NC0025453_Tax Certification_20201229

r
DIVISION OF WATER RESOURCES TCN:
APPLICATION FOR TAX CERTIFICATION This application is to be used only for waste treatment systems and equipment Rev.
& EXEMPTION FORM TC-WQ under the authority of the NC Division of Water Resources(DWR) 01/29/2016
DIRECTIONS:Complete and mail signed copies of the application form and all supporting information to both: 1)the County Tax Administrator for the County in which the facility is located(one copy)
AND 2)to the NC Division of Water Resources,Surface Water Protection Section,1617 Mail Service Center,Raleigh,NC 27699-1617(two copies). Type or print in blue or black ink. A separate
application package is required for each facility where property proposed for tax certification is located.
THIS APPLICATION WILL NOT BE PROCESSED WITHOUT COMPLETE AND ACCURATE INFORMATION. If you have any questions regarding this application,please call the local tax office or the
NC Division of Water Resources at 919/807-6300 or their web site at https://ox.deg.prod.nc.gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/npdes-wastewater/tax-
certification for more specific contact information.
Please Note:
a)Tax Certifications will only be processed for facilities under the authority of the DWR and only if the DWR has found that the described property:
1.Has been or will be constructed or installed;
2.Complies with or that plans therefore which have been submitted to the DWR indicate that it will comply with the requirements of the Environmental Management Commission;
3.Is being effectively operated or will,when completed,be required to operate in accordance with the terms and conditions of the permit,certificate of approval,or other document of approval
issued by the DWR;and
4.Has or,when completed,will have as its PRIMARY rather than incidental purpose the reduction of water pollution;
5.Is being used exclusively(100%)for waste treatment.
b)If approved,the Tax Certification issued will incorporate all requested assets at the facility that meet the criteria for Tax Certification by DWR. Therefore this application must include any new assets
for which Tax Certification is being requested,as well as any assets previously receiving Tax Certification from DWR for which Tax Certification is still needed.
A.Applicant(Applicant is the owner of,and taxpayer for,the property described in this application for tax certification.)
Name of Applicant: Name of Facility:
Grifols Therapeutics LLC Grifols Therapeutics LLC
Address of Applicant,if different from facility where property located: Physical Address of Facility where property located(no P.O.Box):
8368 US Highway 70 West Clayton,NC 27520
(address) (city) (zip) (street address) (city) (zip)
Business Relationship of Applicant to facility where property located:
County where property located: Johnston
Name of Contact Person at Facility where property located:
David Auge
Does the Applicant hold any NC Division of Water Resources Permits? 919-359-4375
®Yes / ❑ No Title: Environmental Manager Phone Number:
If yes,please list NCDES permit#NC0025453
VED
Permit No(s):
If approved,will this be the first Tax Certification issued for this Facility? If no,attach any previously issued DEC 2 9 2020
❑ Yes / ® No tax certifications t�'
B.Complete this Section only if the Operator/User of the facility and equipment is different from the Owner of the facility. NCDEO/DWR/NPDER
Name of Operator/User:
Operator/User Address:
(address) (city) (zip)
Operator/User Contact Name:
Relationship between Operator/User of facility and equipment and applicant:
***ATTACH A PROCESS SCHEMATIC TO YOUR APPLICATION The number of each item for which Tax Certification is being requested must be shown on the schematic*** Application continues on
Next page

DIVISION OF WATER RESOURCES TAX CERTIFICATION & EXEMPTION APPLICATION PAGE 2
Waste Treatment Systems & Equipment: Waste treatment systems&equipment must be used exclusively for the abatement of water pollution Rev.0 9/01 2 01 3
For owa Use Was asset listed in Asset Number. %of time item is Is this asset
For county only•A- Year of Original Historical
Use Only Approved-o• Descnption of Waste Treatment Systems or Equipment the permit(Yes/No) Vehicle Identification How is this equipment used for pollution abatement? used for pollution replacing a prior
Disapproved Number(VIN) abatement Acquisition Cost" asset?
See Attached Schedule
2
3
5
6
7
9
9
10
11
12
13
14
15
Attach additional pages if necessary
•H the asset is listed in the DWq permit.the description must be identical as listed on the current permit.If the asset is not specifically listed in the DWG permit,the applicant must attach detailed information as to why the asset should qualify for Tax Certification.
When certifying systems or equipment,DENR is not certifying the cost of the equipment or the year of acquisition.
Facilities: To qualify for tax certification,the building or section of building being applied for,must be used exclusively for water pollution prevention. A sketch of the building,square footage along with details
as to how the building is used for water pollution prevention,is required.
Land: To qualify for tax certification,the land must be used exclusively for water pollution prevention. A schematic diagram of the facility detailing the land being applied for is required. The amount of land
(acreage)is required and how this land is being used to prevent water pollution. For wastewater treatment and irrigation system list separately the acreage used for actual treatment from the acreage required by
the facility's water quality permit for buffers and setbacks.
SIGNATURE:
I hereby certify that the above equipment,facilities and/or land are used for the purpose stated.and that the information presented in this application is accurate. Furthermore,I certify that any portable or mobile
equipment listed on this application will be used exclusively in the state of North Carolina.
Applicant Signature: ,� rt-ext-- Title:Tax Director Date: 12/14/20
(print name also)
NOTICE: The penalty for fa Y se st ement,representation or certification Of: Grifols Therapeutics LLC
herein includes imprisonment and/or the assessment of civil penalties. (Name of Applicant Business Entity) rc-wo

DIVISION OF WATER QUALITY TAX CERTIFICATION & EXEMPTION APPLICATION
Waste Treatment Systems & Equipment: Waste treatment systems& equipment must be used exclusively for the abatement of water pollution
For For DWQ Use Only A Asset listed %of use for Original Replacing
County Approved'D•• Description of Waste Treatment systems or in the Asset pollution Year of Historical an existing
Use Only Disapproved Equipment permit? Number How is this equipment used for pollution abatement? abatement Acquisition Cost asset?
1 Wastewater Treatment Plant Upgrade-Phase I No 6001727 A new 1-million gallon Equalization Tank(EQ),used to 100% 2019-2020 7.040.021 No
6001728 attenuate flow and organic loading,will be installed to
6001731 supplement inventory control management to work with the
6001782 existing EQ tank. The new EQ tank will have an internal mixing
6001726 system that uses compressed air(blower)via a compressor to
6001820 produce coarse air bubbles that keeps the solids mixed. In
order to manage inventory of wastewater from the new and
existing EQ tankage,3 new centrifugal pumps will be installed
between the existing Headworks Building and exiting EQ tank
to allow for multiple transfer options between EQ tanks. After
the wastewater leaves the new EQ tanks,it will be filtered by
new automatic filters to a particle size of 1mm. This small
particle size removal will allow for good mixing without buildups
on the internal media in the downstream MBBR units. To
support the Electrical,Instrumentation.and Automation
requirements of both Phases,a new MCC Building will be built
on a re-purposed existing foundation.

Project Location: Clayton
WWTP Upgrade PH 1 k , 4 -
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V%ASTMATER TREATMENT FACILITES-GR FOLS TO TOM1N OF CLAYTON \
M Equipment Legend\
Greg- Existing/Re-used
Blue= Phase I Scope
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Yellow-- Phase II Scope
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EXISTING EQUIPMENT -s- ern.
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REQUIRED EQUIPMENT FOR i �
DISCHARGE TO TOWN POST JUNE 2022 X'. °� ,
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Process Flow Diagram if =_ i _ j' ° t:� ffi_

Grifols Therapeutics LLC
Pollution Control Assets - Johnston County
Johnston County (1-1-20)
Asset Description Cap.Date Acquis.Cost
2000010402 MACH EQUP CLARIFICATION EQUIPMENT 9/15/1983 80,540
2000011209 MACH EQUIPCLARIFICATION 95BS03 EAST 6/15/1990 146,422
2000011210 MACH EQUIPSUBSURFACE AERATORS 6/15/1990 66,571
2000014376 WATERTREATFLOCCULATION TANK MIXER 7/15/1996 6,000
2000014381 WATERTREATWWTU FACILITY UPGR 7/15/1996 167,703
2000014382 WATERTREATKEYSTONE FIG 999 12"VALVE 7/15/1996 5,000
2000014393 COMPACTIONPLAS/REC TRASH COMPACTOR 10/15/1996 33,094
Total pollution control property exempted prior to 4/16/2004 505,330
*46%
Agreed upon property tax value 232,452
2000030636 Reactor Moving Bed Biofilm(MBBR)Sys 1 95BF03 8/1/2008 466,325
2000030637 Reactor Moving Bed Biofilm(MBBR)Sys 2 95BF04 8/1/2008 466,325
2000030640 Mixing Box MBBR System 8/1/2008 23,061
2000030642 Blower 150HP Kaeser Omega FB790C MBBR 1 95VB09 8/1/2008 41,966
2000030643 Blower 150HP Kaeser Omega FB790C MBBR 1 95VB010 8/1/2008 41,966
2000030644 Added Blower,Inc HP 8/1/2008 137,928
2000030646 Emergency eyewash showers 8/1/2008 5,696
2000030647 Auto Screen Filter 8/1/2008 17,009
2000030648 PCS Electrical Operating DeltaV WasteWater Sys Upg 8/1/2008 1,015,131
2000030649 Level And Flow Instruments for New WWTP System 8/1/2008 221,447
2000030650 Foundation-Moving Bed Biofilm Reactor System 8/1/2008 608,191
2000030651 Foundation 2160SF Bldg Metal Sludge Storage 8/1/2008 520,985
2000030652 Tank 40000 GAL Storage Waste Sludge 1 95BF07 8/1/2008 117,951
2000030653 Tank 40000 GAL Storage Waste Sludge 2 95BF08 8/1/2008 117,951
2000030654 Mixer/Motor Drives 95RA03 for Sludge Storage Tanks 8/1/2008 99,428
2000030655 Mixer/Motor Drives 95RA04 for Sludge Storage Tanks 8/1/2008 99,428
2000030656 Foundation Waste Water Sludge Storage Tanks 8/1/2008 157,969
2000030657 Decant Pump Equip&alarm Sludge Storage Bldg Sys 8/1/2008 102,732
2000030658 DAF Unit-Equipment and Controls 8/1/2008 634,182
2000030659 Foundation 1600SF DAF Bldg 8/1/2008 227,152
2000030661 Pump Progressive CavityNSD Seepex 52-6L 95P017 8/1/2008 37,474
2000030662 Pump Progressive CavityNSD Seepex 52-6L 95P018 8/1/2008 37,474
2000030663 Mechanical/PipingNalves-Sludge Storage Building 8/1/2008 63,911
2000030664 Mechanical/PipingNalves-DAF Building 8/1/2008 98,010
2000030665 Mechanical/PipingNalves-Waste Sludge Strg Tanks 8/1/2008 28,826
2000030666 Mechanical/PipingNalves-MovingBed Biofilm Reactor 8/1/2008 49,941
2000030667 Mechanical/PipingNalves-Yard Piping 8/1/2008 375,378
2000030668 Structural Services-Platform Metal MBBR System 8/1/2008 40,357
2000030669 Structural Srv-Platform Metal Access Sludge Stg BI 8/1/2008 74,949
2000030670 Structural Srv-Platform Metal Access Sludge Tanks 8/1/2008 17,296
2000030671 Structural Services-Platform Metal Access DAF Bldg 8/1/2008 57,653
2000030672 Sludge Storage Building 8/1/2008 163,158
2000030673 Dissolved Air Flotation Building 8/1/2008 153,357
2000030674 Site Development-Asphalt Paving,Site Grading 8/1/2008 77,445
Total pollution control property exempted in 2008 6,398,049
Page 1 of 3

Grifols Therapeutics LLC
Pollution Control Assets - Johnston County
Johnston County (1-1-20)
Asset Description Cap.Date Acquis.Cost
2000032528 Dissolved Air Flotation Unit VW TP 5/19/2011 692,096
2000032529 Pump-Seepex DAF Sludge Pump WWTP 5/19/2011 31,780
2000032530 Liquid Sampler(Dipper)-Hach SIGMA Md#1600 WWTP 5/19/2011 7,657
2000032531 Liquid Sampler(Dipper)-Hach SIGMA Md#1600 WWTP 5/19/2011 7,394
2000032532 Electrical Panel Enclosure-Hoffman#A483008LP w/ 5/19/2011 26,684
2000032533 Climate Controlled FRP Enclosure 5/19/2011 101,689
2000032534 Electrical Installation for leased CO2 skid WWTP 5/19/2011 206,509
2000032264 Aqua Guard Sanitary Sewer Screen 95FB02 between 1/1/2011 245,557
2000032265 Canopy for Aqua Guard Sanitary Sewer Screen 95FB02 1/1/2011 43,746
2000032266 Concrete Footings for Aqua Guard Sanitary Sewer 1/1/2011 13,536
Total pollution control property exempted in 2010&2011 1,376,647
2000032990 Dual Pump Skid w/2 40hp pumps for increase flow 3/1/2012 197,968
2000032991 Screen Filter Md#16PEER1-w/3000 Micron Screen 3/1/2012 72,587
2000032990 Capital Interest-Dual Pump Skid w/2 40hp pumps 3/1/2012 23,124
2000032992 Screen Filter Md#16PEER1-w/3000 Micron Screen 3/1/2012 32,909
2000032993 Actuator-Dezurik part#2086155 6"#PEC for WWTP 3/1/2012 6,663
Total pollution control property exempted in 2011 &2012 333,250
2000033531 Tomco Pressurized Solution Feed Unit-CO2 Solution 2/1/2013 67,058
2000033539 Rosemount Flow Meter-DAF Feed Pumping Station 2/1/2013 5,588
2000033540 Pump-10 hp Duplex Self Priming Dakota Pump 2/1/2013 34,596
2000033541 Pump-10 hp Duplex Self Priming Dakota Pump 2/1/2013 34,596 1
2000033542 Danfoss VFD with bypass conductors-includes valves 2/1/2013 34,596
2000033543 Danfoss VFD with bypass conductors-includes valves 2/1/2013 34,596
2000033622 DR3900 Spectrophotometer with RFID 4/1/2013 3,716
2000033716 Capitalized Interest-WWTP Capacity Increase 5/1/2013 125,400
2000033716 Equalization Tank 95BF01 at WWTP 1.0MM Gallon 5/1/2013 1,062,990
2000033717 IR Blowers(air compressors)95VB13 for EQ Tank 5/1/2013 179,142
2000033718 IR Blowers(air compressors)95VB14 for EQ Tank 5/1/2013 179,066
2000033719 SANITAIRE Stainless Steel Fixed Header Aeration 5/1/2013 51,591
2000033720 Solid State Starter NEMA 4 for EQ Tank at WWTP 5/1/2013 16,104
2000033721 Solid State Starter NEMA 4 for EQ Tank at WWTP 5/1/2013 16,104
2000033722 Aftercooler 95WA07 installed on Blowers 95VB13 5/1/2013 8,940
2000033723 Aftercooler 95WA08 installed on Blowers 95VB14 5/1/2013 8,940
2000033724 Reverse Osmosis Unit-EQ Tank WWTP 5/1/2013 6,063
2000033725 Electrical Panels,wiring,cable trays,construction 5/1/2013 286,427
2000033726 Influent/Effluent Piping including pipe supports 5/1/2013 126,620
2000033727 Influent/Effluent Strainer Piping including pipe 5/1/2013 221,652
2000033728 Process Air Piping including pipe supports 5/1/2013 108,262
2000033729 Sump Pumps&piping inlet&outlet-EQ tank95BF01 5/1/2013 33,881
2000033730 Defoamer/Spray Ring Piping-EQ Tank 95BF01 5/1/2013 70,263
2000033731 Filter Piping Drain-EQ Tank 95BF01 5/1/2013 49,908
2000033732 CO2 System Piping-EQ Tank 95BF01 5/1/2013 17,190
2000033733 EQ Overflow Piping including pipe supports 5/1/2013 47,409
2000033734 Geopiers and Concrete Slab for EQ Tank at WWTP 5/1/2013 529,016
Total pollution control property exempted in 2011,2012&2013 3,359,714
Page2of3

Grifols Therapeutics LLC
Pollution Control Assets - Johnston County
Johnston County (1-1-20)
Asset Description Cap.Date Acquis.Cost
5009013 DAF POLYMER FEED SYSTEM 4/25/2014 29,617
Total pollution control property exempted in 2013&2014 29,617
5009439 GT3288: WASTE TREATMENT MBBR TANK REPLACEMENT 8/28/2015 964,939
5009443 GT3160: WWTP GRIT REMOVAL EQUIPMENT 8/31/2015 329,058
5009444 GT3160: WWTP PARKSON AQUA GUARD 8/31/2015 331,631
5009445 GT3160: WWTP LIGHTNIN MIXER 16Q5(2) 8/31/2015 38,549
5009446 GT3160: WWTP GORMAN RUPP STATION 8/31/2015 56,435
5009447 GT3160: WWTP NESGEAR LV SWITHGEAR 8/31/2015 489,909
5009442 GT3160: WWTP SITE PREP&HEADW BLDG 8/31/2015 3,520,988
5009486 GT3160: WWTP SITE PREP&HEADW BLDG ADDL 12/31/2015 7,964
Total pollution control property exempted in 2013,2014,2015 5,739,475
5009520 GT3288:WASTE TREATMENT MBBR TANK REPLACEMENT ADDN 2/16/2016 1,410
Total pollution control property exempted in 2016 1,410
Page 3 of 3

TOWN OF CLAYTON
"SERVICE" OPERATIONS CENTER "ENVIRONMENT'
ELECTRIC SERVICE •CAR°! PUBLIC WORKS
[phone] tit , 'y [phone]
D
VEHICLE MAINTENANCE WATER RECLAMATION
[phone] / [phone]
February 26,2020
Chuck Blatchley
Grifols Therapeutics
8368 US 70 Business West
Clayton,NC 27520
Re: Industrial User Permit Modification
Mr.Blatchley:
Enclosed please the renewed Industrial User Permit#0001-02. Please replace the amended sheets to the
current permit.The NC Department of Environmental Quality,Division of Water Resources requested that
Total Dissolved Solids monitoring be added to the existing permit. Also a typo was corrected in regards to
the due day of monthly reports.
If any parts,measurement frequencies.or sampling requirements contained in this permit are unacceptable
to you,you have the right to an adjudicatory hearing upon written request within thirty(30)days following
receipt of this letter. Unless such demand is made,this decision shall be final and binding.
Please contact me directly at 919-553-1536 if you have any questions.
Sincerely, /1
ift‘s Warren
Town of Clayton,Wastewater Operations Superintendent
Copy: Adam Lindsay,Town of Clayton,NC
Rich Cappola,Town of Clayton,NC
Chandra Coats,Johnston County Public Utilities
Monte Hassan,NCDEQ
653 Highway 42 West•P.O.Box 879•Clayton,North Carolina 27520•[phone]•Fax[phone]

TOWN OF CLAYTON
"SERVICE" OPERATIONS CENTER "ENVIRONMENT'
ELECTRIC SERVICE /wrARo\ PUBLIC WORKS
[phone] �*9 r� 1*y [phone]
VEHICLE MAINTENANCE WATER RECLAMATION
[phone] [phone]
June 29,2017
Sergi Roura,President
Grifols Therapeutics
8368 US 70 Business West
Clayton,NC 27520
Re: Amended Industrial User Permit
Mr.Roura:
Enclosed please the renewed Industrial User Permit#0001-02.Please read all sections carefully as some
language was amended to reflect name changes and EPA requirements.
Please note the sampling responsibility for the facility remains assigned to the Control Authority(Town of
Clayton)or its designee.The only exception is the daily flow rate. Grifols has a right to split samples
during any event. Should Grifols decide to collect samples on the effluent the results will need to be
submitted to the Control Authority.
Grifols submitted an up to date spill and slug control plan and should plan to continue implementation.
The current treatment option to discharge the higher strength wastewater will expire in 2020 unless the
agreement is renewed.It is expected that this renewal up to 900,000 gallons per day will happen as
previously discussed with Johnston County.However,ultimately compliance with this permit is the
responsibility of Grifols. Should the agreement not be renewed the limits would be expected to return to
domestic strength levels.
If any parts,measurement frequencies,or sampling requirements contained in this permit are unacceptable
to you,you have the right to an adjudicatory hearing upon written request within thirty(30)days following
receipt of this letter. Unless such demand is made,this decision shall be final and binding.
Please contact me directly at 919-553-1536 if you have any questions.
Sincerely,
J es Warren
Town of Clayton,Wastewater Operations Superintendent
Copy: Adam Lindsay,Town of Clayton,NC
Tim Simpson,Town of Clayton,NC
Chandra Coats,Johnston County Public Utilities
Chuck Blatchley,Grifols
Monte Hassan,NCDEQ
653 Highway 42 West•P.O.Box 879•Clayton,North Carolina 27520•[phone]•Fax[phone]

TOWN OF CLAYTON
"S OPERATIONS CENTER §
suer.>sic SERVICE R kk PUBLIC WORKS
[phone] ►,� 1 p [phone]
VEHICLE MAINTENANCE ?'— WATER RECLAMATIO1,
[phone] 1.,, [phone]
August 28,2017
Sergi Roura,President
Grifols Therapeutics
8368 US 70 Business West
Clayton,NC 27520
Re: Industrial User Permit Renewal
Mr.Roura:
Enclosed please the renewed Industrial User Permit#0001-02.Please replace the amended sheets to the
current permit.The amended sheets were necessary due to comments by the North Carolina Department of
Environmental Quality Pretreatment Unit.The detection levels for several metals were changed and two
minor typos corrected.The Town was required to base the EPA categorical limits on the combined waste
stream formula.
If any parts,measurement frequencies,or sampling requirements contained in this permit are unacceptable
to you,you have the right to an adjudicatory hearing upon written request within thirty(30)days following
receipt of this letter. Unless such demand is made,this decision shall be final and binding.
Please contact me directly at 919-553-1536 if you have any questions.
Sincerely,
es Warren
Town of Clayton,Wastewater Operations Superintendent
Copy: Adam Lindsay,Town of Clayton,NC
Tim Simpson,Town of Clayton,NC
Chandra Coats,Johnston County Public Utilities
Chuck Blatchley,Grifols
Monte Hassan,NCDEQ
653 Highway 42 Weot•P.O.Box 879•Clayton,No th CaxoUaa 27520•[phone]•Pax(919)553-t541

Town of Clayton
Control Authority and/or Municipality
PERMIT
Industrial User Pretreatment Permit (IUP)
To Discharge Wastewater Under the
Industrial Pretreatment Program
0001-02 439.20
IUP Number 40 CFR Categorytii Applicable)
In compliance with the provisions of North Carolina General Statute 143-215.1, any
applicable federal categorical pretreatment regulations, all other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Control Authority and/or Municipality Sewer Use Ordinance. The
following Industry, hereafter referred to by name or as the permittee:
Industry name,permittee:
Grifols Therapeutics, Inc.
Facility Located at Street Address
8368 US 70 West
City
Clayton
State,Zip
North Carolina 27520
is hereby authorized to discharge wastewater from the facility located at the above listed
address into the sanitary sewer collection system and the wastewater treatment facility of
the Control Authority and/or Municipality listed below:
IUP Control Authority and/or Municipality WWTP name:
Little Creek Water Reclamation Facility
NPDES Number:
NC0025453
WWTP Address:
Durham Street Ext. (PO Box 879)
City,State.Zip
Clayton, North Carolina 27520
in accordance with effluent limitations, monitoring requirements, and all other conditions
set forth in Parts I, II, and III of this Industrial User Pretreatment Permit (IUP).
Effective date, this permit and the authorization to discharge shall become
effective at midnight on this date:.
March 1, 2020
Expiration date,this permit and the authorization to discharge shall expire at
midnight on this date:
June 30, 2022
oZ/a 12026 alp
Date signed J5arren,Water Reclamation Superintendent

Town of Clayton
Control Authority and/or Municipality
PERMIT
Industrial User Pretreatment Permit(IUP)
To Discharge Wastewater Under the
Industrial Pretreatment Program
0001-02 439.20
IUP Number 40 CFR Category(if Applicable)
In compliance with the provisions of North Carolina General Statute 143-215.1, any
applicable federal categorical pretreatment regulations, all other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Control Authority and/or Municipality Sewer Use Ordinance. The
following Industry,hereafter referred to by name or as the permittee:
industry name,permlttee:
Grifols Therapeutics, Inc.
Facility Located at Street Address
8368 US 70 West
City
Clayton
State,Zip
North Carolina 27520
is hereby authorized to discharge wastewater from the facility located at the above listed
address into the sanitary sewer collection system and the wastewater treatment facility of
the Control Authority and/or Municipality listed below:
IUP Control Authority and/or Municipality WWTP name:
Little Creek Water Reclamation Facility
NPDES Number:
NC0025453
WWTP Address:
Durham Street Ext. (PO Box 879)
City,State.Zip
Clayton,North Carolina 27520
in accordance with effluent limitations, monitoring requirements, and all other conditions
set forth in Parts I, II, and III of this Industrial User Pretreatment Permit(IUP).
Effective date, this permit and the authorization to discharge shall become
effective at midnight on this date:.
July 01, 2017
Expiration date,this permit and the authorization to discharge shall expire at
midnight on this date:
June 30, 2022
P-0-1P v?eY .20/ 116,
Date signed Warren,Water Reclamation Superintendent

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
IUP, PART I, OUTLINE:
A.) IUP Basic Information
B.) IUP Modification History
C.) Authorization Statement
D.) Description of Discharges
E.) Schematic and Monitoring Locations
F.) Effluent Limits &Monitoring Requirements
G.) Definitions and Limit Page(s)notes
A. IUP Basic Information:
Receiving Control Authority&WWTP name: POTW NPDES#
Little Creek Water Reclamation Facility NC0025453
IUP Name: IUP Number:
Grifols Therapeutics, Inc. 0001-02
IUP Effective date: Pipe Numbers,list all regulated pipes:
July 01,2017 001 -
IUP Expiration date: IUP 40 CFR#(if applicable),or N/A:
June 30, 2022 439.20
B. IUP History. A Complete Permit History is required):
Effective Date Renewal or Description of changes over previous IUP.
Modification
9/25/01 Modification Added new CIU stds.for Acetone,n-Amyl Acetate,
Ethyl Acetate,Isopropyl Acetate,Methylene Chloride.
7/01/02 Renewal Dropped Cn limit. Added Pb limit. Reduced NH3-N
monitoring freq. Dropeed CIU sampling for Permittee.
Dropped PP sampling. Changed all Town monitoring to
1/6 months.
4/30/03 Mod. Increased flow to 450,000 gpd
3/01/04 Mod. Increased flow to 500,000 gpd
4/01/05 Mod. Name Changed to Talecris from Bayer
2

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
7 01 07 Renewal Decreased Pb monitoring frequency to 1/6 months.
Added limits for Zn. Decreased T Nitrogen limit to 20
mg/L.
7/23/10 Modification Updated process information,increased monitoring
frequency for T-nitrogen&ammonia Amyl Acetate,
Ethyl Acetate,Isopropyl Acetate,Methylene Chloride
?!11!t 1 • Modification Increased flow to 550,000 gpd,Increased limits for
BOD,TSS,COD,Zinc,Acetone,n-Amyl Acetate.Ethyl
Acetate,Isopropyl Acetate,Methylene Chloride,
modified limits for total nitrogen,decreased monitoring
frequency for total nitrogen,ammonia and phosphorus,
Acetone,n-Amyl Acetate,Ethyl Acetate,Isopropyl
Acetate,Methylene Chloride. Extended reporting date to
end of month.Dropped lead limit.
3/07/12 Mod. Name Change to Grifols from Talecris.
07/01/12 Renewal Permit renewal,Increase flow to 650,000 gpd.Removed
Zinc limit.
04/22/2013 Interim limits Interim limits established to allow treatability study.
Increased BOD,COD,TSS,t-Phos.and T-Nitrogen
limits for the period of 04/22/2013 to 06/21/2013.
06/05/2013 Interim limits Extended interim limits for BOD,TSS,T-Phos and T-
Nitrogen until 07/01/2013.
08/17/2015 Modification Permit modified to allow Grifols to discharge MBBR
effluent.
09/16/2015 Modification Permit modified to remove maximum daily limits for
BOD,COD,TSS
07/01/2017 Renewal Permit renewal(amended to NC DEQ requirements
8/23/17.)
03/01/2020 Modification Added TDS monitoring,Corrected report due by date.
3

Industrial User Pretreatment Permit (IUP)
PARTI
Specific Conditions
C.) Authorization Statement:
1.) The Permittee is hereby authorized to discharge wastewater in accordance
with the effluent limitations,monitoring requirements, and all other conditions
set forth in this Industrial User Pretreatment Permit (IUP) into the sewer
collection system and wastewater treatment facility of the Control Authority
and/or Municipality.
2.) The Permittee is hereby authorized to continue operation of and discharge
wastewater from the following treatment or pretreatment facilities. These
facilities must correspond to the treatment units listed on both the application
and inspection forms.
IU Treatment Units
List all Treatment Units: Descriptions:
Influent Bar Screen wl EQ Tank Removal of large solids.Able to bypass EQ tank if necessary.
bypass provision.
Equalization Tanks w/pH (1)One million equalization tank w/pH adjustment(carbon dioxide,
adjustment mag hydroxide).
MBBR 356000 gallon process train.
Chemical feed Ammonium hydroxide,Carbon Dioxide
3.) The Permittee is hereby authorized to, if required by the Control Authority
and/or Municipality and after receiving Authorization to Construct (A to C)
from the Control Authority and/or Municipality, construct and operate
additional pretreatment units as needed to meet final effluent limitations.
D.) Description of IUP Discharge(s):
1. Describe the discharge(s)from all regulated pipes.
Pipe# 001 , Description of Discharge:
Effluent from Mixed Bed Biological Reactor serving Grifols.
Grifols: process, wash down, domestic, cooling (non contact and HVAC),boiler,
and cooling tower blow down water.
4

_ Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
E.) Schematic and Monitoring Locations:
The facility schematic and description of monitoring location(s) given below must
show enough detail such that someone unfamiliar with the facility could readily find
and identify the monitoring location(s) and connection to the sewer. Include and
identify all regulated pipes.
5

GrNols WWTP Process Flow Schematic
Clayton,NC
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e/a R.morai -
Lilt 1heWn Magnetic Flow Meter /
. %:
1 New 1..MG EgonEn io Tank i1 Mars LaMGF.*rel(ntl w Took 1
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a .—� N.M1M1aHow ^•••-•• t I
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M.ch.nical Screen No. f `�
f
Influent Ye al.waler 1 - i
I 1 1
I Tank No.t Ed.Transfer Pump
I 1
f i • l
1 o '
Mechanical SenM N..2 �
f L1R StationMBSR taininsticleti 1 1
1 Palm flnuJrlrrY
flex enyR..M rn ng?Cep.cUsn : - --
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1 Johnston County Effluent Parallel Thaw
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11
Edging MSSR N0.1 Edging MSSR Ne.7
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J i

IUP, Part 1 Section F: Receiving POTW name LCWRF IU name=> Grifols
Receiving POTW NPDES#—> NC0025453 IUP#_> 0001-02
Effluent Limits and Monitoring Requirements Effective date for these Limits=> 07/01/2017 Pipe#=> 001
Expiration date for these Limits=> 06/30/2022 40 CFR#_> 439.20
The Permittee may discharge from this specific if not applicable put N/A
Pipe number according to these specific dates, THE LIMITS ON THIS PAGE ARE,(Check one below):
effluent limits, and monitoring requirements LIMITS for ENTIRE permit period =>
INTERIM Limits for period# 1 =>
INTERIM Limits for period#2 =>
FINAL Limits Page => X
Concentration Limits Frequencies
Sample Required
Collection Detection
Weekly Method Level .
Daily Max Average Units By Industry By POTW (C or G) Mg/1
1 Flow 1.10 .90 MGD Daily Meter -
2 BOD - 800 mg/L 3/week C 2 '
3 COD - 1500 mg/L 1 3/week C 5
4 TSS - 1200 mg/L 3/week C 2
5 Temperature 66 - C° 3/week G -
6 pH 6-9 - Std. Units 3/week G -
OTHER PARAMETERS:Please List Alphabetically
7 Ammonia—N *** - - mg/L 3/week C 0.3
8 Arsenic - - mg/L 1/3 months C 0.003
9 Barium - - mg/L 1/3 months C 0.01
10 Cadmium - - mg/L 1/3 months C 0.002
11 Chloride - - mg/L 1/3 months C -
12 Chromium - - mg/L 1/3 months C 0.002
13 Copper - - mg/L 1/3 months C 0.002
14 Cyanide - - mg/L 1/3 months G 0.01
15 Fluoride - - mg/L 1/3 months C -
16 Lead - - mg/L 1/3 months C 0.01
17 Mercury** - - mg/L 1/3 months C 0.0002
18 Molybdenum - - mg/L 1/3 months C 0.005
19 Nickel - - mg/L 1/6 months C 0.005
20 T Nitrogen*** 80 mg/L 3/week C -
7

21 T Phosphorous 12 mg/L 3/week C _ -
22 Selenium - - mg/1. 1/3 months C 0.01
23 Silver - - mg/I 1/3 months C 0.001
24 Zinc - - mg/I 1/3months C 0.01
25 Acetone 7.216 - mg/1 - 1/6 months G .5
26 n-Amyl acetate 7.216 - mg/1 - 1/6 months G .5
27 Ethyl acetate 7.216 - mg/1 - 1/6/months G .5
28 Isopropyl acetate I 7.216 mg/I 1/6 months G 5 _
29 Methylene .616 - mg/1 - 1/6 months G .5
Chloride
30 Total Dissolved - - Mg/I 1/3 months C 12
Solids
**No mercury shall be discharged. Mercury concentrations less than the detection level will be considered compliant.
***Ammonia and T-Nitrogen sampling will be done on the same day.
(See next section,IUP,Part I,Section G. for Definitions and Limit Page(s)notes)
8

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
G.) Definitions and Limit Page(s) notes:
In addition to the definitions in the Town of Clayton Sewer Use Ordinance the
following definitions and requirements apply:
1. Composite Sample:
Unless defined differently below, a composite sample for the monitoring
requirements of this IUP, is defined as the automatic or manual collection
of one grab sample of constant volume, not less than 100 ml, collected
every hour during the entire discharge period on the sampling day.
Sampling day shall be a typical production, and discharge day.
2. Composite Sample, alternative definition:
A composite sample for the monitoring requirements of this IUP is the
same as described above unless specifically defined below as the
automatic or manual collection of constant volume and constant time grab
samples collected and composited according to the following criteria:
specific volume of each grab sample= 1000 Milliliters
specific time interval between samples= 6 Hours
total duration of sample collection period= 24 Hours
Total number of grab samples to be composited= 4 Samples
3. Daily Monitoring Frequency
Daily Monitoring Frequency as specified in this IUP shall mean each day
of discharge.
4. Grab Sample
Grab sample for the monitoring requirements of this IUP, is defined as a
single "dip and take" sample collected at a representative point in the
discharge stream.
5. Instantaneous measurement
An Instantaneous measurement for the monitoring requirements of this
IUP is defined as a single reading,observation, or measurement.
9

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
G.) Definitions and Limit Page(s) notes: (continued)
6. Monitoring and Reporting
All Monitoring shall be performed by a state certified laboratory by
standard methods. All data shall be reported to the Division as specified
in Part II. 2) of this permit, note that violations shall be reported within 24
hours, and that all sampling (even if done more frequently than required)
shall be summarized on forms approved by the Division and sent to the
following address by the last day of the following month:
James Warren,Water Reclamation Superintendent
Town of Clayton
Post Office Box 879
Clayton,North Carolina 27520
7. Notice to Permittees
Permittee is subject to the thirty(30)general conditions attached, found in
Part II of this permit.
10

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
Outline of PART II,
1. Representative Sampling 16. Federal and/or State Laws
2. Reporting 17. Penalties
3. Test Procedures 18. Need to Halt or Reduce
4. Additional Monitoring by 19. Transferability
Permittee
5. Duty to comply 20. Property Rights
6. Duty to Mitigate 21. Severability
7. Facilities Operation, Bypass 22. Modification, Revocation,
Termination
8. Removed substances 23. Reapplication
9. Upset Conditions 24. Dilution Prohibition
10. Right of Entry 25. Reports of Changed Conditions
11. Availability of Records 26. Construction of pretreatment
facilities
12. Duty to provide information 27. Reopener
13. Signatory Requirements 28. Categorical Reopener
14. Toxic Pollutants 29. General Prohibitive Standards
15. Civil and Criminal Liability 30. Reports of Potential Problems
1. Representative Sampling
Samples and measurements taken as required herein shall be representative of the volume and
nature of the monitored discharge. All samples shall be taken at the monitoring points specified in
this permit and, unless otherwise specified, before the effluent joins or is diluted by any other
wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to,and approval by,the permit issuing authority.
2. Reporting
a.) Monitoring results obtained by the permittee shall be reported on forms specified by the
Control Authority and/or Municipality,postmarked no later than the last day of the month
following the month in which the samples were taken. If no discharge occurs during a
reporting period(herein defined as each calendar month) in which a sampling event was
to have occurred, a form with the phrase "no discharge" shall be submitted. Copies of
these and all other reports required herein shall be submitted to the Control Authority
and/or Municipality and shall be sent to the following address:
James Warren
Water Reclamation Superintendent
Town of Clayton
PO Box 879
Clayton,NC 27520
b.) If the sampling performed by the permittee indicates a violation,the permittee shall notify the
Control Authority and/or Municipality within 24 hours of becoming aware of the violation.
The permittee shall also repeat the sampling and analysis and submit the results of the repeat
analysis to the Control Authority and/or Municipality within 30 days after becoming aware of
the violation.
11

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
c.) If no self-monitoring is required by this IUP, and the sampling performed by the Control
Authority and/or Municipality indicates a violation,the Control Authority and/or Municipality
shall repeat the sampling and analysis and receive the results of the repeat analysis within 30
days after becoming aware of the violation.
3. Test Procedures
Test procedures for the analysis of pollutants shall be performed in accordance with the techniques
prescribed in 40 CFR part 136 and amendments thereto unless specified otherwise in the
monitoring conditions of this permit.
4. Additional Monitoring by Permittee
If the permittee monitors any pollutant at the location(s) designated herein more frequently than
required by this permit,using approved analytical methods as specified above,the results of such
monitoring shall be submitted to the Control Authority and/or Municipality. The Control
Authority and/or Municipality may require more frequent monitoring or the monitoring of other
pollutants not required in this permit by written notification.
5. Duty to Comply
The permittee must comply with all conditions of this permit. Any permit noncompliance
constitutes a violation of the Control Authority and/or Municipality Sewer Use Ordinance and is
grounds for possible enforcement action.
6. Duty to Mitigate - Prevention of Adverse Impact
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of
this permit which has a reasonable likelihood of adversely affecting human health,the POTW,the
waters receiving the POTW's discharge,or the environment.
7. Facilities Operation, Bypass
The permittee shall at all times maintain in good working order and operate as efficiently as
possible, all control facilities or systems installed or used by the permittee to achieve compliance
with the terms and conditions of this permit. Bypass of treatment facilities is prohibited except
when approved in advance by the Control Authority and/or Municipality. Bypass approval shall
be given only when such bypass is in compliance with 40 CFR 403.17.
8. Removed Substances
• Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control
of wastewaters shall be disposed of in a manner such as to prevent any pollutants from such
materials from entering the sewer system. The permittee is responsible for assuring its compliance
with any requirements regarding the generation,treatment,storage,and/or disposal of"Hazardous
waste"as defined under the Federal Resource Conservation and Recovery Act.
9. Upset Conditions
An "upset" means an exceptional incident in which there is an unintentional and temporary
noncompliance with the catergorical Pretreatment Standards of this permit because of factors
beyond the reasonable control of the permittee. An upset does not include noncompliance to the
extent caused by operational error, improperly designed or inadequate treatment facilities,lack of
preventative maintenance,or careless or improper operations.
12

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
An upset may constitute an affirmative defense for action brought for the noncompliance. The
permittee has the burden of proof to provide evidence and demonstrate that none of the factors
specifically listed above were responsible for the noncompliance.
10. Right of Entry
The permittee shall allow the staff of the State of North Carolina Department of Environment
Quality,Division of Water Resources,the Regional Administrator of the Environmental Protection
Agency, the Control Authority and/or Municipality, and/or their authorized representatives,upon
the presentation of credentials:
1. To enter upon the permittee's premises where a real or potential discharge is located or
in which records are required to be kept under the terms and conditions of this permit;
and
2. At reasonable times to have access to and copy records required to be kept under the
terms and conditions of this permit;to inspect any monitoring equipment or monitoring
method required in this permit;and to sample any discharge of pollutants.
11. Availability of Records and Reports
The permittee shall retain records of all monitoring information, including all calibration and
maintenance records as well as copies of reports and information used to complete the application
for this permit for at least three years. All records that pertain to matters that are subject to any
type of enforcement action shall be retained and preserved by the permittee until all enforcement
activities have concluded and all periods of limitation with respect to any and all appeals have
expired.
Except for data determined to be confidential under the Sewer Use Ordinance,all reports prepared
in accordance with terms of this permit shall be available for public inspection at the Control
Authority and/or Municipality. As required by the Sewer Use Ordinance,effluent data shall not be
considered confidential.
12. Duty to Provide Information
The permittee shall furnish to the Director of Public Works or his/her designees, within a
reasonable time, any information which the Director, his/her designee, or the Division of Water
Resources may request to determine whether cause exists for modifying,revoking and reissuing,or
terminating this permit or to determine compliance with this permit. The permittee shall also
furnish,upon request,copies of records required to be kept by this permit.
13. Signatory Requirements
All reports or information submitted pursuant to the requirements of this permit must be signed and
certified by the Authorized Representative as defined under the Sewer Use Ordinance. If the
designation of an Authorized Representative is no longer accurate because a different individual or
position has responsibility for the overall operation of the facility, or overall responsibility for
environmental matters for the company, a new authorization satisfying the requirements of this
section must be submitted to the Water Reclamation Superintendent prior to or together with any
reports to be signed by an authorized representative.
14. Toxic Pollutants
If a toxic effluent standard or prohibition(including any schedule of compliance specified in such
effluent standard or prohibition) is established under Section 307(a) of the Federal Clean Water
Act for a toxic pollutant which is present in the discharge and such standard or prohibition is more
stringent than any limitation for such pollutant in this permit, this permit may be revised or
13

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
modified in accordance with the toxic effluent standard or prohibition and the permittee so
notified.
15. Civil and Criminal Liability
Nothing in this permit shall be construed to relieve the permittee from civil or criminal penalties
for noncompliance.
16. Federal and/or State Laws
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties established pursuant to any
applicable Federal and/or State law or regulation.
17. Penalties
The Sewer Use Ordinance of the Control Authority and/or Municipality provides that any person
who violates a permit condition is subject to a civil penalty not to exceed$25,000 dollars per day
of such violation.
Under state law, (NCGS 143-215.6B), under certain circumstances it is a crime to violate terms,
conditions, or requirements of pretreatment permits. It is a crime to knowingly make any false
statement,representation,or certification in any record or other document submitted or required to
be maintained under this permit, including monitoring reports or reports of compliance or
noncompliance. These crimes are enforced at the prosecutorial discretion of the local District
Attorney.
18. Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity to maintain compliance with the conditions of the permit.
19. Transferability
This permit shall not be reassigned or transferred or sold to a new owner, new user, different
premises,or a new or changed operation without approval of the Town.
20. Property Rights
This permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights,nor any infringement of Federal,State or local laws or regulations.
21. Severability
The provisions of this permit are severable and,if any provision of this permit or the application of
any provision of this permit to any circumstance is held invalid,the application of such provision
to other circumstances and the remainder of this permit shall not be affected thereby.
22. Permit Modification, Revocation, Termination
This permit may be modified,revoked and reissued or terminated with cause in accordance to the
requirements of the Control Authority and/or Municipality Sewer Use Ordinance and North
Carolina General Statute or implementing regulations.
14

•
Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
23. Re-Application for Permit Renewal
The permittee is responsible for filing an application for reissuance of this permit at least 180 days
prior to its expiration date.
24. Dilution Prohibition
The permittee shall not increase the use of potable or process water or in any other way attempt to
dilute the discharge as a partial or complete substitute for adequate treatment to achieve
compliance with the limitations contained in this permit.
25. Reports of Changed Conditions
The permittee shall give notice to the Control Authority and/or Municipality of any planned
significant changes to the permittee's operations or system which might alter the nature,quality,or
volume of its wastewater at least 180 days before the change. The permittee shall not begin the
changes until receiving written approval from the Control Authority and/or Municipality. Also see
Part II,30 below for additional reporting requirements for spill/slug issues.
26. Construction
No construction of pretreatment facilities or additions thereto shall be begun until Final Plans and
Specifications have been submitted to the Control Authority and/or Municipality and written
approval and an Authorization to Construct(A to C)have been issued.
27. Reopener
The permit shall be modified or,alternatively,revoked and reissued to comply with any applicable
effluent standard or limitation for the control of any pollutant shown to contribute to toxicity of the
WWTP effluent or any pollutant that is otherwise limited by the POTW discharge permit. The
permit as modified or reissued under this paragraph may also contain any other requirements of
State or Federal pretreatment regulations then applicable.
28. Categorical Reopener
This permit shall be modified, or alternatively, revoked and reissued, to comply with any
applicable effluent standard or limitation issued or approved under Sections 302(b)(2)(C)and(D),
304(b)(2),and 307(a)(2)of the Clean Water Act,if the effluent standard or limitation so issued or
approved:
1.) contains different conditions or is otherwise more stringent than any effluent
limitation in this permit;or
2.) controls any pollutant not limited in this permit.
The permit as modified or reissued under this paragraph shall also contain any other requirements
of the Act then applicable.
29. General Prohibitive Standards
The permittee shall comply with the general prohibitive discharge standards in 40 CFR 403.5 (a)
and(b)of the Federal pretreatment regulations.
15

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
30. Potential Problems
The permittee shall provide protection from accidental and slug discharges of prohibited materials
and other substances regulated by this permit. The permittee shall also notify the POTW
immediately of any changes at its facility affecting the potential for spills and other accidental
discharge, discharge of a non-routine, episodic nature,a non-customary batch discharge,or a slug
load as defined in the Sewer Use Ordinance.
Additionally, the permittee shall notify by telephone the Control Authority and/or Municipality
immediately of all discharges that could cause problems to the POTW including any slug loadings
as defined in the Sewer Use Ordinance. If the permittee experiences such a discharge,they shall
inform the Control Authority and/or Municipality immediately upon the first awareness of the
commencement of the discharge. Notification shall include location of the discharge, type of
waste,concentration and volume if known and corrective actions taken by the permittee. A written
follow-up report thereof shall be filed by the permittee within five(5) days,unless waived by the
Control Authority and/or Municipality.
16

Industrial User Pretreatment Permit (IUP)
PART III
Special Conditions
1. Slug/Spill Control Measures
In addition to the requirements in Part II, 30, the Permittee shall complete
installation and/or commence implementation, operation, and/or maintenance of
the following specific protection Measures, Activities, Plans. Etc. (Items without
specific completion dates, or marked as "Continuous." must be performed for the
entire duration of the permit):
Required
Completion/
Implementation
Description of Measure,Activity, Plan, etc. Date
Implement approved Slug/Spill Control Plan. The plan shall Continuous
include but is not limited to:
• description of discharge practices, including non-
routine batch discharges
• description of stored chemicals
• procedures for immediately notifying the POTW of
slug discharges that would cause a violation of 40
CFR 403.5(b), with procedures for follow up
notification within 5 days;
• and if necessary, procedures to prevent adverse
impact from accidental spills, permit limit
excursions, including inspection and maintenance of
storage areas, handling and transfer of materials,
loading and unloading operations, control of plant
site run-off, worker training,building of containment
structures or equipment, measures for containing
toxic organic pollutants (including solvents), and/or
measures and equipment for emergency response.
The permittee shall provide updates to the Control Authority as required by Part
II, 30, of this IUP. Modifications to the measures shall be approved by the
Control Authority prior to installation/implementation. If a measure fails, the
Control Authority shall be notified within 24 hours.
2. Flow Measurement Requirements
(For SIUs with discharge flow meters)
The Control Authority shall maintain appropriate discharge flow measurement
devices and methods consistent with approved scientific practices to ensure the
accuracy and reliability of measurements of the volume of monitored discharges.
Devices installed shall be a continuous recording flow meter capable of measuring
17

Industrial User Pretreatment Permit (IUP)
PART III
Special Conditions
flows with a maximum deviation of less than 10% from true discharge rates
throughout the range of expected discharge volumes. The devices shall be
installed, calibrated, and maintained to ensure accuracy. The meter shall be
calibrated every six (6) months. Modifications to the flow metering equipment
shall be approved by the Control Authority prior to installation. If a required flow
measurement device fails,the Control Authority shall be notified within 24 hours.
3. Certified Laboratory Analysis
Pollutant analysis to be submitted to the Control Authority shall be performed by
a Laboratory that is certified by the State of North Carolina (or others as approved
by the Control Authority) in the analysis of the pollutant in wastewater. Organic
analysis for categorical limitations shall meet quality control standards set forth in
EPA method 1666.
10. Combined Wastestream Formula Flow Condition
(for Categorical Industrial Users only)
Regulated Categorical Process Flow:
The permittee shall have available flow monitoring equipment at such locations as
necessary to measure the total daily volume of wastewater discharged that is
covered by 40 CFR 439.20. This flow monitoring equipment shall also be
capable of measuring flows with a maximum deviation of less than 10%from true
discharge rates throughout the range of expected discharge volumes,however it is
not required that it be continuous recording. The frequency shall be daily and data
shall be collected and reported as required in Part II, 1-4 of this IUP.
Modifications to the flow metering equipment shall be approved by the Control
Authority prior to installation.
18

IUP Synopsis
A. IUP Basic Information
Receiving POTW name: POTW NPDES#:
Little Creek Water Reclamation Facility NC0025453
IUP name: IUP Number:
Grifols Therapeutics,Inc. 0001-02
IUP Effective date: Pipe Numbers,list all regulated pipes:
July 1,2017 001
IUP expiration date: IUP 40 CFR#,if applicable:
June 30,2022 439.20
B. IUP Survey&Application form
Attach a completed copy of the Industrial User Wastewater Survey&
Application Form(see appendix 6-A)
C. IU Inspection form
Attach a copy of an Industrial User Inspection Form(see chapter 7)completed
by the Control Authority within the past 12 months.
D. RATIONALE FOR LIMITATIONS:
As listed on the IUP Limits Page(s), PART I, Section F of the IUP.
RATIONALE#1:
Review of IU Monitoring Data,with no Over Allocation situation:
The following pollutants were assigned numerical limits in this IUP based
on a review of monitoring data for the permittee to determine what ranges of
concentrations are currently being discharged. To account for sample
variability a factor was applied to the monitoring data to determine the
permit limit. Permit limits assigned by the Local IUP Control Authority can
not result in an Over Allocation situation for any pollutants.
BOD
COD
TSS
Total Nitrogen
Total Phosphorus
1

IUP Ss nolsis
RATIONALE#2a:
Categorical Industrial Limits,with no Over Allocation situation:
Check here if Combined Wastestream Formula (CWF) or other categorical
limits calculations were used. If used, Please attach calculations: (see CWF
Spreadsheet,Appendix 6-F)
Were used(attach calculations) I x
Were not used
Total Regulated Wastestream= 517,000 gls.= Process water + wash down
water.
Total Diluted Wastestream= 71,000 gls.= Domestic + Cooling water +
Boiler/Cooling tower blowdown.
Total Wastestream= 588,000 gls. avg. daily.
Combined Wastestream Formula= (Total Regulated Wastestream/ Total
Wastestream)= 517,000/588,000= .88
The following pollutants were assigned numerical limits in this IUP based
on the categorical regulations for monthly limits. These limits do not result
in over allocations.
Acetone: 8.2 mg/1 * .88=7.216 mg/1
n-Amyl Acetate: 8.2 mg/1 * .88=7.216 mg/1
Ethyl Acetate: 8.2 mg/I * .88 =7.216
Isopropyl Acetate: 8.2 mg/1 * .88=7.216
Methylene Chloride .7 mg/1 * .88= .616 mg/1
RATIONALE#3 a:
Over Allocation Prevention,with IU pollutant reduction:
The following pollutants were assigned numerical limits in this IUP based
on allocating the Maximum Allowable Industrial Loading (MAIL)
determined with the Headworks Analysis (HWA) among all Industrial
Users. The total loading of each pollutant from all permitted discharges
does not exceed the MAIL. These limits do not result on over allocations.
RATIONALE#3b:
Interim Limits for IU pollutant reduction:
2

IUP Synopsis
RATIONALE#4:
4.) Other Rationale for Limitations:
The following rationale was used for developing IUP Limits.
Parameter Rationale
BOD Study performed by Hazen &
COD Sawyer.
TSS
T-Nitrogen
T-Phosphorus
RATIONALE#5a:
Non-Categorical Parameters where No Limit needed or assigned in an IUP:
The following pollutants were not assigned numerical limits in this IUP
because the loadings for these pollutants from this IU were less than 5% of
the MARL, or extra reserve capacity was available. The loading of these
pollutants from this IU is considered insignificant at this time. One half of
detection limit used for less than values.
Pollutant 1 Avg SIU lbs/day 5%0 MAHL,lbs/day
Arsenic ! 11 .01656 Monitor only
Silver 11 .012176 .4258
Cadmium .00 11 .2879
Chromium ■ .0025�' .012176 .671
iCo•,-r .0387 .188491 .8175
.0025 IIIIEElga.MIKEEIMP
Lead .0025 .012176 .8515
Mercu .0001 .000487 _ .0014
Molybdenum .0059 .028736 1 .0091.
Nickel .0047 .022892 .4258
Selenium 11 .024353 Monitor onl
Ammonia-N 1.5 7.30584 99.04
1 Zinc 1
L t
Flow avg. 589 m d
3

ROY COOPER
I MN
MICHAEL S. REGAN
G u ruu,
Water Resources S. JAY ZIMMERMAN
ENVIRONMENTAL DUALITY
Uirr<9nl
January 31,2017
Mr. David Auge
Grifols Therapeutics, Inc.
Property Owner
8368 US Highway 70 West
Clayton,NC 27520
Subject: Tax Certification for Pollution Abatement Equipment
Real and Personal Property
Tax Certification Number TCS-RH-235
Grifols Therapeutics, Inc.
Johnston County
Dear Mr. Auge:
As per your request, the staff of the Division of Water Resources have completed
our review of the Tax Certification Request for real and personal property that we
received from your office on December 19,2016.
Please find attached a copy of Tax Certification Number TCS-RH-235 that has been
issued by this office to Grifols Therapeutics,Inc. for the facility located in Johnston
County.
Please note that as part of this Tax Certification process the DENR staff did not
make any efforts to confirm either the cost of the item(s) certified or the year of
acquisition.
If there is a need for any additional information or clarification, please do not
hesitate to contact Brianna Young at [e-mail] or 919-807-6388.
Sin erely,
c(i,y/
John E. Hennessy, Super�+fsor
Compliance&Expedited Permitting Unit
Attachment
Cc: File Copy
State of North Carolina I Environmental Quality I Water Resources
1617 Mail service Center I Raleigh,North Carolina 27699-1617
919 707 9000

t:a
Water Resources
ENVIRONMENTAL QUALITY
North Carolina Division of Water Resources
TAX CERTIFICATION NUMBER TCS-RH-235
In accordance with the provisions of the North Carolina General Statutes G.S.105-275.(8)this is to certify that
Storms Farm located at:
8368 US Highway 70 West
Clayton,NC 27520
Johnston County
filed a request for tax certification for real and personal property covered under the Division of Water
Resources Permit Number NC0025453 with the Town of Clayton, which has a permit with Grifols
Therapeutics,Inc.
Staff of the Division of Water Resources inspected these treatment units and/or equipment on
January 13, 2017 and found based on the information supplied by the applicant that the facilities and/or
equipment listed on the attached application meet the following requirements for Tax Certification:
1. The property has been, or will be, constructed or installed;
2. The property complies with,or if still under construction will comply with,the requirements of
the EMC;
3. The property is being effectively operated, or will when completed be required to operate, in
accordance with the terms and conditions of approvals issued by the EMC; and
4. The property has,or when completed will have,as its primary rather than incidental purpose the
reduction of water pollution resulting from the discharge of sewage or waste.
Please note that as part of this Tax Certification process the DEQ staff did not make any efforts to
confirm either the cost of the items certified or the year of their acquisition.
DATE TAX CERTIFICATION ISSUED:January 31,2017
E. Hennessy, Supervisor
ompliance&Expedited Permitting Unit
cc: Tax Administrator,Johnston County
Central Files
Raleigh Regional Office Files

Tax Certification Inspection Report Determination
Facility- Grifols Therapeutics,Inc.
Tax Certification Number- TCS-RH-235
Inspection Date• /2816 -
1/13 12017
ALL ITEMS LISTED QUALIFY FOR TAX CERTIFICATIO 411011, No
1. Wastewater treatment headworks upgrade Qualifies? No
Comments: See! P,t S of media* cr-/ st/t,P.fil s`wafiwl��t-vl,..c ice, A
,
_ 1/r/14 e'� T trot 1I fowl o l¢ 0([r.Al Lro itg I..Ni> t-(r 5llr n,; 5 (r ..i/i J .�nai
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2. Wastewater treatment MBBR tank replacement
Qualifies? lalP No
Comments: <e , 1 r.,
File name Grifols Therapeutics inspection form(003)
Date printed May 20.2016
Page No 1 of 1

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NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory Donald R. van der Vaart
Governor Secretary
September 3, 2015
Mr. David Auge,Environmental Manager
Grifols Therapeutics,Inc.
8368 Us Highway 70 West
Clayton,NC 27520
Subject: Tax Certification for Pollution Abatement Equipment
Real and Personal Property
Tax Certification Number TCS-RH-216
Tax Certification Number TCS-RH-218
Grifols Therapeutics Wastewater Treatment Plant
Permit No.NC0025453
Johnston County
Dear Mr. Auge:
As per your request,the staff of the Division of Water Resources have completed our
review of the Tax Certification Request for real and personal property that we
received from your office on January 5, 2015.
Please fmd attached a copy of Tax Certification Number TCS-RH-216&TCS-RH-218
that has been issued by this office to Grifols Therapeutics,Inc. for the facility located in
Johnston County.
Please note that as part of this Tax Certification process the DENR staff did not
make any efforts to confnm either the cost of the item(s) certified or the year of
acquisition.
If there is a need for any additional information or clarification, please do not
hesitate to contact Sonia Gregory at [e-mail] or 919-807-6333.
incere ,
John E. Hennessy, S--=sor
Complaince&Expedited Permitting Unit
Attachment
Cc: File Copy
1617 Mail Service Center,Raleigh,North Carolina 27699-1617
Phone:[phone]/http://portal.ncdenr.org/webiwq
An Equal Opportunity\Affirmative Action Employer—Made in part by recycled paper

_ .
AT=11,;,111rA
NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
North Carolina Division of Water Resources
TAX CERTIFICATION NUMBER TCN-RH-216
TAX CERTIFICATION NUMBER TCN-RH-218
In accordance with the provisions of the North Carolina General Statutes G.S.105-275.(8)this is to certify that
Grifols Therapeutics,Inc located at:
Grifols Therapeutics, Inc.
8368 US Highway 70 West(Business)
Clayton,NC 27520
Johnston County
filed a request for tax certification for real and personal property covered under the Division of Water
Resources Permit Number NC0025453
Staff of the Division of Water Resources inspected these treatment units and/or equipment on August 31,2015
and found based on the information supplied by the applicant that the facilities and/or equipment listed on the
attached application meet the following requirements for Tax Certification:
1. The property has been,or will be, constructed or installed;
2. The property complies with,or if still under construction will comply with,the requirements of
the EMC;
3. The property is being effectively operated, or will when completed be required to operate, in
accordance with the terms and conditions of approvals issued by the EMC; and
4. The property has,or when completed will have,as its primary rather than incidental purpose the
reduction of water pollution resulting from the discharge of sewage or waste.
Please note that as part of this Tax Certification process the DENR staff did not make any efforts to
confirm either the cost of the items certified or the year of their acquisition.
DATE TAX CERTIFICATION ISSUED: Se• embe, 3 2015
j �o''E. Hennessy, Superviso
ompliance&Expedited Permitting Unit
cc: Tax Administrator,Johnston County
Central Files
Raleigh Regional Office Files

AltA
RICDEIR
North Carolina Department of Environment and Natural Resources
Pat McCrory Kim H.Colson, P.E. John E. Skvarla, III
Governor Acting Director, Division of Water Infrastructure Secretary-DENR
December 27,2013
Mr. David Auge,Environmental Manager
Grifols Therapeutics, Inc.
83.68 US Highway 70 West
Clayton,NC 27520
Subject: Tax Certification for Pollution Abatement Equipment,
Real and Personal Property
Tax Certification Number TCS-RH-216
Tax Certification Number TCS-RH-218
2/22/2013,Tax Certification Inspection
Grifols Therapeutics Wastewater Treatment Plant
Pretreatment Permit No. 0001-02
Clayton,NC,Johnston County
Dear Mr. Auge:
The Grifols Therapeutics Wastewater Treatment Plant was inspected for Tax
Certification purposes on 2/22/2013. Updates to your Tax Certifications are considered effective
from the date equipment was installed and operational.
Grifols, Talecris, Bayer WWTP equipment and operations at the same site have
previously been inspected and certified for Tax Certification and Exemption purposes for
Wastewater Treatment under authority of DWQ and the Environmental Management
Commission (EMC). The WWTP is located at 8368 US Highway 70 West in Clayton, NC
27520 in Johnston County. The facility holds Pretreatment Permit No. 0001-02 issued by the
Town of Clayton. Tax Certification requires continued compliance with all Division of Water
Quality and Environmental Permits. Should compliance not be maintained please notify James
Warren at the Town of Clayton WWTP, The NC-DWR-Regional Office, this office, and the
Johnston County Tax office.
A copy of your Tax Certificate and Inspection Determination Form are attached to this
letter. Copies are also sent to the County Tax Office. During the inspection and review it was
determined that all items listed on your application are being used exclusively for Wastewater
Treatment and are therefore eligible to receive tax certification. No items listed were determined
to be ineligible for Tax Certification.
Please note that as part of this Tax Certification process, the inspector did not make any
efforts to confirm either the cost of the items certified, the year of acquisition, if items have
received other Tax Certifications from Air Quality, Solid Waste or other agencies, or if items
that have previously received Wastewater Treatment Tax Certification are still present and
operational.
FILE NAME!TCERT-2013-tsp,Grifols-Clayton,F0-Trans-Letter,TCS-RH-218-218.doox
NC-DENR,DWI,Division of Water Infrastructure, !,.ncgenr.or4/Web/WI/ 919-707.9160
NC-DENR,DWR,Division of Water Resources, '3tpr.org/ 919-707-9000 NjOr C/a+ryoi na
MAIL ADOFRESS: 1833 Mail Service Center,Raleigh NC 27899-i633 `, 1'K�s4i K I
TAX CERTIFICATIONS: TCS-RH-218,and TCS-RH-218,INSPECTION DATE: 2/22/2013
Cc distribution: Original,Town of Clayton,Johnston County Tax Office,NC-DWR

ALVA
Mat
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
TAX CERTIFICATION NUMBER TCS-RH-216
TAX CERTIFICATION NUMBER TCS-RH-218
In accordance with the provisions of the North Carolina General Statutes C.S. 105-275.(8),
this is to certify that:
GRIFOLS THERAPEUTICS, INC.
PRETREATMENT WASTEWATER TREATMENT PLANT
8368 US Highway 70 West(Business), Clayton NC 27520,in JOHNSTON COUNTY
filed a request for tax certification for real and personal property covered under the
Town of Clayton Pretreatment Permit No. 0001-02
to discharge Pretreated Industrial Wastewater to the Town of Clayton's
Little Creek Wastewater Reclamation Facility NPDES Permit No. NC0025453
Staff of the Division of Division of Water Quality inspected these wastewater treatment facilities and
equipment on February 22.2013. As of this date,based on the inspection and information supplied
by the applicant all the equipment and facilities listed on the attached application that meet the
following requirements for Tax Certification are eligible.
1. The property has been,or will be,constructed or installed;
2. The property complies with,or if still under construction will comply with,the
requirements of the EMC;
3. The property is being effectively operated,or will when completed be required to operate,
in accordance with the terms and conditions of approvals issued by the EMC; and
4. The property has, or when completed will have, as its primary rather than incidental
purpose the reduction of water pollution resulting from the discharge of sewage or waste. t
Items listed that are not eligible for Tax certification: none
Please note that as part of this Tax Certification process,the DENR staff did not make any efforts to
• confirm either the cost of the items certified or the year of their acquisition. This WWTP Facility
has previously been inspected for Tax Certification. Tax Certification requires continued
compliance with Clayton and DWQ&DWR Permit conditions.
DATE TAX CER'I'WlCATION ISSUED: December 27,2013
•
Tom S. Poe
Construction and Wastewater Treatment Inspector
NC-Division of Water Infrastructure
cc: Tax Administrator,JOHNSTON COUNTY
NC-DWI,Division of Water Infrastructure Tax Certification Files
NC-DWR,Division of Water Resources Tax Certification Files,
Town of Clayton
Ar*somminrwmamwramm-^G::..._.sr-.---•_.. "• mrTMIcssia.TMW saw:••Y•",fiY:t'Y•:••'•` 'Y''•%.••AY"•—•.^•Gii.`_JaYti">W"Y...v.—woww�'.°]""^•"'1P1!'.r`W�V!! •�

Mr. David Auge, Environmental Manager, Grifols Therapeutics, Inc.
836E US Highway 70 West(Business), Clayton, NC 27520
TAX CERTIFICATIONS: TCS-RH-216 and TCS-RH-218
INSPECTION DATE: 2/22/2013
If you have any questions, you may contact me at([e-mail]), or at 919-616-
4245 (cell). Future Tax certifications will be processed by others in the Division of Water
Resources that you may contact at 919-707-9000, http://www.ncwater.org/ or by e-mail to
([e-mail],).
Sincerely,
s
Tom S. Poe,
Construction and WWTP Inspector
NC-DWI,Division of Water Infrastructure
List of Attachments:
1. Transmittal Letter
2. Tax Certificate
3. Determination Forms,(a list of items from application that were certified)
4. Application Forms submitted by Grifols
cc: NC-DWR,Tax Certification Files
James Warren,Water Reclamation Superintendent,
P.O. Box 879, Clayton, NC 27520
Pat Goddard,Johnston County Tax Administrator
P.O. Box 451, Smithfield,NC 27577,
Phone: [phone], Fax: [phone]
E-Mail: taxaffice®johnstonnc.com
File name -rCERT-2013-tep,Grifds-Clayton,FO-Trans-Letter,TCS-RH•218-218.docx TAX CERTIFICATIONS: TCS-RH-216,&TCS-RH-218
NC-DENR,DWI,Division of Water Infrastructure, .1/portal n[,; 919-707.9180 INSPECTION DATE: 2/22/2013
NC-DENR,DWR,Division of Water Resources, ryW, ater.ora/ 919-707-9000 TRANSMITTAL LETTER PAGE: 2 of 2
Mail Address; 1633 Mail Service Center,Raleigh NC 27699-1633

GRIFOLS, CLAYTON, NC Tax Certification Inspection: 2/22/2013
TO: TAX CERTIFICATION FILES,and others
FROM: TOM S.POE
DATE: 2/22/2013
SUBJECT: TAX CERTIFICATION
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File name: TCERT-2013-tsp,Gritols-CIayton,MEMO-w-PHOTOS•2013-02-22,Pgs-w6-2x3s.docx DATE: 2/22/2013
NC•DENR,DWI,Division of Water Infrastructure,httoJ/ooRel.ncdenr.o 919-707-9100 PAGE: 1 of 2
NC-DENR,BWR,Division of Water Resources,Ditto://www.ncwater.orro/ 919-707-9000
Mail Address: 1833 Mali Service Center.Raleigh NC 27899.1833

GRIFOL5, CLAYTON, NC Tax Certification Inspection: 2/22/2013
TO: TAX CERTIFICATION FILES,and others
FROM: TOM S.POE
DATE: 2/22/2013
SUBJECT: TAX CERTIFICATION,TCS-RH-218
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NC-DENR,DWI,Division of Water infrastructure, L;lln.4 919-707-9160 PAGE: 2 of 2
NC-DENR,25WR,Division of Water Resources, fiww, 919-707-8000
Mall Address: 1633 Mail Service Center,Raleigh NC 27699-1633

TAX CERT No. TCS-RH-213 Inspection Date: 5/12/201
FACILITY. TALECRIS BIOTHERAPEUTICS WWTP COUNTY- JOHNSTON COUNTY
ADDRESS: 8368 Highway 70 West(Bus.), Clayton, NC 27520 CONTACTS: David Auge, 919-359-4375
Pretreatment Permit No_ 0001-02, Clayton NPDES No. NC0025453 CG&L, Tom Poe
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NCDF.NR,DWQ Tax Certification, CG&L 919-733-6900,www.nccgi.net
Fare name r TCERT-2013-tsp,Grifols-Clayton,M02-Site-maps.docx

Tax Certification Inspection Report Determination
Facility Grifols Therapeutics, Inc.
Tax Certification Number ..TCS-RH-216
Inspection Date• 2/22/2013
ZO
ALL ITEMS LISTED QUALIFY FOR TAX CERTIFICATION: Yes Q No 0
1. Dissolved Air Flotation System(DAF) Qualifies? 416, No
Comments:
As demonstrated by Mr.David Auge
2. Sanitary Sewer Mechanical Bar Screen Filter System
Qualifies? Yes No
Comments:
As demonstrated by Mr.David Auge
3. WWTP Flow Increase Improvement Qualifies? 4220 No
Comments:
As demonstrated by Mr.David Auge
4. WWTP Capacity Increase for NFF Qualifies? 1§20 No
Comments:
As demonstrated by Mr.David Auae
File name: Grifols-Determination-LisLTCS-RH-216.doc
Date plated: December 25,2013
Page No. 1 of 1

Tax Certification Inspection Report Determination a
Facility Grifols Therapeutics, Inc.
Tax Certification Number TCS-RH-218
Inspection Date• ..2/22/2013
I I D
ALL ITEMS LISTED QUALIFY FOR TAX CERTIFICATION: Yes Q No 0
1. WWTP Flow Increase Improvement Qualifies? lab No
Comments:
As explained by David Auge on 2/22/2013
2. WWTP Capacity Increase for NFF Qualifies? Yes No
Comments:
As explained by David Auge on 2/22/2013
Photographs attached
File name: Grifols-Determination-List,TCS-RH-218.doc
Date printed: December 25,2013
Page No. 1 of 1

w
it A
IRat
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H.Sullins Dee Freeman
Governor Director Secretary
December 28,2011
Mr.David Auge,Environmental Manager
Taleoris Biotherapeutics,Inc.
8368 US Highway 70 West
Clayton,NC 27520
Subject: Tax Certification for Pollution Abatement Equipment,
Real and Personal Property
Tax Certification Number TCS-RH-213
Talecris Biotherapeutics Wastewater Treatment Plant
Pretreatment Permit No.0001-02
Clayton,NC,Johnston County
Dear Mr.Auge:
The Division of Water Quality has completed the review of the Tax Certification request
for real and personal property for the Talecris Biotherapeutics Wastewater Treatment Plant. The
WWTP is located at 8368 US Highway 70 West in Clayton,NC 27520 in Johnston County. The
facility holds Pretreatment Permit No.0001-02 issued by the Town of Clayton under authority of
their Little Creek Water Reclamation Facility with DWQ issued NPDES Permit No,
NC0025453. Permit No.NCG060039 was not considered for Tax Certification purposes.
The Talecris Wastewater Treatment Plant was inspected for Tax Certification purposes
on 5/6/2011. Updates to the Talecris Tax Certification are considered effective from this date.
Talecris has previously been inspected and certified for Tax Certification and Exemption
purposes for Wastewater Treatment and the reduction of water pollution under authority of
DWQ and the Environmental Management Commission(EMC)on 11/13/2008,2005, 1/1/2007,
and 7/9/2001 (under the name of Bayer)
Tax Certification requires continued aimpa/once with all Div ion of Water Quality
Perrni4. Should compliance not be maintained please notify James Warren at the Town of
Claytin WWTP,our Regional Office,this office,and your county Tax office.
A copy of your Tax Certificate and Inspection Determination Form are attached to this
letter. Copies are also sent to the County Tax Office. During the inspection and review it was
determined that all items listed on your application are being used exclusively for Wastewater
Treatment and are therefore eligible to receive tax certification. No items were determined to be
not eligible for Tax Certification.
File name:2011-TCert Talecris-Claytom o.Co,F1-Trans-Lettecdocx
Cc distribution: Original,Town of Clayton,Johnston County Tax Office,DWQ-C(&l,DWQ-Central,DWQ-RRO
Construction Grants and Loans Section,1633 Mail Service Center Raleigh NC 27699.1633 IO l i1C�TQ�Ifla
Phone:[phone]/FAX [phone]/Internet www.nccgl.net, DENR Customer Service 1-877-623-6748
An Equal Opportunity/Affirmative Action Employer—50%Recycled/10%Post Consumer Paper 1
jyd-y fyaI4f

Mr. David Auge, Environmental Manager,Talecris
8368 US Highway 70 West(Business),Clayton, NC 27520
Tax Certification for Wastewater Treatment
Page 2 of 2
Please note that as part of this Tax Certification process, the inspector did not make any
efforts to confirm either the cost of the items certified, the year of acquisition, if items have
received other Tax Certifications from Air Quality, Solid Waste or other agencies, or if items
that have been previously listed for Wastewater Treatment Tax Certification are still present and
operational.
For future Tax Certifications please provide a list of all properties and assets for which
you currently have or want Wastewater Tax Certification,a copy of previous Tax Certifications,
a flow schematic of your WWTP,and a statement of compliance with permit conditions. If you
have any questions,please contact Tom Poe at([e-mail]),phone[phone]),
or Mark Hubbard,Assistant Chief,DWQ Construction Grants and Loans Section at
(mark.hubbard(Qncdenr.gov),phone[phone]), or fax[phone]).
Sincerely,
1 ► S.
Tom.S.Poe,Inspector
Construction Grants and Loans Section
List of Attachments,(to Applicant,County Tax Department,and to DWQ Files)
1. Transmittal Letter
2. Tax Certificate
3. Determination Form
A list of items on your Application Form that were inspected and certified,
or noted as not eligible to be Certified.
4. Photos of Facility
5. Map(s): Showing the site,WWTP area, and vicinity for location and access to site.
* Tax Certification Package Check List(with CG&L copy only)
ITEMS SUBM1YUI�D BY APPLIACNT:
6. Cover Letter
7. Application Form for Tax Certification
Attachments to Application Form: (Pretreatment Permit,Previous Tax Certifications)
8. Site plan and/or tax maps
9. Wastewater Treatment Permit(s)
Pretreatment Permit issued by the Town of Clayton IUP 0001-02)
(issued 7/23/2010,expires 6/30/2012)
cc: DWQConstruction Grants and Loans Section,Tax Certification Files
DWQ Central Office Files
DWQ Raleigh Region Office
James Warren,Water Reclamation Superintendent,P.O.Box 879,Clayton,NC 27520
Pat Goddard,Johnston County Tax Administrator,[e-mail]
P.O.Box 451, Smithfield,NC 27577, Phone:[phone], Fax: [phone]
DWQ,CG&L Tax Certification
File name: 2011 TCert,Talecrls-Clayton;Io-Co,F1-Trans-Letter.doa

Arai
NORTH CAROLrNA DEPARTMENT OF
2i4VtRONMENTAND NATURAL RESOURCES
North Carolina Division of Water Quality
TAX CERTIFICATION NUMBER TCS-RII-213
In accordance with the provisions of the North Carolina General Statutes G.S. 105-275.(8),
this is to certify that:
TALECRIS BIOTUERAPEUTICS,INC.
PRETREATMENT WASTEWATER TREATMENT PLANT
8368 US Highway 70 West(Business),Clayton NC 27520,in JOHNSTON COUNTY
filed a request for tax certification for real and personal property covered under the
Town of Clayton Pretreatment Permit No.0001-02
to discharge Pretreated Industrial Wastewater to the Town of Clayton's
Little Creek Wastewater Reclamation Facility NPDES Permit No. NC0025453
Staff of the Division of Division of Water Quality inspected these wastewater treatment facilities and
equipment on May 12.2011. As of this date,based on the inspection and information supplied by the
applicant all the equipment and facilities listed on the attached application that meet the following
requirements for Tax Certification are eligible.
1. The property has been,or will be,constructed or installed;
2. The property complies with,or if still under construction will comply with,the
requirements of the EMC;
3. The property is being effectively operated,or will when completed be required to operate,
in accordance with the terms and conditions of approvals issued by the EMC;and
4. The property has, or when completed will have, as its primary rather than incidental
purpose the reduction of water pollution resulting from the discharge of sewage or waste.
Items listed that are not eligible for Tax certification: none
Please note that as part of this Tax Certification process,the DENR staff did not make any efforts to
confirm either the cost of the items certified or the year of their acquisition. This Facility has
previously been Tax Certified for their wastewater treatment on several dates including/1/13/2008
and 7/9/2001. Tax Certification requires continued compliance with Clayton and DWQ Permit
conditions,
DATE TAX CERTIFICATION ISSUED: December 2 ,2011
P9 2
Mark L. Hubbard,P.E.,Assistant Chief
Project Management Branch
Construction Grants and Loans Section
cc: Tax Administrator,JOHNSTON COUNTY
DWQ Construction Giauts&Loans Section Tax Certification Files
DWQ Central Files,DWQ Raleigh Regional Files,Town of Clayton

Tax Certification Inspection Report Determination
FACILITY: TALECRIS BIOTHERAPEUTTCS WWTP
Inspection Date. 5/12/2010
Tax Certification No:......
Town of Clayton Pretreatment Permit No.0001-02
Town of Clayton NPDES Permit No.NC0025453
LOCATION: 8368 highway 70 West(Business),Clayton,NC 27520
COUNTY: JOHNSTON COUNTY
CONTACTS: David Auge,Environmental Manager(919-359-4375)
[e-mail]
Previous Tax Certification Dates&Numbers:
11/13/2008, TCS-RH-191
Facility was previously Permitted and Certified as Bayer
2005,2007,files incomplete
7/9/2001, TCS-RH-020
ALL ITEMS LISTED QUALIFY FOR TAX CERTIFICATION: Yes ® No❑
1. Dissolved Air FIotation System(DAF) Qualifies? Yes El No ❑
Comments:
2. Foundation for CO2 Tank Qualifies? Yes I No 0
Comments:
3. SanitarySewer Mechanical Bar Screen
crxn Filter System
Qualifies? Yes Ed No 0
Comments;
4. WWTP Dual 40 HP Pump Skid Qualifies? Yes Q No ❑
Comments:
File name:1011-TCart,Titecrie-Cteyton4o-Co,F3a-Dete:ado-Let-pamdoc

TAX CERTIFICATION INSPECTION DETERMINATION:
FACILITY:..»........»..... BIOTHERAPEUTICS WWTP
Inspection Date. ...».5/12/2010
Tax Certification No:..»Mp.TCS-RS-213
Town of Clayton Pretreatment Permit No.0001-02
Town of Clayton NPDES Permit No.NC0025453
LOCATION: 8368 highway 70 West(Business),Clayton,NC 27520
COUNTY: JOHNSTON COUNTY
CONTACTS: David Auge,Environmental Manager(919-359-4375)
[e-mail]
Previous Tax Certification Dates&Numbers:
11/13/2008, TCS-RH-191
Facility was previously Permitted and Certified as Bayer
2005,2007,files incomplete
7/9/2001, TCS-RH-020
Au ITEMS LISTED QUALIFY FOR TAX CERTIFICATION: Yes® NoD
ELIGIBLE ITEMS INCLUDE:
1. Dissolved Air Flotation System(DAP)WWTP Qualifies? Yes® No 0
2. Foundation for CO2 Tank Qualifies? Yes m No 0
3. Sanitary Sewer Mechanical Bar Screen Filter System,Qualifies? Yes 0 No 0
4. WWTP Dual 40 HP Pump Skid Qualifies? Yes 0 No 0
Comments: The equipment is installed and photographs were taken. The WWTP and listed
equipment appear to comply with permit requirements,be effectively operated, and that the
primary purpose is the reduction of water pollution
NON-ELIGIBLE and/or PARTIALLY ELIGIBLE ITEMS:
• NONE
Please note:
ELIGIBLE for Tex Certification,
Only the portions of any properties and equipment that are permitted by DWQ as necessary for
the treatment end disposal of wastewater are certified for tax purposes. This includes portions of
property required for access,maintenance,operation, Inspection, and buffer zones that are listed
in the Pretreatment and/or DWQ Parings) are also certified for tax purposes. Treatment
Facilities must be compliant with permit condition to be eligible for tax certification. Self reporting
of noncompliance is expected for Tax Certttbatlon.
NOT ELIGIBLE for Tax Certification,
Any parts of any propertiee that are not used exclusively (100%) for permitted wastewater
treatment and disposal are not certified for tax purposes. Any equipment or t eatment facilities
that are not operational,property maintained,and compliant with permit conditions are not eligible
for Tax Certification.
DM,CG&L Tex Certification InspectionDetermination
File Name 2011-T ,Talents-Claytat4o-Co,F5b-Determination-Lst.doc

• o W A r�p Governor Michael F.Easley,Goveor
r
William G.Ross Jr.,Secretary
ii� •_• tir
North Carolina Department of Environment and Natural Resources
?
p Coleen H.Sullins,Director
- Division of Water Quality
November 13,2008
Mr. Alfred P.Marzetti
Talecris Biotherapeutics,Inc.
8368 US Highway 70 West
Clayton,NC 27320
Subject: Tax Certification for Pollution Abatement Equipment
Real and Personal Property
Tax Certification Number TCS-RH-191
Talecris Biotherapeutics,Inc.,North Carolina
Johnston County
Dear Mr. Marzetti:
As per your request, the staff of the Division of Water Quality has completed the review
of the Tax Certification Request for real and personal property that was received from your
office on September 18,2008.
Please find attached a copy of Tax Certification Number TCS-RH-I91 that has been
issued by this office to Talecris Biotherapeutics, Inc.for the facility located in Johnston County.
A copy of this Certification is being sent to the Johnston County Tax Office along with a copy of
this letter. During the review, this office identified item(s) that did not meet the established
criteria to receive tax certification. The item(s) not receiving certifications are identified on the
Tax Certification.
Please note that as part of this Tax Certification process that the DENR staff did not make
any efforts to confirm either the cost of the items certified or the year of acquisition.
If there is a need for any additional information or clarification,please do not hesitate to
contact either Mr. Antonio Evans of our staff at [e-mail] or 919-715-6220 or
Mark Hubbard at [e-mail] or 919-715-6224.
Sincerely,
GGG '&10
aniel M.BI 'sdell,P.E., Section Chief
Construction Grants and Loans Section
AVE/sd
Attachment
Cc: Ms.Pat Goddard,Johnston County Assessor
Construction Grants and Loans Section
Raleigh Regional Office(Bany Herzberg)
PERCS Dana Foley(Pretreatment Permit#001-02 under NPDES Permit NC0025453)
Construction Grants and Loans Section Me
1633 ll
Mail Service Center Raleigh NC 27699-1633 n r' OI11Q�
Phone:[phone]/FAX:[phone]/Internet:www.nccgl.net Nor
An Fount Onoortunity/Affirmative Action Employer—50%Recycled/10%Post Consumer Paper ( �r

lf�
•
1-5)
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
•
North Carolina Division of Water Quality
.1 TAX CERTIFICATION NIJMBER TCN:TCS-Rll-191
In accordance with the provisions of the North Carolina General Statutes G.S.105-275.(8)this is to certify
. that:
• TALECRIS BIOTHERAPEUTICS,INC.
8368 US HIGHWAY 70 WEST
CLAYTON,NORTH CAROLINA
JOHNSTON COUNTY
filed a request for tax certification for real and personal property covered under the Pretreatment Permit
Number 0001-02 that discharges to the Little Creek Water Reclamation Facility,NPDES Permit Number
1 NC0025453.
1. Staff of the Division of Division of Water Quality inspected these treatment units and/or equipment on
• November 3, 2008 and found based on the information supplied by the applicant that the facilities and/or
equipment listed on the attached application with the exception of the following item: 10(ten)-MBBR Spare
50 HP Pump from the application form meets the following requirements for Tax Certification:
1. The property has been, or will be, constructed or installed;
2. The property complies with,or if still under construction will comply with,the requirements of
the EMC;
3. The property is being effectively operated, or will when completed be required to operate,in
accordance with the terms and conditions of approvals issued by the EMC;and
4. The property has,or when completed will have,as its primary rather than incidental purpose the
reduction of water pollution resulting from the discharge of sewage or waste.
Please note that as part of this Tax Certification Process that the DENR sfgffdid not make any efforts
to confirm either the cost of the items certified or the year of their acquisition.
DATE TAX CERTIFICATION ISSUED:November 13,2008
1
111/z / 444
Daniel M.Blaisdell,P.E., Section Chief
Construction Grants and Loans Section
Cc: Ms. Pat Goddard,Johnston County Assessor
Construction Grants and Loans Section
Raleigh Regional Office(Barry Herzberg)
• PERCS Dana Foley(Pretreatment Permit#0001-02 under NPDES Permit NC0025453)
Q3-01-07

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I
Stale of pi orth Carogina. 143r.44:1Wr
.
Departnuant of Environment .
and NatL aff Resourcesh 1 ,.. fVfl
v r r
' ,J ,
pivgsnon ofi , Rcz
�averlu�ls � � r ,,a
htoR-rN cAzauwa.Dr., -rr of •
Mvchaed F. Ea fey, Governor osivIRONNIENT AND NARJ2AL RESOURCS
. William G. Rq s, Jt-., Secretary
Kerr L Steve.s, Director
' DIVISION OF WATER QUALITY
July 9,2001
.
Mr.•Doug Homer •
/o Grant Thorntt n, LLP
1101 Walnut,S.E.b a 1900
Kansas City,MCA 64106-2l43 •
' Subject: Tax Certification
Bayer Corporation
Facilities
ter Pretreatment
� - Industrial Wastewa
• • • Certificate of Approval
• No. TCS-RH020
1 Johnston County
DearMr.Homer:
' •
cation CS-RH020 coverirn.g the
Transmitted here •th are two (2) copies of the Talc Cerfifi )
wastewater tre. ■• -is t facilities that have bean constructed in accordance with the Town of
Clayton Industrial. User Pretreatment Permit No. 0001-97, which became effective on June 30,
• 1997, was m.ocii ff d on November 12, 1997, expires on.Time 30,2002, and is issued to Bayer
Corporation_
Bayer Corpora-idol may use this Certification to obtain tax benefits in accordance with the
appropriate North Carolina General Statutes [NCGS 105-275(8)]. The items included in the
certification are iii lulled on the attached list_ Staff from the Division of Water Quality's Raleigh
Regional Office h ye confirmed the construction of the items on the list,but have not attempted
to judge any prop,rty tax values.
5
., 1
I

•
-1
NORTH CAROLTNA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
RALEIGH, NORTH CAROLIN4_
TAX CER'1'ThICATION
•
(Franchise/Privilege;Amnrtzatian;Property)
In •
accord provisions mi nce the of the General Statutes of North Carolina(G.S. 105-275(8)),
thiq is to certify t -
BASrER CORPORATION
JOHNSTON COTJNTY
has been issued dustrial User Pretreatment Pen'mt No- 0001-97 for the operation of a
wastewater pretr4 the facility that iff ohargea to the Town of Clayton Wastewater Treatment
Plant. Tlie waste ter pretreatment facilities consist of the items that are included on the
Attachrn ent I Eq; ipment List,which is attached to this document These wastewater
•
pretreatment faci4 ties were-cnns'ructed at the Bayer Corporation faclity in Johnston County and
are being operate! .in accordance with the Town of Clayton Industrial User Pretreatment Permit
No_ 0001-97.
The Environmen,: Management Commission(EMC)-and the Department of Environment and
Natural Resource: have found that the facility referenced above:
a. has been constructed and placed into operation; and
b. complies with the requirements of the EMC;and
• c. is being operated in accordance with the terms and conditions of
Industrial Pretreatment Per]it No_ 0001-97,which became
effective on Tune 30; 1997; and
•
d. has as its primary,rather than its incidental purpose,the reduction
of pollution resulting from the operation of the facility.
.

August 8,2006
Mr.Robert Souza
Principal Engineer
Utilities Department
Talexis Biotherapeutics,Inc.
8368 US 70 West
Clayton,North Carolina 27520
Subject Authorization to Construct Permit
Talecris Biothapeutics Wf
Treatment Facility Upgrade and Expansion
Industrial User Permit(IUP)0001-02
Dear Mr.Souza:
Reference is made to:(1) your February 1. 2006 letter requesting an Authorization to
Construct (ATC) Permit for construction of the proposed Talecris's Wastewater
Treatment Facility Upgrade and Expansion, (2) July 20, 2006 letter from Stearns &
Whaler, PLLC, that provides responses to our review comments on the supporting
documents submitted with the request fox ATC Permit, and (3) August 7, 2006 e-mail
from John Brinkley concerning addition of third blower with necessary piping
modifications at the MBBR tanks. We have reviewed the responses provided in the July
20, 2006 letter and found to be satisfactory. Authorization is hereby granted for
construction of the proposed Talecris's wastewater treatment facility upgrade and
expansion to handle increase in BOD and COD Loadings with the stipulation that the
construction of the proposed facilities shall not proceed. until the Town receives a
complete revised set of contract documents signed and sealed by a Professinr'el Engineer
in The State of North Carolina.The construction and installation will include:
1. Two stage MBBR system, designed to handle 0.5 mgd average daily flow with
average BODS and COD loadings of 13,340 lbs/day and 20,000 lbs/day,
respectively
2. Ammonium hydrox;rie feed system for nitrogen feed to MBBR system. The
system will include one 10,000 gallon bulk storage tank, and two chemical feed
pumps(0.02 20 gal/hr capacity,each).
3. Use of the misting liquid alura storage tank and installation of two new alum
dosing pumps(0.02-4.5 gal/hr capacity,each).

4. Defoamer chemical feed system consisting of one bufx defoamer chemical tank
and two defoamer metering pumps(0.002-1.0 gal/hr capacity,each).
5. One 500 gpm capacity Dissolved Air Flotation system complete with one DAF
tank,two air dissolution pumps (100 gpm capacity,each),two progressive cavity
sludge pumps (150 gpm capacity, Pseli),and two polymer feed pumps (0.025-1.0
gph capacity,each).
6. Two aerated sludge holding tanks(40,000 gal capacity,each),each equipped with
10 hp miser/aerator.
7. A new sludge storage building (Pre-engineered metal building) to house three
sludge storage containers for sludge dewatering and disposal needs,and
8. All associated valves,piping electrical and controls and appurtenances.
The Autholization to Construct is issued in accordance with Part II,Paragraph 26 of the
Pretreatment Permit No.0001-02,and shall be subject to revocation unless the wastewater
treatment facilities are constructed in accordance with the conditions and limitations
specified In the Permit Number 0001-02, and in accordance with the final plans and
. specifications submitted for review. A copy of the authorized plans and specifications
sh 11 be murintsfrwl on file at the pretreatment facility.
Upon completion of construction and prior to operation of this permitted wastewater
treatment system improvements a certification must be received by the Town of Clayton
from a Professional Engineer certifying that the permitted improvements has been
installed in accordance with the Pretreatment Permit,this Authorization to Construct and
the approved plans and specifications,
Talecris must notify the Town of Clayton at least 48 hours in advance of operation of
installed facilities so That an in-place inspection can be made. Such notification shall be
Diade during normal office hours of 8:00 A.M. until 5:00 P.M. on Monday to Friday,
excluding Town holidays. •
The sludge generated from these facilities must be disposed of in accordance with G.S.
143-215.1 and in a manner approved by the North Carolina Division of Water Quality.
The issuance of this Permit does not preclude the Permittee from complying with any anti
all statutes, rule, regulations, or ordinances of the Town, the State, or the Federal
Government. Failure to abide by the requirements contained in.this Authoiize:6m to
Construct may subject to an enforcement action by the Town,the State, or the Federal
Government in accordance with the Town's Sewer Use Ordinance, North Carolina
General Statue's 143-215.6Ato 143-215.6C,and Federal Regulations.
Following the commissioning of the proposed plant improvements, effluent from the
DAF will be conveyed to the existing aeration basin followed by the two existing
clarifiers before being discharged to the Town's wastewater collection and treatment
system. A lockable valve shall be installed on the DAF effluent discharge pipe to the
Towles wastewater collection and treatment system.This valve will have a lock provided
by the Town.The intent of such arrangement is to operate the new treatment facilities in
series with the existing wastewater treatment system to gather necessary DAF effluent
quality data to support the direct discharge of DAF effluent to the Town's wastewater
collection system. in order to meet the reliability criteria Talecris shall provide another

DAF unit prior to the removal of the existing aeration basin and.clarifiers facilities for the
Talecris'a expansion needs.
In the event that the facilities fail to perform satisfactorily, including the creation of
nuisance conditions, the Pezmittee shalt take iTnTneriiRte corrective action and notify the
Town. Construction of additional or replacement pretreatment facilities will require
another Authorization to Construct.
If you have any questions concerning this matter,please call me at 919-S53-1536.
Sincerely,
fames Warren
LCWRF Superintendent
C: Tim Simpson,Director of Public Utilities.
Shenker Misty, The Wooten Company
1

TOWN OF CLAYTON
"SERVICE" OPERATIONS CENTER -ENVIRONMENT'
ELECTRIC SERVICE /GA Rp. PUBLIC WORKS
[phone] ,z._. ;'\
[phone] 1�
VEHICLE MAINTENANCE ;1 1ZO ' WATER RECLAMATION
[phone] ;`= [phone]
October 13, 2016
Rob Souza
Utilities Operations Engineering Manager
Grifols Therapeutics
8368 US 70 West
Clayton, NC 27520
Re:Temporary Limits
Mr.Souza:
As you are aware, Hurricane Matthew resulted in the flooding of the Johnston County Water
Reclamation Facility.As an emergency measure the Town was requested to divert the complete flow
from East Clayton Industrial Area pump station to Clayton. We expect the Johnston County Facility will
be back in service within thirty days.
In order to protect the Clayton plant from upset,the following temporary limits will be in place.
Daily flow: 680,000 gpd on a monthly average,900,000 gpd maximum.
BOD: 300 mg/I on a monthly average.
TSS: 300 mg/I on a monthly average.
Ammonia: 20 mg/I on a monthly average.
Total Nitrogen: 25 mg/I on a monthly average.
Total Phosphorus: 10 mg/I on a monthly average.
You may contact me directly at 919-553-1536 if you have questions.
erely,
fafnes Warren
Town of Clayton
Wastewater Operations Superintendent
Copy:
Tim Simpson,Town of Clayton
Deborah Gore, PERCs NCDEQ
653 Highway 42 West•P.O.Box 879•Clayton.North Carolina 27520•[phone]•Fax[phone]

TOWN OF CLAYTON
"SERVICE" OPERATIONS CENTER "ENVIRONMENT"
ELECTRIC SERVICE , CA l PUBLIC WORKS
[phone] ,�� �� [phone]
Q L�M_
VEHICLE MAINTENANCE zT�N WATER RECLAMATION
[phone] GZ [phone]
September 18, 2015
Certified Mail
Sergi Roura, President
Grifols Therapeutics
8368 US 70 Business West
Clayton,NC 27520
Re: Amended Industrial User Permit
Mr. Roura:
Enclosed please find an amended Industrial User Permit#0001-02. Please attach the new
permit to your current permit.
This amended permit no longer contains maximum daily limits for COD, BOD and TSS.
The maximum daily flowrate was increased to 1.1 mgd with a weekly average of.9 mgd.
The flow limits are necessary to prevent overflow situations at the pump station.
Please note the sampling responsibility for the facility has been reassigned to the Control
Authority(Town of Clayton)or its designee. The only exception is the daily flow rate.
Grifols has a right to split samples during any event. Should Grifols decide to collect
samples on the effluent the results will need to be submitted to the Control Authority.
Grifols will need to submit an updated Spill and Slug control plan by December 31, 2015.
This plan will need to include the new facility and its associated waste streams and a plan
to manage the MBBR effluent during shut down periods.
Grifols will need to keep the existing treatment units post MBBR viable for a minimum
of one year as per the Development Agreement between Grifols and the Town of
Clayton.
If any parts, measurement frequencies, or sampling requirements contained in this permit
are unacceptable to you, you have the right to an adjudicatory hearing upon written
request within thirty (30) days following receipt of this letter. Unless such demand is
made,this decision shall be final and binding.
Please contact me directly at 919-553-1536 if you have any questions.
653 Highway 42 West•P.O. Box 879•Clayton,North Carolina 27520•[phone]•Fax[phone]

Sincerely,
es Warren
Town of Clayton, Wastewater Operations Superintendent
Copy: Steve Biggs
John Brinkley
Tim Broome
Tim Simpson

Town of Clayton
Control Authority and/or Municipality
PERMIT
Industrial User Pretreatment Permit(IUP)
To Discharge Wastewater Under the
Industrial Pretreatment Program
0001-02 439.20
IUP Number 40 CFR Category(if Applicable)
In compliance with the provisions of North Carolina General Statute 143-215.1, any
applicable federal categorical pretreatment regulations, all other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Control Authority and/or Municipality Sewer Use Ordinance. The
following Industry, hereafter referred to by name or as the permittee:
Industry name,permittee:
Grifols Therapeutics, Inc.
Facility Located at Street Address
8368 US 70 West
City
Clayton
State,Zip
North Carolina 27520
is hereby authorized to discharge wastewater from the facility located at the above listed
address into the sanitary sewer collection system and the wastewater treatment facility of
the Control Authority and/or Municipality listed below:
IUP Control Authority and/or Municipality WWTP name:
Little Creek Water Reclamation Facility
NPDES Number:
NC0025453
WWfP Address:
Durham Street Ext. (PO Box 879)
City,State,Zip
Clayton,North Carolina 27520
in accordance with effluent limitations, monitoring requirements, and all other conditions
set forth in Parts I, II, and III of this Industrial User Pretreatment Permit(IUP).
Effective date,this permit and the authorization to discharge shall become
effective at midnight on this date:.
September 16,2015
Expiration date,this permit and the authorization to discharge shall expire al
midnight on this date:
June 30, 2017
kPaiN6.(4 /(o/ Zv(5 ai G cP,
Date signed Warren,Wa er Reclamation Superintendent

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
IUP, PART I, OUTLINE:
A.) IUP Basic Information
B.) IUP Modification History
C.) Authorization Statement
D.) Description of Discharges
E.) Schematic and Monitoring Locations
F.) Effluent Limits&Monitoring Requirements
G.) Definitions and Limit Page(s)notes
A. IUP Basic Information:
Receiving Control Authority&WWTP name: POTW NPDES#:
Little Creek Water Reclamation Facility NC0025453
IUP Name: IUP Number:
Grifols Therapeutics, Inc. 0001-02
IUP Effective date: Pipe Numbers,list all regulated pipes:
September 17, 2015 001
IUP Expiration date: IUP 40 CFR#(if applicable),or N/A:
June 30,2017 439.20
B. IUP History. A Complete Permit History is required):
Effective Date Renewal or Description of changes over previous IUP.
Modification
9/25/01 Modification Added new CIU stds.for Acetone,n-Amyl Acetate,
Ethyl Acetate,Isopropyl Acetate,Methylene Chloride.
7/01/02 Renewal Dropped Cn limit. Added Pb limit. Reduced NH3-N
monitoring freq. Dropeed CIU sampling for Permittee.
Dropped PP sampling. Changed all Town monitoring to
1/6 months.
4/30/03 Mod. Increased flow to 450,000 gpd
3/01/04 Mod. Increased flow to 500,000 gpd
4/01/05 Mod. Name Changed to Talecris from Bayer
2

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
7/01/07 Renewal Decreased Pb monitoring frequency to 1/6 months.
Added limits for Zn. Decreased T Nitrogen limit to 20
mg/L.
7/23/10 Modification Updated process information,increased monitoring
frequency for T-nitrogen&ammonia Amyl Acetate,
Ethyl Acetate,Isopropyl Acetate,Methylene Chloride
2/11/11 Modification Increased flow to 550,000 gpd,Increased limits its for
BOD,TSS,COD,Zinc,Acetone,n-Amyl Acetate,Ethyl
Acetate,Isopropyl Acetate,Methylene Chloride,
modified limits for total nitrogen,decreased monitoring
frequency for total nitrogen,ammonia and phosphorus,
Acetone,n-Amyl Acetate,Ethyl Acetate,Isopropyl
Acetate,Methylene Chloride.Extended reporting date to
end of month.Dropped lead limit.
3/07/12 Mod. Name Change to Grifols from Talecris.
07/01/12 Renewal Permit renewal,Increase flow to 650,000 gpd.Removed
Zinc limit.
04/22/2013 Interim limits Interim limits established to allow treatability study.
Increased BOD,COD,TSS,t-Phos.and T-Nitrogen
limits for the period of 04/22/2013 to 06/21/2013.
06/05/2013 Interim limits Extended interim limits for BOD,TSS,T-Phos and T-
Nitrogen until 07/01/2013.
08/17/2015 Modification Permit modified to allow Grifols to discharge MBBR
effluent.
09/16/2015 Modification Permit modified to remove maximum daily limits for
BOD,COD,TSS
3

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
C.) Authorization Statement:
1.) The Permittee is hereby authorized to discharge wastewater in accordance
with the effluent limitations, monitoring requirements,and all other conditions
set forth in this Industrial User Pretreatment Permit (IUP) into the sewer
collection system and wastewater treatment facility of the Control Authority
and/or Municipality.
2.) The Permittee is hereby authorized to continue operation of and discharge
wastewater from the following treatment or pretreatment facilities. These
facilities must correspond to the treatment units listed on both the application
and inspection forms.
IU Treatment Units
List all Treatment Units: Descriptions:
Influent Bar Screen w/EQ Tank Removal of large solids.Able to bypass EQ tank if necessary.
bypass provision.
Equalization Tanks w/pH (I)One million equalization tank w/pH adjustment(carbon dioxide,
adjustment mag hydroxide).
MBBR 356000 gallon process train.
Chemical feed Ammonium hydroxide,Carbon Dioxide
3.) The Permittee is hereby authorized to, if required by the Control Authority
and/or Municipality and after receiving Authorization to Construct (A to C)
from the Control Authority and/or Municipality, construct and operate
additional pretreatment units as needed to meet final effluent limitations.
D.) Description of IUP Discharge(s):
1. Describe the discharge(s)from all regulated pipes.
Pipe# 001 , Description of Discharge:
Effluent from Mixed Bed Biological Reactor serving Grifols.
Grifols: process, wash down, domestic, cooling (non contact and HVAC), boiler,
and cooling tower blow down water.
4

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
E.) Schematic and Monitoring Locations:
The facility schematic and description of monitoring location(s) given below must
show enough detail such that someone unfamiliar with the facility could readily find
and identify the monitoring location(s) and connection to the sewer. Include and
identify all regulated pipes.
5

Grifols WWTP Process Flow Schematic
Clayton,NC
1
1 --- ---
Gat Removal
Litt Station atavistic Flow Meter
'-••--................c: r".........-------
1 New 1.0 MG Equalization Tank i Future 1.0 MG Equalization Tank I,
pH per---• (Saluting) 1
t
i
r-I rt ltetenafatlott -.-•
Tank Ma1 \\\\*.''\ _-,� i
1 �AOtlltiOn •�-. t
1 1
Mechanical Screen No.t 1 r___..Influent Wastewater 1 I I
•
I ; I Nwtralmit°n -------
• 1 Tank Na 2 Ea.Transfer Pumps
Ig' I .
1 QI'l
Mechanical .1-11)--' N.
Screen No.2 1
• •
I ; US Station MDR Ms. . Mee i Future Transfer Pamp
• GM SYasAinglDeemlMYg
1 /
Screen Washing/Compaction 1Q/ ^_
� f
1 1
Dramosew
i
Johnston Coin Effluent Pershell Fluke
1 . Effluent to the
t POTW
Composite sa{utpler
Flow&pH t
I
r-- Screen Ftite a • > Permit Compldnce Sampling Location
ff/ t r t
-------\\
I1 I (....--j
FrtereSeoeapther `-
Existing MBBR No.1 Existing MBBR No.2
'''‘..***"----. i-
FIMeMBMNw 3
CO,Addition
v t 1 1

IUP Part 1 Section F: Receiving POTW name=> LCWRF IU name=> Grifols
Receiving POTW NPDES#_> NC0025453 IUP#_> 0001-02
Effluent Limits and Monitoring Requirements Effective date for these Limits=> 09/16/2015 Pipe#_> 001
Expiration date for these Limits=> 06/30/2017 40 CFR#=> 439.20
The Permittee may discharge from this specific if not applicable put N/A
Pipe number according to these specific dates, THE LIMITS ON THIS PAGE ARE,(Check one below):
LIMITS for ENTIRE permit period => X
effluent limits, and monitoring requirements INTERIM Limits for period# 1 =>
INTERIM Limits for period#2 =>
FINAL Limits Page =>
Concentration Limits Frequencies
Required
Sample Laborator
Collection y
Weekly Method Detection
Daily Max Average Units By Industry By POTW (C or G) Level
1 Flow 1.1 .9 MOD Daily Meter -
2 BOD - 800 mg/L 3/week C 2
3 COD - 1500 mg/L 3/week C 5
4 TSS - 1200 mg/L 3/week C 2
5 Temperature 66 - C° 3/week G -
6 pH 6-9 - Std.Units 3/week G -
OTHER PARAMETERS;Please List Alphabetically
7 Ammonia—N *** - - mg/L 3/week C 0.3
8 Arsenic - - mg/L 1/3 months C 0.01
9 Barium - - mg/L 1/3 months C 0.01
10 Cadmium - - mg/L 1/3 months C 0.002
11 Chloride - - mg/L 1/3 months C -
12 Chromium - - mg/L 1/3 months C 0.005
13 Copper - - mg/L 1/3 months C 0.002
14 Cyanide - - mg/L 1/3 months G 0.01
15 Fluoride - - mg/L 1/3 months C -
16 Lead - - mg/L 1/3 months C 0.01
17 Mercury** - - mg/L 1/3 months C 0.0002
18 Molybdenum - - mg/L 1/3 months C 0.1
19 Nickel - - mg/L 1/6 months C 0.01
20 T Nitrogen*** 80 mg/L 3/week C -
6

21 T Phosphorous 12 mg/L 3/week C -
22 Selenium - - mg/L 1/3 months C 0.01
23 Silver - - mg/1 1/3 months C 0.005
24 Zinc - - mg/I 1/3months C 0.01
25 Acetone 8.2 - mg/1 - 1/6 months G .5
26 n-Amyl acetate 8.2 - mg/I - 1/6 months G .5
27 Ethyl acetate 8.2 - mg/1 - 1/6/months G .5
28 Isopropyl acetate 8.2 - mg/1 - 1/6 months G .5
29 Methylene .7 - mg/I - 1/6 months G .5
Chloride
**No mercury shall be discharged. Mercury concentrations Ies14s than the detection level will be considered compliant.
***Ammonia and T-Nitrogen sampling will be done on the same day.
(See next section,IUP,Part I,Section G.for Definitions and Limit Page(s)notes)
7

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
G.) Definitions and Limit Page(s) notes:
In addition to the definitions in the Town of Clayton Sewer Use Ordinance the
following definitions and requirements apply:
1. Composite Sample:
Unless defined differently below, a composite sample for the monitoring
requirements of this IUP, is defined as the automatic or manual collection
of one grab sample of constant volume, not less than 100 ml, collected
every hour during the entire discharge period on the sampling day.
Sampling day shall be a typical production, and discharge day.
2. Composite Sample, alternative definition:
A composite sample for the monitoring requirements of this IUP is the
same as described above unless specifically defined below as the
automatic or manual collection of constant volume and constant time grab
samples collected and composited according to the following criteria:
specific volume of each grab sample= 1000 Milliliters
specific time interval between samples= 6 Hours
total duration of sample collection period= 24 Hours
Total number of grab samples to be composited= 4 Samples
3. Daily Monitoring Frequency
Daily Monitoring Frequency as specified in this IUP shall mean each day
of discharge.
4. Grab Sample
Grab sample for the monitoring requirements of this IUP, is defined as a
single "dip and take" sample collected at a representative point in the
discharge stream.
5. Instantaneous measurement
An Instantaneous measurement for the monitoring requirements of this
IUP is defined as a single reading, observation,or measurement.
8

Industrial User Pretreatment Permit (IUP)
PART I
Specific Conditions
G.) Definitions and Limit Page(s) notes: (continued)
6. Monitoring and Reporting
All Monitoring shall be performed by a state certified laboratory by
standard methods. All data shall be reported to the Division as specified
in Part II. 2) of this permit, note that violations shall be reported within 24
hours, and that all sampling (even if done more frequently than required)
shall be summarized on forms approved by the Division and sent to the
following address by the last day of the following month:
James Warren, Water Reclamation Superintendent
Town of Clayton
Post Office Box 879
Clayton,North Carolina 27520
7. Notice to Permittees
Permittee is subject to the thirty(30)general conditions attached, found in
Part II of this permit.
9

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
Outline of PART II,
1. Representative Sampling 16. Federal and/or State Laws
2. Reporting 17. Penalties
3. Test Procedures 18. Need to Halt or Reduce
4. Additional Monitoring by 19. Transferability
Permittee
5. Duty to comply 20. Property Rights
6. Duty to Mitigate 21. Severability
7. Facilities Operation, Bypass 22. Modification, Revocation,
Termination
8. Removed substances 23. Reapplication
9. Upset Conditions 24. Dilution Prohibition
10. Right of Entry 25. Reports of Changed Conditions
11. Availability of Records 26. Construction of pretreatment
facilities
12. Duty to provide information 27. Reopener
13. Signatory Requirements 28. Categorical Reopener
14. Toxic Pollutants 29. General Prohibitive Standards
15. Civil and Criminal Liability 30. Reports of Potential Problems
1. Representative Sampling
Samples and measurements taken as required herein shall be representative of the volume and
nature of the monitored discharge. All samples shall be taken at the monitoring points specified in
this permit and, unless otherwise specified, before the effluent joins or is diluted by any other
wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to,and approval by,the permit issuing authority.
2. Reporting
p g
a.) Monitoring results obtained by the permittee shall be reported on forms specified by the
Control Authority and/or Municipality, postmarked no later than the twentieth day of the
month following the month in which the samples were taken. If no discharge occurs
during a reporting period (herein defined as each calendar month) in which a sampling
event was to have occurred, a form with the phrase "no discharge" shall be submitted.
Copies of these and all other reports required herein shall be submitted to the Control
Authority and/or Municipality and shall be sent to the following address:
James Warren
Water Reclamation Superintendent
Town of Clayton
PO Box 879
Clayton,NC 27520
b.) If the sampling performed by the permittee indicates a violation,the permittee shall notify the
Control Authority and/or Municipality within 24 hours of becoming aware of the violation.
The permittee shall also repeat the sampling and analysis and submit the results of the repeat
analysis to the Control Authority and/or Municipality within 30 days after becoming aware of
the violation.
10

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
3. Test Procedures
Test procedures for the analysis of pollutants shall be performed in accordance with the techniques
prescribed in 40 CFR part 136 and amendments thereto unless specified otherwise in the
monitoring conditions of this permit.
4. Additional Monitoring by Permittee
If the permittee monitors any pollutant at the location(s) designated herein more frequently than
required by this permit, using approved analytical methods as specified above, the results of such
monitoring shall be submitted to the Control Authority and/or Municipality. The Control
Authority and/or Municipality may require more frequent monitoring or the monitoring of other
pollutants not required in this permit by written notification.
5. Duty to Comply
The permittee must comply with all conditions of this permit. Any permit noncompliance
constitutes a violation of the Control Authority and/or Municipality Sewer Use Ordinance and is
grounds for possible enforcement action.
6. Duty to Mitigate - Prevention of Adverse Impact
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of
this permit which has a reasonable likelihood of adversely affecting human health, the POTW,the
waters receiving the POTW's discharge,or the environment.
7. Facilities Operation, Bypass
The permittee shall at all times maintain in good working order and operate as efficiently as
possible, all control facilities or systems installed or used by the permittee to achieve compliance
with the terms and conditions of this permit. Bypass of treatment facilities is prohibited except
when approved in advance by the Control Authority and/or Municipality. Bypass approval shall
be given only when such bypass is in compliance with 40 CFR 403.17.
8. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control
of wastewaters shall be disposed of in a manner such as to prevent any pollutants from such
materials from entering the sewer system. The permittee is responsible for assuring its compliance
with any requirements regarding the generation,treatment, storage, and/or disposal of"Hazardous
waste"as defined under the Federal Resource Conservation and Recovery Act.
9. Upset Conditions
An "upset" means an exceptional incident in which there is an unintentional and temporary
noncompliance with the effluent limitations of this permit because of factors beyond the reasonable
control of the permittee. An upset does not include noncompliance to the extent caused by
operational error, improperly designed or inadequate treatment facilities, lack of preventative
maintenance,or careless or improper operations.
An upset may constitute an affirmative defense for action brought for the noncompliance. The
permittee has the burden of proof to provide evidence and demonstrate that none of the factors
specifically listed above were responsible for the noncompliance.
11

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
10. Right of Entry
The permittee shall allow the staff of the State of North Carolina Department of Environment and
Natural Resources, Division of Water Quality, the Regional Administrator of the Environmental
Protection Agency, the Control Authority and/or Municipality, and/or their authorized
representatives,upon the presentation of credentials:
1. To enter upon the permittee's premises where a real or potential discharge is located or
in which records are required to be kept under the terms and conditions of this permit;
and
2. At reasonable times to have access to and copy records required to be kept under the
terms and conditions of this permit;to inspect any monitoring equipment or monitoring
method required in this permit;and to sample any discharge of pollutants.
11. Availability of Records and Reports
The permittee shall retain records of all monitoring information, including all calibration and
maintenance records as well as copies of reports and information used to complete the application
for this permit for at least three years. All records that pertain to matters that are subject to any
type of enforcement action shall be retained and preserved by the permittee until all enforcement
activities have concluded and all periods of limitation with respect to any and all appeals have
expired.
Except for data determined to be confidential under the Sewer Use Ordinance,all reports prepared
in accordance with terms of this permit shall be available for public inspection at the Control
Authority and/or Municipality. As required by the Sewer Use Ordinance,effluent data shall not be
considered confidential.
12. Duty to Provide Information
The permittee shall furnish to the Director of Public Works or his/her designees, within a
reasonable time, any information which the Director, his/her designee, or the Division of Water
Quality may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating this permit or to determine compliance with this permit. The permittee shall also
furnish,upon request,copies of records required to be kept by this permit.
13. Signatory Requirements
All reports or information submitted pursuant to the requirements of this permit must be signed and
certified by the Authorized Representative as defined under the Sewer Use Ordinance. If the
designation of an Authorized Representative is no longer accurate because a different individual or
position has responsibility for the overall operation of the facility, or overall responsibility for
environmental matters for the company, a new authorization satisfying the requirements of this
section must be submitted to the Water Reclamation Superintendent prior to or together with any
reports to be signed by an authorized representative.
14. Toxic Pollutants
If a toxic effluent standard or prohibition(including any schedule of compliance specified in such
effluent standard or prohibition) is established under Section 307(a) of the Federal Clean Water
Act for a toxic pollutant which is present in the discharge and such standard or prohibition is more
stringent than any limitation for such pollutant in this permit, this permit may be revised or
modified in accordance with the toxic effluent standard or prohibition and the permittee so
notified.
12

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
15. Civil and Criminal Liability
Nothing in this permit shall be construed to relieve the permittee from civil or criminal penalties
for noncompliance.
16. Federal and/or State Laws
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve
the permittee from anyresponsibilities, liabilities, orpenalties establishedpursuant to any
P
applicable Federal and/or State law or regulation.
17. Penalties
The Sewer Use Ordinance of the Control Authority and/or Municipality provides that any person
who violates a permit condition is subject to a civil penalty not to exceed$25,000 dollars per day
of such violation.
Under state law, (NCGS 143-215.6B), under certain circumstances it is a crime to violate terms,
conditions, or requirements of pretreatment permits. It is a crime to knowingly make any false
statement,representation,or certification in any record or other document submitted or required to
be maintained under this permit, including monitoring reports or reports of compliance or
noncompliance. These crimes are enforced at the prosecutorial discretion of the local District
Attorney.
18. Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary
to halt or reduce the permitted activity to maintain compliance with the conditions of the permit.
19. Transferability
This permit shall not be reassigned or transferred or sold to a new owner, new user, different
premises,or a new or changed operation without approval of the Town.
20. Property Rights
This permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights,nor any infringement of Federal,State or local laws or regulations.
21. Severability
The provisions of this permit are severable and, if any provision of this permit or the application of
any provision of this permit to any circumstance is held invalid, the application of such provision
to other circumstances and the remainder of this permit shall not be affected thereby.
22. Permit Modification, Revocation, Termination
This permit may be modified,revoked and reissued or terminated with cause in accordance to the
requirements of the Control Authority and/or Municipality Sewer Use Ordinance and North
Carolina General Statute or implementing regulations.
23. Re-Application for Permit Renewal
The permittee is responsible for filing an application for reissuance of this permit at least 180 days
prior to its expiration date.
13

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
24. Dilution Prohibition
The permittee shall not increase the use of potable or process water or in any other way attempt to
dilute the discharge as a partial or complete substitute for adequate treatment to achieve
compliance with the limitations contained in this permit.
25. Reports of Changed Conditions
The permittee shall give notice to the Control Authority and/or Municipality of any planned
significant changes to the permittee's operations or system which might alter the nature,quality,or
volume of its wastewater at least 180 days before the change. The permittee shall not begin the
changes until receiving written approval from the Control Authority and/or Municipality. Also see
Part II,30 below for additional reporting requirements for spill/slug issues.
26. Construction
No construction of pretreatment facilities or additions thereto shall be begun until Final Plans and
Specifications have been submitted to the Control Authority and/or Municipality and written
approval and an Authorization to Construct(A to C)have been issued.
27. Reopener
The permit shall be modified or,alternatively,revoked and reissued to comply with any applicable
effluent standard or limitation for the control of any pollutant shown to contribute to toxicity of the
WWTP effluent or any pollutant that is otherwise limited by the POTW discharge permit. The
permit as modified or reissued under this paragraph may also contain any other requirements of
State or Federal pretreatment regulations then applicable.
28. Categorical Reopener
This permit shall be modified, or alternatively, revoked and reissued, to comply with any
applicable effluent standard or limitation issued or approved under Sections 302(b)(2)(C)and(D),
304(b)(2),and 307(a)(2)of the Clean Water Act, if the effluent standard or limitation so issued or
approved:
1.) contains different conditions or is otherwise more stringent than any effluent
limitation in this permit;or
2.) controls any pollutant not limited in this permit.
The permit as modified or reissued under this paragraph shall also contain any other requirements
of the Act then applicable.
29. General Prohibitive Standards
The permittee shall comply with the general prohibitive discharge standards in 40 CFR 403.5 (a)
and(b)of the Federal pretreatment regulations.
14

Industrial User Pretreatment Permit (IUP)
PART II
General Conditions
30. Potential Problems
The permittee shall provide protection from accidental and slug discharges of prohibited materials
and other substances regulated by this permit. The permittee shall also notify the POTW
immediately of any changes at its facility affecting the potential for spills and other accidental
discharge, discharge of a non-routine,episodic nature,a non-customary batch discharge, or a slug
load as defined in the Sewer Use Ordinance.
Additionally, the permittee shall notify by telephone the Control Authority and/or Municipality
immediately of all discharges that could cause problems to the POTW including any slug loadings
as defined in the Sewer Use Ordinance. If the permittee experiences such a discharge,they shall
inform the Control Authority and/or Municipality immediately upon the first awareness of the
commencement of the discharge. Notification shall include location of the discharge, type of
waste,concentration and volume if known and corrective actions taken by the permittee. A written
follow-up report thereof shall be filed by the permittee within five (5) days, unless waived by the
Control Authority and/or Municipality.
15

Industrial User Pretreatment Permit (IUP)
PART III
Special Conditions
1. Slug/Spill Control Measures
In addition to the requirements in Part II, 30, the Permittee shall complete
installation and/or commence implementation, operation, and/or maintenance of
the following specific protection Measures, Activities, Plans. Etc. (Items without
specific completion dates, or marked as "Continuous." must be performed for the
entire duration of the permit):
Required
Completion/
Implementation
Description of Measure,Activity, Plan, etc. Date
Implement approved Slug/Spill Control Plan. The plan shall Continuous
include but is not limited to:
• description of discharge practices, including non-
routine batch discharges
• description of stored chemicals
• procedures for immediately notifying the POTW of
slug discharges that would cause a violation of 40
CFR 403.5(b), with procedures for follow up
notification within 5 days;
• and if necessary, procedures to prevent adverse
impact from accidental spills, permit limit
excursions, including inspection and maintenance of
storage areas, handling and transfer of materials,
loading and unloading operations, control of plant
site run-off, worker training, building of containment
structures or equipment, measures for containing
toxic organic pollutants (including solvents), and/or
measures and equipment for emergency response.
The permittee shall provide updates to the Control Authority as required by Part
II, 30, of this IUP. Modifications to the measures shall be approved by the
Control Authority prior to installation/implementation. If a measure fails, the
Control Authority shall be notified within 24 hours.
2. Flow Measurement Requirements
(For SIUs with discharge flow meters)
The Control Authority shall maintain appropriate discharge flow measurement
devices and methods consistent with approved scientific practices to ensure the
accuracy and reliability of measurements of the volume of monitored discharges.
Devices installed shall be a continuous recording flow meter capable of measuring
16

Industrial User Pretreatment Permit (I P( U )
PART III
Special Conditions
flows with a maximum deviation of less than 10% from true discharge rates
throughout the range of expected discharge volumes. The devices shall be
installed, calibrated, and maintained to ensure accuracy. The meter shall be
calibrated every six (6) months. Modifications to the flow metering equipment
shall be approved by the Control Authority prior to installation. If a required flow
measurement device fails,the Control Authority shall be notified within 24 hours.
3. Certified Laboratory Analysis
Pollutant analysis to be submitted to the Control Authority shall be performed by
a Laboratory that is certified by the State of North Carolina (or others as approved
by the Control Authority) in the analysis of the pollutant in wastewater. Organic
analysis for categorical limitations shall meet quality control standards set forth in
EPA method 1666.
10. Combined Wastestream Formula Flow Condition
(for Categorical Industrial Users only)
Regulated Categorical Process Flow:
The permittee shall have available flow monitoring equipment at such locations as
necessary to measure the total daily volume of wastewater discharged that is
covered by 40 CFR 439.20. This flow monitoring equipment shall also be
capable of measuring flows with a maximum deviation of less than 10% from true
discharge rates throughout the range of expected discharge volumes, however it is
not required that it be continuous recording. The frequency shall be daily and data
shall be collected and reported as required in Part II, 1-4 of this IUP.
Modifications to the flow metering equipment shall be approved by the Control
Authority prior to installation.
17

IUP Synopsis
A. IUP Basic Information
Receiving POTW name: POTW NPDES#:
Little Creek Water Reclamation Facility NC0025453
IUP name: IUP Number:
Grifols Therapeutics,Inc. 0001-02
IUP Effective date: Pipe Numbers,list all regulated pipes:
08/17/2015 001
IUP expiration date: IUP 40 CFR#,if applicable:
June 30,2017 439.20
B. IUP Survey&Application form
Attach a completed copy of the Industrial User Wastewater Survey&
Application Form(see appendix 6-A)
C. IU Inspection form
Attach a copy of an Industrial User Inspection Form (see chapter 7) completed
by the Control Authority within the past 12 months.
D. RATIONALE FOR LIMITATIONS:
As listed on the IUP Limits Page(s), PART I, Section F of the IUP.
RATIONALE#1:
Review of IU Monitoring Data, with no Over Allocation situation:
The following pollutants were assigned numerical limits in this IUP based
on a review of monitoring data for the permittee to determine what ranges of
concentrations are currently being discharged. To account for sample
variability a factor was applied to the monitoring data to determine the
permit limit. Permit limits assigned by the Local IUP Control Authority can
not result in an Over Allocation situation for any pollutants.
BOD
COD
TSS
Total Nitrogen
Total Phosphorus
1

IUP Synopsis
RATIONALE#2a:
Categorical Industrial Limits, with no Over Allocation situation:
Check here if Combined Wastestream Formula (CWF) or other categorical
limits calculations were used. If used, Please attach calculations: (see CWF
Spreadsheet, Appendix 6-F)
Were used(attach calculations)
Were not used I x
The following pollutants were assigned numerical limits in this IUP based
on the categorical regulations. These limits do not result in over allocations.
Acetone
n-Amyl Acetate
Ethyl Acetate
Isopropyl Acetate
Methylene Chloride
RATIONALE#3a:
Over Allocation Prevention,with IU pollutant reduction:
The following pollutants were assigned numerical limits in this IUP based
on allocating the Maximum Allowable Industrial Loading (MAIL)
determined with the Headworks Analysis (HWA) among all Industrial
Users. The total loading of each pollutant from all permitted discharges
does not exceed the MAIL. These limits do not result on over allocations.
RATIONALE#3b:
Interim Limits for IU pollutant reduction:
The following p assigned were assi ned interim numerical limits in this IUP
to allow time for the industry to come compliance with final limits that will
not in over allocations.
N/A
2

IUP Synopsis
RATIONALE#4:
4.) Other Rationale for Limitations:
The following rationale was used for developing IUP Limits.
Parameter Rationale
BOD Study performed by Hazen &
COD Sawyer.
TSS
T-Nitrogen
T-Phosphorus
RATIONALE#5a:
Non-Categorical Parameters where No Limit needed or assigned in an IUP:
The following pollutants were not assigned numerical limits in this IUP
because the loadings for these pollutants from this IU were less than 5% of
the MAHL, or extra reserve capacity was available. The loading of these
pollutants from this IU is considered insignificant at this time.
Pollutant Avg SIU mg/1 Avg SIU lbs/day 5%MAHL, lbs/day
Arsenic Monitor Only
Silver .041 .222 .4258
Cadmium .00025 .014 .2879
Chromium <.005 <.027 .671
Copper .07025 .393 .8175
Cyanide <.005 <.027 .1703
Lead .008 .043 .8515
Mercury <.0002 <.0001 .0014
Molybdenum <.010 <.0054 .0091
Nickel <.010 <.0054 .4258
Selenium Monitor Only
Ammonia-N Monitor Only
3