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Home My WebLink AboutWQ0014136_Regional Office Historical File Pre 2018 (2)RECEIVED/NCDENR/DWR FEB 11 2019 WQROS MOORESVILLE REGIONAL OFFICE ROCKY RIVER W. W.T.P Mooresville (704) 662-8470 Town ®f Mooresville FAX (704) 662-8473 NORTH CAROLINA POST OFFICE BOX 878 MOORESVILLE, NC 28115 NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699 01/28/19 Subject: 2018 Annual Sludge Report, WQ0014136 Town of Mooresville Residuals Land Application Program Following is the information requested to accompany our Land Application report. Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy Rd. Mooresville, N.C. 28115 Phone: 704-662-8470 Responsible official and facility contact — Larry Hendren, Biosolids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-799-4063 (Part A) and (Part B) No Land Application for 2018 under Permit WQ0014136 All sewage sludge that was not generated into Class A was dewatered and taken to a lined land fill for disposal. Total tons = 3 943.8 5 or Dry metric tons = 465.11 (See attached hauling summary sheet). Laboratory results from TCLP are included in this report. On December 13th, 2018, The Town of Mooresville officially rescinded our Land Application Permit No. WQ0014136 in a letter addressed to Troy Doby with the NC Division of Water Resources. A copy of this notice is included in this report. (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Larry Hendren, Biosolids Coordinator Signature: Date 1--LOt-1-N Reviewed by: Jamie Levis, WWTP Plant Manager Signature: Date�'�'� /� 2018 Class 8 Sludge Totals Date Hauler* Loads hauled Quantity (tons) Average per load January I - I d 1/3/2018 S 4 102.33 25.58 1/11/2018 S 1 25.93 25.93 1/12/2018 S 1 26.71 26.71 1/22/2018 S 3 71.53 23.84 1/24/2018 S 3 75.66 25.22 1/25/2018 S 1 18.46 18.46 1/31/2018 .S 4 97.80 24.45 Monthly Total 17 418.42 24.31 February 2/6/2018 S 4 90.38 22.60 2/12/2018 S 3 70.56 23.52 2/15/2018 S 4 87.22 21.81 2/26/2018 S 3 77.02 25.67 2/27/2018 S 3 71.50 23.83 Monthly Total 17 396.68 23.49 March 3/6/2018 S 3 71.47 23.82 3/7/2018 S 3 71.39 23.80 3/12/2018 S 2 48.36 24.18 3/13/2018 S 3 67.77 22.59 3/21/2018 S 1 26.33 26.33 3/22/2018 S 2 51.39 25.70 3/28/2018 S 5 108.51 21.70 3/30/2018 S 3 73.88 24.63 *** 3/21/2018 S 1 25.26 25.26 *** 3/22/2018 S 1 21.27 21.27 *** 3/30/2018 S 1 24.82 24.82 *** 3/30/2018 S 1 25.54 25.54 Monthly Total 26 615.99 24.14 April 4/2/2018 S 3 75.66 25.22 4/3/2018 S 3 76.92 25.64 4/5/2018 S 2 51.46 25.73 4/6/2018 S 3 79.18 26.39 4/17/2018 S 3 79.49 26.50 4/18/2018 S 3 72.94 24.31 4/20/2018 S 4 86.41 21.60 Monthly Total 21 522.06 25.06 2018 Class B Sludge Totals May 5/15/2018 S 4 82.59 20.65 5/23/2018 S 2 41.61 20.81 5/24/2018 S 3 59.47 19.82 Monthly Total 9 - 183.67 19.82 June 6/12/2018 S 4 88.21 22.05 Monthly Total 4 88.21 22.05 July 7/18/2018 S 1 17.88 17.88 7/19/2018 S 3 61.09 20.36 7/20/2018 S 2 30.12 15.06 7/24/2018 S 2 37.97 18.99 Monthly Total 8 147.06 18.07 August 0.00 Monthly Total 0 0 0.00 September 9/12/2018 S 4 83.03 20.76 9/13/2018 S 3 66.81 22.27 Monthly Total 7 149.84 21.51 October 10/10/2018 S 7 126.05 18.01 10/12/2018 S 1 22.05 22.05 Monthly Total 8 148.1 20.03 November 11/15/2018 S 2 38.99 19.50 11/16/2018 S 2 42.06 21.03 11/19/2018 S 3 68.31 22.77 11/20/2018 S 3 66.25 22.08 11/21/2018 S 2 41.16 20.58 11/26/2018 S 1 26.51 26.51 11/27/2018 S 4 94.9 23.73 11/28/2018 S 3 68.89 22.96 11/29/2018 S 3 66.95 22.32 Monthly Total 23 514.02 22.39 2018 Class B Sludge Totals December 12/4/2018 S 4 88.65 22.16 12/5/2018 S 3 70.69 23.56 12/6/2018 S 4 85.51 21.38 12/7/2018 S 2 47.05 23.53 12/12/2018 S 2 46.48 23.24 12/13/2018 S 3 72.44 24.15 12/14/2018 S 1 20.19 20.19 12/17/2018 S 3 64.92 21.64 12/18/2018 S 3 73.72 24.57 12/19/2018 S 3 72.18 24.06 12/20/2018 S 1 24.41 24.41 12/21/2018 S 1 23.35 23.35 12/28/2018 S 1 21.08 21.08 12/31/2018 S 2 49.13 24.57 Monthly Total 33 759.8 22.99 Year Totals 173 3943.85 20.32 Corrected for % solids 0.14 552.14 dry metric tons 500.89 *** Loads with astrisks on the date line were completed on incorrect manifest forms and show as Class B Monofill Material, but they are in fact our standard Class B Sludge. * M - Mooresville *S-SYNAGRO Full -Service Analytical & Environmental Solutions LABORATORIES INC. Town of Mooresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Class B Sludge Lab Submittal Date: 01/16/2018 Prism Work Order: 8010221 Case Narrative 02/01 /2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. i Terri W. Cole Project Manager Data Qualifiers Key Reference: Reviewed By Terri W. Cole Project Manager "' -"0- � CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/625-0409 Page 1 of 6 �r'I I Sample Receipt Summary �_ ISM Full -Service Analytical & Environmental solutions 02/01/2018 _.=. LA00RATORIEy ING Prism Work Order: 8010221 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Class B 8010221-01 Solid 01/16/18 01/16/18 Samples were received in good condition at 4.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629.6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041626-0409 Page 2 of 6 Laboratory Deport ISM I EnviService Analytical s Environmental Solutions 02/01/2018 LABORATORIES ING Town of Mooresville/RR WWTP Project: Class B Sludge Client Sample ID: Class B Attn: Whitney Munroe Prism Sample ID: 8010221-01 P. O. Box 878 Prism Work Order: 8010221 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/16/18 08:25 Time Submitted: 01/16/18 12:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 13.0 % by 0.100 0.100 1 *SM2540 G 1/22/18 14:16 TJY P8A0320 Weight Paint Filter Liquids Pass g 1.0 0.0 1 *9095A 1/30/18 10:44 SLS P8A0444 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL mg/kg dry 0.38 0.041 1 *8082A 1/29/18 22:22 JMC P8A0432 Aroclor 1221 BRL mg/kg dry 0.75 0.30 1 *8082A 1/29/18 22:22 JMC P8A0432 Aroclor 1232 BRL mg/kg dry 0.75 0.098 1 *8082A 1/29/18 22:22 JMC P8A0432 Aroclor 1242 BRL mg/kg dry 0.38 0.10 1 *8082A 1/29/18 22:22 JMC P8A0432 Aroclor 1248 BRL mg/kg dry 0.38 0.075 1 *8082A 1/29/18 22:22 JMC P8A0432 Aroclor 1254 BRL mg/kg dry 0.38 0.093 1 *8082A 1/29/18 22:22 JMC P8A0432 Aroclor 1260 BRL mg/kg dry 0.38 0.047 1 *8082A 1/29/18 22:22 JMC PBA0432 Surrogate Recovery Control Limits Tetrachloro-m-xylene 59 % 36-182 Decachlorobiphenyl 45 % 34-182 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 1/24/18 8:30 JAB P8A0331 TCLP Extraction Complete N/A 1 *1311 ZHE 1/26/18 9:00 ANG P8A0378 TCLP Metals Mercury BRL mg/L 0.010 0.000030 1 *7470A 1/24/18 16:25 JAB P8A0344 Arsenic BRL mg/L 0.050 0.016 1 *6010D 1/26/18 18:43 JAB P8A0399 Barium BRL mg/L 5.0 0.0040 1 *6010D 1/26/18 18:43 JAB P8A0399 Cadmium BRL mg/L 0.025 0.00075 1 *6010D 1/26/18 18:43 JAB P8A0399 Chromium BRL mg/L 0.25 0.0018 1 *6010D 1/26/18 18:43 JAB P8A0399 Lead BRL mg/L 0.050 0.0040 1 *6010D 1/26/18 18:43 JAB P8A0399 Selenium BRL mg/L 0.10 0.028 1 *6010D 1/26/18 18:43 JAB P8A0399 Silver BRL mg/L 0.25 0.0020 1 *6010D 1/26118 18:43 JAB PBA0399 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0.00086 1 *808113 1/29/18 18:30 JMC PBA0353 Dieldrin BRL mg/L 0.00050 0.000070 1 *8081B 1/29/18 18:30 JMC P8A0353 Endrin BRL mg/L' 0.00050 0.000075 1 *8081B 1/29/18 18:30 JMC P8A0353 gamma-BHC BRL mg/L 0.00050 0.000065 1 *8081B 1/29/18 18:30 JMC P8A0353 Heptachlor BRLCCV mg/L 0.00050 0.000085 1 *8081B 1/29/18 18:30 JMC P8A0353 Heptachlor Epoxide BRL mg/L 0.00050 0.000065 1 *8081B 1/29/18 18:30 JMC P8A0353 Methoxychlor BRLCCV mg/L 0.00050 0.00020 1 *8081B 1/29/18 18:30 JMC P8A0353 Toxaphene BRL mg/L 0.025 0.00037 1 *8081B 1/29/18 18:30 JMC P8A0353 Surrogate Recovery Control Limits Decachlorobiphenyl 106 % 13-186 Tetrachloro-m-xylene 70 % 40-134 TCLP Semivolatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 7041625-0409 Page 3 of 6 i. IFull -Service Analytical & Environmental Solutions LABO TORIE5 ING Laboratory Report 02/01/2018 Town of Mooresville/RR WWTP Project: Class B Sludge Client Sample ID: Class B Attn: Whitney Munroe Prism Sample ID: 8010221-01 P. O. Box 878 Prism Work Order: 8010221 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 01/16/18 08:25 Time Submitted: 01/16/18 12:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 2,4,5-Trichlorophenol BRL mg/L 0.25 0.0016 1 *8270D 1/29/18 19:04 JMV P8A0411 2,4,6-Trichlorophenol BRL mg/L 0.10 0.0018 1 *8270D 1/29/18 19:04 JMV P8A0411 2,4-Dinitrotoluene BRL mg/L 0.050 0.0014 1 *8270D 1/29/18 19:04 JMV P8A0411 2-Methylphenol BRL mg/L 0.050 0.0018 1 *8270D 1/29/18 19:04 JMV P8A0411 3/4-Methylphenol BRL mg/L 0.050 0.0015 1 *8270D 1/29/18 19:04 JMV P8A0411 Hexachlorobenzene BRL mg/L 0.050 0.0013 1 *8270D 1/29/18 19:04 JMV P8A0411 Hexachlorobutadiene BRL mg/L 0.050 0.0021 1 *8270D 1/29/18 19:04 JMV PBA0411 Hexachloroethane BRL mg/L 0.050 0.0017 1 *8270D 1/29/18 19:04 JMV P8A0411 Nitrobenzene BRL mg/L 0.050 0.0026 1 *8270D 1/29/18 19:04 JMV P8A0411 Pentachlorophenol BRL mg/L 0.25 0.0012 1 *8270D 1/29/18 19:04 JMV P8A0411 Pyridine BRL mg/L 0.25 0.0010 1 *8270D 1/29/18 19:04 JMV P8A0411 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 84 % 43-140 2-Fluorobiphenyl 83 % 44-119 2-Fluorophenol 53 % 19-119 Nitrobenzene-d5 77 % 44-120 Phenol-d5 35 % 11-52 Terphenyl-d14 78 % 50-134 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg/L 0.035 0.00083 1 *826013 1/27/18 1:49 KDM PSA0420 1,2-Dichloroethane BRL mg/L 0.025 0.00066 1 *8260B 1/27/18 1:49 KDM P8A0420 1,4-Dichlorobenzene BRL mg/L 0.38 0.00050 1 *8260B 1/27/18 1:49 KDM P8A0420 Benzene BRL mg/L 0.025 0.00048 1 *8260B 1/27/18 1:49 KDM P8A0420 Carbon Tetrachloride BRL mg/L 0.025 0.0011 1 *8260B 1/27118 1:49 KDM P8A0420 Chlorobenzene BRL mg/L 5.0 0.00062 1 *8260B 1/27/18 1:49 KDM P8A0420 Chloroform BRL mg/L 0.30 0.00076 1 *8260B 1127/18 1:49 KDM P8A0420 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0024 1 *8260B 1/27/18 1:49 KDM P8A0420 Tetrachloroethylene BRL mg/L 0.035 0.00098 1 *8260B 1/27/18 1:49 KDM P8A0420 Trichloroethylene BRL mg/L 0.025 0.00078 1 *8260B 1/27/18 1:49 KDM P8A0420 Vinyl chloride BRL mg/L 0.020 0.00097 1 *8260B 1/27/18 1:49 KDM P8A0420 Surrogate Recovery Control Limits 4-Bromofluorobenzene 96 % 80-124 Dibromofluoromethane 93 % 75-129 Toluene-d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/525-0409 Page 4 of 6 Sample Extraction Data Prep Method: Default Prep GenChem Lab Number Batch Initial Final Date/Time 8010221-01 P8A0444 100 g 100 mL 01/30/18 10:44 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 8010221-01 P8A0320 30 g 30 g 01/22/18 14:16 I Prep Method: 3650C GC Lab Number Batch Initial Final Date/Time 8010221-01 P8A0432 30.65 g 10 mL 01/29/18 15:30 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 8010221-01 P8A0378 12.5 g 250 mL 01/25/18 15:45 8010221-01 P8A0331 100 g 2000 mL 01/23/18 14:08 Prep Method: 3010A Lab Number Batch Initial Final Date/Time 8010221-01 P8A0399 10 mL 50 mL 01/26/18 10:20 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 8010221-01 PSA0344 20 mL 30 mL 01/24/18 10:10 Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 8010221-01 P8A0353 200 mL 10 mL 01/25/18 11:00 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 8010221-01 P8A0411 200 mL 1 mL 01/29/18 11:30 Prep Method:6030B Lab Number Batch Initial Final Date/Time 8010221-01 P8A0420 1 mL 10 mL 01/26/18 11:46 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 8010221-01 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/626-0409 Page 5 of 6 •xim rrrr rrn, sot n Full -Service Analytical & S� M w, Environmental Solutions ''LABORATORIES, INC. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 - Fax: 7041525-0409 Client Company Name: —To #a,_ ®P, Report To/Contaa t Name: Wi6aq ASImmg-, Reporting Address: >6. drr&�qh�Lt me, N I /, CRAM OF CUSTODY RECORD PAGE_] ®� � QUOTE ## TO EMSURE PROPER BILLIMG: Project Name: 44S Short Hold Analysis: (NO) UST Project: s) *Please ATTACH any project specific reporting (QC LEVE provisions and/or QC Requirements Invoice To: Address: a'llone. w- oPurchase Order No./Billing Reference TO BE FILLED INI BY CLIENT/SAMPLIMG PERSONNEL Email Address' Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days E®®Type: PDF °�E1tCe@—®that "Working Days" ❑ 6-9 Daysstandard 10 days ❑Rush Work Must Be Certification: N9ELAC D®® FL IBC Pre -Approved Site Location Name:Samples received after 14:00 will be processed next business day. SC OTHER MIA Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ [Mo (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES *NO CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY MATRIX (SOIL, WATER OR SAMPLE CONTAINER PRESERVA- TIVES ANALYSIS ftQUESTED �� ®ems® �' �e, R RI4S PRISM LAB *TYPE FOURS SLUDGE) SEE BELOW NO. SIZE @1 �® ID NO. '�1 ✓�� t}t�%r.�.� `�� °lam �� 1 y �a a• Sampler's Signature ' a— �4 �� Sampled By (Print Name) L Q�l�t ��r� y, Affiliation Upon relinquishing, this Chain ! tody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any_vAknges after analyses have been initialized. Reinquished By: (Signature) Received By: (Sjgnl3ture) Da Military/Hours Additional Comments i SlteAlnval:.Timo Y- a�^� Rahn wished B SI ur q Y• ( ) Received•By: (Signat're) ate �� Slto Departure Tllltg. •h Relinquished By; ignature) e d For P�sfn Laboratories B,y/�' Date ) 61cst'rv\ Field Teeh Fe9 a� 1 ��-� r�i G---."`_' .a�•tj B`U J Z :� � / Ptllleage . Method yf Ipment: E: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. ZOC Group No. _ SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY. ^ f x / 2 _L .46 Fe.d rw O UPS ❑ Hand -delivered ><PrIsm Field Service ❑ Other DRINKING LANDFILL o0 L® Q NO ® SCI © NO ❑ SC GI N®U ®SCTER I l7 NO ®SLATERSOLID ®SCE ®NC O SC ®NC SC ®NC ® SC ®NC ®SC U o I ■ ■ ❑ ❑ ❑ r 1 *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) a.�}R7 ,l):,l,a L / '�Rocky River Wastewater Treatment Plant Town of Mooresville 369 Johnson dairy Rd. Mooresville, North Carolina 28117 December 13'', 2018 Troy Doby, PE, Engineer Division of Water Recourses Water Quality Permitting, Non -Discharge permitting 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Rescinding of RLAP permit No. WQ0014136 Dear Mr. Doby, Please accept this letter as official notice to rescind The Town of Mooresville's RLAP permit No. WQ0014136. The Town of Mooresville wishes to rescind their RLAP permit effective immediately based on previous history of not being utilized. Mr. Doby, if you or the division should have any other questions or concerns, please don't hesitate to reach out to me or the Town's Utility Director (Allison Kraft, PE) akraftnmooresvillenc.gov. Sincerely, James A Levis Wastewater Treatment Plant Manager cc:Allison Kraft Edward Watson, NCDWR Town of Mooresville: NORTKCAROLINA, NCQENR-DWQ, Information Processing ,-Unit 1,617 M'diis-e-iP i ip ' Center Raleigh, NC-27699 02,12.7/`1 t, ROCKY:. RIVER, W."N.T.P TELEPHONE'(794) 602-'..8470 fA.X(704)_-§634473- POST-oFFICE BOX8791, m6ORE§VILLEjNC,,28115, Subject-:12017'Annual Sludgo,Rcipojrt, W66014136 Town of MdofesvilleAesiduals Land Application]Program— —Amend; Reoott d i _ , "C uO to,spreadsheei- alcuilafiomerror F.Qtlowi j the in ' ion 49 s format' - k.equested 16 accompanyur an jo �o �L d,.A- plicat nreport, F,61itY - Rocky River Wastewater Treatment Facility 36911ohnson Ddiry Rd. Phone- 704=662-8470 Responsible official and facility. contact." Tom Wyn n, Operations Supervisor PO. Box,-878 N16 re9ville, NC 2`8115, I- P � I � I __ ''I Phone- 704-77994054 (Part, A) and(N4.9) No Land Application for 20.0 under Permit W -, All 1 sewage, sludge that- was not geiiprated into Class' A.m. was de"' wdt6'f6d.dAdtAkontb-A'I"med"lind fill for 41sposal. Total tons = 1.719...46 or, Dry inetr'je tons218.19- (Seoattach&d hatilin ingsaniniary sheet). Laboratory fe§ultg fr6in T CLP -are,in.04ded, in't'his "rep.aft'.1 ,(Part,c), 1..edffi'fy under penalty of law Ahaf the; above -n.f formation, is,to..the best otniyyknow ledge and belief,true and accurate and, complete. I am aware:-that,there are si;g'n caft penaftie§",fot: if a sub Tw-fti N96 information, Pg I ion, iiicludingthe� possibility of fines and: imprisonment for knowing violations:, Prepared by: Tom E. —Wynn, jOperations Supervisor f Date: Reviewed. by: Jamie. Levis, WWTP Plant ManageLr 2017 Landfill -Sludge Total Date Hauler* loads hauled Civantiiy (tong). Average per load January 1/30/2017 S 2 49.53 24.77 1/.,3Q/2017 SA9 1 _ „ . 19 65 19.66 1/31/2017 S -2 44.36 '22.19 1/31/2107 SAB 2, 34 38 17,11. Monthly Total' 7 147.99 20.95. February 2/7/2017 S 3; 7Q.4.7 23.40, 2/7/2017 SAB :1, 20:41 . _ . 20.41 -2/8/2017 S. 3 76.14 25.39 2/8/2017 SAB, 2 " 34.7 17.35; 2/22/2017 S. 4 91.12 22.3 2/22/2017 SAB 2 3909 19.554, Monthly Total` 15 331.93 21.49 March 3/14/2017 S. 5 116.74 23.35 3/14/2017 SAB 2 383.7 19.19 3/17/2017 Si. 4 94.62 23:66: 3/17/2017 SAB' 2. 4556 3/24/2017 S 4 98 89 24.72 3/2:4/2017 SAB- 1 18.14 18.14 3/31/2017 S 5 119.98 23.80: 3/31/2017 SAB, 1. 20.46' 20.46 Monthly Total 24 551.7 22.01, Aoril 4/7 ,2017 S, 4 89,92 22.48 Monthly Total 4 89.92 - 22.48. May No Hauling Monthly Total, 0 0, U.00 June 6/6/2017 S 4 99.03 24.76 6/22/2017 St 2 41.54 20.77 Monthly Total 6' 140.57 22.76 July 7/'4/2017 S 4 87.83 21.96 7/11/2017 S, 3 63.56 21.19 2017 Landfill Sludge Total 7/1-4/2017 S 4 79.32 19;,8 3 7/17/2017 S 1 18.36 Monthly Total. 12 240.07' '20.3$' August 8/25/2017 S 2, 36.48 18.24- Monthly Total 2 36.48 1-8.24, September Na, Hauling Wntfily.Total a, 0 0600 October 10/21/2016 S 4, 76.92 19.21 Monthly Total 4, 76-.92 19.23- NbVem4er N&Hauling: Monthly Total 0 0 0.00 D6cember. 12/20/2017 S 4: 94,88 23,72 Monthly Total 4 941.88 23.72 Year TotcIN, 78 1719.46 is.93 Corrected for % solids 0.14 240..7 . 2 dry metric tons 218.38 M =- Mooresville *S-SYNAGRO *Ai3-Class -A9,BMixed Town of Mooresville NORTH CAROUNA ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 RECEIVEDINIC0ENRIDWR NCDENR-D WQ 02/07/ 18 Information Processing Unit WQROS 1617 Mail Service Center y11(IOORESVILLE REGIONAL OFFICE Raleigh, NC 27699 Subject: 2017 Annual Sludge Report, WQ0014136 Town of Mooresville Residuals Land Application Program Following is the information requested to accompany our Land Application report. Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy Rd. Mooresville, N.C. 28115 Phone: 704-662-8470 Responsible official and facility contact — Tom Wynn, Operations Supervisor P.O. BOX 878 Mooresville, NC 28115 Phone: 704-799-4054 (Part A) and (Part B) No Land Application for 2017 under Permit WQ0014136. All sewage sludge was not generated into Class A was dewatered and taken to a lined land fill for disposal. Total tons = 3290.99 or Dry metric tons = 417.97 (See attached hauling summary sheet). Laboratory results from TCLP are included in this report. (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Tom E. Wynn, Operations Supervisor Reviewed by: Jamie Levis, WWTP Plant Manager Signa r n Z —,( 2. Date /'� I/ 1 Signat . Date 2017 Landfill Sludge Total Date Hauler* Loads hauled Quantity (tons) Average per load January 1/30/2017 S 2 49.53 24.77 1/30/2017 SAB 1 19.66 19.66 1/31/2017 S 2 44.36 22.18 1/31/2107 SAB 2 34.38 17.19 Monthly Total 7 147.93 20.95 February 2/7/2017 S 3 70.47 23.49 2/7/2017 SAB 1 20.41 20.41 2/8/2017 S 3 76.14 25.38 2/8/2017 SAB 2 34.7 17.35 2/22/2017 S 4 91.12 22.78 2/22/2017 SAB 2 39.09 19.55 Monthly Total 15 331.93 21.49 March 3/14/2017 S 5 116.74 23.35 3/14/2017 SAB 2 38.37 19.19 3/17/2017 S 4 94.62 23.66 3/17/2017 SAB 2 45.56 22.78 3/24/2017 S 4 98.89 24.72 3/24/2017 SAB 1 18.14 18.14 3/31/2017 S 5 118.98 23.80 3/31/2017 SAB 1 20.46 20.46 Monthly Total 24 551.76 22.01 April 4/7/2017 S 4 89.92 22.48 Monthly Total 4 89.92 22.48 May No Hauling Monthly Total 0 0 0.00 June 6/6/2017 S 4 99.03 24.76 6/22/2017 S 2 41.54 20.77 Monthly Total 6 140.57 22.76 July 7/4/2017 S 4 87.83 21.96 7/11/2017 S 3 63.56 21.19 I/ 'Town Of M, "ooresvi-filU NOkf[IdAROUNA NCDtNR-))WQ Iufoririatzon Processing; Unit L617 Marl Service Center - Raleigh;. N' It'll- O-. . . I . ZW OA-V 19 RIICKYJIIV TE,,EPI 8 , �A"64j 64441 POST-OFFICEBOX 878 .mo P P, r-S V, I LtE„ NP ; 811 S4b t-ZOIOAnnual' Sludge Report, ,WQ,0'014136.,Town ofMooresvdie..Residuals"Land-Appfication Prqgram-Amended report due to,'spreadsheet.,eatculaiioft-,,error FbllbWii,ig-is--the-inforrnation,requested --toaccompany our .Land Application, rep ,M ilit ale, � Y. -Ro4yRi-ver Wastewater Ti atitift Facility 369 J,olirisonDa-i�x'y,-�k'4' Moor,esvill,p,-,N,;' GI-2, , 84'15 Phoifd,--'-704.:662-8,4-7-o Responsible official and facility _contact TOM Wynn, 'glosdids -Coordinator P.O. ROx 8718; Mooresvillei,NC'M15 phohpr--704499-4054 (Nitt-A),'afid „Patt B), No, Land Application for 20I'6'-,underTemiit W00014136 A11. sew . ge sludge Was'deWatdred and takeh t6-,,alined land tilt for: disposal'. Total. tans:=.3343,.5-(S.ee, attached hauling svmm" -sheet};, ary, Laboratory results from TOLP`_are included in _this rep6ft; (part C). Dcertify,,Jihd& Oafialty:of Idw.thqt,the!above;informatio,n,is,, la the best of rAy knowledge. and befiefl.truo and accurate. and Oornpl!ae. L a-m..'aw-areAhatIhdke are significant penalties f6r - submittina false information, iripludingft p ssibffity Of fries and itriprisom-nen tfknowing, , owing, violadons' 1r06-red by-.% -Tom E. W. na, as70H&Coordinator Rivf6we'd.,by: Jamie Uvi§, EhVir. Coftliande Supervisor; 2016 LANDFILL SLUP6E TOTAL, ,Diatef Loads..�auled Qdantityftofis)� Av&.ageperload January. 7Haulier!k S 3' 6T 4. 22<41 1,/6/,2-0,16-,, �S 5 90,.,92 1/19/20'I6, s 6 117.,51 19.65 Monthly Total f4 276-.07 Febtqaxy 2/5/2016 -S. .4 80.61 20.15 2/19/20167 S, 4 76;.46 19,12 16,54 20.69 Mbhift, TOta"L 16 322.57 19.99 March ,3A/20161 - " ; s A 84.77 21.59 3/7120I6 S. 4 93.9.5 70199'. 3/8/2016,; s & 127.16 3129no16- S 9 172.03, 21- M-onthly'46tal' 21 447.91 21.32. April 4/1/2016L 5 4 26.03 3-. 71.61 23.87 �.87 M 20A E4 "tR gROMMM "own, 887 5 VMMRilu 9T - 4/29/2016 s .5.1 96.54.19.31 Monthly Total. -1.9. 376.19 16.21- may 5/2/2616 S. 61 142.59 23.77 5/3/2016 s 5 105.54, 21M. 5/5/2'016 8 . 26.2 .2 1 Q 1 8 5/6/2016 s 79.39 R -26.46 5/10/2016 s I94.96: 24.37 5/13/2016 s 4 66-.92 16.73 5A712016 s 8 24,12 2, 44.94 22.47 5/20/2016 s 1 21.39 21.39 5/24/2616 2(139 2133 Monthly total 22.aQ - ---------- June NO'HAULING Monthlylotal 0' 0 0.00 July 7/7/1016 SAB 2 22.72 11.3.6 201& l;ANF3FILi. SLUOGE TOTAL: 7/8/2416 SAB 3 - 31`9' 1063 r 13 7Q Monthly TotaC - _ 20 25Q':66 12 39 August: 421 21.05. ,8j9/2.016� S�1B: 2 353 17 65 8/11/2016` S 3... 733 8/17/2Q16 S 5' 11896: _ . 23.74' Z2 _ ._ - 269661.73 . September . - - , 9/3/2016 - S, 4 84:.84 21.22: Monthty.Total 8486; October. 1tl/21/ t71fi 5 . 4 .7 92 I�iontily Total': . '_ 4: 76.92.. NQVbmb6e 11/1%201G. S, 4: 73 82:. 18.46 22.94. 11/30/2016 :SAB? 6. �4.95 1416 Mortithly Total 18' 34231 20.70 Decemiger mo.Haulin"g Monthiy Total S Q ,0l 0.00 Year Totals; 167, 334ZZ1 16.31 .. _ :. ,. M Mooresville' * S. = SYNAGRO Q W-�A Bid .- * AB Class A&B:'Mixed 2017 Landfill Sludge Total 7/14/2017 S 4 79.32 19.83 7/17/2017 S 1 18.36 18.36 Monthly Total 12 249.07 20.33 August 8/25/2017 S 2 36.48 18.24 Monthly Total 2 36.48 18.24 September No Hauling Monthly Total 0 0 0.00 October 10/21/2016 S 4 76.92 19.23 Monthly Total 4 76.92 19.23 November No Hauling Monthly Total 0 0 0.00 December 12/20/2017 S 4 94.88 23.72 Monthly Total 4 94.88 23.72 Year Totals 149 3290.99 19.63 Corrected for % solids 0.14 460.74 dry metric tons 417.97 * M - Mooresville * S - SYNAGRO * AB - Class A&B Mixed I Full -Service Analytical & M � j Environmental Solutions LABORATORIES, INC. Town of Mooresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC certification No. 99012 Project: Class B Sludge Lab Submittal Date: 12/14/2016 Prism Work Order. 6120257 Case Narrative 01 /02/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. i Terri W. Cole Project Manager Reviewed By Terri W. Cole Project Manager Data Qualifiers Key Reference: CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525.0409 Page 1 of 11 I Full -Service Analytical & Environmental Solutions LABORATORM Sample Receipt Summary 01 /02/2017 Prism Work Order: 6120257 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Class B 6120257-01 Solid 12/13/16 12/14/16 Samples were received in good condition at 2.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/526-0409 Page 2 Of 11 Full Service Analytical & Laboratory Report/,®I M I Environmental Solutions 01/02/2017 L.,, � LABORATORIES, INC. Town of Mooresville/RR WWTP Project: Class B Sludge Client Sample ID: Class B Attn: Whitney Munroe Prism Sample ID: 6120257-01 P. O. Box 878 Prism Work Order: 6120257 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 12/13/16 06:42 Time Submitted: 12/14/16 12:25. Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 14.1 % by 0.100 0.100 1 'SM2540 G 12/21/16 16:13 JLB P61-0378 Weight Paint Filter Liquids Pass g 1.0 0.0 1 '9095A 12/20/16 11:03 SLS P61-0327 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL mg/kg dry 0.35 0.039 1 "8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1221 BRL mg/kg dry 0.71 0.28 1 '8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1232 BRL mg/kg dry 0.71 0.092 1 `8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1242 BRL mg/kg dry 0.35 0.094 1 '8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1248 BRL mg/kg dry 0.35 0.071 1 '8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1254 BRL mg/kg dry 0.35 0.088 1 '8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1260 BRL mg/kg dry 0.35 0.045 1 '8082A 12/29/16 14:27 JMC P61-0446 Surrogate Recovery Control Limits Tetrachloro-m-xylene 83 % 36-182 Decachlorobiphenyl 95 % 34-182 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 ZHE 12/20/16 10:00 ANG P61-0305 TCLP Extraction Complete N/A 1 *1311 12/20/16 6:40 JAB P61-0315 TCLP Metals Mercury BRL mg/L 0.010 0.000030 1 '7470A 12/20/16 12:39 JAB 1361-0321 Arsenic BRL mg/L 0.050 0.012 1 '6010D 12/21/16 17:19 bgm P61-0326 Barium BRL mg/L 5.0 0.0065 1 '6010D 12/21/16 17:19 bgm P61-0326 Cadmium BRL mg/L 0.025 0.00065 1 `6010D 12/21/16 17:19 bgm P61-0326 Chromium BRL mg/L 0.25 0.0038 1 `6010D 12/21/16 17:19 bgm P61-0326 Lead BRL mg/L 0.050 0.0080 1 `6010D 12/21/16 17:19 bgm P61-0326 Selenium BRL mg/L 0.10 0.022 1 '6010D 12/21/16 17:19 bgm P61-0326 Silver BRL mg/L 0.25 0.00050 1 '6010D 12/21/16 17:19 bgm 1361-0326 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRLCCV mg/L 0.0025 0.000094 1 '8081B 12/28/16 14:22 JMC P61-0364 Dieldrin BRL mg/L 0.00050 0.000022 1 '8081B 12/28/16 14:22 JMC P61-0364 Endrin BRL mg/L 0.00050 0.000020 1 `8081B 12/28/16 14:22 JMC P61-0364 gamma-BHC BRL mg/L 0.00050 0.000013 1 '8081B 12/28/16 14:22 JMC P61-0364 Heptachlor BRL mg/L 0.00050 0.000015 1 '8081 B 12/28/16 14:22 JMC P61-0364 Heptachlor Epoxide BRL mg/L 0.00050 0.000018 1 '8081 B 12/28/16 14:22 JMC P61-0364 Methoxychlor BRL mg/L 0.00050 0.000033 1 '8081B 12/28/16 14:22 JMC P61-0364 Toxaphene BRL mg/L 0.025 0.00032 1 '8081B 12/28/16 14:22 JMC P61-0364 Surrogate Recovery Control Limits Decachlorobiphenyl 53 % 13-186 Tetrachloro-m-xylene 78 % 40-134 TCLP Semivolatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 Of 11 Laboratory Report R. I Fun -Service Analytical & r SM Environmental Solutions 01/02/2017 _,.-ORATCRIE; INC. Town of Mooresville/RR WWTP Project: Class B Sludge Client Sample ID: Class B Attn: Whitney Munroe Prism Sample ID: 6120257-01 P. O. Box 878 Prism Work Order: 6120257 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 12/13/16 06:42 Time Submitted: 12/14/16 12:25 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst Date/Time Batch ID 2,4,5-Trichlorophenal BRL mg/L 0.25 0.0016 1 `8270D 12/21/16 23:57 JMV P61-0357 2,4,6-Trichlorophenal BRL mg/L 0.10 0.0018 1 '8270D 12/21/16 23:57 JMV P61-0357 2,4-Dinitrotoluene BRL mg/L 0.050 0.0014 1 '8270D 12/21/16 23:57 JMV P61-0357 2-Methylphenol BRL mg/L 0.050 ' 0.0018 1 '8270D 12/21/16 23:57 JMV P61_0357 3/4-Methylphenol BRL mg/L 0.050 0.0015 1 '8270D 12/21/16 23:57 JMV P61_0357 Hexachlorobenzene BRL mg/L 0.050 0.0013 1 `8270D 12/21/16 23:57 JMV P61_0357 Hexachlorobutadiene BRL mg/L 0.050 0.0021 1 "8270D 12/21/16 23:57 JMV P61_0357 Hexachloroethane BRL mg/L 0.050 0.0017 1 '8270D 12/21/16 23:57 JMV P61-0357 Nitrobenzene BRL mg/L 0.050 0.0026 1 '8270D - 12/21/16 23:57 JMV P61_0357 Pentachlorophenol BRL mg/L 0.25 0.0012 1 '8270D 12/21/16 23:57 JMV P61_0357 Pyridine BRL mg/L 0.25 0.0010 1 '8270D 12/21/16 23:57 JMV P61-0357 Surrogate Recovery Control Limits 2,4,6-Tribromaphenol 65 % 43-140 2-Fluorobiphenyl 53 % 44-119 2-Fluorophenol 28 % 19-119 Nitrobenzene-d5 48 % 44-120 Phenol-d5 19 % 11-52 Terphenyl-d14 64 % 50-134 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg/L 0.035 0.00083 1 '8260B 12/21/16 17:21 KDM P61_0370 1,2-Dichloroethane BRL mg/L 0.025 0.00066 1 '8260B 12/21/16 17:21 KDM P61_0370 1,4-Dichlorobenzene BRL mg/L 0.38 0.00050 1 `8260B 12/21/16 17:21 KDM P61_0370 Benzene BRL mg/L 0.025 0.00048 1 `8260B 12/21/16 17:21 KDM P61-0370 Carbon Tetrachloride BRL mg/L 0.025 0.0011 1 '8260B 12/21/16 17:21 KDM 1361-0370 Chlorobenzene BRL mg/L 5.0 0.00062 1 '8260B 12/21/16 17:21 KDM P61_0370 Chloroform BRL mg/L 0.30 0.00076 1 '8260B 12/21/16 17:21 KDM P61_0370 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0024 1 '8260B 12/21/16 17:21 KDM P61_0370 Tetrachloroethylene BRL mg/L 0.035 0.00098 1 '8260B 12/21/16 17:21 KDM P61_0370 Trichloroethylene BRL mg/L 0.025 0.00078 1 '8260B 12/21/16 17:21 KDM P6L0370 Vinyl chloride BRL mg/L 0.020 0.00097 1 '826013 12/21/16 17:21 KDM P61_0370 Surrogate Recovery Control Limits 4-13romofluorobenzene 97 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 113 %. 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041525-0409 Page 4 of 11 Sample Extraction Data Prep Method: Default Prep GenChem Lab Number Batch Initial Final Date/Time 6120257-01 P61-0327 100 g 100 mL 12/20/16 11:03 Prep Method: Solids, Dry weight Lab Number Batch Initial Final Date/Time 6120257-01 P6L0378 30 g 30 g 12/21/16 16:13 Prep Method: 3550C GC Lab Number Batch Initial Final Date/Time 6120257-01 P61-0446 30.08 g 10 mL 12/29/16 8:45 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 6120257-01 P6L0305 25 g 500 mL 12/19/16 15:00 6120257-01 P6L0315 100 g 2000 mL 12/19/16 14:30 Prep Method:3010A Lab Number Batch Initial Final Date/Time 6120257-01 P6L0326 10 mL 50 mL 12/20/16 9:45 Prep Method:7470A Lab Number Batch Initial Final Date/Time 6120257-01 P6L0321 20 mL 30 mL 12/20/16 8:00 Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 6120257-01 P61-0364 200 mL 10 mL 12/21/16 15:15 Prep Method: 3610C MS Lab Number Batch Initial Final Date/Time 6120257-01 P61-0357 200 mL 1 mL 12/21/16 12:20 Prep Method: 6030B Lab Number Batch Initial Final Date/Time 6120257-01 P6L0370 1 mL 10 mL 12/21/16 8:43 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 6120257-01 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/626-0409 Page 5 Of 11 ` Full -Service CHAIN ®F CUSTODY RECORD PRISMEnvironmental Solutions PAGE_ OF QUOTE # TOO ENSURE PROPER BILLING: LABORATORIES, INC Oj 95 `� 449 Springbrook Road • Charlotte, NC 28217 Project Name: r`a ,i Y •/'�� V Phone 704/529-6364 - Fax: 7041525-0409 Short Hold Analysis: a (NO) UST Project: (Yes) Client Company Name: Dom_®� !v A �I��— 'Please ATTACH any project specific reporting (QC LEVE01 III IV) provisions and/or QC Requirements Report To/Contact Name: t UPIf jD®. ® 8 Invoice To: � Ott.. ®� %� ®"w , ar- t�� Reporting Address: Address: YES NO NIA Samples INTACT upon arrival? O Received ON WET ICE? PROPER PRESERVATIVES Indicated? Received WITHIN HOLDING TIMES? _ N CUSTODY.SEALS,INTACT?` a VOLATILES reed W/OUT'HEAbSPACE? FIR PI R CONTAINERS.used? fc.MP Therm ID �� _ Observed : ' C h Corr 2, �1°G Phone: 3►1700 3231v Fax (Yes)`(No e:_ Purchase Order No.lBilling Reference Email Address: I� aoM0WK" �i2 . i11C oUl� Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days EDD Type: PD _EXCeI_Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush Work Must Be Pre -Approved Site Location Name: Samples received after 14:00 will be processed next business day. Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC DoD FL NC SC OTHER N/A / Water Chlorinated: YES_ NO P/ / Sample Iced Upon Collection: YES ✓ NO p p CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA- TIVES ANALYSIS REQUESTED �7 , o � � �\ MARXS a .�!o �� PRISM LAB ID NO. *TYPE SEE BELOW NO. SIZE Sampler's Signa re 1, � Sampled By (Print Name) �/ �� Affiliation , . . • Site Arrival Time: Upon relinquishing, this Chain of Custody is your authorization for Prism to p o eed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for a y changes after analyses have been initialized. R inquis ed By: (Signature Received By: (Signal e) Date t Military/Hours Additional Comments: SitB.DBparture.T.ime�:.. .: , R linqulshed By: (S n lure) Received By: (Signature) Date ee Field Tech Fll Relinquished By: (Signature) celved For nsm Laboratories By: Date j,, j V C .�j Mileage: _ Method of Shipment: NOTE: A L SAMPLE C LERS SHOULD BE TAPED SHUT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. SAMPLES ARE NOT CEPTED AND VERIFIED AGAINST C UNTIL RECEIVED AT THE LABORATORY. ❑ Fed Ex ❑ UPS ❑ Hand -delivered Prism Field Service ❑ Other COG Group No. NPDES' IU ST: GROUNDWATER: DRINKING VVATER: SOLID WASTE: RIC GERGLA LANUtILL U I t1ER: ❑NC❑SC NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NCOSC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ACCESS ANAL Y` TUCAL.i. 11gc. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECT ID 6120257 LABORATORY REPORT NUMBER 1612F67 Primary Data Review By Chris Pafford Project Manager, AES DATE December 22, 2016 Secondary Data Review By Ashley Amick Project Manager, Access Analytical aamickpaaxs-inc.com PLEASE NOTE: - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDIIEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 1 of 5 Page 7 of 11 E f Fa Full -Service Analytical & SM I Environmental Solutions � VIeORATORIE$ INC. SUBCONTRACT ORDER /(0 0 Certifi io NELAC_ USACE Prism Laboratories, Inc. SC Other 61120257 SENDING LABORATORY: RECEIVING .LABORATORY: Prism Laboratories, Inc. Analytical Environmental Services, Inc. P. O. Box.240543 3080 Presidential Parkway Charlotte, NC 28224-0543 Atlanta, GA 30340 Phone: 800-529-6364 Phone :(770) 457-8177 Fax: 704-525-0409 Fax: NA Project Manager: Ten? W. Cole Analysis Due Expires Laboratory ID Comments Sample ID: 6120257-01 Solid Sampled:l2/13/16 06:42` Herbicides TCLP (Sub) 12/20/16 06:42 Containers Supplied: t v-&- 1� // `(/ I �v /elb Foll'eased By Date ' / YReceived By Dat6 Released By ate' Received By /✓� Date Released By Date Received By C Gt Date Released By Date Received By Date age 2 or 5 Analytical Environmental Services, Inc Date: 22-Dec-16 Client: Prism Laboratories Client Sample ID: CLASS B Lab Order 1612F67 Tag Number: 6120257-01 Project Name: 6120257 Collection Date: 12/13/2016 6:42:00 AM Lab ID: 1612F67-001A Matrix: Solid Analyses Result Qual MDL Reporting Limit Units BatchID DF Date Analyzed Analyst HERBICIDES, TCLP SW1311/8151A (SW3510C) 2,4,5-TP (Silvex) BRL 0.064 0.20 mg/L 235131 1 12/21/2016 17:02 AW 2,4-D BRL 0.076 0.20 mg/L 235131 1 12/21/201617:02 AW Surr: DCAA 79.5 0 50.1-132 %REC 23513I 1 12/21/2016 17:02 AW Qualifiers: " value exceeds maximum contaminant level BRL Not Detected at MDL H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank E Estimatedvalue above quantitation range S Spike Recovery outside limits due to matrix > Greater than Result value J Estimated value detected below Reporting Limit t Less than Result value Page 3 of 5 E Page 9 of 11 Analytical Environmental Services, Iuc.- Sample%Cooler Receipt Checldist Client �l "�'� Work Order Number Checklist completed by Sign a ate Carriername:FedEx UPS_ Courier_ Client,_ USMaiI_ Other Shipping container/cooler in good condition? Yes ✓ No _ Not Present _ Custody seals intact on shipping container/cooler? Yes _ No _ Not Present ✓ Custody seals intact on sample bottles? Yes _ No _ Not Present "/ Container/Temp Blauktemperatureincompliance? (0°<_6°C)*Yes ✓ No _ Cooler #1 - II °- Cooler #2 Cooler #3 Cooler #4 Cooler#5 Cooler #6 Chain of custody present? Yes /� No Chain of custody signed when relinquished and received? Yes t/ No _ Chain of custody agrees with sample labels? Yes No _ Samples in proper containeribottle? Yes No _ Sample containers intact? Yes No _ Sufficient sample volume for indicated test? Yes No _ All samples received within holding time? Yes l/ No _ Was TAT marked on the COC7 Yes , No v Proceed with Standard TAT as per project history? Yes o _ Not Applicable _ water - VOA vials have zero headspace? No VOA vials submitted _ Yes — No _ Water - pH acceptable upon receipt? Yes _ No _ Not Applicable T Adjusted? Checked by Sample Condition: Good_ Other(Explain) (For diffusive samples or ARIA lead) Is a known blank included? Yes _ No — See Case Narrative for resolution of the Non -Conformance. Samples do nothave to comply with the given range for certain paramoters. \1Aes server\11SampleReceiptVyDocuznentACOCs andpHAdjustmentSheet\Samplo Cooler RodptChecklist Revl.rtf Page 4 of 5 Analytical Environmental Services, Inc Client: Prism Laboratories Project Name: 6120257 Worlcorder: 1612F67 Date: 22-Dec-16 ANALYTICAL QC SUMMARY REPORT BatchlD: 235131 Sample ID: NIB-235131 Client ID: Units: mg/L Prep Date: 12/20/2016 Run No: 332718 SampleType: MBLK TestCode: HERBICIDES, TCLP SW1311/8151A BatchlD: 235131 Analysis Date: 12/21/2016 Seq No: 7249626 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) BRL 0.20 2,4-D BRL 0.26 Surr: DCAA 0.3855 0 0.5000 77.1 50.1 132 Sample ID: LCS-235131 Client ID: Units: mg/L Prep Date: 12/20/2016 Run No: 332718 SampleType: LCS TestCode: IIERB1CIDEs, TCLP SW131118151A BatchID: 235131 Analysis Date: 12/21/2016 Seq No: 7249627 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 0.4033 0.20 0.5000 80.7 50.7 117 2,4-D 0.4238 0.20 0.5000 84.8 50.1 119 Surr: DCAA 0.3983 0 0.5000 79.7 50.1 132 Sample ID: 1612F67-001AMS Client ID: CLASS B Units: mg/L Prep Date: 12/20/2016 Run No: 332718 SampleType: MS TestCode: HERBICIDES, TCLP SW1311/8151A BatchID: 235131 Analysis Date: 12/21/2016 Seq No: 7250398 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 0.4357 0.20 0.5000 87.1 46.3 126 2,4-D 0.5359 0.20 0.5000 107 43.3 132 Surr: DCAA 0.4266 0 0.5000 85.3 50.1 132 Qualifiers: > Greater than Result value < Less than Result value B Analyte detected in the associated method blank (Q (D BRL Below, reporting limit E Estimated (value above quantitatiou range) H Holding times for preparation or analysis exceeded J Estimated value detected below Reporting Limit N Analyte not NELAC certified R. RPD outside limits due to matrix page 5 of 5 Rpt Lint Reporting Limit S Spike Recovery outside limits due to matrix Town of Mooresville NORTH CAROLINA NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699 01/26/17 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 INCDgNR►®W� MOORESVILLER(Ci$Y (017 WQROS MOORESVILLE REGIONAL OFFICE Subject: 2016 Annual Sludge Report, WQ0014136 Town of Mooresville Residuals Land Application Program Following is the information requested to accompany our Land Application report. Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy Rd. Mooresville, N.C. 28115 Phone: 704-662-8470 Responsible official and facility contact — Tom Wynn, Biosolids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-799-4054 (Part A) and (Part B) No Land Application for 2016 under Permit WQ0014136. All sewage sludge was dewatered and taken to a lined land fill for disposal. Total tons = 6410.9 (See attached hauling summary sheet). Laboratory results from TCLP are included in this report. (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Tom E. Wynn, Biosolids Coordinator Reviewed by: Jamie Levis, Envir. Compliance Supervisor Signat e: E Date Signa re: -.7 — 2 Date 2016 LANDFILL SLUDGE TOTAL Date Hauler* Loads hauled Quantity (tons) Average per load January 1/5/2016 S 3 67.24 22.41 1/6/2016 S 5 90.92 18.18 1/29/2016 S 6 117.91 19.65 Monthly Total 14 276.07 20.08 February 2/5/2016 S 4 80.61 20.15 2/19/2016 S 4 76.46 19.12 2/26/2016 S 8 165.5 20.69 Monthly Total 16 322.57 19.99 March 3/4/2016 S 3 64.77 21.59 3/7/2016 S 4 83.95 20.99 3/8/2016 S 6 127.16 21.19 3/29/2016 S 8 172.03 21.50 Monthly Total 21 447.91 21.32 April 4/1/2016 S 4 80.11 20.03 4/5/2016 S 3 71.61 23.87 4/22/2016 SA 2 27.55 13.78 4/23/2016 ° SA 2- 20.55 10.28 4/25/2016 SA 8 79.87 9.98 4/29/2016 S 5 96.54 19.31 Monthly Total 19 376.23 16.21 May 5/2/2016 S 6 142.59 23.77 5/3/2016 S 5 105.54 21.11 5/5/2016 S 1 26.28 26.28 5/6/2016 S 3 79.39 26.46 5/10/2016 S 8 194.96 24.37 5/13/2016 S 4 66.92 16.73 5/17/2016 S 8 192.98 24.12 5/19/2016 S 2 44.94 22.47 5/20/2016 S 1 21.39 21.39 5/24/2016 S 1 21.33 21.33 Monthly Total 39 896.32 22.80 June NO HAULING Monthly Total 0 0 0.00 July 7/7/2016 SAB 2 22.72 11.36 7/8/2016 SAB 3 31.9 10.63 2016 LANDFILL SLUDGE TOTAL 7/13/2016 SAB 2 27.4 13.70 7/20/2016 SA 10 128.44 12.84 7/21/2016 SA 3 40.2 , 13.40 . Monthly Total 20 250.66 12.39 August 8/9/2016 S 2 42.1 21.05 8/9/2016 SAB 2 35.3 17.65 8/11/2016 S 3 73.3 24.43 8/17/2016 S 5 118.96 23.79 Monthly Total 12 269.66 21.73 September 9/13/2016 S 4 84.86 21.22 Monthly Total 4 84.86 21.22 October 10/21/2016 S 4 76.92 19.23 Monthly Total 4 76.92 19.23 November 11/1/2016 S 4 73.82 18.46 11/9/2016 S 8 183.54 22.94 11/30/2016 SAB 6 84.95 14.16 Monthly Total 18 342.31 20.70 December No Hauling #DIV/0! Monthly Total S 0 0 #DIV/0! Year Totals 325 6410.95 #DIV/0! * M - Mooresville * S - SYNAGRO * A - Class A Biosolid * AB - Class A&B Mixed *P; ism ABORATORIES, INC. Full -Service Analytical & Environmental Solutions Town of Mooresville/RR WWTP Whitney Munroe P. O. Box 878 Mooresville, NC 2811'5 NC Certification No. 402 NC Drinking Water Cart No. 37735 SC Certification No. 99012 Project: Class B Sludge Lab Submittal Date: 12/14/2016 Prism Work Order: 6120257 Case Narrative 01 /02/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Terri W. Cole Project Manager Data Qualifiers Key Reference: Reviewed By Terri W. Cole Project Manager CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/629-6364 - Fax: 704/525-0409 Page 1 of 11 9R FullService Analytical s i Environmental Solutions LABORATORIES, INQ Sample Receipt Summary 01 /02/2017 Prism Work Order: 6120257 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Class B 6120257-01 Solid 12/13/16 12/14/16 Samples were received in good condition at 2.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-800/629-6364 - Fax: 704/526-0409 Page 2 of 11 Laboratory Report r �n Full -Service Analytical & R I 1 V 1 Environmental Solutions 01/02/2017 � +'-IABOPATOPIE$ ING Town of Mooresville/RR WWTP Project: Class B Sludge Client Sample ID: Class B -, Attn: Whitney Munroe Prism Sample ID: 6120257-01 P. O. Box 878 Prism Work Order: 6120257 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 12/13/16 06:42 Time Submitted: 12/14/16 12:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 14:1 % by 0.100 0.100 1 *SM2540 G 12/21/16 16:13 -JLB P61-0378 Weight Paint Filter Liquids Pass g 1.0 0.0 1 *9095A 12/20/16 11:03 SLS P6LO327 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL mg/kg dry 0.35 0.039 1 *8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1221 BRL mg/kg dry 0.71 0.28 1 *8082A 12/29/16 14:27 JMC P6L0446 Aroclor 1232 BRL mg/kg dry 0.71 0.092 1 *8082A 12/29/16 14:27 JMC P6L0446 Aroclor 1242 BRL mg/kg dry 0.35 0.094 1 *8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1248 BRL mg/kg dry 0.35 0.071 1 *8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1254 BRL mg/kg dry 0.35 0.088 1 *8082A 12/29/16 14:27 JMC P61-0446 Aroclor 1260 BRL mg/kg dry 0.35 0.045 1 *8082A 12/29/16 14:27 JMC P61-0446 Surrogate Recovery Control Limits Tetrachloro-m-xylene 83 % 36-182 Decachlorobiphenyl 95 % 34-182 TCLP Extraction by EPA 1311 TCLP Extraction Complete N/A 1 *1311 ZHE 12/20/16 10:00 ANG P61-0305 TCLP Extraction Complete N/A 1 *1311, 12/20/16 6:40 JAB P6L0315 TCLP Metals Mercury BRL mg/L 0.010 0.000030 1 *7470A 12/20/16 12:39 JAB . P61-0321 Arsenic BRL mg/L 0.050 0.012 1 *6010D 12/21/16 17:19 bgm P6L0326 Barium BRL mg/L 5.0 0.0065 1 *6010D 12/21/16 17:19 bgm PGL0326 Cadmium BRL mg/L 0.025 0.00065 1 *6010D 12/21/96 17:19 bgm P61-0326 Chromium BRL mg/L 0.25 0.0038 1 *6010D 12/21/16 17:19 bgm P61-0326 Lead BRL mg/L 0.050 0.0080 1 *6010D 12/21/16 17:19 bgm P6L0326 Selenium BRL mg/L 0.10 0.022 1 *6010D 12/21/16 17.19 bgm P61-0326 Silver BRL mg/L 0.25 0.00050 1 *6010D 12/21/16 17:19 bgm P61-0326 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRLCCV mg/L 0.0025 0.000094 1 *8081B 12/28/16 14:22 JMC P6L0364 Dieldrin BRL mg/L 0.00050 0.000022 1 *8081B 12/28/16 14:22 JMC P61-0364 Endrin BRL mg/L 0.00050 0.000020 1 *8081B 12/28/16 14:22 JMC P61-0364 gamma-BHC BRL mg/L 0.00050 0.000013 1 *8081B 12/28/16, 14:22 JMC P61-0364 Heptachlor BRL mg/L 0.00050 0.000015 1 *8081B 12/28/16 14:22 JMC P6LO364 Heptachlor Epoxide BRL mg/L 0.00050 0.000018 1 *8081B 12/28/16 14:22 JMC P6L0364 Methoxychlor BRL mg/L 0.00050 0.000033 1 *8081B 12/28/16 14:22 JMC P61-0364 Toxaphene BRL mg/L 0.025 0.00032 1 *8081B 12/28/16 14:22 JMC P61-0364 Surrogate Recovery Control Limits Decachlorobiphenyl 53 % 13-186 Tetrachloro-m-xylene 78 % 40-134 TCLP Semivolatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 11 Laboratory Report dP I Analytical & 01/02/2017 EFull Environmental Solutions nvironmental "L -RATORIES, ING Town of Mooresville/RR WWTP Project: Class B Sludge Client Sample ID: Class B Attn: Whitney Munroe Prism Sample ID: 6120257-01 P. O. Box 878 Prism Work Order: 6120257 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 12/13/16 06:42 Time Submitted: 12/14/16 12:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 2,4,5-Trichlorophenol BRL mg/L 0.25 0.0016 1 *8270D 12/21/16 23:57 JMV P61-0357 2,4,6-Trichlorophenol BRL mg/L 0.10 0.0018 1 *8270D 12/21/16 23:57 JMV P61-0357 2,4-Dinitrotoluene BRL mg/L 0.050 0.0014 1 *8270D 12/21/16 23:57 JMV P61-0357 2-Methylphenol BRL mg/L 0.050 0.0018 1 *8270D 12/21/16 23:57 JMV P61-0357 3/4-Methylphenol BRL mg/L 0.050 0.0015 1 *8270D 12/21/16 23:57 JMV P6L0357 Hexachlorobenzene BRL mg/L 0.050 0.0013 1 *8270D 12/21/16 23:57 JMV P61-0357 Hexachlorobutadiene BRL mg/L 0.050 0.0021 1 *8270D 12/21/16 23:57 JMV P6L0357 Hexachloroethane BRL mg/L 0.050 0.0017 1 *8270D 12/21/16 23:57 JMV P6L0357 Nitrobenzene BRL mg/L 0.050 0.0026 1 *8270D 12/21/16 23:57 JMV P61-0357 Pentachlorophenol BRL mg/L 0.25 0.0012 1 *82700 12/21/16 23:57 JMV P61-0357 Pyridine BRL mg/L 0.25 0.0010 1 *8270D 12/21/16 23:57 JMV P61-0357 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 65 % 43-140 2-Fluorobiphenyl 53 % 44-119 2-Fluorophenol 28 % 19-119 Nitrobenzene-d5 48 % 44-120 Phenol-d5 19 % 11-52 Terphenyl-d14 64 % 50-134 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRL mg/L 0,035 0.00083 1 *8260B 12/21/16 17:21 KDM P61-0370 1,2-Dichloroethane BRL mg/L 0.025 0.00066 1 *8260B 12/21/16 17:21 KDM P61-0370 1,4-Dichlorobenzene BRL mg/L 0.38 0.00050 1 *8260B 12/21/16 17:21 KDM P61-0370 Benzene BRL mg/L 0.025 0.00048 1 *8260B 12/21/16 17:21 KDM PBL0370 Carbon Tetrachloride BRL mg/L 0.025 0.0011 1 *8260B 12/21/16 17:21 KDM P61-0370 Chlorobenzene BRL mg/L 5.0 0.00062 1 *8260B 12/21/16 17:21 KDM P61-0370 Chloroform BRL mg/L 0.30 0.00076 1 *8260B 12/21/16 17:21 KDM P61-0370 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.0024 1 *826013 12/21/16 17:21 KDM P6L0370 Tetrachloroethylene BRL mg/L 0.035 0.00098 1 *8260B 12/21/16 17:21 KDM P61-0370 Trichloroethylene BRL mg/L 0.025 0.00078 1 *8260B 12/21/16 17:21 KDM P61-0370 Vinyl chloride BRL mg/L 0.020 0.00097 1 *8260B 12/21/16 17:21 KDM P61-0370 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 113 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/625-0409 Page 4 of 11 Sample Extraction Data Prep Method: Default Prep GenChem Lab Number Batch Initial Final Date/Time 6120257-01 P61-0327 100 g 100 mL 12/20/16 11:03 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 6120257-01 P61-0378 30 g 30 g 12/21/16 16:13 Prep Method: 3550C GC Lab Number Batch Initial Final Date/Time 6120257-01 P61-0446 30.08 g 10 mL 12/29/16 8:45 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 6120257-01 P61-0305 25 g 500 mL 12/19/16 15:00 6120257-01 P61-0315 100 g 2000 mL 12/19/16 14:30 Prep Method: 3010A Lab Number Batch Initial Final Date/Time 6120257-01 P61-0326 10 mL 50 mL 12/20/16 9:45 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 6120257-01 P61-0321 20 mL 30 mL 12/20/16 8:00 Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 6120257-01 P61-0364 200 mL 10 mL 12/21/16 15:15 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 6120257-01 P61-0357 200 mL 1 mL 12/21/16 12:20 Prep Method: 5030B Lab Number Batch Initial Final Date/Time 6120257-01 1261-0370 1 mL 10 mL 12/21/16 8:43 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 6120257-01 Herbicides TCLP (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Page 5 of 11 Phone: 704I529-6354 -Toll Free Number: 1-800/529-6364 -Fax: 704/525-0409 CHAIN OF CUSTODY RECORD iFull -Service Analytical & I S M x'': Environmental Solutions PAGE OF _ QU807E # TOO ENSURE PROPER BILLINGr LABORAI'01`1IE4. INC n f �� .• �Q 449 Springbrook Road - Charlotte, NC 213217 Project Name: Phone 7041529.6364 - Fax: 704/525-0409 Short Hold Analysis: a (No) UST Project: (Yes) Client Company Name: To *Please ATTACH any project specific reporting (QC LEVE0i Ill IV) provisions and/or QC Requirements 11 Report To/Contact Name: 1 u4IB0. • p P. 8 Invoice To: ifdui. o �I� � ®oCL'bw� l� Reporting Address: . ®• D Address: eon& i lka W- -Ul YES N0 AIASamples INTACT upon arnval? Received ON WET ICE?,• PROPER PRESERVATIVES indicated?— Received WITHIN HOLDING TIMES?,—.JSTODYtSEALSINTACTY"VDLATILESTecd WlOUT HEADSPACE? 7. PROPER 6&hTAINERS used? TEMP ThermlD:I observed _°C !:Corr Phone:3'i-9 W 32Jk Fax (Yes)•(NM:a Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Email Address: lr.1r1�Dmf� . IBC •tA�, Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC EDD Type: PD _Excel_Other Rush Work Must Be "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ pre -Approved Sc OTHER N/A Site Location Name: Samples received after 14:00 will be processed next business day. / Site Location Physical Address: Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Water Chlorinated: YES_ NO V / RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced on Collection: YES ✓ NO p p CLIENT DATE TIME COLLECTED MATRIX (SOIL, SAMPLE CONTAINER PRESERVA- ANALYSIS. REQUESTED PRISM *TYPE NO. SIZE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES ARKS LAB ID NO. HOURS SLUDGE) SEE BELOW ��441/k�vo)A�/tem AN, 50 e, �d !✓� KAA/ Sampler's Signa re Sampled By (Print Name) Affiliation Upon relinquishing, this Chain of Custody Is your authorization for Prism to p ogeed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for aiy changes after analyses have been initialized. R inquis ed B : (Sig)ature Received By: (Sign at ) / Date J Military/Hours Additional Comments: Sitr3.Ar�ival Time:' - �t R Ilnquished By: (S n ure) Received By: (Signature) Date ' Site Departure:Tim..e: Relinquished By: (Signature)!, l �l celved For rism Laboratories By, Date 4 � �� ^L� Reid Tech. Fee 'Mileage: Method of Shipment: NOTE: A L SAMPLE C LERS SHOULD BE TAPED SHUT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. coc Group No. SAMPLES ARE NOT CEPTED AND VERIFIED AGAINST C UNTIL RECEIVED AT THE LABORATORY. ❑ Fed Ex ❑ UPS ❑ Hand Prism Field Service ❑ Other I a1 V `G1 J -delivered ❑ NC ❑ SC ❑ NC ❑ SC El NC ❑ SCT tR• El NC I El SCATE�: I a NC El SC E' ❑❑ NC ❑ SC ❑❑ NC ❑ SC ❑ NC F❑ SC ❑ NC ❑ SC *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECTID 6120257 LABORATORY REPORT NUMBER 1612F67 Primary Data Review By Chris Pafford Project Manager, AES DATE December 22, 2016 Secondary Data Review By Ashley Amick Project Manager, Access Analytical aamickpaaxs-inc.com PLEASE NOTE: - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 1 of 5 Page 7 of 11 N ISM Full -Service Analytical & OR I Environmental Solutions 11 PK LABORATORIE$ INC. SUBCONTRACT ORDER /i0 %r(d7 Certifi gfio NELAC_ USACE Prism Laboratories, Inc. SC Other 6120257 SENDING LABORATORY: RECEIVING LABORATORY: Prism Laboratories, Inc. Analytical Environmental Services, Inc. P. O. Box.240543 3080 Presidential Parkway Charlotte, NC 28224-0543 Atlanta, GA 30340 Phone: 800-529-6364 Phone :(770) 457-8177 Fax: 704-525-0409 Fax: NA Project Manager: Terri W. Cole Analysis Due Expires Laboratory ID Comments Sample ID: 6120257-01 Solid Sampled:IV13/16 06:42 MINE Herbicides TCLP (Sub) 12/20/16 06:42 Containers Supplied: Uh`i// Released By Date Received By Date Released By Date Received By Date Page 2 o Analytical Environmental Services, Inc Date: 22-Dec-16 Client: Prism Laboratories Client Sample ID: CLASS B Lab Order 1612F67 Tag Number: 6120257-01 Project Name: 6120257 Collection Date: 12/13/2016 6:42:00 AM Lab ID: 1612F67-001A Matrix: Solid Analyses Result Qual MDL Reporting Units BatchID DI+ Date Analyzed Analyst Limit HERBICIDES, TCLP SW1311/8151A 2,4,5-TP (Silvex) BRL 2,4-D BRL Sutr: DCAA 79.5 Qualifiers: " Value exceeds maximum contaminant level BRL Not Detected at MDL H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Analyte detected in the associated method blank (SW3510C) 0.064 0.20 mg/L 235131 1 12/21/201617:02 AW 0.076 0.20 mg/L 235131 1 12/21/201617:02 AW 0 50.1-132 %REC 235131 1 12/21/201617:02 AW E Estimated value above quantitation range S Spike Recovery outside limits due to matrix > Greater than Result value J Estimated value detected below Reporting Limit < Less than Result value Page 3 of 5 Page 9 of 11 Amalytical Environmental Services, Inc.- Sample/Cooler Receipt Checklist i - - Client �� ' �'� Work Order Number 1= Checklist completed by Sign afV Data Carriername:FedEx TIPS_ Courier_ Client_ US Mail_ Other Shipping container/cooler in good condition? Yes No ^ Not Present _ Custody seals intact on shipping container/cooler? Yes - No _ NotPresent ✓ Custody seals intact on sample bottles? Yes - No _ NotPresent Container/Temp Blank temperature in compliance? (0°<_6eC)* Yes ✓ No _ Cooler #1 Cooler #2 Cooler 43 Cooler #4 Cooler#5 Cooler #6 Chain of custody present? Yes No Chain of custody signed when relinquished andreceived? Yesy No _ Chain of custody agrees with sample labels? Yes No _ Samples in proper container/bottle7 Yes No _ Sample containers intact? Yes ± No _ Sufficient sample volume for indicated test? Yes No _ Ail samples received within holding time? Yes !/. No r Was TAT marked on the COC? Yes _ No Proceed with Standard TAT as per prof act history? Yes o _ Not Applicable _ water - VOA vials have zero headspace? No VOA vials submitted � Yes _ No _ Water - pH acceptable upon receipt? Yes No _ Not Applicable Adjusted? Checked by Sample Condition: Good_ Other(Explain) (For diffusive samples or AIHA lead) Is a Down blank included? Yes _ No t See Case Narrative for resolution of the Non -Conformance, *Samples do nothave to comply with the given range for certain parameters. V MesL server111SampleReceipt\MyDommentsMCs and pH Adjustment ShectlSample Cooler Recipe Checklist Revl.rtf Page 4 of 5 l: Page 10 of l l is N Analytical Environmental Services, Inc Client: Prism Laboratories Project Name: 6120257 Worlcorder: 16121767 Date: 22-Dec-16 ANALYTICAL QC SUMMARY REPORT BatchlD: 235131 Sample ID: NO-235131 Client ID: Units: mg/L Prep Date: 12/20/2016 Run No: 332718 SampleType: NJBLK TestCode: HERBICIDES, TCLP SW1311/8151A BatchlD: 235131 Analysis Date: 12/21/2016 Seq No: 7249626 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) BRL 0.20 2,4-D BRL 0.26 Surr: DCAA 0.3855 0 0.5000 77.1 50.1 132 Sample ID: LCS-235131 Client ID: Units: mg/L Prep Date: 12/20/2016 Run No: 332718 SampleType: LCS TestCode: HERBICIDES, TCLP SW1311/8151A BatchID: 235131 Analysis Date: 12/21/2016 Seq No: 7249627 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 0.4033 0.20 0,5000 80.7 50.7 117 2+13 0.4238 0.20 0.5000 84.8 50.1 119 Surr: DCAA 0.3983 0 0.5000 79.7 50.1 132 Sample ID: 1612F67-001AMS Client ID: CLASS B Units: mg/L Prep Date: 12/20/2016 Run No: 332718 SampleType: MS TestCode: HERBICIDES, TCLP SW131118151A BatehID: 235131 Analysis Date: 12/21/2016 Seq No: 7250398 Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual 2,4,5-TP (Silvex) 0.4357 0.20 0.5000 87.1 46.3 126 2,4-D 0.5359 0.20 0.5000 107 43.3 132 Surr: DCAA 0.4266 0 0.5000 85.3 50.1 132 Qualifiers: > Greater than Result value < Less than Resultvalue B Analyte detected in the associated method blank co (D BRL Below reporting limit E Estimated (value above quantitation range) H Holding times for preparation or analysis exceeded J Estimated value detected below Reporting Limit N Analyze not NELAC certified R RPD outside limits due to matrix page 5 of 5 Rpt Lint Reporting Limit 5 Spike Recovery outside limits due to matrix '•