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HomeMy WebLinkAboutWQ0001863_Regional Office Historical File Pre 2018 (14)Schutte, Maria
From: Schutte, Maria
Sent: Thursday, April 05, 2018 10:40 AM
To: 'Adam Brigman'
Cc: 'david Johnson@mtholly.us'; 'doug.shoutd@mtholly.us'; Gregory, Sonia
Subject: RE: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information
Request
Adam,
Thank you for the additional information in this and the March 29th, 2018 email. I have no further questions.
Sincerely,
Maria Schutte
From: Adam Brigman [mailto:abrigman@SYNAGRO.com]
Sent: Wednesday, April 04, 2018 5:25 PM
To: Schutte, Maria <maria.schutte@ncdenr.gov>; david.johnson@mtholly.us
Cc: doug.shoutd@mtholly.us; Gregory, Sonia <Sonia.Gregory@ncdenr.gov>; Pitner, Andrew <andrew.pitner@ncdenr.gov>;
Robert Roth <rroth@SYNAGRO.com>
Subject: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request
� i;$ Y= r7 {G �rtrl rfM1 ✓ ri';, . :;r..,l<<;: .: a i •.i r # c iie 2 5 21'li.. J C� p4. ,tol _ nA _ n , ©�e 11rN EG t n,:: t. f` 1 I {[ t f E] A
Par labs just sent me the additional page to the 30-Day Bench Test report, it is attached. If you have any more questions just let
me know.
From: Schutte, Maria[mailto:maria.schutteCCncdenr.gov]
Sent: Tuesday, March 27, 2018 6:52 PM
To: david.johnson@mtholly.us
Cc: doug.shoutd(a)mtholly.us; Gregory, Sonia; Pitner, Andrew; Adam Brigman
Subject: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request
Mr. Johnson,
This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A
report copy was received in the Mooresville office on March 51h, 2018. Upon review, the following additional information is
requested:
• Please send calculations for, or request an amended Soils Report from your contract lab to include, the Exchangeable
Sodium Percentage (ESP) parameter in accordance with permit condition IV.S. of your permit (copied below for your
convenience). It is the permittees responsibility to ensure all parameters are sampled, requested on the COC and
reported as required, including the appropriate units of measure, in -line with NCDA recommendations. This issue was
brought to your attention last year (see attached email) and needs to be corrected now and for future reports.
• The second sheet of the Par Lab report is missing for the 1-17-17, 30-day Bench analysis. Please submit the missing
page, showing the "extended aeration" testing.
Please email the requested information to me or contact me with any questions.
Sincerely,
Maria
5. ii annuil repre5eritative oils. anal}his (i.c:, 81an6rd Soil Fertility A-natysis} s lill b'd 66nducted'on.
each land application site=_listed-in Alta-Biller-t 13 nil' kylilich a r�.sidgals limit applica,tior c4citt`.will.
occur in the ycear T6 is. nill.yrsis shall be in, accordance with ti e-*!G. tidattce on SoiiI
S.anlpfjng'' loc4tod sri the-Sait�Pling-litstruetions sr�etion-ef tile. NC Delrarwic-iit of Aaricuktivic
Consumer Services' �.vebs.ire (lttt� r'��tw�t+.ttta�,r:�ovfa�ran�Tttia'pii.bs.ht1�1}. The Perniiitee
ataintain their ctsul s and =r descriptipq of it-c saniplidg methodologie-k used to defertitntc,sotl fc tility;
fora peridd at': lest, tlian frvc� �srs,:aitd: siral3 he tttade. -t�ailohle to file DFvrs on.t.ppi regtt�t., Af a-.
ininistitini, the: Standard Sk')R Fertility a-nalysis shall include the following psIralnctc rs: .
,acidity.
� E.r•.chattgeable Saidiutt .Vercent> t;e
; ,Pltn�liarus I
13asc Saluratio.n (bycal;c;illminl)
Magnesium
� Potss;iutat
r C ICditil]
lv ail tli 5
Siai3ittnx,
Cation Exdl1 nge Capacity
Percent Humid ,Witer
11t1C-
pH
Maria Schutte
Environmental Specialist
Water Quality Regional Operations Section
Division of Water Resources
North Carolina Department of Environmental Quality
704 663 1699 office
704 235 2184 direct
Maria. schutte(a-)ncdenr.gov
610 East Center Avenue
Suite 301
Mooresville, NC 28115
-:�>-'Nothing Compares. -
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
0
Schutte, Maria
From: Schutte, Maria
Sent: Thursday, April 05, 2018 10:40 AM
To: 'Adam Brigman'
Cc: 'david Johnson@mtholly.us'; 'doug.shoutd@mtholly.us'; Gregory, Sonia
Subject: RE: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information
Request
Adam,
Thank you for the additional information in this and the March 29th, 2018 email. I have no further questions.
Sincerely,
Maria Schutte
From: Adam Brigman [mailto:abrigman@SYNAGRO.com]
Sent: Wednesday, April 04, 2018 5:25 PM
To: Schutte, Maria <maria.schutte@ncdenr.gov>; david.johnson@mtholly.us
Cc: doug.shoutd@mtholly.us; Gregory, Sonia <Sonia.Gregory@ncdenr.gov>; Pitner, Andrew <andrew.pitner@ncdenr.gov>;
Robert Roth <rroth@SYNAGRO.com>
Subject: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request
CAUTION:
Par labs just sent me the additional page to the 30-Day Bench Test report, it is attached. If you have any more questions just let
me know.
From: Schutte, Maria fmailto:maria.schutte@ncdenr.gov]
Sent: Tuesday, March 27, 2018 6:52 PM
To: david.johnson@mtholly.us
Cc: doug.shoutd@mtholly.us; Gregory, Sonia; Pitner, Andrew; Adam Brigman
Subject: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request
Mr. Johnson,
This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A
report copy was received in the Mooresville office on March 51h, 2018. Upon -review, the following additional information is
requested:
• Please send calculations for, or request an amended Soils Report from your contract lab to include, the Exchangeable
Sodium Percentage (ESP) parameter in accordance with permit condition IV.S. of your permit (copied below for your
convenience). It is the permittees responsibility to ensure all parameters are sampled, requested on the COC and
reported as required, including the appropriate units of measure, in -line with NCDA recommendations. This issue was
brought to your attention last year (see attached email) and needs to be corrected now and for future reports.
• The second sheet of the Par Lab report is missing for the 1-17-17, 30-day Bench analysis. Please submit the missing
page, showing the "extended aeration" testing.
Please email the requested information to me or contact me with any questions.
Sincerely,
Maria
1
5. An annual representative soils analysis (i.e.. Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment S on which a residuals land application evert will
occur in the respective calcndar year. This analysis shall be in accordance with the "Guidance on Soil
Sampling" located in the Sampling Instructions section of the NC Department of Agriculture 8c
Consumer Services' website(littp:ll«,rvw.nc<7gr.,govlagronoml;pubs.htm). 'Ric Pertninee shall
maintain these results and a description of the sampling methodologies used to determine soil fertility
fora period of no.less than rive years, and shall be made available to the Division upon request. At a
minimum, the Standard Soil Fertility Analysis shall include [lie following parameters,
Acidity
Exchangeable Sodium
Phosphorus
Base Saturation (by calculation)
Magnesium
Potassium
Calcium
Manganese
Sodium
Cation Exchange Capacity
Percent Humic Matter
Zinc
Copper
pH !
-
Maria Schutte
Environmental Specialist
Water Quality Regional Operations Section
Division of Water Resources
North Carolina Department of Environmental Quality
704 663 1699 office
704 235 2184 direct
Maria. schutte(a-ncdenr.gov
610 East Center Avenue
Suite 301
Mooresville, NC 28115
-::�:"othing Compares -,-,-
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Schutte, Maria
From: Adam Brigman <abrigman@SYNAGRO.com>
Sent: Thursday, March 29, 2018 7:29 AM
To: Schutte, Maria
Cc: doug.shoutd@mtholly.us; Gregory, Sonia; Pitner, Andrew; Robert Roth;
david.johnson@mtholly.us
Subject: [External] RE: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information
Request
Attachments: ESP Soil samples.pdf
CAUTION:
I'm still waiting on the lab to get me the missing page of the 30-Day bench, but I wanted to go ahead and send you this
document that shows the ESP values for the soil reports done through waypoint. Waypoint does not include ESP on the report
since it is considered the same as the Percent Sodium found in the Base Saturation. I will get the missing 30-Day Bench test page
to you as soon as the lab gets it to me.
From: Schutte, Maria [mailto:maria.schutte@ncdenr.gov]
Sent: Tuesday, March 27, 2018 6:52 PM
To: david.johnson@mtholly.us
Cc: doug.shoutd@mtholly.us; Gregory, Sonia; Pitner, Andrew; Adam Brigman
Subject: WQ0001863 City of Mt. Holly 2017 Annual Report - Additional Information Request
Mr. Johnson,
This email will serve as the Acknowledgement of Receipt of the 2017 Annual Report for the referenced residuals permit. A
report copy was received in the Mooresville office on March 5th, 2018. Upon review, the following additional information is
requested:
• Please send calculations for, or request an amended Soils Report from your contract lab to include, the Exchangeable
Sodium Percentage (ESP) parameter in accordance with permit condition IV.5. of your permit (copied below for your
convenience). It is the permittees responsibility to ensure all parameters are sampled, requested on the COC and
reported as required, including the appropriate units of measure, in -line with NCDA recommendations. This issue was
brought to your attention last year (see attached email) and needs to be corrected now and for future reports
• The second sheet of the Par Lab report is missing for the 1-17-17, 30-day Bench analysis. Please submit the missing
page, showing the "extended aeration" testing.
Please email the requested information to me or contact me with any questions.
Sincerely,
Maria
,5, An annual representative soils ;analysis (i.e.. Standard Soil Fertility Analysis) shall be conducted on
each land application site: listed in Attachment R on which to residuals land application eveltt will
oecur in the respective calendar year. This analysts shall be in aceordancc wilh the "Guidance on Soil
Sampling" located in the Sampling Instructions seetion of the NC nepnrtnaeni of Agriculture
Consumer Services' website(lit tp:tlww%%,.nc:agr.goviagronomi1pubs.hiIn). The Permiuce shall
maintain these results and a du%cription of the: sampling nwihodologics used to detennine sail fertility
for a period of no leis than five year,, and shall be made (avail-nhic to the Di%�sion upon request, At a
mininiurn, the Swndard Sail fertility ,Analysis shrill include elie following pan, meters,
Acidity
E;elttangeahic sodituni.I'et-centoge
Phosphorus
Hasc Sniuratiola (by calculation)
Magnesium
� Potassivait
Calcium
Manganese
Sodiuni
Cation Exchange Capacity �
Percent l-littntiC Mahe;,
� Fine
Copper
PH
�a
Maria Schutte
Environmental Specialist
Water Quality Regional Operations Section
Division of Water Resources
North Carolina Department of Environmental Quality
704 663 1699 office
704 235 2184 direct
Maria. schutteCaD-ncdenr.gov
610 East Center Avenue
Suite 301
Mooresville, NC 28115
----"Nothing Compares.,-,-,_.
Ik
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
PA
PROMPT•ACCU RATE- RELIABLE
LABORATORIES, INC
WWW.PARLABS.COM
Crucible
Tare Wt (g)
Sample(g)
Dried Wt(g)
Burned Wt(g)
TS%
VS%
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
■ CITY OF MT HOLLY 1ST EVENT
126327
■ • 01/17/17
■ ■ • 02/14/17
As Received Day 0 Day 7 Day 14 Day 21 Day 28
01/17/18 01/17/17 01/24/17 01131 /17 02/07/17 02/14/17
X10
X10
X2
X10
X2
X10
22.7037
22.7037
25.0632
22.7043
25.0655
22.7064
37.0990
37.0990
36.4780
36.4427
39.0083
36.5308
22.9513
22.9513
25.2550
22.9420
25.3039
22.9469
22.7636
25.1111
22.7646
25.1267
22.7683
1.72%
1.72%
1.68%
1.73%
1.71 %
1.74%
75.81 %
75.03%
74.63%
74.33%
74.26%
0.005059436
x
0.001614599
TS
0.2476
VS
0.1877
Volatile Fraction In 0.44074
t
P.O. Box 411483 ■ Charlotte, NC 28241-1483
Phone: (704) 588.83330 Fax: (704) 588-S335
0.004889025
x
0.001694461
TS
0.2405
VS
0.1786
Volatile Fraction Out: 0.42687
RAF;Z
RROMRT•ACCU RATE- RGLIA9 LE
I.AB®RATORIES, II C
WWW. PARLASS. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
CITY OF MT HOLLY 1ST EVENT
126327
01/17/17
02/14/17
Start: End:
TS g
0.2476
0.2405
TS%
1.72%
1.74%
VS (g)
0.1877
0.1786
VS%
75.81 %
74.26%
yIN
0.005059
yOUT
0.00488903
FSVR (Mass Balance)
3.37%
FSVR (Van Kleeck)
7.92%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241.1483
Phone: (704) 588.8333 a Fax: (704) 588-8335
1WA�,
Page 1 of 1
Report Number: 17-340-0506
Account Number: 46441
Send To: Synagro Central LLC/ Charlotte
Adain Brigman
12701 Lancaster Hwy
Pineville NC 28134
c
0
Waypognt.
ANALYTICAL
'Every acre... Every year.
SOIL ANALYSIS REPORT
nata Rarnivnri. igiris/?nm7 Data OfAnalvsis' 12/07/2017 Date Of Renort: 12107/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax 804-271-6446
www.waypointanalytical.com
Grower: Tony Jones
City of Mt Holly
Analytical Mothod(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WIV
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
pprn Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meg1100g
meg1100g
46-02
12318
5,5
150
4 VL
48 VL
177 H
853 M
28 VL
6.0
6.82
1.1
7.1
H
NC = 3
NC = 25
MIN
46-04
12319
5.8
150
2 VL
40 VL
165 H
787 M
45 L
6.1
6.84
0.9
6.5
H
M1N
NC = 2
NC = 20
46-05
12320
5.7
150
2 VL
38 VL
172 H
823 M
42 L
6.0
6.82
1.1
6.9
H
NC = 2
NC = 19
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
soluble salts
Sample ID
E
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
%
%
%
%
m Rate
ppm
m Rate
ppm
Pp m Rate
Pp m Rate
m Rate
ppm
pp m Rate
PP m Rate
mslcm Rate
46-02
1.7
20.8
60.1
1.7
15.5
34 H
0.6 VL
46 H
50 H
1.8 H
0.3 VL
e
NC=71
NC=15.0
NC=288
NC=90.Q
46.04
1.6
21.2
60.5
3.0
13.8
69 VH
0.7 VL
41 H
47 H
1.3 M
0.3 VL
2
NC=144
NC=17:5
NC=256
NC=65.0
J O
46-05
1.4
20.8
59.6
2.6
1 15.9
76 VH
0.6 VL
36 H
58 VH
1.1 M
0.3 VL
,
NC = 158
NC = 15.0
NC = 226
NC = 55,0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to somple(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (nlili-mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: pprn x 2 = Ibs1A, Soluble Analysis prepared by: waypohN Analytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by ?of;,, lnc �1
Pauric McGroary
r
Page 1 of 1
Report Number: 17-073-0791
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
3
Waypoint
ANALYTICAL
"Every acre...Every year. ",M
Date Received: 03/14/2017 Date Of Analvsis: 03/16/2017
Farm ID: NC-MG-37
SOIL ANALYSIS REPORT
Date Of Resort: 03/16/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Grower: Dale Connell
Mt Holly 50-1701
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On ignition Water pH
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
%
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
01
03535
5.4
150
29 L
74 L
185 VH
602 M
4 VL
6.2
0.7
5.5
H
NC = 24
NC = 36
MIN
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Sample ID
S
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
%
%
%
a/a
RR m Rate
Rp m Rate
RR m Rate
m Rate
ppm
m Rate
ppm
pp m Rate
ppm Rate
ms/cm Rate
.01
3A
28.0
54.7
0.3
12.7
7 VL
5.9 H
54 VH
93 VH
3.1 VH
0.3 VL
NC = 15
NC = 147.5
NC = 338
NC = 155.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), IbsJA This report applies to sample(&) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (mild -mhos per centimeter), meg1100g maximum of thirty days after testing. by ��`c G H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc.
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 1 of 1
Report Number: 17-073-0790
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Date Received: 03/14/2017 Date Of Analvsis: 03/15/2017
Farm ID: NC-LT-46
SOIL ANALYSIS REPORT
Date Of Report: 03/15/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Grower: Tony Jones
Mt Holly 50-1701
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
WfV
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E,C
Sample ID
Field ID
Lab
Number
%
Soil
IbslA
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
PH
Index
meg11009
megl.100g
01
03532
6.5
150
91 H
62 L
127 M
1009 M
8 VL
6.1
6.83
1.0
7.3
I MIN
H
NC=76
NC=32
03
03533
7.1
150
36 M
55 VL
148 H
833 M
13 VL
6.1
6.84
0.9
6.5
VH
MIN
NC = 30
NC = 28
08
03534
6.1
150
86 H
51 VL
167 H
750 M
10 VL
6.3 ,
0.6 -
5.9
H
MIN
NO = 72
NO = 26
Percent
Base
Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron.
Soluble Salts
Sample ID
ES
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
%
%
%
°lo
pp m Rate
pp m Rate
pp m Rate
pp m Rate
pp m Rate
pp m Rate
pp m Rate
ms/cm Rate
01
2.2
14.6
69.1
0.5
13.7
4 VL
8.4 VH
20 M
127 VH
6.6 VH
0.5 L
O 5
NC=8
NC=210.0
NC=125
NC=330.0
'
03
2.2
19.0
64.1
0.9
13.8
15 L
4.7 H
41 H
62 VH
3.5 VH
0.4 L
1
NC=256
NC=175.0
t/• f
NC=31
NC=117.5
08
2.2
23.6
63.6
0.7
10.2
13 L
9.5 VH
23 H
76 VH
4.9 VH
0.5 L
'
NC = 27
NC = 237.5
NO = 144
NO = 245.0
Values on this report represent the plant available nutrients In the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This repod applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), mslcm (milli -mhos per centimeter), megf100g maximum of thirty days after testing. by
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs1A, Soluble Analysis prepared by: Waypoint Analytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts mslcm x 640 = ppm.
Pauric McGroary
Charlotte Water 2016
Soil ESP
Field
Na (PPM)
Na (meq/100g)
CEC (meq/100g)
ESP
LT-46-02
28
0.122
7.1.
1.7
LT-46-04
45
0.196
6.5
3.0
LT-46-05
42
0.183
6.9
2.7
LT-46-01
8
0.035
7.3
0.5
LT-46-03
13
0.056
6.5
0.9
LT-46-08
10
0.044
5.9.
0.7
MG-37-01
4
0.017
5.5
0.3
#DIV/0!
#DIV/0!
#DIV/0!
#DIV/0!
#DIV/0!
#DIVIO!
#DIV/0!
#DIV/0!
#DIV/0!
Equations: Na (meq/100g)= (Na PPM x 2)/460
ESP=((Na meq/100g)/CEC) x 100
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RECEIVEDINCCEP1RfD F°
1VIAR. � 201�'
W()ROS
MOORESV ILLS REGIONAL OFFICE
City of Mount Holly, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001863
2017 ANNUAL REPORT
City of Mount Holly, NC
Residuals Land Application Program
2017 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis,
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00001863 County Gaston Year 2017
Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NCO021156 & 01-36-020
Land Application Operator Synagro Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summarv:
Total number of application fields in the permit: 21
Total number of fields utilized for land application during the year: 11
Total amount of dry tons applied during the year for all application sites: 252.66
Total number of acres utilized for land application during the year: 157.1
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit. .
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under.penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting fals nformation, including the psibility of fines and imprisonment for
knowing violations." a 111
Dannv Jackson City Manager A . �-�7-/d
Per iitte Name and Title (type or print) Si atu of PU` ttee Date
AbAre of P eparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2017 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
MOUNT HOLLY, NC
MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
February 2017
353,400.00
G
24.91
D
March 2017
297,600.00
G
20.97
D
June 2017
638,600.00
G
60.97
D
July 2017
682,000.00
G
52.33
D
October 2017
675,800.00
G
56.08
D
December 2017
700,600.00
G
37.40
D
YEARLY TOTAL
3,348,000.00
G
252.66
D
DRY METRIC
TONS
22.59
19.01
55.29
47.46
50.87
33.90
229.12
2/1 /2018
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863
Facility Name: MOUNT HOLLY, NC
NPDES# : NCO021166
or WQ# (residual only)
WWTP Name: MOUNT HOLLY WWTP
Residuals Analysis Data
a
Product Type AEDLIQ
AEDLIQ
AEDLIQ
Date Sampled (grab) or 01/17/17
05/08/17
06/15/17
Date Composited
Percent Solids 1.69
2.29
1.84
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TK17
Ammonia -Nitrogen
Nitrate and Nitrite
Laboratory
Waypoint Analytical Virginia Inc.
AEDLIQ AEDLIQ
09/06/17 10/31/17
1.99 1.28
<3
4.5
<3
<3
3.39
<2
<2
<2
<2
<2
1.48
0.481
0.433
0.54
<0.4
289
236
207
175
157
453
418
497
483
402
35.1
26.4
22.2
18.5
16.1
<5
5.02
<5
<5
<5
21.4
15
14
15.2
17.1
<5
5.2
<5
<5
5.23
730
672
773
758
692
13800
12900
13100
11100
10800
68800
7b900
70300
65000
56600
26500
16500
15100
13500
12400
259
114
859
328
2760
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pen_ajties�for submittt-qfalse information, including the possibility of fines and imprisonment for knowing violations."
Date
DENR FORM RSSF (6/2003) Printed: Tuesday - February 13, 201B at 08:53:56 for: 1701 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863 Laboratory
Facility Name: MOUNT HOLLY, NC Waypoint Analytical Virginia Inc.
NPDES# : NCO021156
or WQ# (residual only)
WWTP Name: MOUNT HOLLY WWTP
Residuals Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Ar! Q
Date Sampled (grab) or 01/17/17
05/08/17
06/15/17
09/06/17
10/31/17
Date Composited
Percent Solids
1.69
2.29
1.84
1.99
1.28
PARAMETERS (mglkg dry weight)
Aluminum
21000
11000
8810
7490
8320
Calcium
9920
9690
12100
10500
10300
Magnesium
2430
2100
2440
2420
2280
pH
7.28
7.49
7.68
7.69
7.62
Potassium
2680
2700
2490
2170
2260
Sodium
7340
6030
6300
6570
6600
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
� Date 6 IV
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (712002) Printed: Tuesday- February 13, 2018 at 08:54:19 for: 1701 01
Page: 1 of 2
Report Number: 17-019-0213
Account Number: 00015
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 61783
Sample Id : Mt Hollyl st event
Waypoint(D
ANALYTICAL
Project : Mt Holly
NC Cert#257
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 1/17/2017 10:20:00
Date Received: 01/19/2017 00:00
Date Reported: 01/26/2017
Total Solids *
1.69
16900
100.0
JM
01/19/2017 17:00
SM-2540G
Moisture `
98.30
100.0
JM
01/19/2017 17:00
SM-2540G
Total Kjeldahl Nitrogen
6.88
68800
10.0
JM
01/20/2017 08:55
SM-4500-NH3C-TKN
Total Phosphorus
1.38
13800
100
JTR
01/24/2017 03:44
6010C
Total Potassium
0.27
2680
1000
JTR
01/24/2017 03:48
6010C
Total Sulfur
1.28
12800
100
JTR
01/24/2017 03:44
6010C
Total Calcium
0.99
9920
100
JTR
01/24/2017 03:44
6010C
Total Magnesium
0.24
2430
100
JTR
01/24/2017 03:44
6010C
Total Sodium
0.73
7340
100
JTR
01/24/2017 03:44
6010C
Total Iron
14400
100
JTR
01/24/2017 03:44
6010C
Total Aluminum
21000
100
JTR
01/24/2017 03:44
6010C
Total Manganese
444
5.00
JTR
01/24/2017 03:44
6010C
Total Copper
453
5.00
JTR
01/24/2017 03:44
6010C
Total Zinc
730
5.00
JTR
01/24/2017 03:44
6010C
Ammonia Nitrogen
2.65
26500
10.0
JM
01/20/2017 08:55
SM-4500-NH3C
Organic N
4.23
42300
10.0
01/20/2017 08:55
CALCULATION
Nitrate+Nitrite-N
259
2.28
SJB
01/23/201713:11
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor
Page: 2 of 2
Report Number: 17-019-0213
Account Number: 00015
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 61783
Sample Id : Mt Holly1st event
D
Waypoin(t.�
ANALYTICAL
Project : Mt Holly
NC Cert#257
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 1/17/2017 10:20:00
Date Received: 01/19/2017 00:00
Date Reported: 01/26/2017
Total Cadmium
<2.00
2.00
JTR
01/24/2017 03:44
6010C
Total Chromium
289
5.00
JTR
01/24/2017 03:44
6010C
Total Nickel
21.4
5.00
JTR
01/24/2017 03:44
6010C
Total Lead
35.1
5.00
JTR
01/24/2017 03:44
6010C
Total Arsenic
<3.00
3.00
JTR
01/24/2017 03:44
6010C
Total Mercury
1.48
0.400
JM
01/25/2017 15:50
SW-7471B
Total Selenium
<5.00
5.00
JTR
01/24/2017 03:44
6010C
pH (Standard Units) *
7.28
1.00
JM
01/20/2017 08:55
SW-9045D
Total Molybdenum
<5.00
5.00
JTR
01/24/2017 03:44
6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , ftLI
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 1/17/2017 11112017-3/31/2017 2.2200
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (7340 x 1.6900) _ 100 = 124.046
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (9920 x 1,6900) = 100 = 167.648
Mg mg/I = (mg mg/kg x % Solids) : 100 = (2430 x 1.6900) _ 100 = 41.067
Na meq = Na mg/I _ Molec.Wgt.Na = 124.046 + 23 = 5.3933
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 167.648 _ 20 = 8.3824
Mg meq = Mg mg/I = Molec.Wgt.Mg = 41.067 _ 12 = 3.42225
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.3933 _ SgrRoot[0.5(8.3824+3.42225)] = 2.21995
Printed: 2/1/2018
Page 1 - 13:03
Page: 1 of 2
Report Number: 17-129-0208
Account Number: 00015
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 63800
Sample Id : Mt Holly 2nd Event 2017
(2)
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Project: Mt Holly 50-1701
REPORT OFANALYSIS Date Sampled: 5/8/2017 09:40:00
Date Received: 05/09/2017 00:00
Date Reported: 05/16/2017
Total Solids *
2.29
22900
100.0
R D
05/09/2017 15:30
SM-2540G
Moisture *
97.70
100.0
R D
05/09/2017 15:30
SM-2540G
Total Kjeldahl Nitrogen
7.09
70900
50.0
R D
05/10/2017 08:45
SM-4500-NH3C-TKN
Total Phosphorus
1.29
12900
100
JTR
05/12/2017 23:26
6010C
Total Potassium
0.27
2700
1000
JTR
05/12/2017 23:31
6010C
Total Sulfur
0.96
9570
100
JTR
05/12/2017 23:26
6010C
Total Calcium
0.97
9690
100
JTR
05/12/2017 23:26
6010C
Total Magnesium
0.21
2100
100
JTR
05/12/2017 23:26
6010C
Total Sodium
0.60
6030
100
JTR
05/12/2017 23:26
6010C
Total Iron
9810
100
JTR
05/12/2017 23:26
6010C
Total Aluminum
11000
100
JTR
05/12/2017 23:26
6010C
Total Manganese
355
5.00
JTR
05/12/2017 23:26
6010C
Total Copper
418
5.00
JTR
05/12/2017 23:26
6010C
Total Zinc
672
5.00
JTR
05/12/2017 23:26
6010C
Ammonia Nitrogen
1.65
16500
50.0
R D
05/10/2017 08:45
SM-4500-NH3C
Organic N
5.44
54400
50.0
05/10/2017 08:45
CALCULATION
Nitrate+Nitrite-N
114
2.23
SJB
05/10/201714:16
4500NO3F-2011
All values are on a dry weight
basis except as noted by asterisk.
Detection limit on all N series is on a wet basis.
Gewr
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page: 2 of 2
Report Number: 17-129-0208
Account Number: 00015
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 63800
Sample Id : Mt Holly 2nd Event 2017
WaypigintAYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project : Mt Holly 50-1701
REPORT OF ANALYSIS Date Sampled: 5/8/2017 09:40:00
Date Received: 05/09/2017 00:00
Date Reported: 05/16/2017
Total Cadmium
<2.00
2.00
JTR
05/12/2017 23:26
6010C
Total Chromium
236
5.00
JTR
05/12/2017 23:26
6010C
Total Nickel
15.0
5.00
JTR
05/12/2017 23:26
6010C
Total Lead
26.4
5.00
JTR
05/12/2017 23:26
6010C
Total Arsenic
4.50
3.00
JTR
05/12/2017 23:26
6010C
Total Mercury
0.481
0.400
SJB
05/11/2017 12:40
SW-7471B
Total Selenium
5.20
5.00
JTR
05/12/2017 23:26
6010C
pH (Standard Units) *
7.49
1.00
R D
05/10/2017 08:45
SW-9045D
Total Molybdenum
5.02
5.00
JTR
05/12/2017 23:26
6010C
Comments:
NC CERT#257
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
pwc-4 P 61ewr
Pauric McGroary
Agronomist
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 5/8/2017 511/2017-613012017 2.1848
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (6030 x 2.2900) _ 100 = 138.087
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (9690 x 2.2900) + 100 = 221.901
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2100 x 2.2900) = 100 = 48.09
Na meq = Na mg/I _ Molec.Wgt.Na = 138.087 _ 23 = 6.00378
Ca meq = Ca mg/I = Molec.Wgt.Ca = 221.901 = 20 = 11.095
Mg meq = Mg mg/I = Molec.Wgt.Mg = 48.09 _ 12 = 4.0075
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.00378 _ SgrRoot[0.5(11.095+4.0075)] = 2.18482
Printed: 2/1 /2018
Page 1 13:03
Page: 1 of 2
Report Number: 17-167-0206
Account Number: 00015
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 64394
Sample Id : Mt Holly 3rd Event
•
WayPAoint,M
NALYTICAL
Project : Mt Holly
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 6115/2017 10:15:00
Date Received: 06/16/2017 00:00
Date Reported: 06/23/2017
Total Solids *
1.84
18400
100.0
JM
06/16/2017 15:25
SM-2540G
Moisture *
98.15
100.0
JM
06/16/2017 15:25
SM-2540G
Total Kjeldahl Nitrogen
7.03
70300
50.0
JM
06/20/2017 08:30
SM-4500-NH3C-TKN
Total Phosphorus
1.31
13100
100
MOS
06/22/2017 13:46
6010C
Total Potassium
0.25
2490
100
MOS
06/22/2017 13:46
6010C
Total Sulfur
1.15
11500
100
MOS
06/22/2017 13:46
6010C
Total Calcium
1.21
12100
100
MOS
06/22/2017 13:46
6010C
Total Magnesium
0.24
2440
100
MOS
06/22/2017 13:46
6010C
Total Sodium
0.63
6300
100
MOS
06/22/2017 13:46
6010C
Total Iron
7890
100
MOS
06/22/2017 13:46
6010C
Total Aluminum
8810
100
MOS
06/22/2017 13:46
6010C
Total Manganese
320 .
5.00
MOS
06/22/2017 13:46
6010C
Total Copper
497
5.00
MOS
06/22/2017 13:46
6010C
Total Zinc
773
5.00
MOS
06/22/2017 13:46
6010C
Ammonia Nitrogen
1.51
15100
50.0
R D
06/20/2017 08:30
SM-4500-NI3C
Organic N
5.52
55200
50.0
06/20/2017 08:30
CALCULATION
Nitrate+Nitrite-N
859
2.3d
SJB
06/21/201713:08
4500NO3F-2011
All values are on a dry weight
basis except as noted by asterisk. Detection
limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in
whole or part, nor may any reference be made
to the wotff, the results, or the company in any advertising, news release, orotherpublic announcements without obtaining ourprior written authorization.
Pauric McGroary
Agronomist
Page: 2 of 2
Report Number: 17-167-0206
Account Number: 00015
Submitted By: Clay Fisackerly
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 64394
Sample Id : Mt Holly 3rd Event
Waypoint(z)
ANALYTICAL
Project : Mt Holly
REPORT OFANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 6/15/2017 10:15:00
Date Received: 06/16/2017 00:00
Date Reported: 06/23/2017
Total Cadmium
<2,00
2.00
MOS
06/22/2017 13:46
6010C
Total Chromium
207
5.00
MOS
06/22/2017 13:46
6010C
Total Nickel
14.0
5.00
MOS
06/22/2017 13:46
6010C
Total Lead
22.2
5.00
MOS
06/22/2017 13:46
6010C
Total Arsenic
<3.00
3.00
MOS
06/22/2017 17:00
6010C
Total Mercury
0.433
0.400
SJB
06/21/201715:57
SW-7471B
Total Selenium
<5.00
5.00
MOS
06/22/2017 13:46
6010C
pH (Standard Units) *
7.68
1.00
R D
06/19/2017 09:00
SW-9045D
Total Molybdenum
<5.00
5.00
MOS
06/22/2017 13:46
6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference he made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Sodium Absorption Ratio Calculation (sAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 6/15/2017 7/1/2017-9/30/2017 1.8482
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (6300 x 1.8400) = 100 = 115.92
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (12100 x 1,8400) + 100 = 222.64
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2440 x 1.8400) + 100 = 44.896
Na meq = Na mg/I = Molec.Wgt.Na = 115.92 _ 23 = 5.04
Ca meq = Ca mg/I - Molec.Wgt.Ca = 222.64 = 20 = 11.132
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 44.896 + 12 = 3.74133
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.04 = SgrRoot[0.5(11.132+3.74133)] = 1.84817
Printed: 2/1 /2018
Page 1 13:04
Page: 1 of 2
Report Number: 17-250-0210
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 55999
Sample Id : Mt Holly 4th Event
'(D
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
/ www.waypointanalytical.com
Project : Mt Holly 4th Event
REPORT OF ANALYSIS Date Sampled: 9/6/2017 09:42:00
Date Received: 09/07/2017 00:00
Date Reported: 09/14/2017
Total Solids *
1.99
19900
100.0
JM
09/07/2017 16:30
SM-2540G
Moisture *
98.00
100.0
JM
09/07/2017 16:30
SM-2540G
Total Kjeldahl Nitrogen
6.50
65000
50.0
R D
09/08/2017 08:45
SM-4500-NH3C-TKN
Total Phosphorus
1.11
11100
100
MOS
09/12/2017 14:51
6010C
Total Potassium
0.22
2170
100
MOS
09/12/2017 14:51
6010C
Total Sulfur
1.31
13100
100
MOS
09/12/2017 14:51
6010C
Total Calcium
1.05
10500
100
MOS
09/12/2017 14:51
6010C
Total Magnesium
0.24
2420
100
MOS
09/12/2017 14:51
6010C
Total Sodium
0.66
6570
100
MOS
09/12/2017 14:51
6010C
Total Iron
8870
100
MOS
09/12/2017 14:51
6010C
Total Aluminum
7490
100
MOS
09/12/2017 14:51
6010C
Total Manganese
359
5.00
MOS
09/12/2017 14:51
6010C
Total Copper
483
5.00
MOS
09/12/2017 14:51
6010C
Total Zinc
758
5.00
MOS
09/12/2017 14:51
6010C
Ammonia Nitrogen
1.35
13500
50.0
R D
09/08/2017 09:30
SM-4500-NH3C
Organic N
5.15
51500
50.0
09/08/2017 08:45
CALCULATION
Nitrate+Nitrite-N
328
2.25
SJB
09/13/201712:46
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page: 2 of 2
Report Number: 17-250-0210
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 55999
Sample Id : Mt Holly 4th Event
(2)
Waypoint
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Project : Mt Holly 4th Event
REPORT OF ANALYSIS Date Sampled: 9/6/2017 09:42:00
Date Received: 09/07/2017 00:00
Date Reported: 09/14/2017
Total Cadmium
<2.00
2.00
MOS
09/12/2017 14:51
6010C
Total Chromium
175
5.00
MOS
09/12/2017 14:51
6010C
Total Nickel
15.2
5.00
MOS
09/12/2017 14:51
6010C
Total Lead
18.5
5.00
MOS
09/12/2017 14:51
6010C
Total Arsenic
<3.00
3.00
MOS
09/12/2017 14:51
6010C
Total Mercury
0.540
0.400
SJB
09/11/2017 15:32
SW-7471B
Total Selenium
<5.00
5.00
SJB
09/14/2017 12:02
6010C
pH*
7.69
1.00
R D
09/08/2017 09:30
SW-9045D
Total Molybdenum
<5.00
5.00
MOS
09/12/2017 14:51
6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
? ram« mC
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 9/6/2017 101112017-11130/2017 2.1140
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (6570 x 1.9900) + 100 = 130.743
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (10500 x 1.9900) = 100 = 208.95
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2420 x 1.9900) _ 100 = 48.158
Na meq = Na mg/I + Molec.Wgt.Na = 130.743 _ 23 = 5.68448
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 208.95 = 20 = 10.4475
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 48.158 -= 12 = 4.01317
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.68448 = SgrRoot[0.5(10.4475+4.01317)] = 2.11403
Printed: 2/1 /2018
Page 1 13:04
Page: 1 of 2
Report Number: 17-305-0201
Account Number: 00015
Submitted By: Adam Brigman
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 56945
Sample Id : Mt. Holly 5th Event N + M
O
Waypoint"
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: Mt. Holly 50-1701
REPORT OF ANALYSIS Date Sampled: 10/31/2017 07:45:00
Date Received: 11/01/2017 00:00
Data Reported: 11/08/2017
Total Solids *
1.28
12800
100.0
R D
11/01/2017 14:00
SM-2540G
Moisture *
98.71
100.0
R D
11/01/2017 14:00
SM-254OG
Total Kjeldahl Nitrogen
5.66
56600
50.0
R D
11/02/2017 08:30
SM-4500-NH3C-TKN
Total Phosphorus
1.08
10800
100
MOS
11/07/2017 13:45
6010C
Total Potassium
0.23
2260
100
MOS
11/07/2017 13:45
6010C
Total Sulfur
1.24
12400
100
MOS
11/07/2017 13:45
6010C
Total Calcium
1.03
10300
100
MOS
11/07/2017 13:45
6010C
Total Magnesium
0.23
2280
100
MOS
11/07/2017 13:45
6010C
Total Sodium
0.66
6600
100
MOS
11/07/2017 13:45
6010C
Total Iron
8400
100
MOS
11/07/2017 13:45
6010C
Total Aluminum
8320
100
MOS
11/07/2017 13:45
6010C
Total Manganese
370
5.00
MOS
11/07/2017 13:45
6010C
Total Copper
402
5.00
MOS
11/07/2017 13:45
6010C
Total Zinc
692
5.00
MOS
11/07/2017 13:45
6010C
Ammonia Nitrogen
1.24
12400
50.0
R D
11/02/2017 08:30
SM-4500-NH3C
Organic N
4.42
44200
50.0
11/02/2017 08:30
CALCULATION
Nitrate+Nitrite-N
2760
2.02
SJB
11/b6/201712:54
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection
limit on all N series is on a wet basis.
0��a
rr
Our reports and letters are for the exclusive and confidential
use of our clients, and may not be reproduced in
whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page: 2 of 2
Report Number: 17-305-0201
Account Number: 00015
Submitted By: Adam Brigman
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 56945
Sample Id : Mt. Holly 5th Event N + M
•
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project : Mt. Holly 50-1701
REPORT OFANALYSIS Date Sampled: 10/31/2017 07:45:00
Date Received: 11/01/2017 00:00
Date Reported: 11/08/2017
Total Cadmium
<2.00
2.00
MOS
11/07/2017 13:45
6010C
Total Chromium
157
5.00
MOS
11/07/2017 13:45
6010C
Total Nickel
17.1
5.00
MOS
11/08/2017 12:21
6010C
Total Lead
16.1
5.00
MOS
11/07/2017 16:39
6010C
Total Arsenic
3.39
3.00
MOS
11/07/2017 13:45
6010C
Total Mercury
<0.400
0.400
SJB
11/06/2017 10:56
SW-7471B
Total Selenium
5.23
5.00
MOS
11/07/2017 16:39
6010C
pH *
7.62
1.00
JM
11/02/2017 08:30
SW-9045D
Total Molybdenum
<5.00
5.00
MOS
11/07/2017 13:45
6010C
Comments:
NC CERT#257, SC CERT#9300 7001
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 10/31/2017 1211/2017-1213112017 1.7292
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (6600 x 1.2800) = 100 = 84.48
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10300 x 1.2800) _ 100 = 131.84
Mg mg/I = (mg mg/kg x % Solids) - 100 = (2280 x 1.2800) = 100 = 29.184
Na meq = Na mg/I _ Molec.Wgt.Na = 84.48 _ 23 = 3.67304
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 131.84 _ 20 = 6.592
Mg meq = Mg mg/I + Molec.Wgt.Mg = 29.184 = 12 = 2.432
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.67304 _ SgrRoot[0.5(6.592+2.432)] = 1.72919
Printed: 2/1/2018
Page 1 13:05
FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: MADISON
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 5.23
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 3.40 ACRES PERMITTED: 3.40
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
T N
Nitrogen
and
(pptn)
Crop
Total
Per Acre
7/26/17
68,200.00 (G)
20058.824
1.84
1.539
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
15,100.00 p
859.00 p
24969
FESCUE
Jul-17
68,200.00 (G)
20,058.824
[7,300.p
1
1
Total Gallons/Ac: 20,058.82
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
77
0.009
0.006
0.637
1.530
0.068
0.001
0.015
0.043
0.015
2.379 40.32
Cumulative lbs/acre
0.009
0.006
0.637
1.530
0.068
0.001
0.015
0.043
0.015
2.379
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
167
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
6 '
XCL
(SIGN LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, InjectionAncorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
FACILITY NAME: MOUNT HOLLY, NC
DWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0006
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 14.75
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90
Page: 1
Lane Applied ***
Date:4 Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
pro
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
MONTH
7/25/17
124,000.00 (G)
13932.584
1.84
1.069
MHAEDL
DRY
0- 1/2"
SUR
0.5
0.30
70,300. p
15,100.00 p
859.00 p
24969
I FESCUE
7/26/17
68,200.00 (G)
7662.9211
1.84
0.588
MHAEDL
DRY
0- 1/2"
SUR
0.5
0.30
70,300. p
15,100.00 p
859.00 p
24969
FESCUE
Jul-17
1 192,200.00 (G)
21,595.505
1
Total Gallons/Ac: 21,595.51
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
83
0.010
0,007
0.686
1.647
0.074
0.001
0.017
0.046
0.017
2.562
43.41
Cumulative lbs/acre
0.061
1 0.039
5.386
1 10.728
1 0.653
0.023
0.145
1 0.530
0.103
15.881
?ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
187
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
i
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X /2 /�//2
;//xe�_
(SI O AND APPLIER) DAE
"leer�� r penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0014
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 10.47
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
Total
Per Acre
7/26/17
136,400.00 (G)
20058.824
1.84
1.539
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,300.p
15,100.00 p
859.00 p
Jul-17
136A .00 (G)
20,058.824
7[��FESCUE
Total Gallons/Ac: 2U,058.82
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
77
0.009
0.006
0.637
1.530
0.068
0.001
0.015
0.043
0.015
2.379 40.32
Cumulative lbs/acre
0.045
0.030
4.346
8.568
0.516
0.017
0.115
0.414
0.079
12.751
Permit PAN Limit (Ibs/acre) Ist Crop/21id Crop
190
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X 2Xl4
(AATUREOF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD
JWNER: DAVID ALLEN PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 48.12
iITE #: NC GA 00045 FIELD# : GA 00045 0001 OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
7/20/17
49,600.00 (G)
2917.647
1.84
0.224
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,300. p
15,100.00 p
859.00 p
24969
I FESCUE
7/21/17
86,800.00 (G)
5105,882
1.84
0.392
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,300. p
15,100.00 p
859.00 p
24969
I FESCUE
7/24/17
130,200.00 (G)
7658.824
1.84
0.588
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,300. p
15,100.00 p
859.00 p
24969
I FESCUE
7/25/17
18,600.00 (G)
1094.118
1.84
0.084
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,300.p
15,100.00 p
859.00 p
24969
FESCUE
Jul-17
285,200.00 (G)
16,776.471
10/16/17
74,400.00 (G)
4376.471
1.99
0.363
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
65,000. p
13,500.00 p
328.00 p
22528
I FESCUE
10/17/17
124,000.00 (G)
7294.118
1.99
0.605
MHAEDL
DRY
0-<1/2"
SUR
I 0.5
0.30
65,000. p
13,500.00 p
328.00 p
22528
I FESCUE
10/18/17
117,800.00 (G)
6929.412
1.99
0.575
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
65,000. p
13,500.00 p
328.00 p
22528
FESCUE
Oct-17
316,200.00 (G)
18,600.001
1
,AGILITY NAME: MOUNT HOLLY, NC
)WNER: DAVID ALLEN
!ITE #: NC GA 00045 FIELD# : GA 00045 0001
ZESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: LLOYD
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 48.12
OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00
Page
Lime Applied ***
Date
LWAc
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
PerResidual
Dry, Wet,
Past 24
Method
zation
zation
TIN
Nitrogen
and
(ppm)
Crop
Total Gallons/Ac: 35,376.47
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Me
Ni
Se
Zn
P
PAN
Annual lbs/acre
134
0.017
0.011
1.073
2.771
0.114
0.003
0.028
0.083
0.028
4.330
67.99
Cumulative lbs/acre
0.034
0.023
2.694
5.912
0.338
0.009
0.061
0.223
0.057
9.245
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
194
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
M AEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
4
X
/ 5 la
("SI ueOF LAND APPLIER) DATE
,drenalty, of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 32.05
SITE #: NC LT 00046 FIELD# : LT 00046 0001 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
A It
Vola-
Miner -
DATE or
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
'Total
Per Acre
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
3/1/17
43,400.00 (G)
3677.966
1.69
0.259
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
68,800.p
26,500.00 p
259.00 p
26199
FESCUE
3/3/17
142,600.00 (G)
12084,746
1.69
0.852
MI-IAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
68,800. p
26,500.00 p
259.00 p
26199
FESCUE
Mar-17
186,000.00 (G)
15,762.712
6/3/17
62,000.00 (G)
5254.237
2.29
0.502
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684
I FESCUE
6/7/17
31,000.00 (G)
2627.119
2.29
0.251
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684 I
FESCUE
6/8/17
105,400.00 (G)
8932.203
2.29
0.853
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,900.p
16,500.00 p
114.00 p
24684
FESCUE
Jun-17
198,400.00 (G)
16,813.559
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
137
0.021
0.011
1.400
2.349
0.163
0.005
0.027
0.096
0.028
3.780
72.08
Cumulative Ibs/acre
0.062
0.038
4.836
8.634
0.613
0.018
0.097
0.413
0.096
13.279
Peanut PAN Limit (lbs/acre) 1st Crop/2nd Crop
173
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
s
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
x��
(*/REOF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 26.14
SITE #: NC LT 00046 FIELD# : LT 00046 0002 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(pp-)
Crop
Total
Per Acre
12/4/17
49,600.00 (G)
1097.345
1.28
0.059
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
22220
I FESCUE
12/5/17
74,400.00 (G)
1646.018
1.28
0.088
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
22220
FESCUE
12/6/17
117,800.00 (G)
2606.195
1.28
0.139
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
56,600.p
12,400.00 p
2,760.00 p
22220
Ij
I FESCUE
12/7/17
136,400.00 (G)
3017.699
1.28
0.161
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
22220
I FESCUE
12/12/17
43,400.00 (G)
960.177
1.28
0.051
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
22220
I FESCUE
12/13/17
68,200.00 (G)
1508.850
1.28
0.081
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
1-2220
FESCUE
Dec-17
489,800.00 (G)
1 10,836.284
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
26
0.004
0.002
0.182
0.465
0.019
<.001
0.006
0.020
0.006
0.801
12.49
Cumulative Ibs/acre
0.362
1 0.074
1 6.016
30.628
2.068
0.065
0.341
1.383
0.162
37.543
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
149
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
i
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X
2 � d l
(SKIN URE OF LAND APPLIER) DATE
"I cert fy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
DWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 26.19
SITE #: NC LT 00046 FIELD# : LT 00046 0003 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90
Page: 1
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner
Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE
DATE or
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
2/28/17
105,400.00 (G)
10646.465
1.69
0.750
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
68,800. p
26,500.00 p
259.00 p
26199
FESCUE
Feb-17
105,400.00 (G)
10,646:465
3/1/17
31,000.00 (G)
3131.313
1.69
0.221
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
68,800. p
26,500.00 p
259.00 p
26199
FESCUE
Mar-17
31,000.00 (G)
3,131.313
6/3/17
18,600.00 (G)
1878.788
2.29
0.179
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684
I FESCUE
6/7/17
93,000.00 (G)
9393.939
2.29
0,897
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684
I FESCUE
6/8/17
62,000.00 (G)
6262.626
2.29
0.598
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684
FESCUE
Jun-17
173,600.00 (G)
17,535.353
i orai Cialions/Ac: 31,313.13
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
134
0.021
0.011
1.352
2.280
0.157
0.004
0.027
0.092
0.027
3.668
70.00
Cumulative lbs/acre
0.069
0.042
5.316
9.518
0.669
0.021
0.108
0.464
0.107
14.528
?ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
171
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
i
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X �' G
(SI OF LAND APPLIER) DATE
"I c ify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
FACILITY NAME: MOUNT HOLLY, NC
DWNER: TONY JONES
3ITE #: NC LT 00046 FIELD# : LT 00046 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 11.25
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 19.40 ACRES PERMITTED: 19.40
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
12/11/17
148,800.00 (G)
7670.103
1.28
0.409
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
F 22220
I FESCUE
12/12/17
62,000.00 (G)
3195.8761
1.28
0.171
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
56,600. p
12,400.00 p
2,760.00 p
22220
FESCUE
Dec-17
210,800.00 (G)
10,865.979
Total Gallons/Ac: 10,865.98
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
26
0.004
0.002
0.182
0.466
0.019
<.001
0.006
0.020
0.006
0.803
12.53
Cumulative Ibs/acre
0.137
0.073
4.579
40.511
1.667
0.085
0.457
1.551
0.158
37.036
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
148
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) .
36.6
34.8
1
i
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X �L
(SIGV&<0F LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pptm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
K Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
'ACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD
)WNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 15.99
:ITE #: NC LT 00046 FIELD# : LT 00046 0005 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
tESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90
Page
Lune Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
6/8/17
12,400.00 (G)
1569.620
2.29
0.150
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
70,900.p
16,500.00 p
114.00 p
1 24684
(FESCUE
6/9/17
155,000.00 (G)
19620.253
2.29
1.874
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684
FESCUE
Jun-17
167,400.00 (G)
21,189.873
A ULQl Uallu11b/Hu: 41,16Y.51
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
100
0.018
0.008
0.955
1.692
0.167
0.002
0.020
0.061
0.021
2.720
52.21
Cumulative lbs/acre
0.037
0.019
2.388
4.099
0.281
0.008
0.048
0.191
0.049
6.169
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
209
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
11339.0
267.9
15.0 375.0
89.0
2500.0
VIHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
x
(SIfURF OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or tng/lcg * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 15.15
;ITE #: NC LT 00046 FIELD# : LT 00046 0008 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
2ESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60
Page
Lune Applied ***
Date
F LbdAc
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE or
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
3/1/17
80,600.00 (G)
12212.121
1.69
0.861
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
68,800. p
26,500.00 p
259.00 p
26199
FESCUE
Mar-17
80,600.00 (G)
12,212.121
1
1
6/3/17
93,000.00 (G)
14090.909
2.29
1.346
MHAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
70,900.p
16,500.00 p
114.00 p
24684
I FESCUE
6/7/17
6,200.00 (G)
939.394
2.29
0.090
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
70,900. p
16,500.00 p
114.00 p
24684
FESCUE
Jun-17
99,200.00 (G)
15,030.303
A.1a, Ua IUII /tW. 4I'L4L.46
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
116
0.018
0.009
1.175
1.980
0.136
0.004
0.023
0.080
0.024
3.186
60.78
Cumulative lbs/acre
0.066
0.041
5.169
9.269
0.652
0.020
0.106
0.455
0.104
14.083
'ermit PAN Limit (lbs/acre) 1st Crop/2nd Crop
171
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
s
1339.0
267.9
15.0 375.0
89.0
2500.0
VIHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
x
11
(SIOF LAND APPLIER) DATE
"I ce fy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = pp- or mg/kg r* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
FACILITY NAME: MOUNT HOLLY, NC
OWNER: DEAN S. CONNELL
SITE #: NC MG 00037 FIELD# : MG 00037 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 47.32
OPERATOR: DEAN S. CONNELL CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 20.20 ACRES PERMITTED: 20.20
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE or
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
p,e,N
Total
Per Acre
MONTH
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
2/27/17
248,000.00 (G)
12277.228
1.69
0.865
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
68,800. p
26,500.00 p
259.00 p
26199
FESCUE
Feb-17
248,000.00 (G)
12,277.228
10/19/17
248,000.00 (G) -
12277.228
1.99
1.019
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
65,000. p
13,500.00 p
328.00 p
22528
I FESCUE
10/20/17
111,600.00 (G)
5524.752
1.99
0.458
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
65,000. p
13,500.00 p
328.00 p
22528
FESCUE
Oct-17
359,600.00 (G)
17,801.980
Total Gallons/Ac: 30,079.21
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
112
0.014
0.009
1.017
2.211
0.115
0.004
0.023
0.082
0.023
3.503
56.68
Cumulative lbs/acre
0.105
0.037
4.524
8.672
0.539
0.019
0.106
0.424
0.090
12.592
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
147
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
I
i
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X
(SIG TURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2018
Summit Environmental Technologies, Inc. N
InSUMMIT 3310 Win St. ��5� Narrative
€NVIROFIME14-Ir L iEr-Hhl0LDGIES, V11C. Cuyahoga Falls, Ohio 44223 WO#: 17010901
Ana.'giffcEi Lebad8F-Pr;e= TEL: (330) 253-8211 FAX.- (330) 253-4485
Website: htto:11i9ivi9.settekcorr Date: 2/10/2017
CLIENT: Synagro, NC 28134
Project: Mt.Holly 50-1701
WorkOrder Narrative:
17010901: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Teclurologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
continents or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
40 ug/mL CCV 1067889: Analytical Comments for svoc-MSTR NPW(8270), Sample 40 ug/mL CCV,
Batch ID R64812 : The SVOC CCV (Batch R64812) exhibited high recovery for 2,4,5-Trichlorophenol;
All reported samples are ND.
lcs-25177 1075432: Analytical Comments for tclp-svoc-herb tclp(8151), Sample lcs-25177, Batch ID
25177 : The TCLP Pest LCS (25177/R65243) exhibited low recovery for Analyte: 2,4,5-TP; Possible
low bias for Analyte:2,4,5-TP in associated samples;
Original
Page 2 of 29
Page 2 of 35
Summit Environmental Technologies, In Qualifiers and Acronyms
summirt 3310 Win E
F71iNIR0Wm1EhaT,aL7EC. IOLDC-IEs, r4c. Cuyahoga Falls, Ohio442.' WO#: 17010901
Anatyt:esi LFbor„&w.1i= TEL: (330) 253-8211 FAX: (330) 253-44�
Website: htto://www.settek.co Date: 2/10/2017
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
x The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
s The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 29
Page 3 of 35
ffflsummlat
,
bn a.lyiAez .�FY30 T�1''11t=T .
CLIENT: Synagro, NC 28134
Project: Mt.Holly 50-1701
Lab SampleID Client Sample ID
17010901-001 Mt.Holly 50-1701
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4485
Website: http://www.settek.corr.
Tag No Date Collected
1/17/2017 10:25:00 AM
Workorder
Sample Summary
WO#: 17010901
10-Feb-17
Date Received Matrix
1/19/201710:00:00 AM Sludge
Page 4 of 29
Page 4 of 35
Summit Environmental Technologies, Inc.
SUMMI;T
DATES REPORT
3310 Win St.
, Cuyahoga Falls, Ohio 44223
f1nnlyidoal
LaLapriitoria.�
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: http://www.settelccom
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
Sample ID
Client Sample ID
Collection Date 1 Matrix Test Name Leachate Date
Prep Date
Analysis Date
17010901-OOIA
Mt.Holly 50-1701
1/17/2017 10:25:00 AM Sludge Flashpoint Determination (1010)
1/24/2017 10:37:31 AM
Ignitability of Solids (SW-846: 1030)
2/9/2017 7:00:00 AM
pH (SW9045D)
1/23/2017 3:46:00 PM
Reactive Cyanide (9014/7.3.3.2)
1/27/2017 3:04:00 PM
Reactive Sulfide (9034)
1/27/2017 3:04:00 PM
SVOC 8270 TCLP BNA List 1/24/2017 4:02:06 PM
1/26/2017 9:30:00 AM
1/26/2017 5:28:00 PM
SVOC SW-846: 8081-TCLP Pesticide! 1/24/2017 4:02:06 PM
1/26/2017 8:30:00 AM
1/26/2017 6:22:00 PM
SVOC SW-846: 8151 Herbicides-TCL 1/24/2017 4:02:06 PM
1/27/2017 5:00:25 PM
2/7/2017 4:53:00 PM
SVOC SW-846: 8151 Herbicides-TCL 1/24/2017 4:02:06 PM
1/27/2017 5:00:25 PM
2/7/2017 4:53:00 PM
TCLP Mercury Analysis (1311/7470) 1/24/2017 4:02:06 PM
1/25/2017 10:00:00 AM
1/25/2017 4:18:00 PM
TCLP Metals Analysis (6010) 1/24/2017 4:02:06 PM
1/25/2017 9:52:01 AM
1/26/2017 11:53:56 AM
VOC by GUMS (8260)-TCLP
1/27/2017 4:07:00 PM
Original
Page 5 of 29
Page 5 of 35
Summit Environmental Technologies, Inc.
EMSUMMAT 3310 Win St.
EtIVIFON&IENT LIEt.HNOLDCIES_.ac-4c_ Cuyahoga Falls, Ohio44223
.4n31yb'c aU-4-baraipda'i TEL: (330) 253-8211 FAX: (330) 253-4485
Website: http://www.settekcorr,
Analytical Report
(base report)
WO#: 17010901
Date Reported: 2/10/2017
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/17/2017 10:25:00 AM
Lab ID: 17010901-001A
Project: Mt.Holly 50-1701
Client Sample ED Mt.Holly 50-1701
Analyses
Result
PQL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (1311/7470)
TCLP Mercury
ND
0.00200
mg/L
1
1/25/2017 4:18:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010C
SW3010A Analyst: VVK
TCLP METALS ANALYSIS (6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
1/26/2017 11:53:56 AM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/26/2017 11:53:56 AM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/26/2017 11:53:56 AM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/26/2017 11:53:56 AM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/26/2017 11:53:56 AM
TCLP Selenium(Se)
ND
0.500
mg/L
1
1/26/2017 11:53:56 AM
TCLP Silver(Ag)
ND
0.500
mg/L
1
1/26/2017 11:53:56 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270C
SW3510C
Analyst: MSM
SVOC 8270 TCLP BNA LIST
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
1/26/2017 5:28:00 PM
2,4,5-Trichlorophenol
ND
0.200
QC+ mg/L
2
1/26/2017 5:28:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
1/26/2017 5:28:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
2
1/26/2017 5:28:00 PM
Cresols, Total
ND
4.00
mg/L
2
1/26/2017 5:28:00 PM
Hexachloro-1,3-butadiene
ND
0.100
mg/L
2
1/26/2017 5:28:00 PM
Hexachlorobenzene
ND
0.100
mg/L
2
1/26/2017 5:28:00 PM
Hexachloroethane
ND
0.0800
. mg/L
2
1/26/2017 5:28:00 PM
Nitrobenzene
ND
0.0800
mg/L
2
1/26/2017 5:28:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
1/26/2017 5:28:00 PM
Pyridine
ND
0.200
mg/L
2
1/26/2017 5:28:00 PM
Surr: 2-Fluorophenol
49.3
10 - 109
%Rec
2
1/26/2017 5:28:00 PM
Surr: Phenol-d6
49.9
10 - 109
%Rec
2
1/26/2017 5:28:00 PM
Surr: Nitrobenzene-d5
65.5
19 - 120
%Rec
2
1/26/2017 5:28:00 PM
Surr: 2,4,6-Tribromophenol
51.2
10 - 120
%Rec
2
1/26/2017 5:28:00 PM
Surr: 2-Fluorobiphenyl
65.6
22 - 117
%Rec
2
1/26/2017 5:28:00 PM
Surr: p-Terphenyl-d14
70.6
34 - 116
%Rec
2
1/26/2017 5:28:00 PM
Qualifiers: H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected at the Reporting Limit PL Permit Limit
R RPD outside accepted recovery limits RL Reporting Detection Limit
W Sample container temperature is out of limit as specified at testcode
Original
Page 6 of 29
Page 6 of 35
Summit Environmental Technologies, Inc. Analytical Report
ffISUMM3310 Win St.
€t�JV1R(*Ni fo%L7ECIANOLDGltS,INC. Cuyahoga Falls, Ohio44223 (base report)
4na;y?r�ai a �aa-�dy ig TEL: (330) 253-8211 FAX. (330) 253-4485 WO#: 17010901
Website: hay.-Iltviviv.settekcorr Date Reported: 2/10/2017
CLIENT: Synagro, NC 28134 Tag Number:
Matrix: SLUDGE Collection Date: 1/17/2017 10:25:00 AM
Lab ID: 17010901-OOIA
Project: Mt.Holly 50-1701
Client Sample ID Mt.Holly 50-1701
Analyses Result PQL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SVOC SW-846: 8081-TCLP PESTICIDES
SW8081A SW3510C Analyst: JBN
Chlordane, total
ND
0.0100
mg/L
1 1/26/2017 6:22:00 PM
Toxaphene
ND
0.0200
mg/L
1 1/26/2017 6:22:00 PM
Endrin
ND
0.00100
mg/L
1 1126/2017 6:22:00 PM
gamma-BHC
ND
0.00100
mg/L
1 1/26/2017 6:22:00 PM
Heptachlor
ND
0.00100
mg/L
1 1/26/2017 6:22:00 PM
Heptachlor epoxide
ND
0.00100
mg/L
1 1/26/2017 6:22:00 PM
Methoxychlor
ND
0.00100
mg/L
1 1/26/2017 6:22:00 PM
Surr: Tetrachloro-m-xylene
70.6
10 - 119
%Rec
1 1/26/2017 6:22:00 PM
TCLP HERBICIDES ANALYSIS (SW846 131118151)
SW8151A
SW8151A Analyst: JBN
SVOC SW-846: 8151 HERBICIDES-TCLP
2,4-D
ND
1.00
mg/L
1 2/7/2017 4:53:00 PM
2,4,5-TP
ND
0.500
mg/L
1 2/7/2017 4:53:00 PM
Surr: DCAA
85.6
20 - 140
%Rec
1 2/7/2017 4:53:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260B
Analyst: MES
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene
ND
0.100
mg/L
1 1127/2017 4:07:00 PM
1,2-Dichloroethane
ND
0.100
mg/L
1 1127/2017 4:07:00 PM
MEK
ND
2.00
mg/L
1 1/27/2017 4:07:00 PM
Benzene
ND
0.100
mg/L
1 1/27/2017 4:07:00 PM
Carbon tetrachloride
ND
0.100
mg/L
1 1/27/2017 4:07:00 PM
Chlorobenzene
ND
0.100
mg/L
1 1/27/2017 4:07:00 PM
Chloroform
ND
0.100
mg/L
1 1/27/2017 4:07:00 PM
Tetrachloroethene
ND
0.100
mg/L
1 1/27/2017 4:07:00 PM
Trichloroethene
ND
0.100
mg/L
1 1/27/2017 4:07:00 PM
Vinyl chloride
ND
0.200
mg/L
1 1/27/2017 4:07:00 PM
Surr: 4-Bromofluorobenzene
98.2
70 - 130
%Rec
1 1/27/2017 4:07:00 PM
Surr: Dibromofluoromethane
100
70 - 130
%Rec
1 1/27/2017 4:07:00 PM
Surr: Toluene-d8
100
70 - 130
%Rec
1 1/27/2017 4:07:00 PM
RCI
REACTIVE CYANIDE (9014/7.3.3.2)
Qualifiers: H Holding times for preparation or analysis exceeded
ND Not Detected at the Reporting Limit
R RPD outside accepted recovery limits
W Sample container temperature is out of limit as specified at testcode
SW9014 Analyst: MS
M Manual Integration used to determine area response
PL Permit Limit
RL Reporting Detection Limit
Original
Page 7 of 29
Page 7 of 35
MSUMMSummit Environmental Technologies, Inc. Analytical Report
IT 3310 Win St.
Fl•lirlRONMEFa'P.aL 1'ECHNOLDCIES, J BG_ Cuyahoga Falls, Ohio 44223 (base report)
t Ftrli�rl,reHi �?e3drrtC?fi?4 TEL: (330) 253-8211 FAX.- (330) 253-4485 W04: 17010901
Website: htttwIliviviv.settek.corr, Date Reported: 2/10/2017
CLIENT:
Synagro, NC 28134 Tag Number:
Matrix:
SLUDGE Collection Date: 1/17/2017 10:25:00 AM
Lab ID:
17010901-001A
Project:
Mt.Holly 50-1701
Client Sample ID Mt.Holly 50-1701
Analyses Result PQL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)
Cyanide, Reactive ND 0.500 mg/Kg 1 1/27/2017 3:04:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030) SW1030 Analyst: RMT
Ignitability Non-flammable. 1 2/9/2017 7:00:00 AM
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 6.85 s.u.@21.00 1 1/23/2017 3:46:00 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE (9034)
Sulfide, Reactive ND 25.0 mg/Kg 1 1/27/2017 3:04:00 PM
Qualitlers: H Holding times for preparation or analysis exceeded
ND Not Detected at the Reporting Limit
R RPD outside accepted recovery limits
W Sample container temperature is out of limit as specified at testcode
M Manual Integration used to determine area response
PL Permit Limit
RL Reporting Detection Limit
Original
Page 8 of 29
Page 8 of 35
"'MIT�. Summit Environmental Technologies, Inc.M5 Sul 3310 Win St. QC SUMMARY REPORT
rraLlBtorrr!9Bnl�a1� PttlHpJ+iL•cG1[S ]�9i Cuyahoga Falls, Ohio44223 WO#: 17010901
r'dnBlysic a,,1 LohDr„ mrie5 TEL: (330) 253-8211 FAX: (330) 253-4489
Website: http://`wivw.settek,com 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: 2SI33
Sample ID: MB-25133
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/25/2017
RunNo: 64742
Nent ID: PBW
Batch ID: 25133
TestNo: SW6010C SW3010A
Analysis Date: ' 1/25/2017
SegNo: 1066749
analyte
Result
PQL SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-25133
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 1/25/2017
RunNo: 64742
client ID: LCSW
Batch ID: 25133
TestNo: SW6010C SW3010A
Analysis Date: 1/25/2017
SegNo: 1066750
4nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.01
0.500
2.000
0
101
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
98.5
80
120
TCLP Cadmium(Cd)
1.98
0.100
2.000
0
99.0
80
120
TCLP Chromium(Cr)
2.00
0.200
2.000
0
100
80
120
TCLP Lead(Pb)
1.98
0.500
2.000
0
99.0
80
120
TCLP Selenium(Se)
1.97
0.500
2.000
0
98.5
80
120
TCLP Silver(Ag)
0.980
0.500
1.000
0
98.0
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
7 Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 9 of 29
Page 9 of 35
Summit Environmental Technologies, Inc. ^r SUMMARY
REPORT
ffJ Sul mmiar 3310 Win St. l� 1. r7 �J lV� i REPORT
1
LI.NllRrJ,'JngEt-l"S.,L'tf=rHtJ0GDti1L5',]t9G Cuyahoga Falls, Ohio44223
d#nalyircr�l-d: l3s�r e rrr�.�, TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901
Website: httb://wivw.settek.co7n 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID• 25139
Sample ID: MB-25139
SampType: MBLK
TestCode: HG TCLP(74 Units: PPM
Prep Date: 1/25/2017
RunNo: 64750
Client ID: PBW
Batch ID: 25139
TestNo: SW7470A SW7470A
Analysis Date: 112512017
SegNo: 1066822
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID: LCS-25139
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/25/2017
RunNo: 64750
Client ID: LCSW
Batch ID: 25139
TestNo: SW7470A SW7470A
Analysis Date: 1/25/2017
SegNo: 1066823
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury 0.00393 0.00200 0.00400 0 98.2 80 120
Sample ID: 17010901-001AMS
SampType: MS
TestCode: HG TCLP(74 Units: PPM
Prep Date: 1/25/2017
RunNo: 64750
Client ID: Mt.Holly 50-1701
Batch ID: 25139
TestNo: SW7470A SW7470A
Analysis Date: 1/25/2017
SegNo: 1066836
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.00394 0.00200 0.00400 0 98.5 75 125
Sample ID: 17010901-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/25/2017
RunNo: 64750
Client ID: Mt.Holly 50-1701
Batch ID: 25139
TestNo: SW7470A SW7470A
Analysis Date: 1/25/2017
SegNo: 1066837
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
TCLP Mercury 0.00391 0.00200 0.00400 0 97.8 75 125 0.00394 0.764 20
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 10 of 29
Page 10 of 35
iS U ir Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
ENVIRCIPM01 Ef1TAL TFaIHNOLoc'nis, .*ic Cuyahoga Falls, Ohio 44223 WO#: 17010901
�1,n�drtt�co,' Lrbaf-arari TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htto://wii,iv.sett6k.coin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: 25139
Sample ID: 17010901-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/25/2017
RunNo: 64750
Client ID: Mt.Holly 50-1701
Batch ID: 25139
TestNo: SW7470A SW7470A
Analysis Date: 1/26/2017
SegNo: 1066837
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 11 of 29
Page 11 of 35
3310 Win St.
Summit Environmental Technologies, Inc.EJ
C SUMMARSumm''l-Wr
REPORT QC SUMMARY
Csf;iPl'I tiL`fP��HCIflLW�IES,tt9,
Cuyahoga Falls, Ohio44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: htW.-1Av14,w.settek.coin
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
BatchID: 25164
Sample ID: MB-25164
SampType: MBLK
TestCode: svoc-BNA T Units: mg/L
Prep Date: 1/26/2017
RunNo: 64812
client ID: PBW
Batch ID: 25164
TestNo: SW8270C SW3510C
Analysis Date: 1/26/2017
SegNo: 1067890
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0200
2,4,5-Trichlorophenol
ND
0.0500
2,4,6-Trichlorophenol
ND
0.0500
2,4-Dinitrotoluene
ND
0.0100
Cresols, Total
ND
1.00
Hexachloro-1,3-butadiene
ND
0.00400
Hexachlorobenzene
ND
0.0100
Hexachloroethane
ND
0.0200
Nitrobenzene
ND
0.0200
Pentachlorophenol
ND
0.0500
Pyridine
ND
0.0500
Surr: 2-Fluorophenol
0.240
Surr: Phenol-d6
0.241
Surr: Nitrobenzene-d5
0.309
Surr: 2,4,6-Tribromophenol
0.263
Surr: 2-Fluorobiphenyl
0.314
Surr: p-Terphenyl-d14
0.360
0.5000
47.9
10
109
0.5000
48.1
10
109
0.5000
61.7
19
120
0.5000
52.6
10
120
0.5000
62.8
22
117
0.5000
72.0
34
116
QC+
'ample ID: LCS-25164
SampType: LCS
TestCode: svoc-BNA_T Units: mg/L
Prep Date: 1/26/2017
RunNo: 64812
Nent ID: LCSW
Batch ID: 25164
TestNo: SW8270C SW3510C
Analysis Date: 1/26[2017
SegNo: 1067891
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit O RSD is greater than RSDlimit Original
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 12 of 29
Page 12 of 35
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
ffJ Summ-ur 3310 Win St.
�N� IRC:Pip.9El'I'��L'PEdH1�CG�GIES,.a6*9 Cuyahoga Falls, Ohio44223
�7.a�ly:aa�Ad�:a€ntor,3e9ri�5 TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: httD://www.settek.com 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: 25164
Sample ID: LCS-25164
SampType: LCS
TestCode: svoc-BNA T Units: mg/L
Prep Date: 1/26/2017
RunNo: 64812
client ID: LCSW
Batch ID: 25164
TestNo: SW8270C SW3510C
Analysis Date: 1/26/2017
SegNo: 1067891
�nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.135
0.0200
0.2000
0
67.3
19.1
126
2,4,5-Trichlorophenol
0.154
0.0500
0.2000
0
77.2
11.7
151
2,4,6-Trichlorophenol
0.148
0.0500
0.2000
0
73.8
12.4
150
2,4-Dinitrotoluene
0.133
0.0100
0.2000
0
66.3
20.6
140
Cresols, Total
ND
1.00
0.4000
0
63.2
10
129
Hexachloro-1,3-butadiene
0.135
0.00400
0.2000
0
67.7
14.7
137
Hexachlorobenzene
0.120
0.0100
0.2000
0
60.2
12
139
Hexachloroethane
0.124
0.0200
0.2000
0
61.8
14.8
132
Nitrobenzene
0.128
0.0200
0.2000
0
63.8
15.6
138
Pentachlorophenol
0.136
0.0500
0.2000
0
67.8
10
156
Pyridine
ND
0.0500
0.2000
0
13.1
10
126
Surr: 2-Fluorophenol
0.308
0.5000
61.5
10
147
Surr: Phenol-d6
0.314
0.5000
62.8
1 D
140
Surr: Nitrobenzene-d5
0.401
0.5000
80.2
10
169
Surr: 2,4,6-Tribromophenol
0.335
0.5000
67.0
10
185
Surr: 2-Fluorobiphenyl
0.369
0.5000
73.9
10
169
Surr: p-Terphenyl-d14
0.424
0.5000
84.7
10
179
QC+
m
Sample ID: 17010934-006AMS
SampType: MS
TestCode: svoc-BNA T Units: mg/L
Prep Date: 1/26/2017
RunNo: 64812
Client ID: BatchQC
Batch ID: 25164
TestNo: SW8270C SW3510C
Analysis Date: 1/26/2017
SegNo: 1067892
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Perm it Limit'
E Value above'quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 13 of 29
Page 13 of 35
Summit Environmental Technologies, Inc.ffl, S rr 3310 Win St. SUM 1 K r, Y M V�
�� SUMMARY T�-���m O
C-,td'11,,90N11!Qr=Y1TAL TEU H NO LOGIE% lm.t Cuyahoga Falls, Ohio44223
nn,flrido,,W-LabDrarorres-- TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901
Website: hQ.-II-v!vw.settek.coin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: 25164
Sample ID: 17010934-006AMSD
SampType: MSD
TestCode: svoc-BNA T Units: mg/L
Prep Date: 1/26/2017
RunNo: 64812
Client ID: BatchQC
Batch ID: 25164
TestNo: SW8270C SW3510C
Analysis Date: 1/26/2017
SegNo: 1067893
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene
0.289
0.0800
0.4000
0
72.2
29
112
0.2680
7.47
30
2,4,5-Trichlorophenol
0.463
0.200
0.4000
0
116
53
123
0.4216
9.40
30
QC+
2,4,6-Trichlorophenol
0.458
0.200
0.4000
0
115
50
125
0.4180
9.22
30
2,4-Dinitrotoluene
0.277
0.0400
0.4000
0
69.3
57
128
0.2572
7.49
30
Cresols, Total
ND
4.00
0.8000
0
75.6
20
125
0
0
30
R
Hexachloro-1,3-butadiene
0.396
0.0160
0.4000
0
99.0
22
124
0.3564
10.5
30
Hexachlorobenzene
0.294
0.0400
0.4000
0
73.5
53
125
0.2752
6.61
30
Hexachloroethane
0.262
0.0800
0.4000
0
65.4
21
115
0.2432
7.29
30
Nitrobenzene
0.371
0.0800
0.4000
0
92.8
45
121
0.2620
34.5
30
R
a,
Pentachlorophenol
0.364
0.200
0.4000
0
91.0
35
138
0.3572
1.89
30
Pyridine
ND
0.200
0.4000
0
35.4
10
126
0
0
30
Rm
Surr: 2-Fluorophenol
0.659
1.000
65.9
10
147
0
m
Surr: Phenol-d6
0.656
1.000
65.6
10
140
0
m
Surr: Nitrobenzene-d5
0.870
1.000
87.0
10
169
0
Surr: 2,4,6-Tribromophenol
0.664
1.000
66.4
10
185
0
Surr: 2-Fluorobiphenyl
0.874
1.000
87.4
10
169
0
Surr: p-Terphenyl-d14
0.886
1.000
88.6
10
179
0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 15 of 29
Page 15 of 35
l'
t
Summit Environmental Technologies, Inc.Sum
3310 Win St.
QC SUMMARY REPORT
Csfl:'b�i h5D,7lPhi,^,L'I'Er;HhJ�L��lea,m9�,
71w�dyEia.a�i FJA Lr3f677ies.
Cuyahoga Falls, Ohio44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: httn:/Avmw.sette%co1n
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
BatchID: 25166
Sample ID: mb-25166
SampType: mblk
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 1/26/2017
RunNo: 64828
client ID: PBW
Batch ID: 25166
TestNo: SW8081A SW3510C
Analysis Date: 112612017
SegNo: 1068224
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00500
Toxaphene
ND
0.0100
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
6.000500 d
Surr: TCMX
5.63
10.00 56.3 10 119
Surr: DCB
6.87
10.00 68.7 10 119
Sample ID: Ics-25166
SampType: Ics
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 1/26/2017
RunNo: 64828
:Iient ID: LCSW
Batch ID: 25166
TestNo: SW8081A SW3510C
Analysis Date: 1/26/2017
SegNo: 1068225
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
cnunn
U.U0494
0.000500
0.00500
0
98.8
20
157
gamma-BHC
0.00450
0.000500
0.00500
0
90.0
22
137
Heptachlor
0.00478
0.000500
0.00500
0
95.7
24
121
Heptachlor epoxide
0.00448
0.000500
0.00500
0
89.5
27
152
Methoxychlor
0.00581
0.000500
0.00500
0
116
10
199
Surr: TCMX
6.69
10.00
66.9
10
119
Surr: DCB
7.95
10.00
79.5
10
119
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 16 of 29
Page 16 of 35
Summit Environmental Technologies, Inc.M5 S U tom 1, or 3310 Win St. QC SUMMARY REPORT
GrdJINCrCBP)1�r1 Y� `Pt'_:HPJ LuGIES, WP , Cuyahoga Falls, Ohio 44223
.�ln,nJipaJ4a,� Lsu�,r�fori�$ WO#: 17010901
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: ht(D://wia)w.settek.coin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: 25166
Sample ID: 17010934-006ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 112612017
RunNo: 64828
Client ID: BatchQC
Batch ID: 25166
TestNo: SW8081A SW3510C
Analysis Date: 112612017
SegNo: 1068226
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL]mit Qua[
Endrin
0.00578
0.00100
0.0100
0
57.8
20
157
QMR
gamma-BHC
0.00494
0.00100
0.0100
0
49.4
22
137
QMR
Heptachlor
0.00551
0.00100
0.0100
0
55.1
24
121
QMR
Heptachlor epoxide
0.00555
0.00100
0.0100
0
55.5
27
152
QMR
Methoxychlor
0.00628
0.00100
0.0100
0
62.8
10
199
mQMR
Surr: TCMX
8.17
20.00
40.9
10
119
Surr: DCB
10.5
20.00
52.7
10
119
Sample ID: 17010934-006amsd
SampType: msd
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 1/26/2017
RunNo: 64828
Client ID: BatchQC
Batch ID: 25166
TestNo: SW8081A SW3510C
Analysis Date: 1/26/2017
SegNo: 1068227
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.00978
0.00100
0.0100
0
97.8
20
157
0.00578
51.4
gamma-BHC
0.00852
0.00100
0.0100
0
85.2
22
137
0.00494
53.3
Heptachlor
0.00901
0.00100
0.0100
0
90.1
24
121
0.00551
48.3
Heptachlor epoxide
0.00954
0.00100
0,0100
0
95.4
27
152
0.00555
52.9
Methoxychlor
0.0113
0.00100
0.0100
0
113
10
199
0.00628
57.0
Surr: TCMX
13.9
20.00
69.4
10
119
0
Surr: DCB
18.1
20.00
90.6
10
119
0
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
30 R
30 R
30 Rm
30 R
30 Rm
Original
Page 17 of 29
Page 17 of 35
Summit Environmental Technologies, Inc. Sumfo,
' v 3310 Win St. V1r1
�� SUMMARY REPORT
RNVIHrM11.ltN CH I:S,_Jut Cuyahoga Falls, Ohio44223 An.ad;TEL: (330) 253-8211 FA- (330) 253-4489Ia�WO#: 17010901
Website: http://wmnv.settek.com 10-Feh-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: 25212
mple ID: mb-25212
SampType: mblk
TestCode: tclp�svoc-her Units: mg/L
Prep Date: 1/27/2017
RunNo: 65243
ent ID: PBW
Batch ID: 25212
TestNo: SW8151A SW8151A
Analysis Date: 2/7/2017
SegNo: 1075436
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 1.00 0 0
2,4,5-TP ND 0.500 0 0
Surr: DCAA 423 500.0 84.6 20 140
Sample ID: Ics-25212
SampType: Ics
TestCode: telp-svoc-her Units: mg/L
Prep Date: 1/27/2017
RunNo: 65243
Client ID: LCSW
Batch ID: 25212
TestNo: SW8151A SW8151A
Analysis Date: 2/7/2017
SegNo: 1075437
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D
ND
1.00 0.500
0 99.3
62.6
125
2,4,5-TP
ND
0.500 0.500
0 67.3
52.5
128
Surr: DCAA
405
500.0
81.1
20
140
mple ID: 17010714-001ams
SampType: ms
TestCode: telp-svoc-her Units: mg1L
Prep Date: 1/27/2017
RunNo: 65243
ent ID: BatchQC
Batch ID: 25212
TestNo: SW8151A SW8151A
Analysis Date: 2/7/2017
SegNo: 1075438
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D
ND
1.00 0.500
0 128
37
105 SQMR
2,4,5-TP
ND
0.500 0.500
0 85.4
38
106
Surr: DCAA
639
500.0
128
20
140
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
Page 18 of 35
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 18 of 29
ffJ
S umfarr
Summit Environmental Technologies, 172c.
3310 Win St.
QC SUMMARY REPORT
rdPd'1�,IRrrP,bfl,gENT.^,L'I'EOHt,JCLO,GIES,.INC
f1r10IJ#V00J 0:,9fvear3,r WO&
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.• (330) 253-4489
WO#: 17010901
Website: _http://wivw.settekeom
10-Feb-17
Client:
Synagro, NC 28134
Project:
MtRolly 50-1701
BatchID: 25212
Sample ID: 17010714-001amsd
SampType: msd
TestCode: telp-svoc-her Units: mg/L
Prep Date: 112712017
RunNo: 65243
client ID: BatchQC
Batch ID: 25212
TestNo: SW8151A SW8151A
Analysis Date: 2/7/2017
SegNo: 1075439
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDUrnit Qua]
2,4-D 1.27 1.00 0.500 0 255 37 105 0.638 66.5 30 RS
2,4,5-TP ND 0.500 0.500 0 89.8 38 106 0 0 30
Surr: DCAA 744 500.0 149 20 140 0 S
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J- Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 19 of 29
Page 19 of 35
i SunsnaitEnvironmental Technologies, Inc.M9 QC SUMMARY REPORTSlor 3310 Win St.
Gft4ir�J•cSIr�BPa1 ,1 'PE�HtdmL•�GIE�,7��C Cuyahoga Falls, Ohio44223
=�l��dlr�ead•I:t�f�.ur3r•�rrP�.K TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: http:Uwiviv.settek.coin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: R64598
Sample ID: LCS-R64598
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@21.5C
Prep Date:
RunNo: 64598
client ID: LCSW
Batch ID: R64598
TestNo: SW9045D
Analysis Date: 1/23/2017
SegNo: 1064310
knalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
PH 6.99 7.000 0 99.9 98.6 101.4
Qualifiers: * Value exceeds Maximum Contaminant Level.
H IIolding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 20 of 29
Page 20 of 35
SUM.
SunsmitEnvironmental Technologies, Inc. QC CTTMM�� T T,-,T®�r�,
�. 3310 Win St. C SUMMARY Y REPORT
1
2114111P, o-U9 kMf-1'r,6.L TFCHWLO`IES, 7P9G Cuyahoga Falls, Ohio 44223
:1,nody r�rA,!:sJ�vr3r?ri TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901
Website: http://www.settekcoin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: R64634
Sample ID: LCS-R64634
SampType: LCS
TestCode: FlashPt S(10 Units: °F
Prep Date:
RunNo: 64634
client ID: LCSS
Batch ID: R64634
TestNo: SW1010
Analysis Date: 1/24/2017
SegNo: 1065062
Nnalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Flashpoint (140°F) 84.0 77.00 0 109 100 110
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 21 of 29
Page 21 of 35
Sul mm'Jor
3310 Win St.
SunimitEnvironnientaZTechnologies, Inc.ffl,
QC SUMMARY REPORT
Cw.'laCrrhft`i�hlorL'I'6t;`F1PJ�t�cfi�,,,etJ
.L�otlesfeaJ l:+�LrFeTr.+s
Cuyahoga Falls, Ohio44223
TEL: (330) 253-8211 FAX- (330) 253-4489
WO#: 17010901
Website: http:lAvij,iv.settek.coni
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
BatchlD: R64863
mple ID: 17010805-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 64863
ent ID: BatchQC
Batch ID: R64863
TestNo: SW9014
Analysis Date: 112712017
SegNo: 1068975
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
snide, Reactive 0.990 0.500 1.000 0.1070 88.3 81.6 122
mple ID: 17010805-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 64863
ent ID: BatchQC
Batch ID: R64863
TestNo: SW9014
Analysis Date: 1/2712017
SegNo: 1068976
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive 0.981 0.500 1.000 0.1070 87.4 81.6 122 0.9900 0.913 5
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
Page 22 of 35
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 22 of 29
siulmmAr Suminit Environrnental Technologies, Inc. 3310 Win St.
Q1SUMMARY
U lilY REPORT
TP®`T
�Aa�,�I�OCSP,9PP5'A,L'I'Er;`HPd�[ J.�IL5',.7j9 Cuyahoga Falls, Ohio 44223
+=!n.uSyvirml! Lalaerzjtaries TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901
Website: httn:/Mvivw.sette%com 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: R64863
Sample ID: MB-R64863
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 64863
;lient ID: PBW
Batch ID: R64863
TestNo: SW9014
Analysis Date: 1/27/2017
SegNo: 1068972
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
�yarnde, Reactive ND 0.500
Sample ID: LCS-R64863
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 64863
client ID: LCSW
Batch ID: R64863
TestNo: SW9014
Analysis Date: 1/27/2017
SegNo: 1068973
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
:yanide, Reactive 1.02 0.500 1.000 0 102 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 23 of 29
Page 23 of 35
i
umm
Summit Environmental Technologies, Inc.S
3310 Win St.
QC SUMMARY "PORT
rtNVIR1'1AM1IEI'IULTECHNda]GIB0$,1M Cuyahoga Falls, Ohio44223
Anafyifo-� �LgbDrarcrries TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: http://Wi4�w.settek.cmii
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
BatchID' R64864
Sample ID: 17010805-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 64864
Client ID: BatchQC
Batch ID: R64864
TestNo: SW9034
Analysis Date: 112712017
SegNo: 1068989
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive 2700 25.0 2800 0 96.4 80 120
mple ID: 17010805-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 64864
ent ID: BatchQC
Batch ID: R64864
TestNo: SW9034
Analysis Date: 1/27/2017
SegNo: 1068990
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ifide, Reactive 2840 25.0 2800 0 101 80 120 2700 5.05 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte, detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
Page 24 of 35
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 24 of 29
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
sumow"i-Ir 3310 Win St.
�f�'dlR rP�I,uSh1Y�,�'I'OCHtdd LOGICS, I* Cuyahoga Falls, Ohio 44223 WO#: 17010901
nahe.rsca/ I_aborata ie4 TEL: (330) 253-8211 FAX. (330) 253-4489
Website: http://ivivw.settek.coin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: R64864
Sample ID: MB-R64864
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 64864
Client ID: PBW
Batch ID: R64864
TestNo: SW9034
Analysis Date: 1/27/2017
SegNo: 1068987
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Sulfide, Reactive ND 25.0
Sample ID: LCS-R64864
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 64864
Client ID: LCSW
Batch ID: R64864
TestNo: SW9034
Analysis Date: 1/2712017
SegNo: 1068988
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2740 25.0 2800 0 97.9 85 115
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
Page 25 of 35
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit Original
R RPD outside accepted recovery limits Page 25 of 29
R5
NtSummi
SunamitEnvironmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
UNIRCIN) ; EPITAL TECHN,0LD,t31re, mic
.1.,aa,llagi�a,� LAdawraro�rir:5
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: http:/hvww.settek.coin
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
BatchlD: R64876
Sample ID: 17011296-001ams
SampType: MS
TestCode: telp-voc-mstr Units: mg/L
Prep Date:
RunNo: 65045
Iient ID: BatchQC
Batch ID: R64876
TestNo: SW8260B
Analysis Date: 1/31/2017
SegNo: 1071977
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.208
0.0200
0.200
0
104
39.9
160
1,2-Dichloroethane
0.208
0.0200
0.200
0
104
42.5
157
MEK
1.18
0.100
1.00
0.0206
116
16.6
227
Benzene
0.226
0.0200
0.200
0
113
38.1
155
Carbon tetrachloride
0.215
0.0200
0.200
0
108
40.8
162
Chlorobenzene
0.216
0.0200
0.200
0
108
35.7
168
Chloroform
-0.217
D.0200
0.200
0
109
18.3
199
Tetrachloroethene
0.236
0.0200
0.200
0
118
10
261
Trichloroethene
0.199
0.0200
0.200
0
99.4
23.8
175
Vinyl chloride
0.158
0.0200
0.200
0
79.2
10
165
Surr:4-Bromofluorobenzene
1030
1000
103
84.6
130
Surr: Dibromofluoromethane
945
1000
94.5
71.4
127
Surr: Toluene-d8
967
1000
96.7
74.6
127
Sample ID: 17011296-001amsd
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 65045
;lient ID: BatchQC
Batch ID: R64876
TestNo: SW8260B
Analysis Date: 1/31/2017
SegNo: 1071978
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.198
0.0200
1,2-Dichloroethane
0.207
0.0200
MEK
1.21
0.100
Benzene
0.220
0.0200
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
P
Second column confirmation exceeds
0.200
0
99.2
39.9
0.200
0
103
42.5
1.00
0.0206
119
16.6
0.200
0
110
38.1
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
160
0.208
4.53
157
0.208
0.483
227
1.18
3.20
155
0.226
2.60
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
25
25
25
25
Original
Page 26 of 29
Page 26 of 35
In'SUPAIWI-T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRG-MVIEVIT LTErHPJOC. -DIES, Dfq,
e2,nalyyir-q1 L'c.giv�a s raigr
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 17010901
Website: http:/hvww.settelf.com
10-Feb-17
Client:
Synagro, NC 28134
Project:
Mt.Holly 50-1701
BatchlD: R64876
Sample ID: 17011296-001amsd
SampType: MSD
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 65045
client ID: BatchQC
Batch ID: R64876
TestNo: SW8260B
Analysis Date: 1/31/2017
SegNo: 1071978
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
Carbon tetrachloride
0.210
0.0200
0.200
0
105
40.8
162
0.215
2.26
25
Chlorobenzene
0.212
0.0200
0.200
0
106
35.7
168
0.216
1.97
25
Chloroform
0.217
0.0200
0.200
0
108
18.3
199
0.217
0.369
25
Tetrachloroethene
0.231
0.0200
0.200
0
116
ID
261
0.236
2.23
25
Trichloroethene
0.194
0.0200
0.200
0
96.8
23.8
175
0.199
2.65
25
Vinyl chloride
0.159
0.0200
0.200
0
79.4
10
165
0.158
0.252
25
Surr:4-Bromofluorobenzene
1030
1000
103
84.6
130
0
25
Surr: Dibromofluoromethane
937
1000
93.7
71.4
127
0
25
Surr: Toluene-d8
966
1000
96.6
74.6
127
0
25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 27 of 29
Page 27 of 35
Summit Environmental Technologies, Inc.M5 QC SUMMARY REPORT
svmm�lrr 3310 Win St.
BhttlR�:rt�ItlCt9�s�`I'k�'HPJOSLz�le5fnjk; Cuyahoga Falls, Ohio44223
WO#: 17010901
"1nijJldaea<<LaLvoratel.riE.s TEL:(330) 253-8211 FAX.- (330) 253-4489
Tfehsite: http:11wi4m,.settekcom 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: R64876
Sample ID: les 10ppb L0123/
SampType: LCS
TestCode: telp-voc-mstr Units: mg/L
Prep Date:
RunNo: 64876
Client ID: LCSW
Batch ID: R64876
TestNo: SWB260B
Analysis Date: 112712017
SegNo: 1069233
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.0110
0.00500
0.0100
0
110
79.4
131
1,2-Dichloroethane
0.0107
0.00500
0.0100
0
107
73.6
137
MEK
0.0580
0.0250
0.0500
0
116
55.1
163
Benzene
0.0108
0.00500
0.0100
0
108
73.1
132
Carbon tetrachloride
0.00992
0.00500
0.0100
0
99.2
63.7
139
Chlorobenzene
0.0104
0.00500
0.0100
0
104
72.3
139
Chloroform
0.0108
0.00500
0.0100
0
108
79.3
129
Tetra chloroethene
0.0106
0.00500
0.0100
0
106
56.2
187
Trichloroethene
0.00932
0.00500
0.0100
0
93.2
64.1
138
Vinyl chloride
0.00902
0.00500
0.0100
0
90.2
22.1
147
Surr:4-Bromofluorobenzene
52.7
50.00
105
80.4
126
Surr: Dibromofluoromethane
47.3
50.00
94.5
70.3
125
Surr: Toluene-d8
49.9
50.00
99.9
82
117
Sample ID: mblk
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 64876
-lient ID: PBW
Batch ID: R64876
TestNo: SW8260B
Analysis Date: 1/27/2017
SegNo: 1069234
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
ND 0.100
1,2-Dichloroethane
ND 0.100
MEK
ND 2.00
Benzene
ND 0.100
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O RSD is greater than RSDlimit Original
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Page 28 of 29
Page 28 of 35
msummlor
Sun:mitEnvironmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
CuPd7.'1RirC8P4iLPa� ,L'I'B HPJ4]L�rilE5,.RiJt Cuyahoga Falls, Ohio44223
!areed LsbDrrstario& TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 17010901
. nwa i
Website: htta://ivwiv.settelccoin 10-Feb-17
Client: Synagro, NC 28134
Project: Mt.Holly 50-1701 BatchID: R64876
Sample ID: mblk
SampType: MBLK
TestCode: tclp-voc-mstr Units: mg/L
Prep Date:
RunNo: 64876
:lient ID: PBW
Batch ID: R64876
TestNo: SW8260B
Analysis Date: 1/27/2017
SegNo: 1069234
>nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
0.100
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.200
Surr: 4-Bromofluorobenzene
47.9
Surr: Dibromofluoromethane
51.2
Surr: Toluene-d8
48.4
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding tines for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
50.00 95.9 70
50.00 102 70
50.00 96.8 70
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
130
130
130
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Original
Page 29 of 29
Page 29 of 35
summit. Environni.cutal `Qechnoliaiggics, Inc.
33 10 Win Strecl
Cliyalkaglk Falls, Ohio 44223
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Summit Environmental Technologies, Inc.
Cooler Receipt Form
Initials cf per<_:nn inspecting tooter and samples: �A
Client, -1'1 (r r'J
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Older Numbe: _. >
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ttaio Recel:cd: 1-1 i`t lime Reccived:� �
Dail; coote-rgsf opened and samples inspected:
Nlurnber of cooler5.'soxes: _
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Shipper' ry Ups U}-It ,4irt;ome Us Postal
%galtc-in pickup - Other:
Packaging: Peanuts B •ri,5 Paper
Foam Mc)re tcE--::
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(see rage 2 for eaan results}
'*Use 1 sheet per sample for Radiological Testing. If sample
is HOT, the Radiclog:cal Safety Officer must be notiiled
immediately
G-D-C filled out prep rly
t:1y N
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Samp'es ;n separate U•ats
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sample rontai-Ws intact'
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Bobbies absent frorn 4G nil- vials"
y
N
P,lffR
" Serrip"es ewitn bear eE <6mm are acceptable.
Indicate buLWo snz:' it y6rrm.
VVasclientcontacied_bDutsamples
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VJill client send ncr: samples
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Client coniact:
Logged in
Page 1 of 9
Page 31 of 35
STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL. QUALITY
RESOURCES
WWA
LAB4.®I ATO CE'I TI'F'I.0 TI N '®, NCH
In accordeninvWth the provisions of M.C.G " ' (1J,• 143-215.3 (a)(f0) and MCAC 214.0800:
Summ. it Environmental Technologies., Inc.
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data tO.DEQ for
compCance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H-0800 is made apart of this certificate.
This certificate does not guarantee valldityofdaia generated, butiridldates the methodology, equipment, qualitycontrol procedures,
records, and proficiency ofthe laboratoryhave been 0amined and found to be. acceptable.
This cerfificate shall be valid until, 12131/20�_.7
Certificate No. 631
N�
Dana'B. Sett-;' 4�
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North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631
Address: 3310 Win Street Effective Date: 1/1/2017
Cuyahoga Falls, DH "223- Expiration Date: 12/31/2017
Date of Last Amendment: 1/5/2016
The above he mod laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby cer5fied for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANIC
SILICA
BOD
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SM 5210 B-2001 (Aqueous)
SW-846 6010 D (Aqueous)
CHLORIDE
SULFATE
SW-846 9056 A (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
COD
sW-846 9056 A (Aqueous)
SM 5220 C-1997 (Aqueous)
SULFIDE
FLUORIDE
SW-846 9034 (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
METAL
SW-846 9056 A (Aqueous)
TCLP METALS
INORGANIC PHENOLS
SW-8461311 (Aqueous)
EPA420.1, Rev. 1978 (Aqueous)
ALUMINUM
NITROGEN, NITRATE
EPA 200.7, Rev. 4.4,1994(Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 9055 A (Aqueous)
EPA 200.8, Rev. 6.4, 1994 (Aqueous)
NITROGEN, NITRITE
SW-946 6020 B (Aqueous)
EPA 300.0,. Rev. 2.1, 1993 (Aqueous)
ANTIMONY
SW-846 9056 A (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
NITROGEN, NO3 + NO2
SW-846 6010 D (Aqueous)
EPA 300.0, Rev. 2.1, 1993 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 9056 A (Aqueous)
SW-846 6020 B (Aqueous)
NITROGEN, TOTAL KJELDAHL
ARSENIC
SM 4500 Norg B-1997 (SM 4500 NH3 D-1997) (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
OIL & GREASE
SW-846 601 D D (Aqueous)
EPA 1664 Rev. B (Aqueous)
EPA 20D.8, Rev. 5.4, 1994 (Aqueous)
SW-846 9071 B (Non -Aqueous)
SW-846 6020 B (Aqueous)
PHOSPHORUS, TOTAL
BARIUM
EPA 200.7, Rev. 4.4 (1094) (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6010 D (Aqueous)
RESIDUE, DISSOLVED 180 C
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SM 2540 C-1997 (Aqueous)
SW-846 6020 B (Aqueous)
RESIDUE, SUSPENDED
BERYLLIUM
SM 2540 D-1997 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
RESIDUE, TOTAL
SW-846 6020 B (Aqueous)
SM 2540 B-1927 (Aqueous)
BORON
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penaltL*s �nna.4t1 rlrtitrv�r °u"arIfFGS SaYJs
as set forth In 15A NCAC 21-1.08D7.
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North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631
Address: 3310 Win Street Effective Date: 1/1/2017
Cuyahoga Falls, OH 44223- Expiration Date: 12/31/2017
Date of Last Amendment: 1/5/2016
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0aoo, is hereby certified for the measurement of the parameters listed below
CERTIFIED PARAMETERS
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-84e 6020 B (Aqueous)
MAGNESIUM
CADMIUM
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 5010 D (Aqueous)
SW-846 6IJ10 D (Aqueous)
MANGANESE
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 6D20 B (Aqueous)
SW-846 5010 D (Aqueous)
CALCIUM
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
EPA 2017, Rev. 4.4, 1994 (Aqueous)
SW-846 5020 B (Aqueous)
SW-846 6010 D (Aqueous)
MERCURY
CHROMIUM TOTAL
EPA 245.1, Rev. 3.0, 1994 (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 7470 A (Aqueous)
SW-846 6010 D (Aqueous)
EPA 1631 E (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
MOLYBDENUM
SW-846 6020 B (Aqueous)
EPA 200.7, Rev. 4.4, 1904 (Aqueous)
COBALT
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 20D.8, Rev. 5.4, 19D4 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6020 B (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
NICKEL
SW-846 6020 B (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
COPPER
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 20D.8, Rev. 6.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 6020 B (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
POTASSIUM
SW-846 6020 B (Aqueous)
EPA 200,7, Rev. 4.4, 1994 (Aqueous)
IRON
SW-846 6010 D (Aqueous)
EPA 200.7, Rev, 4.4, 1904 (Aqueous)
SELENIUM
SW-846 6010 D (Aqueous)
EPA 20D,7, Rev. 4.4, 1994 (Aqueous)
LEAD
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4. 1994 (Aqueous)
EPA 20D.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6010 D (Aqueous)
SW-848 6020 8 (Aqueous)
EPA 200.8, Rev, 5.4, 1994 (Aqueous)
SILVER
SW-845 6D20 B (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
LITHIUM
SW-846 6010 D (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 200.8, Rev. 6A, 1994 (Aqueous)
This certification requires malntance of an acceptable quality assurance
as set forth In 15A NCAC 2H,0807.
program, use of approved methodology, and aetlsfactory performance on evaluation samples. Laboratories are subject to civil penalties a�6ror=u3d Beal �n fUrJnP.aePr�P9
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North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Lab Name: Summit Environmental Technologies, Inc. Certificate Number: 631
Address: 3310 Win Street Effective Date: 1/1/2017
Cuyahoga Falls, OH 44223- Expiration Date: 12/31/2017
Date of Last Amendment: 1/5/2016
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
r
CERTIFIED PARAMETERS
SW-846 6020 B (Aqueous)
CHLORINATED PHENOLICS
SODIUM
EPA 1653, Rev. A, 1997 (Aqueous)
EPA 200.7, Rev, 4.4, 1994 (Aqueous)
EXTRACTABLE PETROLEUM HYDROCARBONS
SW-846 8010 D (Aqueous)
MADEP, May 2004, Rev. 1.1 (Aqueous)
STRONTIUM
NONHALOGENATED VOLATILE, ORGANICS
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
SW-846 801B C (Aqueous)
SW-846 8010 D (Aqueous)
PESTICIDES, ORGANOCHLORINE
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
EPA 808 (Aqueous)
SW-846 6020 B (Aqueous)
SW-846 8081 B (Aqueous)
THALLIUM
POLYCHLORINATED BIPHENYLS (PCBs)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
EPA 608 (Aqueous)
SW-846 6010 D (Aqueous)
SW-846 8082 A (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
PURGEABLE, ORGANICS
SW-846 5020 B (Aqueous)
EPA 624 (Aqueous)
TIN
SW-846 B260 B (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
TOTAL ORGANIC HALIDES
SW-846 6D10 D (Aqueous)
SW-846 9020 B (Aqueous)
VANADIUM
TPH DIESEL RANGE, ORGANICS
EPA 200.8, Rev. 6.4, 1994 (Aqueous)
SW-846 8015 C (Aqueous)
SW-846 6020 B (Aqueous)
TPH GASOLINE RANGE, ORGANICS
ZINC
SW-846 8015 C (Aqueous)
EPA 200.7, Rev. 4.4, 1994 (Aqueous)
VOLATILE PETROLEUM HYDROCARBONS
SW-846 6D10 D (Aqueous)
MADEP, May 2004, Rev. 1.1 (Aqueous)
EPA 200.8, Rev. 5.4, 1994 (Aqueous)
SW-846 6020 B (Aqueous)
ORGANIC
TCLP ORGANICS
SW-846 1311 (Aqueous)
ADSORBABLE ORGANIC HALIDES
EPA 1650, Rev. C, 1997 (Aqueous)
BASE NEUTRAUACID, ORGANICS
EPA 625 (Aqueous)
SW-846 8270 D (Aqueous)
a
CHLORINATED ACID HERBICIDES
SW-846 8151 A (Aqueous)
This certification requires maintenes of an acceptable quality assurance program, use of approved methodology, and satisfactoryperformance on evaluation samples. Laboratories are subject to civil penalties w4,br deca,,d,'m qn Par h11==j:k
asset forth In 15A NCAC 2H,0807.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 01/01/17 To 03/31/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative perlormed Mass
A or Mass 13 corn fete the ionowing momtorm
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
Coliform
power per gram
MPN
MPN/g
event
sludge
SM9221E
of total solids
CFU
57,000
88,376
1,000,000
CFU/g
Event
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Mt. 5
Option/Alt. 6
Option/Alt. 7
Option/Mt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying - Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification i c udinE5:4Laqq
fine and imprisonment."
Doug Shoutd / ORC g5
Pre er me d Title pe or print) Land p r N�d Title (if applicable) (type or print)
11 �UFl
S ature fPrep arer* Date Si antDated`Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Case Narrative '
•_=''_:: ,, NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735 01/19/2017
M I Environmental Solutions SC Certification No. 99012
BORATORIES, INC.
Synagro
Clay Fisackerly
12701 Lancaster Hwy.
Pineville, NC 28134
Project: 2017 Production
Lab Submittal Date: 01/17/2017
Prism Work Order: 7010215
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative dotes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P,O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Sample Receipt Summary
Full -Service Analytical & !�
S Environmental Solutions 01/19/2017
YY ORATORIE$ ING
Prism Work Order: 7010215
Client Sample iD
Lab Sample ID
(Matrix
Date Sampled
Date Received
Mt. Holly 50-1701
7010215-01
Solid
01/17/17
01/17/17
Mt. Holly 50-1701
7010215-02
Solid
01/17/17
01/17/17
Mt. Holly 50-1701
7010215-03
Solid
01/17/17
01/17/17
Mt. Holly 50-1701
7010215-04
Solid
01/17/17
01/17/17
Mt. Holly 50-1701
7010215-05
Solid
01/17/17
01/17/17
Mt. Holly 50-1701
7010215-06
Solid
01/17/17
01/17/17
Mt. Holly 50-1701
7010215-07
Solid
01/17/17
01/17/17
Samples were received at 13.9 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 -Toll Free Number. 1-8001529-6364 - Fax: 7041525-0409
r:
r , M
LABORATORIES, INC.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagro
Sample DatelTime Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: 704/529-6364
Fax: 704/525-0409
Project Name: Mt. dolly 50-1701
1/17/17 10:15 Project ID: Mt. Holly 50-1701 1st Event
1/17/17 12:20 COC Group: 7010215
Prism
Sample
ID
Client
Sample ID
Fecal Coliforifi ifi
Sollds(cfulg)
SM9222 D
Reporting
Limit
% Solids SM2640 G
Analysis DatelTime
7010215-01
Clariant Corp.
61000 A
61000
1.65
1/17/17 12:25
7010215-02
Clariant Corp.
1000.000
57000
1.74
1117/17 12:25
7010215-03
Clariant Corp.
58000 A
58000
1.73
1117/17 12:25
7010215-04
Clariant Corp.
60000 A
60000
1.66
1117117 12:25
7010215-05
Clariant Corp.
57000 A
57000
1.76
1117/17 12:25
7010215-06
Clariant Corp.
60000 A
60000
1.66
1117117 12:25
7010215-07
Clariant Corp.
58000 A
58000
1.73
1117/17 12:25
WiN[�Tl
Prism Sample ID: 7010216
Note: All results are reported on a dry -weight basis.
Geometric Mean: 88376 cfu/g
Reporting Limit: 58696
A: The result is less than the reporting limit. At the request of the client, the value reported equals the value of the reporting lin
12
Data Reviewed By: � r, '�/�j?'rr� �(`Project Manager: C. Rusmisell
Review Date: 1-19-17 Approval Date: 1-19-17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
,)
07
Full -Service Analytical &
Environmental Solutions
LA130RATORIES, INC.
449 Springbrook Road - Charlot4e, NC 28217
Phone 7041529-6364 n Fax: 704/525-0409
Client Company Name: S_'c��•fi veJ
Deport To/Contact Name:
Roiling Address:
((ne'yitif, a
Phone. til' --LI- ,29t Fax (Yes) h9a
Ernail Address:
EDD Type: PDF r�EXcel_Other
Site Location Name:
Site Location Physical Address:
TIME
MATRIX
CLIENT
DATE
COLLECTED
(SOIL,
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
HOURS
SLUDGE)
PAGE �A, ou: L nuo-rE a To ENSURE PROPER BILLING-
ProjectName: Wlt %ADV�m 5 ,—�'U 31
Short Hold Analysis: (Yes) (N®) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 I1 11I IV)
provisions and/or QC Requirements
Invoice To:
Address.
Purchase Order Mo./Billing Reference C1 ��=I 1'tt TO OBE FILLED IN EV CLIENT/SAMPLENG PERSONNEL
Requested Due Date ® 1 Day 0 2 Days ® 3 Days ® 4 Days E3 5 Days Certification: NELAC Doa FL IBC A
"Working Days" 0 6-9 Days ® Standard 10 days ® Rush ork dust Be Sc OTHER
NIA
Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO `ij
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection. YES �L MO
SAMPLE CONTAINER • ANALYSIS REQUEST�D PRISM
PRESERVA-
*TYPE NO. SIZE TIVES
SEE BELOW
�1 4
.1-
U
Sampler's Signature 'UM. + • �. U °P ) � Sampled By (Print Name) L.VW 11 c;-� ' Itt Affiliation s .
Upon relinquishing, this Chain of Custody is your A thoriaation for Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINSTJOeUNTIL RECEIVED AT THE LABORATORY.
D Fed Ex ❑ UPS ❑ Hand -delivered O Prism Field Service O Other
IOUTER IATER E1NC ®SLANDFILL
® NC ® SC El NC ® SC © NC ® SC ® NC D SC ® NC ® SC2 ®SCNCC I ® N® SCI ® NC ® SC
® -I ®
*CCNTa rYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined /OA = Volatile Organics Analysis (Zero Head Space)
REMARKS LAD
ID NO.
Additional Comments:
0,fy�
'Ur1—e
,t
Site ]je ° partUrw T11Ylp I' �
C)RICINAI_
PA
PRO mPT- Ao:u,ame.szAecE
LABOP—A-TORIES,INC
W� N : R! : s 0,*%l
2722R2 2y awAE23Es
Attn: c2 FISACKERLY
SYRAc 0
127e1 LANCASTER HWY
2IR IEEE, K2 28134-
>. ! T K»2E: JAN l;
TE: 02Z22Z17
S 2c2 MATRIX- scSE NUMBER- 2e32
_DA7E S242cz»- 01/17/17 . TIRESAMPLED- 1030
.m2 zs7N p- 01/17/ 7 Kyt32 C1 RECETV - DJ
I:Mz RECEIVED- 1242 DETTv22ED BY- 2a PE SAMPLE- Grp
Page l o£ 1
ANALYSIS
to DAY BENCH SCALE ?Es
2KatYSis
K y 2r 1 TI2E BY RESc1T UNITS
R 01/17z17 RE ATTACHED
LABORATORY DIRECIPOR�� \� & •�.
P.O. Box $lga•Cbr.t NC226Q 483
ebw:(m%588 2.Fax: E+12&g
RALF:Z
PROMPT•ACOU RATE•RE LIABLE
LABORAT®R.IES, INC
WWW.RARLABS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
■ CITY OF MT HOLLY 1ST EVENT
• 126327
• ■ • 01/17/17
■ ■ • 02/14/17
Start: End:
TS (9)
0.2476
0.2405
TS%
1.72%
1.74%
VS ()
0.1877
0.1786
VS%
75.81%
74.26%
I N
0.005059
OUT
0.00488903
FSVR Mass Balance)
3.37%
FSVR (Van Kleeck)
7.92%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: (704) 588-8333 0 Fax: (704) 588-8335
PAR
L4BORATORIES, INC.
www.pariabs.com ,
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone (704) 588-8333
Fax (704) 588-8335
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc, and the North
-..11.... n.......i........ -1 C...d...n......,1..t —A KI-i I Dunn .
Company Name (billing)
SYNAGRO CENTRAL
Comments/ Special Instructions
6'Rcl u _to, dgl
i"A�u e\xn" ,<` ca v 7" �ICRS
�c�k � be C�4��d to ,
9620
Address
12701 LANCASTER HWY
City, State Et zip code
PINEVILLE NC 28134
Point of Contact Et Telephone Number Claq FISQcwL
Sample
Taken By: SIGNATURE a�L� PRINTED NAME CIG �'i�`�
ARE SAMPLES FOR STATE or EPA REPORTING? YES (ENO
'`Sample Type: DW ww GWMW HW Soil Other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (YIN): Oechlorination Necessary (Y/N):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Datemme
Collection
DateMme
Analyses
Requested
CIN ac W. HD114 14814ffa
403(DI�
�eocj�
Scale-u es;h®n
ReligQylshed by: uate! 1 ime rcecenrea ate/ i ime
Relinquish by: J Daterrime Received by: Daterrime
" C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste —See
Other Side
ANNUAL .PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 04/O1/17 To 06/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
lI appiicaDie ro atternauve periormea l.lass
A or t-iass 15 com lere Lne ionowing monnOrm
aaia:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6
Coliform
power per gram
NUN
MPN/g
event
sludge
SM9221E
of total solids
CFU
420,000
439,869
450,000
CFU/g
Event
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Mt. 6
(Alk Stabilization)
Option/Mt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench) X
Option/Alt. 7
(Drying —Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction .
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statem ent attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the informatiori used to determine that the ppathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification*cludin fine and imprisonment."
DougShoutd / ORC I �/� y�MAM
Prep er N. me Title e o mt) Land rier Naml6and Title (if applicable) (type or print)
Si re of reparer* Date Si of Land Applier (if applicable) ate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
A RR� S M
LABORATORIES, INQ
Synagro
Clay Fisackerly
12701 Lancaster Hwy.
Pineville, NC 28134
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: 2017 Production
Lab Submittal Date: 05/08/2017
Prism Work Order. 7050126
0511012017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P,O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529.6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409
AFull-Sti
� S Environmenvicetal
Analytical s
,ARM Environmental Solutions
✓r L aowom Es, WC.
Sample Receipt Summary
05/1012017
Prism Work Order: 7050126
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Mt Holly 2nd Event - 1
7050126-01
Solid
05/08/17
05/08/17
Mt Holly 2nd Event - 2
7050126-02
Solid
05/08/17
05/08/17
Mt Holly 2nd Event - 3
7050126-03
Solid
05/08/17
05/08/17
Mt Holly 2nd Event - 4
7050126-04
Solid
05/08/17
05/08/17
Mt Holly 2nd Event - 5
7050126-05
Solid
05/08/17
05/08/17
Mt Holly 2nd Event - 6
7050126-06
Solid
05/08/17
05/08/17
Mt Holly 2nd Event - 7
7050126-07
Solid
05/08/17
05/08/17
Samples were received in good condition at 5.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364-Toll Free Number. 1-800/529-6364 -Fax: 7041525-0409
QM
BORATORIES, INC.
. . . . . . . . . . . . . . . .
NC Certification No. 402
SO Certification No. 99012
NO Drinking Water Cart. No. 37735
Client Name: Synagro
Sample Date/Time Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P.O. Box 240543
Charlotte, NO 28224-0543
Phone: 7041529-6364
Fax: 704/525-0409
Project Name: City of Mt. Holly
5-8-17 09:20 Project ID: Mt. Holly 2nd Event
5-8-17 10:10 COC Group: 7050126
- Prism
Sample
ID
Client
Sample ID
Fecal iff oliform in
Sollds(cfulg)
SM9222 D
Reporting
Limit
% Solids SM2540 G
Analysis Date/Time
7050126-01
MtHolly 2nd Even i
420000 A
420000
2.40
5-8-17 12:00
7050126-02
Mt Holly 2nd Event
450000 A
450000
2.24
5-8-17 12:00
7050126-03
Mt Holly 2nd Even
430000 A
430000
2.30
5-8-17 12:00
7050126-04
Mt Holly 2nd Event
440000 A
440000
2.28
5-8-17 12:00
7050126-05
IMt Holly 2nd Event
450000 A
450000
2.23
5-8-17 12:00
7050126-06
IVIL Holly 2nd Event
440000 A
440000
2.26
5-8-17 12-00
7050126-07
Mt. Holly 2nd Even
450000 A
450000
2.23
5-8-17 12:00
Geometric Mean Calculation:
Prism Sample ID.- 7050126 Geometric Mean: 439889 A cf u/g
Reporting Limit: 439869
Note: All results are reported on a dry -weight basis.
A: The result is less than the reportiV0, limit. At the request of the client, the value reported equals the value of the reporting
limit.
Data Reviewed By: e. Project Manager: C. Rusmisell
Review Date: 5-10-17 Approval Date: 5-10-17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
r;q•,trr�•; ,'C "'•'r' .'I{;
@r HARN OF CUSTOW®Y RECORD
:•I; I
Full -Service Analytical &
Environmental Solutions
�t LABORATORIES, INC.
iS'
449 Springbrook Road • Charlotte, NC 28217
Phone 7041529-6364 • Fax: 7041525-0409
Client Company Name: C")- i%�r4.)
Reporrd To/Contact Narrte:
Report! ng� Address: v--1 I CR-0 z_,t u• r _
P106Q i, U-e_ 00,:2,0
PAGE 0 OF _ QUOTE 9 TO ENSURE PROPER BILLING:
Project Name:0AL 4i W 6—HdO
Short Hold Analysis) (Yes) (Noy' -1JST Project: (Yes) (NO)
*Please ATTACH any Oroject specific reporting (QC LEVEL 1 1l I11 IV)
provisions and/or QC Requirements
Invoice To:
Address:
Phone: .,- 1r ax (Yes)
Purchase Order No./Billing Reference TO BE FILLED IN BY CLIEN ISAMP@ LNG PERSONNEL
(Email Address: n
J r G�6$�r Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days O 5 Days Certification: N�L�yC ®®®
FL NC
EDO Type: PDF k Excel ® r
yp _
—,
Rush Work Must Be
"Working Days" ❑ 6-9 Days ❑Standard 10 days ❑ pp SC OTHER
Pre -Approved
NIA
�/.I �,� p
Site (Location Name: . 9�r 1'� o-_I¢ rQ Y%
d i Samples received after 14:00 will be processed next business day.
NO
Slte Location Physical Ad ess:
�— Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Upon Collection: YESlj'`
//���
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
—
TIME
MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTS®
(SOIL, PRE' REMARKS LAB
SAMPLE DESCRIPTION COLLECTED MILITARY
WATER OR 'TYPE TIVE5
NO. SIZE
ID NO.
HOURS
SLUDGE) SEE BELOW
y
y
I CIE
F--ece
C,jN-Cvv
9Vl_0
'
Li
Oki
o
1✓�cr�.r
�
L
Ing 9-
a
�_- �p
S fa
Sampler's Signature
ei pled By (Print Name) 6-,.N la Affiliation ward'
Upon relinquishing, this Chain 9f Custody is your aut
rization for Prism to proceed wlth06e analyses as reque ed above. Any changes must
I o
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
a
Rel'rt�uj hed By: (Sign re)
Received B Si nature Date Military/Hours
y: (Signature) ) Additional Comments:
'
Stt�Airhial Tltiie I `, '
Rellnq fished : (Signature)
Received By: (Signature) Dale
I 7 ( rjr r
5ttefp�pdrture-Tlrn"d - `"'=°
Relinquished By: (Signature)
Received ForPrism�L bdraidrle,, Data
FIEfdTeC(1 F}3e rr rr '
t 01y111eao
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUS� Y SEALS FOR TRANSPORTATIONTO THE LABORATORY. COG Group No.
r ,r
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service ❑ OtherNPDES:
UST: DRINKING CERCLA ILL OTHER:
ASC E. PO
C®SCI ®NC ®SC ❑ NC ❑ SC 9
❑ NC-0 SC 1
®S4ICUATER. I NC ®LID
NC I fRC ®SC I NC SC SC NC ®SC
®NC
®
AI
*CONW TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined /OA = Volatile Organics Analysis (Zero Head Space)
p &ANK
PROM PT•ACCLIRATE• RELIABLE
11A33(:)3ZA-F0P,I:ES, IWC
WW%V.PARLABS.CU1Ni
REPORT OF ANALYSES
Attn: CLAY FISACKERLY
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: MAR 17
DATE: 05/01/17
SAMPLE NUMBER-
127107
SAMPLE ID- MT.
HOLLY
SAMPLE MATRIX- SO
DATE SAMPLED-
03/29/17
TIME SAMPLED- 1030
DATE RECEIVED-
03/29/17
SAMPLER- CF
RECEIVED BY- DJ
TIME RECEIVED-
1213
DELIVERED BY-
CF
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD
DATE
TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST
VAR
03/29/17
RE ATTACHED
LA30RATORY DIRECTOR--
P.O. Box 411483 • Charlotte, NC 28241-1483
Phoric: (704) 588-8333 a Fax: (704) 588-8335
PAAF;Z
PROM PT•ACCU RATE•RELIAOLE
LABORATORIES, INC
WWW.PARLABS.COM
30 ®ay Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
MOUNT HOLLY
127107
• 03/29/17
l a • 04/26/17
Start: End:
TS g
0.2120
0.2117
TS%
1.83%
1.83%
VS g)
0.1655
0.1613
VS%
78.07%
76.19%
N
0.005064
yOUT
0-00493843
FSVR (Mass Balance)
2.48%
FSVR Van Kleeck)
10.08%
FSVR Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone; (704) 588-8333 • Fax:(704):88-8335
P Am,
AR
PROMPT•ACCU RATE• RELIABLE
LABORATORIES, INC
W W W.PARLABS.COM
Crucible
Tare Wt (g)
Sample(g)
Dried Wt(g)
Burned Wt(g)
TS%
VS%
30 ®ay Bench Scale Extended Aeration Vest
Percent Volatile Solids Reduction
SYNAGRO
■ MOUNT HOLLY
127107
■ • 03/29/17
■ ■ • 04/26/17
As Received Day 0 Day 7 Day 14 Day 21 Day 28
nz»0117 nA1n-117 nd/12117 nd/19/17 04/26/17
X28
X28
X24
X29
X30
X28 -
21.0947
21.0947
21.2216
28.7940
32.4196
21.0948
32.1745
32.6814
32.8792
39.1226
43.8166
32.6622
21.3853
21.3067
21.4338
28.9809
32.6293
21.3065
21.1412
21.2708
28.8374
32,4687
21.1452
2.62%
1.83%
1.82%
1.81 %
1.84%
1.83%
78.07% 1,
76.81%1
76.78%1
76.59%1
76.19%
0.005064043
x
0.001422828
TS )
0.212
VS
0.1655
Volatile Fraction In: 0.42666
P.O. Box 411483 s Charlotte, NC 28241.1483
Phone: (704) 588-8333 a Fax- (704) 588.8335
0.00493843
x
0.001543068
TS
0.2117
VS (
0.1613
Volatile Fraction Out: 0.41632
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
DRAIN OF CUSTODY
PAR Laboratories, Inc
Phone (704) 588-8333
Fax (704).588-8335
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Company Name (bitting)
Comments/ Special Instructions
?CM 182&
°�z Soles
oe1
4V\11 2--�'v r'r
Sh\Ojka \:�k
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State Et zip code
PINEVILLE NC 28134
Point of Contact @ Telephone Number
CLAY FISACKERLY 704-574-5291
Sample
Taken By: SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? Y,ES NO
*Sample Type: DW Wyy GWMW HW Soil other 131&kl
Sample Temp at time of sampling: 0 C Sample Temp upon receipt: ° C
**Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (Y/N): Dechlorination Necessary (YIN):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
DatelTime
Collection
Date/Time
Analyses
Requested
"tY1�, t-lolly
,�
3-a9 _/ 3a
Kei
Rel
0
Received by:
Date(fime
—Zy l
* C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See
Other Side
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 07/01/17 To 09/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitorinjZ data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6
Coliform
power per gram
MPN
MPN/g
event
sludge
SM9221E
of total solids
CFU
560,000
628,770
700,000
CFU/g
Event
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
0ption/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench) X
Option/Alt. 7
(Drying —Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certificati ' chiding ine and imprisonment."
-DougShoutd / ORC ��
Pre er ame Tit type or print) Land ,�pl' r Name dZd Title (if applicable) (type or print)
2-J%
giKature f reparer* Date Si o and Applier (if applicable) date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
NC Certification No. 402 Case Narrative
IFull Service Analytical & NC Drinking Water Carl No. 37735 06/19/2017
Environmental Solutions SC Certification No.99012
MORATORIES,II\O.
Synagro
Clay Fisackerly
12701 Lancaster Hwy.
Pineville, NC 28134
Project: 2017 Production
Lab Submittal Date: 06/15/2017
Prism Work Order: 7060323
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 _
Phone: 7041529-6364 -Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
E IS I Fullironmee Analytical s
Environmental Solutions
Sample Receipt Summary
06/19/2017
r_
Prism Work Order: 7060323
Client. Sample ID Lab Sample ID Matrix Date Sampled Date Received
Mt Holly 3rd Event - 1
7060323-01
Solid
06/15/17
06/16/17
Mt Holly 3rd Event - 2
7060323-02
Solid
06/15/17
06/15/17
Mt Holly 3rd Event - 3
7060323-03
Solid
06/15/17
06/15/17
Mt Holly 3rd Event-4
7060323-04
Solid
06/15/17
06/15/17
Mt Holly 3rd Event - 5
7060323-05
Solid
06/15/17
06/15/17
Mt Holly 3rd Event - 6
7060323-06
Solid
06/15/17
06/15/17
Mt Holly 3rd Event - 7
7060323-07
Solid
06/15/17
06/15/17
Samples were received in good condition at 3.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409
..._<....41'.'-•.__-- '-'] v--..--�:._._... ��-.o-+--�.ec-_-.:e'.' - t._ti'+_.__:'.-�_�.:«e »C:e'..am,:v:'i.R� _„_•-d w_ n-.... ^.. ..-_.-v .._ .. ..... aaa_.�-- _. Y-�.-.... , . � - - •-__^nw •....t ..
AI I AR0RAT0RIE S, INC.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagro
Sample Date/Time Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P..O. Box 240543
Charlotte, NC 28224-0543
Phone: 704/529-6364
Far,: 704/525-0409
Project Name: City of Mt. Holly
6-15-17 10:01 Project ID: lint. Holly 3rd Event
6-15-17 11:10 COC Group: 7060323
rBsi
Sample
ID
Client
Sample ID
eca C®i orm In
Solids(cfu/g)
SM9222 D
Reporting
Limit
% Solids SM2540 G
Analysis Date/Time
0323-01
Mt Holly 3rd Event
560000 A
560000
1.80
6-15-17 15:08
0323-0
L
Mt. Holly 3rd Event
610000 A
610000
1.65
6-15-17 15:08
7060323-03
Mt. Holly 3rd Event
620000 A
620000
1.60
6-15-17 15:08
7060323-04
Mt. Holly 3rd Event
630000 A
630000
1.59
6-15-17 15:08
7060323-05
Mt. Holly 3rd Event
650000 A
650000
1.53
6-15-17 15:08
7060323-06
Mt. Holly 3rd Event
700000 A
700000
1.42
6-15-17 16:08
7060323-07
Mt Holly 3rd Event
640000 A
640000
1.57
6-15-17 15:08
Geometric Mean Calculation:
Prism Sample ID: 7060323 Geometric Mean: 628770 A cfu/g
Reporting Limit: 628770
Note: All results are reported on a dry -weight basis.
A: The result is less than the reporting limit. At the request of the client, the value reported equals the value of the reporting
limit. ;
Y B
Data Reviewed By: t?I'ojectManager: C. Rusmisell
Review Date: 6-19-17 Approval Date: 6-19-17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, lne.
.. � �`.i'1!,_fJ:1:r:r.:l:lYi•rv...r:J:!:...,.J....-....J.J.rJJ.J.1.L._J.. JJ�J.......v_...r�......._._.�......_.._....................�,_u+..u�v.w...u.a�.u�.u.u.ulr.w_rJJ..ul.,.r.ua.f.�u�_,..,���i,��_r.r���.�.r_riw��.ria��,�.u��.r��.u.r.r���siui.u.�..rye.r_..y..,_�..._�y..--_r_�W..�...J .+.�ri.r_�...LL��ur—..r_
r
Full -Service Analytic al &
Solutions
Environmental
n � ��IY ��'ti ',.r''LA130RATOnIrS,1INC.
449 Sgringbr•ook Road ^ Charlotte, NC 282.17
Phone 704/529-6364 ° Pax: 704/525-0409
Client Company Name: � dL
Report To/Contact Name:
Reporting Address: _ , � a;IL-ke
p
1011152512111
II S+.., alp • �'ee�� ski w.
PAGE OF _L QUOTE IfTO ENSURE PROPER 131ILLIe NG
Project Namne: WW ail V U
Short Hold Analysis: (Yes) o) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111 111 lV)
provisions and/or QC Requirements
Invoice To:
Address:
Plane afl 11ll Fax (Yes) :
Purchase OrderNo.1SII1ing Reference
TO BE FILLED IN BY CLBE1e9TISAMPLING PERSONNEL
Email Address: L���'� ���� � a ��-�
-�---�'�'
' � �'° Requested Due Date ® 1 Day ® 2 Days D 3 Days ® 4 Days ® 5 Days
Certification:
NELAC ®®® VcL It9C
EDD Type: PDF�Excel Othper
"Working Days" ® 6-9 Days ® Standard 10 days ® RushrWork Mdust Be
Sc OTHER MIA
Site Location Name: W±1 W011 l
Samples received after 14:00 will be processed next business day.
Site Location Physical Address'
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated:
YES— NO_. Z.
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
CC,,,,��
Sample Iced Upon C®Ilecti®n: YES Y- NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
N
ID NO.
HOURS
SLUDGE)
SEE BELOW
p
i
�y
�o
ppp
m
U b c, �
Ijf{
0
�rL
Eispr
Sampler's Signature ��✓
Sampled By (Print Name) a£ f iP es�(— Affiliation
Upon relinquishing, dais Chain Af Custody is your a
rizatlon for Prisms to proceed with the analyses as requested above. Any change?muskad;
for
r 11
submitted in Writing to the PrismProject Manager.
There wiil be charges any Changes after analyses have been Initialized.
11Li uP� J�rs�
Relinquished B':Vii", ture) H
Received By: (Signature) Date Military/Hours1r❑
Additional Comments: 51§�%AtFival Time
Relinquished By: (Signs re)
Received By: (Signature) Date
SI{(3 )o�arfll)(jfitrp�,¢
r I r
NMI
Relinquished By: (Signature)
Received For Is Lab o des By: Date J' r
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT IN T LS STODY SEAFOR TRANSPORTATION TO THE LABORATORY. COC Gr up No.
i- t - -�
SAMPLES ARE NOT ACCEPTED AND VERIFIED
AGAINST Cbd UNTIL RECEIVED AT THE LABORATORY.
0 "°��� � �•
O Fed F�c Q UPS ❑ Hand -delivered ❑Prism Field Service
❑Other
NPDES: UST: GROUNDWATER:
DRINKING WATER: SOLID WASTE: RCRA: C%CLA LANDFILL OTHER:
❑NCQS.0 ®NC ®SC ®NC ©SC
®NC ®SC ANC ®SC ®NC®SCI ANC 35C ®NC ®SC ®NC ®SC
'
rrlrtrat
*CONTAI YPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined C DA = Volatile Organics Analysis (Zero Head Space)
PAR
PROMPT•ACOU RATE- RELIABLE
IAgORA'I'ORIRS' Il`TC
WWW.PARLABS.COM
REPORT OF ANALYSES
Attn: CLAY FISACKERLY
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: JUN 17
DATE: 07/18/17
SAMPLE NUMBER- 127966 SAMPLE ID- MT. HOLLY 3RD EVENT
DATE `SAMPLED- 06/15/17
DATE RECEIVED- 06/15/17 SAMPLER- CF
TIME RECEIVED- 1138 DELIVERED BY- CF
Page 1 of 1
ANALYSIS
30 DAY BENCH SCALE TEST
ANALYSIS
METHOD DATE TIME BY
SAMPLE MATRIX- SO
TIME SAMPLER- 1012
RECEIVED BY- DJ
TYPE SAMPLE- Pumped
RESULT UNITS
VAR. 06/15/17 1315 RE ATTACHED
LABORATORY DIRECTOR r_. =fir •� - C�., _
g P.O. Box 411483 e Charlotte, NC 28241-1483
Phone: (704) 588-8333 - Fax: (704) 588-8335
pb- L
PROM PT-A000 RATE. RELIAB L-E:
I,ABOPCXCIPCEES, UITC
WWW.PAR!_ASS.COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
N F
S1]���t14��1ppPWE Ili � � � � �z � � �MT
HOLLYR D EVENT
Start: End:
TS (9)
0.2096
0.2062
TS%
1.95%
1.94%
VS (g)
0.1624
0.1561
VS%
77.48%
75.70%
ylN
0.005039
yOUT
19.00486191
FSVR (Mass Balance)
3.51 %
FSVR (Van Kleeck)
9.45%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <16%
YES
1?o. Box411483 * charlotte,NC28241-1483
Phone: (704) 588-8333 • Fax: (704) 588-8335
r ."
PL.),k
PROMPT•AGCi] RATE- R ELIA81-E
1,ABORATORIES, INC
W W W.PARLABS.COM
Crucible
Tare Wt (g)
Sample(g)
Dried Wt(g)
Burned Wt(g)
TS%
VS%
34 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
SAMP1 E 1D :MT HOLLY
SAiVIPL.E # � i�
3M
�STAfLT DATA � �
As Received Day 0 Day 7 Day 14 Day 21 Day 28
AaMGl.97 na/11114 7 nA19Q147 07/06147 07/13/17
X9
X26
X15
X24
X9
21.4804
20.8652
21.9479
22.0096
21.4798
32.2307
31.8612
33.9042
33.0071
32.1067
21.6900
21,0818
22.1763
22.2252
21.6860
_ . _
21.5276
20.9163
22,0025
22.0617
21.5299
##DIV101
1.95%
1.97%
1.91%
1.96%
1.94%
77.48%1
76.41%1
76.09%1
75.83%1
75.70%
0.005038674
x
0.001464442
TS )
0.2096
VS (
0.1624
Volatile Fraction In: 0.39733
P.O. Box411483 • Charlotte, NC 28241-1483
Phone: (704.) 588-8333 • Fax: (704) 588-8335
gftG22mg
0.004861914
x
0.001560422
TS
0.2062
VS
0.1561
Volatile Fraction Out: 0.39021
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone (704) 588-8333
Fax (704),588-8335
Shipping-, Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carolina Department of Environmental and Natural Resources.
Company Name (bitting) Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State if zip code Q, S('}' j�� �� ek,
PINEVILLE NC 28134 Ao Cedl}c-,& b-doio
Point of Contact Et Telephone Number
CLAY FISACKERLY 704-574-5291����
Sample
Taken By: SIGNATURE PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES �/ NO
*Sample Type: Dw Ww GWMW HW Soil Other ►
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
*"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No nla
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Daterf rime
Collection
Date/Time
Analyses
Requested
iY1�. l olly 30-.I)CXL) fan '
t �i
! 0 -WA3 &0
V11
Kelln i eo py: uatel I ime Recelvea by'! f' j uate/ I Ime
466
Relinquish d y: Date/Time Received by: y ( DateMme
* C=Composite G=Grab DW=Drinking Water WW=Wastewater GWIAW=Groundwater Monitoring Well HW=Hazardous Waste **See
Other Side
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 10/01/17 To 11/30/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment ThermophiIic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf annlirnhir to altPrnnfiva narfnrmPA Wlgcc A nr C'Incc R) rmm�ia+a +ha f.U.- — m ,+nri I. +.,-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 ffi
Coliform
power per gram
MPN
MPN/g
event
sludge
SM9221E
of total solids
430,000
536,950
610,000
CFU/g
Event
sludge
SM92221)
CFU
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 NTN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Ation/Alt. 1
Option/Alt.2
Option/Alt 3 Option/Alt.4
reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying— Stable) (Drying— Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
T "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment"
Doug Shoutd / ORC
Preparerilame an -Title (type or print)
4igenaturoffreparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 2T.1102 (26)
�.P'11�72-_;I
.e-� BORATORIES, INC.
Synagro
Adam Brigman
12701 Lancaster Hwy.
Pineville, NC 28134
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutions SC Certification No. 99012
Project: 2017 Production
Lab Submittal Date: 09/06/2017
Prism Work Order: 7090068
Case Narrative
09/08/2017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Marrative Notes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Cara C. Rusmisell
Project Manager
Data Qualifiers Ivey Reference:
Reviewed By Cara C. Rusmisell
Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409
7 B S Full -Service Analytical &
Environmental Solutions
` =1'L ..Mxcmm INC.
Sample Receipt Summary
09/08/2017
Prism Work Order: 7090068
Client Sample I®
Lab Sample ID
Matrix
Date Sampled
Date Received
Mt Holly 4th Event -1
7090068-01
Solid
09/06/17
09/06/17
Mt Holly 4th Event - 2
7090068-02
Solid
09/06/17
09/06/17
Mt Holly 4th Event - 3
7090068-03
Solid
09/06/17
09/06/17
Mt Holly 4th Event - 4
7090068-04
Solid
09/06/17
09/06/17
Mt Holly 4th Event - 5
7090068-05
Solid
09/06/17
09/06/17 '
Mt Holly 4th Event - 6
7090068-06
Solid
09/06/17
09/06/17
Mt Holly 4th Event - 7
7090068-07
Solid
09/06117
09/06/17
Samples were received in good condition at 5.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543
Phone: 7041529-6364 - To 11 Free Number: 1-800/529-6364 - Far.: 7041525-0409
'M
. �
A=s!
1 ..� f _
`jLABORATORIES, INC.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagro
Sample Date/Time Collected:
Sample Date/Time Submitted:
449 Springbrook Rd.
P.O. Box 240543
Full -Service Analytical & Charlotte, NC 28224-0543
Environmental Solutions Phone: 704/529-6364
Fax: 704/525-0409
Project Name: obit. Holly
9-6-17 09:42 Project ID: Mt. Golly 4th Event
9-6-17 10:45 C®C Group: 709006E
Prism
Sample
ID
Client
Sample ID
Fecal Co Q orm in
Solids(cfulg)
SM9222 D
Reporting
Limit
% Solids SM2640 G
Analysis Date/Time
7060068-01
1 Mt Holly4th Event
610000 A
610000
1.64
9-6-17 12:02
7060068-02
Mt. Holly4th Event
560000 A
560000
1.77
9-6-17 12:02
7060068-03
Mt. Holly 4th Event
570000 A
570000
1.76
9-6-17 12:02
7060068-04
Mt Holly 4th Event
530000 A
530000
1.90
9-6-17 12:02
7060068-05
Mt Holly 4th Event
500000 A
500000
2.01
9-6-17 12:02
7060068-06
Mt. Holly 4th Event
430000 A
430000
2.30
6-17 12:02
7060068-07
Mt Holly 4th Event
580000 A
580000
1.73
if9-:6:-712:02
Geometric Mean Calculation:
Prism Sample ID: 7090068 Geometric Mean: 536950 A cfu/g
Deporting Limit: 536950
Note: All results are reported on a dry -weight basis.
A: The result is less than the reporting Jimit. At the request of the client, the value reported equals the value of the reporting
h r
limit.-
f
Data Reviewed By: Poject Manager: C. RUsmisell
Review Date: 9-8-17 ,approval Date: 9-8-17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
I
,r FullService Analytical p
�i W i �.� v Environmental Solutions
'1
LABORATORIES, INC.
449 Springbrook Road • Charlotte, NC 28217
Phone 7041529-6364 Fax: 7041525-0409
Client Company Mame: � d tCi G r J
(Report To/Contact Nang 4,1t1 ✓y) Errs m'ta'ti
Reporting Address:
L),ieyal'1.2 All.. Lli�S Y
VAGE___L_ OF _ QU07E # 40 E'pNSUIl PROPER SOLU.11MG:
Project Name: JV i ' I I`! ) o l ly
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL I II III IV)
provisions and/or QC Requirements
Invoice To: split i;-f-0
Address:
Phone: 70LI '- - ) - ° 6s�l I Fax (Yes) (6):
Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: 0 r <radvrclan � SY� sty .: CG�rn
— ,�—� Requested Due Date ❑ 1 Day ® 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification.
NELAC DOD FL NC
EDD Type: PDF }C Excel Other
"Working Days" ❑ 6-9 Days ❑ Standard 10 days Q Rush Worlc Must Be
Pre -Approved
SC OTHER NIA
Site Location Name: A/Va No II
Samples received after 14:00 will be processed next business day.
Site Location Physical Address:
Turnaround time Is based on business days, excluding weekends and holidays.
Water ChlorlInated: YES_ NO N
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES ,>\' NO —
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
REMARKS
LAB
*TYPE
NO.
SIZE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
TIVES
ID NO.
HOURS
SLUDGE)
SEE BELOW
eI-
G ev
(),`
Of
j
J
7
o!
Sampled By Name) ! aRJ2 f', E t �t A'! Affiliation
Sampler's Signature
(Print
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
f
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
}'
Relinquished r�r
Received By: (Signature) D e Military Hours
Additional Comments: ' ' f
Site �pnv !I Ytme
R ,l
Relinquished e : (Signature)
Received By: Date -
Site Pgpartufe,T!ntb' - �., .;
Relinquished By: (Signature)
"�'
Received F r Prls Labo ries By: 4 per^ pate
; FIe1d TeclrFec
,.� � _ ;
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUST DY SEALS FOR TRANSPO.RTATIOWTO THE LABORATORY. COC Group No.
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COC UNTI ECEIVED AT THE LABO TORY.
t) }(
v (.�u ��
❑ Fed Ex ❑ UPS ❑ Hand-derivered ❑ Prism Field Service ❑
Other U
NPOES: I UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: RCLA LAN®FILL OTHER:
CENC
'
❑NC❑SC ❑NC ©SC ❑NC ❑SC ❑NC
❑SC I ❑NC ®SC ®NC❑5C ❑®SC ❑NC El 0NC Ell SC
r
r-O —1 ❑ ❑
❑ ❑ ❑ ❑ ❑
,onlnlAl
*CONTA TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined IOA = Volatile Organics Analysis (Zero Head Space)
I\Rn—,
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 11/01/17 To 12/31/17
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air.Drying Composting Aerobic Digestion
Anaerobic Digestion
it appucaDie to airernauve periormea t-
ass A or mass is corn fete ine ionowing monitoring
aata:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6
Coliform
power per gram
MPN
MPN/g
event
sludge
SM9221E
of total solids
CFU
1,000,000
1,152,409
1,300,000
CFU/g
Event
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
OptioriWt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Mt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench) X
Option/Mt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including P
e and imprisonment."
Doug Shoutd / ORC a � ?�1 �� 55
Prepa e d Titl (type or print) Land p ier Name and Title (if applicable) (type or print)
r
ignature o Prepare Date Sigdg, r Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
C %M
Ta :>
��-e�.,-s��: IABORA70RIES INC,
Synagro
Adam Brigman
12701 Lancaster Hwy.
Pineville, NC 28134
NO Certification No. 402
Full -Service Analytical & NO Drinking Water Cert No. 37735
Environmental Solutions SO Certification No. 99012
Project: 2017 Production
Lab Submittal Date: 10/31/2017
Prism Work Order: 7100541
�3
t'
t
Case Narrative
11 /02/2017
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This report contains a total of 4 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
6. -�
Cara C. Rusmisell
Project Manager
Reviewed By Cara C. Rusmisell
Project Manager
Data Qualifiers Key Reference:
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NO 28224-0543
Phone: 704/529-6364 -Toll Free Number 1-800/529-6364 - Fax: 7041525-0409
Sample RecMpt Summat
F ll-Se�l.e Analytical&
PRISM I Environmental Solutions 11/0212017
Prism Work Order: 7100541
Client Sample ID Lob Sample ID Matrix Date Sampled Date Received
5th Event 1
7100541-01
Solid
10/31/17
10/31/17
5th Event 2
7100541-02
'Solid
10/31/17
10/31117
5th Event 3
7100541-03
Solid
10131/17
10/31/17
5th Event 4
7100541-04
Solid
10/31117
10131117
5th Event 5
7100541-05
Solid
10/31/17
10/31/17
5th Event 6
7100541-06
Solid
10/31/17
10131/17
5th Event 7
7100541-07
Solid
10/31/17
10131117
Samples were received in good condition at 4.8 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.D. Box 240543 - Charlotte, NC 28224-0543
Phone: 7041529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409
..... ........ ..... VEm.-
BORATORIES, INC.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert. No. 37735
Client Name: Synagro
Sample Date/Time Collected:
Sample Date/Time Submitted:
Full -Service Analytical &
Environmental Solutions
449 Springbrook Rd.
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: 704/529-6364
Fax: 7041525-0409
Project Name: Mt. Dolly
10-31-17 07:45 Project ID: 5th Event
10-31-17 09:00 CGC Group: 7100541
rlsrra
Sample
ID
Client
Sample ID
'eea C®I orsxa in
Solids(ctu/g)
SM9222 D
Reporting
Limit
% Solids SM2540 G
Analysis Date/Time.
7100541-01
Mt. Holly 5th Event
1200000 A
1200000
0.830
10-31-17 10:45
7100541 02
Mt. Holly 5th Event
1100000 A
1100000
0.940
10-31-17 10:45
7100541-03
Mt. Holly 5th Event
—
1100000 A
_[
1100000
—
0.910
10-31-17 10:45
7100541-04
Mt Holly5th Event
1000000 A
1000000
0.970
10-31-17 10:45
7100541-05
Mt. Holly5th Event
1100000 A
1 100000
0.890
10-31-17 10:45
Mt. Holly 5th Event
1300000 A
1300000
0.790
10-31-17 10:45
E
Mt Holly 5th Event
1300000 A
1300000
0.750
10-31-17 10:45
Geometric Mean CalcuIR166i:
Prism Sample ID: 7100541 Geometric Mean: 1152409 A cfu/g
Reporting Limit: 1152409
Note: All results are reported on a dry -weight basis.
A: The result is less than the report g limit. At the request of the client, the value reported equals the value of the reporting
limit. /I ;
� Data Reviewed By:; yf '�Zl ' Y t'roject Manager: C. Rusmisell
Review Date: 11-2-17 Approval Date: 11-2-17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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CHAIN OF CUSTODY RECORD
r o r
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Full -service Anal rtleal
w'
� +4 t pp g p'
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i c
y , }; y Environmental Solutions PAGt of l QUO'TE0TOENSUREPROPER0116ILINGa
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44.9 Sprincdbrook Road > Charlotte, HC 28217 Project Name:
Phone 704/529-6364 Fax: 7041525-0409 Short Hold Analysis: (Yes) j o) UST Project: (Yes) (NO)
"Please ATTACH any project specific reporting [QC LEVEL 1 li III IV)
Client Company Name: �yg!�4'—v
—���' provisions and/or QC Requirements
Report To/Contact Name: r9q i3ri',2-?k6 -) Invoice To:
Reporting Address: 12.70+ Q tatCrd.m- •Nlrwt. Address:
Phone:701 6, 0G 1' 1( Fax (Yes)W):
�, PlarchaBe �Irder N®.!Filling Reference
C• kA4 ( 4_,0a4lr,0
TO SE FILLED IN EY CLIENT/SAMPLING PERSONNIEL
/
Email Address: ,'4c1°' . ,ce.,71
�
EDD Type: PDP' ?,/ Excel
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days m 4 Days 05 Days
RushBe
"Working h Work
Certification: NELAC ®®® FL NO ar '
_Other'
Days" ❑ 6-9 Days ® Standard 10 days ❑
Site Location Name: 1144 e 4e�t+!# Iy --s o — I s 0 tf
dust
re
Samples received after 14:00 will be processed next business day.
SC OTHER NIA
Site Location Physical Address:
Turnaround time Is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ N® v
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
r'
Sample Iced Upon Collection: YES V NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I
TIME
MATRIX
SAMPLE CONTAINER
ANALYSIS
REQUESTED
PRISM
CLIENT
DATE
COLLECTED
(SOIL,
PRESERVA-
at'
REMARKS
LAB
*TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
NO.
SIZE
TIMES
A10011"
ID NO.
HOURS
SLUDGE)
SEE BELOW
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Sampler's Signature dJ�(7
Sampler's
Sampled By (Print Name) ,�1^f64? r!Gr y dl1i Affiliation
Upon relinquishing, this Chain of Custody is your authorization
for Prism to proceed with the analyses as requested above. Any changes roust be
submitted in writing to the Prison Project Manager, There will be charges for any changes after analyses have been initialized.
°
Relinquished By: (Signature)
,
Received By: (Signature) Date
qq 1 �y
Military/Hours �a
Additional Comments: 1,Sit�/�f•t'Ivaf,,;�jm�. ,' l, +t
Relinquished By: (Signature) d
Received By: (Signature) Date
OlemrlI T(1no + ('$�
Relinquished By: (Signature)
Receiy or Prism Laboratories By: Date c g '°�
— I y
�i ,'°jj°'�
1 `"' �J 1 1
d 4:+'"d.°'
Method of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COG Group No.
t 9 J
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST COG UNTIL RECEIVED AT THE LABORATORY.
{
�I 10 CT 1
O Fed Ex ❑ UPS ® Hand -delivered ❑ Prism Field Service O
Other
NPDES, UST. GROUNDWATER:DRINKING WATER:' SOLID WASTE: RCRA. CERCLA LANDFILL OTHER:
❑NC❑SC ❑NC ®SC ❑NC ❑SC ❑NC
El I ❑NC El SC ❑NC❑SC El ®SC ❑NC ❑SC
I '
©NC ®SC
❑ ❑ ❑ ❑
❑ c ❑ ❑ -
❑ !r^1n;t11
*CONTJ TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined VOA = Volatile Organics Analysis (Zero Head Space)
0
Am
P
PROMPT-ACCURATE' yR,E[+LIAVB�LE:
T t,-�
\VNN'N'.PARLABS.('0Nl
REPOR': OF AtiA_Y: ES
Attn: ADAM BRIG -MAN
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, N_' 28134-
PROJECT NAME: SEP 17
DATE: 10/10/17
SAMPLE NUMBER- 129036 SAMPLE ID- MT. y' LLY 4TH EVENT SAMPLE MATRIX- SO
DATE SAMPLED- 09/06/17 TIME SAMPLED- 0942
DATE RECEIVED- 09/06/17 SAMPLER- AB RECEIVED BY- DJ
TIME' RECEIVED 1111 DELIVERED BY -CAB TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS METHOD -DA` E' TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 09/06/17 RE ATTACHED
LABORATORY DIRECT,):-.
11.0. Box 411443 ° Charlotte. INC 2S'241-14,N }
Phone: (/04) 588 33 - Fay: (704) 58845335
s
P
PROM PT•ACCU RATE• RELIA9 LE
I..ABORA-FORTES, INC
WWW. RARLAE3S. COM
30 ®ay Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAGRO
r MT. HOLLY 4TH EVENT
129036
09/06/17
• 10/05/17
Start: End:
TS ()
0.1963
0.1808
TS%
1.66%
1.63%
VS ()
0.1523
0.1371
VS%
77.59%
75.83%
I N
0.00437
OUT
0.00401875
FSVR (Mass Balance)
8.04%
FSVR (Van Kleeck)
9.38%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box411483 • Charlotte, NC 28241-1483
Phone: (704) 588-8333 0 Fax: (704) 588-8335
P Am
PRO MPT•ACCU RATE -RELIABLE
LABORATORIES, INC
W W W.PARI-ABS.COM
Crucible
Tare Wt (g)
Sample(g)
Dried Wt(g)
Burned Wt(g)
TS%
VS%
3.0 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
SYNAG RO
MT. HOLLY 4TH EVENT
129036
09/06/17
s • 10/05/17
As Received Day 0
09/06/17 09/07/17
Day 7 Day 14 Day 21 Day 28
09/14/17 09121/17 09/28/17 10/05/17
X15
X18
X5
X18
X22
X18
21.9490
23.0242
20.5204
23.0241
22.3086
23.0250
35.2112
34.8509
32.3846
34.4477
33.4244
34.1151
22,2421
23.2205
20.7114
23.2126
22,4909
23.2058
23.0682
20.5638
23.0671
22.3508
23.0687
2.21 %
1.66%
1.61 %
1.65%
1.64%
1.63%
77.59%1
77.28%1
77.19%1
76.85%1
75.83%
0.004370045
x
0.001262521
TS ()
0.1963
VS ()
0.1523
Volatile Fraction In: 0.46741
P.O. Box411483 • Charlotte, NC 28241-1483
Phone: (704)SSS•8333 • Fax: (704)5SS-8335
0.004018748
x
0.001280968
TS {
0.1808
VS )
0.1371
Volatile Fraction Out: 1 0.46521
L
RALABORATORIES,
, INC.
www.pariabs.com
CHA ®F CUSTODY
PAR Laboratories, Inc
Phone (704) 588-8333
Fax (704) 588-8335
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carnlina Denartment of Environmental and Natural Resources.
Company Name (billing)
Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
l !17 y I Ae (� V el 1J`` 'I �GoL i' e
J Q �,Jf e Ne edS 40 b e
City, State Et zip code
PINEVILLE NC 28134
�e �t('c l
d. d �8 below e ow ZG/
Point of Contact iY Telephone Number }/ Z
__n �/EI9A ril DIV .ac}�pj �`} -) — 650 .Lu L/
_ v I l r
Sample
Taken By
SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
"Sample Type: DW Ww GWMW HW Soil Other r'o
Sample Temp at time of sampling: ° C Sample Temp upon receipt: 0 C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N):
Client Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Daterrime
Collection
Datef rime
Analyses
(Requested
ffi , HollY 30- aY e1,101
113 L ven'r
X
q � �7
` ' `IZl%r
sQ- dtifU eh�h
C)P
I
Relinquished by: Dgte ime Received by: Dateffime
�i',w✓_`Cr G' -C'4
Relinquis ed by: D&e/Time Received by: Date/Time
C=Composite G=Grab DW=Drinking Water W1N=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See
Other Side
Agricultural Lime Application Log
2017
Project: City of Mt Holly
Field
(state -county -site -field)
Grower
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date
Applied
Total
Acres
NC-GA-41-01
Greg Springs
6.3
0.0
0.0
NC-GA-41-06
Greg Springs
6.3
0.0
0.0
NC-GA-41-14
Greg Springs
6.4
0.0
0.0
NC-GA-45-01
David Allen
6.1
0
0.0
NC-LT-46-01
Ton Jones
6.1
0
0.0
NC-LT-46-02
Ton Jones
6
0
0.0
NC-LT-46-03
Tony Jones
6.1
0
0.0
NC-LT-46-04
Tony Jones
6.1
0
0
NC-LT-46-05
Ton Jones
6
0
0
NC-LT-46-08
Tony Jones
6.3
0
0
NC-MG-37-01
Dale Connell
6.2
0
0
* lime has been ordered but not spread
NCDA&CS Ai mic Division Phone: (919) 733-2655 Website: www.nc-,..y.)v/agronomi/ Report No. FY18-�,�i.2239
Greg
Springs �y <-�m•_••„•• g Advisor: Synagro
Predictive 410 West Catawba Ave 12701 Lancaster H
wy
Mount Holly, NC 28120 Pineville, NC 28134
i=. Soil Report Mehlich-3 Extraction
4
r••>� .' Sampled County :Gaston
Links to Helpful Information
Client ID: 452256 Advisor ID: 449334
Sampled: Received: 08/11/2017 completed: 09/01/2017 Farm: NC-GA-41
Agronomist's Comments:
This report provides Test Results and Recommendations for each sample submitted for testing. Look for Lime Recommendations and N-P-K Fertilizer Recommendations. The lime
recommendation is always listed next to the first crop and will be based on the higher target pH if the pH targets for crop 1 and crop 2 differ. Application at the indicated rate will raise soil
pH to the optimal level for the plant you specified and should be sufficient for 2 to 3 years, depending on soil type. Common target pH values are as follows: 5.0 for azalea, camellia,
rhododendron and mt. laurel; 5.5 for centipedegrass; 6.0 for other lawn grasses, shrubbery, and; flowering plants; and 6.5 for vegetable gardens. N-P-K Recommendations are based on the
nitrogen (N) needs of the plants being grown and the soil test results for phosphorus (P-1) and potassium (K-1); a 50 to 70 index for either is optimum. If the exact fertilizer cannot be found,
find the closest match and ad'ust the rate accordin I . Refer to "Understanding the Soil Report" last page of this report) for additional explanation and links to helpful information.
Sample ID: 41-06
Recommendations: Lime . Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 70 90 0 0 0 0 0 0
Note: 12
2-
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.36 0.91 9.4 92 0.8 6.3 29 26 63 27 60 224 146 208 208 400 0.1 1
Sample ID: 41-01
Recommendations: Lime Nutrients (Ib/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0
Note: 12
2-
Test Results [units - WIV in g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-Al Cu-1 Na ESP SS-1 NO3-N
0.41 0.93 15.2 93 1.1 6.3 67 143 59 29 65 272 176 370 370 180 0.2 1
Iorth Carolina
' �i�IY:�CyiP �141SL 1�111rL1 C1a111hIc5}li>IA
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner ofAciriculture
NCDA&CS A ------ mic Division Phone: (919) 733-2655 Website: www.nLay,.yov/agronomi/ Report No. FY18-bLUu2239
Greg Springs Page 2 of 3
Sample ID: 41-14
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
100
0 0
0 0
0 0
Note: 12
2-
Test Results [units - W/V in g/cnn ; CEC and Na in meq/100 cm3; NO3-N
in mg/dnr ]:
Soil Class:
Mineral
HM% W/V CEC
BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.46 0.82 12.5
94 0.8 6.4 98 19
67 27 83
195
129
448 448
485 0.2 2
NCDA&CS A_ mic Division Phone: (919) 733-2655 Website: www.n( ov/agronomi/ Report No. FY1E, __j2239
Greg Springs Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rat(
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncacrr.gov/agronomi/obpart4.html fsFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize)
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, CA, S-I, SS-1, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagrpov/agronomi/uvrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS -I
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index
NCDA&CS / r omic Division Phone: (919) 733-2655
Website: www.n
_ jov/agronomi/
Report No. FY10-0L-Lj01248
L l.lpq
.. : a �� tli
Client:
David Allen
Advisor: Synagro
Predictive
110 Helton Rd
12701 Lancaster Hwy
k ra wu�
fit~I
Cherryville, NC 28021
Pineville, NC 28134
Soil Report Mehlich-3
Extraction
Sampled County: Gaston
Links to Helpful Information
Client ID: 452255
Advisor ID: 449334
Sampled: Received: 0712712017 Completed: 08/04/2017
Farm: NC-GA-45
Sample ID: 45-01
Recommendations. Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, E 1.2
50-70 90
60
0 0
0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 80
90
0 0
0
0
0 0
Note: 12
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cn-P; NO3-N in mg/dnr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-I K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.46 1.05 7.6 80 1.5 6.1 24 23
58 21 37
1601
970 976
102
102
118 0.1 1
North Carolina
is+It;i4,�ia°Jnlwf I�i.nul�'i��ItirCi55141�
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture
NCDA&CS A _ imic Division Phone: (919) 733-2655
Website: www.n". u..uov/agronomi/
Report No. FY1b-oL_uJ1248
David Allen
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg/
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
M-0
N
mineral -organic soil class
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmVl#sFind information that
P-I
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS -I
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine)
Zn-I
zinc index
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagrgov/agronomi/uvrst.htm
Page 1 of 1
Report Number: 17-073-0790
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Waypoint
ANALYTICAL
"Every acre... Every year.'4M
Date Received: 03/14/2017 Date Of Analysis: 03/15/2017
Farm ID: NC-LT-46
SOIL ANALYSIS REPORT
Date Of Report: 03/15/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax 804-271-6446
www.waypointanalytical.com
Grower: Tony Jones
Mt Holly 50-1701
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Sample ID
Field ID
Lab
Number
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
%,
Rate
Soil
Class
Ib/A
s
M3 ..
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
PH
Buffer
Index
H
meq/100g
meq/100g
01
03532
.6.5
H
150
91 H
NC = 76
62 L
NC = 32
127 M
1009 M
8 VL
6.1
6.83
1.0
7.3
MIN
03
03533
7.1
VH
150
36 MT
NC = 30
55 VL
NC = 28
148 H
833 M
13 VL
6.1
6.84
0.9
6.5
MIN
08
03534
6.1
H
150
86 H
NC = 72
51 VL
NC = 26
167 H
750 M
10 VL
6.3
0.6
5.9
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NON
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
01
2.2
14.5
69.1
0.5
13.7
4 VL
NC=8
8.4 VH
NC=210.0
20 M
NC=125
127 VH
6.6 VH
NC=330.0
0.5 L
03
2.2
19.0
64.1
0.9
13.8
15 L
NC=31
4.7 H
NC=117.5
41 H
NC=256
62 VH
3.5 VH
NC=175.0
1.4 L
08
2.2
23.6
63.6
0.7
10.2
13 L
NC=27
9.5 VH
NC=237.5
23 H
NC=144
76 VH
4.9 VH
NC=245.0
0.5 L
values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested, samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: P z`
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm.
Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary
Page 1 of 1
Report Number: 17-340-0506
Account Number:46441
Send To: Synagro Central LLC/ Charlotte
Adam Brigman
12701 Lancaster Hwy
Pineville NC 28134
e
Waypoint
ANALYTICAL
"Every acre... Every year. "rn+
SOIL ANALYSIS REPORT
Date Received: 12/06/2017 Date Of Analysis: 12/07/2017 Date Of Report: 12/07/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax 804-271-6446
www.waypointanalytical.com
Grower: Tony Jones
City of Mt Holly
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Field ID
Lab
Number
°
�°
Rate
Soil
Class
Ibs/A
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
meq/100g
46-02
12318
5.5
H
150
4 VL
NC=3
48 VL
NC=25
177 H
853 M
28 VL
6.0
6.82
1.1
7.1
MIN
46-04
12319
5.8
HH
150
2 VL
NC = 2
40 VL
NC = 20
165 H
787 M
45 L
6.1
6.84
0.9
6.5
46-05
12320
5.7
H
150
2 VL
NC = 2
38 VL
NC = 19
172 H
823 M
42 L
6.0
6.82
1.1
6.9
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NO,N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
46-02
1.7
20.8
60.1
1.7
15.5
34 H
NC=71
0.6 VL
NC=15.0
46 H
NC=288
50 H
1.8 H
NC=90.0
0.3 VL
46-04
1.6
21.2
60.5
3.0
13.8
69 VH
NC=144
0.7 VL-
NC=17.5
41 H
NC=256
47 H
1.3 M
NC=65.0
0.3 VL
46-05
1.4
20.8
59.6
2.6
15.9
76 VH
NC=158
0.6 VL
NC=15.0
36 H
NC=225
58 VH
1.1 M
NC=55.0
0.3 VL
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: �aµri�
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
Analysis prepared by: WaypolntMalytical Virginia, Inc.
Pauric McGroary
Page 1 of 1
Report Number: 17-073-0791
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Waypoint
A
NALYTICAL
"Every acre... Every year."Tu
no4o ao..oi —4- nR/1A/7n17 nat. rlf Annlvcic- mvi';;/7nl7
Farm ID: NC-MG-37
SOIL ANALYSIS REPORT
Date Of Renort: 03/16/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Grower: Dale Connell
Mt Holly 50-1701
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
OM
wN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
%
Soil
M3
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
Rate
Class
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
01
03535
5.4
150
29 L
74 L
185 VH
602 M
4 VL
5.2
0.7
5.5
H
I NC = 24
NC = 38
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
Field ID
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
01
3.4
28.0
54.7
0.3
12.7
7 VL
5.9 H
54 VH
93 VH
3.1 VH
0.3 VL
NC=15
N6=147.5
NC=338
NC=155.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), los/A i nis report appnes to sampiets) testeu. aampies
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: WaypointAnalytical Virginia, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
by: ?W11 m'` 6001
Pauric McGroary
Schutte, Maria
From: Schutte, Maria
Sent: Tuesday, April 11, 2017 5:56 PM
To: 'david Johnson@mtholly.us'
Cc: Jonathan Jordan@mtholly.us'; 'ray.clemmer@mtholly.us'; 'Clay Fisackerly'; Gregory,
Sonia
Subject: WQ0001863 Mt. Holly 2016 Annual Report Receipt and Additional Information Request
Mr. Johnson,
This.email will serve as the Acknowledgement of Receipt of the 2016 Annual Report for the referenced residuals
permit. A report copy was received in the Mooresville office on March 6th, 2017. My comments and additional
information requests are noted below and were discussed with Jonathan Jordan during the March 28th inspection.
Waypoint labs does not include the Exchangeable Sodium Percentage (ESP) calculations in their soil
reports. The missing information needs to be submitted for each field (a table with field ID and calculated ESP is
acceptable), per Permit Condition IV.5.
• Verify contract lab is performing the 30day bench in accordance with the procedure. The dates displayed on the
Sept/Oct PAR labs report appear to be <30days. There is often an additional lab bench sheet that shows
readings overtime and that should be included with the report.
• A 3.01 % solids is recorded for the first quarter (2/18/16); however, the lab results show a 1.96% .solids. This will
affect all parameter calculations for the fields applied during the first quarter. The resulting PAN and total
metals data will actually be lower not greater, so there is no concern of an over application, but the "Application
Field Summary" forms need to be corrected for accurate cumulative totals going forward.
Please contact me with any questions and email your response with the requested additional information.
Thank You!
Maria
Maria Schutte
Environmental Specialist
Water Quality Regional Operations Section
Division of Water Resources
North Carolina Department of Environmental Quality
704 663 1699 office
704 235 2184 direct
Maria. schutte(aD_ncdenr.gov
610 East Center Avenue
Suite 301
Mooresville, NC 28115
Err,ad ccrrospomdonce to aria ro;aa this address is subject to the
North Carolina Public Records Law and may be disclosed to third parries.
- 71�
REcmVLD/NCDENR10WR
WQROS
MOORESVILLE REGIONAL OFFICE
rj
FEB 2 7 2017
City of Mount Holly, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001863
2016 ANNUAL REPORT
City of Mount Holly, NC
Residuals Land Application Program
2016 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and SAR Calculation
Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00001863 County Gaston Year 2016
Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NC0021156 & 01-36-020
Land Application Operator Synna ro Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 21
Total number of fields utilized for land application during the year: 10
Total amount of dry tons applied during the year for all application sites: 198.46
Total number of acres utilized for land application during the year: 140.5
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. Allother monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting fal information, ' clud' g the possibility of fines and imprisonment for
knowing violations."
Danny Jackson, City Manager b ^ 1 l
Permittee Name and Title (type or print) i pg Date
FEDy
F'V AA
201
Ygnature of eparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2016 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
-,'iVIOUNT HOLLY, NC
MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
DRY METRIC
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
March 2016
527,000.00
G
66.14
D
59.99
June 2016
657,200.00
G
57.27
D
51.94
September 2016
471,200.00
G
37.31
D
33.86
November 2016
620,000.00
G
37.74
D
34.24
YEARLY TOTAL
2,275,400.00
G
198.46
D
180.03
1 /25/2017
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863
Facility Name: MOUNT HOLLY, NC
NPDES# : NCO021156
or WQ# (residual only)
WWTP Name: MOUNT HOLLY W/WTP
Residuals Analysis Data /
Product Type AEDLIQ
Date Sampled (grab) or 02/18/16
Date Composited
Percent Solids
PARAMETERS (mg/kg dry weight)
Arsenic
Cadmium
Mercury
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
Laboratory
WAYPOINT ANALYTICAL
Waypoint Analytical Virginia Inc.
AEDLIQ AEDLIQ AEDLIQ *..
04/19/1607/28/16� 09/26/16'
2.09 1.90 1.46
3
<3
3
<3
<2
<2
<2
<2
1.1
1
1.7
1.2
257,
258
298
328
476
516
548
578
37
36
38
50.7
<5
6
7
<5
22
24
34
26
<5
<5
<5
<5
768
857
881
898
14500
15400
13500
13500
52600
56500
50000
50300
4590
7660
10500
9520
<2
<2
<2
<5.42
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
JURE OF' PREPARER)
:SSF (5/2003)
Date-2-44 7
Printed: Wednesday - January 25 2017 at 11:56:37 for: 1701 01
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001863
Facility Name: MOUNT HOLLY, NC
NPDES# : NCO021156
or WQ# (residual only)
WWTP Name: MOUNT HOLLY WWTP
Residuals Analysis Data
Product Type
Date Sampled (grab) or
Date Composited
Percent Solids
AEDLIQ
02/18/16
PARAMETERS (mg/kg dry weight)
Aluminum
Calcium
Magnesium
pH
Potassium
Sodium
Laboratory
WAYPOINT ANALYTICAL
Waypoint Analytical Virginia Inc.
i
f
AEDLIQ
AEDLIQ
AEDLIQ
04/19/16
07/28/16
09/26/16
3.01
2.09
1.90
1.46
24100
23000
28700
20200
11100
11700
10900
13400
2470
2640
2490
2940
7.33
7.37
7.39
7.51
2610
2830
1860
2200
5830
7040
6010
9110
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
M111
NR - Data Not Reported or Data Not Required
Date 2`ce : t7
DENR FORM RSSF-B (7/2002) Printed: Wednesday - January 25, 2017 at 11:57:04 for: 1701 01
Page: 1 of 2
Report Number: 16-050-0202
Account Number: 00015
Send To: SYNAGRO CENTRAL/MT HOLLY
WAYNE BRADY
12701 LANCASTER HWY
PINEVILLE , NC 28134
(2)
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Project: MT HOLLY WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 2/18/2016 14:00:00
Lab Number: 55117 Date Received: 02/19/2016 00:00
Sample Id : MY HOLLY WWTP 50-1701 1ST EVENT Date Reported: 02/24/2016
Total Solids
Moisture *
Total Kjeldahl Nitrogen
Total Phosphorus
Total Potassium
Total Sulfur
Total Calcium
Total Magnesium
Total Sodium
Total Iron
Total Aluminum
Total Manganese
Total Copper
Total Zinc
Ammonia Nitrogen
Organic N
Nitrate+ N itrite-N
98.04
5.26
1.45
0.26
1.38
1.11
0.25
0.58
0.46
4.80
52600
14500
2610
13800
11100
2470
5830
14900
24100
437
476
768
4590
48010
<2.00
<2.0
100.0
RD
02119/201614:30
SM-254OG
100.0
RD
02/19/201614:30
SM-2540G
10.0
JM
02/22/2016 08:44
SM-4500-NH3C-TKN
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
100
KM
02/22/2016 10:46
SW 6010C
5
KM
02/22/2016 10:46
SW 6010C
5
KM
02/22/2016 10:46
SW 6010C
5
KM
02/22/2016 10:46
SW 6010C
10.0
JM
02/22/2016 08:44
SM-4500-NH3C
10.0
02/22/2016 08:44
CALCULATION
2.00
JM
02/22/2016 08:45
SM-450ONO3F
2.0
KM
02/22/2016 10:46
SW 6010C
on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
hpany in any advertising, news release, or other public announcements without obtaining our prior written authorization.
0091910 f•7C
Page: 2 of 2
Report Number: 16-050-0202
Account Number: 00015
Send To: SYNAGRO CENTRAL/MT HOLLY
WAYNE BRADY
12701 LANCASTER HWY
PINEVILLE , NC 28134
0
Waypoin,(Zt
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: MT HOLLY WWTP
NC CERT#257
REPORT" OF ANALYSIS
Date Sampled: 2/18/2016 14:00:00
Lab Number: 55117
Date Received: 02/19/2016 00:00
Sample Id : MY HOLLY WWTP 50-1701 1ST EVENT
Date Reported: 02/24/2016
�PARAMETtR RESULT
RESULT
QUANTITATION
METHOD
Total Chromium
257
5
KM
02/22/2016 10:46 SW 6010C
Total Nickel
22
5
KM
02/22/2016 10:46 SW 6010C
Total Lead
37
5
KM
02/22/2016 10:46 SW 6010C
Total Arsenic
3.0
3.0
KM
02/22/2016 10:46 SW 6010C
Total Mercury
1.1
0.4
KM
02/23/2016 09:00 SW-7471 B
Total Selenium
<5.0
5.0
KM
02/22/2016 10:46 SW 6010C
pH (Standard Units) * 7.33
2.00
JM
02/22/2016 08:44 SW-9045D
Total Molybdenum
<5
5
KM
02/22/2016 10:46 SW 6010C
Comments:
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: John Culp
Project Name: City of Mt. Holly WWTP Biosolids
Project Number:50-1701
Lot Number:RC16061
Date Completed:03/1712016
Lucas Odom
Project Manager
LABORATORY_
ACCREDITATION
ION
I. BUREAU
���• ACCREDITEO roue roza
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: RC16061
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Synagro
Lot Number: RC16061
Sample Number Sample ID Matrix Date Sampled Date Received
001 CITY OF MT HOLLY WWTP % SOLID 1ST EVENT Solid 03/16/2016 0805 03/16/2016
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Synagro
Lot Number: RC16061
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 CITY OF MT HOLLY VWVfP % SOLID Solid % Solids SM 2540G 3.01 % 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Client:Synagro Laboratory ID:RC16061-001
Description: CITY OF MT HOLLY WWTP % SOLID 1ST EVENT Matrix: Solid
Date Sampled:03/16/2016 0805 % Solids: 3.01 03/17/2016 0111
r1ate Received: 03/1612016
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids) SM 2540G 1 03/17/2016 0111 HMA 98618
CAS Analytical
Parameter Number Method Result Q PQL Units Run
% Solids SM 254OG 3.01 % 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > M DL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
,sere applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W'
ealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Chain of Custody
..�k
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
' SHEALY ENVIRONMENTAL SERVICES, INC.
ean3-7Faxluaobaa��7Za172I` , Telephone No. 71-9D
1~ vAv.sheslyllab.com
Number 4 45 8 8
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on,1e6 o0ar atrangamenfg arg made. AnSINdwrrtso,fGY *) cyc * a:�- P,r.Er I RUMf
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SHEALY ENVIRONMENTAL SERVICES, INC.
-11u3)!?F,nAror)mw1113 Service;, 11w- Fake i of L
330vurratni Nitmb= Elkalve Vau-! rR103,12036
Sample &�Qeipt Cheeldist (SRQ)
Coolcr lnsper,tr4 byldaw \—.r,s Lot
Means of receipt. 'ES1 Ujmt lEl UPS [] FMEx El Other
VWE] 11
No
1Z
1, weTe cufuody seals present on the cookT?
Yes U
JELJLJ
NA L-�T
2. If wstvdy seaTs were resent, we
.
pH strip TD, cl scrip 11):
Cooler ID/01riginal tewpaatare upon rwcjpt'T)t"4ved (conected) temp-7aturcupon receipt
"C Oc
IZC—thalk, [aTemperatur- Blank E.] Against Bottles IRGun. lD-.. S- JP, Gun Correc9on Factor: 2Qt=,_:°Q
Method of roolant., wet ice ❑ R1 Ue Ire EJ Dryloe. ❑ N-Ma
3. If lerrip1mture of any cooler cumded 6,011(%,was 11rcftet klanaggr nedifficd?
pM to X:itti' ma W-raee� (CirvIe One).
fled hy: hone I - -- it i faw -
Yes El
No ❑
-,NAFZ
4, 19 lie. commerciil courier's packinig slip atuachod to this form?
NaFos El
5, Wcrv, piftper eustody_p 'A --Z �qcedurts (relinquishe Ire eive foil nvcd?
M3 ❑
P
16, Wcre %ample [IN listed on the COC?
Y,. -3
No C1
17, Were gample 1D.% listed on all saMlc <;ontaiaers?
Yes Ler
NoEl
8. Was oulledion date be time fisted an the COC?
Yes
No
9, Was Im elistedonalls
YCS
No EJ—
.1
10- Did all container label itifo=ation (iD, date; (imp) air with the HOC?
Yes
No F1
11. lk"tere tesis to bo pCeLormi;d liste4 on the Coe'?
Y�A- [2�'
No El
12. Did all sample arrivu- in the pCoper containers fbr carh tm( antYar in good oondirion
ken, lids 014 ew)?
y
YeS
N0
13. Was adequate 5 a to volu ale al-aflable?
7-
- di-e holding time or 48 hu=, whkhever come; first?
14� Were all sampics rcceiwil within J,,'
Yes El
No
15. Were any samples containers missia_Wexr=s& (v,11rcl t; one) =Vles not listicd on COC?
16- Werebubble-s present>"pea-sip'' 4'or 6Dun in diaoveow) in any VOA vials?
ties _
NGEJ
IV" all las received at: a pH -of <,2?'L--
Yes F❑—
I
-W-
clo
NA
19. Wwo all rw4nide and'ar sulfide samples ro=-o--d aL a pH > 111
Yes ❑No
1. 9- Were all applivable NHITIC-Mleyaniddphenol (-'Urngfr );5aTnpte& rree of msidual
Yrs
Ala OfNti
L far I ?
ed -3n the COC 0 C Sa!R11 CS
Yes
wc, [37
NAU
2 1, Ware client remarkshequests rcquesttd dilixtians, MS(NISD designations, utc--)
correctly transcribed frorA else COO into ffie commcut wulion in
77 17-
No [0'
the quote number used I Rkcn kont thrw- Container label'?
SamploPmervation (Must be mmpleed, for any sample(s) inwrmadypr�ievved or with headspace.)
;wro recciNrcut -1111;VITeL�JL[y pi-eseived and tJ 3ovore-filgly in
sample rweiving with M7SOA, iUO!, U-6U05R4
sampic(k)
wvrc =cuivud with bubbles >6 nini In diameter.
saniples(s) wtye received vAth TRO >02-1 mg (lf 921 is No) and :47-7r,
adjwqted. accordingly in satngle rooeiving- ".%rith sodium thiostilfine (Na7.9;,,Oi) with Shealy ID:
SO DrinkIng Watcr Project Sample(s) pEl wrific-d to bu ` 2 by Datec
Sato wcrcnot rqcrived ata PN of.<2 and wore aLsted accardingty using SR4
Sample labels applied by-. Verified by:- Date
QqMgLelits:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 2/18/2016 111/2016-3/3112016 2.2547
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) — 100 = (5830 x 3.0100) _ 100 = 175.483
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (11100 x 3.0100) _ 100 = 334.11
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2470 x 3.0100) _ 100 = 74.347
Na meq = Na mg/I = Molec.Wgt.Na = 175.483 _ 23 = 7.6297
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 334.11 = 20 = 16.7055
Mg meq = Mg mg/1= Molec.Wgt.Mg = 74.347 _ 12 = 6.19558
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.6297 + SgrRoot[0.5(16.7055+6.19558)] = 2.25473
Printed: 1/25/2017
Page 1 11:59
Page: 1 of 2
Report Number: 16-111-0203
Account Number: 00015
Submitted By: DREW CULP
Send To: SYNAGRO CENTRAL/MT HOLLY
WAYNE BRADY
12701 LANCASTER HWY
PINEVILLE , NC 28134
Lab Number: 56806
Sample Id: 2ND EVENT
D
Waypoint(
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: MT HOLLY WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/19/2016 09:30:00
Date Received: 04/20/2016 00:00
Date Reported: 04/22/2016
Total Solids *
2.09
20900
100.0
JM
04/20/2016 13:45
SM-2540G
Moisture *
97.91
-100.0
JM
04/20/2016 13:45
SM-254OG
Total Kjeldahl Nitrogen
5.65
56500
10.0
JM
04/21/2016 09:20
SM-4500-NH3C-TKN
Total Phosphorus
1.54
15400
100
KM
04/21/2016 11:14
SW 6010C
Total Potassium
0.28
2830
100
KM
04/21/2016 11:14
SW 6010C
Total Sulfur
1.42
14200
100
KM
04/21/2016 11:14
SW 6010C
Total Calcium
1.17
11700
100
KM
04/21/2016 11:14
SW 6010C
Total Magnesium
0.26
2640
100
KM
04/21/2016 11:14
SW 6010C
Total Sodium
0.70
7040
100
KM
04/21/2016 11:14
SW 6010C
Total Iron -
15100
100
KM
04/21/2016 11:14
SW 6010C
Total Aluminum
23000
100
KM
04/21/2016 11:14
SW 6010C
Total Manganese
430
5
KM
04/21/2016 11:14
SW 6010C
Total Copper
516
5
KM
04/21/2016 11:14
SW 6010C
Total Zinc
857
5
KM
04/21/2016 11:14
SW 6010C
Ammonia Nitrogen
0.77
7660
10.0
JM
04/21/2016 09:20
SM-4500-NH3C
Organic N
4.88
48840
10.0
04/21/2016 09:20
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
04/21/2016 09:20
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
04/21/2016 11:14
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made (�
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 16-111-0203
Account Number: 00015
Submitted By: DREW CULP
Send To: SYNAGRO CENTRAL/MT HOLLY
WAYNE BRADY
12701 LANCASTER HWY
PINEVILLE , NC 28134
Lab Number: 56806
Sample Id: 2ND EVENT
Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: MT HOLLY WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/19/2016 09:30:00
Date Received: 04/20/2016 00:00
Date Reported: 04/22/2016
Total Chromium
258
5
KM
04/21/2016 11:14
SW 6010C
Total Nickel
24
5
KM
04/21/2016 11:14
SW 6010C
Total Lead
36
5
KM
04/21/2016 11:14
SW 6010C
Total Arsenic
<3.0
3.0
KM
04/21/2016 11:14
SW 6010C
Total Mercury
1.0
0.4
KM
04/21/2016 09:00
SW-7471B
Total Selenium
<5.0
5.0
KM
04/21/2016 11:14
SW 6010C
pH (Standard Units) *
7.37
2.00
JM
04/21/2016 09:29
SW-9045D
Total Molybdenum
6
5
KM
04/21/2016 11:14
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "As", "Cr", "Fe", "Pb", "Se", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 4/19/2016 41112016-7/31/2016 2.2056
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (7040 x 2.0900) = 100 = 147.136
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (11700 x 2.0900) = 100 = 244.53
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2640 x 2.0900) = 100 = 55.176
Na meq = Na mg/I = Molec.Wgt.Na = 147.136 _ 23 = 6.39722
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 244.53 _ 20 = 12.2265
Mg meq = Mg mg/I = Molec.Wgt.Mg = 55.176 _ 12 = 4.598
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.39722 _ SgrRoot[0.5(12.2265+4.598)] = 2.20564
Printed: 1/25/2017
Page 1 11:59
Page: 1 of 2
Report Number: 16-211-0218
Account Number: 00015
Submitted By: Drew Culp
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 58651
Sample Id : 3rd event
•
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Project: Mt Holly WWTP
NC Cert#257
REPORT OF ANALYSIS
Date Sampled: 7/28/2016 09:00:00
Date Received: 07/29/2016 00:00
Date Reported: 08/05/2016
Total Solids *
1.90
19000
100.0
JM
07/29/2016 14:15
SM-2540G
Moisture *
98.10
100.0
JM
07/29/2016 14:15
SM-2540G
Total Kjeldahl Nitrogen
5.00
50000
10.0
JM
08/02/2016 09:35
SM-4500-NH3C-TKN
Total Phosphorus
1.35
13500
100
km
08/01/2016 13:27
SW 6010C
Total Potassium
0.19
1860
100
km
08/01/2016 13:27
SW 6010C
Total Sulfur
1.52
15200
100
km
08/01/2016 13:27
SW 6010C
Total Calcium
1.09
10900
100
km
08/01/2016 13:27
SW 6010C
Total Magnesium
0.25
2490
100
km
08/01/2016 13:27
SW 6010C
Total Sodium
0.60
6010
100
km
08/01/2016 13:27
SW 6010C
Total Iron
15600
100
km
08/01/2016 13:27
SW 6010C
Total Aluminum
28700
100
km
08/01/2016 13:27
SW 6010C
Total Manganese
439
5
km
08/01/2016 13:27
SW 6010C
Total Copper
548
5
km
08/01/2016 13:27
SW 6010C
Total Zinc
881
5
km
08/01/2016 13:27
SW 6010C
Ammonia Nitrogen
1.05
10500
10.0
JM
08/02/2016 09:35
SM-4500-NH3C
Organic N
3.95
39500
10.0
08/02/2016 09:35
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
08/01/2016 08:50
SM-450ONO3F
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 6wm
4LOur reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ,
to the work, the results, or the company In any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor
Page: 2 of 2
Report Number: 16-211-0218
Account Number: 00015
Submitted By: Drew Culp
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
D
Waypoin(t,"
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project: Mt Holly WWTP
NC Cert#257
REPORT OF ANALYSIS
Date Sampled: 7/28/2016 09:00:00
Lab Number: 58651
Date Received: 07/29/2016 00:00
Sample Id : 3rd event
Date Reported: 08/05/2016
PARAMETER RESULT
RESULT
QUANTITATION
METHOD
Total Cadmium
<2.0
2.0
km
08/01/2016 13:27 SW 6010C
Total Chromium
298
5
km
08/01/2016 13:27 SW 6010C
Total Nickel
34
5
km
08/01/2016 13:27 SW 6010C
Total Lead
38
5
km
08/01/2016 13:27 SW 6010C
Total Arsenic
3.0
3.0
km
08/01/2016 13:27 SW 6010C
Total Mercury
1.7
0.4
CC
08/02/2016 16:05 SW-7471 B
Total Selenium
<5.0
5.0
km
08/01/2016 13:27 SW 6010C
pH (Standard Units) * 7.39
2.00
JM
08/01/2016 08:44 SW-9045D
Total Molybdenum
7
5
km
08/01/2016 13:27 SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE
PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Cr", "Mo",
"Na", AND "Ni".
THE LCS WAS OUT OF LIMITS FOR
"Se". THE MATRIX SPIKE WAS OUT OF
LIMITS FOR "N031NO2-N", "AI", "P", "Se", "S", AND "Zn".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 7/28/2016 811/2016-9130/2016 1.8569
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (6010 x 1.9000) = 100 = 114.19
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10900 x 1.9000) _ 100 = 207.1
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2490 x 1.9000) = 100 = 47.31
Na meq = Na mg/I = Molec.Wgt.Na = 114.19 = 23 = 4.96478
Ca meq = Ca mg/I t- Molec.Wgt.Ca = 207.1 = 20 = 10.355
Mg meq = Mg mg/I = Molec.Wgt.Mg = 47.31 = 12 = 3.9425
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.96478 _ SgrRoot[0.5(10.355+3.9425)] = 1.85689
Printed: 1/25/2017
Page 1 11:59
Page: 1 of 2
Report Number: 16-273-0203 '
•
Account Number: 00015 7621 Whitepine Road, Richmond, VA 23237
Submitted By: Marshall Puryear Waypoint
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Send To: Synagro Central LLC/ MT Holly Project : Mt Holly
Wayne Brady NC Cert#257
12701 Lancaster Highway
Pineville, NC 28134
REPORT OFANALYSIS
Date Sampled: 9/26/2016 10:00:00
Lab Number: 59991
Date Received:
09/29/2016 00:00
Sample Id : Mt Holly
Date Reported:
10/06/2016
PARAMETER
RESULT
RESULT
QUANTITATION
METHOD
Total Solids *
1.46
14600
100.0
R D
09/29/2016 15:20
SM-2540G
Moisture *
98.53
100.0
R D
09/29/2016 15:20
SM-2540G
Total Kjeldahl Nitrogen
5.03
50300
10.0
JM
09/30/2016 08:50
SM-4500-NH3C-TKN
Total Phosphorus
1.35
13500
100
MOS
10/03/2016 11:51
6010C
Total Potassium
0.22
2200
100
MOS
10/03/2016 11:51
6010C
Total Sulfur
1.65
16500
100
MOS
10/03/2016 11:51
6010C
Total Calcium
1.34
13400
100
MOS
10/03/2016 11:51
6010C
Total Magnesium
0.29
2940
100
MOS
10/03/2016 11:51
6010C
Total Sodium
0.91
9110
100
MOS
10/03/2016 11:51
6010C
Total Iron
16300
100
MOS
10/03/2016 11:51
6010C
Total Aluminum
20200
100
MOS
10/03/2016 11:51
6010C
Total Manganese
510
5.00
MOS
10/03/2016 11:51
6010C
Total Copper
578
5.00
MOS
10/03/2016 11:51
6010C
Total Zinc
898
5.00
MOS
10/03/2016 11:51
6010C
Ammonia Nitrogen
0.95
9520
10.0
JM
09/30/2016 08:50
SM-4500-NH3C
Organic N
4.08
40780
10.0
09/30/2016 08:50
CALCULATION
Nitrate+Nitrite-N
<5.42
5.42
SJB
09/30/201614:17
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , me'�
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor
Page: 2 of 2
Report Number: 16-273-0203
Account Number: 00015
Submitted By: Marshall Puryear
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville, NC 28134
Lab Number: 59991
Sample Id : Mt Holly
o
Waypoint.�
ANALYTICAL
Project : Mt Holly
NC Cert#257
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Date Sampled: 9/26/2016 10:00:00
Date Received: 09/29/2016 00:00
Date Reported: 10/06/2016
Total Cadmium
<2.00
2.00
MOS
10/03/2016 11:51
6010C
Total Chromium
328
5.00
MOS
10/03/2016 11:51
6010C
Total Nickel
26.0
5.00
MOS
10/03/2016 11:51
6010C
Total Lead
50.7
5.00
MOS
10/03/2016 11:51
6010C
Total Arsenic
<3.00
3.00
MOS
10/03/2016 11:51
6010C
Total Mercury
1.20
0.400
JM
10/03/2016 12:00
SW-7471B
Total Selenium
<5.00
5.00
MOS
10/03/2016 11:51
6010C
pH (Standard Units) *
7.51
JM
09/30/2016 09:25
SW-9045D
Total Molybdenum
<5.00
5.00
MOS
10/03/2016 11:51
6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Laboratory Supervisor
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY 9/26/2016 1011/2016-1213112016 2.2375
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (9110 x 1.4600) - 100 = 133.006
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (13400 x 1.4600) _ 100 = 195.64
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2940 x 1.4600) _ 100 = 42.924.
Na meq = Na mg/I _ Molec.Wgt.Na = 133.006 _ 23 = 5.78287
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 195.64 _ 20 = 9.782
Mg meq = Mg mg/I + Molec.Wgt.Mg = 42.924 _ 12 = 3.577
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.78287 _ SgrRoot[0.5(9.782+3.577)] = 2.23754
Printed: 1/25/2017
Page 1 11:59
FACILITY NAME: MOUNT HOLLY, NC
OWNER: GREG SPRINGS
SITE #: NC GA 00041 FIELD# : GA 00041 0006
RESIDUAL SOURCE(S):* See list at bottom of report
_]ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CECIL
PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 16.70
OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.90 ACRES PERMITTED: 8.90
Page: 1
Lime Applied ***
Date Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
A li
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
m
(pp )
Crop
Total
Per Acre
9/12/16
124,000.00 (G)
13932.584
1.90
1.104
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00
17102
I FESCUE
9/13/16
74,400.00 (G)
8359.551
1.90
0.662
MIIAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
p
2.00
17102
I FESCUE
9/15/16
12,400.00 (G)
1393.258
1.90
0.110
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
p
2.00 p
17102
FESCUE
Sep-16
1 210,800.00 (G)
23,685.393
Total Gallons/Ac: 23,685.39
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual Ibs/acre
64
0.011
0.008
1.118
2.057
0.143
0.006
0.026
0.128
0.019
3.307
50.67
Cumulative Ibs/acre
0.051
0.032
4.700
9.081
0.579
0.021
0.128
0.484
0.087
13.319
Permit PAN Limit (lbs/acre) lst Crop/2nd Crop
i
,
i
1
r,
s is t
�1
z s°
f
sr
s
t +
i
209
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1
1339.0
267.9
15.0 ' ` l
375.0
89.0
2500.0 i
s
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
. &M 9"�"
V - - a- (0- 9,01-4
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: GREG SPRINGS PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 9.83
SITE #: NC GA 00041 FIELD# : GA 00041 0010 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90
Page : 1
Lane Applied ***
Date
+_Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solid s
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKI�I
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm )
Crop
p
Total
Per Acre
9/13/16
31,000.00 (G)
3924.051
1.90
0.311
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00 p
F 17102
I FESCUE
9/14/16
68,200.00 (G)
8632.911
1.90
0.684
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00 p
17102
FESCUE
9/15/16
24,800.00 (G)
3139.241
1.90
0.249
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00 p
17102
FESCUE
Sep-16
1 124,000.00 (G)
15,696.203
brat uauonsiac: 1S,696.111
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
43
0.007
0.005
0.741
1.363
0.095
0.004
0.017
0.085
0.012
2.191
33.58
Cumulative lbs/acre
0.033
0.022
3.339
6.504
0.404
0.014
0.092
0.335
0.059
9.397
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
q
i
209
t
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 (, 375.0
89.0
2500 0 f 9
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
x &A qL 2t" Lq- IF - 1 -4
(SIGNATURE OF LAND APPLIER) V DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, IN7 -Injection, SUR1N -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: GREG SPRINGS PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 10.81
SITE #: NC GA 00041 FIELD# : GA 00041 0014 OPERATOR: GREG SPRINGS CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.80 ACRES PERMITTED: 6.80
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
m
(pp )
Crop
p
Total
Per Acre
9/13/16
37,200.00 • (G)
5470.588
1.90
0.433
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00 p
17102
I FESCUE
9/14/16
74,400.00 (G)
10941.176
1.90
0.867
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00 p
17102
I FESCUE
9115116
24,800.00 (G)
3647.059
1.90
0.289
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,000. p
10,500.00 p
2.00 p
17102
FESCUE
Sep-16
1 136,400.00 (G)
20,058.823
iotat vauons/Ac: zu,u.smu
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Anttuallbs/acre
54
0.010
0.006
0.947
1.742
0.121
0.005
0.022
0.108
0.016
2.800
42.91
Cumulative lbs/acre
0.036
0.023
3.709
7.038
0.448
0.016
0.100
0.371
0.063
10.372'
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
e
p�
��
} �'
i C '�
f °'i
209
!
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
I15.0
1339.0
267.9
375.0
89.0
I
c ,LLy
4,
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X ok qo(,"f,�4 9_-(,0-r4
(SIGNATURE OF LAND APPLIER) T DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: LLOYD
OWNER: DAVID ALLEN PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 28.64
SITE #: NC GA 00045 FIELD# : GA 00045 0001 OPERATOR: DAVID ALLEN CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.00 ACRES PERMITTED: 17.00
Page
Lane Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
6/13/16
105,400.00 (G)
6200.000
2.09
0.540
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
I FESCUE
6/14/16
86,800.00 (G)
5105.882
2.09
0,445
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
Ij FESCUE
6/16/16
136,400.00 (G)
8023.529
2.09
0.699
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18414
FESCUE
Jun-16
1 328,600.00 (G)
1 19,329.411
1
1 otai liaisons/Ac: 19,SLY.41
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
62
0.010
0.007
0.869
1.739
0.121
0.003
0.020
0.081
0.017
2.887
51.89
Cumulative Ibs/acre
71,
0.017
0.012
1.621
3.142
0.224
0.007
0.032
0.140
0.029
4.915
t
—
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
_
4��'
.-,
' �� I
:�
J
216
ri
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
tI
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
X9-(0-r-7
(SIGNATURE OF LAND APPLIER) 61 DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 35.41
SITE #: NC LT 00046 FIELD# : LT 00046 0001 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.80 ACRES PERMITTED: 11.80
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
. ons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Solids
P r
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm )
Crop
p
Total
3/
Per Acre
MONTH
3/24/16
31,000.00 (G)
26 1 9
3.01
0 30
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16700
I FESCUE
3/25/16
148,800.00 (G)
12610.1 9
3.01
.583
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16700
I FESCUE
3/29/16
24,800.00 (G)
210 .6 5
3.01
0.264
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16100
FESCUE
Mar-16
204,600.00 (G)
17,338.98
6/17/16
12,400.00 (G)
1050.847
2.09
0.092
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
I FESCUE
6/20/16
99,200.00 (G)
8406.780
2.09
0.733
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
FESCUE
Jun-16
111,600.00 (G)
9,457.627
I otal Gallons/Ac: 26,796.61
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
103
0.018
0.012
1.544
2.923
0.220
0.006
0.032
0.135
0.030
4.756
88.50
Cumulative Ibs/acre
0.041
0.027
3.436
6.285
0.450
0.014
0.070
0.317
0.068
9.500
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
17
t
T'Ik
209
yti
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0it
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
\R OF r.ANn APPLIER) DATE
f law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
- Not Required % = percent p = ppm or mg/kg
NJ - Injection, SURIN - Incorporation
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
*** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 23.03
SITE #: NC LT 00046 FIELD# : LT 00046 0002 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 45.20 ACRES PERMITTED: 45.20
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
m
(pp )
Crop
p
Total
Per Acre
11/15/16
111,600.00 (G)
2469.027
1.46
0.150
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,300.p
9,520.00 p
5.42 p
16999
I FESCUE
11/16/16
155,000.00 (G)
3429.204
1.46
0.209
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,300.p -
9,520.00 p
5.42 p
16999
FESCUE
11/17/16
111,600.00 (G)
2469.027
1.46
0.150
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,300.p
9,520.00 p
5.42 p
16999
FESCUE
Nov-16
378,200.00 (G)
8,367.258
1 ULUI UdIlUllb/11 . 0,JU-/.Lb
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
Annuallbs/acre
17
0.003
0.002
0.334
0.589
0.052
0.001
0.005
0.027
0.005
0.915 13.75
Cumulative lbs/acre
0.358
0.071
5.834
30.163
2.049
0.064
0.335
1.363
0.156
36.742
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop;
r
R
-'�
7,77
1`
209
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
' '
15 0 375.0
89.0
2500.0
,.
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
x &8
(SIGNATURE Oq LAND APPLIER) 4f DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 30.80
SITE #: NC LT 00046 FIELD# : LT 00046 0003 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 9.90 ACRES PERMITTED: 9.90
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
Tons
Cond.
Precip.
cation
tilt-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
SoiidS
Pb
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
Total
Per Acre
3/23/16
124,000.00 (G)
12525. 3
3.01
1.5172
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16700
FESCUE
3/24/16
31,000.00 (G)
3131 13
3.01
9293
MHAEDL
DRY
0-<I/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16700
FESCUE
Mar-16
' 155,000.00 (G)
15,656. 6
6/17/16
86,800.00 (G)
8767.677
2.09
0.764
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
I FESCUE
6/20/16
43,400.00 (G)
4383.838
2.09
0.382
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18414
FESCUE
Jun-16
130,200.00 (G)
13,151.515
total tJanons/Ac: L2i,bus.ub
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
108
0.019
0.012
1.602
3.054
0.228
0.007
0.033
0.141
0.031
4.983
92.29
Cumulative lbs/acre
0.048
0.032
3.964
7.238
0.513
0.016
0.082
0.372
0.080
10.860
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
;.
2 09
lay'
FD Cumulative Pollutant LoadingRate Limit lbs/acre
( )
36.6
34.8
1339.0
267.9
'
15 0 `i 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
11 q -7
X
',IGNATURYOF LAND APPLIER) U DATE
-1-tify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
ated the information submitted. I am aware that there are significant penalties for submitting false infornation, including the possibility of fines and imprisonment for Icnowing violations."
)rted or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
ace, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 14.72
SITE #: NC LT 00046 FIELD# : LT 00046 0004 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):"` See list at bottom of report ACRES UTILIZED: 19.40 ACRES PERMITTED: 19.40
Page : 1
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acre
Solids
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TI{N
Nitrogen
and
(pprn )
Crop
p
i�io.»i
1.4b
U•U16
1VIMAU
LKx
U-11/L"
JUK
u.c
u.su
cusuu.p
y,JLU.UU p
5.42 p
16999
FESCUE
11/18/16
124,000.00 (G)
6391.753
1.46
0.389
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,300. p
9,520.00 p
5.42 p
16999
I FESCUE
11/21/16
93,000.00 (G)
4793.814
1.46
0.292
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
50,300. p
9,520.00 p
5.42 p
16999
FESCUE
Nov-16
241,800.00 (G)
12,463.918
Total Gallons/Ac:
12,463.92
TOTALS:
As
Cd
Cr
Cu
Ph
Hg
Mo
Ni
Se
Zn
P
PAN
Annual lbs/acre
26
0.005
0.003
0.498
0.877
0.077
0.002
0.008
0.039
0.008
1.363
20.49
Cumulative Ibs/acre
0.133
0.070
4.397
40.045
1.649
0.084
0.451
1.531
0.152
36.233
::. f
:!
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
" 1
1
s
209
J
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89:0
2500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
X Q1-4
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
FACILITY NAME: MOUNT HOLLY, NC
OWNER: TONY JONES
SITE #: NC LT 00046 FIELD# : LT 00046 0007
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: PACOLET
PERMIT #: W00001863 ANNUAL DRY TONS APPLIED: 8.56
OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.00 ACRES PERMITTED: 7.00
Page
'Line Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
DATE or
o
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
Total
Per Acre/
MONTH
! -�
SolI ss
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitro en
g
and
m
(pp )
Crop
\
3/29/16
68,200.00 (G)
9742� 57
3.01
1.21
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
52,600.p
4,590.00 p
2.00 p
16700
FESCUE
Mar-16
68,200.00 (G)
9,742.857
iuLal vaucus/tic. Y,/ JL.bU
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Za
P
PAN
Annuallbs/acre
41
0.007
0.005
0.629
1.164
0.090
0.003
0.012
0.054
0.012
1.878
35.46
Cumulative lbs/acre
0.030
0.020
2.436
4.364
0.309
0.009
0.050
0.229
0.050
6.257
J
-,'
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
it
188
ic
T"
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 ;; 1 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"T - "Ify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
d the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = N-' Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: MOUNT HOLLY, NC PREDOMINANT SOIL SERIES: CECIL
OWNER: TONY JONES PERMIT #: WQ0001863 ANNUAL DRY TONS APPLIED: 20.02
SITE #: NC LT 00046 FIELD# : LT 00046 0008 OPERATOR: TONY JONES CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.60 ACRES PERMITTED: 6.60
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
Dry
Site
Inches
Appli-
Vola-
Miner -
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
MONTH
Total
Per Acr/
s
j
er
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
3/24/16
62,000.00 (G)
9393.939
3.01
1.179
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16700
I FESCUE
3/25/16
37,200.00 (G)
5636.36
3.01
0.707
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
52,600. p
4,590.00 p
2.00 p
16700
FESCUE
Mar-16
99,200.00 (G)
15,030.30 ,
_
6/17/16
43,400.00 (G)
6575,758
2.09
0.573
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
I FESCUE
6/20/16
43,400.00 (G)
6575.758
2.09
0.573
MHAEDL
DRY
0-<1/2"
SUR
0.5
0.30
56,500. p
7,660.00 p
2.00 p
18484
FESCUE
Jun-16
86,800.00 (G)
13,151.516
1 ULal vallonS/Ac: AZs,-L6i.6Z
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
105
0.018
0.012
1.561
2.979
0.222
0.006
0.033
0.138
0.030
4.862
90.01
Cumulative lbs/acre
0.048
0.032
3.994
7.289
0.516
0.016
0.083
0.375
0.080
10.898
s,
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
'
y I
=
s
209
{
4
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
'LAND APPLIER) DATE
alty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
�tion submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
t or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2017
Summit Environmental Technologies, Inc.
JO 3310 Win St.
f--UVlR0t4folP,'TALTF:CHNOLOGIEs;,Yy Cuyahoga Falls, Ohio44223
Arralyrcal Lsbarainaaa, TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httn://www.settek.com
May 03, 2016
Drew Culp/Reports&Invoices
Synagro, NC 28134
12701 Lancaster Hwy
Pineville, NC 28134
TEL: 704-752-8673
FAX: (704) 752-8736
RE: MT Holly WWTP
Dear Drew Culp/Reports&Invoices: Order No.: 16021266
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/19/2016 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Bachar Najm
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943,
Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana
04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New
Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001,
Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Region 8 8TMS-L, USDAIAPHIS P330-11-00244, Utah OH009232011-1,
Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010
Page 1 of 30
Summit Environmental Technologies, Inc. Case Narrative
summrr 3310 Win St.
FUVIRONNIEt,!tALIECW40LaG,155: utc. Cuyahoga Falls, Ohio 44223 WO#: 16021266
Ara;,ftir_a1 L:yi eraiur+e TEL: (330) 253-8211 FAX: (330) 253-4489
Website: htty.-1Avivw.settek.com Date: 5/3/2016
CLIENT: Synagro, NC 28134
Project: MT Holly WWTP
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Paginated Report including Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports, and copies of the Chain of Custody Documents are supplied with this
sample set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation
(LOQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Analysis performed by DBM, VRM, or SFG were performed at Summit Labs 2704 Eatonton Highway
Haddock, GA 31033
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report.
The information contained in,this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
This report is believed to meet all of the requirements of NELAC or the accrediting / certifying agency.
Any comments or problems with the analytical events associated with this report are noted below.
Analytical Comments for SVOC-BNA TCLP(8270), Sample LCS-18991, Batch ID 18991 : The TCLP
SVOC LCS (Batch 18991) exhibited high recovery for Surrogate: 2,4,6-Tribromophenol; All other
Revision v2
Page 2 of 30
Summit Environmental Technologies, Inc. Case Narrative
SUMMAIT 3310 Win St.
MVIzOMMEXIMLIECSNOLOG1ES,W(7. Cuyahoga Falls, Ohio44223 WO#: 16021266
Anai,.tii7al Ln1' araT"Or1eq TEL: (330) 253-8211 FAX: (330) 253-4489
Website: hyp:Uwww.settekcom Date: 5/3/2016
CLIENT: Synagro, NC 28134
Project: MT Holly WWTP
surrogates exhibited recoveries within Acceptance Limits.
Analytical Comments for tclp-svoc-herb_tclp(8151), Sample les-19008, Batch ID 19008 : The TCLP
Herbicides LCS (Batch 19008) exhibited high recovery for 2,4-D; All samples were ND.
Analytical Comments for TCLP-SVOC-Herb_TCLP(8321), Sample LCSD-R50514, Batch ID R50514 :
The TCLP Herbicides LCSD (Batch 50514) exhibited outlying recoveries and RPDs;
Analytical Comments for TCLP-SVOC-Herb_S(8321), Sample LCSD-R50630, Batch ID R50630 : The
TCLP Herbicides LCSD (Batch R50630) exhibited high recoveries; All samples were ND.
Analytical Comments for TCLP-SVOC-Herb_S(8321), Sample LCS-R50630, Batch ID R50630: The
TCLP Herbicides LCS (Batch R50630) exhibited high recoveries; All samples were ND.
Revision v2
Page 3 of 30
Summit Environmental Technologies, In Qualifiers and Acronyms
fT sumMIT 3310 Win 5
UAI ROWENTAL IZ'-H IOLO Tics, INC. Cuyahoga Falls, Ohio 442� WO#: 16021266
Angly cal Lzboratorlez. TEL: (330) 253-8211 FAX.- (330) 253-446
Website: htto://wivw.settekco. Date: 5/3/2016
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL '
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision v2
Page 4 of 30
Summit Environmental Technologies, Inc. Workorder
S IF 3310 Win St.
FIRVIR010,1E11,JYi13_r cir]La�;_s; ;pt�. Cuyahoga Falls, Ohio 44223 Sample Summary
l'ir,.afyticsf LEbaraform". TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 16021266
Website: hgpa/www.settekcom 03 May-16
CLIENT: Synagro, NC 28134
Project: MT Holly WWTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
16021266-001 MT. Holly WWTP 2/18/2016 2/19/2016 9:30:00 AM Sludge
Page 5 of 30
fr!SUMMIT
Summit Enviroi7mental Technologies, Inc. Analytical Report
3310 Win St.
`VIFONMENTALT_CIt OLaml :wi,-_ Cuyahoga Falls, Ohio44223 (base report)
Arralvtri73i Laf orafones TEL: (330) 253-8211 FAX.' (330) 253-4489 WO#: 16021266
Website: hyp.-11wiv19.settek.com Date Reported: 5/3/2016
CLIENT:
Synagro, NC 28134 Tag Number:
Matrix:
SLUDGE Collection Date: 2/18/2016
Lab ID:
16021266-001A
Project:
MT Holly WWTP
Client Sample ID MT. Holly WWTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 6.77 s.u.@20.3C 1 2/26/2016 3:59:00 PM
Qualifiers: `
Value exceeds Maximum Contaminant Level.
E
Value above quamitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Revision v2
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
U
Samples with CalcVal <MDL
Page 6 of 30
summloff-
Summit Environmental Technologies, Inc.
WO#:
16021266
rNVIR7NhIENIAL1.2cW40LZG;=5,zht:
3310 Win St.
Cuyahoga Falls, Ohio44223
Date Reported:
5/3/2016
I.r:alvtir-sl Laboratories
TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro, NC 28134
Website: htto:/hmwiv.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
2/19/2016
Project#:
MT Holly WWT
TCLP Metals Analysis (6010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
MT. Holly WWTP
001
2/18/2016 TCLP Arsenic(As)
0.500
ND mg/L
Sludge
EPA 6010 C
1
5.00
2/29/2016
VVK
MT. Holly WWTP
001
2/18/2016 TCLP Barium(Ba)
5.00
ND mg/L
Sludge
EPA 6010 C
1
100
2/29/2016
VVK
MT. Holly WWTP
001
2/18/2016 TCLP Cadmium(Cd)
0.100
ND mg/L
Sludge
EPA 6010 C
1
1.00
2/29/2016
VVK
MT. Holly WWTP
001
2/18/2016 TCLP Chromium(Cr)
0.200
ND mg/L
Sludge
EPA 6010 C
1
5.00
2/29/2016
VVK
MT. Holly WWTP
001
2/18/2016 TCLP Lead(Pb)
0.500
ND mg/L
Sludge
EPA 6010 C
1
5.00
2/29/2016
VVK
MT. Holly WWTP
001
2/18/2016 TCLP Selenium(Se)
0.500
ND mg/L
Sludge
EPA 6010 C
1
1.00
2/29/2016
VVK
MT. Holly WWTP
001
2/18/2016 TCLP Silver(Ag)
0.500
ND mg/L
Sludge
EPA 6010 C
1
5.00
2/29/2016
VVK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
MT. Holly WWTP 001 2/18/2016 TCLP Mercury 0.00200 ND mg/L Sludge EPA 7470 A 1 0.200 2/29/2016 MFW
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
MT. Holly WWTP
001
2/18/2016 Chlordane, total
0.0250 ND mg/L
Sludge
EPA 8081 B
1
0.0300
2/29/2016
JBN
MT. Holly WWTP
001
2/1812016 Toxaphene
0.0500 ND mg/L
Sludge
EPA 8081 B
1
0.500
2/29/2016
JBN
MT. Holly WWTP
001
2/18/2016 Endrin
0.00250 ND mg/L
Sludge
EPA 8081 B
1
0.0200
2/29/2016
JBN
MT. Holly WWTP
001
2/18/2016 gamma-BHC
0.00250 ND mg/L
Sludge
EPA 8081 B
1
0.400
2/29/2016
JBN
MT. Holly WWTP
001
2/18/2016 Heptachlor
0.00250 ND mg/L
Sludge
EPA 8081 B
1
0.00800
2/29/2016
JBN
MT. Holly WWTP
001
2/18/2016 Heptachlor epoxide 0.00250 ND mg/L
Sludge
EPA 8081 B
1
0.00800
2/29/2016
JBN
MT. Holly WWTP
001
2/18/2016 Methoxychlor
0.00250 ND mg/L
Sludge
EPA 8081 B
1
10.0
2/29/2016
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
MT. Holly WWTP
001
2/18/2016 1,1-Dichloroethene
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 1,2-Dichloroethane
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 MEK
2.00
ND mg/L
MT. Holly WWTP
001
2/18/2016 Benzene
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 Carbon tetrachloride
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 Chlorobenzene
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 Chloroform
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 Tetrachloroethene
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 Trichloroethene
0.100
ND mg/L
MT. Holly WWTP
001
2/18/2016 Vinyl chloride
0.200
ND mg/L
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
Sludge
EPA 8260 B 1
0.700 2/26/2016 MES
0.500 2/26/2016 MES
200 2/26/2016 MES
0.500 2/26/2016 MES
0.500 2/26/2016 , MES
100 2/26/2016 MES
6.00 2/26/2016 MES
0.700 2/26/2016 MES
0.500 2/26/2016 MES
0.200 2/26/2016 MES
Page 7 of 30
� -
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
16021266
P,IVIRONMEW6iLIECHNOLGGES. ;NtM
Cuyahoga Falls, Ohio44223
Date Reported:
5/3/2016
etr H ytlr_at Laboratories
TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro, NC 28134
Website: httP.-hivww.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
2/19/2016
Project#:
MT Holly WWT
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
MT. Holly WWTP
001
2/18/2016 1,4-Dichlorobenzene
0.200
ND mg/L
Sludge
EPA 8270 C
2
7.50
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 2,4,5-Trichlorophenol
0.500
ND mg/L
Sludge
EPA 8270 C
2
400
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 2,4,6-Trichlorophenol
0.500
ND mg/L
Sludge
EPA 8270 C
2
2.00
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 2,4-Dinitrotoluene
0.100
ND, mg/L
Sludge
EPA 8270 C
2
0.130
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 Cresols, Total
10.0
ND mg/L
Sludge
EPA 8270 C
2
200
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 Hexachloro-1,3-
0.100
ND mg/L
Sludge
EPA 8270 C
2
0.500
2/29/2016
CxA
butadiene
MT. Holly WWTP
001
2/18/2016 Hexachlorobenzene
0.100
ND mg/L
Sludge
EPA 8270 C
2
0.130
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 Hexachloroethane
0.200
ND mg/L
Sludge
EPA 8270 C
2
3.00
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 Nitrobenzene
0.200
ND mg/L
Sludge
EPA 8270 C
2
2.00
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 Pentachlorophenol
0.500
ND mg/L
Sludge
EPA 8270 C
2
100
2/29/2016
CxA
MT. Holly WWTP
001
2/18/2016 Pyridine
0.500
ND mg/L
Sludge
EPA 8270 C
2
5.00
2/29/2016
CxA
SVOC SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
MT. Holly WWTP
001 2/18/2016 2,4-D
5.00 ND mg/L
Sludge
EPA 8321 A
1
10.0
3/4/2016
BJH
MT. Holly WWTP
001 2/18/2016 2,4,5-TP
0.500 ND mg/L
Sludge
EPA 8321 A
1
1.00
3/4/2016
BJH
Page 8 of 30
Summit Environmental Technologies, Inc.
WO#:
16021266
WJ -,
3310 Win St.
FES* y
RNIVRONMENShLIEC-8W)LbutES,JNr,
Cuyahoga Falls, Ohio44223
Date Reported:
5/3/2016
Arar f.cal Lzilorarorles TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro, NC 28134
Website: htto://1vww.settek.com
Address:
12701 Lancaster Hwy
Pineville NC 28134
Received:
2/19/2016
Project#:
MT Holly WWT
Client ID# Lab ID# Collected Analyte
Result Units
Matrix Method DF RL Run Analyst
MT. Holly VVWTP 001
MT. Holly WVVTP 001
MT. Holly WVVTP 001
2/18/2016 Flashpoint (140°F)
2/18/2016 Cyanide, Reactive
2/18/2016 Sulfide, Reactive
>140 °F
Sludge
EPA 1010
1
2/22/2016
TAH
ND mg/Kg
Sludge
EPA 9014
1
0.500 2/26/2016
MS
ND mg/Kg
Sludge
EPA 9034
1
25.0 2/26/2016
MS
Page 9 of 30
Summit Environmental Technologies, Inc.
14"oftolhirt 3310Win St. QC SUMMARY REPORT
E:-NNI UNPUNIP,l. I I.i.3 ?&1L(t1J1!z'a.ING, Cuyahoga Falls, Ohio44223 WO#: 16021266
Anattdl.cai Laborwurie� TEL: (330) 253-8211 FAX- (330) 253-4489
Website: hUp:/hvww.sette1ccom 03 May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18975
Sample ID MB-18975
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 212912016
RunNo: 50370
client ID: PBW
Batch ID: 18975
TestNo: SW6010C SW3010A
Analysis Date: 2/2912016
SegNo: 790118
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.500
TCLP Silver(Ag)
ND
0.500
Sample ID LCS-18975
SampType: LCS
TestCode:
Mtl-TCLP-7(6 Units: mg/L
Prep Date: 212912016
RunNo: 50370
'lient ID: LCSW
Batch ID: 18975
TestNo:
SW6010C SW3010A
Analysis Date: 212912016
SegNo: 790119
4nalyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.10
0.500
2.000
0
105
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
105
80
120
TCLP Cadmium(Cd)
2.06
0.100
2.000
0
103
80
120
TCLP Chromium(Cr)
2.01
0.200
2.000
0
101
80
120
TCLP Lead(Pb)
2.10
0.500
2.000
0
105
80
120 -
TCLP Selenium(Se)
2.10
0.500
2.000
0
105
80
120
TCLP Silver(Ag)
0.920
0.500
1.000
0
92.0
80
120
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 10 of 30
Sununit Environmental Technologies, Inc. C SUMMARY REPORT
3310 Win St. `�
�:wlHarar+naNl+�J. wa:r.a�€attLu�tl a; Inr.ti. Cuyahoga Falls, Ohio44223 WO#: 16021266
ff1summm
l.�ai1 fi.caf Lab r so,rtt�s TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htto:/hvtvw.settefc.coni 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18981
Sample ID 16021355-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/29/2016
RunNo: 50368
Client ID: BatchQC
Batch ID: 18981
TestNo: SW7470A SW7470A
Analysis Date: 2/2912016
SegNo: 790066
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury 0.00419 0.00200 0.00400 0 105 75 125
Sample ID 16021355-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/2912016
RunNo: 50368
Client ID: BatchQC
Batch ID: 18981
TestNo: SW7470A SW7470A
Analysis Date: 2/29/2016
SegNo: 790067
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00415 0.00200 0.00400 0 104 75 125 0.00419 0.959 20
Sample ID MB-18980
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/29/2016
RunNo: 50368
Client ID: PBW
Batch ID: 18981
TestNo: SW7470A SW7470A
Analysis Date: 2/2912016
SegNo: 790128
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
TCLP Mercury ND 0.00200
Sample ID LCS-18980
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/29/2016
RunNo: 50368
Client ID: LCSW
Batch ID: 18981
TestNo: SW7470A SW7470A
Analysis Date: 2/29/2016
SegNo: 790129
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00403 0.00200 0.00400 0 101 80 120
Qualifiers: Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
Revision V2
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits Page 11 of 30
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
1; JM , 3310 Win St.
IHV'Nrrn,N I RL 91-.CIl-la-dULSJJItti,, INC Cuyahoga Falls, Ohio 44223 WO#: 16021266
Ana.tvUraf l ,Thorato,rir=s TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htto://wivw.setteh.com 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18981
Sample ID LCS-18980
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/29/2016
RunNo: 50368
DI]ent ID: LCSW
Batch ID: 18981
TestNo: SW7470A SW7470A
Analysis Date: 2/29/2016
SegNo: 790129
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighUrnit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: " Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 12 of 30
i
1 Sumnsit Environmental Technolo res, Inc.
3310 Win St. QC SUMMARY REPORT
LMYIH.0 Nb71; P, L.N. d d.C.` TAJLWJI1 :Si, JPtC. Cuyahoga Falls, Ohio 44223 WO#: 16021266
k, t rtlril.cai L;Tbo,rsto�Fe.. TEL: (330) 253-82I J FAX.(330) 253-4489
Website: htm:/hvwiv.setlek.conz 03-May-16
Client: Synagro, NC 28134
Projeet: MT Holly WWTP BatehID: 18984
Sample ID mb-18984 SampType: mblk TestCode: tclp-svoc-cpe Units: mg/L Prep Date: 2/29/2016 RunNo: 50380
I
Client ID: PBW Batch ID: 18984 TestNo: SW8081A SW3610C Analysis Date: 2/2912016 SegNo: 790297
Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua]
Chlordane, total ND 0.0250
Toxaphene
ND
0.0500
Endrin
ND
0.00250
gamma-BHC
ND
0.00250
eptachlor
ND
0.00250
Heptachlor epoxide
ND
0.00250
Methoxychlor
ND
0.00250
Sample ID Ics-18984
SampType: Ics
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 2/29/2016
RunNo: 50380
Client ID: LCSW
Batch ID: 18984
TestNo: SW8081A SW3510C
Analysis Date: 2/29/2016
SegNo: 790298
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
0.0286
0.00250
0.0250
0
115
20
157
C 0.0223
0.00250
0.0250
0
89.4
22
137
0.0257
0.00250
0.0250
0
103
24
121
epoxide 0.0259
0.00250
0.0250
0
104
27
152
or 0.0303
0.00250
0.0250
0
121
1
199
* Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
Revision v2
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits Page 13 of 30
F� wd Summit Environmental Technologies, Inc. QC SUMMARY REPORT
MIT 3310 Win St.
e ra:ulH,4aaru;r i.al. r:a�nar�auU rts; IRC Cuyahoga Falls, Ohio 44223 WO#: 16021266
naayrth.,z L baratrarte� TEL: (330) 253-8211 FAX. (330) 253-4489
Website: hgp.-Iliviv3v.settelf.com 03-11ay-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18984
Sample ID 16021331-001ams
SampType: ms
TestCode: tclp-svoc-cpe Units: mg/L
Prep Date: 212912016
RunNo: 50380
:lient ID: BatchQC
Batch ID: 18984
TestNo: SW8081A SW3510C
Analysis Date: 2/2912016
SegNo: 790299
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.0278
0.00250
0.0250
0
ill
20
157
gamma-BHC
0.0214
0.00250
0.0250
0
85.5
22
137
Heptachlor
0.0212
0.00260
0.0250
0
84.9
24
121
Heptachlor epoxide
0.0246
0.00250
0.0250
0
98.5
27
152
Methoxychlor
0.0274
0.00250
0.0250
0
110
1
199
'ample ID 16021331-001amsd
SampType: msd
TestCode: telp-svoc-cpe Units: mg/L
Prep Date: 2/29/2016
RunNo: 50380
'lient ID: BatchQC
Batch ID: 18984
TestNo: SW8081A SW3510C
Analysis Date: 212912016
SegNo: 790300
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Endrin
0.0218
0.00250
0.0250
0
87.1
20
157
0.0278
24.2
30
gamma-BHC
0.0179
0.00250
0.0250
0
71.4
22
137
0.0214
17.9
30
Heptachlor
0.0173
0.00250
0.0250
0
69.2
24
121
0.0212
20.3
30
Heptachlor epoxide
0.0195
0.00250
0.0250
0
77.9
27
152
0.0246
23.4
30
Methoxychlor
0.0212
0.00250
0.0250
0
84.6
1
199
0.0274
25.7
30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 14 of 30
-7�,:Zr. pw Summit Environmental Technologies, Inc. C SUMMARY REPORT
3310 Win ,St.
er<: INV P•ann:N J,AJ, 4 1atPNUL.r1J1t51 lh: Cuyahoga Falls, Ohio 44223 WO#: 16021266
Anal 1Phw-i1 L7boratarke:� TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htm✓/wwiv.setteh.com 03-May-I6
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18991
Sample ID MB-18991
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/29/2016
RunNo: 50394
client ID: PBW
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790622
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDL]mit Qua[
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0200
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Sample ID LCS-18991
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/29/2016
RunNo: 50394
'Iient ID: LCSW
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790623
knalyte,
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,4-Dichlorobenzene 0.745
0.100
1.000 0 74.5
10
134
2,4,5-Trichlorophenol 0.992
0.250
1.000 0 99.2
27
154
2,4,6-Trichlorophenol 1.01
0.250
1.000 0 101
27
154
2,4-Dinitrotoluene 0.942
0.0200
1.000 0 94.2
29
149
Cresols, Total ND
5.00
3.000 0 55.2
20
125
Hexachloro-1,3-butadiene 0.849
0.0200
1.000 0 84.9
14
126
Qualifiers: * Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
ReVIS10ri V2
MC Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits Page 15 of 30
_ Summit Environmental Technologies, bzc. n ���� //�� ,�� 77�� 7�
L 3310 Win St. QC SU1�11�1-tS.itY REPORT
L-NNIk4"rabiwr4l.IsVLLtIH ULUUJLS,;NS::. Cuyahoga Falls, Ohio44223 WO#: 16021266
I. � 6nali Wcwf Laborworip: r TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httv:/hviviv.settek.com 03-May-I6
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID• 18991
iample ID LCS-18991
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/29/2016
RunNo: 50394
;lient ID: LCSW
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790623
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Hexachlorobenzene
0.986
0.0200
1.000
0
98.6
1
162
Hexachloroethane
0.764
0.100
1.000
0
76.4
30
123
Nitrobenzene
0.887
0.100
1.000
0
88.7
25
190
Pentachlorophenol
0.777
0.250
1.000
0
77.7
4
186
Pyridine
ND
0.250
1.000
0
22.2
5
130
Sample ID 16021356-003AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/29/2016
RunNo: 50394
:;lient ID: BatchQC
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790626
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene 0.818
0.200
1.000 D 81.8
10
134
2,4,5-Trichlorophenol ND
0.500
1.000 0 0
27
154
S
2,4,6-Trichlorophenol ND
0.500
1.000 0 0
27
154
S
2,4-Dinitrotoluene 0.987
0.0400
1.000 0 98.7
29
149
Cresols, Total ND
10.0
3.000 0 58.9
20
125
Hexachloro-1,3-butadiene 0.947
0.0400
1.000 0 94.7
14
126
Hexachlorobenzene 1.08
0.0400
1.000 0 108
1
162
Hexachloroethane 0.832
0.200
1.000 0 83.2
30
123
Nitrobenzene 0.961
0.200
1.000 0 96.1
25
190
Pentachlorophenol 0.719
0.500
1.000 0 71.9
4
186
Pyridine ND
0.500
1.000 0 43.2
5
130
QMR
Qualifiers: Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O RSD is greater than RSDlimit
Revision V2
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
Page 16 of 30
Summit Environmental Technologies, Inc.
mmsuI g QC SUMMARY REPORT
3310 Win St.
L:r,A-1K,carT,1P;NIfM, 0'+:ch9Y•dauJS3tza.!NC Cuyahoga Falls, Ohio44223 WO#: 16021266
+I.rtatrti.c�i L:7Morar❑ri TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htto://www.sette%com 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18991
Sample ID 16021356-003AMSD
SampType: MSD
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/2912016
RunNo: 50394
-lient ID: BatchQC
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790627
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.722
0.200
1.000
0
72.2
10
134
0.8180
12.5
30
2,4,5-Trichlorophenol
ND
0.500
1.000
0
0
27
154
0
0
30 S
2,4,6-Trichlorophenol
ND
0.500
1.000
0
0
27
154
0
0
30 S
2,4-Dinitrotoluene
0.874
0.0400
1.000
0
87.4
29
149
0.9870
12.1
30
Cresols, Total
ND
10.0
3.000
0
51.9
20
125
0
0
30
Hexachloro-1,3-butadiene
0.853
0.0400
1.000
0
85.3
14
126
0.9470
10.4
30
Hexachlorobenzene
0.935
0.0400
1.000
0
93.5
1
162
1.082
14.6
30
Hexachloroethane
0.749
0.200
1.000
0
74.9
30
123
0.8320
10.5
30
Nitrobenzene .
0.859
0.200
1.000
0
85.9
25
190
0.9610
11.2
30
Pentachlorophenol
0.641
0.500
1.000
0
64.1
4
186
0.7190
11.5
30
Pyridine
ND
0.500
1.000
0
30.9
5
130
0
0
30 R
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 17 of 30
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
sumnin 3310 Win St.
LMVIH)NNII;hi:u- a �a ea taLU�i�s; WC Cuyahoga Falls, Ohio44223 WO#: 16021266
; nzaltq?-ml i_abo:rarvfies TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httU:/Avww.settelc.com 03 May-16
Client: Synagro, NC 28134
Project: NIT Holly WWTP BatchID: 18991
Sample ID LCS-18991
SampType: LCS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/29/2016
RunNo: 50371
client ID: LCSW
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790126
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.713
0.100
1.000
0
71.3
10
134 m
2,4,5-Trichlorophenol
0.996
0.250
1.000
0
99.6
27
154
2,4,6-Trichlorophenol
1.03
0.250
1.000
0
103
27
154
2,4-Dinitrotoluene
0.940
0.0200
1.000
0
94.0
29
149
Cresols, Total
ND
5.00
3.000
0
55.4
20
125
Hexachloro-1,3-butadiene
0.848
0.0200
1.000
0
84.9
14
126
Hexachlorobenzene
0.986
0.0200
1.000
0
98.6
1
162
Hexachloroethane
0.764
0.100
1.000
0
76.5
30
123 m
Nitrobenzene
0.887
0.100
1.000
0
88.7
25
190
Pentachlorophenol
0.790
0.250
1.000
0
79.0
4
186
Pyridine
ND
0.250
1.000
0
22.2
5
130
Sample ID MB-18991
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 212912016
RunNo: 50371
:lient ID: PBW
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790127
%nalyte
Result
PQL SPK value SPK Ref Val
%REC LowUrnit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene ND
0.100
2,4,5-Trichlorophenol ND
0.250
2,4,6-Trichlorophenol ND
0.250
2,4-Dinitrotoluene ND
0.0200
Cresols, Total ND
5.00
Hexachloro-1,3-butadiene ND
0.0200
Qualifiers: k Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M Manual Integration used to determine
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O RSD is greater than RSDlimit Revision v2
P Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits Page 18 of 30
r - Summit Environmental Technologies, Inc. QC SUMMARY REPORT
I , 3310 Win St.
r
<' Ix. rtrnav i ah I i:C,MilULQilI`S; !NiC. Cuyahoga Falls, Ohio 44223 WO#: 16021266
ArTztilrticRf La bor rwhr f TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http://wtvw.settelr.cont 03 May-l6
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: 18991
Sample ID MB-18991
SampType: MBLK
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/29/2016
RunNo: 50371
Client ID: PBW
Batch ID: 18991
TestNo: SW8270C SW3510C
Analysis Date: 2/29/2016
SegNo: 790127
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Hexachlorobenzene
ND
0.0200
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0,250
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 19 of 30
�-r-^ Summit Environmental Technologies, Inc.
�a ,yAMRIWAhox I T 3310 win St. QC SUMMARY REPORT
tc�rarnrnaiPk a i.� wtiuw�r,�s,.irtr�. Cuyahoga Falls, Ohio44223 WO#: 16021266
!1 rafiaErRf L 7uorwtorle5 TEL: (330) 253-8211 FAX.- (330) 253-4489
website: http:/hvrvw.settek.conz 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50088
Sample ID LCS-R50088
SampType: LCS
TestCode: FlashPt_S(10 Units: °F
Prep Date:
RunNo: 50088
'lient ID: LCSS
Batch ID: R50088
TestNo: SW1010
Analysis Date: 2/22/2016
SegNo: 784873
knalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Flashpoint (140°F) 83.0 77.00 0 108 100 110
Qualifiers: r Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to detennine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 20 of 30
Summit Environmental Technologies,Inc. QC SUMMARY REPORT
U M f, ni 3310 Win St.
LMVIKU NMUN i Al. a t;�r:rur,�uutrs�i�es; INC. Cuyahoga Falls, Ohio 44223 WO#: 16021266
r?aildl.aaf Lzbo,rgioriF�4 TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http://ivlvw.settek.coni 03 May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50283
Sample ID MB-R50283
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: PBW
Batch ID: R50283
TestNo: SW9034
Analysis Date: 212612016
SegNo: 788524
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Sulfide, Reactive ND 25.0
Sample ID LCS-R50283
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: LCSW
Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/26/2016
SegNo: 788525
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 81.8 25.0 86.00 0 95.1 85 115
Sample ID 16021626-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: BatchQC
Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/26/2016
SegNo: 788526
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 84.6 25.0 86.00 0 98.4 75 125
Sample ID 16021626-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: BatchQC
Batch ID: R50283
TestNo: SW9034
Analysis Date: 212612016
SegNo: 788527
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
82.6 25.0
86.00 0 96.0 75
125
84.60 2.39 30
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit Revision v2
P
Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits Page 21 of 30
Summit Environmental Technologies, Inc.IT 3310 Win St. QC SUMMARY REPORT
r lkc ramti:r Ifu, a r.� �r uLUt�a; artc Cuyahoga Falls, Ohio 44223
WO#: 16021266
f!.rr<ttl,rtl.raP TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: hqp.-1 www.settek.cotn 03-May-I6
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50283
Sample ID 16021626-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 50283
Client ID: BatchQC
Batch ID: R50283
TestNo: SW9034
Analysis Date: 2/2612016
SegNo: 788527
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: * Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits M Manual Integration used to determine
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit 0 RSD is greater than RSDlimit Revision V2
P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Page 22 of 30
Summit Environmental Technolo es, Inc.
��, F: 3310WinSt. QC SUMMARY REPORT
crovlrrr-"Nru:NM, a i:r atdUl_v+;i. s; irrc. Cuyahoga Falls, Ohio44223 WO#: 16021266
;1,,r,y1_,�L'.cal LaboyworFP6 TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httn://ivivii,.settelc.coni 03 May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID• R50284
Sample ID MB-R50284
SampType: MBLK
TestCode:
Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
Client ID: PBW
Batch ID: R50284
TestNo:
SW9014
Analysis Date: 2/2612016
SegNo: 788536
Analyte
Result
PQL
SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Cyanide, Reactive ND 0.500
Sample ID LCS-R50284
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
Client ID: LCSW
Batch ID: R50234
TestNo: SW9014
Analysis Date: 2/26/2016
SegNo: 788537
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.04 0.500 1.000 0 104 85 110
Sample ID 16021626-OD1AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
Client ID: BatchQC
Batch ID: R50284
TestNo: SW9014
Analysis Date: 2/26/2016
SegNo: 788539
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.01 0.500 1.000 0 101 85 110
Sample ID 16021626-OOIAMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
Client ID: BatchQC
Batch ID: R50284
TestNo: SW9014
Analysis Date: 2/26/2016
SegNo: 788540
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Cyanide, Reactive 0.965 0.500 1.000 0 96.5 85 110 1.010 4.56 20
Qualifiers: :k Value exceeds Maximum Contaminant Level. B Analyte detected in the associated Method Blank
H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits
MC Value is below Minimum Compound Limit. ND Not Detected at the Reporting Limit
P Second column confirmation exceeds PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
Revision V2
O RSD is greater than RSDlimit
R RPD outside accepted recovery limits Page 23 of 30
Summit Environmental Technologies, Inc. �C SUMMARY REPORT' p � �v 3310 Win St.
r_c.,airc r�rnr;n i. h a i.� rtt ciL[t 3r�s; ;r Cuyahoga Falls, Ohio 44223
_ _ pk.naairidc��i L.Ti?nr9ro,��e� TEL: (330) 253-8211 FAX.- (330) 253-4489
WO#: 16021266
Website: http://wiviv.settelr com 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50284
Sample ID 16021626-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 50284
Client ID: BatchQC
Batch ID: R50284
TestNo: SW9014
Analysis Date: 2/2612016
SegNo: 788540
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qua]
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 24 of 30
SUMIAIT
Summit Environmental Technologies, Inc.
3310Win St. QC SUMMARY REPORT
tri'AlIKU NMUN
I A6 A 1A:NWUL4i:i1:-S:
NC Cuyahoga Falls, Ohio 44223 WO#: 16021266
a
Lxibrp
-8211 FAX (330) 253-4489natVUmfP
Website: hitp://ivivw.settek.com 03-May-I6
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50317
Sample ID LCS 20PPB ABS022
SampType: LCS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
,lient ID: LCSW
Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/26/2016
SegNo: 789008
%nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
M-Dichloroethene
0.223
0.100
0.200
0
112
79.4
131
1,2-Dichloroethane
0.210
0.100
0.200
0
105
73.6
137
MEK
ND
2.00
1.00
0
104
55.1
163
Benzene
0.204
0.100
0.200
0
102
73.1
132
Carbon tetrachloride
0.215
0.100
0.200
0
107
63.7
139
Chlorobenzene
0.196
0.100
0.200
0
98.0
72.3
139
Chloroform
0.206
0.100
0.200
0
103
79.3
129
Tetrachloroethene
0.185
0.100
0.200
0
92.5
56.2
187
Trichloroethene
0.214
0.100
0.200
0
107
64.1
138
Vinyl chloride
- ND
0.200
0.200
0
95.3
22.1
147
Sample ID
LCSD 20PPB ABS02 SampType: LCSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
;lient ID:
LCSS02 Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/26/2016
SegNo: 789009
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
1,1-Dichloroethene
0.227
0.100
0.200 0 114
79.4
131
0.223 1.64
25
1,2-Dichloroethane
0.206
0.100
0.200 0 103
73.6
137
0.210 2.36
25
MEK
ND
2.00
1.00 0 95.2
55.1
163
0 0
25
Benzene
0.211
0.100
0.200 0 106
73.1
132
0.204 3.37
25
Carbon tetrachloride
0.222
0.100
0.200 0 ill
63.7
139
0.215 3.07
25
Chlorobenzene
0.200
0.100
0.200 0 100
72.3
139
0.196 2.22
25
Chloroform
0.206
0.100
0.200 0 103
79.3
129
0.206 0.146
25
Qualifiers: *
Value exceeds Maximum Contaminant Level.
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
Revision V2
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
0
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 25 of 30
s
Summit Environmental Technologies, Inc.
umftn3310 Wit St. QC SUMMARY REPORT
L!91HQrarv;N1Al. ,JNC; Cuyahoga Falls, Ohio44223 WO#: 16021266
A.,at4,tf.caf L bo,raior er TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http:/hvivw.settekcom 03 May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50317
Sample ID
LCSD 20PP13 ABS02 SampType: LCSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
'lient ID:
LCSS02 Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/26/2016
SegNo: 789009
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
Tetrachloroethene 0.193 0.100 0.200 0 96.3 56.2 187 0.185 4.03 25
Trichloroethene 0.216 0.100 0.200 0 108 64.1 138 0.214 1.07 25
Vinyl chloride ND 0.200 0.200 0 95.4 22.1 147 0 0 25
Sample ID MBLK
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
,lient ID: PBW
Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/26/2016
SegNo: 789010
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.100
1,2-Dichloroethane
ND
0.100
MEK
ND
2.00
Benzene
ND
0.100
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
0.100
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.200
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
B Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 26 of 30
t` Summit Environmental TechnoloWrac.
331OWininSt. QC SUMMARY REPORT
era IIKV'Nmur%,uki- R ia;MNULUC]I-'b,.INC. Cuyahoga Falls, Ohio 44223 WO#: 16021266
_ Ai a( fla'if Laborstorir:� TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: httl2:llwwiv.sett6lc.coni 03 May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID• RS0317
Sample ID 16021599-001ams
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
client ID: BatchQC
Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/2612016
SegNo: 789025
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.209
0.100
0.200
0
104
39.9
160
1,2-Dichloroethane
0.190
0.100
0.200
0
94.8
42.5
157
MEK
ND
2.00
1.00
0
102
16.6
227
Benzene
0.192
0.100
0.200
0
96.2
38.1
155
Carbon tetrachloride
0.201
0.100
0.200
0
101
40.8
162
Chlorobenzene
0.182
0.100
0.200
0
90.8
35.7
168
Chloroform
0.187
0.100
0.200
0
93.4
18.3
199
Tetrachloroethene
0.185
0.100
0.200
0
92.4
10
261
Tiichooroethene
0.231
0.100
0.200
0
115
23.8
175
Vinyl chloride
ND
0.200
0.200
0
80.1
10
165
Sample ID 16021599-001amsd
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
client ID: BatchQC
Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/26/2016
SegNo: 789026
�nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.210
0.100
0.200 0 105
39.9
160
0.209 0.526
25
1,2-Dichloroethane
0.199
0.100
0.200 0 99.6
42.5
157
0.190 4.89
25
MEK
ND
2.00
1.00 0 97.5
16.6
227
0 0
25
Benzene
0.198
0.100
0.200 0 99.1
38.1
155
0.192 2.97
25
Carbon tetrachloride
0.206
0.100
0.200 0 103
40.8
162
0.201 2.16
25
Chlorobenzene
0.193
0.100
0.200 0 96.5
35.7
168
0.182 6.03
25
Chloroform
0.199
0.100
0.200 0 99.6
18.3
199
0.187 6.32
25
Qualifiers: *
Value exceeds Maximum Contaminant Level,
B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
J
Analyte detected below quantitation limits
M
Manual Integration used to determine
MC
Value is below Minimum Compound Limit.
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
Revision V2
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
Page 27 of 30
S
Summit Environmental Technolo ies, Inc.
U M m 3310 Win St. QC SUMMARY REPORT
LNNIH:UNM1;rJirtl. A I;C"NULUJH:s, VC Cuyahoga Falls, Ohio44223 WO#: 16021266
y_ !4 zr(4-, ; rRf Lzbor.9lorrca TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http://lvivw.settelc.com 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50317
Sample ID 16021599-001amsd
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 50317
client ID: BatchQC
Batch ID: R50317
TestNo: SW8260B
Analysis Date: 2/26/2016
SegNo: 789026
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Tetra chloroethene 0.190 0.100 0.200 0 95.2 10 261 0.185 2.99 25
Trichloroethene 0.212 0.100 0.200 0 106 23.8 175 0.231 8.59 25
Vinyl chloride ND 0.200 0.200 0 84.0 10 165 0 0 25
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits
Revision v2
Page 28 of 30
Et Summit Environmental Technologies, Inc. (� r SUMMARY 771tr nTnORr�,
3310 Win St. QC S l.J 1V11�' AR i REPORT
tNVIrtar•1rnlaNIPI,91;CHNULrJ'jK:S;1N'C Cuyahoga Falls, Ohio44223
WO#: 16021266
?1,.r:-tf4�2�'.cr7f C:Tia��.r9ro,rrr� r TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: hU12.-1 vivtiv.sette&cont 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID• R50630
Sample ID 16021626-001AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID: BatchQC
Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 798230
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
2,4-D
57.6
5.00
50.00
0
115
37
105
S
2,4,5-TP
61.8
0.500
50.00
0
124
38
106
S
Sample ID 16021626-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID: BatchQC
Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 798231
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D 57.1 5.00 50.00 0 114 10 150 57.56 0.855 30
2,4,5-TP 61.7 0.500 50.00 0 123 10 150 61.78 0.190 30
Qualifiers: * Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
P Second column confirmation exceeds
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected at the Reporting Limit
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine
R0V1SlOri V2
0 RSD is greater than RSDlimit
R RPD outside accepted recovery limits Page 29 of 30
Summit Environmental Technologies, Inc. QC SUMMARY REPORT
j'
3310 Win St.
er:;v�rs�aNPUNIRI.0J.i-- N1JL41J1_1S:M Cuyahoga Falls, Ohio44223 WO#: 16021266
aina(vtlu3f L.Tbar.gtu.6eF TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http://iviviv.settelc.coni 03-May-16
Client: Synagro, NC 28134
Project: MT Holly WWTP BatchID: R50630
Sample ID MB-R50630
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID: PBW
Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 795495
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D ND 5.00
2,4,5-TP ND 0.500
Sample ID LCS-R50630
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID: LCSW
Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 795496
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
2,4-D
56.9
5.00
50.00
0
114
37
105
S
2,4,5-TP
59.2
0.500
50.00
0
118
38
106
S
Sample ID LCSD-R50630
SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 50630
Client ID: LCSS02
Batch ID: R50630
TestNo: SW8321A
Analysis Date: 3/4/2016
SegNo: 795497
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 56.4 5.00
50.00 0 113 37
105
56.92 0.912
30 S
2,4,5-TP 62.0 0.500
50.00 0 124 38
106
59.23 4.61
30 S
Qualifiers: * Value exceeds Maximum Contaminant Level.
B Analyte detected in the associated Method Blank
E
Value above quantitation range
H Holding times for preparation or analysis exceeded
J Analyte detected below quantitation limits
M
Manual Integration used to determine
Revision v2
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P Second column confirmation exceeds
PL Permit Limit
R
RPD outside accepted recovery limits
Page 30 of 30
=r-r-11SUMMIT
CNVIR0Mmt:N'rAL 'i EQHN0L0GI ES. iNr-,
33Yfl WJtn Street
Analysis Request f Chain of Custody
For Sumutit 13aviroYtmental Technologies,1w. use only
Page- f of f
SI=ENE -
CSicin Nanrc
S na ro Certtra4
Prr�jty t Ittt ntiticatian
i 77. f OL-L t( UW7p
Address
92
�
t h•
Q
fl
1z fl
II
i �
�
Anal PAramet.m
andM1tid5
Client Address
y Pinov111e NC, 28134
12701 Lancswr 4w
1,
•
Client Phone
704-752-8673
Report 1b
DREW
Cllen[ Fax No, / In Receive Ilccults by Fax ;
704-762 srsso
Pb NUMIler
1 d
Con Iar.1 P n nn
GiL'
Quu1r Noinbur
&,mVled Byf.V
OMW L.LW,,y
if Ohio VAP Samples
Sample Ideatitientiai
Date
:cam dr
"'
-led
a G. o -170 of
t7d-f$-
SL
r
x
l
i
. Re11tt
ubbad b
1%tc
Time
Received
by -.)Ale
Thne
Notes, I Comment$:
Received in >i ab by.
I Date
Time
Rush Regnestedt _ Day(s)
lotus[ be ap roved h+ Lab majulger
U
D47
Rev. 1s
Summit Environmental Technologies, Inc.
Cooler Receipt Form
04H6rtr.
Initials of person inspecfing cooler and samples:
�
Client
Order €Number, ! a 2.i,e U
Date Received: /fF Time Received: '7
Date coolers) opened and samples Inspected:
Number of CoolerslBoxes:
NIA
Shipper: D�C UPS DHL Airborne US Postal
Walk-in Pickup Other.
Packaging: Peanuts bl Paper Foam None Other.
Tape on coolerlbox:
N NIA
Custody Seals Intact
Y dp N/A
C-O-C in pl tj
N NIA
ice t/ l3tue ice
present / absent I melted NIA
Sample Temperature IR Gun 916020469 CF L °C
y 'C N/A
Radiofogicai Testing Instrument serial #35127
Y N
(see page 2 for scan results)
—Use 4 sheet per sample for Radiological Testing. Ifsample is HOT, the Radlological Safety Officer mast be natilled
Immediately.
C Q C filled out properly
N NIA
Samples in separate bags
N NIA
Sample containers intact`
Y,�/ N NIA
*If no, list broken sarnple(s):
Sample label(s).complete (ID. date, etc.)
6
N
N/A
Labet(s) agree with C-O-C
e
N
N/A
Correct containers used
N
NIA
Sufficient sample received
N
NIA
Samples receFvsd within holding time
G/
N
Bubbles absent from 40 mL vials"
Y
N
NIA
"Samples with bubbles <6mm are accr..piable.
Indicate bubble size i€>6mm.
Was client contacted about samples
Y N
Will client send new samples
Y N
Client contact
Datemme:
Logged in by:
Comments:
Page 1 of 2
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number:
WWTP Name: Mt Holly WWTP NPDES Number:
Monitoring Period: From 01/01/16 To 04/30/16
WQ 0001863
NCO021156
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
H nnnlienhle to niternntive nP.rfnrmerl Wines A nr C19QQ Rl rmmn1PtP fhP fallnwina mnnifnrina dhfa-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
Coliform
power per gram
MPN
157,342
161,435
163,349
MPN/g
0
event
sludge
SM9221E
of total solids
CFU
CFU/g
quarterly
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Jonathan Jordan / ORC
Prep r Name and Tit (type or print)
ignature o r er* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
PRO h4PT•ACCLI RATE• REUTAE3L.E
LABORATORIES, INC
WN"N'TAR LARS.COM
REPORT OF ANALYSES
Attri: DREW CULP
SYNAGRO PROJECT NAME: FEB 16
12701 LANCASTER HWY DATE: 03/17/16
PINEVILLE, NC 28134-
SAMPLE NUMBER- 122363 SAMPLE ID- MT. HOILY 50-1701 1ST EVENT SAMPLE MATRIX•- SO
DATE SAMPLED- 02/18/16 TIME SAMPLED- 0815
DATE RECEIVED- 02/18/16 SAMPLER- DC RECEIVED BY- DJ
TIME RECEIVED 0927 DELIVERED BY- DC TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 02/18/16 1500 RE 161,435 MPN/g
LABORATORY DIRECTOR �i.r 7_.r-•"Z�-�"'
P.O. Box 411483 • Charlotte, NC 28241-1483
Plione: (704) 588-8333 , Ftex: (704) 588-8335
PA
PROMPT -ACCURATE- RELIABLE
LEiBOItATORIES, INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NO Cert # 20; SC Cert # 99003001
�LIENT NAME
SAMP,�LE DATE
MOM
RNALYSIS .� �, �
AN,i4LYSiS METN�DDMRI
� � - • - +
A, •`
122363
1
4,066
2.55%
159,539.39
2
4,084
2.50%
163,348.65
3
4,116
2.52%
163,321.84
4
4,141
2.65%
162,383.79
5
4,066
2.49%
1 163 277.53
6
3,949
2.51%
167,341.95
7
4.088
2.54%
160,934.52
PFftbi Coljfdrm W
L5. -f
Geotnetr�e I1lieara •
PAR CHAIN OF CUSTODY
ueaRaro»,as uva PAR Laboratories, Inc
Phone (704) 588-8333
www.parlabs.com Fax (704) 588-8335
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It Is essential that all Information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North
Company Name (billing) Comments/
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State & zip code
€'INEVILLE NC 28134
Point of Contact It Telephone Number
DREW r-uLP 7ot4-57'f-52Q j
taken By: SIGNATURE
ft
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES k NO
*Sample Type: DW WW GWMW HW Soil Other
Sample Temp at time of sampling: a C Sample Temp upon receipt: 0 C
"Field Preserved: Yes _No _Teflon Liner/Zero Headspace: Yes No _ nla
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
(lent Sample I.D.
(Sample Location I Number)
Camp
Grab
Prasew.
set Up
Date/Time
Collection
Date/Time
Analyses
Requested
m , L Z o/
X
02-I t3 -I(o
09 : 5'
C44- Goy
�t}`fi
AST i' .2.0
W /77f
!Yi -3 S aF
nnIuiyuiz+unu u vaiei I lit It: Uarer I Ime
oa-W-IG40q; 2
Relinquished by. Datemme Received by: Datemme
"C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste -See
Outer Side
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 05/01/16 To 06/30/16
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf annlicahle to alternative nerformed (Class A or Class M comnlete the following, monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
th
2x10 to the 6
Coliform
power per gram
MPN
381,219
386,385
389,848
MPN/g
0
event
sludge
SM9221E
of total solids
CFU
CFU/g
quarterly
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Mt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Jonathan Jordan / ORC
Pre er Name and T' le (type or print)
ignature of rep er* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
P AA11 R
PROM PT•ACCU RATE -RE LIABLE
LABORATORIES, INC
WNVMV PARLABS.COM
R EPORT OF ANALYSES
Attn: DREW CULP
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: APR 16
DATE: 05/31/16
SAMPLE NUMBER- 122988 SAMPLE ID- CITY OF MT. HOLLY 2ND EVENT SAMPLE MATRIX- SO
DATE SAMPLED- 04/19/16 TIME SAMPLED- 0940
DATE RECEIVED- 04/19/16 SAMPLER- DC RECEIVED BY- DJ
TIME RECEIVED- 1145 DELIVERED BY- DC TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
FECAL COLIFORM (GEOM. MEAN)
ANALYSIS
METHOD DATE TIME BY RESULT UNITS
SM 9221 E 04/19/16 RE 386,385 MPN/g
LABORATORY DIRECTOR
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: (704) 588-8333 • Fax: (704) 588-8335
PAF;Z
PROMFT•ADC;URATE• RELIABLE
I.ABOIZATO.RIES, INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
SYNAGRO
CITY OF MT. HOLLY 2ND EVENT
04/19/16
FECAL COLIFORM, GEOMETRIC MEAN
• • SM 9221 E
10122988
1
.
8,077
2.08%
389,058.75
2
7,995
2.07%
385,825.85
3
7,987
2.08%
383,975.43
4
8,031
2.06%
389,848.93
5
7,929
2.08%
381,219.07
6
8,089
2.09%
387,021.30
7
8,028
2.07%
387,815.06
Fecal Coliform
Geometric Mean= _; •
LLAF? CHAIN ®F CUSTODY
OORATOMEs,rNc. PAR Laboratories, Inc
Phone (704) 588-8333
www.partabs.com Fax (704) 588-8335
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR laboratories, Inc. and the North
t,aronna Ue arrment or tnYlronmental ana Natural Kesources.
Company Name (billing) Comments/ Special Instructions
SYNAGRO CENTRAL
Address
12701 LANCASTER HWY
City, State Et zip code
PINEVILLE NC 28134
Point of Contact Et Telephone Number
D99W CUL_P 704-5711-5-2?1
Sample
Taken By: SIGNATURE
PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO
*Sample Type: DW WW GWMW HW Soil other
Sample Temp at time of sampling: 0 C Sample Temp upon receipt: ° C
"Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No _ n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
(lent Sample I.D.
Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/rime
Collection
Dateri-ime
Analyses
Requested
G/ OF N7 h- &
X
o •qo
� � Coc�Fc,
,01(o
Cse-
oy: uatei 11 rtecely )y: DatelTime
by: Datelftime Received by: Date/Time
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste **See
Other Side
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt Holly WQ Permit Number: WQ 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 07/01/16 To 09/30/16
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf a,.,,l—hlo 4n al*orna4ivn nnrf--A !('lace A nr ('lace R) rmmnlrte thr fnllnwinv mnnitnrina rlatn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency'
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6t
Coliform
power per gram
MPN
249,517
302,287
354,440
MPN/g
0
event
sludge
SM9221B
of total solids
CFU
CFU/g
quarterly
sludge
SM9222D
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake)
Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1.106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Jonathan Jordan / ORC
Prep r Name and Title (type or print)
a�6 17
(5Z of P e er* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
RA R
PRO h7PT•ACCURATE• RELIABLE
LABORATORIES, INC
1YWWPARLA6S.CON1
Attn: DREW CULP
SYNAGRO
12701 LANCASTER HWY
PINEYIL•LE, NC 2.8134-
REPORT OF ANALYSES.
PROJECT NAME: JUL 16
DATE: 08/19/16
SAMPLE NUMBER- 124172 SAMPLE ID- MT. HOLLY WWTP 50-1701 3RD EV SAMPLE MATRIX- SO
DATE SAMPLED- 07/28/16 TIME SAMPLED- 0930
MATE RECEIVED- 07/28/16 SAMPLER- DC RECEIVED BY- CT
TIME RECEIVED- 1011 DELIVERED SY- DC TYPE SAMPLE- Grab
Page 1 or 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORI✓ (GEOM. MEAN) SM 9221 E 07/28/16 1550 RE 302,287 MPN/g
LABORATORY DIRECTOR `is -r_,-
P.O. Box 411483 • Charlotte, NC 28241-1483
Phone: (704) 588-8333 • Fax: (704) 588-8335
PAFZ
PROMPT•ACCU RATE- RELIABLE
LABORATORIES INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
SYNAGRO
MT. HOLLY WWTP 60-1701 3RD EVENT
07/28/16
FECAL COLIFORM, GEOMETRIC MEAN
SM 9221 E
1
6,734
1.90%
354,440.08
124172
2
4,969
1.91 %
260,450.29
3
5,907
1.91%
309,256.74
4
5,832
1.91 %
305,359.23
5
6,602
1.90%
347,449.03
6
4,741
1.90%
249,517.60
7
5,859
1.92%
305,175.78
-- - - -- -- ---'-' --I
Fecal Coliform
Geometric Mean= _j
>�
GRAIN! OF CUSTODY
PAA Phone (704) 588-8333
PROMPT'ACCUR4TE*RELfABLE Fax (704) 588-8335
LABOR.ATORIES, INC
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
it is essential that all information be recorded on this Chain of Custody document for acceptance by PAR taboratoriPs_ Inn nnrr rha M—fh
yarouna ue arunenr or cnvrronmemar
r
mpany Name (billing)
Address
,270/
City, State Et zip code
Point of Contact & Telephone Number
f�22r.� G4 0 ?° `l - S7,1 - S zy/
Comments/ Special Instructions
sampie
Taken By: SIGNATURE PRINTED NAME !i Cu
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
*Sample Type: Dw ww GVVMW HW Soil other
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes No Teflon Liner/Zero Headspace: Yes No _ n/a
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (Y/N):
tientSample I.D.Setp
Sample Location / Number)
Italy
Cotle;'ibn ",
Preserv. Date -rime Datefi-ime
aif
ec Yrest ii""
jLLn/ WW 1Up
i_tL%-'j�
��co.� GO��ir✓h
3a (r w4
j
M ry 2
wl
Relinquished by:
Datemme
* C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Mt
WWTP Name: Mt
Monitoring Period:
Holly WQ Permit Number:
FIolly WWTP NPDES Number:
From 10/01/16 To 12/31/16
VQ 0001863
NCO021156
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlirnhle to niternative nerfnrmed (( ncc A nr Class R) rmmnlete the fnllnwino mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6
Coliform
power per gram
NUN
341,941
346,491
350,020
MPN/g
0
event
sludge
SM9221E
of total solids
CFU
CFU/g
quarterly
sludge
SM9222D
1000 NUN per gram of
total solids (dry weight)
MPN/g
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Mt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt: 5
Optiori.Wt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Jonathan Jordan / ORC
Preparer ame and Title (type or print)
S' ature of P er* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Late
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
PAR
PROM PT-ACCU RATE -RE LlASLE
LABORATORIES, INC
W WW.PARLABS.00M
REPORT OF ANALYSES
Attn: DREW CULP
SYNAGRO
12701 LANCASTER HWY
PINEVILLE, NC 28134-
PROJECT NAME: SEP 16
DATE: 11/01/16
SAMPLE NUMBER- 124968 SAMPLE ID- MT HOLLY SAMPLE MATRIX- SO
DATE SAMPLED- 09/26/16 TIME SAMPLED- 1100
DATE RECEIVED- 09/26/16 SAMPLER- MP RECEIVED BY- DJ
TIME RECEIVED- 1210 DELIVERED BY- MP TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
30 DAY BENCH SCALE TEST VAR 09/26/16 RE ATTACHED
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 09/26/16 1600 RE 346,491 MPN/g
'-'� •� f f_^,%yam
LABORATORY DIRECTOR
P.O. Box 411483 - Charlotte, NC 28241-1483
Phone: (704) 588-8333 • Fax: (704) 588-8335
AM
RAA R
PROMPT•ACCURATE•RELIA9 LE
I.ABORATORSES, INC
WWW. PARLABS. COM
30 Day Bench Scale Extended Aeration Test
Percent !Volatile Solids Reduction
CLIENT NAME: -
�SA�MPLE
��SAMPLE # a. * ;
START DATE:
i • M..
Start: End:
TS ()
0.2035
0.1941
TS% .
1.51 %
1.49%
VS ()
0.1447
0.1346
VS%
71.11%
69.35%
IN
0,004214
OUT
0.00397164
FSVR (Mass Balance)
5.74%
FSVR (Van Kleeck)
8.07%
FSVR (Mass Balance) <15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box411483 ® Charlotte, NC 28241-1483
Phone: (704) 588-833 3 0 Fax: (704) 588-8335
RA
PROMPT'
ACCURATE- RELIABLE
LABOPUNTOP-MSS INC
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert# 20; SC Cert # 99003001
WENT NAMEc• `
- •
tSAMPLE ID °
SAMPLE. DATE: {
ANALYSIS-
I&YAWN
•
GEOMETRIC
FECAL COLIFORM,
"LYjMt-TjHQP,,4wn"wM
•
�
o e
e e
•
124968
1
5,237
1.51 %
346,799.82
2
5,176
1.50%
345,082.57
3
5,202
1.49%
349,128.28
4
5,250
1.50%
350,020.35
5
5,224
1.50%
348,263.52
6
1 5,199
1 1.51 %
344, 274.17
7
1 5,198
1 1.52%
341, 941.13
Feeal_Coliform
�Geoti%etric Mepn= 1 • •
CHAIN OF CUSTODY
Phone (704) 588-8333
P R r3 M tyP•AQCLIRaT Fax (704) 588-8335
L-A-BORATORiES, I1%TC
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custndv dnaumanr fnr --+— — h„ oe o I —
t:am"na uepartment of Lnvironmentai and Natural Resources
C�any Nam (billing)
U
Add s�
/-/ 'a Z:
City, State rt zip code
IN06 -2) 7
Point of Contact $ Telep one Number
Comments/ Special Instructions
aafnple
Taken By: SIGNATURE PRINTED NAME
ARE SAMPLES FOR STATE or EPA REPORTING? YES NO
`Sample Type: DW ww GWtVW Nw Soil other v
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
"Field Preserved: Yes No _Teflon LinerlZero Neadspace: Yes No _ nla
Residual Chlorine checked at time of sampling (YIN): Dechlorination Necessary (YIN):
Iient Sample'D.
Sample Loca#]ott /Number)
."CarA
7
'.GiaE3
-R�esety:
Set f7:
ll'ateliJme
Calleciio6'
aateTmie
ReRa�st'ech j ;`
: ' -fry f..•
r ,'of/y 20
� /.,
(; lJ
i y D telTime Heceived by: uatei i ime
R linauished bv.— Datefr-ime Received by: Date/Time
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=hazardous Waste
Agricultural Lime Application Log
2016
Project: Mt. Holly 50-1701 * lime has been ordered
Field
Grower
Soil
Lime Requirement
Tons/Acre
Date
(state -county -site -field)
pH
(from soil analysis)
Applied
Applied
[Total
Acres
NU-CAA-41-Ub
vreg Springs
6./
1 0 tons/acre
N/A
N/A
NC-GA-41-10
Greg Springs
6.4
0 tons/acre
N/A
N/A
NC-GA-41-14
Greg Springs
6.3
0 tons/acre
N/A
N/A
NC-GA-45-01
David Allen
5.9
0 tons/acre
N/A
N/A
NC-LT-46-01
Tony Jones
6.2
0 tons/acre
N/A
N/A
NC-LT-46-02
Tony Jones
6.0
0 tons/acre
N/A
N/A
NC-LT-46-03
Tony Jones
6.3
0 tons/acre
N/A
N/A
NC-LT-46-04
Tony Jones
6.3
0 tons/acre
N/A
N/A
NC-LT-46-07
Tony Jones
6.4
0 tons/acre
N/A
N/A
NC-LT-46-08
Tony Jones
6.1
0 tons/acre
N/A
N/A
TOTAL 1 0.0
Page 1 of 2
Report Number: 17-003-0913
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Waypointo
ANALYTICAL
"Every acre... Every year."rM
Date Received: 01/03/2017 Date Of Analysis: 01/04/2017
Farm ID: NC-GA-41
SOIL ANALYSIS REPORT
Date Of Report: 01/06/2017
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax 804-271-6446
www.waypointanalytical.com
Grower: Greg Springs
Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Sample ID
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Field ID
Lab
Number
%
Rate
Soil
Class
Ib/A
s
M3
ppm Rate
ppm Rate
ppm Rate
K
ppm Rate
Mg
ppm Rate
Ca
ppm Rate
Na
ppm Rate
Soil
pH
Buffer
Index
H
meq/100g
megl100g
06
05850
5.4
H
146
51 H
NC = 42
37 VL
NC = 19
270 VH
1088 M
43 L
6.7
0.4
8.4
MIN
10
05851
8.7
VH
150
91 H
NC = 76
45 VL
NC = 23
343 VH
1268 M
36 VL
6.4
0.9
10.4
MIN
14
05852
7.4
VH
150
82 H
NC = 68
30 VL
NC = 15
350 VH
12116 M
39 VL
6.3
1.1
10.7
MIN
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble salts
Sample ID
Field ID
K
%
Mg
%
Ca
%
Na
%
H
%
NO,N
ppm Rate
S
ppm Rate
Zn
ppm Rate
Mn
ppm Rate
Fe
ppm Rate
Cu
ppm Rate
B
ppm Rate
SS
ms/cm Rate
06
1.1
26.8
64.8
2.2
4.8
14 L
NC=29
8.6 VH
NC=215.0
39 H
NC=244
77 VH
4.8 VH
NC=240.0
0.5 L
10
1.1
27.5
61.0
F.5
8.7
16 M
NC=33
14.8 VH
NC=370.0
33 H
NC=2)6
79 VH
5.3 VH
NC=265.0
0.8 M
14
0.7
27.3
60.1
1.6
[10.3
16 M
NC=33
15.1 VH
NC=377.5
31 H
NC=194
90 VH
5.9 VH
NC=295.0
0.7 M
values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. me GCoivy/
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: " o
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: WaypolntAnalytical Virginia, Inc.
Pauric McGroary
Page 2 of 2
Report Number: 17-003-0913
Account Number: 00015
Send To: Synagro Central LLC/ MT Holly
Wayne Brady
12701 Lancaster Highway
Pineville NC 28134
Date Received: 01/03/2017
Date Of Report: 01/06/2017
o
Waypoint,"
ANALYTICAL
"Every acre... Every year. "TM
Farm ID: NC-GA-41
SOIL FERTILITY RECOMMENDATIONS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Grower: Greg Springs
Sample ID
Yield Goal
Lime
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Field ID
Intended Crop
Tons
Tons/A
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
06
Fescue Hay
4
0.0
50
30
250
0
15
0
0
0
0
0
10
Fescue Hay
4
0.0
50
30
250
0
13
0
0
0
0
0
14
Fescue Hay
4
0.0
50
30
250
0
13
0
0
0
0
0
Comments:
Sample(s) : 10,14 Crop: Fescue Hay
Apply additional 50 pounds of nitrogen after every cutting and harvest of hay.
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary
NCDA&CS i— ___omic Division Phone: (919) 733-2655
Predictive
}t Soil Report
VVeosite: wwW.n....y..,jov/agronomi/ Report No. FYT.---30494
Client: David Allen Advisor: Synagro
110 Helton Rd 12701 Lancaster Hwy
Cherryville, NC 28021 Pineville, NC 28134
Mehlich-3 Extraction
Sampled County : Gaston
Sampled: Received: 07/12/2016 completed: 07/20/2016
Fans: NC-GA-45
Links to Helpful Information
Sample ID: 01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 80
60
0
0
0 0
0 0
Note: 12
1.00 tons/acre; 10/2015
2-
Test Results [units - W[V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.46 1.04 8.6 86 1.2 5.9 25 37 59 24
36 888
550
97 97
109 0.1 1
North Carolina
�iiN;it�i�:r Jn»c Fi�mcl �Gn�ntuirs:;lc�io
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox
NCDA&CS / _..omic Division Phone: (919) 733-2655 Website: www.r _ jov/agronomi/ Report No. FY1 , -oL-uD0494
David Allen
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi16bpart4.htmY sFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizei
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%o, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomiluyrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index
Page 1 of 1
Report Number: 16-084-0666
Account Number: 00015
Send To: SYNAGRO CENTRAL/MT HOLLY
WAYNE BRADY
12701 LANCASTER HWY
PINEVILLE NC 28134
Waypoint0
ANALYTICAL
"Every acre... Every year.
SOIL ANALYSIS REPORT
Date Received: 03/24/2016 Date Of Analysis: 03/25/2016 Date Of Report: 03/25/2016
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 a Fax 804-271-6446
www.waypointanalytical.com
Grower: TONY JONES
NC-LT-46
MT HOLLY 50-1701
Analytical Method(s): Mehlich 3 Lime Index Loss On Ignition Water pH
Sample ID
Lab
OM
WN
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Field ID
Number
%
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Rate
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
01
24652
6.8
150
194 VH
90 L
177 M
1604 H
20 VL
6.2
1.4
11.2
MIN
H
NO = 162
NO = 46
03
24653
8.0
150
83 H
137 M
206 H
1437 M
26 VL
6.3
1.1
10.5
MIN
VH
NO = 69
NC = 70
07
F6,4
7'5
150
95 H
53 VL
168 H
1359 H
18 VL
6.4
0.8
9.2
MIN
VH
NO = 79
NO= 27
08
24656
8'6
150
192 VH
116 M
283 H
1239 M
27 VL
6.1
6.79
1.4
10.4
MIN
VH
NO = 160
NO = 59
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Field ID
K
Mg
Ca
Na
H
NC N
S
Zn
Mn
Fe
Cu
B
SS
Cl
AI
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm
Rate
ppm Rate
ppm
01
13 L
15.2 VH
58 VH
12.4 VH
2.1
13.2
71.6
0.8
12.5
171 VH
1.0 M
0.27
VL
NC=27
NC=380.0
NC=363
NC=620.0
03
12 L
8.0 H
77 VH
5.5 VH
3.3
16.3
68.4
1.1
10.5
104 VH
0.8 M
0.27
VL
NC=25
NC=200.0
NC=481
NC=275.0
07
13 L
8.4 VH
39 H
4.8 VH
1.5
15.2
73.9
0.9
8.7
108 VH
0.9 M
0.13
VL
NO = 27
NO = 210.0
NO = 244
NO = 240.0
08
18 M
16.8 VH
38 H
8.4 VH
2.9
22.7
59.6
1.1
13.5
132 VH
1.0 M
0.22
VL
NO = 37
NC = 420.0
NO = 238
NO = 420.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. to G�N�
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by:
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: Waypoint Analytical Virginia, Inc.
Pauric McGroary
NCDA&CS.L.y.—..omicDivision Phone: (919)733-2655 Website: www.n„aU,..gov/agronomi/
Report No. FY1',�,'u16999
Client: Tony Jones
Advisor:
Synagro
Predictive
':.
1418 Nature Preserve Trl.
Denver, NC 28037
12701 Lancaster Hwy
Pineville, NC 28134
�
Soil Report Mehlich-3 Extraction
r #'
Sampled County: Lincoln
Sampled: Received: 11/21/2016 Completed: 12/20/2016
Farm: NC-LT-46
Links to Helpful Information
Sample ID: 02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0 0
0
0
0
Note: 12
2-
Test Results [units - W/V in g/cn•r3; CEC and Na in meq/100 crrr3; NO3-N in mg/drn3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.46 1.01 13.2 90 1.3 6.0 73 107 62 24
56 179 124 315
315
550
0.1 1
Sample ID: 04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0 120-200 50
0 0 0 0
0
0
0
Note: 12
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cnr3; NO3-N in mg/dn�]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.32 1.04 13.2 93 0.9 6.3 38 138 63 25
54 362 230 215
215
406
0.1 1
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox
NCDA&CS / r omic Division Phone: (919) 733-2655 Website: www.n__,..gov/agronomi/ ReportNo. FYI —_ 16999
Tony Jones Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full r
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I. and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagrgovlagronomilobpart4.htmy sFind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilize]
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routine,
available)] indicate levels of plant nutrients or other fertility measurement. Visit www•ncagrqov/agronomiluvrst.htm
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN.
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop I
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index