE$ ING
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta-Lime #3
Attn: Andy Smith Prism Sample ID: 3060010-03
P.O. Box 1111 Prism Work Order: 3060010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Datefrime
ID
General Chemistry Parameters
% Solids 82.9
% by
0.100
0.100 1
`SM2540 G 614/13 14:10 ANG
P31`0048
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 614/13 9:26 MES
P3F0070
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 13

Full -Service Analytical
Rt ISM
Environmental Solutions
LABORATORIES, INO
Laboratory Report
06/10/2013
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime #4
Attn: Andy Smith Prism Sample ID: 3060010-04
P.O. Box 1111 Prism Work Order: 3060010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 70.4 % by 0.100 0.100 1 'SM2540 G 6/4113 14:10 ANG P3F0048
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 6/4/13 9:26 MES P3F0070
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240M - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 13

L7 i Full -Service Analytical 8
IS MI Environmental Solutions
�"FLABORATORIES INC
Laboratory Report
06/10/2013
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime #5
Attn: Andy Smith Prism Sample ID: 3060010-05
P.O. Box 1111 Prism Work Order: 3060010
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 82.5 % by 0.100 0.100 1 •SM2540 G 6/4113 14:10 ANG P3170048
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 6/4/13 9:26 MES P3F0070
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 13

I n Full -Service Analytical s
' V' Environmental Solutions
= LABBRATORFE9, INC.
Laboratory Report
06110/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime #6
Attn: Andy Smith
Prism Sample ID: 3060010-06
P.O. Box 1111
Prism Work Order: 3060010
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
73.9 % by
0.100
0.100 1 *SM2540 G 6/4113 14:10 ANG
P3F0048
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 *SM9221 E 6/4113 9:26 MES
P3F0070
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 13

E Full -Service Analytical 8
R ISM Environmental Solutions
""ORATORIES, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
06/10/2013
Project: StaLime Client Sample ID: Sta-Lime #7
Prism Sample ID: 3060010-07
Prism Work Order: 3060010
Sample Matrix: Solid Time Collected: 06/03/13 10:45
Time Submitted: 06/03/13 15:05
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 70.3
% by
0.100
0.100 1
'SM2540 G 6/4/13 14:10 ANG
P3F0048
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 6/4/13 9:26 MES
P3F0070'
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 13

h C; �. Full -Service Analytical &
14 R I S Environmental Solutions
4.:
"ram __RATORIEs ING.
Level II QC Report
6/10/13
City of Statesville, NC Project: StaLime Prism Work Order: 3060010
Attn: Andy Smith Time Submitted: 6/3/2013 3:05:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3F0057 - 3050B
Blank (P3F0057-BLK1)
Prepared & Analyzed: 06/05/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3F0057-BSI)
Prepared & Analyzed: 06/05/13
Arsenic
23.2
0.25
mg/kg wet
24.51 95
80-120
Cadmium
22.6
0.25
mg/kg wet
24.51 92
80-120
Copper
24.7
0.49
mg/kg wet
24.51 101
80-120
Lead
22.9
0.25
mg/kg wet
24.51 94
80-120
Nickel
22.5
0.98
mg/kg wet
24.51 92
80-120
Selenium
23.1
0.49
mg/kg wet
24.51 94
80-120
Zinc
23.9
2.5
mg/kg wet
24.51 97
80-120
Batch P3F0062 - 7471 B
Blank (1133F0062-BLK1)
Prepared: 06/05/13 Analyzed: 06/06/13
Mercury
BRL
0.019
mg/kg wet
LCS (P3F0062-BS1)
_
Prepared: 06/05/13 Analyzed: 06/06/13
Mercury
0.474
0.020
mg/kg wet
0.4237 112
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 10 of 13

k
&,RAISMFull-Service AnalyticalV' Environmental Solutions
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
6/10/13
Prism Work Order: 3060010
Time Submitted: 6/3/2013 3:05:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3F0048 - Default Prep Metals
Blank (P3F0048-BLK1) Prepared & Analyzed: 06/04/13 _
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 13

Level II QC Report
I %�
Full -Service Analytical
6/10/1 3
r ( ' V'
Environmental Solutions
i� LABORATONI ES IN
City of Statesville, NC
Project:
Stal-ime
Prism Work Order: 3060010
Attn: Andy Smith
Time Submitted: 6/3/2013 3:05:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P3F0070 - NO PREP
Blank (P3F0070-BLK1)
Prepared & Analyzed: 06/04/13
Fecal Coliforms
BRL
0.2
MPN/g wet
Sample Extraction
Data
Prep Method: Default Prep Metals
Lab Number
Batch
Initial
Final
Daterrime
3060010-01
P3F0048
30 g
30 mL
06/04/13 14:10
3060010-02
P3F0048
30 g
30 mL
06/04/13 14:10
3060010-03
P3F0048
30 g
30 mL
06/04/13 14:10
3060010-04
P3F0048
30 g
30 mL
06/04/13 14:10
3060010-05
P3F0048
30 g
30 mL
06/04/13 14:10
3060010-06
P3F0048
30 g
30 mL
06/04/13 14:10
3060010-07
P3F0048
30 g
30 mL
06/04/13 14:10
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
3060010-01
P3F0057
2 g
50 mL
06/05/13 9:00
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime
3060010-01
P3F0062
0.57 g
50 mL
06/05/13 12:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 13

kr ism
Full-Service Analytical &
CHAIN OF CUSTODY RECORD
Environmental Solutions
PAGE — OP _ QUOTE # TO ENSURE PROPER BILLING:
rLABORATORIES INC.
r. n�
449 Springbtook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 Project Name:
Phone: [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name:+ ✓ If S�a�rSt'a Ire *Please ATTACH any project specific reporting (QC LEVEL 1 II III Iv)
provisions and/or QC Requirements
Report To/Contact Name: Q JIB 9tin � ll
Invoice To:
Reporting Address: 1� S). 'Bost' I'm Address:
S
. �� YES NO tJ/A`
Ipon arrival?
ICE? Temp
7777
iVATIVES•tndlcated?
Phone:`%, 4- S'78- 3w 3,3 Fax es (No):79q- 979-At!_6
purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NO
EDD Type: PDF_ Excel _Onther
rJtd� t'�e L!'CGTP
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work dust Be
business day.
Sc OTHER N/A
Site Location Name:
Samples received after 15:00 will be processed next
Site Location Physical Addrr�ess:)03 AA F. ,,,,
�
Turnaround time Is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— NO _
S�A�CS;'; JIB AB�
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
I
SAMPLE CONTAINER
PRESERVA-
ANALYSES
/
REQUESTED
/
j �
PRISM
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
HOURS
WATER OR
SLUDGE)
'TYPE
SEE BELOW
NO
SIZE
TIVES
���
/ /
/� / REMARKS
/
/ /
ID N0.
Sia "4 m
a _. 3• 1
10 !'1 J
cL
3
- -
--
C
-
-
Pb
I/
till
A) +
�; r
Sampler's Signature alelzY
Sampled By (Print Name) CC� �� K
Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be ctiqrges for any changes after analyses have been initialized.
Rat fished By: (Signet e)%/ Re v By: (SI nature) „ , D 1, Military/H
�P ➢id�z /a • bL1 tZ'� / �jJ(! /tl id
Reli hed By (SI t r Re ei y: (Signature) E Date
/73 AM
wened By: (Slgnawra) -
60I)AI i <
Comments
,Z
Sde Arnval Time ['I
Site Departure Tlme ..
Feld Tech Fee
wl
.0 d of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTOD ALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
C SAMPLES ARE NOT C EPTED AND VERIFIED AGAINST COO UNTIL R CE D AT THE LABORATORY. (p f � ' A,
W Ex ❑ UPS ❑ Hand -delivered P ism Field Service ❑ Other (fj9�
O
w E ❑ SCI US ❑ NO ❑ SC ! ❑R C N❑ SCTER: D❑ RINO SO El
SOLID NC ❑ SC E. I ❑ NC RCRA ❑ SC ❑ NO L❑ SC, ❑ NO LANDFILL❑ SC I ❑ NO ❑ SC ,
❑ ❑ ❑ ❑ — _ ❑— ■—._. ■ ❑—...— Cat'iG7, 'AL
CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

P SM
�r IABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP Certification No. L2307
Project: StaLime
Lab Submittal Date: 06/17/2013
Prism Work Order: 3060381
Case Narrative
06/25/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report'should not be` -reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 8

Full -Service Analytical &
Ism Environmental Solutions
'.�-O-RIMINC.
Sample Receipt Summary
06/25/2013
Prism Work Order: 3060381
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
3060381-01 Solid 06/17/13 06/17/13
Samples received in good condition at 32.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc_
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 8

Laboratory Report
c Full -Service Analytical &
/b'RISMEnvironmental Solutions
06/25/2013
''-` �'r`LA60RATOPIEg ING
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3060381-01
P.O. Box 1111
Prism Work Order: 3060381
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 06/17/13 10:15
Time Submitted: 06/17/13 15:10
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
80.2
% by
0.100
0.100
1 *SM2540 G 6/21/13 9:30
MEH
P3F0378
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1 *SM9221 E 6/18/13 10:15
MES
P3F0445
mL
Total Metals
Mercury
0.13
mg/kg dry
0.023
0.0079
1 *7471B 6119113 15:27
MEH
P3F0329
Arsenic
9.1
mg/kg dry
0.32
0.073
1 *6010C 6119/13 5:24
BGM
P3F0295
Cadmium
BRL
mg/kg dry
0.31
0.041
1 *6010C 6/21/13 22:33
BGM
P3F0354
Copper
43
mg/kg dry
0.63
0.12
1 *6010C 6/19113 5:24
BGM
P3F0295
Lead
9.7
mg/kg dry
0.32
0.042
1 *6010C 6/19/13 19:49
BGM
P3F0295
Nickel
110
mg/kg dry
1.3
0.011
1 *6010C 6/19113 19:49
BGM
P3F0295
Selenium
BRL
mg/kg dry
0.63
0.14
1 *6010C 6/19113 5:24
BGM
P3F0295
Zinc
41
mg/kg dry
3.2
0.43
1 *6010C 6119/13 19:49
BGM
P31F0295
This report should not be reproduced, except in its entirety, without the.written.consent of Prism Laboratories,, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 8

Level II QC Report! •+ ISM Full -Service Analytical & 6/25/13
Environmental Solutions
�LABORATOflIE$ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime
Reporting
Analvte Result Limit Units
Prism Work Order: 3060381
Time Submitted: 6/17/2013 3:10:00PM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P3F0295 - 3050B
Blank (P3F0295-BLKI) _
_ _
Prepared: 06/18/13 Analyzed: 06/19/13
Arsenic
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3F0295-BS1)
Prepared: 06/18/13 Analyzed: 06/19/13
Arsenic
25.3
0.25
mg/kg wet
25.00 101 80-120
Copper
30.0
0.50
mg/kg wet
25.00 120 80-120
Lead
21.9
0.25
mg/kg wet
25.00 88 80-120
Nickel
22.6
1.0
mg/kg wet
25.00 90 80-120
Selenium
24.3
0.50
mg/kg wet
25.00 97 80-120
Zinc
22.7
2.5
mg/kg wet
25.00 91 80-120
Batch P3F0329 - 7471 B
Blank (133F0329-BLK1) Prepared & Analyzed: 06/19/13 _.
Mercury BRL 0.019 mg/kg wet
LCS (P3F0329-BSI) Prepared & Analyzed: 06/19/13
Mercury 0.467 0.021 mg/kg wet 0.4310 108 80-120
Batch P3F0354 - 3050B
Blank (P3F0354-BLK1) _ Prepared: 06/20/13 Analyzed: 06/21/13 _
Cadmium BRL 0.25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 Of 8

■ Level II QC Report
/Of,
���OpFull=Service Analytical& 6/25/13
f � V' Environmental Solutions
"aonATOPIE$ ING
City of Statesville, NC Project: StaLime Prism Work Order: 3060381
Attn: Andy Smith Time Submitted: 6/17/2013 3:10:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P31F0354 - 3050B
LCS (P3F0354-BS1) _ Prepared: 06/20/13 Analyzed: 06/21/13
Cadmium 23.5 0.25 mg/kg wet 25.38 93 80-120
This report should not be reproduced, except its entirety, without the written consent of Prism Laboratories, Inc.
_,. ,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 8

14�111117---&...
�I S M Full -Service Analytical s
I Environmental Solutions
Level II QC Report
6/25/13
City of Statesville, NC Project: Stal-ime Prism Work Order: 3060381
Attn: Andy Smith Time Submitted: 6/17/2013 3:10:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3FO378 - NO PREP
Blank (P3FO378-BL_K1) _ Prepared: 06/20/13 Analyzed 06/21/13
% Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety,. without the written consent of Prism Laboratories,, Inc,.. ,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 8

Ismn Full -Service Analytical 8
� V I Environmental Solutions
AAMMZILABO RIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
6/25/13
Prism Work Order: 3060381
Time Submitted: 6/17/2013 3:10:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P31F0445 - NO PREP
Blank (P3F0445-BLK1) _ _ _ Prepared & Analyzed: 06/18/13
Fecal Coliforms BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Daterrime
3060381-01
P3F0354
1.98 g
50 mL
06/20/13 9:50
3060381-01
P3F0295
1.97 g
50 mL
06/18/13 9:15
3060381-01
P3F0295
1.97 g
50 mL
06/18/13 9:15
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
3060381-01 P3F0329 0.64 g 50 mL 06/19/13 9:35
This report should not be reproduced, except in its entirety,,. without the written consent of Prism. Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 8

CHAIN OF CUSTODY
Full -Service AnalytiCUSTODYRECORD
Environmental Solutions PAGE _ OF _ QUOTE it To ENSURE PROPER BILLING: Samples INTACT upon arrivals
a
'-, ,,-;;1„'.--1.,•' �AaORAToaieS. ING. Recelvetl ON WET ICE?
449 5pringbrook Road • P.Q. Box 240543 ®Charlotte, NO 28224-0543 Project Name: PROPER PRESERVATIVES Indlcated7 _ r� 7777
Phase: 704/529-G3GR •Fax: [phone] Short Hold Analysis: (Yes) (No) USTProject: (Yes) (No) Received WITHIN HOLDING TIMES ✓
Client Company Name: `Please ATTACH any projects specific reporting (QC LEVEL I II III
�';�Y o ' S��,Ieswr Ile
p p g ( CUSTODY SEAS INTACT
provisions and/or QC Requirements VOLATILES recd'W/OUT HEAD4PAE�
Report To/Contact Name: A o . cj S m ; � h
Invoice To: PROPER CONTAINERS used -- —
Reporting Address: Tlaaa Ili@
Address:
Phone: t1011-978- 3ar312 Fax es (No): 704.973- "7459 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC—
EDD Type: PDF— Excel —Other "Working Days" ❑ 6-9 Days Cl Standard 10 days ❑ Rushh WPro-Apork Mdust Be
rj;,tr+ i,',c:.c:.�t �L:1.:illP SC_OTHER N/A
Site Location Name: Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 69-a Bd i9 FOLd- r Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO
C- _
C, O (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
S �'0 esy, I le f4c RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
ANALYSES REQUESTED PRISM
TIME MATRIX
SAMPLE CONTAINER / ye /' i
CLIENT DATE CO_L_LE_CTE_D (SOIL, PRESERVA- \ /kC REMARKS LAB
OR "TYPE TIVES / � / ' s, / i ID NO.
SAMPLE DESCRIPTION
COLLECTED
MILITARY
HOURS
WATER
SLUDGE)
SEE BELOW
NO.
SIZE
7
N� -
Sampler's Signature
Upon relinquishing, this Chain of Custoc
submitted in writing to the Prism Projec
R 11 ulshed By: (Signatr) L
Reline{ /she By: (Signature
i 1 �••'` /ram//.n s' �':—�
S I P
Sampled
is your authorization f
Aanaqer. There will be
i (Print Name) A
Prism to proceed with the ai
targes for any changes after
IV By: (Signature �I y ?
( //�lf l
14
I Affiliation
as requested above. Any changes must be
s have been initialized.
Date
onal Comments:
N thod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WIT uSTODY SEALS FOR'TRANSPORTATION TO THE LAt$UMA t UHY.
a SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST GOO NTIL RECEIVED AT THE LABORATORY.
CD .7 COO��
I
0 ed Ex ❑ UPS ❑ Hand -delivered V01ism Field Service 0 Other
DES: j UST: GR NDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
Do NO ❑ SCI ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC I ❑ NO Cl SC I ❑ NO ❑ SC
ONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

JI®I M
Full-Service Analytical &
Environmental Solutions
LABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Quarterly Parameters)
Lab Submittal Date: 07/01/2013
Prism Work Order: 3070006
Case Narrative
07/12/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
7. ��' �_ a_ (_ �
Reviewed By Robbi A. Jones
President/Project Manager
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 8

"dC I n n Full -Service Analytical &
( ' V' Environmental Solutions
.���IABOMTORIE$ ING
Sample Receipt Summary
07/12/2013
Prism Work Order: 3070006
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3070006-01 Solid 07/01/13 07/01/13
Samples received in good condition at 3.9 degrees C unless otherwise noted
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 8

Laboratory Report
)fp'7 ,� Full -Service Analytical &
zt lira\ I S 1 V 1 I Environmental Solutions 07/12/2013
422�ViA80—TORIEsING.
City of Statesville, NC Project: StaLime (Quarterly Client Sample ID: Sta-Lime
Attn: Andy Smith Parameters) Prism Sample ID: 3070006-01
P.O. Box 1111 Prism Work Order: 3070006
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/01/13 14:23
Time Submitted: 07/01/13 15:55
Parameter '
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
1000
mg/kg
380
32
5
*Calculation
719/13 15:25
CLB
[CALC]
% Solids
80.2
% by
0.100
0.100
1
*SM2540 G
7/2113 15:15
MJO
P3G0067
Weight
Nitrate/Nitrite as N
7.7
mg/kg dry
6.2
0.69
1
*SM4500-NO3 F
7/2113 8:52
CLB
P3G0030
Phosphorus -Total
1700
mg/kg dry
120
18
40
*SM4500-P F
719/13 11:22
CLB
P3G0087
Total Kjeldahl Nitrogen
4200
mg/kg dry
1600
130
5
*351.2
719/13 15:25
CLB
P3G0163
Ammonia as N
57
mg/kg
5.0
0.48
1
*SM4500-NH3 G
7/3/13 11:57
CLB
P3G0048
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1
*SM9221 E
7/2/13 13:00
MES
P3130093
mL
Total Metals
Mercury
0.21
mg/kg dry
0.025
0.0084
1
*74718
7/2/13 15:17
BGM
P3G0042
Arsenic
20
mg/kg dry
3.1
0.71
10
*6010C
7/11113 15:37
BGM
P3G0052
Cadmium
BRL
mg/kg dry
3.1
0.40
10
*6010C
7/11/13 15:37
BGM
P3G0052
Copper
290
mg/kg dry
6.1
1.2
10
*6010C
7/10/13 0:28
BGM
P3G0052
Lead
14
mg/kg dry
3.1
0.41
10
*6010C
7/11/13 15:37
BGM
P3G0052
Nickel
180
mg/kg dry
12
0.11
10
*6010C
7/11/13 15:37
BGM
P3130052
Potassium
4700
mg/kg dry
150
20
10
*6010C
7111/13 15:37
BGM
P3G0052
Selenium
BRL
mg/kg dry
6.1
1.4
10
*6010C
7/11/13 15:37
BGM
P3130052
Sodium
5100
mg/kg dry
150
39
10
*6010C
7110113 0:28
BGM
P3G0052
Zinc
57
mg/kg dry
31
4.2
10
*6010C
7111113 15:37
BGM
P3G0052
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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E" �/ Ap Full -Service Analytical &
I S I Y O I Environmental Solutions
••�L ORATORIES -
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3GO042 - 7471 B
Level II QC Report
7/12/13
Project: Stal-ime (Quarterly Parameters) Prism Work Order: 3070006
Time Submitted: 7/1/2013 3:55:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P3130042-BLK1) Prepared & Analyzed: 07/02/13
Mercury BRL 0.020 mg/kg wet
LCS (P3G0042-13SI) Prepared & Analyzed: 07/02/13
Mercury 0.444 0.020 mg/kg wet 0.4167 107 80-120
Batch P3GO052 - 3050B
Blank (1133130052-BLK1)
Prepared: 07/02/13 Analyzed: 07/11/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
13
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Sodium
BRL
13
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3GO052-BS1)
Prepared: 07/02/13 Analyzed: 07/11/13
Arsenic
22.4
0.25
mg/kg wet
25.13 89 80-120
Cadmium
22.2
0.25
mg/kg wet
25.13 89 80-120
Copper
24.3
0.50
mg/kg wet
25.13 97 80-120
Lead
22.5
0.25
mg/kg wet
25.13 90 80-120
Nickel
23.0
1.0
mg/kg wet
25.13 92 80-120
Potassium
480
13
mg/kg wet
502.5 96 80-120
Selenium
21.7
0.50
mg/kg wet
25.13 86 80-120
Sodium
478
13
mg/kg wet
502.5 95 80-120
Zinc
22.2
2.5
mg/kg wet
25.13 88 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Level II QC Report
r �11 ,p\//�' Full -Service Analytical & 7/12/13
I V , �r , I Environmental Solutions
,�XV LABORATORIES INO .
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (Quarterly Parameters)
Prism Work Order: 3070006
Time Submitted: 7/1/2013 3:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result B/%REC Limits RPD Limit Notes
Batch P3130030 - NO PREP
Blank (P3G0030-BLKI) Prepared & Analyzed: 07/02/13 _
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P3GO030-BSI) Prepared & Analyzed: 07/02/13
Nitrate/Nitrite as N 51.6 5.0 mg/kg wet 50.00 103 80-120
Matrix Spike (P3G0030-MS1) Source: 3070006-01 Prepared & Analyzed: 07/02/13
Nitrate/Nitrite as N 65.2 6.2 mg/kg dry 62.34 7.73 92 80-120
Matrix Spike Dup (P3G0030-MSD1) Source: 3070006-01 Prepared & Analyzed: 07/02/13
Nitrate/Nitrite as N 66.0 6.2 mg/kg dry 62.34 7.73 94 80-120 1 20
Batch P3GO048 - NO PREP
Blank (P3GO048-BLK1) Prepared: 07/02/13 Analyzed: 07/03/13
Ammonia as N BRL 5.0 mg/kg
LCS (P3GO048-BS1) Prepared: 07/02/13 Analyzed: 07/03/13
Ammonia as N 2.38 0.10 mg/kg 2.500 95 80-120
Matrix Spike (P3G0048-MS1) Source: 3070006-01 Prepared: 07/02/13 Analyzed: 07/03/13
Ammonia as'N 130 5.0 mg/kg 125.0 56.6 59 80-120 MI
Matrix Spike Dup (P3GO048-MSD1) Source: 3070006-01 Prepared: 07/02/13 Analyzed: 07/03/13
Ammonia as N 132 5.0 mg/kg 125.0 56.6 60 . 80-120 1 20 MI
Batch P3130067 - Default Prep Metals
Blank (P3GO067-BLK1) Prepared & Analyzed: 07/02/13
% Solids 100. 0.100 % by Weight
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ei R ISFull-Service Analytical
,
Environmental Solutions
;a'J LABORATORIES ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
P3130087 - SM4500-PB5
Blank (P3G0087-BLK1
Phosphorus -Total
Project: StaLime (Quarterly Parameters)
Level II QC Report
7/12/13
Prism Work Order: 3070006
Time Submitted: 7/1/2013 3:55:OOPM
Reporting Spike Source %REC
Result Limit Units Level Result %REC Limits RPD
BRL 2.5 mg/kg wet
07/03/13 Analyzed: 07/09/13
RPD
Limit Notes
LCS (P3GO087-BSI) Prepared: 07/03/13 Analyzed: 07/09/13
Phosphorus -Total 99.4 2.5 mg/kg wet 100.0 99 90-110
Matrix Spike (P3GO087-MS1) Source: 3070006-01 Prepared: 07/03/13 Analyzed: 07/09/13
Phosphorus -Total 1820 120 mg/kg dry 124.7 1660 124 80-120 MC
Matrix Spike Dup (P3GO087-MSD1) Source: 3070006-01 Prepared: 07/03/13 Analyzed: 07/09/13
Phosphorus -Total 1810 120 mg/kg dry 124.7 1660 116 80-120 0.6 20
Batch P3G0163 - 351.2
Blank (P3G0163-BLK1) Prepared: 07/08/13 Analyzed: 07/09/13
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P3G0163-BS1) Prepared: 07/08/13 Analyzed: 07/09/13
Total Kjeldahl Nitrogen 128 25 mg/kg wet 125.0 102 90-110
Matrix Spike (P3GO163-MS1) Source: 3070006-01 Prepared: 07/08/13 Analyzed: 07/09/13
Total Kjeldahl Nitrogen 10400 1600 mg/kg dry 6234 4220 99 90-110
Matrix Spike Dup (P3G0163-MSD1) Source: 3070006-01 Prepared: 07/08/13 Analyzed: 07/09/13
Total Kjeldahl Nitrogen 9370 1600 mg/kg dry 6234 4220 - 83 90-110 10 20 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Level II QC Report
q I Full -Service Analytical & 7/12/13
R ISM Environmental Solutions
'i LABORATORIES ING.
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 3070006
Attn: Andy Smith Time Submitted: 7/1/2013 3:55:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3GO093 - NO PREP
Blank (P3GO093-BLK1) Prepared & Analyzed: 07/02/13
Fecal Coliforms BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
3070006-01
P3G0163
0.05 g
25 mL
07/08/13 11:35
Prep Method: Default Prep Metals
Lab Number
Batch
Initial
Final
Daterrime
3070006-01
P3G0067
30 g
30 mL
07/02/13 15:15
Prep Method: SM4500-PBS
Lab Number
Batch
Initial
Final
Daterrime
3070006-01
P3G0087
1 g
50 mL
07/03/13 1211
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
3070006-01
P3G0052
2.03 g
50 mL
07/02/13 9:30
3070006-01
P3G0052
2.03 g
50 mL
07/02/13 9:30
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/rime
3070006-01
P3G0042
0.6 g
50 mL
07/02/13 11:36
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Full -Service Analytical & %orgAINF CUSTODY RECORD
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� r PAGE _ OF — QUOTE N TO ENSURE PROPER BIdO_BPd®:
s°uoonATonir_s.INC.
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Phone: [phone] Fax: [phone] Short Hold Analysis: (Yes) (NO) UST Project: (Yes) (No)
Client'Company Name +�j� a ��� c, Y; ��F "Please ATTACH any project specific reporting (QC LEVEL 1 11 III IV)
Report To/Contact Name: A .,.iy y S . A provisions and/or QC Requirements
O, h3oX lift Invoice To:
Reporting Address: Address:
SEA4e3V,'11t- NC
Phone:701-M-:3q.37 Fax D(No):101'-8?$-Bd•3s'"
Purchase Order No./Billing Reference TO BE 1=IEEE® IN BY CLIENT/SAMPLING PERSONNEL
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�our� �'�a'c1c G:3C:d i (� PP SC_OTHER N/A
Site Location Name: Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 603 `, If FAem li? a Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO _
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
T T RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME MATRIX ANALYSES REQUESTED \A
SAMPLE CONTAINER 2' PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- / �� / / % REMARKS ID B
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR `TYPE NO. SIZE TIVES
HOURS SLUDGE) SEE BELOW
.7-1-4 1 1Wd3
Rl
PA
1d� T)
IJ a T
M
Sampler's Signature T� GL/`��c� r�Z' , Sampled By (Print Name)a� y ✓_a --�� I Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin fished By: (Signature) . Recei ign ro Date Milita
mgws . ,aignaru w. .....•.`�.,.,._..,..__ —,. A_•�o I
od of Shipment: NOTE, ALL SAMPLE COOLE67
RS SHOULD BE TAPED SHUT WITH CUSTOD E S FO NSPORTATION TO THE LABORATORY. OC Group No.
CD SAMPLES ARE NOT AC EPTED AND VERIFIED AGAINST COG UNTIL RECEIVED A LABORATORY. �l A (�
0 ed Ex ❑ UPS ❑ Hand-delivered/A Prism Field Service ❑ Other
00 DES* UST:
C ❑ SC ❑ C ❑ SC O NU 0 CTER: UDRINKINGSCATER: 0SOLID WASTE: I a NC 0 SC p❑ NCCLA LANDFILL ❑ SC 1 0 NC 0 SC I O NC p SC
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
i tA➢ t' K �X .. >
Additional Comments:

"T NC Certification No. 402
SC Certification No. 99012 Case Narrative
PC' a rf- Full -Service Analytical & NC Drinking Water Cert No. 37735
j� I S 1 V 1 .I Environmental Solutions VA Certification No. 460211 07/29/2013
LABORATORIES INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/15/2013
Statesville, NC 28687 Prism Work Order: 3070292
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call'if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
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I S Full -Service Analytical
A
M n Environmental
' � I Environmental Solutions
& LABORATORIESl-
Sample Receipt Summary
07/29/2013
Prism Work Order: 3070292
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3070292-01 Solid 07/15/13 07/15/13
Samples received in good condition at 3.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Laboratory Report
RRI^; Full -Service Analytical &
` I S M Environmental Solutions 07/29/2013
t L .-T—M INC.
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3070292-01
P.O. Box 1111 Prism Work Order: 3070292
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/15/13 13:10
Time Submitted: 07/15/13 15:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
78.8
% by
0.100
0.100
1
*SM2540 G
7/17/13 15:30
ANG
P3Gd305
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
7/16/13 12:34
MES
P3G0379
Total Metals
Mercury
0.18
mg/kg dry
0.026
0.0087
1
*74716
7/27/13 13:47
MEH
P3G0504
Arsenic
16
mg/kg dry
3.2
0.73
10
*6010C
7/20113 10:46
BGM
P3G0317
Cadmium
BRL
mg/kg dry
3.2
0.41
10
*6010C
7/20/13 10:46
BGM
P3G0317
Copper
26
mg/kg dry
0.63
0.12
1
*6010C
7/19/13 4:49
BGM
173G0317
Lead
9.7
mg/kg dry
0.32
0.043
1
*6010C
7/19/13 4:49
BGM
P3130317
Nickel
90
mg/kg dry
1.3
0.011
1
*6010C
7/19/13 4:49
BGM
P3130317
Selenium
BRL
mg/kg dry
0.63
0.14
1
*6010C
7/19/13 4:49
BGM
P3G0317
Zinc
52
mg/kg dry
32
4.3
10
*6010C
7/20113 10:46
BGM
P3G0317
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Full -Service Analytical &
i.n Environmental Solutions
ISM
�""�RORATO—,% INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3GO317 - 3050B
Project: StaLime
Reporting
Result Limit Units
Level II QC Report
7129/13
Prism Work Order: 3070292
Time Submitted: 7/15/2013 3:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P3GO317-BLK1)
Prepared: 07/17/13 Analyzed: 07/19/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3GO317-BSI)
Prepared 07/17/13 Analyzed: 07/19/13
Arsenic
23.9
0.25
mg/kg wet
25,38 94
80-120
Cadmium
23.3
0.25
mg/kg wet
25.38 92
80-120
Copper
26.2
0.51
mg/kg wet
25.38 103
80-120
Lead
23.0
0.25
mg/kg wet
25.38 91
80-120
Nickel
23.9
1.0
mg/kg wet
25.38 94
80-120
Selenium
23.1
0.51
mg/kg wet
25.38 91
80-120
Zinc
23.3
2.5
mg/kg wet
25.38 92
80-120
Batch P3130504 - 7471 B
Blank (P3GO504-BLK1)
Prepared & Analyzed: 07/27/13
Mercury
BRL
0.020
mg/kg wet
LCS (P3G0504-BS1)
Prepared & Analyzed: 07/27/13
Mercury
0.415
0.019
mg/kg wet
0.4032 103
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 4 of 7

�A
I Full -Service Analytical &
S M Environmental Solutions
I AEO-TONIE9. ING
City of Statesville, NC - Project: StaLime
Attn: Andy Smith ,
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
7/29113
Prism Work Order: 3070292
Time Submitted: 7/15/2013 3:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3GO305 - NO PREP
Blank (P3GO305-BLK1) Prepared & Analyzed: 07117/13
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Page 5 of 7

Full -Service Analytical &
� I S M Environmental Solutions Adg�'
s
ns I.p80MTORIES, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: Stal-ime
Level II QC Report
7/29/13
Prism Work Order: 3070292
Time Submitted: 7/15/2013 3:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3GO379 - NO PREP
Blank (P3GO379-BLK1) Prepared & Analyzed: 07/16/13
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
3070292-01
P3G0317
2 g
50 mL
07/17/13 9:00
3070292-01
P3G0317
2 g
50 mL
07/17/13 9:00
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime
3070292-01 P3G0504 0.59 g
50 mL 07/27/13 10:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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.kV
Full -Service Analytical &
Environmental Solutions
'LHBORATORIES, INQ
449 Springbrook Road P.O. Box 240543 - Charlotte, NC 28224-0543
Phone:[phone] . Fax:[phone]
Client Company Name:C:4'y o
Report To/Contact Name: A Y7 g y Sbw'
Reporting Address:? 0 - Bo k' till
34.6esy:lle AlC
0CFMIAIN OF CUSTODY RECORD
PAGE OF _ QUOTE # TO ENSURE PROPER BILLONGr
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone:%Oil- I y" 3y•3tf Fax es (No): 7411- S t S" ' S655 Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Re s Days ❑ 3 Days ❑ 4 Days Y ❑ 5 Days Y
Requested Due Date ❑ 1 Day Y ❑ 2 Da
Certification: NELAC USACE FL INC
EDD Type: PDF_ Excel—�— Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
�s`c..�s iJ�91e2.?! Pre -Approved
SC OTHER N/A
/paertsr
Site Location Name: Samples received after 15:00 will be processed next business day.
Site Location Physical Address:6`� 3 Be if F.,m. PT Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
W5
J P RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection:: YES NO
arp p p
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
MATRIX
(SOIL,
WATER OR
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSE MUESTED
�f�
/ REMARKSID
PRISM
LAB
NO.
'TYPE-
HOURS
SLUDGE)
SEE BELOW
NO
SIZE
{��/
/
Av4,..Iy�s�
- -
—
--
---
--
�6
t----------
�' �r"
Sampler's Signature r� c'�� Sampled By (Print Name) „ �'� �� Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be D
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
Relln shed By: (Signature / Reb lived By. Sign Date Military/Hours Additional Comments:Site An ivau,
Rell hed By: re} �7 Recelved By: (Slgnatu Date Site Departure Tlme
`/3 G�
shed By: (SI h ature) Rec Iv Pris boratorles By: Date '.
od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WTrH`CV8T9DY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
O SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST 'OC RECEIVED AT THE LABORATORY.
/(p
-4 C/
-NAPrism
d Ex ❑ UPS ❑ Hand -delivered Field Service ❑ Other
O_ o
US GF TER. ATER: SOLIDWASTQ LLANDFILL
C Cl ❑ NC ❑ SC ❑ NO ❑ SCI ❑ NCEIRINKI❑ SC NO ❑ SCE ❑ NO Q SC ❑ NO ❑ SC ❑ NC D SC ❑ NO ❑ SC
-t.U1V I AI NCY9 I r rC t'UUCJ: N = F1I IUJI7I U = UIUCH to = Ulaaa I = naauu, I " = I onul I- 11Icu -IN v vn — ­uw tom.. , •.........r.-....�

t
• NC Certification No. 402 Case Narrative
r.; SC Certification No. 99012
e NC Drinkinq Water Cert No. 37735
Full -Service Analytical & 07/30/2013
IL I S 1 �I 1 I Environmental Solutions VA Certification No. 460211
•-' iaaonnroRies INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: Sludge (Hazardous Testing)
Andy Smith
P.O. Box 1111 Lab Submittal Date: 07/15/2013
Statesville, NC 28687 Prism Work Order: 3070297
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Reactivity and TCLP Herbicide analysis was subcontracted to GCAL. Laboratory report is attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V l..
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 18

1-fib-H,
IFull-Service al Solutio sga Environmental Solutions
LABORATORM
Sample Receipt Summary
07/30/2013
Prism Work Order: 3070297
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3070297-01 Solid 07/15/13 07/15/13
Samples received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18

,:....:_ Laboratory Report
Full -service Analytical
9 S
r Environmental Solutions
07/30/2013
' '�-`���-YW-qoR TORIES, ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Sample Matrix: Solid
Client Sample ID: Sta-Lime
Prism Sample ID: 3070297-01
Prism Work Order: 3070297
Time Collected: 07/15/13 13:00
Time Submitted: 07/15/13 15:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Corrosivity-pH 12 pH Units 1 *9045D 7/17113 10:50 JAB P3G0312
Ignitability Pass mm/sec 0.10 1 *1030 7/17/13 11:10 JAB P3G0330
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
7/17/13 9:00
MEH
P3G0315
TCLP Extraction
Complete
N/A
1
*1311 ZHE
7/23/13 10:45
ANG
P3G0398
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000041
1
*7470A
7/17/13 15:28
MEH
P3G0320
Arsenic
0.083
mg/L
0.050
0.0050
1
*6010C
7/19/13 1:38
BGM
P3G0316
Barium
BRL
mg/L
5.0
0.0010
1
*6010C
7/19/13 1:38
BGM
P3G0316
Cadmium
BRL
mg/L
0.025
0.00022
1
*6010C
7/19/13 1:38
BGM
P3G0316
Chromium
BRL
mg/L
0.25
0.0020
1
*6010C
7/19/13 1:38
BGM
P3G0316
Lead
BRL
mg/L
0.050
0.0030
1
*6010C
7/19/13 1:38
BGM
P3G0316
Selenium
BRL
mg/L
0.10
0.012
1
*6010C
7/19/13 1:38
BGM
P3G0316
Silver
BRL
mg/L
0.25
0.0013
1
*6010C
7/19/13 1:38
BGM
P3G0316
TCLP Organochlorine Pesticides by GC/ECD
Chlordane
BRL
ug/L
2.5
0.12
1
*8081B
7/25/13 23:30
JMV
P3G0340
Dieldrin
BRL
ug/L
0.50
0.0046
1
*8081B
7/25/13 23:30
JMV
P3G0340
Endrin
BRL
ug/L
0.50
0.0046
1
*8081B
7/25/13 23:30
JMV
P3130340
gamma-BHC
BRL
ug/L
0.50
0.0049
1
*8081B
7/25/13 23:30
JMV
P3G0340
Heptachlor
BRL
ug/L
0.50
0.0077
1
*8081B
7/25/13 23:30
JMV
P3G0340
Heptachlor Epoxide
BRL
ug/L
0.50
0.0046
1
*8081B
7/25/13 23:30
JMV
P3G0340
Methoxychlor
BRL
ug/L
0.50
0.0087
1
*8081B
7125/13 23:30
JMV
P3G0340
Toxaphene
BRL
ug/L
25
0.15
1
*8081B
7/25/13 23:30
JMV
P3G0340
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
115 %
13-186
Tetrachloro-m-xylene
77 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25 0.010 1
*8270D
7/22113 22:13
KC
P3G0359
2,4,6-Trichlorophenol
BRL
mg/L
0.10 0.011 1
*8270D
7/22113 22:13
KC
P3G0359
2,4-Dinitrotoluene
BRL
mg/L
0.050 0.0059 1
*8270D
7/22/13 22:13
KC
P3G0359
2-Methylphenol
BRL
mg/L
0.050 0.012 1
*8270D
7122113 22:13
KC
P3G0359
3/4-Methylphenol
BRL
mg/L
0.050 0.0098 1
*8270D
7/22/13 22:13
KC
P3G0359
Hexachlorobenzene
BRL
mg/L
0.050 0.0039 1
*8270D
7/22/13 22:13
KC
P3G0359
Hexachlorobutadiene
BRL
mg/L
0.050 0.016 1
*8270D
7/22/13 22:13
KC
P3G0359
Hexachloroethane
BRL
mg/L
0.050 0.018 1
*8270D
7/22/13 22:13
KC
P3130359
Nitrobenzene
BRL
mg/L
0.050 0.014 1
*8270D
7122/13 22:13
KC
P3G0359
Pentachlorophenol
BRL
mg/L
0.25 0.0092 1
*8270D
7/22113 22:13
KC
P3G0359
Pyridine
BRL
mg/L
0.25 0.011 1
*8270D
7/22/13 22:13
KC
P3G0359
Surrogate
Recovery
Control Limits
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O.
Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page
3 of 18

Laboratory Report
C �Full
h I S M
-Service Analytical &
I Environmental Solutions
07/30/2013
Y.LABORnTORIES ING
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3070297-01
P.O. Box 1111
Prism Work Order: 3070297
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 07/15/13 13:00
Time Submitted: 07/15/13 15:25
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
2,4,6-Tribromophenol
104 %
49-109
2-Fluorobiphenyl
88 %
55-96
2-Fluorophenol
51 %
27-74
Nitrobenzene-d5
86 %
53-99
Phenol-d5
36 %
11-52
Terphenyl-d14
85 %
42-133
TCLP•Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
ug/L
35 0.078
1 '8260B 7/24/13 9:16
VHL
P3G0428
1,2-Dichloroethane
BRL
ug/L
25 0.14
1 '8260B 7/24/13 9:16.
VHL
P3G0428
1,4-Dichlorobenzene
BRL
ug/L
380 0.068
1 '8260B 7/24/13 9:16
VHL
P3G0428
Benzene
BRL
ug/L
25 0.072
1 '8260B 7/24/13 9:16
VHL
P3G0428
Carbon Tetrachloride
BRL
ug/L
25 0.12
1 '8260B 7/24/13 9:16
VHL
P3G0428
Chlorobenzene
BRL
ug/L
5000 0.061
1 '8260B 7/24113 9:16
VHL
P3G0428
Chloroform
BRL
ug/L
300 0.089
1 '8260B 7/24/13 9:16
VHL
P3G0428
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
10000 0.90
1 '8260B 7/24/13 9:16
VHL
P3G0428
Tetrachloroethylene
BRL
ug/L
35 0.069
1 `8260B 7/24/13 9:16
VHL
P3130428
Trichloroethylene
BRL
ug/L
25 0.054
1 `8260B 7124/13 9:16
VHL
P3G0428
Vinyl chloride
BRL
ug/L
10 0.16
1 '8260B 7/24/13 9:16
VHL
P3G0428
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
106 %
80-124
Dibromofluoromethane
83 %
75-129
Toluene-d8
110 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 18

Sample Extraction Data
Prep Method: 1311
Lab Number
Batch Initial
Final
Date/Time
3070297-01
P3G0398 25 g
500 mL
07/22/13 15:00
3070297-01
P3G0315 100 g
2000 mL
07/16/13 15:45
Prep Method: 3010A
Lab Number
Batch Initial
Final
Datefrime
3070297-01
P3G0316 10 mL
50 mL
07/17/13 12:00
Prep Method: 7470A
Lab Number
Batch Initial
Final
Daterrime
3070297-01
P3G0320 20 mL
30 mL
07/17/13 11:50
Prep Method: 3510C GC
Lab Number
Batch Initial
Final
Daterrime
3070297-01
P3G0340 200 mL
10 mL
07/18/13 9:15
Prep Method: 3510C MS
Lab Number
Batch Initial
Final
Daterrime
3070297-01
P3G0359 200 mL
1 mL
07/19/13 9:00
Prep Method: 5030E
Lab Number
Batch Initial
Final
Daterrime
3070297-01
P3G0428 10 mL
10 mL
07/23/13 10:10
Subcontracted Analyses
The following analyses were subcontracted to Gulf Coast
Analytical Labs, Inc.
Lab Number
Analysis
3070297-01
Herbicides TCLP (Sub)
3070297-01
Reactivity, Cyanide (Sub)
3070297-01
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18

r
Full -Service Analytical & CHAIN F CUSTODY E®
5I S M I
�r Environmental Solutions PAGE _ OF QUOTE # TO ENSURE PROPER BILLING:
„'rj�y!• LA90RATORIES, ING
4,19 Springbrook goad * F,O. Box 240543 * Charlotte, NC 28224-0543 Project Name:
Phone: [phone] Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
1 / *Please ATTACH any project specific reporting (QC LEVEL 111111 1V)
Client Company Name: r'" provisions and/or QC Requirements
Report To/Contact Name: Invoice To:
Reporting Address: Address:
YES 10 N/4'
Samples INTACT upolY archaic N
—
ReceiVed ON WET ICETTemp 1
_
PROPER PR'SE:RVATIVES indicated?
—
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACTc
V01 ATILES ES-reedd W/OUT HEADSi?gCEc
PROPER CON.TAINERS,iisedc
-�. --
Phone: Fax (Yes) (No): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification' NELAC USAGE FL NC
EDD Type: PDF._ Excel —Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days p Rush Work Must Be
Pre -Approved SC OTHER N/A
Site Location Name: Samples received after 15:00 will be processed next business day. Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO —
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) —
TIME MAT Rlx ANALYSES REQUESTED PRISM
CLIENT
DATE
COLLECTED
(SOIL,
SAMPLE CONTAINER
PRESERVA-
j / / / / REMARKS
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
ID NO.
HOURS
SLUDGE)
SEE BELOW
;
rs�srW11
/TCi
T
Re- ---.
TU " .et3a
�o
Sampler's Signature Sampled By (Print Name) @/ Affiliation
Upon relinquishing, this pain oVeustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
suUmitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Rel Ished By: (Signa re) Recei e Bynature Date Military/Hoyt Additional Comments:
/ t
/r G72.. ' . �
Rel' ed By: (SI Rec ed By; (Signature) ' ate
in ed By: (Signs -) L f J Received For Prism Labor, tortes By: Date} —
w _ ` �.J'f_3 / G MliPage
r� thod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH TO ALS FOR TRANSPORTATION TO THE LABORATORY. COC Group o. y
CD SAMPLES ARE NOT, CCEPTED AND VERIFIED AGAINST CDC UNTI IVED AT THE LABORATORY, f G�
O Fed Ex ❑ UPS ❑ Hand -delivered sm Field Service ❑ Other
—n
DES: UST: GR UNDWATER: DRINKING WATER: SOLID WASTE: ! RCRA: CERCLA LANDFILL I OTHER:
O0 NC ❑ SC ❑ NC p SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ Sc ❑ NC O SC
❑ -- - I ❑ — .. I ❑ _.. ❑ —_ _ ❑ _. —.—--._.._ i ❑ ._ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
3070297
LABORATORY REPORT NUMBER
213071717
DATE
07/22/2013
Primary Data Review By
Authorized Signature
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 GSRI
Avenue, Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP
certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of
GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Page 7 of 18

NELAP CERTIFICATE NUMBER 01955
DOD FLAP CERTIFICATE NUMBER ADE - 1482
ANALYTICAL RESULTS
PERFORMED BY
GULF COAST ANALYTICAL LABORATORIES, INC.
7979 GSRI Avenue
Baton Rouge, LA 70820
Report Date 07/22/2013
GCAL Report 21
Deliver To Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
Attn Robbi Jones
Project 3070297

CASE NARRATIVE
Client: Access Analytical Report: 213071717
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the sample cross-reference page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).

Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the
Environmental Protection Agency or other recognized agencies. The samples and their corresponding
extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention
period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations Utilized in this Report
ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
00:00 Reported as a time equivalent to 12:00 AM
Reporting Flags Utilized in this Report
J Indicates the result is between the MDL and RDL
U Indicates the compound was analyzed for but not detected
B Indicates the analyte was detected in the associated Method Blank
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with
NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results
contained within this report relate only to the samples reported. The documented results are presented
-within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as
a permanent record thereof. The results contained within this report are intended for the use of the client.
Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with the NELAC standard and terms and conditions of the
contract and Statement of Work both technically and for completeness, for other than the conditions in the
case narrative. Release of the data contained in this hardcopy data package and in the
computer -readable data submitted has been authorized by the Quality Assurance Manager or his/her
designee, as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the
DOD QSM as specified in the contract if applicable.
Authorized Signature
GCAL REPORT 213071717
THIS REPORT CONTAINS _ PAGES.
Page 10 of 18

-----------------
Report Sample Summary
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
21307171701 STA-LIME Solid 07/15/2013 13:00 07/17/2013 09:45
GOAL Report 213071717
Page 11 of 18

Summary of Compounds Detected
There were no detects
GCAL Report 213071717
Page 12 of 18

SV
1311/8151A
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
071181201 310-00 511945 SW-846 1311/8151A 1 07/19/2013 20:16 TLS 512172
CASO
Parameter
94-75-7
2,4'-D
93-72-1
2,4,5-TP (Silvex)
CAS#
Surrogate
19719-28-9
DCAA
SW-846 Ch.7/9012A
Result
RDL
MDL
Units
0.001000
0.00500
0.00100
mg/L
0.001000
0.00500
0.00100
mg/L
Conc. Spiked Conc.Rec
Units
% Recovery
Rec Limits
20 11.5
ug/L
58
18 - 136
Prep
e al Prep Batch Prep Method Dilution Analyzed By Analytical Batch
P' I p / Date L 07 20 13 09:00 511931 Sw, 846 7.3.3.2 1 07/2212013 09:00 MCP 512159
CAS# Parameter
57-12-5R Reactivity Cyanide
SW-846 Ch.7/9034
Prep Batch Prep Method Dilution Analyzed By Analytical Batch
Prep Dale
07FI201201 3 09.00 511932 SW-846 7.3.4.2 1 07122/2013 10:00 DNIT 512161
CAS# Parameter
18496-25-8R Reactivity Sulfide
RESULTS REPORTED ON A DRY WEIGHT BASIS
GCAL Report 213071717
Result
RDL
MDL
Units
800
80
80
mg/kg

General Chromatography Quality Control Summary
Analytical Batch 512172
Client 1D
MB511945
LCS511945
LCSD511945
Prep Batch 511945
GCAL ID
1214805
1214806
1214807
Prep Method SW-846
Sample Type
Method Blank
LCS
LCSD
8151A
Prep Date
07/18/2013 10:00
07/18/2013 10:00
07/18/2013 10:00
Analytical Date
07/19/2013 15:07
07/19/2013 15:35
07/19/2013 17:00
Matrix
Water
Water
Water
SW-8461311/8151A
Units
mg/L
Spike
Result
Control
Result
RPD
Added
Result
% R
LiFMh % R
% R
RPD
Limit
94-75-7 2,4'-D
0.001000
0.00100
0.00099
0.00082
82
29 - 143
0.00085
86
4
40
93-72-1 2,4,5-TP (Silvex)
0.00100U
0.00100
0.00100
0.00087
87
44 - 130
0.00089
89
2
40
Surrogate
19719-28-9 DCAA
1.5
75
2
1.57
79
18 - 136
1.47
74
Analytical Batch 512172
Client ID
STA-LIME
1214552MS
1214552MSD
Prep Batch 511945
GCAL ID
21307171701
1215179
1215180
Prep Method SW-846
Sample Type
SAMPLE
MS
MSD
8151A
Prep Date
07/18/2013 10:00
07/18/2013 10:00
07/18/2013 10:00
Analytical Date
07/19/2013 20:16
07/19/2013 20:44
07/19/2013 21:12
Matrix
Solid
Solid
Solid
SW-846131118151A
Units
mg/L
Spike
Result
Control
Result
RPD
Added
Result
% R
LilbU % R
% R
RPD
Limit
94-75-7 2,4'-D
0.00000
0.00100
0.00991
0.00896
90
30 - 164
0.00800
81
11'
40
93-72-1 2,4,5-TP (Silvex)
0.00000
0.00100
0.01000
0.01000
100
42 - 155
0.00886
89
12
40
Surrogate
19719-28-9 DCAA
11.5
58
20
17.5
88
18 - 136
15.4
77
IM
fv
N GCAL Report 213071717
Jh-
00

General Chemistry Quality Control Summary
Analytical Batch 512159
Client ID
MB511931
LCS511931
Prep Batch 511931
GCAL ID
1214744
1214745
Prep Method SW-846
Sample Type
Method Blank
LCS
7.3.3.2
Prep Date
07/20/2013 09:00
07/20/2013 09:00
Analytical Date
07/22/2013 08:55
07/22/2013 08:56
Matrix
Solid
Solid
SW-846 Ch.719012A
Units mg/kg
Spike
Result
Control
Result
RAtided
% R
Limits % R
57-12-5R Reactivity Cyanide
25OU 250
1 2501
8.6
3
1 - 25
Analytical Batch 512159
Client ID
SOUTH ASH BASIN
1214156DUP
Prep Batch 511931
GCAL ID
21307161601
1214746
Prep Method SW-846
Sample Type
SAMPLE
DUP
7.3.3.2
Prep Date
07/20/2013 09:00
07/20/2013 09:00
Analytical Date
07/22/2013 08:56
07/22/2013 08:57
Matrix
Solid
Solid
SW-846 Ch.7/9012A
Units mglkg
Result
RPD
Result RDL
RPD
Limit
57-12-5R Reactivity Cyanide
0.0 250
0.0
0
25
GCAL Report 213071717

General Chemistry Quality Control Summary
Analytical Batch 512161
Client ID
MB511932
LCS511932
Prep Batch 511932
GOAL ID
1214747
1214748
Prep Method SW-846
Sample Type
Method Blank
LCS
7.3.4.2
Prep Date
07/20/2013 09:00
07/20/2013 09:00
Analytical Date
07/22/2013 10:00
07/22/2013 10:00
Matrix
Solid
Solid
SW-846 Ch.7/9034
units mg/kg
Spike
Result
Control
Result
RAUded
% R
Limits % R
18496-25-8R Reactivity Sulfide
80U 80
6891
216
31
20 - 114
Analytical Batch 512161
Client ID
SOUTH ASH BASIN
1214156DUP
Prep Batch 511932
GCAL ID
21307161601
1214749
Prep Method SW-846
Sample Type
SAMPLE
DUP
7.3.4.2
Prep Date
07/20/2013 09:00
07/20/2013 09:00
Analytical Date
07/22/2013 10:00
07/22/2013 10:00
Matrix
Solid
Solid
SW-846 Ch.7/9034
units mg/kg
Result
RPD
Result RDL
RPD
Limit
18496-25-8R Reactivity Sulfide
0 80
0
0
25
GCAL Report 213071717

Full -Service Analytical &
*1
Environmental Solutions
SM
SUBCONTRACT .
CONTRACT ORDER
. Cettif ation- NELAC— USAGE
Prism Laboratdriesjnc.
SC_ Other tj C_
3070207 N/A
SENDING LABORATORY- RECEIVING LABORATORY:
Prism Laboratories, Inc. 6uirCoast.Analytical Ubs, Inc.
P. O. Box 240543 7979 GSRI Avenue
Charlotte, NC.28224-0543 Baton Rouge;.
-I,A,7082.0
Phone: [phone] Phone .:[phone]
Fax: [phone] Fax: [phone]
PrqjqctManagcr: -Robbikknes
Analysis Due Expires Laboratory ID 'Connuenig 11
sample M'.-307.0Z97:.' Q! .Solid s
Reactivity;
SuM e. u
-,'Cyanide taubll
Containers Supplied: GUS-
13'13;00
13 13,00
13 11.-.00
--------- - e
Released By
Released,By Date, 4 777=
40ceived By Date
Page I of 1
Page 17 of 18

(D
00
0
COOLERS
DISCREPANCIES
LABORATORY PRESERVATIONS
Airbill
Temp(oC)
jWne
lNone
7962 4327 2693
3.6 (F2--)
NOTES
Revision 1.4
Paige -1

i NC Certification No. 402 Case Narrative
T SC Certification No. 99012
! b Full -Service Analytical & NC Drinking Water Cert No. 37735
® A Ism
Y 08/09/2013
a Environmental Solutions VA Certification No. 460211
t.
a=' 'ueoenToaies INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111. Lab Submittal Date: 07/29/2013
Statesville, NC 28687 Prism Work Order: 3070577
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
ter..
Reviewed By Steven H. Guptill For Robbi A. Jones
Project Manager
A % Solids determined outside the 7-day hold time.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 13

k
Full-Service Anal tical & Sample Receipt Summary
/���n:-ii I Environmental Solutions 08/09/2013
SM �80R MRIES. ING
Prism Work Order: 3070577
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
3070577-01
Solid
07/29/13
07/29/13
Sta-Lime
3070577-02
Solid
07/29/13
07/29/13
Sta-Lime
3070577-03
Solid
07/29/13
07/29/13
Sta-Lime
3070577-04
Solid
07/29/13
07/29/13
Sta-Lime
3070577-05
Solid
07/29/13
07/29/13
Sta-Lime
3070577-06
Solid
07/29/13
07/29/13
Sta-Lime
3070577-07
Solid
07/29/13
07/29/13
Samples received in good condition at 5.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13

Laboratory Report
A� ��� J
E I `-■ Full -Service Analytical environmental Solutions
08/09/2013
'�` IABORATORIE$ INF
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3070577-01
P.O. Box 1111 Prism Work Order: 3070577
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 93.5 % by 0.100 0.100 - 1 *SM2540 G 7/31113 16:00 ANG P31-10008
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 7/30/13 13:35 MES P31-10022
Total Metals
Mercury
0.13
mg/kg dry
0.023
0.0076
1
*7471B
8/1/13 16:21
MEH
P31-110006
Arsenic
13
mg/kg dry
0.27
0.061
1
*6010C
8l7/13 21:32
PJF
P3G0589
Cadmium
BRL
mg/kg dry
0.27
0.035
1
*6010C
817/13 21:32
PJF
P3G0589
Copper
28
mg/kg dry
0.53
0.10
1
*6010C
817/13 21:32
PJF
P3G0589
Lead
9.0
mg/kg dry
0.27
0.036
1
*6010C
8/7/13 21:32
PJF
P3G0589
Nickel
110
mg/kg dry
1.1
0.0095
1
*6010C
817/13 21:32
PJF
P3G0589
Selenium
BRL
mg/kg dry
0.53
0.12
1
*6010C
8/7/13 21:32
PJF
P3G0589
Zinc
44
mg/kg dry
2.7
0.36
1
*6010C
8/7/13 21:32
PJF
P3G0589
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13

Full -Service Analytical &
% I M I Environmental Solutions
trc= ��"�w' LABORATORIES ING
Laboratory Report
08/09/2013
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3070577-02
P.O. Box 1111 Prism Work Order: 3070577
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 92.6 A % by 0.100 0.100 1 'SM2540 G 817/13 13:30 ANG 1331i0125
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 7/30113 13:35 MES P31-10022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 13

Laboratory Report
n Full -Service Analytical
I S Environmental Solutions
ICI &
08/09/2013
vRO LA80-TOP M INC.
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3070577-03
P.O. Box 1111
Prism Work Order: 3070577
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
94.7 A % by
0.100
0.100 1 `SM2540 G 817/13 13:30 ANG
P31­110125
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 'SM9221 E 7/30/13 13:35 MES
P3H0022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

E.^ Full -Service Analytical &
isM
Environmental Solutions
LAR
Laboratory Report
08/09/2013
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3070577-04
P.O. Box 1111 Prism Work Order: 3070577
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 87.9 A % by 0.100 0.100 1 'SM2540 G 817/13 13:30 ANG P3H0125
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 "SM9221 E 7130/13 13:35 MES P31­10022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 13

Laboratory Report
Full -Service Analytical &
� „„,,��� (1� � /A� Environmental Solutions
� ,� ISM
d?R
08/09/2013
X = -Vti�'LA-Tonws, INC.
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3070577-05
P.O. Box 1111
Prism Work Order: 3070577
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter
Result Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
82.4 A % by
0.100
0.100 1 *SM2540 G 8/7/13 13:30 ANG
P31-10125
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 *SM9221 E 7/30/13 13:35 MES
P31-10022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 13

Laboratory'Report-
P�': f n Full -Service Analytical &
� R I S 1 V 1 Environmental Solutions 08/09/2013
-tY'-' u'� LABORATORIES ING
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3070577-06
P.O. Box 1111 Prism Work Order: 3070577
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 94.6 A % by 0.100 0.100 1 *SM2540 G 817/13 13:30 ANG P3H0125
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 . *SM9221 E 7/30/13 13:35 MES P3H0022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 13

Laboratory Report
1 -II Environmental
Analytical &
r-1 �,; Environmental Solutions 08/09/2013
�TIA50-OHIE$ ING
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime
Attn: Andy Smith Prism Sample ID: 3070577-07
P.O. Box 1111 Prism Work Order: 3070577
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 07/29/13 13:40
Time Submitted: 07/29/13 14:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DaterTime ID
General Chemistry Parameters
% Solids 94.8 A % by 0.100 0.100 1 'SM2540 G 8/7/13 13:30 ANG P3H0125
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 'SM9221 E 7/30/13 13:35 MES P31-10022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 13

::.- Level II QC Report
f
MR-mRI S Full -Service Analytical s 8/9/13
C"`a Environmental Solutions
; Y' LABORATORIES. ING
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime
Reporting
Analyte Result Limit Units
Batch P3130589 - 3050B
Prism Work Order: 3070577
Time Submitted: 7/29/2013 2:45:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (11"3130589-BLK1)
Prepared: 07/31/13 Analyzed: 08/07/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
L_CS (P3GO589-BSI)
Prepared: 07/31/13 Analyzed: 08/07/13
Arsenic
26.2
0.25
mg/kg wet
24.63 106 80-120
Cadmium
25.4
0.25
mg/kg wet
24.63 103 80-120
Copper
26.4
0.49
mg/kg wet
24.63 107 80-120
Lead
25.2
0.25
mg/kg wet
24.63 102 80-120
Nickel
24.8
0.99
mg/kg wet
24.63 101 80-120
Selenium
25.7
0.49
mglkg wet
24.63 105 80-120
Zinc
25.7
2.5
mg/kg wet
24.63 104 80-120
Batch P3H0006 - 7471 B
Blank (P3H0006-BLK1) Prepared: 07/31/13 Analyzed: 08/01/13
Mercury BRL 0.021 mg/kg wet
LCS (P3H0006-BSI) Prepared: 07/31/13 Analyzed: 08/01/13
Mercury 0.431 0.020 mg/kg wet 0.4167 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 13

r
E" Full -Service Analytical &
I S M I Environmental Solutions
92!2 ' n8O0.nTORIEr INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
8/9/13
Prism Work Order: 3070577
Time Submitted: 7/29/2013 2:45:OOPM
Analyte
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3H0008 - NO PREP
Blank (P3H0008-BLK1)
Prepared & Analyzed: 07/31/13
% Solids
Duplicate (P31-10008-DUP1)
100 0.100 % by Weight
Source: 3070577-01 Prepared & Analyzed: 07/31/13
Solids
Batch P3HO125 - NO PREP
91.9 0.100 % by Weight 93.5 2 20
Blank (P3H0125-1BLK1)
Prepared & Analyzed: 08/07/13
% Solids
100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 771
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 13

Level 11 QC Report
S Full -Service Analytical - 8/9/13
g �Environmental Solutions
'"%- ����'i+�U190RATDRIES ING _
City of Statesville, NC Project: StaLime Prism Work Order: 3070577
Attn: Andy Smith Time Submitted: 7/29/2013 2:45:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
- ---Batch P3H0022 - NO PREP
Blank (P3H0022-BLK1) Prepared & Analyzed: 07/30/13 _
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Daterrime
3070577-01 P3G0589 2 g 50 mL 07/31/13 9:30
Prep Method: 7471E
Lab Number Batch Initial Final Daterrime
3070577-01 P31­10006 0.57 g 50 mL 07/31/13 15:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 13

CHAIN Full -Service Analytical &
R I S M F CUSTODY RECORD
Environmental Solutions PAGE _ OF _ QUOTE # TO ENSURE PROPER BILLING:
BORATORIES, INC.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Project Name:
Phone: [phone] - Fax: [phone] Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: C � V Of ��4CS►^:11/ C *Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)
Report To/Contact Name � y y ; } �+ provisions and/or QC Requirements
Reporting Address: � 0. f3oX fill � n� Invoice To:
f4C Address:
Phone:IU7-4 f0 3N3O Fax qYesb (No):IVN-0 0-00,5
Purchase Order No./Billing Reference TO DE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Da ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Y Y Y Certification: NELAC USACE FL NC
EDD Type: PDF_ Excel Other "Working Days" Cl 6-9 Days ❑ Standard 10 days ❑ RushPre-Work
Must Be pproved SC OTHER N/A
Site Location Name: Fom rf M C. eelr )'b W TP Samples received after 15:00 will be processed next business day.
Site Location Physical Address:693 Be. of FQ"',D F - Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO _
P /VC (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
C RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX ANALYSES REQUESTED
SAMPLE CONTAINER � PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- /� LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES REMARKS ID NO. ! `/ / / / /
HOURS SLUDGE) SEE BELOW - i
/ d
Sampler's Signature `�
Upon relinquishing, this Chain of Custod
submitted in writing to the Prism Project
Rel y,ZZ sha By: (Slgna�, )
Reli. shed By: (Signature)
is your authorization for Prism to proceed
Manager. There will be charges4or any5;h''
aK Affiliation
analyses as requested above. Any changes must be
ar an.IVses have been initialized.
s SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COCJjNTIL RECEIVIrD AT THE LABORATORY. '
W ed Ex ClUPS ❑ Hand -delivered / Prism Field Service ElOther
O_
I UST: I OTER: D
W NC ❑ SC ❑ NC SC ❑ NC ❑ SC NICKI0 SC ATER. ❑ NC ❑ SC E. R
❑ NC ❑ SC] ❑ NC L❑ SC CINC LANDFILL❑ SC ❑ NC ❑ SC
�o- ❑ _ ❑ �❑ - - ❑ _❑ ❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
7 Fe c,a [ I �4-
Additional Comments:
,m}r: +G,NA .

NC Certification No. Case Narrative
SC Certification No. 990 99012
Full -Service Analytical & NC Drinkinq Water Cert No. 37735
j {M R 08/21 /2013
t Environmental Solutions VA Certification No. 460211 I %S
LABORATORIES, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 08/12/2013
Statesville, NC 28687 Prism Work Order: 3080240
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a �•
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 Of 7

Full -Service Analytical &
yT
RIS
RM
Environmental Solutions
Sample Receipt Summary
08/21 /2013
Prism Work Order: 3080240
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta Lime
3080240-01 Solid 08/12/13 08/12/13
Samples received in good condition at 5.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
v�
y�- Full -Service
Analytical &
3 `11 Environmental
I
Solutions
08/21/2013
�-r..�.. - LABORATORIES INC.
-
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta Lime.
Attn: Andy Smith
Prism Sample ID: 3080240-01
P.O. Box 1111
Prism Work Order: 3080240
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 08/12/13 11:59
Time Submitted: 08/12/13 14:45
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
72.2
% by
0.100
0.100
1 *SM2540 G 8/16/13 17:30
ANG
P3H0337
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 SM9221 E 8/13/13 11:48
MES
P3H0258
Total Metals
Mercury
0.15
mg/kg dry
0.027
0.0092
1 *7471B 8119113 18:15
BGM
P31­10345
Arsenic
1.1
mg/kg dry
0.35
0.080
1 *6010C 8/13/13 21:25
BGM
P3H0211
Cadmium
BRL
mg/kg dry
0.35
0.045
1 *6010C 8/13/13 21:25
BGM
P31­10211
Copper
29
mg/kg dry
0.69
0.14
1 *6010C 8/13/13 21:25
BGM
P3H0211
Lead
6.6
mg/kg dry
0.35
0.046
1 *6010C 8113/13 21:25
BGM
P3H0211
Nickel
81
mg/kg dry
1.4
0.012
1 *6010C 8/13/13 21:25
BGM
P3H0211
Selenium
1.5
mg/kg dry
0.69
0.16
1 *6010C 8113/13 21:25
BGM
P31­10211
Zinc
38
mg/kg dry
3.5
0.47
1 *6010C 8113/13 21:25
BGM
P3H0211
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 -'Fax: [phone] r Page 3 of 7

p I EService Analytical
Environmental Solutions
. ,�.... .--ORATORIE$INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P3HO211 - 3050B
Project: Stal-ime
Level II QC Report
8/21 /13
Prism Work Order: 3080240
Time Submitted: 8/12/2013 2:45:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P3H0211-BLK1)
Prepared & Analyzed: 08/13/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3HO211-BS1)
Prepared & Analyzed: 08/13/13
Arsenic
24.7
0.25
mg/kgmglkg wet
25.25 98
80-120
Cadmium
24.6
0.25
mg/kg wet
25.25 98
80-120
Copper
27.0
0.51
mg/kg wet
25.25 107
80-120
Lead
24.6
0.25
mg/kg wet
25.25 97
80-120
Nickel
25.0
1.0
mg/kg wet
25.25 99
80-120
Selenium
23.9
0.51
mg/kg wet
25.25 95
80-120
Zinc
24.7
2.5
mg/kg wet
25.25 98
80-120
Batch P3HO345 - 7471 B
Blank (P3H0345-BLK1)
Prepared & Analyzed: 08/19/13
Mercury
BRL
0.020
mg/kg wet
LCS (P3HO345-BS1)
Prepared & Analyzed: 08/19/13
Mercury
0.461
0.020
mg/kg wet
0.4237 109
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 7

!'r I I Full -Service Analytical &
Fir Environmental Solutions
_.-._. _.
LABORATORIESING.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
8/21 /13
Prism Work Order: 3080240
Time Submitted: 8/12/2013 2:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3H0337 - NO PREP
Blank (P3HO337-BLK1) Prepared & Analyzed: 08/16/13
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 7

h I S Full -Service Analytical
�j�Environmental
_ Enronmental Solutions
LABORATORIES, (-
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
8121 /13
Prism Work Order: 3080240 .
Time Submitted: 8/12/2013 2:45:OOPM
Reporting , Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3HO258 - NO PREP
Blank (P3H0258-BLK1) Prepared & Analyzed: 08/13/13
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
3080240-01
P31­10211
2 g
50 mL
08/13/13 10:00
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
3080240-01
P31­10345
0.61 g
50 mL
08/19/13 10:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 OTT-]

CHAIN O CUSTODY
y Futi-Servi,,e Analytical u YES NO N/A
F1 1 ' `a C'.n Ult'Onmental ;oiutl�Jns 8'AGE Or _ QUOTE # TO ENSURE PROPER SILLONG: Samples INTACT upon an ival? � �.
vPannio9ius. ui;. Received ON WET ICE? Tc mp �r— -- --- ---
Project Name:
40 Sprinoclook Fto d P.O. Box 240543 • Charlotte, ^IC 2822-1-0543 PROPER PRESERVAI IVES:indicated?
Phone: [phone] Fax: [phone] Short Hold Analysis: (Yes) (NO) UST Project: (Yes) (No)
.� � d "Please ATTACH any project specific reporting (QC LEVEL 1 11 III M Received W SEALS
HOLDING TIMES?
Client Company Name: fA �'� n''� provisions and/or QC Requirements CUSTODY SEALS INTACT? --
Report To/Contact Name: ea iv �e�ro d �a VOLATILES rec'd W/OUT HEADSPACE? _ _ ....—
�. Invoice To:
Reporting Address: s Vie' sd d fi PROPER CONTAINERS used?
Address:
Phone: 1 V " 6- _ -:3 n Fax (Yes) (No):
Purchase Order No./Billing Reference
TO RE FILLED IN BYCLIENT/SAMPLII\lG PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days O 3 Days ❑ 4 Days ❑ 5 Days
Certification- NELAC USACE FL
NC_
EDD Type: PDF_ Excel _Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days p Rush Work Must Be
_ r
Site Location Name: F"� . N Pa ') h • �"
Pre -Approved
SC_ OTHER N/A
Samples received after 15:00 will be processed next business day.
Site Location Physical Address: C
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES _ NO
p
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIEN'0
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
_
PRESERVA-
,�
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
*TYPE
NO.
SIZE
TIVES
F ;
%yr
a0 REMARKS
ti.; -"
ID NO.
HOURS
SLUDGE)
SEE BELOW
Sampler's Signatures n='�' Sampled By (Print Name)
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed
subrritted in writing to the Prism Project Manager. There will be arges for any cN
Reli tp iished By: (Sign'ture)®r . D H `y� R'ecei ed B (SiSly{/lu e)
Relinqu ed By: (Signr�"//j /p ,� },,,-R`ecEived By: (Sign(at e)
3 6. be 0 3 a'.�. Affiliation
with the analyses as requested above. Any changes must be
naes after analvses have been Initialized.
Additional Comments:
9
(D SAMPLES ARE NOT AC EPTED AND VERIFIED AGAINST COC TIL RECEIVED ATTHE LABORATORY.
ed-Ex D UPS ❑ Hand -delivered 1 rism Field Service ❑ Other
DES : UST: CaR UN®WATER: DRINKINGWATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: I t'
C ❑ SC ❑ NC Li SC ❑ NC ❑ SC ❑ NC ❑ SC U NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC
❑ ❑ ❑ ..- -- ❑ - ❑ ❑ .. ❑ -- ❑
NTAINER TYKE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

NC Certification No. 402
SC Certification No. 99012 Case Narrative
gy!m. Full -Service Analytical & NC Drinkinq Water Cert No. 37735
!j7 I S M � Environmental Solutions VA Certification No. 460211 09/16/2013
p' LABORATORIES, INC. DOD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 09/09/2013
Statesville, NC 28687 Prism Work Order: 3090124
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V L.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 7

/''�'� Full -Service Analytical8 Sample Receipt Summary
environmental Solutions 09/16/2013
Prism Work Order: 3090124
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3090124-01 Solid 09/09/13 09/09/13
Samples were received in good condition at 3.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 0f 7

Laboratory Report
Full -Service
Analytical &
Environmental Solutions
ABR
RISM
09/16/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3090124-01
P.O. Box 1111
Prism Work Order: 3090124
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/09/13 13:15
Time Submitted: 09/09/13 15:10
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch .
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
91.7
% by
0.100
0.100
1 *SM2540 G 9/12113 10:10
ANG
P310215
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1 'SM9221 E 9/10/13 12:58
MES
P310254
mL
Total Metals
Mercury
0.16
mg/kg dry
0.023
0.0079
1 *7471B 9/11113 14:09
MEH
P310175
Arsenic
7.6
mg/kg dry
0.82
0.19
3 *6010C 9/12/13 1:35
BGM
P310121
Cadmium
BRL
mg/kg dry
0.82
0.11
3 *6010C 9/12/13 1:35
BGM
P310121
Copper
26
mg/kg dry
1.6
0.32
3 *6010C 9112113 1:35
BGM
P310121
Lead
9.6
mg/kg dry
0.82
0.11
3 *6010C 9112/13 1:35
BGM
P3I0121
Nickel
91
mg/kg dry
3.3
0.029
3 *6010C 9112113 1:35
BGM
P310121
Selenium
BRL
mg/kg dry
1.6
0.37
3 *6010C 9/12113 1:35
BGM
P3I0121
Zinc
40
mg/kg dry
8.2
1.1
3 *6010C 9112/13 1:35
BGM
P310121
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

I Full -Service Analytical &
PRISM Environmental Solutions
LA60ftATORIE$ INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
9/16/13
Prism Work Order: 3090124
Time Submitted: 9/9/2013 3:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P310121 - 3050B
Blank (P310121-BLK1)
Prepared & Analyzed: 09/10/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.98
mg/kg wet
Selenium
BRL
0.49
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P310121-BSI)
-
Prepared & Analyzed: 09/10/13
Arsenic
24.8
0.25
mg/kg wet
25.38 98
80-120
Cadmium
23.9
0.25
mg/kg wet
25.38 94
80-120
Copper
25.1
0.51
mg/kg wet
25.38 99
80-120
Lead
24.1
0.25
mg/kg wet
25.38 95
80-120
Nickel
23.8
1.0
mg/kg wet
25.38 94
80-120
Selenium
24.2
0.51
mg/kg wet
25.38 95
80-120
Zinc
23.8
2.5
mg/kg wet
25.38 94
80-120
Batch P310175 - 7471 B
Blank (P310175-BLK1)
Prepared & Analyzed: 09/11/13
Mercury
BRL
0.020
mg/kg wet
LCS (P310175-BSI)
Prepared & Analyzed: 09/11/13
Mercury
0.415
0.018
mg/kg wet
0.3846 108
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 7

Full -Service Analytical & �� -
�{ Environmental Solutions
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
9/16/13
Prism Work Order: 3090124
Time Submitted: 9/9/2013 3:1O:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P310215 - NO PREP
Blank (P310215-BLK1) Prepared & Analyzed: 09/12/13
Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 O 7

; P R I Environmental
Analytical
//1 Environmental Solutions
�11////" � , 7 - LABORATORIES (-
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
9116/13
Prism Work Order: 3090124
Time Submitted: 9/9/2013 3:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P310254 - NO PREP
Blank (P310254-BLK1) Prepared & Analyzed: 09/10/13
Fecal Coliforms BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Date/Time
3090124-01 P310121 2 g 50 mL 09/10/13 8:30
Prep Method: 7471E
Lab Number Batch Initial Final Daterrime
3090124-01 P310175 0.56 g 50 mL 09/11/13 10:50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 7

ONANN OF CUSTODY RECORD
Full -Service Analytical
k.nvrronrnent.,al Sohitions
PAGE — OF — QUOTE I/ TO ENSURE PROPER SOLLDNO:
!A00RA70RIES, 111C.
-,A9 Springbrook Road,, P.O. Box 240543 , Charlotte, 1,1C 28224-0543 Project Name:
Phone: 704/529­3,354 - ax; 704/525-0409 Short Hold Analysis: (Yes) (NO) UST Project: (Yes) (No)
Client Company Name: C;1V *Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)
'A �J provisions and/or OC Requirements
Report To/Contact Name: Invoice To:
Reporting Address: P • BOX D D 11 Address:
Phone: 3-1:15 Fax [Yes )(No):12 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAIMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date U 1 Day 0 2 Days ❑El 3 Days 0 4 Days ❑0 5 Days Certification: NELAC—USAGE —FL NC_
EDD Type: PDF_ Excel —Other "Working Days" Ci 6-9 Days C3 Standard 10 days C] Rush Work Must Be
Pre -Approved SC OTHER N/A
Site Location Name: F'OeArOu Creek Samples received after 15:00 will be processed next business day.
Site Location Physical Address:03 801 F6,rm Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO-
3WO'Eve'Ite (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
ANALYSES SES REQUESTED QUESTED PRISM
TIME MATRIX SAMPLE CONTAINER
CLIENT DATE COLLECTED (SOIL, PRESERVA- LAB
*TYPE REMARKS
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE
Samples INTACT upon a . n va
Y�L�S NO
N/A
Received ON WET ICE? Temp
PROPER PRESERVATIVES irt0diced?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES rec'd WOUT HEADSPACE?
PROPER CONTAINERS used?
04
E.
5 Dal
Sampler's Signature' Sampled By (Print Name) �)&Jwa arl Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charge r y c"r190 after analyses have been initialized.
R1> h,d by: (Stgn&re) 7Veo by.,,k�ign elre)111­1� /ltar
p��q Mil
2
Al.
RelinqWshed By: (Signature)
Date
_—A
SAMP - T C 01X AND VERIFIED AGAINST COC UNitfi- RECEIVED HE LABORATORY.
0 UPS C3 Hand I ZI Prism Fleld ServIce _J Other
DRINKING WATER: SOLID WASTE: RCRA: OTHER:
DES: I UST: C3 'SC � GROUNDWATER: 1 L NC SC
CERCLA SC LANDFILL
F D SC
NC C3 SC 0 NC 0SC 0 NC 0 SC ONC OSC C] NC 0 ONC J Q NC 0 SC U NC
0 0
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
ye �2
Site Arrival Tinne:
Site Departure Time:
Field -rech Fee:
Mileage:

NC Certification No. 402 Case Narrative
SC Certification No. 99012
Mt J Full -Service Analytical & NC Drinking water Cert No. 37735 09/23/2013
7 Environmental Solutions VA Certification No. 460211
--- DOD ELAP: L-A-B Accredited Certificate No. L2307
LABORATORIES, INC.
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 09/16/2013
Statesville, NC 28687 Prism Work Order: 3090286
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Samples were received by the lab at ambient temperature.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
/.,
Robbi A. Jones
President/Project Manager
Reviewed By Steven H. Guptill For Robbi A. Jones
Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 13

PRISMFull -Service Analytical &
. Environmental Solutions
LABORATORIES INC.
Sample Receipt Summary
09/23/2013
Prism Work Order: 3090286
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Sta-Lime
3090286-01
Solid
09/16/13
09/16/13
Sta-Lime 2
3090286-02
Solid
09/16/13
09/16/13
Sta-Lime 3
3090286-03
Solid
09/16/13
09/16/13
Sta-Lime 4
3090286-04
Solid
09/16/13
09/16/13
Sta-Lime 5
3090286-05
Solid
09/16/13
09/16/13
Sta-Lime 6
3090286-06
Solid
09/16/13
09/16/13
Sta-Lime 7
3090286-07
Solid
09/16/13
09/16/13
Samples were received at 29.2 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 13

Laboratory Report
^^ Full -Service
I
Analytical &
09/23/2013
Environmental
... -._ .
LABORATORIES INC.
Solutions
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3090286-01
P.O. Box 1111
Prism Work Order: 3090286
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
82.3
% by
0.100
0.100
1 *SM2540 G 9/18/13 13:45
ANG
P310316
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1 *SM9221 E 9117/13 12:40
MES
P310371
Total Metals
Mercury
0.26
mg/kg dry
0.026
0.0086
1 *7471B 9/18/13 15:45
MEH
P310314
Arsenic
7.0
mg/kg dry
0.30
0.044
1 *6010C 9/19113 23:00
BGM
P310310
Cadmium
BRL
mg/kg dry
0.30
0.0028
1 *6010C 9/19/13 23:00
BGM
P310310
Copper
34
mg/kg dry
0.60
0.0075
1 *6010C 9119/13 23:00
BGM
P310310
Lead
7.3
mg/kg dry
0.30
0.035
1 *6010C 9/19/13 23:00
BGM
P310310
Nickel
80
mg/kg dry
1.2
0.0097
1 *6010C 9/19/13 23:00
BGM
P310310
Selenium
1.2
mglkg dry
0.60
0.072
1 *6010C 9/19/13 23:00
BGM
P310310
Zinc
50
mg/kg dry
3.0
0.020
1 *6010C 9/19/13 23:00
BGM
P310310
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 0f 13

Full -Service Analytical &
Environmental Solutions
LA ORATORIES INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
0912312013
Client Sample ID: Sta-Lime 2
Prism Sample ID: 3090286-02
Prism Work Order: 3090286
Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 89.0 % by 0.100 0.100 1 *SM2540 G 9/18113 13:45 ANG P310316
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2
1 *SM9221 E 9/17/13 12:40 MES P310371
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 13

Laboratory Report
�r-P R I S Fun -Service analytical s 09/23/2013
Environmental Solutions
�' LABORATORIES INC.
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime 3
Attn: Andy Smith Prism Sample ID: 3090286-03
P.O. Box 1111 Prism Work Order: 3090286
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 86.1 % by 0.100 0.100 1 *SM2540 G 9/18113 13:45 ANG P310316
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 9/17/13 12:40 MES P310371
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

Laboratory Report
Full-Service Analytical 8
Environmental Solutions
RIS
FIEs-
09/23/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime 4
Attn: Andy Smith
Prism Sample ID: 3090286-04
P.O. Box 1111
Prism Work Order: 3090286
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids 85.5
% by
0.100
0.100 1 'SM2540 G 9118/13 13:45 ANG P310316
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 9/17113 12:40 MES P310371
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 0f 13

R I S E V I I Full -Service Analytical
Environmental Solutions
_......�..... LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
09/23/2013
Project: StaLime Client Sample ID: Sta-Lime 5
Prism Sample ID: 3090286-05
Prism Work Order: 3090286
Sample Matrix: Solid Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids 89.1
% by
0.100
0.100 1 `SM2540 G 9/18/13 13:45 ANG
P310316
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 9/17113 12:40 MES
P310371
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 13

Laboratory Report
Full-Service Analytical &/IEnvironmental
��,,�' PRIS
Solutions
.lRM
09/23/2013
City of Statesville, NC
Project: Stal-ime
Client Sample ID: Sta-Lime 6
Attn: Andy Smith
Prism Sample ID: 3090286-06
P.O. Box 1111
Prism Work Order: 3090286
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids 84.9
% by
0.100
0.100 1 'SM2540 G 9/18113 13:45 ANG
P310316
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 9/17/13 12:40 MES
P310371
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 13

�y
P R I F� AAA Full -Service Analytical 8 Laboratory Report
��i Environmental Solutions 09/23/2013
f'.;-
-ORATORIES, INC.
City of Statesville, NC Project: StaLime Client Sample ID: Sta-Lime 7
Attn: Andy Smith Prism Sample ID: 3090286-07
P.O. Box 1111 Prism Work Order: 3090286
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/16/13 00:00
Time Submitted: 09/16/13 14:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 84.5 % by 0.100 0.100 1 *SM2540 G 9/18113 13:45 ANG P310316
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 9/17/13 12:40 MES P310371
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 13

/' PF—I I S 9 V® I Full -Service Analytical &
Environmental Solutions
*:.• _ - LAOORATORIES, INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Level II QC Report
9/23/13
Prism Work Order: 3090286
Time Submitted: 9/16/2013 2:50:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P310310 - 3050B
Blank (P310310-BLK1)
Prepared: 09/18/13 Analyzed:
09/19/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.99
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P310310-BSI)
Prepared: 09/18/13 Analyzed: 09/19/13
Arsenic
23.5
0.25
mg/kg wet
24.88 94
80-120
Cadmium
22.7
0.25
mg/kg wet
24.88 91
80-120
Copper
24.4
0.50
mg/kg wet
24.88 98
80-120
Lead
22.6
0.25
mg/kg wet
24.88 91
80-120
Nickel
22.6
1.0
mg/kg wet
24.88 91
80-120
Selenium
22.9
0.50
mg/kg wet
24.88 92
80-120
Zinc
22.8
2.5
mg/kg wet
24.88 92
80-120
Batch P310314 - 7471 B
Blank (P310314-BLK1)
Prepared & Analyzed: 09/18/13
Mercury
BRL
0.018
mg/kg wet
LCS (P310314-BSI)
Prepared & Analyzed: 09/18/13
Mercury
0,455
0.021
mg/kg wet
0.4386 104
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 13

Full -Service Analytical
PRISM
�L=Environmental Solutions
6- LABORATORIES INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
9/23/13
Prism Work Order: 3090286
Time Submitted: 9/16/2013 2:50:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P310316 - NO PREP
Blank (P310316-BLK1) Prepared & Analyzed: 09/18/13
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 13

Full -Service Analytical &
P R Environmental Solutions
����4 LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
9/23/13
Prism Work Order: 3090286
Time Submitted: 9/16/2013 2:50:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P310371 - NO PREP
Blank (P310371-BLK1)
Prepared & Analyzed: 09/17/13
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch
Initial
Final Daterrime
3090286-01 P310310
2.04 g
50 mL 09/18/13 9:15
Prep Method: 7471B
Lab Number Batch
Initial
Final Daterrime
3090286-01 P310314 0.57 g
50 mL 09/18/13 10:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 13

Full -Service Analytical & C��1`�J O CUSTODY RECORD
s. 6r1<`E3Environmental Solutions PAGE _ OF _ QUOTE 0 TO ENSURE PROPER BILLING:
LABORATORIES irlc.
Spntig,,7rook Road a P.O. Box 240543 a Charlotte, NC 23224-0543 Project Name:
?hone '704/529-636r! Far.: 704r52Ci-�0!4Gs Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: CA i 3 11es '.`61,M> ti "Please ATTACH any project specific reporting (QC LEVEL I II Ill M
c,•,i-� provisions and/or OC Requirements
Repol-t To/Contact Name: Ar>��� -r,
Reporting Address: J,�� 111}
Invoice To:
SFaS� ll� Address:
l,�FI-�7�- 3�138 la•Y-$7�'-�G'��
Samples INTACT upon arrival? 1 j' C-
rl.
Received ON WET ICE? Temp _
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES iec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
YES
NO
N/A I
Phone: Fax (Yes) (No):
Purchase Order No./Billing Reference
TO RE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email'(Yes) (No) Email Address
Requested Due Date ❑ 1 Day ] 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL NC_
EDD Type: PDF_ Excel _Other
"Working Days" O 6-9 Days ❑ Standard 10 days ❑ Work Must Be
Pre -
Site Location Name: Fl ii rn4 ce- e CkW LL TP Samples received after 15:00 will be processed next business day.
SC OTHER N/A
Site Location Physical Address: 03 D01 roac,n7 Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO —
�+
'C
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Id Upon Collection: YES NO
Iced p
.J T
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES
REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
�4"
LAg
"TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
T IVES
' Ci ;/
.!'
:' /%a REMARKS
ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE N, / w
p / 6
'a - A Ir7Ca.. ... 3 � �V itdC °r f ( 14
Pb
Sampler's Signature /i'a�
Upon relinquishing, this Chain of
submitted in writing to the Prism
Ala
/� 9 .at - a Sampled By (Print Name) 4y"4 72 W}+rrCA; Affiliation
;ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
'roject Manager. There will b charges for any changes after analyses have been initialized.
Rec 'ved By: (Sign re) Date Militai
Fgfee&Y7ed By: (Signature ( D to
Additional Comments:
Site Arrival Time:
Sito Departure Time:
Field Tech Fee:
Mileage: --- —
4FsWd By: (Signature)
R cetve'dFor Prism Lab O es By:
I Date
(D
d of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT tMj H CUSTODY S S FOR TRANSPORTATION TO
THE LABORATORY.
COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST C C UNTIL RECE1, , D AT THE LABORATORY,
°''
CJ //
~
OJ
Ex ❑ LIPS O Hand -delivered
°P sm Field Service ❑ Other
ES: UST: G
DWATER: DRINKING WATER: I SOLID WASTE: RCRA:
CERCLA LANDFILL OTHER:
w
❑SC: pNC ❑SC ❑
C ❑SC ❑NC DSC C]NC pSC ❑NC CI SC, ❑NC CISC, ❑NC 0SC ❑NC USC
NTAINER TYPE CODES:
A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap
VOA = Volatile Organics Analysis (Zero Head Space)

Full -Service Analytical &
P rRI I S M � Environmental Solutions
-:v ^ LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DOD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime (Quarterly Parameters)
Lab Submittal Date: 10/08/2013
Prism Work Order: 3100177
Case Narrative
10/16/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
) ��;' �_ I � C, - (_
Reviewed By Robbi A. Jones
President/Project Manager
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 8

Sample Receipt Summary
Full -Service Analytical &
PR.
. Environmental Solutions 10/16/2013
'._LA00RATOfl1ES INC.
Prism Work Order: 3100177
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3100177-01 Solid 10/08/13 10/08/13
Samples were received in good condition at 3.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 8

Full -Service Analytical &
""PRISM
r'PR M I Environmental Solutions
!.i, `y LABORATORIES INC.
Laboratory Report
10/16/2013
City of Statesville, NC Project: StaLime (Quarterly Client Sample ID: Sta-Lime
Attn: Andy Smith Parameters) Prism Sample ID: 3100177-01
P.O. Box 1111 Prism Work Order: 3100177
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/08/13 12:07
Time Submitted: 10/08/13 14:40
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
440
mglkg
81
6.9
1
*Calculation 10/15113 9:23
CLB
[CALC]
Solids
72.2
% by
0.100
0.100
1
*SM2540 G 10110113 15:13
ANG
P3J0214
Weight
Nitrate/Nitrite as N
20
mglkg dry
6.9
0.76
1
*SM4500-NO3 F 10/10/13 11:00
CLB
P3J0209
Phosphorus -Total
2000
mg/kg dry
69
10
20
*SM4500-P F 10/11/13 9:19
CLB
P3J0212
Total Kjeldahl Nitrogen
1900
mg/kg dry
350
29
1
*351.2 10/14/13 12:03
CLB
P3J0260
Ammonia as N
90
mglkg
5.0
0.43
1
*SM4500-NH3 G 10115M3 9:23
CLB
P3J0252
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E 10/9/13 12:07
MES
P3J0224
Total Metals
Mercury
0.16
mg/kg dry
0.029
0.0097
1
*7471B
10/15/13 14:16
MEH
P3J0291
Arsenic
6.9
mg/kg dry
0.34
0.050
1
*6010C
10/10/13 19:20
BGM
133J0204
Cadmium
BRL
mg/kg dry
0.34
0.0033
1
*6010C
10/10/13 19:20
BGM
P3J0204
Copper
30
mg/kg dry
0.69
0.0086
1
*6010C
10/10/13 19:20
BGM
P3J0204
Lead
9.0
mg/kg dry
0.34
0.040
1
*6010C
10110/13 19:20
BGM
P3J0204
Nickel
91
mg/kg dry
1.4
0.011
1
*6010C
10/10/13 19:20
BGM
P3J0204
Potassium
4900
mg/kg dry
170
11
10
*6010C
10/14/13 18:15
BGM
P3J0204
Selenium
BRL
mg/kg dry
0.69
0.083
1
*6010C
10/10/13 19:20
BGM
P3J0204
Sodium
540
mg/kg dry
17
0.16
1
*6010C
10/10/13 19:20
BGM
P3J0204
Zinc
41
mglkg dry
3.4
0.023
1
*6010C
10/10/13 19:20
BGM
P3J0204
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 8

Level II QC Report
%� Analytical
10/16/13
�' 9 I S�
I Environmental s
, �' I Environmental Solutions
h!`
--' LABORATORIES INC.
City of Statesville, NC
Project:
Stal-ime (Quarterly
Parameters)
Prism Work Order: 3100177
Attn: Andy Smith
Time Submitted: 10/8/2013 2:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result
%REC
Limits RPD Limit Notes
Batch P3J0204 - 3050B
Blank (P3J0204-BLK1)
Prepared & Analyzed: 10/10/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
12
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3J0204-BS1)
Prepared & Analyzed: 10/10/13
Arsenic
22.9
0.25
mg/kg wet
24.51
94
80-120
Cadmium
22.6
0.25
mg/kg wet
24.51
92
80-120
Copper
23.9
0.49
mg/kg wet
24.51
98
80-120
Lead
22.5
0.25
mg/kg wet
24.51
92
80-120
Nickel
22.5
0.98
mg/kg wet
24.51
92
80-120
Potassium
476
12
mg/kg wet
490.2
97
80-120
Selenium
22.3
0.49
mg/kg wet
24.51
91
80-120
Sodium
479
12
mg/kg wet
490.2
98
80-120
Zinc
22.3
2.5
mg/kg wet
24.51
91
80-120
Batch P3J0291 - 7471 B
Blank (P3J0291-BLK1) Prepared & Analyzed: 10/15/13
Mercury BRL 0.020 mg/kg wet
LCS (P3JO291-BSI) Prepared & Analyzed: 10/15/13
Mercury 0.469 0.021 mg/kg wet 0.4386 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 8

I Full -Service Analytical &
Il' Environmental Solutions
1 LABORATORIES IOC.
Level II QC Report
10/16/13
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 3100177
Attn: Andy Smith Time Submitted: 10/8/2013 2:40:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte _ Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3JO209 - NO PREP
Blank (P3J0209-BLK1)
Prepared & Analyzed: 10/10/13
Nitrate/Nitrite as N
BRL
5.0
mg/kg wet
LCS (P3JO209-BS1)
Prepared & Analyzed: 10/10/13
Nitrate/Nitrite as N
50.2
5.0
mg/kg wet
50.00 100 80-120
Batch P3JO212 - SM4500-PB5
Blank(P3JO212-BLK1)
— -
Prepared: 10/10/13 Analyzed: l0/11/13
Phosphorus -Total
BRL
2.5
mg/kg wet
LCS (P3J0212-BSI)
Prepared_ 10/10/13 Analyzed: 10/11/13
Phosphorus -Total
97.0
2.5
mg/kg wet
100.0 97 90-110
Batch P3JO214 - NO PREP
Blank (P3JO214-BLK1)
Prepared & Analyzed: 10/10/13
% Solids
100
0.100
/o by Weight
Batch P3JO252 - NO PREP
Blank (P3JO252-BLK1)
Prepared & Analyzed_ 10/15/13
Ammonia as N
BRL
5.0
mg/kg
LCS (P3J0252-BS1)
Prepared & Analyzed: 10/15/13
Ammonia as N
128
5.0
mg/kg
125.0 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 8 I

%s Full -Service Analytical &
PRISM I Environmental Solutions
,✓ LABORATORIES INC.
Level II QC Report
10/16/13
City of Statesville, NC Project: Stal-ime (Quarterly Parameters) Prism Work Order: 3100177
Attn: Andy Smith Time Submitted: 10/8/2013 2:40:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting
Spike Source
%REC RPD
Analyte
Result Limit Units
Level Result %REC
Limits RPD Limit Notes
Batch P3JO252 - NO PREP
Matrix Spike (P3J0252-MS1)
Source: 3100177-01
Prepared & Analyzed: 10/15/13
Ammonia as N
198 5.0 mg/kg
125.0 90.2 86
80-120
Matrix Spike Dup (P3J0252-MSD1)
Source: 3100177-01
Prepared & Analyzed: 10/15/13
Ammonia as N
194 5.0 mg/kg
125.0 90.2 83
80-120 2 20
Batch P3JO260 - 351.2
Blank (P3JO260-BLK1)
Prepared & Analyzed: 10/14/13
Total Kjeldahl Nitrogen
BRL 25 mg/kg wet
LCS (P3J0260-BS1)
Prepared & Analyzed: 10/14/13
Total Kjeldahl Nitrogen
133 25 mg/kg wet
125.0 106
90-110
Matrix Spike (P3J0260-MS1)
Source: 3100177-01
Prepared & Analyzed: 10/14/13
Total Kjeldahl Nitrogen
13300 3500 mg/kg dry
6925 1880 165
90-110 M
Matrix Spike Dup (P3JO260-MSD1)
Source: 3100177-01
Prepared & Analyzed: 10/14/13
Total Kjeldahl Nitrogen
13800 3500 mg/kg dry
6925 1880 172
90-110 4 20 M
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 8

Level II QC Report
' Full -Service Analytical & 10/16/13
Environmental Solutions
LABORATORIES INC.
City of Statesville, NC Project: StaLime (Quarterly Parameters) Prism Work Order: 3100177
Attn: Andy Smith Time Submitted: 10/8/2013 2:40:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source °/REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3JO224 - NO PREP
Blank (P3J0224-BLK1)
Prepared & Analyzed: 10/09/13
Fecal Coliforms
BRL
0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch
Initial
Final Daterrime
3100177-01 P3J0260
0.05 g
25 mL 10/14/13 10:38
Prep Method: SM4500-PBS
Lab Number Batch
Initial
Final Daterrime
3100177-01
P3J0212
1 g
50 mL
10/10/13 13:35
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Daterrime
3100177-01
P3J0204
2.02 g
50 mL
10/10/13 9:00
3100177-01
P3J0204
2.02 g
50 mL
10/10/13 9:00
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Daterrime
3100177-01 P3J0291 0.58 g 50 mL 10/15/13 12:06
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 Of 8

CHARM F C TY E
o!
. 3
e
R
Full -Service Analytical a
Environmental Soiuiiol:s
PROPERsoo.a.laso:
; ; fr. ^-=
Sarnples INTACT upon arrival?
YES NO N/A
PAGE_ or: _ ouovE n'ro ENSURE
_AaoRc.Toni=_S• m:;.
Received ON WET ICE? Temp------
Sprinclbroolc Road ^ P.O. Box 240543 ^ Charlotte, NG 28224-0543
Phore-
Project Name:
Short bold Analysis: (Yes) (NO) UST Project: (Yes) (No)
PROPER PRESERVATIVES indicated?_—
704/5.29-8354 a Fax: [phone]) p
Client Company Name: C rj y
*Please ATTACH any project specific reporting (QC LEVEL 1 11 Ili IV)
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
—r _5
Report To/Contact Name: �+ �� / ��� )'+
provisions and/or QC Requirements
VOLATILES reed WIOUT HEADSPACE?
Reporting Address: R 0 III I
Invoice To:
PROPER CONTAINERS used?
Address:
---- - -- —
- -- -----
s fqc
Phone: 7��- `"$-3Y3 Fax le's�)(No):7_21-`�'Z.S'.,f `4
Purchase Order No./Billing Reference
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
EDD Type: PDF_ Excel —Other _ Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ RuPresAW Work
Must B
ved
Site Location Name: FO "d 1T �:^C,, t l u `' Samples received after 15:00 will be processed next business day.
Site Location Physical Address: Imo; 11' �. Turnaround time is based on business days, excluding weekends and holidays
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER
CLIENT DATE COLLECTED (SOIL, PRESERVA- ` Or
r2
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TYPE TIVES�•
HOURS SLUDGE) SEE BELOW NO. SIZE
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC USACE EL NC_
e
SC OTHER N/A
Water Chlorinated: YES_ NO —
Sample Iced Upon Collection: YES NO
ANALYSES REQUESTED PRISM
4 LAB
A� REMARKS ID NO.
.�. � 43i bt •a r' �Y�_ _
S C'
Z"
Samplers Signature„ �"kvW� �y�G`y Sampled By (Print Name)►t VII`7Q,1101 LG ✓'E`ld Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be char ny changes after analyses have been initialized.
Re I ilshecl By: (sign3 ure) �, ✓ �yy/' Rec ' d ure) Date Militai
M NOTE• AL MP ERS SHOULD BE TAPED SHUT WITH, STODY SE FOR TRANSPORTATION TO THE LABORATORY.
(rD b
(D SAM P` ART CCEPTED AND VERIFIED AGAINST COC 0,1711. RECEIV -D AT THE LABORATORY.
CO
ed Ex =1 UPS ❑ Hand -delivered D Prism Field Service :2 Other
00
DES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
NC U SC J NC ❑ SC ❑ NC ❑ SC ❑ NC p SC i ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC , ❑ NC ❑ SC ❑ NC ❑ SC
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments
Site Arrival Time:
Site Departure Time:
Field Tech Fee:
Mileage: —'I

Full -Service Analytical &
JP 1;E)"M
Environmental Solutions
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinkinq Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 10/21/2013
Prism Work Order: 3100479
Case Narrative
10/28/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 7

I Sample Receipt Summary
,) Environmental
Service Analytical s 10/28/2013
Environmental Solutions
-_-- -Aa O-A Prism Work Order: 3100479
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3100479-01 Solid 10/21/13 10/21/13
Samples were received in good condition at 5.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
f Full -Service
Analytical 8
Environmental
.. .., ._ LPaOflPTOflIES INC.
Solutions
10/28/2013
City of Statesville, NC
Project: StaLime
Client Sample ID:
Sta-Lime
Attn: Andy Smith
Prism Sample ID:
3100479-01
P.O. Box 1111
Prism Work Order: 3100479
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/21/13 11:44
Time Submitted:
10/21/13 16:20
Parameter
Result
Units
Report
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
90.6
% by
0.100
0.100
1 *SM2540 G
10/24/13 15:57
ANG
P3J0508
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/100
1
1 *SM9221 E
10/22/13 10:28
MES
P3J0475
mL
Total Metals
Mercury
0.12
mglkg dry
0.020
0.0069
1 *7471B
10/26/13 12:14
MEH
P3J0539
Arsenic
4.9
mg/kg dry
0.28
0.040
1 *6010C
10122113 23:07
BGM
P3J0435
Cadmium
BRL
mg/kg dry
0.28
0.0026
1 *6010C
10/22/13 23:07
BGM
P3J0435
Copper
26
mg/kg dry
0.55
0.0070
1 *6010C
10/22113 23:07
BGM
P3J0435
Lead
9.4
mg/kg dry
0.28
0.032
1 *6010C
10/22/13 23:07
BGM
P3J0435
Nickel
83
mg/kg.dry
1.1
0.0090
1 *6010C
10/22/13 23:07
BGM
P3J0435
Selenium
BRL
mg/kg dry
0.55
0.067
1 *6010C
10/22/13 23:07
BGM
P3J0435
Zinc
36
mg/kg dry
2.8
0.019
1 *6010C
10/22/13 23:07
BGM
P3J0435
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

Level II QC Report
" I e� qqq I Full -Service Analytical & 10/28/13
.(/, Environmental Solutions
!..: ;'.a.... LABORATORIES INC.
City of Statesville, NC Project: Stal-ime Prism Work Order: 3100479
Attn: Andy Smith Time Submitted: 10/21/2013 4:20:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P3JO435 - 3050B
Blank (P3JO435-BLK1)
Prepared & Analyzed: 10/22/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3JO435-BSI)
Prepared & Analyzed: 10/22/13
Arsenic
25.3
0.25
mg/kgmg/kg wet
25.13 101 80-120
Cadmium
25.6
0.25
mg/kg wet
25.13 102 80-120
Copper
27.7
0.50
mg/kg wet
25.13 110 80-120
Lead
25.5
0.25
mg/kg wet
25.13 101 80-120
Nickel
25.2
1.0
mg/kg wet
25.13 100 80-120
Selenium
24.2
0.50
mg/kg wet
25.13 96 80-120
Zinc
25.1
2.5
mg/kg wet
25.13 100 80-120
Batch P3J0539 - 7471 B
Blank (P3JO539-BLK1)
Prepared: 10/25/13 Analyzed: 10/26/13
Mercury
BRL
0.020
mg/kg wet
LCS (P3J0539-BS1)
Prepared: 10/25/13 Analyzed: 10/26/13
Mercury
0.473
0.021
mg/kg wet
0.4310 110 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 7

" P I S Full- Service Analytical
Environmental Solutions
Z.._s'.., LA00RATOPIES INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
10/28/13
Prism Work Order: 3100479
Time Submitted: 10/21/2013 4:20:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3JO508 - NO PREP
Blank (P3J0508-BLK1) Prepared & Analyzed: 10/24/13
% Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 7

Level II QC Report
'*PRISM
Full -Service Analytical &
10/28/13
LABORATORIES INC.
Environmental Solutions
City of Statesville, NC
Project: StaLime Prism Work Order: 3100479
Attn: Andy Smith
Time Submitted: 10/21/2013
4:20:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC
RPD
Analyte
Result Limit Units Level Result %REC Limits RPD
Limit Notes
Batch P3JO475 - NO PREP
Blank (P3J0475-BLK1)
Prepared & Analyzed: 10/22/13
Fecal Coliforms
BRL 1 MPN/100 mL
Sample Extraction Data
Prep Method: 3050E
Lab Number
Batch Initial Final Daterrime
3100479-01
P3J0435 2 g 50 mL 10/22/13 9:15
Prep Method: 7471E
Lab Number
Batch Initial Final Date/rime
3100479-01
P3J0539 0.65 g 50 mL 10/25/13 15:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 6 of 7

CORD
Pull -Service Analytical CHAIN F CUSTODY RE
a r� Environmental Solutions PAGE _ Or _ QUOTE # TO ENSURE PROPERSOLLONG:
;J S;:i; qg rook ,-%Gael c P.O. ,Sox 2405,13 ^ Charlotte.,NC 28224-0543 Project Name:
Phonr.: 704/529-6364 Pax: 704/525-0409 // Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: y o SEa4'r'_l 6'+ Ile *Please ATTACH any project specific reporting (iaC LEVEL I II III IV)
Report To/Contact Name: ((}} rr yy pp provisions and/or OC Requirements
Invoice
Reporting Address: Rf+T0[, �Address::
ox III
.704e,Ty, He 14C
7 41 41-%?7 - 3°r3Q 7 J.V73-s
Samples INTACT upon arrival?
Receiver.) ON WET ICE? Temp '
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES,?
CUSTODY SEALS INTACT?
I .
VOLATILES rec'rJ W/OUT HEADSP. CE?
PROPER CONTAINERS used?
YES NO N/A
Phone: Fax es (No): +� purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ t Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC USACE FL
NC
EDD Type: PDF_ Excel Other
"Working
Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Site Location Name• ram r4 h Creek LC'L.. E_ P
Pre -Approved ►
SC_ OTHER N/A
Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 0,5 Be H Farm R Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES _ NO _
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
p
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
// \ i•
:`
LAB
*TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
' `T.: '
j`� REMARKS
ID NO.
HOURS
SLUDGE)
SEE BELOW
NO.
SIZE
r �L
/ �2; ,;
/
S4pp''��/ pp
k.� C'.:
9/ 1p
��`a!'i�J
..
��'qV
J
J` 1�
Sampler's Signature uc-'�a� C' Sampled By (Print Name) �� a'1 �V��A! ►C!C I Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Reli�n ;shed By: (SignaflI I Receiv n Date MUltai
i'I'-IIL4 ra �raz�rlC ', . �L•%r .rzsr- L
For
Es
Additional Comments:
e�y
Site Arrival Time:
Site. Departure Time:
—_
Field Tech Fee:
Mileage:
.,hod of Shi n : NOTE;,ALL SAMPJff COOLERS SHOULD BE TAPED SHUT WI CUSTODY SEAL ; FOR TRANSPORTATION TO THE LABORATORY. CUU UMID NO.
SA LES`AREN T ACCEPTED AND VERIFIED AGAINST COO UNTIL RECEIVEQ'AT THE LABORATORY.
-- Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service ❑ Olher s
DES: i UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: N'
~ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC
ONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

Full -Service Analytical &
RR I SMEnvironmental Solutions
LABORATORIES INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinkinq Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 11/05/2013
Prism Work Order: 3110075
Case Narrative
11/12/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a_. (a_rV__
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 7

Full -Service Analytical &
//r
�P R I Environmental Solutions
L 08O '.m.s INC.
Sample Receipt Summary
11 /12/2013
Prism Work Order: 3110075
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime
3110075-01 Solid 11/04/13 11/05/13
Samples were received in good condition at 5.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 0f 7

tr><�
I %� FWLService
Analytical
Laboratory Report
f% I I Environmental
s
Solutions
11/12/2013
__
LABORATORIES INC.
City of Statesville, NC
Project: StaLime
Client Sample ID:
Sta-Lime
Attn: Andy Smith
Prism Sample ID:
3110075-01
P.O. Box 1111
Prism Work Order: 3110075
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/04/13 14:10
Time Submitted:
11/05/13 09:30
Parameter
Result Units
Report
MDL
Dilution Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids
76.6
% by
0.100
0.100
1 *SM2540 G
11/6/13 13:22
MEH
P3K0105
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E
11/5/13 13:20
MES
P3K0129
Total Metals
Mercury
0.14
mg/kg dry
0.027
0.0093
1 *7471B
11/11/13 15:14
MEH
P31(0193
Arsenic
5.7
mg/kg dry
0.32
0.047
1 *6010C
11/12/13 1:35
BGM
P31<0185
Cadmium
BRL
mg/kg dry
0.32
0.0031
1 *6010C
11/12/13 1:35
BGM
P3K0185
Copper
29
mg/kg dry
0.65
0.0081
1 *6010C
11/12M3 1:35
BGM
P3K0185
Lead
12
mg/kg dry
0.32
0.038
1 *6010C
11/12/13 1:35
BGM
P3K0185
Nickel
99
mg/kg dry
1.3
0.011
1 *6010C
11/12/13 1:35
BGM
P3K0185
Selenium
BRL
mg/kg dry
0.65
0.078
1 *6010C
11/12/13 1:35
BGM
P31<0185
Zinc
50
mg/kg dry
3.2
0.022
1 *6010C
11/12/13 1:35
BGM
P31K0185
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

Level II QC Report
I Full -Service Analytical 8
P R 6 S AAAA
Environmental Solutions 11/12/13
'.- _ —ORATORIE$INC.
City of Statesville, NC Project: Stal-ime Prism Work Order: 3110075
Attn: Andy Smith Time Submitted: 11/5/2013 9:30:OOAM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source °/REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P31<0185 - 3050B
Blank (P3KO185-BLK1)
Prepared: 11/11/13 Analyzed: 11/12/13
Arsenic
BRL
0.26
mg/kg wet
Cadmium
BRL
0.26
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.26
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
BRL
2.6
mg/kg wet
LCS (P3KO185-BS1)
Prepared: 11/11/13 Analyzed: 11/12/13
Arsenic
23.2
0.25
mg/kg wet
24.51 95 80-120
Cadmium
23.3
0.25
mg/kg wet
24.51 95 80-120
Copper
25.9
0.49
mg/kg wet
24.51 106 80-120
Lead
23.8
0.25
mg/kg wet
24.51 97 80-120
Nickel
23.6
0.98
mg/kg wet
24.51 96 80-120 `
Selenium
21.9
0.49
mg/kg wet
24.51 89 80-120
Zinc
22.9
2.5
mg/kg wet
24.51 94 80-120
Batch P31<0193 - 7471 B
Blank (1331<0193-BLK1)
Prepared & Analyzed: 11/11/13
Mercury
BRL
0.019
mg/kg wet
LCS (P3KO193-BS1)
Prepared & Analyzed: 11/11/13
Mercury
0.413
0.018
mg/kg wet
0.3846 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1.8001529-6364 - Fax: [phone] Page 4 of 7

-PRISM
y Full -Service Analytical &
� R I Environmental Solutions
_..- LABORATORIES INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Level II QC Report
11/12/13
Prism Work Order: 3110075
Time Submitted: 11/5/2013 9:30:00AM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3K0105 - NO PREP
Blank (P3K0105-BLK1) Prepared & Analyzed: 11/06/13
% Solids 100 0.100 % by Weight
Duplicate (P3K0105-DUP7) Source: 3110075-01 Prepared & Analyzed: 11/06/13
% Solids 77.5 0.100 % by Weight 76.6 1 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 7

Full -Service Analytical
Environmental Solutionss
LA60RATOFIES INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
11/12/13
Prism Work Order: 3110075
Time Submitted: 11/5/2013 9:30:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3KO129 - NO PREP
Blank (P3KO129-BLK1) Prepared & Analyzed: 11/05/13
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch Initial Final Daterrime
3110075-01 P31<0185 2.02 g 50 mL 11/11/13 0:51
Prep Method: 7471B
Lab Number Batch Initial Final Date/Time
3110075-01 P3K0193 0.57 g 50 mL 11/11/13 12:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6 of 7

„� '�� � � Full -Service Analytical � � OFRECORDCUSTODRECORD�_Pis � I a !7 'i l E:.nvu-oomeni al Solutions PAGE _ of _ QUOTE # TO ENSURE PROPER SULLBNG:
Spv41obiootc Poad 1 P.O. Sox 244.543 , (:fiarlot.e, NO 28224-0543 Project Name:
Phuwl: 704/529.6354 , Fax: [phone] / Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Client Company Name:C : 4v o .5 Cal S,,,, itee *Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or OC Requirements
Report To/Contact Name: A n:i. J r�:-i �
Invoice To:
Reporting Address: 1). o ox ii i
Address:
Od �O �c:51'a �a� HC..
NO NIA
Samples INTACT upon arrival?,,,, E
ON WET ICE? Temp(I-
Received
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?—
CUSTODYSEALSINTACT?
VOLATILES rec'd W/OUT HEADS PACE? _.
PROPER CONTAINERS used?...-._--
Phone:704- V'79- 3'l3 o Fax es (No): %0-/- 5' 7S'- ,yLL,5
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING; PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
q Y Y
Certification: NELAC USAGE FL NC_
EDD Type: PDF_ E)ccel _Other
y//
a a
P
"Working Days” ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
SC OTHER N/A
Site Location Name: 111",r pB C, eek IA) +
Samples received after 15:00 will be processed next business day.
—
Site Location Physical Address: r�� )� rs ✓'�
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— NO
//
S�JJ(
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
�S'C ti ►'"' ive
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
_
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
! \�;% �'
REMARK
LAB
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
*TYPE
TIVES �` ;'
kC ,
NO.
HOURS SLUDGE) SEE BELOW NO. SIZE
�i
61-q9.� Ali % J+ 6 Na r
C2
Sc
Sampler's Signatureia_f Sampled By (Print Name)y'�/ r`�'C K I Affiliation
Upon relinquishing, this Chain of'Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
0
linquished By: (Sign re) - Received'f.7or Prism Laboratories By: I vale
Q Ahod o1 Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC G oup No.
CD SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY. U
0 Fed Ex ❑ UPS ❑ Hand -delivered rism Field Service ❑ Other
DES: I UST: I GROUNDWATER: DRINKING `HATER: SOLID WASTE: RCRA: I CERCLA LANDFILL OTHER:
NC ❑ SCi O NC ❑ SC ❑ 1C ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC: ❑ NC U SC ❑ NC ❑ SC ❑ NC ❑ SC
_ ❑ U -.- ❑ - I ❑ __. . _— ❑ . _ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
fl7. ¢. t_'II Y
Additional Comments:
01
Site Arrival Time:
Site Departure Time:
Field Tech Fee:
Mileage: —
'SEERE'-YERSESFOR,�'�"
T,ERMS�B�CONDi1T,1�0[!�S't

%FI*
Fayetteville Division
2592 Hope Mills Rd
®. Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
City of Statesville
Mr. Andy Smith Project: Sta-lime/Sludge Sample - 4th Creek WWTP
Post Office Box 1111
Statesville NC, 28687-1111
Sta-lime/Sludge Sample, Grab
1310353-01
Date Reported: November 15, 2013
Date Received: October 15, 2013
Date Sampled: October 28, 2013
Sampled By: Andy Smith
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Baltimore Division
Salmonella <0.037 MPN/4g 11/4/13 0:00 BLT EPA 1682
% Solids 70.67 % 10/30/13 0:00 BLT SM 2540 G-1997
QC Duplicate Results
Analyte Result Units Source RPD Lnnit
Salmonella ND MPN/4g 'fnonel 50
Not state certified for testing requested.
State Certifications:
NCDNR # I 1
NCDOH #37714
USDA #3787
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 1 of 1

NC Certification No.Case Narrative
SC Certification No. 990 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735 12/04/2013
AP ISM Environmental Solutions vA Certification No. 460211
LABORATORIES, INC. DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
City of Statesville, NC Project: StaLime
Andy Smith
P.O. Box 1111 Lab Submittal Date: 11/18/2013
Statesville, NC 28687 Prism Work Order: 3110377
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report,
Respectfully,
PRISM LABORATORIES, INC.
V L..
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* . Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This reportshould not be reproduced, except_in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 13

t. Full -Service Analytical &
PRISM I Environmental Solutions
LABORATORIES
INC-
Sample Receipt Summary
12/04/2013
Prism Work Order: 3110377
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Sta-Lime/Fecal #1
3110377-01
Solid
11/18/13
11/18/13
Sta-Lime Fecal] #2
3110377-02
Solid
11/18/13
11/18/13
Sta-Lime Fecall #3
3110377-03
Solid
11/18/13
11/18/13
Sta-Lime Fecall #4
3110377-04
Solid
11/18/13
11/18/13
Sta-Lime Fecal] #5
3110377-05
Solid
11/18/13
11/18/13
Sta-Lime Fecall #6
3110377-06
Solid
11/18/13
11/18/13
Sta-Lime Fecall #7
3110377-07
Solid
11/18/13
11/18/13
Samples were received at 26.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 13

Laboratory ReportFull-Service
t"F
Analytical &
r PRISM IEnvironmental
LABORATORIES INC.
Solutions
12/0412013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime/Fecal #1
Attn: Andy Smith
Prism Sample ID: 3110377-01
P.O. Box 1111
Prism Work Order: 3110377
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter
Result
Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
69.0
% by
0.100
0.100
1 *SM2540 G 11/20/13 17:30 CGP
P31<0444
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 11/19/13 9:30 MES
P31<0437
Total Metals
Mercury
0.13
mg/kg dry
0.029
0.0098
1 *7471B 11/21/13 11:12 MEH
P3K0426
Arsenic
5.1
mg/kg dry
0.36
0.053
1 *6010C 11/27/13 20:02 BGM
P3K0549
Cadmium
BRL
mg/kg dry
0.36
0.0035
1 *6010C 11/27/13 20:02 BGM
P31<0549
Copper
28
mg/kg dry
0.73
0.0092
1 *6010C 11/27/13 20:02 BGM
P3K0549
Lead
8.2
mg/kg dry
0.36
0.043
1 *6010C 12/2/13 23:54 BGM
P3K0549
Nickel
100
mg/kg dry
1.5
0.012
1 *6010C 11/27/13 20:02 BGM
P31K0549
Selenium
BRL
mg/kg dry
0.73
0.088
1 *6010C 11/27/13 20:02 BGM
P31<0549
Zinc
56
mg/kg dry
3.6
0.025
1 *6010C 11/27/13 20:02 BGM
P3K0549
This report should not be reproduced, except in its entirety, without the written consent of Prism. Lagoratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 13

Laboratory Report
ZRRISM
Full-Service Analytical &
Environmental Solutions 12/04/2013
LABORATORIES INC.
City of Statesville, NC Project: StaLime Client Sample ID:. Sta-Lime Fecall #2
Attn: Andy Smith Prism Sample ID: 3110377-02
P.O. Box 1111 Prism Work Order: 3110377
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 68.2 % by 0.100 0.100 1 *SM2540 G 11/20/13 17:30 CGP P31<0444
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/19/13 9:30 MES P31<0437
This report should not be reproduced, except in its entirety, without the written consent of Prism, Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 13

Lab®ratory Rep®rt
Full -Service
'PRISM
Analytical &
/y,-<� Environmental Solutions
/,- � •.,, LABOPnTORIES ING.
12/04/2013
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime Fecall #3
Attn: Andy Smith
Prism Sample ID: 3110377-03
P.O. Box 1111
Prism Work Order: 3110377
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter
Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
General Chemistry Parameters
Solids
69.1 % by 0.100
0.100 1 'SM2540 G 11/20/13 17:30 CGP P3K0444
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry 0.3
1 'SM9221 E 11/19/13 9:30 MES P31<0437
This,report should„not be reproduced, except in its entirety, without
the written consent of Prism Laboratories, Inc,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
e
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 13

li Full -Service Analytical s
Environmental Solutions
�'. ueoantoaiEs wc.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
12/04/2013
Client Sample ID: Sta-Lime Fecal] #4
Prism Sample ID: 3110377-04
Prism Work Order: 3110377
Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 68.0 % by 0.100 0.100 1 `SM2540 G 11/20/13 17:30 CGP P31<0444
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/19/13 9:30 MES P31<0437
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 13

`-1 Full -Service Analytical &
Environmental Solutions
�- LABORATORIES INC.
City of Statesville, NC
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Laboratory Report
12/04/2013
Project: Stal-ime Client Sample ID: Sta-Lime Fecall #5
Prism Sample ID: 3110377-05
Prism Work Order: 3110377
Sample Matrix: Solid Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 69.0 % by 0.100 0.100 1 'SM2540 G 11/20/13 17:30 CGP P31<0444
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 'SM9221 E 11/19/13 9:30 MES P3K0437
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc... _.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 1�

r� R 1 S M
Full-Service Analytical 8Environmental Solutions
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687 Sample Matrix: Solid
Laboratory Report
12/04/2013
Client Sample ID: Sta-Lime Fecal[ #6
Prism Sample ID: 3110377-06
Prism Work Order: 3110377
Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 68.5
% by
0.100
0.100 1
*SM2540 G 11/20/13 17:30 CGP
P3K0444
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 11/19/13 9:30 MES
P31<0437
This report should not be reproduced, except -in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 13

rf' P R I S m
FullService Analytical
(/P�JEnvironmental Solutions
!- LABORATORIES INC.
Laboratory Report
12/04/2013
City of Statesville, NC Project: Stal-ime Client Sample ID: Sta-Lime Fecall #7
Attn: Andy Smith Prism Sample ID: 3110377-07
P.O. Box 1111 Prism Work Order: 3110377
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 11/18/13 11:50
Time Submitted: 11/18/13 16:20
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Solids 69.7 % by 0.100 0.100 1 `SM2540 G 11/20/13 17:30 CGP P31(0444
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 'SM9221 E 11/19/13 9:30 MES P31<0437
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 Of 13

r Full -Service Analytical &
(/J*r P ' Environmental Solutions
/_� .- LABORATORIES. INC.
City of Statesville, NC Project: Stal-ime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Level II QC Report
1214/13
Prism Work Order: 3110377
Time Submitted: 11/18/2013 4:20:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P31<0426 - 7471 B
Blank (P3K0426-BLKI)
Prepared: 11/20/13 Analyzed: 11/21/13
Mercury
BRL
0.021
mg/kg wet
LCS (P3K0426-BS1)
Prepared: 11/20/13 Analyzed: 11/21/13
Mercury
0.448
0.019
mg/kg wet
0.3968 113 80-120
Batch P31<0549 - 3050B
Blank (P3K0549-BLK1)
Prepared: 11/26/13 Analyzed: 11/27/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3K0549-BSI)
Prepared: 11/26/13 Analyzed: 11/27/13
Arsenic
23.4
0.25
mg/kgmg/kg wet
24.75 94 80-120
Cadmium
19.8
0.25
mg/kg wet
24.75 80 80-120
Copper
24.2
0.50
mg/kg wet
24.75 98 80-120
Lead
21.8
0.25
mg/kg wet
24.75 88 80-120
Nickel
22.6
0.99
mg/kg wet
24.75 91 80-120
Selenium
23.5
0.50
mg/kg wet
24.75 95 80-120
Zinc
23.2
2.5
mg/kg wet
24.75 94 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax:.[phone]
Page 10 of 13

Level II QC Report
"' P R 9 I Full -Service Analytical 12/4l13
Environmental Solutions
LABORATORIES. INC.
City of Statesville, NC Project: StaLime Prism Work Order: 3.110377
Attn: Andy Smith Time Submitted: 11/18/2013 4:20:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P31<0444 - NO PREP
Blank (P3K0444-BLK1) Prepared & Analyzed: 11/20/13
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. _
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 13

Level II QC Report
P I S Full -Service Analytical 12/4/13
/
%f Environmental Solutions
LABORATORIES INC.
City of Statesville, NC Project: StaLime Prism Work Order: 3110377
Attn: Andy Smith Time Submitted: 11/18/2013 4:20:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3KO437 - NO PREP
Blank (P3KO437-BLK1) Prepared & Analyzed: 11/19/13
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Datef'rime
3110377-01 P31<0549 1.99 g 50 mL 11/26/13 11:00
3110377-01 P3K0549 1.99 g 50 mL 11/26/13 11:00
Prep Method: 7471B
Lab Number Batch Initial Final Daterrime
3110377-01 P3K0426 0.6 g 50 mL 11/20/13 9:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 12 of 13

PRISIM,
F.11-Service Analytical 8, CHMN F CUSTODY RECORD
IEnuironment3l Solutions PAGE _ OF _ d8f00YE N Y® ENSURE PROPER ®9LLYddG:
_-, UABORATOnIE& INC.
449 Spr€ngbrook' Road = P.O. Box 240543 - Charlotte, NO 28224-0543 Project Name:
P bare:: 704/529-6364 Sax: 704/5.25-0409 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
Client Company Name: CA V lit *Please ATTACH any project specific reporting (QC LEVEL 111 Ill IV)
{� provisions and/or OC Requirements
(Report To/Contact Name.. -in9, '�'�)� Invoice To:
(Reporting Address: 1, R`';; a d d tr tl
Address:
��:.` NO N/A
Samples INTACT upon
Received ON WET ICE? Temp C �`•� �� _ _—
PROPER PRESERVATIVES indicated? _
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?',
VOLATILES rer,'d W/OUT HEADSPACE?
PROPER CONTAINERS used?_—.--
Phone:70`4 - 31 T- q 3F Fax es (No):70?- O °3' �� `� `> Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address Requested Due Date U 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC_
EDD Type: PDF__ Excel _Other_. "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
ar v +-1 (> rt�t', CSy % � Proved SC OTHER N/A
Site Location Name: _ Samples received after 15:00 will be processed next businesss day.
Site Location Physical Address: �� e' �a °'r'° Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES— NO —
Site
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection. YES _ NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- *°" j `0� ' LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE TIVES REMARKS ID NO.
HOURS SLUDGE) SEE BELOW NO. SIZE
— �G3 _
/
Sampler's Signatures r L r -1 z�'T: Sampled By (Print Name) /' r `' '} C Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Reli fished By: (Signsturo) r J /) v Rerveiv ppd By: (Signa/tyLJ�) Da%�(e M,i}litai
Relinq By: (Signature) ._,,i /• �° .F .,y• �"'y" '" '
ling i y: (Signature) Receive or Prism Laboratorie By: ;" Date
-J
ethod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITHICUSTODY SEALS FOR TRANSPOR ATION TO THE LABORATORY. COC Group No.
(D SAMPLES ARE NOT AC EPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. Y-F•-
� 4
W Fed Ex ❑ UPS ❑ Hand -delivered P ism Field Service ❑ Other
0 PDES: UST: GR UNDWATER: DRINKING WATER: I SOLID WASTE: RA: CERCLA LANDFILL OTHER:
w NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC p SC ❑ NC U SC ❑ NC ❑ SC
ONTAINER TYPE CODES: A = Amber C = Clear 6 = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
Additional Comments:
Site ArrivalTime:
Site Departure Time:
Field Tech Fee:

X�/' ISM I Full -Service Analytical &
/' Environmental Solutions
PR
/;,�• LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinkinq Water Cert No. 37735
VA Certification No. 460211
DOD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 12/04/2013
Prism Work Order: 3120083
Case Narrative
12/12/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Steven H. Guptill For Robbi A. Jones
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Pagel o

!! P R I S Full -Service Analytical
{4° Environmental Solutions
-
LABORATORIES. INC.
Sample Receipt Summary
12/12/2013
Prism Work Order: 3120083
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3120083-01 Solid 12/04/13 12/04/13
Samples were received in good condition at 4.3 degrees C unless otherwise noted.
This report should not, be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
f'P I Full -Service
Analytical
12/12/2013
/ Environmental Solutions
/.:... ' LAROPATORIES ING
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Prism Sample ID: 3120083-01
Attn: Andy Smith
Prism Work Order: 3120083
P.O. Box 1111
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/04/13 12:17
Time Submitted: 12/04/13 16:45
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
70.3
% by
0.100
0.100
1 *SM2540 G 1216/13 16:00
MJO
P31-0183
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 12/5/13 12:10
MES
P3L0169
Total Metals
Mercury
0.13
mglkg dry
0.030
0.010
1 *7471B 12/9113 14:56
MEH
P31-0177
Arsenic
5.0
mglkg dry
0.35
0.051
1 *6010C 12/10/13 0:04
BGM
P31-0156
Cadmium
BRL
mg/kg dry
0.35
0.0033
1 *6010C 12/10/13 0:04
BGM
P31-0156
Copper
28
mg/kg dry
0.69
0.0087
1 *6010C 12/10/13 0:04
BGM
P31-0156
Lead
8.2
mg/kg dry
0.35
0.041
1 *6010C 12/10/13 0:04
BGM
P31-0156
Nickel
100
mg/kg dry
1.4
0.011
1 *6010C 12/10/13 0:04
BGM
P31-0156
Selenium
BRL
mg/kg dry
0.69
0.084
1 *6010C 12/10/13 0:04
BGM
P31-0156
Zinc
50
mg/kg dry
3.5
0.024
1 *6010C 12/10/13 0:04
BGM
P31-0156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 7

Level II QC Report
I S M I Full -Service Analytical & 12/12/13
1rl Environmental Solutions
_.-T.-s' .-
City of Statesville, NC Project: StaLime Prism Work Order: 3120083
Attn: Andy Smith Time Submitted: 12/4/2013 4:45:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3LO156 - 3050B
Blank (P3L0156-BLK1)
Prepared & Analyzed: 12/09/13
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.49
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.98
mg/kg wet
-
Selenium
BRL
0.49
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P3L0156-BS1)
-
Prepared & Analyzed: 12/09/13
- -- - -
Arsenic
9.30
0.26
mg/kg wet
10.26 91
80-120
Cadmium
9.56
0.26
mg/kg wet
10.26 93
80-120
Copper
10.4
0.51
mg/kg wet
10.26 101
80-120
Lead
9.82
0.26
mg/kg wet
10.26 96
80-120
Nickel
9.63
1.0
mg/kg wet
10.26 94
80-120
Selenium
8.95
0.51
mg/kg wet
10.26 87
80-120
Zinc
9.36
2.6
mg/kg wet
10.26 91
80-120
Batch P311_0177 - 7471 B
Blank (P3L0177-BLK1)
Prepared & Analyzed: 12/09/13
Mercury
BRL
0.020
mg/kg wet
Prepared & Analyzed: 12/09/13
LCS (P31-0177-113SI)
Mercury
0.447
0.020
mg/kg wet
0.4098 109
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 �
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] I Page 4 of 7

i- Full -Service Analytical &
fl P RI BORATORM
Environmental Solutions
��-
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters -(duality Control
Level II QC Report
12/12/13
Prism Work Order: 3120083
Time Submitted: 12/4/2013 4:45:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P31-0183 - NO PREP
Blank (P3LO183-BLK1) Prepared & Analyzed: 12/06/13
Solids 99.9 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 7

Level II QC Report
'Y
Full -service Analytical &
12/12/13
� I Environmental Solutions
LABORATORIES INC
City of Statesville, NC
Project: StaLime Prism Work Order: 3120083
Attn: Andy Smith
Time Submitted: 12/4/2013 4:45:OOPM
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3LO169 - NO PREP
Blank (P3LO169-BLK1)
Prepared & Analyzed: 12/05/13
Fecal Coliforms
BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050E
Lab Number Batch
Initial Final Date/Time
3120083-01 P31-0156 2.05 g 50 mL 12/09/13 9:30
Prep Method: 7471B
Lab Number Batch Initial Final Date/Time
3120083-01 P31-0177 0.56 g
50 mL 12/09/13 12:05
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 7

CHAIN F CUSTODY RECORD
Fu11ervie Analytical &P I,� Solutions PAGE _ Or- QUOTE 0 TO ENSURE PnOPEi <QOLLING:
uA1,30RA10tacs INC.
44 `;(,1 gbr, ,k Road ^ P-0. 'Box a4O543 ^ CiaaaJoite, rJC 28224-0543
Project Name:
phonn; 04/52J-6364 fax: [phone] Short Hold Analysis: (Yes) (NO) UST Project: (Yes) (No)
r �>� *Please ATTACH any project specific reporting (QC LEVEL I li III IV)
Client Company Name: C4, d , `r �' t'
P` y �- provisions and/or QC Requirements
Report To/Contact Name. A :, , S o-,7 A h
Invoice To:
Reporting Address: ' 113 o x 36 6 S Address:
YES NO .
N/A.
Samples INTACT upon arrival? t(, j p
v�
p
Received ON WET ICE? Temp _',_ _ ✓ _
,. —
ti
PROPER PRESERVATIVES indicated? __
._._
Received WITHIN HOLDING TIMES?
--
-._
CUSTODY SEALS INTACT?_—
VOLATILES lead W/OUT HEADSPACE?.
PROPER CONTAINERS used?--
It�'r�- 8'7b"- 3`/ 'Far, es (No):'� - � 5' TO DE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Phone: Purchase Order No./Billing Reference
Email (Yes) (No) Email Address Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC
EDD Type: PDF_ Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
�t C'r ��` dkc L� T Pre -Approved $C OTHER N/A
Site Location Name: � 'J � ' _ _ d Samples received after 15:00 will be processed next business day. —
Site Location Physical Address: L'� 0° G'� 4 °� Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES — NO
��
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES _ NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED PRISM
CLIENT DATE COLLECTED (SOIL, PRESERVA- LAB
S� yb REMARKS
COLLECTED MILITARY WATER OR *TYPE TIVES ID NO.
SAMPLE DESCRIPTION
HOURS SLUDGE) SEE BELOW NO, SIZE.
id-q- J3 M ' 1 -7 P
T7FT
Sampler's Signature 1 = � r' � Sampled By (Print Name) tr to r Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the dnalyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be arges for any changes after analyses have been initialized.
Rellnpuished By: (Signature) , Recei ed By: (Si t e D to Mili)tyary�/LHours Additional Comments:
R&&ga By: (Signal r Dale
Relic 4tfi5fied By: (Signalur Recelved 9Prism LaboralOZ.Date
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT -CUSTODY SEALS FOR TR ORTATION TO E LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST jdC UNTIL RECEIVED AT THE L ORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered rism Field Service O Other
NPDES: j UST: I GR DWATER: DRINKING WATER: I SOLID WASTE: �RCRA: CERCLA LANDFILL OTHER:
❑NC CSC❑NC ❑SC ❑ C ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC :SC ❑NC ❑5CI ❑NC ❑SC ❑NC ❑SC
❑ ❑ ❑ -. ❑ .- . — ❑ ❑ ❑ - ❑ - ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

I I Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Project: StaLime
Lab Submittal Date: 12/16/2013
Prism Work Order: 3120307
Case Narrative
12/23/2013
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 7

Sample Receipt Summary
P R I S I Full -Service Analytical 12/23/2013
Environmental Solutionss
LABORATORIES INC.
` Prism Work Order: 3120307
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Sta-Lime 3120307-01 Solid 12/16/13 12/16/13
Samples were received at 18.5 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 7

Laboratory Report
Full -Service
Analytical &
12/23/2013
/FRISRIE$I�IC. Environmental
Solutions
City of Statesville, NC
Project: StaLime
Client Sample ID: Sta-Lime
Attn: Andy Smith
Prism Sample ID: 3120307-01
P.O. Box 1111
Prism Work Order: 3120307
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 12/16/13 11:05,
Time Submitted: 12/16/13 14:50
Parameter
Result Units
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
Solids
65.3
% by
0.100
0.100
1 *SM2540 G 12119/13 16:05
MJO
P31-0370
Weight
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1 *SM9221 E 12/17/13 11:00
MES
P31-0345
Total Metals
Mercury
0.11
mglkg dry
0.033
0.011
1 *7471B 12/18/13 13:30
MEH
P31-0316
Arsenic
5.2
mg/kg dry
0.38
0.055
1 *6010C 12/18/13 19:45
BGM
P31-0315
Cadmium
BRL
' mg/kg dry
0.38
0.0036
1 *.6010C 12/18/13 19:45
BGM
PK0315
Copper
30
mg/kg dry
0.75
0.0095
1 *6010C 12/18/13 19:45
BGM
P3L0315
Lead
8.3
mg/kg dry
0.38
0.044
1 *6010C 12/18/13 19:45
BGM
P31-0315
Nickel
110
mglkg dry
1.5
0.012
1 *6010C 12/18/13 19:45
BGM
P31-0315
Selenium
BRL
mg/kg dry
0.75
0.091
1 *6010C 12/18/13 19:45
BGM
P31-0315
Zinc
52
mglkg dry
3.8
0.026
1 *6010C 12/18/13 19:45
BGM
1331-0315
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 7

Level II QC Report
,T ISM I Full -Service Analytical & 12/23/13
Environmental Solutions
�_�. LA©ORATORIES ING
City of Statesville, NC Project: Stal-ime Prism Work Order: 3120307
Attn: Andy Smith Time Submitted: 12/16/2013 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P311-0315 - 3050B
Blank (P3L0315-BLK1)
-
Prepared .& Analyzed: 12/18/13
Arsenic
BRL
0.26
mg/kg wet
Cadmium
BRL
0.26
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.26
mg/kg wet
Nickel
BRL
1.0
mg/kg wet
Selenium
BRL
0.51
mg/kg wet
Zinc
IBRL
2.6
mg/kg wet
LCS (P3LO315-BS1)
Prepared & Analyzed: 12/18/13
Arsenic
21.1
0.25
mg/kg wet
24.63 86
80-120
Cadmium
19.9
0.25
mg/kg wet
24.63 81
80-120
Copper
23.1
0.49
mg/kg wet
24.63 94
80-120
Lead
20.4
0.25
mg/kg wet
24.63 83
80-120
Nickel
21.0
0.99
mg/kg wet
24.63 85
80-120
Selenium
20.3
0.49
mg/kg wet
24.63 82
80-120
Zinc
21.0
2.5
mg/kg wet
24.63 85
80-120
Batch P31L0316 - 7471 B
Blank (P3L0316-BLK1)
Prepared & Analyzed: 12/18/13
Mercury
BRL
0.021
mg/kg wet
LCS (P311-0316-113SI)
Prepared & Analyzed: 12/18/13
Mercury
0.460
0.020
mg/kg wet
0.4237 109
80-120
This repbrt should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 7

Level II QC Report
// f' Full -Service Analytical & 12/23/13
f,.t P Environmental Solutions
�T_.....-- LA00PATORIES INC.
City of Statesville, NC Project: StaLime Prism Work Order: 3120307
Attn: Andy Smith Time Submitted: 12/16/2013 2:50:OOPM
P.O. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P31LO370 - NO PREP
Blank (P31-0370-BLK1) Prepared & Analyzed: 12/19/13
% Solids 100 0.100 % by Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 7

: t P R I S I Full -Service Analytical
YNEnvironmental Solutions
LABORATORIES INC.
City of Statesville, NC Project: StaLime
Attn: Andy Smith
P.O. Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Level II QC Report
12/23/13
Prism Work Order: 3120307
Time Submitted: 12/16/2013 2:50:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P3L0345 - NO PREP
Blank (P3L0345-BLK1) Prepared & Analyzed: 12/17/13
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
3120307-01
P31-0315
2.03 g
50 mL
12/18/13 9:00
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Daterrime
3120307-01
P31-0316
0.55 g
50 mL
12/18/13 9:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 7

CAO OF CUSTODY RECORD
a.,.
��a,
a
I Full -Service Analytical :?•
F� z
YES NO NIA
i_nvironmental Solutions
PAGE _ OF _ OUOTU Jl TO ENSURE PROPER BILLONO:
Samples INTACT upon arrival?
_� ._.._ _ ---------
i
LAP.OR VORIFS, INC.
Received ON WET ICE?: Temp
„i �rrinc}kro<?fc Roadn P.O. Box 7_40543 = Charlotte, NC 28?.21-0!343
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
PROPER PRESERVATIVES indicated?
Phone: 7L'4/c:29-6364 Fax: [phone]
Received WITHIN HOLDING TIMES?
Client Company Name: C , 4 o Ea r".5 a'r c'
'`Please ATTACH any project specific reporting (QC LEVEL 1 11 111 M
CUSTODY SEALS INTACT?
—�
1cw� �t
provisions and/or LAC Requirements
V LATILES rec'd W/OUT HEADSPACE?
`-
Report To/Confect Name: �
Reporting Address: `� • ' 1 j B
Invoice To:
ROPER CONTAINERS use
-
Address:
Phone- i` � 7�- 3ti3 � Fax �'es (No): %°� purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email (Yes) (No) Email Address
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification. NELAC USACE FL NC_
EDD Type: PDF_ Excel _Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be
Pre -Approved
Sc OTHER N/A
Site Location Name: ro'.t ere e CA W L-. i T P Samples received after 15:00 will be processed next business day.
Site Location Physical Address: 3 W& F Turnaround time is based on business days, excluding weekends and holidays.
Wafer Chlorinated: YES _ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT}
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES
REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
/ O� ;' /%
' REMARKS
LAB
'TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
�r
k� ,%
ID NO.
J HOURS SLUDGE) SEE BELOW NO. SIZE �Z j g�
i
Seal-f,'n-1e /d -/d-i 3 100,5 S N� s � ;.
_
Pb
N�
ZN
Sampler sSignature /IJ G Sampled By (Print Name) n c�'a'r l c' 1G Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
Reliioished By: (Signature) R' ' ed By: (nature) /�✓ Date / Militai
By: (Signature)
linquish B y: (Signature) Ffecdtive r Prism Labor ,bytes by:
I tea•=
1r/%�— — L
3: ( Te
Additional Comments
Site Arrival Time:
Site Departure Time:
Field Tech Fee:
Miloage:
thod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WI-
CUSTODY SEAS FOR TRANSPORTATION TO THE LABORATORY.
COC Group No.
Cn
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CO
UNTIL RECEN60 AT THE LABORATORY.
/
v
Fed Ex ❑ UPS 7 Hand -delivered Prism Field Service ❑ Other
DES:
UST: i GR UNDWATER:
DRINKING WATER:
SOLID WASTE: RCRA:
CERCLA
LANDFILL
OTHER:
v
NC ❑ SC
❑ NC ❑ SC ' ❑ C ❑ SC
❑ NC ❑ SC
❑ NC ❑ SC ❑ NC ❑ SC
❑ NC ❑ SC
❑ NC ❑ SC
I [aNC ElSC
--❑ —._I❑ -. ❑
ONTAINER TYPE CODES: A = Amber C = Clear G = Glass
-- ❑_... _. ❑ ❑ ❑ ❑ _
P = Plastic; TL = Teflon -Lined Cap VOA Volatile Organics Analysis (Zero Head Space)

City Of Statesville Alkaline Stabilization Record For
. Process To .Further Reduce Pathogens (PFRP)
BIN # 5
Setup Date: 1- 3 0 - 13
Removal From Bin Date: ,2-1-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1- 30 - 13
10: 0 0
Initial PH: la, 69
5�
Q� W
Corrected PH: 13 4 �2 (?)
a-1-13
11:45Aol
Final PH: 12. 4 0
d5
R l,W
Corrected PH:Ia1•`1a
Has 72 Hour & PH Criteria Been Met? Y N
BIN # $
Setup Date: d - 5-13
Removal From Bin Date: d- 8-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
-5-13
11'00
Initial PH: la. 61
800
RAW
Corrected PH: 1a.7$
-13
19: o o
Final PH: Id .70
8
w
Corrected PH: 1 �2 . 816
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 3- 9-13
Removal From Bin Date: 3--11-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3- 2-13
1` 15 �`�
Initial PH: 12,73
goo
pow
Corrected PH: I;1,9.3
3 - li -13
a f "''
Final PH: 1�,$3
®
R
Corrected PH: i3; 0 3
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date: 3 -It
-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3 13-1'�
Q Am
Initial
Initial PH: /2. 7
q 00
RW
PH: 11.1
3 -/ $- /3
P+�1
Final PH: 1,1,
R
Corrected PH: 12. q7
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 3-1y-13
Removal From Bin Date: 3a1q-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
-1�-1�
pM
InitialPH: Ia•85
0
PAW
Corrected PH: 13,0 1
3- l"i-13,
I FM
Final PH: 1;l•93
goo
RkW
Corrected PH: 13,`
Has 72 Hour & PH Criteria Been Met? UY N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: )- I)-)3
Removal From Bin Date: % - /y- /3
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1- )1- 11
1 N : i
Initial PH:
Corrected PH:
-lu- 13
U?:3?
Final PH:
0
4
%films
Corrected PH: )a.'7�^
Has 72 Hour & PH Criteria Been Met? ® N
BIN # S
Setup Date: I-/y-/s
Removal From Bin Date: i- / 7- /3
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
j- ) y-12
Initial PH: )a,&o
b
a LW
Corrected PH: , p
b �; �j p
Final PH: la,-70
10,
Corrected PH: l a, 9U
Has 72 Hour & PH Criteria Been Met? N
BIN # (
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: Io2t�oU
c
A L Ld
Corrected PH: j, 4f U
- jV- Is
I y:00
Final PH: (�, 7U
g L t,,c)
Corrected PH: ),1 , R7
Has 72 Hour & PH Criteria Been Met? O N
BIN # S
Setup Date: /)
Removal From Bin Date: /,- ,3
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
f, 13
; dS
Initial PH: (a I . -a
� b
Corrected PH: la,
�31-13
) : 10
Final PH: 12,61
Corrected PH: 1,21 7
Has 72 Hour & PH Criteria Been Met? Y N
BIN # z {
Setup Date: I-) V- I -b
Removal From Bin Date: I - 31- 13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
}
`
Initial PH: la, (p
L W
Corrected
orrected PH: 1 /
a'�' )3
) 2.'q a
Final PH: a ,-7
( 0
R Ltd
Corrected PH: j '� .,yi
Has 72 Hour & PH Criteria Been Met? N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # y
Setup Date: 3 - I g - 13
Removal From Bin Date: 3- a 1-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3- I$-13
I ON 5
Initial PH: 12.11
q 0
Corrected PH: 1,2, S 8 3
-a l-�3
I o ®S
Final PH: I a.'?Q
Rim
Corrected PH: i2. qg
Has 72 Hour & PH Criteria Been Met? N
BIN # 3
Setup Date: 3- a0- 13
Removal From Bin Date: 3-aa-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
^i3
Initial PH: 1a•IY3
170
Corrected PH: j,J.Qq
Final PH: 1 a .q
90
�� w
Corrected PH • 13,,
Has 72 Hour & PH Criteria Been Met? UY N
BIN # $
Setup Date: 3-a 7-13
Removal From Bin Date: y- I- 13
Date
Time
I PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-� 7-I 3
1' 3�
Initial PH: iA.'%
90
�� 1�
Corrected PH: , Q
-1-13
P"�
Final PH: / 2 .
O
�`
Corrected PH: l�.qq
Has 72 Hour & PH Criteria Been Met? UY N
BIN #
Setup Date: 5-,A?-)3
Removal From Bin Date: 9- /- 13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-27-13
1 3®
Initial PH: I�2 .']
4 ®
i VV
Corrected PH: Ia,
Final PH: 141. Ir
n 0
`�
Corrected PH: I ,2.c? q
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: y- y-13
Removal From Bin Date: il-
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 12.1-3
O
Corrected PH: 1A , 83
14-t013
a Pm
Final PH: ja,73
0
RAW
Corrected PH: I V? 3
Has 72 Hour & PH Criteria Been Met? - Z N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: 4-11-13
Removal From Bin Date: q-1-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
q-II- 3.
1 30 Pin
Initial
Initial PH: U. 63
0
RR
PH: IA.83
4-11-13
S A•n
Final PH: 1,Z.13
0 0
Corrected PH: 1.I.43
Has 72 Hour & PH Criteria Been Met? Y N
BIN # .3
Setup Date: Ll-1a-13
Removal From Bin Date: Ll-15-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Y-/1-/3
/1 P>» a
Initial PH: /2,73
100
R4 W
Corrected PH: /a. 93
y-1�-13
Am
Final PH: 171.33
900
Rl>�
Corrected PH: 12.9 9
Has 72 Hour & PH Criteria Been Met? Y N
BIN # y
Setup Date: 1- I4-13
Removal From Bin Date: 4-A A-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
4-0-13
'Z Pm
Initial PH: 12.87
90
�/` W
Corrected PH: 13.0
4-.Ia-13
a:3oPM
Final PH: 1�.47
�
9 0
Rlr v�1
Corrected PH: I Z
Has 72 Hour & PH Criteria Been Met? CY) N
BIN #
Setup Date: y-dal- 13
Removal From Bin Date: cl-iag -13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
y-as-t_3
11 Am
Initial PH: / g3
900
R�z�
Corrected PH:13,03
o7%y7PM
Final PH: 1,2,q
Q�%O
R4
Corrected PH: 1�3y 1
Has 72 Hour & PH Criteria Been Met? CY) N
BIN # 3
Setup Date: °(-ay-13
Removal From Bin Date: 14-2 -13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�: �� pen
Initial PH: l a , (
900
Rkw
Corrected PH:
y -a9-13
7:15A �"�
Final PH: I;A,7 _:T_
90
Corrected PH: Ia, 8 9
Has 72 Hour & PH Criteria Been Met? =N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 4
Setup Date: 4-ay-1,3
Removal From Bin Date: y-a ,iI3
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 1;1, 4
n 00
�i
Corrected PH: jj. 8,
Final PH: 12,-1
0
Q
R�
Corrected PH: j,?, '9
Has 72 Hour & PH Criteria Been Met?. UY N
BIN # 5
Setup Date: Y 30 -1 3
Removal From Bin Date: 5- 2-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg: C For 12 Hrs.
Operator
4-30-/
.3
jn7:`��
Initial PH: la, %
q0 0
Rl w
Corrected PH: 12, 9
G-
/0 . it
Final PH: 12,
0
�o
Corrected PH: 11.g9
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: y- 3o-V 3
Removal From Bin Date: 5- 2.13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 12 , 7
` 0
Corrected PH: la, 9
PH: Ll.�orrected
% o
R k w
[Final
PH: 1 j .4 9
Has 72 Hour & PH Criteria Been Met? Y N
BIN # I
Setup Date: ► 3
Removal From Bin Date: S /143
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 12.75
o
Corrected PH: 11,9
%o o
Final PH: /4, Sr
(70
Corrected PH: 1d , 415
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 3
Setup Date: .'"-a?0-l_3
Removal From Bin Date: 5-23-13
l Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
2,0 -13
Of PM
Initial PH: 11. 5 11
700
Rol w
Corrected PH: 1 a,? 1
b - a3-Ij
2:45Pin
Final PH: 1,�,(y
v
70
[Corrected PH: 12.78
Has 72 Hour & PH Criteria Been Met? nY N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # Y
Setup Date: S-2a-13
Removal From Bin Date:5-a3- 13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: Ia . _5
QOO
Rkw
Corrected PH: 12.7
PH: I�.9
®inal 0
rCorrected PH: 1.1
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 1;
Setup Date: 5- a$-1.3
Removal From Bin Date: 5-31-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
`� ��`�
Initial PH: /,2, 5
900
RA, W
Corrected PH: /a,
y-3/-I3
i Pm
Final PH:
q0 6
R/,w
Corrected PH: 12.8
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 7
Setup Date: 5- 3 0 -13
Removal From Bin Date: -13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
S- 30 -13.
a : to PM
Initial PH: 0 . 5
9 0 9
14 W
Corrected PH: la .
1�:5o Ann
Final PH: Ia.,6
q0,
R h VV
Corrected PH: 1 a. 8
Has 72 Hour & PH Criteria Been Met? Y N
BIN # $
Setup Date: 5 31-13
Removal From Bin Date: 4- 1-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
S 3/-13
1 1''"�
Initial PH: �,�,6
t-,
! 5,0
R 1nI
Corrected PH: 11.7
6- y i3
11: 5� AA
Final PH: /a .. i/
75
Corrected PH: /,2, Y 3
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 4 • /0 -13
Removal From Bin Date: 5-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
1-3
P
Vq0A1
Initial PH: 11,�a
Corrected PH: 12, VI
-/?-13
A
%� 1 a m
Final PH: 1,7a
o
9 0
R 1v w
Corrected PH: 1j. q I
Has 72 Hour & PH Criteria Been Met? Y N

,City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN # 3
Setup Date:-%/-13
Removal From Bin Date: 1.-1�=13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
�!-l3
Initial PH: 12.79
O
q®
Rmv
Corrected PH: 12,9A
p
/0„"
Final PH: 1 a ,$
Corrected PH: 12 .Q q I
Has .72 Hour & PH Criteria Been Met? N
BIN # =i
Setup Date: i- CA-13
Removal From Bin Date: 6-15-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: 11.83
900
RAW
Corrected PH: 12 , 9 9
1-/7/3
A
7`-Z0r^
Final PH:
®
R4 t-'`
Corrected PH: I3,OJi
Has 72 Hour & PH Criteria Been Met? [YTN
BIN # F
Setup Date: 6..Aq-/3
Removal From Bin Date: 6- a7-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
y_,
-a 3
a P m
Initial PH: ia,53
a
PAW
Corrected PH: 1a, 73
Final PH: 12, g 3
Corrected PH: 1,243
Has 72 Hour & PH Criteria Been Met?
VY N
BIN # 7
Setup Date• 025.-/ 3
Removal From Bin Date: d 9Y-13
,Date
Time
PH. >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
62543
�`�
Initial PH: 0.53
`70�
��
Corrected PH: 1a.7.3
Final PH: 12.e3
0
Corrected PH: 12.E 3
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: 9-Ll-13
Removal From Bin Date: 9-7-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Q-4-13.
in:30ri
Initial PH: 12. L15
�0o
RAW
Corrected PH: 11.15
9- 9-1�
,'�03er1
Final PH: 11, 1
90o
Corrected PH: � 1,2,
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date: 10-5-13,
Removal From Bin Date: )o -11-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-�- J3
f3: �3
Initial PH: 19.7
90
Corrected PH: 12, 8q
10-1,V 13
67'1 ¢
Final PH: 1 � . 8
90 ®
?t w
Corrected PH: 12. q7
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 0
301
ISetup Date: 10- `d -1.3
Removal From Bin Date: i d -13^ 13
Date
Time
I PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH: la, R
Q'0
Corrected PH: 13,a
i0-14-13
4:dS
Final PH: l a , 9
o
Corrected PH: 13,
Has 72 Hour & PH Criteria Been Met?
fY N
BIN # 5
Setup Date: /0 - /y-13
Removal From Bin Date: /0-1 `i-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-I�1-13
13:4
Initial PH: jA, 7A
9 �a
��
Corrected PH: I2,9
/0 - �b �3
a I'M
Final PH: �a•$�
0
��
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN # oo
Setup Date: /0- 2q-13
Removal From Bin Date: 1/-/-13
Date
Time
. PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
to-a-13
/ P n
Initial PIS: 14 7
q 0 d
`RAW
Corrected PH: 1I.f9
a; 3o prn
Final PH: Q. 9
p
6
R4 �
Corrected PH: 1219
Has 72 Hour & PH Criteria Been Met? N

City Of Statesville Alkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
.BIN # o 7
Setup Date: 10- 30-3 3
Removal From Bin Date: 11-a - 13
Date
Time
IPH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-30-13
.d '
Initial PH: 12 7
0
90
Rkw
Corrected PH:1�. 83
Final PH: 1.1 , k
7011
Corrected PH: 14.99
Has 72 Hour & PH Criteria Been Met? UY N
BIN # 6
Setup Date: 11-4-13,
Removal From Bin Date: 11- 7- 13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
11-y-13
j� 5a P
Initial PH: la, 9
o
q Q
RAW
Corrected PH: Id, 89
3
/: /sue
Final PH:
lCorrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 5
Setup Date: JI-$-13
Removal From Bin Date: j/- ,?-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
q
®9. dl*4
Initial PH: 12. Si
o
®
R���
Corrected PH: 13,0
Final PH: /;2A
ffo o
��
Corrected PH: /3,
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
q
Setup Date:
Removal From Bin Date: /1--9-13
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
11-6-13
Initial PH: 1 �2 , '71
900
Corrected PH: 1 a.• `i
Final PH: /a e Ir
0 G o
R� W
Corrected PH: /W, 9
Has 72 Hour & PH Criteria Been Met? Y N
BIN # 8
Setup Date: If /3
Removal From Bin Date: /J- / q- / 3
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
A Pr'7
Initial PH: /�. Y,5
t� o 0
`7
%P.� 1n1
Corrected PH: i3,0
il- 1 b -13
04:db'i�
Final PH: /,�,q
®
R4 IV
Corrected PH: 13 0
Y N
Has 72 Hour & PH Criteria Been Met? Qj

City Of StatesvilleAlkaline Stabilization Record For
Process To Further Reduce Pathogens (PFRP)
BIN #
Setup Date: 13
Removal From Bin Date: j/-,�J_ /
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
//
Initial PH: /,?, L73
a
90
RA LQ
Corrected PH: /3 j
Final PH: 13, 0
3 ®d
RA �
Corrected PH: 13.2
Has 72 Hour & PH Criteria Been Met? ® N
BIN # `%
Setup Date: )a- j`%- 1,3
Removal From Bin Date: 1q-;Z 0- 1'S
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
iaI?-13
!0"`n
Initial PH: /Z 11
goo
R� w-
Corrected PH: 1.2. 7 9,
/,�• do I3
a rn
Final PH: /a, 7
n
Corrected PH: 12, 8�
Has 72 Hour & PH Criteria Been Met? LY) N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met?. Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
PH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial PH:
Corrected PH:
Final PH:
Corrected PH:
Has 72 Hour & PH Criteria Been Met? Y N

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:j Third
Biosolids Permit Number: v
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
16247
013
.5
8:31 am
A
8:36am
300 __Amilliliters
1.7 1% Dry Solids
10.5 degrees Celsius
11.3 degrees Celsius
0.0
8.7
1.0
2.63 mg Oxygen/hr
0.52 mg Oxygen/g/hr
11 degrees Celsius
1.838459212
Temperature Corrected Specific Oxygen Uptake Rate:5mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Third
Biosolids Permit Number: t
Date:
Digester Temperature:
Sampling Date/Time: 1/'I
Sampled By:
Analysis Date/Time: 1/3/
Analyzed By: ..r
Sample Volume:
Total Solids:'
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
v 6.83
6.78
6.72
6.65
r,
6.58
b.4y
6.38
�. 6.36
Slope:
Intercept:
Correlation Coefficient:
)016247
W2013
14.2
8:23arn
SA
13 8:27am
SA
300
1.8
14.4
14.7
0.0
7.1
0.9
milliliters
% Dry Solids
degrees Celsius
deqrees Celsius
Oxygen Uptake Rate: 2.55 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.47 mg Oxygen/g/hr
Average Temperature: 15 degrees Celsius
Temperature Correction Factor: 1.402551731
Temperature Corrected Specific Oxygen Uptake Rate 066� mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
ree
� 1/4/13 9:18am I
1 1/4/2013 9:26am 8
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
=Zzzar_�
1.8 % Dry Solids
11.3 degrees Celsius
13.5 s�degrees Celsius
0.0
9.3
1.0
1.40 mg Oxygen/hr
0.26 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rater 0.45 f1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP .
Biosolids Permit Number:
WQ0016247
Date:
1/7/2013
Digester Temperature:
t 11.2
Sampling Date/Time:
1/7/13 10:35am
Sampled By:
SA
Analysis Date/Time:'
1/7/2013 10:39am
Analyzed By:
SA
Sample Volume:
s 300 milliliters
R
Total Solids:
1.8 % Dry Solids
Beginning Temperature:''
14.4 degrees Celsius
End Temperature:
14.8 degrees Celsius
Dissolved Oxygen Level
6.78
6.69
Slope:
Intercept:
Correlation Coefficient. -
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.7
1.0
3.49 mg Oxygen/hr
0.65 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate 0 91 mg Oxygen/g/hr
L v
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:.
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
-Beginning Temperature:
End Temperature:
Third C
WC
1
7.
1/8/1
1/8/2(
x
Dissolved Oxygen Level
(mg/1)
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
I/2013
,�..,�.
11.8
1:42am
SA
3 1:46am
SA�
300
1.8
0.0
8.1
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.66 mg Oxygen/hr
0.49 mg Oxygen/g/hr
12 degrees Celsius
1.71818618
Temperature Corrected Specific Oxygen Uptake Rate:•.85 .z._ mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Third Creek WWTP
W00016247
_T 1 /9/2013
14.6
L.1.11/13 9:05am
� 1/y/'LUI� y:iiam
Slope:
Intercept. -
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
300 milliliters
1.9 ;% Dry Solids
14.9�degrees Celsius
15.2 gdegrees Celsius
0.0
7.9
1.0
2.21 mg Oxygen/hr
0.39 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate 0.54 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Third Creek WWT
Biosolids Permit Number: WQ0 6247
Date: 1/10/2013
Digester Temperature: 13.4
Sampling Date/Timer ' 1/10/13 8:51am
Sampled By: `9T SA
Analysis Date/Time. 1/10/2013 8 59ar
Analyzed By: SA
Sample Volume: 300
Total Solids: 1.9
Beginning Temperature: 13.6
End Temperature: 14.55
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.1
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1.08 mg Oxygen/hr
0.19 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.25
1
8.14
2
8.07
3
8.02
4
7.99
5
7.97
6
7.95
7
7.93
8
7.9
9
7.86
10
7.83
11
7.8
12
7.78
13
7.76
14
7.74
15
7.7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Third Creek WWTP
W00016247
4/2/2013
12.1
4/2/13 7:26am
SA
4/2/13 7:32am
SA
300
1.8
12.2
14.5
0.0
8.2
1.0
milliliters
Yo Dry Solids
degrees Celsius
legrees Celsius
1.88 mg Oxygen/hr
0.35 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.99
1
8.91
2
8.86
3
8.79
4
8.73
5
8.66
6
8.58
7
8.57
8
8.55
9
8.57
10
8.5
11
8.47
12
8.46
13
8.45
14 -
8.46
15
8.43
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/3/2013
12.6
4/3/13 8:16am
SA
4/3/13 8:25am
SA
300
1.7
13.1
14.4
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.15 mg Oxygen/hr
0.42 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 0.63 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name.
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature.
End Temperature
Dissolved Oxygen Level
(mg/1)
7.64
7.64
7.62
7.61
7.59
7.57
7.56
7.55
7.55
7.53
7.52
45
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/4/2013
14.4
4/4/13 8:04am
SA
4/4/13 8:12am
SA
300
1.7
14.9
15.9
0.0
7.6
1.0
,,milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.80 mg Oxygen/hr
0.16 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Third Creek WWTP
Biosolids Permit Number:
VV00016247
Date:
4/5/2013
Digester Temperature:
14.1
Sampling Date/Time:
4/5/13 9:31am
Sampled By:
SA
Analysis Date/Time:
4/5/13 9:36am
Analyzed By:
SA
Sample Volume:
300
milliliters
Total Solids:
1.7
% Dry Solids
Beginning Temperature:
14.3
degrees Celsius
End Temperature:
15.1
degrees Celsius
Dissolved Oxygen Level
(mg/1)
8.17
8.18
8.13
8.11
8.06
8.08
8.08
8.02
7.88
7.86
7.86
7.72
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.2
1.0
1.99 mg Oxygen/hr
0.39 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:j 0.55 =mg Oxygenlg/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date.
Digester Temperature.
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.38
1
7.41
2
7.43
3
7.43
4
7.42
5
7.44
6
7.42
7
7.43
8
7.41
9
7.42
10
7.4
11
7.37
12
7.36
13
7.36
14
7.34
15
7.33
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Third Creek WWTP
W00016247
4/8/2013
18.3
4/8/13 1:26pm
SA
4/8/13 1:33pm
SA
300
1.7
18.3
18
0.0
7.4
0.7
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.32 mg Oxygen/hr
0.06 mg Oxygen/g/hr
18 degrees Celsius
1.1449
Temperature Corrected Specific Oxygen Uptake Rate:j 0.07 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.72
1
7.68
2
7.64
3
7.63
4
7.62
5
7.62
6
7.63
7
7.64
8
7.65
9
7.65
10
7.64
11
7.63
12
7.59
13
7.55
14
7.51
15
7.48
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W Q 0016247
4/9/2013
18.3
4/9/13 8:40pm
SA
4/9/13 8:46pm
SA
300
1.7
16.4
16.8
0.0
7.7
0.8
-nilliliters
% Dry Solids
legrees Celsius
Degrees Celsius
0.61 mg Oxygen/hr
0.12 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.15 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date.
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes). (mg/1)
0
8.07
1
7.96
2
7.92
3
7.85
4
7.8
5
7.76
6
7.72
7
7.68
8
7.64
9
7.58
10
7.58
11
7.55
12
7.48
13
7.45
14
7.4
15
7.82
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
4/1 /2013
14.7
4/1/13 9:23am
SA
4/1/13 9:28am
SA
300
1.7
15.2
16.1
milliliters
Yo Dry Solids
legrees Celsius
legrees Celsius
2.00 mg Oxygen/hr
0.39 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:1 0.51 1mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek W1
WQ001624'
7/1 /2013
22.4
7-1-13 12:14
SA
7/1/2013 12:7
SA
300
1.7
21.6
21.2
Dissolved Oxygen Level
6.56
6.42
6.32
6.24
6.15
6.05
5.97
5.89
5.78
5.72
5.62
5.54
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature. -
Temperature Correction Factor:
a
m
milliliters
% Dry Solids
degrees Celsius
deorees Celsius
0.1
6.8
1.0
5.18 mg Oxygen/hr
1.02 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.97 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.48
1
6.44
2
6.42
3
6.32
4
6.28
5
6.25
6
6.2
7
6.16
8
6.07
9
6.05
10
5.99
11
5.96
12
5.94
13
5.9
14
5.81
15
5.7
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific
Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP III
7/2/2013
22.4
7/2/13 9:46
SA
7/2/2013 9:50am
300
1.7
20.8
20.3
0.0
6.5
1.0
illiliters
Dry Solids
agrees Celsius
:arees Celsius
2.92 mg Oxygen/hr
0.57 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:j 0.55 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
7/3/2013
22.3
7/3/13 8:12
SA
7/3/2013 8:20am
SA
300
1.7
22.1
20.9
0.0
7.1
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
2.67 mg Oxygen/hr
0.52 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate: 0.48 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
m
7.09
6.79
6.76
6.7
6.67
0
6.61
a
6.57
6.56
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
7/5/2013
21
7/5/13 8:05
SA
7/5/2013 8:12am
SA
300
1.7
20.9
20.6
0.0
7.1
1.0
milliliters
% Dry Solids
legrees Celsius
legrees Celsius
2.54 mg Oxygen/hr
0.50 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.47 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
Third Creek WWTP
mil
%
de(
de(
WQ0016247
7/8/2013
21
7/8/13 9:58
SA
7/8/2013 10:06am
SA
300
1.7
22.3
21.6
liliters
Dry Solids
3rees Celsius
frees Celsius
Slope: 0.0
Intercept: 6.6
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.63 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.51 mg Oxygen/g/hr
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.907029478
Temperature Corrected Specific Oxygen Uptake Rate:1 0.47 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
6.49
1
6.47
2
6.42
3
6.39
4
6.38
5
6.36
6
6.35
7
6.3
8
6.3
9
6.27
10
6.25
11
6.24
12
6.23
13
6.2
14
6.18
15
6.14
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
W00016247
7/9/2013
21.8
7/9/13 8:14
SA
7/9/2013 8:19am
SA
300
1.6
21.8
0.0
6.5
1.0
Ililiters
Dry Solids
grees Celsius
arees Celsius
1.29 mg Oxygen/hr
0.27 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.26 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling. Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
6.53
1
6.49
2
6.45
3
6.39
4
6.33
5
6.3
6
6.27
7
6.23
8
6.18
9
6.16
10
6.11
11
6.06
12
6.01
13
5.94
14
5.89
15
5.84
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
7/10/2013
21.9
7/10/13 7:08
SA
7/10/2013 7:16am
SA
300
1.5
21.5
20.7
Slope: 0.0
Intercept: 6.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.68 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.60 mg Oxygen/g/hr
Average Temperature: 21 degrees Celsius
Temperature Correction Factor: 0.952380952
Temperature Corrected Specific Oxygen Uptake Rate:1 0.57 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time.-
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes) (mg/1)
0
7.79
1
7.97
2
7.92
3
7.91
4
7.87
5
7.84
6
7.84
7
7.83
8
7.82
9
7.82
10
7.81
11
7.76
12
7.7
13
7.67
14
7.62
15
7.59
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient
Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WO0016247
1 10-1-13 11:52am I
I 10/1/13 11:58 1
300
1.8
19.6
19.8
illiliters
Dry Solids
,grees Celsius
,arees Celsius
0.0
7.9
0.9
1.16 mg Oxygen/hr
0.22 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.22 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WW
WQ0016247
10/2/2013
19.6
10/2/13 13:43
SA
10/2/13 13:47
SA
300
1.8
19.5
19.4
Time Dissolved Oxygen Level
(minutes).
(mg/I)
0
8.17
1
8.12
2
8.11
3
8.09
4
8.06
5
8.06
6
8.05
7
8
8
7.98
9
7.95
10
7.92
11
7.9
12
7.86
13
7.81
14
7.76
15
7.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature. -
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
deqrees Celsius
0.0
8.2
1.0
1.64 mg Oxygen/hr
0.30 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.33 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WQ0016247
10/3/2013
19.3
10/3/13 9:03
SA
10/3/13 9:10
SA
300
1.8
19.4
19.2
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.96
1
7.94
2
7.9
3
7.87
4
7.85
5
7.82
6
7.79
7
7.77
8
7.74
9
7.73
10
7.68
11
7.67
12
7.63
13
7.61
14
7.57
15
7.54
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.0
1.0
1.64 mg Oxygen/hr
0.30 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.33 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature.
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.91
1
7.88
2
7.86
3
7.84
4
7.82
5
7.79
6
7.75
7
7.72
8
7.69
9
7.65
10
7.62
11
7.59
12
7.59
13
7.57
14
7.52
15
7.47
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10/4/2013
19.3
10/4/13 12:23
SA
10/4/13 12:31
SA
300
1.8
19.5
19.3
0.0
7.9
1.0
milliliters
Yo Dry Solids
legrees Celsius
9egrees Celsius
1.72 mg Oxygen/hr
0.32 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.34 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) .(mg/1)
0
7.9
1
7.87
2
7.85
3
7.82
4
7.77
5
7.77
6
7.75
7
7.74
8
7.7
9
7.68
10
7.66
11
7.63
12
7.6
13
7.58
14
7.56
15
7.52
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Third Creek WWTP
WQ0016247
10/6/2013
19.8
10/6/13 10:03
SA
10/6/13 10:12
SA
300
T
19.8
19.5
0.0
7.9
1.0
Ililiters
Dry Solids
grees Celsius
grees Celsius
1.45 mg Oxygen/hr
0.27 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.27 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time,
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
WO0016247
10/7/2013
19.1
10/7/13 9:48
SA
10/7/13 9:57
SA
300
1.8
19
18.7
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
8.03
1
8
2
7.96
3
7.94
4
7.9
5
7.88
6
7.86
7
7.81
8
7.77
9
7.74
10
7.71
11
7.69
12
7.65
13
7.6
14
7.58
15
7.55
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
8.0
1.0
1.94 mg Oxygen/hr
0.36 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:1 0.38 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Third Creek WW i P
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
W00016247
10/9/2013
19.2
10/9/13 8:52
SA
10/9/13 9:03
SA
300
1.8
19
18.8
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.93
1
7.9
2
7.86
3
7.83
4
7.81
5
7.79
6
7.76
7
7.74
8
7.72
9
7.71
10
7.68
11
7.65
12
7.64
13
7.61
14
7.59
15
7.56
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.0
7.9
1.0
1.40 mg Oxygen/hr
0.26 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time-
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
r0urtn LreeK VVVV I F'f
1 /2/2013
e
12.7
1/2/13 1.35 PM
�RG
_BJ_
300 ^� milliliters
1.48 % Dry Solids
12.8 degrees Celsius
13.3 degrees Celsius
0.0
8.7
0.7
1.92 mg Oxygen/hr
0.43 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 0.69 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
1 /3/2013
14.3
1/3/13 1:00 PM
LC
1/3/13 1:05 PM
BJ
300
1.48
14.2
14.6
Dissolved Oxygen Level
(mg/1)
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1.81 mg Oxygen/hr
0.41 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:�0.61 i mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek WWTP
Biosolids Permit Number:
Date: 1 /4/2013
Digester Temperature: 12.6
Sampling Date/Time: 1/4/13 1:50 PM
Sampled By: _ LC
Analysis Date/Time: 1/4/13 1:55 PM�
Analyzed By: _ BJ
Sample Volume: 300 milliliters
Total Solids: 1.53 % Dry Solids
Beginning Temperature: 12.8 degrees Celsius
End Temperature: 14 degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
10.1
1.0
3.45 mg Oxygen/hr
0.75 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1.21 J mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Fourth Creek WWTP
milliliters
% Dry Solids
1 /7/2013
14.1
1/7/13 12:40 PM
LC
1/7/13 12:48 PM
BJ _
300
1.48
Beginning Temperaturel 13.2 degrees Celsius
End Temperature 13.6degrees Celsius
Dissolved Oxygen Level
(mg/1)
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
9.9
1.0
3.36 mg Oxygen/hr
0.76 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:: _ 1.21mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date. -
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate. -
Average Temperature:
Temperature Correction Factor:
rourtn LreeK VVVV I h'
1 /8/2013
13.3
1/8/13 12:38 PM
LC
1/8/13 12:47 PM
300
1.56
13.6
13.8
0.1
9.9
0.9
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.54 mg Oxygen/hr
0.76 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.14 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
8.43
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.1
9.0
1.0
3.30 mg Oxygen/hr
0.74 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.11 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
7
RG
300 milliliters
1.48 % Dry Solids
13.8 degrees Celsius
15.4 T degrees Celsius
0.1
9.6
1.0
4.13 mg Oxygen/hr
0.93 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 1.30 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek
4/1/20'
17.8
4/1/13 12:z
LC
4/1/13 12::
BJ
300
1.41
17
17.6
Dissolved Oxygen Level
6.36
C3
6.28
6.15
6.08
6.03
5.99
5.86
5.82
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
nfu>IXT111r
milliliters
% Dry Solids
degrees Celsius
decrees Celsius
0.0
6.5
0.7
2.37 mg Oxygen/hr
0.56 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.69 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/I)
0
7.22
1
7.7
2
7.83
3
7.67
4
7.45
5
7.47
6
7.58
7
7.64
8
7.6
9
7.53
10
7.5
11
7.39
12
7.38
13
7.37
14
7.36
15
7.28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Fourth Creek WWTP
4/2/2013
17.9
4/2/13 12:38 PM
LC
4/2/13 12:48 PM
BJ
300
1.43
17.2
0.0
7.6
0.5
Ililiters
Dry Solids
grees Celsius
grees Celsius
1.03 mg Oxygen/hr
0.24 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate: 0.29 img Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific.Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.31
1
7.38
2
7.5
3
7.64
4
7.67
5
7.72
6
7.72
7
7.69
8
7.75
9
7.85
10
7.7
11
7.62
12
7.58
13
7.48
14
7.41
15
7.28
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
4/3/2013
18.4
4/3/13 12:43 PM
LC
4/3/13 12:54 PM
BJ
300
T
17.3
17.5
0.0
7.6
0.0
0.07 mg Oxygen/hr
0.02 mg Oxygen/g/hr
17 degrees Celsius
1.225043
Temperature Corrected Specific Oxygen Uptake Rate:1 0.02 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
8.8
1
8.78
2
8.86
3
8.84
4
8.67
5
8.57
6
8.42
7
8.34
8
8.38
9
8.35
10
8.21
11
8.14
12
8
13
8.21
14
8.2
15
8.22
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
4/4/2013
12.5
4/4/13 12:41 PM
RG
300
1.3
13.1
a
14.3
0.1
8.8
0.9
liliters
Dry Solids
arees Celsius
grees Celsius
3.23 mg Oxygen/hr
0.83 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate:1 1.24 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWT
Biosolids Permit Number:
Date:
4/5/2013
Digester Temperature:
12.6
Sampling Date/Time:
4/5/13 9:51 AM
Sampled By:
RG
Analysis Date/Time:
4/5/13 10:00 AM
Analyzed By:
BJ
Sample Volume:
300
Total Solids:
1.32
Beginning Temperature:
12.8
End Temperature:
13.9
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
7.35
7.35
7.41
7.4
7.33
7.26
7.24
7.18
7.12
7.02
6.93
6.87
6.8
6.7
6.64
6.57
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.5
1.0
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
3.51 mg Oxygen/hr
0.89 mg Oxygen/g/hr
13 degrees Celsius
1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:1 1.42 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature.
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By.
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
7.15
1
7.06
2
7.08
3
7.12
4
7.15
5
7.12
6
7.07
7
7.05
8
7
9
6.93
10
6.89
11
6.82
12
6.8
13
6.72
14
6.69
15
6.6
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
4/8/2013
19
4/8/13 1:39 PM
RG
4/8/13 1:45 PM
BJ
300
1.34
19.1
19.2
0.0
7.2
0.9
rilliliters
Yo Dry Solids
legrees Celsius
legrees Celsius
2.10 mg Oxygen/hr
0.52 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes) (mg/1)
0
6.04
1
5.96
2
5.96
3
5.92
4
5.84
5
5.86
6
5.81
7
5.89
8
5.85
9
5.84
10
5.81
11
5.83
12
5.78
13
5.79
14
5.77
15
5.78
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient
Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
4/9/2013
19
4/9/13 1:00 PM
RG
4/9/13 1:10 PM
BJ
300
1.31
19
18.4
Ililiters
Dry Solids
grees Celsius
grees Celsius
0.86 mg Oxygen/hr
0.22 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes) .
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek M
7/1 /2113
24.2
7/1/13 12:20 P
I RG
7/1/13 12:32 P
BJ
300
1.69
24.5
24.4
Dissolved Oxygen Level
4.
4.25
3.59
3.51
s
3.49
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.1
4.5
1.0
4.65 mg Oxygen/hr
0.92 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.75 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Fourth Creek WWTP
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
7/2/2013
25
7/2/13 10:09 AM
RG
7/2/13 10:17 AM
BJ
300
1.48
24.9
23
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
4.75
1
4.66
2
4.72
3
4.67
4
4.67
5
4.6
6
4.54
7
4.49
8
4.48
9
4.33
10
4.19
11
4.21
12
4.19
13
4.15
14
4.1
15
4.06
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
0.1
4.8
1.0
3.01 mg Oxygen/hr
0.68 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.56 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
5.46
1
5.34
2
5.34
3
5.31
4
5.26
5
5.24
6
5.16
7
5.12
8
5.03
9
4.93
10
4.9
11
4.83
12
4.77
13
4.72
14
4.69
15
4.63
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
I-ourtn UreeK VVVV I F'
7/3/2013
23.8
7/3/13 9:57 AM
RG
7/3/13 10:04 AM
BJ
300
1.63
23.9
23.5
0.1
5.5
1.0
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
3.36 mg Oxygen/hr
0.69 mg Oxygen/g/hr
24 degrees Celsius
0.822702475
Temperature Corrected Specific Oxygen Uptake Rate: 0.57 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek WWTP
Biosolids Permit Number:
Date:
7/5/2013
Digester Temperature:
24.5
Sampling Date/Time:
7/5/13 9:50 AM
Sampled By:
RG
Analysis Date/Time:
7/5/13 10:00 AM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.45
% Dry Solids
Beginning Temperature:
24.5
degrees Celsius
End Temperature:
24.4
degrees Celsius
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
6.44
6.38
6.34
6.26
6.23
6.19
6.12
6.08
5.92
5.89
5.8
5.73
5.69
5.62
5.58
5.54
Slope:
0.1
Intercept:
6.5
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
3.82 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.88 mg Oxygen/g/hr
Average Temperature:
24 degrees Celsius
Temperature Correction Factor:
0.822702475
Temperature Corrected Specific
Oxygen Uptake Rate: 0.72 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
mg/1
5.29
5.2
5.18
5.06
5.15
5.12
5.07
5.01
4.95
4.91
4.85
4.78
4.73
4.67
4.67
Fourth Creek WWTP
7/8/2013
26
7/8/13 12:57 PM
LC
7/8/13 1:02 PM
BJ
300
1.4
lliliters
Dry Solids
grees Celsius
arees Celsius
Slope: 0.0
Intercept: 5.3
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.73 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.65 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.51 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
. Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
7.09
7.05
7.07
7.07
7.09
7.04
6.92
6.83
6.79
6.72
6.64
6.61
6.57
6.5
6.48
6.45
Fourth Creek WWTP.
7/9/2013
26
7/9/13 12:55 PM
LC
7/9/13 1:02 PM
BJ
300
1.48
26
Ililiters
Dry Solids
grees Celsius
arees Celsius
Slope:
0.0
Intercept:
7.2
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
2.98 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.67 mg Oxygen/g/hr
Average Temperature:
26 degrees Celsius
Temperature Correction Factor:
0.746215397
Temperature Corrected Specific
Oxygen Uptake Rate: 0.50 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:F
Fourth Creek V\
7/10/2013
26.8
7/10/13 12:55
LC
7/10/13 1:02
BJ
300
1.34
25.7
24
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
TM
Mv
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
0.0
7.0
0.8
1.36 mg Oxygen/hr
0.34 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:j 0.27 n mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Fourth Creek 1l�
Biosolids Permit Number:
Date: 10/1 /2013
Digester Temperature: 20.4
Sampling Date/Time: 10/1/13 2:30 P
Sampled By: LC
Analysis Date/Time: 10/1/13 2:38 P
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes) (mg/1)
0
7.21
1
7.26
2
7.09
3
7.03
4
6.95
5
6.92
6
6.93
7
6.83
8
6.79
9
6.73
10
6.78
11
6.76
12
6.81
13
6.84
14
6.71
15
6.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient
Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2
illiliters
Dry Solids
agrees Celsius
�arees Celsius
0.0
7.1
0.9
1.91 mg Oxygen/hr
0.32 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.32 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes)
(mg/1)
0
7.21
1
7.26
2
7.09
3
7.03
4
6.95
5
6.92
6
6.93
7
6.83
8
6.79
9
6.73
10
6.78
11
6.76
12
6.81
13
6.84
14
6.71
15
6.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature
Correction Factor:
Fourth Creek WWTP
10/1 /2013
20.4
10/1/13 2:30 PM
LC
10/1/13 2:38 PM
BJ
300
1.49
20.3
20.1
0.0
7.1
0.9
milliliters
% Dry Solids
legrees Celsius
legrees Celsius
1.91 mg Oxygen/hr
0.43 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.43 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek 1NW I H
Biosolids Permit Number:
Date:
10/3/2013
Digester Temperature:
20.1
Sampling Date/Time:
10/3/13 9:56 AM
Sampled By:
RG
Analysis Date/Time:
10/3/13 10:01 AM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.5
% Dry Solids
Beginning Temperature:
20.1
degrees Celsius
End Temperature:
18.5
degrees Celsius
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
(mg/1)
7.53
7.56
7:5
7.43
7.37
7.37
7.4
7.32
7.28
7.26
7.23
7.21
7.19
7.15
7.16
7.14
0
Slope:
0.0
Intercept:
7.5
Correlation Coefficient:
1.0
Oxygen Uptake Rate:
1.71 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.38 mg Oxygen/g/hr
Average Temperature:
19 degrees Celsius
Temperature Correction Factor:
1.07
Temperature Corrected Specific
Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1)
.0
6.41
1
6.62
2
6.63
3
6.51
4
6.56
5
6.56
6
6.49
7
6.53
8
6.5
9
6.47
10
6.45
11
6.4
12
6.37
13
6.31
14
6.2.
15
6.12
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/4/2013
20
10/4/13 10:15 AM
RG
10/4/13 10:23 AM
BJ
300
1.67
20
19.8
-nilliliters
% Dry Solids
legrees Celsius
legrees Celsius
1.44 mg Oxygen/hr
0.29 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.29 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Fourth Creek WWTP
Biosolids Permit Number:
Date:
10/7/2013
Digester Temperature:
21
Sampling Date/Time:
10/7/13 12:33 PM
Sampled By:
RG
Analysis Date/Time:
10/7/13 12:38 PM
Analyzed By:
BJ
Sample Volume:
300
milliliters
Total Solids:
1.55
% Dry Solids
Beginning Temperature:
21.2
degrees Celsius
End Temperature:
19.8
degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.1
7.8
0.9
3.30 mg Oxygen/hr
0.71 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 0.68 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids:
Beginning Temperature
End Temperature
Time Dissolved Oxygen Level
(minutes) (mg/1).
0
6.39
1
6.38
2
6.26
3
6.34
4
6.32
5
6.36
6
6.32
7
6.33
8
6.29
9
6.27
10
6.24
11
6.2
12
6.18
13
6.13
14
6.11
15
6.09
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/8/2013
20.1
10/8/13 12:37 PM
RG
10/8/13 12:42 PM
BJ
300
1.6
20.1
19.5
0.0
6.4
0.9
-milliliters
% Dry Solids
legrees Celsius
legrees Celsius
1.10 mg Oxygen/hr
0.23 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: 0.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name
Biosolids Permit N mber
Date
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/1)
0
6.79
1
6.75
2
6.81
3
6.73
4
6.71
5
6.71
6
6.63
7
6.57
8
6.67
9
6.59
10
6.57
11
6.56
12
6.53
13
6.49
14
6.47
15
6.44
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Fourth Creek WWTP
10/9/2013
19.6
10/9/13 12:53 PM
RG
10/9/13 1:02 PM
300 milliliters
1.6 % Dry Solids
19.7 degrees Celsius
19.1 degrees Celsius
0.0
6.8
1.0
1.41 mg Oxygen/hr
0.29 mg Oxygen/g/hr
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate:j 0.31 =mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.